Process Stability of Ultrasonic-Wave-Assisted Gas Metal Arc Welding

Science.gov (United States)

Fan, Chenglei; Xie, Weifeng; Yang, Chunli; Lin, Sanbao; Fan, Yangyang

2017-10-01

As a newly developed arc welding method, ultrasonic-wave-assisted arc welding successfully introduced power ultrasound into the arc and weld pool, during which the ultrasonic acts on the top of the arc in the coaxial alignment direction. The advanced process for molten metals can be realized by using an additional ultrasonic field. Compared with the conventional gas metal arc welding (GMAW), the welding arc is compressed, the droplet size is decreased, and the droplet transfer frequency is increased significantly in ultrasonic-wave-assisted GMAW (U-GMAW). However, the stability of the metal transfer has deep influence on the welding quality equally, and the ultrasonic wave effect on the stability of the metal transfer is a phenomenon that is not completely understood. In this article, the stabilities of the short-circuiting transfer process and globular transfer process are studied systematically, and the effect of ultrasonic wave on the metal transfer is analyzed further. The transfer frequency and process stability of the U-GMAW process are much higher than those of the conventional GMAW. Analytical results show that the additional ultrasonic wave is helpful for improving welding stability.

Ultrasonic-assisted manufacturing processes: Variational model and numerical simulations

KAUST Repository

Siddiq, Amir

2012-04-01

We present a computational study of ultrasonic assisted manufacturing processes including sheet metal forming, upsetting, and wire drawing. A fully variational porous plasticity model is modified to include ultrasonic softening effects and then utilized to account for instantaneous softening when ultrasonic energy is applied during deformation. Material model parameters are identified via inverse modeling, i.e. by using experimental data. The versatility and predictive ability of the model are demonstrated and the effect of ultrasonic intensity on the manufacturing process at hand is investigated and compared qualitatively with experimental results reported in the literature. © 2011 Elsevier B.V. All rights reserved.

Development of a jet-assisted polycrystalline diamond drill bit

Energy Technology Data Exchange (ETDEWEB)

Pixton, D.S.; Hall, D.R.; Summers, D.A.; Gertsch, R.E.

1997-12-31

A preliminary investigation has been conducted to evaluate the technical feasibility and potential economic benefits of a new type of drill bit. This bit transmits both rotary and percussive drilling forces to the rock face, and augments this cutting action with high-pressure mud jets. Both the percussive drilling forces and the mud jets are generated down-hole by a mud-actuated hammer. Initial laboratory studies show that rate of penetration increases on the order of a factor of two over unaugmented rotary and/or percussive drilling rates are possible with jet-assistance.

Built-up edge investigation in vibration drilling of Al2024-T6.

Science.gov (United States)

Barani, A; Amini, S; Paktinat, H; Fadaei Tehrani, A

2014-07-01

Adding ultrasonic vibrations to drilling process results in an advanced hybrid machining process, entitled "vibration drilling". This study presents the design and fabrication of a vibration drilling tool by which both rotary and vibrating motions are applied to drill simultaneously. High frequency and low amplitude vibrations were generated by an ultrasonic transducer with frequency of 19.65 kHz. Ultrasonic transducer was controlled by a MPI ultrasonic generator with 3 kW power. The drilling tool and workpiece material were HSS two-flute twist drill and Al2024-T6, respectively. The aim of this study was investigating on the effect of ultrasonic vibrations on built-up edge, surface quality, chip morphology and wear mechanisms of drill edges. Therefore, these factors were studied in both vibration and ordinary drilling. Based on the achieved results, vibration drilling offers less built-up edge and better surface quality compared to ordinary drilling. Copyright © 2014 Elsevier B.V. All rights reserved.

Log response of ultrasonic imaging and its significance for deep mineral prospecting of scientific drilling borehole-2 in Nanling district, China

International Nuclear Information System (INIS)

Xiao, Kun; Zou, Changchun; Xiang, Biao; Yue, Xuyuan; Zhou, Xinpeng; Li, Jianguo; Zhao, Bin

2014-01-01

The hole NLSD-2, one of the deepest scientific drilling projects in the metallic ore districts of China, is the second scientific drilling deep hole in the Nanling district. Its ultimate depth is 2012.12 m. This hole was created through the implementation of continuous coring, and the measuring of a variety of geophysical well logging methods was performed over the course of the drilling process. This paper analyzes the characteristic responses of the fracture and fractured zone by ultrasonic imaging log data, and characterizes various rules of fracture parameters which change according to drilling depth. It then discusses the denotative meaning of the log results of polymetallic mineralization layers. The formation fractures develop most readily in a depth of 100∼200 m, 600∼850 m and 1450∼1550 m of the hole NLSD-2, and high angle fractures develop most prominently. The strike direction of the fractures is mainly NW-SE, reflecting the orientation of maximum horizontal principal stress. For the polymetallic mineralization layer that occurred in the fractured zone, the characteristic response of ultrasonic imaging log is a wide dark zone, and the characteristic responses of conventional logs displayed high polarizability, high density, high acoustic velocity and low resistivity. All the main polymetallic mineralization layers are developed in fractures or fractured zones, and the fractures and fractured zones can be identified by an ultrasonic imaging log, thus the log results indirectly indicate the occurrence of polymetallic mineralization layers. Additionally, the relationship between the dip direction of fractures and the well deviation provides guidance for straightening of the drilling hole. (paper)

Grain fragmentation in ultrasonic-assisted TIG weld of pure aluminum.

Science.gov (United States)

Chen, Qihao; Lin, Sanbao; Yang, Chunli; Fan, Chenglei; Ge, Hongliang

2017-11-01

Under the action of acoustic waves during an ultrasonic-assisted tungsten inert gas (TIG) welding process, a grain of a TIG weld of aluminum alloy is refined by nucleation and grain fragmentation. Herein, effects of ultrasound on grain fragmentation in the TIG weld of aluminum alloy are investigated via systematic welding experiments of pure aluminum. First, experiments involving continuous and fixed-position welding are performed, which demonstrate that ultrasound can break the grain of the TIG weld of pure aluminum. The microstructural characteristics of an ultrasonic-assisted TIG weld fabricated by fixed-position welding are analyzed. The microstructure is found to transform from plane crystal, columnar crystal, and uniform equiaxed crystal into plane crystal, deformed columnar crystal, and nonuniform equiaxed crystal after application of ultrasound. Second, factors influencing ultrasonic grain fragmentation are investigated. The ultrasonic amplitude and welding current are found to have a considerable effect on grain fragmentation. The degree of fragmentation first increases and then decreases with an increase in ultrasonic amplitude, and it increases with an increase in welding current. Measurement results of the vibration of the weld pool show that the degree of grain fragmentation is related to the intensity of acoustic nonlinearity in the weld pool. The greater the intensity of acoustic nonlinearity, the greater is the degree of grain fragmentation. Finally, the mechanism of ultrasonic grain fragmentation in the TIG weld of pure aluminum is discussed. A finite element simulation is used to simulate the acoustic pressure and flow in the weld pool. The acoustic pressure in the weld pool exceeds the cavitation threshold, and cavitation bubbles are generated. The flow velocity in the weld pool does not change noticeably after application of ultrasound. It is concluded that the high-pressure conditions induced during the occurrence of cavitation, lead to grain

Minimization of the hole overcut and cylindricity errors during rotary ultrasonic drilling of Ti-6Al-4V

Science.gov (United States)

Nasr, M.; Anwar, S.; El-Tamimi, A.; Pervaiz, S.

2018-04-01

Titanium and its alloys e.g. Ti6Al4V have widespread applications in aerospace, automotive and medical industry. At the same time titanium and its alloys are regarded as difficult to machine materials due to their high strength and low thermal conductivity. Significant efforts have been dispensed to improve the accuracy of the machining processes for Ti6Al4V. The current study present the use of the rotary ultrasonic drilling (RUD) process for machining high quality holes in Ti6Al4V. The study takes into account the effects of the main RUD input parameters including spindle speed, ultrasonic power, feed rate and tool diameter on the key output responses related to the accuracy of the drilled holes including cylindricity and overcut errors. Analysis of variance (ANOVA) was employed to study the influence of the input parameters on cylindricity and overcut error. Later, regression models were developed to find the optimal set of input parameters to minimize the cylindricity and overcut errors.

The Machining of Hard Mold Steel by Ultrasonic Assisted End Milling

Directory of Open Access Journals (Sweden)

Ming Yi Tsai

2016-11-01

Full Text Available This study describes the use of ultrasonic-assisted end milling to improve the quality of the machined surface of hard Stavax (modified AISI 420 mold steel and to reduce the amount of work involved in the final polishing process. The effects of input voltage, the stretch length and cutter holding force on the amplitude of the ultrasonic vibration used were measured. The effect of ultrasonic frequency (25 and 50 kHz and amplitude (0, 2.20 and 3.68 μm as well as the effect of the rake angle (6° and −6° and the cutter helix angle (25°, 35° and 45° on tool wear and quality of the workpiece surface finish were also investigated. It was found that the ultrasonic amplitude increased with cutter stretch length and input voltage, as expected. The amplitude remained constant when the cutter holding force exceeded 15 N. The experimental results showed that the ultrasonic amplitude had an optimum value with respect to surface finish. However, large amplitude ultrasonics did not necessarily improve quality. Furthermore, the cutters used for ultrasonic-assisted milling show less wear than those used for normal milling. It was also found that a positive rake angle and cutters with a large helix angle gave a better surface finish.

A Study of Polishing Feature of Ultrasonic-Assisted Vibration Method in Bamboo Charcoal

Directory of Open Access Journals (Sweden)

Hsin-Min Lee

2017-01-01

Full Text Available Focusing on the feature of porosity in bamboo charcoal, this study applies the ultrasonic-assisted vibration method to perform surface polishing of the silicon wafer workpiece. The self-developed bamboo charcoal polishing spindle and ultrasonic- assisted vibration mechanism are attached to a single lapping machine. In the machining process, ultrasonic vibration enables the diamond slurry to smoothly pass through the microscopic holes of bamboo charcoal; the end of the bamboo charcoalis able to continue machining on the surface of the workpiece through the grasping force which exists in the microscopic holes. Under the polishing and machining parameters of ultrasonic-assisted vibration, with a diamond slurry concentration of 0.3%, the experimental results show a polishing time of 20 min, a loading of 25 N on the workpiece surface, a spindle speed of 1200 rpm, a vibration frequency of 30 kHz and the original surface roughness value of Ra 0.252 μm equals that of a mirror-like surface at Ra 0.017 μm. These research results prove that by using bamboo charcoal and ultrasonic-assisted vibration for polishing, a very good improvement can be achieved on the workpiece surface.

Acoustic Emission and Echo Signal Compensation Techniques Applied to an Ultrasonic Logging-While-Drilling Caliper.

Science.gov (United States)

Yao, Yongchao; Ju, Xiaodong; Lu, Junqiang; Men, Baiyong

2017-06-10

A logging-while-drilling (LWD) caliper is a tool used for the real-time measurement of a borehole diameter in oil drilling engineering. This study introduces the mechanical structure and working principle of a new LWD caliper based on ultrasonic distance measurement (UDM). The detection range is a major performance index of a UDM system. This index is determined by the blind zone length and remote reflecting interface detection capability of the system. To reduce the blind zone length and detect near the reflecting interface, a full bridge acoustic emission technique based on bootstrap gate driver (BGD) and metal-oxide-semiconductor field effect transistor (MOSFET) is designed by analyzing the working principle and impedance characteristics of a given piezoelectric transducer. To detect the remote reflecting interface and reduce the dynamic range of the received echo signals, the relationships between the echo amplitude and propagation distance of ultrasonic waves are determined. A signal compensation technique based on time-varying amplification theory, which can automatically change the gain according to the echo arrival time is designed. Lastly, the aforementioned techniques and corresponding circuits are experimentally verified. Results show that the blind zone length in the UDM system of the LWD caliper is significantly reduced and the capability to detect the remote reflecting interface is considerably improved.

DYNAMIC MODELLING OF VIBRATIONS ASSISTED DRILLING

Directory of Open Access Journals (Sweden)

Mathieu LADONNE

2015-05-01

Full Text Available The number of multi-materials staking configurations for aeronautical structures is increasing, with the evolution of composite and metallic materials. For drilling the fastening holes, the processes of Vibration Assisted Drilling (VAD expand rapidly, as it permits to improve reliability of drilling operations on multilayer structures. Among these processes of VAD, the solution with forced vibrations added to conventional feed to create a discontinuous cutting is the more developed in industry. The back and forth movement allows to improve the evacuation of chips by breaking it. This technology introduces two new operating parameters, the frequency and the amplitude of the oscillation. To optimize the process, the choice of those parameters requires first to model precisely the operation cutting and dynamics. In this paper, a kinematic modelling of the process is firstly proposed. The limits of the model are analysed through comparison between simulations and measurements. The proposed model is used to develop a cutting force model that allows foreseeing the operating conditions which ensure good chips breaking and tool life improvement.

Ultrasonic-assisted extraction and in vitro antioxidant activity of polysaccharides from Agaricus bisporus.

Science.gov (United States)

Qiao, De-Liang; Zhao, Feng; Huang, Hai-Zhong; Fan, Chun-Chun; Han, Lei

2012-08-01

To optimize ultrasonic-assisted extraction parameters of polysaccharides from Agaricus bisporus and evaluate antioxidant activities of A. bisporus polysaccharides. Polysaccharides from A. bisporus was extracted by using methods of ultrasonic-assisted hot water lixiviation, ethanol precipitation, Sevag's deproteination and ethanol precipitation again. Extraction temperature, extraction time, ratio of water to raw material and ultrasonic power were selected in single-factor tests. Based on the single-factor tests, parameters combination for the ultrasonic-assisted extraction of A. bisporus polysaccharides was optimized by using four-factor-three-level orthogonal test. Antioxidant activities (reductive potential, superoxide anion scavenging activity and H2O2 scavenging activity) of A. bisporus polysaccharides were evaluated in vitro. Optimum conditions for the extracting of A. bisporus polysaccharides were extracting temperature 65 degrees C, extracting time 40 min, ratio of water to raw material 30 mL/g and ultrasonic power 170 w. Practicing this optimal condition, extraction yield of polysaccharides from A. bisporus was 5.6 014%. In crude polysaccharides of A. bisporus, carbohydrates content, determined by applying the phenol-sulfuric acid method, was 75.48%. Polysaccharides of A. bisporus could reduce ferric ion, scavenge superoxide anion and hydrogen peroxide in a dose-dependent manner. Utrasonic-assisted extraction could be used in the extracting of A. bisporus polysaccharides. Polysaccharides of A. bisporus, had direct and potent antioxidant activities, might be developed and utilized as natural antioxidant.

Comparative performance evaluation of conventional and ultrasonic assisted bleaching of cotton fabric

International Nuclear Information System (INIS)

Farooq, A.; Ashraf, M.A.

2013-01-01

Summary: Conventional bleaching process is an important and quality influencing process for textile wet processors. However, the process requires high energy consumption, and is slow and time consuming. In the present research work, cotton woven fabric was bleached with different bleaching agents using conventional and ultrasonic assisted techniques. After bleaching whiteness index, weight loss and tensile strength of samples were measured and compared statistically. The results showed that ultrasonic energy intensifies the diffusion of chemicals and increases the production of hydroxyl radicals which catalyze the bleaching process. Ultrasonic assisted bleaching proved to be a novel technique that can produce better results than conventional bleaching process even at low temperature and in less time. (author)

Ultrasonic-Assisted Extraction and Antioxidant Activity of Flavonoids ...

African Journals Online (AJOL)

Purpose: To identify the main flavonoid in Adinandra nitida leaf, employ response surface methodology to optimize its ultrasonic-assisted extraction, and determine the antioxidant activity of the obtained extract. Methods: The main flavonoid in Adinandra nitida leaf was obtained by traditional solvent extraction and ...

Surface quality prediction model of nano-composite ceramics in ultrasonic vibration-assisted ELID mirror grinding

Energy Technology Data Exchange (ETDEWEB)

Zhao, Bo; Chen, Fan; Jia, Xiao-feng; Zhao, Chong-yang; Wang, Xiao-bo [Henan Polytechnic University, Jiaozuo (China)

2017-04-15

Ultrasonic vibration-assisted Electrolytic in-process dressing (ELID) grinding is a highly efficient and highly precise machining method. The surface quality prediction model in ultrasonic vibration-assisted ELID mirror grinding was studied. First, the interaction between grits and workpiece surface was analyzed according to kinematic mechanics, and the surface roughness model was developed. The variations in surface roughness under different parameters was subsequently calculated and analyzed by MATLAB. Results indicate that compared with the ordinary ELID grinding, ultrasonic vibration-assisted ELID grinding is superior, because it has more stable and better surface quality and has an improved range of ductile machining.

Acoustic Emission and Echo Signal Compensation Techniques Applied to an Ultrasonic Logging-While-Drilling Caliper

Directory of Open Access Journals (Sweden)

Yongchao Yao

2017-06-01

Full Text Available A logging-while-drilling (LWD caliper is a tool used for the real-time measurement of a borehole diameter in oil drilling engineering. This study introduces the mechanical structure and working principle of a new LWD caliper based on ultrasonic distance measurement (UDM. The detection range is a major performance index of a UDM system. This index is determined by the blind zone length and remote reflecting interface detection capability of the system. To reduce the blind zone length and detect near the reflecting interface, a full bridge acoustic emission technique based on bootstrap gate driver (BGD and metal-oxide-semiconductor field effect transistor (MOSFET is designed by analyzing the working principle and impedance characteristics of a given piezoelectric transducer. To detect the remote reflecting interface and reduce the dynamic range of the received echo signals, the relationships between the echo amplitude and propagation distance of ultrasonic waves are determined. A signal compensation technique based on time-varying amplification theory, which can automatically change the gain according to the echo arrival time is designed. Lastly, the aforementioned techniques and corresponding circuits are experimentally verified. Results show that the blind zone length in the UDM system of the LWD caliper is significantly reduced and the capability to detect the remote reflecting interface is considerably improved.

Study on Electric field assisted low frequency (20 kHz) ultrasonic spray

Science.gov (United States)

Chae, Ilkyeong; Seong, Baekhoon; Marten, Darmawan; Byun, Doyoung

2015-11-01

Ultrasonic spray is one of the fabulous techniques to discharge small size of droplets because it utilizes ultrasonic vibration on nozzle. However, spray patterns and size of ejected droplet is hardly controlled in conventional ultrasonic spray method. Therefore, here we present electric field assisted ultrasonic spray, which combined conventional technique with electric field in order to control spray pattern and droplet size precisely. Six kinds of various liquid (D.I water, Ethanol, Acetone, Iso-propanol, Toluene, Hexane) with various dielectric constants were used to investigate the mechanism of this method. Also, PIV (Particle Image Velocimetry) was used and various variables were obtained including spray angle, amplitude of liquid vibration, current, and size distribution of ejected droplets. Our electric field assisted ultrasonic spray show that the standard deviation of atomized droplet was decreased up to 39.6%, and it shows the infinite possibility to be utilized in various applications which require precise control of high transfer efficiency. This work was supported by the Basic Science Research Program through the National Research Foundation of Korea (NRF) funded by the Ministry of Education, Science and Technology (2014-023284).

The Auto-Gopher Deep Drill

Science.gov (United States)

Badescu, Mircea

2014-01-01

Subsurface penetration by coring, drilling or abrading is of great importance for a large number of space and earth applications. An Ultrasonic/Sonic Drill/Corer (USDC) has been in development at JPL's Nondestructive Evaluation and Advanced Actuators (NDEAA) lab as an adaptable tool for many of these applications. The USDC uses a novel drive mechanism to transform the high frequency ultrasonic or sonic vibrations of the tip of a horn into a lower frequency sonic hammering of a drill bit through an intermediate free-flying mass. The USDC device idea has been implemented at various scales from handheld drills to large diameter coring devices. A series of computer programs that model the function and performance of the USDC device were developed and were later integrated into an automated modeling package. The USDC has also evolved from a purely hammering drill to a rotary hammer drill as the design requirements increased form small diameter shallow drilling to large diameter deep coring. A synthesis of the Auto-Gopher development is presented in this paper.

A Combined Structural and Electromechanical FE Approach for Industrial Ultrasonic Devices Design

Science.gov (United States)

Schorderet, Alain; Prenleloup, Alain; Colla, Enrico

2011-05-01

Ultrasonic assistance is widely used in manufacturing, both for conventional (e.g. grinding, drilling) and non-conventional (e.g. EDM) processes. Ultrasonic machining is also used as a stand alone process for instance for micro-drilling. Industrial application of these processes requires increasingly efficient and accurate development tools to predict the performance of the ultrasonic device: the so-called sonotrode and the piezo-transducer. This electromechanical system consists of a structural part and of a piezo-electrical part (actuator). In this paper, we show how to combine two simulation softwares—for stuctures and electromechanical devices—to perform a complete design analysis and optimization of a sonotrode for ultrasonic drilling applications. The usual design criteria are the eigenfrequencies of the desired vibrational modes. In addition, during the optimization phase, one also needs to consider the maximum achievable displacement for a given applied voltage. Therefore, one must be able to predict the electromechanical behavior of the integrated piezo-structure system, in order to define, adapt and optimize the electric power supply as well as the control strategy (search, tracking of the eigenfrequency). In this procedure, numerical modelling follows a two-step approach, by means of a solid mechanics FE code (ABAQUS) and of an electromechanical simulation software (ATILA). The example presented illustrates the approach and describes the obtained results for the development of an industrial sonotrode system dedicated to ultrasonic micro-drilling of ceramics. The 3D model of the sonotrode serves as input for generating the FE mesh in ABAQUS and this mesh is then translated into an input file for ATILA. ABAQUS results are used to perform the first optimization step in order to obtain a sonotrode design leading to the requested modal behaviour—eigen-frequency and corresponding dynamic amplification. The second step aims at evaluating the dynamic

Ultrasonic assisted extraction - an alternative for sample preparation (M4)

International Nuclear Information System (INIS)

Santos Junior, P.; Barbosa Junior, F.; Krug, F.J.; Trevizan, L.C.; Nobrega, J.A.

2002-01-01

Full text: In the last years the ultrasound assisted metal extraction has been frequency proposed as a simple and inexpensive alternative for sample preparation of biological and inorganic samples. The extraction effect is considered as being caused by acoustic cavitation, that is, bubble formation and subsequent disruptive action. The collapse of bubbles created by sonication of solutions results in the generation of extremely high local temperature and pressure gradients, which may be regarded as localized 'hot spots'. On a timescale of about 10 -10 s, effective local pressures and temperature of about 10 5 atm and about 5000 K, respectively, are generated under sonochemical conditions. Usually, this method uses a diluted acid medium decreasing blank values and reducing both reagents and time consumption compared to traditional wet digestion systems using conductive or microwave-assisted heating. Furthermore, sonication can also allow the preparation of samples directly within the sample container, thereby preventing sample losses and minimizing sample contamination. Although some controversial results concerning metals extraction behavior have been reported, they could be explained by analyte-matrix interaction and the ability of the ultrasonic processor to generate ultrasound (i.e. the use of an ultrasonic bath or an ultrasonic probe at different power, frequency, and amplitude). This contribution presents a review of ultrasound assisted metal extraction and recent performance data obtained in our laboratory for determination of elements in biological materials, soils and sediments by ICP-OES and ETAAS. The effect of extraction parameters, such as type and concentration of the leaching solution, sonication time and performance of ultrasonic processor (bath or probe) will be presented. (author)

Real time monitoring of accelerated chemical reactions by ultrasonication-assisted spray ionization mass spectrometry.

Science.gov (United States)

Lin, Shu-Hsuan; Lo, Ta-Ju; Kuo, Fang-Yin; Chen, Yu-Chie

2014-01-01

Ultrasonication has been used to accelerate chemical reactions. It would be ideal if ultrasonication-assisted chemical reactions could be monitored by suitable detection tools such as mass spectrometry in real time. It would be helpful to clarify reaction intermediates/products and to have a better understanding of reaction mechanism. In this work, we developed a system for ultrasonication-assisted spray ionization mass spectrometry (UASI-MS) with an ~1.7 MHz ultrasonic transducer to monitor chemical reactions in real time. We demonstrated that simply depositing a sample solution on the MHz-based ultrasonic transducer, which was placed in front of the orifice of a mass spectrometer, the analyte signals can be readily detected by the mass spectrometer. Singly and multiply charged ions from small and large molecules, respectively, can be observed in the UASI mass spectra. Furthermore, the ultrasonic transducer used in the UASI setup accelerates the chemical reactions while being monitored via UASI-MS. The feasibility of using this approach for real-time acceleration/monitoring of chemical reactions was demonstrated. The reactions of Girard T reagent and hydroxylamine with steroids were used as the model reactions. Upon the deposition of reactant solutions on the ultrasonic transducer, the intermediate/product ions are readily generated and instantaneously monitored using MS within 1 s. Additionally, we also showed the possibility of using this reactive UASI-MS approach to assist the confirmation of trace steroids from complex urine samples by monitoring the generation of the product ions. Copyright © 2014 John Wiley & Sons, Ltd.

Rotary Percussive Auto-Gopher for Deep Drilling and Sampling

Science.gov (United States)

Bar-Cohen, Yoseph; Badescu, Mircea; Sherrit, Stewart

2009-01-01

The term "rotary percussive auto-gopher" denotes a proposed addition to a family of apparatuses, based on ultrasonic/ sonic drill corers (USDCs), that have been described in numerous previous NASA Tech Briefs articles. These apparatuses have been designed, variously, for boring into, and/or acquiring samples of, rock or other hard, brittle materials of geological interest. In the case of the rotary percussive autogopher, the emphasis would be on developing an apparatus capable of penetrating to, and acquiring samples at, depths that could otherwise be reached only by use of much longer, heavier, conventional drilling-and-sampling apparatuses. To recapitulate from the prior articles about USDCs: A USDC can be characterized as a lightweight, low-power jackhammer in which a piezoelectrically driven actuator generates ultrasonic vibrations and is coupled to a tool bit through a free mass. The bouncing of the free mass between the actuator horn and the drill bit converts the actuator ultrasonic vibrations into sonic hammering of the drill bit. The combination of ultrasonic and sonic vibrations gives rise to a hammering action (and a resulting chiseling action at the tip of the tool bit) that is more effective for drilling than is the microhammering action of ultrasonic vibrations alone. The hammering and chiseling actions are so effective that the size of the axial force needed to make the tool bit advance into soil, rock, or another material of interest is much smaller than in ordinary rotary drilling, ordinary hammering, or ordinary steady pushing. The predecessor of the rotary percussive auto-gopher is an apparatus, now denoted an ultrasonic/sonic gopher and previously denoted an ultrasonic gopher, described in "Ultrasonic/ Sonic Mechanism for Drilling and Coring" (NPO-30291), NASA Tech Briefs Vol. 27, No. 9 (September 2003), page 65. The ultrasonic/sonic gopher is intended for use mainly in acquiring cores. The name of the apparatus reflects the fact that, like a

Enzyme-catalyzed synthesis and kinetics of ultrasonic-assisted biodiesel production from waste tallow.

Science.gov (United States)

Adewale, Peter; Dumont, Marie-Josée; Ngadi, Michael

2015-11-01

The use of ultrasonic processing was evaluated for its ability to achieve adequate mixing while providing sufficient activation energy for the enzymatic transesterification of waste tallow. The effects of ultrasonic parameters (amplitude, cycle and pulse) and major reaction factors (molar ratio and enzyme concentration) on the reaction kinetics of biodiesel generation from waste tallow bio-catalyzed by immobilized lipase [Candida antarctica lipase B (CALB)] were investigated. Three sets of experiments namely A, B, and C were conducted. In experiment set A, two factors (ultrasonic amplitude and cycle) were investigated at three levels; in experiment set B, two factors (molar ratio and enzyme concentration) were examined at three levels; and in experiment set C, two factors (ultrasonic amplitude and reaction time) were investigated at five levels. A Ping Pong Bi Bi kinetic model approach was employed to study the effect of ultrasonic amplitude on the enzymatic transesterification. Kinetic constants of transesterification reaction were determined at different ultrasonic amplitudes (30%, 35%, 40%, 45%, and 50%) and enzyme concentrations (4, 6, and 8 wt.% of fat) at constant molar ratio (fat:methanol); 1:6, and ultrasonic cycle; 5 Hz. Optimal conditions for ultrasound-assisted biodiesel production from waste tallow were fat:methanol molar ratio, 1:4; catalyst level 6% (w/w of fat); reaction time, 20 min (30 times less than conventional batch processes); ultrasonic amplitude 40% at 5 Hz. The kinetic model results revealed interesting features of ultrasound assisted enzyme-catalyzed transesterification (as compared to conventional system): at ultrasonic amplitude 40%, the reaction activities within the system seemed to be steady after 20 min which means the reaction could proceed with or without ultrasonic mixing. Reversed phase high performance liquid chromatography indicated the biodiesel yield to be 85.6±0.08%. Copyright © 2015 Elsevier B.V. All rights reserved.

Improvement of copper plating adhesion on silane modified PET film by ultrasonic-assisted electroless deposition

International Nuclear Information System (INIS)

Lu Yinxiang

2010-01-01

Copper thin film on silane modified poly(ethylene terephthalate) (PET) substrate was fabricated by ultrasonic-assisted electroless deposition. The composition and topography of copper plating PET films were characterized by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD) and atomic force microscopy (AFM), respectively. Peel adhesion strength, as high as 16.7 N/cm, was achieved for the planting copper layer to the modified PET substrate with ultrasonic-assisted deposition; however, a relative low value as 11.9 N/cm was obtained for the sample without ultrasonic vibration by the same measurement. The electrical conductivity of Cu film was changed from 7.9 x 10 4 to 2.1 x 10 5 S/cm by using ultrasonic technique. Ultrasonic operation has the significant merits of fast deposition and formation of good membranes for electroless deposition of Cu on PET film.

Elastic-Plastic Behaviour of Ultrasonic Assisted Compression of Polyvinyl Chloride (PVC) Foam

Science.gov (United States)

Muhalim, N. A. D.; Hassan, M. Z.; Daud, Y.

2018-04-01

The present study aims to investigate the elastic-plastic behaviour of ultrasonic assisted compression of PVC closed-cell foam. A series of static and ultrasonic compression test of PVC closed-cell foam were conducted at a constant cross head speed of 30 mm/min on dry surface condition. For quasi-static test, specimen was compressed between two rigid platens using universal testing machine. In order to evaluate the specimen behavior under ultrasonic condition, specimen was placed between a specifically design double-slotted block horn and rigid platen. The horn was designed and fabricated prior to the test as a medium to transmit the ultrasonic vibration from the ultrasonic transducer to the working specimen. It was tuned to a frequency of 19.89 kHz in longitudinal mode and provided an average oscillation amplitude at 6 µm on the uppermost surface. Following, the characteristics of stress-strain curves for quasi-static and ultrasonic compression tests were analyzed. It was found that the compressive stress was significantly reduced at the onset of superimposed ultrasonic vibration during plastic deformation.

Characterising the acoustoplastic effect in an ultrasonically assisted metal forming process

International Nuclear Information System (INIS)

Aziz, S A; Lucas, M

2012-01-01

An investigation through experiments and finite element analysis (FEA) has been carried out to study the effects of applying ultrasonic oscillations to the lower platen in forming tests for two different metals. Previous research has shown that by applying ultrasonic vibrations to the lower platen in compression tests on pure aluminium specimens, the resulting stress-strain relationship can be characterised by a temporary effective softening of the material properties during intervals of ultrasonic excitation. The current research demonstrates this effect in two different metal specimens and additionally shows that finite element simulations can be used to model the behaviour in terms of both volume and surface effects. In this study, the ultrasonic excitation was introduced both prior to and post yield and the process simulations were developed in the FEA software Abaqus. The data recorded from experiments and predicted by the FEA illustrate how ultrasonically assisted metal forming can result in a lowering of the static flow stress, consistent with the effective material softening proposed previously in studies of the acoustoplastic effect.

Artificial Intelligence Assists Ultrasonic Inspection

Science.gov (United States)

Schaefer, Lloyd A.; Willenberg, James D.

1992-01-01

Subtle indications of flaws extracted from ultrasonic waveforms. Ultrasonic-inspection system uses artificial intelligence to help in identification of hidden flaws in electron-beam-welded castings. System involves application of flaw-classification logic to analysis of ultrasonic waveforms.

A review on feasibility study of ultrasonic assisted machining on aircraft component manufacturing

Science.gov (United States)

Hafiz, M. S. A.; Kawaz, M. H. A.; Mohamad, W. N. F.; Kasim, M. S.; Izamshah, R.; Saedon, J. B.; Mohamed, S. B.

2017-12-01

Inconel 718 has been widely used in aerospace because of its excellent mechanical properties such as good corrosion resistance, strong creep resistance and high fatigue strength. However, these excellent properties also lead to heavy tool damage and high cutting force in the milling process. There is no reported investigation on ultrasonic assisted machining (UAM) of Inconel 718 parts. In this paper, UAM is proposed as the potential technique to reduce tool damage and the cutting force of Inconel 718 parts. This review paper provides an overview of UAM to investigate the relationship between the tool wear and the cutting force with ultrasonic vibration compared to without ultrasonic vibration assisted. Throughout the study, the UAM scopes are related to the tool life of coated carbide insert, the force generated during the cutting process and also the final surface finish of the workpiece by using various parameters during the machining activity.

Experimental Investigation on the Material Removal of the Ultrasonic Vibration Assisted Abrasive Water Jet Machining Ceramics

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Tao Wang

2017-01-01

Full Text Available The ultrasonic vibration activated in the abrasive water jet nozzle is used to enhance the capability of the abrasive water jet machinery. The experiment devices of the ultrasonic vibration assisted abrasive water jet are established; they are composed of the ultrasonic vibration producing device, the abrasive supplying device, the abrasive water jet nozzle, the water jet intensifier pump, and so on. And the effect of process parameters such as the vibration amplitude, the system working pressure, the stand-off, and the abrasive diameter on the ceramics material removal is studied. The experimental result indicates that the depth and the volume removal are increased when the ultrasonic vibration is added on abrasive water jet. With the increase of vibration amplitude, the depth and the volume of material removal are also increased. The other parameters of the ultrasonic vibration assisted abrasive water jet also have an important role in the improvement of ceramic material erosion efficiency.

Component based modelling of piezoelectric ultrasonic actuators for machining applications

International Nuclear Information System (INIS)

Saleem, A; Ahmed, N; Salah, M; Silberschmidt, V V

2013-01-01

Ultrasonically Assisted Machining (UAM) is an emerging technology that has been utilized to improve the surface finishing in machining processes such as turning, milling, and drilling. In this context, piezoelectric ultrasonic transducers are being used to vibrate the cutting tip while machining at predetermined amplitude and frequency. However, modelling and simulation of these transducers is a tedious and difficult task. This is due to the inherent nonlinearities associated with smart materials. Therefore, this paper presents a component-based model of ultrasonic transducers that mimics the nonlinear behaviour of such a system. The system is decomposed into components, a mathematical model of each component is created, and the whole system model is accomplished by aggregating the basic components' model. System parameters are identified using Finite Element technique which then has been used to simulate the system in Matlab/SIMULINK. Various operation conditions are tested and performed to demonstrate the system performance

Structural Phase Evolution in Ultrasonic-Assisted Friction Stir Welded 2195 Aluminum Alloy Joints

Science.gov (United States)

Eliseev, A. A.; Fortuna, S. V.; Kalashnikova, T. A.; Chumaevskii, A. V.; Kolubaev, E. A.

2017-10-01

The authors examined the structural and phase state of fixed joints produced by method of friction stir welding (FSW) and ultrasonic-assisted friction stir welding (UAFSW) from extruded profile of aluminum alloy AA2195. In order to identify the role of ultrasonic application in the course of welding, such characteristics, as volume fraction and average size of secondary particles are compared in the base material and stir zones of FSW and UAFSW joints. By applying the methods of SEM and TEM analysis, researchers established the complex character of phase transitions as a result of ultrasonic application.

Study on the effect of thermal property of metals in ultrasonic-assisted laser machining

International Nuclear Information System (INIS)

Lee, Hu Seung; Kim, Gun Woo; Park, Jong Eun; Cho, Sung Hak; Yang, Min Yang; Park, Jong Kweon

2015-01-01

The laser machining process has been proposed as an advanced process for the selective fabrication of electrodes without a mask. In this study, we adapt laser machining to metals that have different thermal properties. Based on the results, the metals exhibit a different surface morphology, heat-affected zone (HAZ), and a recast layer around the machined surface according to their thermal conductivity, boiling point, and thermal diffusivity. Then, we apply ultrasonic-assisted laser machining to remove the recast layer. The ultrasonic-assisted laser machining exhibits a better surface quality in metals with higher diffusivity than those having lower diffusivity

Experimental Investigation of Ultrasonic Vibration Assisted Turning of 304 Austenitic Stainless Steel

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Ping Zou

2015-01-01

vibration method is employed to scheme out a machining system of ultrasonic vibration assisted turning (MS-UAT. The experiments for turning the workpiece of ASS 304 are conducted with and without ultrasonic vibration using the designed MS-UAT, and then the 3D morphology evaluation parameters Sa and Sq are applied to characterize and analyse the machined surface. The experimental results obtained demonstrate that the process parameters in UAT of ASS 304 have obvious effect on the 3D surface topography and surface roughness of machined workpiece, and the appropriate choice of various process parameters, including ultrasonic amplitude, feed rate, depth of cut, and cutting speed, can enhance the machined surface quality efficiently to make the machining effect of UAT much better than that of CT.

[Optimization of ultrasonic-assisted extraction of total flavonoids from leaves of the Artocarpus heterophyllus by response surface methodology].

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Wang, Hong-wu; Liu, Yan-qing; Wang, Yuan-hong

2011-07-01

To investigate the ultrasonic-assisted extract on of total flavonoids from leaves of the Artocarpus heterophyllus. Investigated the effects of ethanol concentration, extraction time, and liquid-solid ratio on flavonoids yield. A 17-run response surface design involving three factors at three levels was generated by the Design-Expert software and experimental data obtained were subjected to quadratic regression analysis to create a mathematical model describing flavonoids extraction. The optimum ultrasonic assisted extraction conditions were: ethanol volume fraction 69.4% and liquid-solid ratio of 22.6:1 for 32 min. Under these optimized conditions, the yield of flavonoids was 7.55 mg/g. The Box-Behnken design and response surface analysis can well optimize the ultrasonic-assisted extraction of total flavonoids from Artocarpus heterophyllus.

The ultrasonically assisted metals recovery treatment of printed circuit board waste sludge by leaching separation.

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Xie, Fengchun; Li, Haiying; Ma, Yang; Li, Chuncheng; Cai, Tingting; Huang, Zhiyuan; Yuan, Gaoqing

2009-10-15

This paper provides a practical technique that realized industrial scale copper and iron separation from printed circuit board (PCB) waste sludge by ultrasonically assisted acid leaching in a low cost, low energy consumption and zero discharge of wastes manner. The separation efficiencies of copper and iron from acid leaching with assistance of ultrasound were compared with the one without assistance of ultrasound and the effects of the leaching procedure, pH value, and ultrasonic strength have been investigated in the paper. With the appropriate leaching procedure, a final pH of 3.0, an ultrasonic generator power of 160 W (in 1l tank), leaching time of 60 min, leaching efficiencies of copper and iron had reached 97.83% and 1.23%, respectively. Therefore the separation of copper and iron in PCB waste sludge was virtually achieved. The lab results had been successfully applied to the industrial scaled applications in a heavy metal recovery plant in city of Huizhou, China for more than two years. It has great potentials to be used in even the broad metal recovery practices.

Drilling, Coring and Sampling Using Piezoelectric Actuated Mechanisms: From the USDC to a Piezo-Rotary-Hammer Drill

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Bar-Cohen, Yoseph; Sherrit, Stewart; Badescu, Mircea; Bao, Xiaoqi

2012-01-01

NASA exploration missions are increasingly including sampling tasks but with the growth in engineering experience (particularly, Phoenix Scout and MSL) it is now very much recognized that planetary drilling poses many challenges. The difficulties grow significantly with the hardness of sampled material, the depth of drilling and the harshness of the environmental conditions. To address the requirements for samplers that could be operated at the conditions of the various bodies in the solar system, a number of piezoelectric actuated drills and corers were developed by the Advanced Technologies Group of JPL. The basic configuration that was conceived in 1998 is known as the Ultrasonic/Sonic Driller/Corer (USDC), and it operates as a percussive mechanism. This drill requires as low preload as 10N (important for operation at low gravity) allowing to operate with as low-mass device as 400g, use an average power as low as 2- 3W and drill rocks as hard as basalt. A key feature of this drilling mechanism is the use of a free-mass to convert the ultrasonic vibrations generated by piezoelectric stack to sonic impacts on the bit. Using the versatile capabilities f the USDC led to the development of many configurations and device sizes. Significant improvement of the penetration rate was achieved by augmenting the hammering action by rotation and use of a fluted bit to remove cuttings. To reach meters deep in ice a wireline drill was developed called the Ultrasonic/Sonic Gopher and it was demonstrated in 2005 to penetrate about 2-m deep at Antarctica. Jointly with Honeybee Robotics, this mechanism is currently being modified to incorporate rotation and inchworm operation forming Auto-Gopher to reach meters deep in rocks. To take advantage of the ability of piezoelectric actuators to operate over a wide temperatures range, piezoelectric actuated drills were developed and demonstrated to operate at as cold as -200oC and as hot as 500oC. In this paper, the developed mechanisms

Effect of Ultrasonic-Assisted Extraction on Phenolic Content of Avocado

International Nuclear Information System (INIS)

Rafidah Husen; Andou, Y.; Amin Ismail; Shirai, Y.

2014-01-01

This study evaluate the effect of ultrasonic application in the extraction process on total phenolic content (TPC) of Hass avocado (Persea americana Mill) pulp. In this study, the solid/ solvent ratio of 1/30 (wt/ vol) and extraction temperature of 40 degree Celsius gave higher TPC value. This ratio and temperature was applied in the ultrasonic-assisted extraction (UAE) of avocado pulp. This study then compared the TPC obtained from the avocado pulp extract without involving ultrasonic and the TPC obtained from the UAE. Results showed that the TPC value of avocado pulp was significantly higher in the UAE (235.77 mg GAE/ 100g dried sample) compared to the TPC in the non-UAE (166.32 mg GAE/ 100g dried sample). The increase in the TPC was between ∼31 % and ∼41 % when 5 to 20 min of ultra sonication applied in the extraction. Ultra sonication duration of 15 min gave the highest TPC where the value was significantly higher compared to the other duration. (author)

Experimental Study of the Ultrasonic Vibration-Assisted Abrasive Waterjet Micromachining the Quartz Glass

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Rongguo Hou

2018-01-01

Full Text Available The ultrasonic vibration is used to enhance the capability of the abrasive water micromachining glass. And, the ultrasonic vibration is activated on the abrasive waterjet nozzle. The quality of the flow is improved, and the velocity of the abrasive is increased because of the addition of the ultrasonic energy. The relevant experimental results indicate that the erosion depth and the material volume removal of the glass are obviously increased when ultrasonic vibration is working. As for the influence of process parameters on the material removal of the glass such as vibration amplitude, system pressure, distance of the standoff, and abrasive size, the experimental results indicate that the system pressure and vibration contribute greatly to the glass material removal. Also, the erosion depth and the volume of material removal are increased with the increase in the vibration amplitude and system pressure. There are some uplifts found at the edge of erosion pit. Then, it can be inferred that the plastic method is an important material removal method during the machining process of ultrasonic vibration-assisted abrasive waterjet.

Dynamic effect in ultrasonic assisted micro-upsetting

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Presz, Wojciech

2018-05-01

The use of ultrasonic assistance in microforming is becoming more and more popular. Mainly due to the beneficial effect of vibrations on the flow of plastic deformation reported already in the 50s of the last century. The influence is of two types: surface and volume. The surface effect is mainly the reduction of friction forces, and volumetric is the impact on the dislocation movement and even on phase transitions. The work focuses on the dynamic aspect of vibration assisted microforming. The use of ultrasonic vibrations at a frequency of 20 kHz and an amplitude of 16 µm, in the micro-upsetting process of an aluminum sample resulted in a high concentration of strain on both ends of the sample - at 14% of the height on both sides. There was observed (in relation to deformations of the sample without vibrations) 150-250% increase and a 50% decrease in strain in the center of the sample. At the same time, the larger deformations occurred from the impact side of the punch. Analyzing the course of forces of the upsetting process in the loading and unloading phase as well as the process of breaking glass samples, the spring deflections of key system elements and their natural frequencies were determined or calculated. Based on the determined or calculated parameters of the test stand, it was shown that during the micro-upsetting process the punch may detach from the sample surface and this is the main reason for the phenomena occurring. Detach of the punch is also the cause of the observed instability of the measurement of force, which should be considered unbelievable in such a situation.

Synthesis of Calcite Nano Particles from Natural Limestone assisted with Ultrasonic Technique

Science.gov (United States)

Handayani, M.; Sulistiyono, E.; Firdiyono, F.; Fajariani, E. N.

2018-03-01

This article represents a precipitation method assisted with ultrasonic process to synthesize precipitated calcium carbonate nano particles from natural limestone. The synthesis of nanoparticles material of precipitated calcium carbonate from commercial calcium carbonate was done for comparison. The process was performed using ultrasonic waves at optimum condition, that is, at temperature of 80oC for 10 minutes with various amplitudes. Synthesized precipitated calcium carbonate nanoparticles were characterized using X-Ray Diffraction (XRD), Scanning Electron Microscope (SEM) and Particle Size Analyzer (PSA). The result of PSA measurements showed that precipitated calcium carbonate nano particles was obtained with the average size of 109 nm.

An Estimation of Wave Attenuation Factor in Ultrasonic Assisted Gravity Drainage Process

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Behnam Keshavarzi

2014-01-01

Full Text Available It has been proved that ultrasonic energy can considerably increase the amount of oil recovery in an immiscible displacement process. Although many studies have been performed on investigating the roles of ultrasonic waves, based on the best of our knowledge, little attention has been paid to evaluate wave attenuation parameter, which is an important parameter in the determination of the energy delivered to the porous medium. In this study, free fall gravity drainage process is investigated in a glass bead porous medium. Kerosene and Dorud crude oil are used as the wetting phases and air is used as the non-wetting phase. A piston-like displacement model with considering constant capillary pressure and applying Corey type approximation for relative permeabilities of both wetting and nonwetting phases is applied. A pressure term is considered to describe the presence of ultrasonic waves and the attenuation factor of ultrasonic waves is calculated by evaluating the value of external pressure applied to enhance the flow using the history matching of the data in the presence and absence of ultrasonic waves. The results introduce the attenuation factor as an important parameter in the process of ultrasonic assisted gravity drainage. The results show that only a low percentage of the ultrasonic energy (5.8% for Dorud crude oil and 3.3% for kerosene is delivered to the flow of the fluid; however, a high increase in oil recovery enhancement (15% for Dorud crude oil and 12% for Kerosene is observed in the experiments. This proves that the ultrasonic waves, even when the contribution is not substantial, can be a significantly efficient method for flow enhancement.

Dog-Bone Horns for Piezoelectric Ultrasonic/Sonic Actuators

Science.gov (United States)

Sherrit, Stewart; Bar-Cohen, Yoseph; Chang, Zensheu; Bao, Xiaoqi

2007-01-01

A shape reminiscent of a dog bone has been found to be superior to other shapes for mechanical-amplification horns that are components of piezoelectrically driven actuators used in a series of related devices denoted generally as ultrasonic/sonic drill/corers (USDCs). The first of these devices was reported in Ultrasonic/Sonic Drill/Corers With Integrated Sensors (NPO-20856), NASA Tech Briefs, Vol. 25, No. 1 (January 2001), page 38. The dog-bone shape was conceived especially for use in a more recent device in the series, denoted an ultrasonic/ sonic gopher, that was described in Ultrasonic/Sonic Mechanisms for Drilling and Coring (NPO-30291), NASA Tech Briefs, Vol. 27, No. 9 (September 2003), page 65. The figure shows an example of a dog-bone-shaped horn and other components of an ultrasonic gopher. Prerequisite to a meaningful description of this development is an unavoidably lengthy recapitulation of the principle of operation of a USDC and, more specifically, of the ultrasonic/sonic gopher as described previously in NASA Tech Briefs. The ultrasonic actuator includes a stack of piezoelectric rings, the horn, a metal backing, and a bolt that connects the aforementioned parts and provides compressive pre-strain to the piezoelectric stack to prevent breakage of the rings during extension. The stack of piezoelectric rings is excited at the resonance frequency of the overall ultrasonic actuator. Through mechanical amplification by the horn, the displacement in the ultrasonic vibration reaches tens of microns at the tip of the horn. The horn hammers an object that is denoted the free mass because it is free to move longitudinally over a limited distance between hard stops: The free mass bounces back and forth between the ultrasonic horn and a tool bit (a drill bit or a corer). Because the longitudinal speed of the free mass is smaller than the longitudinal speed of vibration of the tip of the horn, contact between the free mass and the horn tip usually occurs at a

Enhanced ultrasonically assisted turning of a β-titanium alloy.

Science.gov (United States)

Maurotto, Agostino; Muhammad, Riaz; Roy, Anish; Silberschmidt, Vadim V

2013-09-01

Although titanium alloys have outstanding mechanical properties such as high hot hardness, a good strength-to-weight ratio and high corrosion resistance; their low thermal conductivity, high chemical affinity to tool materials severely impair their machinability. Ultrasonically assisted machining (UAM) is an advanced machining technique, which has been shown to improve machinability of a β-titanium alloy, namely, Ti-15-3-3-3, when compared to conventional turning processes. Copyright © 2013 Elsevier B.V. All rights reserved.

Antiproliferative activity of Curcuma phaeocaulis Valeton extract using ultrasonic assistance and response surface methodology.

Science.gov (United States)

Wang, Xiaoqin; Jiang, Ying; Hu, Daode

2017-01-02

The objective of the study was to optimize the ultrasonic-assisted extraction of curdione, furanodienone, curcumol, and germacrone from Curcuma phaeocaulis Valeton (Val.) and investigate the antiproliferative activity of the extract. Under the suitable high-performance liquid chromatography condition, the calibration curves for these four tested compounds showed high levels of linearity and the recoveries of these four compounds were between 97.9 and 104.3%. Response surface methodology (RSM) combining central composite design and desirability function (DF) was used to define optimal extraction parameters. The results of RSM and DF revealed that the optimum conditions were obtained as 8 mL g -1 for liquid-solid ratio, 70% ethanol concentration, and 20 min of ultrasonic time. It was found that the surface structures of the sonicated herbal materials were fluffy and irregular. The C. phaeocaulis Val. extract significantly inhibited the proliferation of RKO and HT-29 cells in vitro. The results reveal that the RSM can be effectively used for optimizing the ultrasonic-assisted extraction of bioactive components from C. phaeocaulis Val. for antiproliferative activity.

Study on Gap Flow Field Simulation in Small Hole Machining of Ultrasonic Assisted EDM

Science.gov (United States)

Liu, Yu; Chang, Hao; Zhang, Wenchao; Ma, Fujian; Sha, Zhihua; Zhang, Shengfang

2017-12-01

When machining a small hole with high aspect ratio in EDM, it is hard for the flushing liquid entering the bottom gap and the debris could hardly be removed, which results in the accumulation of debris and affects the machining efficiency and machining accuracy. The assisted ultrasonic vibration can improve the removal of debris in the gap. Based on dynamics simulation software Fluent, a 3D model of debris movement in the gap flow field of EDM small hole machining assisted with side flushing and ultrasonic vibration is established in this paper. When depth to ratio is 3, the laws of different amplitudes and frequencies on debris distribution and removal are quantitatively analysed. The research results show that periodic ultrasonic vibration can promote the movement of debris, which is beneficial to the removal of debris in the machining gap. Compared to traditional small hole machining in EDM, the debris in the machining gap is greatly reduced, which ensures the stability of machining process and improves the machining efficiency.

Endoscopically Assisted Drilling, Exposure of the Fundus through a Presigmoid Retrolabyrinthine Approach: A Cadaveric Feasibility Study.

Science.gov (United States)

Muelleman, Thomas; Shew, Matthew; Alvi, Sameer; Shah, Kushal; Staecker, Hinrich; Chamoun, Roukouz; Lin, James

2018-01-01

The presigmoid retrolabyrinthine approach to the cerebellopontine angle is traditionally described to not provide access to the internal auditory canal (IAC). We aimed to evaluate the extent of the IAC that could be exposed with endoscopically assisted drilling and to measure the percentage of the IAC that could be visualized with the microscope and various endoscopes after drilling had been completed. Presigmoid retrolabyrinthine approaches were performed bilaterally on 4 fresh cadaveric heads. We performed endoscopically assisted drilling to expose the fundus of the IAC, which resulted in exposure of the entire IAC in 8 of 8 temporal bone specimens. The microscope afforded a mean view of 83% (n = 8) of the IAC. The 0°, 30°, 45°, and 70° endoscope each afforded a view of 100% of the IAC in 8 of 8 temporal bone specimens. In conclusion, endoscopic drilling of the IAC of can provide an extradural means of exposing the entire length of the IAC while preserving the labyrinth.

Rotary ultrasonic machining of CFRP: A comparison with grinding.

Science.gov (United States)

Ning, F D; Cong, W L; Pei, Z J; Treadwell, C

2016-03-01

Carbon fiber reinforced plastic (CFRP) composites have been intensively used in various industries due to their superior properties. In aircraft and aerospace industry, a large number of holes are required to be drilled into CFRP components at final stage for aircraft assembling. There are two major types of methods for hole making of CFRP composites in industry, twist drilling and its derived multi-points machining methods, and grinding and its related methods. The first type of methods are commonly used in hole making of CFRP composites. However, in recent years, rotary ultrasonic machining (RUM), a hybrid machining process combining ultrasonic machining and grinding, has also been successfully used in drilling of CFRP composites. It has been shown that RUM is superior to twist drilling in many aspects. However, there are no reported investigations on comparisons between RUM and grinding in drilling of CFRP. In this paper, these two drilling methods are compared in five aspects, including cutting force, torque, surface roughness, hole diameter, and material removal rate. Copyright © 2015 Elsevier B.V. All rights reserved.

Ultrasonically Assisted Single Point Diamond Turning of Optical Mold of Tungsten Carbide

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Zhanjie Li

2018-02-01

Full Text Available To realize high efficiency, low/no damage and high precision machining of tungsten carbide used for lens mold, a high frequency ultrasonic vibration cutting system was developed at first. Then, tungsten carbide was precisely machined with a polycrystalline diamond (PCD tool assisted by the self-developed high frequency ultrasonic vibration cutting system. Tool wear mechanism was investigated in ductile regime machining of tungsten carbide. The cutter back-off phenomenon in the process was analyzed. The subsequent experimental results of ultra-precision machining with a single crystal diamond tool showed that: under the condition of high frequency ultrasonic vibration cutting, nano-scale surface roughness can be obtained by the diamond tool with smaller tip radius and no defects like those of ground surface were found on the machined surface. Tool wear mechanisms of the single crystal diamond tool are mainly abrasive wear and micro-chipping. To solve the problem, a method of inclined ultrasonic vibration cutting with negative rake angle was put forward according to force analysis, which can further reduce tool wear and roughness of the machined surface. The investigation was important to high efficiency and quality ultra-precision machining of tungsten carbide.

Salt-Assisted Ultrasonic Deaggregation of Nanodiamond.

Science.gov (United States)

Turcheniuk, K; Trecazzi, C; Deeleepojananan, C; Mochalin, V N

2016-09-28

We report a new facile, inexpensive, and contaminant-free technique of salt-assisted ultrasonic deaggregation (SAUD) of nanodiamond into single-digit particles stable in aqueous colloidal solution in a wide pH range. The technique utilizes the energy of ultrasound to break apart nanodiamond aggregates in sodium chloride aqueous slurry. In contrast to current deaggregation techniques, which introduce zirconia contaminants into nanodiamond, the single-digit nanodiamond colloids produced by SAUD have no toxic or difficult-to-remove impurities and are therefore well-suited to produce nanodiamonds for numerous applications, including theranostics, composites, and lubrication, etc. Requiring only aqueous slurry of sodium chloride and standard horn sonicator, and yielding highly pure well-dispersed nanodiamond colloids, the technique is an attractive alternative to current nanodiamond deaggregation protocols and can be easily implemented in any laboratory or scaled up for industrial use.

ZnO nanowire/TiO2 nanoparticle photoanodes prepared by the ultrasonic irradiation assisted dip-coating method

International Nuclear Information System (INIS)

Gan Xiaoyan; Li Xiaomin; Gao Xiangdong; Zhuge Fuwei; Yu Weidong

2010-01-01

Hybrid ZnO/TiO 2 photoanodes for dye-sensitized solar cells were prepared by combining ZnO nanowire (NW) arrays and TiO 2 nanoparticles (NPs) with the assistance of the ultrasonic irradiation assisted dip-coating method. Results show that the ultrasonic irradiation was an efficient way to promote the gap filling of TiO 2 NPs in the interstices of ZnO NWs. Hybrid ZnO NW/TiO 2 NP electrodes prepared with ultrasonic treatment exhibited better gap filling efficiency and higher visible absorptance. The overall conversion efficiency of the hybrid electrode was 0.79%, representing 35% improvement compared with that of the traditional one (0.58%). The enlarged surface area and improved attachments of TiO 2 NPs onto the walls of ZnO NWs induced by the application of ultrasonic irradiation may be the underlying reason. Electrochemical impedance spectroscopy measurements indicated that hybrid electrodes combined the advantages of improved electron transport along the ZnO NWs and increased surface area provided by infiltrated TiO 2 NPs, both of which are responsible for the improved cell efficiency.

Effects of Ultrasonics-Assisted Face Milling on Surface Integrity and Fatigue Life of Ni-Alloy 718

Science.gov (United States)

Suárez, Alfredo; Veiga, Fernando; de Lacalle, Luis N. López; Polvorosa, Roberto; Lutze, Steffen; Wretland, Anders

2016-11-01

This work investigates the effects of ultrasonic vibration-assisted milling on important aspects such us material surface integrity, tool wear, cutting forces and fatigue resistance. As an alternative to natural application of ultrasonic milling in brittle materials, in this study, ultrasonics have been applied to a difficult-to-cut material, Alloy 718, very common in high-temperature applications. Results show alterations in the sub-superficial part of the material which could influence fatigue resistance of the material, as it has been observed in a fatigue test campaign of specimens obtained with the application of ultrasonic milling in comparison with another batch obtained applying conventional milling. Tool wear pattern was found to be very similar for both milling technologies, concluding the study with the analysis of cutting forces, exhibiting certain improvement in case of the application of ultrasonic milling with a more stable evolution.

Ultrasonic assisted hot metal powder compaction.

Science.gov (United States)

Abedini, Rezvan; Abdullah, Amir; Alizadeh, Yunes

2017-09-01

Hot pressing of metal powders is used in production of parts with similar properties to wrought materials. During hot pressing processes, particle rearrangement, plastic deformation, creep, and diffusion are of the most effective powder densification mechanisms. Applying ultrasonic vibration is thought to result in great rates of densification and therefore higher efficiency of the process is expected. This paper deals with the effects of power ultrasonic on the densification of AA1100 aluminum powder under constant applied stress. The effects of particle size and process temperature on the densification behavior are discussed. The results show that applying ultrasonic vibration leads to an improved homogeneity and a higher relative density. Also, it is found that the effect of ultrasonic vibration is greater for finer particles. Copyright © 2016 Elsevier B.V. All rights reserved.

Ultrasonically-assisted Thermal Stir Welding System

Science.gov (United States)

Ding, R. Jeffrey (Inventor)

2014-01-01

A welding head assembly has a work piece disposed between its containment plates' opposing surfaces with the work piece being maintained in a plastic state thereof at least in a vicinity of the welding head assembly's stir rod as the rod is rotated about its longitudinal axis. The welding head assembly and the work piece experience relative movement there between in a direction perpendicular to the rod's longitudinal axis as the work piece is subjected to a compressive force applied by the containment plates. A first source coupled to the first containment plate applies a first ultrasonic wave thereto such that the first ultrasonic wave propagates parallel to the direction of relative movement. A second source coupled to the second containment plate applies a second ultrasonic wave thereto such that the second ultrasonic wave propagates parallel to the direction of relative movement.propagates parallel to the direction of relative movement.

Drilling Performance of Rock Drill by High-Pressure Water Jet under Different Configuration Modes

Directory of Open Access Journals (Sweden)

Songyong Liu

2017-01-01

Full Text Available In the rock drilling progress, the resistant force results in tools failure and the low drilling efficiency; thus, it is necessary to reduce the tools failure and enhance the drilling efficiency. In this paper, different configuration modes of drilling performance assisted with water jet are explored based on the mechanism and experiment analysis of rock drilling assisted with water jet. Moreover, the rotary sealing device with high pressure is designed to achieve the axial and rotation movement simultaneously as well as good sealing effect under high-pressure water jet. The results indicate that the NDB and NFB have better effects on drilling performance compared with that of NSB. Moreover, the high-pressure water jet is helpful not only to reduce the drill rod deflection, but also to reduce the probability of drill rod bending and improve the drill rod service life.

Optimization of ultrasonic-assisted extraction of pomegranate (Punica granatum L.) seed oil.

Science.gov (United States)

Tian, Yuting; Xu, Zhenbo; Zheng, Baodong; Martin Lo, Y

2013-01-01

The effectiveness of ultrasonic-assisted extraction (UAE) of pomegranate seed oil (PSO) was evaluated using a variety of solvents. Petroleum ether was the most effective for oil extraction, followed by n-hexane, ethyl acetate, diethyl ether, acetone, and isopropanol. Several variables, such as ultrasonic power, extraction temperature, extraction time, and the ratio of solvent volume and seed weight (S/S ratio) were studied for optimization using response surface methodology (RSM). The highest oil yield, 25.11% (w/w), was obtained using petroleum ether under optimal conditions for ultrasonic power, extraction temperature, extraction time, and S/S ratio at 140 W, 40 °C, 36 min, and 10 ml/g, respectively. The PSO yield extracted by UAE was significantly higher than by using Soxhlet extraction (SE; 20.50%) and supercriti cal fluid extraction (SFE; 15.72%). The fatty acid compositions were significantly different among the PSO extracted by Soxhlet extraction, SFE, and UAE, with punicic acid (>65%) being the most dominant using UAE. Copyright © 2012 Elsevier B.V. All rights reserved.

Mapping of an ultrasonic bath for ultrasound assisted extraction of mangiferin from Mangifera indica leaves.

Science.gov (United States)

Kulkarni, Vrushali M; Rathod, Virendra K

2014-03-01

The present work deals with the mapping of an ultrasonic bath for the maximum extraction of mangiferin from Mangifera indica leaves. I3(-) liberation experiments (chemical transformations) and extraction (physical transformations) were carried out at different locations in an ultrasonic bath and compared. The experimental findings indicated a similar trend in variation in an ultrasonic bath by both these methods. Various parameters such as position and depth of vessel in an ultrasonic bath, diameter and shape of a vessel, frequency and input power which affect the extraction yield have been studied in detail. Maximum yield of mangiferin obtained was approximately 31 mg/g at optimized parameters: distance of 2.54 cm above the bottom of the bath, 7 cm diameter of vessel, flat bottom vessel, 6.35 cm liquid height, 122 W input power and 25 kHz frequency. The present work indicates that the position and depth of vessel in an ultrasonic bath, diameter and shape of a vessel, frequency and input power have significant effect on the extraction yield. This work can be used as a base for all ultrasonic baths to obtain maximum efficiency for ultrasound assisted extraction. Copyright © 2013 Elsevier B.V. All rights reserved.

An ultrasonic corer for planetary rock sample retrieval

International Nuclear Information System (INIS)

Harkness, P; Cardoni, A; Lucas, M

2009-01-01

Several recent and planned space projects have been focussed on surface rovers for planetary missions, such as the U.S. Mars Exploration Rovers and the European ExoMars. The main functions of similar extraterrestrial vehicles in the future will be moving across planetary surfaces and retrieving rock samples. This paper presents a novel ultrasonic rock sampling tool tuned in a longitudinal-torsional mode along with the conceptual design of a full coring apparatus for preload delivery and core removal. Drilling and coring bits have been designed so that a portion of the longitudinal motion supplied by the ultrasonic transducer is converted into torsional motion. Results of drilling/coring trials are also presented.

Ultrasonic-assisted chemical reduction synthesis and structural characterization of copper nanoparticles

Science.gov (United States)

Anh-Nga, Nguyen T.; Tuan-Anh, Nguyen; Thanh-Quoc, Nguyen; Ha, Do Tuong

2018-04-01

Copper nanoparticles, due to their special properties, small dimensions and low-cost preparation, have many potential applications such as in optical, electronics, catalysis, sensors, antibacterial agents. In this study, copper nanoparticles were synthesized by chemical reduction method with different conditions in order to investigate the optimum conditions which gave the smallest (particle diameter) dimensions. The synthesis step used copper (II) acetate salt as precursor, ascorbic acid as reducing agent, glycerin and polyvinylpyrrolidone (PVP) as protector and stabilizer. The assistance of ultrasonic was were considered as the significant factor affecting the size of the synthesized particles. The results showed that the copper nanoparticles have been successfully synthesized with the diameter as small as 20-40 nm and the conditions of ultrasonic waves were 48 kHz of frequency, 20 minutes of treated time and 65-70 °C of temperature. The synthesized copper nanoparticles were characterized by optical absorption spectrum, scanning electron microscopy (SEM), and Fourier Transform Infrared Spectrometry.

Optimization of Ultrasonic-Assisted Extraction of Cordycepin from Cordyceps militaris Using Orthogonal Experimental Design

Directory of Open Access Journals (Sweden)

Hsiu-Ju Wang

2014-12-01

Full Text Available This study reports on the optimization of the extraction conditions of cordycepin from Cordyceps militaris by using ultrasonication. For this purpose, the orthogonal experimental design was used to investigate the effects of factors on the ultrasonic-assisted extraction (UAE. Four factors: extraction time (min, ethanol concentration (%, extraction temperature (°C and extraction frequency (kHz, were studied. The results showed that the highest cordycepin yield of 7.04 mg/g (86.98% ± 0.23% was obtained with an extraction time of 60 min, ethanol concentration of 50%, extraction temperature of 65 °C and extraction frequency of 56 kHz. It was found that the cordycepin extraction yield increased with the effect of ultrasonication during the extraction process. Therefore, UAE can be used as an alternative to conventional immersion extraction with respect to the recovery of cordycepin from C. militaris, with the advantages of shorter extraction time and reduced solvent consumption.

Sandia's Geothermal Advanced Drill Rig Instrumentation Assists Critical Oil and Gas Drilling Operation

International Nuclear Information System (INIS)

Staller, George E.; Whitlow, Gary

1999-01-01

On November 23, 1998, an 18,000-foot-deep wild-cat natural gas well being drilled near Bakersfield, CA blew out and caught fire. All attempts to kill this well failed, and the well continues to flow under limited control, producing large volumes of natural gas, salt water, and some oil. The oil and some of the water is being separated and trucked off site, and the remaining gas and water is being burned at the well head. A relief well is being drilled approximately one-quarter mile away in an attempt to intercept the first well. If the relief well is successful, it will be used to cement in and kill the first well. Epoch Wellsite Services, Inc., the mud-logging company for the initial well and the relief well, requested Sandia's rolling float meter (RFM) for these critical drilling operations. The RFM is being used to measure the mud outflow rate and detect kicks while drilling the relief well, which will undoubtedly encounter reservoir conditions similar to those responsible for the blow out. Based on its prior experience with the RFM, Epoch believes that it is the only instrument capable of providing the level of accuracy and response to mudflow needed to quickly detect kicks and minimize the risk of a blowout on this second critical well. In response to the urgent request from industry, Sandia and Epoch technicians installed the RFM on the relief well return line, and completed its initial calibration. The data from the RFM is displayed in real-time for the driller, the companyman, and the toolpusher via Epochs RIGWATCH Drilling Instmmentation System. The RFM has already detected several small kicks while drilling toward the annulus of the blown out well. A conventional paddle meter is located downstream of the RFM to provide redundancy and the opportunity to compare the two meters in an actual drilling operation, The relief well is nearing 14,000 feet deep, targeting an intercept of the first well near 17,600 feet. The relief well is expected to be completed in

Co-treatment of spent cathode carbon in caustic and acid leaching process under ultrasonic assisted for preparation of SiC.

Science.gov (United States)

Yuan, Jie; Xiao, Jin; Li, Fachuang; Wang, Bingjie; Yao, Zhen; Yu, Bailie; Zhang, Liuyun

2018-03-01

Spent cathode carbon (SCC) from aluminum electrolysis has been treated in ultrasonic-assisted caustic leaching and acid leaching process, and purified SCC used as carbon source to synthesize silicon carbide (SiC) was investigated. Chemical and mineralogical properties have been characterized by X-ray diffraction (XRD), X-ray fluorescence (XRF), scanning electron microscopy (SEM), and thermogravimetry and differential scanning calorimetry (TGA-DSC). Various experimental factors temperature, time, liquid-solid ratio, ultrasonic power, and initial concentration of alkali or acid affecting on SCC leaching result were studied. After co-treatment with ultrasonic-assisted caustic leaching and acid leaching, carbon content of leaching residue was 97.53%. SiC power was synthesized by carbothermal reduction at 1600 °C, as a result of yield of 76.43%, and specific surface area of 4378 cm 2 /g. This is the first report of using purified SCC and gangue to prepare SiC. The two industrial wastes have been used newly as secondary sources. Furthermore, ultrasonic showed significant effect in SCC leaching process. Copyright © 2017 Elsevier B.V. All rights reserved.

Ultrasonic-assisted enzymatic extraction of phenolics from broccoli (Brassica oleracea L. var. italica) inflorescences and evaluation of antioxidant activity in vitro.

Science.gov (United States)

Wu, Hao; Zhu, Junxiang; Yang, Long; Wang, Ran; Wang, Chengrong

2015-06-01

An efficient ultrasonic-assisted enzymatic extraction technique was applied to extracting phenolics from broccoli inflorescences without organic solvents. The synergistic model of enzymolysis and ultrasonication simultaneously was selected, and the enzyme combination was optimized by orthogonal test: cellulase 7.5 mg/g FW (fresh weight), pectinase 10 mg/g FW, and papain 1.0 mg/g FW. The operating parameters in ultrasonic-assisted enzymatic extraction were optimized with response surface methodology using Box-Behnken design. The optimal extraction conditions were as follows: ultrasonic power, 440 W; liquid to material ratio, 7.0:1 mL/g; pH value of 6.0 at 54.5 ℃ for 10 min. Under these conditions, the extraction yield of phenolics achieved 1.816 ± 0.0187 mg gallic acid equivalents/gram FW. The free radical scavenging activity of ultrasonic-assisted enzymatic extraction extracts was determined by 1,1-diphenyl-2-picrylhydrazyl·assay with EC50 values of 0.25, and total antioxidant activity was determined by ferric reducing antioxidant power assay with ferric reducing antioxidant power value of 0.998 mmol FeSO4/g compared with the referential ascorbic acid of 1.184 mmol FeSO4/g. © The Author(s) 2014 Reprints and permissions: sagepub.co.uk/journalsPermissions.nav.

The effect of thermal conductivity of the tool electrode in spark-assisted chemical engraving gravity-feed micro-drilling

International Nuclear Information System (INIS)

Mousa, M; Allagui, A; Ng, H D; Wüthrich, R

2009-01-01

Spark-assisted chemical engraving (SACE) is a non-traditional micro-machining technology based on electrochemical discharge phenomena. In SACE gravity-feed micro-drilling, various parameters including the thermal properties of the tool electrode play a significant role in the process. Based on a series of experiments using tool electrodes with different thermal properties, the effect in SACE gravity-feed micro-drilling is discussed. It is demonstrated that machining with higher thermal conductivity tool electrodes results in faster machining during the discharge regime and slower machining during the hydrodynamic regime of SACE gravity-feed micro-drilling

Ultrasonic stress evaluation through thickness of a stainless steel pressure vessel

International Nuclear Information System (INIS)

Javadi, Yashar; Pirzaman, Hamed Salimi; Raeisi, Mohammadreza Hadizadeh; Najafabadi, Mehdi Ahmadi

2014-01-01

This paper investigates ultrasonic method in stress measurement through thickness of a pressure vessel. Longitudinal critically refracted (L CR ) waves are employed to measure the welding residual stresses in a vessel constructed from austenitic stainless steel 304L. The acoustoelastic constant is measured through a hydro test to keep the pressure vessel intact. Hoop and axial residual stresses are evaluated by using different frequency range of ultrasonic transducers. The welding processes of vessel shell and caps are simulated by a 3D finite element (FE) model which is validated by hole-drilling method. The residual stresses calculated by FE simulation are then compared with those obtained from the ultrasonic measurement while a good agreement is observed. It is demonstrated that the residual stresses through thickness of the stainless steel pressure vessel can be evaluated by combining FE and L CR method (known as FEL CR method). - Highlights: • The main goal is ultrasonic evaluation of through thickness stresses. • Welding processes of a stainless steel pressure vessel are modelled by FE. • The hole-drilling method is used to validate the FE results. • Residual stresses are measured by four different series of ultrasonic transducers. • The comparison between ultrasonic and FE results show an acceptable agreement

PROSPECTS FOR APPLICATION OF FLEXIBLE ULTRASONIC WAVEGUIDE SYSTEMS IN MEDICINE AND ENGINEERING

Directory of Open Access Journals (Sweden)

V. T. Minchenya

2010-01-01

Full Text Available The article presents comprehensive review of current and possible future applications of flexible ultrasonic waveguides in medicine and engineering. Issues of design, modelling and manufacturing of flexible waveguides are considered. The article also presents some results of the authors in this field, particularly modelling techniques developed for the design of flexible waveguides and ultrasonic technologies and equipment for ultrasonic thromboectomy, heating of frozen fuel and ultrasonic drilling of brittle materials. Novel technology for manufacturing flexible waveguides based on electrolytic-plasma machining is also described

Wear reduction through piezoelectrically-assisted ultrasonic lubrication

International Nuclear Information System (INIS)

Dong, Sheng; J Dapino, Marcelo

2014-01-01

Traditional lubricants are undesirable in harsh aerospace environments and certain automotive applications. Ultrasonic vibrations can be used to reduce and modulate the effective friction coefficient between two sliding surfaces. This paper investigates the relationship between friction force reduction and wear reduction in ultrasonically lubricated surfaces. A pin-on-disc tribometer is modified through the addition of a piezoelectric transducer which vibrates the pin at 22 kHz in the direction perpendicular to the rotating disc surface. Friction and wear metrics including volume loss, surface roughness, friction forces and apparent stick-slip effects are measured without and with ultrasonic vibrations at three different sliding velocities. SEM imaging and 3D profilometry are used to characterize the wear surfaces and guide model development. Over the range of speeds considered, ultrasonic vibrations reduce the effective friction force up to 62% along with a wear reduction of up to 49%. A simple cube model previously developed to quantify friction force reduction is implemented which describes wear reduction within 15% of the experimental data. (paper)

Effects of ultrasonic assisted cooking on the chemical profiles of taste and flavor of spiced beef.

Science.gov (United States)

Zou, Yunhe; Kang, Dacheng; Liu, Rui; Qi, Jun; Zhou, Guanghong; Zhang, Wangang

2018-09-01

The objective of this study was to assess the effects of ultrasonic assisted cooking on the chemical profiles of spiced beef taste and flavor. Ultrasound power with 0 W, 400 W, 600 W, 800 W and 1000 W (frequency of 20 kHz) were used for cooking 120 min. The sodium chloride, sugar, free amino acids (FAAs), 5'-ribonucleotides, lipid oxidation, volatile flavor substance contents and electronic nose of spiced beef were determined. Results showed that ultrasonic treatment could significantly increase the content of sodium chloride in beef sample (P  0.05). With the ultrasonic treatment, the types and relative content of volatile flavor substances were significantly increased (P alcohols and ketones. However, there was no significant variation among the different ultrasound power groups (P > 0.05). This result was consistent with the measurement of electronic nose. Data points of control samples were away from ultrasonic treatment groups, while data points of different ultrasonic treatment groups were flock together. The results indicate that the application of ultrasound during cooking has a positive effect on chemical profiles of spiced beef taste and flavor, particularly for the power of 800 W. Copyright © 2018 Elsevier B.V. All rights reserved.

Vehicle tracking for an evasive manoeuvres assistant using low-cost ultrasonic sensors.

Science.gov (United States)

Jiménez, Felipe; Naranjo, José E; Gómez, Oscar; Anaya, José J

2014-11-28

Many driver assistance systems require knowledge of the vehicle environment. As these systems are increasing in complexity and performance, this knowledge of the environment needs to be more complete and reliable, so sensor fusion combining long, medium and short range sensors is now being used. This paper analyzes the feasibility of using ultrasonic sensors for low cost vehicle-positioning and tracking in the lane adjacent to the host vehicle in order to identify free areas around the vehicle and provide information to an automatic avoidance collision system that can perform autonomous braking and lane change manoeuvres. A laser scanner is used for the early detection of obstacles in the direction of travel while two ultrasonic sensors monitor the blind spot of the host vehicle. The results of tests on a test track demonstrate the ability of these sensors to accurately determine the kinematic variables of the obstacles encountered, despite a clear limitation in range.

Vehicle Tracking for an Evasive Manoeuvres Assistant Using Low-Cost Ultrasonic Sensors

Directory of Open Access Journals (Sweden)

Felipe Jiménez

2014-11-01

Full Text Available Many driver assistance systems require knowledge of the vehicle environment. As these systems are increasing in complexity and performance, this knowledge of the environment needs to be more complete and reliable, so sensor fusion combining long, medium and short range sensors is now being used. This paper analyzes the feasibility of using ultrasonic sensors for low cost vehicle-positioning and tracking in the lane adjacent to the host vehicle in order to identify free areas around the vehicle and provide information to an automatic avoidance collision system that can perform autonomous braking and lane change manoeuvres. A laser scanner is used for the early detection of obstacles in the direction of travel while two ultrasonic sensors monitor the blind spot of the host vehicle. The results of tests on a test track demonstrate the ability of these sensors to accurately determine the kinematic variables of the obstacles encountered, despite a clear limitation in range.

Binary Solvent Extraction System and Extraction Time Effects on Phenolic Antioxidants from Kenaf Seeds (Hibiscus cannabinus L.) Extracted by a Pulsed Ultrasonic-Assisted Extraction

OpenAIRE

Yu Hua Wong; Hwee Wen Lau; Chin Ping Tan; Kamariah Long; Kar Lin Nyam

2014-01-01

The aim of this study was to determine the best parameter for extracting phenolic-enriched kenaf (Hibiscus cannabinus L.) seeds by a pulsed ultrasonic-assisted extraction. The antioxidant activities of ultrasonic-assisted kenaf seed extracts (KSE) were determined by a 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging capacity assay, 2,2′-azino-bis(3-ethylbenzothiazoline-6-sulphonic acid) (ABTS) radical scavenging assay, β -carotene bleaching inhibition assay, and ferric reducing antioxi...

Recent progress in online ultrasonic process monitoring

Science.gov (United States)

Wen, Szu-Sheng L.; Chen, Tzu-Fang; Ramos-Franca, Demartonne; Nguyen, Ky T.; Jen, Cheng-Kuei; Ihara, Ikuo; Derdouri, A.; Garcia-Rejon, Andres

1998-03-01

On-line ultrasonic monitoring of polymer co-extrusion and gas-assisted injection molding are presented. During the co- extrusion of high density polyethylene and Santoprene ultrasonic sensors consisting of piezoelectric transducers and clad ultrasonic buffer rods are used to detect the interface between these two polymers and the stability of the extrusion. The same ultrasonic sensor also measures the surface temperature of the extruded polymer. The results indicate that temperature measurements using ultrasound have a faster response time than those obtained by conventional thermocouple. In gas-assisted injection molding the polymer and gas flow front positions are monitored simultaneously. This information may be used to control the plunger movement.

Enhanced Sonocatalytic Degradation of Rhodamine B by Graphene-TiO2 Composites Synthesized by an Ultrasonic-Assisted Method%Enhanced Sonocatalytic Degradation of Rhodamine B by Graphene-TiO2 Composites Synthesized by an Ultrasonic-Assisted Method

Institute of Scientific and Technical Information of China (English)

ZHU Lei; Trisha GHOSH; Chong-Yeon PARK; MENG Ze-Da; OH Won-Chun

2012-01-01

A series of graphene-TiO2 composites was fabricated from graphene oxide and titanium n-butoxide (TNB) by an ultrasonic-assisted method.The structure and composition of the nanocomposites were characterized by Raman spectroscopy,BET surface area measurements,X-ray diffraction,transmission electron microscopy,and ultraviolet-visible absorption spectroscopy.The average size of the TiO2 nanoparticles on the graphene nanosheets was controlled at around 10-15 nm without using surfactant,which is attributed to the pyrolysis and condensation of dissolved TNB into TiO2 by ultrasonic irradiation.The catalytic activity of the composites under ultrasonic irradiation was determined using a rhodamine B (RhB) solution.The graphene-TiO2 composites possessed a high specific surface area,which increased the decolorization rate for RhB solution.This is because the graphene and TiO2 nanoparticles in the composites interact strongly,which enhances the photoelectric conversion of TiO2 by reducing the recombination ofphotogenerated electron-hole pairs.

Process optimization for ultrasonic vibration assisted polishing of micro-structured surfaces on super hard material

Science.gov (United States)

Sun, Zhiyuan; Guo, Bing; Rao, Zhimin; Zhao, Qingliang

2014-08-01

In consideration of the excellent property of SiC, the ground micro-structured surface quality is hard to meet the requirement - consequently the ultrasonic vibration assisted polishing (UVAP) of micro-structures of molds is proposed in this paper. Through the orthogonal experiment, the parameters of UVAP of micro-structures were optimized. The experimental results show that, abrasive polishing process, the effect of the workpiece feed rate on the surface roughness (Ra), groove tip radius (R) and material removal rate (MRR) of micro-structures is significant. While, the UVAP, the most significant effect factor for Ra, R and MRR is the ultrasonic amplitude of the ultrasonic vibration. In addition, within the scope of the polishing process parameters selected by preliminary experiments, ultrasonic amplitude of 2.5μm, polishing force of 0.5N, workpiece feed rate of 5 mm·min-1, polishing wheel rotational speed of 50rpm, polishing time of 35min, abrasive size of 100nm and the polishing liquid concentration of 15% is the best technology of UVAP of micro-structures. Under the optimal parameters, the ground traces on the micro-structured surface were removed efficiently and the integrity of the edges of the micro-structure after grinding was maintained efficiently.

Ultrasonic-assisted production of biodiesel from transesterification of palm oil over ostrich eggshell-derived CaO catalysts.

Science.gov (United States)

Chen, Guanyi; Shan, Rui; Shi, Jiafu; Yan, Beibei

2014-11-01

In this study, waste ostrich eggshell-derived calcium oxide (denoted as CaO(OE)) particles were synthesized and explored as cost-effective catalysts for the ultrasonic-assisted transesterification of palm oil. The physicochemical properties of the resultant catalysts were characterized by XRD, N2 adsorption, XRF and Hammett indicator, while the catalytic activity was evaluated through transesterification of palm oil with methanol under ultrasonic conditions. More specifically, the CaO(OE) showed comparable catalytic activity to the one derived from commercial calcium carbonate (denoted as CaO(Lab)). Moreover, under ultrasonic conditions, the catalytic activity of CaO(OE) could be enhanced significantly. The maximum yield of fatty acid methyl esters could reach 92.7% under the optimal condition of reaction time of 60 min with ultrasonic power of 60% (120 W), methanol-to-oil ratio of 9:1, and catalyst loading of 8 wt.%. The results indicated that the CaO(OE) catalysts showed good catalytic performance and reusability, and may potentially reduce the cost of biodiesel production. Copyright © 2014 Elsevier Ltd. All rights reserved.

Ultrasonic-assisted synthesis of monodisperse single-crystalline silver nanoplates and gold nanorings.

Science.gov (United States)

Jiang, Li-Ping; Xu, Shu; Zhu, Jian-Min; Zhang, Jian-Rong; Zhu, Jun-Jie; Chen, Hong-Yuan

2004-09-20

A simple sonochemical route was developed for the crystal growth of uniform silver nanoplates and ringlike gold nanocrystals in a N,N-dimethylformamide solution. The platelike structures were generated from the selective growth on different crystal planes in the presence of poly(vinylpyrrolidone) and the ultrasonic-assisted Ostwald ripening processes. The silver nanoplates in solution served as the templates for the synthesis of ringlike gold crystals via a displacement reaction. Both the silver nanoplates and gold nanorings were highly oriented single crystals with (111) planes as the basal planes. Copyright 2004 American Chemical Society

Thumb-size ultrasonic-assisted spectroscopic imager for in-situ glucose monitoring as optional sensor of conventional dialyzers

Science.gov (United States)

Nogo, Kosuke; Mori, Keita; Qi, Wei; Hosono, Satsuki; Kawashima, Natsumi; Nishiyama, Akira; Wada, Kenji; Ishimaru, Ichiro

2016-03-01

We proposed the ultrasonic-assisted spectroscopic imaging for the realization of blood-glucose-level monitoring during dialytic therapy. Optical scattering and absorption caused by blood cells deteriorate the detection accuracy of glucose dissolved in plasma. Ultrasonic standing waves can agglomerate blood cells at nodes. In contrast, around anti-node regions, the amount of transmitted light increases because relatively clear plasma appears due to decline the number of blood cells. Proposed method can disperse the transmitted light of plasma without time-consuming pretreatment such as centrifugation. To realize the thumb-size glucose sensor which can be easily attached to dialysis tubes, an ultrasonic standing wave generator and a spectroscopic imager are required to be small. Ultrasonic oscillators are ∅30[mm]. A drive circuit of oscillators, which now size is 41×55×45[mm], is expected to become small. The trial apparatus of proposed one-shot Fourier spectroscopic imager, whose size is 30×30×48[mm], also can be little-finger size in principal. In the experiment, we separated the suspension mixed water and micro spheres (Θ10[mm) into particles and liquid regions with the ultrasonic standing wave (frequency: 2[MHz]). Furthermore, the spectrum of transmitted light through the suspension could be obtained in visible light regions with a white LED.

Ultrasonic-assisted Aqueous Extraction and Physicochemical Characterization of Oil from Clanis bilineata.

Science.gov (United States)

Sun, Mingmei; Xu, Xiao; Zhang, Qiuqin; Rui, Xin; Wu, Junjun; Dong, Mingsheng

2018-02-01

Ultrasound-assisted aqueous extraction (UAAE) was used to extract oil from Clanis bilineata (CB), a traditional edible insect that can be reared on a large scale in China, and the physicochemical property and antioxidant capacity of the UAAE-derived oil (UAAEO) were investigated for the first time. UAAE conditions of CB oil was optimized using response surface methodology (RSM) and the highest oil yield (19.47%) was obtained under optimal conditions for ultrasonic power, extraction temperature, extraction time, and ultrasonic interval time at 400 W, 40°C, 50 min, and 2 s, respectively. Compared with Soxhlet extraction-derived oil (SEO), UAAEO had lower acid (AV), peroxide (PV) and p-anisidine values (PAV) as well as higher polyunsaturated fatty acids contents and thermal stability. Furthermore, UAAEO showed stronger antioxidant activities than those of SEO, according to DPPH radical scavenging and β-carotene bleaching tests. Therefore, UAAE is a promising process for the large-scale production of CB oil and CB has a developing potential as functional oil resource.

Ultrasonic-assisted solution combustion synthesis of porous Na{sub 3}V{sub 2}(PO{sub 4}){sub 3}/C: formation mechanism and sodium storage performance

Energy Technology Data Exchange (ETDEWEB)

Chen, Qiuyun; Liu, Qing [Huazhong University of Science and Technology, State Key Laboratory of Materials Processing and Die and Mould Technology (China); Chu, Xiangcheng; Zhang, Yiling [Tsinghua University, State Key Laboratory of New Ceramic and Fine Processing (China); Yan, Youwei; Xue, Lihong, E-mail: xuelh@hust.edu.cn; Zhang, Wuxing, E-mail: zhangwx@hust.edu.cn [Huazhong University of Science and Technology, State Key Laboratory of Materials Processing and Die and Mould Technology (China)

2017-04-15

Solution combustion synthesis (SCS) is an effective and rapid method for synthesizing nanocrystalline materials. However, the control over size, morphology, and microstructure are rather limited in SCS. Here, we develop a novel ultrasonic-assisted solution combustion route to synthesize the porous and nano-sized Na{sub 3}V{sub 2}(PO{sub 4}){sub 3}/C composites, and reveal the effects of ultrasound on the structural evolution of NVP/C. Due to the cavitation effects generated from ultrasonic irradiation, the ultrasonic-assisted SCS can produce honeycomb precursor, which can be further transformed into porous Na{sub 3}V{sub 2}(PO{sub 4}){sub 3}/C with reticular and hollow structures after thermal treatment. When used as cathode material for Na-ion batteries, the porous Na{sub 3}V{sub 2}(PO{sub 4}){sub 3}/C delivers an initial discharge capacity of 118 mAh g{sup −1} at 0.1 C and an initial coulombic efficiency of 85%. It can retain 93.8% of the initial capacity after 120 cycles at 0.2 C. The results demonstrate that ultrasonic-assisted SCS can be a new strategy to design crystalline nanomaterials with tunable microstructures.

Synthesis of hydroxyapatite nanoparticles by a novel ultrasonic assisted with mixed hollow sphere template method

Science.gov (United States)

Gopi, D.; Indira, J.; Kavitha, L.; Sekar, M.; Mudali, U. Kamachi

Hydroxyapatite (HAP) is the main inorganic component of bone material and is widely used in various biomedical applications due to its excellent bioactivity and biocompatibility. In this paper, we have reported the synthesis of hydroxyapatite nanoparticles by a novel ultrasonic assisted mixed template directed method. In this method glycine-acrylic acid (GLY-AA) hollow spheres were used as an organic template which could be prepared by mixing of glycine with acrylic acid. The as-synthesized HAP nanoparticles were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and tunnelling electron microscope (TEM) to investigate the nature of bonding, crystallinity, size and shape. The thermal stability of as-synthesized nanoparticles was also investigated by the thermo gravimetric analysis (TGA). The effect of ultrasonic irradiation time on the crystallinity and size of the HAP nanoparticles in presence of glycine-acrylic acid hollow spheres template were investigated. From the inspection of the above results it is confirmed that the crystallinity and size of the HAP nanoparticles decrease with increasing ultrasonic irradiation time. Hence the proposed synthesis strategy provides a facile pathway to obtain nano sized HAP with high quality, suitable size and morphology.

Soft Sensing of Non-Newtonian Fluid Flow in Open Venturi Channel Using an Array of Ultrasonic Level Sensors—AI Models and Their Validations

Science.gov (United States)

Viumdal, Håkon; Mylvaganam, Saba

2017-01-01

In oil and gas and geothermal installations, open channels followed by sieves for removal of drill cuttings, are used to monitor the quality and quantity of the drilling fluids. Drilling fluid flow rate is difficult to measure due to the varying flow conditions (e.g., wavy, turbulent and irregular) and the presence of drilling cuttings and gas bubbles. Inclusion of a Venturi section in the open channel and an array of ultrasonic level sensors above it at locations in the vicinity of and above the Venturi constriction gives the varying levels of the drilling fluid in the channel. The time series of the levels from this array of ultrasonic level sensors are used to estimate the drilling fluid flow rate, which is compared with Coriolis meter measurements. Fuzzy logic, neural networks and support vector regression algorithms applied to the data from temporal and spatial ultrasonic level measurements of the drilling fluid in the open channel give estimates of its flow rate with sufficient reliability, repeatability and uncertainty, providing a novel soft sensing of an important process variable. Simulations, cross-validations and experimental results show that feedforward neural networks with the Bayesian regularization learning algorithm provide the best flow rate estimates. Finally, the benefits of using this soft sensing technique combined with Venturi constriction in open channels are discussed. PMID:29072595

Ultrasonic-Assisted Extraction of Raspberry Seed Oil and Evaluation of Its Physicochemical Properties, Fatty Acid Compositions and Antioxidant Activities.

Directory of Open Access Journals (Sweden)

Hui Teng

Full Text Available Ultrasonic-assisted extraction was employed for highly efficient separation of aroma oil from raspberry seeds. A central composite design with two variables and five levels was employed and effects of process variables of sonication time and extraction temperature on oil recovery and quality were investigated. Optimal conditions predicted by response surface methodology were sonication time of 37 min and extraction temperature of 54°C. Specifically, ultrasonic-assisted extraction (UAE was able to provide a higher content of beneficial unsaturated fatty acids, whereas conventional Soxhlet extraction (SE resulted in a higher amount of saturated fatty acids. Moreover, raspberry seed oil contained abundant amounts of edible linoleic acid and linolenic acid, which suggest raspberry seeds could be valuable edible sources of natural γ-linolenic acid products. In comparison with SE, UAE exerted higher free radical scavenging capacities. In addition, UAE significantly blocked H2O2-induced intracellular reactive oxygen species (ROS generation.

Synthesis of hydroxyapatite nanoparticles by a novel ultrasonic assisted with mixed hollow sphere template method.

Science.gov (United States)

Gopi, D; Indira, J; Kavitha, L; Sekar, M; Mudali, U Kamachi

2012-07-01

Hydroxyapatite (HAP) is the main inorganic component of bone material and is widely used in various biomedical applications due to its excellent bioactivity and biocompatibility. In this paper, we have reported the synthesis of hydroxyapatite nanoparticles by a novel ultrasonic assisted mixed template directed method. In this method glycine-acrylic acid (GLY-AA) hollow spheres were used as an organic template which could be prepared by mixing of glycine with acrylic acid. The as-synthesized HAP nanoparticles were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and tunnelling electron microscope (TEM) to investigate the nature of bonding, crystallinity, size and shape. The thermal stability of as-synthesized nanoparticles was also investigated by the thermo gravimetric analysis (TGA). The effect of ultrasonic irradiation time on the crystallinity and size of the HAP nanoparticles in presence of glycine-acrylic acid hollow spheres template were investigated. From the inspection of the above results it is confirmed that the crystallinity and size of the HAP nanoparticles decrease with increasing ultrasonic irradiation time. Hence the proposed synthesis strategy provides a facile pathway to obtain nano sized HAP with high quality, suitable size and morphology. Copyright © 2012 Elsevier B.V. All rights reserved.

Laser induced ultrasonic phased array using full matrix capture data acquisition and total focusing method.

Science.gov (United States)

Stratoudaki, Theodosia; Clark, Matt; Wilcox, Paul D

2016-09-19

Laser ultrasonics is a technique where lasers are employed to generate and detect ultrasound. A data collection method (full matrix capture) and a post processing imaging algorithm, the total focusing method, both developed for ultrasonic arrays, are modified and used in order to enhance the capabilities of laser ultrasonics for nondestructive testing by improving defect detectability and increasing spatial resolution. In this way, a laser induced ultrasonic phased array is synthesized. A model is developed and compared with experimental results from aluminum samples with side drilled holes and slots at depths of 5 - 20 mm from the surface.

Economic environmental management of drilling operations

International Nuclear Information System (INIS)

Longwell, H.J.; Akers, T.J.

1992-01-01

This paper presents significant environmental and regulatory initiatives developed by Exxon's New Orleans Drilling Organization. Specifically, the paper will cover drilling waste minimization techniques and disposal options, recycling of drilling waste streams, and environmentally managed drilling location design considerations. The implementation of some of these initiatives at Exxon's Chalkley field land locations have resulted in a fifty percent reduction in drilling location waste management costs. Some of these same initiatives have been successfully applied to Exxon's barge drilling locations. For operations at the environmentally sensitive Mobile Bay, Exxon contracted with a local company and assisted in the development of an economically and environmentally superior drilling waste disposal and treatment system. In summary, it is possible for drilling operators to pro-actively manage escalating environmental and regulatory challenges through the implementation of economic and practical initiatives

Fluoroscopy-Guided Percutaneous Vertebral Body Biopsy Using a Novel Drill-Powered Device: Technical Case Series

International Nuclear Information System (INIS)

Wallace, Adam N.; Pacheco, Rafael A.; Tomasian, Anderanik; Hsi, Andy C.; Long, Jeremiah; Chang, Randy O.; Jennings, Jack W.

2016-01-01

BackgroundA novel coaxial biopsy system powered by a handheld drill has recently been introduced for percutaneous bone biopsy. This technical note describes our initial experience performing fluoroscopy-guided vertebral body biopsies with this system, compares the yield of drill-assisted biopsy specimens with those obtained using a manual technique, and assesses the histologic adequacy of specimens obtained with drill assistance.MethodsMedical records of all single-level, fluoroscopy-guided vertebral body biopsies were reviewed. Procedural complications were documented according to the Society of Interventional Radiology classification. The total length of bone core obtained from drill-assisted biopsies was compared with that of matched manual biopsies. Pathology reports were reviewed to determine the histologic adequacy of specimens obtained with drill assistance.ResultsTwenty eight drill-assisted percutaneous vertebral body biopsies met study inclusion criteria. No acute complications were reported. Of the 86 % (24/28) of patients with clinical follow-up, no delayed complications were reported (median follow-up, 28 weeks; range 5–115 weeks). The median total length of bone core obtained from drill-assisted biopsies was 28 mm (range 8–120 mm). This was longer than that obtained from manual biopsies (median, 20 mm; range 5–45 mm; P = 0.03). Crush artifact was present in 11 % (3/28) of drill-assisted biopsy specimens, which in one case (3.6 %; 1/28) precluded definitive diagnosis.ConclusionsA drill-assisted, coaxial biopsy system can be used to safely obtain vertebral body core specimens under fluoroscopic guidance. The higher bone core yield obtained with drill assistance may be offset by the presence of crush artifact

Fluoroscopy-Guided Percutaneous Vertebral Body Biopsy Using a Novel Drill-Powered Device: Technical Case Series

Energy Technology Data Exchange (ETDEWEB)

Wallace, Adam N., E-mail: wallacea@mir.wustl.edu; Pacheco, Rafael A., E-mail: pachecor@mir.wustl.edu; Tomasian, Anderanik, E-mail: tomasiana@mir.wustl.edu [Washington University School of Medicine, Mallinckrodt Institute of Radiology (United States); Hsi, Andy C., E-mail: hsia@path.wustl.edu [Washington University School of Medicine, Division of Anatomic Pathology, Department of Pathology & Immunology (United States); Long, Jeremiah, E-mail: longj@mir.wustl.edu [Washington University School of Medicine, Mallinckrodt Institute of Radiology (United States); Chang, Randy O., E-mail: changr@wusm.wustl.edu [Washington University School of Medicine (United States); Jennings, Jack W., E-mail: jenningsj@mir.wustl.edu [Washington University School of Medicine, Mallinckrodt Institute of Radiology (United States)

2016-02-15

BackgroundA novel coaxial biopsy system powered by a handheld drill has recently been introduced for percutaneous bone biopsy. This technical note describes our initial experience performing fluoroscopy-guided vertebral body biopsies with this system, compares the yield of drill-assisted biopsy specimens with those obtained using a manual technique, and assesses the histologic adequacy of specimens obtained with drill assistance.MethodsMedical records of all single-level, fluoroscopy-guided vertebral body biopsies were reviewed. Procedural complications were documented according to the Society of Interventional Radiology classification. The total length of bone core obtained from drill-assisted biopsies was compared with that of matched manual biopsies. Pathology reports were reviewed to determine the histologic adequacy of specimens obtained with drill assistance.ResultsTwenty eight drill-assisted percutaneous vertebral body biopsies met study inclusion criteria. No acute complications were reported. Of the 86 % (24/28) of patients with clinical follow-up, no delayed complications were reported (median follow-up, 28 weeks; range 5–115 weeks). The median total length of bone core obtained from drill-assisted biopsies was 28 mm (range 8–120 mm). This was longer than that obtained from manual biopsies (median, 20 mm; range 5–45 mm; P = 0.03). Crush artifact was present in 11 % (3/28) of drill-assisted biopsy specimens, which in one case (3.6 %; 1/28) precluded definitive diagnosis.ConclusionsA drill-assisted, coaxial biopsy system can be used to safely obtain vertebral body core specimens under fluoroscopic guidance. The higher bone core yield obtained with drill assistance may be offset by the presence of crush artifact.

Cybersonics: Tapping into Technology

Science.gov (United States)

2001-01-01

With the assistance of Small Business Innovation Research (SBIR) funding from NASA's Jet Propulsion Laboratory, Cybersonics, Inc., developed an ultrasonic drill with applications ranging from the medical industry to space exploration. The drill, which has the ability to take a core sample of the hardest granite or perform the most delicate diagnostic medical procedure, is a lightweight, ultrasonic device made to fit in the palm of the hand. Piezoelectric actuators, which have only two moving parts and no gears or motors, drive the components of the device, enabling it to operate in a wide range of temperatures. The most remarkable aspect of the drill is its ability to penetrate even the hardest rock with minimal force application. The ultrasonic device requires 20 to 30 times less force than standard rotating drills, allowing it to be safely guided by hand during operation. Also, the drill is operable at a level as low as three watts of power, where conventional drills require more than three times this level. Potential future applications for the ultrasonic drill include rock and soil sampling, medical procedures that involve core sampling or probing, landmine detection, building and construction, and space exploration. Cybersonics, Inc. developed an ultrasonic drill with applications ranging from the medical industry to space exploration.

High Temperature Piezoelectric Drill

Science.gov (United States)

Bao, Xiaoqi; Bar-Cohen, Yoseph; Sherrit, Stewart; Badescu, Mircea; Shrout, Tom

2012-01-01

Venus is one of the planets in the solar systems that are considered for potential future exploration missions. It has extreme environment where the average temperature is 460 deg C and its ambient pressure is about 90 atm. Since the existing actuation technology cannot maintain functionality under the harsh conditions of Venus, it is a challenge to perform sampling and other tasks that require the use of moving parts. Specifically, the currently available electromagnetic actuators are limited in their ability to produce sufficiently high stroke, torque, or force. In contrast, advances in developing electro-mechanical materials (such as piezoelectric and electrostrictive) have enabled potential actuation capabilities that can be used to support such missions. Taking advantage of these materials, we developed a piezoelectric actuated drill that operates at the temperature range up to 500 deg C and the mechanism is based on the Ultrasonic/Sonic Drill/Corer (USDC) configuration. The detailed results of our study are presented in this paper

Profitable ultrasonic assisted microwave disintegration of sludge biomass: Modelling of biomethanation and energy parameter analysis.

Science.gov (United States)

Kavitha, S; Rajesh Banu, J; Kumar, Gopalakrishnan; Kaliappan, S; Yeom, Ick Tae

2018-04-01

In this study, microwave irradiation has been employed to disintegrate the sludge biomass profitably by deagglomerating the sludge using a mechanical device, ultrasonicator. The outcomes of the study revealed that a specific energy input of 3.5 kJ/kg TS was found to be optimum for deagglomeration with limited cell lysis. A higher suspended solids (SS) reduction and biomass lysis efficiency of about 22.5% and 33.2% was achieved through ultrasonic assisted microwave disintegration (UMWD) when compared to microwave disintegration - MWD (15% and 20.9%). The results of biochemical methane potential (BMP) test were used to estimate biodegradability of samples. Among the samples subjected to BMP, UMWD showed better amenability towards anaerobic digestion with higher methane production potential of 0.3 L/g COD representing enhanced liquefaction potential of disaggregated sludge biomass. Economic analysis of the proposed method of sludge biomass pretreatment showed a net profit of 2.67 USD/Ton respectively. Copyright © 2018 Elsevier Ltd. All rights reserved.

Comparative study on conventional, ultrasonication and microwave assisted extraction of γ-oryzanol from rice bran.

Science.gov (United States)

Kumar, Pramod; Yadav, Devbrat; Kumar, Pradyuman; Panesar, Paramjeet Singh; Bunkar, Durga Shankar; Mishra, Diwaker; Chopra, H K

2016-04-01

In present study, conventional, ultrasonic and microwave assisted extraction methods were compared with the aim of optimizing best fitting solvent and method, solvent concentration and digestion time for high yield of γ-oryzanol from rice bran. Petroleum ether, hexane and methanol were used to prepare extracts. Extraction yield were evaluated for giving high crude oil yield, total phenolic content (TPC) and γ-oryzanol content. Gas chromatography-mass spectrophotometry was used for the determination of γ-oryzanol concentration. The highest concentration of γ-oryzanol was detected in methanolic extracts of microwave treatment (85.0 ppm) followed by ultrasonication (82.0 ppm) and conventional extraction method (73.5 ppm). Concentration of γ-oryzanol present in the extracts was found to be directly proportional to the total phenolic content. A combination of 80 % methanolic concentration and 55 minutes digestion time of microwave treatment yielded the best extraction method for TPC and thus γ-oryzanol (105 ppm).

Enzymolysis-ultrasonic assisted extraction, chemical characteristics and bioactivities of polysaccharides from corn silk.

Science.gov (United States)

Chen, Shuhan; Chen, Haixia; Tian, Jingge; Wang, Jia; Wang, Yanwei; Xing, Lisha

2014-01-30

An enzymolysis-ultrasonic assisted extraction (EUAE) procedure of corn silk polysaccharides (CSPS) was established and the physicochemical properties, antioxidant and anticancer activities of CSPS were studied. Orthogonal test and response surface methodology were applied to optimize the extraction parameters. The optimum enzymolysis and ultrasonic conditions were cellulase content of 7.5% for 150 min at 55 °C and liquid-solid ratio of 31.8 for 34.2 min at 66.3 °C, respectively. Under these conditions, the yield of CSPS increased from 4.56% to 7.10%. CSPS obtained by hot water and EUAE were composed of rhamnose, arabinose, xylose, mannose, galactose and glucose with molecular ratios of 4.17:17.33:5.59:18.65:19.11:35.14 and 8.83:15.77:7.92:12.39:11.15:43.94, respectively. Their molecular weight distributions were 10.52 × 10(4) and 6.88 × 10(4)Da, respectively. CSPS obtained by EUAE showed morphological and conformation changes and higher antioxidant and anticancer activities compared with CSPS extracted by hot water. Copyright © 2013 Elsevier Ltd. All rights reserved.

Nanosized zero-valent iron as Fenton-like reagent for ultrasonic-assisted leaching of zinc from blast furnace sludge

Energy Technology Data Exchange (ETDEWEB)

Mikhailov, Ivan, E-mail: ivan.mikhailov@misis.ru [National University of Science and Technology “MISiS”, 4 Leninskiy prospekt, Moscow, 119049 (Russian Federation); Komarov, Sergey [Tohoku University, 6-6-02 Aramaki Aza Aoba, Aoba-ku, Sendai, 980-8576 (Japan); Levina, Vera; Gusev, Alexander; Issi, Jean-Paul; Kuznetsov, Denis [National University of Science and Technology “MISiS”, 4 Leninskiy prospekt, Moscow, 119049 (Russian Federation)

2017-01-05

Highlights: • nZVI is used as Fenton-like reagent for activation of Zn leaching from the BFS. • nZVI has positive effect on kinetics of Zn leaching though with some loss of efficiency. • A complex ultrasonic-assisted method for BFS recycling is proposed. - Abstract: Ultrasonic-assisted sulphuric acid leaching combined with a Fenton-like process, utilizing nanoscale zero-valent iron (nZVI), was investigated to enhance the leaching of zinc from the blast furnace sludge (BFS). The leaching of iron (Fe) and zinc (Zn) from the sludge was investigated using Milli-Q water/BFS ratio of 10 and varying the concentration of hydrogen peroxide, sulphuric acid, the temperature, the input energy for ultrasound irradiation, and the presence or absence of nZVI as a Fenton reagent. The results showed that with 1 g/l addition of nZVI and 0.05 M of hydrogen peroxide, the kinetic rate of Zn leaching increased with a maximum dissolution degree of 80.2%, after 5 min treatment. In the absence of nZVI, the maximum dissolution degree of Zn was 99.2%, after 15 min treatment with 0.1 M of hydrogen peroxide. The rate of Zn leaching at several concentrations of hydrogen peroxide is accelerated in the presence of nZVI although a reduction in efficiency was observed. The loss of Fe was no more than 3%. On the basis of these results, the possible route for BFS recycling has been proposed (BFS slurry mixed with sulphuric acid and hydrogen peroxide is recirculated under ultrasonic irradiation then separated).

SIIA: a knowledge-based assistant for the SAFT ultrasonic inspection system(a)

International Nuclear Information System (INIS)

Melton, R.B.; Doctor, S.R.; Taylor, T.T.; Badalamente, R.V.

1987-01-01

SIIA(b) is a knowledge-based system designed to assist in making the operation of the Synthetic Aperture Focussing Technique (SAFT) Ultrasonic Inspection System more reliable and efficient. This paper reports on their effort to develop a prototype version of SIIA to demonstrate the feasibility of using knowledge-based systems in nondestructive evaluation (NDE). The first section of the paper describes the structure of the problem and their conceptual design of the knowledge-based system. The next section describes the current state of the prototype SIIA system and relates some of their experiences in developing the system. The final section discusses their plans for future development of SIIA and the implications of this type of system for other NDE techniques and applications

Experimental Investigation on the Performance of Grinding Assisted Electrochemical Discharge Drilling of Glass

Directory of Open Access Journals (Sweden)

Ladeesh V G

2016-01-01

Full Text Available Grinding assisted electrochemical discharge drilling (G-ECDD is a novel technique for producing micro and macro holes in brittle materials including advanced ceramics and glass, both efficiently and economically. G-ECDD involves the use of a rotating diamond core drill as the tool in a normal electrochemical discharge machine setup. The material removal happens by a combination of thermal melting due to electric discharges, followed by grinding action of diamond grits and chemical etching action. In this study, the effect of process parameters like voltage, duty cycle, cycle time and electrolyte concentration on material removed (MR was investigated systematically using response surface methodology. Analysis of variance was performed to identify the significant factors and their percentage contribution. The most significant factor was found to be duty cycle followed by voltage, cycle time and concentration. A quadratic mathematical model was developed to predict MR. Tool wear was found for different frequencies and voltages. Higher tool wear was observed for high frequency above 5kHz pulsed DC supply at high voltage of 110V. Tool wear at the end face of the tool was found to be a significant problem affecting the tool life.

Acoustic softening in metals during ultrasonic assisted deformation via CP-FEM

KAUST Repository

Siddiq, Amir

2011-01-01

In this paper, a phenomenological crystal plasticity model is modified to account for acoustic (ultrasonic) softening effects based on the level of ultrasonic intensity supplied to single and polycrystalline metals. The material parameters are identified using the inverse modeling approach by interfacing the crystal plasticity model with an optimization tool. The proposed model is validated and verified by comparing the microstructure evolution with experimental EBSD results reported in the literature. The model is able to capture the ultrasonic softening effect and the results show that as the ultrasonic intensity increases, the plastic deformation also increases. Differences in the stress-strain response are explained based on the slip system orientation tensor (Schmidt factors) which depends upon the crystal orientation. © 2010 Elsevier B.V. All rights reserved.

Multi-criteria optimization for ultrasonic-assisted extraction of antioxidants from Pericarpium Citri Reticulatae using response surface methodology, an activity-based approach.

Science.gov (United States)

Zeng, Shanshan; Wang, Lu; Zhang, Lei; Qu, Haibin; Gong, Xingchu

2013-06-01

An activity-based approach to optimize the ultrasonic-assisted extraction of antioxidants from Pericarpium Citri Reticulatae (Chenpi in Chinese) was developed. Response surface optimization based on a quantitative composition-activity relationship model showed the relationships among product chemical composition, antioxidant activity of extract, and parameters of extraction process. Three parameters of ultrasonic-assisted extraction, including the ethanol/water ratio, Chenpi amount, and alkaline amount, were investigated to give optimum extraction conditions for antioxidants of Chenpi: ethanol/water 70:30 v/v, Chenpi amount of 10 g, and alkaline amount of 28 mg. The experimental antioxidant yield under the optimum conditions was found to be 196.5 mg/g Chenpi, and the antioxidant activity was 2023.8 μmol Trolox equivalents/g of the Chenpi powder. The results agreed well with the second-order polynomial regression model. This presented approach promised great application potentials in both food and pharmaceutical industries. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Acoustic softening in metals during ultrasonic assisted deformation via CP-FEM

KAUST Repository

Siddiq, Amir; El Sayed, Tamer S.

2011-01-01

In this paper, a phenomenological crystal plasticity model is modified to account for acoustic (ultrasonic) softening effects based on the level of ultrasonic intensity supplied to single and polycrystalline metals. The material parameters

Study of Defect Sizing in Carbon Steel Butt Welds using Conventional Ultrasonic Technique and Phased Array Ultrasonic

International Nuclear Information System (INIS)

Amry Amin Abas; Noorhazleena Azaman; Mohd Yusnisyam Mohd Yusoff

2016-01-01

Ultrasonic testing is a proven reliable method which is able to detect and measure the size of defects in butt welds with acceptable tolerance. Recent advancement of technology has introduced a computerized technique which is phased array. Phased array employs focal law that enable focusing and steering of beam at the active aperture axis. This enables one line scanning but covering the whole weld volume as compared to conventional technique which employs aster scan and multiple probes to completely cover the whole weld volume. Phased array also gives multiple data view which assist the interpreter. This paper is about the study of these two techniques and technical analysis of comparison between the two. The conventional technique is performed using GE USM GO with 4 MHz 45 degrees shear wave probe. The phased array technique uses OLYMPUS OMNISCAN MX2 with 5L64 linear array probe with 16 elements aperture and 55 degrees wedge emitting shear wave into the specimen. Sensitivity of both techniques are based on 1.5 mm Side Drilled Hole. The results are compared and analysis such as defect sizing and defect type determination are performed. (author)

Humvee Armor Plate Drilling

National Research Council Canada - National Science Library

2004-01-01

When drilling holes in hard steel plate used in up-armor kits for Humvee light trucks, the Anniston Army Depot, Anniston, Alabama, requested the assistance of the National Center for Defense Manufacturing and Machining (NCDMM...

Optimization of ultrasonic assisted extraction of antioxidants from black soybean (Glycine max var) sprouts using response surface methodology.

Science.gov (United States)

Lai, Jixiang; Xin, Can; Zhao, Ya; Feng, Bing; He, Congfen; Dong, Yinmao; Fang, Yun; Wei, Shaomin

2013-01-16

Response surface methodology (RSM) using a central composite design (CCD) was employed to optimize the conditions for extraction of antioxidants from black soybean (Glycine max var) sprouts. Three influencing factors: liquid-solid ratio, period of ultrasonic assisted extraction and extraction temperature were investigated in the ultrasonic aqueous extraction. Then Response Surface Methodology (RSM) was applied to optimize the extraction process focused on DPPH radical-scavenging capacity of the antioxidants with respect to the above influencing factors. The best combination of each significant factor was determined by RSM design and optimum pretreatment conditions for maximum radical-scavenging capacity were established to be liquid-solid ratio of 29.19:1, extraction time of 32.13 min, and extraction temperature of 30 °C. Under these conditions, 67.60% of DPPH radical-scavenging capacity was observed experimentally, similar to the theoretical prediction of 66.36%.

Aluminium sensitized spectrofluorimetric determination of fluoroquinolones in milk samples coupled with salting-out assisted liquid-liquid ultrasonic extraction

Science.gov (United States)

Xia, Qinghai; Yang, Yaling; Liu, Mousheng

2012-10-01

An aluminium sensitized spectrofluorimetric method coupled with salting-out assisted liquid-liquid ultrasonic extraction for the determination of four widely used fluoroquinolones (FQs) namely norfloxacin (NOR), ofloxacin (OFL), ciprofloxacin (CIP) and gatifloxacin (GAT) in bovine raw milk was described. The analytical procedure involves the fluorescence sensitization of aluminium (Al3+) by complexation with FQs, salting-out assisted liquid-liquid ultrasonic extraction (SALLUE), followed by spectrofluorometry. The influence of several parameters on the extraction (the salt species, the amount of salt, pH, temperature and phase volume ratio) was investigated. Under optimized experimental conditions, the detection limits of the method in milk varied from 0.009 μg/mL for NOR to 0.016 μg/mL for GAT (signal-to-noise ratio (S/N) = 3). The relative standard deviations (RSD) values were found to be relatively low (0.54-2.48% for four compounds). The calibration graph was linear from 0.015 to 2.25 μg/mL with coefficient of determinations not less than 0.9974. The methodology developed was applied to the determination of FQs in bovine raw milk samples. The main advantage of this method is simple, accurate and green. The method showed promising applications for analyzing polar analytes especially polar drugs in various sample matrices.

Drilling a better pair : new technologies in SAGD directional drilling

Energy Technology Data Exchange (ETDEWEB)

Zimmer, C.; Richter, D. [Statoil Canada Ltd., Calgary, AB (Canada); Person, J.; Tilley, J.; Bittar, M. [Halliburton Energy Services, Calgary, AB (Canada)

2010-07-01

The Leismer Demonstration Project (LDP) is the first of 8 proposed major steam assisted gravity drainage (SAGD) projects for Statoil's Kai Kos Dehseh (KKD) asset in the Athabasca oil sands deposit. The bitumen resources are expected to produce approximately 2.2 billion barrels of oil over approximately 35 years with a peak production of 220,000 bbl/day. To date, 23 well pairs have been drilled on 4 drilling pads. The precise placement of well pairs is among the most important factors in a successful SAGD drilling program. The producer well must be placed in relation to the reservoir boundaries. It must also be accurately twinned with the injector well. A strong focus on technological innovation is needed in order to deliver on these high expectations in unconsolidated formations, such as the McMurray oil sands. Lateral SAGD pairs are often drilled with conventional steerable mud motors and logging-while-drilling (LWD) resistivity measurements, but this combination imposes certain limitations in terms of wellbore quality and placement. Several industry firsts were successfully implemented at the Statoil LDP, including a combination of the newest and most cutting-edge directional, measurement, and LWD technology. The keystone of these industry firsts was the use of a soft formation modified, point-the-bit rotary steerable system (RSS), used on 20 horizontal wells. The RRS was combined with an ultra deep azimuthal resistivity sensor to provide precise geosteering along the bottom bed boundary in the producer wells, resulting in improved reservoir capture and reservoir characterization. This paper described the new drilling system and its impact on the progressive future of directional drilling in SAGD. 8 refs., 1 tab., 22 figs.

Preparation of fluorescent nanodiamond suspensions using bead-assisted ultrasonic disintegration

Science.gov (United States)

Głowacki, Maciej J.; Gardas, Mateusz; Ficek, Mateusz; Sawczak, Mirosław; Bogdanowicz, Robert

2017-08-01

Nitrogen-vacancy (N-V) centers are the most widely studied crystallographic defect in the diamond lattice since their presence causes strong and stable fluorescence. The negative charge state of the defect (NV-) is especially desired because of its potential for quantum information processing. In this study, fluorescent suspensions of diamond particles have been produced by microbead-assisted ultrasonic disintegration of commercially obtained diamond powder containing N-V color centers. Zirconium dioxide ZrO2 was chosen as an abrasive and a mixture of deionized water and dimethyl sulfoxide (DMSO) was used as a solvent. Raman spectrum of the starting material has been obtained and the resulting liquids have been measured in terms of photoluminescence. Moreover, thin layer of the diamond particles has been deposited on a silicon substrate and examined using scanning electron microscopy (SEM). During the course of the experiment a new method, which uses sodium chloride NaCl as an abrasive, has been proposed. The results of fluorescence measurements of the suspension prepared using this technique are highly promising.

Laboratory ultrasonic pulse velocity logging for determination of elastic properties from rock core

Science.gov (United States)

Blacklock, Natalie Erin

During the development of deep underground excavations spalling and rockbursting have been recognized as significant mechanisms of violent brittle failure. In order to predict whether violent brittle failure will occur, it is important to identify the location of stiffness transitions that are associated with geologic structure. One approach to identify the effect of geologic structures is to apply borehole geophysical tools ahead of the tunnel advance. Stiffness transitions can be identified using mechanical property analysis surveys that combine acoustic velocity and density data to calculate acoustic estimates of elastic moduli. However, logistical concerns arise since the approach must be conducted at the advancing tunnel face. As a result, borehole mechanical property analyses are rarely used. Within this context, laboratory ultrasonic pulse velocity testing has been proposed as a potential alternative to borehole mechanical property analysis since moving the analysis to the laboratory would remove logistical constraints and improve safety for the evaluators. In addition to the traditional method of conducting velocity testing along the core axis, two new methodologies for point-focused testing were developed across the core diameter, and indirectly along intact lengths of drill core. The indirect test procedure was implemented in a continuous ultrasonic velocity test program along 573m of drill core to identify key geologic structures that generated transitions in ultrasonic elastic moduli. The test program was successful at identifying the location of geologic contacts, igneous intrusions, faults and shear structures. Ultrasonic values of Young's modulus and bulk modulus were determined at locations of significant velocity transitions to examine the potential for energy storage and energy release. Comparison of results from different ultrasonic velocity test configurations determined that the indirect test configuration provided underestimates for values of

Experiments on Ultrasonic Lubrication Using a Piezoelectrically-assisted Tribometer and Optical Profilometer.

Science.gov (United States)

Dong, Sheng; Dapino, Marcelo

2015-09-28

Friction and wear are detrimental to engineered systems. Ultrasonic lubrication is achieved when the interface between two sliding surfaces is vibrated at a frequency above the acoustic range (20 kHz). As a solid-state technology, ultrasonic lubrication can be used where conventional lubricants are unfeasible or undesirable. Further, ultrasonic lubrication allows for electrical modulation of the effective friction coefficient between two sliding surfaces. This property enables adaptive systems that modify their frictional state and associated dynamic response as the operating conditions change. Surface wear can also be reduced through ultrasonic lubrication. We developed a protocol to investigate the dependence of friction force reduction and wear reduction on the linear sliding velocity between ultrasonically lubricated surfaces. A pin-on-disc tribometer was built which differs from commercial units in that a piezoelectric stack is used to vibrate the pin at 22 kHz normal to the rotating disc surface. Friction and wear metrics including effective friction force, volume loss, and surface roughness are measured without and with ultrasonic vibrations at a constant pressure of 1 to 4 MPa and three different sliding velocities: 20.3, 40.6, and 87 mm/sec. An optical profilometer is utilized to characterize the wear surfaces. The effective friction force is reduced by 62% at 20.3 mm/sec. Consistently with existing theories for ultrasonic lubrication, the percent reduction in friction force diminishes with increasing speed, down to 29% friction force reduction at 87 mm/sec. Wear reduction remains essentially constant (49%) at the three speeds considered.

Study on residual stresses in ultrasonic torsional vibration assisted micro-milling

Science.gov (United States)

Lu, Zesheng; Hu, Haijun; Sun, Yazhou; Sun, Qing

2010-10-01

It is well known that machining induced residual stresses can seriously affect the dimensional accuracy, corrosion and wear resistance, etc., and further influence the longevity and reliability of Micro-Optical Components (MOC). In Ultrasonic Torsional Vibration Assisted Micro-milling (UTVAM), cutting parameters, vibration parameters, mill cutter parameters, the status of wear length of tool flank are the main factors which affect residual stresses. A 2D model of UTVAM was established with FE analysis software ABAQUS. Johnson-Cook's flow stress model and shear failure principle are used as the workpiece material model and failure principle, while friction between tool and workpiece uses modified Coulomb's law whose sliding friction area is combined with sticking friction. By means of FEA, the influence rules of cutting parameters, vibration parameters, mill cutter parameters, the status of wear length of tool flank on residual stresses are obtained, which provides a basis for choosing optimal process parameters and improving the longevity and reliability of MOC.

Optimization of ultrasonic-assisted extraction of natural antioxidants from rice bran using response surface methodology.

Science.gov (United States)

Tabaraki, Reza; Nateghi, Ashraf

2011-11-01

Ultrasonic technology was applied for extraction of polyphenols and antioxidants from the rice bran using ethanol as a food grade solvent. Response surface methodology (RSM) was used to optimize experimental conditions for extraction of polyphenols and antioxidants. Three independent variables such as solvent percentage (%), temperature (°C) and time (min) were studied. Effect of ethanol concentration was found to be significant on all responses. Total phenolic content (TPC) varied from 2.37 to 6.35mg gallic acid equivalent/g of dry sample. Antioxidant activity of the extracts was determined by the ferric reducing antioxidant power (FRAP) assay and scavenging activity of 1,1-diphenyl-2-picrylhydrazyl (DPPH) radical. FRAP and DPPH values varied from 31.74 to 57.23μmol Fe(2+)/g of dry sample and 16.88% to 55.61% inhibition, respectively. Extraction yields ranged from 11 to 20.2%. Optimal ultrasonic-assisted extraction (UAE) conditions were identified as 65-67% ethanol, 51-54°C, 40-45min. The experimental values agreed with those predicted by SRM models, thus indicating suitability of the model employed and the success of RSM in optimizing the extraction conditions. Copyright © 2011 Elsevier B.V. All rights reserved.

Neurosurgical robotic arm drilling navigation system.

Science.gov (United States)

Lin, Chung-Chih; Lin, Hsin-Cheng; Lee, Wen-Yo; Lee, Shih-Tseng; Wu, Chieh-Tsai

2017-09-01

The aim of this work was to develop a neurosurgical robotic arm drilling navigation system that provides assistance throughout the complete bone drilling process. The system comprised neurosurgical robotic arm navigation combining robotic and surgical navigation, 3D medical imaging based surgical planning that could identify lesion location and plan the surgical path on 3D images, and automatic bone drilling control that would stop drilling when the bone was to be drilled-through. Three kinds of experiment were designed. The average positioning error deduced from 3D images of the robotic arm was 0.502 ± 0.069 mm. The correlation between automatically and manually planned paths was 0.975. The average distance error between automatically planned paths and risky zones was 0.279 ± 0.401 mm. The drilling auto-stopping algorithm had 0.00% unstopped cases (26.32% in control group 1) and 70.53% non-drilled-through cases (8.42% and 4.21% in control groups 1 and 2). The system may be useful for neurosurgical robotic arm drilling navigation. Copyright © 2016 John Wiley & Sons, Ltd.

Report on achievements in fiscal 1998. Venture business growing type consortium - small business creating infrastructure (Research and development of ultrasonic vibration machining and electrochemical reaction compound high-efficiency and ultra precision damage-free machining); 1998 nendo chochoonpa shindo denki kagaku hanno fukugogata konoritsu choseimitsu damage free kakoho no kenkyu kaihatsu seika hokokusho. 2

Energy Technology Data Exchange (ETDEWEB)

NONE

2000-03-01

The present research and development is intended to establish the ultrasonic vibration machining process (ultrasonic vibration means vibration with frequency band exceeding 60 kHz), and ultrasonic vibration machining and electrochemical reaction compound machining process. The following research assignments were executed: (1) development of an ultrasonic vibration machining device and tools, (2) fundamental study on ultrasonic vibration grinding, (3) development of an ultrasonic vibration machining and electrochemical reaction compound damage-free grinding device and tools, and (4) development of ultrasonic vibration machining and electrochemical reaction compound damage-free grinding technology. The achievements in the current fiscal year may be summarized as follows: (1) an ultrasonic vibration rotating main-shaft unit and an electrically insulated tool holder were developed; (2) developments were made on a grinding process by using a micro-diameter grinding wheel supported by ultrasonic vibration, a micro field pick-up unit process using the same wheel, fabrication of micro tools by means of the ultrasonic vibration grinding, processing by using a drill with very small diameter based on the ultrasonic vibration grinding, and a technology to drill holes by means of ultrasonic vibration using a machine-made drill; (3) an ultrasonic vibration rotating main shaft unit with variable amplitude at 75 kHz was developed; and (4) an interface reaction compound grinding process supported by ultrasonic vibration was developed. (NEDO)

An evaluation of flowmeters for the detection of kicks and lost circulation during drilling

Energy Technology Data Exchange (ETDEWEB)

Schafer, D.M.; Loeppke, G.E.; Glowka, D.A.; Scott, D.D. (Sandia National Labs., Albuquerque, NM (United States)); Wright, K.E. (Ktech Corp., Albuquerque, NM (United States))

1991-01-01

An independent evaluation of current industry standard and state-of-the-art drilling fluid inflow and outflow meters was conducted during the drilling of a geothermal exploratory well. Four different types of fluid inflow meters and three different types of fluid outflow meters were tested and evaluated during actual drilling operations. The tested drilling fluid inflow meters included conventional pump stroke counters, rotary pump speed counters, magnetic flow meters, and a Doppler ultrasonic flow meter. On the return flow line, a standard paddle meter, an acoustic level meter, and a prototype rolling float meter were evaluated to measure drilling fluid outflow rates. The prototype outflow meter utilizes a rolling float which rides on the surface of the flow thereby measuring the fluid height in the pipe. Both the prototype meter and the conventional paddle meter were also extensively tested under a variety of drilling conditions in a full-scale laboratory test facility. The meters were evaluated and compared on the basis of reliability and accuracy, and the results are presented in the paper.

Ultrasonic Vibration Assisted Grinding of Bio-ceramic Materials: Modeling, Simulation, and Experimental Investigations on Edge Chipping

Science.gov (United States)

Tesfay, Hayelom D.

Bio-ceramics are those engineered materials that find their applications in the field of biomedical engineering or medicine. They have been widely used in dental restorations, repairing bones, joint replacements, pacemakers, kidney dialysis machines, and respirators. etc. due to their physico-chemical properties, such as excellent corrosion resistance, good biocompatibility, high strength and high wear resistance. Because of their inherent brittleness and hardness nature they are difficult to machine to exact sizes and dimensions. Abrasive machining processes such as grinding is one of the most widely used manufacturing processes for bioceramics. However, the principal technical challenge resulted from these machining is edge chipping. Edge chipping is a common edge failure commonly observed during the machining of bio-ceramic materials. The presence of edge chipping on bio-ceramic products affects dimensional accuracy, increases manufacturing cost, hider their industrial applications and causes potential failure during service. To overcome these technological challenges, a new ultrasonic vibration-assisted grinding (UVAG) manufacturing method has been developed and employed in this research. The ultimate aim of this study is to develop a new cost-effective manufacturing process relevant to eliminate edge chippings in grinding of bio-ceramic materials. In this dissertation, comprehensive investigations will be carried out using experimental, theoretical, and numerical approaches to evaluate the effect of ultrasonic vibrations on edge chipping of bioceramics. Moreover, effects of nine input variables (static load, vibration frequency, grinding depth, spindle speed, grinding distance, tool speed, grain size, grain number, and vibration amplitude) on edge chipping will be studied based on the developed models. Following a description of previous research and existing approaches, a series of experimental tests on three bio-ceramic materials (Lava, partially fired Lava

Synthesis of cobalt-containing mesoporous catalysts using the ultrasonic-assisted “pH-adjusting” method: Importance of cobalt species in styrene oxidation

Energy Technology Data Exchange (ETDEWEB)

Li, Baitao, E-mail: btli@scut.edu.cn; Zhu, Yanrun; Jin, Xiaojing

2015-01-15

Cobalt-containing SBA-15 and MCM-41 (Co-SBA-15 and Co-MCM-41) mesoporous catalysts were prepared via ultrasonic-assisted “pH-adjusting” technique in this study. Their physiochemical structures were comprehensively characterized and correlated with catalytic activity in oxidation of styrene. The nature of cobalt species depended on the type of mesoporous silica as well as pH values. The different catalytic performance between Co-SBA-15 and Co-MCM-41 catalysts originated from cobalt species. Cobalt species were homogenously incorporated into the siliceous framework of Co-SBA-15 in single-site Co(II) state, while Co{sub 3}O{sub 4} particles were loaded on Co-MCM-41 catalysts. The styrene oxidation tests showed that the single-site Co(II) state was more beneficial to the catalytic oxidation of styrene. The higher styrene conversion and benzaldehyde selectivity over Co-SBA-15 catalysts were mainly attributed to single-site Co(II) state incorporated into the framework of SBA-15. The highest conversion of styrene (34.7%) with benzaldehyde selectivity of 88.2% was obtained over Co-SBA-15 catalyst prepared at pH of 7.5, at the mole ratio of 1:1 (styrene to H{sub 2}O{sub 2}) at 70 °C. - Graphical abstract: Cobalt-containing mesoporous silica catalysts were developed via ultrasonic-assisted “pH-adjusting” technique. Compared with Co{sub 3}O{sub 4} in Co-MCM-41, the single-site Co(II) state in Co-SBA-15 was more efficient for the styrene oxidation. - Highlights: • Fast and cost-effective ultrasonic technique for preparing mesoporous materials. • Incorporation of Co via ultrasonic irradiation and “pH-adjusting”. • Physicochemical comparison between Co-SBA-15 and Co-MCM-41. • Correlation of styrene oxidation activity and catalyst structural property.

Rapid determination of volatile constituents in safflower from Xinjiang and Henan by ultrasonic-assisted solvent extraction and GC–MS

OpenAIRE

Jia, Ling-Han; Liu, Yi; Li, Yu-Zhen

2011-01-01

The total volatile components were extracted from safflower by ultrasonic-assisted solvent extraction (USE) and their chemical constituents were analyzed by gas chromatographyâmass spectrometry (GCâMS) to provide scientific basis for the quality control of safflower. Five different solvents (diethyl ether, ethanol, ethyl acetate, dichloromethane and acetone) were used and compared in terms of number of volatile components extracted and the peak areas of these components in TIC. The results sh...

Ultrasonic Nebulizer Assisted LIBS: a Promising Metal Elements Detection Method for Aqueous Sample Analysis

International Nuclear Information System (INIS)

Zhong Shilei; Zheng Ronger; Lu Yuan; Cheng Kai; Xiu Junshan

2015-01-01

A newly developed approach for trace metal elements detection for aqueous samples analysis is presented in this paper. The idea of this approach is to improve ablation efficiency by transforming the liquid sample into a dense cloud of droplets using an ultrasonic nebulizer. The resulting droplets are then subjected to analysis by laser induced breakdown spectroscopy (LIBS). A purpose-built ultrasonic nebulizer assisted LIBS (UN-LIBS) system has been applied to the analysis of aqueous samples at trace levels of concentration. Experimental investigations of solution samples were carried out with various dissolved trace metal elements (Mn, Zn, Cu, Pb, Fe, Mg and Na) using this approach. The characteristics of UN-LIBS signal of the elements were investigated regarding the lifetime and S/B ratio and the calibration curves for trace metal elements analyses. The obtained LODs are comparable or much better than the LODS of the reported signal enhancement approaches when the laser pulse energy was as low as 30 mJ. The good linearity of calibration curves and the low LODs shows the potential ability of this method for metal elements analysis application. The density of the electrons was calculated by measuring the Stark width of the line of H α . The possible mechanism of the LIBS signal enhancement of this approach was briefly discussed. (paper)

Ultrasonic examination of JBK-75 strip material

International Nuclear Information System (INIS)

Cook, K.V.; Cunningham, R.A. Jr.; Lewis, J.C.; McClung, R.W.

1982-12-01

An ultrasonic inspection system was assembled to inspect the JBK-75 stainless steel sheath material (for the Large Coil Project) for the Westinghouse-Airco superconducting magnet program. The mechanical system provided for handling the 180-kg (400-lb) coils of strip material [1.6 mm thick by 78 mm wide by 90 to 120 m long (0.064 by 3.07 in. by 300 to 400 ft)], feeding the strip through the ultrasonic inspection and cleaning stations, and respooling the coils. We inspected 54 coils of strip for both longitudinal and laminar flaws. Simulated flaws were used to calibrate both inspections. Saw-cut notches [0.28 mm deep (0.011 in., about 17% of the strip thickness)] were used to calibrate the longitudinal flaw inspections; 1.59-mm-diam (0.063-in.) flat-bottom holes drilled halfway through a calibration strip were used to calibrate the laminar flaw tests

Ultrasonic testing of austenitic stainless steel welds

International Nuclear Information System (INIS)

Nishino, Shunichi; Hida, Yoshio; Yamamoto, Michio; Ando, Tomozumi; Shirai, Tasuku.

1982-05-01

Ultrasonic testing of austenitic stainless steel welds has been considered difficult because of the high noise level and remarkable attenuation of ultrasonic waves. To improve flaw detectability in this kind of steel, various inspection techniques have been studied. A series of tests indicated: (1) The longitudinal angle beam transducers newly developed during this study can detect 4.8 mm dia. side drilled holes in dissimilar metal welds (refraction angle: 55 0 from SUS side, 45 0 from CS side) and in cast stainless steel welds (refraction angle: 45 0 , inspection frequency: 1 MHz). (2) Cracks more than 5% t in depth in the heat affected zones of fine-grain stainless steel pipe welds can be detected by the 45 0 shear wave angle beam method (inspection frequency: 2 MHz). (3) The pattern recognition method using frequency analysis technology was presumed useful for discriminating crack signals from spurious echoes. (author)

Preparation and Characterization of Nanofibrillated Cellulose from Bamboo Fiber via Ultrasonication Assisted by Repulsive Effect

Directory of Open Access Journals (Sweden)

Zhijun Hu

2017-01-01

Full Text Available Nanofibrillated celluloses (NFCs have recently drawn much attention because of their exceptional physicochemical properties. However, the existing preparation procedures either produce low yields or severely degrade the cellulose and, moreover, are not energy efficient. The purpose of this study was to develop a novel process using ultrasonic homogenization to isolate fibrils from bamboo fiber (BF with the assistance of negatively charged entities. The obtained samples were characterized by the degree of substitution (DS of carboxymethyl, Fourier-transform infrared (FT-IR spectroscopy, X-ray diffraction (XRD, thermogravimetric analysis, and transmission electron microscopy (TEM. The results showed that an NFC yield could be obtained above 70% through this route. The enzyme hydrolysis could enhance the surface charge of the fiber, and mechanical activation facilitates an increase in the DS. The disintegrating efficiency of the cellulose fibrils significantly depended on the input power of ultrasonication and the DS. FT-IR spectra confirmed the occurrence of the carboxymethylation reaction based on the appearance of the characteristic signal for the carboxyl group. From XRD analysis, it was observed that the presence of the carboxyl groups makes the isolation more efficient attributed to the ionic repulsion between the carboxylate groups of the cellulose chains.

Mathematical modeling of a single stage ultrasonically assisted distillation process.

Science.gov (United States)

Mahdi, Taha; Ahmad, Arshad; Ripin, Adnan; Abdullah, Tuan Amran Tuan; Nasef, Mohamed M; Ali, Mohamad W

2015-05-01

The ability of sonication phenomena in facilitating separation of azeotropic mixtures presents a promising approach for the development of more intensified and efficient distillation systems than conventional ones. To expedite the much-needed development, a mathematical model of the system based on conservation principles, vapor-liquid equilibrium and sonochemistry was developed in this study. The model that was founded on a single stage vapor-liquid equilibrium system and enhanced with ultrasonic waves was coded using MATLAB simulator and validated with experimental data for ethanol-ethyl acetate mixture. The effects of both ultrasonic frequency and intensity on the relative volatility and azeotropic point were examined, and the optimal conditions were obtained using genetic algorithm. The experimental data validated the model with a reasonable accuracy. The results of this study revealed that the azeotropic point of the mixture can be totally eliminated with the right combination of sonication parameters and this can be utilized in facilitating design efforts towards establishing a workable ultrasonically intensified distillation system. Copyright © 2014 Elsevier B.V. All rights reserved.

Ultrasonic-assisted preparation of graphene oxide carboxylic acid polyvinyl alcohol polymer film and studies of thermal stability and surface resistivity.

Science.gov (United States)

Li, Yongshen; Li, Jihui; Li, Yuehai; Li, Yali; Song, Yunan; Niu, Shuai; Li, Ning

2018-01-01

In this paper, flake graphite, nitric acid and acetic anhydride are used to prepare graphene oxide carboxylic acid (GO-COOH) via an ultrasonic-assisted method, and GO-COOH and polyvinyl alcohol polymer (PVA) are used to synthesize graphene oxide carboxylic acid polyvinyl alcohol polymer (GO-COOPVA) via the ultrasonic-assisted method, and GO-COOPVA is used to manufacture graphene oxide carboxylic acid polyvinyl alcohol polymer film (GO-COOPVA film) via a solidification method, and the structure and morphology of GO-COOH, GO-COOPVA and GO-COOPVA film are characterized, and the thermal stability and surface resistivity are measured in the case of the different amount of GO-COOH. Based on the characterization and measurement, it has been successively confirmed and attested that carboxyl groups implant on 2D lattice of GO to form GO-COOH, and GO-COOH and PVA have the esterification reaction to produce GO-COOPVA, and GO-COOPVA consists of 2D lattice of GO-COOH and the chain of PVA connected in the form of carboxylic ester, and GO-COOPVA film is composed of GO-COOPVA, and the thermal stability of GO-COOPVA film obviously improves in comparison with PVA film, and the surface resistivity of GO-COOPVA film clearly decreases. Copyright © 2017 Elsevier B.V. All rights reserved.

Preliminary study on rotary ultrasonic machining of Bk-7 optical glass rod

International Nuclear Information System (INIS)

Hamzah, E.; Izman, S.; Khoo, C.Y.; Zainal Abidin, N.N.

2007-01-01

This paper presents an experimental observation on rotary ultrasonic machining (RUM) of BK7 optical glass rod. BK7 is a common technical optical glass for high quality optical components due to its high linear optical transmission in the visible range and is chemically stable. RUM is a hybrid machining process that combines the material removal mechanisms of diamond grinding and ultrasonic machining (USM) and it is non-thermal, non-chemical, creates no change in the microstructure, chemical or physical properties of the work piece. In the RUM, a controlled static load is applied to the rotating core drill with metal bonded diamond abrasive and is ultrasonically vibrated in the axial direction. A water-soluble coolant was used to cool the tool and sample during machining processes. By using DOE (Design of Experiment) approach, the effect of spindle speed and feed rate to the ultrasonic machinability had been developed. The main effects and two-factor interactions of process parameters (spindle speed) and feed rate) on output variables (MRR, surface roughness, opaqueness, chipping thickness and chipping size) are studied. (author)

Wellsite computers--their increasing role in drilling operations

International Nuclear Information System (INIS)

Keenan, P.G.; Dyson, P.M.

1981-01-01

The increasing expense and complexity of exploration drilling, coupled with rapid advances in computer and microprocessor technology, have led to the development of computer-assisted wellsite logging units from their humble beginnings as simple hot wire gas detectors. The main applications of this technology can be recognized in the following areas: (a) Safety of wellsite personnel, rig and downhole equipment. (b) Increased drilling efficiency with the resultant time and cost savings. (c) Simulation of possible events allowing comparisons between actual and expected data to assist decision making at the wellsite. (d) Storage of data on tape/disk to allow rapid retrieval of data for postwell analysis and report production. 6 refs

Ultrasonic-assisted extraction of phenolic and antioxidative compounds from lizard tail (Houttuynia cordata Thunb.

Directory of Open Access Journals (Sweden)

Trakul Prommajak

2014-02-01

Full Text Available Lizard tail (Houttuynia cordata Thunb. is an Asian herb which has many biological activities, including antioxidative property from polyphenolic compounds. Response surface methodology and Box-Behnken design were employed to study the effect of extraction temperature (30 to 70°C, extraction time (10 to 30 min, ethanol concentration (30 to 70%, and solvent to sample ratio (2 to 6 ml/g on ultrasonic-assisted extraction of phenolic compounds from lizard tail and antioxidant capacity of the herb extract. Extraction temperature was the most relevant factor on the responses. Optimal condition was the extraction temperature of 70°C for 30 min, using 60% ethanol concentration at the solvent to sample ratio of 5 ml/g. Model adequacies were confirmed by extraction at the optimal condition and normality of standardized residuals.

Ultrasonic assisted production of starch nanoparticles: Structural characterization and mechanism of disintegration.

Science.gov (United States)

Boufi, Sami; Bel Haaj, Sihem; Magnin, Albert; Pignon, Frédéric; Impéror-Clerc, Marianne; Mortha, Gérard

2018-03-01

In this paper, the disintegration of starch (waxy and standard starch) granules into nanosized particles under the sole effect of high power ultrasonication treatment in water/isopropanol is investigated, by using wide methods of analysis. The present work aims at a fully characterization of the starch nanoparticles produced by ultrasonication, in terms of size, morphology and structural properties, and the proposition of a possible mechanism explaining the top-down generation of starch nanoparticles (SNPs) via high intensity ultrasonication. Dynamic light scattering measurements have indicated a leveling of the particle size to about 40nm after 75min of ultrasonication. The WAXD, DSC and Raman have revealed the amorphous character of the SNPs. FE-SEM. AFM observations have confirmed the size measured by DLS and suggested that SNPs exhibited 2D morphology of platelet-like shapes. This morphology is further supported by SAXS. On the basis of data collected from the different characterization techniques, a possible mechanism explaining the disintegration process of starch granules into NPs is proposed. Copyright © 2017 Elsevier B.V. All rights reserved.

Ultrasonic assisted rapid synthesis of high uniform super-paramagnetic microspheres with core-shell structure and robust magneto-chromatic ability

Energy Technology Data Exchange (ETDEWEB)

Zhang, Wenyan, E-mail: wiseyanyan@jit.edu.cn [College of Material Engineering, Jinling Institute of technology, Nanjing (China); Chen, Jiahua [College of Material Engineering, Jinling Institute of technology, Nanjing (China); Wang, Wei [Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites, Nanjing Tech University, Nanjing (China); School of Physics and Optoelectronic Engineering, Nanjing University of Information Science & Technology, Nanjing (China); Lu, GongXuan [State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000 (China); Hao, Lingyun [College of Material Engineering, Jinling Institute of technology, Nanjing (China); Ni, Yaru; Lu, Chunhua; Xu, Zhongzi [Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites, Nanjing Tech University, Nanjing (China); State Key Laboratory of Materials-Oriented Chemical Engineering, College of Materials Science and Engineering, Nanjing Tech University, Nanjing (China)

2017-03-15

Super-paramagnetic core-shell microspheres were synthesized by ultrasonic assisted routine under low ultrasonic irradiation powers. Compared with conventional routine, ultrasonic effect could not only improve the uniformity of the core-shell structure of Fe{sub 3}O{sub 4}@SiO{sub 2}, but shorten the synthesis time in large scale. Owing to their hydrophilicity and high surface charge, the Fe{sub 3}O{sub 4}@SiO{sub 2} microspheres could be dispersed well in distilled water to form homogeneous colloidal suspension. The suspensions have favorable magneto-chromatic ability that they sensitively exhibit brilliant colorful ribbons by magnetic attraction. The colorful ribbons, which distributed along the magnetic lines, make morphology of the magnetic fields become “visible” to naked eyed. Those colorful ribbons originate from strong magnetic interaction between the microspheres and magnetic fields. Furthermore, the magneto-chromatic performance is reversible as the colorful ribbons vanished rapidly with the removing of magnetic fields. The silica layer effectively enhanced the acid resistance and surface-oxidation resistance of theFe{sub 3}O{sub 4}@SiO{sub 2} microspheres, so they could exhibit stable magnetic nature and robust magneto-chromatic property in acid environment. - Graphical abstract: The Graphical abstract shows the sensitive magneto-chromatic ability, the acid resistance ability as well as the magneto-chromatic mechanism of the Fe{sub 3}O{sub 4} and Fe{sub 3}O{sub 4}@SiO{sub 2} suspension. - Highlights: • Sensitive and reversible robust magneto-chromatic property under magnetic attraction. • Morphology of magnetic field “visible” to naked eyes. • Enhance acid resistance and surface-oxidation resistance. • Ultrasonic effect largely shorten the synthesis time of high uniform microspheres.

Ultrasonic assisted rapid synthesis of high uniform super-paramagnetic microspheres with core-shell structure and robust magneto-chromatic ability

International Nuclear Information System (INIS)

Zhang, Wenyan; Chen, Jiahua; Wang, Wei; Lu, GongXuan; Hao, Lingyun; Ni, Yaru; Lu, Chunhua; Xu, Zhongzi

2017-01-01

Super-paramagnetic core-shell microspheres were synthesized by ultrasonic assisted routine under low ultrasonic irradiation powers. Compared with conventional routine, ultrasonic effect could not only improve the uniformity of the core-shell structure of Fe_3O_4@SiO_2, but shorten the synthesis time in large scale. Owing to their hydrophilicity and high surface charge, the Fe_3O_4@SiO_2 microspheres could be dispersed well in distilled water to form homogeneous colloidal suspension. The suspensions have favorable magneto-chromatic ability that they sensitively exhibit brilliant colorful ribbons by magnetic attraction. The colorful ribbons, which distributed along the magnetic lines, make morphology of the magnetic fields become “visible” to naked eyed. Those colorful ribbons originate from strong magnetic interaction between the microspheres and magnetic fields. Furthermore, the magneto-chromatic performance is reversible as the colorful ribbons vanished rapidly with the removing of magnetic fields. The silica layer effectively enhanced the acid resistance and surface-oxidation resistance of theFe_3O_4@SiO_2 microspheres, so they could exhibit stable magnetic nature and robust magneto-chromatic property in acid environment. - Graphical abstract: The Graphical abstract shows the sensitive magneto-chromatic ability, the acid resistance ability as well as the magneto-chromatic mechanism of the Fe_3O_4 and Fe_3O_4@SiO_2 suspension. - Highlights: • Sensitive and reversible robust magneto-chromatic property under magnetic attraction. • Morphology of magnetic field “visible” to naked eyes. • Enhance acid resistance and surface-oxidation resistance. • Ultrasonic effect largely shorten the synthesis time of high uniform microspheres.

Ultrasonic assisted biodiesel production of microalgae by direct transesterification

Science.gov (United States)

Kalsum, Ummu; Mahfud, Mahfud; Roesyadi, Achmad

2017-03-01

Microalgae are considered as the third generation source of biofuel and an excellent candidate for biofuel production to replace the fossil energy. The use of ultrasonic in producing biodiesel by direct transesterification of Nannochloropsis occulata using KOH as catalyst and methanol as a solvent was investigated. The following condition were determined as an optimum by experimental evaluates:: 1: 15 microalga to methanol (molar ratio); 3% catalyst concentration at temperature 40°C after 30 minute of ultrasonication. The highest yield of biodiesel produced was 30.3%. The main components of methyl ester from Nannochloropsis occulata were palmitic (C16 :0),, oleic (C18:1), stearic (C18;0), arahidic (C20:0) and myristic (C14:0). This stated that the application of ultrasounic for direct transesterificaiton of microalgae effectively reduced the reaction time compared to the reported values of conventional heating systems.

Investigation of the visible light photocatalytic activity of BiVO4 prepared by sol gel method assisted by ultrasonication.

Science.gov (United States)

Deebasree, J P; Maheskumar, V; Vidhya, B

2018-07-01

Visible light induced photocatalyst BiVO 4 with monoclinic scheelite structure has been synthesised via sol gel method assisted by ultrasonication. The prepared samples were characterised using X-ray diffraction (XRD), scanning electron microscope (SEM), UV-Vis diffused reflectance spectroscopy (DRS) techniques. The photocatalytic efficiency was evaluated by decolourisation of MB under visible light irradiation. The effect of ultrasound output power on the properties of BiVO 4 during and after preparation by sol-gel method has been compared with normal agitated sample (As prepared). The power of ultrasonic vibration has been varied and an ideal output power which yields better catalytic efficiency is determined. BiVO 4 sonicated with 80 W during preparation 80 W (D) exhibited relatively high surface area, better surface morphology and better catalytic efficiency compared to other samples which were sonicated with 100, 160 and 200 W. The results signify that the photodegradation rate of BiVO 4 80 W (D) sample is high up to 96% in 90 min compared to other samples. Change in morphology leading to better catalytic efficiency was obtained just by exposing the sample to ultrasonic radiation without addition of any surfactant. The recovery test showed that the sample was stable for four consecutive cycles. Using radical test, a reasonable mechanism for photodegradation has been proposed. Copyright © 2018 Elsevier B.V. All rights reserved.

Surfactant-assisted ultrasonic spray pyrolysis of nickel oxide and lithium-doped nickel oxide thin films, toward electrochromic applications

Energy Technology Data Exchange (ETDEWEB)

Denayer, Jessica [Group of Research in Energy and Environment for MATerials (GREENMAT), University of Liège, allée de la chimie 3, 4000 Liège (Belgium); Bister, Geoffroy [Environmental and Material Research Association (CRIBC-INISMa), avenue gouverneur cornez 4, 7000 Mons (Belgium); Simonis, Priscilla [Laboratory LPS, University of Namur, rue de bruxelles 61, 5000 Namur (Belgium); Colson, Pierre; Maho, Anthony [Group of Research in Energy and Environment for MATerials (GREENMAT), University of Liège, allée de la chimie 3, 4000 Liège (Belgium); Aubry, Philippe [Environmental and Material Research Association (CRIBC-INISMa), avenue gouverneur cornez 4, 7000 Mons (Belgium); Vertruyen, Bénédicte [Group of Research in Energy and Environment for MATerials (GREENMAT), University of Liège, allée de la chimie 3, 4000 Liège (Belgium); Henrist, Catherine, E-mail: catherine.henrist@ulg.ac.be [Group of Research in Energy and Environment for MATerials (GREENMAT), University of Liège, allée de la chimie 3, 4000 Liège (Belgium); Lardot, Véronique; Cambier, Francis [Environmental and Material Research Association (CRIBC-INISMa), avenue gouverneur cornez 4, 7000 Mons (Belgium); Cloots, Rudi [Group of Research in Energy and Environment for MATerials (GREENMAT), University of Liège, allée de la chimie 3, 4000 Liège (Belgium)

2014-12-01

Highlights: • Surfactant-assisted USP: a novel and low cost process to obtain high quality nickel oxide films, with or without lithium dopant. • Increased uniformity and reduced light scattering thanks to the addition of a surfactant. • Improved electrochromic performance (coloration efficiency and contrast) for lithium-doped films by comparison with the undoped NiO film. - Abstract: Lithium-doped nickel oxide and undoped nickel oxide thin films have been deposited on FTO/glass substrates by a surfactant-assisted ultrasonic spray pyrolysis. The addition of polyethylene glycol in the sprayed solution has led to improved uniformity and reduced light scattering compared to films made without surfactant. Furthermore, the presence of lithium ions in NiO films has resulted in improved electrochromic performances (coloration contrast and efficiency), but with a slight decrease of the electrochromic switching kinetics.

Forage pétrolier assisté par jet Jet-Assisted Oil Drilling

Directory of Open Access Journals (Sweden)

Bardin C.

2006-11-01

Full Text Available La destruction des roches par jet est une technique qui présente un réel intérêt dans le domaine du forage pétrolier comme en témoignent les études déjà réalisées sur le sujet depuis une vingtaine d'années. Des essais sur chantier ont fait apparaître des améliorations substantielles en vitesse d'avancement grâce aux outils combinés mécaniques et jets haute pression. Cet article explique, après une courte bibliographie sur le sujet, les motivations d'une nouvelle étude menée par l'institut Français du Pétrole (IFP au sein de l'Association de Recherche sur les Techniques d'Exploitation du Pétrole (ARTEP. L'objectif de cette étude est d'utiliser le pouvoir destructeur de la cavitation dans le cas des forages profonds en utilisant les capacités de pompage actuellement disponibles sur chantier. Cet objectif nécessite le développement d'une technique capable de créer une cavitation érosive à sigma = 2. 5 ; sigma étant défini par le rapport de la pression à l'aval du dispositif cavitant sur la chute de pression dans ce même dispositif. L'érosion de cavitation étant très dépendante des conditions de pression et de température, il a été nécessaire de concevoir des moyens d'essai permettant de simuler les conditions de fond de forage dans le cas de forage par grande profondeur. Le banc d'essai (70 MPa, 120 °C est présenté dans ce papier, ainsi que quelques essais relatifs à la destruction des roches par jet. The destruction of rocks by jetting is an important technique in the field of cil drilling, as shown by research done on this subject for some 20 years now. Fields tests have revealed substantial improvements in rates of penetration with the use of combined mechanical and high-pressure jet bits. After a brief bibliography on the subject, this paper explains the motives for a new research project being car-ried out by Institut Français du Pétrole (IFP within the ARTEP association (Association de Recherche

Spectroscopic investigation on assisted sonocatalytic damage of bovine serum albumin (BSA) by metronidazole (MTZ) under ultrasonic irradiation combined with nano-sized ZnO

Science.gov (United States)

Gao, Jingqun; Liu, Bin; Wang, Jun; Jin, Xudong; Jiang, Renzheng; Liu, Lijun; Wang, Baoxin; Xu, Yongnan

2010-11-01

The previous work proved that the bovine serum albumin (BSA) could be damaged under the combined action of ultrasonic irradiation and ZnO. In this work, the assisted sonocatalytic damage of BSA using metronidazole (MTZ) as a sensitizer was further investigated by means of UV-vis and fluorescence spectra. The results indicated that the adding of MTZ could obviously promote the sonocatalytic damage of BSA under ultrasonic irradiation in the presence of nano-sized ZnO powder. Furthermore, it was found that the damage degree of BSA was aggravated by some influencing factors except ionic kind and strength. In addition, the damage site of BSA was also studied with synchronous fluorescence technology. It was found that the damage site was mainly at tryptophan (Trp) residue.

Binary solvent extraction system and extraction time effects on phenolic antioxidants from kenaf seeds (Hibiscus cannabinus L.) extracted by a pulsed ultrasonic-assisted extraction.

Science.gov (United States)

Wong, Yu Hua; Lau, Hwee Wen; Tan, Chin Ping; Long, Kamariah; Nyam, Kar Lin

2014-01-01

The aim of this study was to determine the best parameter for extracting phenolic-enriched kenaf (Hibiscus cannabinus L.) seeds by a pulsed ultrasonic-assisted extraction. The antioxidant activities of ultrasonic-assisted kenaf seed extracts (KSE) were determined by a 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging capacity assay, 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulphonic acid) (ABTS) radical scavenging assay, β -carotene bleaching inhibition assay, and ferric reducing antioxidant power (FRAP) assay. Total phenolic content (TPC) and total flavonoid content (TFC) evaluations were carried out to determine the phenolic and flavonoid contents in KSE. The KSE from the best extraction parameter was then subjected to high performance liquid chromatography (HPLC) to quantify the phenolic compounds. The optimised extraction condition employed 80% ethanol for 15 min, with the highest values determined for the DPPH, ABTS, and FRAP assay. KSE contained mainly tannic acid (2302.20 mg/100 g extract) and sinapic acid (1198.22 mg/100 g extract), which can be used as alternative antioxidants in the food industry.

Binary Solvent Extraction System and Extraction Time Effects on Phenolic Antioxidants from Kenaf Seeds (Hibiscus cannabinus L.) Extracted by a Pulsed Ultrasonic-Assisted Extraction

Science.gov (United States)

Lau, Hwee Wen; Nyam, Kar Lin

2014-01-01

The aim of this study was to determine the best parameter for extracting phenolic-enriched kenaf (Hibiscus cannabinus L.) seeds by a pulsed ultrasonic-assisted extraction. The antioxidant activities of ultrasonic-assisted kenaf seed extracts (KSE) were determined by a 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging capacity assay, 2,2′-azino-bis(3-ethylbenzothiazoline-6-sulphonic acid) (ABTS) radical scavenging assay, β-carotene bleaching inhibition assay, and ferric reducing antioxidant power (FRAP) assay. Total phenolic content (TPC) and total flavonoid content (TFC) evaluations were carried out to determine the phenolic and flavonoid contents in KSE. The KSE from the best extraction parameter was then subjected to high performance liquid chromatography (HPLC) to quantify the phenolic compounds. The optimised extraction condition employed 80% ethanol for 15 min, with the highest values determined for the DPPH, ABTS, and FRAP assay. KSE contained mainly tannic acid (2302.20 mg/100 g extract) and sinapic acid (1198.22 mg/100 g extract), which can be used as alternative antioxidants in the food industry. PMID:24592184

Binary Solvent Extraction System and Extraction Time Effects on Phenolic Antioxidants from Kenaf Seeds (Hibiscus cannabinus L. Extracted by a Pulsed Ultrasonic-Assisted Extraction

Directory of Open Access Journals (Sweden)

Yu Hua Wong

2014-01-01

Full Text Available The aim of this study was to determine the best parameter for extracting phenolic-enriched kenaf (Hibiscus cannabinus L. seeds by a pulsed ultrasonic-assisted extraction. The antioxidant activities of ultrasonic-assisted kenaf seed extracts (KSE were determined by a 2,2-diphenyl-1-picrylhydrazyl (DPPH radical scavenging capacity assay, 2,2′-azino-bis(3-ethylbenzothiazoline-6-sulphonic acid (ABTS radical scavenging assay, β-carotene bleaching inhibition assay, and ferric reducing antioxidant power (FRAP assay. Total phenolic content (TPC and total flavonoid content (TFC evaluations were carried out to determine the phenolic and flavonoid contents in KSE. The KSE from the best extraction parameter was then subjected to high performance liquid chromatography (HPLC to quantify the phenolic compounds. The optimised extraction condition employed 80% ethanol for 15 min, with the highest values determined for the DPPH, ABTS, and FRAP assay. KSE contained mainly tannic acid (2302.20 mg/100 g extract and sinapic acid (1198.22 mg/100 g extract, which can be used as alternative antioxidants in the food industry.

Coiled tubing drilling with supercritical carbon dioxide

Science.gov (United States)

Kolle , Jack J.

2002-01-01

A method for increasing the efficiency of drilling operations by using a drilling fluid material that exists as supercritical fluid or a dense gas at temperature and pressure conditions existing at a drill site. The material can be used to reduce mechanical drilling forces, to remove cuttings, or to jet erode a substrate. In one embodiment, carbon dioxide (CO.sub.2) is used as the material for drilling within wells in the earth, where the normal temperature and pressure conditions cause CO.sub.2 to exist as a supercritical fluid. Supercritical carbon dioxide (SC--CO.sub.2) is preferably used with coiled tube (CT) drilling equipment. The very low viscosity SC--CO.sub.2 provides efficient cooling of the drill head, and efficient cuttings removal. Further, the diffusivity of SC--CO.sub.2 within the pores of petroleum formations is significantly higher than that of water, making jet erosion using SC--CO.sub.2 much more effective than water jet erosion. SC--CO.sub.2 jets can be used to assist mechanical drilling, for erosion drilling, or for scale removal. A choke manifold at the well head or mud cap drilling equipment can be used to control the pressure within the borehole, to ensure that the temperature and pressure conditions necessary for CO.sub.2 to exist as either a supercritical fluid or a dense gas occur at the drill site. Spent CO.sub.2 can be vented to the atmosphere, collected for reuse, or directed into the formation to aid in the recovery of petroleum.

Analysis of the application of poly-nanocrystalline diamond tools for ultra precision machining of steel with ultrasonic assistance

Science.gov (United States)

Doetz, M.; Dambon, O.; Klocke, F.; Bulla, B.; Schottka, K.; Robertson, D. J.

2017-10-01

Ultra-precision diamond turning enables the manufacturing of parts with mirror-like surfaces and highest form accuracies out of non-ferrous, a few crystalline and plastic materials. Furthermore, an ultrasonic assistance has the ability to push these boundaries and enables the machining of materials like steel, which is not possible in a conventional way due to the excessive tool wear caused by the affinity of carbon to iron. Usually monocrystalline diamonds tools are applied due to their unsurpassed cutting edge properties. New cutting tool material developments have shown that it is possible to produce tools made of nano-polycrystalline diamonds with cutting edges equivalent to monocrystalline diamonds. In nano-polycrystalline diamonds ultra-fine grains of a few tens of nanometers are firmly and directly bonded together creating an unisotropic structure. The properties of this material are described to be isotropic, harder and tougher than those of the monocrystalline diamonds, which are unisotropic. This publication will present machining results from the newest investigations of the process potential of this new polycrystalline cutting material. In order to provide a baseline with which to characterize the cutting material cutting experiments on different conventional machinable materials like Cooper or Aluminum are performed. The results provide information on the roughness and the topography of the surface focusing on the comparison to the results while machining with monocrystalline diamond. Furthermore, the cutting material is tested in machining steel with ultrasonic assistance with a focus on tool life time and surface roughness. An outlook on the machinability of other materials will be given.

Ultrasonic hot powder compaction of Ti-6Al-4V.

Science.gov (United States)

Abedini, Rezvan; Abdullah, Amir; Alizadeh, Yunes

2017-07-01

Power ultrasonic has been recently employed in a wide variety of manufacturing processes among which ultrasonic assisted powder compaction is a promising powder materials processing technique with significant industrial applications. The products manufactured by the powder metallurgy commonly consist of residual porosities, material impurities, structural non-homogeneities and residual stress. In this paper, it is aimed to apply power ultrasonic to the hot consolidation process of Ti-6Al-4V titanium alloy powder in order to improve mechanical properties. To do this, the effects of ultrasonic power and process temperature and pressure were considered and then deeply studied through a series of experiments. It was shown that the addition of ultrasonic vibration leads to a significant improvement in the consolidation performance and the mechanical strength of the fabricated specimens. Copyright © 2017 Elsevier B.V. All rights reserved.

Optimization of ultrasonic-assisted extraction of total carotenoids from peach palm fruit (Bactris gasipaes) by-products with sunflower oil using response surface methodology.

Science.gov (United States)

Ordóñez-Santos, Luis Eduardo; Pinzón-Zarate, Lina Ximena; González-Salcedo, Luis Octavio

2015-11-01

The present study reports on the extraction of total carotenoids from peach palm fruit by-products with sunflower oil. Response surface methodology (RSM) was used to investigate the effect of process variables on the ultrasound-assisted extraction (UAE). Three independent variables including ultrasonic intensity (764-1528, W/m(2)), temperature (25-45°C), and the extraction time (10-30 min). According to the results, the optimal UAE condition was obtained with an ultrasonic intensity of 1528 W/m(2), extraction temperature of 35°C and extraction time of 30 min. At these conditions, extraction maximum extraction of total carotenoids as 163.47 mg/100 g dried peel. The experimental values under optimal condition were in good consistent with the predicted values. Copyright © 2015 Elsevier B.V. All rights reserved.

Ultrasonic-assisted synthesis of aqueous CdTe/CdS QDs in salt water bath heating

Energy Technology Data Exchange (ETDEWEB)

Zhu, Yinglian [College of Food Science and Engineering, Ocean University of China, Qingdao 266003, Shandong Province (China); College of Food Science and Engineering, Qingdao Agricultural University of China, Qingdao 266109, Shandong Province (China); Li, Chunsheng; Xu, Ying [College of Food Science and Engineering, Ocean University of China, Qingdao 266003, Shandong Province (China); Wang, Dongfeng, E-mail: wangdf@ouc.edu.cn [College of Food Science and Engineering, Ocean University of China, Qingdao 266003, Shandong Province (China)

2014-09-01

Highlights: • Ultrasonic promotes formation of crystal nucleus and QDs were synthesized in 0.5 h. • The new heating method provides a PLQY of up to 97.13%. • The synthesis mechanism of the core shell structure of the CdTe/CdS QDs was inferred. • The preparation method was efficient, simple and clean. - Abstract: A novel simple method for fast and efficient synthesis of aqueous CdTe/CdS quantum dots (QDs) with core–shell structure was developed by using salt water bath heating with the ultrasonic-assisted technique in this paper. The formation of crystal nucleus was promoted by ultrasonic and CdTe/CdS QDs with blue fluorescence were synthesized only in 0.5 h. The heat source was bath heating in salt water solution at 60% NaCl and the heating temperature could reach 105 °C. The heating method solved the biggest drawback of low photoluminescence quantum yield (PLQY) of ordinal bath heating in water. The preparation was cheap, simple and had less pollution to the environment. The properties of the CdTe/CdS QDs were thoroughly investigated by ultraviolet–visible (UV–vis), photoluminescence (PL), transmission electron microscope (TEM), laser size analysis, fourier transform infrared spectra (FTIR), X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Different CdTe/CdS QDs with core shell structure were efficiently synthesized and the maximum PLQY could reach 97.13% when refluxing at 105 °C for 2 h. These QDs exhibited uniform dispersity, high fluorescence intensity, good optical property and long life of fluorescent. The synthesis mechanism of the core shell structure of the QDs was inferred that the Cd{sup 2+} might coordinate with sulfur (S) as well as thiol propionate (–SCH{sub 2}CH{sub 2}COO{sup −1}) to constitute two relatively thick compound layers on the QDs surface as passive shells.

Ultrasonic assisted consolidation of commingled thermoplastic/glass fibers rovings

Directory of Open Access Journals (Sweden)

Francesca eLionetto

2015-04-01

Full Text Available Thermoplastic matrix composites are finding new applications in different industrial area thanks to their intrinsic advantages related to environmental compatibility and processability. The approach presented in this work consists in the development of a technology for the simultaneous deposition and consolidation of commingled thermoplastic rovings through to the application of high energy ultrasound. An experimental equipment, integrating both fiber impregnation and ply consolidation in a single process, has been designed and tested. It is made of an ultrasonic welder, whose titanium sonotrode is integrated on a filament winding machine. During winding, the commingled roving is at the same time in contact with the mandrel and the horn. The intermolecular friction generated by ultrasound is able to melt the thermoplastic matrix and impregnate the reinforcement fibers. The heat transfer phenomena occurring during the in situ consolidation were simulated solving by finite element (FE analysis an energy balance accounting for the heat generated by ultrasonic waves and the melting characteristics of the matrix. To this aim, a calorimetric characterization of the thermoplastic matrix has been carried out to obtain the input parameters for the model. The FE analysis has enabled to predict the temperature distribution in the composite during heating and cooling The simulation results have been validated by the measurement of the temperature evolution during ultrasonic consolidation.The reliability of the developed consolidation equipment was proved by producing hoop wound cylinder prototypes using commingled continuous E-glass rovings and Polypropylene (PP filaments. The consolidated composite cylinders are characterized by high mechanical properties, with values comparable with the theoretical ones predicted by the micromechanical analysis.

[Remediation efficiency of lead-contaminated soil at an industrial site by ultrasonic-assisted chemical extraction].

Science.gov (United States)

Wang, Xin-jie; Huang, Jin-lou; Liu, Zhi-qiang; Yue, Xi

2013-09-01

This research chose five lead-contaminated sites of a lead-acid battery factory to analyze the speciation distribution and concentration of lead. Under the same conditions (0.1 mol x L(-1) EDTA,30 min, 25 degrees C), the removal effect of heavy metal was compared between ultrasonic-assisted chemical extraction (UCE) and conventional chemical extraction ( CCE), and the variation of lead speciation was further explored. The results showed that the lead removal efficiency of UCE was significantly better than CCE. The lead removal efficiency of WS, A, B, C and BZ was 10.06%, 48.29%, 48.69%, 53.28% and 36.26% under CCE. While the removal efficiency of the UCE was 22.42%, 69.31%, 71.00%, 74.49% and 71.58%, with the average efficiency higher by 22%. By comparing the speciation distribution of the two washing methods, it was found that the acid extractable content maintained or decreased after UCE, whereas it showed an increasing trend after CCE. The reduction effect of the reducible was as high as 98% by UCE. UCE also showed a more efficient reduction effect of the organic matter-sulfite bounded form and the residual form. Hence, it is feasible to improve the washing efficiency of heavy metal contained in soil by conducting the cleaning process with the help of ultrasonic wave, which is a simple and fast mean to remove lead from contaminated sites.

Structure and properties of fixed joints formed by ultrasonic-assisted friction-stir welding

Energy Technology Data Exchange (ETDEWEB)

Fortuna, S. V., E-mail: s-fortuna@ispms.ru; Ivanov, K. V., E-mail: ikv@ispms.ru; Eliseev, A. A., E-mail: alan@ispms.ru [Institute of Strength Physics and Materials ScienceTomsk, 634055 (Russian Federation); Tarasov, S. Yu., E-mail: tsy@ispms.ru; Ivanov, A. N., E-mail: ivan@ispms.ru; Rubtsov, V. E., E-mail: rvy@ispms.ru; Kolubaev, E. A., E-mail: eak@ispms.ru [Institute of Strength Physics and Materials ScienceTomsk, 634055 (Russian Federation); National Research Tomsk Polytechnic University, Tomsk, 634050 (Russian Federation)

2015-10-27

This paper deals with structure and properties of aluminum alloy 7475 and its joints obtained by friction stir welding including under ultrasonic action. Microhardness measurements show that ultrasonic action increases strength properties of the joints. Optical and transmission electron microscopy reveals that this effect is related to the precipitation of tertiary coherent S-and T-phase particles.

Ultrasonic sectional imaging for crack identification. Part 1. Confirmation test of essential factors for ultrasonic imaging

International Nuclear Information System (INIS)

Sasahara, Toshihiko

2008-01-01

Since the first reports of inter-granular stress corrosion crack (IGSCC) in boiling water reactor (BWR) pipe in the 1970s, nuclear power industry has focused considerable attention on service induced crack detection and sizing using ultrasonic examination. In recent years, phased array systems, those reconstruct high quality flaw images at real time are getting to apply for crack detection and sizing. But because the price of phased array systems are expensive for inspection vendors, field application of phased array systems are limited and reliable ultrasonic imaging systems with reasonable price are expected. This paper will discuss cost effective ultrasonic equipment with sectional image (B-scan) presentation as the simplified imaging system for assisting ultrasonic examination personnel. To develop the simplified B-scan imaging system, the frequency characteristics of IGSCC echoes and neighboring geometry echoes such as base-metal to weld interface and inner surface of a pipe are studied. The experimental study confirmed the reflectors have different frequency characteristics and 2MHz is suitable to visualize IGSCC and 5MHz and higher frequency are suitable to reconstruct geometry images. The other study is the amplifier selection for the imaging system. To reconstruct images of IGSCC and geometry echoes, the ultrasonic imaging instrument with linear amplifier has to adjust gain setting to the target. On the other hand, the ultrasonic imaging instrument with logarithmic amplifier can collect and display wider dynamic range on a screen and this wider dynamic range are effective to visualize IGSCC and geometry echoes on a B-scan presentation at a time. (author)

Advanced Drilling through Diagnostics-White-Drilling

International Nuclear Information System (INIS)

FINGER, JOHN T.; GLOWKA, DAVID ANTHONY; LIVESAY, BILLY JOE; MANSURE, ARTHUR J.; PRAIRIE, MICHAEL R.

1999-01-01

A high-speed data link that would provide dramatically faster communication from downhole instruments to the surface and back again has the potential to revolutionize deep drilling for geothermal resources through Diagnostics-While-Drilling (DWD). Many aspects of the drilling process would significantly improve if downhole and surface data were acquired and processed in real-time at the surface, and used to guide the drilling operation. Such a closed-loop, driller-in-the-loop DWD system, would complete the loop between information and control, and greatly improve the performance of drilling systems. The main focus of this program is to demonstrate the value of real-time data for improving drilling. While high-rate transfer of down-hole data to the surface has been accomplished before, insufficient emphasis has been placed on utilization of the data to tune the drilling process to demonstrate the true merit of the concept. Consequently, there has been a lack of incentive on the part of industry to develop a simple, low-cost, effective high-speed data link. Demonstration of the benefits of DWD based on a high-speed data link will convince the drilling industry and stimulate the flow of private resources into the development of an economical high-speed data link for geothermal drilling applications. Such a downhole communication system would then make possible the development of surface data acquisition and expert systems that would greatly enhance drilling operations. Further, it would foster the development of downhole equipment that could be controlled from the surface to improve hole trajectory and drilling performance. Real-time data that would benefit drilling performance include: bit accelerations for use in controlling bit bounce and improving rock penetration rates and bit life; downhole fluid pressures for use in the management of drilling hydraulics and improved diagnosis of lost circulation and gas kicks; hole trajectory for use in reducing directional

Synthetic Aperture Focusing Technique in Ultrasonic Inspection of Coarse Grained Materials

Energy Technology Data Exchange (ETDEWEB)

Stepinski, Tadeusz (Uppsala Univ., Signals and Systems, Box 528, SE-751 20 Uppsala (Sweden))

2007-12-15

Experience from the ultrasonic inspection of nuclear power plants has shown that large focused transducers are relatively effective in suppressing grain (structure) noise. Operation of a large focused transducer can be thought of as an integration (coherent summation) of individual beams reflected from the target and received by individual points at the transducer surface. Synthetic aperture focusing technique (SAFT), in its simplest version mimics an acoustic lens used for focusing beams at a desired point in the region of interest. Thus, SAFT should be able to suppress the grain noise in the similar way as the focused transducer does. This report presents the results of investigation of SAFT algorithms applied for post-processing of ultrasonic data acquired in inspection of coarse grained metals. The performance of SAFT in terms of its spatial (cross-range) resolution and grain noise suppression is studied. The evaluation is made based on the experimental data obtained from the ultrasonic inspection of test specimens with artificial defects (side drilled holes). SAFT algorithms for both contact and immersion mode are introduced and experimentally verified

Vapor-liquid equilibrium of ethanol/ethyl acetate mixture in ultrasonic intensified environment

Energy Technology Data Exchange (ETDEWEB)

Mahdi, Taha; Ahmad, Arshad; Ripin, Adnan Nasef; Mohamed, Mahmoud [Universiti Teknologi Malaysia, Johor Bahru (Malaysia)

2014-05-15

A vapor-liquid equilibrium (VLE) study was conducted on ethanol/ethylacetate mixture as a preliminary step towards developing an ultrasonic-assisted distillation process for separating azeotropic mixtures. The influence of ultrasonic intensity and frequency on the vapor-liquid equilibrium (VLE) of the mixture was examined using a combination of four ultrasonic intensities in range of 100-400W/cm{sup 2} and three frequencies ranging from 25-68 kHz. The sonication was found to have significant impacts on the VLE of the system as it alters both the relative volatility and azeotrope point, with preference to lower frequency operation. A maximum relative volatility of 2.32 was obtained at an intensity of 300 W/cm{sup 2} and a frequency of 25 kHz coupled with complete elimination of ethanol-ethyl acetate azeotrope. Results from this work were also congruent with some experimental and theoretical works presented in the literature. These findings set a good beginning towards the development of an ultrasonic assisted distillation that is currently in progress.

Vapor-liquid equilibrium of ethanol/ethyl acetate mixture in ultrasonic intensified environment

International Nuclear Information System (INIS)

Mahdi, Taha; Ahmad, Arshad; Ripin, Adnan Nasef; Mohamed, Mahmoud

2014-01-01

A vapor-liquid equilibrium (VLE) study was conducted on ethanol/ethylacetate mixture as a preliminary step towards developing an ultrasonic-assisted distillation process for separating azeotropic mixtures. The influence of ultrasonic intensity and frequency on the vapor-liquid equilibrium (VLE) of the mixture was examined using a combination of four ultrasonic intensities in range of 100-400W/cm 2 and three frequencies ranging from 25-68 kHz. The sonication was found to have significant impacts on the VLE of the system as it alters both the relative volatility and azeotrope point, with preference to lower frequency operation. A maximum relative volatility of 2.32 was obtained at an intensity of 300 W/cm 2 and a frequency of 25 kHz coupled with complete elimination of ethanol-ethyl acetate azeotrope. Results from this work were also congruent with some experimental and theoretical works presented in the literature. These findings set a good beginning towards the development of an ultrasonic assisted distillation that is currently in progress

Optimizing drilling performance using a selected drilling fluid

Science.gov (United States)

Judzis, Arnis [Salt Lake City, UT; Black, Alan D [Coral Springs, FL; Green, Sidney J [Salt Lake City, UT; Robertson, Homer A [West Jordan, UT; Bland, Ronald G [Houston, TX; Curry, David Alexander [The Woodlands, TX; Ledgerwood, III, Leroy W.

2011-04-19

To improve drilling performance, a drilling fluid is selected based on one or more criteria and to have at least one target characteristic. Drilling equipment is used to drill a wellbore, and the selected drilling fluid is provided into the wellbore during drilling with the drilling equipment. The at least one target characteristic of the drilling fluid includes an ability of the drilling fluid to penetrate into formation cuttings during drilling to weaken the formation cuttings.

Ultrasonic Testing

Energy Technology Data Exchange (ETDEWEB)

Lee, Hyeong Jun; Kuk, Jeong Han

2002-02-15

This book introduces ultrasonic testing, which tells of outline of ultrasonic testing, principle of ultrasonic testing, prosperities of ultrasonic waves, radiographic test and ultrasonic test, basic theory on ultrasonic testing, mode conversion, transmission and diffraction, ultrasonic flaw detection and probe, standard test piece and reference test piece, like KS(JIS) ASME and ASTM, classification and properties of ultrasonic testing, straight beam method, angle beam method, ASME SEC.V.Art.5 ASTMA 388 and KS B 0817 Korean industrial standard.

Generating porosity spectrum of carbonate reservoirs using ultrasonic imaging log

Science.gov (United States)

Zhang, Jie; Nie, Xin; Xiao, Suyun; Zhang, Chong; Zhang, Chaomo; Zhang, Zhansong

2018-03-01

Imaging logging tools can provide us the borehole wall image. The micro-resistivity imaging logging has been used to obtain borehole porosity spectrum. However, the resistivity imaging logging cannot cover the whole borehole wall. In this paper, we propose a method to calculate the porosity spectrum using ultrasonic imaging logging data. Based on the amplitude attenuation equation, we analyze the factors affecting the propagation of wave in drilling fluid and formation and based on the bulk-volume rock model, Wyllie equation and Raymer equation, we establish various conversion models between the reflection coefficient β and porosity ϕ. Then we use the ultrasonic imaging logging and conventional wireline logging data to calculate the near-borehole formation porosity distribution spectrum. The porosity spectrum result obtained from ultrasonic imaging data is compared with the one from the micro-resistivity imaging data, and they turn out to be similar, but with discrepancy, which is caused by the borehole coverage and data input difference. We separate the porosity types by performing threshold value segmentation and generate porosity-depth distribution curves by counting with equal depth spacing on the porosity image. The practice result is good and reveals the efficiency of our method.

Well drilling by rotary percussive drill above ground

International Nuclear Information System (INIS)

Sabatier, G.

1987-01-01

Originally, the Well Drilling Section of Cogema used only the diamond core drilling technique. The appearance of independent rotation for compressed air rock drills has led to the use and to the development of this drilling system, as a drill core is not indispensable, when the material of the search is radioactive. During the last few years, hydraulic drills have replaced the compressed air drills and have resulted in a very marked improvement: - of the penetration rates; - of the depth achieved. The Well Drilling Section of Cogema has to drill about 400 km per year with rock drills above ground and holds also the record for depth achieved with this technique, i.e. 400 m in granite. In France, the costs of these types of drilling are for the same depth of the order of one-quarter of the core drilling and half of the drilling with a down-the-hole drill. Cogema has greatly developed the types of well logging which now permits the extension of this type of drilling to the search for other materials than uranium [fr

Rehabilitation with 4 zygomatic implants with a new surgical protocol using ultrasonic technique.

Science.gov (United States)

Mozzati, Marco; Mortellaro, Carmen; Arata, Valentina; Gallesio, Giorgia; Previgliano, Valter

2015-05-01

When the residual bone crest cannot allow the placement of standard implants, the treatment for complete arch rehabilitation of severely atrophic maxillae can be performed with 4 zygomatic implants (ZIs) and immediate function with predictable results in terms of aesthetics, function, and comfort for the patient. However, even if ZIs' rehabilitations showed a good success rate, this surgery is difficult and need a skillful operator. Complications in this kind of rehabilitation are not uncommon; the main difficulties can be related to the reduced surgical visibility and instrument control in a critical anatomic area. All the surgical protocols described in the literature used drilling techniques. Furthermore, the use of ultrasonic instruments in implant surgery compared with drilling instruments have shown advantages in many aspects of surgical procedures, tissues management, enhancement of control, surgical visualization, and healing. The aim of this study was to report on the preliminary experience using ultrasound technique for ZIs surgery in terms of safety and technical improvement. Ten consecutive patients with severely atrophic maxilla have been treated with 4 ZIs and immediate complete arch acrylic resin provisional prostheses. The patients were followed up from 30 to 32 months evaluating implant success, prosthetic success, and patient satisfaction with a questionnaire. No implants were lost during the study period, with a 100% implant and prosthetic success rate. Within the limitations of this preliminary study, these data indicate that ultrasonic implant site preparation for ZIs can be a good alternative to the drilling technique and an improvement for the surgeon.

Ultrasonic assisted dyeing: dyeing of acrylic fabrics C.I. Astrazon Basic Red 5BL 200%.

Science.gov (United States)

Kamel, M M; Helmy, H M; Mashaly, H M; Kafafy, H H

2010-01-01

The dyeing of acrylic fabrics using C.I. Astrazon Basic Red 5BL 200% has been studied with both conventional and ultrasonic techniques. The effect of dye concentration, dye bath pH, ultrasonic power, dyeing time and temperature were studied and the resulting shades obtained by dyeing with both techniques were compared. Colour strength values obtained were found to be higher with ultrasonic than with conventional heating. The results of fastness properties of the dyed fabrics were studied. X-ray and Scanning Electron Microscope SEM were carried out on dyed samples using both methods of dyeing to find out an explanation for the better dyeability of acrylic fabrics with (US) method. Dyeing kinetics of acrylic fabrics using C.I. Astrazon Basic Red 5BL 200% using conventional and ultrasonic conditions were compared. The time/dye-uptake isotherms are revealing the enhanced dye-uptake in the second phase of dyeing. The values of dyeing rate constant, half-time of dyeing and standard affinity and ultrasonic efficiency have been calculated and discussed.

Radiation-Force Assisted Targeting Facilitates Ultrasonic Molecular Imaging

Directory of Open Access Journals (Sweden)

Shukui Zhao

2004-07-01

Full Text Available Ultrasonic molecular imaging employs contrast agents, such as microbubbles, nanoparticles, or liposomes, coated with ligands specific for receptors expressed on cells at sites of angiogenesis, inflammation, or thrombus. Concentration of these highly echogenic contrast agents at a target site enhances the ultrasound signal received from that site, promoting ultrasonic detection and analysis of disease states. In this article, we show that acoustic radiation force can be used to displace targeted contrast agents to a vessel wall, greatly increasing the number of agents binding to available surface receptors. We provide a theoretical evaluation of the magnitude of acoustic radiation force and show that it is possible to displace micron-sized agents physiologically relevant distances. Following this, we show in a series of experiments that acoustic radiation force can enhance the binding of targeted agents: The number of biotinylated microbubbles adherent to a synthetic vessel coated with avidin increases as much as 20-fold when acoustic radiation force is applied; the adhesion of contrast agents targeted to αvβ3 expressed on human umbilical vein endothelial cells increases 27-fold within a mimetic vessel when radiation force is applied; and finally, the image signal-to-noise ratio in a phantom vessel increases up to 25 dB using a combination of radiation force and a targeted contrast agent, over use of a targeted contrast agent alone.

Deep Drilling and Sampling via the Wireline Auto-Gopher Driven by Piezoelectric Percussive Actuator and EM Rotary Motor

Science.gov (United States)

Bar-Cohen, Yoseph; Badescu, Mircea; Sherrit, Stewart; Zacny, Kris; Paulsen, Gale L; Beegle, Luther; Bao, Xiaoqi

2012-01-01

The ability to penetrate subsurfaces and perform sample acquisition at depths of meters is critical for future NASA in-situ exploration missions to bodies in the solar system, including Mars and Europa. A corer/sampler was developed with the goal of acquiring pristine samples by reaching depths on Mars beyond the oxidized and sterilized zone. To developed rotary-hammering coring drill, called Auto-Gopher, employs a piezoelectric actuated percussive mechanism for breaking formations and an electric motor rotates the bit to remove the powdered cuttings. This sampler is a wireline mechanism that is incorporated with an inchworm mechanism allowing thru cyclic coring and core removal to reach great depths. The penetration rate is being optimized by simultaneously activating the percussive and rotary motions of the Auto-Gopher. The percussive mechanism is based on the Ultrasonic/Sonic Drill/Corer (USDC) mechanism that is driven by piezoelectric stack and that was demonstrated to require low axial preload. The Auto-Gopher has been produced taking into account the a lessons learned from the development of the Ultrasonic/Sonic Gopher that was designed as a percussive ice drill and was demonstrated in Antarctica in 2005 to reach about 2 meters deep. A field demonstration of the Auto-Gopher is currently being planned with objective of reaching as deep as 3 to 5 meters in tufa subsurface.

Response Surface Methodology Optimization of Ultrasonic-Assisted Extraction of Acer Truncatum Leaves for Maximal Phenolic Yield and Antioxidant Activity.

Science.gov (United States)

Yang, Lingguang; Yin, Peipei; Fan, Hang; Xue, Qiang; Li, Ke; Li, Xiang; Sun, Liwei; Liu, Yujun

2017-02-04

This study is the first to report the use of response surface methodology to improve phenolic yield and antioxidant activity of Acer truncatum leaves extracts (ATLs) obtained by ultrasonic-assisted extraction. The phenolic composition in ATLs extracted under the optimized conditions were characterized by UPLC-QTOF-MS/MS. Solvent and extraction time were selected based on preliminary experiments, and a four-factors-three-levels central composite design was conducted to optimize solvent concentration ( X ₁), material-to-liquid ratio ( X ₂), ultrasonic temperature ( X ₃) and power ( X ₄) for an optimal total phenol yield ( Y ₁) and DPPH• antioxidant activity ( Y ₂). The results showed that the optimal combination was ethanol:water ( v : v ) 66.21%, material-to-liquid ratio 1:15.31 g/mL, ultrasonic bath temperature 60 °C, power 267.30 W, and time 30 min with three extractions, giving a maximal total phenol yield of 7593.62 mg gallic acid equivalent/100 g d.w. and a maximal DPPH• antioxidant activity of 74,241.61 μmol Trolox equivalent/100 g d.w. Furthermore, 22 phenolics were first identified in ATL extract obtained under the optimized conditions, indicating that gallates, gallotannins, quercetin, myricetin and chlorogenic acid derivatives were the main phenolic components in ATL. What's more, a gallotannins pathway existing in ATL from gallic acid to penta- O -galloylglucoside was proposed. All these results provide practical information aiming at full utilization of phenolics in ATL, together with fundamental knowledge for further research.

Preparation of graphene-enhanced nickel-phosphorus composite films by ultrasonic-assisted electroless plating

Science.gov (United States)

Yu, Qian; Zhou, Tianfeng; Jiang, Yonggang; Yan, Xing; An, Zhonglie; Wang, Xibin; Zhang, Deyuan; Ono, Takahito

2018-03-01

To improve the mechanical properties of nickel-phosphorus (Ni-P) mold material for glass molding, an ultrasonic-assisted electroless plating method is proposed for the synthesis of graphene-enhanced nickel-phosphorus (G-Ni-P) composite films on heat-resistant stainless steel (06Cr25Ni20). Graphene flakes are prepared by an electrochemical exfoliation method. The surface roughness of the as-plated G-Ni-P composite plating is Ra 2.84 μm, which is higher than that of the Ni-P plating deposited using the same method. After annealing at 400 ºC for 2 h, the main phase of the G-Ni-P composite is transformed to crystalline Ni3P with an average grain size of 32.8 nm. The Vickers hardness and Young's modulus of the G-Ni-P composite are increased by 8.0% and 8.2% compared with the values of Ni-P, respectively. The detailed plating process is of great significance for the fabrication of G-Ni-P mold materials with enhanced mechanical properties.

Study for increasing micro-drill reliability by vibrating drilling

International Nuclear Information System (INIS)

Yang Zhaojun; Li Wei; Chen Yanhong; Wang Lijiang

1998-01-01

A study for increasing micro-drill reliability by vibrating drilling is described. Under the experimental conditions of this study it is observed, from reliability testing and the fitting of a life-distribution function, that the lives of micro-drills under ordinary drilling follow the log-normal distribution and the lives of micro-drills under vibrating drilling follow the Weibull distribution. Calculations for reliability analysis show that vibrating drilling can increase the lives of micro-drills and correspondingly reduce the scatter of drill lives. Therefore, vibrating drilling increases the reliability of micro-drills

Method and apparatus for jet-assisted drilling or cutting

Science.gov (United States)

Summers, David Archibold; Woelk, Klaus Hubert; Oglesby, Kenneth Doyle; Galecki, Grzegorz

2012-09-04

An abrasive cutting or drilling system, apparatus and method, which includes an upstream supercritical fluid and/or liquid carrier fluid, abrasive particles, a nozzle and a gaseous or low-density supercritical fluid exhaust abrasive stream. The nozzle includes a throat section and, optionally, a converging inlet section, a divergent discharge section, and a feed section.

Characterization of 2.25Cr1Mo welded ferritic steel plate by using diffractometric and ultrasonic techniques

Energy Technology Data Exchange (ETDEWEB)

Cernuschi, F.; Ghia, S. [Ente Nazionale per l`Energia Elettrica, Milan (Italy); Albertini, G.; Ceretti, M.; Rustichelli, F. [Ancona Univ. (Italy). Ist. di Fisica Medica; Castelnuovo, A.; Depero, L. [Univ. degli studi, Brescia.Fac. di ingegneria, dip. di ingegneria meccanica (Italy); Giamboni, S.; Gori, M. [Centro Elettrotecnico Sperimentale Italiano (CESI), Milan (Italy)

1995-12-01

Four different techniques (X-ray and neutron diffraction, ultrasonic birefringence and incremental hole drilling method) were applied for evaluating residual stress in a butt-welded ferritic steel palte. Measurements were carried out both before and after welding. Effects of post-welding heat treatment is also considered. A comparison between results obtained by using four different techniques is done.

A comparison of accelerated solvent extraction, Soxhlet extraction, and ultrasonic-assisted extraction for analysis of terpenoids and sterols in tobacco.

Science.gov (United States)

Shen, Jinchao; Shao, Xueguang

2005-11-01

The performance of accelerated solvent extraction in the analysis of terpenoids and sterols in tobacco samples was investigated and compared with those of Soxhlet extraction and ultrasonically assisted extraction with respect to yield, extraction time, reproducibility and solvent consumption. The results indicate that although the highest yield was achieved by Soxhlet extraction, ASE appears to be a promising alternative to classical methods since it is faster and uses less solvent, especially when applied to the investigation of large batch tobacco samples. However, Soxhlet extraction is still the preferred method for analyzing sterols since it gives a higher extraction efficiency than other methods.

Ultrasonic Extraction of Antioxidants from Chinese Sumac (Rhus typhina L.) Fruit Using Response Surface Methodology and Their Characterization

OpenAIRE

Lai, Jixiang; Wang, Huifang; Wang, Donghui; Fang, Fang; Wang, Fengzhong; Wu, Tao

2014-01-01

For the first time, response surface methodology (RSM) using a Box-Behnken Design (BBD) was employed to optimize the conditions for ultrasonic assisted extraction (UAE) of antioxidants from Chinese sumac (Rhus typhina L.) fruits. Initially, influencing factors such as liquid-solid ratio, duration of ultrasonic assisted extraction, pH range, extraction temperature and ethanol concentration were identified using single-factor experiments. Then, with respect to the three most significant influen...

Study on the extraction of dioscin by the ultrasonic- assisted ethanol

African Journals Online (AJOL)

aghomotsegin

2014-02-19

Feb 19, 2014 ... 1Shaanxi University of Science and Technology, Key laboratory of Auxiliary ... the effect on extraction yield of dioscin of frequency of ultrasonic, the period of ..... steroidal saponins on Taiwanese yam cultivar (Dioscorea.

Ultrasonically assisted extraction of calcium and ash from char

Science.gov (United States)

Mathumba, E. E.; Mbaya, R. K. K.; Kolesnikov, A.

2018-03-01

This study characterized and removed calcium and ash content from char to improve the chemical quality of char as reductant for titanium smelting application. Calcium in char can be classified in two parts: mineral matter and cationic metals associated with organic matrix. Virgin and chemically treated char was characterized by using ISO 1171, wet chemistry methods, ISO 19579, XRF, and B.E.T. methods. In this present work, demineralization of char with mild chemical leachants such as acetic acid, citric acid, gluconic acid and Ethylene Diamine Tetra Acetic acid with three different ultrasonic power input (150 W, 270 W and 300 W) and semi-dual frequency of 40 kHz tank was investigated. Actual power dissipated into the system was calculated from the calorimetric measurement. An optimum set of process parameters are identified and validated. The ultrasound technology was compared with soaking technology to determine the efficiency of ultrasound system for the removal of calcium. The removal of calcium was exponentially higher with ultrasonic treatment than without it. Results revealed that mild chemical reagents do not harm the carbon content of char. It is evident from the results that amongst the leachants used; acetic and citric acid has caused significant removal of mineral phases.

Sequential Combination of Microwave- and Ultrasound-Assisted Extraction of Total Flavonoids from Osmanthus fragrans Lour. Flowers

Directory of Open Access Journals (Sweden)

Jianfeng Yu

2017-12-01

Full Text Available Microwave-assisted and ultrasound-assisted extraction assays were used to isolate total flavonoids (TF from Osmanthus fragrans flowers. The effects of the solid-liquid ratio, ethanol concentration, microwave power, microwave extraction time, ultrasonic power and ultrasonic extraction time on the yield of TF were studied. A sequential combination of microwave- and ultrasound-assisted extraction (SC-MUAE methods was developed, which was subsequently optimized by Box-Behnken design-response surface methodology (BBD-RSM. The interaction effects of the ethanol concentration (40–60%, microwave extraction time (5–7 min, ultrasonic extraction time (8–12 min and ultrasonic power (210–430 W on the yield of TF were investigated. The optimum operating parameters for the extraction of TF were determined to be as follows: ethanol concentration (48.15%, microwave extraction time (6.43 min, ultrasonic extraction time (10.09 min and ultrasonic power (370.9 W. Under these conditions, the extraction yield of TF was 7.86 mg/g.

Augmented reality application for training in pipe defects ultrasonic investigation

Directory of Open Access Journals (Sweden)

Amza Cătălin Gheorghe

2017-01-01

Full Text Available The paper presents the development process of an Augmented Reality (AR application used for training operators in using ultrasonic equipment for non-destructive testing (NDT of pipework. The application provides workers useful information regarding the process steps, the main components of ultrasonic equipment and the proper modality of placing, aligning and moving it on pipe and weld. Using tablet or mobile phone device, an operator can see on screen written details and images on standardized working method, thus offering assistance during the training process. Allowing 3D augmented visualization of ultrasonic equipment overlaid on the real-world environment consisting in pipes and welds, the AR application makes the NDT process easier to understand and learn, as the initial evaluation results showed.

Deposition of Ni-CGO composite anodes by electrostatic assisted ultrasonic spray pyrolysis method

International Nuclear Information System (INIS)

Chen, J.-C.; Chang, C.-L.; Hsu, C.-S.; Hwang, B.-H.

2007-01-01

Deposition of composite films of Ni and Gd-doped ceria was carried out using the electrostatic assisted ultrasonic spray pyrolysis method for the first time. The composite films were highly homogeneous, as revealed by element mapping via energy-dispersive spectrometry. Scanning electron microscope examinations revealed that deposition temperature and electric field strength had profound influence on resultant microstructure, while composition of the precursor solution had little effect. A highly porous cauliflower structure ideal for solid oxide fuel cell anode performance was obtained with a deposition temperature of 450 deg. C under an electric field introduced by an applied voltage of 12 kV. Films obtained with a lower deposition temperature of 250 deg. C or a higher applied voltage of 15 kV resulted in denser films with low porosity, while lower applied voltages of 7 or 5 kV resulted in thinner or discontinuous films due to the insufficient electrostatic attraction on the aerosol droplets. As revealed by AC impedance measurement, the area specific resistances of the Ni-CGO anode with porous cauliflower structure were rather low and a value of 0.09 Ω cm 2 at 550 deg. C was obtained

Enhanced electrochemical performance of nano-sized LiFePO4/C synthesized by an ultrasonic-assisted co-precipitation method

International Nuclear Information System (INIS)

Liu Youyong; Cao Chuanbao

2010-01-01

A simple and effective method, the ultrasonic-assisted co-precipitation method, was employed to synthesize nano-sized LiFePO 4 /C. A glucose solution was used as the carbon source to produce in situ carbon to improve the conductivity of LiFePO 4 . Ultrasonic irradiation was adopted to control the size and homogenize the LiFePO 4 /C particles. The sample was characterized by X-ray powder diffraction, field-emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM). FE-SEM and TEM show that the as-prepared sample has a reduced particle size with a uniform size distribution, which is around 50 nm. A uniform amorphous carbon layer with a thickness of about 4-6 nm on the particle surface was observed, as shown in the HRTEM image. The electrochemical performance was demonstrated by the charge-discharge test and electrochemical impedance spectra measurements. The results indicate that the nano-sized LiFePO 4 /C presents enhanced discharge capacities (159, 147 and 135 mAh g -1 at 0.1, 0.5 and 2 C-rate, respectively) and stable cycling performance. This study offers a simple method to design and synthesis nano-sized cathode materials for lithium-ion batteries.

Ultrasonic Substrate Vibration-Assisted Drop Casting (SVADC) for the Fabrication of Photovoltaic Solar Cell Arrays and Thin-Film Devices.

Science.gov (United States)

Eslamian, Morteza; Zabihi, Fatemeh

2015-12-01

A simple, low-cost, versatile, and potentially scalable casting method is proposed for the fabrication of micro- and nano-thin films, herein termed as ultrasonic "substrate vibration-assisted drop casting" (SVADC). The impingement of a solution drop onto a substrate in a simple process called drop casting, usually results in spreading of the liquid solution and the formation of a non-uniform thin solid film after solvent evaporation. Our previous and current supporting results, as well as few similar reports by others, confirm that imposing ultrasonic vibration on the substrate can simply convert the uncontrollable drop casting method into a controllable coating technique. Therefore, the SVADC may be used to fabricate an array of emerging thin-film solar cells, such as polymer, perovskite, and quantum-dot solar cells, as well as other small thin-film devices, in a roll-to-roll and automated fabrication process. The preliminary results demonstrate a ten-fold increase in electrical conductivity of PSS made by SVADC compared with the film made by conventional drop casting. Also, simple planar perovskite solar cells made here using SVADC show promising performance with an efficiency of over 3 % for a simple structure without performing process optimization or using expensive materials and treatments.

Development and evaluation of a meter for measuring return line fluid flow rates during drilling

Energy Technology Data Exchange (ETDEWEB)

Loeppke, G.E.; Schafer, D.M.; Glowka, D.A.; Scott, D.D.; Wernig, M.D. (Sandia National Labs., Albuquerque, NM (United States)); Wright, E.K. (Ktech Corp., Albuquerque, NM (United States))

1992-06-01

The most costly problem routinely encountered in geothermal drilling is lost circulation, which occurs when drilling fluid is lost to the formation rather than circulating back to the surface. The successful and economical treatment of lost circulation requires the accurate measurement of drilling fluid flow rate both into and out of the well. This report documents the development of a meter for measuring drilling fluid outflow rates in the return line of a drilling rig. The meter employs a rolling counterbalanced float that rides on the surface of the fluid in the return line. The angle of the float pivot arm is sensed with a pendulum potentiometer, and the height of the float is calculated from this measurement. The float height is closely related to the fluid height and, therefore, the flow rate in the line. The prototype rolling float meter was extensively tested under laboratory conditions in the Wellbore Hydraulics Flow Facility; results from these tests were used in the design of the field prototype rolling float meter. The field prototype meter was tested under actual drilling conditions in August and September 1991 at the Long Valley Exploratory Well near Mammoth Lakes, Ca. In addition, the performance of several other commercially available inflow and outflow meters was evaluated in the field. The tested inflow meters included conventional pump stroke counters, rotary pump speed counters, magnetic flowmeters, and an ultrasonic Doppler flowmeter. On the return flow line, a standard paddlemeter, an acoustic level meter, and the prototype rolling float meter were evaluated for measuring drilling fluid outflow rates.

Applied orthogonal design for filtrating conditions of ultrasonic ...

African Journals Online (AJOL)

user

2011-03-28

Mar 28, 2011 ... ultrasonic-assisted extraction from plant-chicory. Yuyan Liu1 ... leaves are grown for consumption in salads and vege- ..... *The highest extraction percentage of the levels is highlighted in bold; **It is the ordinal numeral for the range sequence ..... of mass transfer in supercritical CO2 extraction processes.

Interracial Structure and Formation Mechanism of Ultrasonic-assisted Brazed Joint of SiC Ceramics with Al-12Si Filler Metals in Air

Institute of Scientific and Technical Information of China (English)

Xiaoguang Chen; Ruishan Xie; Zhiwei Lai; Lei Liu; Jiuchun Yan; Guisheng Zou

2017-01-01

Ultrasonic-assisted brazing of SiC ceramics was performed by filling with an Al--12Si alloy at a low temperature of 620 ℃ in air.The interfacial characteristics and formation mechanism were investigated.The joint shear strength reached 84-94 MPa using the ultrasonic time of 2-16 s.The fracture morphology showed that the fracture path initiated and propagated in the joint alloy.The thin film of amorphous SiO2 that formed on the SiC surface was non-uniformly decomposed and diffused into the liquid Al-12Si alloy under the cavitation erosion effect of ultrasound.Abnormal isolated blocks of Al2SiO5 compounds formed at the interface between Al--12Si and a thicker SiO2 layer formed during the thermal oxidation treatment of the SiC ceramic.The SiO2 layer on the SiC ceramic did not hinder or impair the wetting and bonding process,and a stronger bond could form between Al-12Si and SiO2 or SiC in ultrasonicassisted brazing.

Metre by metre: Advances in drilling technology are unlocking the doors to stubborn reserves

Energy Technology Data Exchange (ETDEWEB)

Jaremko, D.

2004-03-01

Advances in drilling technology such as horizontal drilling, controlled pressure drilling, underbalanced or reduced overbalanced drilling, steam assisted cavity drainage, the modified magnetic ranging system and a growing arsenal of on-line controls such as measurement-while drilling (MWD) and logging-while-drilling (LWD) are constantly enlarging the sites to which operators can go, the range of the pay zone that they can conquer, and to design increasingly site-specific approaches to deal with the change of formation characteristics from location to location. This article provides an overview of recent advances, focusing on underbalanced, balanced and reduced overbalanced drilling, and latest versions of data acquisition systems such as MWD and LWD which are capable of operating at twice the speed of conventional systems and provide accurate data even under the extremely difficult conditions found in hostile offshore environment.

Automatic real time drilling support on Ekofisk utilizing eDrilling

Energy Technology Data Exchange (ETDEWEB)

Rommetveit, Rolv; Bjorkevoll, Knut S.; Halsey, George W.; Kluge, Roald; Molde, Dag Ove; Odegard, Sven Inge [SINTEF Petroleum Research, Trondheim (Norway); Herbert, Mike [HITEC Products Drilling, Stavanger (Norway); ConocoPhillips Norge, Stavanger (Norway)

2008-07-01

eDrilling is a new and innovative system for real time drilling simulation, 3D visualization and control from a remote drilling expert centre. The concept uses all available real time drilling data (surface and downhole) in combination with real time modelling to monitor and optimize the drilling process. This information is used to visualize the wellbore in 3D in real time. eDrilling has been implemented in an Onshore Drilling Center in Norway. The system is composed of the following elements, some of which are unique and ground-breaking: an advanced and fast Integrated Drilling Simulator which is capable to model the different drilling sub-processes dynamically, and also the interaction between these sub-processes in real time; automatic quality check and corrections of drilling data; making them suitable for processing by computer models; real time supervision methodology for the drilling process using time based drilling data as well as drilling models / the integrated drilling simulator; methodology for diagnosis of the drilling state and conditions. This is obtained from comparing model predictions with measured data. Advisory technology for more optimal drilling. A Virtual Wellbore, with advanced visualization of the downhole process. Dat low and computer infrastructure. e-Drilling has been implemented in an Onshore Drilling Center on Ekofisk in Norway. The system is being used on drilling operations, and experiences from its use are presented. The supervision and diagnosis functionalities have been useful in particular, as the system has given early warnings on ECD and friction related problems. This paper will present the eDrilling system as well as experiences from its use. (author)

Ultrasonic testing

Energy Technology Data Exchange (ETDEWEB)

Song, Sung Jin [Sungkwunkwan Univ., Seoul (Korea, Republic of); Jeong, Hyun Jo [Wonkwang Univ., Iksan (Korea, Republic of)

2004-02-15

For the proper performance of ultrasonic testing of steel welded joints, and anisotropic material it is necessary to have sound understanding on the underlying physics. To provide such an understanding, it is beneficial to have simulation tools for ultrasonic testing. In order to address such a need, we develop effective approaches to simulate angle beam ultrasonic testing with a personal computer. The simulation is performed using ultrasonic measurement models based on the computationally efficient multi-Gaussian beams. This reach will describe the developed ultrasonic testing models together with the experimental verification of their accuracy.

Development of application technology of ultrasonic wave sensor; Choonpa sensor oyo gijutsu no kaihatsu

Energy Technology Data Exchange (ETDEWEB)

Hosoya, H; Hikita, N; Sasaki, H; Kore, H [Mazda Motor Corp., Hiroshima (Japan)

1997-10-01

We have developed parking assist system, which informs a driver the closing point and distance to the objects such as other vehicle, wall and pole around the own vehicle at parking area and makes parking maneuverability easy. This system is based on the range detection technology using ultrasonic wave sensor. We have improved the detecting ability in short range of about 20cm by reducing the reverberation of transmitting wave signal and controlling sensitivities of signal intensity and threshold line. We will show mainly the improvement of short range detection of ultrasonic wave sensor, and briefly the performance of parking assist system. 1 ref., 14 figs., 1 tab.

New drilling optimization technologies make drilling more efficient

Energy Technology Data Exchange (ETDEWEB)

Chen, D.C.-K. [Halliburton Energy Services, Calgary, AB (Canada). Sperry Division

2004-07-01

Several new technologies have been adopted by the upstream petroleum industry in the past two decades in order to optimize drilling operations and improve drilling efficiency. Since financial returns from an oil and gas investment strongly depend on drilling costs, it is important to reduce non-productive time due to stuck pipes, lost circulation, hole cleaning and well bore stability problems. The most notable new technologies are the use of computer-based instrumentation and data acquisition systems, integrated rig site systems and networks, and Measurement-While-Drilling and Logging-While-Drilling (MWD/LWD) systems. Drilling optimization should include solutions for drillstring integrity, hydraulics management and wellbore integrity. New drilling optimization methods emphasize information management and real-time decision making. A recent study for drilling in shallow water in the Gulf of Mexico demonstrates that trouble time accounts for 25 per cent of rig time. This translates to about $1.5 MM U.S. per well. A reduction in trouble time could result in significant cost savings for the industry. This paper presents a case study on vibration prevention to demonstrate how the drilling industry has benefited from new technologies. 13 refs., 10 figs.

Ultrasonic coal-wash for de-ashing and de-sulfurization. Experimental investigation and mechanistic modeling

Energy Technology Data Exchange (ETDEWEB)

Ambedkar, B. [Indian Institute of Technology Madras, Chennai (India). Dept. of Chemical Engineering

2012-07-01

This study focuses on the physical aspects of ultrasonic de-ashing and de-sulfurization, such as cavitation, streaming and their combined effects. Ambedkar Balraj proposes an ultrasound-assisted coal particle breakage mechanism and explores aqueous and solvent-based ultrasonic techniques for de-ashing and de-sulfurization. Ambedkar designs a Taguchi L-27 fractional-factorial matrix to assess the individual effects of key process variables. In this volume he also describes process optimization and scale-up strategies. The author provides a mechanism-based model for ultrasonic reagent-based coal de-sulfurization, proposes a flow diagram for ultrasonic methods of high-throughput coal-wash and discusses the benefits of ultrasonic coal-wash. Coal will continue to be a major fuel source for the foreseeable future and this study helps improve its use by minimising ash and sulfur impurities.

Casing drilling

Energy Technology Data Exchange (ETDEWEB)

Heenan, D. [Tesco Corp., Calgary, AB (Canada)

2003-07-01

This paper reviewed the experience that Tesco has gained by drilling several wells using only casings as the drill stem. Tesco has manufactured a mobile and compact hydraulic drilling rig called the Casing Drilling {sup TM} system. The system could be very effective and efficient for exploration and development of coalbed methane (CBM) reserves which typically require extensive coring. Continuous coring while drilling ahead, along wire line retrieval, can offer time savings and quick core recovery of large diameter core which is typically required for exploration core desorption tests. The proposed system may also have the potential to core or drill typically tight gas sands or underbalanced wells with air or foam. This would reduce drilling fluid damage while simultaneously finding gas. Compared to conventional drill pipes, Casing Drilling {sup TM} could also be effective with water production from shallow sands because of the smaller annual clearance which requires less air volumes to lift any produced water. 9 figs.

A method for the preparation of curcumin by ultrasonic-assisted ammonium sulfate/ethanol aqueous two phase extraction.

Science.gov (United States)

Xu, Guangkuan; Hao, Changchun; Tian, Suyang; Gao, Feng; Sun, Wenyuan; Sun, Runguang

2017-01-15

This study investigated a new and easy-to-industrialized extracting method for curcumin from Curcuma longa rhizomes using ultrasonic extraction technology combined with ammonium sulfate/ethanol aqueous two-phase system (ATPS), and the preparation of curcumin using the semi-preparative HPLC. The single-factor experiments and response surface methodology (RSM) were utilized to determine the optimal material-solvent ratio, ultrasonic intensity (UI) and ultrasonic time. The optimum extraction conditions were finally determined to be material-solvent rate of 3.29:100, ultrasonic intensity of 33.63W/cm 2 and ultrasonic time of 17min. At these optimum conditions, the extraction yield could reach 46.91mg/g. And the extraction yields of curcumin remained stable in the case of amplification, which indicated that scale-up extraction was feasible and efficient. Afterwards, the semi-preparative HPLC experiment was carried out, in which optimal preparation conditions were elected according to the single factor experiment. The prepared curcumin was obtained and the purity could up to 85.58% by the semi-preparative HPLC. Copyright © 2016 Elsevier B.V. All rights reserved.

Optimization of ultrasonic-assisted extraction of antioxidant compounds from Guava (Psidium guajava L.) leaves using response surface methodology.

Science.gov (United States)

Kong, Fansheng; Yu, Shujuan; Feng, Zeng; Wu, Xinlan

2015-01-01

To optimization of extraction of antioxidant compounds from guava (Psidium guajava L.) leaves and showed that the guava leaves are the potential source of antioxidant compounds. The bioactive polysaccharide compounds of guava leaves (P. guajava L.) were obtained using ultrasonic-assisted extraction. Extraction was carried out according to Box-Behnken central composite design, and independent variables were temperature (20-60°C), time (20-40 min) and power (200-350 W). The extraction process was optimized by using response surface methodology for the highest crude extraction yield of bioactive polysaccharide compounds. The optimal conditions were identified as 55°C, 30 min, and 240 W. 1,1-diphenyl-2-picryl-hydrazyl and hydroxyl free radical scavenging were conducted. The results of quantification showed that the guava leaves are the potential source of antioxidant compounds.

Dissemination of aerosol and splatter during ultrasonic scaling: A pilot study

Directory of Open Access Journals (Sweden)

H.R. Veena

2015-05-01

Full Text Available Summary: Context: Routine dental procedures produce aerosol and splatter, which pose a potential risk to the clinician and dental personnel, as well as the immunocompromised patient. Reports indicate that the ultrasonic scaler is the greatest producer of aerosol and splatter. Aims: The study aimed to evaluate the contamination distance, contamination amount and contamination duration of aerosol produced during ultrasonic scaling. Methods and materials: The study was performed on a mannequin fitted with phantom jaws on a dental chair. Mock scaling was done for 15 min using an auto-tuned magnetostrictive ultrasonic scaler with the simultaneous use of a low volume saliva ejector. An ultrafiltrate-containing fluorescent dye was used in the reservoir supplying the scaler unit. Filter paper discs were placed in different positions and distances in the operatory. Immediately following scaling, the filter paper discs were replaced with new ones. This was done every 30 min for a total duration of 90 min. Results: Maximum contamination was found on the right arm of the operator and left arm of the assistant. Contamination was also found on the head, chest and inner surface of the face mask of the operator and of the assistant. The aerosol was found to remain in the air up to 30 min after scaling. Conclusions: The occupational health hazards of dental aerosols can be minimized by following simple, inexpensive precautions. Keywords: Aerosol, Splatter, Infection control, Aerosol contamination in dentistry, Dental unit water lines, Ultrasonic scaling

Safety and efficacy of cervical laminoplasty using a piezosurgery device compared with a high-speed drill.

Science.gov (United States)

Li, Kunpeng; Zhang, Wen; Li, Bin; Xu, Hui; Li, Zhong; Luo, Dawei; Zhang, Jingtao; Ma, Jinzhu

2016-09-01

Piezosurgery is a relatively new osteotomy technique using microvibrations of scalpels at ultrasonic frequencies to perform safe and effective osteotomies without damage to adjacent soft tissue, which is widely used in spinal, oral, and maxillofacial surgery. We hypothesized that such a device could also be useful in cervical laminoplasty. The purpose of this study was to compare the safety and efficacy of a piezosurgery device with those of a highspeed drill in cervical laminoplasty. A prospectively randomized clinical study was designed. Forty-two consecutive patients were enrolled in the study. All patients underwent modified expansive open-door laminoplasty and were randomly divided into 2 groups according to the instrument for transection of the lamina, using high-speed drill (drill group) or piezosurgery device (piezosurgery group). The operation time, intraoperative blood loss, and postoperative drainage were recorded. Japanese Orthopedic Association (JOA) score and visual analogue scale (VAS) as clinical assessments were quantified. No significant difference was observed in the operation time between the 2 groups. In the piezosurgery group, there were less loss of the intraoperative blood and postoperative drainage compared with the drill group. However, clinical results (VAS and JOA scores) showed no significant difference between both groups during the all follow-up periods. The piezosurgery is a useful instrument and at least as safe and efficacious as the conventional high-speed drill in cervical laminoplasty.

Importance of drill string assembly swivel in horizontal drilling

Directory of Open Access Journals (Sweden)

Edmund Tasak

2006-10-01

Full Text Available A part of the drill string – the swivel (rotational connector – accomplishes an important task in the horizontal drilling. Its malfunctioning makes it impossible to draw in ( install large diameter and length pipelines. The causes of the connector break-down during the horizontal drilling are investigated in the paper. The drilling has been made for twenty inches gas pipeline installation during reaming operations. A trouble was encountered making good work conditions of a system consisting of the drilling machine drill string reamer swivel tube shield of Cardan joint and the gas pipeline 500 m long. In this case, the swivel brokes down and the planned operation was not finished. The assessment of improper drilling conditions, selection of operation system components, and drilling parameters and the insufficient technological supervising have created an excessive risk of failure. A proper application of technical analysis would considerably decrease the hazard of failure which cause large costs, delays and decrease of confidence to the drilling contractor and pipeline installation.

Drilling comparison in "warm ice" and drill design comparison

DEFF Research Database (Denmark)

Augustin, L.; Motoyama, H.; Wilhelms, F.

2007-01-01

For the deep ice-core drilling community, the 2005/06 Antarctic season was an exciting and fruitful one. In three different Antarctic locations, Dome Fuji, EPICA DML and Vostok, deep drillings approached bedrock (the ice-water interface in the case of Vostok), emulating what had previously been...... achieved at NorthGRIP, Greenland, (summer 2003 and 2004) and at EPICA Dome C2, Antarctica (season 2004/05). For the first time in ice-core drilling history, three different types of drill (KEMS, JARE and EPICA) simultaneously reached the depth of 'warm ice' under high pressure. After excellent progress...... at each site, the drilling rate dropped and the drilling teams had to deal with refrozen ice on cutters and drill heads. Drills have different limits and perform differently. In this comparative study, we examine depth, pressure, temperature, pump flow and cutting speed. Finally, we compare a few...

Photocatalytic Graphene-TiO2 Thin Films Fabricated by Low-Temperature Ultrasonic Vibration-Assisted Spin and Spray Coating in a Sol-Gel Process

Directory of Open Access Journals (Sweden)

Fatemeh Zabihi

2017-05-01

Full Text Available In this work, we communicate a facile and low temperature synthesis process for the fabrication of graphene-TiO2 photocatalytic composite thin films. A sol-gel chemical route is used to synthesize TiO2 from the precursor solutions and spin and spray coating are used to deposit the films. Excitation of the wet films during the casting process by ultrasonic vibration favorably influences both the sol-gel route and the deposition process, through the following mechanisms. The ultrasound energy imparted to the wet film breaks down the physical bonds of the gel phase. As a result, only a low-temperature post annealing process is required to eliminate the residues to complete the conversion of precursors to TiO2. In addition, ultrasonic vibration creates a nanoscale agitating motion or microstreaming in the liquid film that facilitates mixing of TiO2 and graphene nanosheets. The films made based on the above-mentioned ultrasonic vibration-assisted method and annealed at 150 °C contain both rutile and anatase phases of TiO2, which is the most favorable configuration for photocatalytic applications. The photoinduced and photocatalytic experiments demonstrate effective photocurrent generation and elimination of pollutants by graphene-TiO2 composite thin films fabricated via scalable spray coating and mild temperature processing, the results of which are comparable with those made using lab-scale and energy-intensive processes.

Ultrasonic testing of austenitic welds and its dependency on the welding process

International Nuclear Information System (INIS)

Tabatabaeipour, S.M.; Honarvar, F.

2009-01-01

This paper describes the ultrasonic testing of austenitic welds prepared by two different welding processes. The tests were carried out by the ultrasonic Time-of-Flight Diffraction (ToFD) technique. Shielded Metal Arc Welding (SMAW) and Gas Tungsten Arc Welding (GTAW) are the welding processes used for preparing the specimens. Identical artificial defects were implanted in both welds during the welding process. Both specimens were examined by the ToFD technique under similar conditions. Metallographic images were also obtained from the cross sectional plane of both the SMA and GTA welds. These images show that the grain orientation in the two welded specimens are different. D-scan images obtained by the ToFD technique from these welds indicates that inspecting the specimens prepared by the SMAW process is easier than the one made by the GTAW process. The results also show that the D-scan images cannot reveal the small vertical drilled holes implanted in the specimens. (author)

Comparative evaluation of maceration and ultrasonic-assisted extraction of phenolic compounds from fresh olives.

Science.gov (United States)

Deng, Junlin; Xu, Zhou; Xiang, Chunrong; Liu, Jing; Zhou, Lijun; Li, Tian; Yang, Zeshen; Ding, Chunbang

2017-07-01

Ultrasonic-assisted extraction (UAE) and maceration extraction (ME) were optimized using response surface methodology (RSM) for total phenolic compounds (TPC) from fresh olives. The main phenolic compounds and antioxidant activity of TPC were also investigated. The optimized result for UAE was 22mL/g of liquid-solid ratio, 47°C of extraction temperature and 30min of extraction time, 7.01mg/g of yielding, and for ME was 24mL/g of liquid-solid ratio, 50°C of extraction temperature and 4.7h of extraction time, 5.18mg/g of yielding. The HPLC analysis revealed that the extracts by UAE and ME possessed 14 main phenolic compounds, and UAE exhibited more amounts of all phenols than ME. The most abundant phenolic compounds in olive extracts were hydroxytyrosol, oleuropein and rutin. Both extracts showed excellent antioxidant activity in a dose-dependent manner. Taken together, UAE could effectively increase the yield of phenolic compounds from olives. In addition these phenolic compounds could be used as a potential source of natural antioxidants. Copyright © 2017 Elsevier B.V. All rights reserved.

Development of vertical drilling apparatus (Terra-Drill); Entwicklung eines Vertikal-Bohrgeraets (Terra-Drill) - Schlussbericht

Energy Technology Data Exchange (ETDEWEB)

Jenne, D.

2009-05-15

This well-illustrated final report for the Swiss Federal Office of Energy (SFOE) reports on the development of a vertical drilling apparatus named Terra-Drill. The various stages of the development of the apparatus, which is based on earlier designs, is discussed. New norms issued in Germany for the size of boreholes for buried vertical heat-exchangers and the appropriate linings to be used are discussed. The new Terra Drill 4407 V drilling apparatus and its testing are discussed. The drill is quoted as being particularly suitable for cramped locations. Technical details are presented and a comprehensive collection of photographs is included. Various preliminary reports and development documentation are included.

Modeling of ultrasonic processes utilizing a generic software framework

Science.gov (United States)

Bruns, P.; Twiefel, J.; Wallaschek, J.

2017-06-01

Modeling of ultrasonic processes is typically characterized by a high degree of complexity. Different domains and size scales must be regarded, so that it is rather difficult to build up a single detailed overall model. Developing partial models is a common approach to overcome this difficulty. In this paper a generic but simple software framework is presented which allows to coupe arbitrary partial models by slave modules with well-defined interfaces and a master module for coordination. Two examples are given to present the developed framework. The first one is the parameterization of a load model for ultrasonically-induced cavitation. The piezoelectric oscillator, its mounting, and the process load are described individually by partial models. These partial models then are coupled using the framework. The load model is composed of spring-damper-elements which are parameterized by experimental results. In the second example, the ideal mounting position for an oscillator utilized in ultrasonic assisted machining of stone is determined. Partial models for the ultrasonic oscillator, its mounting, the simplified contact process, and the workpiece’s material characteristics are presented. For both applications input and output variables are defined to meet the requirements of the framework’s interface.

Research towards ultrasonic systems to assist in-vessel manipulations in liquid metal cooled reactors

International Nuclear Information System (INIS)

Dierckx, Marc; Van-Dyck, Dries

2013-06-01

We describe the state of the art of the research towards ultrasonic measurement methods for use in lead-bismuth cooled liquid metal reactors. Our current research activities are highly focused on specific tasks in the MYRRHA system, which is a fast spectrum research reactor cooled with the eutectic mixture of lead and bismuth (LBE) and is conceived as an accelerator driven system capable of operating in both sub-critical and critical mode. As liquid metal is opaque to light, normal visual feedback during fuel manipulations in the reactor vessel is not available and must therefore be replaced by a system that is not hindered by the opacity of the coolant. In this respect ultrasonic measurement techniques have been proposed and even developed in the past for operation in sodium cooled reactors. To our knowledge, no such systems have ever been deployed in lead based reactors and we are the first to have a research program in this direction as will be detailed in this paper. We give an overview of the acoustic properties of LBE and compare them with the properties of sodium and water to theoretically show the feasibility of ultrasonic systems operating in LBE. In the second part of the paper we discuss the results of the validation experiments in water and LBE. A typical scene is ultrasonically probed by a mechanical scanning system while the signals are processed to render a 3D visualization on a computer screen. It will become clear that mechanical scanning is capable of producing acceptable images but that it is a time consuming process that is not fit to solve the initial task to providing feedback during manipulations in the reactor vessel. That is why we propose to use several dedicated ultrasonic systems each adapted to a specific task and capable to provide real-time feedback of the ongoing manipulations, as is detailed in the third and final part of the paper. (authors)

Drilling bits for deep drilling and process for their manufacture

Energy Technology Data Exchange (ETDEWEB)

Rhode, H.; Juergens, R.; Feenstra, R.; Busking, B.E.

1978-11-30

The invention concerns a drilling head or a drilling bit for use in deep drilling in underground formations and particularly concerns a drilling bit with a drilling bit body, which has a shank and a hollow space, which is connected with a duct extending through the shank. The drilling bit body has several separate cutting elements for removing material from the floor of a borehole and hydraulic devices for cooling and/or cleaning the cutting elements are provided.

Experimental Setup for Ultrasonic-Assisted Desktop Fused Deposition Modeling System

OpenAIRE

Maidin, S.; Muhamad, M. K.; Pei, Eujin

2014-01-01

Fused deposition modeling (FDM) is an additive manufacturing (AM) process that has been used in various manufacturing fields. However, the drawback of FDM is poor surface finish of part produced, leading to surface roughness and requires hand finishing. In this study, ultrasonic technology will be integrated into a desktop FDM system. Ultrasound has been applied in various conventional machining process and shows good machined surface finish. However, very little research regarding the applic...

Study on optimizing ultrasonic irradiation period for thick polycrystalline PZT film by hydrothermal method.

Science.gov (United States)

Ohta, Kanako; Isobe, Gaku; Bornmann, Peter; Hemsel, Tobias; Morita, Takeshi

2013-04-01

The hydrothermal method utilizes a solution-based chemical reaction to synthesize piezoelectric thin films and powders. This method has a number of advantages, such as low-temperature synthesis, and high purity and high quality of the product. In order to promote hydrothermal reactions, we developed an ultrasonic assisted hydrothermal method and confirmed that it produces dense and thick lead-zirconate-titanate (PZT) films. In the hydrothermal method, a crystal growth process follows the nucleation process. In this study, we verified that ultrasonic irradiation is effective for the nucleation process, and there is an optimum irradiation period to obtain thicker PZT films. With this optimization, a 9.2-μm-thick PZT polycrystalline film was obtained in a single deposition process. For this film, ultrasonic irradiation was carried out from the beginning of the reaction for 18 h, followed by a 6 h deposition without ultrasonic irradiation. These results indicate that the ultrasonic irradiation mainly promotes the nucleation process. Copyright © 2012 Elsevier B.V. All rights reserved.

Ultrasonic signature

International Nuclear Information System (INIS)

Borloo, E.; Crutzen, S.

1974-12-01

The unique and tamperproof identification technique developed at Ispra is based on ultrasonic Non-Destructive-Techniques. Reading fingerprints with ultrasonic requires high reproducibility of standard apparatus and transducers. The present report gives an exhaustive description of the ultrasonic technique developed for identification purposes. Different applications of the method are described

The use of drilling by the U.S. Antarctic program

Energy Technology Data Exchange (ETDEWEB)

Wade, M.C.; Webb, J.W.; Hedberg, W.H.

1994-08-01

This report on drilling in the Antarctic has been prepared by the U.S. National Science Foundation (NSF) to assist principal investigators and others in complying with the National Environmental Policy Act (NEPA) and the Antarctic Treaty of 1961. Implementing regulations for NEPA are spelled out in 40 CFR 1500-1508. Environmental protection under the Antarctic Treaty is addressed in the Protocol on Environmental Protection to the Antarctic Treaty (hereafter referred to as the Protocol), which was adopted by 26 countries in 1991. In the United States, responsibility for compliance with these requirements rests with the NSF Office of Polar Programs (OPP), which manages the U.S. Antarctic Program (USAP). The USAP recognizes the potentially profound impacts that its presence and activities can have on the antarctic environment. In its extensive support of operations and research in Antarctica, the USAP uses all practical means to foster and maintain natural conditions while supporting scientific endeavors in a safe and healthful manner. Reducing human impacts on the antarctic environment is a major goal of the USAP. The USAP`s operating philosophy is based on broad yet reasonable and practical assumptions concerning environmental protection. The USAP maintains three year-round stations on the continent to support scientific research. Research and associated support operations at these stations and camps sometimes involve drilling into ice, soil, or ocean sediments. In order to comply with NEPA and the Protocol, it is necessary for principal investigators and others to assess the environmental effects of drilling. This report has been prepared to assist in this process by describing various drilling technologies currently available for use in Antarctica, generally characterizing the potential environmental impacts associated with these drilling techniques, and identifying possible mitigation measures to reduce impacts.

NEW HIGH STRENGTH AND FASTER DRILLING TSP DIAMOND CUTTERS

Energy Technology Data Exchange (ETDEWEB)

Robert Radtke

2006-01-31

The manufacture of thermally stable diamond (TSP) cutters for drill bits used in petroleum drilling requires the brazing of two dissimilar materials--TSP diamond and tungsten carbide. The ENDURUS{trademark} thermally stable diamond cutter developed by Technology International, Inc. exhibits (1) high attachment (shear) strength, exceeding 345 MPa (50,000 psi), (2) TSP diamond impact strength increased by 36%, (3) prevents TSP fracture when drilling hard rock, and (4) maintains a sharp edge when drilling hard and abrasive rock. A novel microwave brazing (MWB) method for joining dissimilar materials has been developed. A conventional braze filler metal is combined with microwave heating which minimizes thermal residual stress between materials with dissimilar coefficients of thermal expansion. The process results in preferential heating of the lower thermal expansion diamond material, thus providing the ability to match the thermal expansion of the dissimilar material pair. Methods for brazing with both conventional and exothermic braze filler metals have been developed. Finite element modeling (FEM) assisted in the fabrication of TSP cutters controllable thermal residual stress and high shear attachment strength. Further, a unique cutter design for absorbing shock, the densification of otherwise porous TSP diamond for increased mechanical strength, and diamond ion implantation for increased diamond fracture resistance resulted in successful drill bit tests.

Ultrasound-assisted oxidative process for sulfur removal from petroleum product feedstock.

Science.gov (United States)

Mello, Paola de A; Duarte, Fábio A; Nunes, Matheus A G; Alencar, Mauricio S; Moreira, Elizabeth M; Korn, Mauro; Dressler, Valderi L; Flores, Erico M M

2009-08-01

A procedure using ultrasonic irradiation is proposed for sulfur removal of a petroleum product feedstock. The procedure involves the combination of a peroxyacid and ultrasound-assisted treatment in order to comply with the required sulfur content recommended by the current regulations for fuels. The ultrasound-assisted oxidative desulfurization (UAOD) process was applied to a petroleum product feedstock using dibenzothiophene as a model sulfur compound. The influence of ultrasonic irradiation time, oxidizing reagents amount, kind of solvent for the extraction step and kind of organic acid were investigated. The use of ultrasonic irradiation allowed higher efficiency for sulfur removal in comparison to experiments performed without its application, under the same reactional conditions. Using the optimized conditions for UAOD, the sulfur removal was about 95% after 9min of ultrasonic irradiation (20kHz, 750W, run at 40%), using hydrogen peroxide and acetic acid, followed by extraction with methanol.

Cavitation occurrence around ultrasonic dental scalers

OpenAIRE

Felver, Bernhard; King, David C; Lea, Simon C; Price, Gareth J; Damien Walmsley, A

2009-01-01

Ultrasonic scalers are used in dentistry to remove calculus and other contaminants from teeth. One mechanism which may assist in the cleaning is cavitation generated in cooling water around the scaler. The vibratory motion of three designs of scaler tip in a water bath has been characterised by laser vibrometry, and compared with the spatial distribution of cavitation around the scaler tips observed using sonochemiluminescence from a luminol solution. The type of cavitation was confirmed by a...

Ultrasonic boiler inspection and economic analysis guidelines

International Nuclear Information System (INIS)

Anon.

1987-01-01

Boiler tube failures cause approximately 6% availability loss of large fossil-fired power generating plants. This loss can be reduced by systematic approaches using ultrasonic examination and root cause failure analysis methods. Two projects sponsored by EPRI have provided utility engineers with guidelines for performing ultrasonic examinations and with details on 22 types of tube failure mechanisms. A manual has been published that provides descriptions of typical locations, superficial appearances, damage mechanisms, metallurgy, microstructural changes, likely root causes, and potential corrective actions. Application of the principles in the manual is being demonstrated in an EPRI-funded project at 10 electric utilities over the next two years. Guidelines have been published that prescribe the activities necessary for ultrasonic examinations of boiler tubes. Eight essential elements of a boiler examination should be performed to assure that possible economic benefits are obtained. Work was supported by EPRI under RP 1890 and RP 1865. A software package has been developed for effectively planning inspections for wall thinning in fossil-fired boiler tubing. The software assists in minimizing costs associated with maintenance, such as inspection and repair, while the life of the boiler is maximized

A Reuse Evaluation for Solar-Cell Silicon Wafers via Shift Revolution and Tool Rotation Using Magnetic Assistance in Ultrasonic Electrochemical Micromachining

Directory of Open Access Journals (Sweden)

P. S. Pa

2013-01-01

Full Text Available A new reuse fabrication using a tool module with rotation and revolution through a process of magnetic assistance in ultrasonic electrochemical micromachining (UEMM for removal of the surface layers from silicon wafers of solar cells is demonstrated. The target of the proposed reuse fabrication method is to replace the current approach, which uses strong acid and grinding and may damage the physical structure of silicon wafers and pollute to the environment. A precisely engineered clean production approach to removal of surface microstructure layers from silicon wafers is to develop a mass production system for recycling defective or discarded silicon wafers of solar cells that can reduce pollution and cost. The high revolution speed of the shift with the high rotation speed of the designed tool increases the discharge mobility and improves the removal effect associated with the high feed rate of the workpiece. High frequency and high power of ultrasonic with large electrolyte flow rate and high magnetic strengths with a small distance between the two magnets provide a large discharge effect and good removal; only a short period of time is required to remove the epoxy film and Si3N4 layer easily and cleanly.

Rapid determination of volatile constituents in safflower from Xinjiang and Henan by ultrasonic-assisted solvent extraction and GC–MS

Directory of Open Access Journals (Sweden)

Ling-Han Jia

2011-08-01

Full Text Available The total volatile components were extracted from safflower by ultrasonic-assisted solvent extraction (USE and their chemical constituents were analyzed by gas chromatography–mass spectrometry (GC–MS to provide scientific basis for the quality control of safflower. Five different solvents (diethyl ether, ethanol, ethyl acetate, dichloromethane and acetone were used and compared in terms of number of volatile components extracted and the peak areas of these components in TIC. The results showed that USE could be used as an efficient and rapid method for extracting the volatile components from safflower. It also could be found that the number of components in the TIC of ethyl acetate extract was more than that in the TIC of other solvent ones. Meanwhile, the volatile components of safflower from Xinjiang Autonomous Region and Henan Province of China were different in chemical components and relative contents. It could be concluded that both the extraction solvents and geographical origin of safflower are responsible for these differences. The experimental results also indicated that USE/GC–MS is a simple, rapid and effective method to analyze the volatile oil components of safflower. Keywords: Safflower, Ultrasonic solvent extraction, Gas chromatography–mass spectrometry (GC–MS

CuY zeolite catalysts prepared by ultrasonication-assisted ion-exchange for oxidative carbonylation of methanol to dimethyl carbonate.

Science.gov (United States)

Woo, Je-Min; Seo, Jung Yoon; Kim, Hyunuk; Lee, Dong-Ho; Park, Young Cheol; Yi, Chang-Keun; Park, Yeong Seong; Moon, Jong-Ho

2018-06-01

The influence of ultrasonication treatment on the catalytic performance of CuY zeolite catalysts was investigated for the liquid-phase oxidative carbonylation of methanol to dimethyl carbonate (DMC). The deammoniation method of NH 4 Y into HY zeolites was optimized and characterized by elemental analyzer, derivative thermogravimetry, Brunauer-Emmett-Teller (BET) analyzer, and powder X-ray diffractometry, revealing that the HY zeolite deammoniated at 400 °C presented the highest surface area, complete ammonium/proton ion exchange, and no structure collapse, rendering it the best support from all the prepared zeolites. CuY zeolites were prepared via aqueous phase ion exchange with the aid of ultrasonication. Upon ultrasonication, the Cu + active centers were uniformly dispersed in the Y zeolites, penetrating the core of the zeolite particles in a very short time. In addition to enhancing the Cu dispersity, the ultrasonication treatment influenced the BET surface area, acid amount, Cu + /Cu 2+ ratio, and also had a relatively small impact on the Cu loading. Consequently, adequate exposure to ultrasonication was able to increase the conversion rate of methanol into dimethyl carbonate up to 11.4% with a comparable DMC selectivity of 23.7%. This methanol conversion is 2.65 times higher than that obtained without the ultrasonication treatment. Copyright © 2018 Elsevier B.V. All rights reserved.

An Experimental Investigation of Cutting Temperature and Tool Wear in 2 Dimensional Ultrasonic Vibrations Assisted Micro-Milling

Directory of Open Access Journals (Sweden)

Ibrahim Mohd Rasidi

2017-01-01

Full Text Available Two dimensional Ultrasonic vibration assisted milling (2D UVAM well knows process that involved in high tech system to generate ultra range of frequency applied to the milling process. More industries nowadays become aware taking this opportunity to improve their productivity without decreasing their product accuracies. This paper investigate a comparative machining between UVAM and conventional machining (CM in tool wear and cutting temperature in milling process. Micro amplitude and sine wave frequency will be generate into the workpiece jig by piezo-actuator. Thus, creating a micro gap that allow heat remove effectively with the chip produces. A more complex tool trajectory mechanics of 2D UVAM has been found during this research. The approaching the tool tip into the workpiece surfaces is affected by the amplitude displacement along the frequency applied. It is found that the tool wear was reduce and surface roughness improvement by applying the 2D UVAM compared to the CM when choosing the optimum amplitude and appropriate frequency.

The Effect of Nano Loading and Ultrasonic Compounding of EVA/LDPE/Nano-magnesium Hydroxide on Mechanical Properties and Distribution of Nano Particles

Science.gov (United States)

Azman, I. A.; Salleh, R. M.; Alauddin, S. M.; Shueb, M. I.

2018-05-01

Blends of Ethylene Vinyl Acetate (EVA) and Low-Density Polyethylene (LDPE) are promising composite which have good mechanical properties to environmental stress cracking. However, they lack fire resistant properties, which limits it usage in wire and cable industry. In order to improve flame retardancy ability, a range of nano-magnesium hydroxide (nano-MH) loading which is from 0 phr to maximum of 20 phr with ultrasonic extrusion 0-100 kHz frequencies have been introduced. Ultrasonic extrusion was used to improve the distribution of nano-MH. It was found that, 10 phr of nano loading with 100 kHz ultrasonic assisted has greater tensile strength compared to the nanocomposite without ultrasonication. Further increase of nano MH loading, will decrease the tensile properties. Better elongation at break was observed at10 phr nano-MH with the frequency of 50 kHz. The sample of 20 phr of nanoMH assisted with 50 kHz ultrasonic exhibits good flexural properties while 10 phr of nano-MH without the ultrasonic assisted demonstrates good in izod impact properties. From the evaluation of mechanical properties studied, it was found that 10 phr of nano-MH has shown the best performance among all the samples tested for EVA/LDPE/nano-MH composites. Transmission Electron Microscopy (TEM) has been conducted on 10 phr sample with different frequencies in order to observe the distribution of nano-MH particles. The sample with 100 kHz frequency shows more uniform dispersion of nano-MH in EVA/LDPE composites. This investigation indicates that the ultrasonic technology can enhance the mechanical properties studied as well as the dispersion of nano particles in the composite.

Ultrasonic horn design for ultrasonic machining technologies

Directory of Open Access Journals (Sweden)

Naď M.

2010-07-01

Full Text Available Many of industrial applications and production technologies are based on the application of ultrasound. In many cases, the phenomenon of ultrasound is also applied in technological processes of the machining of materials. The main element of equipments that use the effects of ultrasound for machining technology is the ultrasonic horn – so called sonotrode. The performance of ultrasonic equipment, respectively ultrasonic machining technologies depends on properly designed of sonotrode shape. The dynamical properties of different geometrical shapes of ultrasonic horns are presented in this paper. Dependence of fundamental modal properties (natural frequencies, mode shapes of various sonotrode shapes for various geometrical parameters is analyzed. Modal analyses of the models are determined by the numerical simulation using finite element method (FEM design procedures. The mutual comparisons of the comparable parameters of the various sonotrode shapes are presented.

Applications of Flexible Ultrasonic Transducer Array for Defect Detection at 150 °C

Directory of Open Access Journals (Sweden)

Jiunn-Woei Liaw

2013-01-01

Full Text Available In this study, the feasibility of using a one dimensional 16-element flexible ultrasonic transducer (FUT array for nondestructive testing at 150 °C is demonstrated. The FUT arrays were made by a sol-gel sprayed piezoelectric film technology; a PZT composite film was sprayed on a titanium foil of 75 µm thickness. Since the FUT array is flexible, it was attached to a steel pipe with an outer diameter of 89 mm and a wall thickness of 6.5 mm at 150 °C. Using the ultrasonic pulse-echo mode, pipe thickness measurements could be performed. Moreover, using the ultrasonic pulse-echo and pitch-catch modes of each element of FUT array, the defect detection was performed on an Al alloy block of 30 mm thickness with a side-drilled hole (SDH of f3 mm at 150 °C. In addition, a post-processing algorithm based on the total focusing method was used to process the full matrix of these A-scan signals of each single transmitter and multi-receivers, and then the phase-array image was obtained to indicate this defect- SDH. Both results show the capability of FUT array being operated at 150 °C for the corrosion and defect detections.

CASING DRILLING TECHNOLOGY

Directory of Open Access Journals (Sweden)

Nediljka Gaurina-Međimurec

2005-12-01

Full Text Available Casing drilling is an alternative option to conventional drilling and uses standard oilfield casing instead of drillstring. This technology is one of the greatest developments in drilling operations. Casing drilling involves drilling and casing a well simultaneously. In casing driling process, downhole tools can be retrieved, through the casing on wire-line, meaning tool recovery or replacement of tools can take minutes versus hours under conventional methods. This process employs wireline-retrievable tools and a drill-lock assembly, permitting bit and BHA changes, coring, electrical logging and even directional or horizontal drilling. Once the casing point is reached, the casing is cemented in place without tripping pipe.

HIGH-POWER TURBODRILL AND DRILL BIT FOR DRILLING WITH COILED TUBING

Energy Technology Data Exchange (ETDEWEB)

Robert Radtke; David Glowka; Man Mohan Rai; David Conroy; Tim Beaton; Rocky Seale; Joseph Hanna; Smith Neyrfor; Homer Robertson

2008-03-31

Commercial introduction of Microhole Technology to the gas and oil drilling industry requires an effective downhole drive mechanism which operates efficiently at relatively high RPM and low bit weight for delivering efficient power to the special high RPM drill bit for ensuring both high penetration rate and long bit life. This project entails developing and testing a more efficient 2-7/8 in. diameter Turbodrill and a novel 4-1/8 in. diameter drill bit for drilling with coiled tubing. The high-power Turbodrill were developed to deliver efficient power, and the more durable drill bit employed high-temperature cutters that can more effectively drill hard and abrasive rock. This project teams Schlumberger Smith Neyrfor and Smith Bits, and NASA AMES Research Center with Technology International, Inc (TII), to deliver a downhole, hydraulically-driven power unit, matched with a custom drill bit designed to drill 4-1/8 in. boreholes with a purpose-built coiled tubing rig. The U.S. Department of Energy National Energy Technology Laboratory has funded Technology International Inc. Houston, Texas to develop a higher power Turbodrill and drill bit for use in drilling with a coiled tubing unit. This project entails developing and testing an effective downhole drive mechanism and a novel drill bit for drilling 'microholes' with coiled tubing. The new higher power Turbodrill is shorter, delivers power more efficiently, operates at relatively high revolutions per minute, and requires low weight on bit. The more durable thermally stable diamond drill bit employs high-temperature TSP (thermally stable) diamond cutters that can more effectively drill hard and abrasive rock. Expectations are that widespread adoption of microhole technology could spawn a wave of 'infill development' drilling of wells spaced between existing wells, which could tap potentially billions of barrels of bypassed oil at shallow depths in mature producing areas. At the same time, microhole

A novel preparation method for drug nanocrystals and characterization by ultrasonic spray assisted electrostatic adsorption

Directory of Open Access Journals (Sweden)

Gao B

2013-10-01

Full Text Available Bing Gao,1–3 Jun Wang,2 Dunju Wang,1,2 Ziqiang Zhu,1,2 Zhiqiang Qiao,2 Guangcheng Yang,2 Fude Nie21School of Material Science and Engineering, Southwest University of Science and Technology, Mianyang, People's Republic of China, 2Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang, Sichuan, People's Republic of China, 3Si Chuan Research Center of New Materials, Mianyang, People's Republic of ChinaPurpose: The purpose of this study was to develop a novel and continuous method for preparing a nanosized particle of drug crystals and to characterize its properties.Materials and methods: A new apparatus was introduced to crystallize nanosized drug crystals of amitriptyline hydrochloride as a model drug. The samples were prepared in the pure state by ultrasonic spray, and elaborated deposition was completed via electrostatic adsorption. Scanning electron microscopy, X-ray powder diffraction, and atomic force microscopy were used to characterize the size of the particles; this was subsequently followed by differential scanning calorimetry.Results and discussion: Nanoparticles of drug crystals were successfully prepared. The size of the drug crystals ranged from 20 nm to 400 nm; the particle size of amitriptyline hydrochloride was approximately 71 nm. The particles were spherical and rectangular in shape. Moreover, the melting point of the nanoparticles decreased from 198.2°C to 196.3°C when compared to raw particle crystals. Furthermore, the agglomeration effect was also attenuated as a result of electrostatic repulsion among each particle when absorbed, and depositing on the inner wall of the gathering unit occurred under the electrostatic effect.Conclusion: Ultrasonic spray-assisted electrostatic adsorption is a very effective and continuous method to produce drug nanocrystals. This method can be applied to poorly water-soluble drugs, and it can also be a very effective alternative for industrial production. Once the

Drilling unit

Energy Technology Data Exchange (ETDEWEB)

Umanchik, N P; Demin, A V; Khrustalev, N N; Linnik, G N; Lovchev, S V; Rozin, M M; Sidorov, R V; Sokolov, S I; Tsaregradskiy, Yu P

1981-01-01

A drilling unit is proposed which includes a hydraulic lifter, hydraulic multiple-cylinder pump with valve distribution and sectional drilling pump with separators of the working and flushing fluid. In order to reduce metal consumption and the overall dimensions of the drilling unit, the working cavity of each cylinder of the hydraulic multiple-cylinder pump is equipped with suction and injection valves and is hydraulically connected to the working cavity by one of the sections of the drilling pump.

Air-coupled method to investigate the lowest-order antisymmetric Lamb mode in stubbed and air-drilled phononic plates

Energy Technology Data Exchange (ETDEWEB)

Zhang, Dongbo; Zhao, Jinfeng, E-mail: jinfeng.zhao@tongji.edu.cn; Li, Libing; Pan, Yongdong; Zhong, Zheng [School of Aerospace Engineering and Applied Mechanics, Tongji University, 100 Zhangwu Road, 200092, Shanghai (China); Bonello, Bernard [CNRS, UMR 7588, Institut des NanoSciences de Paris, F-75005, Paris (France); Wei, Jianxin [State Key Laboratory of Petroleum Resources and Prospecting, China University of Petroleum, 18 Xuefu Road, 102249, Pekin (China)

2016-08-15

In this work, we applied a robust and fully air-coupled method to investigate the propagation of the lowest-order antisymmetric Lamb (A{sub 0}) mode in both a stubbed and an air-drilled phononic-crystal (PC) plate. By measuring simply the radiative acoustic waves of A{sub 0} mode close to the plate surface, we observed the band gaps for the stubbed PC plate caused by either the local resonance or the Bragg scattering, in frequency ranges in good agreement with theoretical predictions. We measured then the complete band gap of A{sub 0} mode for the air-drilled PC plate, in good agreement with the band structures. Finally, we compared the measurements made using the air-coupled method with those obtained by the laser ultrasonic technique.

Air-coupled method to investigate the lowest-order antisymmetric Lamb mode in stubbed and air-drilled phononic plates

Directory of Open Access Journals (Sweden)

Dongbo Zhang

2016-08-01

Full Text Available In this work, we applied a robust and fully air-coupled method to investigate the propagation of the lowest-order antisymmetric Lamb (A0 mode in both a stubbed and an air-drilled phononic-crystal (PC plate. By measuring simply the radiative acoustic waves of A0 mode close to the plate surface, we observed the band gaps for the stubbed PC plate caused by either the local resonance or the Bragg scattering, in frequency ranges in good agreement with theoretical predictions. We measured then the complete band gap of A0 mode for the air-drilled PC plate, in good agreement with the band structures. Finally, we compared the measurements made using the air-coupled method with those obtained by the laser ultrasonic technique.

An Investigation of Finite Element Analysis (FEA on Piezoelectric Compliance in Ultrasonic Vibration Assisted Milling (UVAM

Directory of Open Access Journals (Sweden)

Ibrahim Rasidi

2018-01-01

Full Text Available Finite element analysis for piezoelectric actuator has been developed in Ansys Software which are a program that can analyses and simulate the dynamic behaviour of piezoelectric. The Ultrasonic Vibration assisted Milling (UVAM experimental having a difficulty to investigate the effect of vibration mechanism where existence of error in material, mechanism and attachment of piezoelectric thus affect the amplitude and frequency of mechanical compliance during the machining of UVAM. This paper will investigate the modelling of piezoelectric compliance and follow the procedures of FEA to accurately predict the dynamic behaviour of compliance. The parameters for simulation of piezoelectric are voltage, electromechanical coupling and frequency. The compliance mechanism is model by using SolidWorks 2014 and imported to Ansys Mechanical APDL Software were the piezoelectric are embedded on the mechanism. Modal analysis and harmonic analysis has been used in order to obtain the mode shape and displacement. The displacement of the compliance mechanism will be compare between simulation and experimental. The dynamic behaviour was discussed in simulation to study the reliability of the compliance mechanism before it safely used in UVAM.

Transparent nanostructured Fe-doped TiO2 thin films prepared by ultrasonic assisted spray pyrolysis technique

Science.gov (United States)

Rasoulnezhad, Hossein; Hosseinzadeh, Ghader; Ghasemian, Naser; Hosseinzadeh, Reza; Homayoun Keihan, Amir

2018-05-01

Nanostructured TiO2 and Fe-doped TiO2 thin films with high transparency were deposited on glass substrate through ultrasonic-assisted spray pyrolysis technique and were used in the visible light photocatalytic degradation of MB dye. The resulting thin films were characterized by scanning electron microscopy (SEM), Raman spectroscopy, photoluminescence spectroscopy, x-ray diffraction (XRD), and UV-visible absorption spectroscopy techniques. Based on Raman spectroscopy results, both of the TiO2 and Fe-doped TiO2 films have anatase crystal structure, however, because of the insertion of Fe in the structure of TiO2 some point defects and oxygen vacancies are formed in the Fe-doped TiO2 thin film. Presence of Fe in the structure of TiO2 decreases the band gap energy of TiO2 and also reduces the electron–hole recombination rate. Decreasing of the electron–hole recombination rate and band gap energy result in the enhancement of the visible light photocatalytic activity of the Fe-doped TiO2 thin film.

Ultrasonically enhanced extraction of bioactive principles from Quillaja Saponaria Molina.

Science.gov (United States)

Gaete-Garretón, L; Vargas-Hernández, Yolanda; Cares-Pacheco, María G; Sainz, Javier; Alarcón, John

2011-07-01

A study of ultrasonic enhancement in the extraction of bioactive principles from Quillaja Saponaria Molina (Quillay) is presented. The effects influencing the extraction process were studied through a two-level factorial design. The effects considered in the experimental design were: granulometry, extraction time, acoustic Power, raw matter/solvent ratio (concentration) and acoustic impedance. It was found that for aqueous extraction the main factors affecting the ultrasonically-assisted process were: granulometry, raw matter/solvent ratio and extraction time. The extraction ratio was increased by Ultrasonics effect and a reduction in extraction time was verified without any influence in the product quality. In addition the process can be carried out at lower temperatures than the conventional method. As the process developed uses chips from the branches of trees, and not only the bark, this research contributes to make the saponin exploitation process a sustainable industry. Copyright © 2010 Elsevier B.V. All rights reserved.

Optimisation of ultrasonic-assisted extraction of phenolic compounds, antioxidants, and anthocyanins from sugar beet molasses.

Science.gov (United States)

Chen, Mingshun; Zhao, Yi; Yu, Shujuan

2015-04-01

Response surface methodology was used to optimise experimental conditions for ultrasonic-assisted extraction (UAE) of functional components from sugar beet molasses. The central composite design (CCD) was used for the optimisation of extraction parameters in terms of total phenolic contents, antioxidant activities and anthocyanins. Result suggested the optimal conditions obtained by RSM for UAE from sugar beet molasses were as follows: HCl concentration 1.55-1.72 mol/L, ethanol concentration 57-63% (v/v), extraction temperature 41-48 °C, and extraction time 66-73 min. In the optimal conditions, the experimental total phenolic contents were 17.36 mg GAE/100mL, antioxidant activity was 16.66 mg TE/g, and total anthocyanins were 31.81 mg/100g of the sugar beet molasses extract, which were well matched the predicted values. Teen compounds, i.e. gallic acid, vanillin, hydroxybenzoic acid, syringic acid, cyanidin-3-O-rutinoside, cyanidin-3-O-glucoside, catechin, delphinidin-3-O-rutinoside, delphinidin-3-O-glucuronide and ferulic acid were determined by HPLC-DAD-MS/MS in sugar beet molasses. Copyright © 2014 Elsevier Ltd. All rights reserved.

Improved dental implant drill durability and performance using heat and wear resistant protective coatings.

Science.gov (United States)

Er, Nilay; Alkan, Alper; İlday, Serim; Bengu, Erman

2018-03-02

Dental implant drilling procedure is an essential step for implant surgery and frictional heat appeared in bone during drilling is a key factor affecting the success of an implant. The aim of this study is to increase the dental implant drill lifetime and performance using heat- and wear-resistant protective coatings hence to decrease the alveolar bone temperature caused by the dental implant drilling procedure. Commercially obtained stainless steel drills were coated with titanium aluminum nitride, diamond-like carbon, titanium boron nitride, and boron nitride coatings via magnetron-sputter deposition. Drilling procedure was performed on a bovine femoral cortical bone under the conditions mimicking clinical practice, where the tests were performed both under water-assisted cooling and under the conditions without any cooling was applied. Coated drill performances and durabilities were compared to that of three commonly used commercial drills which surfaces are made from namely; zirconia, black diamond and stainless steel. Protective coatings with boron nitride, titanium boron nitride and diamond-like carbon have significantly improved drill performance and durability. Especially boron nitride-coated drills have performed within safe bone temperature limits for 50 drillings even without any cooling is applied. Titanium aluminium nitride coated drills did not show any improvement over commercially obtained stainless steel drills. Surface modification using heat and wear resistant coatings is an easy and highly effective way to improve implant drill performance and durability, which can reflect positively on surgical procedure and healing period afterwards. The noteworthy success of different types of coatings is novel and likely to be applicable to various other medical systems.

Enhancement of submarine pressure hull steel ultrasonic inspection using imaging and artificial intelligence

Science.gov (United States)

Hay, D. Robert; Brassard, Michel; Matthews, James R.; Garneau, Stephane; Morchat, Richard

1995-06-01

The convergence of a number of contemporary technologies with increasing demands for improvements in inspection capabilities in maritime applications has created new opportunities for ultrasonic inspection. An automated ultrasonic inspection and data collection system APHIUS (automated pressure hull intelligent ultrasonic system), incorporates hardware and software developments to meet specific requirements for the maritime vessels, in particular, submarines in the Canadian Navy. Housed within a hardened portable computer chassis, instrumentation for digital ultrasonic data acquisition and transducer position measurement provide new capabilities that meet more demanding requirements for inspection of the aging submarine fleet. Digital data acquisition enables a number of new important capabilites including archiving of the complete inspection session, interpretation assistance through imaging, and automated interpretation using artificial intelligence methods. With this new reliable inspection system, in conjunction with a complementary study of the significance of real defect type and location, comprehensive new criteria can be generated which will eliminate unnecessary defect removal. As a consequence, cost savings will be realized through shortened submarine refit schedules.

Treatment of tanneries waste water by ultrasound assisted electrolysis process

International Nuclear Information System (INIS)

Farooq, R.; Ahmed, Z.; Gilani, M. A.; Durrani, M.; Mahmood, Q.; Shaukat, S. F.; Choima, N.

2013-01-01

The leather industry is a major producer of wastewater and solid waste containing potential water and soil contaminants. Considering the large amount and variety of chemical agents used in skin processing, the wastewaters generated by tanneries are very complex. Therefore, the development of treatment methods for these effluents is extremely necessary. In this work the electrochemical treatment of a tannery wastewater by ultrasound assisted electrochemical process, using stainless steel and lead cathode and titanium anodes was studied. Effect of ultrasound irradiation at various ultrasonic intensities 0, 40, 60 and 80% on electrochemical removal of chromium was investigated. Experiments were conducted at two pH conditions of pH 3 and 9. Significant removal of chromium was found at pH 3 and it was also noticed that by increasing ultrasonic intensities, percentage removal of chromium and sulfate also increases. The optimum removal of chromium and sulfate ions was observed at 80% ultrasonic intensity. The technique of electrolysis assisted with ultrasonic waves can be further improved and can be the future waste water treatment process for industries. (author)

Effect of Electropulsing-Assisted Ultrasonic Nanocrystalline Surface Modification on the Surface Mechanical Properties and Microstructure of Ti-6Al-4V Alloy

Science.gov (United States)

Ye, Yongda; Wang, Haibo; Tang, Guoyi; Song, Guolin

2018-05-01

The effect of electropulsing-assisted ultrasonic nanocrystalline surface modification (EP-UNSM) on surface mechanical properties and microstructure of Ti-6Al-4V alloy is investigated. Compared to conventional ultrasonic nanocrystalline surface modification (UNSM), EP-UNSM can effectively facilitate surface roughness and morphology, leading to excellent surface roughness (reduced from Ra 0.918 to Ra 0.028 μm by UNSM and Ra 0.019 μm by EP-UNSM) and smoother morphology with less cracks and defects. Surface friction coefficients are enhanced, resulting in lower and smoother friction coefficients. In addition, the surface-strengthened layer and ultra-refined grains are significantly enhanced with more severe plastic deformation and a greater surface hardness (a maximum hardness value of 407 HV and an effective depth of 550 μm, in comparison with the maximum hardness value of 364 HV and effective depth of 300 μm obtained by conventional UNSM). Remarkable enhancement of surface mechanical properties can be attributed to the refined gradient microstructure and the enhanced severe plastic deformation layer induced by coupling the effects of UNSM and electropulsing. The accelerated dislocation mobility and atom diffusion caused by the thermal and athermal effects of electropulsing treatment may be the primary intrinsic reasons for these improvements.

Parameter analysis on the ultrasonic TSV-filling process and electrochemical characters

Science.gov (United States)

Wang, Fuliang; Ren, Xinyu; Wang, Yan; Zeng, Peng; Zhou, Zhaohua; Xiao, Hongbin; Zhu, Wenhui

2017-10-01

As one of the key technologies in 3D packaging, through silicon via (TSV) interconnection technology has become a focus recently. In this paper, an electrodeposition method for TSV filling with the assistance of ultrasound and additives are introduced. Two important parameters i.e. current density and ultrasonic power are studied for TSV filling process and electrochemical properties. It is found that ultrasound can improve the quality of TSV-filling and change the TSV-filling mode. The experimental results also indicate that the filling rate enhances more significantly with decreasing current density under ultrasonic conditions than under silent conditions. In addition, according to the voltammetry curve, the increase of ultrasonic power can significantly increase the current density of cupric reduction, and decrease the thickness of diffusion layer. So that the reduction speed of copper ions is accelerated, resulting in a higher TSV-filling rate.

Ultrasonic inspection

International Nuclear Information System (INIS)

Satittada, Gannaga

1984-01-01

Ultrasonic inspection is one of the most widely used methods for nondestructive inspection. The beam of high-frequency sound wave, ultrasonic wave, is introduced into the material. It travels through the material with some attendant loss of energy and can be reflected at interfaces. The reflected beam is detected and analyzed. Ultrasonic inspection is used to detect flaws in metal parts as well as in welded, brazed and bonded joints during research work and developing production and service. It is also used to detect and locate porosity, pipe, and flakes. In addition, it can be used for the measurement of metal thickness. Ultrasonic inspection is therefore used for quality control and material inspection in all major industries

A new drilling method-Earthworm-like vibration drilling.

Science.gov (United States)

Wang, Peng; Ni, Hongjian; Wang, Ruihe

2018-01-01

The load transfer difficulty caused by borehole wall friction severely limits the penetration rate and extended-reach limit of complex structural wells. A new friction reduction technology termed "earthworm-like drilling" is proposed in this paper to improve the load transfer of complex structural wells. A mathematical model based on a "soft-string" model is developed and solved. The results show that earthworm-like drilling is more effective than single-point vibration drilling. The amplitude and frequency of the pulse pressure and the installation position of the shakers have a substantial impact on friction reduction and load transfer. An optimization model based on the projection gradient method is developed and used to optimize the position of three shakers in a horizontal well. The results verify the feasibility and advantages of earthworm-like drilling, and establish a solid theoretical foundation for its application in oil field drilling.

Some aspects of finite element modelling of ultrasonically aided micro-EDM of CoCr alloys

Directory of Open Access Journals (Sweden)

Ghiculescu Daniel

2017-01-01

Full Text Available The paper deals with finite element modelling of micromachining CoCr alloys by ultrasonically aided electrical discharge machining. This hybrid machining process has two components: a thermal one due to EDM, and a mechanical one to ultrasonic assistance. Both components were modelled using Thermal and Structural Mechanics time dependent modules of Comsol Multiphysics. The results were compared with the experimental data obtained in our laboratories, proving a good agreement and offering some solutions for machining optimization.

Ceria nanocubic-ultrasonication assisted dispersive liquid-liquid microextraction coupled with matrix assisted laser desorption/ionization mass spectrometry for pathogenic bacteria analysis.

Science.gov (United States)

Abdelhamid, Hani Nasser; Bhaisare, Mukesh L; Wu, Hui-Fen

2014-03-01

A new ceria (CeO2) nanocubic modified surfactant is used as the basis of a novel nano-based microextraction technique for highly sensitive detection of pathogenic bacteria (Pseudomonas aeruginosa and Staphylococcus aureus). The technique uses ultrasound enhanced surfactant-assisted dispersive liquid-liquid microextraction (UESA-DLLME) with and without ceria (CeO2) followed by matrix assisted laser desorption/ionization mass spectrometry (MALDI-MS). In order to achieve high separation efficiency, we investigated the influential parameters, including extraction time of ultrasonication, type and volume of the extraction solvent and surfactant. Among various surfactants, the cationic surfactants can selectively offer better extraction efficiency on bacteria analysis than that of the anionic surfactants due to the negative charges of bacteria cell membranes. Extractions of the bacteria lysate from aqueous samples via UESA-DLLME-MALDI-MS were successfully achieved by using cetyltrimethyl ammonium bromide (CTAB, 10.0 µL, 1.0×10(-3) M) as surfactants in chlorobenzene (10.0 µL) and chloroform (10.0 µL) as the optimal extracting solvent for P. aeruginosa and S. aureus, respectively. Ceria nanocubic was synthesized, and functionalized with CTAB (CeO2@CTAB) and then characterized using transmission electron microscopy (TEM) and optical spectroscopy (UV and FTIR). CeO2@CTAB demonstrates high extraction efficiency, improve peaks ionization, and enhance resolution. The prime reasons for these improvements are due to the large surface area of nanoparticles, and its absorption that coincides with the wavelength of MALDI laser (337 nm, N2 laser). CeO2@CTAB-based microextraction offers lowest detectable concentrations tenfold lower than that of without nanoceria. The present approach has been successfully applied to detect pathogenic bacteria at low concentrations of 10(4)-10(5) cfu/mL (without ceria) and at 10(3)-10(4) cfu/mL (with ceria) from bacteria suspensions. Finally, the

Drilling reorganizes

Science.gov (United States)

Richman, Barbara T.

As the first in a proposed series of steps that would move scientific ocean drilling from its own niche within the National Science Foundation's (NSF) Directorate for Astronomical, Atmospheric, Earth, and Ocean Sciences (AAEO) into the agency's Division of Ocean Sciences, Grant Gross, division director, has been appointed acting director of the Office of Scientific Ocean Drilling (OSOD). Gross will retain the directorship of the division, which also is part of AAEO. Allen M. Shinn, Jr., OSOD director for nearly 2 years, has been reassigned effective July 10 to a position in NSF's Office of Planning and Resource Management.The move aims to tie drilling operations more closely to the science with which it is associated, Gross said. This first step is an organizational response to the current leaning toward using a commercial drilling vessel as the drilling platform, he said. Before the market for such commercial drill ships opened (Eos, February 22, 1983, p . 73), other ship options for scientific ocean drilling included refurbishing the aging Glomar Challenger or renovating, at great expense, the Glomar Explorer. A possible next step in the reorganization is to make OSOD the third section within the Ocean Sciences Division. Currently, the division is divided into the Oceanographic Facilities and Support Section and the Ocean Sciences Research Section.

New method to enhance the extraction yield of rutin from Sophora japonica using a novel ultrasonic extraction system by determining optimum ultrasonic frequency.

Science.gov (United States)

Liao, Jianqing; Qu, Baida; Liu, Da; Zheng, Naiqin

2015-11-01

A new method has been proposed for enhancing extraction yield of rutin from Sophora japonica, in which a novel ultrasonic extraction system has been developed to perform the determination of optimum ultrasonic frequency by a two-step procedure. This study has systematically investigated the influence of a continuous frequency range of 20-92 kHz on rutin yields. The effects of different operating conditions on rutin yields have also been studied in detail such as solvent concentration, solvent to solid ratio, ultrasound power, temperature and particle size. A higher extraction yield was obtained at the ultrasonic frequency of 60-62 kHz which was little affected under other extraction conditions. Comparative studies between existing methods and the present method were done to verify the effectiveness of this method. Results indicated that the new extraction method gave a higher extraction yield compared with existing ultrasound-assisted extraction (UAE) and soxhlet extraction (SE). Thus, the potential use of this method may be promising for extraction of natural materials on an industrial scale in the future. Copyright © 2015 Elsevier B.V. All rights reserved.

Effects of a Short Drilling Implant Protocol on Osteotomy Site Temperature and Drill Torque.

Science.gov (United States)

Mihali, Sorin G; Canjau, Silvana; Cernescu, Anghel; Bortun, Cristina M; Wang, Hom-Lay; Bratu, Emanuel

2018-02-01

To establish a protocol for reducing the drilling sequence during implant site preparation based on temperature and insertion torque. The traditional conventional drilling sequence (used several drills with 0.6-mm increment each time) was compared with the proposed short drilling protocol (only used 2 drills: initial and final drill). One hundred drilling osteotomies were performed in bovine and porcine bones. Sets of 2 osteotomy sites were created in 5 bone densities using 2 types of drilling protocols. Thermographic pictures were captured throughout all drilling procedures and analyzed using ThermaCAM Researcher Professional 2.10. Torque values were determined during drilling by measuring electrical input and drill speed. There were statistically significant differences in bone temperature between the conventional and short drilling protocols during implant site preparation (analysis of variance P = 0.0008). However, there were no significant differences between the 2 types of drilling protocols for both implant diameters. Implant site preparation time was significantly reduced when using the short drilling protocol compared with the conventional drilling protocol (P drilling protocol proposed herein may represent a safe approach for implant site preparation.

Influence of ultrasonic frequency on the regeneration of silica gel by applying high-intensity ultrasound

International Nuclear Information System (INIS)

Zhang Weijiang; Yao Ye; Wang Rongshun

2010-01-01

Ultrasonic frequency is the key parameter considered in ultrasonic applications. In order to provide a basic knowledge about the influence of ultrasonic frequency on the regeneration of silica gel assisted by power ultrasound, the experiments about silica gel regeneration under the radiation of constant-power (60 W) ultrasound with different frequencies (i.e., 23, 27, and 38 kHz) and that without ultrasound were carried out at different regeneration temperatures (i.e., 35, 45, 55, and 65 deg. C). The experimental results showed that the lower frequency was beneficial for the application of power ultrasound in the regeneration of silica gel. The fact was theoretically explained by the ultrasonic power attenuation model which indicates that the ultrasound of lower frequency will lead to more uniform energy distribution and hence achieve higher efficiency of utilization. Meanwhile, the effect of ultrasonic frequency on silica gel regeneration would be influenced by the regeneration temperature and the moisture ratio in silica gel. As investigated in this study, the effect of ultrasonic frequency on the regeneration would be more significant at the lower regeneration temperature or at the higher moisture ratio in silica gel. In addition, the mean regeneration speed model of silica gel dependent of the regeneration temperature and the ultrasonic frequency was established according to the experimental data.

Response surface optimization of the ultrasonic-assisted extraction of edible brown pigment from Macadamia shells

Science.gov (United States)

Liu, Y. Y.; Liu, Y. J.; Gong, X.; Li, J. H.

2017-09-01

The ultrasonic extraction of Edible brown pigment from macadamia shells was researched using response surface methodology (RSM) with 3 factors and 3 levels. A Box-Behnken design (BBD) was employed to investigate the effects of Solvent concentration, ratio of water to raw material and extraction time on the extraction yield of brown pigment. By using this new method, the optimum extraction condition was obtained as follows: Ultrasonic treating time 71 min, solvent to sample ratio of 23 mL/g, Alcohol concentrations 62%. Under the optimized condition, the experimental yield of brown pigment was 0.636g.

Radiometric and ultrasonic testing of vibrating roller compacting effects

International Nuclear Information System (INIS)

Prikryl, F.; Habarta, J.; Kovarikova, E.

1977-01-01

A hole was filled with two layers of concrete mixture. Each layer was compacted using a Dynapac CA 25 vibrating roller 10,000 kg in weight, operating with a frequency of 30 Hz. A concrete block thus produced had dimensions of 11.0x2.5 m and a height of 1.6 m. After the concrete block hardening (roughly 120 days) drill cores were bored and bulk density was determined using nondestructive methods. Bulk density determination of the concrete between the drill cores was conducted using a 137 Cs emitter of an activity of 89 GBq, a FHZ-88b Geiger-Mueller counter was used as the detector. The emitter and detector were placed to touch the bore wall and were lowered to different depths in 10 cm increments. 10 count rate values were measured in each depth. The measurement time was chosen such that the decay statistical error did not exceed 1;. Bulk density of the individual segments of the drill cores was determined using 60 Co of an activitBy of 55 Mq as the radiation source and a TESLA 20/100 GWl GM counter as the detector. The detector operating voltage was 1240 V. Ultrasonic measurements were conducted using the USME-5 instrument. The measured bulk density values show that the compacting of a concrete layer 80 cm in thickness using a vibrating roller is sufficiently efficient. Both nondestructive methods were well proven, the results show that bulk density values in different depths differ due to concrete moisture content. (J.P.)

Scanning Ultrasonic Spectroscopy System Developed for the Inspection of Composite Flywheels

Science.gov (United States)

Martin, Richard E.; Baaklini, George Y.

2002-01-01

was able to successfully detect all the defects in the material. Ultrasonic spectroscopy results for a second specimen are shown along with a conventional ultrasonic C-scan. The second specimen is a section of a flywheel subcomponent that has a series of drilled holes and notches. This specimen is employed as a defect detection standard to evaluate the various nondestructive evaluation methods under consideration. Scanning results demonstrate the ability of the system to detect flaws on the order of 10 mils in the radial direction and 5 mils in the circumferential direction. Work conducted to date has shown that scanning ultrasonic spectroscopy is a viable tool for the inspection of composite flywheel systems. Ongoing development work is focused on refining the system and scanning parameters for improved resolution and defect detection.

Effects of high power ultrasonic vibration on temperature distribution of workpiece in dry creep feed up grinding.

Science.gov (United States)

Paknejad, Masih; Abdullah, Amir; Azarhoushang, Bahman

2017-11-01

Temperature history and distribution of steel workpiece (X20Cr13) was measured by a high tech infrared camera under ultrasonic assisted dry creep feed up grinding. For this purpose, a special experimental setup was designed and fabricated to vibrate only workpiece along two directions by a high power ultrasonic transducer. In this study, ultrasonic effects with respect to grinding parameters including depth of cut (a e ), feed speed (v w ), and cutting speed (v s ) has been investigated. The results indicate that the ultrasonic vibration has considerable effect on reduction of temperature, depth of thermal damage of workpiece and width of temperature contours. Maximum temperature reduction of 25.91% was reported at condition of v s =15m/s, v w =500mm/min, a e =0.4mm in the presence of ultrasonic vibration. Copyright © 2017 Elsevier B.V. All rights reserved.

Structural and optical properties of Cu2ZnSnS4 synthesized by ultrasonic assisted sol-gel method

Science.gov (United States)

Rajwar, Birendra Kumar; Sharma, Shailendra Kumar

2018-05-01

Cu2ZnSnS4 (CZTS) nanocrystals were synthesized by a simple ultrasonic assisted sol-gel method using two different solvents. Structure and purity of the phase formed were investigated using X-ray diffraction (XRD) and Raman measurements. The average crystallite size were estimated by using Scherrer's formula and found to be 2.09 and 7.15 nm. Raman study reveals the kesterite-phase of prepared samples. The influence of solvent in the morphologies of prepared samples was investigated by field emission scanning electron microscopy (FESEM). Ultraviolet-visible-near-infrared absorption measurement was carried out to calculate the optical band gap of samples. Oxidation state of the constitute elements of as-prepared samples were investigated by X-ray photoelectron spectroscopy (XPS) analysis and the results are in good agreement with the literature. The surface area and pore volume were estimated after analysis of nitrogen adsorption-desorption isotherm curves and found to be 16.5 m2/gm and 0.01 cm3/gm respectively.

Analysis of Trace Quaternary Ammonium Compounds (QACs) in Vegetables Using Ultrasonic-Assisted Extraction and Gas Chromatography-Mass Spectrometry.

Science.gov (United States)

Xiang, Lei; Wang, Xiong-Ke; Li, Yan-Wen; Huang, Xian-Pei; Wu, Xiao-Lian; Zhao, Hai-Ming; Li, Hui; Cai, Quan-Ying; Mo, Ce-Hui

2015-08-05

A reliable, sensitive, and cost-effective method was developed for determining three quaternary ammonium compounds (QACs) including dodecyltrimethylammonium chloride, cetyltrimethylammonium chloride, and didodecyldimethylammonium chloride in various vegetables using ultrasonic-assisted extraction and gas chromatography-mass spectrometry. The variety and acidity of extraction solvents, extraction times, and cleanup efficiency of sorbents were estimated to obtain an optimized procedure for extraction of the QACs in nine vegetable matrices. Excellent linearities (R(2) > 0.992) were obtained for the analytes in the nine matrices. The limits of detection and quantitation were 0.7-6.0 and 2.3-20.0 μg/kg (dry weight, dw) in various matrices, respectively. The recoveries in the nine matrices ranged from 70.5% to 108.0% with relative standard deviations below 18.0%. The developed method was applied to determine the QACs in 27 vegetable samples collected from Guangzhou in southern China, showing very high detection frequency with a concentration of 23-180 μg/kg (dw).

Surgical drill system and surgical drill bit to be used therein

NARCIS (Netherlands)

Margallo Balbas, E.; Wieringa, P.A.; French, P.J.; Lee, R.A.; Breedveld, P.

2007-01-01

Surgical drill system comprising a mechanical drill bit and means for imaging the vicinity of the drill bit tip, said means comprising: at least one optical fiber having a distal end and a proximal end, said distal end being located adjacent said drill bit tip, an optical processing unit, said

Ultrasonic mammography

International Nuclear Information System (INIS)

Hueneke, B.

1982-01-01

608 women are examined by means of ultrasonic mammography during the period of 1 year. 432 patients were examined with the compound method with the U.I. Octoson, a water tank scanner, and 176 patients with the real time method with a directly connected linear-array-scanner. The following results were obtained at the end of the examination period: In the ultrasonic and also in the X-ray mammogram tumour diameters can be determined with an error rate of +- 30%. In the diagnosing of carcinomas, a significant dependence of the exactness on the sice of the tumour is found for the combination of the five methods tested (clinical examination, X-ray mammography, ultrasonic mammography, thermography, cytology). Classifying the individual methods with regard to their exactness, X-ray mammography ranks in front of ultrasonic mammography. Mastopathic changes in the breast can be screened by means of ultrasonic mammography. The structure of the changes can be determined more exactly than with an X-ray picture which is due to the possibility of differentiating solid and cystic structures. In diagnosing fibro-adenomas and establishing diagnoses on young women with dense gland bodies, ultrasonic mammography is superior to radiology both in the ability of screening a finding of a fibro-adenoma (US=88%, X-ray=75%) and in the possibility of classifying it as ''more benign than malignant''. (orig./MG) [de

Ultrasonic physics

CERN Document Server

Richardson, E G

1962-01-01

Ultrasonic Physics, Second Edition, provides an introduction to the fundamental principles of ultrasonic physics. The book opens with a discussion of the sources of ultrasound. This is followed by separate chapters on the properties and detection of ultrasonic radiation; measurement of propagation constants, i.e., the velocity and absorption, of ultrasound; ultrasound propagation in gases, liquids, and solids; and ultrasound propagation in aerosols, suspensions, and emulsions. The final chapter covers miscellaneous physical and physico-chemical actions, including dispersion and coagulation of

Slow drilling speeds for single-drill implant bed preparation. Experimental in vitro study.

Science.gov (United States)

Delgado-Ruiz, R A; Velasco Ortega, E; Romanos, G E; Gerhke, S; Newen, I; Calvo-Guirado, J L

2018-01-01

To evaluate the real-time bone temperature changes during the preparation of the implant bed with a single-drill protocol with different drill designs and different slow drilling speeds in artificial type IV bone. For this experimental in vitro study, 600 implant bed preparations were performed in 10 bovine bone disks using three test slow drilling speeds (50/150/300 rpm) and a control drilling speed (1200 rpm). The temperature at crestal and apical areas and time variations produced during drilling with three different drill designs with similar diameter and length but different geometry were recorded with real-life thermographic analysis. Statistical analysis was performed by two-way analysis of variance. Multiple comparisons of temperatures and time with the different drill designs and speeds were performed with the Tukey's test. T Max values for the control drilling speed with all the drill designs (D1 + 1200; D2 + 1200; D3 + 1200) were higher compared to those for the controls for 11 ± 1.32 °C (p drilling at 50 rpm resulted in the lowest temperature increment (22.11 ± 0.8 °C) compared to the other slow drilling speeds of 150 (24.752 ± 1.1 °C) and 300 rpm (25.977 ± 1.2 °C) (p drilling speeds compared to that for the control drilling speed. Slow drilling speeds required significantly more time to finish the preparation of the implant bed shown as follows: 50 rpm > 150 rpm > 300 rpm > control (p drill protocol with slow drilling speeds (50, 150, and 300 rpm) without irrigation in type IV bone increases the temperature at the coronal and apical levels but is below the critical threshold of 47 °C. The drill design in single-drill protocols using slow speeds (50, 150, and 300 rpm) does not have an influence on the thermal variations. The time to accomplish the implant bed preparation with a single-drill protocol in type IV bone is influenced by the drilling speed and not by the drill design. As the speed decreases, then

Reduced abrasion drilling fluid

NARCIS (Netherlands)

2010-01-01

A reduced abrasion drilling fluid system and method of drilling a borehole by circulating the reduced abrasion drilling fluid through the borehole is disclosed. The reduced abrasion drilling fluid comprises a drilling fluid, a first additive and a weighting agent, wherein the weighting agent has a

Reduced abrasion drilling fluid

NARCIS (Netherlands)

2012-01-01

A reduced abrasion drilling fluid system and method of drilling a borehole by circulating the reduced abrasion drilling fluid through the borehole is disclosed. The reduced abrasion drilling fluid comprises a drilling fluid, a first additive and a weighting agent, wherein the weighting agent has a

Design of embedded system to determine liquid refractive index based on ultrasonic sensor using an ATMega328

Science.gov (United States)

Radiyonoa, Y.; Surantoro, S.; Pujayanto, P.; Budiharti, R.; Respati, Y. S.; Saputro, D. E.

2018-05-01

The occurrence of the broken pencil shadow into a glass of water becomes an interesting matter to be learned. The students of senior high school still find difficulty in determining liquid refractive index. To overcome this problem, it needs to develop an experimental tool to determine liquid refractive index by utilizing the newest technology. It is expected to be useful for students. This study is aimed to (1) make the design of physics learning experimental tool determinant of a liquid refractive index assisted by microcontroller based on ultrasonic sensors ATMega328 (2) explain the working principle and experimental result of liquid refractive indexing instrument assisted with ATMega328 microcontroller based ultrasonic sensor. This research used the experimental method. The result of the research shows design of physics learning experimental tool determinant of a liquid refractive index assisted by microcontroller based on ultrasonic sensors ATMega328 that has relative counting mistake of 0.36% on the measurement of aquades liquid refractive index, relative mistake of 0.18% on the 5% NaCl measurement, 0.24% on 5% glucose, and relative mistake of 0.50% on the measurement of 5 % fructose liquid refractive index. It has been created a proper device to be used in determining liquid refractive index.

Growth and Properties of Cl- Incorporated ZnO Nanofilms Grown by Ultrasonic Spray-Assisted Chemical Vapor Deposition.

Science.gov (United States)

Chen, Tingfang; Wang, Aiji; Kong, Lingrui; Li, Yongliang; Wang, Yinshu

2016-04-01

Pure and Cl- incorporated ZnO nanofilms were grown by the ultrasonic spray-assisted chemical vapor deposition (CVD) method. The properties of the nanofilms were investigated. The effects of growth temperature and Cl- concentration on the crystal structure, morphology, and optical properties of the nanofilms were studied. Temperature plays an important role in the growth mode and morphology of the pure nanofilms. Preferential growth along the c-axis occurs only at modulating temperature. Lower temperature suppresses the preferential growth, and higher temperature suppresses the growth of the nanofilms. The morphologies of the nanofilms change from lamellar and spherical structures into hexagonal platelets, then into separated nanoparticles with an increase in the temperature. Incorporating Cl- results in the lattice contracting gradually along with c-axis. Grains composing the nanofilms refine, and the optical gap broadens with increasing of Cl- concentration in growth precursor. Incorporating Cl- could reduce oxygen vacancies and passivate the non-irradiated centers, thus enhancing the UV emission and suppressing the visible emission of ZnO nanofilms.

Ionic Liquid-Based Ultrasonic-Assisted Extraction of Secoisolariciresinol Diglucoside from Flaxseed (Linum usitatissimum L. with Further Purification by an Aqueous Two-Phase System

Directory of Open Access Journals (Sweden)

Zhi-Jian Tan

2015-09-01

Full Text Available In this work, a two-step extraction methodology of ionic liquid-based ultrasonic-assisted extraction (IL-UAE and ionic liquid-based aqueous two-phase system (IL-ATPS was developed for the extraction and purification of secoisolariciresinol diglucoside (SDG from flaxseed. In the IL-UAE step, several kinds of ILs were investigated as the extractants, to identify the IL that affords the optimum extraction yield. The extraction conditions such as IL concentration, ultrasonic irradiation time, and liquid–solid ratio were optimized using response surface methodology (RSM. In the IL-ATPS step, ATPS formed by adding kosmotropic salts to the IL extract was used for further separation and purification of SDG. The most influential parameters (type and concentration of salt, temperature, and pH were investigated to obtain the optimum extraction efficiency. The maximum extraction efficiency was 93.35% under the optimal conditions of 45.86% (w/w IL and 8.27% (w/w Na2SO4 at 22 °C and pH 11.0. Thus, the combination of IL-UAE and IL-ATPS makes up a simple and effective methodology for the extraction and purification of SDG. This process is also expected to be highly useful for the extraction and purification of bioactive compounds from other important medicinal plants.

Synthesis spherical porous hydroxyapatite/graphene oxide composites by ultrasonic-assisted method for biomedical applications.

Science.gov (United States)

Duan, Peizhen; Shen, Juan; Zou, Guohong; Xia, Xu; Jin, Bo; Yu, Jiaxin

2018-04-10

Spherical porous hydroxyapatite (SHA)/graphene oxide (GO) composites with different GO (w/w) content of 16%, 40%, and 71% have been fabricated through a facile and controllable ultrasonic-assisted method at room temperature. The products were characterized by x-ray diffraction, field emission scanning electron microscopy, thermogravimetric analysis, mechanical testing and biomimetic mineralization. Results showed SHA were covered by GO, and SHA/GO composites had an irregular surface with different degrees of wrinkles. The elastic modulus and hardness of SHA/GO-3 composites were up to 12.45 ± 0.33 GPa and 686.67 ± 26.95 MPa, which indicated that the contents of GO had an effect on SHA/GO composites. And the mechanical properties of SHA/GO-2 composites were similar to SHA particles. The biomimetic mineralization in SBF solution showed the bone-like apatite layer on composites surface, which demonstrated that the SHA/GO materials had osseointegration property. Moreover, in vitro cytocompatibility of SHA/GO-2 composites and pure GO were evaluated by cell adhesion and proliferation tests using MC3T3-E1 cells, which demonstrated that the SHA/GO composites can act as a good template for the cells growth and adhesion. These results suggested that the SHA/GO composites will be a promising material for biomedical application.

Application of Box-Behnken design for ultrasonic-assisted extraction of polysaccharides from Paeonia emodi.

Science.gov (United States)

Ahmad, Ajaz; Alkharfy, Khalid M; Wani, Tanveer A; Raish, Mohammad

2015-01-01

The objective of the present work was to study the ultrasonic assisted extraction and optimization of polysaccharides from Paeonia emodi and evaluation of its anti-inflammatory response. Specifically, the optimization of polysaccharides was carried out using Box-Behnken statistical experimental design. Response surface methodology (RSM) of three factors (extraction temperature, extraction time and liquid solid ratio) was employed to optimize the percentage yield of the polysaccharides. The experimental data were fitted to quadratic response surface models using multiple regression analysis with high coefficient of determination value (R) of 0.9906. The highest polysaccharide yield (8.69%) as per the Derringer's desirability prediction tool was obtained under the optimal extraction condition (extraction temperature 47.03 °C, extraction time 15.68 min, and liquid solid ratio 1.29 ml/g) with a desirability value of 0.98. These optimized values of tested parameters were validated under similar conditions (n = 6), an average of 8.13 ± 2.08% of polysaccharide yield was obtained in an optimized extraction conditions with 93.55% validity. The anti-inflammatory effect of polysaccharides of P. emodi were studied on carrageenan induced paw edema. In vivo results showed that the P. emodi 200mg/kg of polysaccharide extract exhibited strong potential against inflammatory response induced by 1% suspension of carrageenean in normal saline. Copyright © 2014 Elsevier B.V. All rights reserved.

Activity plan: Directional drilling and environmental measurements while drilling

International Nuclear Information System (INIS)

Myers, D.A.

1998-01-01

This activity plan describes the testing of directional drilling combined with environmental measurements while drilling at two Hanford Site locations. A cold test is to be conducted at the 105A Mock Tank Leak Facility in the 200 East Area. A hot test is proposed to be run at the 216-B-8 tile field north of the 241-B Tank Farm in 200 East Area. Criteria to judge the success, partial success or failure of various aspects of the test are included. The TWRS program is assessing the potential for use of directional drilling because of an identified need to interrogate the vadose zone beneath the single-shell tanks. Because every precaution must be taken to assure that investigation activities do not violate the integrity of the tanks, control of the drill bit and ability to follow a predetermined drill path are of utmost importance and are being tested

Case drilling - an innovative approach to reducing drilling costs

Energy Technology Data Exchange (ETDEWEB)

Madell, G.; Tessari, R. M. [Tesco Corp., Calgary, AB (Canada); Warren, T. [Tesco Drilling Technology, Calgary, AB (Canada)

1999-11-01

Casing drilling is introduced as a new drilling technique that uses standard oil field casing to simultaneously drill and case the well. The technology includes both rig and downhole equipment, customized to function effectively as an integrated drilling system. This paper describes the testing program designed to identify and overcome technical challenges. Although not fully optimized, it appears that the system is functional. Test results indicate the need for improvements in the pump down cement float equipment and the tools and procedures for drilling up the cement plugs. The pump down latch and retrieval system also needs to be further developed and tested for high angle directional applications. Cost savings in the range of 10 to 15 per cent are expected for trouble-free wells. By eliminating the cost of unscheduled events encountered in troublesome wells, cost savings may reach as high as 30 per cent. 3 refs., 7 figs.

Activity plan: Directional drilling and environmental measurements while drilling

Energy Technology Data Exchange (ETDEWEB)

Myers, D.A.

1998-07-16

This activity plan describes the testing of directional drilling combined with environmental measurements while drilling at two Hanford Site locations. A cold test is to be conducted at the 105A Mock Tank Leak Facility in the 200 East Area. A hot test is proposed to be run at the 216-B-8 tile field north of the 241-B Tank Farm in 200 East Area. Criteria to judge the success, partial success or failure of various aspects of the test are included. The TWRS program is assessing the potential for use of directional drilling because of an identified need to interrogate the vadose zone beneath the single-shell tanks. Because every precaution must be taken to assure that investigation activities do not violate the integrity of the tanks, control of the drill bit and ability to follow a predetermined drill path are of utmost importance and are being tested.

Environmental Measurement-While-Drilling System and Horizontal Directional Drilling Technology Demonstration, Hanford Site

International Nuclear Information System (INIS)

Williams, C.V.; Lockwood, G.J.; Normann, R.A.; Myers, D.A.; Gardner, M.G.; Williamson, T.; Huffman, J.

1999-01-01

The Environmental Measurement-While-Drilling (EMWD) system and Horizontal Directional Drilling (HDD) were successfully demonstrated at the Mock Tank Leak Simulation Site and the Drilling Technology Test Site, Hanford, Washington. The use of directional drilling offers an alternative to vertical drilling site characterization. Directional drilling can develop a borehole under a structure, such as a waste tank, from an angled entry and leveling off to horizontal at the desired depth. The EMWD system represents an innovative blend of new and existing technology that provides the capability of producing real-time environmental and drill bit data during drilling operations. The technology demonstration consisted of the development of one borehole under a mock waste tank at a depth of approximately minus8 m (minus27 ft.), following a predetermined drill path, tracking the drill path to within a radius of approximately1.5 m (5 ft.), and monitoring for zones of radiological activity using the EMWD system. The purpose of the second borehole was to demonstrate the capability of drilling to a depth of ∼ -21 m (-70 ft.), the depth needed to obtain access under the Hanford waste tanks, and continue drilling horizontally. This report presents information on the HDD and EMWD technologies, demonstration design, results of the demonstrations, and lessons learned

Synthesis of conductive semi-transparent silver films deposited by a Pneumatically-Assisted Ultrasonic Spray Pyrolysis Technique

Energy Technology Data Exchange (ETDEWEB)

Zaleta-Alejandre, E.; Balderas-Xicoténcatl, R. [Centro de Investigación y de Estudios Avanzados-IPN, Departamento de Física, , Apdo. Postal 14-470, Del, Gustavo A. Madero, C.P. 07000, México, D.F. (Mexico); Arrieta, M.L. Pérez [Universidad Autónoma de Zacatecas, Unidad Académica de Física, Calzada Solidaridad esq. Paseo, La Bufa s/n, C.P. 98060, Zacatecas, México (Mexico); Meza-Rocha, A.N.; Rivera-Álvarez, Z. [Centro de Investigación y de Estudios Avanzados-IPN, Departamento de Física, , Apdo. Postal 14-470, Del, Gustavo A. Madero, C.P. 07000, México, D.F. (Mexico); Falcony, C., E-mail: cfalcony@fis.cinvestav.mx [Centro de Investigación y de Estudios Avanzados-IPN, Departamento de Física, , Apdo. Postal 14-470, Del, Gustavo A. Madero, C.P. 07000, México, D.F. (Mexico)

2013-10-01

Highlights: • We deposited metallic silver films without post-deposition annealing. • The spray pyrolysis technique is of low cost and scalable for industrial applications. • We obtained deposition rate of 60 nm min{sup −1} at 300 °C. • The average resistivity was 1E−7 Ω m. • Semi-transparent silver films were obtained at 350 °C and deposition time of 45 s. -- Abstract: The synthesis and characterization of nanostructured silver films deposited on corning glass by a deposition technique called Pneumatically-Assisted Ultrasonic Spray Pyrolysis are reported. Silver nitrate and triethanolamine were used as silver precursor and reducer agent, respectively. The substrate temperatures during deposition were in the range of 300–450 °C and the deposition times from 30 to 240 s. The deposited films are polycrystalline with cubic face-centered structure, and crystalline grain size less than 30 nm. Deposition rates up to 600 Å min{sup −1} were obtained at substrate temperature as low as 300 °C. The electrical, optical, and morphological properties of these films are also reported. Semi-transparent conductive silver films were obtained at 350 °C with a deposition time of 45 s.

Synthesis of conductive semi-transparent silver films deposited by a Pneumatically-Assisted Ultrasonic Spray Pyrolysis Technique

International Nuclear Information System (INIS)

Zaleta-Alejandre, E.; Balderas-Xicoténcatl, R.; Arrieta, M.L. Pérez; Meza-Rocha, A.N.; Rivera-Álvarez, Z.; Falcony, C.

2013-01-01

Highlights: • We deposited metallic silver films without post-deposition annealing. • The spray pyrolysis technique is of low cost and scalable for industrial applications. • We obtained deposition rate of 60 nm min −1 at 300 °C. • The average resistivity was 1E−7 Ω m. • Semi-transparent silver films were obtained at 350 °C and deposition time of 45 s. -- Abstract: The synthesis and characterization of nanostructured silver films deposited on corning glass by a deposition technique called Pneumatically-Assisted Ultrasonic Spray Pyrolysis are reported. Silver nitrate and triethanolamine were used as silver precursor and reducer agent, respectively. The substrate temperatures during deposition were in the range of 300–450 °C and the deposition times from 30 to 240 s. The deposited films are polycrystalline with cubic face-centered structure, and crystalline grain size less than 30 nm. Deposition rates up to 600 Å min −1 were obtained at substrate temperature as low as 300 °C. The electrical, optical, and morphological properties of these films are also reported. Semi-transparent conductive silver films were obtained at 350 °C with a deposition time of 45 s

Combined use of ultrasonic-assisted liposuction and semicircular periareolar incision for the treatment of gynecomastia.

Science.gov (United States)

Esme, Danielle L; Beekman, Werner H; Hage, J Joris; Nipshagen, Martine D

2007-12-01

Of the wide range of excisional and liposuction techniques used to correct gynecomastia, so far, no single one was suitable for all grades of gynecomastia. We introduce ultrasonic-assisted liposuction (UAL) combined with conventional liposuction and partial gland resection without skin excision as the standard surgical technique for all such grades. Twenty-eight men (aged 17 to 80 years) were consecutively treated from March 2004 through April 2006 for grade Ia (n = 3), Ib (n = 2), IIa (n = 6), IIb (n = 6), III (n = 8), or IV (n = 3) gynecomastia. Their characteristics and the outcome of surgery were retrospectively assessed. A mean of 848 mL (range, 300 to 1400 mL) of liquefied breast tissue was aspirated, and 31 g (range, 3 to 180 g) of fibroglandular tissue were excised per breast. No immediate or delayed adjuvant skin reduction was needed in any of the patients. Moderate postoperative ecchymosis was observed in 2 patients, but no complications were encountered in this series. The cosmetic outcome was good to excellent in all. UAL in combination with gland resection through a minimal caudal semicircular periareolar incision and conventional liposuction effectively corrects all grades of gynecomastia. This combination has little morbidity, requires no skin excision, and leads to uniformly good esthetic results.

Tribological behavior of Al-WC nano-composites fabricated by ultrasonic cavitation assisted stir-cast method

Science.gov (United States)

Pal, Arpan; Poria, Suswagata; Sutradhar, Goutam; Sahoo, Prasanta

2018-03-01

In the present study, the effects of WC nano-particles content on the microstructure, hardness, wear, and friction behavior of aluminum matrix composites are investigated. Al-WC nano composites with varying wt% of WC (0, 1, 1.5, and 2) are fabricated using ultrasonic cavitation assisted stir-cast method. The microstructure of the nano-composite samples is analyzed using optical microscopy and scanning electron microscopy. Elemental composition is determined by energy dispersive x-ray analysis. Vicker’s microhardness test is performed in different locations on the composite sample surface with a load of 50 gf and 10s dwell time. Wear and friction of the composites under dry sliding is studied using a pin-on-disk tribotester for varying normal load (10–40 N) and sliding speed (0.1–0.4 m/s). Uniform distribution of nano-WC is observed over composite surface without noticeable clustering. Reinforcement of nano-WC particles improves wear resistance and frictional behavior of the composite. Hardness is seen to increase with increase in wt% of nano-particles. Wear behavior of composites depends on formation of layers over the surface mixed with oxidized debris and counter-face particles. Wear mechanism changes from adhesion to abrasion with increase in wt% of hard nano particles.

Ionic liquids based simultaneous ultrasonic and microwave assisted extraction of phenolic compounds from burdock leaves

International Nuclear Information System (INIS)

Lou Zaixiang; Wang Hongxin; Zhu Song; Chen Shangwei; Zhang Ming; Wang Zhouping

2012-01-01

The ionic liquids based simultaneous ultrasonic and microwave assisted extraction (IL-UMAE) technique was first proposed and applied to isolate compounds. The ionic liquids comprising a range of four anions, five 1-alkyl-3-methylimidazolium derivatives were designed and prepared. The results suggested that varying the anion and cation both had apparent effects on the extraction of phenolics. The results also showed that irradiation power, time and solid–liquid ratio significantly affected the yields. The yields of caffeic acid and quercetin obtained by IL-UMAE were higher than those by regular UMAE. Compared with conventional heat-reflux extraction (HRE), the proposed approach exhibited higher efficiency (8–17% enhanced) and shorter extraction time (from 5 h to 30 s). The results indicated ILUMAE to be a fast and efficient extraction technique. Moreover, the proposed method was validated by the reproducibility and recovery experiments. The ILUMAE method provided good recoveries (from 96.1% to 105.3%) with RSD lower than 5.2%, which indicated that the proposed method was credible. Based on the designable nature of ionic liquids, and the rapid and highly efficient performance of the proposed approach, ILUMAE provided a new alternative for preparation of various useful substances from solid samples.

Ultrasonic pretreatment of woodchips for the conversion of cellulose to glucose for bioethanol production

International Nuclear Information System (INIS)

Tutun Nugraha; Rettyana Ayuputri; Mohammad Ihsan

2010-01-01

In this study, lignocellulosic biomass i.e. the woodchips of Albacia tree (Paraserianthes falcataria) were given different pretreatment methods, i.e. chemical (acid) and physical (ultrasonic). The pretreatment was given in order to convert the cellulose to glucose for the production of bioethanol. 1 % H_2SO_4 was applied for the acid pretreatment. Ultrasound pretreatment was carried out at varied time (10, 20 and 30 minutes) at 600 W, 20 khz before or after the acid pretreatment. Enzymatic attack of the pretreated sample was also applied to enhance the saccharification process of cellulose. The objective of the research was to determine the most effective ultrasonic duration and the best combination of method for enzymatic hydrolysis of the woodchips. The data showed that the highest yield of glucose was achieved at 20 minutes ultrasonic time. It was also found that substantial amount of hydrolysis of cellulose to glucose occur during the ultrasonic stage even without the presence of acid or cellulose enzyme. It is likely that the highly energetic ultrasonic process alone could assist in enhancing rate of hydrolysis of lignocellulosic cellulose into glucose. (author)

Eddy current and ultrasonic fuel channel inspection at Karachi Nuclear Power Plant

International Nuclear Information System (INIS)

Mayo, W.R.; Alam, M.M.

1997-01-01

In November of 1993 and in-service inspection was performed on eight fuel channels in the Karachi Nuclear Power Plant (KANUPP) reactor. The workscope included ultrasonic and eddy current volumetric examinations, and eddy current measurement of pressure-to calandria tube gap. This paper briefly discusses the planning strategy of the ultrasonic and eddy current examinations, and describes the equipment developed to meet the requirements, followed by details of the actual channel inspection campaign. The presented nondestructive examinations assisted in determining fitness for service of KANUPP reactor channels in general, and confirmed that the problems associated with channel G12 were not generic in nature. (author)

Application of focus-variation Technique in Measurements of Ultrasonic Vibrations of Grinding pins

Directory of Open Access Journals (Sweden)

Wdowik Roman

2015-01-01

Full Text Available The paper presents the application of focus-variation technique in measurements of ultrasonic vibrations of grinding pins. Ultrasonic vibrations of tools are applied in ultrasonic assisted grinding. Their measurements are significant for development of this hybrid machining process. Alumina and zirconia ceramic materials in the final fired state were machined in experiments which are known as scratch tests. Diamond grinding pin was used as a tool to machine scratches. Marks of diamond grains, left on the surface of workpieces after machining process, were investigated using The Infinite Focus Real 3D optical microscope. Focus-variation is the principle of operation of this microscope. Investigations concerned possibilities of measurements of an amplitude of axial and radial vibrations in the case of two ceramic materials. Results of performed measurements are presented and discussed for selected machining parameters.

The Swedish Deep Drilling Program - an emerging scientific drilling program and new infrastructure.

Science.gov (United States)

Lorenz, Henning; Juhlin, Christopher

2010-05-01

Scientific drilling projects imply numerous aspects that are difficult to handle for individual research groups. Therefore, about three years ago a joint effort was launched in the Swedish geoscientific community to establish a national program for scientific drilling, the Swedish Deep Drilling Program (SDDP). Soon afterwards, several working groups established drilling proposals with Nordic and, also, international participation. With this serious interest in scientific drilling SDDP was able to successfully promote the Swedish membership in ICDP which commenced in 2008. Two SDDP projects achieved workshop grants from the International Continental Scientific Drilling Program (ICDP) in 2009. In the same year the Swedish Research Council decided to support an application for a truck-mounted drill rig - a big success for the SDDP working group. Scientific Drilling infrastructure: SDDP envisages a mobile platform that is capable of core drilling to at least 2500 m depth. The procurement will be made during 2010 and first operations are planned for 2011. This drill rig is primarily intended for use in the SDDP drilling projects, but will be rented out to other scientific drilling projects or even commercial enterprises in the remaining time to cover maintenance and future upgrade costs. SDDP's drill rig will be unique in Europe and complementary to the deep drilling InnovaRig of the GFZ German Research Centre for Geosciences. Until now, drilling to 2000 - 3000 m implied the use of a full-sized drill rig like the InnovaRig or the mobilization of a core drill rig from another continent. This gap will now be filled by Sweden's upcoming scientific drilling infrastructure. Drilling projects and proposals: Presently, SDDP serves six projects: "Collisional Orogeny in the Scandinavian Caledonides" (COSC; ICDP workshop spring 2010), the "Postglacial Fault Drilling Project" (PFDP; ICDP workshop autumn 2010), a "Deep Rock Laboratory" (DRL), "Palaeoproterozoic Mineralized Volcanic

Drilling cost analysis

International Nuclear Information System (INIS)

Anand, A.B.

1992-01-01

Drilling assumes greater importance in present day uranium exploration which emphasizes to explore more areas on the basis of conceptual model than merely on surface anomalies. But drilling is as costly as it is important and consumes a major share (50% to 60%) of the exploration budget. As such the cost of drilling has great bearing on the exploration strategy as well as on the overall cost of the project. Therefore, understanding the cost analysis is very much important when planning or intensifying an exploration programme. This not only helps in controlling the current operations but also in planning the budgetary provisions for future operations. Also, if the work is entrusted to a private party, knowledge of in-house cost analysis helps in fixing the rates of drilling in different formations and areas to be drilled. Under this topic, various factors that contribute to the cost of drilling per meter as well as ways to minimize the drilling cost for better economic evaluation of mineral deposits are discussed. (author)

Effect of Ultrasonic Frequency on Lactic Acid Fermentation Promotion by Ultrasonic Irradiation

Science.gov (United States)

Shimada, Tadayuki; Ohdaira, Etsuzo; Masuzawa, Nobuyoshi

2004-05-01

The authors have been researching the promotion of lactic acid fermentation by ultrasonic irradiation. In the past research, it was proven that ultrasonic irradiation is effective in the process of fermentation, and the production of yoghurt and kefir was promoted. In this study, the effect of the ultrasonic frequency in this fermentation process was examined. In the frequency range of this study, it was found that the action of fermentation promotion was exponentially proportionate to the irradiated ultrasonic frequency.

Electromagnetic ultrasonic guided waves

CERN Document Server

Huang, Songling; Li, Weibin; Wang, Qing

2016-01-01

This book introduces the fundamental theory of electromagnetic ultrasonic guided waves, together with its applications. It includes the dispersion characteristics and matching theory of guided waves; the mechanism of production and theoretical model of electromagnetic ultrasonic guided waves; the effect mechanism between guided waves and defects; the simulation method for the entire process of electromagnetic ultrasonic guided wave propagation; electromagnetic ultrasonic thickness measurement; pipeline axial guided wave defect detection; and electromagnetic ultrasonic guided wave detection of gas pipeline cracks. This theory and findings on applications draw on the author’s intensive research over the past eight years. The book can be used for nondestructive testing technology and as an engineering reference work. The specific implementation of the electromagnetic ultrasonic guided wave system presented here will also be of value for other nondestructive test developers.

Ultrasonic viewing device

International Nuclear Information System (INIS)

Ito, Juro.

1979-01-01

Purpose: To improve the safety of reactor operation by enabling to detect the states and positions of fuel assemblies over a wide range with a set of ultrasonic viewing device comprising a rotatable ultrasonic transmitter-receiver and a reflector mounted with an adjustable angle. Constitution: A driving portion for a ultrasonic viewing device is provided to a rotary plug closing the opening of a reactor vessel and a guide pipe suspending below the coolant level is provided to the driving portion. An ultrasonic transmitter-receiver is provided at the end of the holder tube in the guide pipe. A reflector is provided at the upper position of the reactor core so as to correspond to the ultrasonic transmitter-receiver. The ultrasonic transmitter-receiver, positioned by the driving portion, performs horizontal movement for scanning the entire surface of the top of the reactor core, as well as vertical movement covering the gap between the upper mechanism on the reactor and the reactor core, whereby the confirmation for the separation of the control rod and the detection for the states of the reactor core can be conducted by the reflection waves from the reflector. (Moriyama, K.)

Robotic Planetary Drill Tests

Science.gov (United States)

Glass, Brian J.; Thompson, S.; Paulsen, G.

2010-01-01

Several proposed or planned planetary science missions to Mars and other Solar System bodies over the next decade require subsurface access by drilling. This paper discusses the problems of remote robotic drilling, an automation and control architecture based loosely on observed human behaviors in drilling on Earth, and an overview of robotic drilling field test results using this architecture since 2005. Both rotary-drag and rotary-percussive drills are targeted. A hybrid diagnostic approach incorporates heuristics, model-based reasoning and vibration monitoring with neural nets. Ongoing work leads to flight-ready drilling software.

Drilling trends in the nineties

International Nuclear Information System (INIS)

1993-01-01

At a conference on various aspects of well drilling in the 1990s, papers were presented on drilling waste management, well completion and workovers, drilling fluids, drilling rig equipment and design, drilling mechanics, drill stem testing and materials, cementing, business management, health and safety, environmental issues, and directional drilling technology. Separate abstracts have been prepared for 46 papers from this conference

Scientific Drilling with the Sea Floor Drill Rig MeBo

Directory of Open Access Journals (Sweden)

Gerold Wefer

2007-09-01

Full Text Available In March 2007 the sea floor drill rig MeBo (short for “Meeresboden-Bohrgerät”, ‘sea floor drill rig’ in German returned from a 17-day scientific cruise with the new German research vessel Maria S. Merian. Four sites between 350 m and 1700 m water depth were sampled at the continental slope off Morocco by push coring and rotary drilling. Up to 41.5-m-long sediment cores were recovered from Miocene, Pliocene, and Pleistocene marls. MeBo bridges the gapbetween conventional sampling methods from standard multipurpose research vessels (gravity corer, piston corer, dredges and drill ships. Most bigger research vessels will be able to support deployment of the MeBo. Since the drill system can be easily transported within 20-ft containers, worldwide operation from vessels of opportunity is possible. With the MeBo a new system is available for marine geosciences that allows the recovery of high quality samples from soft sediments and hard rock from the deep sea withoutrelying on the services of expensive drilling vessels.

Drilling contract issues

International Nuclear Information System (INIS)

Davison, G.B.; Worden, D.R.; Borbridge, G.K.D.

1997-01-01

Some selected issues which are facing both operators and contractors in drilling for oil and gas, such as the allocation of risk by contract and by statute and the implementation of new technologies, were discussed. There are three varieties of written drilling contracts used in Canada: (1) day work and meterage contracts, (2) master drilling agreements, and (3) contracts that are used in construction projects that do not specifically relate to drilling. Issues relevant to the contractual allocation of risk, to implementing new drilling technologies, to reconciling contract and statute liability, and the formation of strategic alliances for mutual benefit, and the factors contributing to the success of such alliances were explored. 12 refs

Modification of Surface Roughness and Area of FeCrAl Substrate for Catalytic Converter using Ultrasonic Treatment

Directory of Open Access Journals (Sweden)

Yanuandri Putrasari

2012-03-01

Full Text Available Surface roughness and area play important role especially in deposition and reaction of the catalyst in the catalytic converter substrate. The aim of this paper is to show the modification of surface roughness and area of FeCrAl substrate for catalytic converter using ultrasonic method. The method was conducted by agitating the FeCrAl in 10 minutes 35 kHz ultrasonic cleaning bath. The  surface roughness, morphology, and chemical components of FeCrAl catalytic converter substrate after ultrasonic treatment were analyzed using atomic force microscope (AFM and examined with scanning electron microscope (SEM in combination with energy dispersive X-ray spectroscopy (EDS. The ultrasonic treatment assisted with Al2O3 powders successfully increased the roughness and surface area of FeCrAl better than SiC powders. 

Combined Ultrasonic Elliptical Vibration and Chemical Mechanical Polishing of Monocrystalline Silicon

Directory of Open Access Journals (Sweden)

Liu Defu

2016-01-01

Full Text Available An ultrasonic elliptical vibration assisted chemical mechanical polishing(UEV-CMP is employed to achieve high material removal rate and high surface quality in the finishing of hard and brittle materials such as monocrystalline silicon, which combines the functions of conventional CMP and ultrasonic machining. In theultrasonic elliptical vibration aided chemical mechanical polishingexperimental setup developed by ourselves, the workpiece attached at the end of horn can vibrate simultaneously in both horizontal and vertical directions. Polishing experiments are carried out involving monocrystalline silicon to confirm the performance of the proposed UEV-CMP. The experimental results reveal that the ultrasonic elliptical vibration can increase significantly the material removal rate and reduce dramatically the surface roughness of monocrystalline silicon. It is found that the removal rate of monocrystalline silicon polished by UEV-CMP is increased by approximately 110% relative to that of conventional CMP because a passive layer on the monocrystalline silicon surface, formed by the chemical action of the polishing slurry, will be removed not only by the mechanical action of CMP but also by ultrasonic vibration action. It indicates that the high efficiency and high quality CMP of monocrystalline silicon can be performed with the proposed UEV-CMP technique.

Optimization of ultrasonic-assisted extraction of bioactive alkaloid compounds from rhizoma coptidis (Coptis chinensis Franch.) using response surface methodology.

Science.gov (United States)

Teng, Hui; Choi, Yong Hee

2014-01-01

The optimum extraction conditions for the maximum recovery of total alkaloid content (TAC), berberine content (BC), palmatine content (PC), and the highest antioxidant capacity (AC) from rhizoma coptidis subjected to ultrasonic-assisted extraction (UAE) were determined using response surface methodology (RSM). Central composite design (CCD) with three variables and five levels was employed, and response surface plots were constructed in accordance with a second order polynomial model. Analysis of variance (ANOVA) showed that the quadratic model was well fitted and significant for responses of TAC, BC, PC, and AA. The optimum conditions obtained through the overlapped contour plot were as follows: ethanol concentration of 59%, extraction time of 46.57min, and temperature of 66.22°C. Verification experiment was carried out, and no significant difference was found between observed and estimated values for each response, suggesting that the estimated models were reliable and valid for UAE of alkaloids. Crown Copyright © 2013. Published by Elsevier Ltd. All rights reserved.

Ultrasonic Evaluation of the Pull-Off Adhesion between Added Repair Layer and a Concrete Substrate

Science.gov (United States)

Czarnecki, Slawomir

2017-10-01

This paper concerns the evaluation of the pull-off adhesion between a concrete added repair layer with variable thickness and a concrete substrate, based on parameters assessed using ultrasonic pulse velocity (UPV) method. In construction practice, the experimental determination of pull-off adhesion f b, between added repair layer and a concrete substrate is necessary to assess the quality of repair. This is usually carried out with the use of pull-off method which results in local damage of the added concrete layer in all the testing areas. Bearing this in mind, it is important to describe the method without these disadvantages. The prediction of the pull-off adhesion of the two-layer concrete elements with variable thickness of each layer might be provided by means of UPV method with two-sided access to the investigated element. For this purpose, two-layered cylindrical specimens were obtained by drilling the borehole from a large size specially prepared concrete element. Those two-layer elements were made out of concrete substrate layer and Polymer Cement Concrete (PCC) mortar as an added repair layer. The values of pull-off adhesion f b of the elements were determined before obtaining the samples by using the semi-destructive pull-off method. The ultrasonic wave velocity was determined in samples with variable thickness of each layer and was then compared to theoretical ultrasonic wave velocity predicted for those specimens. The regression curve for the dependence of velocity and pull-off adhesion, determined by the pulloff method, was made. It has been proved that together with an increase of ratio of investigated ultrasonic wave velocity divided by theoretical ultrasonic wave velocity, the pull-off adhesion value f b between added repair layer with variable thickness and a substrate layer also increases.

South African drilling

International Nuclear Information System (INIS)

Anon.

1984-01-01

According to the president of the South African Drilling Association, the drilling industry is meeting head-on the challenges created by the worldwide recession. The paper is a synopsis of several of the papers presented at the SADA symposium and a look at several mining-related drilling projects in South Africa. These papers include grouting techniques, the use of impregnated bits in hard rock drilling, tunnel boring for mines, surveying improvement methods and the use of explosives to increase groundwater yield

Radial vibration and ultrasonic field of a long tubular ultrasonic radiator.

Science.gov (United States)

Shuyu, Lin; Zhiqiang, Fu; Xiaoli, Zhang; Yong, Wang; Jing, Hu

2013-09-01

The radial vibration of a metal long circular tube is studied analytically and its electro-mechanical equivalent circuit is obtained. Based on the equivalent circuit, the radial resonance frequency equation is derived. The theoretical relationship between the radial resonance frequency and the geometrical dimensions is studied. Finite element method is used to simulate the radial vibration and the radiated ultrasonic field and the results are compared with those from the analytical method. It is concluded that the radial resonance frequency for a solid metal rod is larger than that for a metal tube with the same outer radius. The radial resonance frequencies from the analytical method are in good agreement with those from the numerical method. Based on the acoustic field analysis, it is concluded that the long metal tube with small wall thickness is superior to that with large wall thickness in producing radial vibration and ultrasonic radiation. Therefore, it is expected to be used as an effective radial ultrasonic radiator in ultrasonic sewage treatment, ultrasonic antiscale and descaling and other ultrasonic liquid handling applications. Copyright © 2013 Elsevier B.V. All rights reserved.

A new drilling method—Earthworm-like vibration drilling

Science.gov (United States)

Wang, Peng; Wang, Ruihe

2018-01-01

The load transfer difficulty caused by borehole wall friction severely limits the penetration rate and extended-reach limit of complex structural wells. A new friction reduction technology termed “earthworm-like drilling” is proposed in this paper to improve the load transfer of complex structural wells. A mathematical model based on a “soft-string” model is developed and solved. The results show that earthworm-like drilling is more effective than single-point vibration drilling. The amplitude and frequency of the pulse pressure and the installation position of the shakers have a substantial impact on friction reduction and load transfer. An optimization model based on the projection gradient method is developed and used to optimize the position of three shakers in a horizontal well. The results verify the feasibility and advantages of earthworm-like drilling, and establish a solid theoretical foundation for its application in oil field drilling. PMID:29641615

Recommended well drilling and testing program

International Nuclear Information System (INIS)

Long, J.; Wilson, C.

1978-07-01

A well drilling and testing program is recommended by Lawrence Berkeley Laboratory to identify the hydrology of deep basalts in the Pasco Basin. The ultimate objective of this program is to assist in determining the feasibility of locating a nuclear waste repository on the Hanford Reservation. The recommended program has been staged for maximum effectiveness. In the first stage, six wells have been identified for drilling and testing which, when coupled with existing wells, will provide sufficient data for a preliminary overview of basin hydrology and a preliminary determination of the hydrologic suitability of the deep basalt for a repository site. The rate at which the first stage wells are drilled and tested will depend upon the date at which a preliminary determination of site suitability is required. It was assumed that a preliminary determination of suitability would be required in 1980, in which case all six first stage wells would be drilled in FY 1979. If the results of the first stage analysis are favorable for repository siting, tentative repository sites can be identified and a second stage hydrology program can be implemented to provide the necessary details of the flow system. To accomplish this stage, a number of deep wells would be required at locations both inside and outside the basin, with specific sites to be identified as the work progresses to obtain maximum utility of existing data. A program is recommended for testing in each new well and for completion of testing in each existing well. Recommended tests include borehole geophysics, pressure and permeability testing, geochemical sampling, tracer testing, hydrofracturing and borehole fracture logging. The entire data collection program is oriented toward providing the information required to establish and verify an accurate numerical model of the Pasco Basin

Ultrasonic decontamination robot

International Nuclear Information System (INIS)

Patenaude, R.S.

1984-01-01

An ultrasonic decontamination robot removes radioactive contamination from the internal surface of the inlet and outlet headers, divider plate, tube sheet, and lower portions of tubes of a nuclear power plant steam generator. A programmable microprocessor controller guides the movement of a robotic arm mounted in the header manway. An ultrasonic transducer having a solvent delivery subsystem through which ultrasonic action is achieved is moved by the arm over the surfaces. A solvent recovery suction tube is positioned within the header to remove solvent therefrom while avoiding interference with the main robotic arm. The solvent composition, temperature, pressure, viscosity, and purity are controlled to optimize the ultrasonic scrubbing action. The ultrasonic transducer is controlled at a power density, frequency, and on-off mode cycle such as to optimize scrubbing action within the range of transducer-to-surface distance and solvent layer thickness selected for the particular conditions encountered. Both solvent and transducer control actions are optimized by the programmable microprocessor. (author)

Ultrasonic testing device

International Nuclear Information System (INIS)

Lawrie, W.E.

1978-01-01

The ultrasonic transmitter made of polarized ferroelectric ceramic material (lead zirconate titanate) is arranged in a strip carrier which allows it to be introduced between the fuel elements of a fuel subassembly in a water cooled nuclear reactor. The ultrasonic transmitter is insulated relative to the carrier. The echo of the ra dal ultrasonic pulse is recorded which changes as faulty water filled fuel elements are detected. (RW) [de

New optimized drill pipe size for deep-water, extended reach and ultra-deep drilling

Energy Technology Data Exchange (ETDEWEB)

Jellison, Michael J.; Delgado, Ivanni [Grant Prideco, Inc., Hoston, TX (United States); Falcao, Jose Luiz; Sato, Ademar Takashi [PETROBRAS, Rio de Janeiro, RJ (Brazil); Moura, Carlos Amsler [Comercial Perfuradora Delba Baiana Ltda., Rio de Janeiro, RJ (Brazil)

2004-07-01

A new drill pipe size, 5-7/8 in. OD, represents enabling technology for Extended Reach Drilling (ERD), deep water and other deep well applications. Most world-class ERD and deep water wells have traditionally been drilled with 5-1/2 in. drill pipe or a combination of 6-5/8 in. and 5-1/2 in. drill pipe. The hydraulic performance of 5-1/2 in. drill pipe can be a major limitation in substantial ERD and deep water wells resulting in poor cuttings removal, slower penetration rates, diminished control over well trajectory and more tendency for drill pipe sticking. The 5-7/8 in. drill pipe provides a significant improvement in hydraulic efficiency compared to 5-1/2 in. drill pipe and does not suffer from the disadvantages associated with use of 6-5/8 in. drill pipe. It represents a drill pipe assembly that is optimized dimensionally and on a performance basis for casing and bit programs that are commonly used for ERD, deep water and ultra-deep wells. The paper discusses the engineering philosophy behind 5-7/8 in. drill pipe, the design challenges associated with development of the product and reviews the features and capabilities of the second-generation double-shoulder connection. The paper provides drilling case history information on significant projects where the pipe has been used and details results achieved with the pipe. (author)

The Hans Tausen drill

DEFF Research Database (Denmark)

Johnsen, Sigfus Johann; Dahl-Jensen, Dorthe; Steffensen, Jørgen Peder

2007-01-01

In the mid-1990s, excellent results from the GRIP and GISP2 deep drilling projects in Greenland opened up funding for continued ice-coring efforts in Antarctica (EPICA) and Greenland (NorthGRIP). The Glaciology Group of the Niels Bohr Institute, University of Copenhagen, was assigned the task...... of providing drilling capability for these projects, as it had done for the GRIP project. The group decided to further simplify existing deep drill designs for better reliability and ease of handling. The drill design decided upon was successfully tested on Hans Tausen Ice Cap, Peary Land, Greenland, in 1995....... The 5.0 m long Hans Tausen (HT) drill was a prototype for the ~11 m long EPICA and NorthGRIP versions of the drill which were mechanically identical to the HT drill except for a much longer core barrel and chips chamber. These drills could deliver up to 4 m long ice cores after some design improvements...

Simulation of Ultrasonic Beam Focusing on a Defect in Anisotropic, Inhomogeneous Media

International Nuclear Information System (INIS)

Jeong, Hyun Jo; Cho, Sung Jong; Erdenetuya, Sharaa; Jung, Duck Yong

2011-01-01

In ultrasonic testing of dissimilar metal welds, application of phased array technique in terms of incident beam focusing is not easy because of complicated material structures formed during the multi-pass welding process. Time reversal(TR) techniques can overcome some limitations of phased array since they are self-focusing that does not depend on the geometrical and physical properties of testing components. In this paper, we test the possibility of TR focusing on a defect within anisotropic, heterogeneous austenitic welds. A commercial simulation software is employed for TR focusing and imaging of a side-drilled hole. The performance of time reversed adaptive focal law is compared with those of calculated focal laws for both anisotropic and isotropic welds

Physical and chemical mechanism underlying ultrasonically enhanced hydrochloric acid leaching of non-oxidative roasting of bastnaesite.

Science.gov (United States)

Zhang, Dongliang; Li, Mei; Gao, Kai; Li, Jianfei; Yan, Yujun; Liu, Xingyu

2017-11-01

In this study, we investigated an alternative to the conventional hydrochloric acid leaching of roasted bastnaesite. The studies suggested that the rare earth oxyfluorides in non-oxidatively roasted bastnaesite can be selectively leached only at elevated temperatures Further, the Ce(IV) in oxidatively roasted bastnaesite does not leach readily at low temperatures, and it is difficult to induce it to form a complex with F - ions in order to increase the leaching efficiency. Moreover, it is inevitably reduced to Ce(III) at elevated temperatures. Thus, the ultrasonically-assisted hydrochloric acid leaching of non-oxidatively roasted bastnaesite was studied in detail, including, the effects of several process factors and the, physical and chemical mechanisms underlying the leaching process. The results show that the leaching rate for the ultrasonically assisted process at 55°C (65% rare earth oxides) is almost the same as that for the conventional leaching process at 85°C. Based on the obtained results, it is concluded that ultrasonic cavitation plays a key role in the proposed process, resulting not only in a high shear stress, which damages the solid surface, but also in the formation of hydroxyl radicals (OH) and hydrogen peroxide (H 2 O 2 ). Standard electrode potential analysis and experimental results indicate that Ce(III) isoxidized by the hydroxyl radicals to Ce(IV), which can be leached with F - ions in the form of a complex, and that the Ce(IV) can subsequently be reduced to Ce(III) by the H 2 O 2. This prevents the Cl - ions in the solution from being oxidized to form chlorine. These results imply that the ultrasonically-assisted process can be used for the leaching of non-oxidatively roasted bastnaesite at low temperatures in the absence of a reductant. Copyright © 2017 Elsevier B.V. All rights reserved.

Effects of pore sizes and oxygen-containing functional groups on desulfurization activity of Fe/NAC prepared by ultrasonic-assisted impregnation

International Nuclear Information System (INIS)

Shu, Song; Guo, Jia-Xiu; Liu, Xiao-Li; Wang, Xue-Jiao; Yin, Hua-Qiang; Luo, De-Ming

2016-01-01

Graphical abstract: - Highlights: • Fe/NAC-60 exhibits the best desulfurization activity. • Different oscillation time can change surface area and pore volume of catalysts. • Ultrasonic oscillation increases Fe dispersion on carrier and effective pores. • Pore sizes play a crucial role during the SO 2 removal. - Abstract: A series of Fe-loaded activated carbons treated by HNO 3 (Fe/NAC) were prepared by incipient impregnation method with or without ultrasonic assistance and characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy with energy disperse spectroscope (SEM-EDS), transmission electron microscopy (TEM) and N 2 adsorption/desorption. The desulfurization activities were evaluated at a fixed bed reactor under a mixed gas simulated from flue gas. The results showed that desulfurization activity from excellent to poor is as follows: Fe/NAC-60 > Fe/NAC-80 > Fe/NAC-30 > Fe/NAC-15 > Fe/NAC-0 > Fe/NAC-100 > NAC. Fe/NAC-60 exhibits the best desulfurization activity and has breakthrough sulfur capacity of 319 mg/g and breakthrough time of 540 min. The introduction of ultrasonic oscillation does not change the form of Fe oxides on activated carbon but can change the dispersion and relative contents of Fe 3 O 4 . The types of oxygen-containing functional groups have no obvious change for all samples but the texture properties show some differences when they are oscillated for different times. The fresh Fe/NAC-60 has a surface area of 1045 m 2 /g and total pore volume of 0.961 cm 3 /g with micropore volume of 0.437 cm 3 /g and is larger than Fe/NAC-0 (823 m 2 /g, 0.733 and 0.342 cm 3 /g). After desulfurization, surface area and pore volume of all samples decrease significantly, and those of the exhausted Fe/NAC-60 decrease to 233 m 2 /g and 0.481 cm 3 /g, indicating that some byproducts deposit on surface to cover pores. Pore size distribution influences SO 2 adsorption, and fresh Fe/NAC-60 has

Drilling contracts and incentives

International Nuclear Information System (INIS)

Osmundsen, Petter; Sorenes, Terje; Toft, Anders

2008-01-01

Shortages of rigs and personnel have encouraged discussion of designing incentive contracts in the drilling sector. However, for the drilling contracts, there are not a large variety of contract types in use. This article describes and analyses incentives for drilling contractors. These are directly represented by the compensation formats utilised in the present and in the consecutive drilling contracts. Indirectly, incentives are also provided by the evaluation criteria that oil companies use for awarding drilling assignments. Changes in contract format pose a number of relevant questions relating to resource management, and the article takes an in-depth look at some of these. Do evaluation criteria for awarding drilling assignments encourage the development of new technology and solutions? How will a stronger focus on drilling efficiency influence reservoir utilisation?

Laser-assisted fabrication of materials

CERN Document Server

Manna, Indranil

2013-01-01

Laser assisted fabrication involves shaping of materials using laser as a source of heat. It can be achieved by removal of materials (laser assisted cutting, drilling, etc.), deformation (bending, extrusion), joining (welding, soldering) and addition of materials (surface cladding or direct laser cladding). This book on ´Laser assisted Fabrication’ is aimed at developing in-depth engineering concepts on various laser assisted macro and micro-fabrication techniques with the focus on application and a review of the engineering background of different micro/macro-fabrication techniques, thermal history of the treated zone and microstructural development and evolution of properties of the treated zone.

Patients' perception of pain during ultrasonic debridement: a comparison between piezoelectric and magnetostrictive scalers.

Science.gov (United States)

Muhney, Kelly A; Dechow, Paul C

2010-01-01

To compare patients' perception of discomfort, vibration and noise levels between piezoelectric and the magnetostrictive ultrasonic units during periodontal debridement. Periodontal debridement was performed on 75 subjects using a split-mouth design. Two quadrants on the same side were instrumented with a piezoelectric ultrasonic device (EMS Swiss Mini Master® Piezon) and the remaining 2 quadrants were instrumented with a magnetostrictive ultrasonic device (Dentsply Cavitron® SPS™). Subjects marked between 0 and 100 along a visual analog scale (VAS) for each of the 3 variables immediately after treatment of each half of the dentition. Scores of the VAS were compared using a nonparametric test for paired data, the Wilcoxon Signed-Rank test. The level of significance was set at ptypes were almost equal. The results show that, on average, patients in this study prefer instrumentation with the piezoelectric as it relates to awareness of associated discomfort and vibration. The results of this study may assist the clinician in the decision over which ultrasonic device may prove more beneficial in decreasing patient discomfort and increasing patient compliance.

Measurement of a 3D Ultrasonic Wavefield Using Pulsed Laser Holographic Microscopy for Ultrasonic Nondestructive Evaluation

Directory of Open Access Journals (Sweden)

Xing Wang

2018-02-01

Full Text Available In ultrasonic array imaging, 3D ultrasonic wavefields are normally recorded by an ultrasonic piezo array transducer. Its performance is limited by the configuration and size of the array transducer. In this paper, a method based on digital holographic interferometry is proposed to record the 3D ultrasonic wavefields instead of the array transducer, and the measurement system consisting of a pulsed laser, ultrasonic excitation, and synchronization and control circuit is designed. A consecutive sequence of holograms of ultrasonic wavefields are recorded by the system. The interferograms are calculated from the recorded holograms at different time sequence. The amplitudes and phases of the transient ultrasonic wavefields are recovered from the interferograms by phase unwrapping. The consecutive sequence of transient ultrasonic wavefields are stacked together to generate 3D ultrasonic wavefields. Simulation and experiments are carried out to verify the proposed technique, and preliminary results are presented.

Production of glutinous rice flour from broken rice via ultrasonic assisted extraction of amylose.

Science.gov (United States)

Setyawati, Yohana Dwi; Ahsan, Sitti Faika; Ong, Lu Ki; Soetaredjo, Felycia Edi; Ismadji, Suryadi; Ju, Yi-Hsu

2016-07-15

In this study, a modified aqueous leaching method by complex formation of amylose with glycerol was employed for reducing the amylose content of starch in broken white rice to less than 2%, so that the resulting starch can be classified to that of glutinous rice flour. By employing ultrasonication in alkaline condition, extraction of amylose could be performed by washing at lower temperature in shorter time compared to the existing aqueous leaching method. The effects of glycerol concentration, alkali concentration, ultrasonication and treatment time on the amylose content of the treated starch were systematically investigated. Under optimum condition, amylose content of broken white rice starch can be reduced from 27.27% to 1.43% with a yield of 80.42%. The changes in the physicochemical properties of the rice flour before and after treatment were studied. Copyright © 2016 Elsevier Ltd. All rights reserved.

Sonochemical analysis of the output of ultrasonic dental descalers

OpenAIRE

King, David

2010-01-01

Ultrasonic descalers are used in dentistry to remove calculus and other contaminants from teeth. One mechanism which may assist in the cleaning is cavitation generated in cooling water around the descaler. The spatial distribution of cavitation around three designs of descaler tips and under three load conditions has been observed using sonochemiluminescence from a luminol solution and compared with the vibratory motion of the tips in a water bath, characterised by scanning laser vibrometry. ...

Dual ultrasonic-assisted dispersive liquid-liquid microextraction coupled with microwave-assisted derivatization for simultaneous determination of 20(S)-protopanaxadiol and 20(S)-protopanaxatriol by ultra high performance liquid chromatography-tandem mass spectrometry.

Science.gov (United States)

Zhao, Xian-En; Lv, Tao; Zhu, Shuyun; Qu, Fei; Chen, Guang; He, Yongrui; Wei, Na; Li, Guoliang; Xia, Lian; Sun, Zhiwei; Zhang, Shijuan; You, Jinmao; Liu, Shu; Liu, Zhiqiang; Sun, Jing; Liu, Shuying

2016-03-11

This paper, for the first time, reported a speedy hyphenated technique of low toxic dual ultrasonic-assisted dispersive liquid-liquid microextraction (dual-UADLLME) coupled with microwave-assisted derivatization (MAD) for the simultaneous determination of 20(S)-protopanaxadiol (PPD) and 20(S)-protopanaxatriol (PPT). The developed method was based on ultra high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) detection using multiple-reaction monitoring (MRM) mode. A mass spectrometry sensitizing reagent, 4'-carboxy-substituted rosamine (CSR) with high reaction activity and ionization efficiency was synthesized and firstly used as derivatization reagent. Parameters of dual-UADLLME, MAD and UHPLC-MS/MS conditions were all optimized in detail. Low toxic brominated solvents were used as extractant instead of traditional chlorinated solvents. Satisfactory linearity, recovery, repeatability, accuracy and precision, absence of matrix effect and extremely low limits of detection (LODs, 0.010 and 0.015ng/mL for PPD and PPT, respectively) were achieved. The main advantages were rapid, sensitive and environmentally friendly, and exhibited high selectivity, accuracy and good matrix effect results. The proposed method was successfully applied to pharmacokinetics of PPD and PPT in rat plasma. Copyright © 2016 Elsevier B.V. All rights reserved.

Study on drilling induced delamination of woven kenaf fiber reinforced epoxy composite using carbide drills

Science.gov (United States)

Suhaily, M.; Hassan, C. H. Che; Jaharah, A. G.; Azmi, H.; Afifah, M. A.; Khairusshima, M. K. Nor

2018-04-01

In this research study, it presents the influences of drilling parameters on the delamination factor during the drilling of woven kenaf fiber reinforced epoxy composite laminates when using the carbide drill bits. The purpose of this study is to investigate the influence of drilling parameters such as cutting speed, feed rate and drill sizes on the delamination produced when drilling woven kenaf reinforced epoxy composite using the non-coated carbide drill bits. The damage generated on the woven kenaf reinforced epoxy composite laminates were observed both at the entrance and exit surface during the drilling operation. The experiments were conducted according to the Box Behnken experimental designs. The results indicated that the drill diameter has a significant influence on the delamination when drilling the woven kenaf fiber reinforced epoxy composites.

Salt-Assisted Ultrasonicated De-Aggregation and Advanced Redox Electrochemistry of Detonation Nanodiamond

Directory of Open Access Journals (Sweden)

Sanju Gupta

2017-11-01

Full Text Available Nanodiamond particles form agglomerates in the dry powder state and this poses limitation to the accessibility of their diamond-like core thus dramatically impacting their technological advancement. In this work, we report de-agglomeration of nanodiamond (ND by using a facile technique namely, salt-assisted ultrasonic de-agglomeration (SAUD. Utilizing ultrasound energy and ionic salts (sodium chloride and sodium acetate, SAUD is expected to break apart thermally treated nanodiamond aggregates (~50–100 nm and produce an aqueous slurry of de-aggregated stable colloidal nanodiamond dispersions by virtue of ionic interactions and electrostatic stabilization. Moreover, the SAUD technique neither has toxic chemicals nor is it difficult to remove impurities and therefore the isolated nanodiamonds produced are exceptionally suited for engineered nanocarbon for mechanical (composites, lubricants and biomedical (bio-labeling, biosensing, bioimaging, theranostic applications. We characterized the microscopic structure using complementary techniques including transmission electron microscopy combined with selected-area electron diffraction, optical and vibrational spectroscopy. We immobilized SAUD produced NDs on boron-doped diamond electrodes to investigate fundamental electrochemical properties. They included surface potential (or Fermi energy level, carrier density and mapping electrochemical (reactivity using advanced scanning electrochemical microscopy in the presence of a redox-active probe, with the aim of understanding the surface redox chemistry and the interfacial process of isolated nanodiamond particles as opposed to aggregated and untreated nanoparticles. The experimental findings are discussed in terms of stable colloids, quantum confinement and predominantly surface effects, defect sites (sp2–bonded C and unsaturated bonds, inner core (sp3–bonded C/outer shell (sp2–bonded C structure, and surface functionality. Moreover, the surface

Drilling technologies in hydrogeological survey

OpenAIRE

Vorlíček, Petr

2014-01-01

This work deals with the drilling technologies used in hydrogeology. The main aim of the work is to explore types of drilling technologies used at hydrogeological drilling wells and modern technologies that could potentially be used in the future. The work also summarizes a historical development of drilling techniques, a drilling process procedure, information obtained from boreholes and the most common types of drilling fluids.

Design and Exploitation Problems of Drill String in Directional Drilling

Directory of Open Access Journals (Sweden)

Bednarz Stanislaw

2004-09-01

Full Text Available Drill string design for directional drilling requires accounting for a number of factors. First, types and expected values of loads should be determined. Then, elements of the drill string should be so selected as to enable realization of the plan at specified loads. Some of additional factors, e. g. purchase, exploitation cost, geological conditions in the bore-hole, washing of the bore-hole, stability, trajectory, rig parameters, accuracy of gauges, pumps parameters remain in conflict. Drill pipes are made of rolled pipes, upset and welded with tool joints to 9,5 m long; the shorter ones can be made of hot forged rods. Exploitation requirements, being a result of practical experience supported by theoretical and laboratory analyses should be a part of syllabuses of technical staff educational programs. Apart from designing the string, it is also vital to lower the risk of a drilling failure. The significance of these aspects seems to be unquestionable.

Diagnostic System of Drill Condition in Laminated Chipboard Drilling Process

Directory of Open Access Journals (Sweden)

Swiderski Bartosz

2017-01-01

Full Text Available The paper presents an on-line automatic system for recognition of the drill condition in a laminated chipboard drilling process. Two states of the drill are considered: the sharp enough (still able to drill holes acceptable for processing quality and worn out (excessive drill wear, not satisfactory from the quality point of view of the process. The automatic system requires defining the diagnostic features, which are used as the input attributes to the classifier. The features have been generated from 5 registered signals: feed force, cutting torque, noise, vibration and acoustic emission. The statistical parameters defined on the basis of the auto regression model of these signals have been used as the diagnostic features. The sequential step-wise feature selection is applied for choosing the most discriminative set of features. The final step of recognition is done by support vector machine classifier working in leave one out mode. The results of numerical experiments have confirmed good quality of the proposed diagnostic system.

Ultrasonic unit for line-by-line ultrasonic scanning of bodies

International Nuclear Information System (INIS)

Soldner, R.

1978-01-01

The ultrasonic unit for medical diagnostics operates by the sectorial scanning principle, which avoids direct coupling of the transducer head to the surface of the body. For this purpose, several transmitter/receiver units (approx. 100) are arranged on a partial ring of a circular arc and the ultrasonic beams, which can be triggered sequentially in time, are directed at a common intersection behind the ultrasonic window of the unit, i.e., outside the unit. A mechanical system is employed to set and adjust the partial ring carrying the transmitter/receiver units. (DG) [de

Horizontal drilling under Lake Erie

Energy Technology Data Exchange (ETDEWEB)

Meller, R.

2001-07-01

Drilling oil wells under Lake Erie calls for horizontal drilling wells to be drilled from shore out into the pay-zone under the lake. The nature and characteristics of horizontal wells as compared to vertical wells are explored. Considerations that have to be taken into account in drilling horizontal wells are explained (the degree of curvature, drilling fluid quality, geosteering in the pay-zone, steering instrumentation, measurements while drilling (MWD), logging while drilling (LWD)). The concept and reasons for extended reach wells are outlined, along with characteristic features of multilateral wells.

Ultrasonic-assisted synthesis of magnetite based MRI contrast agent using cysteine as the biocapping coating

International Nuclear Information System (INIS)

Ahmadi, Reza; Malek, Mahrooz; Hosseini, Hamid Reza Madaah; Shokrgozar, Mohammad Ali; Oghabian, Mohammad Ali; Masoudi, Afshin; Gu Ning; Zhang Yu

2011-01-01

Highlights: ► We used cysteine as surfactant to synthesize stable magnetite-based ferrofluids. ► pH increase from 11 to 12 led to particle size decrease from 19.58 to 10.02 nm. ► Cytotoxicity assay showed that synthesized particles were biocompatible. ► MRI results showed that magnetite particles were accumulated in lymph nodes. - Abstract: Magnetite nanoparticles (mean particle size ranging from 10 to 20 nm) were prepared by a biomolecule-assisted solution-phase approach under ultrasonic irradiation. Cysteine was used as the capping agent in the solution. The results show that cysteine could be an efficient biocapping agent in producing Fe 3 O 4 nanoparticles. The crystal structure and magnetic properties of the nanoparticles were characterized by XRD and VSM techniques, respectively. FT-IR was used to investigate the presence of cysteine on the nanoparticles surface. The influence of pH value of the solution on the size distribution and hydrodynamic size of nanoparticles were studied by TEM and DLS methods, respectively. The MTT assay performed by incubation of L929 cells, showed the good biocompability of synthesized ferrofluids. In vitro T1 and T2 relaxivity measurements along with in vivo studies, which were conducted on rats, demonstrate that synthesized nanoparticles are applicable as the contrast agents, especially for imaging of the lymphatic system.

Feasibility study of ultrasonic elliptical vibration-assisted reaming of carbon fiber reinforced plastics/titanium alloy stacks.

Science.gov (United States)

Geng, Daxi; Zhang, Deyuan; Li, Zhe; Liu, Dapeng

2017-03-01

The production of high quality bolt holes, especially on the carbon fiber reinforced plastics/titanium alloy (CFRP/Ti) stacks, is essential to the manufacturing process in order to facilitate part assembly and improve the component mechanical integrity in aerospace industry. Reaming is widely used as a mandatory operation for bolt holes to meet the strict industry requirements. In this paper, the ultrasonic elliptical vibration-assisted reaming (UEVR) which is considered as a new method for finish machining of CFRP/Ti stacked holes is studied. The paper outlines an analysis of tool performance and hole quality in UEVR compared with that in conventional reaming (CR). Experimental results show that the quality of holes was significantly improved in UEVR. This is substantiated by monitoring cutting force, hole geometric precision and surface finish. The average thrust forces and torque in UEVR were decreased over 30% and 60% respectively. It is found that, during first 45 holes, better diameter tolerance (IT7 vs. IT8), smaller diameter difference of CFRP and Ti holes (around 3μm vs. 12μm), better geometrical errors were achieved in UEVR as compared to CR. As for surface finish, both of the average roughness and hole surface topography in UEVR were obviously improved. Copyright © 2016 Elsevier B.V. All rights reserved.

Alteration in the IRDP drill hole compared with other drill holes in Iceland

Science.gov (United States)

Kristmannsdóttir, Hrefna

1982-08-01

The overall alteration pattern in the drill hole at Reydarfjördur is very similar to alteration patterns observed in Icelandic geothermal areas and in low-grade metamorphosed basalts in deep crustal sections elsewhere in Iceland. However more detail is obtained by the study of the IRDP drill core than by study of drill cuttings sampled in previous drill holes in Iceland. A comparatively high fossil thermal gradient is obtained at Reydarfjördur by a combination of mineral stability data and the observed occurence of secondary minerals. This high gradient is consistent with the measured dike dilation at the drill site and the location of the drill site adjacent to a central volcano.

Arthroscopically assisted stabilization of acute high-grade acromioclavicular joint separations in a coracoclavicular Double-TightRope technique: V-shaped versus parallel drill hole orientation.

Science.gov (United States)

Kraus, Natascha; Haas, Norbert P; Scheibel, Markus; Gerhardt, Christian

2013-10-01

The arthroscopically assisted Double-TightRope technique has recently been reported to yield good to excellent clinical results in the treatment of acute, high-grade acromioclavicular dislocation. However, the orientation of the transclavicular-transcoracoidal drill holes remains a matter of debate. A V-shaped drill hole orientation leads to better clinical and radiologic results and provides a higher vertical and horizontal stability compared to parallel drill hole placement. This was a cohort study; level of evidence, 2b. Two groups of patients with acute high-grade acromioclavicular joint instability (Rockwood type V) were included in this prospective, non-randomized cohort study. 15 patients (1 female/14 male) with a mean age of 37.7 (18-66) years were treated with a Double-TightRope technique using a V-shaped orientation of the drill holes (group 1). 13 patients (1 female/12 male) with a mean age of 40.9 (21-59) years were treated with a Double-TightRope technique with a parallel drill hole placement (group 2). After 2 years, the final evaluation consisted of a complete physical examination of both shoulders, evaluation of the Subjective Shoulder Value (SSV), Constant Score (CS), Taft Score (TF) and Acromioclavicular Joint Instability Score (ACJI) as well as a radiologic examination including bilateral anteroposterior stress views and bilateral Alexander views. After a mean follow-up of 2 years, all patients were free of shoulder pain at rest and during daily activities. Range of motion did not differ significantly between both groups (p > 0.05). Patients in group 1 reached on average 92.4 points in the CS, 96.2 % in the SSV, 10.5 points in the TF and 75.9 points in the ACJI. Patients in group 2 scored 90.5 points in the CS, 93.9 % in the SSV, 10.5 points in the TF and 84.5 points in the ACJI (p > 0.05). Radiographically, the coracoclavicular distance was found to be 13.9 mm (group 1) and 13.4 mm (group 2) on the affected side and 9.3 mm (group 1

Ultrasonically assisted hydrothermal synthesis of activated carbon-HKUST-1-MOF hybrid for efficient simultaneous ultrasound-assisted removal of ternary organic dyes and antibacterial investigation: Taguchi optimization.

Science.gov (United States)

Azad, F Nasiri; Ghaedi, M; Dashtian, K; Hajati, S; Pezeshkpour, V

2016-07-01

Activated carbon (AC) composite with HKUST-1 metal organic framework (AC-HKUST-1 MOF) was prepared by ultrasonically assisted hydrothermal method and characterized by FTIR, SEM and XRD analysis and laterally was applied for the simultaneous ultrasound-assisted removal of crystal violet (CV), disulfine blue (DSB) and quinoline yellow (QY) dyes in their ternary solution. In addition, this material, was screened in vitro for their antibacterial actively against Methicillin-resistant Staphylococcus aureus (MRSA) and Pseudomonas aeruginosa (PAO1) bacteria. In dyes removal process, the effects of important variables such as initial concentration of dyes, adsorbent mass, pH and sonication time on adsorption process optimized by Taguchi approach. Optimum values of 4, 0.02 g, 4 min, 10 mg L(-1) were obtained for pH, AC-HKUST-1 MOF mass, sonication time and the concentration of each dye, respectively. At the optimized condition, the removal percentages of CV, DSB and QY were found to be 99.76%, 91.10%, and 90.75%, respectively, with desirability of 0.989. Kinetics of adsorption processes follow pseudo-second-order model. The Langmuir model as best method with high applicability for representation of experimental data, while maximum mono layer adsorption capacity for CV, DSB and QY on AC-HKUST-1 estimated to be 133.33, 129.87 and 65.37 mg g(-1) which significantly were higher than HKUST-1 as sole material with Qm to equate 59.45, 57.14 and 38.80 mg g(-1), respectively. Copyright © 2016 Elsevier B.V. All rights reserved.

A self propelled drilling system for hard-rock, horizontal and coiled tube drilling

Energy Technology Data Exchange (ETDEWEB)

Biglin, D.; Wassell, M.

1997-12-31

Several advancements are needed to improve the efficiency and reliability of both hard rock drilling and extended reach drilling. This paper will present a Self Propelled Drilling System (SPDS) which can grip the borehole wall in order to provide a stable platform for the application of weight on bit (WOB) and resisting the reactive torque created by the downhole drilling motor, bit and formation interaction. The system will also dampen the damaging effects of drill string vibration. This tool employs two hydraulically activated anchors (front and rear) to grip the borehole wall, and a two-way thrust mandrel to apply both the drilling force to the bit, and a retraction force to pull the drill string into the hole. Forward drilling motion will commence by sequencing the anchor pistons and thrust mandrel to allow the tool to walk in a stepping motion. The SPDS has a microprocessor to control valve timing, sensing and communication functions. An optional Measurement While Drilling (MWD) interface can provide two-way communication of critical operating parameters such as hydraulic pressure and piston location. This information can then be telemetered to the surface, or used downhole to autonomously control system parameters such as anchor and thrust force or damping characteristics.

ATUCHA I NPP - Emergency drill practice

International Nuclear Information System (INIS)

Sanda, Alejandro; Rosales, Gabriel

2008-01-01

River Parana de las Palmas; -) Safe location for affected citizens; -) Iodide Potassium pills distribution; -) Safety plan for Lima and adjacent islands; -) Reception of evacuated people; -) Wounded people triage; -) Derivation of contaminated wounded people, Decontamination; -) Social Assistance for affected people; -) Nuclear Regulatory inspection of tasks and procedures; -) Radiological monitoring of the contaminated zone. Once the drill is over, the procedure is jointly analyzed by the participants. After the meeting the corrective actions necessary in case of a real emergency are set. (author)

Laser Drilling - Drilling with the Power of Light

Energy Technology Data Exchange (ETDEWEB)

Iraj A. Salehi; Brian C. Gahan; Samih Batarseh

2007-02-28

Gas Technology Institute (GTI) has been the leading investigator in the field of high power laser applications research for well construction and completion applications. Since 1997, GTI (then as Gas Research Institute- GRI) has investigated several military and industrial laser systems and their ability to cut and drill into reservoir type rocks. In this report, GTI continues its investigation with a 5.34 kW ytterbium-doped multi-clad high power fiber laser (HPFL). When compared to its competitors; the HPFL represents a technology that is more cost effective to operate, capable of remote operations, and requires considerably less maintenance and repair. Work performed under this contract included design and implementation of laboratory experiments to investigate the effects of high power laser energy on a variety of rock types. All previous laser/rock interaction tests were performed on samples in the lab at atmospheric pressure. To determine the effect of downhole pressure conditions, a sophisticated tri-axial cell was designed and tested. For the first time, Berea sandstone, limestone and clad core samples were lased under various combinations of confining, axial and pore pressures. Composite core samples consisted of steel cemented to rock in an effort to represent material penetrated in a cased hole. The results of this experiment will assist in the development of a downhole laser perforation or side tracking prototype tool. To determine how this promising laser would perform under high pressure in-situ conditions, GTI performed a number of experiments with results directly comparable to previous data. Experiments were designed to investigate the effect of laser input parameters on representative reservoir rock types of sandstone and limestone. The focus of the experiments was on laser/rock interaction under confining pressure as would be the case for all drilling and completion operations. As such, the results would be applicable to drilling, perforation, and

Modeling pellet impact drilling process

Science.gov (United States)

Kovalyov, A. V.; Ryabchikov, S. Ya; Isaev, Ye D.; Ulyanova, O. S.

2016-03-01

The paper describes pellet impact drilling which could be used to increase the drilling speed and the rate of penetration when drilling hard rocks. Pellet impact drilling implies rock destruction by metal pellets with high kinetic energy in the immediate vicinity of the earth formation encountered. The pellets are circulated in the bottom hole by a high velocity fluid jet, which is the principle component of the ejector pellet impact drill bit. The experiments conducted has allowed modeling the process of pellet impact drilling, which creates the scientific and methodological basis for engineering design of drilling operations under different geo-technical conditions.

Optimization of Ionic Liquid Based Simultaneous Ultrasonic- and Microwave-Assisted Extraction of Rutin and Quercetin from Leaves of Velvetleaf (Abutilon theophrasti by Response Surface Methodology

Directory of Open Access Journals (Sweden)

Chunjian Zhao

2014-01-01

Full Text Available An ionic liquids based simultaneous ultrasonic and microwave assisted extraction (ILs-UMAE method has been proposed for the extraction of rutin (RU, quercetin (QU, from velvetleaf leaves. The influential parameters of the ILs-UMAE were optimized by the single factor and the central composite design (CCD experiments. A 2.00 M 1-butyl-3-methylimidazolium bromide ([C4mim]Br was used as the experimental ionic liquid, extraction temperature 60°C, extraction time 12 min, liquid-solid ratio 32 mL/g, microwave power of 534 W, and a fixed ultrasonic power of 50 W. Compared to conventional heating reflux extraction (HRE, the RU and QU extraction yields obtained by ILs-UMAE were, respectively, 5.49 mg/g and 0.27 mg/g, which increased, respectively, 2.01-fold and 2.34-fold with the recoveries that were in the range of 97.62–102.36% for RU and 97.33–102.21% for QU with RSDs lower than 3.2% under the optimized UMAE conditions. In addition, the shorter extraction time was used in ILs-UMAE, compared with HRE. Therefore, ILs-UMAE was a rapid and an efficient method for the extraction of RU and QU from the leaves of velvetleaf.

Ultrasonic-assisted extraction and in-vitro antioxidant activity of polysaccharide from Hibiscus leaf.

Science.gov (United States)

Afshari, Kasra; Samavati, Vahid; Shahidi, Seyed-Ahmad

2015-03-01

The effects of ultrasonic power, extraction time, extraction temperature, and the water-to-raw material ratio on extraction yield of crude polysaccharide from the leaf of Hibiscus rosa-sinensis (HRLP) were optimized by statistical analysis using response surface methodology. The response surface methodology (RSM) was used to optimize HRLP extraction yield by implementing the Box-Behnken design (BBD). The experimental data obtained were fitted to a second-order polynomial equation using multiple regression analysis and also analyzed by appropriate statistical methods (ANOVA). Analysis of the results showed that the linear and quadratic terms of these four variables had significant effects. The optimal conditions for the highest extraction yield of HRLP were: ultrasonic power, 93.59 W; extraction time, 25.71 min; extraction temperature, 93.18°C; and the water to raw material ratio, 24.3 mL/g. Under these conditions, the experimental yield was 9.66±0.18%, which is well in close agreement with the value predicted by the model 9.526%. The results demonstrated that HRLP had strong scavenging activities in vitro on DPPH and hydroxyl radicals. Copyright © 2014 Elsevier B.V. All rights reserved.

Comparison of Enzymatic and Ultrasonic Extraction of Albumin from Defatted Pumpkin (Cucurbita pepo Seed Powder

Directory of Open Access Journals (Sweden)

Gia Loi Tu

2015-01-01

Full Text Available In this study, ultrasound- and enzyme-assisted extractions of albumin (water-soluble protein group from defatted pumpkin (Cucurbita pepo seed powder were compared. Both advanced extraction techniques strongly increased the albumin yield in comparison with conventional extraction. The extraction rate was two times faster in the ultrasonic extraction than in the enzymatic extraction. However, the maximum albumin yield was 16 % higher when using enzymatic extraction. Functional properties of the pumpkin seed albumin concentrates obtained using the enzymatic, ultrasonic and conventional methods were then evaluated. Use of hydrolase for degradation of cell wall of the plant material did not change the functional properties of the albumin concentrate in comparison with the conventional extraction. The ultrasonic extraction enhanced water-holding, oil-holding and emulsifying capacities of the pumpkin seed albumin concentrate, but slightly reduced the foaming capacity, and emulsion and foam stability.

Performance investigation on the ultrasonic atomization liquid desiccant regeneration system

International Nuclear Information System (INIS)

Yang, Zili; Zhang, Kaisheng; Hwang, Yunho; Lian, Zhiwei

2016-01-01

was less than 7.0% of total energy cost. Moreover, when the UARS is integrated with the ultrasonic atomization assisted dehumidifier, energy savings can reach up to 60.4% as compared with the packed-bed system. This study validated the feasibility and energy saving potential of applying ultrasonic atomization technology to liquid desiccant regeneration systems.

Methods to ensure optimal off-bottom and drill bit distance under pellet impact drilling

Science.gov (United States)

Kovalyov, A. V.; Isaev, Ye D.; Vagapov, A. R.; Urnish, V. V.; Ulyanova, O. S.

2016-09-01

The paper describes pellet impact drilling which could be used to increase the drilling speed and the rate of penetration when drilling hard rock for various purposes. Pellet impact drilling implies rock destruction by metal pellets with high kinetic energy in the immediate vicinity of the earth formation encountered. The pellets are circulated in the bottom hole by a high velocity fluid jet, which is the principle component of the ejector pellet impact drill bit. The paper presents the survey of methods ensuring an optimal off-bottom and a drill bit distance. The analysis of methods shows that the issue is topical and requires further research.

Ultrasonic extraction, antioxidant and anticancer activities of novel polysaccharides from Chuanxiong rhizome.

Science.gov (United States)

Hu, Jie; Jia, Xuejing; Fang, Xiaobin; Li, Peng; He, Chengwei; Chen, Meiwan

2016-04-01

Ultrasonic-assisted extraction technology was employed to prepare Ligusticum chuanxiong Hort polysaccharide. Single factor test and orthogonal experimental design were used to optimize the extraction conditions. The results showed that the optimal extraction conditions consisted of ultrasonic temperature of 80°C, ultrasonic time of 40 min and water to raw material ratio of 30 mL/g. Three novel polysaccharides fractions, LCX0, LCX1 and LCX2, were isolated and purified from the crude polysaccharides using DEAE-52 cellulose and Sephadex G-100 column chromatography. The molecular weight and monosaccharide composition of three LCX polysaccharides fractions were analyzed with gel permeation chromatography (GPC) and HPLC analysis, respectively. Furthermore, the antioxidant and in vitro anticancer activities of the polysaccharides were investigated. Compared with LCX0, LCX2 and LCX1 showed relative higher antioxidant activity and inhibitory activity to the growth of HepG2, SMMC7721, A549 and HCT-116 cells. It is suggested that the novel polysaccharides from rhizome of L. chuanxiong could be promising bioactive macromolecules for biomedical use. Copyright © 2016. Published by Elsevier B.V.

Improved techniques for the ultrasonic characterization of graphite

International Nuclear Information System (INIS)

Cook, K.V.; Simpson, W.A.

1981-01-01

Near-conventional pulse-echo flaw detection techniques can be successfully applied to graphite material. If the specimen configuration (i.e., length-to-diameter ratio) is conducive to the choice of ultrasonic test parameters dictated by the material screening tests, then only the test sensitivity needs to be established. Conventional test block approaches to calibration work well; however, uniform homogeneity of the specimens to be tested must be assumed (depending on the graphite, this may be an invalid assumption). Sensitivities that we have demonstrated typically detect 0.5- to 0.75-mm (0.020 to 0.030-in.) reflectors at depths up to 102 mm (4 in.) for GRAPHNOL (drilled holes, not flat bottom). Other materials may dictate inspection for much larger discontinuities. The least sensitive tests performed to date (using the storage oscilloscope approach) required flat-bottom holes of 6.35 mm (0.250 in.) in diameter for calibration. This relatively insensitive test was necessary because of the billet length and material characteristics

A new approach involving a multi transducer ultrasonic system for cleaning turbine engines' oil filters under practical conditions.

Science.gov (United States)

Nguyen, Dinh Duc; Ngo, Huu Hao; Yoon, Yong Soo; Chang, Soon Woong; Bui, Hong Ha

2016-09-01

The purpose of this paper is to provide a green technology that can clean turbine engine oil filters effectively in ships using ultrasound, with ultrasonic devices having a frequency of 25kHz and different powers of 300W and 600W, respectively. The effects of temperature, ultrasonic cleaning times, pressure losses through the oil filter, solvent washing, and ultrasonic power devices were investigated. In addition, the cleaning efficiency of three modes (hand washing, preliminary washing and ultrasonic washing) were compared to assess their relative effectiveness. Experimental results revealed that the necessary ultrasonic time varied significantly depending on which solvent was used for washing. For instance, the optimum ultrasonic cleaning time was 50-60min when the oil filter was cleaned in a solvent of kerosene oil (KO) and over 80min when in a solvent of diesel oil (DO) using the same ultrasonic generator device (25kHz, 600W) and experimental conditions. Furthermore, microscopic examination did not reveal any damage or breakdown on or within the structure of the filter after ultrasonic cleaning, even in the filter's surfaces at a constantly low frequency of 25kHz and power specific capacity (100W/gal). Overall, it may be concluded that ultrasound-assisted oil filter washing is effective, requiring a significantly shorter time than manual washing. This ultrasonic method also shows promise as a green technology for washing oil filters in turbine engines in general and Vietnamese navy ships in particular, because of its high cleaning efficiency, operational simplicity and savings. Copyright © 2016 Elsevier B.V. All rights reserved.

Ultrasonic grinding method

International Nuclear Information System (INIS)

Miyahara, Shuji.

1990-01-01

An ultrasonic generator and a liquid supply nozzle are opposed to an object to be ground and a pump is started in this state to supply an organic solvent. Matters to be decontaminated which adheres to the surface of the object to be ground and are difficult to be removed by a mere mechanical removing method can be eliminated previously by the surface active effect of the organic solvent such as ethanol prior to the oscillation of the ultrasonic generator. Subsequently, when the ultrasonic generator is oscillated, scales in the floated state can be removed simply. Further, since the organic solvent can penetrate to provide the surface active effect even in such a narrow portion that the top end of the ultrasonic generator is difficult to the intruded at the surface of the object to be ground, the decontaminating treatment can be applied also to such a narrow portion. (T.M.)

Evaluate of the Effects of Drilling with Varying Spindle Speed Using Different Thickness of GFRP on the Damage Factor

Directory of Open Access Journals (Sweden)

Keong Woo Tze

2014-07-01

Full Text Available Composite have been widely used in industries which such as aircraft structural components, electric and electronics components, aerospace, and oil and gas fields due to their superior mechanical properties. Among machining process, drilling can be considered as one of the most important process in final machining of composite. In this research, vacuum assisted resin infusion method is use in fabricating the glass fiber reinforcement polymer samples, where different thickness of GFRP were used in the drilling process with different spindle speed. The results show that the temperature influences the damage factor of the drilling. Higher spindle speed will generate higher temperature that softens the matrix thus generating lower damage factor. The suitable drill bit temperature is between 150-200°C

Qualification of phased array ultrasonic examination on T-joint weld of austenitic stainless steel for ITER vacuum vessel

Energy Technology Data Exchange (ETDEWEB)

Kim, G.H. [ITER Korea, National Fusion Research Institute, Daejeon 305-333 (Korea, Republic of); Park, C.K., E-mail: love879@hanmail.net [ITER Korea, National Fusion Research Institute, Daejeon 305-333 (Korea, Republic of); Jin, S.W.; Kim, H.S.; Hong, K.H.; Lee, Y.J.; Ahn, H.J.; Chung, W. [ITER Korea, National Fusion Research Institute, Daejeon 305-333 (Korea, Republic of); Jung, Y.H.; Roh, B.R. [Hyundai Heavy Industries Co. Ltd., Ulsan 682-792 (Korea, Republic of); Sa, J.W.; Choi, C.H. [ITER Organization, Route de Vinon-sur-Verdon, CS 90 046, 13067 St. Paul Lez Durance Cedex (France)

2016-11-01

Highlights: • PAUT techniques has been developed by Hyundai Heavy Industries Co., LTD (HHI) and Korea Domestic Agency (KODA) to verify and settle down instrument calibration, test procedures, image processing, and so on. As the first step of development for PAUT technique, Several dozens of qualification blocks with artificial defects, which are parallel side drilled hole, embedded lack of fusion, embedded repair weld notch, and so on, have been designed and fabricated to simulate all potential defects during welding process. Real UT qualification group-1 for T-joint weld was successfully conducted in front of ANB inspector. • In this paper, remarkable progresses of UT qualification are presented for ITER vacuum vessel. - Abstract: Full penetration welding and 100% volumetric examination are required for all welds of pressure retaining parts of the ITER Vacuum Vessel (VV) according to RCC-MR Code and French Order of Nuclear Pressure Equipment (ESPN). The NDE requirement is one of important technical issues because radiographic examination (RT) is not applicable to many welding joints. Therefore the ultrasonic examination (UT) has been selected as an alternative method. Generally the UT on the austenitic welds is regarded as a great challenge due to the high attenuation and dispersion of the ultrasonic signal. In this paper, Phased array ultrasonic examination (PAUT) has been introduced on double sided T-shape austenitic welds of the ITER VV as a major NDE method as well as RT. Several dozens of qualification blocks with artificial defects, which are parallel side drilled hole, embedded lack of fusion, embedded repair weld notch, embedded parallel vertical notch, and so on, have been designed and fabricated to simulate all potential defects during welding process. PAUT techniques on the thick austenitic welds have been developed taking into account the acceptance criteria. Test procedure including calibration of equipment is derived and qualified through

Review of casing while drilling technology

Directory of Open Access Journals (Sweden)

Pavković Bojan

2016-01-01

Full Text Available Conventional drilling methods have been plagued with huge operational and financial challenges, such as cost of purchasing, inspecting, handling, transporting the drill equipment and most importantly, tripping in-and-out of the drill string whenever the Bottom Hole Assembly (BHA needs a replacement, needs of wiper trip or when total depth is reached. The tripping in-and-out of the drill string not only contributes to Non Productive Time (NPT but also leads to well control difficulties including wellbore instability and lost circulation. All this has led Oil and Gas industry, as well as any other engineering industry, to seek for new ways and methods in order to reduce these problems. Thanks to the advances in technical solutions and constant improvements of conventional drilling methods, a new drilling method - casing while drilling has been developed. Casing Drilling encompasses the process of simultaneously drilling and casing a well, using the active casing and thus optimizes the production. This paper presents a review of casing while drilling method (CwD and its practical usage in drilling wells. The comparison of conventional drilling method and casing while drilling is also presented. The CwD method achieves significantly better results than conventional drilling method.

Deep drilling KLX 02. Drilling and documentation of a 1700 m deep borehole at Laxemar, Sweden

Energy Technology Data Exchange (ETDEWEB)

Andersson, O [VBB VIAK AB, Malmoe (Sweden)

1994-08-01

In this report the preparation and execution of the deep core drilling KLX 02 is described. The hole was drilled with the wireline methods, NQ dimension (diameter 76 mm), to a final depth of 1700.5 m. Prior to core drilling a diameter 215 mm pilot hole was pre drilled to 200 m with controlled hammer drilling (DTH). In this hole casing and air-lift equipment was installed with the aim to support the circulation of drilling fluid. During core drilling there was a measurement of major drilling parameters and drilling fluid in and out of hole. As a fluid tracer uranine was used. Each 300 m of core drilling air-lift pump tests were performed. After completion a flow-meter log was run to finalize the project phase. It can be concluded that both the pre drilling and core drilling methods used proved to be successful. No severe technical problem occurred. However, potential risks have been pointed at in the report. The air-lift system functioned only partly and has to be modified for further use. Also the technique for monitoring of drilling parameters needs improvement as does the method for air-lift pump tests with packer. The organisation model for planning and realization functioned satisfactory and can be recommended for similar future projects. 9 refs, numerous tabs and figs.

Deep drilling KLX 02. Drilling and documentation of a 1700 m deep borehole at Laxemar, Sweden

International Nuclear Information System (INIS)

Andersson, O.

1994-08-01

In this report the preparation and execution of the deep core drilling KLX 02 is described. The hole was drilled with the wireline methods, NQ dimension (diameter 76 mm), to a final depth of 1700.5 m. Prior to core drilling a diameter 215 mm pilot hole was pre drilled to 200 m with controlled hammer drilling (DTH). In this hole casing and air-lift equipment was installed with the aim to support the circulation of drilling fluid. During core drilling there was a measurement of major drilling parameters and drilling fluid in and out of hole. As a fluid tracer uranine was used. Each 300 m of core drilling air-lift pump tests were performed. After completion a flow-meter log was run to finalize the project phase. It can be concluded that both the pre drilling and core drilling methods used proved to be successful. No severe technical problem occurred. However, potential risks have been pointed at in the report. The air-lift system functioned only partly and has to be modified for further use. Also the technique for monitoring of drilling parameters needs improvement as does the method for air-lift pump tests with packer. The organisation model for planning and realization functioned satisfactory and can be recommended for similar future projects. 9 refs, numerous tabs and figs

ULTRASONIC ASSEMBLY [REVIEW

Directory of Open Access Journals (Sweden)

PORAV Viorica

2015-05-01

Full Text Available The paper exposes the possibility of machine producesers to optimize the costs of clothes assembling. Ultrasonic systems being frequently utilized have many advantages on semi products of synthetic textile and technical textile. First of all, sewing – cutting process can be accomplished under high speeds and rate of losses can be minimized. Cutting seal applications are frequently used for underwear and sportswear. Slicing and unit cutting machines, as well as portable sealing machines are available for labeling sector. Products such as bag, pocket and cover can be sewed in a seamless manner for promotion purposes. All objects in terms of accessories are obtained in same standard. Our quilting machines are preferred in worldwide due to its threadless, high quality sealing. An alternative to the classic sewing assembly, with thread and needles is ultrasonic seaming. In ultrasonic welding, there are no connective bolts, nails, soldering materials, or adhesives necessary to bind the materials together. Ultrasonic is defined as acoustic frequencies above the range audible to the human ear. Ultrasonic frequencies are administered to the fabric from the sonotrode of bonding machine. The high frequency and powerful energy produced, when is release in one special environment, the ultrasound heating this environment. The ability to ultrasonic weld textiles and films depend on their thermoplastic contents and the desired end results. The paper defines the weld ability of more common textiles and films. The welding refers to all types of bonding and sealing, as in point bonding of fabric, or continuous sealing of film.

Drilling subsurface wellbores with cutting structures

Science.gov (United States)

Mansure, Arthur James; Guimerans, Rosalvina Ramona

2010-11-30

A system for forming a wellbore includes a drill tubular. A drill bit is coupled to the drill tubular. One or more cutting structures are coupled to the drill tubular above the drill bit. The cutting structures remove at least a portion of formation that extends into the wellbore formed by the drill bit.

New method based on combining ultrasonic assisted miniaturized matrix solid-phase dispersion and homogeneous liquid-liquid extraction for the determination of some organochlorinated pesticides in fish

International Nuclear Information System (INIS)

Rezaei, Farahnaz; Hosseini, Mohammad-Reza Milani

2011-01-01

Highlights: → Ultrasonic assisted miniaturized matrix solid-phase dispersion combined with HLLE was developed as a new method for the extraction of OCPs in fish. → The goal of this combination was to enhance the selectivity of HLLE procedure and to extend its application in biological samples. → This method proposed the advantages of good detection limits, lower consumption of reagents, and does not need any special instrumentation. - Abstract: In this study, ultrasonic assisted miniaturized matrix solid-phase dispersion (US-MMSPD) combined with homogeneous liquid-liquid extraction (HLLE) has been developed as a new method for the extraction of organochlorinated pesticides (OCPs) in fish prior to gas chromatography with electron capture detector (GC-ECD). In the proposed method, OCPs (heptachlor, aldrin, DDE, DDD, lindane and endrin) were first extracted from fish sample into acetonitrile by US-MMSPD procedure, and the extract was then used as consolute solvent in HLLE process. Optimal condition for US-MMSPD step was as follows: volume of acetonitrile, 1.5 mL; temperature of ultrasound, 40 deg. C; time of ultrasound, 10 min. For HLLE step, optimal results were obtained at the following conditions: volume of chloroform, 35 μL; volume of aqueous phase, 1.5 mL; volume of double distilled water, 0.5 mL; time of centrifuge, 10 min. Under the optimum conditions, the enrichment factors for the studied compounds were obtained in the range of 185-240, and the overall recoveries were ranged from 39.1% to 81.5%. The limits of detection were 0.4-1.2 ng g -1 and the relative standard deviations for 20 ng g -1 of the OCPs, varied from 3.2% to 8% (n = 4). Finally, the proposed method has been successfully applied to the analysis of the OCPs in real fish sample, and satisfactory results were obtained.

New method based on combining ultrasonic assisted miniaturized matrix solid-phase dispersion and homogeneous liquid-liquid extraction for the determination of some organochlorinated pesticides in fish

Energy Technology Data Exchange (ETDEWEB)

Rezaei, Farahnaz [Department of Analytical Chemistry, Faculty of Chemistry, Iran University of Science and Technology, Narmak, Tehran 16846 (Iran, Islamic Republic of); Hosseini, Mohammad-Reza Milani, E-mail: drmilani@iust.ac.ir [Department of Analytical Chemistry, Faculty of Chemistry, Iran University of Science and Technology, Narmak, Tehran 16846 (Iran, Islamic Republic of); Electroanalytical Chemistry Research Center, Iran University of Science and Technology, Narmak, Tehran 16846 (Iran, Islamic Republic of)

2011-09-30

Highlights: {yields} Ultrasonic assisted miniaturized matrix solid-phase dispersion combined with HLLE was developed as a new method for the extraction of OCPs in fish. {yields} The goal of this combination was to enhance the selectivity of HLLE procedure and to extend its application in biological samples. {yields} This method proposed the advantages of good detection limits, lower consumption of reagents, and does not need any special instrumentation. - Abstract: In this study, ultrasonic assisted miniaturized matrix solid-phase dispersion (US-MMSPD) combined with homogeneous liquid-liquid extraction (HLLE) has been developed as a new method for the extraction of organochlorinated pesticides (OCPs) in fish prior to gas chromatography with electron capture detector (GC-ECD). In the proposed method, OCPs (heptachlor, aldrin, DDE, DDD, lindane and endrin) were first extracted from fish sample into acetonitrile by US-MMSPD procedure, and the extract was then used as consolute solvent in HLLE process. Optimal condition for US-MMSPD step was as follows: volume of acetonitrile, 1.5 mL; temperature of ultrasound, 40 deg. C; time of ultrasound, 10 min. For HLLE step, optimal results were obtained at the following conditions: volume of chloroform, 35 {mu}L; volume of aqueous phase, 1.5 mL; volume of double distilled water, 0.5 mL; time of centrifuge, 10 min. Under the optimum conditions, the enrichment factors for the studied compounds were obtained in the range of 185-240, and the overall recoveries were ranged from 39.1% to 81.5%. The limits of detection were 0.4-1.2 ng g{sup -1} and the relative standard deviations for 20 ng g{sup -1} of the OCPs, varied from 3.2% to 8% (n = 4). Finally, the proposed method has been successfully applied to the analysis of the OCPs in real fish sample, and satisfactory results were obtained.

Effects of pore sizes and oxygen-containing functional groups on desulfurization activity of Fe/NAC prepared by ultrasonic-assisted impregnation

Energy Technology Data Exchange (ETDEWEB)

Shu, Song [College of Architecture and Environment, Sichuan University, Chengdu 610065, Sichuan (China); Guo, Jia-Xiu, E-mail: guojiaxiu@scu.edu.cn [College of Architecture and Environment, Sichuan University, Chengdu 610065, Sichuan (China); National Engineering Technology Research Center for Flue Gas Desulfurization, Chengdu 610065, Sichuan (China); Sichuan Provincial Environmental Protection Environmental Catalysis and Materials Engineering Technology Center, Chengdu 610065, Sichuan (China); Liu, Xiao-Li [National Engineering Technology Research Center for Flue Gas Desulfurization, Chengdu 610065, Sichuan (China); Wang, Xue-Jiao [College of Architecture and Environment, Sichuan University, Chengdu 610065, Sichuan (China); Yin, Hua-Qiang [College of Architecture and Environment, Sichuan University, Chengdu 610065, Sichuan (China); National Engineering Technology Research Center for Flue Gas Desulfurization, Chengdu 610065, Sichuan (China); Sichuan Provincial Environmental Protection Environmental Catalysis and Materials Engineering Technology Center, Chengdu 610065, Sichuan (China); Luo, De-Ming [National Engineering Technology Research Center for Flue Gas Desulfurization, Chengdu 610065, Sichuan (China)

2016-01-01

Graphical abstract: - Highlights: • Fe/NAC-60 exhibits the best desulfurization activity. • Different oscillation time can change surface area and pore volume of catalysts. • Ultrasonic oscillation increases Fe dispersion on carrier and effective pores. • Pore sizes play a crucial role during the SO{sub 2} removal. - Abstract: A series of Fe-loaded activated carbons treated by HNO{sub 3} (Fe/NAC) were prepared by incipient impregnation method with or without ultrasonic assistance and characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy with energy disperse spectroscope (SEM-EDS), transmission electron microscopy (TEM) and N{sub 2} adsorption/desorption. The desulfurization activities were evaluated at a fixed bed reactor under a mixed gas simulated from flue gas. The results showed that desulfurization activity from excellent to poor is as follows: Fe/NAC-60 > Fe/NAC-80 > Fe/NAC-30 > Fe/NAC-15 > Fe/NAC-0 > Fe/NAC-100 > NAC. Fe/NAC-60 exhibits the best desulfurization activity and has breakthrough sulfur capacity of 319 mg/g and breakthrough time of 540 min. The introduction of ultrasonic oscillation does not change the form of Fe oxides on activated carbon but can change the dispersion and relative contents of Fe{sub 3}O{sub 4}. The types of oxygen-containing functional groups have no obvious change for all samples but the texture properties show some differences when they are oscillated for different times. The fresh Fe/NAC-60 has a surface area of 1045 m{sup 2}/g and total pore volume of 0.961 cm{sup 3}/g with micropore volume of 0.437 cm{sup 3}/g and is larger than Fe/NAC-0 (823 m{sup 2}/g, 0.733 and 0.342 cm{sup 3}/g). After desulfurization, surface area and pore volume of all samples decrease significantly, and those of the exhausted Fe/NAC-60 decrease to 233 m{sup 2}/g and 0.481 cm{sup 3}/g, indicating that some byproducts deposit on surface to cover pores. Pore size distribution

Green synthesis of dimension-controlled silver nanoparticle–graphene oxide with in situ ultrasonication

International Nuclear Information System (INIS)

Hui, K.S.; Hui, K.N.; Dinh, D.A.; Tsang, C.H.; Cho, Y.R.; Zhou, Wei; Hong, Xiaoting; Chun, Ho-Hwan

2014-01-01

Graphical abstract: -- Abstract: A green chemical approach to control the dimensions of Ag nanoparticle-decorated graphene oxide (AgNP–GO) composites was proposed by in situ ultrasonication of a mixture of AgNO 3 and GO solution with the assistance of vitamin C acting as an environmentally friendly reducing agent at room temperature. The AgNP–GO composites were characterized by X-ray diffraction, transmission electron microscopy, energy-dispersive spectroscopy, Fourier transform infrared spectroscopy, Raman spectra and ultraviolet–visible absorption spectra. The results demonstrated that Ag nanoparticles with an average diameter of ∼15 nm were uniformly dispersed on the surface of GO nanosheets by in situ ultrasonication of 1 min with vitamin C. Increasing the ultrasonication times resulted in Ag nanoparticles with tunable dimensions ranging from 15 to 55 nm being formed on the surface of GO nanosheets. The amount of silver nitrate and the ultrasonication time play a key role in the control of the dimension of Ag nanoparticles on GO, and a formation mechanism of the as-prepared AgNP–GO composites is proposed. This study provides a guide to controlling the dimensions of AgNP–GO composites, which may hold promise as advanced materials for various analytical applications such as catalysis, sensors and microchips

Combination of Ultrasonic Vibration and Cryogenic Cooling for Cutting Performance Improvement of Inconel 718 Turning

Science.gov (United States)

Lin, S. Y.; Chung, C. T.; Cheng, Y. Y.

2011-01-01

The main objective of this study is to develop a thermo-elastic-plastic coupling model, based on a combination skill of ultrasonically assisted cutting and cryogenic cooling, under large deformation for Inconel 718 alloy machining process. The improvement extent on cutting performance and tool life promotion may be examined from this investigation. The critical value of the strain energy density of the workpiece will be utilized as the chip separation and the discontinuous chip segmentation criteria. The forced convection cooling and a hydrodynamic lubrication model will be considered and formulated in the model. Finite element method will be applied to create a complete numerical solution for this ultrasonic vibration cutting model. During the analysis, the cutting tool is incrementally advanced forward with superimposed ultrasonic vibration in a back and forth step-by-step manner, from an incipient stage of tool-workpiece engagement to a steady state of chip formation, a whole simulation of orthogonal cutting process under plane strain deformation is thus undertaken. High shear strength induces a fluctuation phenomenon of shear angle, high shear strain rate, variation of chip types and chip morphology, tool-chip contact length variation, the temperature distributions within the workpiece, chip and tool, periodic fluctuation in cutting forces can be determined from the developed model. A complete comparison of machining characteristics between some different combinations of ultrasonically assisted cutting and cryogenic cooling with conventional cutting operation can be acquired. Finally, the high-speed turning experiment for Inconel 718 alloy will be taken in the laboratory to validate the accuracy of the model, and the progressive flank wear, crater wear, notching and chipping of the tool edge can also be measured in the experiments.

To drill or not to drill? An econometric analysis of US public opinion

International Nuclear Information System (INIS)

Mukherjee, Deep; Rahman, Mohammad Arshad

2016-01-01

Offshore drilling in the United States (US) has been the subject of public and political discourse due to multiple reasons which include economic impact, energy security, and environmental hazard. Consequently, several polls have been conducted over time to gauge public attitude towards offshore drilling. Nevertheless, the economic literature on this issue is sparse. This paper contributes to the literature and analyzes support for offshore drilling based on demographic, economic, social, belief, and shock (e.g. spill) factors. The data is taken from ten nationwide surveys conducted before, during and after the British Petroleum (BP) oil spill and analyzed within the framework of discrete choice model. The results from an ordinal probit model demonstrate that age, annual household income, affiliation to Republican Party, and residence in oil-rich states positively affect the probability of strong support and reduce the probability of strong opposition for offshore drilling. In contrast, the female gender, higher education, association to Democratic Party, and environmental concern affect opinion in opposite direction. Marginal effects show that belief about environmental consequences of drilling has the highest impact on opinion. Binary probit model also yields a similar result and suggests that BP oil disaster resulted in a transient decrease in support for offshore drilling. - Highlights: •US public opinion on offshore drilling is analyzed based on ten national polls. •Ordinal and binary probit models are utilized to identify the underlying factors that shape public opinion. •Belief about environmental cost of drilling and educational attainment have the highest negative impact on opinion. •Age, income, affiliation to Republican party and oil-rich states positively affect support for drilling. •BP oil spill resulted in a transient decrease in support for offshore drilling.

The ICDP Snake River Geothermal Drilling Project: preliminary overview of borehole geophysics

Science.gov (United States)

Schmitt, Douglas R.; Liberty, Lee M.; Kessler, James E.; Kuck, Jochem; Kofman, Randolph; Bishop, Ross; Shervais, John W.; Evans, James P.; Champion, Duane E.

2012-01-01

Hotspot: The Snake River Geothermal Drilling Project was undertaken to better understand the geothermal systems in three locations across the Snake River Plain with varying geological and hydrological structure. An extensive series of standard and specialized geophysical logs were obtained in each of the wells. Hydrogen-index neutron and γ-γ density logs employing active sources were deployed through the drill string, and although not fully calibrated for such a situation do provide semi-quantitative information related to the ‘stratigraphy’ of the basalt flows and on the existence of alteration minerals. Electrical resistivity logs highlight the existence of some fracture and mineralized zones. Magnetic susceptibility together with the vector magnetic field measurements display substantial variations that, in combination with laboratory measurements, may provide a tool for tracking magnetic field reversals along the borehole. Full waveform sonic logs highlight the variations in compressional and shear velocity along the borehole. These, together with the high resolution borehole seismic measurements display changes with depth that are not yet understood. The borehole seismic measurements indicate that seismic arrivals are obtained at depth in the formations and that strong seismic reflections are produced at lithological contacts seen in the corresponding core logging. Finally, oriented ultrasonic borehole televiewer images were obtained over most of the wells and these correlate well with the nearly 6 km of core obtained. This good image log to core correlations, particularly with regards to drilling induced breakouts and tensile borehole and core fractures will allow for confident estimates of stress directions and or placing constraints on stress magnitudes. Such correlations will be used to orient in core orientation giving information useful in hydrological assessments, paleomagnetic dating, and structural volcanology.

High-accuracy drilling with an image guided light weight robot: autonomous versus intuitive feed control.

Science.gov (United States)

Tauscher, Sebastian; Fuchs, Alexander; Baier, Fabian; Kahrs, Lüder A; Ortmaier, Tobias

2017-10-01

Assistance of robotic systems in the operating room promises higher accuracy and, hence, demanding surgical interventions become realisable (e.g. the direct cochlear access). Additionally, an intuitive user interface is crucial for the use of robots in surgery. Torque sensors in the joints can be employed for intuitive interaction concepts. Regarding the accuracy, they lead to a lower structural stiffness and, thus, to an additional error source. The aim of this contribution is to examine, if an accuracy needed for demanding interventions can be achieved by such a system or not. Feasible accuracy results of the robot-assisted process depend on each work-flow step. This work focuses on the determination of the tool coordinate frame. A method for drill axis definition is implemented and analysed. Furthermore, a concept of admittance feed control is developed. This allows the user to control feeding along the planned path by applying a force to the robots structure. The accuracy is researched by drilling experiments with a PMMA phantom and artificial bone blocks. The described drill axis estimation process results in a high angular repeatability ([Formula: see text]). In the first set of drilling results, an accuracy of [Formula: see text] at entrance and [Formula: see text] at target point excluding imaging was achieved. With admittance feed control an accuracy of [Formula: see text] at target point was realised. In a third set twelve holes were drilled in artificial temporal bone phantoms including imaging. In this set-up an error of [Formula: see text] and [Formula: see text] was achieved. The results of conducted experiments show that accuracy requirements for demanding procedures such as the direct cochlear access can be fulfilled with compliant systems. Furthermore, it was shown that with the presented admittance feed control an accuracy of less then [Formula: see text] is achievable.

Percussive Augmenter of Rotary Drills for Operating as a Rotary-Hammer Drill

Science.gov (United States)

Aldrich, Jack Barron (Inventor); Bar-Cohen, Yoseph (Inventor); Sherrit, Stewart (Inventor); Badescu, Mircea (Inventor); Bao, Xiaoqi (Inventor); Scott, James Samson (Inventor)

2014-01-01

A percussive augmenter bit includes a connection shaft for mounting the bit onto a rotary drill. In a first modality, an actuator percussively drives the bit, and an electric slip-ring provides power to the actuator while being rotated by the drill. Hammering action from the actuator and rotation from the drill are applied directly to material being drilled. In a second modality, a percussive augmenter includes an actuator that operates as a hammering mechanism that drives a free mass into the bit creating stress pulses that fracture material that is in contact with the bit.

Comparison of Enzymatic and Ultrasonic Extraction of Albumin from Defatted Pumpkin (Cucurbita pepo)
Seed Powder.

Science.gov (United States)

Tu, Gia Loi; Bui, Thi Hoang Nga; Tran, Thi Thu Tra; Ton, Nu Minh Nguyet; Man Le, Van Viet

2015-12-01

In this study, ultrasound- and enzyme-assisted extractions of albumin (water-soluble protein group) from defatted pumpkin ( Cucurbita pepo ) seed powder were compared. Both advanced extraction techniques strongly increased the albumin yield in comparison with conventional extraction. The extraction rate was two times faster in the ultrasonic extraction than in the enzymatic extraction. However, the maximum albumin yield was 16% higher when using enzymatic extraction. Functional properties of the pumpkin seed albumin concentrates obtained using the enzymatic, ultrasonic and conventional methods were then evaluated. Use of hydrolase for degradation of cell wall of the plant material did not change the functional properties of the albumin concentrate in comparison with the conventional extraction. The ultrasonic extraction enhanced water-holding, oil-holding and emulsifying capacities of the pumpkin seed albumin concentrate, but slightly reduced the foaming capacity, and emulsion and foam stability.

In-process and post-process measurements of drill wear for control of the drilling process

Science.gov (United States)

Liu, Tien-I.; Liu, George; Gao, Zhiyu

2011-12-01

Optical inspection was used in this research for the post-process measurements of drill wear. A precision toolmakers" microscope was used. Indirect index, cutting force, is used for in-process drill wear measurements. Using in-process measurements to estimate the drill wear for control purpose can decrease the operation cost and enhance the product quality and safety. The challenge is to correlate the in-process cutting force measurements with the post-process optical inspection of drill wear. To find the most important feature, the energy principle was used in this research. It is necessary to select only the cutting force feature which shows the highest sensitivity to drill wear. The best feature selected is the peak of torque in the drilling process. Neuro-fuzzy systems were used for correlation purposes. The Adaptive-Network-Based Fuzzy Inference System (ANFIS) can construct fuzzy rules with membership functions to generate an input-output pair. A 1x6 ANFIS architecture with product of sigmoid membership functions can in-process measure the drill wear with an error as low as 0.15%. This is extremely important for control of the drilling process. Furthermore, the measurement of drill wear was performed under different drilling conditions. This shows that ANFIS has the capability of generalization.

UV laser drilling of SiC for semiconductor device fabrication

Energy Technology Data Exchange (ETDEWEB)

Krueger, Olaf; Schoene, Gerd; Wernicke, Tim; John, Wilfred; Wuerfl, Joachim; Traenkle, Guenther [Ferdinand-Braun-Institut fuer Hoechstfrequenztechnik, Gustav-Kirchhoff-Str. 4, 12489 Berlin (Germany)

2007-04-15

Pulsed UV laser processing is used to drill micro holes in silicon carbide (SiC) wafers supporting AlGaN/GaN transistor structures. Direct laser ablation using nanosecond pulses has been proven to provide an efficient way to create through and blind holes in 400 {mu}m thick SiC. When drilling through, openings in the front pads are formed, while blind holes stop {approx}40 {mu}m before the backside and were advanced to the electrical contact pad by subsequent plasma etching without an additional mask. Low induction connections (vias) between the transistor's source pads and the ground on the backside were formed by metallization of the holes. Micro vias having aspect ratios of 5-6 have been processed in 400 {mu}m SiC. The process flow from wafer layout to laser drilling is available including an automated beam alignment that allows a positioning accuracy of {+-}1 {mu}m with respect to existing patterns on the wafer. As proven by electrical dc and rf measurements the laser-assisted via technologies have successfully been implemented into fabrication of AlGaN/GaN high-power transistors.

Preliminary evaluation of uranium deposits. A geostatistical study of drilling density in Wyoming solution fronts

International Nuclear Information System (INIS)

Sandefur, R.L.; Grant, D.C.

1976-01-01

Studies of a roll-front uranium deposit in Shirley Basin Wyoming indicate that preliminary evaluation of the reserve potential of an ore body is possible with less drilling than currently practiced in industry. Estimating ore reserves from sparse drilling is difficult because most reserve calculation techniques do not give the accuracy of the estimate. A study of several deposits with a variety of drilling densities shows that geostatistics consistently provides a method of assessing the accuracy of an ore reserve estimate. Geostatistics provides the geologist with an additional descriptive technique - one which is valuable in the economic assessment of a uranium deposit. Closely spaced drilling on past properties provides both geological and geometric insight into the occurrence of uranium in roll-front type deposits. Just as the geological insight assists in locating new ore bodies and siting preferential drill locations, the geometric insight can be applied mathematically to evaluate the accuracy of a new ore reserve estimate. By expressing the geometry in numerical terms, geostatistics extracts important geological characteristics and uses this information to aid in describing the unknown characteristics of a property. (author)

Development of computational tool to interpret real time Pd (Pressure While Drilling) data; Desenvolvimento de ferramenta computacional interpretadora de dados de PWD (Pressure While Drilling) em tempo real

Energy Technology Data Exchange (ETDEWEB)

Gandelman, Roni Abensur; Waldmann, Alex Tadeu de Almeida; Martins, Andre Leibsohn [Centro de Pesquisas da Petrobras (CENPES). Gerencia de Tecnologia de Engenharia de Poco (Brazil)], e-mails: roniag@petrobras.com.br, awaldmann@petrobras.com.br, aleibsohn@petrobras.com.br; Teixeira, Gleber Tacio; Aragao, Atila Fernando Lima [E and P Servicos. Gerencia de Servicos de Poco (Brazil)], e-mail: gleber@petrobras.com.br, atila_aragao@petrobras.com.br; Rezende, Mauricio Seiji; Kern, Eduardo; Maliska Junior, Clovis [Engineering Simulation and Scientific Software (ESSS), (Brazil)], e-mails: mauricio@esss.com.br, kern@esss.com.br, coi@esss.com.br

2008-12-15

Drilling offshore oil wells is a very expensive and complex process, in which all the efforts must be taken to keep the annular pressure between a minimum pressure (pore pressure) and a maximum pressure (fracture pressure) which define the operational window limits. Several phenomena impact the bottom hole annular pressures, such as: ineffective hole cleaning, gel breaking when circulation is resumed, drill string movement (surge and swab), trips, pills displacement, kicks, etc. The correct interpretation of pressure while drilling (PWD) data is a very powerful toll to identify and prevent these phenomena. Nowadays, an expert monitors bottom hole pressures data and identifies undesirable events. The main goal of this project is the development of a computational tool to monitor pressure (and mud logging) data in real time to identify the causes of abnormal pressure variations, helping the operators to take decisions rapidly. Besides that, the tool allows the user to handle PWD data in a flexible architecture. This flexibility allows the incorporation of new methods of events identification as they are developed. The ultimate goals is to obtain a tool which serves both for the key study of the problems and physical, specific phenomena found during drilling, both for real-time monitoring to assist professionals involved in the process. (author)

Active Suppression of Drilling System Vibrations For Deep Drilling

Energy Technology Data Exchange (ETDEWEB)

Raymond, David W.; Blankenship, Douglas A.; Buerger, Stephen; Mesh, Mikhail; Radigan, William Thomas; Su, Jiann-Cherng

2015-10-01

The dynamic stability of deep drillstrings is challenged by an inability to impart controllability with ever-changing conditions introduced by geology, depth, structural dynamic properties and operating conditions. A multi-organizational LDRD project team at Sandia National Laboratories successfully demonstrated advanced technologies for mitigating drillstring vibrations to improve the reliability of drilling systems used for construction of deep, high-value wells. Using computational modeling and dynamic substructuring techniques, the benefit of controllable actuators at discrete locations in the drillstring is determined. Prototype downhole tools were developed and evaluated in laboratory test fixtures simulating the structural dynamic response of a deep drillstring. A laboratory-based drilling applicability demonstration was conducted to demonstrate the benefit available from deployment of an autonomous, downhole tool with self-actuation capabilities in response to the dynamic response of the host drillstring. A concept is presented for a prototype drilling tool based upon the technical advances. The technology described herein is the subject of U.S. Patent Application No. 62219481, entitled "DRILLING SYSTEM VIBRATION SUPPRESSION SYSTEMS AND METHODS", filed September 16, 2015.

Quality Parameters of Curcuma Longa L. Extracts by Supercritical Fluid Extraction (SFE) and Ultrasonic Assisted Extraction (UAE)

International Nuclear Information System (INIS)

Zaibunnisa Abdul Haiyee; Siti Hafsah Mohd Shah; Khudzir Ismail; Nooraain Hashim; Wan Iryani Wan Ismail

2016-01-01

Turmeric is one of the prominently use herbal plants due to its diverse beneficial effects especially in Indian medicine. The rhizome part of the turmeric contains valuable compounds which have been said to owe its antimicrobial effects, anti-cancer, anti-inflammatory and enhance wound healing. Due to its short-life span and perishable properties, the conversion of the rhizome into turmeric extract is desirable. Several methods have been used for extraction such as Soxhlet extraction and pressurized liquid extraction (PLE). However, these techniques are tedious, laborious, time consuming and involves the usage of toxic organic solvent, of which safeness of the end product is doubtful. In this study, a rapid, reliable and green extraction method of supercritical fluid extraction (SFE) and ultrasonic assisted extraction (UAE) were used. SFE without modifier has resulted in 0.0006 mg/ 100 g of curcuminoids concentration and 5.62 % of yield (dry weight basis). UAE using ethanol was able to produce significantly the highest yield (6.40 %, dry weight basis) and the highest curcuminoids concentration (0.1020 mg/ 100 g). However, SFE was able to produce extract that contain significantly higher major volatile compounds; tumerone, ar-turmerone and curlone. Therefore, this study proves that both extraction methods were able to produce high quality turmeric extract. (author)

Optimization of Ultrasonic-Assisted Extraction of Flavonoid Compounds and Antioxidants from Alfalfa Using Response Surface Method.

Science.gov (United States)

Jing, Chang-Liang; Dong, Xiao-Fang; Tong, Jian-Ming

2015-08-26

Ultrasonic-assisted extraction (UAE) was used to extract flavonoid-enriched antioxidants from alfalfa aerial part. Response surface methodology (RSM), based on a four-factor, five-level central composite design (CCD), was employed to obtain the optimal extraction parameters, in which the flavonoid content was maximum and the antioxidant activity of the extracts was strongest. Radical scavenging capacity of the extracts, which represents the amounts of antioxidants in alfalfa, was determined by using 2,2'-azino-bis (3-ethylbenzothiazoline-6-sulphonicacid) (ABTS) and 2,2'-diphenyl-1-picrylhydrazyl (DPPH) methods. The results showed good fit with the proposed models for the total flavonoid extraction (R² = 0.9849), for the antioxidant extraction assayed by ABTS method (R² = 0.9764), and by DPPH method (R² = 0.9806). Optimized extraction conditions for total flavonoids was a ratio of liquid to solid of 57.16 mL/g, 62.33 °C, 57.08 min, and 52.14% ethanol. The optimal extraction parameters of extracts for the highest antioxidant activity by DPPH method was a ratio of liquid to solid 60.3 mL/g, 54.56 °C, 45.59 min, and 46.67% ethanol, and by ABTS assay was a ratio of liquid to solid 47.29 mL/g, 63.73 °C, 51.62 min, and 60% ethanol concentration. Our work offers optimal extraction conditions for total flavonoids and antioxidants from alfalfa.

Construction and accuracy assessment of patient-specific biocompatible drill template for cervical anterior transpedicular screw (ATPS insertion: an in vitro study.

Directory of Open Access Journals (Sweden)

Maoqing Fu

Full Text Available BACKGROUND: With the properties of three-column fixation and anterior-approach-only procedure, anterior transpedicular screw (ATPS is ideal for severe multilevel traumatic cervical instabilities. However, the accurate insertion of ATPS remains challenging. Here we constructed a patient-specific biocompatible drill template and evaluated its accuracy in assisting ATPS insertion. METHODS: After ethical approval, 24 formalin-preserved cervical vertebrae (C2-C7 were CT scanned. 3D reconstruction models of cervical vertebra were obtained with 2-mm-diameter virtual pin tracts at the central pedicles. The 3D models were used for rapid prototyping (RP printing. A 2-mm-diameter Kirschner wire was then inserted into the pin tract of the RP model before polymethylmethacrylate was used to construct the patient-specific biocompatible drill template. After removal of the anterior soft tissue, a 2-mm-diameter Kirschner wire was inserted into the cervical pedicle with the assistance of drill template. Cadaveric cervical spines with pin tracts were subsequently scanned using the same CT scanner. A 3D reconstruction was performed of the scanned spines to get 3D models of the vertebrae containing the actual pin tracts. The deviations were calculated between 3D models with virtual and actual pin tracts at the middle point of the cervical pedicle. 3D models of 3.5 mm-diameter screws were used in simulated insertion to grade the screw positions. FINDINGS: The patient-specific biocompatible drill template was constructed to assist ATPS insertion successfully. There were no significant differences between medial/lateral deviations (P = 0.797 or between superior/inferior deviations (P = 0.741. The absolute deviation values were 0.82±0.75 mm and 1.10±0.96 mm in axial and sagittal planes, respectively. In the simulated insertion, the screws in non-critical position were 44/48 (91.7%. CONCLUSIONS: The patient-specific drill template is biocompatible, easy

Combination probe for optically assisted ultrasonic velocity-change imaging aimed at detecting unstable blood vessel plaque

Science.gov (United States)

Tanigawa, Shohei; Mano, Kazune; Wada, Kenji; Matsunaka, Toshiyuki; Horinaka, Hiromichi

2016-04-01

Blood vessel plaque with a large lipid core is at risk of becoming thrombus and is likely to induce acute heart disease. To prevent this, it is necessary to determine not only the plaque's size but also its chemical composition. We, therefore, made the prototype of a combination probe to diagnose carotid artery plaque. It is used to differentiate propagation characteristics between light spectra and ultrasonic images. By propagating light and ultrasound along a common direction, it is possible to effectively warm the diagnosis domain. Moreover, the probe is thought to be compact and be easy to use for diagnosing human carotid artery plaque. We applied the combination probe to a carotid artery phantom with a lipid area and obtained an image of the ultrasonic velocity change in the fatty area.

Ultrasound-assisted oxidative desulfurization of bunker-C oil using tert-butyl hydroperoxide.

Science.gov (United States)

Tang, Qiong; Lin, Song; Cheng, Ying; Liu, Sujun; Xiong, Jun-Ru

2013-09-01

This work investigated the ultrasonic assisted oxidative desulfurization of bunker-C oil with TBHP/MoO3 system. The operational parameters for the desulfurization procedure such as ultrasonic irradiation time, ultrasonic wave amplitude, catalyst initial concentration and oxidation agent initial concentration were studied. The experimental results show that the present oxidation system was very efficient for the desulfurization of bunker-C oil and ~35% sulfur was removed which was dependent on operational parameters. The application of ultrasonic irradiation allowed sulfur removal in a shorter time. The stronger the solvent polarity is, the higher the sulfur removal rate, but the recovery rate of oil is lower. The sulfur compounds in bunker-C oil reacted with TBHP to produce corresponding sulfoxide, and further oxidation produced the corresponding sulfone. Copyright © 2013 Elsevier B.V. All rights reserved.

Drilling for scientific purpose

Energy Technology Data Exchange (ETDEWEB)

Tanaka, Shoichi

1987-09-01

Drilling for scientific purpose is a process of conducting geophysical exploration at deep underground and drilling for collecting crust samples directly. This is because earth science has advanced to get a good understanding about the top of the crust and has shifted its main interest to the lower layer of the crust in land regions. The on-land drilling plan in Japan has just started, and the planned drilling spots are areas around the Minami River, Hidaka Mts., kinds of the Mesozoic and Cenozoic granite in outside zone, the extension of Japan Sea, Ogasawara Is., Minami-Tori Is., and active volcanos. The paper also outlines the present situation of on-land drilling in the world, focusing on the SG-3rd super-deep well SG-3 on the Kola Peninsula, USSR, Satori SG-1st well SG-1 in Azerbaidzhan S.S.R, V.S.S.R, Sweden's wells, Cyprus' wells, Bayearn well Plan in West Germany, and Salton Sea Scientific Drilling Program in the U.S. At its end, the paper explains the present situation and the future theme of the Japanese drilling technique and points out the necessity of developing equipment, and techniques. (14 figs, 5 tabs, 26 refs)

Optimization of oil yield from Hevea brasiliensis seeds through ultrasonic-assisted solvent extraction via response surface methodology

Directory of Open Access Journals (Sweden)

Val Irvin F. Mabayo

2018-01-01

Full Text Available The demand for oil has been increasing vastly over time, and the source of this has slowly been diminishing. The use of non-food feedstock is seen as a promising alternative source for the production of bio-based fuel. In this study, rubber (Hevea brasiliensis seeds were utilized as biomass in bio-oil production considering that these are non-edible and considered wastes in rubber tree plantations. In the oil extraction process, the rubber seed kernels were oven dried at 100 °C for 24 h, powdered and then dried further at 105 °C for 4 h. After characterization, optimization study was done using Design Expert 7.0 software through central composite design of the response surface methodology. Ultrasonication technology was employed in the oil extraction process which significantly reduced the reaction time needed for extraction to 15 min compared the conventional extraction method of at least 8 h. An optimum rubber seed oil (RSO yield of 30.3 ± 0.3% was obtained using 15 g biomass, 5:1 n-hexane to biomass (mL g−1 ratio, 50 μm resonance amplitude and 60 ± 5 °C temperature at 15 min reaction time. The oil yield at optimum condition was found to have 0.89 g mL−1 density at room temperature, 26.7 cSt kinematic viscosity at 40 °C and high heating value of 39.2 MJ kg−1. The Fourier Transform Infrared Radiation spectroscopy analysis of the RSO, at optimum condition, showed the presence of carboxylic acid and ester carbonyl functional groups which are good indicators as a potential source of biodiesel. Keywords: Hevea brasiliensis, Oil extraction, Optimization, Response surface methodology, Rubber seed oil, Ultrasonic-assisted solvent extraction

Ultrasonic sounding and monitoring of the excavation damaged zone in a soft supported gallery

International Nuclear Information System (INIS)

Balland, Cyrille; Souley, Mountaka; Morel, Jacques

2012-01-01

gallery GCS (gallery with soft support and oriented parallel to the horizontal major stress) has predicted an extension of EDZ between 1.4 and 1.9 m according to the front advancement, the position around the gallery (roof, bottom and gallery side) and the rock characteristics. Moreover, a former experimentation showed that below the bottom of a gallery with this same orientation, ultrasonic velocity falls related to the damage were significant up to 2 m deep. The area of interest of experimentation OHZ encompasses at least this area with in addition one reference measurement in the undisturbed area. To escape heterogeneous variations of clay layers and the main anisotropy effect, two devices were selected with a triplet of horizontal drillings in the siding and a doublet of vertical drillings in the bottom of the gallery. P-wave tomographic data allowed rebuilding the images of the velocity on the 4 plans defined by the drillings. These images have shown a significant perturbation of the velocity field over 1.8 m deep in the gallery side. This area has been associated with the EDZ whose extension is of the same order of magnitude as which had been modeled during the blind predictions. Furthermore, there is an area of 0.4 m in depth on this siding with very low velocities or disappearance of ultrasonic rays in the 3 plans. That can be associated with fracturing of argillites. This very low velocity zone is not visible at the bottom, where velocity perturbations are much lower, with constant velocity over 1.6 m. The containment of the concrete floor, which is particularly thick at this location, might play a role in this observation. Finally, some anomalies of velocity are still visible beyond the end of the zone associated with the EDZ. They are probably caused by isolated fractures that occurred during excavation of the gallery and identified on extracted cores from the drillings. The magnitude of these anomalies would suggest that these fractures are closed. A program

The characteristic and dispersion stability of nanocellulose produced by mixed acid hydrolysis and ultrasonic assistance.

Science.gov (United States)

Niu, Fuge; Li, Mengya; Huang, Qi; Zhang, Xiuzhen; Pan, Weichun; Yang, Jiansheng; Li, Jianrong

2017-06-01

Axiolitic shape nanocellulose particles were prepared using a combined mixed acid hydrolysis and ultrasonic treatment. The crystallinity, morphology and stability properties of cellulose were characterized to investigate the mechanism of nanocellulose formation and stability. It was found the hydrodynamic radius decreased from 205nm to 89nm, and the crystallinity index of the nanocellulose increased from 62.90% to 72.31% with an increase in hydrolysis time from 2 to 10h. Sulfate esters and sulfonate group were present in the nanocellulose, and released more COH groups after hydrolysis. The ζ-potential of cellulose decreased from -11.5 to -43.8mV after 10h of hydrolysis. These results illustrated the amorphous characteristic of cellulose was removed after acid hydrolysis and ultrasonic treatment. The higher ζ-potential and relatively small cellulose particles caused a more stable suspension, suggesting that electrostatic interactions played an important role in maintaining the stability and dispersibility of the nanocellulose particles. Copyright © 2017 Elsevier Ltd. All rights reserved.

Remote consulting based on ultrasonic digital immages and dynamic ultrasonic sequences

Science.gov (United States)

Margan, Anamarija; Rustemović, Nadan

2006-03-01

Telematic ultrasonic diagnostics is a relatively new tool in providing health care to patients in remote, islolated communities. Our project facility, "The Virtual Polyclinic - A Specialists' Consulting Network for the Islands", is located on the island of Cres in the Adriatic Sea in Croatia and has been extending telemedical services to the archipelago population since 2000. Telemedicine applications include consulting services by specialists at the University Clinical Hospital Center Rebro in Zagreb and at "Magdalena", a leading cardiology clinic in Croatia. After several years of experience with static high resolution ultrasonic digital immages for referral consulting diagnostics purposes, we now also use dynamic ultrasonic sequences in a project with the Department of Emmergency Gastroenterology at Rebro in Zagreb. The aim of the ongoing project is to compare the advantages and shortcomings in transmitting static ultrasonic digital immages and live sequences of ultrasonic examination in telematic diagnostics. Ultrasonic examination is a dynamic process in which the diagnostic accuracy is highly dependent on the dynamic moment of an ultrasound probe and signal. Our first results indicate that in diffuse parenchymal organ pathology the progression and the follow up of a disease is better presented to a remote consulting specialist by dynamic ultrasound sequences. However, the changes that involve only one part of a parenchymal organ can be suitably presented by static ultrasonic digital images alone. Furthermore, we need less time for digital imaging and such tele-consultations overall are more economical. Our previous telemedicine research and practice proved that we can greatly improve the level of medical care in remote healthcare facilities and cut healthcare costs considerably. The experience in the ongoing project points to a conclusion that we can further optimize remote diagnostics benefits by a right choice of telematic application thus reaching a

Ultrasonic flow meter

NARCIS (Netherlands)

Lötters, Joost Conrad; Snijders, G.J.; Volker, A.W.F.

2014-01-01

The invention relates to an ultrasonic flow meter comprising a flow tube for the fluid whose flow rate is to be determined. The flow meter comprises a transmitting element for emitting ultrasonic waves, which is provided on the outer jacket of the flow tube. A receiving element, which is provided on

30 CFR 57.7052 - Drilling positions.

Science.gov (United States)

2010-07-01

... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Drilling positions. 57.7052 Section 57.7052... SAFETY AND HEALTH SAFETY AND HEALTH STANDARDS-UNDERGROUND METAL AND NONMETAL MINES Drilling and Rotary Jet Piercing Drilling-Surface and Underground § 57.7052 Drilling positions. Persons shall not drill...

Ultrasonic Low-Friction Containment Plate for Thermal and Ultrasonic Stir Weld Processes

Science.gov (United States)

Graff, Karl; Short, Matt

2013-01-01

The thermal stir welding (TSW) process is finding applications in fabrication of space vehicles. In this process, workpieces to be joined by TSW are drawn, by heavy forces, between "containment plates," past the TSW tool that then causes joining of the separate plates. It is believed that the TSW process would be significantly improved by reducing the draw force, and that this could be achieved by reducing the friction forces between the workpieces and containment plates. Based on use of high-power ultrasonics in metal forming processes, where friction reduction in drawing dies has been achieved, it is believed that ultrasonic vibrations of the containment plates could achieve similar friction reduction in the TSW process. By applying ultrasonic vibrations to the containment plates in a longitudinal vibration mode, as well as by mounting and holding the containment plates in a specific manner such as to permit the plates to acoustically float, friction between the metal parts and the containment plates is greatly reduced, and so is the drawing force. The concept was to bring in the ultrasonics from the sides of the plates, permitting the ultrasonic hardware to be placed to the side, away from the equipment that contains the thermal stir tooling and that applies clamping forces to the plates. Tests demonstrated that one of the major objectives of applying ultrasonics to the thermal stir system, that of reducing draw force friction, should be achievable on a scaled-up system.

HYDRATE CORE DRILLING TESTS

Energy Technology Data Exchange (ETDEWEB)

John H. Cohen; Thomas E. Williams; Ali G. Kadaster; Bill V. Liddell

2002-11-01

The ''Methane Hydrate Production from Alaskan Permafrost'' project is a three-year endeavor being conducted by Maurer Technology Inc. (MTI), Noble, and Anadarko Petroleum, in partnership with the U.S. DOE National Energy Technology Laboratory (NETL). The project's goal is to build on previous and ongoing R&D in the area of onshore hydrate deposition. The project team plans to design and implement a program to safely and economically drill, core and produce gas from arctic hydrates. The current work scope includes drilling and coring one well on Anadarko leases in FY 2003 during the winter drilling season. A specially built on-site core analysis laboratory will be used to determine some of the physical characteristics of the hydrates and surrounding rock. Prior to going to the field, the project team designed and conducted a controlled series of coring tests for simulating coring of hydrate formations. A variety of equipment and procedures were tested and modified to develop a practical solution for this special application. This Topical Report summarizes these coring tests. A special facility was designed and installed at MTI's Drilling Research Center (DRC) in Houston and used to conduct coring tests. Equipment and procedures were tested by cutting cores from frozen mixtures of sand and water supported by casing and designed to simulate hydrate formations. Tests were conducted with chilled drilling fluids. Tests showed that frozen core can be washed out and reduced in size by the action of the drilling fluid. Washing of the core by the drilling fluid caused a reduction in core diameter, making core recovery very difficult (if not impossible). One successful solution was to drill the last 6 inches of core dry (without fluid circulation). These tests demonstrated that it will be difficult to capture core when drilling in permafrost or hydrates without implementing certain safeguards. Among the coring tests was a simulated hydrate

Ultrasound-Assisted Transient Liquid Phase Bonding of Magnesium Alloy Using Brass Interlayer in Air

Institute of Scientific and Technical Information of China (English)

Zhiwei Lai; Ruishan Xie; Chuan Pan; Xiaoguang Chen; Lei Liu; Wenxian Wang; Guisheng Zou

2017-01-01

The microstructure evolution and oxide film behavior in ultrasound-assisted transient liquid phase (U-TLP) bonding of Mg alloy were investigated by applying different ultrasonic time at 460℃ withbrass interlayer in air.The results indicated that with increasing ultrasonic time,brass interlayer disappeared gradually and the Mg-Cu-Zn eutectic compounds were formed.The eutectic compounds in the joint decreased as the ultrasonic time increased further.The oxide removal process was divided into four steps.Continuous oxide film at the interface was partially fractured by ultrasonic vibration,and then suspended into liquid by undermining eutectic reaction.After that,the suspended oxide film was broken into small oxide fragments by ultrasonic cavitation effect,which was finally squeezed out of the joint by ultrasonic squeeze action.In addition,the mechanical properties of the joints were investigated.The maximum shear strength of the joint reached 105 MPa,which was 100％ of base metal.

30 CFR 56.7052 - Drilling positions.

Science.gov (United States)

2010-07-01

... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Drilling positions. 56.7052 Section 56.7052... SAFETY AND HEALTH SAFETY AND HEALTH STANDARDS-SURFACE METAL AND NONMETAL MINES Drilling and Rotary Jet Piercing Drilling § 56.7052 Drilling positions. Persons shall not drill from— (a) Positions which hinder...

Improving the trajectory of transpedicular transdiscal lumbar screw fixation with a computer-assisted 3D-printed custom drill guide

Directory of Open Access Journals (Sweden)

Zhen-Xuan Shao

2017-07-01

Full Text Available Transpedicular transdiscal screw fixation is an alternative technique used in lumbar spine fixation; however, it requires an accurate screw trajectory. The aim of this study is to design a novel 3D-printed custom drill guide and investigate its accuracy to guide the trajectory of transpedicular transdiscal (TPTD lumbar screw fixation. Dicom images of thirty lumbar functional segment units (FSU, two segments of L1–L4 were acquired from the PACS system in our hospital (patients who underwent a CT scan for other abdomen diseases and had normal spine anatomy and imported into reverse design software for three-dimensional reconstructions. Images were used to print the 3D lumbar models and were imported into CAD software to design an optimal TPTD screw trajectory and a matched custom drill guide. After both the 3D printed FSU models and 3D-printed custom drill guide were prepared, the TPTD screws will be guided with a 3D-printed custom drill guide and introduced into the 3D printed FSU models. No significant statistical difference in screw trajectory angles was observed between the digital model and the 3D-printed model (P > 0.05. Our present study found that, with the help of CAD software, it is feasible to design a TPTD screw custom drill guide that could guide the accurate TPTD screw trajectory on 3D-printed lumbar models.

Computer automation of ultrasonic testing. [inspection of ultrasonic welding

Science.gov (United States)

Yee, B. G. W.; Kerlin, E. E.; Gardner, A. H.; Dunmyer, D.; Wells, T. G.; Robinson, A. R.; Kunselman, J. S.; Walker, T. C.

1974-01-01

Report describes a prototype computer-automated ultrasonic system developed for the inspection of weldments. This system can be operated in three modes: manual, automatic, and computer-controlled. In the computer-controlled mode, the system will automatically acquire, process, analyze, store, and display ultrasonic inspection data in real-time. Flaw size (in cross-section), location (depth), and type (porosity-like or crack-like) can be automatically discerned and displayed. The results and pertinent parameters are recorded.

Ultrasound assisted, thermally activated persulfate oxidation of coal tar DNAPLs.

Science.gov (United States)

Peng, Libin; Wang, Li; Hu, Xingting; Wu, Peihui; Wang, Xueqing; Huang, Chumei; Wang, Xiangyang; Deng, Dayi

2016-11-15

The feasibility of ultrasound assisted, thermally activated persulfate for effective oxidation of twenty 2-6 ringed coal tar PAHs in a biphasic tar/water system and a triphasic tar/soil/water system were investigated and established. The results indicate that ultrasonic assistance, persulfate and elevated reaction temperature are all required to achieve effective oxidation of coal tar PAHs, while the heating needed can be provided by ultrasonic induced heating as well. Further kinetic analysis reveals that the oxidation of individual PAH in the biphasic tar/water system follows the first-order kinetics, and individual PAH oxidation rate is primary determined by the mass transfer coefficients, tar/water interfacial areas, the aqueous solubility of individual PAH and its concentration in coal tar. Based on the kinetic analysis and experimental results, the contributions of ultrasound, persulfate and elevated reaction temperature to PAHs oxidation were characterized, and the effects of ultrasonic intensity and oxidant dosage on PAHs oxidation efficiency were investigated. In addition, the results indicate that individual PAH degradability is closely related to its reactivity as well, and the high reactivity of 4-6 ringed PAHs substantially improves their degradability. Copyright © 2016 Elsevier B.V. All rights reserved.

Ultrasonic inspection of austenitic welds

International Nuclear Information System (INIS)

Baikie, B.L.; Wagg, A.R.; Whittle, M.J.; Yapp, D.

1976-01-01

The ultrasonic examination of austenitic stainless steel weld metal has always been regarded as a difficult proposition because of the large and variable ultrasonic attenuations and back scattering obtained from apparently similar weld deposits. The work to be described shows how the existence of a fibre texture within each weld deposit (as a result of epitaxial growth through successive weld beads) produces a systematic variation in the ultrasonic attenuation coefficient and the velocity of sound, depending upon the angle between the ultrasonic beam and the fibre axis. Development work has shown that it is possible to adjust the welding parameters to ensure that the crystallographic texture within each weld is compatible with improved ultrasonic transmission. The application of the results to the inspection of a specific weld in type 316 weld metal is described

Irradiation Testing of Ultrasonic Transducers

International Nuclear Information System (INIS)

Daw, J.; Rempe, J.; Palmer, J.; Tittmann, B.; Reinhardt, B.; Kohse, G.; Ramuhalli, P.; Montgomery, R.; Chien, H.T.; Villard, J.F.

2013-06-01

Ultrasonic technologies offer the potential for high accuracy and resolution in-pile measurement of numerous parameters, including geometry changes, temperature, crack initiation and growth, gas pressure and composition, and microstructural changes. Many Department of Energy-Office of Nuclear Energy (DOE-NE) programs are exploring the use of ultrasonic technologies to provide enhanced sensors for in-pile instrumentation during irradiation testing. For example, the ability of single, small diameter ultrasonic thermometers (UTs) to provide a temperature profile in candidate metallic and oxide fuel would provide much needed data for validating new fuel performance models. Other efforts include an ultrasonic technique to detect morphology changes (such as crack initiation and growth) and acoustic techniques to evaluate fission gas composition and pressure. These efforts are limited by the lack of existing knowledge of ultrasonic transducer material survivability under irradiation conditions. To address this need, the Pennsylvania State University (PSU) was awarded an Advanced Test Reactor National Scientific User Facility (ATR NSUF) project to evaluate promising magnetostrictive and piezoelectric transducer performance in the Massachusetts Institute of Technology Research Reactor (MITR) up to a fast fluence of at least 10 21 n/cm 2 (E> 0.1 MeV). This test will be an instrumented lead test; and real-time transducer performance data will be collected along with temperature and neutron and gamma flux data. By characterizing magnetostrictive and piezoelectric transducer survivability during irradiation, test results will enable the development of novel radiation tolerant ultrasonic sensors for use in Material and Test Reactors (MTRs). The current work bridges the gap between proven out-of-pile ultrasonic techniques and in-pile deployment of ultrasonic sensors by acquiring the data necessary to demonstrate the performance of ultrasonic transducers. (authors)

Applications of optical sensing for laser cutting and drilling.

Science.gov (United States)

Fox, Mahlen D T; French, Paul; Peters, Chris; Hand, Duncan P; Jones, Julian D C

2002-08-20

Any reliable automated production system must include process control and monitoring techniques. Two laser processing techniques potentially lending themselves to automation are percussion drilling and cutting. For drilling we investigate the performance of a modification of a nonintrusive optical focus control system we previously developed for laser welding, which exploits the chromatic aberrations of the processing optics to determine focal error. We further developed this focus control system for closed-loop control of laser cutting. We show that an extension of the technique can detect deterioration in cut quality, and we describe practical trials carried out on different materials using both oxygen and nitrogen assist gas. We base our techniques on monitoring the light generated by the process, captured nonintrusively by the effector optics and processed remotely from the workpiece. We describe the relationship between the temporal and the chromatic modulation of the detected light and process quality and show how the information can be used as the basis of a process control system.

30 CFR 33.34 - Drilling test.

Science.gov (United States)

2010-07-01

... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Drilling test. 33.34 Section 33.34 Mineral... MINING PRODUCTS DUST COLLECTORS FOR USE IN CONNECTION WITH ROCK DRILLING IN COAL MINES Test Requirements § 33.34 Drilling test. (a) A drilling test shall consist of drilling a set of 10 test holes, without...

Processing surface sizing starch using oxidation, enzymatic hydrolysis and ultrasonic treatment methods--Preparation and application.

Science.gov (United States)

Brenner, Tobias; Kiessler, Birgit; Radosta, Sylvia; Arndt, Tiemo

2016-03-15

The surface application of starch is a well-established method for increasing paper strength. In surface sizing, a solution of degraded starch is applied to the paper. Two procedures have proved valuable for starch degradation in the paper mill: enzymatic and thermo-oxidative degradation. The objective of this study was to determine achievable efficiencies of cavitation in preparing degraded starch for surface application on paper. It was found that ultrasonic-assisted starch degradation can provide a starch solution that is suitable for surface sizing. The molecular composition of starch solutions prepared by ultrasonic treatment differed from that of starch solutions degraded by enzymes or by thermo-oxidation. Compared to commercial degradation processes, this resulted in intensified film formation and in greater penetration during surface sizing and ultimately in a higher starch content of the paper. Paper sized with ultrasonically treated starch solutions show the same strength properties compared to commercially sized paper. Copyright © 2015 Elsevier Ltd. All rights reserved.

Research progress on microstructure evolution of semi-solid aluminum alloys in ultrasonic field and their rheocasting

Directory of Open Access Journals (Sweden)

Wu Shusen

2014-07-01

Full Text Available The effects of ultrasonic vibration (UV treatment on microstructure of semi-solid aluminum alloys and the application of UV in rheocasting process are reviewed. Good semi-solid slurry can be produced by high-intensity UV process for aluminum alloys. The microstructures of Al-Si, Al-Mg and Al-Cu alloys produced by rheocasting assisted with UV are compact and with fine grains. The mechanical properties of the UV treated alloys are increased by about 20%-30%. Grain refinement of the alloys is generally considered because of cavitation and acoustic streaming caused by UV. Apart from these mechanisms, a hypothesis of the fuse of dendrite root caused by capillary infiltration in the ultrasonic field, as well as a mechanism of crystallites falling off from the mould-wall and crystal multiplication by mechanical vibration effect in indirect ultrasonic vibration are proposed to explain the microstructure evolution of the alloys.

Ultrasonic and hydrothermal mediated synthesis routes for functionalized Mg-Al LDH: Comparison study on surface morphology, basic site strength, cyclic sorption efficiency and effectiveness.

Science.gov (United States)

Ezeh, Collins I; Tomatis, Marco; Yang, Xiaogang; He, Jun; Sun, Chenggong

2018-01-01

Amine functionalized layered double hydroxide (LDHs) adsorbents prepared using three different routes: co-precipitation, sono-chemical and ultrasonic-assisted high pressure hydrothermal. The prepared adsorbent samples were characterized using X-ray diffraction (XRD), X-ray Photoelectron Spectroscopy (XPS), Scanning electron microscope-Energy dispersive X-ray spectroscopy (SEM-EDX), Temperature Programmed Desorption (TPD), Brunauer-Emmett-Teller (BET), and Thermogravimetric analysis (TGA), respectively. The performance of the prepared adsorbents was tested in a controlled thermal-swing adsorption process to measure its adsorption capacity, regeneration and cyclic efficiencies subsequently. The characterisation results were compared with those obtained using the conventional preparation routes but taking into account of the impact of sonochemical and hydrothermal pre-treatment on textural properties, adsorption capacity, regeneration and cyclic efficiencies. Textural results depicts a surge in surface area of the adsorbent synthesised by hydrothermal route (311m 2 /g) from 25 to 171m 2 /g for conventional and ultrasonic routes respectively. Additionally, it has been revealed from the present study that adsorbents prepared using ultrasonic-assisted hydrothermal route exhibit a better CO 2 uptake capacity than that prepared using sonochemical and conventional routes. Thus, the ultrasonic-assisted hydrothermal treatment can effectively promote the adsorption capacity of the adsorbent. This is probably due to the decrease of moderate (M-O) and weak (OH - groups) basic sites with subsequent surge in the number of strong basic sites (O 2- ) resulting from the hydrothermal process. Moreover, the cyclic adsorption efficiency of the ultrasonic mediated process was found to be 76% compared with 60% for conventional and 53% for hydrothermal routes, respectively. According to the kinetic model analysis, adsorption mechanism is mostly dominated by physisorption before amine

Ultrasonic dip seal maintenance system

International Nuclear Information System (INIS)

Poindexter, A.M.; Ricks, H.E.

1978-01-01

Disclosed is a system for removing impurities from the surfaces of liquid dip seals and for wetting the metal surfaces of liquid dip seals in nuclear components. The system comprises an ultrasonic transducer that transmits ultrasonic vibrations along an ultrasonic probe to the metal and liquid surfaces of the dip seal thereby loosening and removing those impurities

Development of an Ionic Liquid-Based Ultrasonic/Microwave-Assisted Simultaneous Distillation and Extraction Method for Separation of Camptothecin, 10-Hydroxycamptothecin, Vincoside-Lactam, and Essential Oils from the Fruits of Camptotheca acuminata Decne

Directory of Open Access Journals (Sweden)

Chunjian Zhao

2016-10-01

Full Text Available An ionic liquid-based ultrasonic/microwave-assisted simultaneous distillation and extraction (IL-UMASDE method for isolating camptothecin (CPT, 10-hydroxycamptothecin (HCPT, vincoside-lactam (VCS-LT, and essential oils (EOs from Camptotheca acuminata Decne fruits was developed. The important parameters were optimized using single-factor and central composite design experiments. The optimum conditions were 0.75 M 1-octyl-3-methylimidazolium ([C8mim]Br as the extraction solvent, a liquid–solid ratio of 13.7 mL/g, an extraction time of 33.2 min, a microwave power of 582 W, and a fixed ultrasonic power of 50 W. The yields of CPT, HCPT, and VCS-LT obtained under the optimum conditions were 2.463, 0.164, and 0.297 mg/g, respectively; these are 1.08-, 1.12-, and 1.04-fold higher, respectively, than those obtained by conventional 55% ethanol heat reflux extraction (HRE. The extraction time for the equilibrium yields of CPT, HCPT and VCS-LT using IL-UMASDE was 33.6%, 58.5%, 63.1%, and 66.8%, respectively, less than the corresponding times using IL-MASDE, IL-ultrasonic-assisted extraction (IL-UAE, 55% ethanol UAE and 55% ethanol HRE. The yield of EOs obtained using IL-UMASDE was 0.793 mg/g, i.e., 1.31-fold higher than that obtained by conventional hydrodistillation extraction (HDE. The components of the EOs obtained using IL-UMASDE and HDE were similar. The extraction time for the equilibrium yields of EOs using IL-UMASDE is 33.6%, 58.5%, 52.6%, and 72.3% lower than those for IL-MASDE, water-UMASDE, water-MASDE, and HDE, respectively. Compared with other extraction methods, IL-UMASDE gave the highest yields of CPT, HCPT, VCS-LT, and EOs and also had the shortest extraction time. IL-UMASDE is a potential green and highly efficient technique for the extraction of CPT, HCPT, VCS-LT, and EOs from Camptotheca acuminata Decne fruits.

A study of an assisting robot for mandible plastic surgery based on augmented reality.

Science.gov (United States)

Shi, Yunyong; Lin, Li; Zhou, Chaozheng; Zhu, Ming; Xie, Le; Chai, Gang

2017-02-01

Mandible plastic surgery plays an important role in conventional plastic surgery. However, its success depends on the experience of the surgeons. In order to improve the effectiveness of the surgery and release the burden of surgeons, a mandible plastic surgery assisting robot, based on an augmented reality technique, was developed. Augmented reality assists surgeons to realize positioning. Fuzzy control theory was used for the control of the motor. During the process of bone drilling, both the drill bit position and the force were measured by a force sensor which was used to estimate the position of the drilling procedure. An animal experiment was performed to verify the effectiveness of the robotic system. The position error was 1.07 ± 0.27 mm and the angle error was 5.59 ± 3.15°. The results show that the system provides a sufficient accuracy with which a precise drilling procedure can be performed. In addition, under the supervision's feedback of the sensor, an adequate safety level can be achieved for the robotic system. The system realizes accurate positioning and automatic drilling to solve the problems encountered in the drilling procedure, providing a method for future plastic surgery.

Newberry exploratory slimhole: Drilling and testing

Energy Technology Data Exchange (ETDEWEB)

Finger, J.T.; Jacobson, R.D.; Hickox, C.E.

1997-11-01

During July--November, 1995, Sandia National Laboratories, in cooperation with CE Exploration, drilled a 5,360 feet exploratory slimhole (3.895 inch diameter) in the Newberry Known Geothermal Resource Area (KGRA) near Bend, Oregon. This well was part of Sandia`s program to evaluate slimholes as a geothermal exploration tool. During and after drilling the authors performed numerous temperature logs, and at the completion of drilling attempted to perform injection tests. In addition to these measurements, the well`s data set includes: over 4,000 feet of continuous core (with detailed log); daily drilling reports from Sandia and from drilling contractor personnel; daily drilling fluid record; and comparative data from other wells drilled in the Newberry KGRA. This report contains: (1) a narrative account of the drilling and testing, (2) a description of equipment used, (3) a brief geologic description of the formation drilled, (4) a summary and preliminary interpretation of the data, and (5) recommendations for future work.

Implementation of improved underbalanced drilling in AbuDhabi onshore field

Science.gov (United States)

Alhammadi, Adel Mohammed

Abu Dhabi Company for Onshore Oil Operations (ADCO) is considering Underbalanced Drilling (UBD) as a means to develop lower permeability units in its fields. In addition to productivity and recovery gains, ADCO also expects reservoir characterization benefits from UBD. Reservoir screening studies were carried out on all of ADCO's reservoirs to determine their applicability for UBD. The primary business benefits of UBD were determined to be reservoir characterization, damage Mitigation, and rate of Penetration "ROP" Improvement. Apart from the primary benefits, some of the secondary benefits of UBD that were identified beforehand included rig performance. Since it's a trial wells, the challenge was to drill these wells safely, efficiently and of course meeting well objectives. Many operators worldwide drill these well in underbalanced mode but complete it overbalanced. In our case the plan was to drill and complete these wells in underbalanced condition. But we had to challenge most operators and come up with special and unique casing hanger design to ensure well control barriers exists while fishing the control line of the Downhole Deployment Valve "DDV". After intensive studies and planning, the hanger was designed as per our recommendations and found to be effective equipment that optimized the operational time and the cost as well. This report will provide better understanding of UBD technique in general and shade on the special designed casing hanger compared to conventional or what's most used worldwide. Even thought there were some issues while running the casing hanger prior drilling but managed to capture the learning's from each well and re-modified the hanger and come up with better deign for the future wells. Finally, the new design perform a good performance of saving the operation time and assisting the project to be done in a safe and an easy way without a major impact on the well cost. This design helped to drill and complete these wells safely with

Microgravity Drill and Anchor System

Science.gov (United States)

Parness, Aaron; Frost, Matthew A.; King, Jonathan P.

2013-01-01

This work is a method to drill into a rock surface regardless of the gravitational field or orientation. The required weight-on-bit (WOB) is supplied by a self-contained anchoring mechanism. The system includes a rotary percussive coring drill, forming a complete sampling instrument usable by robot or human. This method of in situ sample acquisition using micro - spine anchoring technology enables several NASA mission concepts not currently possible with existing technology, including sampling from consolidated rock on asteroids, providing a bolt network for astronauts visiting a near-Earth asteroid, and sampling from the ceilings or vertical walls of lava tubes and cliff faces on Mars. One of the most fundamental parameters of drilling is the WOB; essentially, the load applied to the bit that allows it to cut, creating a reaction force normal to the surface. In every drilling application, there is a minimum WOB that must be maintained for the system to function properly. In microgravity (asteroids and comets), even a small WOB could not be supported conventionally by the weight of the robot or astronaut. An anchoring mechanism would be needed to resist the reactions, or the robot or astronaut would push themselves off the surface and into space. The ability of the system to anchor itself to a surface creates potential applications that reach beyond use in low gravity. The use of these anchoring mechanisms as end effectors on climbing robots has the potential of vastly expanding the scope of what is considered accessible terrain. Further, because the drill is supported by its own anchor rather than by a robotic arm, the workspace is not constrained by the reach of such an arm. Yet, if the drill is on a robotic arm, it has the benefit of not reflecting the forces of drilling back to the arm s joints. Combining the drill with the anchoring feet will create a highly mobile, highly stable, and highly reliable system. The drilling system s anchor uses hundreds of

Influence of Drilling Parameters on Torque during Drilling of GFRP Composites Using Response Surface Methodology

Science.gov (United States)

Mohan, N. S.; Kulkarni, S. M.

2018-01-01

Polymer based composites have marked their valuable presence in the area of aerospace, defense and automotive industry. Components made of composite, are assembled to main structure by fastener, which require accurate, precise high quality holes to be drilled. Drilling the hole in composite with accuracy require control over various processes parameters viz., speed, feed, drill bit size and thickens of specimen. TRIAC VMC machining center is used to drill the hole and to relate the cutting and machining parameters on the torque. MINITAB 14 software is used to analyze the collected data. As a function of cutting and specimen parameters this method could be useful for predicting torque parameters. The purpose of this work is to investigate the effect of drilling parameters to get low torque value. Results show that thickness of specimen and drill bit size are significant parameters influencing the torque and spindle speed and feed rate have least influence and overlaid plot indicates a feasible and low region of torque is observed for medium to large sized drill bits for the range of spindle speed selected. Response surface contour plots indicate the sensitivity of the drill size and specimen thickness to the torque.

Control procedure for well drilling operations

Energy Technology Data Exchange (ETDEWEB)

Bourdon, J C

1988-09-09

A control procedure of rotary drilling operations is proposed. It uses the Drill off test. The drill-off test permits to determine the rock drill speed variation as a function of the wright applied on the top of the pipe. We can deduce from that a rock drill wear parameter. The method permits to prevent a rupture and its grave economic consequences.

Multi-state autonomous drilling for lunar exploration

Directory of Open Access Journals (Sweden)

Chen Chongbin

2016-10-01

Full Text Available Due to the lack of information of subsurface lunar regolith stratification which varies along depth, the drilling device may encounter lunar soil and lunar rock randomly in the drilling process. To meet the load safety requirements of unmanned sampling mission under limited orbital resources, the control strategy of autonomous drilling should adapt to the indeterminable lunar environments. Based on the analysis of two types of typical drilling media (i.e., lunar soil and lunar rock, this paper proposes a multi-state control strategy for autonomous lunar drilling. To represent the working circumstances in the lunar subsurface and reduce the complexity of the control algorithm, lunar drilling process was categorized into three drilling states: the interface detection, initiation of drilling parameters for recognition and drilling medium recognition. Support vector machine (SVM and continuous wavelet transform were employed for the online recognition of drilling media and interface, respectively. Finite state machine was utilized to control the transition among different drilling states. To verify the effectiveness of the multi-state control strategy, drilling experiments were implemented with multi-layered drilling media constructed by lunar soil simulant and lunar rock simulant. The results reveal that the multi-state control method is capable of detecting drilling state variation and adjusting drilling parameters timely under vibration interferences. The multi-state control method provides a feasible reference for the control of extraterrestrial autonomous drilling.

Optimum fluid design for drilling and cementing a well drilled with coil tubing technology

Energy Technology Data Exchange (ETDEWEB)

Swendsen, O.; Saasen, A.; Vassoy, B. [Statoil (Norway); Skogen, E.; Mackin, F.; Normann, S. H.

1998-12-31

The strategy, design and drilling fluid and cementing operations in the first two wells drilled with coil tubing technology in the Gullfaks field in the Tampen Spur Area of the Norwegian sector of the North Sea are discussed. The drilling fluid use was a solids-free potassium formate/polymer brine-based fluid with a density of 1,50-1.56 g/cc, with flow properties characterized by very low fluid loss due to high extensional viscosity, a low viscosity at all shear rates, and a low degree of shear-thinning. The low viscous drilling fluid is considered to have been the major contributing factor in achieving excellent hole cleaning, no differential sticking, successful setting of cement kick-off plugs, problem-free running of the liner, and excellent zonal isolation when cementing the liner. These experiences led the authors to conclude that it is possible to formulate a brine-based solids-free drilling fluid with low viscosity and fluid loss properties for most formation pressure regimes, and that such a drilling fluid is well suited to drilling highly deviated slim hole wells where hole cleaning and differential sticking present special challenges. 12 refs., 2 tabs., 3 figs.

Heat generated by dental implant drills during osteotomy-a review: heat generated by dental implant drills.

Science.gov (United States)

Mishra, Sunil Kumar; Chowdhary, Ramesh

2014-06-01

Osseointegration is the more stable situation and results in a high success rate of dental implants. Heat generation during rotary cutting is one of the important factors influencing the development of osseointegration. To assess the various factors related to implant drills responsible for heat generation during osteotomy. To identify suitable literature, an electronic search was performed using Medline and Pubmed database. Articles published in between 1960 to February 2013 were searched. The search is focused on heat generated by dental implant drills during osteotomy. Various factors related to implant drill such effect of number of blades; drill design, drill fatigue, drill speed and force applied during osteotomies which were responsible for heat generation were reviewed. Titles and abstracts were screened, and literature that fulfilled the inclusion criteria was selected for a full-text reading. The initial literature search resulted in 299 articles out of which only 70 articles fulfils the inclusion criteria and were included in this systematic review. Many factors related to implant drill responsible for heat generation were found. Successful preparation of an implant cavity with minimal damage to the surrounding bone depends on the avoidance of excessive temperature generation during surgical drilling. The relationship between heat generated and implant drilling osteotomy is multifactorial in nature and its complexity has not been fully studied. Lack of scientific knowledge regarding this issue still exists. Further studies should be conducted to determine the various factors which generate less heat while osteotomy such as ideal ratio of force and speed in vivo, exact time to replace a drill, ideal drill design, irrigation system, drill-bone contact area.

Technology strategy for cost-effective drilling and intervention; Technology Target Areas; TTA4 - Cost effective drilling and intervention

Energy Technology Data Exchange (ETDEWEB)

2007-07-01

The main goals of the OG21 initiative are to (1) develop new technology and knowledge to increase the value creation of Norwegian oil and gas resources and (2) enhance the export of Norwegian oil and gas technology. The OG21 Cost-effective Drilling and Intervention (CEDI) Technology Target Area (TTA) has identified some key strategic drilling and well intervention needs to help meet the goals of OG21. These key strategic drilling and well intervention needs are based on a review of present and anticipated future offshore-Norway drilling and well intervention conditions and the Norwegian drilling and well intervention industry. A gap analysis has been performed to assess the extent to which current drilling and well intervention research and development and other activities will meet the key strategic needs. Based on the identified strategic drilling and well intervention needs and the current industry res each and development and other activities, the most important technology areas for meeting the OG21 goals are: environment-friendly and low-cost exploration wells; low-cost methods for well intervention/sidetracks; faster and extended-reach drilling; deep water drilling, completion and intervention; offshore automated drilling; subsea and sub-ice drilling; drilling through basalt and tight carbonates; drilling and completion in salt formation. More specific goals for each area: reduce cost of exploration wells by 50%; reduce cost for well intervention/sidetracks by 50%; increase drilling efficiency by 40%; reduce drilling cost in deep water by 40 %; enable offshore automated drilling before 2012; enable automated drilling from seabed in 2020. Particular focus should be placed on developing new technology for low-cost exploration wells to stem the downward trends in the number of exploration wells drilled and the volume of discovered resources. The CEDI TTA has the following additional recommendations: The perceived gaps in addressing the key strategic drilling and

Ultrasonic neuromodulation

Science.gov (United States)

Naor, Omer; Krupa, Steve; Shoham, Shy

2016-06-01

Ultrasonic waves can be non-invasively steered and focused into mm-scale regions across the human body and brain, and their application in generating controlled artificial modulation of neuronal activity could therefore potentially have profound implications for neural science and engineering. Ultrasonic neuro-modulation phenomena were experimentally observed and studied for nearly a century, with recent discoveries on direct neural excitation and suppression sparking a new wave of investigations in models ranging from rodents to humans. In this paper we review the physics, engineering and scientific aspects of ultrasonic fields, their control in both space and time, and their effect on neuronal activity, including a survey of both the field’s foundational history and of recent findings. We describe key constraints encountered in this field, as well as key engineering systems developed to surmount them. In closing, the state of the art is discussed, with an emphasis on emerging research and clinical directions.

Hazardous impact of toxic metals on tobacco leaves grown in contaminated soil by ultrasonic assisted pseudo-digestion: Multivariate study

International Nuclear Information System (INIS)

Arain, Mohammad Balal; Kazi, Tasneem Gul; Jamali, Mohammad Khan; Jalbani, Nusrat; Afridi, Hassan Imran; Kandhro, Ghulam Abbas; Ansari, Rehana; Sarfraz, Raja Adil

2008-01-01

Tobacco leaves (Nicotiana tabacum L.), agricultural soil and pollute irrigated lake water samples were collected during 2005-2006 and analyzed for Cd and Ni by electrothermal atomic absorption spectrometry (ETAAS). A simple and efficient procedure was investigated for the complete decomposition of tobacco leaves using ultrasonic assisted acid pseudo-digestion method (UPDM). A Plackett-Burman experimental design was used as a multivariate strategy for the evaluation of seven factors/variables at once, while central composite were used to found optimum values of significant variables. The accuracy of the proposed methods was assessed by analyzing certified reference (CRM); Virginia tobacco leaves (CTA-VTL-2). The results being compared with those obtained by conventional wet acid digestion method. The result obtained by optimized method showed good agreement with the certified values and sufficiently high recovery 97.8 and 98.7% for Cd and Ni, respectively. Under optimal conditions, the detection limits (3σ) were evaluated to be 0.019 μg g -1 for Cd and 0.37 μg g -1 for Ni. The proposed method was successfully applied to the determination of Cd and Ni in raw, processed tobacco and different branded cigarettes samples

Hazardous impact of toxic metals on tobacco leaves grown in contaminated soil by ultrasonic assisted pseudo-digestion: Multivariate study

Energy Technology Data Exchange (ETDEWEB)

Arain, Mohammad Balal [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: bilal_ku2004@yahoo.com; Kazi, Tasneem Gul [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: tgkazi@yahoo.com; Jamali, Mohammad Khan [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: mkhanjamali@yahoo.com; Jalbani, Nusrat [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: nussaratjalbani_21@yahoo.com; Afridi, Hassan Imran [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: hassanimranafridi@yahoo.com; Kandhro, Ghulam Abbas [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: gakandhro@yahoo.com; Ansari, Rehana [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: rehana_ansari_57@yahoo.com; Sarfraz, Raja Adil [Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro 76080 (Pakistan)], E-mail: rajaadilsarfraz@gmail.com

2008-06-30

Tobacco leaves (Nicotiana tabacum L.), agricultural soil and pollute irrigated lake water samples were collected during 2005-2006 and analyzed for Cd and Ni by electrothermal atomic absorption spectrometry (ETAAS). A simple and efficient procedure was investigated for the complete decomposition of tobacco leaves using ultrasonic assisted acid pseudo-digestion method (UPDM). A Plackett-Burman experimental design was used as a multivariate strategy for the evaluation of seven factors/variables at once, while central composite were used to found optimum values of significant variables. The accuracy of the proposed methods was assessed by analyzing certified reference (CRM); Virginia tobacco leaves (CTA-VTL-2). The results being compared with those obtained by conventional wet acid digestion method. The result obtained by optimized method showed good agreement with the certified values and sufficiently high recovery 97.8 and 98.7% for Cd and Ni, respectively. Under optimal conditions, the detection limits (3{sigma}) were evaluated to be 0.019 {mu}g g{sup -1} for Cd and 0.37 {mu}g g{sup -1} for Ni. The proposed method was successfully applied to the determination of Cd and Ni in raw, processed tobacco and different branded cigarettes samples.

A fractional Fourier transform analysis of the scattering of ultrasonic waves

Science.gov (United States)

Tant, Katherine M.M.; Mulholland, Anthony J.; Langer, Matthias; Gachagan, Anthony

2015-01-01

Many safety critical structures, such as those found in nuclear plants, oil pipelines and in the aerospace industry, rely on key components that are constructed from heterogeneous materials. Ultrasonic non-destructive testing (NDT) uses high-frequency mechanical waves to inspect these parts, ensuring they operate reliably without compromising their integrity. It is possible to employ mathematical models to develop a deeper understanding of the acquired ultrasonic data and enhance defect imaging algorithms. In this paper, a model for the scattering of ultrasonic waves by a crack is derived in the time–frequency domain. The fractional Fourier transform (FrFT) is applied to an inhomogeneous wave equation where the forcing function is prescribed as a linear chirp, modulated by a Gaussian envelope. The homogeneous solution is found via the Born approximation which encapsulates information regarding the flaw geometry. The inhomogeneous solution is obtained via the inverse Fourier transform of a Gaussian-windowed linear chirp excitation. It is observed that, although the scattering profile of the flaw does not change, it is amplified. Thus, the theory demonstrates the enhanced signal-to-noise ratio permitted by the use of coded excitation, as well as establishing a time–frequency domain framework to assist in flaw identification and classification. PMID:25792967

Ultrasonic colour Doppler imaging

DEFF Research Database (Denmark)

Evans, David H; Jensen, Jørgen Arendt; Nielsen, Michael Bachmann

2011-01-01

Ultrasonic colour Doppler is an imaging technique that combines anatomical information derived using ultrasonic pulse-echo techniques with velocity information derived using ultrasonic Doppler techniques to generate colour-coded maps of tissue velocity superimposed on grey-scale images of tissue...... anatomy. The most common use of the technique is to image the movement of blood through the heart, arteries and veins, but it may also be used to image the motion of solid tissues such as the heart walls. Colour Doppler imaging is now provided on almost all commercial ultrasound machines, and has been...

Ultrasonic flowmeters

International Nuclear Information System (INIS)

Wittekind, W.D.

1979-01-01

A prototype ultrasonic flowmeter was assembled and tested. The theoretical basis of this prototype ultrasonic flowmeter is reviewed; the equipment requirements for a portable unit are discussed; the individual electronic modules contained in the prototype are described; the operating procedures and configuration are explained; and the data from preliminary calibrations are presented. The calibration data confirm that the prototype operates according to theoretical predictions and can indeed provide nonintrusive flow measurements to predicted accuracies for pipes larger than two inches, under single phase stable flow conditions

Evacuation drill at CMS

CERN Multimedia

Niels Dupont-Sagorin and Christoph Schaefer

2012-01-01

Training personnel, including evacuation guides and shifters, checking procedures, improving collaboration with the CERN Fire Brigade: the first real-life evacuation drill at CMS took place on Friday 3 February from 12p.m. to 3p.m. in the two caverns located at Point 5 of the LHC.   CERN personnel during the evacuation drill at CMS. Evacuation drills are required by law and have to be organized periodically in all areas of CERN, both above and below ground. The last drill at CMS, which took place in June 2007, revealed some desiderata, most notably the need for a public address system. With this equipment in place, it is now possible to broadcast audio messages from the CMS control room to the underground areas.   The CMS Technical Coordination Team and the GLIMOS have focused particularly on preparing collaborators for emergency situations by providing training and organizing regular safety drills with the HSE Unit and the CERN Fire Brigade. This Friday, the practical traini...

Stakeholder acceptance analysis ResonantSonic drilling

International Nuclear Information System (INIS)

Peterson, T.

1995-12-01

This report presents evaluations, recommendations, and requirements concerning ResonantSonic Drilling (Sonic Drilling), derived from a three-year program of stakeholder involvement. Sonic Drilling is an innovative method to reach contamination in soil and groundwater. The resonant sonic drill rig uses counter-rotating weights to generate energy, which causes the drill pipe to vibrate elastically along its entire length. In the resonant condition, forces of up to 200,000 pounds are transmitted to the drill bit face to create a cutting action. The resonant energy causes subsurface materials to move back into the adjacent formation, permitting the drill pipe to advance. This report is for technology developers and those responsible for making decisions about the use of technology to remediate contamination by volatile organic compounds. Stakeholders' perspectives help those responsible for technology deployment to make good decisions concerning the acceptability and applicability of sonic drilling to the remediation problems they face

Drilling of bone: A comprehensive review

Science.gov (United States)

Pandey, Rupesh Kumar; Panda, S.S.

2013-01-01

Background Bone fracture treatment usually involves restoring of the fractured parts to their initial position and immobilizing them until the healing takes place. Drilling of bone is common to produce hole for screw insertion to fix the fractured parts for immobilization. Orthopaedic drilling during surgical process causes increase in the bone temperature and forces which can cause osteonecrosis reducing the stability and strength of the fixation. Methods A comprehensive review of all the relevant investigations carried on bone drilling is conducted. The experimental method used, results obtained and the conclusions made by the various researchers are described and compared. Result Review suggests that the further improvement in the area of bone drilling is possible. The systematic review identified several consequential factors (drilling parameters and drill specifications) affecting bone drilling on which there no general agreement among investigators or are not adequately evaluated. These factors are highlighted and use of more advanced methods of drilling is accentuated. The use of more precise experimental set up which resembles the actual situation and the development of automated bone drilling system to minimize human error is addressed. Conclusion In this review, an attempt has been made to systematically organize the research investigations conducted on bone drilling. Methods of treatment of bone fracture, studies on the determination of the threshold for thermal osteonecrosis, studies on the parameters influencing bone drilling and methods of the temperature measurement used are reviewed and the future work for the further improvement of bone drilling process is highlighted. PMID:26403771

Influence of drill helical direction on exit damage development in drilling carbon fiber reinforced plastic

Science.gov (United States)

Bai, Y.; Jia, Z. Y.; Wang, F. J.; Fu, R.; Guo, H. B.; Cheng, D.; Zhang, B. Y.

2017-06-01

Drilling is inevitable for CFRP components’ assembling process in the aviation industry. The exit damage frequently occurs and affects the load carrying capacity of components. Consequently, it is of great urgency to enhance drilling exit quality on CFRP components. The article aims to guide the reasonable choice of drill helical direction and effectively reduce exit damage. Exit observation experiments are carried out with left-hand helical, right-hand helical and straight one-shot drill drilling T800S CFRP laminates separately. The development rules of exit damage and delamination factor curves are obtained. Combined with loading conditions and fracture modes of push-out burrs, and thrust force curves, the influence of drill helical direction on exit damage development is derived. It is found that the main fracture modes for left-hand helical, right-hand helical, and straight one-shot drill are mode I, extrusive fracture, mode III respectively. Among them, mode III has the least effect on exit damage development. Meanwhile, the changing rate of thrust force is relative slow for right-hand helical and straight one-shot drill in the thrust force increasing phase of stage II, which is disadvantaged for exit damage development. Therefore, straight one-shot drill’s exit quality is the best.

Pulsed ultrasonic stir welding system

Science.gov (United States)

Ding, R. Jeffrey (Inventor)

2013-01-01

An ultrasonic stir welding system includes a welding head assembly having a plate and a rod passing through the plate. The rod is rotatable about a longitudinal axis thereof. During a welding operation, ultrasonic pulses are applied to the rod as it rotates about its longitudinal axis. The ultrasonic pulses are applied in such a way that they propagate parallel to the longitudinal axis of the rod.

Ultrasonic stir welding process and apparatus

Science.gov (United States)

Ding, R. Jeffrey (Inventor)

2009-01-01

An ultrasonic stir welding device provides a method and apparatus for elevating the temperature of a work piece utilizing at least one ultrasonic heater. Instead of relying on a rotating shoulder to provide heat to a workpiece an ultrasonic heater is utilized to provide ultrasonic energy to the workpiece. A rotating pin driven by a motor assembly performs the weld on the workpiece. A handheld version can be constructed as well as a fixedly mounted embodiment.

Heat accumulation during sequential cortical bone drilling.

Science.gov (United States)

Palmisano, Andrew C; Tai, Bruce L; Belmont, Barry; Irwin, Todd A; Shih, Albert; Holmes, James R

2016-03-01

Significant research exists regarding heat production during single-hole bone drilling. No published data exist regarding repetitive sequential drilling. This study elucidates the phenomenon of heat accumulation for sequential drilling with both Kirschner wires (K wires) and standard two-flute twist drills. It was hypothesized that cumulative heat would result in a higher temperature with each subsequent drill pass. Nine holes in a 3 × 3 array were drilled sequentially on moistened cadaveric tibia bone kept at body temperature (about 37 °C). Four thermocouples were placed at the center of four adjacent holes and 2 mm below the surface. A battery-driven hand drill guided by a servo-controlled motion system was used. Six samples were drilled with each tool (2.0 mm K wire and 2.0 and 2.5 mm standard drills). K wire drilling increased temperature from 5 °C at the first hole to 20 °C at holes 6 through 9. A similar trend was found in standard drills with less significant increments. The maximum temperatures of both tools increased from drill sizes was found to be insignificant (P > 0.05). In conclusion, heat accumulated during sequential drilling, with size difference being insignificant. K wire produced more heat than its twist-drill counterparts. This study has demonstrated the heat accumulation phenomenon and its significant effect on temperature. Maximizing the drilling field and reducing the number of drill passes may decrease bone injury. © 2015 Orthopaedic Research Society. Published by Wiley Periodicals, Inc.

Imaging techniques for ultrasonic testing

International Nuclear Information System (INIS)

2013-01-01

These seminar proceedings contain 16 lectures on the following topics: 1. From imaging to quantification - ultrasound methods in medical diagnostics; 2. SAFT, TOFD, Phased Array - classical applications and recent developments in ultrasonic imaging; 3. Innovative ultrasonic imaging methods in research and application; 4. Industrial ultrasonic testing of fibre-reinforced structures of complex geometry; 5. Visualisation of crack tips in the inspection of wheel set shafts with longitudinal boreholes as a means of avoiding unnecessary wheel set changes; 6. Areal analysis of the propagation of Lamb waves on curved, anisotropic structures; 7. High-resolution representation in immersion technique testing; 8. Variants in generating images from phased array measurement data - practical examples involving copper, carbon-fibre reinforced plastic and other materials; 9. GIUM - an unconventional method of microstructure imaging using ultrasonic stimulation and laser vibrometry scanning; 10. Innovative air-ultrasonic testing concepts for improved imaging; 11. Use of imaging methods for improving the quality of test results from nondestructive testing; 12. Modelling and visualisation of EMUS stimulation for transducer optimisation; 13. Use of SAFT in the manufacture of energy conversion machines; 14. Ultrasonic imaging tests for improved defect characterisation during weld seam inspection on longitudinally welded large-diameter pipes; 15. SAFT reconstruction for testing austenitic weld seams and dissimilar metal weld seams for transverse cracks; 16. Imaging-based optimisation method for quantitative ultrasonic testing of anisotropic inhomogeneous austenitic welded joints with determination and utilisation of their elastic properties. One contribution has been abstracted separately. [de

Optimization of Ultrasonic-Assisted Extraction of Flavonoid Compounds and Antioxidants from Alfalfa Using Response Surface Method

Directory of Open Access Journals (Sweden)

Chang-Liang Jing

2015-08-01

Full Text Available Ultrasonic-assisted extraction (UAE was used to extract flavonoid-enriched antioxidants from alfalfa aerial part. Response surface methodology (RSM, based on a four-factor, five-level central composite design (CCD, was employed to obtain the optimal extraction parameters, in which the flavonoid content was maximum and the antioxidant activity of the extracts was strongest. Radical scavenging capacity of the extracts, which represents the amounts of antioxidants in alfalfa, was determined by using 2,2′-azino-bis (3-ethylbenzothiazoline-6-sulphonicacid (ABTS and 2,2′-diphenyl-1-picrylhydrazyl (DPPH methods. The results showed good fit with the proposed models for the total flavonoid extraction (R2 = 0.9849, for the antioxidant extraction assayed by ABTS method (R2 = 0.9764, and by DPPH method (R2 = 0.9806. Optimized extraction conditions for total flavonoids was a ratio of liquid to solid of 57.16 mL/g, 62.33 °C, 57.08 min, and 52.14% ethanol. The optimal extraction parameters of extracts for the highest antioxidant activity by DPPH method was a ratio of liquid to solid 60.3 mL/g, 54.56 °C, 45.59 min, and 46.67% ethanol, and by ABTS assay was a ratio of liquid to solid 47.29 mL/g, 63.73 °C, 51.62 min, and 60% ethanol concentration. Our work offers optimal extraction conditions for total flavonoids and antioxidants from alfalfa.

Quality in drilling operations

Energy Technology Data Exchange (ETDEWEB)

Duncan, E; Gervais, I [Sedco Forex Jacintoport Facility, Channelview, TX (United States); Le Moign, Y; Pangarkar, S; Stibbs, B [Sedco Forex, Montrouge (France); McMorran, P [Sedco Forex, Pau (France); Nordquist, E [Dubai Petroleum Company, Dubai (United Arab Emirates); Pittman, T [Sedco Forex, Perth (Australia); Schindler, H [Sedco Forex, Dubai (United Arab Emirates); Scott, P [Woodside Offshore Petroleum Pty. Ltd., Perth (Australia)

1997-12-31

Driven by cost and profitability pressures, quality has taken on new meaning and importance in the oil field during the past decade. In drilling operations, new initiatives have led to cooperative team efforts between operators and drilling contractors to enhance quality. In this article examples are given of how one drilling contractor, by adopting a quality culture, is reaping major benefits for its clients as well as its employees. 22 figs., 19 refs.

Quality in drilling operations

Energy Technology Data Exchange (ETDEWEB)

Duncan, E.; Gervais, I. [Sedco Forex Jacintoport Facility, Channelview, TX (United States); Le Moign, Y.; Pangarkar, S.; Stibbs, B. [Sedco Forex, Montrouge (France); McMorran, P. [Sedco Forex, Pau (France); Nordquist, E. [Dubai Petroleum Company, Dubai (United Arab Emirates); Pittman, T. [Sedco Forex, Perth (Australia); Schindler, H. [Sedco Forex, Dubai (United Arab Emirates); Scott, P. [Woodside Offshore Petroleum Pty. Ltd., Perth (Australia)

1996-12-31

Driven by cost and profitability pressures, quality has taken on new meaning and importance in the oil field during the past decade. In drilling operations, new initiatives have led to cooperative team efforts between operators and drilling contractors to enhance quality. In this article examples are given of how one drilling contractor, by adopting a quality culture, is reaping major benefits for its clients as well as its employees. 22 figs., 19 refs.

Performance of ultrasonic and hydrogen peroxide technologies in removal of Bisphenol A from Aqueous solution

Directory of Open Access Journals (Sweden)

MH Dehghani

2016-05-01

Full Text Available Introduction:BPA is a non biodegradable antioxidant that has greatly hazardous for human and animals health. and Because of the eliminating alone fewness amount of the BPA during the wastewater treatment, wastewater that contains BPA can be source of pollution in aqueous solution. The objective of this study was Performance of ultrasonic and H2O2 technologies in removal of BPA from aqueous solution. Methods:Experiments of sonochemical was carried out with use of unit ultrasonicator (Elma, which in the two power 300 and 500W, frequencies at 35 and 130KHz. Hydrogen Peroxide in concentrations at 5, 15 and 30mg/lit was applied. Initial concentration BPA at limits 2, 5, 20 and 50 mg/lit which For measuring concentration of BPA used from Spectrometer UV/VIS Lambada 25 Perkin Elmer, Shelton unit. Results:The results demonstrated that hybrid ultrasonic and peroxide Hydrogen processes with Efficiency 98.65%,  has the highest efficiency in the removal of BPA. The most decomposition rate achieved at the frequency of 130 KHz and 500W assisted by 30mg/lit H2O2 at pH 11. Also the results demonstrated that with pH increase destruction rate BPA the increased by any three processes (ultrasonic, H2O2 and both hybrid. Conclusion:The results demonstrated that hybrid ultrasonic and peroxide Hydrogen processes can be used as a clean method and friendly environment for waters treatment are contains desirable BPA.

Drilling history of core hole DB-15

International Nuclear Information System (INIS)

Diediker, L.D.; Ledgerwood, R.K.

1980-09-01

This core hole was drilled to obtain hydrologic and chemical data on the permeable zones of the Saddle Mountains and Wanapum Formations. These data were obtained by testing the zones that were penetrated during drilling. This testing-as-drilled method reduced the potential problems of interflow and water contamination. This report summarizes the drilling and coring operations; geologic logging, hydrologic testing, and geophysical logging activities; and cementing operations of DB-15 during drilling. The successful completion of DB-15 demonstrated that hydrologic testing can be conducted during core drilling operations. More reliable head measurements and uncontaminated representative water samples from isolated permeable zones, which have not been exposed to potential open borehole cross-flow and head equilibration problems, were benefits derived from the testing-as-drilled method. Disadvantages of the technique were a longer time to complete the borehole caused by time required for testing and increased drilling costs due to rig standby time during testing. Extension of the testing-as-drilled method to the drilling of future core holes is recommended. An evaluation should be made of the required hydrologic data and expected borehole stratigraphy before and during drilling to allow uninterrupted drilling in zones of low permeability that can be tested after drilling is complete

A vision for drilling

Energy Technology Data Exchange (ETDEWEB)

Millheim, K. [Montanuniversitaet Leoben (Austria)

1995-12-31

The future of drilling lies in its relationship with the oil and gas industry. This paper examines how the future of drilling is seen from the view point of the exploration manager, the drilling contractor, the drilling engineer and the company president or managing director. The various pressures on the oil and gas industry are examined, such as environmental issues, alternative energy sources, and the price of oil which determines how companies are run. Exploration activity is driven by the price of oil and gas. The development of wells with multiple horizontal wells or multiple horizontal wells with tributaries will reduce the cost of exploration. Companies will rely less and less on reservoir simulation and more on cheap well-bores, multi-lateral well-bores and will exploit oil that could not be exploited before. The cost of exploratory drilling will need to be kept down so that in the future the industry will get better at economically finding fields at the 10 million to 20 million barrel range that would not have been possible before. The future is expected to see drilling contractors tunnelling, making sewerage lines and drilling 10,000 foot wells with purpose built rigs. Franchising will become a feature of the industry as will the use of databases to answer key technical questions. Offshore platforms will be built to be moveable and disposable. The industry is capable of solving problems, meeting challenges and making ideas work, providing much hope for the future. 10 figs., 1 photo.

Deep-Time drilling in the Australian Archean: the Agouron Institute geobiological drilling project. (Invited)

Science.gov (United States)

Buick, R.

2010-12-01

The Agouron Institute has sponsored deep-time drilling across the South African Archean-Proterozoic boundary, investigating the rise of oxygen over an onshore-offshore environmental transect. It is now supporting a drilling program in the Australian Archean of the Pilbara Craton, addressing a similar theme but with the added goal of resolving controversy over the age and origin of hydrocarbon biomarker molecules in ancient kerogenous shales. As these have been claimed to provide evidence for the evolution of oxygenic photosynthesis long before the rise of atmospheric oxygen to persistently high levels during the ~2.3 Ga “Great Oxidation Event”, their syngenesis with their host shales is thus of critical importance for the interpretation of Earth’s early oxygenation history. During the first drilling season, 3 holes were drilled using techniques and equipment to minimize organic geochemical contamination (new drill-string components cleaned before drilling potentially biomarker-bearing rocks, pre-contamination of drilling fluid with a synthetic organic compound of similar geochemical characteristics to biomarkers, sterile cutting and storage of samples immediately upon retrieval from the core-barrel). The initial hole was a blank control for organic geochemistry, drilled into rocks too metamorphosed to retain biomarker molecules. These rocks, cherts, carbonates and pelites of the 3.52 Ga Coucal Formation, Coonterunah Group, have been metamorphosed to upper greenschist facies at temperatures near 500°C and so should have had any ancient soluble hydrocarbons destroyed. However, because they contain both carbonate and organic carbon, these rocks can instead provide isotopic information about the earliest evolution of biological metabolism as they possess residues of both the reactant and product sides of the carbon-fixation reaction. The second hole sampled an on-shore section of carbonates and kerogenous shales in the ~2.65 Ga Carawine Dolomite and Lewin Shale

Drilling miniature holes, Part III

Energy Technology Data Exchange (ETDEWEB)

Gillespie, L.K.

1978-07-01

Miniature components for precision electromechanical mechanisms such as switches, timers, and actuators typically require a number of small holes. Because of the precision required, the workpiece materials, and the geometry of the parts, most of these holes must be produced by conventional drilling techniques. The use of such techniques is tedious and often requires considerable trial and error to prevent drill breakage, minimize hole mislocation and variations in hole diameter. This study of eight commercial drill designs revealed that printed circuit board drills produced better locational and size repeatability than did other drills when centerdrilling was not used. Boring holes 1 mm in dia, or less, as a general rule did not improve hole location in brass or stainless steel. Hole locations of patterns of 0.66-mm holes can be maintained within 25.4-..mu..m diametral positional tolerance if setup misalignments can be eliminated. Size tolerances of +- 3.8 ..mu..m can be maintained under some conditions when drilling flat plates. While these levels of precision are possible with existing off-the-shelf drills, they may not be practical in many cases.

Avoiding pollution in scientific ocean drilling

International Nuclear Information System (INIS)

Francis, T.J.G.

1999-01-01

Scientific ocean drilling has been carried out in the world's oceans since the nineteen sixties. From 1968-83 the Deep Sea Drilling Project (DSDP), managed by the Scripps Institution of Oceanography in California under a contract with the US National Science Foundation, employed the drilling vessel Glomar Challenger for this purpose. In January 1985 the Ocean Drilling Program (GDP), operated by Texas A and M University, began operations with the drillship JOIDES Resolution which continue to this day. The principal funding agency remains the US National Science Foundation, but since its inception GDP has been an international program and currently receives financial support from 21 countries. The ODP operates globally and, as with DSDP before it, drills without a riser or blowout preventer in a wide range of geological environments. Water depths at GDP drill sites have ranged from 38 m to 5969 m, but are typically within the range 1000-5000 m. Depths of penetration at GDP drill sites, while generally less than 1000 m, have ranged up to 2111 m below the sea floor. The drilling fluid is seawater, although occasional slugs of mud are circulated to clean or condition the hole. Thus drilling is carried out without well control, i.e. without the ability to control pressures within the well. Because of the absence of well control, it is vital to ensure that the drillship does not drill into an accumulation of oil or gas. Drilling into a charged reservoir and causing oil or gas to escape into the marine environment is recognised as the main pollution hazard in scientific ocean drilling

FPGA Implementation of an Amplitude-Modulated Continuous-Wave Ultrasonic Ranger Using Restructured Phase-Locking Scheme

Directory of Open Access Journals (Sweden)

P. Sumathi

2010-01-01

Full Text Available An accurate ultrasonic range finder employing Sliding Discrete Fourier Transform (SDFT based restructured phase-locked loop (RPLL, which is an improved version of the recently proposed integrated phase-locking scheme (IPLL, has been expounded. This range finder principally utilizes amplitude-modulated ultrasonic waves assisted by an infrared (IR pilot signal. The phase shift between the envelope of the reference IR pilot signal and that of the received ultrasonic signal is proportional to the range. The extracted envelopes are filtered by SDFT without introducing any additional phase shift. A new RPLL is described in which the phase error is driven to zero using the quadrature signal derived from the SDFT. Further, the quadrature signal is reinforced by another cosine signal derived from a lookup table (LUT. The pulse frequency of the numerically controlled oscillator (NCO is extremely accurate, enabling fine tuning of the SDFT and RPLL also improves the lock time for the 50 Hz input signal to 0.04 s. The percentage phase error for the range 0.6 m to 6 m is about 0.2%. The VHDL codes generated for the various signal processing steps were downloaded into a Cyclone FPGA chip around which the ultrasonic ranger had been built.

Full-field ultrasonic inspection for a composite sandwich plate skin-core debonding detection using laser-based ultrasonics

Science.gov (United States)

Chong, See Yenn; Victor, Jared J.; Todd, Michael D.

2017-04-01

In this paper, a full-field ultrasonic guided wave method is proposed to inspect a composite sandwich specimen made for an aircraft engine nacelle. The back skin/core interface of the specimen is built with two fabricated disbond defects (diameters of 12.7 mm and 25.4 mm) by removing areas of the adhesive used to bond the back skin to the core. A laser ultrasonic interrogation system (LUIS) incorporated with a disbond detection algorithm is developed. The system consists of a 1-kHz laser ultrasonic scanning system and a single fixed ultrasonic sensor to interrogate ultrasonic guided waves in the sandwich specimen. The interest area of 400 mm × 400 mm is scanned at a 0.5 mm scan interval. The corresponding full-field ultrasonic data is obtained and generated in the three-dimensional (3-D) space-time domain. Then, the 3-D full-field ultrasonic data is Fourier transformed and the ultrasonic frequency spectra are analyzed to determine the dominant frequency that is sensitive to the disbond defects. Continuous wavelet transform (CWT) based on fast Fourier transform (FFT) is implemented as a single-frequency bandpass filter to filter the full-field ultrasonic data in the 3-D space-time domain at the selected dominant frequency. The LUIS has shown the ability to detect the disbond with diameters of 11 mm and 23 mm which match to the pre-determined disbond sizes well. For future research, a robust signal processing algorithm and a model-based matched filter will be investigated to make the detection process autonomous and improve detectability

21 CFR 872.4850 - Ultrasonic scaler.

Science.gov (United States)

2010-04-01

... DEVICES DENTAL DEVICES Surgical Devices § 872.4850 Ultrasonic scaler. (a) Identification. An ultrasonic scaler is a device intended for use during dental cleaning and periodontal (gum) therapy to remove calculus deposits from teeth by application of an ultrasonic vibrating scaler tip to the teeth. (b...

Horizontal Directional Drilling-Length Detection Technology While Drilling Based on Bi-Electro-Magnetic Sensing

Directory of Open Access Journals (Sweden)

Yudan Wang

2017-04-01

Full Text Available The drilling length is an important parameter in the process of horizontal directional drilling (HDD exploration and recovery, but there has been a lack of accurate, automatically obtained statistics regarding this parameter. Herein, a technique for real-time HDD length detection and a management system based on the electromagnetic detection method with a microprocessor and two magnetoresistive sensors employing the software LabVIEW are proposed. The basic principle is to detect the change in the magnetic-field strength near a current coil while the drill stem and drill-stem joint successively pass through the current coil forward or backward. The detection system consists of a hardware subsystem and a software subsystem. The hardware subsystem employs a single-chip microprocessor as the main controller. A current coil is installed in front of the clamping unit, and two magneto resistive sensors are installed on the sides of the coil symmetrically and perpendicular to the direction of movement of the drill pipe. Their responses are used to judge whether the drill-stem joint is passing through the clamping unit; then, the order of their responses is used to judge the movement direction. The software subsystem is composed of a visual software running on the host computer and a software running in the slave microprocessor. The host-computer software processes, displays, and saves the drilling-length data, whereas the slave microprocessor software operates the hardware system. A combined test demonstrated the feasibility of the entire drilling-length detection system.

Effects of implant drilling parameters for pilot and twist drills on temperature rise in bone analog and alveolar bones.

Science.gov (United States)

Chen, Yung-Chuan; Hsiao, Chih-Kun; Ciou, Ji-Sih; Tsai, Yi-Jung; Tu, Yuan-Kun

2016-11-01

This study concerns the effects of different drilling parameters of pilot drills and twist drills on the temperature rise of alveolar bones during dental implant procedures. The drilling parameters studied here include the feed rate and rotation speed of the drill. The bone temperature distribution was analyzed through experiments and numerical simulations of the drilling process. In this study, a three dimensional (3D) elasto-plastic dynamic finite element model (DFEM) was proposed to investigate the effects of drilling parameters on the bone temperature rise. In addition, the FE model is validated with drilling experiments on artificial human bones and porcine alveolar bones. The results indicate that 3D DFEM can effectively simulate the bone temperature rise during the drilling process. During the drilling process with pilot drills or twist drills, the maximum bone temperature occurred in the region of the cancellous bones close to the cortical bones. The feed rate was one of the important factors affecting the time when the maximum bone temperature occurred. Our results also demonstrate that the elevation of bone temperature was reduced as the feed rate increased and the drill speed decreased, which also effectively reduced the risk region of osteonecrosis. These findings can serve as a reference for dentists in choosing drilling parameters for dental implant surgeries. Copyright © 2016 IPEM. Published by Elsevier Ltd. All rights reserved.

The effect of drilling parameters for surface roughness in drilling of AA7075 alloy

Directory of Open Access Journals (Sweden)

Yaşar Nafiz

2017-01-01

Full Text Available AA7075 aluminum alloy has been very popular significantly interest in the production of structural components in automotive and aviation applications due to its high strength, low density, good plasticity and better machinability comparable to many metals. Particularly, final products must have uniformly high quality to ensure essential safety standards in the aircraft industry. The optimization of hole quality which can variable according to tool geometry and drilling parameters is important in spite of high machinability rate of AA7075 alloy. In this study, the effects of drilling parameters on average surface roughness (Ra has been investigated in drilling of AA7075 with tungsten carbide drills. Machining experiments were performed with three different drill point angles and three different levels of cutting parameters (feed rate, cutting speed. The effects of drilling parameters on thrust force has been determined with ANOVA in %95 confidence level. Feed rate was determined as the most important factor on Ra according to ANOVA results. Moreover, it was shown that increasing feed rate leads to increase of Ra while increasing drill point angle leads to decrease of Ra. The optimum surface roughness was obtained with point angle of 130°, cutting speed of 40 m/min and feed rate of 0.1 mm/rev, thereby the validity of optimization was confirmed with Taguchi method.

Ultrasonic extraction of antioxidants from Chinese sumac (Rhus typhina L.) fruit using response surface methodology and their characterization.

Science.gov (United States)

Lai, Jixiang; Wang, Huifang; Wang, Donghui; Fang, Fang; Wang, Fengzhong; Wu, Tao

2014-06-27

For the first time, response surface methodology (RSM) using a Box-Behnken Design (BBD) was employed to optimize the conditions for ultrasonic assisted extraction (UAE) of antioxidants from Chinese sumac (Rhus typhina L.) fruits. Initially, influencing factors such as liquid-solid ratio, duration of ultrasonic assisted extraction, pH range, extraction temperature and ethanol concentration were identified using single-factor experiments. Then, with respect to the three most significant influencing factors, the extraction process focusing on the DPPH· scavenging capacity of antioxidants was optimized using RSM. Results showed that the optimal conditions for antioxidant extraction were 13.03:1 (mL/g) liquid-solid ratio, 16.86 min extraction time and 40.51% (v/v) ethanol, and the desirability was 0.681. The UPLC-ESI-MS analysis results revealed eleven kinds of phenolic compounds, including four major rare anthocyanins, among the antioxidants. All these results suggest that UAE is efficient at extracting antioxidants and has the potential to be used in industry for this purpose.

Ultrasonic Bat Deterrent Technology

Energy Technology Data Exchange (ETDEWEB)

Kinzie, Kevin; Rominger, Kathryn M.

2017-12-14

The project objective was to advance the development and testing of an Near commercial bat-deterrent system with a goal to increase the current GE deterrent system effectiveness to over 50% with broad species applicability. Additionally, the research supported by this program has provided insights into bat behavior and ultrasonic deterrent design that had not previously been explored. Prior research and development had demonstrated the effectiveness of a commercial-grade, air-powered, ultrasonic bat deterrent to be between 30-50% depending upon the species of bat. However, the previous research provided limited insight into the behavioral responses of bats in the presence of ultrasonic deterrent sound fields that could be utilized to improve effectiveness. A unique bat flight room was utilized to observe the behavioral characteristics of bats in the presence of ultrasonic sound fields. Behavioral testing in the bat flight facility demonstrated that ultrasonic sounds similar to those produced by the GE deterrent influenced the activities and behaviors, primarily those associated with foraging, of the species exposed. The study also indicated that continuous and pulsing ultrasonic signals had a similar effect on the bats, and confirmed that as ultrasonic sounds attenuate, their influence on the bats’ activities and behavior decreases. Ground testing at Wolf Ridge Wind, LLC and Shawnee National Forest assessed both continuous and pulsing deterrent signals emitted from the GE deterrent system and further enhanced the behavioral understanding of bats in the presence of the deterrent. With these data and observations, the existing 4-nozzle continuous, or steady, emission ultrasonic system was redesigned to a 6-nozzle system that could emit a pulsing signal covering a larger air space around a turbine. Twelve GE 1.6-100 turbines were outfitted with the deterrent system and a formal three-month field study was performed using daily carcass searches beneath the 12

3D Model Optimization of Four-Facet Drill for 3D Drilling Simulation

Directory of Open Access Journals (Sweden)

Buranský Ivan

2016-09-01

Full Text Available The article is focused on optimization of four-facet drill for 3D drilling numerical modelling. For optimization, the process of reverse engineering by PowerShape software was used. The design of four-facet drill was created in NumrotoPlus software. The modified 3D model of the drill was used in the numerical analysis of cutting forces. Verification of the accuracy of 3D models for reverse engineering was implemented using the colour deviation maps. The CAD model was in the STEP format. For simulation software, 3D model in the STEP format is ideal. STEP is a solid model. Simulation software automatically splits the 3D model into finite elements. The STEP model was therefore more suitable than the STL model.

Ultrasonic imaging of materials under unconventional circumstances

Energy Technology Data Exchange (ETDEWEB)

Declercq, Nico Felicien, E-mail: declercqdepatin@gatech.edu; McKeon, Peter, E-mail: declercqdepatin@gatech.edu; Liu, Jingfei; Shaw, Anurupa [Georgia Institute of Technology, UMI Georgia Tech - CNRS 2958, George W. Woodruff School of Mechanical Engineering, Georgia Tech Lorraine, Laboratory for Ultrasonic Nondestructive Evaluation, 2 rue Marconi, 5070 Met-technopole (France); Slah, Yaacoubi [Institut de Soudure, 4 Bvd Henri Becquerel, Espace Cormontaigne, 57937 Yutz (France)

2015-03-31

This paper reflects the contents of the plenary talk given by Nico Felicien Declercq. “Ultrasonic Imaging of materials” covers a wide technological area with main purpose to look at and to peek inside materials. In an ideal world one would manage to examine materials like a clairvoyant. Fortunately this is impossible hence nature has offered sufficient challenges to mankind to provoke curiosity and to develop science and technology. Here we focus on the appearance of certain undesired physical effects that prohibit direct imaging of materials in ultrasonic C-scans. Furthermore we try to make use of these effects to obtain indirect images of materials and therefore make a virtue of necessity. First we return to one of the oldest quests in the progress of mankind: how thick is ice? Our ancestors must have faced this question early on during migration to Northern Europe and to the America’s and Asia. If a physicist or engineer is not provided with helpful tools such as a drill or a device based on ultrasound, it is difficult to determine the ice thickness. Guided waves, similar to those used for nondestructive testing of thin plates in structural health monitoring can be used in combination with the human ear to determine the thickness of ice. To continue with plates, if an image of its interior is desired high frequency ultrasonic pulses can be applied. It is known by the physicist that the resolution depends on the wavelength and that high frequencies usually result in undesirably high damping effects inhibiting deep penetration into the material. To the more practical oriented engineer it is known that it is advantageous to polish surfaces before examination because scattering and diffraction of sound lowers the image resolution. Random scatterers cause some blurriness but cooperating scatters, causing coherent diffraction effects similar to the effects that cause DVD’s to show rainbow patterns under sunlight, can cause spooky images and erroneous

Drilling technology advances on four fronts

Energy Technology Data Exchange (ETDEWEB)

Budd, G.

2002-01-01

Trends and advances in drilling technology are discussed. Four different major trends have been identified. One of these is proprietary case drilling which is said to allow operators to simultaneously drill, case, and evaluate oil and gas wells. In proprietary case drilling, the well is drilled with standard oil field casing which remains in the hole all the time, eliminating the need for tripping. Drill bits and other downhole tools are lowered via wireline inside the casing and latched to the last joint of casing. Wells are drilled either by rotating the casing or by using a downhole mud motor for steering, using conventional directional tools. This technology was introduced by Tesco and is marketed in 25 countries along with a full range of drilling products and services. Super single rigs are an other trend which, owing to their versatility, combined with relatively small environmental footprint have become the rig of choice in a growing number of drilling programs. Super single rigs use 45-ft. joints of drill pipe, more versatile top drives and they have an automated pipe handling system. Super singles can be used on both vertical and slant wells and offer advantages of lower costs, higher efficiencies and greater drilling depths. Given their low environmental impact hydraulic capability, super singles also find application where zero disturbance rules are in effect, as for example, in some parts of southern Alberta. Directional drilling and MWD are most associated with SAGD projects but they also have been used and made significant difference in other spheres of oil recovery as well. The fact is that about 35 percent of wells drilled today are drilled with some form of directional drilling; this will stimulate the growth of ever more advanced MWD technology. Northern rigs are in a class of their own in that here the emphasis is on keeping the crew warm, as opposed to lots of gadgets. The most immediately-visible heat-conserving modification is the 60-ft wind

Quality control of disinfection in ultrasonic baths

Energy Technology Data Exchange (ETDEWEB)

Schoene, H. [Technical University Dresden (Germany). Faculty of Mechanical Engineering; Jatzwauk, L. [University Hospital of the Technical University Dresden (Germany). Abt. Krankenhaushygiene

2002-07-01

Numerous investigations under laboratory conditions confirmed the microbicidal efficacy of ultrasonication. Morphological destruction was shown on bacteria and fungi as well as on different virus species. Ultrasonic treatment seems to increase the effect of different antibiotics and disinfectants. Reasons for this synergism are largely unknown and uninvestigated, but the active principle seems to bee the dispersing effect of ultrasonication in combination with the destruction of cell wall or cell membrane. Unfortunately no validation of test conditions exists for most of these investigations, regarding intensity and frequency of ultrasonic waves, temperature of liquid medium and measurement of cavitation which is an essential part of physical and chemical effects in ultrasonic baths. In contrast to most laboratory experiments sound density of ultrasound for treatment of medical instruments is below 1 W/cm{sup 2} because instruments will be destroyed under stronger ultrasonic conditions. The frequency is below 50 KHz. This paper describes bactericidal and fungicidal effects of low- intensity-ultrasonication and its synergistical support to chemical disinfection. (orig.)

Drillings at Veitsivaara in Hyrynsalmi

International Nuclear Information System (INIS)

Hinkkanen, H.; Oehberg, A.

1990-04-01

According to Governmen's decision in principle Teollisuuden Voima Oy is obliged to make bedrock investigations for the final disposal of the spent fuel produced by its power plant in Olkiluoto. Areas in Kuhmo, Hyrynsalmi, Sievi, Konginkangas and Olkiluoto were selected for the preliminary site investigations to be carried out during years 1987-1992. In Veitsivaara, Hyrynsalmi the investigation program was started in April 1987. During years 1987-1988 a deep borehole (1002 m) and 4 and 500 m deep additional boreholes were core drilled in the area. Various parameters were measured from the flushing water during the drilling. Corelogging included collecting detailed data of fractures and determining the weathering degree and petrographical properties. Rock mechanical properties, uniaxial compressive strength, Young's modulus and Poisso's ratio were measured from core samples. The flushing water needed in the drillings was pumped from 100 m deep borehole wells drilled with down-the-hole method in the vicinity of the borehole. The water was labeled with 2 tracers before use. About 75 m deep hole was percussion drilled near the borehole KR1. The spreading of the flushing water in the upper part of bedrock and the quality off the ground of the groundwater were studied by taking watersamples from the hole. 30 vertical holes were core drilled down to the depth of 10 m in bedrock with a light drilling unit. Drilling was carried out in order to determine the thickness of the overburden, to investigate the geophysical anomaly sources and to support geological mapping in areas covered with overburden. Groundwater hydraulics is one of the main subjects during the preliminary site investigation phase. For that reason 7 multilevel piezometers were installed on the site to monitore hydraulic head in 3 levels in the uppermost part of bedrock. The work consisted of borehole drillings to the depth of 100 m, geophysical borehole loggings and installation of piezometers. In addition

Development and Application of an Ultrasonic Gas Flowmeter

International Nuclear Information System (INIS)

Hwang, Won Ho; Jeong, Hee Don; Park, Sang Gug; Jhang, Kyung Young

2002-01-01

This paper describes the development and the field application of the ultrasonic gas flowmeter for accurate measurement of the volumetric flow rate of gases in a harsh environmental conditions in iron and steel making company. This ultrasonic flowmeter is especially suited for measuring LDG, COG, BFG gases produced in iron and steel making process. This is a transit time type ultrasonic flowmeter. We have developed the transmitting and receiving algorithm of ultrasonic wave and the ultrasonic signal processing algorithm to develope a transit time type ultrasonic flowmeter. We have evaluated the performance of ultrasonic flowmeter by the calibration system with Venturi type standard flowmeter. We has confirmed its reliability by extensive field tests for a year in POSCO, iron and steel making company. Now we have developed the commercial model of ultrasonic flowmeter and applied to the POSCO gas line

Ultrasonic Tomography Imaging for Liquid-Gas Flow Measurement

Directory of Open Access Journals (Sweden)

Muhammad Jaysuman PUSPPANATHAN

2013-01-01

Full Text Available This research was carried out to measure two-phase liquid – gas flow regime by using a dual functionality ultrasonic transducer. Comparing to the common separated transmitter–receiver ultrasonic pairs transducer, the dual functionality ultrasonic transceiver is capable to produce the same measurable results hence further improvises and contributes to the hardware design improvement and system accuracy. Due to the disadvantages and the limitations of the separated ultrasonic transmitter–receiver pair, this paper presents a non-invasive ultrasonic tomography system using ultrasonic transceivers as an alternative approach. Implementation of ultrasonic transceivers, electronic measurement circuits, data acquisition system and suitable image reconstruction algorithms, the measurement of a liquid/gas flow was realized.

Casing drilling - first experience in Brazil; Casing drilling - primeira experiencia no Brasil

Energy Technology Data Exchange (ETDEWEB)

Placido, Joao Carlos Ribeiro; Medeiros, Fernando; Lucena, Humberto; Medeiros, Joao Carlos Martins de; Costa, Vicente Abel Soares Rosa da; Silva, Paulo Roberto Correa da [PETROBRAS, Rio de Janeiro, RJ (Brazil); Alves, Renato J.M. [Tesco, London (United Kingdom)

2004-07-01

This paper describes the 'Casing Drilling' technology and its first experience in Brazil. This new process of casing while drilling was first developed to reduce costs. This system integrates the drilling process and casing running in one operation, promoting a more efficient well construction system, reducing trip time and costs of drill pipes and their transportation. Besides, this methodology intends to eliminate hole problems related to trouble zones with abnormal pressure with loss circulation, to overcome zones with wellbore instabilities, and to facilitate well control. Two companies have been identified using this technology: Tesco and Weatherford. However, there are differences between the techniques used by these companies, which are described in this paper. In the first experience in Brazil, it was decided to field test the technology developed by Tesco. This paper describes the preparation, the operation and the results of this first test. (author)

Slant rigs offer big payoffs in shallow drilling

International Nuclear Information System (INIS)

Smith, J.; Edwards, B.

1992-01-01

Slant hole drilling technology can result in considerable savings over conventionally drilled deviated holes because mud motors and deviation control with measurement while drilling tools are usually unnecessary. The benefits of using slant hole rigs for development drilling improve after the bit walk tendencies and the correct bottom hole assemblies have been determined for a particular area. This article discusses three recent drilling operations that successfully used slant drilling technology on land-based projects: drilling for heavy oil in Alberta, drilling for gas in Alberta, and drilling a river crossing for a gas pipeline in British Columbia. These examples demonstrate the flexibility of slant drilling technology

Ultrasound-Assisted Extraction: Effect of Extraction Time and Solvent ...

African Journals Online (AJOL)

Purpose: To investigate the influence of extraction conditions assisted by ultrasound on the quality of extracts obtained from Mesembryanthemum edule shoots. Methods: The extraction procedure was carried out in an ultrasonic bath. The effect of two solvents (methanol and ethanol) and two extraction times (5 and 10 min) ...

Drillings at Kivetty in Konginkangas

International Nuclear Information System (INIS)

Hinkkanen, H.; Oehberg, A.

1990-05-01

According to Government's decision in principle Teollisuuden Voima Oy is obliged to make bedrock investigations for the final disposal of the spent fuel produced by its power plant in Olkiluoto. Areas in Kuhmo, Hyrynsalmi, Sievi, Konginkangas and Olkiluoto were selected for the preliminary site investigations to be carried out during years 1987-1992. In Kivetty, Konginkangas the investigation program was started in spring 1988. During years 1988-1989 a deep borehole (1019 m) and 4 about 500 m deep additional boreholes were core drilled in the area. The structure of the holes makes it possible to carry out many investigations in the holes. Various parameters were measured from the flushing water during the drilling. Corelogging included collecting detailed data of fractures and determining the weathering degree and petrographical properties. Rock mechanical properties, uniaxial compressive strength, Young's modulus and Poisson's ratio were measured from core samples. The flushing water needed in the drillings was pumped from 100 m deep borehole wells drilled with down-the-hole method in the vicinity of the borehole. The water was labeled with 2 tracers before use. 30 vertical holes were core drilled down to the depth of 10 m in bedrock with a light drilling unit. Drilling was carried out in order to determine the thickness of the overburden to investigate the geophysical anomaly sources and to support geological mapping in areas covered with overburden. Groundwater hydraulics is one of the main subjects during the preliminary site investigation phase. For that reason 7 multilevel piezometers were installed on the site to monitore hydraulic head in 3 levels in the uppermost part of bedrock. The work consisted of borehole drillings to the depth of 100 m, geophysical borehole loggings and installation of piezometers. In addition about 65 shotholes were drilled for VSP-, tubewave and seismic measurements

Drillings at Syyry in Sievi

International Nuclear Information System (INIS)

Hinkkanen, H.; Oehberg, A.

1990-10-01

According to Government's decision in principle Teollisuuden Voima Oy is obliged to make bedrock investigations for the final disposal of the spent fuel produced by its power plant in Olkiluoto. Areas in Kuhmo, Hyrynsalmi, Sievi, Konginkangas and Olkiluoto were selected for the preliminary site investigations to be carried out during years 1987-1992. In Syyry, Sievi the investigation program was started in spring 1988. During years 1988-1989 a deep borehole (1022 m) and 4 about 500-700 m deep additional boreholes were core drilled in the area. The structure of the holes makes it possible to carry out many investigations in the holes. Various parameters were measured from the flushing water during the drilling. Corelogging included collecting detailed data of fractures and determining the weathering degree and petrographical properties. Rock mechanical properties, uniaxial compressive strength, Young's modulus and Poisson's ratio were measured from core samples. The flushing water needed in the drillings was pumped from 100 m deep borehole wells drilled with down-the-hole method in the vicinity of the borehole. The water was labeled with 2 tracers before use. 35 vertical holes were core drilled down to the depth of 10-20 m in bedrock with a light drilling unit. Drilling was carried out in order to determine the thickness of the overburden, to investigate the geophysical anomaly sources and to support geological mapping in areas covered with overburden. Groundwater hydraulics is one of the main subjects during the preliminary site investigation phase. For that reason 7 multilevel piezometers were installed on the site to monitore hydraulic head in 3 levels in the uppermost part of bedrock. The work consisted of borehole drillings to the depth of 100 m, geophysical borehole loggings and installation of piezometers. In addition about 85 shotholes were drilled for VSP-, tubewave and seismic measurements

Drilling rig

Energy Technology Data Exchange (ETDEWEB)

Galiopa, A A; Yegorov, E K

1981-01-04

A drilling rig is proposed which contains a tower, lifter in the form of n infinite chain, and mobile rotator with holding device connected to the chain, and pipe holder. In order to accelerate the auxiliary operations to move the drilling string and unloaded rotator, the rotator is equipped with a clamp with means for transverse connection of it to both branches of the chain, while the pipe holders equipped with a clamp with means of connecting it to one of the branches of the chain.

Ultrasonic Stir Welding

Science.gov (United States)

Nabors, Sammy

2015-01-01

NASA Marshall Space Flight Center (MSFC) developed Ultrasonic Stir Welding (USW) to join large pieces of very high-strength metals such as titanium and Inconel. USW, a solid-state weld process, improves current thermal stir welding processes by adding high-power ultrasonic (HPU) energy at 20 kHz frequency. The addition of ultrasonic energy significantly reduces axial, frictional, and shear forces; increases travel rates; and reduces wear on the stir rod, which results in extended stir rod life. The USW process decouples the heating, stirring, and forging elements found in the friction stir welding process allowing for independent control of each process element and, ultimately, greater process control and repeatability. Because of the independent control of USW process elements, closed-loop temperature control can be integrated into the system so that a constant weld nugget temperature can be maintained during welding.

Pressured drilling riser design for drilling in ultra deep water with surface bop

Energy Technology Data Exchange (ETDEWEB)

Zhang, J.; Morrison, D.; Efthymiou, M.; Lo, K.H. [Shell Global Solutions, 78 - Velizy Villacoublay (France); Magne, E.; Leach, C. [Shell Internationale Exploration and Production (Netherlands)

2002-12-01

In conventional drilling with a semi-submersible rig valuable rig time is used to run and retrieve the BOP and its accessories on the seabed, and this time increases with water depth. Furthermore, use of the conventional sub-sea BOP requires a large-diameter riser, which requires substantial rig storage and deck load capacity prior to installation. It also requires high riser-tensioning capacity or additional buoyancy. Thus as the water depth increases, it leads to a need for heavy duty 4. and 5. generation rigs with escalation in costs. The high cost of deep-water drill rigs is leading to the development of Surface BOP technology. In this development, the BOP is placed above sea level and the riser is simply a continuation of the casing (typical diameter 13-3/8''). This eliminates the need for a heavy 21'' riser and for running the BOP to the sea bed and retrieving it. Moreover, the reduced tension requirement for the smaller riser extends the water depth capability of 3. generation drilling semi-submersibles, enabling them to drill in deeper waters. A critical success factor for this development is the ability to design the riser/casing to withstand high internal pressures due to well kicks, in addition to environmental loads, and to restrict vessel offsets within certain limits so as not to overload the riser under the prevailing weather conditions. This paper addresses the design considerations of a pressured drilling riser that can be used with a surface BOP in deep-water. Key design issues that are sensitive to ultra-deep-water applications are discussed. The technical aspects of using (disposable) standard casing with threaded connector for the drilling riser are discussed, with a particular emphasis on the connector fatigue-testing program to quantify the stress concentration factor for fatigue design. Emerging composite material offers some alternatives to the steel riser when drilling in ultra-deep water Design issues related to the

Development of coaxial ultrasonic probe for fatty liver diagnostic system using ultrasonic velocity change

Science.gov (United States)

Hori, Makoto; Yokota, Daiki; Aotani, Yuhei; Kumagai, Yuta; Wada, Kenji; Matsunaka, Toshiyuki; Morikawa, Hiroyasu; Horinaka, Hiromichi

2017-07-01

A diagnostic system for fatty liver at an early stage is needed because fatty liver is linked to metabolic syndrome. We have already proposed a fatty liver diagnosis method based on the temperature coefficient of ultrasonic velocity. In this study, we fabricated a coaxial ultrasonic probe by integrating two kinds of transducers for warming and signal detection. The diagnosis system equipped with the coaxial probe was applied to tissue-mimicking phantoms including the fat area. The fat content rates corresponding to the set rates of the phantoms were estimated by the ultrasonic velocity-change method.

Extended Reach Drilling on the example of Reelwell Drilling Method: Influence examination of different drill pipes on drilling performance on Idun field on the Norwegian Continental Shelf by PGNiG Norway AS.

OpenAIRE

Krol, Dariusz Pawel

2011-01-01

Master's thesis in Petroleum engineering Horizontal or extended reach drilling is incredibly fast growing technology. Although in some areas of the world ERD is still novelty, most of oil companies have been using the technology reliably and successfully for dozens of years. And those companies want to improve well-worn solutions to obtain better performance, thereby reducing costs. One of the main aspects that affects drilling performance and efficiency is adequate choice of drill pipe...

Pitch-catch only ultrasonic fluid densitometer

Science.gov (United States)

Greenwood, M.S.; Harris, R.V.

1999-03-23

The present invention is an ultrasonic fluid densitometer that uses a material wedge and pitch-catch only ultrasonic transducers for transmitting and receiving ultrasonic signals internally reflected within the material wedge. Density of a fluid is determined by immersing the wedge into the fluid and measuring reflection of ultrasound at the wedge-fluid interface. 6 figs.

Trends in the Drilling Waste Management

Directory of Open Access Journals (Sweden)

Lucyna Czekaj

2006-10-01

Full Text Available Petroleum Industry is trying to achieve sustainable development goals. Each year new solutions are implemented to minimize the environmental impact of drilling operations. The paper presents trends in the drilling waste management caused by introducing the sustainable development into the petroleum industry. Old solutions such as the drilling waste disposal at the waste dump or dumping ground are not acceptable from the environmental point of view. The paper presents an analysis of new solutions as the sustainable solutions. The most important problem is the chemical pollution in cuttings and the waste drilling mud. The industrial solutions as well as the laboratory research on the pollution removing from drilling wastes are analysed. The most promising method seems to be the recycling and design for the environment of drilling mud.

Depth estimation of laser glass drilling based on optical differential measurements of acoustic response

Science.gov (United States)

Gorodesky, Niv; Ozana, Nisan; Berg, Yuval; Dolev, Omer; Danan, Yossef; Kotler, Zvi; Zalevsky, Zeev

2016-09-01

We present the first steps of a device suitable for characterization of complex 3D micro-structures. This method is based on an optical approach allowing extraction and separation of high frequency ultrasonic sound waves induced to the analyzed samples. Rapid, non-destructive characterization of 3D micro-structures are limited in terms of geometrical features and optical properties of the sample. We suggest a method which is based on temporal tracking of secondary speckle patterns generated when illuminating a sample with a laser probe while applying known periodic vibration using an ultrasound transmitter. In this paper we investigated lasers drilled through glass vias. The large aspect ratios of the vias possess a challenge for traditional microscopy techniques in analyzing depth and taper profiles of the vias. The correlation of the amplitude vibrations to the vias depths is experimentally demonstrated.

Under sodium ultrasonic imaging system for PFBR

International Nuclear Information System (INIS)

Patankar, V.H.; Lalwani, S.K.; Agashe, A.A.

2014-01-01

Under Sodium UltraSonic Scanner (USUSS) has been developed to detect the growth and protrusion of fuel sub-assemblies of PFBR, submerged in liquid sodium by using the ultrasonic imaging technique during reactor shut-down when liquid sodium is at 180 ℃. The imaging is carried out prior to every Fuel handling operation. Electronics Division, BARC has designed and developed an 8-Channel Ultrasonic Imaging System (UIS) which consists of 4 downward viewing and 4 side viewing ultrasonic transducers alongwith pulser-receiver, signal processing electronics hardware and software. An automated mechanical scanner developed by IGCAR houses sodium immersible transducers to image the fuel sub assemblies. The system has been successfully tested with dummy protruding and grown FSAs, submerged under liquid sodium. Such ultrasonic imaging systems are not available to India from international market. The USUSS developed indigenously has all the features available in similar systems developed by other countries. After every imaging campaign, the mechanical scanner containing ultrasonic transducers is stored in the Argon filled storage-pit. Before every campaign of USUSS, it is necessary to check the healthiness of the sodium immersible and contaminated ultrasonic transducers, as the under-sodium scanner is decontaminated once in five years. For this purpose, a novel Non Contact Ultrasonic Inspection System (NCUIS) has been designed and developed by Electronics Division, BARC to check the functionality of the high-temperature and contaminated transducers of USUSS, using air-coupled ultrasonic technique. (author)

CFPL installs products pipeline with directional drilling

International Nuclear Information System (INIS)

Anon.

1996-01-01

Central Florida Pipeline Company (CFPL), a subsidiary of GATX Terminals Corp., Tampa, FL, has used directional drilling under seven water bodies in Hillsborough, Polk and Osceola Counties in constructing its new pipeline from Tampa to Orlando. Primary reason for using directional drilling is to protect the environment by minimizing water turbidity while the 16-inch diameter, 109-mile refined petroleum products pipeline is being installed. Total cost of the project is pegged at $68.5 million. Directional drilling enabled the pipe to be placed about 20 feet below the bottom of: The Alafia River in Riverview with 999 feet drilled; Port Sutton Channel near the Port of Tampa with 2,756 feet drilled; Reedy Creek Swamp at the intersection of Interstate 4 and Highway 192 which had 1,111 feet drilled; Wetland number-sign 70 southwest of Lake Wales with 1,575 feet drilled; Peace River south of Bartow had 2,470 feet drilled; Bonnet Creek west of Kissimmee had 693 feet drilled. Shingle Creek near the borders of Osceola and Orange Counties with 1,700 feet drilled. This paper reviews the design plans for construction and the emergency response plans should a rupture occur in the line