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Sample records for techniques caracterizacao da

  1. Microstructural characterization of porous materials by X-ray microtomography and gamma ray transmission techniques; Caracterizacao da microestrutura de materiais porosos por microtomografia de raios X e transmissao de raios gama

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    Moreira, Anderson Camargo

    2006-07-01

    This work presents the application of the X-ray microtomography and gamma ray transmission techniques for the microstructure characterization of different kinds of materials. Total porosity, pore size distribution and the two point correlation functions were measured. The two point correlation function, which allows the reconstruction of 3D models, was carried out for two samples. Seven ceramic tablets of Alumina (Al{sub 2}O{sub 3}), seven tablets of Boron Carbide (B{sub 4}C), three samples of sedimentary rocks and one sample of Titanium foam were analyzed. The experimental set up for the Gamma Ray Transmission technique consisted of: a 2'' x 2'' crystal NaI(Tl) detector, an {sup 241} Am radioactive source (59,53 keV, 100 mCi), an automatic micrometric table for the sample XZ movement and standard gamma spectrometry electronics. Two microtomography systems were used: a Fein Focus system, constituted by an X-ray tube, operated at 160 kV and 0.3 to 1.1 mA, a CCD camera and the movement sample system, and a Skyscan system, model 1072, with a X-ray tube operated at 100 kV and 100{mu}A, and a CCD camera. The ceramic tablets, analyzed by the gamma ray transmission technique presented results for most of the porosities data with smaller confidence intervals and inside the intervals supplied by the tablets manufacturer. The Titanium porous sample was analyzed by the two techniques, its microtomography images achieved a resolution of 17{mu}m, obtained employing the Fein Focus system. For both techniques, this sample showed high porosity, which allows its application for this purpose. The sandstones samples were analyzed by the Skyscan system, achieving resolutions of 19{mu}m, 11{mu}m and 3.8{mu}m for each sample, respectively. The resolutions of 11{mu}m and 3.8{mu}m were the ones that generated better 2D sections for the respective samples and, consequently, more reliable porosities. The 3.8{mu}m resolution was the one that best quantified the pore size

  2. Characterization of a clay from Vitoria da Conquista, Bahia, Brazil, by thermal analysis; Caracterizacao de uma argila de Vitoria da Conquista, BA, por analise termica

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    Oliveira, O.M.; Zandonadi, A.R.; Martins, M.V. Surmani; Carrio, J.A.G.; Munhoz Junior, A.H. [Universidade Presbiteriana Mackenzie, Sao Paulo, SP (Brazil)

    2010-07-01

    Kaolinitic clays are vastly used in ceramic industry. Light coloration burned clays are very useful in the coatings production because of their aesthetic. In this work clay material from Vitoria da Conquista (south-west Bahia, Brazil) was characterized by various techniques. Differential Scanning Calorimetry (DSC) shows a kaolinite characteristic curve with an endothermic peak at 492 deg C, which corresponds to the kaolinite - metakaolinite transformation. Transformation alpha to beta quartz is characterized by a 573 deg C peak. The samples were also characterized by water absorption and x rays powder diffraction. The 1100 deg C burned samples were tested by rupture tension with acceptable results. (author)

  3. Characterization of electric arc furnace dust aiming reuse; Caracterizacao da poeira de aciaria eletrica visando o seu reaproveitamento

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    Grillo, F.F.; Oliveira, E.B.G.; Oliveira, J.R. de, E-mail: fgrillo@ifes.edu.b [Instituto Federal de Ciencia e Tecnologia do Espirito Santo (IFES), Vitoria, ES (Brazil); Telles, V.B.; Tenorio, J.A.S. [Universidade de Sao Paulo (USP), SP (Brazil)

    2010-07-01

    This work aims to study the characterize of steelmaking dust, from the primary refining of steel in Electric Arc Furnace, in order to verify feasibility of reuse through the addition of hot metal in the form of briquette. The techniques used to characterize the dust was chemical analyses, size separation tests, X-ray diffraction analyses (XRD), Scanning Electron Microscopy (SEM). After characterization, was the calculation of reductant considering the complete reduction of iron oxides and then to briquetting. The waste sample is composed essentially of spherical particles and has a very small particle size (85% below 10 {mu}m). The XRD has presented compounds such as ZnFe{sub 2}O{sub 4}, Fe{sub 3}O{sub 4}, ZnO e SiO{sub 2}. This work showed that its possible recovery approximately 92% of metal iron from dust generated during steelmaking.This (author)

  4. The importance of using diffraction of X ray in clays characterization; A importancia da utilizacao da difracao de raios X na caracterizacao de argilas

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    Piccoli, R.; Nascimento, G.C.; Vitoretti, P.P.; Wernck, A.S.W., E-mail: rosaura@sc.senai.b [SENAI, Criciuma, SC (Brazil). Centro de Tecnologia em Ceramica; Perdona, C.R. [Universidade Barriga Verde, Cocal do Sul, SC (Brazil). Curso de Engenharia Ceramica; Perucchi, P. [Universidade do Extremo Sul Catarinense, Criciuma, SC (Brazil). Curso de Ciencia e Engenharia de Materiais

    2009-07-01

    The objective of this work is to demonstrate how the identification of crystalline phases and deg of crystallinity by diffractometry technique of X-ray (XRD) combined with chemical analysis of a sample can help in the study and characterization of raw materials, mainly those used in ceramic compositions. This study also aims to address the inherent limitations of this technique in relation to types of crystalline phases present in the sample of interest for analysis. (author)

  5. Physicochemical characterization of ceramics from Sao Paulo II archaeological site; Caracterizacao fisico-quimica da ceramica do sitio arqueologico Sao Paulo II

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    Ribeiro, Rogerio Baria

    2013-08-01

    Archaeometry is a consolidated field with a wide application of nuclear analytical techniques for the characterization, protection, and restoration of archaeological pieces. This project aimed at studying the elementary chemical composition of 70 ceramic fragments samples from Sao Paulo II archaeological site, located along the Solimoes River channel, next to Coari city, in Brazilian Amazon. The characterization of samples was performed by neutron activation analysis (NAA). By the determination of 24 elements in the ceramic fragments ( Ce, Co, Cr, Cs, Eu, Fe, Hf, K, La, Lu, Na, Nd, Sb, Sm. Rb, Se, Ta, Tb, Th, U, Yb and Zn), it was possible to define groups of samples regarding the similarity/dissimilarity in elementary chemical composition. For such a task, the multivariate statistical methods employed were cluster analysis (C A), principal component analysis (PCA) and discriminant analysis (DA). Afterwards, seven ceramic fragments were selected based on the groups previously established, for the characterization of the site temporal horizon. Those ceramic fragments were analyzed by thermoluminescence (TL) and EPR for dating purposes. The firing temperatures were determined by electron paramagnetic resonance (EPR) technique, in order to infer about some aspects of the ceramic manufacture employed by the ancient peoples that lived in Sao Paulo 11. By the results obtained in this study, it was possible to identify the quantity of clay sources employed by the ceramists and the age of the ceramic pieces. Therefore, the results of this research may contribute to the study on the occupation dynamics in the pre-colonial Brazilian Amazon. (author)

  6. Isolation and characterization of delta toxin from the venom of Crotalus durissus terrificus; Isolamento e caracterizacao da delta toxina do veneno de Crotalus durissus terrificus

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    Campos, Lucelia de Almeida

    2006-07-01

    The Crotalus durissus terrificus venom has been so far described as being of low complexity, with four major components described: convulxin, gyroxin, crotoxin and crotamine. In recent studies, other components of this venom were characterized as, for example, an analgesic factor. In 1980, Vital Brazil predicted the existence of a toxin which could be involved in platelet aggregation, and named it delta toxin. However, this toxin has never been isolated or characterized. The aim of the present work was to purify and characterize this toxin. After FPLC size exclusion chromatography followed by reverse phase HPLC, an homogeneous fraction was obtained, with a molecular weight of 14,074.92 Da. When analyzed by SOS-PAGE, this toxin presented an anomalous behavior, with a molecular weight of 14 kDa, while in 2D gels, spots around 40 kDa and with an isoelectrical point between 4 and 5 were observed suggesting isoforms with glicosilation microheterogeneity. After trypsin digestion, the fragments were submitted to the swissprot databank showing high homology (43% coverage, 15 matching peptides) with trocarin, a prothrombin activator from Tropidechis carinatus. These data were further confirmed by aminoacid analysis. The toxin was tested for its ability to activate factor II and X using synthetic substrates. Our data indicate a direct activation of factor X. The same toxin also behaved as a potent direct platelet aggregation activator on washed platelets. Assays with specific inhibitors indicate that neither metalloproteinase, nor serinoproteinase or t lectin domains are involved in the aggregating activity, since EDTA, benzamidin and D-galactose did not inhibit the toxin. In the present work, we were able to identify, purify and characterize a new toxin from the brazilian rattlesnake. It behaved as predicted by Vital-Brazil and displayed direct factor X activating properties, also inducing platelet aggregation, even at low concentrations. Our data also indicate that it is

  7. Cloning, periplasmic expression, purification and structural characterization of human ribosomal protein L10; Clonagem, expressao, purificacao e caracterizacao estrutural da proteina ribossomal L10 humana recombinante

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    Pereira, Larissa Miranda

    2009-07-01

    The ribosomal protein L10 (RP L10) is a strong candidate to be included in the class of tumor suppressor proteins. This protein, also denominated as QM, is known to participate in the binding of ribosomal subunits 60S and 40S and the translation of mRNAs. It has a molecular weight that varies between 24 and 26 kDa and an isoelectric point of (pI) 10.5. The sequence of the protein QM is highly conserved in mammals, plants, invertebrates, insects and yeast which indicates its critical functions in a cell. As a tumor suppressor, RP L10 has been studied in strains of Wilm's tumor (WT-1) and tumor cells in the stomach, where was observed a decrease in the amount of its mRNA. More recently, the RP L10 was found in low amounts in the early stages of prostate adenoma and showed some mutation in ovarian cancer, what indicates its role as a suppressor protein in the development of these diseases. It has also been described that this protein interacts with c-Jun and c-Yes inhibiting growth factors and consequently, cell division. This work has an important role on the establishment of soluble expression of QM to give base information for further studies on expression that aim to evaluate the specific regions where it acts binding the 60S and 40S ribosomal subunits and translation, as well as its binding to proto-oncogenes. The cDNA for QM protein was amplified by PCR and cloned into periplasmic expression vector p3SN8. The QM protein was expressed in E. coli BL21 (DE3) in the region of cytoplasm and periplasm, the best condition was obtained from the expression of the recombinant plasmid QM p1813{sub Q}M at 25 degree C or 30 degree C, the soluble protein was obtained with small amounts of contaminants. The assays of secondary structure showed that the QM protein is predominantly alpha-helix, but when it loses the folding, this condition changes and the protein is replaced by {beta}- sheet feature. (author)

  8. Biochemical and pharmacological characterization of irradiated crotamine by gamma rays of {sup 60}Co; Caracterizacao bioquimica e farmacologica da crotamina irradiada por raios gama de {sup 60}Co

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    Oliveira, Karina Corleto

    2014-07-01

    The serum production in Brazil, the only effective treatment in cases of snakebites, uses horses that although large size, have reduced l lifespan compared with horses not immunized. Ionizing radiation has been shown as an excellent tool in reducing the toxicity of venoms and toxins isolated, and promote the achievement of better immunogens for serum production, and contributing to the welfare of serum-producing animals. It is known, however, that the effects of ionizing radiation on protein are characterized by various chemical modifications, such as fragmentation, cross-linking due to aggregation and oxidation products generated by water radiolysis. However, the action of gamma radiation on toxins is not yet fully understood structurally and pharmacologically, a fact that prevents the application of this methodology in the serum production process. So we proposed in this paper the characterization of crotamine, an important protein from the venom of Crotalus durissus terrificus species, irradiated with {sup 60}Co gamma rays. After isolating the toxin by chromatographic techniques and testing to prove the obtaining of pure crotamine, it was irradiated with gamma rays and subjected to structural analysis, Fluorescence and Circular Dichroism. Using high hydrostatic pressure tests were also conducted in order to verify that the conformational changes caused by radiation suffer modifications under high pressures. From the pharmacological point of view, muscle contraction tests were conducted with the objective of limiting the action of crotamine in smooth muscle as well as the change in the action of toxin caused structural changes to the front. Analysis of Circular Dichroism and Fluorescence showed changes in structural conformation of crotamine when subjected to gamma radiation and that such changes possibly occurring in the secondary and tertiary structure of the protein. The observed in pharmacological tests showed that the irradiated crotamine was less effective

  9. Morphologic characterization and quantitative analysis on in vitro bacteria by nuclear techniques of measurement; Caracterizacao morfologica e analise quantitativa de bacterias in vitro por tecnicas nucleares de medidas

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    Lopes, Joana D' Arc Ramos

    2001-10-01

    The great difficulty to identify microorganisms (bacteria) from infectious processes is related to the necessary time to obtain a reliable result, about 72 hours. The purpose of this work is to establish a faster method to characterize bacterial morphologies through the use of neutron radiography, which can take about 5 hours. The samples containing the microorganisms, bacteria with different morphologies, after the appropriate microbiologic procedures were incubated with B{sup 10} for 30 minutes and soon after deposited in a plate of a solid detector of nuclear tracks (SSNTD), denominated CR-39. To obtain the images relative to bacteria, the detector was submitted to the flow of thermal neutrons of the order of 2.2 x 10{sup 5} n/cm{sup 2}.s from the J-9 channel of the Reactor Argonauta (IEN/CNEN). To observe the images from bacteria in each sample under an optical microscope, the sheets were chemically developed. The analysis of the images revealed morphologic differences among the genera (Gram positive from Gram-negative and coccus from bacillus), in samples containing either isolated or mixed bacteria. We thus verified the viability of the technique to achieve morphological characterization of different microorganisms. A quantitative approach seemed also to be feasible with the technique. The whole process took about 2 hours. (author)

  10. Characterization, analysis and dating of archaeological ceramics from the Amazon basin through nuclear techniques; Caracterizacao, analise e datacao de ceramicas arqueologicas da Bacia Amazonica atraves de tecnicas nucleares

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    Latini, Rose Mary

    1998-07-01

    The aim of this work is to contribute to the research in the reconstruction of part of the pre-history of the Amazon Basin by means of an analytical methods combined with multivariate analysis, given a analytic basis that can be continued by the archaeological work, through the identification, classification, provenance and dating the ceramics found in different archaeological sites of the Hydro graphic Basin of the Purus river. Neutron activation analysis in conjunction multivariate statistical methods were used for the identification and classification and thermoluminescence was used for the dating. Chemical composition results were in better agreement with archaeological classification for the archaeologically define Iquiri, Quinan and Xapuri phases and less characteristics the Iaco and Jacuru archaeological phase were not well characterized. An homogeneous group was established by most of the samples collected from the Los Angeles Archaeological Site (LA) and was distinct from all the other groups analysed. The provenance studies made with ceramics collected at this site shows that they were made with clay from nearby river (Rio Ina). From the LA ceramics dating the average date of site occupation was 1660 years. The ceramic dating results from the external wall of a circular earth wall construction confirm the relation with the local pre-history. Beyond the Acre material two urns were dated from the Archaeological Site Morro Grande and Sao Jose at Araruama, Rio de Janeiro. (author)

  11. Characterization of the oligosaccharide structure of human glycosylated prolactin (G-hPRL) native and recombinant; Caracterizacao da estrutura oligossacaridica de prolactina glicosilada humana (G-hPRL) nativa e recombinante

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    Marcos Vinicius Nucci Capone

    2013-07-01

    Human prolactin (hPRL) is a polypeptide hormone secreted by the anterior pituitary under the regulation of the hypothalamus, involved in a variety of biological processes such as mammary gland development and lactation. The recombinant product is important in medical diagnosis and treatment of failure of lactation. This hormone may occur in the form of non-glycosylated protein (NGhPRL) and glycosylated (G-hPRL) with molecular weights of approximately 23 and 25 kilodalton (kDa), respectively; has a single N-glycosylation site located at asparagine (Asn) position 31, which is partially occupied, thus being a particularly interesting model of glycosylation. The biological activity of G-hPRL is lower compared to NG-hPRL (~4 times) and its physiological function is not well defined: the portion of carbohydrate appears to have an important role in the hormone biosynthesis, secretion, biological activity, and plasma survival of the hormone. The main objective of this study was to compare the structures of N-glycans present in glycosylated pituitary prolactin (G-hPRL-NHPP) with those present in the recombinant. To obtain the recombinant G-hPRL the production was performed in laboratory scale from Chinese hamster ovary cells (CHO), genetically modified and adapted to growth in suspension. Cycloheximide (CHX), whose main effect was to increase the ratio G-hPRL/NG-hPRL from 5% to 38% was added to the culture medium, thereby facilitating the purification of G-hPRL. The G-hPRL was purified in two steps, a cation exchanger followed by a purification by reversed-phase high performance liquid chromatography (RP-HPLC) which demonstrated the efficient separation of the two isoforms of hPRL. Recombinant G-hPRL-IPEN was well characterized by several techniques confirming its purity and biological activity, including comparisons with other reference preparation of pituitary origin purchased from the {sup N}ational Hormone & Peptide Program (NHPPU. S.){sup .} The composition of N

  12. Characterization of Al{sub 2}O{sub 3}:C dosemeters for photon dosimetry using OSL technique; Caracterizacao de dosimetros de Al{sub 2}O{sub 3}:C para dosimetria de fotons utilizando a tecnica OSL

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    Villani, D.; Almeida, S.B.; Campos, L.L., E-mail: dvillani@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2016-07-01

    The optically stimulated dosimetry (OSL) has gained prominence in clinical and academic applications in Brazil. In this paper, we present results of the characterization OSL dosimeters Al{sub 2}O{sub 3}:C (TLD-500) manufactured by Rexon™ Components and TLD Systems in a RISØ reader, model TL/OSL-DA-20 for dosimetry of high-energy photon beams. All reader parameters, and its variations were evaluated. (author)

  13. Impregnation of 12-tungstophosphoric acid on silica - part I: determination of impregnation parameters, characterization and evaluation of catalytic activity; Impregnacao do acido 12-fosfotungstico em silica - parte I: determinacao de parametros de impregnacao, caracterizacao e avaliacao da atividade catalitica

    Energy Technology Data Exchange (ETDEWEB)

    Scroccaro, Karine Isabel; Tanobe, Valcineide Oliveira de Andrade; Cocco, Lilian Cristina; Yamamoto, Carlos Itsuo, E-mail: karineisabel@yahoo.com.br [Universidade Federal do Parana, Curitiba, PR (Brazil). Centro Politecnico. Dept. de Engenharia Quimica; Wypych, Fernando [Universidade Federal do Parana, Curitiba, PR (Brazil). Centro Politecnico. Dept. de Quimica

    2012-07-01

    Catalyst based on Kegging-type heteropolyacids (H{sub 3}PW{sub 12}O{sub 40} - HPA), supported on SiO{sub 2} (H{sub 3}PW), were prepared by the impregnation method under different thermal treatment conditions. The materials were characterized by different instrumental techniques and used as catalysts in the methyl esterification reactions of stearic acid. Using the catalyst with 15% of HPA, conversions higher than 60% were obtained after 2 h of reaction at 65 deg C. Recovery studies using hot-filtration with ethanol at 75 deg C showed satisfactory activity for two additional reaction cycles. (author)

  14. Characterization of dispersion of a nano composites PP/TiO{sub 2} non modified; Caracterizacao da dispersao dos nanocompositos de PP/TiO{sub 2} nao modificados

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    Soares, Igor L.; Tavares, Maria I.B.; Silva, Vanessa A. da; Legramanti, Cintia, E-mail: igorl@ima.ufrj.br [Universidade Federal do Rio de Janeiro - UFRJ, Instituto de Macromoleculas - IMA (Brazil); Luetkmeyer, Leandro [Universidades Federais do Mato Grosso - UFMT, Escritorio de Inovacao Tecnologica - EIT (Brazil)

    2011-07-01

    Polymeric nano composites are composite materials where an inorganic particle, which has a dimension in the nanometer range, is dispersed in a polymer matrix. Nano composites, using polypropylene (PP) as matrix polymer and titanium dioxide (TiO{sub 2}) as filler, have great versatility in marketing applications, this factor is inherent in the PP and the inherent ability photo degraded TiO{sub 2} particles. This combination can lead to a widely used material and a degradation time after discharge reduced, there by becoming, a residue of low environmental impact. This study aimed to evaluate the dispersion and particle distribution of TiO{sub 2}, non modified, in PP matrix, using the process of preparation by melt extrusion pathway and characterization of the materials obtained: on the molecular dynamics, using low field NMR solid state, measures the relaxation time spin-network (T{sub 1}H); morphology using XRD technique, and thermal analysis technique with the TGA of pure PP and nano composites PP/TiO{sub 2}. (author)

  15. Characterization of solid wastes from kraft pulp industry for ceramic materials development purposes; Caracterizacao de residuos solidos da industria de celulose tipo kraft visando sua aplicacao no desenvolvimento de materiais ceramicos

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    Rodrigues, L.R.; Francisco, M.A.C.O.; Sagrillo, V.P.D.; Louzada, D.M.; Entringer, J.M.S. [Instituto Federal do Espirito Santo (IFES), Vitoria, ES (Brazil)

    2016-07-01

    The Kraft pulp industry generates a large amount of solid wastes. Due this large quantity, the target of this study is characterize inorganic solid wastes, dregs, grits and lime mud, from the step of reagents recovery of Kraft process, aiming evaluate the potentiality of their use as alternative raw material on development of ceramic materials. Initially, the wastes were dried and ground, then they were subjected to the following characterization techniques: pH analysis, particle size analysis, X ray fluorescence, X ray diffraction, differential thermal analysis and thermogravimetric analysis and scanning electron microscopy. According to the results, it may be concluded that these wastes could be used as raw material in production of red ceramic and luting materials. (author)

  16. Characterization of an ecological binder for mortars obtained from recycling of ladle furnace slag; Caracterizacao de aglomerante ecologico para argamassas obtido a partir da reciclagem de escoria de forno panela

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    Marinho, A.B.; Santos, C.M.; Fontes, W.C.; Matias, A.C.P.; Brigolini, G.J.; Peixoto, R.A.F. [Universidade Federal de Ouro Preto (UFOP), MG (Brazil). Departamento de Engenhaira Civil; Carvalho, J.F., E-mail: josemaria.carvalho@ufv.br [Universidade Federal de Vicosa (UFV), MG (Brazil). Departamento de Engenharia Civil

    2016-07-01

    A sustainable binder obtained from recycling of a ladle furnace slag from Piracicaba, Sao Paulo, was produced in Laboratory of Construction Materials of Federal University of Ouro Preto (UFOP). A characterization work was performed and the results are presented. The physical, chemical and mineralogical properties was obtained using, among others, the following techniques: X-ray fluorescence (XRF), X-ray diffraction (XRD) with Rietveld refining method, optical microscopy and Scanning electronic microscopy (SEM) with energy dispersive spectroscopy (EDS). The chemical analysis showed predominance of CaO and SiO{sub 3}; the mineralogical analysis pointed the predominant presence of calcium-olivine, merwinite and pyroxene and; the images showed predominance of angulous and elongated grains. According to results, the material was classified as a hydraulic binder, with characteristics comparable to hydraulic limes. (author)

  17. Evaluating factorial kriging for seismic attributes filtering: a geostatistical filter applied to reservoir characterization; Avaliacao da krigagem fatorial na filtragem de atributos sismicos: um filtro geoestatistico aplicado a caracterizacao de reservatorios

    Energy Technology Data Exchange (ETDEWEB)

    Mundim, Evaldo Cesario

    1999-02-01

    In this dissertation the Factorial Kriging analysis for the filtering of seismic attributes applied to reservoir characterization is considered. Factorial Kriging works in the spatial, domain in a similar way to the Spectral Analysis in the frequency domain. The incorporation of filtered attributes via External Drift Kriging and Collocated Cokriging in the estimate of reservoir characterization is discussed. Its relevance for the reservoir porous volume calculation is also evaluated based on comparative analysis of the volume risk curves derived from stochastic conditional simulations with collocated variable and stochastic conditional simulations with collocated variable and stochastic conditional simulations with external drift. results prove Factorial Kriging as an efficient technique for the filtering of seismic attributes images, of which geologic features are enhanced. The attribute filtering improves the correlation between the attributes and the well data and the estimates of the reservoir properties. The differences between the estimates obtained by External Drift Kriging and Collocated Cokriging are also reduced. (author)

  18. Chemometrics application in fuel's MTR type chemical characterization by X-ray fluorescence; Aplicacao da quimiometria para caracterizacao quimica de combustiveis tipo MTR por fluorescencia de raios-X

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    Silva, Clayton Pereira da

    2012-07-01

    In Brazil and worldwide the nuclear power has occupied a prominent position with many applications in industry, power generation, environment and medicine, improving the quality of tests and treatments, therefore people's lives. Uranium is the main element used in nuclear facilities and it s employed as base material to generation of electricity in the manufacture of radiopharmaceuticals. In the '50s, during the Cold War, the then newly created International Atomic Energy Agency proposed to oversee nuclear facilities and encourage the manufacture of nuclear fuels with low-enriched uranium (LEU) fuel came then type Material Test Reactor (MTR), manufactured initially in U{sub 3}O{sub 8} and U{sub 3}Si{sub 2} later, both dispersed in aluminum. The use of this technology requires a constant improvement of all processes involving the manufacture of MTR subject to several international protocols, which seek to ensure the reliability of the fuel from the standpoint of practical and environmental. In this context, the control of impurities, from the point of view of neutron economy, directly affects the quality of any nuclear fuel, so strict control is necessary. The literature has reported procedures which, beyond generating residues, are lengthy and costly, they need calibration curve and consequently reference materials. The aim of this work is to establish and validate a methodology for nondestructive quantitative chemical analysis, low cost and analysis time, as well as minimize the generation of waste, for multielement determination of major constituents (Utotal and Si) and impurities (B, Mg, Al, Cr, Mn, Fe, Co, Ni, Cu, Zn, Mo, Cd and others) present in U3O8 and U{sub 3}Si{sub 2}, meeting the needs of nuclear reactors in the nuclear fuel qualification type MTR. For that purposes, will be applied the X-ray fluorescence technique which allows fast chemical and nondestructive analysis, aside from sample preparation procedures that do not require previous chemical

  19. Chemometrics application in fuel's MTR type chemical characterization by X-ray fluorescence; Aplicacao da quimiometria para caracterizacao quimica de combustiveis tipo MTR por fluorescencia de raios-X

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Clayton Pereira da

    2012-07-01

    In Brazil and worldwide the nuclear power has occupied a prominent position with many applications in industry, power generation, environment and medicine, improving the quality of tests and treatments, therefore people's lives. Uranium is the main element used in nuclear facilities and it s employed as base material to generation of electricity in the manufacture of radiopharmaceuticals. In the '50s, during the Cold War, the then newly created International Atomic Energy Agency proposed to oversee nuclear facilities and encourage the manufacture of nuclear fuels with low-enriched uranium (LEU) fuel came then type Material Test Reactor (MTR), manufactured initially in U{sub 3}O{sub 8} and U{sub 3}Si{sub 2} later, both dispersed in aluminum. The use of this technology requires a constant improvement of all processes involving the manufacture of MTR subject to several international protocols, which seek to ensure the reliability of the fuel from the standpoint of practical and environmental. In this context, the control of impurities, from the point of view of neutron economy, directly affects the quality of any nuclear fuel, so strict control is necessary. The literature has reported procedures which, beyond generating residues, are lengthy and costly, they need calibration curve and consequently reference materials. The aim of this work is to establish and validate a methodology for nondestructive quantitative chemical analysis, low cost and analysis time, as well as minimize the generation of waste, for multielement determination of major constituents (Utotal and Si) and impurities (B, Mg, Al, Cr, Mn, Fe, Co, Ni, Cu, Zn, Mo, Cd and others) present in U3O8 and U{sub 3}Si{sub 2}, meeting the needs of nuclear reactors in the nuclear fuel qualification type MTR. For that purposes, will be applied the X-ray fluorescence technique which allows fast chemical and nondestructive analysis, aside from sample preparation procedures that do not require previous

  20. L-alanine detector characterization for dosimetry of small fields in SBRT with VMAT techniques; Caracterizacao do detector de L-alanina para dosimetria de campos pequenos em SBRT com a tecnica de VMAT

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    Mazaro, Sarah J.; Peres, Leonardo [Instituto Nacional de Cancer (INCA), Rio de Janeiro, RJ (Brazil); Baffa, Oswaldo, E-mail: sarahmazaro@yahoo.com.br [Universidade de Sao Paulo (USP), Ribeirao Preto, SP (Brazil). Faculdade de Filosofia, Ciencias e Letras. Departamento de Fisica

    2016-07-01

    New radiotherapy treatment techniques have some problems such as: the dosimetric and geometric of the beam and small fields. Determination of the prescribed dose on the target volume in small fields is hampered due to lack of lateral electronic equilibrium and steep dose gradient along the edges of fields. The choice of radiation better detector becomes important in the dosimetry of small fields. Alanine detector has been shown to be a good choice for measurements of high doses of radiation in small fields. This study aims to characterize the L-alanine detector through the dosimetric tests for SBRT in VMAT techniques. L-alanine response showed a strong linear correlation with the dose (R ² = 0.9865), with significant angles and dose rate dependencies (14%) and (15%) respectively, and minor with the small field size (maximum 4% deviation). (author)

  1. Characterization of gadolinia-doped ceria with manganese addition synthesized by the cation complexation technique; Caracterizacao de ceria-gadolinia e ceria-gadolinia-manganes sintetizados pelo metodo de complexacao de cations

    Energy Technology Data Exchange (ETDEWEB)

    Yang, J.D.; Muccillo, R.; Muccillo, E.N.S., E-mail: enavarro@usp.b [Instituto de Pesquisas Energeticas e Nucleares (CCTM/IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro de Ciencia e Tecnologia de Materiais; Rocha, R.A. [Universidade Federal do ABC (CEMCSA/UFABC), Santo Andre, SP (Brazil). Centro de Engenharia, Modelagem e Ciencias Sociais Aplicadas

    2010-07-01

    Ceria-based compounds may be used for several technological applications like catalysts, grinding media and materials for electrolyte and electrodes in solid oxide fuel cells. For most of these applications fine powders are required. In this work, nanostructured ceria powders containing 20 mol % gadolinia with and without manganese addition were synthesized by the cation complexation technique. The prepared powders were calcined at 600 deg C for thermal decomposition of the metal citrate precursors. Results of X-ray diffraction, scanning electron microscopy and specific surface area evidenced the role of manganese on physical characteristics of the nanostructured materials. The cation complexation technique revealed to be a promising method for obtaining nanostructured powders with high yield and suitable physical properties for several technological applications. (author)

  2. Operative technique and early experience for robotic-assisted laparoscopic nephroureterectomy (RALNU) using da Vinci Xi.

    Science.gov (United States)

    Darwiche, Fadi; Swain, Sanjaya; Kallingal, George; Punnen, Sanoj; Manoharan, Murugesan; Parekh, Dipen J; Gonzalgo, Mark L

    2015-01-01

    Robotic-assisted laparoscopic nephroureterectomy (RALNU) has been previously utilized for management of upper tract urothelial carcinoma. The da Vinci Xi surgical system was released in April of 2014. We describe our operative technique and early experience for RALNU using the da Vinci Xi system highlighting unique features of this surgical platform. A total of 10 patients with a diagnosis of upper tract urothelial carcinoma underwent RALNU using the da Vinci Xi system between April and November of 2014. A novel, oblique "in line" robotic trocar configuration was utilized to access the upper abdomen (nephrectomy portion) and pelvis (bladder cuff excision) without undocking. The port hopping feature of da Vinci Xi was utilized to facilitate optimal, multi-quadrant visualization during RALNU. Robotic-assisted laparoscopic nephroureterectomy was successfully completed without open conversion in all 10 patients. Mean operative time was 184 min (range 140-300 min), mean estimated blood loss was 121 cc (range 60-300 cc), and mean hospital stay was 2.4 days. Final pathology demonstrated high grade urothelial carcinoma in all patients. Surgical margins were negative in all patients. No intra-operative complications were encountered. One patient developed a pulmonary embolus after being discharged. No patients required a blood transfusion. Mean patient follow-up was 130 days (range 15-210 days). The use of da Vinci Xi with a novel, oblique "in line" port configuration and camera port hopping technique allows for an efficient and reproducible method for RALNU without the need for repositioning the patient or the robot during surgery.

  3. Comparing the da Vinci si single console and dual console in teaching novice surgeons suturing techniques.

    Science.gov (United States)

    Crusco, Salvatore; Jackson, Tiffany; Advincula, Arnold

    2014-01-01

    Robot-assisted laparoscopic surgery is often taught with the surgical mentor at the surgeon console and the trainee at the patient's bedside. The da Vinci dual console (Intuitive Surgical, Sunnyvale, California) allows a surgical mentor to teach with both the mentor and the trainee working at a surgeon console simultaneously. The purpose of this study is to evaluate the effectiveness of the dual console versus the single console for teaching medical students robotic tasks. Forty novice medical students were randomized to either the da Vinci single-console or dual-console group and were taught 4 knot-tying techniques by a surgical mentor. The students were timed while performing the tasks. No statistically significant differences in mean task times were observed between the single- and dual-console groups: interrupted stitch with a 2-handed knot (300 seconds for single vs 294 seconds for dual, P=.59), interrupted stitch with a 1-handed knot (198 seconds for single vs 212 seconds for dual, P=.88), figure-of-8 stitch with a 2-handed knot (261 seconds for single vs 219 seconds for dual, P=.20), and figure-of-8 stitch with a 1-handed knot (200 seconds for single vs 199 seconds for dual, P=.53). No significant difference was observed in performance time when teaching knot-tying techniques to medical students using the da Vinci dual console compared with the single console. More research needs to be performed on the utility of the da Vinci dual console in surgical training.

  4. The radiological safety in the use of nuclear technique -activities developed by Centro de Desenvolvimento da Tecnologia Nuclear - CNEN

    International Nuclear Information System (INIS)

    Wakabayashi, T.; Pereira, E.G.; Hirayama, T.

    1991-01-01

    The activities developed by the Centro de Desenvolvimento da Tecnologia Nuclear - CDTN supporting the users of nuclear techniques are described. The methodology used and future plans for the group are shown. (E.G.)

  5. Total robotic radical rectal resection with da Vinci Xi system: single docking, single phase technique.

    Science.gov (United States)

    Tamhankar, Anup Sunil; Jatal, Sudhir; Saklani, Avanish

    2016-12-01

    This study aims to assess the advantages of Da Vinci Xi system in rectal cancer surgery. It also assesses the initial oncological outcomes after rectal resection with this system from a tertiary cancer center in India. Robotic rectal surgery has distinct advantages over laparoscopy. Total robotic resection is increasing following the evolution of hybrid technology. The latest Da Vinci Xi system (Intuitive Surgical, Sunnyvale, USA) is enabled with newer features to make total robotic resection possible with single docking and single phase. Thirty-six patients underwent total robotic resection in a single phase and single docking. We used newer port positions in a straight line. Median distance from the anal verge was 4.5 cm. Median robotic docking time and robotic procedure time were 9 and 280 min, respectively. Median blood loss was 100 mL. One patient needed conversion to an open approach due to advanced disease. Circumferential resection margin and longitudinal resection margins were uninvolved in all other patients. Median lymph node yield was 10. Median post-operative stay was 7 days. There were no intra-operative adverse events. The latest Da Vinci Xi system has made total robotic rectal surgery feasible in single docking and single phase. With the new system, four arm total robotic rectal surgery may replace the hybrid technique of laparoscopic and robotic surgery for rectal malignancies. The learning curve for the new system appears to be shorter than anticipated. Early perioperative and oncological outcomes of total robotic rectal surgery with the new system are promising. Copyright © 2016 John Wiley & Sons, Ltd. Copyright © 2016 John Wiley & Sons, Ltd.

  6. Analogue to Digital and Digital to Analogue (AD/DA) Conversion Techniques: An Overview

    CERN Multimedia

    CERN. Geneva

    2002-01-01

    The basic ideas behind modern Analogue to Digital and Digital to Analogue (AD/DA) conversion methods will be introduced: a general view of the importance of these devices will be given, along with the digital representation of time-varying, real-world analogue signals. Some CERN applications will be outlined. The variety of conversion methods, their limitations, error sources and measurement methods will form the major part of this presentation. A review of the technological progress in this field over the last 30 years will be presented, concluding with the present 'state of the art' and a quick look at what is just around the corner. This Technical Training Seminar is in the framework of the FEED-2002 Lecture Series, and it is a prerequisite to attending to any of the FEED-2002 Terms. FEED-2002 is a two-term course that will review the techniques dealing with closed loop systems, focussing on time-invariant linear systems. (free attendance, no registration required) More information on the FEED-2002 ...

  7. Técnica para o estudo da anatomia da epiderme foliar de batata A technique for the anatomical study of potato leaf epidermis

    Directory of Open Access Journals (Sweden)

    Fernanda Bastos Segatto

    2004-10-01

    Full Text Available Embora a batata (Solanum tuberosum seja uma espécie de grande valor econômico, são poucas as informações disponíveis sobre a anatomia foliar, principalmente de características estruturais da epiderme. O estudo da anatomia foliar assume grande importância básica, para a ecologia e fisiologia, e aplicada para a fitopatologia e o melhoramento genético. Este trabalho teve por objetivo identificar uma técnica histológica que permite a confecção de lâminas semipermanentes para avaliar a epiderme foliar, em vista frontal, de um grande número de plantas de batata em um curto período de tempo. O corte paradérmico a mão livre, o método de Jeffrey e as técnicas de hidróxido de potássio e de impressão da epiderme foram avaliados. Lâminas semipermanentes foram confeccionadas da secção frontal da epiderme de folíolos principais do terço médio de plantas de batata. A impressão da epiderme em lâmina foi a única técnica que possibilitou a avaliação adequada de todos os clones de batata utilizados. A impressão da epiderme é uma técnica muito rápida, de baixo custo e de fácil execução, que atende os requisitos necessários para a identificação e seleção de características anatômicas de um grande número de plantas em um programa de melhoramento genético de batata.Even though potato (Solanum tuberosum is an economically important crop, information about leaf characteristics of anatomical structure has not been well studied. Studies of leaf epidermis have significance for basic fields as ecology and physiology and for applied fields as plant pathology and breeding. The objective of this research was to identify a fast and easy technique to prepare semi-permanent slides for studying the anatomy of potato leaf epidermis. Para dermal free hand cut, Jeffrey method, potassium hydroxide and epidermal fingerprint on glass slide techniques were evaluated. Semi-permanent slides were prepared from the longitudinal section of

  8. Da Lat Nuclear Research Reactor. Role and perspective in the development of radioisotope and nuclear technique application in Vietnam

    International Nuclear Information System (INIS)

    Tran Ha Anh; Tran Khac An; Ngo Phu Khang; Nguyen Mong Sinh

    1995-01-01

    The Da Lat Nuclear Research Reactor is playing a central role in the development of both the Nuclear Research Institute and nuclear application in our country. Thanks to this main scientific tool, the Nuclear Research Institute nearly 10 years after the completion of its renovation from the previous American-made TRIGA MARK 2 reactor is being able to implement numerous scientific and technological research projects and to develop significant applications of radioisotopes and various nuclear techniques. A general overview of the research and development activities of the Institute based on the Da Lat Nuclear Research Reactor is given as well as those aiming at ensuring its safe, reliable and efficient operation and at enlarging the perspectives of its utilisation in the future. (authors). 5 refs., 1 fig., 1 tab

  9. Characterization and obtainment of thin films based on N,N,N-trimethyl chitosan and heparin through the technical layer-by-layer; Caracterizacao e obtencao de filmes finos de N,N,N-trimetil quitosana e heparina atraves da tecnica layer-by-layer

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2011-07-01

    Thin films of Heparin (HP) and N,N,N-trimethyl chitosan (TMC) with a high degree of quaternization (DQ) were obtained at pH 7.4 through the layer-by-layer (LbL) technique. Polystyrene (PS) was oxidized with aqueous solution of sodium persulfate and subsequently employed as substrate. The characterization of TMC and the respective determination of DQ were performed through {sup 1}H NMR spectroscopy. The thin films de TMC/HP were characterized by FTIR-ATR and AFM. Both techniques confirmed the adsorption of TMC and HP in surface of the PS. The increasing of the bilayers provides a decrease of the projections and/or roughness, further of minimizing the depressions at the surface of the films. Studies of thin films the base of TMC/HP prepared from the LbL technique has not been reported in the literature. It is expected that the thin films of TMC/HP present anti-adhesive and antimicrobial properties. (author)

  10. Aplication of the stereolithography technique in complex spine surgery Aplicação da técnica de estereolitografia em cirurgias complexas da coluna

    Directory of Open Access Journals (Sweden)

    Wellingson Silva Paiva

    2007-06-01

    Full Text Available Many techniques have been proposed for surgical training as a learning process for young surgeons or for the simulation of complex procedures. Stereolithograpfy, a rapid prototyping technique, has been presented recently as an option for these purposes. We describe the case of a 12 years old boy, diagnosed with Ewing´s sarcoma in the cervical spine. After a surgical simulation accomplished in the prototype, built by stereolithography, the patient was submitted to a C4 corpectomy and to a C4 and C3 laminectomy with anterior and posterior fixation, a non intercurrence procedure. This technique is an innovative and complementary tool in diagnosis and therapy. As a result, it is easier for the surgeon to understand the complexity of the case and plan the approach before any surgical procedure.Lesões tumorais da coluna podem representar um grande desafio para equipe cirúrgica. A estereolitografia é uma técnica de construção de peças anatômicas a partir de desenhos gráficos ou exames radiológicos. Apresentamos um paciente de 12 anos, com quadro de cervicobraquialgia à direita com diagnóstico de sarcoma de Ewing. Ao exame neurológico, o paciente apresentava-se com paresia em MSD grau IV e leve hipoestesia em dermátomos de C6 à T1 à direita. RM evidenciou edema intra e extra-ósseo com compressão medular e instabilidade cervical. Realizada simulação cirúrgica no protótipo construído por estereolitografia. Foi submetido a corpectomia de C4 e a laminectomia C4 e C3, com fixação anterior e posterior, procedimento sem intercorrências. A estereolitografia é ferramenta inovadora no auxílio diagnóstico e terapêutico. Seu uso permite ao cirurgião entender fisicamente o sítio da lesão, estudar a via de acesso e perceber a real complexidade do caso antes do procedimento cirúrgico.

  11. Neutronic characterization of cylindrical core of minor excess reactivity in the nuclear reactor IPEN/MB-01 from the measure of spatial and energetic distribution of neutron flux distribution; Caracterizacao do nucleo cilindrico de menor excesso de reatividade do reator IPEN/MB-01, pela medida da distribuicao espacial e energetica do fluxo de neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Aredes, Vitor Ottoni Garcia

    2014-07-01

    In this work was conducted the mapping of the thermal and epithermal neutrons flux and the energy spectrum of the neutrons in the reactor core IPEN/MB-01 for a cylindrical core configuration with minor excess reactivity, which is 28 x 28 fuel rods arranged in north-south and east-west directions. The calibration of control rods for this configuration determined their excess reactivity. The lower excess reactivity in the core decreased neutron flux disturbance caused by the neutron absorbing rods , given that the nuclear reactor was operated with the rods almost completely removed . Was used the 'Activation Analysis Technique' with the thin foil activation detectors ( infinitely diluted and hyper-pure), of different materials that work in different energy ranges, to calculate the saturation activity, used for determining the neutron flux and in the SANDBP code as input for the calculation of the neutrons energy spectrum. To discriminate thermal and epithermal flux , was used the 'Cadmium RatioTechnique' . The activation detectors were distributed in a total of 140 radial and axial positions in the reactor core and 16 irradiation, with bare and covered with cadmium activation foils. A model of this configuration was simulated by MCNP-5 code to determine the cadmium correction factor and comparison of the results obtained experimentally. The cylindrical configuration desired, with 17% less fuel than the standard rectangular configuration (28 x 26 fuel rods), reached criticality with the control rods approximately 90% removed, which decreased considerably the disturbance in neutron flux. Given the highest power density of the 28 x 28 cylindrical core, the neutron flux increased by over 50% in the central regions of the core compared to the values of the 28 x 26 standard rectangular core. (author)

  12. Spatial distribution of metals in soil samples from Zona da Mata, Pernambuco, Brazil using XRF technique

    International Nuclear Information System (INIS)

    Fernandez, Zahily Herrero; Santos Junior, Jose Araujo dos; Amaral, Romilton dos Santos; Menezes, Romulo Simoes Cezar; Santos, Josineide Marques do Nascimento; Bezerra, Jairo Dias; Damascena, Kennedy Francys Rodrigues; Silva, Edvane Borges da; Silva, Alberto Antonio da

    2015-01-01

    Soil contamination is today one of the most important environmental issues for society. In the past, soil pollution was not considered as important as air and water contamination, because this was more difficult to be controlled, becoming an important topic in studies of environmental protection worldwide. Based on this, this paper provides information on the determination of metals in soil samples collected in Zona da Mata, Pernambuco, Brazil, where normally the application of pesticides, insecticides and other agricultural additives are used in a disorderly manner and without control. A total of 24 sampling points were monitored. The analysis of Mn, Fe, Ni, Zn, Br, Rb, Sr, Pb, Ti, La, Al, Si and P were performed using Energy Dispersive X-Ray Fluorescence. In order to assess the development of analytical method, inorganic Certified Reference Materials (IAEA-SOIL-7 and SRM 2709) were analyzed. In each sampling site, the geoaccumulation index were calculated to estimate the level of metal contamination in the soil, this was made taking into account the resolution 460 of the National Environmental Council (CONAMA in Portuguese). The elemental distribution patterns obtained for each metal were associated with different pollution sources. This assessment provides an initial description of pollution levels presented by metals in soils from several areas of Zona da Mata, providing quantitative evidence and demonstrating the need to improve the regulation of agricultural and industrial activities. (author)

  13. The Da Vinci Xi and robotic radical prostatectomy-an evolution in learning and technique.

    Science.gov (United States)

    Goonewardene, S S; Cahill, D

    2017-06-01

    The da Vinci Xi robot has been introduced as the successor to the Si platform. The promise of the Xi is to open the door to new surgical procedures. For robotic-assisted radical prostatectomy (RARP)/pelvic surgery, the potential is better vision and longer instruments. How has the Xi impacted on operative and pathological parameters as indicators of surgical performance? This is a comparison of an initial series of 42 RARPs with the Xi system in 2015 with a series using the Si system immediately before Xi uptake in the same calendar year, and an Si series by the same surgeon synchronously as the Xi series using operative time, blood loss, and positive margins as surrogates of surgical performance. Subjectively and objectively, there is a learning curve to Xi uptake in longer operative times but no impact on T2 positive margins which are the most reflective single measure of RARP outcomes. Subjectively, the vision of the Xi is inferior to the Si system, and the integrated diathermy system and automated setup are quirky. All require experience to overcome. There is a learning curve to progress from the Si to Xi da Vinci surgical platforms, but this does not negatively impact the outcome.

  14. Spatial distribution of metals in soil samples from Zona da Mata, Pernambuco, Brazil using XRF technique

    Energy Technology Data Exchange (ETDEWEB)

    Fernandez, Zahily Herrero; Santos Junior, Jose Araujo dos; Amaral, Romilton dos Santos; Menezes, Romulo Simoes Cezar; Santos, Josineide Marques do Nascimento; Bezerra, Jairo Dias; Damascena, Kennedy Francys Rodrigues, E-mail: zahily1985@gmail.com, E-mail: jaraujo@ufpe.br, E-mail: romilton@ufpe.br, E-mail: rmenezes@ufpe.br, E-mail: neideden@hotmail.com, E-mail: jairo.dias@ufpe.br, E-mail: kennedy.eng.ambiental@gmail.com [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Centro de Tecnologia e Geociencias. Departamento de Energia Nuclear; Alvarez, Juan Reinaldo Estevez, E-mail: jestevez@ceaden.cu [Centro de Aplicaciones Tecnologicas y Desarrollo Nuclear (CEADEN), Havana (Cuba); Silva, Edvane Borges da, E-mail: edvane.borges@pq.cnpq.br [Universidade Federal de Pernambuco (UFPE), Vitoria de Santo Antao, PE (Brazil). Nucleo de Biologia; Franca, Elvis Joacir de; Farias, Emerson Emiliano Gualberto de, E-mail: ejfranca@cnen.gov.br, E-mail: emersonemiliano@yahoo.com.br [Centro Regional de Ciencias Nucleares do Nordeste (CRCN-NE/CNEN-PE), Recife, PE (Brazil); Silva, Alberto Antonio da, E-mail: alberto.silva@barreiros.ifpe.edu.br [Instituto Federal de Educacao, Ciencia e Tecnologia de Pernambuco (IFPE), Barreiros, PE (Brazil)

    2015-07-01

    Soil contamination is today one of the most important environmental issues for society. In the past, soil pollution was not considered as important as air and water contamination, because this was more difficult to be controlled, becoming an important topic in studies of environmental protection worldwide. Based on this, this paper provides information on the determination of metals in soil samples collected in Zona da Mata, Pernambuco, Brazil, where normally the application of pesticides, insecticides and other agricultural additives are used in a disorderly manner and without control. A total of 24 sampling points were monitored. The analysis of Mn, Fe, Ni, Zn, Br, Rb, Sr, Pb, Ti, La, Al, Si and P were performed using Energy Dispersive X-Ray Fluorescence. In order to assess the development of analytical method, inorganic Certified Reference Materials (IAEA-SOIL-7 and SRM 2709) were analyzed. In each sampling site, the geoaccumulation index were calculated to estimate the level of metal contamination in the soil, this was made taking into account the resolution 460 of the National Environmental Council (CONAMA in Portuguese). The elemental distribution patterns obtained for each metal were associated with different pollution sources. This assessment provides an initial description of pollution levels presented by metals in soils from several areas of Zona da Mata, providing quantitative evidence and demonstrating the need to improve the regulation of agricultural and industrial activities. (author)

  15. Development and characterization of monolithic fuel miniplate alloy U-2.5Zr-7.5Nb, coated in zircaloy; Desenvolvimento e caracterizacao do combustivel nuclear tipo placa monolitico da liga U-2,5Zr-7,5Nb revestido em zircaloy

    Energy Technology Data Exchange (ETDEWEB)

    Machado, Geraldo Correa

    2014-06-01

    The autocthonal production of nuclear fuel in Brazil for test and research reactors is restricted to MTR (Material Test Reactor) fuel type dispersion plate, using U3Si2 alloy, coated and dispersed in aluminum, developed by IPEN-SP for use in IEA-R1 reactor. Moreover, the UO{sub 2} fuel rod type for power reactors is manufactured by Rezende (RJ) with a German technology by INB under license. Currently, Brazil is performing two programs of developing reactors. Currently, Brazil is developing two reactors. One of them is the development, by CNEN, the Brazilian Multipurpose Reactor (RMB), for testing, research and radioisotope production. The other one is the development a power reactor for naval propulsion, conducted by the Brazilian Navy. This dissertation presents the development and characterization of monolithic fuel miniplate alloy U-2.5Zr-7.5Nb, coated in zircaloy (ZRY), on a laboratory scale. Due to its innovative features and properties, this fuel can be used as fuel in both test reactors, research and producing radioisotopes for power reactors as small and medium sizes. Thus, this high potential fuel can be used in domestic reactors currently under development. The development of monolithic fuel plate type is made using the technique called 'picture-frame' where a sandwich composed of a monolith alloy U-2.5Zr- 7.5Nb coupled to a frame and coated sheets of Zry is obtained. The alloy U-2.5Zr-7.5Nb was obtained by melting in an induction furnace and then was cast into rectangular ingots of graphite, thus achieving an ingot with approximate dimensions of 170 x 50 x 60 mm. The obtained ingot was hot rolled at 850 ºC, with a 50 % reduction in thickness, in order to refine the raw structure of fusion. Samples cut from the alloy U-2.5Zr-7.5Nb, with dimensions 20 x 20 x 6 mm were placed in frames and plates Zry and joined by TIG (Tungsten Inert Gas) under an atmosphere of argon, obtaining a set of 10 mm thick, 45 mm wide and 100 mm long. The sandwiches were

  16. Repository for high level wastes in Brazil: the Leitz HS 1350 platinum employed for helping the geological characterization of the candidate areas; Repositorio de rejeito de alto nivel (RANR) no Brasil: o emprego da platina Leitz HS 1350 no auxilio para caracterizacao geologica de areas candidatas

    Energy Technology Data Exchange (ETDEWEB)

    Lima, Tatiana A. Fernandes de; Oliveira, Elizabeth Kerpe de; Rios, Francisco Javier [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil)]. E-mail: tafl@cdtn.br

    2007-07-01

    One of the preliminary stages for the choice of the appropriated local is the geological study. The granitic rocks are the best choice for construction of high level radioactive wastes repository. In the minerals associated to the rock there are small quantities of imprisoned fluids denominated fluid inclusions (FI), were heating coming from the waste radioactive decays can cause crackling of the wastes and migration of the fluids to the heat source. These studies require to be in routine a ultra heating platin (up to 1350 degree C) calibrated, coupled to the petrographic microscope (microthermometry). The tests performed viewed the calibration and placing into routine the platin, by using analytical standards such as fusion temperature covering the heating range (the substances potassium dichromate, barium nitrate, lithium fluorate copper and other two standards of Chaixmeca platin). The Leitz Heating Stage 1350 platin is presently installed and operating at Laboratory of Fluid Inclusions and Metallogenesis of the CDTN/Brazil, for using of this technique. (author)

  17. Synthesis and characterization of organically modified silica gel with 4-amino-5-(4-pyridyl)-4h-1 ,2,4-triazole-3-thiol (APTT); Sintese e caracterizacao da silica gel organofuncionalizada com 4-amino-5-(4-piridil)-4h-1,2,4-triazol-3-tiol (APTT)

    Energy Technology Data Exchange (ETDEWEB)

    Magossi, M.S.; Carmo, D.R. do, E-mail: maiaramagossi@gmail.com [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP), Ilha Solteira, SP (Brazil). Faculdade de Engenharia

    2014-07-01

    This work object the preparation and characterization of a silica gel (SG) organically with a triazole compound, 4-amino-5-(4-pyridyl)-4H-1,2,4-triazole-3- thiol (APTT). The prepared organofunctionalized material (SGAPTT) was preliminarily characterized by spectroscopic techniques such as: Spectroscopy in the Region of Infrared (FTIR), Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy X-ray (EDX). The vibrational spectrum (FTIR) showed characteristic bands of the starting materials, such as bands at ∼ 1120cm{sup -1} related to the asymmetric stretching Si-O-Si (νSi-O-Si) as well as the bands between 1350 and 1650 cm{sup -1} assigned vibrations and deformations of the ring APTT. The SGAPTT material was tested as support for adsorption of cupric ions in aqueous solution, ethanol and 42% ethanol. The maximum amount of copper (II) adsorbed (Nf {sup max.}) was 22.0 × 10{sup -5} mol g{sup -1}, 31.4 × 10-5 mol g-1 and 47.17 × 10{sup -5} mol g{sup -1} to aqueous media, 42% ethanol and 99% ethanol respectively. (author)

  18. Development and characterization of ceramic composites alumina-titania based reinforced with lanthanum oxide for fabrication of inert coatings for metallic tanks of the oil industry; Desenvolvimento e caracterizacao de compositos ceramicos baseados em alumina-titania reforcados com oxido de lantanio para fabricacao de revestimentos inertes em tanques metalicos da industria petrolifera

    Energy Technology Data Exchange (ETDEWEB)

    Bandeira, J.M.; Yadava, Y.P.; Silva, N.D.G.; Ferreira, R.A.S., E-mail: julianamb91@gmail.com, E-mail: yadava@ufpe.br [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Centro de Tecnologia e Geociencias. Departamento de Engenharia Mecanica

    2016-07-01

    Crude petroleum is highly corrosive causing superficial degradation in metallic tanks used for storage and transportation of this material, which causes a serious problem in the oil industry. An alternative to solve this problem is to use some kind of coating that is inert to this kind of corrosion. Alumina and titania are interesting materials for several engineering applications because, when compared with other ceramic materials, they present superior mechanical properties, e.g. high mechanical strength, good chemical stability and high fracture toughness combined with good wear resistance and a coefficient of thermal expansion close to the iron's, which makes them fit to use in ceramic hardening process and coating. In this paper, alumina-titania ceramic composites with 5%, 10%, 15% and 20% of titania (TiO2) and reinforced with 2% of lanthanum oxide of were produced by thermo-mechanical processing and sintering techniques at 1350 deg C. In these composites, microstructure and mechanical properties were analyzed using X-ray spectroscopy, optical microscopy, scanning electron microscopy and Vickers hardness in order to evaluate their applicability. X-ray spectroscopy showed the formation of composite without the presence of other phases. Optical microscopy and scanning electron microscopy showed a homogeneous microstructure in terms of particle size and distribution. Vickers hardness test showed a gradual decrease in hardness with the addition of titania. The composite with 5% of titania and 2% of lanthanum oxide is the best choice for structural applications. The composites were submerged in crude petroleum for 30 days to study their stability in such environment. Through the analysis of X-ray spectroscopy, optical microscopy and Vickers hardness before and after the submersion in crude petroleum, it was not observed structural or microstructural degradation nether alterations in mechanical properties. This way, it was concluded that these composites have

  19. Characterization of sediments laid on Solimoes/Amazonas river flood plains, using energy dispersive X-ray fluorescence technique; Caracterizacao dos sedimentos depositados nas planicies de inundacao do Rio Solimoes/Amazonas, utilizando a tecnica de fluorescencia de raios-X por dispersao de energia

    Energy Technology Data Exchange (ETDEWEB)

    Carneiro, Ana E.V. [Universidade Metodista de Piracicaba (UNIMEP), Sao Paulo, SP (Brazil); Nascimento Filho, Virgilio F. do [Sao Paulo Univ., Piracicaba, SP (Brazil). Escola Superior de Agricultura Luiz de Queiroz]|[Centro de Energia Nuclear na Agricultura (CENA), Piracicaba, SP (Brazil)

    1997-10-01

    This paper proposes sediment analysis with high light elements fraction using dispersive energy X-ray fluorescence technique with radioisotopic excitation, The proposed procedure is based on the Fundamental Parameters for analytical elements (Z {>=} 13) evaluation, and coherent and incoherent scattered radiation for quantification of the light fraction of the matrix (Z < 13). Laid sediments samples on Solimoes/Amazonas river flood plains were analyzed, determining simultaneously the Al, Si, K, Ca, Ti, Fe, Sc, V, Mn, Cu, Zn, Rb, Sr and Zr element concentrations, thus allowing chemical characterization and spatial variability, and some mineralogical and weathering sediments aspects. (author). 15 refs., 11 tabs.

  20. Hydrogeological characterization of Itataia mine, Ceara, Brazil; Caracterizacao hidrogeologica da jazida de Itataia, CE

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Jose Roberto de Alcantara e

    2003-07-01

    This work analyzes the geological-geotechnical-geophysical behavior, aiming to define the characteristics of a karstic-fissural aquifer in the mid-northern region of the State of Ceara, named as Itataia Phosphor-Uranium Deposit. This area is constituted of marbles and gneisses from Itataia Group, which are morphologically located at a higher point to the south and at a lower point to the north, related to Paleoproterozoic Era. Fracture system led to the implantation of two karstic marble phases, being the oldest from Cambrian Period and the most recent from Tertiary/Quaternary Period. Porosity is secondary to fractures, fissures and crushed zones which act as hydraulic channels for groundwater flow. Major geophysics defined conducting lines are controlled by normal fractures and faults in both N70 deg E and N80 deg W directions, and secondarily in both N10 deg E and N30 deg W directions, dipping 70 deg -85 deg into the northern quadrant of the main axes. Fault characteristics are typical of graben and horst patterns. Rocks in the area are distributed into three classes of geotechnical massif: healthy rock, moderately altered and fractured rock, and strongly altered and fractured rock. The latter occurs predominantly in the center of the area, from the soil surface to an average depth of 150 meters. Groundwater flow is characterized by fractures which enlarged by the karstic phenomenon dissolution, and then become closer as deeper they are. This flow may be slower or even discontinue in light of silty-argillaceous alteration material that fill the open fracture gaps. Water level is not lower than 5 m or higher than 90 m, averaging by 30 m ali over the area. The synoptic piezometry map shows a general south-north direction; however in the southwestern portion - the recharge zone - it takes the south direction, while in the southeastern portion it takes the southeast direction. (author)

  1. Olive oil sensory defects classification with data fusion of instrumental techniques and multivariate analysis (PLS-DA).

    Science.gov (United States)

    Borràs, Eva; Ferré, Joan; Boqué, Ricard; Mestres, Montserrat; Aceña, Laura; Calvo, Angels; Busto, Olga

    2016-07-15

    Three instrumental techniques, headspace-mass spectrometry (HS-MS), mid-infrared spectroscopy (MIR) and UV-visible spectrophotometry (UV-vis), have been combined to classify virgin olive oil samples based on the presence or absence of sensory defects. The reference sensory values were provided by an official taste panel. Different data fusion strategies were studied to improve the discrimination capability compared to using each instrumental technique individually. A general model was applied to discriminate high-quality non-defective olive oils (extra-virgin) and the lowest-quality olive oils considered non-edible (lampante). A specific identification of key off-flavours, such as musty, winey, fusty and rancid, was also studied. The data fusion of the three techniques improved the classification results in most of the cases. Low-level data fusion was the best strategy to discriminate musty, winey and fusty defects, using HS-MS, MIR and UV-vis, and the rancid defect using only HS-MS and MIR. The mid-level data fusion approach using partial least squares-discriminant analysis (PLS-DA) scores was found to be the best strategy for defective vs non-defective and edible vs non-edible oil discrimination. However, the data fusion did not sufficiently improve the results obtained by a single technique (HS-MS) to classify non-defective classes. These results indicate that instrumental data fusion can be useful for the identification of sensory defects in virgin olive oils. Copyright © 2016 Elsevier Ltd. All rights reserved.

  2. 2D and 3D optical diagnostic techniques applied to Madonna dei Fusi by Leonardo da Vinci

    Science.gov (United States)

    Fontana, R.; Gambino, M. C.; Greco, M.; Marras, L.; Materazzi, M.; Pampaloni, E.; Pelagotti, A.; Pezzati, L.; Poggi, P.; Sanapo, C.

    2005-06-01

    3D measurement and modelling have been traditionally applied to statues, buildings, archeological sites or similar large structures, but rarely to paintings. Recently, however, 3D measurements have been performed successfully also on easel paintings, allowing to detect and document the painting's surface. We used 3D models to integrate the results of various 2D imaging techniques on a common reference frame. These applications show how the 3D shape information, complemented with 2D colour maps as well as with other types of sensory data, provide the most interesting information. The 3D data acquisition was carried out by means of two devices: a high-resolution laser micro-profilometer, composed of a commercial distance meter mounted on a scanning device, and a laser-line scanner. The 2D data acquisitions were carried out using a scanning device for simultaneous RGB colour imaging and IR reflectography, and a UV fluorescence multispectral image acquisition system. We present here the results of the techniques described, applied to the analysis of an important painting of the Italian Reinassance: `Madonna dei Fusi', attributed to Leonardo da Vinci.

  3. Does transition from the da Vinci Si to Xi robotic platform impact single-docking technique for robot-assisted laparoscopic nephroureterectomy?

    Science.gov (United States)

    Patel, Manish N; Aboumohamed, Ahmed; Hemal, Ashok

    2015-12-01

    To describe our robot-assisted nephroureterectomy (RNU) technique for benign indications and RNU with en bloc excision of bladder cuff (BCE) and lymphadenectomy (LND) for malignant indications using the da Vinci Si and da Vinci Xi robotic platform, with its pros and cons. The port placement described for Si can be used for standard and S robotic systems. This is the first report in the literature on the use of the da Vinci Xi robotic platform for RNU. After a substantial experience of RNU using different da Vinci robots from the standard to the Si platform in a single-docking fashion for benign and malignant conditions, we started using the newly released da Vinci Xi robot since 2014. The most important differences are in port placement and effective use of the features of da Vinci Xi robot while performing simultaneous upper and lower tract surgery. Patient positioning, port placement, step-by-step technique of single docking RNU-LND-BCE using the da Vinci Si and da Vinci Xi robot are shown in an accompanying video with the goal that centres using either robotic system benefit from the hints and tips. The first segment of video describes RNU-LND-BCE using the da Vinci Si followed by the da Vinci Xi to highlight differences. There was no need for patient repositioning or robot re-docking with the new da Vinci Xi robotic platform. We have experience of using different robotic systems for single docking RNU in 70 cases for benign (15) and malignant (55) conditions. The da Vinci Xi robotic platform helps operating room personnel in its easy movement, allows easier patient side-docking with the help of its boom feature, in addition to easy and swift movements of the robotic arms. The patient clearance feature can be used to avoid collision with the robotic arms or the patient's body. In patients with challenging body habitus and in situations where bladder cuff management is difficult, modifications can be made through reassigning the camera to a different port with

  4. Vírus da leucemia felina: análise da classificação da infecção, das técnicas de diagnóstico e da eficácia da vacinação com o emprego de técnicas sensíveis de detecção viral Feline leukemia virus: infection outcomes, diagnostic techniques and vaccine efficacy analysis employing sensitive techniques of virus detection

    Directory of Open Access Journals (Sweden)

    Andreza Soriano Figueiredo

    2011-11-01

    Full Text Available O Vírus da leucemia felina (FeLV pertence à família Retroviridae, gênero Gammaretrovirus. Diferentemente de outras retroviroses, uma parcela dos gatos jovens e adultos exposta ao FeLV não apresenta antigenemia/viremia, de acordo com as técnicas convencionais de detecção viral, como isolamento em cultivo celular, imunofluorescência direta e ELISA. O emprego de técnicas de maior sensibilidade para detecção e quantificação viral, como o PCR quantitativo, permitiu a identificação de animais positivos para a presença de DNA proviral e RNA na ausência de antigenemia/viremia e, com isso, um refinamento da análise das diferentes evoluções da infecção. Assim, reclassificou-se a patogenia do FeLV em 4 categorias: infecção abortiva, regressiva, latente e progressiva. Foi possível também detectar DNA proviral e RNA em animais considerados imunes ao FeLV após vacinação. Diante disso, os objetivos desta revisão de literatura foram demonstrar as implicações da utilização de técnicas sensíveis de detecção viral na interpretação e classificação da infecção do FeLV e rever as técnicas de detecção do vírus para fins de diagnóstico. Além disso, apresentar os resultados referentes à eficácia da vacinação contra o FeLV com a utilização dessas técnicas.Feline leukemia virus (FeLV belongs to the Retroviridae family, genus Gammaretrovirus. Unlike other retroviruses, a portion of FeLV exposed animals eliminates antigenemia/viremia, according to convectional techniques of virus detection, such as isolation in cell culture, direct fluorescent antibody test and ELISA. The use of more sensitive techniques to detect and quantify viruses enabled the detection of proviral DNA and RNA in cats with undetectable antigenemia/viremia, and thus the refinement of the different infection outcomes analysis. As a result, FeLV pathogenesis was reclassified in 4 categories: abortive, regressive, latent and progressive infections. It

  5. Estudo do gesto instrumental sob o prisma da Labanotation: o exemplo da Tapping Technique em Percussion Study I para violão solo de Arthur Kampela

    Directory of Open Access Journals (Sweden)

    Ledice Fernandes-Weiss

    2018-04-01

    Full Text Available Este estudo parte dos efeitos de percussão criados por Arthur Kampela em seu Percussion Study I visando compreender o movimento físico e o gesto instrumental do violonista como um fenômeno orgânico, intimamente relacionado com o gesto sonoro. Para tanto, utilizamos como ferramenta de análise a notação de movimentos coreográficos criada por Rudolf von Laban; este sistema é aplicado aos gestos requeridos para se realizarem cinco passagens da obra de Kampela onde os efeitos de percussão estão particularmente presentes. A partir da leitura dos cinetogramas criados, podemos observar uma predominância de movimentos em ricochete e outros efeitos percussivos que, além de promover um melhor relaxamento muscular, corroboram no impacto visual que a peça causa por sua gestualidade corporal. Observamos também que há uma notável exploração espacial do instrumento. Ao abordarmos o fazer musical de um ponto de vista coreográfico, entendemos este como um complexo que inclui o som produzido, os gestos e movimentos do performer, sua energia, seu corpo e o espaço que o circunda.

  6. Characterization of the perovskite La{sub 0,9}Sr{sub 0,1}Ga{sub 0,2}O{sub 2,85} prepared by cation complexation; Caracterizacao da perovsquita La{sub 0,9}Sr{sub 0,1}Ga{sub 0,2}O{sub 2,85} preparada pela tecnica de complexacao de cations

    Energy Technology Data Exchange (ETDEWEB)

    Reis, S.L.; Grosso, R.L.; Muccillo, E.N.S., E-mail: shirley.reis@usp.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2012-07-01

    Strontium and magnesium doped lanthanum gallate exhibits perovskite-type structure and high ionic conductivity. Other features of this ceramic material are large electrolytic regime and negligible electronic conductivity. These characteristics are responsible for the potential use of this solid electrolyte in solid oxide fuel cells operating at intermediate temperatures (~∼500-700 deg C). In this work, the composition La{sub 0.9}Sr{sub 0.1}Ga{sub 0.8}Mg{sub 0.2}O{sub 2.85} was prepared by the cation complexation technique aiming to obtain powder and sintered specimens with good chemical and structural homogeneities. X-ray diffraction results evidence that single phase was obtained, within the limitations of the technique, in samples sintered at 1350 deg C/4 h, with relative density above 92%. (author)

  7. Proposta metodológica para a avaliação da técnica da pedalada de ciclistas: estudo de caso Methodological proposal for evaluation of the pedaling technique of cyclists: a case study

    Directory of Open Access Journals (Sweden)

    Fernando Diefenthaeler

    2008-04-01

    Full Text Available No estudo da biomecânica do ciclismo diversas técnicas têm sido utilizadas para descrever e compreender o movimento da pedalada. O objetivo deste estudo é propor uma metodologia para a avaliação de ciclistas sob o ponto de vista das forças aplicadas no pedal. Um ciclista de elite foi avaliado por meio de um protocolo que consistiu em alterar o selim em quatro diferentes posições (deslocado para cima, para baixo, para frente e para trás a partir da posição de referência, especificamente, aquela adotada para treinamento pelo ciclista. A mudança no ajuste do selim foi de 1 cm. A bicicleta do atleta foi acoplada a um ciclossimulador magnético. A carga do teste foi normalizada por um critério fisiológico (segundo limiar ventilatório, simulando o ritmo de prova do atleta. O pedal direito foi substituído por um pedal bidimensional instrumentado para registrar as forças normal e tangencial. A média do impulso angular da força efetiva foi calculada a partir de dez ciclos consecutivos de pedalada. As mudanças na posição do selim modificaram o impulso da força efetiva em relação à posição de referência. Sendo assim, o protocolo é eficaz e pode ser aplicado em diferentes situações.Many techniques have been used in biomechanics to describe the cycling movement. The purpose of this study is to proposal a specific methodology to evaluation the forces applied on the pedal. An experienced elite cyclist was submitted to a protocol which consisted of four different saddle positions (upward, downward, forward, and backward assuming as reference position the one used by the cyclist in training and competition. The displacement of the saddle was of 1cm in all tests. The individual's bicycle was connected to a magnetic cycle simulator. The load was normalized by a physiological criterion (ventilatory threshold, to simulate the cyclist's race rhythm. The right regular pedal was replaced by a 2D instrumented pedal to record the force

  8. Medida da visão em candelas: description of a psychophysical technique to quantify luminous intensity

    Directory of Open Access Journals (Sweden)

    Airton Leite Kronbauer

    2011-04-01

    Full Text Available OBJETIVO: Desenvolver um método e um dispositivo para quantificar a visão em candela (cd. Os estudos de medida da visão são importantes para todas as ciências visuais. MÉTODOS: É um estudo teórico e experimental. Foram descritos os detalhes do método psicofísico e da calibração do dispositivo. Foram realizados testes preliminares em voluntários. RESULTADOS: É um teste psicofísico simples e com resultado expresso em unidades do sistema internacional de medidas. Com a descrição técnica será possível reproduzir o experimento em outros centros de pesquisa. CONCLUSÃO: Os resultados aferidos em intensidade luminosa (cd são uma opção para estudo visual. Esses resultados possibilitarão extrapolar medidas para modelos matemáticos e para simular efeitos individuais com dados aberrométricos.

  9. Synthesis and characterization of the perovskite Sm{sub 0.5}Sr{sub 0.5}CoO{sub 3} for using as cathode in solid oxide fuel cells; Sintese e caracterizacao da provsquita Sm{sub 0.5}Sr{sub 0.5}CoO{sub 3} para utilizacao como catodo em celulas a combustivel de oxido solido

    Energy Technology Data Exchange (ETDEWEB)

    Blanco, P.H.L.; Muccillo, R.; Muccillo, E.N.S. [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)], e-mail: enavarro@usp.br

    2008-07-01

    Solid oxide fuel cells are basically constituted by ceramic materials, a solid electrolyte sandwiched between two electrodes. A number of ceramic materials with perovskite structure have been proposed to act as electrode material due to the combination of their physical and chemical properties along with compatibility with the solid electrolyte. In this work the mixed oxide Sm{sub 0,5}Sr{sub 0,5}CoO{sub 3} was synthesized by the cation complexation technique. This perovskite oxide has been proposed as cathode in solid oxide fuel cells that operates in the intermediate temperature range ({approx} 500 to {approx} 700 deg C). Citric acid was used as complexant agent. The thermal decomposition of the precursor material occurs in several stages up to 600 deg C. After calcinations at 700 deg C the mixed oxide exhibits the characteristic perovskite phase of Sm{sub 0,5} Sr{sub 0,5}CoO{sub 3} the microstructure of the thermally decomposed material consists of porous agglomerates. This technique allowed for obtaining a single phase material at a relatively lower temperature. (author)

  10. Tratamento da síndrome do túnel ulnar pela técnica da epicondilectomia parcial medial do cotovelo Treatment of cubital tunnel syndrome using the technique of medial partial epicondylectomy of the elbow

    Directory of Open Access Journals (Sweden)

    Marcio Eduardo de Melo Viveiros

    2008-12-01

    Full Text Available OBJETIVO: Analisamos retrospectivamente os resultados de 21 casos de síndrome cubital tratados cirurgicamente com a técnica da epicondilectomia parcial medial. MÉTODOS: No período de fevereiro de 2001 a outubro de 2006, 21 pacientes com síndrome do canal cubital foram tratados pela técnica da epicondilectomia parcial medial do cotovelo associada à neurólise do nervo ulnar. Destes, 12 (57,1% eram do sexo masculino. O lado direito foi o acometido em 15 (71,4% pacientes. A média da idade dos pacientes foi de 51,6 anos. Pela graduação de McGowan, seis (28,6% pacientes encontravam-se no grau I, 11 (52,3%, no grau II e quatro (19,1%, no grau III do período pré-operatório. RESULTADOS: O tempo médio de acompanhamento pós-operatório foi de 25,7 meses. No pós-operatório, os pacientes foram avaliados conforme a escala de pontos de Bishop, sendo que nove (42,8% apresentavam resultados excelentes, sete (33,3%, bons, três (14,2%, regulares e dois (9,5%, ruins. Nesta série, não se encontraram como complicações a instabilidade em valgo residual, a lesão permanente do nervo ulnar, a recidiva da compressão ou a subluxação do nervo ulnar. As complicações encontradas foram perda do arco de movimento em um (4,7% caso, infecção superficial em um (4,7% e um (4,7% com dor residual. CONCLUSÃO: Os resultados apresentados permitem concluir que a epicondilectomia parcial medial do cotovelo associada à neurólise do nervo ulnar é eficiente e segura para o tratamento da síndrome do canal cubital.OBJECTIVE: The authors made a retrospective analysis of the results of 21 cases of cubital syndrome that were surgically treated with the partial medial epicondylectomy. METHODS: From February 2001 to October 2006, 21 patients with cubital tunnel syndrome were treated with the technique of elbow partial medial epicondylectomy associated to neurolysis of the ulnar nerve. Of these patients, 12 (57.1% were male. The right side was involved in 15 (71

  11. Western´s decline, culture tragedy and Titan´s rise: genealogical elements of the discussion of technique in Heidegger Declínio do ocidente, tragédia da cultura e ascensão dos Titãs: elementos genealógicos da discussão da técnica em Heidegger

    Directory of Open Access Journals (Sweden)

    Francisco Rüdiger

    2008-06-01

    Full Text Available The article intends to signalize the debts of the Heideggerian meditation on technique from the ideas of three thinkers: Simmel, Spengler and Ernst Jünger. After sketches up the context in which they arisen, the article focuses in their main thesis to confront them with the way they are appropriate by Heidegger. The article concludes stressing the transcendent character of the points in it analyzed to the enlightenment of the question of technique according to Heidegger. Keywords: Heidegger and the question of technique. Technique and modern culture. Quer-se com o texto apontar as dívidas da reflexão heideggeriana sobre a técnica moderna para com as idéias de três pensadores: Simmel, Spengler e Ernst Jünger. Depois de breve contextualização do problema, o essencial das teses de cada um é posto à luz e confrontado com sua apropriação por parte de Heidegger. Indicando conexões e rupturas, conclui-se chamando à atenção para o interesse transcendente dos pontos em questão. Palavras-chave: Heidegger e a questão da técnica. Técnica e cultura moderna.

  12. Plastia da valva mitral com a técnica do "Duplo Teflon": resultados de 10 anos Mitral valve repair with "Double Teflon" technique: 10-year results

    Directory of Open Access Journals (Sweden)

    Carlos Manuel de Almeida Brandão

    2007-12-01

    Full Text Available OBJETIVO: O objetivo deste trabalho é apresentar os resultados clínicos tardios da plástica da valva mitral com a técnica do "Duplo Teflon". MÉTODOS: A plástica de "Duplo Teflon" consiste em técnica de reparo mitral com ressecção quadrangular da cúspide posterior, anuloplastia segmentar com plicatura do anel com de fios com "pledgets" sobre uma tira de Teflon, e sutura borda a borda da cúspide. Entre abril de 1994 e dezembro de 2003, 133 pacientes com diagnóstico de insuficiência mitral degenerativa com alongamento ou rotura de cordas da cúspide posterior foram submetidos à plástica com esta técnica. A idade média foi de 60,4 anos e 60,9% eram do sexo feminino. Quanto à avaliação clínica no pré-operatório, 29,3% dos pacientes estavam em classe funcional IV, 55,7% em classe III e 15,0% em classe II. Técnicas associadas de plástica mitral foram utilizadas em 15,2% dos pacientes, sendo a mais comum o encurtamento de cordas. Vinte e seis (19,5% pacientes foram submetidos a operações associadas. RESULTADOS: Houve um (0,75% óbito hospitalar. No período pós-operatório tardio, 95,5% dos sobreviventes estavam em classe funcional I. As taxas linearizadas de tromboembolismo, reoperação e óbito foram 0,9%, 0,3% e 0,6% pacientes/ano, respectivamente. A sobrevida atuarial em 10 anos foi de 94,1% ± 3,6%. As sobrevidas atuariais livre de tromboembolismo e reoperação foram de 97,3 ± 1,5% e 99,2 ± 0,8%, respectivamente. Não houve casos de endocardite ou hemólise. CONCLUSÃO: A plástica da valva mitral com a técnica do "Duplo Teflon" apresenta baixa morbi-mortalidade e boa evolução clínica tardia.OBJECTIVE: The purpose of this paper is to present the late clinical results of mitral valve repair with the "Double Teflon" technique. METHODS: "Double Teflon" technique consists of a quadrangular resection of the posterior leaflet, annulus plication with "pledgetted" stitches over a Teflon patch, and leaflet suture. Between

  13. Diagnóstico da pneumonia enzoótica suína pela técnica da imunoperoxidase Immunoperoxidase technique for diagnosis of enzootic pnemonia in swine

    Directory of Open Access Journals (Sweden)

    F.C. Ribeiro

    2004-12-01

    Full Text Available Avaliou-se a técnica da imunoperoxidase como método auxiliar para a detecção de Mycoplasma hyopneumoniae em suínos naturalmente infectados. Foram colhidos 80 fragmentos de pulmões de 40 animais provenientes de granjas consideradas negativas e 40 de granjas com diagnóstico positivo de pneumonia enzoótica. Com a utilização de soro policlonal específico (IgG de coelho anti- M. hyopneumoniae observou-se correlação positiva de 77% entre os diagnósticos microscópicos e imunoistoquímicos, enquanto que a correlação entre os diagnósticos macroscópico e imunoistoquímico foi de 49%. Nas granjas consideradas negativas observou-se presença de discreta imunorreação em 22,5% dos casos, o que poderia indicar a existência de reação cruzada com outros microrganismos. Nas granjas com diagnóstico positivo para pneumonia enzoótica a técnica da peroxidase-anti-peroxidase (PAP revelou diferentes graus de intensidade, variando de fraca imunomarcação até espesso depósito amarronzado no epitélio ou na luz das vias aéreas, ou ainda no interior de macrófagos, com relação direta entre a intensidade das lesões e da imunorreação. A técnica imunoistoquímica possui sensibilidade de 95% e especificidade de 77,5%, podendo ser recomendada como ferramenta auxiliar, rápida e de baixo custo para o diagnóstico de pneumonia enzoótica suína em laboratórios de rotina em histopatologia.The immunoperoxidase technique as an auxiliary method for the detection of Mycoplasma hyopneumoniae in naturally infected pigs was evaluated. Eighty lung fragments of which 40 from animals of farms considered negatives and 40 of farms with positive diagnosis of enzootic pneumonia were collected. The results obtained with polyclonal specific serum (IgG of rabbit anti - M. hyopneumoniae evidentiated a positive correlation of 77% between microscopic and immunohistochemical diagnoses, while the correlation between the macroscopic and immunohistochemical diagnoses

  14. Comparison of NDA and DA measurement techniques for excess Pu powders at the Hanford Site: Operator and IAEA experience

    International Nuclear Information System (INIS)

    Welsh, T.L.; McRae, L.P.; Delegard, C.H.

    1995-06-01

    Quantitative physical measurements are necessary components of the International Atomic Energy Agency (IAEA) nuclear material safeguards verification regime. In December 1994, IAEA safeguards were initiated on an inventory of plutonium-bearing oxide and scrap items in Vault 3 of the 2736-Z Building of the Plutonium Finishing Plant on the United States Department of Energy's (USDOE) Hanford Site. The material originated in the United States nuclear weapons complex. The diversity of the chemical form and the heterogenous physical form of the plutonium in this inventory were expected to challenge the target precision and accuracy of methods employed by IAEA: quantitative destructive analytical techniques (which are susceptible to sampling error) and quantitative coincident neutron measurements (which rely on knowledge of the material's chemical form and purity). Because of the diverse and heterogenous nature of plutonium-bearing scrap, plant operations increasingly have adopted calorimetric techniques both for item inventory measurements and for verification purposes. During the recent advent of IAEA safeguards at Vault 3, a set of destructive and nondestructive methods were applied to a number of inventory items (cans of plutonium-bearing powders) with widely ranging chemical purities. Results of these measurements, gathered by the operator's and IAEA's laboratories and instruments as well as by instruments from Pacific Northwest Laboratory and USDOE's Los Alamos National Laboratory (LANL), are presented and statistically compared

  15. Totally extraperitoneal (TEP) bilateral hernioplasty using the Single Site® robotic da Vinci platform (DV-SS TEP): description of the technique and preliminary results.

    Science.gov (United States)

    Cestari, A; Galli, A C; Sangalli, M N; Zanoni, M; Ferrari, M; Roviaro, G

    2017-06-01

    Laparoendoscopic single site totally extraperitoneal (TEP) hernia repair showed to be a feasible alternative to conventional laparoscopic hernia repair; nevertheless single site surgery, with the loss of instruments triangulation can be a demanding procedure. To overcome those hurdles, the Single Site® (SS) platform of the da Vinci (DV) Si robotic system enables to perform surgical procedures through a 25-mm skin incision, with a stable 3D vision and restoring an adequate triangulation of the surgical instruments. We present in details the technique and the preliminary results of DV-SS TEP, to our knowledge the first cases reported in literature. In March 2016, three consecutive male patients (mean age 46.6 years-mean BMI 25.3) with bilateral symptomatic inguinal hernia were submitted to DV-SS TEP in our institutions. Feasibility, codification of the technique, operative time and perioperative outcomes were recorded. All the procedures were completed as scheduled, with no conversion to other techniques. Mean operative time was 98.6 min, ranging between 155 and 55 min, reflecting the learning curve of the operating room team on this new procedure. No intraoperative or postoperative complications were experienced and all the patients were discharged within 24 h after surgery. Patients reported satisfactory postoperative course, with no recurrence of inguinal hernia and satisfaction in cosmetic result at 6-month follow-up. DV-SS TEP inguinal hernia repair showed to be feasible and effective surgical option for bilateral groin hernia repair. Patients' outcome was uneventful, with optimal cosmetic results. Further studies comparing this innovative technique to TEP or LESS TEP should be promoted.

  16. Synthesis and characterization particles of Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtained by the citrate-EDTA technique; Sintese e caracterizacao de particulados de Ba{sub 0,50}Sr{sub 0,50}Co{sub 0,80}Fe{sub 0,20}O{sub 3} obtidos pela tecnica dos citratos-EDTA

    Energy Technology Data Exchange (ETDEWEB)

    Bonturim, E; Vargas, R A; Andreoli, M; Seo, E S.M., [Instituto de Pesquisas Energeticas e Nucleares (CCTM/IPEN/CNEN-SP), Sao Paulo, SP (Brazil). Centro de Ciencia e Tecnologia de Materiais

    2010-07-01

    The Ba{sub (1-x)}Sr{sub (x)}Co{sub (1-y)}Fe{sub (y)}O{sub (3)} (BSCF) has been studied as a cathode material for Intermediate Temperature Solid Oxide Fuel Cell, due to its better ion and electron conduction. This work aims to study the synthesis of the compound obtained from the citrate-EDTA technique. Thermogravimetric analysis indicated the formation of the compound above 800 deg C. The materials calcined at temperatures of 700, 800 and 900 deg C for 5 h showed cubic pseudo-perovskite structure, according to the literature. By analysis of X-ray fluorescence were obtained powders with nominal chemical composition in the temperature range studied. The micrographs obtained by SEM and particle size distribution analysis showed the formation of particle with diameters below 1 micron. (author)

  17. Characterization of limestone of region South and Southeast of Para; Caracterizacao de calcario da regiao Sul e Sudeste do Para

    Energy Technology Data Exchange (ETDEWEB)

    Marinho, A.R.O.; Vieira, J.H.A.; Antunes Junior, L.V.; Medeiros, A.C.; Souza, G.P., E-mail: marabaonline@gmail.com [Universidade Federal do Sul e Sudeste do Para (FEMAT/UNIFESSPA), Maraba, PA (Brazil)

    2014-07-01

    Limestone is used in daily activities, and it is common the use of products containing calcium carbonate in various applications, from construction to food production, air purification to sewage treatment, the sugar refining materials for the toothpaste, the manufacture of glass and steel in the manufacture of paper, plastics, paints, ceramics and many others. The Limestone present in the region of south and southeast of Para is presented in deposits that have not been explored on a large scale, being justified a deepening in characteristics thereof. For the characterization of the material, gross samples were comminuted by crushing and ball mill, sieved and then separated into aliquots. In the end were used fluorescence analysis of X-ray, diffraction X-rays, determination of the moisture and loss on ignition of the material at 950 °C for one hour, obtaining results of a dolomitic limestone. (author)

  18. Preliminary characterization of dose in personnel of interventional radiology; Caracterizacao preliminar da dose em profissionais de radiologia intervencionista

    Energy Technology Data Exchange (ETDEWEB)

    Godolfim, Laura Larre; Anes, Mauricio; Bacelar, Alexandre; Lykawka, Rochelle [Hospital de Clinicas de Porto Alegre (HCPA), Porto Alegre, RS (Brazil)

    2016-07-01

    Exposure to X-rays of Interventional Radiology professionals (IR) impacts in the high dose rate received by these individuals, and there are reports of biological effects of this professional activity. Therefore, it is fomented greater control over the doses received by these workers. This research intends to characterize the doses received by the professionals during IR procedures. We evaluated the doses of radiologists, anesthesiologists and nursing staff of the Hospital de Clinicas de Porto Alegre, through measures with dosimeters of the OSL type, distributed in up to six regions of the body of these professionals. Until now were accompanied 33 cholangiography procedures and 29 embolization procedures. As a preliminary result, it was possible to identify a wide variation between doses of the professionals of the same function in each procedure. In overview, the dose of the professionals presented in descending order as a radiologist 1> radiologist 2 > anesthetist > nursing. (author)

  19. Characterization of ionizing radiation effects on human skin allografts; Caracterizacao dos efeitos da radiacao ionizante em pele humana para aloenxerto

    Energy Technology Data Exchange (ETDEWEB)

    Bourroul, Selma Cecilia

    2004-07-01

    The skin has a fundamental role in the viability of the human body. In the cases of extensive wounds, allograft skin provides an alternative to cover temporarily the damaged areas. After donor screening and preservation in glycerol (above 85%), the skin can be stored in the Skin Banks. The glycerol at this concentration has a bacteriostatic effect after certain time of preservation. On the other hand, skin sterilization by ionizing radiation may reduces the quarantine period for transplantation in patients and its safety is considered excellent. The objectives of this work were to establish procedures using two sources of ionizing radiation for sterilization of human skin allograft, and to evaluate the skin after gamma and electron beam irradiation. The analysis of stress-strain intended to verify possible effects of the radiation on the structure of preserved grafts. Skin samples were submitted to doses of 25 kGy and 50 kGy in an irradiator of {sup 60}Co and in an electron beam accelerator. Morphology and ultra-structure studies were also accomplished. The samples irradiated with a dose of 25 kGy seemed to maintain the bio mechanic characteristics. The gamma irradiated samples with a dose of 50 kGy and submitted to an electron beam at doses of 25 kGy and 50 kGy presented significant differences in the values of the elasticity modulus, in relation to the control. The analysis of the ultramicrographies revealed modifications in the structure and alterations in the pattern of collagen fibrils periodicity of the irradiated samples. (author)

  20. Clinical, radiographic and scintigraphic aspects of the trapeziometacarpal osteoarthritis; Caracterizacao clinica, radiografica e cintilografica da osteoartrose trapeziometacarpiana

    Energy Technology Data Exchange (ETDEWEB)

    Kaziyama, Helena Hideko Seguchi

    1996-12-31

    Trapeziometacarpal osteoarthritis occurs mainly in women during the menopausal period. It is related to manual activities and is usually bilateral. The onset is insidious and the evolution is slow and progressive. It is characterized by of strength and pain in the basis of the thumb resulting in limitation of the use and function of the hand. The diagnosis of this condition is based on the physical examination. The manouver of compression axial-rotation of the trapezimetacarpal joint is a common positive finding. Typical findings of osteoarthritis are present in the radiological studies. Scintigraphic images have a predictive value. The early diagnosis is important to avoid the risk factors and to prevent disabilities of the hand. (author) 102 refs., 18 figs., 10 tabs.

  1. Characterization of application of acu sandstone in ceramic mass; Caracterizacao da aplicacao do arenito acu na massa ceramica

    Energy Technology Data Exchange (ETDEWEB)

    Nobrega, L.F.P.M.; Souza, M.M.; Gomes, Y.S.; Fernandes, D.L., E-mail: junior.luiz09@hotmail.com [Universidade Federal do Rio Grande do Norte (DIAREN/UFRN), Natal, RN (Brazil). Laboratorio de Processamento Mineral e Residuo

    2016-07-01

    The sandstone is a sedimentary rock formed mainly by quartz grains. In Rio Grande do Norte, there is the Potiguar Basin with the Jandaira and Acu Formations. The latter consists of thick layers of whitish-colored sandstones. It stands out as a water storage facility in the state, but it is also used for building aggregates. This article aimed at the use of the sandstone of this formation in the ceramic mass for coating. Initially, the material was sampled. It went through the comminution process to achieve the required granulometry. After this, three formulations were made to incorporate this new material into the traditional ones. The methods were performed according to ISO 13816. After sintering at 1200 °C, the specimens were subjected to the physical tests. A positive result was obtained for the use of the Acu sandstone in low concentrations. It is clear, therefore, its use in ceramics for coating.

  2. Viscosity and density study for characterization of oil mixtures; Estudo da viscosidade e densidade para caracterizacao das misturas de petroleo

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Michelle I.; Azevedo, Vildomar S.; Jacinto, Tulio Wagner B. [Aurizonia Petroleo S.A, Natal, RN (Brazil); Vieira, Mariane; Vidal, Rosangela Regia Lima; Garcia, Rosangela Balaban [Universidade Federal do Rio Grande do Norte (UFRN), Natal, RN (Brazil)

    2008-07-01

    The oil can be defined as a mixture of hydrocarbons and sulphur, nitrogen and oxygenated organic derivatives at lower amount. There is a practical difficulty of analytical determination of the oil composition, mainly due to the large quantity of medium and heavy oil fractions. For heavier fractions, it is necessary to infer the composition of the cut from properties that can be readily obtained in the laboratory, such as refraction index, density and viscosity. The analysis of oil composition and its fractions is important information on various aspects (IOB et al., 1996): determining the operating conditions of refining, selection of suitable catalysts and mixing operations ('blending'), the economic evaluation of mixtures and analysis of environmental impact due to emissions. The first study on characterization of fractions of the oil was reported by Hill and Coats (1928), who set an empirical relationship between the density and Saybolt viscosity named viscosity-density constant (VGC). The statement was obtained from the analysis of the density with the oil viscosity changes. Physical properties such as density, boiling point and viscosity can be used to classify the oil. The aim of this work was to classify oil fractions based on viscosity-density constant, using mixtures of oils with different APIs. The results showed that there is an optimum composition for each mixture, and the addition of more oil of medium classification does not lead to potential commercial oil. (author)

  3. Preparation and characterization of hybrid materials from natural chrysotile; Preparacao e caracterizacao de materiais hibridos a partir da crisotila natural

    Energy Technology Data Exchange (ETDEWEB)

    Giraldelli, M.G.; Silva, M.L.C.P., E-mail: marciogiraldelli@hotmail.co [Universidade de Sao Paulo (EEL/USP), Lorena, SP (Brazil). Escola de Engenharia

    2010-07-01

    Special attention has been given to the development of new materials from natural chrysotile. This fiber has about 40% silicon oxide in its structure with an outer layer of brucite (MgOH{sub 2}). With the aim of obtaining a material with a more uniform structure, acid leaching was performed to remove the outer layer of brucite, resulting in a silicon oxide hydrate. This material was used as support for the deposition of Nb{sub 2}O{sub 5}.nH{sub 2}O. The Nb{sub 2}O{sub 5}.nH{sub 2}O was prepared by conventional precipitation using as starting material niobium metallic. In this study, we performed the synthesis and characterization of the material SiO{sub 2}.nH{sub 2}O / Nb{sub 2}O{sub 5}.nH{sub 2}O 1:1. Both chrysotile as niobium are widely available national resources, which confirms the economic viability of resource use. The materials studied were characterized by XRD, SEM and TG/DTG. (author)

  4. Clinical, radiographic and scintigraphic aspects of the trapeziometacarpal osteoarthritis; Caracterizacao clinica, radiografica e cintilografica da osteoartrose trapeziometacarpiana

    Energy Technology Data Exchange (ETDEWEB)

    Kaziyama, Helena Hideko Seguchi

    1997-12-31

    Trapeziometacarpal osteoarthritis occurs mainly in women during the menopausal period. It is related to manual activities and is usually bilateral. The onset is insidious and the evolution is slow and progressive. It is characterized by of strength and pain in the basis of the thumb resulting in limitation of the use and function of the hand. The diagnosis of this condition is based on the physical examination. The manouver of compression axial-rotation of the trapezimetacarpal joint is a common positive finding. Typical findings of osteoarthritis are present in the radiological studies. Scintigraphic images have a predictive value. The early diagnosis is important to avoid the risk factors and to prevent disabilities of the hand. (author) 102 refs., 18 figs., 10 tabs.

  5. Characterization of AA7050 aluminium alloy processed by ECAP; Caracterizacao da liga de aluminio AA7050 processada por ECAP

    Energy Technology Data Exchange (ETDEWEB)

    Cardoso, K.R.; Guido, V. [Universidade do Vale do Paraiba (UNIVAP), Sao Jose dos Campos, SP (Brazil). Inst. de Pesquisa e Desenvolvimento; Travessa, D.N. [Empresa Brasileira de Aeronautica (EMBRAER), Sao Jose dos Campos, SP (Brazil); Jorge Junior, A.M. [Universidade Federal de Sao Carlos (DEMa/UFSCar), SP (Brazil). Dept. de Engenharia de Materiais

    2010-07-01

    The commercial AA7050 aluminium alloy in the solution heat treated condition (W) was processed by ECAP through route A. Two pressing temperatures (room and 150 deg C and velocities (5 and 30mm/min) were used, as well as different number of passes. The effect of such variables on the microstructure evolution was evaluated using optical and transmission electron microscopy with EDX microanalysis, and xray diffraction. It was found that the microstructure has been refined by ECAP, as a result of subgrains formed within deformation bands. ECAP at 150 deg C resulted in intense precipitation of plate like {eta} phase, which evolves to equiaxial morphology as the number of passes increases. (author)

  6. Robotic-assisted laparoscopic radical nephrectomy using the Da Vinci Si system: how to improve surgeon autonomy. Our step-by-step technique.

    Science.gov (United States)

    Davila, Hugo H; Storey, Raul E; Rose, Marc C

    2016-09-01

    Herein, we describe several steps to improve surgeon autonomy during a Left Robotic-Assisted Laparoscopic Radical Nephrectomy (RALRN), using the Da Vinci Si system. Our kidney cancer program is based on 2 community hospitals. We use the Da Vinci Si system. Access is obtained with the following trocars: Two 8 mm robotic, one 8 mm robotic, bariatric length (arm 3), 15 mm for the assistant and 12 mm for the camera. We use curved monopolar scissors in robotic arm 1, Bipolar Maryland in arm 2, Prograsp Forceps in arm 3, and we alternate throughout the surgery with EndoWrist clip appliers and the vessel sealer. Here, we described three steps and the use of 3 robotic instruments to improve surgeon autonomy. Step 1: the lower pole of the kidney was dissected and this was retracted upwards and laterally. This maneuver was performed using the 3rd robotic arm with the Prograsp Forceps. Step 2: the monopolar scissors was replaced (robotic arm 1) with the robotic EndoWrist clip applier, 10 mm Hem-o-Lok. The renal artery and vein were controlled and transected by the main surgeon. Step 3: the superior, posterolateral dissection and all bleeders were carefully coagulated by the surgeon with the EndoWrist one vessel sealer. We have now performed 15 RALRN following these steps. Our results were: blood loss 300 cc, console time 140 min, operating room time 200 min, anesthesia time 180 min, hospital stay 2.5 days, 1 incisional hernia, pathology: (13) RCC clear cell, (1) chromophobe and (1) papillary type 1. Tumor Stage: (5) T1b, (8) T2a, (2) T2b. We provide a concise, step-by-step technique for radical nephrectomy (RN) using the Da Vinci Si robotic system that may provide more autonomy to the surgeon, while maintaining surgical outcome equivalent to standard laparoscopic RN.

  7. Comparison of NDA and DA measurement techniques for excess plutonium powders at the Hanford Site: Statistical design and heterogeneity testing

    International Nuclear Information System (INIS)

    Welsh, T.L.; McRae, L.P.; Delegard, C.H.; Liebetrau, A.M.; Johnson, W.C.; Theis, W.; Lemaire, R.J.; Xiao, J.

    1995-06-01

    Quantitative physical measurements are a n component of the International Atomic Energy Agency (IAEA) nuclear material m ampersand guards verification regime. In December 1994, LA.FA safeguards were initiated on an inventory of excess plutonium powder items at the Plutonium Finishing Plant, Vault 3, on the US Department of Energy's Hanford Site. The material originl from the US nuclear weapons complex. The diversity of the chemical form and the heterogenous physical form of this inventory were anticipated to challenge the precision and accuracy of quantitative destructive analytical techniques. A sampling design was used to estimate the degree of heterogeneity of the plutonium content of a variety of inventory items. Plutonium concentration, the item net weight, and the 240 Pu content were among the variables considered in the design. Samples were obtained from randomly selected location within each item. Each sample was divided into aliquots and analyzed chemically. Operator measurements by calorimetry and IAEA measurements by coincident neutron nondestructive analysis also were performed for the initial physical inventory verification materials and similar items not yet under IAEA safeguards. The heterogeneity testing has confirmed that part of the material is indeed significantly heterogeneous; this means that precautionary measures must be taken to obtain representative samples for destructive analysis. In addition, the sampling variability due to material heterogeneity was found to be comparable with, or greater than, the variability of the operator's calorimetric measurements

  8. Application of gamma irradiation technique for the preservation of propolis; Aplicacao da tecnica de irradiacao gama para preservacao de propolis

    Energy Technology Data Exchange (ETDEWEB)

    Matsuda, Andrea Harumi

    2002-07-01

    Irradiation has been recognized as an efficient method for the reduction of deteriorating and pathogenic microorganisms in foods. Propolis is a resinous product made by bees from material processed by the bee's own metabolism and resins from plants. The aim of this work was the application of gamma irradiation technique for the preservation of propolis, because of its efficiency in the reduction of the microbial load. The changes on the total flavonoids content, phenolic compounds and other characteristics required for the qualification and characterization of Brazilian propolis were also analysed. Propolis samples from Juiz de Fora region, Minas Gerais, were irradiated in a {sup 60}Co source, with doses from 0 to 10kGy for the microbiological analyses and 5.0, 7.0 and 10.0kGy for the physico-chemical analyses. The physico-chemical that have been made were: determination of total flavonoids content, semi-quantitative determination of phenolic compounds (artepelin-C, kempferol, chrysin, galangin and quercetin), dry matter analysis, humidity, ash content, mechanical mass and waxes. The ionizing radiation has shown to be efficient in the reduction of the microbial load. Total coliforms determination showed a great reduction with the dose of 3kGy and concerning mesophile aerobic bacteria a systematic reduction was observed, achieving values <10 UFC/g for the dose of 10kGy; similar results was obtained for molds and yeasts. Salmonella assays were negative for all samples. There was no significant alteration on total flavonoids contents nor on the composition of phenolic compounds as a consequence of radiation application at the assayed conditions. The complementary analyses of dry matter and humidity contents, ashes, mechanical mass and waxes did not shown changes after irradiation even with the maximum dose of 10kGy, remaining the results within the standards required by the Brazilian legislation. (author)

  9. Aplicações da cultura de tecidos vegetais em fruteiras do Cerrado Applications of tissue culture techniques in Brazilian Cerrado fruit trees

    Directory of Open Access Journals (Sweden)

    Hernane Fernandes Pinhal

    2011-07-01

    Full Text Available Atualmente, percebe-se uma preocupação em relação às plantas do cerrado, com grande enfoque nas fruteiras em função de suas características e usos. Apesar de ser uma área ainda pouco explorada, é crescente o número de estudos dessas espécies nativas, dentre eles, os que abrangem as técnicas de cultura de tecidos. Isso se deve uma vez que essa ferramenta biotecnológica permite a propagação de espécies com dificuldade de germinação, minimiza o problema de sementes recalcitrantes, promove a produção de mudas em larga escala, complementa bancos de germoplasma e facilita as trocas de materiais genéticos. Dessa maneira, esta revisão visa a sumarizar o histórico e panorama atual das aplicações da cultura de tecidos em fruteiras do cerrado, proporcionando sustentação para novos estudos.Currently, it's been given a huge concern to the cerrado plants, focusing on fruit trees due to their characteristics and uses. Despite being a fairly unexplored area, the number of studies on these native species has increased, especially those involving tissue culture techniques. That's because this biotechnological tool provides the propagation of species with germination difficulty, reduces problems of recalcitrant seeds, promotes large scale seedling production, complements germplasm banks and facilitates the exchange of genetic materials. Therefore, this review summarizes the history and current situation of tissue culture techniques applied to Brazilian Cerrado fruit trees, providing support to further studies.

  10. Proposta metodológica para a avaliação da técnica da pedalada de ciclistas: estudo de caso Methodological proposal for evaluation of the pedaling technique of cyclists: a case study

    OpenAIRE

    Fernando Diefenthaeler; Rodrigo Rico Bini; Eduardo Nabinger; Orlando Laitano; Felipe Pivetta Carpes; Carlos Bolli Mota; Antônio Carlos Stringhini Guimarães

    2008-01-01

    No estudo da biomecânica do ciclismo diversas técnicas têm sido utilizadas para descrever e compreender o movimento da pedalada. O objetivo deste estudo é propor uma metodologia para a avaliação de ciclistas sob o ponto de vista das forças aplicadas no pedal. Um ciclista de elite foi avaliado por meio de um protocolo que consistiu em alterar o selim em quatro diferentes posições (deslocado para cima, para baixo, para frente e para trás) a partir da posição de referência, especificamente, aque...

  11. Uso da fáscia temporal na suspensão frontal: descrição da técnica cirúrgica - Relato de caso Use of temporal fascia in frontalis suspension: description of the surgical technique - Case report

    Directory of Open Access Journals (Sweden)

    Tânia Pereira Nunes

    2004-04-01

    Full Text Available OBJETIVOS: Familiarizar o oftalmologista com a anatomia da região temporal, descrever a técnica cirúrgica da retirada da fáscia temporal e da suspensão frontal e analisar as vantagens e desvantagens da fáscia temporal na suspensão frontal. MÉTODOS: Revisão do prontuário de uma paciente com blefaroptose grave que foi submetida à suspensão frontal com fáscia temporal. Revisão da anatomia da fossa temporal e das técnicas cirúrgicas. RESULTADOS: Bom resultado estético e funcional foi conseguido no caso descrito. CONCLUSÃO: A fáscia temporal é boa opção na suspensão frontal com algumas vantagens: é um tecido autógeno, de fácil obtenção e mínima morbidade no pós-operatório.PURPOSE: To familiarize the ophthalmologist with the anatomy of the temporal region, to describe the surgical technique of temporal fascia harvest and frontalis suspension and to demonstrate advantages and disadvantages of temporal fascia in frontalis suspension. METHODS: Review of the clinical and surgical data of one case with severe blepharoptosis who underwent frontalis suspension using temporal fascia. Review of the anatomy of the temporal fossa and the surgical techniques. RESULTS: Good esthetic and functional results were obtained in this case. CONCLUSION: Temporal fascia is a good choice for frontalis suspension with some advantages: it is autogenous, it is easily harvested and it yields minimal post-operative morbidity.

  12. Nova técnica: translocação aórtica e pulmonar com preservação da valva pulmonar New technique: aortic and pulmonary translocation with preservation of pulmonary valve

    Directory of Open Access Journals (Sweden)

    Gláucio Furlanetto

    2010-03-01

    Full Text Available Realizamos com sucesso novo procedimento cirúrgico, em duas crianças portadoras de transposição das grandes artérias associada a comunicação interventricular e obstrução da via de saída do ventrículo esquerdo. A cirurgia consiste na realização de translocação aórtica com a valva aórtica e as artérias coronárias para o ventrículo esquerdo, após a ampliação da via de saída desse ventrículo e da comunicação interventricular com pericárdio autólogo fixado em glutaraldeído, associada à translocação do tronco pulmonar para o ventrículo direito, conservando integralmente a valva pulmonar.We applied successfully, a new surgical technique, in two children with transposition of the great arteries with ventricular septal defect and left ventricular outflow tract obstruction, that utilized aortic translocation with the aortic valve and the coronary arteries to the left ventricle, after correction of left outflow tract obstruction and correction of the ventricular septal defect, associated to pulmonary root translocation to the right ventricle, conserving integrally the pulmonary valve.

  13. Tratamento da pseudartrose infectada da tíbia pelo método de Ilizarov: técnica do encurtamento agudo com subseqüente alongamento Treatment of infected pseudoarthrosis of the tibia by Ilizarov's method: technique using acute compression and subsequent distraction

    Directory of Open Access Journals (Sweden)

    Jorge Luiz Borges

    2007-09-01

    Full Text Available OBJETIVO:Comprovar a eficácia do tratamento da pseudartrose infectada da tíbia pelo método de Ilizarov, utilizando a técnica do encurtamento agudo do foco da pseudartrose com posterior alongamento ósseo. MÉTODOS: Foram estudados 20 pacientes adultos portadores de pseudartrose unilateral infectada da tíbia, tratados no período entre novembro de 1993 e setembro de 2000. No pós-operatório, os pacientes foram avaliados quanto a dor, necessidade de órtese, avaliação da mobilidade articular, retorno às atividades normais do dia-a-dia e/ou do trabalho, consolidação da pseudartrose, cura da infecção, existência de deformidades ósseas, discrepância no comprimento dos membros e consolidação óssea na área do regenerado ósseo. RESULTADOS: Os resultados funcionais foram: excelentes em 10 pacientes (50%, bons em oito (40%, regulares em um (5% e ruins em um paciente (5%. O tempo de consolidação da pseudartrose, do segmento ósseo alongado e o tempo de uso do fixador foram proporcionais à extensão da perda óssea. CONCLUSÃO: O método de Ilizarov, associado ao encurtamento agudo com subseqüente alongamento ósseo, mostrou-se eficaz para o tratamento da pseudartrose infectada da tíbia.OBJECTIVE: To verify the effectiveness of treating the infected pseudoarthrosis of the tibia by Ilizarov's method using the technique of acute compression of the focus of pseudoarthrosis with later bone distraction. METHODS: 20 adult patients with unilateral infected pseudoarthrosis of the tibia treated from November 1993 to September 2000 were studied. In the postoperative period, the patients were evaluated for pain, orthesis requirement, joint mobility, return to daily life activities and/or to work, union of the pseudoarthrosis, cure of the infection, presence of bone deformities, discrepancy in limb length, and bone union in the bone regenerate area. RESULTS: Functional results were: excellent in 10 patients (50%, good in eight (40%, regular in

  14. Incidência e fatores predisponentes da migração da fundoplicatura pela técnica de Nissen-Rossetti no tratamento da doença do refluxo Gastroesofágico Incidence and predisponent factors for the migration of the fundoplication by Nissen-Rossetti technique in the surgical treatment of GERD

    Directory of Open Access Journals (Sweden)

    Paulo Afonso Nunes Nassif

    2012-06-01

    Full Text Available RACIONAL: A doença do refluxo gastroesofágico é uma das enfermidades do trato gastrointestinal mais frequentes atualmente. A fundoplicatura de Nissen-Rossetti é técnica operatória muito empregada para o tratamento cirúrgico, sendo a migração intratorácica da válvula uma das principais complicações. OBJETIVO: Avaliar a incidência da migração da fundoplicatura e seus fatores de risco. MÉTODO: Analisou-se retrospectivamente 207 prontuários de pacientes submetidos à fundoplicatura videolaparoscópica pela técnica de Nissen-Rossetti para tratamento da doença do refluxo. As variáveis analisadas foram: sexo, idade, esofagite, grau de esofagite, tamanho da hérnia, alargamento da cárdia, encurtamento esofágico. Para as variáveis quantitativas, foi considerado o teste t de Student. Para as nominais, foi considerado o teste de Qui-quadrado ou o teste exato de Fisher. Valores de pBACKGROUND: Gastroesophageal reflux is the gastrointestinal tract disease most frequently find nowadays. The Nissen-Rossetti fundoplication is widely used for the surgical treatment, and intrathoracic migration of the valve is the most frequent complication. AIM: To assess the incidence of the fundoplication and its risk factors. METHODS: Were analyzed retrospectively medical records of 207 patients undergoing laparoscopic fundoplication by the Nissen-Rossetti technique for the treatment of reflux disease. The variables analyzed were: sex, age, esophagitis grade, size of the herniation, enlargement of the cardia and esophageal shortening. For quantitative variables, was considered the Student's t test. For the nominal, was considered the chi-square or Fisher's exact test. P values ​​<0.05 were considered statistically significant. RESULTS: Of the total, 135 were women (65.22% and 72 men (34.78% with mean age of 47.43 years. The size of the hernia varied between 2 and 6 cm. Two hundred patients had esophagitis (96.62% and 113 (56.50% grade I, 75 grade

  15. Characterization of the natural rubber from new rubber tree clones of PB 300 series; Caracterizacao da borracha natural dos novos clones de seringueira da serie PB 300

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Maycon J.; Spinelli, Rafaela O.; Moreno, Rogerio M.B.; Mattoso, Luiz H.C.; Martins, Maria Alice, E-mail: maria-alice.martins@embrapa.br [Embrapa Instrumentacao/LNNA, Sao Carlos, SP (Brazil); Scaloppi Junior, Erivaldo J. [Instituto Agronomico (IAC), Votuporanga, SP (Brazil). Centro de Seringueira e Sistemas Agroflorestais; Goncalves, Paulo de S. [Instituto Agronomico (IAC), Campinas, SP (Brazil)

    2015-07-01

    The natural rubber (NR) is present in more than 2500 species of plants, being the Hevea brasiliensis the most commercially exploited. It is a raw material of great importance to the Brazilian economy, but the country faces a production's deficit, having to import about 60% of its consumption. In this work , the latex obtained from rubber tree of new clones of PB series 300 (PB 311, PB 312, PB 314 , PB 326, PB 346 and PB 350 ) and RRIM 600 (control) were characterized by dry rubber content (DRC), total solids content, distribution of particle size, Zeta potential, thermogravimetry, differential scanning calorimetry, infrared in the spectroscopy (FTIR), nuclear magnetic resonance (NMR) and technological properties. The DRC values ranged from 33% to 40%, and total solids of 38% to 44%. All of the clones showed average particle diameter between 180.0 to 192.1 nm, excluding clones PB 326 and PB 346 with 150.0 nm and 157.9 nm, respectively. The NMR spectra and FTIR showed that the structure of the natural rubber from all clones studied is cis -1,4- polyisoprene. Natural rubber from the new clones showed good thermal stability up to 285 °C and glass transition temperature of -64 °C. (author)

  16. Fishing activity characterization in areas under influence of seismic activity; Caracterizacao da atividade pesqueira em areas sob influencia da atividade sismica

    Energy Technology Data Exchange (ETDEWEB)

    Fuse, Izabel Yukimi; Zanella, Joao Francisco Illa Font; Eliseire Junior, Dirceu; Pereira, Edisio [Hidrosfera Oceanografia e Meio Ambiente, Rio de Janeiro, RJ (Brazil); Souza, Sergio Augusto Coelho de; Ferraz, Alexandre; Costa, Leandro Soares da; Vidal, Leonardo; Duppre, Mauricio [Okeanos Consultoria e Meio Ambiente Ltda. (Brazil); Uller, George [CGG do Brasil, Rio de Janeiro, RJ (Brazil)

    2004-07-01

    Seismic surveys are an important method in prospecting for oil and gas reservoirs in the marine environment. The ELPN/IBAMA has required that companies develop an adequate social programme in parallel with the seismic surveys to establish a better interaction with the communities influenced by these operations and reduce possible negative effects. Between January and October 2003, CGG Brazil studied coastal communities in the following areas. BM-CE-1 e BM -CE-2, Ceara; Fragata, BM-ES-5 e BM-ES-6, Espirito Santo; BM BAR-1 e BM BAR-3, Maranhao and BM-C-25 and BM-C-16 off Campos basin. Communities and groups that could potentially be influenced by the surveys were visited to mitigate direct and indirect impacts. Preliminary results show that fisheries were the main group to be monitored. A standard questionnaire was used to characterize the local fisheries and interviews were held with fishermen, boat owners and members of the fishery industries (n=422). In Ceara the fishery is typically handmade and occurs in water depths up to 200 meters. The main boat propulsion is sail and the 'Cacoeira' is the most popular gear used. Off Espirito Santo, small and medium motored boats are usually used and line is the main gear among the fishermen. At Barreirinhas (Maranhao), boats are usually up to 14 meters long, and operate in water depths of up to 120 metres. Again the 'cacoeira' is the proffered gear. We concluded that Programs carried out by CGG reached their purpose. This is confirmed by low incident rate between seismic ships and the fisheries fleet. (author)

  17. Autotransplante de cordas tendíneas: nova técnica para o tratamento cirúrgico da insuficiência mitral por rotura de cordas tendíneas da cúspide anterior Allotransplantation of chordae tendineae: new technique for the surgical approach of mitral insufficiency

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    Francisco Gregori Jr

    1992-12-01

    Full Text Available Uma das causas mais freqüentes de prolapso valvar mitral, com conseqüente regurgitação, é a rotura de cordas tendíneas. Várias técnicas têm sido empregadas em tal situação. Entretanto, a substituição valvar mitral tem sido o procedimento mais utilizado. E apresentada uma nova técnica cirúrgica empregada em 4 pacientes com insuficiência valvar mitral severa devido a rotura de cordas tendíneas da cúspide anterior da valva mitral. Um autotransplante de cordas da valva tricúspide para a valva mitral é realizado. Em 2 casos, um retalho é retirado da cúspide anterior da valva tricúspide com cordas tendíneas e parte do músculo papilar correspondente. Nos outros 2 casos a cúspide posterior da valva tricúspide foi retirada, inteiramente, com cordas e músculo papilar. Na primeira variante técnica, a cúspide anterior da valva tricúspide foi reparada e, na segunda, através, da plicatura do anel, a valva tricúspide foi transformada em bicúspide. A peça retirada é transplantada para a valva mitral, sendo suturada a cúspide doadora com a cúspide anterior da valva mitral e o músculo papilar doador com o topo do músculo papilar posterior da valva mitral em 3 casos e com o músculo papilar anterior e 1 caso. Os 4 pacientes foram reestudados clínica e laboratorialmente aos 15, 11, 2 e 1 mês de pós-operatório, respectivamente, com execelente evolução. Apesar da limitada experiência, acreditamos ser esta nova técnica uma boa alternativa para o tratamento cirúrgico da insuficiência mitral por rotura de cordas tendíneas da cúspide anterior.One of the most frequent causes of mitral valve prolapse is rupture of the chordae tendineae. Several techniques have been used to correct severe mitral regurgitation. However, mitral valve replacement is the principal surgical approach to it. We describe a technique used in four patients with marked mitral regurgitation due to ruptured chordae tendineae of the anterior leaflet. We

  18. Ampliação da técnica violonística de mão esquerda: um estudo sobre a pestana Extended left-hand guitar technique: a study on the barré

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    Bruno Madeira

    2013-06-01

    Full Text Available A técnica instrumental é um elemento da performance musical em constantes reformulações. Com o objetivo principal de estender a técnica violonística da pestana, o presente artigo foi dividido em três partes: (1 conceituações gerais sobre técnica instrumental; (2 a partir de métodos instrumentais dos últimos quatrocentos anos, um breve histórico da pestana foi delineado com o objetivo de recolher informações técnicas sobre sua realização, (3 sugestões e exemplificações de procedimentos não usuais de pestana (com dedos diferentes do indicador, de falange, bisagra e cruzada, encontrados de forma muito resumida na escassa bibliografia sobre o assunto e cuja aplicabilidade é verificada no repertório.Instrumental technique is an element of musical performance in constant reformulation. With the main objective of expanding the guitar technique of barring, this study was divided into three parts: (1 general concepts about instrumental technique; (2 from instrumental methods of the past four hundred years, a brief history of the barré was outlined in order to collect technical information about its realization, (3 suggestions and examples of unusual barring procedures (with different fingers, phalanx barré, hinge barré, crossed barré, found in the scarce bibliography and which applicability is verified in the repertoire.

  19. Avaliação do efeito da expansão rápida da maxila na via aérea superior, por meio da nasofibroscopia: descrição da técnica e relato de caso Evaluation of the effect of rapid maxillary expansion on the upper airway using nasofibroscopy: case report and description of the technique

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    Edmilsson Pedro Jorge

    2011-02-01

    Full Text Available A finalidade deste artigo é avaliar o efeito da expansão rápida da maxila (ERM na via aérea superior. Por intermédio de um caso clínico, será relatado como indivíduos com atresia da maxila e com comprometimento da função naso-respiratória podem beneficiar-se com a ERM. Para entender melhor as alterações morfológicas decorrentes do paciente com problemas respiratórios, deve-se conhecer a anatomia e a fisiologia do sistema respiratório. Entretanto, não se pode esquecer que o tratamento deste paciente é multidisciplinar, envolvendo o ortodontista, otorrinolaringologista e a fonoaudióloga.The aim of the present investigation is to evaluate the effect of rapid maxillary expansion (RME on the upper airway. A clinical case is presented to describe how patients with atresic maxilla and reduced naso-respiratory function can have benefits from rapid maxillary expansion. In order to better understand the morphological alterations present in patients with respiratory disorders, it is necessary to understand the respiratory system's anatomy and physiology. However, it is relevant to mention that this patient undergoes a multidisciplinary treatment, involving the orthodontist, the otorhinolaryngologist and the phonoaudiologist.

  20. Calibração da técnica de moiré aplicada a perfilometria de protótipos mecânicos Calibration method applied to a moiré technique in experiments of mechanical archetypes

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    Túlio Seabra Gomes

    2009-04-01

    Full Text Available A perfilometria é uma técnica amplamente utilizada na construção de mapas e gráficos de relevos aplicados a uma vasta área do conhecimento. Frente às necessidades de suprir a demanda da indústria e da área de desenvolvimento de protótipos quanto a técnicas não invasivas na investigação da superfície de materiais em geral, o presente trabalho buscou propor uma metodologia de calibração aplicada à técnica de moiré para investigações perfilométricas em protótipos mecânicos buscando baixos custos e flexibilidade. A técnica de moiré consiste na comparação de dois retículos periódicos, onde um segue o comportamento da superfície do objeto (retículo modelo - Rm e outro não está deformado, seguindo o comportamento de um plano de referência, (retículo de referência - Rr. A luz que passa entre os retículos se sobrepõe formando padrões de moiré ou franjas de moiré que se comportam como ondas senoidais. Nos ensaios de calibração, usou-se um cone de relevo conhecido para a determinação de uma constante de correção de mapas gerados digitalmente. Os ensaios realizados aplicaram a metodologia para a determinação do perfil de um mouse de computador e para a determinação da deformação de uma chapa metálica. A metodologia proposta para a calibração da técnica de moiré mostrouse capaz de realizar os mapeamentos, com resolução máxima na ordem de centésimos de milímetros, podendo então ser usada em aplicações com níveis de precisão inferiores a essa ordem.Profilometry is a measurement technique widely used in map and relief graphic construction, being applied to vast areas of knowledge. The aim of the present investigation was to introduce a calibration method applied to a moiré technique in experiments of mechanical archetypes, with low cost and flexibility, due to the need for supplying demands from both industry and mechanical archetype development for non-invasive techniques. The moir

  1. Anuloplastia sem suporte para tratamento da insuficiência mitral reumática Non-supported mitral annuloplasty technique for treatment of rheumatic mitral insufficiency

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    Renato A. K Kalil

    1992-09-01

    Full Text Available Desde 1974, temos empregado anuloplastia sem suporte para tratamento da insuficiência mitral de etiologia reumática em uma população predominantemente jovem. A avaliação dos resultados tardios forma a base deste relato. São 154 pacientes com insuficiência mitral isolada (sem estenose ou dupla lesão, sendo 55 (36% do sexo masculino e 99 (64% do feminino, idade média = 36 ± 16 (5 a 73 anos; as lesões associadas foram: 47 lesões aórticas, 21 tricuspídeas e 2 comunicações interatriais; a classe funcional pré-operatória foi I-II em 19% e III-IV em 81 % e o índice cardiotorácico 0,61 ± 0,10. Todos os pacientes foram submetidos a uma anuloplastia similar à descrita por WOOLER et alii 21 que consiste na redução da porção mural do anel mitral obtida pela aplicação de dois pontos ancorados em feltros nas comissuras, sem comprometer a extensão de cúspide septal. Quando necessário, procedimentos adicionais sobre as cordas tendíneas foram realizados. Nenhum paciente recebeu suporte anular por anel ou barra posterior. A mortalidade precoce foi de 3 (1,9% pacientes: falência miocárdica (1 e embolia pulmonar (2. A mortalidade tardia foi de 9 (5,8%, falência miocárdica (3, septicemia (1, embolia pulmonar (1 e morte súbita (1 e causa desconhecida (3. Reoperações foram realizadas em 28 (18,2% casos, dos quais 2 (1,3% por disfunção de prótese aórtica. Sopro sistólico residual esteve presente em 48% dos casos. Complicações tardias: embolias sistêmicas 5,8% (1/3 como prótese aórtica, endocardite infecciosa 1,3% e embolia pulmonar 0,7%. Classe funcional pós-operatória (p. a. foi I - II em 84% e III - IV em 16%; índice cardiotorácico p. o. 0,58 ± 0,10. Probalidade atuarial de sobrevida tardia é estimada em 79,5 ± 5,3% aos 10 anos e 71,0 ± 7,4% aos 14 anos. Sobrevida sem eventos: 67,9 ± 8,9% aos 10 anos e 56,1 ± 11,7% aos 14 anos. A insuficiência mitral reumática pode ser tratada efetivamente por anuloplastia

  2. Characterization of natural bentonite by NMR; Caracterizacao de bentonitas naturais por ressonancia magnetica nuclear

    Energy Technology Data Exchange (ETDEWEB)

    Leite, Sidnei Q.M.; Dieguez, Lidia C [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia; Menezes, Sonia M.C. [PETROBRAS, Rio de Janeiro, RJ (Brazil). Centro de Pesquisas; San Gil, Rosane A.S. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Inst. de Quimica

    1994-12-31

    Solid state NMR as well as several other instrumental chemical analysis techniques were used in order to characterize two natural occurring bentonite. The methodology is described. The NMR spectra, together with the other used techniques suggest that the observed differences are due to iron inclusions in tetrahedral and octahedral sites 5 refs., 3 figs., 5 tabs.

  3. Comparison of three techniques for skin total irradiation with electrons; Comparacao de tres tecnicas de irradiacao total da pele com eletrons

    Energy Technology Data Exchange (ETDEWEB)

    Batista, Delano V.S., E-mail: dbatista@ird.gov.b [Instituto de Radioprotecao e Dosimetria (IRD/CNEN-RJ), Rio de Janeiro, RJ (Brazil); Instituto Nacional de Cancer (INCa), Rio de Janeiro, RJ (Brazil); Bardella, Lucia H. [Instituto Nacional de Cancer (INCa), Rio de Janeiro, RJ (Brazil); Rosa, Luiz A.R. da, E-mail: lrosa@ird.gov.b [Instituto de Radioprotecao e Dosimetria (IRD/CNEN-RJ), Rio de Janeiro, RJ (Brazil)

    2011-10-26

    This paper compared three techniques of skin total irradiation with electrons: 1) horizontal positioning, 2) vertical positioning - rotatory technique and 3) vertical positioning - six fields technique. For that, a anthropomorphic phantom was positioned according to the recommendation for each technique and was i radiated at the linear accelerator by using the 6 MeV electrons. Radiochromic films were positioned on the surface in various regions of the phantom for measurement of absorbed dose. A ionization chamber was positioned inside of equivalent issue plates for dose evaluation due to the photons produced by electron stopping. The technique 2 and 3 have shown too similar in the results and number or discrepant points (8 and 10 respectively) of prescription lower than the technique 1 (22 points). The total body dose of photons of the 1, 2 and 3 techniques was 2.2%, 5.3% and 5.2% respectively

  4. Estratégia de análise da qualidade de madeira de Eucalyptus sp. para produção de celulose A laboratory technique to establish Eucalyptus sp. wood quality for kraft pulp production

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    José Lívio Gomide

    2004-06-01

    Full Text Available Estudou-se uma nova técnica laboratorial de análise de qualidade da madeira de Eucalyptus sp. para produção de polpa celulósica kraft. A técnica consiste em realizar, simultaneamente, quatro cozimentos de cavacos utilizando diferentes cargas de álcali ativo para estabelecer a característica de deslignificação da madeira. Pelo uso de equações de regressão, calcula-se o álcali ativo necessário para obter o número kappa desejado, o rendimento, a viscosidade e álcali consumido para o kappa objetivo. Os estudos estatísticos evidenciaram que uma única batelada de quatro cozimentos é suficiente, não sendo necessário realizar repetições.A new laboratory technique was tested to determine Eucalyptus sp. wood quality for kraft pulp production. This technique consists in performing four cooks simultaneously using different active alkali charges to establish the wood delignification characteristics. Based on regression equation it is possible to determine the alkali charge necessary to obtain a desired kappa number and the yield, viscosity and the alkali consumed for the target kappa. Statistical analysis demonstrated that a set of four cooks without replication is sufficient to determine the wood quality characteristics.

  5. Técnicas em cirurgia bariátrica: uma revisão da literatura = Bariatric surgery techniques: a literature review

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    Zeve, Jorge Luiz de Mattos

    2012-01-01

    Full Text Available Introdução: A obesidade é uma condição clínica crônica de etiologia multifatorial cujo fracasso no tratamento clínico e terapêutico levam a necessidade de uma intervenção mais eficaz, a cirúrgica. As cirurgias bariátricas podem modificar apenas o estômago, a fim de reduzir o espaço para o alimento e promover a sensação de saciedade, ou em complemento o intestino delgado, visando uma diminuição do local para absorção de nutrientes. Objetivo: Revisar as técnicas de intervenção em cirurgia bariátrica utilizadas no mundo atual, no intuito de compreender as decisões do cirurgião no que diz respeito à escolha das mesmas, tendo por base comparações dessas técnicas. Materiais e Métodos: Realizou-se estudo exploratório tipo revisão bibliográfica nas bases de dados SciELO, LILACS, PubMed, Bireme, sob os seguintes indexadores: técnicas em cirurgia bariátrica, derivação biliopancreática, gastroplastia vertical com bandagem, banda gástrica ajustável, gastrectomia vertical, cirurgia de derivação gástrica, derivações gástricas em Y de Roux, derivação biliopancreática com gastrectomia vertical e preservação pilórica. Resultados: De 66 referências relativas às técnicas em cirurgia bariátrica analisadas, 40 foram selecionadas entre capítulos de obras bibliográficas, consensos, revisões sistemáticas, meta-análises, estudos clínicos randomizados e controlados. Foram revisadas técnicas cirúrgicas para tratamento da obesidade classificadas como: restritivas, predominantemente restritivas e mal absortivas. Conclusão: Atualmente, diferentes técnicas cirúrgicas no tratamento da obesidade são reconhecidas e recomendadas no mundo inteiro. A escolha da técnica pelo cirurgião irá se basear em informações sobre seu mecanismo de funcionamento, resultados e riscos, que podem ser obtidas através de relevantes publicações científicas

  6. THE NOVELS ULYSSES AND TUTUNAMAYANLAR IN POINT OF STREAM OF CONSCIOUSNESS TECHNIQUE / ULYSSES ve TUTUNAMAYANLAR’DA BİLİNÇ AKISI TEKNİĞİ

    Directory of Open Access Journals (Sweden)

    Dr. Serdar ODACI

    2009-01-01

    Full Text Available By the modernism in novel, to introduce the innerworld of characters, stream of consciousness is used as anew narration technique. James Joyce has used identicalexamples of stream of consciousness technique inUlysses. The novel Tutunamayanlar written by Oğuz Atayhas an important position for Turkish novel. This novelbelonged to the writer who had followed the way modernism in Turkish literature. In this study these twonovels are examined in point of stream of consciousnesstechnique.

  7. Recuperação da topografia de ovos por meio da técnica de moiré e calibração independente Eggs' topography recovery by means of the moiré technique and by an independent calibration

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    Gleice C. de A. e Silva

    2011-04-01

    Full Text Available A recuperação da topografia de ovos por meio de análise de imagens digitais permite, de forma não destrutiva, a estimativa das massas da gema, da clara, da casca e totais, que são produtos amplamente utilizados na esfera industrial. O presente trabalho buscou desenvolver uma metodologia para a recuperação da forma tridimensional de ovos por meio de análise de imagens, em especial usando a técnica de moiré. Foram utilizados ovos de diferentes tamanhos, classificados em: XL (mais de 73 g, L (63 a 73 g, M (53 a 63 g e S (até 53 g. Em cada teste realizado em laboratório, um ovo, aleatoriamente selecionado, foi iluminado com a projeção de grades, e as imagens foram capturadas e processadas para a obtenção da forma tridimensional do objeto pela técnica de moiré (TM. As dimensões dos seus eixos principais foram medidas por meio de um paquímetro, sendo usadas como referência para calibração da TM. Equações empíricas foram ajustadas para a correção das dimensões, apresentando coeficiente de determinação de 0,961; 0,955 e 0,988. A TM mostrou-se adequada para a recuperação da topografia de ovos, proporcionando erros menores ou iguais a 5,47%, com a clara necessidade de uma calibração independente, nas três dimensões, e sem a necessidade de usar um objeto calibrador.The recovery of the topography of eggs using digital images analysis allows the prediction with a non-destructive and with a non-contact way of the egg mass, yolk, egg white, and eggshell, which are products widely used in the industrial sphere. The present research seeks to develop a methodology to recovery the tridimensional shape of eggs through image analysis, in particular by the moiré technique with the proposition of an independent calibration. For the accomplishment of this research, eggs of different sizes classified in XL (more than 73g, L (63 to 73g, M (53 to 63 g, and S (until 53 g were used. In each test realized at the laboratory, one egg

  8. Técnicas para avaliação da consolidação de suspensões cerâmicas com o uso de diferentes ligantes Techniques for setting evaluation of ceramic suspensions with different binders

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    I. R. Oliveira

    2007-06-01

    Full Text Available O desenvolvimento de concretos refratários avançados exige uma otimização simultânea das propriedades reológicas (fluidez e trabalhabilidade e do tempo de desmoldagem desses materiais. Geralmente, tais propriedades, bem como as variáveis que as influenciam, são avaliadas diretamente no concreto refratário por meio de medidas de fluidez e da resistência mecânica. Tal procedimento demanda tempo e limita a investigação sobre todas as possíveis combinações de variáveis que podem influenciar o mecanismo de consolidação a partir de diferentes agentes ligantes. Neste contexto, esse trabalho tem como objetivo apresentar técnicas alternativas que podem facilitar a avaliação da consolidação de suspensões cerâmicas com o uso de diferentes ligantes, correlacionando propriedades macroscópicas como trabalhabilidade e o tempo de desmoldagem de concretos refratários. Tais técnicas consistem em medidas de condutividade elétrica, da temperatura, dos módulos de armazenamento (G' e de perda (G" dos materiais (ensaios reológicos oscilatórios, e da resistência do material a uma deformação axial imposta (ensaios reológicos de força normal.The development of advanced refractory castables demands a simultaneous optimization of rheological properties (fluidity and workability and the time for demolding. Generally, such properties and the variables that influence them, (temperature and additives are directly evaluated in the refractory castable. Nevertheless, such procedure demands time and limits the investigation related to the variables that can influence the suspensions consolidation mechanism. In this context, the objective of this work is to present alternative techniques that could better evaluate the setting of ceramic suspensions containing different binders. The results obtained can be correlated with castable macroscopic properties such as workability and demolding time. These techniques comprise the measurements of

  9. Study of Rn-222 exhalation in phosphogypsum through the adsorption technique in activated coal; Estudo da exalacao de Rn-222 em fosfogesso por meio da tecnica de adsorcao em carvao ativado

    Energy Technology Data Exchange (ETDEWEB)

    Nisti, Marcelo Bessa; Campos, Marcia Pires de, E-mail: mbnisti@ipen.b, E-mail: mpcampos@ipen.b [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2011-10-26

    The radon exhalation was estimated through the adsorption in activated carbon technique. Classified as TENORM, the radon exhalation determination on the phosphogypsum piles was performed through the adsorption ratio of radon in activated carbon, from the concentration of descendants of {sup 222}Rn, {sup 214}Pb and {sup 214}Bi obtained by gamma spectrometry. The results obtained in this work were compatibles with the values found in the literature

  10. Preparation and characterization of bentonite organo clay; Preparacao de caracterizacao de argilas bentonitas organofilicas

    Energy Technology Data Exchange (ETDEWEB)

    Bertagnolli, C.; Almeida Neto, A.F. [Universidade Estadual de Campinas (UNICAMP), SP (Brazil). Fac. de Engenharia Quimica. Lab. de Engenharia Ambiental; Silva, M.G.C., E-mail: meuris@feq.unicamp.b [Universidade Estadual de Campinas (UNICAMP), SP (Brazil). Fac. de Engenharia Quimica

    2009-07-01

    Bentonite clays organically modified have great potential use for environmental remediation, especially in the separation of organic compounds from the water. The aim of this work was the preparation of organophilic clays from 'Verde-Lodo' bentonite clay with the quaternary ammonium salts cetyl-pyridinium chloride and benzalkonium chloride. The materials obtained were characterized by XRD, thermogravimetric analyses, Helium picnometry, SEM and energy dispersive X-ray techniques. The results show consistently successful synthesis of the organoclay through the increase in the basal spacing, as well as salt elimination picks and presence of carbon and chlorine in the modified clays; they are inexistent elements in the natural clay. (author)

  11. Tratamento dos desarranjos da articulação radio-ulnal distal pela técnica de Sauvé-Kapandji. Resultados preliminares Treatment of the distal radioulnar articulation disorders by the Sauvé-Kapandji technique

    Directory of Open Access Journals (Sweden)

    Nilton Mazzer

    2001-03-01

    Full Text Available Foi realizado um estudo retrospectivo de 10 casos de desarranjo da articulação radio-ulnal distal tratados pela técnica de Sauvé-Kapandji. Os desarranjos eram resultantes de trauma (7, degeneração (2 e doença congênita (1 e as principais queixas pré-operatórias eram a dor, limitação da prono-supinação e deformidade. A idade média dos pacientes na época da operação era de 37,8 anos. Os pacientes foram submetidos a avaliação clínico-funcional e radiografica com um seguimento pós-operatório médio de 28,3 meses, particular atenção tendo sido dada a uma incidência radiográfica anteroposterior sob esforço de preensão manual. Todos os pacientes obtiveram melhora de suas queixas e o resultado final foi considerado satisfatório (excelente e bom em 8, e insatisfatório (regular 2. A artrodese da articulação radio-ulnal consolidou em 9 casos, independentemente do tipo de fixação empregado. O exame radiográfico sob esforço mostrou que todos os pacientes apresentavam deslocamento radial da ulna, mas isso aparentemente não interferiu com a função. Concluiu-se que a técnica de Sauvé-Kapandji é eficiente para o tratamento dos desarranjos da articulação radio-ulnal distal, pois ela não implica em perda funcional importante.A retrospective study of 10 cases of derrangement of the distal radioulnar joint treated with the technique of Sauvé-Kapandji was carried out. Derrangements resulted from trauma (7, degeneration (2 and congenital disease (1 and the main preoperative complaints were pain, limitation of pronation and supination and deformity. The patients' average age by the time of the operation was 37.8 years (range: 19 - 68 years. All were submitted to clinical, functional and radiographic evaluation at 28.3 months after the operation on average, particular attention being paid to an anteroposterior X-ray view with the hand in a moderate hand grip effort. All patients improved from their complaints and the final

  12. Citologia de impressão da superfície ocular: técnica de exame e de coloração Impression cytology of the ocular surface: examination technique and staining procedure

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    Jeison de Nadai Barros

    2001-04-01

    Full Text Available Objetivo: Apresentar uma técnica de exame e de coloração de amostras de citologia de impressão da superfície ocular desenvolvida em serviço de referência. Método: Obtiveram-se 28 amostras de citologia de impressão de pacientes com alterações da superfície ocular no Setor de Doenças Externas Oculares no período de julho a novembro de 1999. Coraram-se e avaliaram-se as amostras microscopicamente no Laboratório de Microbiologia Ocular, do Departamento de Oftalmologia da Universidade Federal de São Paulo - Escola Paulista Medicina. Resultados: Desenvolveu-se um modelo de papel de filtro com ápice, base e abertura lateral, que forneceu seu posicionamento correto no olho no momento da colheita e na lâmina para a fixação e coloração. A técnica de coloração descrita, que usa ácido periódico-Schiff, hematoxilina e Papanicolaou, é um procedimento econômico e fácil, cora as células caliciformes de róseo e as epiteliais de roxo. Conclusões: A técnica de exame mostrou-se ideal na avaliação celular das amostras de citologia de impressão. A citologia de impressão é um método bastante confiável para o estudo da superfície ocular, no acompanhamento da evolução de patologias externas, e provou ser um procedimento realmente simples, mais barato e mais confortável para o paciente que as biópsias invasivas.Purpose: To present an examination technique and to standardize the staining procedure of samples of impression cytology of the ocular surface in a reference service. Methods: 28 samples of impression cytology were obtained from patients with ocular surfaces alterations of the External Eye Diseases Sector in the period of July to November 1999. They were stained and microscopically evaluated in the Ocular Microbiology Laboratory of the Federal University of São Paulo. Results: We developed a design of a filter paper with apex, base and lateral opening that promoted its adequate position both in the eye at collection

  13. Bio-inspired synthesis and characterization of superparamagnetic particles; Sintese e caracterizacao bioinspirada de particulas superparamagneticas

    Energy Technology Data Exchange (ETDEWEB)

    Castro, Vinicius F., E-mail: vfc_mg@yahoo.com.br [Universidade Federal de Itajuba (UNIFEI), MG (Brazil); Queiroz, Alvaro A.A. [Universidade Federal de Itajuba (UNIFEI), MG (Brazil). Centro de Estudos e Inovacao em Materiais Biofuncionais Avancados

    2012-08-15

    This paper discusses the bio-inspired synthesis of type YFeAl ferrites encapsulated into polyglycerol dendrimers (PGLD) generation 3. The structure and morphological properties of the system YFeAl/PGLD was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The magnetic properties were studied through the techniques of Moessbauer spectroscopy and magnetization. The cytotoxicity of the nanoparticles encapsulated in dendrimers PGLD G3 at the cell membrane was studied against mammalian cell line CHO.K1 measuring the amount of lactate dehydrogenase (LDH) released by the cell damage. Microscopy TEM and XRD analysis indicate that spherical nanoparticles were obtained highly crystalline and monodisperse with size 20 nm

  14. A methodology for semiautomatic taxonomy of concepts extraction from nuclear scientific documents using text mining techniques; Metodologia para extracao semiautomatica de uma taxonomia de conceitos a partir da producao cientifica da area nuclear utilizando tecnicas de mineracao de textos

    Energy Technology Data Exchange (ETDEWEB)

    Braga, Fabiane dos Reis

    2013-07-01

    This thesis presents a text mining method for semi-automatic extraction of taxonomy of concepts, from a textual corpus composed of scientific papers related to nuclear area. The text classification is a natural human practice and a crucial task for work with large repositories. The document clustering technique provides a logical and understandable framework that facilitates the organization, browsing and searching. Most clustering algorithms using the bag of words model to represent the content of a document. This model generates a high dimensionality of the data, ignores the fact that different words can have the same meaning and does not consider the relationship between them, assuming that words are independent of each other. The methodology presents a combination of a model for document representation by concepts with a hierarchical document clustering method using frequency of co-occurrence concepts and a technique for clusters labeling more representatives, with the objective of producing a taxonomy of concepts which may reflect a structure of the knowledge domain. It is hoped that this work will contribute to the conceptual mapping of scientific production of nuclear area and thus support the management of research activities in this area. (author)

  15. MICROBIOLOGICAL EVALUATION OF EGG SHELL POWDER AND OPTIMIZATION OF ITS PREPARATION TECHNIQUE AVALIAÇÃO MICROBIOLÓGICA DO PÓ DA CASCA DE OVO E OTIMIZAÇÃO DA TÉCNICA DE ELABORAÇÃO DO PRODUTO

    Directory of Open Access Journals (Sweden)

    Maria Margareth Veloso Naves

    2007-09-01

    Full Text Available

    The objective of this research was to analyze the microbiological profile of hen egg shell powder distributed to poor communities as an alternate calcium source, and optimizing powder preparation technique through efficient hygiene and sanitary safety. The sampling was carried out in the distribution units of Pastoral da Criança program of the Catholic Church, in Goiânia municipality, Brazil. Ten egg shell powder samples were collected in the preparation places of product, at different moments during September to December 2001. It was observed that some samples presented considerable levels of aerobic mesophilic, total coliforms (at 35C, and moulds and yeasts, but not contamination with thermotolerant coliforms (at 45C, Staphylococcus aureus, Bacillus cereus, and Salmonella sp. Egg shell powder produced through the standard technique, which included essentially washing egg shells, immersion in chlorinated solution, boiling, drying, and milling process, did not show contamination by microorganisms. It was concluded that the optimized technique assures process efficiency and hygienic and sanitary quality for the product.

    KEY-WORDS: Calcium; food microbiology; food analysis; food contamination.

    A pesquisa teve o objetivo de analisar o perfil microbiológico do pó da casca de ovo de galinha distribuído a comunidades carentes, como fonte alternativa de cálcio, bem como otimizar a técnica de elaboração do produto, visando eficácia e segurança em termos higiênico-sanitários. A amostragem foi realizada em unidades de distribuição do programa Pastoral da Criança, da Igreja Católica, em Goiânia-GO, Brasil. Foram coletadas dez amostras do pó da casca de ovo, nos locais de produção e em diferentes momentos, nos meses de setembro a dezembro de 2001. Os resultados revelaram que

  16. Effect of gamma radiation on the growth of Aspergillus Flavus aflatoxins producer and on the use of polymerase chain reaction technique (PCR) in samples of maize grains artificially inoculated; Efeitos da radiacao gama no crescimento de Aspergillus flavus produtor de aflatoxinas e no emprego da tecnica da Reacao em Cadeia da Polimerase (RCP) em amostras de graos de milho inoculadas artificialmente

    Energy Technology Data Exchange (ETDEWEB)

    Aquino, Simone

    2003-07-01

    The aim of this present study was to verify the effects of gamma radiation on the growth of Aspergillus flavus Link aflatoxins producer; to demonstrate the application of Polymerase Chain Reaction (PCR) technique in the diagnostic of A. Flavus, as well to verify the effect of radiation in the profile of DNA bands. Twenty samples of grains maize with 200 g each were individually irradiated with 20 kGy, to eliminate the microbial contamination. In following, the samples were inoculated with an toxigenic A. flavus (1x10{sup 6} spores/ml), incubated for 15 days at 25 deg C with a relative humidity of around 97,5% and irradiated with 0, 2; 5 and 10 kGy. The samples, 5 to each dose of irradiation, were individually analyzed for the number of fungal cells, water activity, viability test (fluorescein diacetate and ethidium bromide), PCR and aflatoxins (AFB) detection. The results showed that the doses used were effective in reducing the number of Colony Forming Units (CFU/g) mainly the doses of 5 and 10 kGy. In addition, the viability test showed a decrease of viable cells with increase of irradiation doses. The reduction of AFB{sub 1} and AFB-2, was more efficient with the use of 2 kGy in comparison with the dose of 5 kGy, while the dose of 10 kGy, degraded the aflatoxins. Thereby, it was observed that AFB2 showed to be more radiosensitive. The use of PCR technique showed the presence of DNA bands, in all samples. (author)

  17. Physico-chemical characterization of human recombinant follicle-stimulating hormone (hFSH) and its subunits by reversed-phase high-performance liquid chromatography ( RP-HPLC): comparison with pituitary hFSH reference preparation from 'National Hormone and Pituitary Program' from USA; Caracterizacao fisico-quimica da foliculotropina humana(hFSH) recombinabte e de suas subunidades, por cromatografia liquida de alta eficiencia (HPLC) em fase reversa: comparacao com a preparacao de referencia de hFSH de origem hipofisaria do ''National Hormone and Pituitary Program'' dos EUA

    Energy Technology Data Exchange (ETDEWEB)

    Loureiro, Renan Fernandes

    2006-07-01

    A reversed-phase high-performance liquid chromatography (RP-HPLC) method for the qualitative and quantitative analysis of intact human folliclestimulating hormone (hFSH) was established and validated for accuracy, precision and sensitivity. Human FSH is a dimeric glycoprotein hormone widely used as a diagnostic analyte and as therapeutic product in reproductive medicine. The technique developed preserves the protein integrity, allowing the analysis of the intact heterodimeric form rather than just of its subunits, as it is the case for the majority of the conditions currently employed. This methodology has also been employed for comparing the relative hydrophobicity of pituitary, urinary and two Chinese hamster ovary (CHO)-derived hFSH preparations, as well as of two other related glycoprotein hormones of the anterior pituitary: human thyroid-stimulating hormone (hTSH) and human luteinizing hormone (hLH). The least hydrophobic of the three glycohormones analyzed was hFSH, followed by hTSH and hLH. A significant difference (p<0.005) was observed in t{sub R} between the pituitary and recombinant hFSH preparations, reflecting structural differences in their carbohydrate moieties. Two main isoforms were detected in urinary hFSH, including a form which was significantly different (p<0.005) for the pituitary and recombinant preparations. The linearity of the dose-response curve (r = 0.9965, n = 15) for this RP-HPLC methodology, as well as an inter-assay precision with relative standard deviation less than 4% for the quantification of different hFSH preparations and a sensitivity of the order of 40 ng, were demonstrated. The chromatographic behavior and relative hydrophobicity of the individual subunits of the pituitary and recombinant preparations were also analyzed. Furthermore, the accurate molecular mass of the individual hFSH subunits and of the heterodimer were simultaneously determined by matrix-assisted laser desorption ionization time-of-flight mass spectral

  18. Determinação das perdas endógenas e da digestibilidade ileal da proteína e dos aminoácidos em suínos utilizando-se duas técnicas Use of different techniques to determine endogenous losses and ileal digestibility of protein and amino acids for swine

    Directory of Open Access Journals (Sweden)

    Leidimara Feregueti Costa

    2008-07-01

    Full Text Available Objetivou-se neste estudo determinar os coeficientes de digestibilidade ileal verdadeira da proteína e dos aminoácidos digestíveis de um extrato protéico de levedura utilizando-se duas técnicas - dieta isenta de proteína (DIP e dieta com caseína hidrolisada enzimaticamente (CHE - para determinação das perdas endógenas de proteína, aminoácidos e nitrogênio. Foram utilizados 12 suínos mestiços, machos castrados, com peso médio de 35 kg, submetidos previamente a cirurgia para implantação da cânula T simples. O delineamento experimental foi o inteiramente casualizado com três tratamentos (dieta com CHE; dieta isenta de proteína (DIP; e dieta com 23% do extrato protéico de levedura - ingrediente teste, quatro repetições e um animal por unidade experimental. As perdas endógenas de ácido glutâmico, ácido aspártico, lisina, arginina e serina diferiram entre as dietas; os maiores valores foram obtidos nos animais que receberam a dieta com CHE. O maior valor de perda endógena do aminoácido glicina foi determinado nos animais alimentados com a dieta DIP. Os coeficientes de digestibilidade ileal verdadeira de metionina, treonina, triptofano e serina determinados pelas perdas endógenas utilizando-se a dieta CHE foram superiores àqueles determinados utilizando a dieta DIP. As quantidades das secreções protéicas e de aminoácidos obtidas pela técnica da CHE foram maiores que as determinadas pela técnica da DIP. Os coeficientes de digestibilidade verdadeira da proteína foram menores e os dos aminoácidos, maiores, quando determinados pela técnica CHE.The objective of this study was to determine the true ileal digestibility coefficients of the protein and digestible amino acid of a yeast protein extract using two techniques - diet without protein (DIP and diet with enzime-hydrolysed casein (CHE - for the determination of protein amino acid and nitrogen losses. Twelve half-breed barrows were used, with average weight of 35

  19. The use of environmental monitoring as a technique to identify isotopic enrichment activities; O uso da monitoracao ambiental como tecnica de identificacao de atividades de enriquecimento isotopico

    Energy Technology Data Exchange (ETDEWEB)

    Buchmann, Jose Henrique

    2000-07-01

    The use of environmental monitoring as a technique to identify activities related to the nuclear fuel cycle has been proposed, by international organizations, as an additional measure to the safeguards agreements in force. The elements specific for each kind of nuclear activity, or nuclear signatures, inserted in the ecosystem by several transfer paths, can be intercepted with better or worse ability by different live organisms. Depending on the kind of signature of interest, the anthropogenic material identification and quantification require the choice of adequate biologic indicators and, mainly, the use of sophisticated techniques associated with elaborate sample treatments. This work demonstrates the technical viability of using pine needles as bioindicators of nuclear signatures associated with uranium enrichment activities. Additionally, it proposes the use of a technique widely diffused nowadays in the scientific community, the High Resolution Inductively Coupled Plasma Mass Spectrometer (HR-ICP-MS), to identify the signature corresponding to that kind of activities in the ecosystem. It can be also found a description of a methodology recently being applied in analytical chemistry,based on uncertainties estimates metrological concepts, used to calculate the uncertainties associated with the obtained measurement results. Nitric acid solutions with a concentration of 0.3 mol.kg{sup -1}, used to wash pine needles sampled near facilities that manipulate enriched uranium and containing only 0.1 {mu}g.kg{sup -1} of uranium, exhibit a {sup 235} U: {sup 238} U isotopic abundance ratio of 0.0092{+-}0.0002, while solutions originated from samples collected at places located more than 200 km far from activities related to the nuclear fuel cycle exhibit a value of 0.0074{+-}0.0002 for this abundance ratio. Similar results were obtained for samples collected in different places permit to confirm the presence of anthropogenic uranium and demonstrate the viability of using

  20. Técnica de separação da membrana de Descemet para transplante de células endoteliais da córnea: estudo experimental em coelhos Technique for separating Descemet membrane for corneal endothelial cells transplantation: experimental study in rabbits

    Directory of Open Access Journals (Sweden)

    Daniel Wasilewski

    2010-02-01

    Full Text Available OBJETIVO: Avaliar a porcentagem de dano endotelial induzido por uma técnica cirúrgica para a separação da membrana de Descemet contendo endotélio sadio, analisar a viabilidade e eficácia desta técnica, e avaliar a porcentagem de dano endotelial causado pela inversão da córnea em câmara anterior artificial. MÉTODOS: As córneas de três grupos de 12 coelhos da linhagem Nova Zelândia foram avaliadas. O grupo 1 foi usado como controle; portanto, as córneas foram analisadas após coletadas e trepanadas. O grupo 2 foi analisado após a inversão da córnea (endotélio para cima na posição convexa, montada em câmara anterior artificial, para o cálculo da porcentagem do dano endotelial induzido por esta inversão. O grupo 3 foi avaliado após a separação entre a membrana de Descemet e o estroma com o uso de substância viscoelástica em córneas invertidas e montadas em câmara anterior artificial. O dano endotelial foi avaliado por meio de fotografias digitais tiradas no microscópio após impregnar o endotélio com vermelho de alizarina. Amostras do grupo 3 foram processadas para avaliação histopatológica. RESULTADOS: O grupo 3 (separação viscoelástica apresentou um índice de lesão celular endotelial de 10,06%, o grupo 2 apresentou um índice de 3,58% e o grupo controle um índice de 0,18% de lesão celular endotelial (pPURPOSE: To evaluate the percentage of endothelial cell damage induced during a surgical technique of Descemet's membrane separation containing healthy endothelium, analyze the viability and efficacy of this technique, and evaluate the percentage of endothelial cell damage caused by inversion of the cornea on an artificial anterior chamber. METHODS: The corneas from three groups of 12 New Zealand rabbits were evaluated. The Group one was used as the control, so the corneas were analyzed after collected and trephinated. The Group two was analyzed after inversion of the cornea (endothelial side up at a convex

  1. Investigation of the corrosion resistance of Ti-13Nb-13Zr alloy by electrochemical techniques and surface analysis; Investigacao da resistencia a corrosao da liga Ti-13Nb-13Zr por meio de tecnicas eletroquimicas e de analise de superficie

    Energy Technology Data Exchange (ETDEWEB)

    Assis, Sergio Luiz de

    2006-07-01

    In this work, the in vitro corrosion resistance of the Ti-13Nb-13Zr alloy, manufactured at a national laboratory, and used for orthopedic applications, has been investigated in solutions that simulate the body fluids. The electrolytes used were 0.9 % (mass) NaCl, Hanks' solution, a culture medium (MEM), and the two last electrolytes, without and with addition of hydrogen peroxide. The aim of peroxide addition was to simulate the conditions found when inflammatory reactions occur due to surgical procedures. The corrosion resistance of alloys commercially in use as biomaterials, Ti-6Al-7Nb and Ti-6Al-4V, as well as of the pure titanium (Ti-cp), was also studied for comparison with the Ti-13Nb-13Zr alloy. The corrosion resistance characterization was carried out by electrochemical and surface analysis techniques. The electrochemical tests used were: open circuit potential measurements as a function of tim; potentiodynamic polarization; and electrochemical impedance spectroscopy (EIE). The impedance experimental diagrams were interpreted using equivalent electric circuits that simulate an oxide film with a duplex structure composed of an internal and compact, barrier type layer, and an external porous layer. The results showed that the corrosion resistance is due mainly to the barrier type layer. The titanium alloys and the Ti-cp showed high corrosion resistance in all electrolytes used. The oxides formed on the Ti-13Nb-13Zr, either naturally or during immersion in MEM ar Hank's solution was characterized by X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (MEV). The results showed that the presence of hydrogen peroxide in MEM promotes the growth of the porous layer and incorporation of mineral ions, besides favouring hydroxyapatite formation. The cytotoxicity of the Ti-13Nb-13Zr alloy was also evaluated and it was shown to be non-toxic. (author)

  2. Investigation of the corrosion resistance of Ti-13Nb-13Zr alloy by electrochemical techniques and surface analysis; Investigacao da resistencia a corrosao da liga Ti-13Nb-13Zr por meio de tecnicas eletroquimicas e de analise de superficie

    Energy Technology Data Exchange (ETDEWEB)

    Assis, Sergio Luiz de

    2006-07-01

    In this work, the in vitro corrosion resistance of the Ti-13Nb-13Zr alloy, manufactured at a national laboratory, and used for orthopedic applications, has been investigated in solutions that simulate the body fluids. The electrolytes used were 0.9 % (mass) NaCl, Hanks' solution, a culture medium (MEM), and the two last electrolytes, without and with addition of hydrogen peroxide. The aim of peroxide addition was to simulate the conditions found when inflammatory reactions occur due to surgical procedures. The corrosion resistance of alloys commercially in use as biomaterials, Ti-6Al-7Nb and Ti-6Al-4V, as well as of the pure titanium (Ti-cp), was also studied for comparison with the Ti-13Nb-13Zr alloy. The corrosion resistance characterization was carried out by electrochemical and surface analysis techniques. The electrochemical tests used were: open circuit potential measurements as a function of tim; potentiodynamic polarization; and electrochemical impedance spectroscopy (EIE). The impedance experimental diagrams were interpreted using equivalent electric circuits that simulate an oxide film with a duplex structure composed of an internal and compact, barrier type layer, and an external porous layer. The results showed that the corrosion resistance is due mainly to the barrier type layer. The titanium alloys and the Ti-cp showed high corrosion resistance in all electrolytes used. The oxides formed on the Ti-13Nb-13Zr, either naturally or during immersion in MEM ar Hank's solution was characterized by X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (MEV). The results showed that the presence of hydrogen peroxide in MEM promotes the growth of the porous layer and incorporation of mineral ions, besides favouring hydroxyapatite formation. The cytotoxicity of the Ti-13Nb-13Zr alloy was also evaluated and it was shown to be non-toxic. (author)

  3. Experimental study of natural two-phase flow circulation using a visualization technique; Estudo experimental da circulacao natural bifasica utilizando uma tecnica de visualizacao

    Energy Technology Data Exchange (ETDEWEB)

    Vinhas, Pedro A.M., E-mail: Pedro_mvinhas@poli.ufrj.br [Universidade Federal do Rio de Janeiro (UFRJ), Rio de Janeiro, RJ (Brazil). Dept. de Engenharia Nuclear; Faccini, Jose L.H., E-mail: faccini@ien.gov.br [Instituto de Engenharia Nuclear (IEN/CNEN-RJ), Rio de Janeiro, RJ (Brazil); Su, Jian, E-mail: sujian@lasme.coppe.ufrj.br [Coordenacao dos Programas de Pos-Graduacao em Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Programa de Engenharia Nuclear

    2013-07-01

    This paper presents an experimental study of natural two-phase flow in a circuit that simulates, on a smaller scale, a typical residual heat removal system of passive reactors APWR (Advanced Pressurized Water Reactor). The circuit was formed by a heater, a heat exchanger and piping. The experimental study was the application of a visualization technique, using a high speed camera, for measuring the size and speed of vapor bubbles generated in the heater with different power heating. The camera was positioned in the central region of the pipe connecting the heater to the heat exchanger, where there is a clear passage. The flow of images were processed and analyzed using commercial software that allowed the determination of the length and velocity of the bubbles. The results were then compared with correlations available in literature.

  4. Tratamento artroscópico da luxação acromio-clavicular pelo método "tight rope" (arthrex® Arthroscopic treatment of acromioclavicular joint dislocation by tight rope technique (arthrex®

    Directory of Open Access Journals (Sweden)

    Luis Alfredo Gómez Vieira

    2009-02-01

    Full Text Available OBJETIVO: Apresentar a técnica cirúrgica artroscópica pelo método "Tight Rope" e a avaliação dos resultados com esta técnica no tratamento da luxação acrômio-clavicular aguda. MÉTODOS: entre agosto de 2006 e maio de 2007, 10 ombros de 10 pacientes com luxação acrômio-clavicular aguda foram submetidos a tratamento artroscópcio pela técnica Tight Rope-Arthrex®. O seguimento mínimo foi de 12 meses, com média de 15 meses. A idade variou de 26 e 42 anos com média de 34 anos. Todos os pacientes eram do sexo masculino. Todos os pacientes foram atendidos na fase aguda da lesão sendo avaliados por radiologia simples (série trauma. Os pacientes foram acompanhados semanalmente no primeiro mês e a cada três meses após o procedimento artroscópico. A avaliação clínica foi feita por meio dos critérios da University of Califórnia at Los Angeles (UCLA. RESULTADOS: Todos os pacientes operados agudamente encontravam-se satisfeitos com os resultados do tratamento cirúrgico artroscópico com uma média de 32,5 pontos na escala de avaliação da UCLA. CONCLUSÃO: O tratamento artroscópico da luxação acrômio-clavicular aguda pelo método "Tight Rope" é uma técnica cirúrgica minimamente invasiva que mostrou-se eficiente para o tratamento destas lesões.OBJECTIVE: Presenting the arthroscopic treatment by Tight Rope - Arthrex® system for acute acromioclavicular dislocation and to evaluate results obtained with this procedure. METHODS: Between August 2006 and May 2007, 10 shoulders of 10 patients with acute acromioclavicular dislocation were submitted to arthroscopic repair using the Tight Rope - Arthrex® system. Minimum follow-up was 12 months, with a mean of 15 months. Age ranged from 26 to 42, mean 34 years. All patients were male. Radiology evaluation was made by trauma series x-ray. The patients were assisted in the first month weekly and after three months after the procedure. Clinical evaluation was based on the University

  5. Vigilância da hanseníase em Olinda, Brasil, utilizando técnicas de análise espacial Leprosy surveillance in Olinda, Brazil, using spatial analysis techniques

    Directory of Open Access Journals (Sweden)

    Tiago Lapa

    2001-10-01

    Full Text Available Contribui-se com o sistema de Vigilância Epidemiológica em nível local por meio de análise espacial em razão do predomínio do caráter urbano da hanseníase em nosso meio e por sua distribuição não homogênea - em parte, pela forma de ocupação e transformação do espaço urbano. Trabalha-se o conceito de risco coletivo pela definição de micro-áreas homogêneas mediante o indicador de carência social, verificando-se sua coerência com padrões da distribuição da hanseníase obtidos da base de dados do SINAN para o Município de Olinda no período 1991-96. Para cada estrato, definido segundo níveis semelhantes dos indicadores, foi calculado o coeficiente de detecção médio para o período. Ao exame da associação entre carência social (risco e coeficiente de detecção de hanseníase obteve-se coeficiente de explicação de 66,1% no modelo multiplicativo, acrescido para 84,3% com a variável renda. Para atender à lógica de intervenção, definiram-se estratos de alto, médio e baixo risco nos distritos sanitários e área programática. A construção desses mapas mostrou-se útil a instrumentalizar o planejamento em nível local.In the State of Pernambuco, Brazil, leprosy has been mainly an urban disease, with an uneven geographical distribution related at least partially to the way urban space has been occupied and transformed. Spatial analysis may thus become an important tool to establish an epidemiological surveillance system for leprosy. Homogeneous micro-areas were defined in the city of Olinda through the integration of two databases, the Population Census and SINAN, and through the use of digital maps and geoprocessing techniques. Census tracts were classified according to a social deprivation index (SDI, and micro-area homogeneity was based on similar values for this indicator. Cluster analysis (K-means was used to define cut-offs between strata. The same procedure was repeated using the income variable only

  6. Diagnosis and characterization of operational conditions of electric power systems; Diagnostico e caracterizacao da condicao operacional de sistemas eletricos de potencia

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Christina Courtouke dos [Companhia Paranaense de Energia (COPEL), Curitiba, PR (Brazil); Tiburcio, Julio Cesar [Escola Federal de Engenharia de Itajuba (EFEI), MG (Brazil)

    1995-12-31

    This work presents a methodology for the realtime diagnosis of a power system in permanent regimen for several states and configurations, providing enough information to help the operator in decision making, resulting in a preventive operation. The methodology is presented, as well as the preliminary results. Also presented are the steps to be followed to the practical implementation of the methodology 2 figs., 1 tab., 7 refs.

  7. Isotopic characterization of uranium in soils of the Ipanema National Forest (FLONA-Ipanema); Caracterizacao isotopica de uranio em solos da Floresta Nacional de Ipanema (FLONA-Ipanema)

    Energy Technology Data Exchange (ETDEWEB)

    Silva, F.B.; Marques, F.H., E-mail: fernandobaliani@yahoo.com.br, E-mail: fernando_henrique06@hotmail.com [Laboratorio de Pocos de Caldas (LAPOC/CNEN-MG), Pocos de Caldas, MG (Brazil); Enzweiler, J.; Ladeira, F.S.B., E-mail: Jacinta@ige.unicamp.br, E-mail: fsbladeira@ige.unicamp.br [Universidade Estadual de Campinas (UNICAMP), Campinas, SP (Brazil). Instituto de Geociencias

    2015-07-01

    The National Forest of Ipanema (FLONA) is situated on a geological anomaly, known as 'Domo de Aracoiaba'. The soils of the area include Oxisols, Inceptsols and Alfisols. The amount of uranium and respective isotope activities in a soil depend on the parental rock and on the pedologic processes. The aim of this study was to investigate the activities for uranium isotopes ({sup 238}U, {sup 234}U, {sup 235}U) and the activity ratio (AR) {sup 234}U/ {sup 238}U or secular equilibrium for different soil types of the area collected at horizons A and B. The amount of uranium showed no significant differences for soils generated from alkaline intrusive rocks and sandstone, however, secular equilibrium was observed for Oxisol (RA = 1), while Inceptsol presented RA> 1 and the other soils, Alfisols, presented RA values <1. (author)

  8. Modification and characterization of the AISI 410 martensitic stainless steels surface; Modificacao e caracterizacao da superficie do aco inoxidavel martensitico AISI 410

    Energy Technology Data Exchange (ETDEWEB)

    Bincoleto, A.V.L. [Universidade Federal de Sao Carlos (PPG-CEM/UFSCar), SP (Brazil). Programa de Pos-Graduacao em Ciencia e Engenharia de Materiais; Nascente, P.A.P. [Universidade Federal de Sao Carlos (DEMa/UFSCar), SP (Brazil). Dept. de Engenharia de Materiais

    2010-07-01

    Steam turbines are used in the generation of more than half the electric energy produced in the world nowadays. It is important the study which aims to improve the efficiency by means of the optimization of leaks and of the aerodynamic profiles, as well as to maintain the integrity of the components. The martensitic stainless steels are widely employed due to the combination of their good mechanical properties with higher corrosion resistance. However, their lower wear resistance and their poor tribological behavior limit their use, since they decrease the component life time. In order to evaluate the improvement in the performance of the AISI 410 stainless steel, several process of surface modification were employed. Five samples were produced: the first one was not treated, the second one received liquid nitriding, the third, gas nitriding, the forth, thermal aspersion of tungsten carbide, and the fifth, boronizing. The samples were characterized by optical microscopy, surface microhardness, and X-ray diffractometry. (author)

  9. Characterization of contaminated oil with tritium, from of production of gas tripolar scintillators; Caracterizacao de oleo contaminado com tritio, proveniente da producao de centelhadores tripolares a gas

    Energy Technology Data Exchange (ETDEWEB)

    Potiens Junior, Ademar J.; Marumo, Julio T.; Goes, Marcos M.; Isiki, Vera L.K. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil)

    2001-07-01

    The objective of this work was to develop a methodology to estimate the activity level present in radioactive oil samples. This oil is derived from vacuum pumps used to produce tension protector of electronic equipment in telecommunication area. The method consisted in obtain a calibration curve in counts per minute versus tritium activity. After the equipment calibration it was analyzed 3 batches of radioactive oil samples. (author)

  10. Characterization and improvement gas diffusion layer of low temperature fuel cell; Caracterizacao e aprimoramento da camada difusora de celulas a combustivel de funcionamento a baixa temperatura

    Energy Technology Data Exchange (ETDEWEB)

    Ramos, C.Z.; Dantas, R.; Oliveira, I.S. de; Azevedo, C.M.N.; Pires, M. [Pontificia Univ. Catolica do Rio Grande do Sul (PUC-RS), Porto Alegre, RS (Brazil). Faculdade de Quimica; Canalli, V. [Pontificia Univ. Catolica do Rio Grande do Sul (PUC-RS), Porto Alegre, RS (Brazil). Faculdade de Engenharia

    2006-07-01

    In low temperature fuel cells the main part is the membrane electrode assembly (MEA). The gas diffusion layer is a component of the MEA, being a composite material constituted by carbon powder and polytetrafluoroethylene, used to increases hydrofobicity, fundamental characteristic in water transport into system. In this work methods were adapted with the aim to a better characterization of the diffusion layer by the measuring the following parameter: contact angle and hysteresis; morphology, thickness and porosity. From these characterization results optimized MEAS will be produced to better fuel cell performance. (author)

  11. Kinetic characterization and of recrystallization of the aluminum alloy 6063 after S work hardening treatment; Caracterizacao e cinetica de recristalizacao da liga de aluminio 6063 apos tratamentos termomecanicos

    Energy Technology Data Exchange (ETDEWEB)

    Esposito, Iara Maria

    2006-07-01

    The aluminum 6063 alloy possesses a great industrial interest, presenting characteristics that justify its frequent use, when compared to the other aluminum alloys: the precipitation hardening and high cold work capacity. These alloys present high ductility, that allows their use in operations with high deformation degrees, as the cold work. The objective of this work is to show comparative analysis of the hardness Vickers of the commercial aluminum 6063 alloy, after cold work with different area reduction degree and thermal treatment. Considering the frequent utilization aluminium 6063 alloy, this work studies the characterization and recrystallization of this alloy, after the plastic deformation in different area reduction degrees, thermal treatment and convenient treatment times - Thermo mechanic Treatments. (author)

  12. EPR response characterization of drugs excipients for applying in accident dosimetry; Caracterizacao da resposta RPE dos excipientes dos medicamentos para aplicacao em dosimetria de acidente

    Energy Technology Data Exchange (ETDEWEB)

    Marczewski, Barbara S.; Rodrigues Junior, Orlando; Galante, Ocimar L.; Costa, Zelia M. da; Campos, Leticia L. [Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil)

    2002-07-01

    Some drugs are widely used by the population and can be employed to dose retrospective. The carbohydrates (saccharides), commonly used as excipients in the pharmaceutical industry, produce a quantity of free radicals after gamma irradiation, making them useful for dosimetry in emergency or accident situations that imply in dose evaluation from the materials found nearly or in contact with victims. In general, EPR signal from pulverized pills of some drugs are very complex due to the variety of components in the formulation. Because of this fact, some pharmaceutical excipients identified in the pill composition were also analysed by EPR spectrometry. On the counter drugs were studied: Cebion glucose, AAS, Aspirina, Conmel, Lacto-Purga and sugar substitutive ZeroCal. The excipients were: lactose, amide, anhydrous glucose and magnesium stearate. In some samples the number of radicals produced increased with the dose, showing a linear response for a dose range of interest and an adequate sensibility for dosimetry in accident cases.

  13. Characterization of the Ni-45wt% Ti shape memory alloy rapidly solidified; Caracterizacao da liga Ni-45wt%Ti com efeito de memoria de forma solidificadas rapidamente

    Energy Technology Data Exchange (ETDEWEB)

    Anselmo, G.C.S.; Castro, W.B. de; Araujo, C.J. de, E-mail: walman@dem.ufcg.edu.b [Universidade Federal de Campina Grande (UAEM/UFCG), PB (Brazil). Unidade Academica de Engenharia Mecanica

    2010-07-01

    One important challenge of microsystems design is the implementation of miniaturized actuation principles efficient at the micro-scale. Shape memory alloys (SMAs) have early on been considered as a potential solution to this problem as these materials offer attractive properties like a high-power to weight ratio, large deformation and the capability to be processed at the micro-scale. shape memory characteristics of Ni-45wt%Ti alloy ribbons prepared by melt spinning were investigated by means of differential scanning calorimetry and X-ray. In these experiments particular attention has been paid to change the velocity of cooling wheel from 30 to 50 m/s. Then the cooling rates of ribbons were controlled. The effect of this cooling rate on martensitic transformation behaviors and structure are discussed. (author)

  14. Preparation and characterization of bentonite clays mixture destined to the removal of heavy metals; Preparacao e caracterizacao da mistura de argilas bentoniticas destinadas a remocao de metais pesados

    Energy Technology Data Exchange (ETDEWEB)

    Almeida Neto, A.F. de; Silva, M.G.C. da, E-mail: ambrosio@feq.unicamp.b [Universidade Estadual de Campinas (UNICAMP), SP (Brazil). Fac. de Engenharia Quimica. Dept. de Termofluidodinamica

    2009-07-01

    In this work a mixture was prepared with 50% wt. of the Bofe and Verde-lodo clays. The characterization methods used they were: thermal analyses (TG and DTG), X-ray diffraction, fisissorption of N{sub 2}, scanning electron microscopy and X-ray energy dispersive spectroscopy. The rehearsals of adsorption we accomplished in system of finite bath using as adsorbent the mixture loamy in natura or it mixes calcined. Starting from TG and DTG a thermal treatment was accomplished to 500 deg C of the loamy mixture. Through the results of the copper adsorption, it was verified that mixes loamy it provokes chemical precipitation of the copper while the calcined sample presents amount metal adsorbed around 7.31 mg of copper/g of adsorbent. The value of removal percentage obtained by the calcined sample it was of 63.02%. (author)

  15. Esterification and characterization of lignin aiming the synthesis of polymeric composite; Esterificacao e caracterizacao da lignina visando a sintese de compositos polimericos

    Energy Technology Data Exchange (ETDEWEB)

    Victor, Priscilla A.; Machado, Fabricio, E-mail: fmachado@unb.br [Universidade de Brasilia (UnB), DF (Brazil). Instituto de Quimica; Goncalves, Silvia B., E-mail: silvia.belem@embrapa.br [Embrapa Agroenergia, Parque Estacao Biologica (PqEB), Brasilia, DF (Brazil)

    2015-07-01

    Lignin is a natural polymer derived from lignocellulosic materials with high availability, presenting a huge potential for production of new materials. Due to its complex macromolecular structure, and its low compatibility with styrene, eucalyptus wood-extracted lignin method was esterified with methacrylic anhydride - exhibiting a yield of 64% - in order to ensure homogeneity in the organic phase into the reaction medium. The evaluation of both the natural and esterified lignin through infrared (IR) spectroscopy showed a decrease of the hydroxyl band, characteristic of natural lignin (3200-3400 cm{sup -1}) and an increase of the characteristic ester band (1720 to 1740 cm{sup -1}). According to nuclear magnetic resonance ({sup 1}H NMR) analysis on esterified lignin, intense peaks were observed in the range from 1.7 to 2.05 ppm (-CH{sub 3}) and 5.4 ppm to 6.2 ppm (=CH{sub 2}), related to methacrylic anhydride. According to the thermogravimetric analysis (TGA), the esterified lignin showed a decrease in its thermal stability when compared to natural lignin, exhibiting two main weight losses between 200 °C and 300 °C and in the interval from 550 °C to 800 °C. Comparatively, the esterified lignin also displayed an increase in its glass transition temperature (Tg = 98 °C) for, when compared to natural lignin, whose Tg value was determined to be equal to 91 °C. (author)

  16. Characterization and evaluation of residue 'grits' of the cellulose industry; Caracterizacao e avaliacao do resisduo 'grits' da industria de celulose

    Energy Technology Data Exchange (ETDEWEB)

    Destefani, A.Z.; Santos, M.M.; Holanda, J.N.F. [Universidade Estadual do Norte Fluminense Darcy Ribeiro (LAMAV/CCT/UENF), Campos dos Goytacazes, RJ (Brazil). Lab. de Materiais Avancados

    2010-07-01

    The cellulose industry generates huge amounts of solid waste residue called 'grits'. These wastes have been willing over time in landfills near the mills. However, this type of disposal is not environmentally friendly and can cause degradation and environmental pollution. In addition, environmental legislation increasingly severe and the high costs of landfill have led the search for new alternatives for final disposition of this abundant waste. In this context, this study is to characterize waste grits, generated by the cellulose industry in the region of Aracruz-ES. The residue samples were characterized in terms of chemical composition, X-ray diffraction, particle size distribution and thermal analysis (DTA and TGA). The characterization of the residual 'grits' demonstrated its potential as a feedstock for production of soil-cement bricks. (author)

  17. Consideration on the technical service quality and the Portugal situation; Consideracoes sobre a qualidade tecnica de servico e caracterizacao da situacao em Portugal

    Energy Technology Data Exchange (ETDEWEB)

    Santana, J.; Afonso, Jose [Entidade Reguladora do Sector Electrico (ERSE), XX (Portugal)

    1999-07-01

    This paper presents some considerations on the technical quality of power supply for the consumption and, for the specific characterization of the Portugal electric sector, a summary analysis of the energy production, transport and distribution activities.

  18. Preparation and characterization of bentonite clay for formation of nanocomposites; Preparacao e caracterizacao da argila bentonita para a formacao de nanocompositos PELMD/MMT

    Energy Technology Data Exchange (ETDEWEB)

    Santos, J.J.M.; Silva, B.L.; Araujo, I.J.C.; Medeiros, A.M.; Melo, J.D.D.; Paskocimas, C.A., E-mail: bismarckengmat@hotmail.com [Universidade Federal do Rio Grande do Norte (DEMat/UFRN), Natal, RN (Brazil). Departamento de Engenharia de Materiais

    2011-07-01

    This study we used the linear medium density polyethylene (PELMD) as polymer matrix and introduced, as reinforcement to increase the mechanical and thermal properties, the green bentonite deposit of Boa Vista/PB, rich montmorillonite (MMT), previously characterized by XRD, that passed by three stages of purification. The first stage was to clean by washing and filtering for removal of coarse material (sand and organic matter), followed by an acid attack. In the second, we used the quaternary ammonium surfactant, in order to increase the distance between the layers of MMT, and the third was removed from the wastewater, using absolute ethanol, finishing the purification of process. Then, the clay was introduced into the polymer matrix by polymerization in solution by intercalation and characterized by XRD. The results showed a partial exfoliation, satisfying the increasing properties. (author)

  19. Structural analysis and magmatism characterization of the Major Gercino shear zone, Santa Catarina State, Brazil; Analise estrutural e caracterizacao do magmatismo da zona de cisalhamento Major Gercino, SC

    Energy Technology Data Exchange (ETDEWEB)

    Passarelli, Claudia Regina

    1996-12-31

    This work describes the geometric and kinematic characteristics of the Major Gercino Shear Zone (MGSZ) in the Canelinha-Garcia area. This shear zone is one of the major lineaments that affect all southern Brazilian precambrian terrains. In Santa Catarina State, it separates, along its whole extension, the supracrustal rocks of the Brusque belt (northern part) from the Granitoid belt (southern). This zone is characterized by a regional NE trend and a dextral sense of movement where ductile-brittle structures predominate. The MGSZ is composed of two mylonitic belts separated by granitoid rocks probably associated to the development of the shear zone. Both shear zones show cataclastic to ultra mylonitic rocks, but mylonites and protomylonites conditions at high strain rate. The calc-alkaline granitoids present in the area can be grouped in two granitoid associations with meta to peraluminous affinities. The Rolador Granitoid Association is characterized by grayish porphyritic biotite-monzogranites and the Fernandes Granitoid Association by coarsed-grained to porphyritic pinkish amphibole-syenogranites. The U-Pb and Rb-Sr ages range from 670 to 590 Ma with the Sr{sup 87} / Sr{sup 86} initial ratios suggesting a crustal contribution in the generation of these rocks. The importance of the pure shear component is also emphasized by the results of the Fry method. Many z axes of the strain ellipses are at high angle to the shear foliation. Symmetric porphyroclasts also corroborate this hypothesis. The micaceous minerals formed during the shear development indicate K-Ar ages around 555 {+-} 15 Ma. Brittle reactivations of the shear zone have been placed by K-Ar in fine-fraction materials at Triassic time (215 {+-} 15 Ma.) 220 refs., 107 figs., 18 tabs., 4 maps

  20. Microstructural characterization aluminium alloys from the addition of boron; Caracterizacao microestrutural de ligas de aluminio a partir da adicao de boro

    Energy Technology Data Exchange (ETDEWEB)

    Nunes, A.G.P.; Pipano, T.F.; Mota, M.A.; Mariano, N.A.; Ramos, E.C.T. [Universidade Federal de Alfenas (UNIFAL), Pocos de Caldas, MG (Brazil). Instituto de Ciencias e Tecnologia

    2014-07-01

    In the electrical industry, the aluminum becomes attractive because it has excellent characteristics for transmitting electricity. The liquid aluminum has in its composition transition elements (zirconium, titanium, vanadium and chromium) that interfere negatively on the quality of the product. The addition of aluminum-boron alloys have been used to remove transition metals through the formation of borides, enabling an increase in electrical conductivity. However, no detailed reports of reactions between boron, transition metals and primary aluminum engines. However, the objective is to determine the stoichiometric composition that enables an increase in electrical conductivity of an aluminum alloy. Samples with different concentrations of boron were characterized by optical emission spectrometry, electrical conductivity and X-ray diffraction. The addition of boron in excess reduces the time in the formation of borides, and enable an increase in electrical conductivity. (author)

  1. Licuri fibers characterization after treatment to produce cellulose nanocrystals; Caracterizacao da fibra de licuri apos tratamento para producao de nanocristais de celulose

    Energy Technology Data Exchange (ETDEWEB)

    Castro, E.G.; Oliveira, J.C.; Miranda, C.S.; Jose, N.M., E-mail: elyane_casft@msn.com [Universidade Federal da Bahia (GECIM/UFBA), Salvador, BA (Brazil). Programa de Pos-Graduacao em Engenharia Quimica. Grupo de Energia e Ciencias dos Materiais

    2014-07-01

    Cellulose nanocrystals have been widely studied in the materials area due to their high aspect ratio, which is directly related to a good performance as mechanical reinforcement. Obtaining this nanocrystals from commercial bleached pulps, as eucalyptus, or microcrystalline cellulose is well studied. Trying to find new extraction sources, exploring better the huge variety of Brazil’s natural fibers and giving the opportunity of development to small communities, the present work verifies the influence of two bleaching methodologies, sodium hypochlorite or hydrogen peroxide, on licuri fibers. Previous washing and mercerization steps were performed before bleaching. The product of each step was analysed by: DSC, TGA, XRD, SEM and FTIR. The yield of each step was also calculated. (author)

  2. Use of nuclear magnetic resonance in the characterization of modified clays; Uso da ressonancia magnetica nuclear na caracterizacao de argilas modificadas

    Energy Technology Data Exchange (ETDEWEB)

    Leite, Sidnei Q.M. [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia; Menezes, Sonia M.C. de [PETROBRAS, Rio de Janeiro, RJ (Brazil). Centro de Pesquisas; Gil, Rosane A.S. San [Universidade Federal, Rio de Janeiro, RJ (Brazil). Inst. de Quimica

    1992-12-31

    This work uses NMR spectroscopy with rotation in the {sup 29} Si, {sup 27} Al and {sup 23} Na magic angles for characterization of clays with Si/Al ratio in the range 3.0 - 16,5, obtained by chemical treatment of commercial samples, under different conditions of leaching with mineral acid 5 refs., 2 figs., 2 tabs.

  3. Preparation and characterization of corn reinforced polymer sheet of fibers; Obtencao e caracterizacao de polimero reforcado com fibras da folha de milho

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Tatiana Martinez; Seo, Emilia Satoshi Miyamaru, E-mail: tatianaltda@hotmail.com, E-mail: esmiyseo@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2016-10-15

    There is a global trend in seeking plant fibers to replace the synthetic fibers to obtain reinforced composites aimed at the use of renewable resources. In this context, this paper aims to develop the process of preparing maize leaf fibers, characterizing them and adapting them for applications in the construction industry and develop a reinforced polymer composite with these fibers. Corn leaves were dried in environmental temperature, treated by mercerizing, then neutralized with acid solution and washed in running water. The characterization of the corn leaf fibers was carried out by X-ray diffraction, X-ray fluorescence, scanning electron microscopy, specific surface area, thermogravimetry and specific mass. The mercerizing treatment was effective, because the maize fibers have characteristics similar to synthetic fibers, leading to a possibility of new technological uses. The polymeric composite material was developed by extrusion processes and injection and tested for tensile testing, differential scanning calorimetry and scanning electron microscopy, thus reused an organic waste that would be disposed of by inserting it in a technological process, contributing to the research and development of new polymeric materials as well as to reduce waste discarded as scrap. (author)

  4. Extraction and characterization of cellulose nano whiskers from balsa wood; Extracao e caracterizacao de nanocristais de celulose obtidos da madeira balsa

    Energy Technology Data Exchange (ETDEWEB)

    Morelli, Carolina L.; Bretas, Rosario E.S., E-mail: bretas@ufscar.br [Universidade Federal de Sao Carlos - UFSCar, Sao Carlos, SP (Brazil); Marconcini, Jose M. [Embrapa Instrumentacao, Sao Carlos, SP (Brazil); Pereira, Fabiano V. [Universidade Federal de Minas Gerais - UFMG, Belo Horizonte, MG (Brazil); Branciforti, Marcia C. [Universidade de Sao Paulo - USP, Sao Carlos, SP (Brazil)

    2011-07-01

    In this study cellulose nano whiskers were obtained from balsa wood. For this purpose, fibers of balsa wood were subjected to hydrolysis reactions for lignin and hemi cellulose digestion and acquisition of nano-scale cellulose. Cellulose nano crystals obtained had medium length and thickness of 176 nm and 7 nm respectively. Infrared spectroscopy and x-ray diffraction showed that the process used for extracting nano whiskers could digest nearly all the lignin and hemi cellulose from the balsa fiber and still preserve the aspect ratio and crystallinity, satisfactory enough for future application in polymer nano composites. Thermogravimetry showed that the onset temperature of thermal degradation of cellulose nano crystals (226 degree C) was higher than the temperature of the balsa fiber (215 degree C), allowing its use in molding processes with many polymers from the molten state.(author)

  5. Preparation and characterization of biocellulose membranes obtained by biosynthesis of bacteria komagataeibacter rhaeticus; Preparacao e caracterizacao de membranas de biocelulose obtidas pela biossintese da bacteria komagataeibacter rhaeticus

    Energy Technology Data Exchange (ETDEWEB)

    Machado, Rachel Temperani A. [Centro Universitario de Araraquara (QUIMERA), Araraquara, SP (Brazil). Lab. de Quimica Medicinal e Medicina Regenerativa; Trovatti, Eliane; Ribeiro, Sidney J.L. [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP), Araraquara, SP (Brazil). Instituto de Quimica; Berreta, Andresa A. [Apis Flora LTDA, Ribeirao Preto, SP (Brazil); Tercjak, Agnieszka; Gutierrez, Juncal; Barud, Hernane S., E-mail: hernane.barud@gmail.com, E-mail: hsbarud@uniara.com.br [Group ' Materials + Technologies' (GMT), Department of Chemical and Environmental Engineering, Polytechnic School, University of the Basque Country (UPV/EHU), San Sebastian (Spain)

    2015-07-01

    This work shows preparation and characterization of bacterial cellulose membranes (CB) produced by Komagataeibacter rhaeticus strain, and strain from ATCC bank, Gluconacetobacter hansenii (ATCC 23769) used as a comparative. Physicochemical assay were done, such as Fourier Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD), Scanning Electron Microscopy couplet to Energy-dispersive X-ray spectroscopy (SEM/EDX). SEM images reveled a compact structure formed by cellulose nanofibers. FTIR spectra are shown characteristics bands of cellulosic materials and XRD shows cellulose native structure, type I cellulose. (author)

  6. Characterization of steel grit recovered from ornamental rocks waste by magnetic separation; Caracterizacao da granalha de aco recuperada do residuo de rochas ornamentais por separacao magnetica

    Energy Technology Data Exchange (ETDEWEB)

    Junca, E.; Telles, V.B.; Rodrigues, G.F.; Oliveira, J.R. de; Tenorio, J.A.S., E-mail: eduardojunca@gmail.co [Universidade de Sao Paulo (USP), SP (Brazil). Dept. de Engenharia Metalurgica e de Materiais; Instituto Federal de Ciencia e Tecnologia do Espirito Santo (IFES), Vitoria, ES (Brazil)

    2010-07-01

    The aim of this work is characterization of steel grit recovered from ornamental rock waste by magnetic separation. The magnetic separation was realized in three steps: first, using a high intensity wet magnetic separator, which used only the remaining magnetic field of equipment. In the second step, the magnetic material obtained in the first phase was subjected to a new manual magnetic separation using rare earth magnets. In a third step, magnetic material obtained with rare earth magnets was subjected to manual magnetic separation using ferrite magnets. After the magnetic separation, the material was sent to characterization which was obtained by chemical analysis, scanning electron microscopy, X-ray diffraction and size analysis. The size analysis showed that the concentrate range from 0,5 to 563,67 {mu}m with 4 wt.% over 100 {mu}m and content metallic iron of 93 wt%. (author)

  7. Methodology for the analysis and characterization of the demand side energy resources; Metodologia para analise e caracterizacao dos recursos energeticos do lado da demanda

    Energy Technology Data Exchange (ETDEWEB)

    Baitelo, Ricardo Lacerda; Udaeta, Miguel Edgar Morales [Universidade de Sao Paulo (USP), SP (Brazil). Dept. de Energia e Automacao Eletricas. Grupo de Energia; Burani, Geraldo Francisco; Grimoni, Jose Aquiles Baesso [Universidade de Sao Paulo (USP), SP (Brazil). Inst. de Energia e Eletrotecnica

    2006-07-01

    This abstract aims at describing briefly a model for the assessment of demand side energy resources This model intends to comprehend every kind of action and measure related to demand side management and energy conservation, evaluating them in a holistic way, into four dimensions: technical-economical, environmental, social and political. Different aspects regarding the resources are also accounted, such as energetic potentials (theoretical, accomplishable and economic). At last, scenarios concerning the introduction of evaluated resources through a period of time are elaborated. (author)

  8. Proposta de um instrumento para avaliação da autonomia do idoso: o Sistema Sênior de Avaliação da Autonomia de Ação (SysSen A new technique for elderly independence evaluation: the Senior System (SysSen

    Directory of Open Access Journals (Sweden)

    Paulo de Tarso Veras Farinatti

    2000-12-01

    álidos e suas equações, estáveis. A comparação com outras técnicas de avaliação revela que o SysSen pode ser útil no estudo da autonomia funcional sob uma perspectiva positiva, fato raro quando se trata de instrumentos de avaliação gerontológica.A new technique - Senior System for Action Autonomy Evaluation (SysSen - used to evaluate elderly, and the strategies of its validation is described. The SysSen is composed by a questionnaire (Senior Questionnaire of Physical Activities - QSAP and a field test (Senior 'Walking and Carrying' Test - TSMP. The QSAP is a four-part interview, assessing the necessities for an autonomous life related to upper body strength (FO and cardiorespiratory capacity (PA. The first one considers home, professional, and free time activities. The second observes the environmental context. The third assesses the difficulties to perform day-to-day activities and the feelings of the subjects towards activities they would like to perform/resume. The last part considers the interviewer's point of view on the assessed information. An index for QSAP overall results is obtained (Expressed Autonomy Index - IAE. In the TSMP, subjects walk 800 m the faster they can, carrying weights according to sex. An index for the physical functional potential for activities that depend on FO and PA is calculated (Potential Autonomy Index - IAP. Both indexes are used to determine a ratio between potential and expressed autonomy (IAP/IAE - the Senior Index for Action Autonomy (ISAC. The SysSen validity was verified by comparing its partial and final results with other evaluation techniques, and by the internal and structural consistence of the indices obtained (construct, content, and external validity. Intra-class reliability was determined by test-retest. The stability of IAE and IAP equations was tested by cross validation. Results show that the instrument is valid, and that its equations are stable. Comparison to other evaluation techniques reveals that Sys

  9. Study of the porosity of synthetic sandstones by nondestructive nuclear techniques; Estudo da porosidade de arenitos sinteticos por tecnicas nucleares nao destrutivas

    Energy Technology Data Exchange (ETDEWEB)

    Marques, Leonardo Carmezini

    2008-07-01

    In this paper, nuclear techniques have been used to describe structural characteristics of ceramic samples. These samples were produced to serve as simulates of sandstones and their mainly component was silica (SiO{sub 2}). Three sets of these samples with different characteristics were analyzed with the gamma ray transmission and the X-ray microtomography. They had the function to describe parameters as porosity point to point and total average porosity, for the transmission case, and 2D sections average porosity, total average porosity and size porous distribution for microtomography, as well as to investigate possible irregularities in bulk sample. The experimental set up for the gamma ray transmission technique consisted of: a 2 x 2 crystal NaI(Tl) detector, an {sup 241}Am radioactive source (59.54 keV, 100 mCi), an automatic micrometric table for the sample XZ movement and standard gamma spectrometry electronics. Lead collimators with 2 mm diameter were placed on the source way out and on the detector entrance. The microtomographic measurements were done with a Skyscan system, model 1172, with a X-ray tube with 20-100 kV of voltage range and a CCD camera. Employing gamma ray transmission method was possible to obtain overall porosity values from 25.8 to 34.0 % and from 24.8 to 29.2 % for samples with parallelepiped and cylinder shape, respectively, for ceramic I set; from 58.5 to 61.0 % and from 57.1 to 61.7 % for the same geometric shape of ceramic II set. The samples analyzed by the microtomography achieved resolutions of 1.73 {mu}m, 0.64 {mu}m and 1.28 {mu}m for samples of ceramic set I, II and III, respectively. This methodology provided average total porosity values from 26.6 to 29.4 %, from 48.4 to 51.0 % and from 28.2 to 30.6 % to I, II and III ceramic sets, respectively. The porous size profiles of each ceramic sample were also measured. (author)

  10. Dynamic system for the evaluation of CIM monitoring and control techniques; Sistema dinamico para avaliacao de tecnicas de monitoracao e controle da CIM

    Energy Technology Data Exchange (ETDEWEB)

    Penna, Monica de Oliveira [PETROBRAS, Rio de Janeiro, RJ (Brazil). Centro de Pesquisas (CENPES). Biotecnologia e Ecossistemas]. E-mail: mpena@cenpes.petrobras.com.br; Baptista, Walmar; Brito, Rosane Fernandes de [PETROBRAS, Rio de Janeiro, RJ (Brazil). Centro de Pesquisas (CENPES). Tecnologia de Materiais, Equipamentos e Corrosao]. E-mails: walmar@cenpes.petrobras.com.br; rosanef@cenpes.petrobras.com.br; Silva, Edilson Domingos da; Nascimento, Juliana Rangel do [Fundacao Gorceix, Ouro Preto, MG (Brazil)]. E-mails: edilson@cenpes.petrobras.com.br; julianarn@cenpes.petrobras.com.br; Coutinho, Claudia M.L.M. [Universidade Federal Fluminense (UFF), Niteroi, RJ (Brazil). Inst. de Biologia. Dept. de Biologia Celular e Molecular

    2002-03-01

    In general, the two main problems associated to the water injection system for secondary petroleum recovery are the corrosion control and the decrease in solid injection in the reservoir. Corrosion problems in injection water systems may have abiotic as well as biotic causes, and the occurrence of reservoir plugs can result from the injection of particles (suspended solids as well as corrosion products), bacteria and fouling formation. Due to the need to implement a methodology for the evaluation of abiotic and biotic corrosive processes, monitoring techniques and MIC control in a dynamic system, an apparatus was built that simulates the characteristics of a water injection system. The apparatus allows monitoring and control of the parameters that, when varied, may influence the performance of the quality of the injected water. The dynamic system was designed to simulate as precisely as possible the conditions that allow the SRB and heterotrophic bacteria to create fouling in a water injection system. This article discusses the dynamic system, analytical methods and some preliminary results. (author)

  11. Técnicas da carta-perdida como instrumento de pesquisa social: um estudo sobre preconceito e ajuda The lost letter technique as a social research instrument: a study of prejudice and helping

    Directory of Open Access Journals (Sweden)

    Abelardo Vinagre da Silva

    1998-01-01

    Full Text Available A técnica da carta perdida foi adaptada para o contexto cultural brasileiro. Trezentas cartas endereçadas e seladas, foram colocadas "por engano", simulando perda, nos pára-brisas de veículos em dois estacionamentos. Um bilhete anexo explicava que o autor se desencontrara do amigo, "dono do carro". O bilhete variou, dando a entender que seu autor era masculino ou feminino (fator 1; tinha características pessoais distintas: homossexual, negro ou grupo controle (fator 2; permitindo a possibilidade de contatos telefônicos, ou não (fator 3, num delineamento 2 x 3 x 2. Quem encontrava a carta, podia enviá-la (comportamento pró-social ou descartá-la. Sessenta e um por cento das cartas foram enviadas. Nenhuma diferença significativa foi encontrada em função das características dos três grupos (controle, negro ou homossexual, de gênero, da interação destes fatores. A possibilidade de telefonar para o remetente, aumentou significativamente o envio de cartas. A técnica mostrou-se promissora por possibilitar, enquanto instrumento não-reativo, o estudo de preconceito e ajuda.The lost-letter technique was adapted to the cultural context of Brazil. Three hundred stamped and addressed letters were placed "by accident", i.e., simulating loss, on the wind shields of private cars in two large parking areas. A attached note explained that the author had missed the owner of the car. The note varied such that the author appeared to be either male or female (Factor 1, have certain personal characteristics, such as being black, homosexual, or control group (Factor 2, and allowed for telephone contact or not with the author (Factor 3 in a 2 x 3 x 2 experimental design. The finder of the letter could either (a post the letter (pro-social behavior or (b ignore it. 60.7% of the letters were posted. No significant difference was found in terms of sex or personal characteristics, nor interaction between these two factors. Being able to telephone the

  12. A importância da integração de dados do diagnóstico das hemopatias The importance of integrating results of several techniques in the diagnosis of hematological diseases

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    Irene Lorand- Metze

    2009-01-01

    Full Text Available A análise diagnóstica da medula óssea compreende classicamente a citologia. Mais recentemente, tornou- se rotina o estudo histológico. Desde o início, tentou- se integrar estes dados, pois, enquanto a citologia fornece uma análise mais detalhada das características das células e permite quantificá- las, a biópsia, por analisar o tecido como um todo, permite o estudo da estrutura do tecido hemopoético, seu estroma e a ocorrência de estruturas estranhas à medula, como granulomas, fibrose e metástases de neoplasias. Com o desenvolvimento de novas tecnologias e o melhor conhecimento das diversas entidades, principalmente em onco- hematologia, além do desenvolvimento de terapias alvo- específicas, tornou- se importante o estudo citogenético/molecular em algumas patologias. Nas leucemias agudas e síndromes linfoproliferativas, a imunofenotipagem tem contribuído de modo decisivo para a classificação correta das diversas neoplasias pelos critérios da OMS. Assim, o diagnóstico hematológico se tornou uma atividade multidisciplinar que integra profissionais de diversas especialidades. Assim se consegue tratar os pacientes de modo mais adequado, além de poder rastrear a doença residual após o tratamento. Isto levou a novas definições de remissão: hematológica, fenotípica, citogenética e molecular. O estudo da medula óssea é importante em algumas hemopatias benignas, como anemias carenciais, que podem se manifestar como pancitopenias. Este estudo deve ser complementado com exames sorológicos e bioquímicos. A mielocultura tem permitido o diagnóstico de infecções, especialmente nos indivíduos imunossuprimidos.The diagnosis of hematologic diseases has traditionally been based on features of peripheral blood and bone marrow (BM cytology. Histologic examination of the BM has been used for the staging of neoplasias when aspiration is not possible due to fibrosis. Cytology permits a better evaluation of cell morphology and a

  13. Comparação dos métodos convencional e Filter Bag Technique da Ankom® (FBT para determinação de fibra em detergente neutro e fibra em detergente ácido Comparison of conventional and Ankom’s filter bag technique (FBT methodologies for determining neutral detergent fiber and acid detergent fiber.

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    Geane Dias Gonçalves

    2000-05-01

    Full Text Available Foram analisadas fibra em detergente neutro (FDN e fibra em detergente ácido (FDA pelo método convencional e pela Filter Bag Technique da Ankom® (FBT, reutilizando os filtros F57 por até seis vezes. Para tanto, fez-se uso dos alimentos: milho moído, farelo de trigo, farelo de soja, farelo de canola, feno de tifton 85, feno de aveia, milheto e silagem de milho. O método FBT mostrou-se eficaz para a determinação de FDN e FDA para a maioria dos alimentos. A reutilização dos filtros F57 na FBT é recomendada de acordo com o tipo de alimento a ser testado. Para alimentos como a silagem de milho e o farelo de canola, a reutilização dos filtros poderá ser feita até seis vezes, já para outros alimentos, recomenda-se menor número de reutilizações. A análise da FDN para o milho, na FBT, não é recomendada.Neutral detergent fiber (NDF and acid detergent fiber (ADF concentrations were analyzed by conventional and ANKOM’s filter bag technique methodologies using F57 filter bags for up to six determinations. The feed samples used were: corn grist, wheat middlings, soybean meal, canola meal, tifton 85 hay, rat hay, millet and corn silage. FBT method was effective for NDF and ADF determination for the majority of feed samples. F57 filters reutilization in FBT is recommended in accordance with the tested feed type. For corn silage and canola meal, F57 filters are recommended to be reutilized up to six times, but for other feeds a lower number of reutilizations is recommended. NDF analysis of corn using FBT is not recommended.

  14. Propagação da corticeira do banhado (Erythrina crista-galli L. (FABACEAE pelo processo de estaquia Propagation of swamp corticeira (Erythrina crista-galli L. (Fabacae by the cutting technique

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    Ariane Gratieri-Sossella

    2008-02-01

    Full Text Available A corticeira-do-banhado é uma árvore nativa com uso ornamental no paisagismo urbano e possui potencial de utilização em áreas desprotegidas e degradadas, devido a sua rusticidade. Entretanto, tendo em vista a dificuldade de obtenção de sementes, pela baixa produção e qualidade destas com a conseqüente desuniformidade da germinação, torna-se necessário aprofundar o estudo de outras formas de propagação dessa espécie. Desse modo, conduziu-se este trabalho na Faculdade de Agronomia e Medicina Veterinária da Universidade de Passo Fundo, com o objetivo de estudar a formação de mudas de Erythrina crista-galli L. pela técnica da estaquia. Em quatro experimentos foram testadas doses do fitorregulador ácido indolbutírico (AIB, em diferentes tipos de estacas (lenhosas, semilenhosas, herbáceas e foliares e substratos. Os resultados indicaram que mini-estacas herbáceas, coletadas de plantas jovens, com menos de 1 ano de idade, são as mais indicadas (75% a 100% de enraizamento, e o uso do AIB diminuiu a mortalidade, ao favorecer o processo do enraizamento. Em razão do ataque de insetos (brocas às plantas no seu hábitat, recomenda-se a técnica de jardim clonal, com a formação de matrizeiros no viveiro, fornecendo material juvenil e sadio em maior escala para a propagação dessa espécie por miniestacas.Swamp corticeira is a native tree with ornamental use in urban landscape gardening with the potential to be used in unprotected and degraded areas due to its rustic feature. However, the difficulty of obtaining seeds due to its low productivity and quality, and consequent lack of uniformity in its germination makes it necessary to search for other forms of propagation of this species. Thus, this study was carried out at the Agronomy and Veterinary Medicine College of Passo Fundo University, aiming to study the formation of Erythrina crista-galli L. cuttings by applying the cutting technique. Doses of phytoregulator Indol Butyric

  15. Studies on survival, biological activities and behavior of Biomphalaria glabrata, the host snail of Schistosomiasis, submitted to increased hydrostatic pressure: a technique Estudos sobre a sobrevivência, atividades biológicas e comportamento de Biomphalaria glabrata, hospedeiro intermediário da esquistossomose, submetido a aumento da pressão hidrostática: uma técnica

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    P. Jurberg

    1988-03-01

    Full Text Available To study changes in survival, in biological activities and behavior of planorbids submitted to increased hydrostatic pressure, we developed a technique using two transparent chambers and a hydraulic piston. The apparatus permitted renewal of the liquid medium without substantial variations in pressure, thus eliminating excretion products and maintaining the desired O2 level and thereby permitting us to evaluate the effects of pressure independently of the occurrence of anoxia. Pressure was maintained without any contact of the liquid medium with compressed air, a situation which reproduced with relative fidelity what occurs in nature and assured the presence of the same amounts of gases in the two observation chambers (Control and Experimental. Biomphalaria glabrata was found to be able to survive at least 48 hours when submitted to 49.02 x 10**4 Pa (equivalent to a water depth of 48.8 m, continuing to day egg masses and showing few behavioral changes when compared with the control group.Para estudar mudanças na sobrevivência, atividades biológicas e comportamento de planorbídeos submetidos a aumento de pressão hidrostática, desenvolvemos uma técnica que utiliza duas câmaras transparentes e um pistão hidráulico. O aparelho permitiu a renovação do meio líquido sem variações substanciais na pressão, eliminando assim os produtos de excreção e mantendo o nível de O2 disseolvido desejado, e desse modo permitido-nos avaliar o efeito da pressão independente da ocorrência de anoxia. A pressão foi mantida sem nenhum contato do meio líquido com o ar comprimido, situação que produziu com relativa fidelildade o que ocorre na natureza, e assegurou a presença da mesma quantidade de gases nas duas câmaras de observação. Biomphalaria glabrata foi capaz de sobreviver pelo menos 48 horas quando submetida a 49,02 x 10 Pa (equivalente a 48 m de profundidade continuando a pôr massas ovíferas, e mostrando poucas modifica

  16. O homem público em julgamento: avaliação da aplicação da técnica "tribunal do júri" para dirigentes municipais em Santa Catarina Public figures on trial: an assessment of the use of the "Law Court" technique for city officials in Santa Catarina, Brazil

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    Eleonor Minho Conill

    1998-10-01

    Full Text Available O presente trabalho descreve a aplicação da técnica "tribunal do júri" ao conjunto de secretários municipais de saúde do Estado de Santa Catarina, para fins de sensibilização à questão dos deveres do administrador público, realizado como parte introdutória de um ciclo de formação para dirigentes municipais em 1997. As diferentes etapas que compõem a técnica são descritas apresentando-se a avaliação dos resultados obtidos. Dos 156 participantes, 98% foram favoráveis à inovação por considerá-la dinâmica/participativa (31%; educativa/reflexiva (27% e por traduzir a realidade (24%. A técnica permitiu a discussão das principais temáticas de interesse para o SUS. Embora os cinco tribunais tenham absolvido o réu, a dimensão ética foi referida por 58% como principal atributo necessário ao homem público.This study describes the "Law Court" technique as applied to City Health Departments in the State of Santa Catarina, in dealing with the issue of obligations on the part of public officials. The project was the first part of a training course for public administrators held in 1997. The article presents the technique's components and results. Some 98% of the 156 participants had a positive opinion of the training course, considering it dynamic/participatory (31%, educational/stimulating reflection (27%, and realistic (24%. The technique fostered the discussion of the main subjects pertaining to the country's Unified Health System (SUS. Although all five juries acquitted the defendants, the issue of ethics was reported by 58% of the participants as the main prerequisite for a public administrator.

  17. Efeito da técnica de curtimento e do método utilizado para remoção da pele da tilápia-do-nilo sobre as características de resistência do couro Effect of tanning technique and methods used for skin removal on leather resistance characteristics of Nile Tilapia

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    Maria Luiza Rodrigues de Souza

    2006-08-01

    Full Text Available Um estudo foi realizado com o objetivo de avaliar os efeitos do método de remoção da pele do filé (com alicate e com máquina e da técnica de curtimento (com ou sem sais de cromo, bioleather sobre a resistência da pele de tilápia-do-nilo (Oreochromis niloticus. Foram retiradas as peles de 40 tilápias (450 g, 20 com uso de alicates e 20 com auxílio de máquina. Após o curtimento e a retirada dos corpos-de-prova, as peles foram encaminhadas a um laboratório aclimatizado (23ºC e 50% de umidade relativa do ar para realização dos testes de resistência em dinamômetro EMIC, com velocidade de afastamento entre cargas de 100 ± 20 mm/mm. O método de retirada da pele do filé não afetou os resultados dos testes de tração e rasgamento progressivo. A pele retirada com a máquina apresentou elongação superior (88,48% à removida com alicate (71,09%. Peles curtidas com sais de cromo (25,54 N/mm; 12,18 N/mm² foram mais resistentes que as curtidas sem sais de cromo (bioleather (13,11 N/mm; 9,89 N/mm². Peles curtidas por estas técnicas (com cromo e bioleather podem ser utilizadas na confecção de vestuários, pois as médias dos testes de tração, alongamento e rasgamento progressivo foram superiores a 9,80 N/mm², 60% e 14,72 N/mm, respectivamente, valores mínimos recomendados para couros curtidos ao cromo.This research evaluated the effect of different methods (fillet skin removal and tanning methods [with or without chromium salts and bioleather] on leather resistance characteristics of Nile Tilapia (Oreochromis niloticus. Skin from 40 tilapias (450 g were removed: 20 by pliers and 20 by machine. After skin tanning, the samples were removed for resistance tests, which were done, in a climatized environment (23ºC and 50% air relative humidity, with EMIC dynamometer, at removal speed of 100 ± 20 mm/mm. No effect of fillet skin removal method on progressive tearing and strength was observed. The method of skin removal by machine

  18. Toracoscopia em eqüinos: técnica e emprego como método de avaliação da cavidade pleural Thoracoscopy in horses: technique and its use as pleural cavity evaluation method

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    André Luis do Valle De Zoppa

    2001-10-01

    Full Text Available Toracoscopia é o método de visibilização da cavidade torácica através de endoscópio rígido ou flexível, indicado como exame auxiliar para diagnóstico das diversas afecções do tórax. Pode ser realizada com o animal sob anestesia geral ou em posição quadrupedal através de anestesia local associada ou não a sedativos. Neste trabalho, foram utilizados seis eqüinos hígidos, que foram submetidos a toracoscopia, em posição quadrupedal, nos dois hemitórax, com intervalo de 15 dias entre cada procedimento. Durante o exame, pôde-se observar as diversas estruturas da cavidade torácica, tais como: músculo diafragma (porção muscular e tendínea, hiato esofágico, mediastino, aorta, troncos dorsal e ventral do nervo vago, ducto torácico, veia ázigos, veias intercostais, músculos intercostais, costelas, tronco nervoso simpático, tronco vascular toracocervical, traquéia, pulmão (lobo cranial e caudal, esôfago, pericárdio, veia cava caudal, nervo frênico e linfonodos aórticos. Discretas alterações foram observadas ao exame físico, laboratorial e ultra-sonográfico no período pós-operatório, sem que trouxessem prejuízos ao desenvolvimento do experimento e recuperação do animal. A toracoscopia mostrou ser exame de auxílio importante, pela facilidade, rapidez de execução, ampla visibilização da cavidade pleural e trauma mínimo ao paciente.Thoracoscopy is the technique based upon the thoracic cavity visualization by means of rigid or flexible endoscope. It is indicated as an additional diagnostic aid to better define thoracic diseases. It can be performed either in an animal subjected to general anesthesia or in a horse standing on stocks with local anesthesia with or without sedative. Six healthy horses were used in this study they were subjected to thoracoscopy in both hemithorax, standing on stocks, with a 15-day interval between each procedure. It was possible to visualize several thoracic structures through

  19. Técnica da instilação de colírios em pacientes portadores de glaucoma crônico Eye drop instillation technique in chronic glaucoma patients

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    Paulo Gelman Vaidergorn

    2003-12-01

    Full Text Available OBJETIVO: Verificar a técnica da instilação de colírio em pacientes portadores de glaucoma crônico. MÉTODOS: Estudo prospectivo realizado em 193 pacientes glaucomatosos. Para cada participante era entregue um frasco de colírio lubrificante (Dunason®, Laboratório Alcon, São Paulo, Brasil e solicitado que realizasse uma instilação. RESULTADOS: Os participantes utilizaram, em média, 1,64 ± 1,26 gotas de colírio por instilação e 54,5% dos pacientes fizeram contato do bico do colírio com a superfície ocular. Em 3,1% das instilações nenhuma gota de medicamento atingiu o olho, com o paciente não se dando conta do fato. A oclusão do ponto lacrimal ou a manutenção do olho fechado por dois minutos após a instilação não foi realizada em 87,0% dos participantes, e 61,6% piscaram repetidas vezes imediatamente após instilar a droga. CONCLUSÕES: Verificou-se que a maior parte dos participantes deste estudo efetuou a instilação do colírio de modo incorreto. Isto significa desperdiçar grande parte do conteúdo do frasco, aumentar as possibilidades de toxicidade sistêmica, não aproveitar a plenitude do efeito hipotensor das drogas e contaminar a extremidade do frasco de colírio. Portanto, o ensino da técnica adequada da instilação de colírio é absolutamente necessária para todos os pacientes.PURPOSE: To observe eye drop instillation technique in chronic glaucoma patients. METHODS: This is a prospective study enrolling 193 glaucomatous patients. Each received a sample of lubricant eye drop bottle (Dunason®, Alcon Laboratories, São Paulo, Brazil and was instructed to use it once. RESULTS: All patients used a mean amount of 1.64 ± 1.26 drops. In 54.5% of the patients, the eyedropper touched the eye and adnexa. In 3.1% the drops were not placed in the eye, without the patient being aware of this. In 87.0% of them, neither the lacrimal point occlusion nor the closure of the eyes for two minutes after instillation were

  20. Intestinal digestibility of protein of adapted forages and by-products in Brazilian Northeast by three-steps technique Digestão intestinal da proteína de forrageiras e co-produtos da agroindústria produzidos no Nordeste Brasileiro por intermédio da técnica de três estágios

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    José Gilson Lousada Regadas Filho

    2010-06-01

    Full Text Available It was aimed to estimate the intestinal digestibility (ID of rumen-undegradable protein (RUDP of several feeds by a three-steps procedure. The evaluated forages were algaroba (Prosopis juliflora, canafístula (Pithecellobium multiflorum, flor-de-seda (Calotropis procera, jitirana (Ipomea sp., juazeiro (Ziziphus joazeiro, mata-pasto (Senna obtusifolia, sabiá (Mimosa caesalpiniaefolia Benth, palma gigante (Opuntia ficus indica and xique-xique (Cereus gounellei, and the agroindustry byproducts were pineapple (Ananas comosus L., barbados cherry (Malpighia emarginata, cashew (Anacardium occidentale, coconut (Cocos nucifera L., melon (Cucumis melo, passion fruit (Passiflora eduli, grape (Vitis labrusca and anatto seeds (Bixa orellana L.. The feeds were incubated in rumen during 16 hours to determine the RUDP, and the residue was submitted to the digestion with pepsin solution during one hour, and pancreatic solution during 24 hours at 38ºC, those residues were analyzed for total nitrogen. The estimative of RUDP forage ranged from 13.37 to 83.6%, and the RUDP by-product ranged from 39.14 to 89.06%. The intestinal digestion of RUDP of the forages ranged from 26.09 to 80.68%, while for by-products varied from 22.26 to 76.82%. The sabiá was the forage that presented the highest intestinal digestibility and digestive rumen-undegradable protein (RUDPd, and the flor-de-seda, the lowest digestibility; while for by-products, melon and cashew presented, respectively, the highest values for DI and RUDP. The coconut presented the lowest values for ID and RUDPd. Although, some formulation systems of diets for ruminant consider that the RUDP present constant ID, the data obtained in this work suggest variation among the different feeds.A pesquisa objetivou estimar a digestibilidade intestinal (DI da proteína não-degradada no rúmen (PNDR de alimentos por intermédio da técnica de três estágios. As forragens avaliadas foram algaroba (Prosopis juliflora

  1. Limpeza da superfície de corte de rebolos por um sistema de ar comprimido na retificação cilíndrica externa de mergulho de materiais cerâmicos refrigerados com a técnica da mínima quantidade de lubrificante (MQL Grinding wheel surface cleaning using a compressed air system, in external plunge grinding of ceramics using the minimum quantity lubricant (MQL technique

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    E. C. Bianchi

    2012-06-01

    Full Text Available Nos processos de retificação, a utilização de fluidos de corte é uma maneira de implementar a qualidade final do processo, pois os fluidos têm como finalidade a lubrificação na área de contato entre a peça e ferramenta e a refrigeração das superfícies, assim evitando danificações na superfície da peça. Com isso, a utilização de fluidos de corte tem sido constantemente estudada, visando diminuir a utilização deste, pois a utilização de fluidos de corte tem seus problemas. O custo do produto final aumenta consideravelmente com o uso de fluidos de corte no processo de retificação, além de que os fluidos de corte são substâncias tóxicas e nocivas tanto às pessoas quanto ao meio ambiente. Portanto, indústrias, universidades e centros de pesquisas são levados a pesquisar métodos alternativos menos prejudiciais ao meio ambiente. Dentre as alternativas surge a técnica da mínima quantidade de lubrificante (MQL, que também tem suas desvantagens, como por exemplo, a formação de um borra de óleo na superfície de corte do rebolo, o que gera uma rugosidade maior na peça. Porém, visando minimizar o problema da formação da borra de óleo podem ser usados jatos de ar comprimido incidindo na superfície de corte do rebolo, com o objetivo de limpar a mesma. Este estudo será feito através da análise da avaliação das variáveis de saída do processo de retificação externa, como o comportamento da rugosidade superficial e dos desvios de circularidade. Através dos resultados obtidos pretende-se estudar a técnica do MQL, visando melhorá-la através da limpeza da superfície de corte do rebolo com jatos de ar comprimido.In grinding, the use of cutting fluids aims to improve the final quality of the process, because their purpose is to lubricate the contact area between workpiece and tool and the surface cooling, thus avoiding damages on the machined part. Therefore, this subject has been constantly studied, in order

  2. Frei José Mariano da Conceição Veloso e a divulgação de técnicas industriais no Brasil colonial: discussão de alguns conceitos das ciências químicas Friar José Mariano da Conceição Veloso and the promotion of industrial techniques in colonial Brazil: discussion of some concepts from the chemical sciences

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    Fernando J. Luna

    2009-03-01

    Full Text Available Na virada para o século XIX, o botânico mineiro frei Veloso desenvolveu intensa atividade de publicação de livros com intuito de divulgar aos colonos do império português técnicas para o melhoramento da produção agrícola e da incipiente indústria química. Este artigo aborda o primeiro tomo da Alographia dos alkalis fixos..., obra que contém artigos, capítulos de livros, cartas e patentes coligidos de uma dezena de autores, especialmente franceses e ingleses, sobre o conhecimento científico e técnico necessário para produção de carbonato de potássio a partir de cinza de plantas autóctones. Alguns conceitos e definições da época da Revolução Química são discutidos, levando em conta como Veloso os traduziu para o português e os introduziu no Brasil por meio de sua obra.At the turn of the 19th century, Minas Gerais Botanist Friar Veloso worked intensely on the publication of books to promote among settlers from the Portuguese empire techniques for improving agricultural production and from the incipient chemistry industry. This article analyzes the first volume of the "Alographia dos alkalis fixos...", a work that includes articles, book chapters, letters and patents from ten authors, particularly French and English, about the scientific and technical knowledge needed for the production of potassium carbonate from the ash of native plants. Some concepts and definitions used at the time of the Chemical Revolution are discussed, considering that Veloso translated them to Portuguese and introduced them to Brazil through his work.

  3. Biomecânica de quatro técnicas de fixação da fratura em quatro partes da cabeça umeral Biomechanics of four techniques for fixation of the four-part humeral head fracture

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    Elpídio da Graça

    2013-02-01

    Full Text Available OBJETIVO: Realizar um estudo biomecânico de quatro técnicas de fixação das fraturas em quatro partes da cabeça umeral. MÉTODOS: A fratura foi reproduzida em 40 úmeros plásticos, divididos em grupos de dez conforme a técnica de fixação, cada uma delas empregando diferentes recursos de fixação, em configurações distintas. Os modelos umerais foram montados em uma escápula de alumínio, com tiras de couro mimetizando os tendões do capuz rotador, e submetidos a ensaios de encurvamento e de torção em uma máquina universal de ensaios, usando a rigidez relativa como parâmetro de avaliação. Montagens com o úmero intacto foram analisadas para comparação. RESULTADOS: O comportamento biomecânico das técnicas de fixação variou dentro de uma ampla faixa, as montagens incluindo a placa DCP e os parafusos de 4,5mm de diâmetro sendo significantemente mais rígidos do que as montagens com os fios de Kirschner e os parafusos 3,5 mm de diâmetro. CONCLUSÃO: As quatro técnicas foram capazes de suportar cargas compatíveis com a demanda fisiológica, mas aquelas com a maior rigidez relativa devem ser as preferidas para finalidades clínicas. Trabalho experimental.OBJECTIVE: To carry out a biomechanical study of four techniques for fixation of four-part humeral head fractures. METHODS: The fracture was reproduced in 40 plastic humeri, divided into groups of ten according to the fixation technique, each one employing different fixation resources, in different configurations. The humeral models were mounted on an aluminum scapula, with leather straps simulating the rotator cuff tendons, and submitted to bending and torsion tests in a universal testing machine, using relative stiffness as an evaluation parameter. Assemblies with intact humeri were analyzed for comparison. RESULTS: The biomechanical behavior of the fixation techniques varied within a wide range, where the assemblies including the DCP plate and the 4.5mm diameter screws

  4. Parâmetros de degradabilidade potencial da matéria seca e da proteína bruta das silagens de seis genótipos de sorgo (Sorghum bicolor (L. Moench, com e sem tanino no grão, avaliados pela técnica in situ Potential degradability parameters of the dry matter and crude protein of six sorghum silage genotypes (Sorghum bicolor (L. Moench, with or without tannin on grain, evaluated by in situ technique

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    Lívio Ribeiro Molina

    2003-02-01

    Full Text Available Para testar o efeito da presença de tanino no grão sobre os parâmetros de degradabilidade potencial da matéria seca e da proteína bruta de seis genótipos de sorgo para silagem, foi conduzido um experimento utilizando a técnica da degradabilidade in situ. Quatro novilhos canulados no rúmen, alimentados individualmente, duas vezes ao dia ad libitum com feno de Tifton 85, foram utilizados para a incubação de silagens de sorgo no estádio de grão leitoso, pertencentes a seis genótipos: BR 303, BR 304, BR 601e AG 2006 (sem tanino no grão; BR 700 e BR 701 (com tanino. Foram incubadas 5 g de amostra nos tempos de incubação: 6, 12, 24, 48, 72 e 96 horas. O tempo zero (t0 foi utilizado para cálculo da fração solúvel. A presença do tanino reduziu a extensão de degradação da matéria seca e da proteína bruta nas silagens de sorgo BR 700 e BR 701. As degradabilidades potenciais destes nutrientes foram influenciada pelo tanino. Não foi observado efeito depressivo do tanino sobre as taxas de degradação para nenhum nutriente, em nenhuma silagem testada.The aim of this experiment was to evaluate the effect of tannin on grain over potential degradability parameters of the dry matter and crude protein of six sorghum silage genotypes by in situ technique. It was used four crossbred steers, canulated in rumen, fed ad libitum twice at day with a diet comprised by Cynodon dactylon hay. Six sorghum silage genotypes, harvested at milk stage, were incubated in the rumen: BR 303, BR 304, BR 601, and AG 2006 (without tannin on grain; BR 700, and BR 701 (with tannin on grain. Five grams of samples were incubated at times: 6, 12, 24, 48, 72, and 96 hours. The time zero (t0 was used to calculate the soluble fraction. Tannin decrease the extent of degradation of dry matter and crude protein of BR 700 and BR 701 sorghum silages. The potential degradabilities of these nutrients were reduced by tannin presence on grain. There was not effect of tannin

  5. Técnicas projetivas na avaliação de aspectos psicopatológicos da anorexia e bulimia Projective techniques in the assessment of psychopathology of patients with anorexia and bulimia

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    Rodrigo Sanches Peres

    2011-08-01

    Full Text Available O presente estudo teve como objetivo verificar a utilização de técnicas projetivas na avaliação de características psicopatológicas de pacientes com transtornos alimentares. Trata-se de uma revisão sistemática de literatura, realizada a partir de buscas nas bases de dados LILACS e Banco de Teses/CAPES com o emprego dos descritores "anorexia" e "bulimia". As referências localizadas foram selecionadas, recuperadas na íntegra e submetidas a uma apreciação qualitativa, organizada em dimensões de análise específicas. As principais características psicopatológicas reportadas foram: passividade, introversão e obsessividade, conflitos, tensões e angústias em relação à figura materna, grave distorção da imagem corporal e tendência à fusão nos relacionamentos interpessoais. Evidenciou-se, ainda, o predomínio de delineamentos metodológicos incipientes. Novas pesquisas envolvendo o emprego de técnicas projetivas no contexto dos transtornos alimentares são necessárias para prover os profissionais de evidências empíricas, que possam ser aproveitadas em protocolos de avaliação multidisciplinar adequados à população brasileira.This study aimed to review the Brazilian literature on the use of projective techniques in the assessment of psychopathological features of patients with eating disorders. It is a systematic literature review from searches on LILACS and CAPES Thesis Databases, with the use of the descriptors "anorexia" and "bulimia". The obtained references were selected and, later, recovered in full version and submitted to a qualitative appreciation, organized in specific dimensions. The main psychopathological features reported were: passivity, introversion and obsessiveness, conflicts, tensions and anxieties in relation to the maternal figure, severe distortion of body image and tendency to merge in interpersonal relationships. The researches analysis revealed predominance of weak methodological designs. New

  6. Avaliação da dor em histeroscopia ambulatorial: comparação entre duas técnicas Pain evaluation in office hysteroscopy: comparison of two techniques

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    Daniela Barreto Fraguglia Quental Diniz

    2010-01-01

    Full Text Available OBJETIVO: comparar a dor referida pelas pacientes submetidas à histeroscopia pela técnica convencional com gás carbônico (CO2 e a vaginohisteroscopia com soro fisiológico (SF 0,9%. MÉTODOS: estudo prospectivo de coorte, realizado em um serviço de histeroscopia ambulatorial. Foram incluídas 117 pacientes com indicação para realizarem o exame, alocadas aleatoriamente em dois grupos. Todas responderam a um questionário epidemiológico e quantificaram a dor esperada antes do exame e sentida após seu término em uma escala verbal de dor de 0 a 10. Para a técnica convencional, foram utilizados espéculo, tração do colo, inserção de ótica de 30º e camisa diagnóstica com diâmetro total 5 mm. A cavidade foi distendida com CO2 sob pressão de 100 mmHg controlada por histeroinsuflador e a biópsia realizada com cureta de Novak. A vaginoscopia foi realizada sem toque, por distensão da vagina com líquido, visualização direta do colo e introdução de ótica com duas camisas de fluxo contínuo com canal acessório de perfil ovalado, totalizando também 5 mm de diâmetro para o conjunto. Foi utilizado SF 0,9% como meio de distensão e a pressão, definida como a necessária para adequada visualização do canal e da cavidade com pressurizador pneumático externo. A biópsia foi realizada de forma dirigida com pinça endoscópica. Foram calculados média e desvio padrão para as variáveis quantitativas e frequência para as qualitativas. O teste t de Student foi utilizado para comparar médias e o teste do qui-quadrado ou exato de Fischer (quando nPURPOSE: to compare the pain reported by patients submitted to hysteroscopy by the standard technique with carbon dioxide (CO2 and to vaginal hysteroscopy with physiological saline (0.9% NaCl. METHODS: this was a prospective cohort study conducted at an ambulatory hysteroscopy service. A total of 117 patients with indication for the exam were included, being randomly assigned to one of the

  7. Synthesis and characterization of magnetic nanoparticles of oxides for dual MnFe{sub 2}O{sub 4} bioseparation, stabilized in fatty acid and the system chitosan - Eu(TTA){sub 3}(TPPO){sub 2}. Studies on the influence of doping with Gd{sup 3+}, Tb{sup 3+}, Ho{sup 3+} e Eu{sup 3+} in structural and magnetic properties; Sintese e caracterizacao de nanoparticulas magneticas de oxidos duplos de MnFe{sub 2}O{sub 4} para biosseparacao, estabilizadas em acido graxo e recobertas pelo sistema quitosana - Eu(TTA){sub 3}(TPPO){sub 2}. Estudo da influencia da dopagem com Gd{sup 3+}, Tb{sup 3+}, Ho{sup 3+} e Eu{sup 3+} nas propriedades estruturais e magneticas

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    Kovacs, Thelma Antunes Rodrigues

    2014-07-01

    This work was synthesized and characterized ferrite magnetic nanoparticles manganese, using the chemical coprecipitation method. By varying the heating time under 98°C (0, 10,20,40,60 3 80 minutes), the molar percentage of doping (1, 3, 5, 7, and 10%), gadolinium, europium, terbium and holmium. Magnetic ferrite nanoparticles and manganese ferrite doped with manganese were synthesized by coprecipitation method starting with chloride solutions of metals (iron (III), manganese (II), europium (III), gadolinium (III), terbium (III) and holmium (III)) and NaOH 5mol.L{sup -1} as precipitating agent. The magnetic nanoparticles were characterized by scanning electron microscopy, infrared spectroscopy, X-ray diffraction, magnetization curves, and thermal analysis. Most of manganese ferrite particles showed superparamagnetic behavior. After the characterization it was found that the samples synthesized manganese ferrite with more than 40 minutes heating time, crystal structure showed the characteristic pattern of the inverted manganese ferrite spinel type. The stabilization of the samples in oleic acid nanoparticles produced with a hydrophobic outer layer and facilitated by coating chitosan biopolymer, since this has a positive charge. Among the doped samples there was no significant change in the magnetic behavior. Several techniques for characterizing these materials have been used such as X-ray diffraction spectrum in the infrared region, magnetization curves and thermal analysis. The resins were tested as magnetic material for the separation of biological materials. In this paper, are used as biological targets separation of bovine serum albumin. (author)

  8. Análise comparativa da técnica da incisão em duplo círculo com as técnicas com incisão periareolar e transareolomamilar de correção cirúrgica da ginecomastia Comparative analysis of the double-circle incision and techniques with periareolar and transareolopapilar incision for the surgical correction of gynecomastia

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    André Alves Cardoso

    2007-09-01

    Full Text Available OBJETIVO: comparar a técnica da incisão em duplo círculo (DC com as técnicas de incisão periareolar (PA e transareolomamilar (TAM, na correção da ginecomastia. MÉTODOS: foram revisados os prontuários de 34 pacientes com ginecomastia submetidos à correção cirúrgica no Hospital das Clínicas de Goiânia de 1999 a 2004. Os pacientes foram divididos em três grupos, de acordo com a técnica cirúrgica utilizada. Comparamos as variáveis numéricas paramétricas usando o teste de Tukey. Para as variáveis nominais, foi utilizado o teste do chi2, ou o teste exato de Fisher, quando necessário. Considerou-se significante o pPURPOSE: to compare the double-circle (DC technique to other techniques, with periareolar (PA and transverse nipple-areolar (TNA incisions, for the surgical correction of gynecomastia. METHODS: we studied the medical files of 34 patients from the Federal University of Goiás, submitted to the surgical correction of gynecomastia, from 1999 to 2004. Patients were divided according to the surgical technique used. The parametric numeric variables were compared by Tukey test. The chi2 or the Fisher's exact test was used for nominal variables. It was considered significant a p value<0.05. RESULTS: the mean age of the patients was 27.9 (+12.5 years. There were 43 gynecomastias, 34 unilateral (79.1% and nine (20.9% bilateral. There were 19 breasts operated (44.2% using DC, 14 (33.6% using PA incision, and 10 (23.3%, TNA incision. The mean drain usage was five days for DC and one day for the others (p<0.01. The suction drain was used in 19 cases (100% of DC and two (22% in TNA. The other patients used drains of Penrose (p<0.01. The mean surgical time was significantly larger for DC (73 minutes than for PA (45 minutes and for TNA (48 minutes. DC was used mainly in voluminous gynecomastias (p=0.04. The complications consisted in three (33% hematomas in TNA (p<0.01 and one (5% in DC; one (11% infection in TNA; two (10% partial

  9. Analysis of the film thickness of a root canal sealer following three obturation techniques Análise da espessura da linha de cimento endodôntico em três técnicas de obturação

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    Gustavo André De Deus

    2003-06-01

    Full Text Available The aim of this study was to obtain a quantitative analysis of the film thickness of a root canal sealer formed after filling by three different techniques. Thirty human maxillary incisors were selected and access cavities were prepared using high-speed diamond stones and water spray. A size #15 K-Flexofile was introduced in the canal of each specimen until it was seen just at the apical foramen. The working length was determined to be 1 mm short of that position and the canals were prepared to an apical size of #45 K-Flexofile. Copious irrigation with 5.25% NaOCl (sodium hypochlorite was used during and after instrumentation. The samples were divided into three groups and obturated as follows: G1 - lateral condensation, G2 - lateral condensation with an accessory cone, and G3 - continuous wave of condensation. The samples were evaluated in the cervical, middle and apical thirds. The film thickness of the root canal sealer was measured through a microscopic evaluation. Statistical analysis was obtained using the Wilcox test. Statistical analysis showed significant differences between G3 and G1, G3 and G2 (p O objetivo deste estudo foi realizar uma análise quantitativa da espessura da linha de cimento endodôntico formada por três técnicas de obturação. Trinta incisivos centrais superiores humanos foram selecionados e acessados de modo convencional. Uma lima nº 15 K-Flexofile foi usada para a verificação da patência foraminal e para determinação do comprimento de trabalho, que foi estabelecido a 1 mm aquém do forame apical. Os canais foram preparados até a lima nº 45. Hipoclorito de sódio a 5,25% foi usado durante toda a instrumentação. Os dentes foram divididos em 3 grupos e obturados pelos seguintes critérios: G1 - condensação lateral; G2 - compressão hidraúlica e G3 - onda de condensação. Os dentes foram seccionados e analisados nos terços cervical, médio e apical. A espessura do filme de cimento foi determinada por

  10. Aplicação de técnicas multivariadas no estudo da divergência genética em cana-de-açúcar Application of multivariate techniques in the study of genetic diversity in sugarcane

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    João de Andrade Dutra Filho

    2011-03-01

    Full Text Available Estudos sobre divergência genética são importantes na identificação de genitores potenciais para a obtenção de novos indivíduos com maior efeito heterótico. Em cana-de-açúcar esses estudos assumem fundamental importância, pois com o passar do tempo as variedades comerciais devem ser substituídas de suas áreas de cultivo, devido a sérios declínios agronômicos e industriais ocasionados pela degenerescência varietal. Sendo assim, o objetivo deste trabalho foi avaliar a divergência genética em progênies de cana-de-açúcar, através de técnicas multivariadas, com base em oito caracteres agroindustriais. O trabalho foi conduzido na área agrícola da Usina Santa Tereza, município de Goiana (PE, durante o ano agrícola 2007/2008. Foi utilizado o delineamento experimental casualizado em blocos completos com cinco repetições. As variáveis analisadas foram: toneladas de pol por hectare, toneladas de cana por hectare, fibra, pol % corrigida, pureza, teor de sólidos solúveis, açúcares redutores e açúcar total recuperável. Após análise de variância e estimação de parâmetros genéticos, a distância generalizada de Mahalanobis foi calculada para quantificar a dissimilaridade. Foram utilizados o método hierárquico de ligações médias (UPGMA e o método de otimização de Tocher. O coeficiente de herdabilidade média foi de alta magnitude para as variáveis TPH e TCH, indicando possibilidade de sucesso na seleção com base nesses caracteres. A metodologia aplicada permitiu a identificação de progênies de maior divergência genética proporcionando ao fitomelhoramento canavieiro da RIDESA sugestão de cruzamentos a serem realizados futuramente.This study aimed to evaluate the genetic diversity in progenies of sugar cane by means of multivariate techniques based on eight agroindustrial traits. The work was carried out in the agricultural area of Usina Santa Teresa, Goiana (PE, during the agricultural year 2007

  11. Estudo comparativo da eficiência de diferentes técnicas de mensuração da concentração espermática em suínos Efficiency of different measurement techniques of sperm concentration in swine

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    Wagner Loesch Vianna

    2004-12-01

    Full Text Available A inseminação artificial (IA em suínos é uma técnica cada vez mais utilizada na suinocultura moderna, pois propicia ao suinocultor vantagens quanto ao desempenho dos reprodutores, ao controle dos cruzamentos e à facilidade na introdução de material genético. Objetivando o aperfeiçoamento da técnica de IA, foram avaliadas a acurácia, a precisão e a robustez do Espermiodensímetro (ESPERMIO e do Espectrofotômetro (ESPECTRO, em comparação à Câmara de Neubauer. Utilizaram-se 142 ejaculados, que revelaram concentrações espermáticas médias (em milhões de sptz/mL e número médio de doses que poderiam ser produzidas, respectivamente, de 229,1 e 22,6; 185,0 e 18,5; 283,6 e 28,0 para a Câmara de Neubauer, o Espectrofotômetro e o Espermiodensímetro. O viés médio (acurácia e o desvio-padrão do viés médio (precisão do ESPECTRO, em comparação à Câmara de Neubauer, foram, respectivamente, de - 44,1 e 52,6, enquanto para o ESPERMIO foram de 54,5 e 44,8 (milhões de sptz/mL. Pode-se inferir que o ESPECTRO tende a subestimar e o ESPERMIO, a superestimar a concentração espermática, em comparação à Câmara de Neubauer. O ESPECTRO foi mais acurado e igualmente preciso que o ESPERMIO. A influência do volume de ejaculado sobre os resultados do ESPERMIO e do ESPECTRO pode ser comprovada pelos resultados de robustez para o volume do ejaculado.Artificial Insemination (AI in swines is a rising technique that has been used during the last years at the swine production systems, because it furnish several advantages to the producers just like boar high efficiency, better breeding control and easiness in introducing foreign genetic materials. Accuracy, precision and robustness for ejaculation volume of spermdensimeter (ESPERMIO and spectrofotometer (ESPECTRO in relation to the Neubauer Count, designed as the standard technique, were evaluated objectifying higher performance of AI technique. A total of 142 boar ejaculation was used

  12. Aplicação da técnica de emissão em tempo máximo de fonação em paciente com disfonia espasmódica adutora: relato de caso Applying the technique of sustained maximum phonation time in a female patient with adductor spasmodic dysphonia: case report

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    Luiz Alberto Alves Mota

    2012-01-01

    Full Text Available A Disfonia Espasmódica Adutora é uma desordem neurológica do processamento motor central, caracterizada por contrações involuntárias e inapropriadas da musculatura fonatória, produzindo uma hiperadução das pregas vocais, o que promove uma voz trêmula, entrecortada e tensa-estrangulada. O objetivo deste estudo foi descrever os parâmetros vocais, acústicos e laríngeos pré e pós-tratamento fonoaudiológico realizado por meio da aplicação da Técnica de Emissão em Tempo Máximo de Fonação (TETMF em paciente com Disfonia Espasmódica de Adução. Esta técnica tem como objetivo promover o aumento da resistência glótica, melhorar a estabilidade fonatória e adequar a coaptação glótica. Participou deste estudo de caso uma paciente de 66 anos de idade, gênero feminino, com Disfonia Espasmódica Adutora. A paciente foi submetida à avaliação otorrinolaringológica e fonoaudiológica pré e pós-aplicação da TETMF. Foi verificada modificação de parâmetros vocais, acústicos e laríngeos, tais como a classificação da disfonia de G3R1B1A0S3I3 para G2R1B1A0S2I2, pitch de grave a adequado, traçado espectrográfico instável para mais estável e expressivo aumento da frequência fundamental média e da intensidade vocal média, além da melhora da eficiência glótica com o fechamento da fenda glótica anteroposterior. A terapia fonoaudiológica com a aplicação da TETMF foi considerada uma adequada opção de tratamento para o caso, tendo em vista os resultados alcançados, com destaque para a qualidade vocal e estabilidade fonatória. Ressalta-se a importância de novos estudos para comprovação da eficácia da técnica no tratamento da Disfonia Espasmódica Adutora.Adductor Spasmodic Dysphonia (ASD is a neurological disorder of central motor processing, characterized by involuntary and inappropriate contractions of the phonatory muscles, producing hyperadduction of the vocal folds, which causes a tremulous, faltering

  13. Efeito de técnicas fisioterápicas sobre os desconfortos músculo-esqueléticos da gestação Effect of physiotherapeutic techniques on musculoskeletal discomforts in pregnancy

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    Marta Helena Souza De Conti

    2003-01-01

    Full Text Available OBJETIVO: estudar os efeitos de técnicas fisioterápicas sobre os desconfortos músculo-esqueléticos na gestação. MÉTODOS: estudo coorte prospectivo, com 71 gestantes nulíparas, de baixo risco, distribuídas conforme a participação (estudo; n=38 ou não (controle; n=33. O Programa Multidisciplinar de Preparo para o Parto e Maternidade constou de 10 encontros (da 18ª à 38ª semana, com atividades educativas, fisioterápicas e de interação. Compararam-se, por questionário específico, no início e final do programa, a ocorrência (presença ou ausência, as características (local, tipo, intensidade, freqüência e duração e a evolução dos desconfortos músculo-esqueléticos. As médias aferidas na avaliação inicial foram comparadas pela análise de variância (ANOVA seguida pelo teste do F. Para o estudo entre as proporções, verificadas no início e no final do programa, utilizou-se o teste do c². A significância estatística foi definida pelo limite de 5% (pPURPOSE: to study the effects of physiotherapeutic techniques applied by the Multidisciplinary Program of Preparation for the Childbirth and Maternity on musculoskeletal discomforts during pregnancy. METHODS: prospective cohort study, with 71 low-risk nulliparous women, distributed according to participation (study: n=38 or not (control; n=33. The Multidisciplinary Program of Preparation for Childbirh and Maternity had 10 meetings (18th to 38th week, with educational, physiotherapeutic, and interaction activities. Occurrence, characteristics, and evolution of musculoskeletal discomforts were compared by means of a specific questionnaire, both at the beginning and at the end of the program. The average of results of the initial assessment was compared through analysis of variance (ANOVA followed by the F test. For the study between proportions in the beginning and at the end of the program the c² was used. The statistical significance was determined at 5% of limit (p<0

  14. Nondestructive analysis of the natural uranium mass through the measurement of delayed neutrons using the technique of pulsed neutron source; Analise nao destrutiva da massa de uranio natural atraves da medida de neutrons atrasados com o uso da tecnica de fonte pulsada de neutrons rapidos

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    Coelho, Paulo Rogerio Pinto

    1979-07-01

    This work presents results of non destructive mass analysis of natural uranium by the pulsed source technique. Fissioning is produced by irradiating the test sample with pulses of 14 MeV neutrons and the uranium mass is calculated on a relative scale from the measured emission of delayed neutrons. Individual measurements were normalised against the integral counts of a scintillation detector measuring the 14 MeV neutron intensity. Delayed neutrons were measured using a specially constructed slab detector operated in anti synchronism with the fast pulsed source. The 14 MeV neutrons were produced via the T(d,n) {sup 4}He reaction using a 400 kV Van de Graaff accelerated operated at 200 kV in the pulsed source mode. Three types of sample were analysed, namely: discs of metallic uranium, pellets of sintered uranium oxide and plates of uranium aluminium alloy sandwiched between aluminium. These plates simulated those of Material Testing Reactor fuel elements. Results of measurements were reproducible to within an overall error in the range 1.6 to 3.9%; the specific error depending on the shape, size and mass of the sample. (author)

  15. Detection of Salmonella sp. from porcine origin: a comparison between a PCR method and standard microbiological techniques Detecção de Salmonella sp. em amostras de origem suína: comparação entre a técnica da Reação em Cadeia da Polimerase e o isolamento bacteriano convencional

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    Sandra Maria Ferraz Castagna

    2005-12-01

    Full Text Available The aim of this study was to compare a polymerase chain reaction (PCR method combined with selective enrichment in Rappaport-Vassiliadis broth (PCR-RVB with standard microbiological techniques (SMT for the generic detection of Salmonella in samples of porcine origin. Two hundred sixty eight field samples consisting of 42 sets of pooled porcine mandibular lymph nodes and tonsils, 44 samples of intestinal content, 38 pork sausage meat samples and 144 samples of feed collected from swine farms were submitted to the PCR-RVB and SMT protocols. Salmonella was detected in 54 samples using the PCR-RVB assay and in 42 samples by SMT, three of the SMT Salmonella-positive samples (one each of S. Derby, S. Panama and S. Typhimurium being Salmonella-negative by PCR-RVB. For the PCR-RVB method 15 Salmonella-positive samples were negative by SMT, a significant difference according to the Mac Nemar's chi-squared test (p=0.0153. Subsequent serological typing of the SMT isolates showed the following Salmonella serovars, the number of positive samples being given in parentheses: Typhimurium (12; Bredeney (10; Panama (5; Saint-paul (5; Minnesota (3; Mbandaka (2; Derby (1; Enteritidis (1; Orion (1 and Salmonella sp. (2. We concluded that, although the use of both PCR-RVB and SMT increased the number of positive samples, the PCR-RVB, due to its higher sensitivity and greater speed in giving results, can be implemented to detect Salmonella in samples of porcine origin.O objetivo desse estudo foi comparar um método de Reação em Cadeia da Polimerase (PCR combinado com enriquecimento seletivo em caldo Rappaport-Vassiliadis (PCR-RVB com as técnicas de isolamento bacteriano convencional (SMT para a detecção do gênero Salmonella em amostras de origem suína. Duzentas e sessenta e oito amostras de campo, compostas por: 42 "pools" de linfonodos mandibulares e tonsilas, 44 amostras de conteúdo intestinal, 38 amostras de massa de embutidos e 144 amostras de ra

  16. Characterization of the wind behavior in Botucatu-SP region (Brazil) by Weibull distributing; Caracterizacao do comportamento eolico da regiao de Botucatu-SP atraves da distribuicao de Weibull

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    Gabriel Filho, Luis Roberto Almeida [Universidade Estadual Paulista (CE/UNESP), Tupa, SP (Brazil). Coordenacao de Estagio; Cremasco, Camila Pires [Faculdade de Tecnologia de Presidente Prudente, SP (Brazil); Seraphim, Odivaldo Jose [Universidade Estadual Paulista (FCA/UNESP), Botucatu, SP (Brazil). Fac. de Ciencias Agronomicas; Cagnon, Jose Angelo [Universidade Estadual Paulista (FEB/UNESP), Bauru, SP (Brazil). Faculdade de Engenharia

    2008-07-01

    The wind behavior of a region can be described by frequency distribution that provide information and characteristics needed for a possible deployment of wind energy harvesting in the region. These characteristics, such as the annual average speed, the variance and shunting line standard of the registered speeds and the density of aeolian power average hourly, can be gotten by the frequency of occurrence of determined speed, that in turn must be studied through analytical expressions. The more adjusted analytical function for aeolian distributions is the function of density of Weibull, that can be determined by numerical methods and linear regressions. Once you have determined this function, all wind characteristics mentioned above may be determined accurately. The objective of this work is to characterize the aeolian behavior in the region of Botucatu-SP and to determine the energy potential for implementation of aeolian turbines. For the development of the present research, was used an Monitorial Young Wind anemometer of Campbell company installed a 10 meters of height. The experiment was developed in the Nucleus of Alternative Energies and Renewed - NEAR of the Laboratory of Agricultural Energize of the Department of Agricultural Engineering of the UNESP, Agronomy Sciences Faculty, Lageado Experimental Farm, located in the city of Botucatu - SP. The geographic localization is defined by the coordinates 22 deg 51' South latitude (S) and 48 deg 26' Longitude West (W) and average altitude of 786 meters above sea level. The analysis was carried through using registers of speed of the wind during the period of September of 2004 the September of 2005. After determined the distribution of frequencies of the hourly average speed of the wind, it was determined function of associated Weibull, thus making possible the determination of the annual average speed of the wind (2,77 m/s), of the shunting line standard of the registered speeds (0,55 m/s), of the coefficient of variation (20%) and of the density of aeolian power average hourly (24,58 W/m{sup 2}). (author)

  17. Evaluation of the mineralogical characterization of several smectite clay deposits of the state of Paraiba, Brazil using statistical analysis of variance; Avaliacao da caracterizacao mineralogica de diversos depositos de argilas esmectiticas do estado da Paraiba utilizando analise estatistica de variancia

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    Gama, A.J.A.; Menezes, R.R.; Neves, G.A.; Brito, A.L.F. de, E-mail: agama@reitoria.ufcg.edu.br [Universidade Federal de Campina Grande (UFCG), PB (Brazil)

    2015-07-01

    Currently over 80% of industrialized bentonite clay produced in Brazil in sodium form for use in various industrial applications come from the deposits in Boa Vista - PB. Recently they were discovered new bentonite deposits situated in the municipalities of Cubati - PB, Drawn Stone - PB, Sossego - PB, and last in olive groves - PB, requiring systematic studies to develop all its industrial potential. Therefore, this study aimed to evaluate chemical characterization several deposits of smectite clays from various regions of the state of Paraíba through the analysis of statistical variance. Chemical analysis form determined by fluorescence x-ray (EDX). Then analyzes were carried out of variance statistics and Tukey test using the statistical soft MINITAB® 17.0. The results showed that the chemical composition of bentonite clay of new deposits showed different amounts of silica, aluminum, magnesium and calcium in relation clays in Boa Vista, and clays imported. (author)

  18. ETBP (Extended True Boiling Point) curve extension of extra heavy crudes; Extensao da curva PEV (Ponto de Ebulicao Verdadeiro) de petroleos extrapesados por destilacao molecular e ampliacao da caracterizacao

    Energy Technology Data Exchange (ETDEWEB)

    Rocha, Rodrigo S.; Batistella, Cesar B.; Maciel, Maria Regina W.; Maciel Filho, Rubens [Universidade Estadual de Campinas (UNICAMP), SP (Brazil). Faculdade de Engenharia Quimica; Medina, Lilian C. [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil). Centro de Pesquisas (CENPES)

    2008-07-01

    For the determination of the TBP (True Boiling Point) Curve, which defines the yield of petroleum products, the ASTM D2892 method for petroleum distillation and ASTM D5236 method for vacuum distillation of heavy hydrocarbons were applied. Furthermore, from these distillations, cuts that are submitted to several analyses to determine its physical-chemical properties are obtained, and all this information generates the evaluation of petroleum. For heavy petroleum, these conventional methods have been limited, since the total distilled percentage determined for temperatures up to 565 deg C (maximum reached with ASTM D5236 method) is lower for these oils, reducing the points of the curve, limiting its information. To improve this data set for heavy oils, a methodology for the extension of TBP curve through molecular distillation was established. It was possible to reach values up to 700 deg C, representing a considerable progress for the extension of TBP curve. The objective of this work is to present the results of Extended TBP curve for a heavy petroleum and characterization carried out through the cuts and residues obtained in molecular distillation of the residue 'Zeta' 400 deg C+ (fancy name), made by ASTM D2892 method. (author)

  19. Study of potentiality of raw material of Crato/CE for use in structural ceramics - part I - technological characterization; Estudo da potencialidade da materia-prima do Crato/CE para utilizacao em ceramica estrutural - parte I - caracterizacao tecnologica

    Energy Technology Data Exchange (ETDEWEB)

    Andrade, J.C.S.; Santos, G.M.; Saldanha, K.M.; Sales Junior, J.C.C.; Nascimento, R.M.; Paskocimas, C.A., E-mail: jean@ufrnet.br [Universidade Federal do Rio Grande do Norte (UFRN), Natal RN (Brazil)

    2011-07-01

    The limitation of information on chemical, mineralogical and thermal characteristics of raw material used in process of manufacture of ceramic products in the region of Cariri, specifically the city of Crato, state of Ceara, motivated the development of this work, since this region ceramics exist that in a general context they appear as important productive chains in the state. The characteristics were evaluated by tests of limit of liquidity, limit of plasticity, index of plasticity, but also by chemical analysis for fluorescence of rays X, analysis of phases for diffraction of rays X, and thermal analysis (thermogratimetric analysis). The results showed that the raw material has excellent size distribution and characteristics acceptable to the processing of structural components of dark color the red, requiring a mixture of clay with coarse less plastic which granulation, that functions as reducer of plasticity. (author)

  20. Concrete hardened characterization using table scanner and microtomography computed; Caracterizacao de concreto endurecido utilizando scaner de mesa e microtomografia computadorizada

    Energy Technology Data Exchange (ETDEWEB)

    Wilson, R.E.; Pessoa, J.R.; Assis, J.T. de, E-mail: jrenatopessoa@gmail.com [Universidade do Estado do Rio de Janeiro (IPRJ/UERJ), RJ (Brazil); Dominguez, D.S.; Dias, L.A.; Santana, M. R. [Universidade Estadual de Santa Cruz (UESC), Ilheus, BA (Brazil)

    2016-07-01

    This paper proposes the use of image processing technologies to analyze hardened concrete samples obtained from table scanner and micro tomography. Techniques will be used to obtain numerical data on the distribution and geometry of aggregates and pores of the concrete, as well as their relative position. It is expected that the data obtained can produce information on the research of concrete pathologies such as AAR, and the freeze / thaw process. (author)

  1. Commissioning of Portal Dosimetry and characterization of an EPID; Comissionamento de Portal Dosimetry e caracterizacao de EPID

    Energy Technology Data Exchange (ETDEWEB)

    Olbi, D.S.; Sales, C.P. [Universidade de Sao Paulo (USP), SP (Brazil). Faculdade de Medicina; Nakandakari, M.V.N., E-mail: diego.olbi@hc.fm.usp.br [Instituto do Cancer do Estado de Sao Paulo, SP (Brazil). Servico de Radioterapia

    2016-07-01

    The development of technologies compensator blocks, MLC, high dose rate accelerators, treatment planning systems, among others, permitted that new treatment techniques in radiotherapy were created. Such techniques have the capacity to modulate radiation beam fluency (IMRT, VMAT), or to deliver high doses in few fractions or unique fractions (SRS). Following the same tendency, quality control of planning became more complex. It is necessary to evaluate the fluency delivered by the accelerator. Its levels of does and its spatial distribution should co-occur with the fluency calculated by TPS. Acquisition of new detector devices in quality control of treatments is fundamental to apply techniques. Portal Vision is a device EPID has the capacity to operate either in image mode or dosimetry mode, with the allowance of Portal Dosimetry. To evaluated planning in IMRT, the device is irradiated using planning e, therefore, the fluency measured is compared with calculated fluency, through gamma analysis. The aim of this work was to perform tests of commissioning of this device. (author)

  2. Associação de técnicas na estimativa da nematodeose gastrintestinal de caprinos Mestiços Anglo Nubiano Association of techniques for estimation of gastrointestinal nematodeosis in Anglo Nubian crossbred goats

    Directory of Open Access Journals (Sweden)

    Marina Santana Rossi Peixoto

    2011-06-01

    Full Text Available A associação de métodos diretos como o exame de fezes, e indiretos como os métodos FAMACHA© e do micro-hematócrito, podem facilitar na classificação de caprinos com relação à resistência e suscetibilidade aos nematoides gastrintestinais. Sessenta caprinos foram avaliados pelo grau FAMACHA©, pela contagem de ovos nas fezes (OPG e volume globular. Por análise de agrupamento hierárquico ascendente foram selecionados aqueles com potencial para resistência aos nematoides gastrintestinais (n=10 e os com potencial para suscetibilidade (n=10. Os caprinos com potencial para suscetibilidade apresentaram os maiores valores do grau FAMACHA©, do OPG, do número de larvas infectantes (L3 de Haemonchus e da concentração de fibrinogênio, e os menores valores de volume globular, proteína total e escore corporal. Foi demonstrado que os graus 3 e 4 foram mais predominantes nos animais com potencial para suscetibilidade, com os percentuais válidos de 45,5 e 30,5 respectivamente, e os graus 2 e 3 nos potenciais para suscetibilidade, com os respectivos percentuais válidos de 34,4 e 51,9. Observou-se que 58,4% dos animais do potencial para suscetibilidade e 90,6% dos potenciais para resistência estavam entre os graus FAMACHA© 1 e 3, o que mostra a maior tendência dos potenciaias para resistência em tolerar a infecção contra nematoides gastrintestinais. O total de estádios jovens e adultos de nematoides dos caprinos com potencial para suscetibilidade foi 2660,4 contra 1669,3 dos potenciaias para resistência. A associação dessas técnicas é um modelo importante na abordagem das nematodeoses em caprinos em condições do semiárido.The association of direct methods, as faecal exams, and indirect methods such as FAMACHA© system and microhematocrit, can facilitate classification of resistant and suscetible goats to gastro-intestinal nematodes. Sixty goats were evaluated using FAMACHA© score, faecal worm egg counts (EPG and packed cell

  3. Determinação da fragilidade ambiental utilizando técnicas de suporte à decisão e SIG Environmental fragility determination using decision support techniques and GIS

    Directory of Open Access Journals (Sweden)

    Annelissa G. Donha

    2006-03-01

    Full Text Available O trabalho objetivou determinar a fragilidade ambiental de uma área no município de Pinhais, região metropolitana de Curitiba, utilizando-se a técnica de avaliação por múltiplos critérios, presente no SIG Idrisi 32. Depois de gerados os mapas de classes de declividade, distância a partir dos rios, distância a partir das nascentes, distância a partir da represa, solos e uso atual, foram atribuídos pesos de importância para cada um dos fatores e através de Combinação Linear Ponderada geradas imagens de fragilidade potencial e emergente. Os mapas gerados com valores entre 0 e 255, foram classificados em 5 intervalos, cada um representando uma classe de fragilidade, sendo elas: muito alta, alta, média, baixa e muito baixa. A avaliação dos resultados se deu a partir de uma tabulação cruzada entre os mapas de fragilidade e cada um dos fatores utilizados, tendo-se concluído que a metodologia obteve bons resultados, pois se observaram a ocorrência dos solos de maior fragilidade, as declividades com maior grau de influência nos processos erosivos e a proximidade maior dos recursos hídricos nas classes de fragilidade mais alta e os solos de menor fragilidade, as menores declividades e a proximidade menor dos recursos hídricos nas classes de fragilidade mais baixa.The work had the objective to determine the environmental fragility of an area in the municipal district of Pinhais, metropolitan area of Curitiba, using the multiple criteria evaluation technique present in the GIS Idrisi 32. After having generated the maps of slope, distance from the rivers, springs and reservoir, soils and current land use, weights of importance were assigned to each one of the factors, and through Weighted Linear Combination images of potential and emerging fragility were generated. The generated maps with values varying between 0 and 255, were classified into five classes each one representing very high, high, medium, low and very low fragility

  4. Synthesis and characterization of polyanhydride derived from castor oil; Sintese e caracterizacao de polianidrido derivado do oleo de mamona

    Energy Technology Data Exchange (ETDEWEB)

    Borges, Fernando de M.; Reis, Roberta Yonara Nascimento; Nobre, Francisco X.; Matos, Jose M.E., E-mail: robertayonara@gmail.com [Universidade Federal do Piaui (UFPI), Teresina, PI (Brazil)

    2015-07-01

    Polyanhydrides are biopolymers already used as drug carriers, that allow the controlled release of the drug in vivo. Currently, these polymers are produced from a polyol, such as ethyleneglycol. In this work we synthesized a polyanhydride from castor oil, from the derivatization of oil via alcoholysis reaction. The oil was then converted to a monoglyceride (MG) by alcoholysis reaction at 140 °C. The MG reacted with phthalic anhydride (PA) at 100 °C, forming the polymer P1. The polymer was characterized by FT-IR, {sup 1}H and {sup 13}C NMR. These techniques allowed confirmation of the polymer formation. (author)

  5. Silicon carbide hollow fiber membranes: obtainment and characterization; Membranas de fibra oca de carbeto de silicio: obtencao e caracterizacao

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, S.S.L.; Ferreira, R.S.B.; Araujo, B.A.; Medeiros, K.M.; Lucena, H.L.; Araujo, E.M., E-mail: sandriely_sonaly@hotmail.com [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Departamento de Engenharia de Materiais

    2016-07-01

    Silicon carbide is a promising material for the production of membranes due to its high melting temperature, thermal shock resistance, excellent mechanical and chemical stability. So, this study aims to characterize silicon carbide membranes in order to apply them in the separation of oil-water. A solution (SiC + PES + 1-Methyl- 2-Pyrrolidone) and through the extrusion technique by immersion precipitation membranes were obtained with hollow fiber geometry was prepared. And then sintered at 1500 ° C. For the characterization analyzes were made XRD, FTIR and SEM to evaluate the morphology and composition of the membranes obtained before and after sintering. (author)

  6. Determination of intestinal digestibility of feeds by three-steps technique / Determinação da digestibilidade intestinal de alimentos pela técnica de três estágios

    Directory of Open Access Journals (Sweden)

    Patrícia Guimarães Pimentel

    2008-08-01

    Full Text Available The objective of this work was to estimate the intestinal digestibility of rumen-undegradable protein (RUDP of feeds by a three-steps procedure. The evaluated feeds were the soybean meal, wheat meal, soybean peel, meat flour and fish flour. Firstly, the feeds were incubated in rumen during 16 hours to determine the rumen-undegradable protein. The residue was submitted to the digestion with pepsin solution during 1 hour, and pancreatic solution during 24 hours at 38ºC. Soon after, those residues were analyzed for total nitrogen (TN. The estimate of RUDP ranged of 22.07% to 91.30% and the intestinal digestibility of RUDP ranged from 35.13% to 80.67%. The soybean peel and the meat flour presented better intestinal digestibility, and the wheat meal presented the lowest digestibility. Although some formulation systems of diets for ruminant consider the intestinal digestibility of dietary protein as being constant, the data obtained in this work suggest that there are variation among the different feeds.O objetivo deste trabalho foi estimar a digestibilidade intestinal da proteína não-degradada no rúmen (PNDR, de alimentos, por intermédio da técnica de três estágios. Os alimentos avaliados foram o farelo de soja, farelo de trigo, casca de soja, farinha de carne e farinha de peixe. Os alimentos foram inicialmente incubados no rúmen por 16 horas, para determinação da PNDR. O resíduo foi submetido à digestão com solução de pepsina, durante 1 hora, e solução de pancreatina a 38ºC, durante 24 horas. Em seguida, esses resíduos foram analisados para nitrogênio total (NT. A estimativa da PNDR variou de 22,07% a 91,30% e a digestibilidade intestinal da PNDR de 35,13% a 80,67%. A casca de soja e a farinha de carne apresentaram melhor digestibilidade intestinal e o farelo de trigo apresentou a menor digestibilidade. Embora alguns sistemas de adequação de dietas para ruminantes considerem a digestibilidade intestinal da proteína diet

  7. Characterization of beta radiation fields using radiochromic films; Caracterizacao de campos de radiacao beta utilizando filmes radiocromicos

    Energy Technology Data Exchange (ETDEWEB)

    Benavente, Jhonny A.; Silva, Teogenes A. da, E-mail: jabc@cdtn.b [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil). Programa de Pos-Graduacao em Ciencia e Tecnologia das Radiacoes, Minerais e Materiais; Meira-Belo, Luiz C.; Reynaldo, Sibele R. [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil)

    2011-07-01

    The objective of this work was to study the response of radiochromic films for beta radiation fields in terms of absorbed dose. The reliability of the EBT model Gafchromic radiochromic film was studied. A 9800 XL model Microtek, transmission scanner, a 369 model X-Rite optical densitometer and a Mini 1240 Shimadzu UV spectrophotometer were used for measurement comparisons. Calibration of the three systems was done with irradiated samples of radiochromic films with 0.1; 0.3; 0.5; 0.8; 1.0; 1.5; 2.0; 2.5; 3.0; 3.5; 4.5 e 5.0 Gy in beta radiation field from a Sr-90/Y-90 source. Calibration was performed by establishing a correlation between the absorbed dose values and the corresponding radiochromic responses. Results showed significant differences in the absorbed dose values obtained with the three methods. Absorbed dose values showed errors from 0.6 to 4.4%, 0.3 to 31.8% and 0.2 to 47.3% for the Microtek scanner, the X-Rite Densitometer and the Shimadzu spectrophotometer, respectively. Due to the easy acquisition and use for absorbed dose measurements, the densitometer and the spectrophotometer showed to be suitable techniques to evaluate radiation dose in relatively homogeneous fields. In the case of inhomogeneous fields or for a two dimension mapping of radiation fields to identify anisotropies, the scanner technique is the most recommended. (author)

  8. TÉCNICAS DE GEOPROCESSAMENTO PARA ANÁLISE MORFOMÉTRICA DA MICROBACIA DO RIBEIRÃO ALTO ÁGUA FRIA – BOFETE (SP / GEOPROCESSING TECHNIQUES TO MORPHOMETRIC ANALYSIS OF ALTO AGUA FRIA STREAM WATERSHED - BOFETE (SP

    Directory of Open Access Journals (Sweden)

    R.C. Nardini

    2016-06-01

    Full Text Available Técnicas de geoprocessamento foram realizadas para a caracterização morfométrica da microbacia do Ribeirão Alto Água Fria – Bofete (SP pelo Sistema de Informação Geográfica, visando à preservação, racionalização do seu uso e recuperação ambiental. A microbacia apresenta uma área de 4012,17 ha e está localizada entre as coordenadas geográficas: 22o 57’ 41” a 23o 02’ 42” S e 48o 11’ 29” a 48o 20’ 09” WGR.  A base cartográfica utilizada foi a carta planialtimétrica de Bofete (SP para extração das curvas de nível e hidrografia, para determinação dos índices morfométricos. Os resultados apresentaram que os baixos valores da densidade de drenagem, associados à presença de rochas permeáveis, facilitam a infiltração da água no solo, diminuindo o escoamento superficial e o risco de erosão e da degradação ambiental. Os baixos valores do fator de forma e do índice de circularidade indica que a microbacia tende a ser mais alongada com menor susceptibilidade à ocorrência de enchentes mais acentuadas. O parâmetro ambiental, coeficiente de rugosidade, permitiu classificar a microbacia para vocação com agricultura.

  9. Synthesis and characterization of type silicoaluminophosphates catalytic support; Sintese e caracterizacao de suportes cataliticos do tipo silicoaluminofosfatico

    Energy Technology Data Exchange (ETDEWEB)

    Leite, C.E.T.; Carvalho, M.W.N.C.; Pereira, K.R.O., E-mail: carlosedisio@hotmail.co [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Unidade Academica de Engenharia Quimica. Lab. de Catalise, Adsorcao e Biocombustiveis

    2010-07-01

    The refining processes, the catalytic hydrocracking is the future of diesel oil in Brazil and the first units are already scheduled to be inaugurated. Among the catalysts used in this process, silicoaluminophosphates (SAPO's) have considerable potential for use as they have been effective in the isomerization of n-alkanes, the isomerization of olefins and alkylation of aromatics. Because of this, the objective is to develop catalysts that will be used in hydrocracking reactions. The media like SAPO-5 were synthesized with different ratios silicon/aluminum, which is used as a catalytic support and have the function of crack organic molecules, since it has acidic character. The materials were characterized by techniques: X-ray diffraction, chemical analysis and textural by BET. After summarizing the media found that they had agreements with the crystalline phases presented in the literature.(author)

  10. Preparation, characterization and certification of uranium isotope reference materials; Preparacao, Caracterizacao e certificacao de materiais de referencia isotopicos de uranio

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira Junior, Olivio Pereira de

    2006-07-01

    This work describes the preparation, characterization and certification of a set of uranium isotope reference materials ranging from 0.5 to 20.0 % of {sup 235}U in mass. The most important concepts of metrology in chemical measurements were applied so that the certified quantities in these materials could be directly traceable to the International System of Units (SI). As a consequence of this approach, these materials can be used in the instruments calibration, estimation of measurement uncertainty, method validation, assessment of performance of analysts, quality control routines and interlaboratory comparison programmes. The most advanced methods and techniques in mass spectrometry, that is, gas source mass spectrometry (GSMS), thermal ionisation mass spectrometry (TIMS) and inductively coupled plasma mass spectrometry (ICPMS) were investigated to identify which are the dominant components in the uncertainty and to quantify its contribution to the final value of the measurement uncertainty of the isotopic ratio. The results obtained were then compared to verify which are the methods and techniques associated to the lowest measurement uncertainty values. The isotope amount ratio n({sup 235}U)/n({sup 238}U) was certified in the materials produced to expanded uncertainties ranging from 0.02 to 0.10 % and the ratios n({sup 234}U)/n({sup 238}U) and n({sup 236}U)/n({sup 238}U), to uncertainties ranging from 0.03 to 2.20 %. These values fully comply to the requirements of the isotopic characterization of nuclear fuel as well as the analysis of environmental samples for nuclear safeguards. (author)

  11. Efeito da facectomia no posicionamento palpebral superior: comparação entre as técnicas de facoemulsificação e a extracapsular Changes in the position of the upper eyelid after cataract surgery: a comparison between phacoemulsification and extracapsular techniques

    Directory of Open Access Journals (Sweden)

    Roberto Pinto Coelho

    2003-10-01

    Full Text Available OBJETIVO: Comparar o efeito de duas técnicas de facectomia (facoemulsificação e extracapsular no posicionamento da pálpebra superior. MÉTODOS: Foi analisado o posicionamento palpebral de dois grupos de pacientes submetidos à cirurgia de catarata: facoemulsificação e extracapsular. As imagens foram digitalizadas (antes e 30 dias após a cirurgia e processadas com o programa NIH 1.62. O posicionamento palpebral foi medido em relação a uma linha horizontal que unia os cantos medial e lateral da fenda palpebral, passando pelo centro da pupila. RESULTADOS: O posicionamento palpebral foi afetado de maneira diferente segundo a técnica utilizada. Na facoemulsificação a diferença média entre a posição palpebral superior pós e pré-operatória foi de -0,54 mm. Na extracapsular esta diferença aumentou para -1,41 mm. O teste t de Student (amostras pareadas mostrou que as médias das diferenças entre os dois grupos são significativamente diferentes (p=0,0068. CONCLUSÃO: A técnica de cirurgia de facoemulsificação induziu menor variação do posicionamento palpebral em relação à cirurgia extracapsular no pós-operatório recente.PURPOSE: To compare changes in the upper eyelid position after cataract surgery with phacoemulsification and extracapsular techniques. METHODS: The upper eyelid position was measured in two groups of patients before and 30 days after cataract surgery performed with phacoemulsification and extracapsular techniques. Palpebral fissure images (before and after the cataract surgery were digitized and then processed using the NIH 1.62 software. Eyelid position was measured relative to a horizontal line passing through the pupil center and connecting both canthi of the palpebral fissure. RESULTS: The palpebral position was differently affected according to the techniques. In phacoemulsification the mean difference between eyelids position before and after surgery was -0.54 mm. In the extracapsular technique this

  12. Plástica da valva mitral em pacientes com insuficiência mitral reumática: técnicas e resultados de 20 anos Mitral valve repair in rheumatic patients with mitral insuficiency: twenty years of techniques and results

    Directory of Open Access Journals (Sweden)

    Pablo Maria Alberto Pomerantzeff

    2009-12-01

    Full Text Available OBJETIVO: A plástica da valva mitral em pacientes reumáticos permanece um desafio. O objetivo deste estudo é analisar a técnica e os resultados da plástica da valva mitral em pacientes com insuficiência mitral reumática. MÉTODOS: Foram analisados, retrospectivamente, 330 pacientes portadores de insuficiência mitral reumática submetidos à plástica da valva mitral no Instituto do Coração do HC-FMUSP, entre 1985 e 2005. A idade média foi de 26,9 ± 15,4 anos e 57,6% dos pacientes eram do sexo feminino. No pré-operatório, 39,5% dos pacientes estavam em classe funcional IV. As técnicas de plástica mais comumente utilizadas foram a anuloplastia posterior com tira de pericárdio bovino em 48,4% dos pacientes e a anuloplastia com anel de Carpentier em 22,6%. As técnicas associadas foram empregadas em 55,2% dos pacientes, sendo as mais comuns: encurtamento de cordas (20% e papilarotomias múltiplas (17,8%. Plástica da valva tricúspide (26,7% e substituição da valva aórtica (27,2% foram os procedimentos associados mais frequentes. RESULTADOS: A mortalidade hospitalar foi 0,9% (três pacientes, sendo dois deles crianças em atividade reumática. As taxas linearizadas de tromboembolismo, endocardite, reoperação e óbito tardio foram de 0,2%, 0,2%, 3,5% e 0,5% pacientes-ano, respectivamente. A sobrevida actuarial foi de 86,4 ± 6,6% em 20 anos. A curva livre de reoperação foi de 30,3 ± 11,1% em 20 anos. CONCLUSÕES: A plástica da valva mitral em pacientes reumáticos é uma técnica factível na correção da insuficiência mitral, com baixa mortalidade operatória.OBJECTIVE: Mitral valve repair in rheumatic patients is still a challenge. The purpose of this study is to analyze the results of mitral valve repair in rheumatic patients in the Heart Institute University of Sao Paulo Medical School. METHODS: Were analyzed retrospectively, between 1985 and 2005, 330 patients submitted to mitral valve repair in the Heart Institute of

  13. Characterization of poly pyrrole/montmorillonite electro polymerised onto Pt; Caracterizacao de filmes PPy/montmorilonita eletropolimerizados sobre Pt

    Energy Technology Data Exchange (ETDEWEB)

    Castagno, K.R.L., E-mail: katiarlc@pelotas.ifsul.edu.b [Instituto Federal Sul-rio-grandense (IFSul), RS (Brazil). Dept. de Quimica; Azambuja, D.S.; Dalmoro, V.; Mauller, R.S. [Universidade Federal do Rio Grande do Sul (UFRGS), Pelotas, RS (Brazil). Inst. de Quimica

    2010-07-01

    In this study films of polypyrrole/montmorillonite (PPy/MT) were electropolymerized on platinum in order to evaluate the performance of this technique in the preparation of nanocomposite materials and to determine the thermal properties and conductivity of the composites. The films were synthesized from a solution containing pyrrole, dodecylbenzene sulfonate, acid and two types of clays: montmorillonite-Na + (MT-Na) and montmorillonite-30B (MT-M). The characterization of the films we have used FT-IR, TEM, XRD, TGA, DSC and resistivity measurement by the four-point van der Pauw method. The study showed that the adopted method of exfoliation and the electropolymerization method used, allows obtaining nanocomposite materials. Analyses of FT-IR, TEM and XRD show that the clays are exfoliated in the polymer matrix. Thermal analysis of the films indicates that the addition of clay reflects an enhancement in the thermal properties of the matrix of PPy, but decreases the conductivity of the same. (author)

  14. Development and characterization of the lead iodide semiconductor detector; Desenvolvimento e caracterizacao do detector semicondutor de iodeto de chumbo

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Icimone Braga de

    2001-07-01

    A methodology for purification and growth of PbI{sub 2} crystal as well as for its characterization as a room temperature radiation detector was developed in this work. Commercial salts were purified using the zone refining method and, for the purified material growth, the Bridgman method was used. To calculate the purification efficiency, studies of the decrease impurities concentrations were made in the salts and in three sections of the materials purified, using the neutron activation analysis technique. The results showed that the impurities segregate preferentially in the ingot final section. A significant decrease of the impurities concentration in function of the purification pass number was observed. The grown crystals presented good crystalline quality according to the results of the X-ray diffraction analysis. To evaluate the crystal as a semiconductor detector, measurements of dark leakage current, resistivity and the response of ({sup 241}Am) alpha particle and ({sup 241}Am, {sup 57}Co, {sup 133}Ba and {sup 137}Cs) gamma rays were carried out. The radiation response is strongly dependent on the crystals purity. The crystals purified with 500 passes exhibited energy resolution of 10% for {sup 241} Am alpha particle and the gamma rays resolution was compatible with the literature. The photosensibility of the PbI{sub 2} crystal found in the wavelength from 400 to 600 nm range suggests an another application at this crystal as a photodetector to be coupled to scintillators. (author)

  15. XPS utilization in the characterization of glycerol based polyesters; Utilizacao de XPS na caracterizacao de poliesteres a base de glicerol

    Energy Technology Data Exchange (ETDEWEB)

    Brioude, M.M.; Miranda, C.S.; Pereira, R.; Ohara, L.; Bargiela, P.; Rocha, M.G.M.C.; Jose, N.M., E-mail: mgcr@ufba.b [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Escola Politecnica. Inst. de Quimica

    2010-07-01

    X-ray photoelectron spectroscopy-XPS allows the determination of all elements of the periodical table, except hydrogen and helium, and is a very used technique for the polymers characterization, its spectra constitutes a 'fingerprint' of the material. Two samples of polymers were prepared from glycerol and fumaric acid and glycerol and terephthalic acid, with a molar ratio of 1:1 and 1:1.5. The general spectra show the presence of carbon and oxygen, the main components of the polymer. From the binding energies values of the C1s and O1s high resolution spectra it was possible to determine the carbon functional groups. Their concentration were determined and the presence of the aromatic carbon in the terephthalic polyesters was observed, and also similar proportions of aliphatic carbon and ester groups in the fumaric acid polyesters. For both polyesters, an amount of carboxyl group appears, indicating the terminal non-reacted groups. These results were confirmed qualitatively by FTIR. (author)

  16. Avaliação de diferentes métodos de sobre-enxertia na substituição da cultivar de macieira (Malus domestica Borkh. Gala por Princesa = Evaluation of different over-grafting techniques to replace 'Gala' for 'Princesa' apple trees (Malus domestica Borkh.

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    Fabiano Simões

    2006-10-01

    Full Text Available Foram comparados quatro métodos de enxertia: garfagem em inglês complicado (GIC; borbulhia lenhosa (BL; garfagem de topo (GT e garfagem meia-fenda esvaziada (GMFE, com o objetivo de avaliar o melhor método para execução da sobre-enxertia na substituição da cultivar de macieira Gala por Princesa. O experimento foi conduzido em São José dos Pinhais – PR, em seis macieiras localizadas em pomar com três anos de idade. As características avaliadas foram: porcentagem de pegamento dos enxertos, porcentagem de enxertos brotados, porcentagem de enxertos dormentes e porcentagem de enxertos mortos. O experimento foi finalizado após 62 dias da instalação. Após esse período conclui-se que a GIC apresentou maiores porcentagens de pegamento e brotação. Esta não se diferenciou da GT em relação à variável pegamento. A BL não é recomendada para a sobre-enxertia em macieiras.Four grafting methods were compared: whip graft, budding graft, cleft graft and the side graft, aiming at evaluating the best techniqueto replace ‘Gala’ for ‘Princesa’ apple trees. The experiment was held in São José dos Pinhais – PR in a 3-year old apple tree yard fruit. Six apple trees were selected for the experiment. The assessed characteristics were carried out by the percentage of grafting success (sprouted, sleeping grafts (no sprouts and dead ones. The experiment was concluded after 62 days of grafting. Results indicated that the budding graft showed to be more effective with a higher index of sprouting. This technique showed no difference concerning the sprouting percentage compared to the whip graft. The budding graft is not recommended to over–graft apple trees.

  17. [Clinical application of Da Vinci surgical system in China].

    Science.gov (United States)

    Jin, Zhenyu

    2014-01-01

    Da Vinci robotic surgical system leads the development of minimally invasive surgical techniques. By using Da Vinci surgical robot for minimally invasive surgery, it brings a lot of advantages to the surgeons. Since 2008, Da Vinci surgeries have been performed in 14 hospitals in domestic cities such as Beijing and Shanghai. Until the end of 2012, 3 551 cases of Da Vinci robotic surgery have been performed, covering various procedures of various surgical departments including the department of general surgery, urology, cardiovascular surgery, thoracic surgery, gynecology, and etc. Robotic surgical technique has made remarkable achievements.

  18. Implementação da técnica de extração de dispersão da matriz em fase sólida ("MSPD" para determinação de resíduos de agrotóxicos em laranjas Implementation of MSPD technique to determination of pesticides residues in oranges

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    Maria Helena W. M. Cardoso

    2004-06-01

    Full Text Available Um método de extração de multiresíduos baseado na técnica de dispersão da matriz em fase sólida ("MSPD", foi otimizado e validado para a extração e análise cromatográfica de 27 agrotóxicos (isômeros a, b, g, d do hexaclorociclohexano (HCH, dieldrin, endrin, heptacloro e seu epóxido (HE, a e b-endosulfan, o,p'-DDD, p,p'-DDD, o,p'-DDE, p,p'-DDE, o,p'-DDT, p,p'-DDT, dicofol, metoxicloro, mirex, hexaclorobenzeno (HCB, clorotalonil, parationa metílica, fenitrotiona, malationa, folpete, diazinona, cis e trans-permetrina em laranjas. A amostra macerada é inicialmente homogeneizada com C18, o homogeneizado é transferido para uma coluna de vidro contendo sílica gel onde se adiciona 10mL de acetato de etila como solvente de eluição. O eluente é concentrado, diluído em isooctano e 1mL deste é injetado no cromatógrafo a gás. Para a separação e quantificação dos 27 agrotóxicos, foi utilizado um CG/DCE. A confirmação dos mesmos foi feita por espectrometria de massas. Para a quantificação dos 27 agrotóxicos utilizou-se a padronização externa. As recuperações dos mesmos variaram de 70 a 120%, considerando-se os níveis de adição agrotóxicos/amostra de 0,02 e 2,0mg/kg. Os limites de quantificação variaram de 0,01 a 0,5mg/kg.A multiresidue method of extraction based on matrix solid-phase dispersion (MSPD technique was optimized and validated for chromatographic analyses of twenty seven pesticides residues [hexachlorocyclohexane (HCH isomers (a, b, g, d, dieldrin, endrin, heptachlor and its epoxide (HE, a and b-endosulfan, o,p'-DDD, p,p'-DDD, o,p'-DDE, p,p'-DDE, o,p'-DDT p,p'-DDT, dicofol, methoxychlor, mirex, hexachlorobenzene (HCB, chlorotalonil, parathion methyl, fenitrothion, malathion, folpet, diazinon, permethrin (cis and trans in oranges. The sample was blended with C18 and then the homogenized sample was introduced onto a glass column containing silica. Ten mL of ethyl acetate was added to the column as elution

  19. Avaliação da aplicabilidade da técnica de maturação in vitro de oócitos humanos e posterior fertilização Evaluation of the usefulness of the in vitro maturation technique of human oocyte and subsequent fertilization

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    Maria Clara Magalhães dos Santos Amaral

    2003-08-01

    Full Text Available OBJETIVO: avaliar a aplicabilidade da técnica de maturação in vitro de oócitos humanos e posterior fertilização. MÉTODOS: estudo prospectivo não randomizado descritivo realizado no período de novembro de 1999 a março de 2001 no qual foram incluídas 15 pacientes com infertilidade tubária e 20 ciclos de fertilização in vitro. Todas assinaram o termo de consentimento livre e esclarecido antes de iniciar o estudo. As pacientes tinham idade entre 18 e 32 anos incompletos, obstrução tubária como causa exclusiva de infertilidade e índice de massa corporal inferior a 25 kg/m². As pacientes receberam 300 UI de hormônio folículo estimulante (FSH recombinante por via intramuscular no segundo dia do ciclo e doses adicionais de 150 UI no quarto e no sexto dia do ciclo. A coleta ovular foi realizada no sétimo dia do ciclo. Os oócitos foram colocados em meio TCM 199 acrescido de antibióticos, piruvato, FSH, gonadotrofina coriônica humana e soro (Serum Substitute Supplement - Irvine Scientific®. Após 48 h de cultivo, os oócitos que atingiram o estágio de metáfase II foram inseminados e os fertilizados foram transferidos. RESULTADOS: foram puncionados 144 folículos com a coleta de 67 oócitos imaturos (46,5%. Quarenta e três oócitos atingiram o estágio de metáfase II (64,2% e foram inseminados. Destes, 30 fertilizaram e 25 embriões foram transferidos para 10 pacientes. Houve uma gravidez com nascimento de um bebê. CONCLUSÃO: concluiu-se que a técnica de maturar oócitos humanos in vitro previamente à fertilização in vitro é técnica exeqüível, capaz de gerar gravidez.PURPOSE: to evaluate the usefulness of the in vitro maturation technique of human oocyte and subsequent fertilization. METHODS: this is a prospective nonrandomized, descriptive study, carried out during the period of November 1999 to March 2001, with 20 cycles of in vitro fertilization of 15 patients with tubal infertility. All signed the written informed

  20. Transcrição reversa na determinação da expressão do mRNA para a enzima conversora de angiotensina testicular em animais tratados com zinco Assessment of the reverse transcriptase polymerase chain reaction technique in the determination of the mRNA expression for the testicular angiotensin-converting enzyme in zinc treated rats

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    Gilberto Simeone Henriques

    2005-12-01

    Full Text Available OBJETIVO: O objetivo deste trabalho foi otimizar as condições reacionais capazes de ocasionar variabilidade e de introduzir erros sistemáticos na reação em cadeia pela polimerase aplicada à análise da expressão gênica da isoforma testicular da enzima conversora de angiotensina. MÉTODOS: Avaliaram-se a concentração de cDNA, a concentração dos iniciadores, a temperatura de hibridização e o número de ciclos de desnaturação, hibridização e extensão. Para tanto, extraiu-se o RNA total por meio da reação com fenol-clorofórmio e isotiocianato de guanidina de amostras de testículos de ratos Wistar alimentados com uma ração contendo zinco. Em seguida, gerou-se o cDNA por transcrição reversa. Utilizando-se iniciadores específicos, amplificaram-se o gene de interesse (isoforma testicular da enzima conversora de angiotensina e o gene controle Gliceraldeído-3-Fosfato-Desidrogenase. As amostras foram então aplicadas em gel de agarose e submetidas à eletroforese, coradas em brometo de etídio e visualizadas sob luz ultravioleta. RESULTADOS: Demonstrou-se que a melhor condição reacional para a reação em cadeia pela polimerase da isoforma testicular da enzima conversora de angiotensina e do Gliceraldeído-3-Fosfato-Desidrogenase foi: (1 concentração inicial de cDNA de 2µg, (2 concentração de iniciadores de 200nM, (3 temperatura de hibridização entre 57,5ºC e 60,1ºC e (4 33 ciclos. CONCLUSÃO: Com essa otimização pôde-se minimizar as interferências sobre a técnica, contribuindo-se para a obtenção de dados comparativos a respeito da expressão gênica da enzima conversora de angiotensina testicular.OBJETIVE: The aim of the present work was to optimize the reaction conditions capable of generating variability and introducing systematic errors in the chain reaction of the polymerase used to analyze the gene expression for the testicular isoform of the angiotensin-converting enzyme. METHODS:The cDNA concentration

  1. Filosofia da análise da estabilidade da liquidez

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    Rodrigo Antônio Chaves da Silva

    2005-07-01

    Full Text Available A informação foi considerada finalidade de nosso conhecimento, até o período em os pensadores e pesquisadores da contabilidade passaram a raciocinar sobre o conteúdo e o significado dos informes. Nesta busca da razão sobre os estados patrimoniais, surgiu a análise contábil que procura por meio de relações e identidades, o significado da dinâmica expressa da estaticamente na informação. O primeiro aspecto que surgiu no objeto de análise foi o estudo da liquidez, que é um dos principais exercícios do patrimônio. A estabilidade também é outro exercício básico e imprescindível, pois este é que promove o equilíbrio do organismo administrativo. A ciência contábil após a sua dignidade científica passou a trilhar caminhos esplendorosos, amparados em doutrina que permite alcançar os píncaros filosóficos. Os estudos concernentes aos aspectos de interação da estabilidade na liquidez são, complexos e somente com os recursos filosóficos da contabilidade se pode estudá-los com o panorama holístico e sublime. A filosofia da contabilidade não é alheia às suas práticas tecnológicas, podendo buscar pontos sublimes de panoramas abrangentes, para o estudo analítico da liquidez e estabilidade, observando todas as dimensionalidades e essencialidades de acontecimentos, na comprovação e orientação dos estados de ineficácia e eficácia patrimonial.

  2. Preparation and characterization of the fish reference material; Preparacao e caracterizacao de um material de referencia de peixe

    Energy Technology Data Exchange (ETDEWEB)

    Ulrich, Joao Cristiano

    2011-07-01

    The certified reference materials (CRMs) play an important role in obtaining measurement results traceable to the International System of Units, through an unbroken chain of comparisons. Thus, the demand for new certified reference materials (CRMs) increases every day in all areas of knowledge. The availability of reference materials, mainly in Brazil is still incipient, given that the demand far exceeds the available variety of these materials. The amount of certified reference materials available in the country is insufficient to meet the need of the scientific community and demands for development of new methodologies. Among the many areas in need of reference materials, we highlight the importance for the food trade balance for these products within the country. The certification of food products, intended both for export and for domestic consumption, requires analysis methods that provide precise and accurate results to ensure product quality. This paper describes the preparation and certification of a reference material in the fish matrix in mercury and methylmercury. The study brings together since the stage of material selection, preparation, development of homogeneity and stability studies and characterization. The certification was performed by means of measurements using two analytical techniques, flow injection analysis - cold vapor atomic absorption spectrometry (FIA-CV-AAS) and isotope dilution applied to mass spectrometry (IDMS), which is a primary method. In this work the standards of the ISO 30 (ABNT 30-34) and ISO Guide 35 was used as the basis for the preparation and characterization of the material. For the calculation of uncertainties was used the GUM and Eurachem guide. As a result, was produced and certified a lot of material in relation to the concentration of mercury (Hg = 0.271 {+-} 0.057 mg g{sup -1}) and methylmercury (MeHg = 0.245 {+-} 0.038 mg g{sup -1}), and informational values of lead and arsenic. (author)

  3. Caracterização e avaliação de processos de seleção de resíduos sólidos urbanos por meio da técnica de mapeamento Characterization and evaluation of selection processes of urban solid waste through mapping technique

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    Kelly Carla Dias Lobato

    2010-12-01

    Full Text Available Este trabalho apresenta os resultados da aplicação da técnica de mapeamento para a caracterização e avaliação dos processos de seleção de resíduos sólidos urbanos (RSU desenvolvidos nas instalações de uma associação de catadores de materiais recicláveis. O trabalho utiliza métodos qualitativos por meio da pesquisa bibliográfica e estudo de caso. O levantamento de dados contou com observação, entrevista e questionário. Dentre as técnicas disponíveis para o mapeamento, foram utilizados o SIPOC, o mapa de processo e o mapofluxograma. O mapeamento de processos como ferramenta gerencial possibilitou a visualização dos processos em diferentes escalas, o relacionamento entre as atividades e o cruzamento de fluxo (transporte dentro do galpão, sendo esse um dos principais gargalos de produção.The objective of this work was to present the application of the mapping technique for characterization and evaluation of procedures for selection of urban solid waste (USW developed in an association of recyclable materials collectors. This work use qualitative methods through bibliographic research and case study. The gathering of data was performed by observation, interviews and questionnaire. Amongst the techniques available for the mapping, SIPOC, process map and flowchart map were used. The process mapping as a management tool made possible the visualization of the processes in different scales, the relationship between the activities and the flow crossing (transportation in the deposits, one of the main bottlenecks of production.

  4. Experimental techniques; Techniques experimentales

    Energy Technology Data Exchange (ETDEWEB)

    Roussel-Chomaz, P. [GANIL CNRS/IN2P3, CEA/DSM, 14 - Caen (France)

    2007-07-01

    This lecture presents the experimental techniques, developed in the last 10 or 15 years, in order to perform a new class of experiments with exotic nuclei, where the reactions induced by these nuclei allow to get information on their structure. A brief review of the secondary beams production methods will be given, with some examples of facilities in operation or under project. The important developments performed recently on cryogenic targets will be presented. The different detection systems will be reviewed, both the beam detectors before the targets, and the many kind of detectors necessary to detect all outgoing particles after the reaction: magnetic spectrometer for the heavy fragment, detection systems for the target recoil nucleus, {gamma} detectors. Finally, several typical examples of experiments will be detailed, in order to illustrate the use of each detector either alone, or in coincidence with others. (author)

  5. Novas estratégias em educação: avaliação da técnica Tribunal do Júri na capacitação de conselheiros na área de saúde da mulher em Santa Catarina, Brasil New educational strategies: evaluation of the Jury Trial technique for training council members in women's health in Santa Catarina, Brazil

    Directory of Open Access Journals (Sweden)

    Eleonor Minho Conill

    2003-04-01

    Full Text Available Descreve-se e avalia-se a técnica Tribunal do Júri, instrumento educativo inovador utilizado em uma oficina piloto sobre Controle Social e Gênero para conselheiros de saúde da Grande Florianópolis, Santa Catarina, Brasil. Estudaram-se sua confiabilidade e validade utilizando a opinião dos participantes complementado com observação qualitativa dos trabalhos. Houve unanimidade na aceitação da técnica por parte dos conselheiros pela "aquisição de conhecimentos" e "por ser participativa, democrática e dinâmica". A avaliação positiva coincide com trabalho anterior feito com secretários municipais, notando-se menor preferência por atividades cognitivas formais que também compunham a oficina. Conclui-se reforçando a importância do uso dessa inovação em capacitações, por ser aceita por públicos distintos, permitir o mapeamento de conteúdo programático e ser útil face a temáticas novas e polêmicas ao favorecer vivências práticas e reflexivas.This article describes and evaluates the Jury Trial technique, an innovative educational instrument used in a pilot workshop on Social Control and Gender by health council members in Greater Metropolitan Florianópolis, Santa Catarina, Brazil. The reliability and validity were studied based on the participants' opinions, complemented by qualitative observation of the work. There was consensus in acceptance of the technique based on "acquisition of knowledge" and the fact that it was participatory, democratic, and dynamic. The positive evaluation agrees with a previous study that interviewed municipal health secretaries, with a smaller preference of formal cognitive activities that were also part of the workshop. The article concludes by emphasizing the importance of this innovative technique in training programs, since it is accepted by different target publics, allows for designing the program contents, and is useful in relation to new and controversial issues since it favors

  6. O desafio da tuberculose na faixa etária pediátrica frente a novas técnicas diagnósticas The challenge of pediatric tuberculosis in face of new diagnostic techniques

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    Flavio R. Sztajnbok

    2009-06-01

    Full Text Available OBJETIVOS: Apresentar uma revisão atualizada sobre os novos métodos para o diagnóstico da tuberculose baseados na produção in vitro de interferon-gama (IFN-γ por células T dos pacientes sob investigação, comparando-os com a tradicional prova tuberculínica. FONTES DOS DADOS: Revisão de literatura utilizando os bancos de dados MEDLINE e LILACS (2000-2008 utilizando as palavras-chave tuberculose, interferon-gama, quantiFERON, ELISPOT e T-SPOT.TB. SÍNTESE DOS DADOS: Esses novos testes mostraram-se, de um modo geral, tão ou mais sensíveis e específicos que a prova tuberculínica, tanto em adultos como em crianças e imunossuprimidos, para o diagnóstico da infecção latente e da doença ativa, apresentando vantagens como a menor interferência da vacinação prévia pelo BCG, menor influência de estados anérgicos e melhor acurácia em crianças menores. Nos Estados Unidos, já estão sendo utilizados em substituição à prova tuberculínica, e apesar dos custos ainda elevados, a Organização Mundial de Saúde vai priorizar a sua viabilidade econômica. CONCLUSÕES: Sempre levando em conta a importância da história clínica e epidemiológica, os novos testes baseados na produção de IFN-γ apresentam resultados promissores e deverão ser considerados na investigação de tuberculose em qualquer paciente, mas especialmente nos grupos de risco, como as crianças e os imunossuprimidos.OBJECTIVES: To present an updated review concerning new assays for diagnosing tuberculosis based on in vitro interferon-gamma production by host T cells, and compare them with tuberculin skin test. SOURCES: A literature review was carried out based on Medline and LILACS databases (2000-2008 searching for the following keywords: tuberculosis, interferon-gamma, quantiFERON, ELISPOT and T-SPOT.TB. SUMMARY OF THE FINDINGS: These new assays proved to have, in general, equal or superior sensitivity and specificity than the tuberculin skin test not only in

  7. Comparação da técnica do saco de náilon móvel com o método de coleta total para determinar a digestibilidade dos nutrientes de alimentos volumosos em eqüinos Comparison of the mobile nylon bag technique with the total collection method to determinate the forages nutrient digestibilities in equine

    Directory of Open Access Journals (Sweden)

    Kleber Villela Araújo

    2000-06-01

    Full Text Available Foram realizados dois ensaios com o objetivo de avaliar a precisão da técnica do saco de náilon móvel em relação ao método de coleta total de fezes, para estimar a digestibilidade aparente dos nutrientes de alimentos volumosos em eqüinos. Foram utilizados seis cavalos adultos sem raça definida, com idade média de sete anos. No primeiro ensaio, foram avaliados os valores de digestibilidade do nutrientes do feno de capim coast-cross, por intermédio da técnica do saco de náilon móvel, com amostra moída em três diferentes granulometrias por meio do método de coleta total de fezes. No segundo ensaio, foram comparados os dois métodos para estimar a digestibilidade, utilizando como alimento teste o capim-elefante. Foi avaliado em laboratório o desaparecimento dos nutrientes das amostras de feno de capim coast-cross e capim-elefante moídas em três diferentes granulometrias, após a lavagem dos sacos em água. Foi usado um delineamento em blocos casualizados, no qual cada cavalo constituiu o bloco, e os métodos de determinação da digestibilidade, os tratamentos. Os resultados mostraram que a técnica do saco de náilon móvel com amostra moída a 1 mm é bom método de estimativa de digestibilidade aparente de MS, EB e hemicelulose, para o feno de capim coast-cross, enquanto para o capim-elefante, a amostra moída a 5 mm é precisa para estimar a digestibilidade aparente da MS, EB e FDN. A moagem das amostras de feno de capim coast-cross e capim-elefante a 1 mm proporcionou a maior perda de partículas dos sacos de náilon, após lavagem em água.Two assays were carried out to evaluate the precision of the mobile nylon bag technique in relation to the total collection method, to estimate the apparent digestibility of nutrients of the forages in equines. Six adult crossbred horses averaging seven years old were used. In first assay, the values of digestibility of the nutrients of coast-cross hay were compared using the mobile nylon

  8. Extração da catarata pela técnica de facoemulsificação em pacientes com uveíte Cataract extraction using the phacoemulsification technique in patients with uveitis

    Directory of Open Access Journals (Sweden)

    Cláudio de Lima Yamane

    2007-08-01

    Full Text Available OBJETIVO: Descrever os resultados da cirurgia de catarata pela técnica de facoemulsificação em pacientes com uveíte. MÉTODOS: Foi realizado estudo retrospectivo pela análise de prontuários de 189 pacientes (242 olhos com uveíte que foram submetidos a cirurgia de catarata pela técnica de facoemulsificação no Setor de Uveítes e Imunologia Ocular do Royal Victoria Hospital, McGill University Health Centre, Montreal, Quebec, Canadá. Os dados foram coletados em fichas protocoladas com informações sobre sexo, idade, classificação da uveíte, descrição cirúrgica e exames pré e pós-operatórios. Os exames pré e pós-operatórios continham informações sobre a data do exame, a melhor acuidade visual corrigida, o exame biomicroscópico, a pressão intra-ocular, os procedimentos realizados e o tratamento em uso. RESULTADOS: A média de acompanhamento pós-operatório foi de 46,8 ± 31,2 meses. A média da acuidade visual pré-operatória encontrada foi de 20/100 e a média de acuidade visual pós-operatória encontrada foi de 20/40. Encontramos 145 olhos (59,5% com acuidade visual melhor ou igual a 20/40 e 26 olhos com piora da acuidade visual. A complicação per-operatória mais encontrada foi a ruptura de cápsula posterior com perda vítrea observada em 7 olhos (3% do total de olhos. A recorrência da uveíte foi a complicação pós-operatória mais freqüente, sendo observada em 73 olhos (30,16%. Outras complicações pós-operatórias observadas foram a atrofia iriana (28,51%, hipertensão intra-ocular (28,09%, membrana epirretiniana (26,44%, opacidade de cápsula posterior (19%, edema macular cistóide (13,63%, hipotonia ocular (12,80%, atrofia do disco óptico (8,67% e sinéquias posteriores (6,61%. CONCLUSÕES: A cirurgia de catarata pela técnica de facoemulsificação é considerada segura e eficaz em pacientes com uveíte. Observamos um bom prognóstico visual no período de acompanhamento pós-operatório, apesar da

  9. ANALYSIS OF Treponema pallidum RECOMBINANT ANTIGENS FOR DIAGNOSIS OF SYPHILIS BY WESTERN BLOTTING TECHNIQUE Análise de antígenos recombinantes de Treponema pallidum no diagnóstico da sífilis utilizando a técnica de Western Blotting

    Directory of Open Access Journals (Sweden)

    Neuza Satomi SATO

    1999-03-01

    Full Text Available Three GST fusion recombinant antigen of Treponema pallidum, described as GST-rTp47, GST-rTp17 and GST-rTp15 were analyzed by Western blotting techniques. We have tested 53 serum samples: 25 from patients at different clinical stages of syphilis, all of them presenting anti-treponemal antibody, 25 from healthy blood donors and three from patients with sexually transmitted disease (STD other than syphilis. Almost all samples from patients with syphilis presented a strong reactivity with GST-rTp17 antigen. Some samples were non-reactive or showed a weak reaction with GST-rTp47 and/or GST-rTp15, and apparently there was no correlation with the stage of disease. There was no seropositivity among blood donors. No sample reacted with purified GST. We concluded that due to their specificity these recombinant antigens can be used as GST fusion protein for development of syphilis diagnostic assays.Os antígenos recombinantes de Treponema pallidum GST-rTp47, GST-rTp17 e GST-rTp15, produzidos em fusão com glutationa S-transferase (GST em E. coli, foram analisados quanto ao potencial diagnóstico da sífilis pela técnica de Western blotting. Foram testadas 53 amostras, sendo 25 de pacientes em diferentes estágios clínicos da sífilis, com resultados positivos no teste treponêmico clássico; 25 amostras procedentes de doadores de banco de sangue, com sorologia negativa e 3 de pacientes com doença sexualmente transmissível não relacionado à sífilis. Todas as amostras de pacientes com sífilis apresentaram alta reatividade com o antígeno GST-rTp17. Quanto aos antígenos GST-rTp47 e GST-Tp15 verificou-se uma variação na presença ou na intensidade da reação em diferentes amostras de pacientes com sífilis, sem mostrar correlação com o estágio da doença. Nenhuma reatividade contra quaisquer desses antígenos foi observada com as amostras do grupo controle. Nenhuma das amostras testadas apresentaram reatividade com a GST purificada. A

  10. Study of a new technique for measuring the travel time of ultrasonic waves using the frequency spectrum; Estudo de uma nova tecnica de medida do tempo de percurso da onda ultra-sonica usando o espectro de frequencia

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Allan Xavier dos

    2010-07-01

    During the operation of a nuclear plant and other industrial plants, the operational time and the exposition to severe working conditions may cause the wear of its components, consequently, compromising the safety and the performance of the installation. The implementation of periodical inspections helps to ensure the safe operation and the best performance of the plant. In this way, the use of ultrasonic techniques for inspection and materials characterization becomes more and more attractive, since they offer quick, precise results and are technically ease to implement. The usual ultrasonic techniques, need to the measure the travelling time of the ultrasonic wave in the material examined in order to extract information useful to characterize it. Thus, the measurement of the travelling time of the ultrasonic wave is the overriding factor in most of the applications made with ultrasound. In this work a new technique was developed for measuring the travelling time of the ultrasonic wave using a Fourier's Fast Transformer (FFT). It will be shown mathematically and experimentally that it is possible to use the ultrasonic signal in the frequency domain to determine the travelling time of the ultrasonic wave. Five experiments were carried out for the experimental validation of this new technique. The materials used were 20 ceramic pastilles with different porosities and 3 aluminum plates of different thicknesses. The obtained results have shown that the new technique proposed in this work was able to determine the travelling time of the ultrasonic wave with the same precision as the conventional technique. It was shown, furthermore, that this new technique is able to measure the travelling time of the ultrasonic wave in situations where the conventional technique cannot be applied greatly expanding the range of application of ultrasonic testing and inspections. (author)

  11. Técnica de oscilações forçadas na análise da resposta broncodilatadora em voluntários sadios e indivíduos portadores de asma brônquica com resposta positiva Using the forced oscillation technique to evaluate bronchodilator response in healthy volunteers and in asthma patients presenting a verified positive response

    Directory of Open Access Journals (Sweden)

    Juliana Veiga Cavalcanti

    2006-04-01

    Full Text Available OBJETIVO: Analisar, através da técnica de oscilações forçadas, pacientes asmáticos com resposta broncodilatadora positiva pelo laudo espirométrico e comparar esses resultados com os obtidos em indivíduos sadios. MÉTODOS: Foram analisados 53 indivíduos não tabagistas, sendo 24 sadios sem história de doença pulmonar e 29 asmáticos com resposta broncodilatadora positiva segundo o laudo espirométrico. Todos foram submetidos à técnica de oscilações forçadas e a espirometria antes e após vinte minutos da administração de salbutamol spray (300 g. Os parâmetros derivados da técnica de oscilações forçadas foram: resistência total, reatância total, resistência extrapolada para o eixo y, coeficiente angular da reta de resistência e complacência dinâmica. Na espirometria, os parâmetros utilizados foram o volume expiratório forçado no primeiro segundo e a capacidade vital forçada. RESULTADOS: No grupo controle, a utilização do broncodilatador produziu alteração significativa na resistência extrapolada para o eixo y (p OBJECTIVE: To use the forced oscillation technique to evaluate asthma patients presenting positive bronchodilator responses (confirmed through spirometry and compare the results with those obtained in healthy individuals. METHODS: The study sample consisted of 53 non-smoking volunteers: 24 healthy subjects with no history of pulmonary disease and 29 asthmatics presenting positive bronchodilator response, as determined through analysis of spirometry findings. All of the subjects were submitted to forced oscillation technique and spirometry immediately before and 20 minutes after the administration of salbutamol spray (300 g. The parameters derived from the forced oscillation technique were total respiratory resistance, total respiratory reactance, resistance extrapolated to the y axis, the slope of resistance, and dynamic compliance. The parameters measured in the spirometry evaluation tests were forced

  12. UM ENGENHEIRO NA EXPOSIÇÃO UNIVERSAL: ANDRÉ REBOUÇAS E OS FANTASMAS DA TÉCNICA AN ENGINEER IN THE UNIVERSAL EXPOSURE: ANDRÉ REBOUÇAS AND THE GHOST OF THE TECHNIQUE

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    ALFREDO CORDIVOLA

    2000-01-01

    Full Text Available Este ensaio propõe uma leitura do Caderno da primeira viagem à Europa escritopelo engenheiro André Rebouças enquanto visitava a Great Exhibition deLondres em 1862. O manuscrito (não publicado até hoje, e conservado naFundação Joaquim Nabuco, em Recife contém minuciosas observações eprojetos feitos por Rebouças. Como viajante, o engenheiro persegue apenasum fim: ser testemunha das novidades da tecnologia. Aprender, copiar, traduzirsão seus objetivos. Seus escritos, portanto, lidam com visões de modernidadee percepções do porvir, e postulam cruzamentos entre periferias e centros,entre os passados pré-industriais e as promessas de um futuro que Rebouçastentaria concretizar no Brasil do Segundo Império.PALAVRAS-CHAVE: Rebouças, viajantes do século XIX,This essay focuses on a travel notebook written by the engineer André Rebouçasin 1862, while he was visiting the Great Exhibition of London. The manuscript,still unpublished and kept at the Fundação Joaquim Nabuco in Recife, containsdetailed observations and projects made by Rebouças. As a traveller, theengineer pursues just one aim: to be a witness of the novelties of technology.To learn, to copy, to translate are his goals. Therefore, his writings deal withvisions of modernity and perceptions of the becoming, and postulate crossesbetween peripheries and centres, between pre-industrial pasts and the promisesof a future that Rebouças would try to make real throughout the Second Empire.

  13. Application of the electrophoretic deposition technique for obtaining Yttria-stabilized zirconia tubes; Aplicacao da tecnica de deposicao eletroforetica para a obtencao de tubos ceramicos de zirconia-itria

    Energy Technology Data Exchange (ETDEWEB)

    Caproni, E.; Muccillo, R., E-mail: ecaproni@gmail.com, E-mail: muccillo@usp.br [Centro de Ciencia e Tecnologia de Materiais, Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2012-01-15

    The electrophoretic deposition (EPD) is recognized as the most versatile technique for processing particulate materials, due to low cost, deposition in minutes and forming of pieces with complex geometry shapes. In this work an experimental setup for the simultaneous conformation of 16 ceramic tubes by EPD was built. Bimodal submicron Yttria-stabilized zirconia particles were deposited into graphite electrodes, after suitably adjusting the rheological characteristics of the suspension in isopropanol. After graphite burning and YSZ sintering at 1500 deg C, the ceramic tubes were characterized by X-ray diffraction, scanning probe microscope, impedance spectroscopy and electrical response as a function of oxygen content. Small dense one end-closed ceramic tubes, fully stabilized in the cubic phase, were successfully obtained by the EPD technique, showing the ability of that technique for processing large quantities of tubular solid electrolytes with electrical response to different amounts of oxygen according to the Nernst law (author)

  14. Delphi technique applied to risk identification and assessment on pipe supports fabrication and erection contracts; Aplicacao da tecnica Delphi para identificacao e avaliacao de riscos na contratacao e montagem de suportes de tubulacao

    Energy Technology Data Exchange (ETDEWEB)

    Cruz, Rodrigo Luiz Neves; Balbi, Diego Junca de Gonzaga [Promon Engenharia, Sao Paulo, SP (Brazil)

    2012-07-01

    Through the years, Risk Management became an accepted subject in Brazilian Organizations, with its own language, techniques and tools; and its processes are being more and more often introduced in its management models. However, risk identification, assessment and management is a difficult task, and can be even more difficult for construction industry-related projects, for these ventures tend to be more dynamic and complex. In this sense, the objective of this paper is to present the application of Delphi technique for risk identification in the erection of piping support. To achieve the desired objective, a literature review of theory references was conducted to understand concepts involved. To apply the technique itself, experts in plant erection were involving. (author)

  15. Development of a polymeric matrix for composite material produced by the filament winding technique; Desenvolvimento de matriz polimerica visando a producao de material composito atraves da tecnica de enrolamento filamentar

    Energy Technology Data Exchange (ETDEWEB)

    Sobrinho, Ledjane Lima; Ferreira, Marisilvia; Bastian, Fernando Luiz [Universidade Federal, Rio de Janeiro, RJ (Brazil). Coordenacao dos Programas de Pos-graduacao de Engenharia

    2005-07-01

    The study of the resin for composite materials to be produced by the filament winding technique is very important, since the good applicability of the technique is in part function of the characteristics of the resin. The objective of this work is the development of a polymeric matrix using vinyl ester resin for composite to be produced by the filament winding technique. Therefore, vinyl ester resin systems developed from Derakane 411-350 by varying the percentage of cure agent and activator. The system which presented the best behavior in tension (Yong's modulus 2,42 GPa, tensile strength = 47,67 MPa, elongation = 7,31 % and fracture toughness 2,67 J), adequate gel time and exothermic peak for the manufacture process was submitted to hygrothermal aging by immersion in water at 60 deg C for a maximum period of 64 days. (author)

  16. Proposal for inclusion of the risk based inspection technique in Regulatory Standard NR 13; Proposta de inclusao da tecnica de inspecao baseada em risco na Norma Regulamentadora NR 13

    Energy Technology Data Exchange (ETDEWEB)

    Esteves, Vinicius Teixeira; Lima, Marco Aurelio Oliveira [Det Norske Veritas Ltda. (DNV), Rio de Janeiro, RJ (Brazil)

    2012-07-01

    In Brazil, the Regulatory Standard n. 13 (NR 13) establishes requirements for the inspection of boilers and pressure vessels which has main objective of preventing accidents with these types of equipment. Additionally, it has the Risk-Based Inspection (RBI) technique as an effective way to manage the mechanical integrity of various types of static mechanical equipment by through an inspection planning based on the risk factor. In this study, it is being proposed to include the RBI technique, in the NR 13, for the planning and definition of periods for the safety inspection of boilers and pressure vessels in order to promote an increase in the operational safety in process industries in Brazil. In this study it was carried out a critical analysis of NR 13 and RBI, and beyond that a bibliographic research of various international documents that relate the operational safety of pressurized equipment with the inspection activity, and the acceptability of RBI by governments, agencies and organizations around the world. It is considered that the inclusion and formal acceptance of RBI technique in the NR 13 must be accompanied by a rigorous control to avoid the 'trivialization' of its use and ensure the implementation rational, efficient and reliable. Finally, it was developed and suggested basic elements and minimum requirements to be inserted in the NR 13, to be attended, in order mandatory, by the companies that choose the implementation and use of the RBI technique as a tool for the planning of safety inspection of boilers and pressure vessels. It is concluded that the formal acceptance of the RBI technique in the NR 13 could aggregate much value to this standard, with regard to the prevention of accidents involving boilers or pressure vessels, and provide a technological jump to the companies that make use of RBI technique in Brazil. (author)

  17. Anatomia microcirúrgica do hipocampo na Amígdalo-hipocampectomia seletiva sob a perspectiva da técnica de Niemeyer e método pré-operatório para maximizar a corticotomia Hippocampal microsurgical anatomy regarding the selective amygdalohippocampectomy in the Niemeyer’s technique perspective and preoperative method to maximize the corticotomy

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    Gustavo Rassier Isolan

    2007-12-01

    Full Text Available O conhecimento da anatomia microcirúrgica do hipocampo tem importância fundamental na cirurgia da epilepsia do lobo temporal. Uma das técnicas mais utilizadas na cirurgia da epilepsia é a técnica de Niemeyer. OBJETIVO: Descrever em detalhes a anatomia do hipocampo e mostrar uma técnica na qual pontos de referências anatômicos pré-operatórios visualizados na RNM são usados para guiar a corticotomia. MÉTODO: Foram utilizados 20 hemisférios cerebrais e 8 cadáveres para dissecções anatômicas microcirúrgicas do lobo temporal e hipocampo para identificação e descrição das principais estruturas do hipocampo. Foram estudados prospectivamente 32 pacientes com epilepsia do lobo temporal refratários ao tratamento clínico submetidos a amígdalo-hipocampectomia seletiva pela técnica de Niemeyer três parâmetros anatômicos foram mensurados na RNM pré operatória e transferidos para o ato cirúrgico. RESULTADOS: O hipocampo foi dividido em cabeça, corpo e cauda e sua anatomia microcirúrgica descrita em detalhes. As medidas adquiridas são apresentadas e discutidas. CONCLUSÃO: A complexa anatomia do hipocampo pode ser entendida de uma forma tridimensional durante dissecções microcirúrgicas. As medidas pré-operatórias mostraram-se guias anatômicos úteis para corticotomia na técnica de Niemeyer.The deep knowledge of hippocampal microsurgical anatomy is paramount in epilepsy surgery. One of the most used techniques is those proposed by Niemeyer. PURPOSE: To describe the hippocampal anatomy in details and to present a technique which preoperative anatomical points in MRI are identified to guide the corticotomy. METHOD: Microsurgical dissections were performed in twenty brain hemispheres and eight cadaveric heads to identify temporal lobe and hippocampus structures. Thirty two patients with drug-resistent temporal lobe epilepsy underwent a selective amygdalohippocampectomy with Niemeyer’s technique being measured three

  18. O controle da hemorragia pós-parto com a técnica de sutura de B-Lynch: série de casos The control of postpartum hemorrhage with the B-Lynch suture technique: a case series

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    Gilberto Nagahama

    2007-03-01

    Full Text Available OBJETIVO: apresentar uma técnica cirúrgica para pacientes submetidas ao parto cesáreo e que evoluem com hemorragia refratária ao uso de medicamentos. MÉTODOS: o critério de seleção das pacientes era falha do tratamento farmacológico no controle da hemorragia pós-parto e o desejo da paciente em preservar o útero. As pacientes foram submetidas ao parto cesáreo e evoluíram com hemorragia pós-parto imediata refratária ao uso de ocitocina, ergometrina e misoprostol. Aplicamos a técnica de sutura descrita por B-Lynch sem modificações. Com fio cromado catgut-2 ou poliglactina-1, transfixamos o útero em seis pontos, conforme padronização. Após compressão manual do útero realizada pelo assistente, o fio é tracionado pelas suas extremidades pelo cirurgião e é aplicado um nó duplo seguido de dois nós simples, para em seguida realizar-se a histerorrafia. RESULTADOS: utilizamos o fio cromado catgut-2 agulhado em três casos e poliglactina-1 agulhado em um. Nos quatro casos houve parada imediata do sangramento vaginal após aplicação da sutura. Não houve qualquer complicação durante a realização do procedimento e nem no puerpério imediato e tardio das quatro pacientes. CONCLUSÕES: esta técnica representa uma alternativa cirúrgica para o manejo da hemorragia pós-parto. Com sua aplicação relativamente fácil, rápida e segura, pode representar uma redução da morbimortalidade materna em nosso país.PURPOSE: to present a surgical technique for patients submitted to caesarean section, which evolves to medicine refractory hemorrhage. METHODS: a case report study, of which the including criteria were failure in the pharmacological treatment to control post-partum hemorrhage, and the patients' request to preserve their uterus. Four patients submitted to caesarean section which evolved to immediate post-partum hemorrhage, refractory to the use of ocytocin, ergometrine and misoprostol, were treated with the suture technique

  19. Contribuições das técnicas projetivas gráficas para a compreensão da personalidade de andarilhos de estrada Contributions of graphic projective techniques for the understanding of highway wanderers' personality

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    Rodrigo Sanches Peres

    2005-08-01

    Full Text Available Estudos indicam que a deserção que caracteriza o estilo de vida dos andarilhos de estrada é multifatorial e envolve fatores sócio-econômicos e psicológicos. O presente estudo visou investigar as principais características da personalidade de andarilhos de estrada. Para tanto, aplicou-se a Bateria de Grafismos de Hammer em 23 andarilhos albergados em uma instituição assistencial. O material coletado foi avaliado e interpretado em função dos critérios de atribuição de significados fornecidos pela literatura científica especializada. Os dados obtidos indicam que os sujeitos possuem uma imagem corporal comprometida por sentimentos de inferioridade e inadequação e uma organização afetiva marcada por conflitos de ordem sexual, pela utilização de mecanismos de defesa primários e por uma veemente tendência ao isolamento nas relações interpessoais. Tais resultados fornecem subsídios para o delineamento de algumas características de personalidade dos sujeitos estudados. Não obstante, a corroboração das hipóteses em questão depende da realização de novos estudos empíricos.Research results indicate that the highway wanderers' desertion involves socioeconomic and psychological factors. The objective of the present study was the investigation of the highway wanderers' personality. For so much, the Hammers' Graphic Battery was applied to a group of 23 highway wanderers sheltered in an caring institution. The collected data was evaluated and interpreted by the utilization of meanings attribution's criteria supplied by the scientific literature. Data analysis indicate that the participants possess a corporal image committed by inferiority feelings and inadequacy and an affective organization marked by sexual conflicts, primary defense mechanisms and a vehement tendency to isolation in interpersonal relationships. Such results supply subsidies for the understanding of some personality characteristics of the researched

  20. A Sintaxe da Janela

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    Luís Antônio Jorge

    1993-12-01

    Full Text Available A preocupação fundamenta! do trabalho é de caráter ontológico: esboçar o problema das significações apriorísticas e autônomas dos elementos que compõem a sintaxe arquitetônica. O trabalho elege um desses elementos: a janela. Este artigo parte da aproximação histórica entre a janela e a secção da pirâmide visual, construção imaginária da teoria da perspectiva renascentista. A consideração da janela na linguagem arquitetônica implica reconhecer uma ambigüidade essencial: a janela deve inserir-se ordenadamente no plano da parede - raciocínio típico da modenatura - mas também relacionar-se com a imagem vista através dela, que extrapola o plano, ressaltando a tridimensionalidade - herança da perspectiva renascentista, fundamentada no espaço euclidiano. Ver janela ou ver através da janela são alternativas que se colocam tanto ao observador interno ao edifício, quanto ao externo. Texto de duplaface, a sintaxe da janela versa sobre o relacionamento desses dois lados

  1. Evaluation of the quality of pet foods using fast techniques and official methods Avaliação da qualidade de rações utilizando métodos rápidos e métodos oficiais

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    Cibele Cristina Osawa

    2008-12-01

    Full Text Available This paper was designed to evaluate the rancidity of 18 pet food samples using the Diamed FATS kits and official AOCS methods for the quantification of free fatty acids, peroxide value and concentrations of malonaldehyde and alkenal in the lipid extracted. Although expiration dates have passed, the samples presented good quality evidencing little oxidative rancidity. The results of this study suggest that the Brazilian pet food market is replete with products of excellent quality due to the competitiveness of this market sector.O presente trabalho teve como objetivo avaliar 18 amostras de rações, utilizando kits Diamed FATS e métodos oficiais da AOCS para quantificações de ácidos graxos livres, índice de peróxido e concentrações de malonaldeído e alquenais no lipídio extraído. Embora estivessem fora do prazo de validade, as amostras apresentaram boa qualidade, indicada pelos baixos valores de rancidez oxidativa. Os resultados deste estudo sugerem que o mercado brasileiro de rações conta com produtos de excelente qualidade, devido à competitividade do setor.

  2. Proposal of a new technique for bile duct reconstruction after iatrogenic injury: study in dogs and review of the literature Reconstrução da via biliar após lesão iatrogênica, proposta de nova técnica: estudo em cães e revisão da literatura

    Directory of Open Access Journals (Sweden)

    Eduardo Crema

    2007-06-01

    Full Text Available PURPOSE: Interposition of a jejunal tube between the common bile duct and duodenum. METHODS: Five adult mongrel dogs of both sexes, weighing on average 22.3 kg (18 to 26.5 kg, were used. Obstructive jaundice was induced by ligation of the distal common bile duct. After one week, a 2.5-cm long jejunal tube was fabricated from a segment of the loop removed 15 cm from the Treitz angle and interposed between the common bile duct and duodenum. RESULTS: The animals presented good clinical evolution and no complications were observed. After 6 weeks, complete integration was noted between the bile duct mucosa, tube and duodenum and a significant reduction in total bilirubin and alkaline phosphatase was observed when compared to the values obtained one week after ligation of the common bile duct. CONCLUSION: The jejunal tube interposed between the dilated bile duct and duodenum showed good anatomic integration and reduced total bilirubin and alkaline phosphatase levels in the animals studied.OBJETIVO: Interposição de um tubo de jejuno entre o colédoco e o duodeno. MÉTODOS: Foram utilizados cinco cães adultos, sem raça definida, de ambos os sexos, com peso médio de 22,3 Kg (18 e 26,5 Kg. Após provocar icterícia obstrutiva pela ligadura do colédoco distal, após uma semana, praticou-se confecção do tubo de jejuno de 2,5 cm de extensão, que foi realizado com um segmento de alça retirado a 15 cm do ângulo de Treitz e a interposição do tubo entre o colédoco e o duodeno. RESULTADOS: Os animais tiveram boa evolução clínica e não apresentaram complicações. Notou-se total integração entre a mucosa da via biliar, do tubo e do duodeno e redução significativa dos valores da bilirrubina total e da fosfatase alcalina após seis semanas, quando comparado com os valores após uma semana de ligadura do colédoco. CONCLUSÃO: O tubo de jejuno interposto entre a via biliar dilatada e o duodeno, apresentou boa integração anatômica e reduziu os

  3. Aplicação da técnica de fio quente na determinação das propriedades térmicas de polímeros fundidos Hot wire technique in the determination of thermal properties of melt polymers

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    Wilson N. dos Santos

    2005-11-01

    Full Text Available A natureza da estrutura molecular dos plásticos torna as propriedades desses materiais fortemente dependentes da temperatura. A condutividade térmica, difusividade térmica e o calor específico, conhecidos como propriedades térmicas, são as três propriedades físicas mais importantes de um material em cálculos de transferência de calor. Valores confiáveis dessas propriedades são essenciais em polímeros, tanto em problemas envolvendo estado estacionário como em estado não estacionário de troca de calor. Hoje, várias técnicas diferentes para a determinação da condutividade térmica e difusividade térmica podem ser encontradas na literatura. Neste trabalho, a técnica de fio quente paralelo é empregada na determinação experimental das propriedades térmicas de polímeros. Três polímeros semi-cristalinos (PEAD, PEBD e PP, e dois polímeros amorfos (PS e HIPS foram selecionados para este trabalho. As medidas experimentais são feitas desde a temperatura ambiente até a, aproximadamente, 50 ºC acima da temperatura de fusão. As amostras são preparadas pelo processo de extrusão, partindo-se do pó ou "pellets" do polímero no estado sólido. Um molde especial de aço inoxidável, em forma de paralelepípedo retangular, provido de isoladores cerâmicos entre o fio quente, o termopar e o próprio molde é utilizado para armazenar a massa polimérica fundida, cujas propriedades térmicas serão medidas. Os resultados experimentais obtidos são comparados com dados disponíveis na literatura e com dados fornecidos pelos fabricantes. Uma análise crítica desta metodologia mostra as vantagens e desvantagens desta técnica experimental em relação à técnica de pulso de energia.The nature of the molecular structure of the plastics makes the properties of such materials markedly temperature dependent. Thermal conductivity, thermal diffusivity and specific heat, namely the thermal properties, are the three most important physical

  4. Metodologia para parametrizar e avaliar a técnica da ''burn-zinc'' no processo de soldagem a ponto por resistência Methodology for parameterize and assessment of the burn-zinc technique in the resistance spot welding process

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    Vinicius Castanheira do Nascimento

    2010-03-01

    Full Text Available Para minimizar os efeitos prejudiciais do zinco na soldagem a ponto por resistência de chapas galvanizadas, utiliza-se uma técnica tradicionalmente denominada ''Burn-Zinc'' (queima do zinco. Porém, existem poucas informações e estudos disponíveis na literatura sobre quando e como utilizá-la. O presente estudo teve a finalidade de avaliar a técnica de ''burn-zinc'', procurando entender melhor o fenômeno. Para tal, foi criada uma metodologia para determinação dos parâmetros ideais para cada combinação de chapa. Uma avaliação desta metodologia foi feita com uma série de soldagens com variações sistemáticas da corrente e pressão em níveis compatíveis para se obter a queima do Zn. Visualização das soldagens através de filmagem em alta velocidade, com sincronização dos sinais elétricos, foi empregada para entender os resultados. Uma vez definidos os parâmetros, soldagens foram realizadas com ou sem a aplicação da técnica. Os procedimentos experimentais propostos mostraram ser eficientes para a verificação e parametrização da técnica ''burn-zinc''. Mas houve evidências que a utilização da técnica nem sempre vai ocasionar redução no tempo total de operação.For minimizing the detrimental effects of zinc during resistance spot welding of galvanized sheets, a technique denominated Burn-Zinc is usually employed. However, there is no much information and studies available in the current literature about when and how to use this technique. The present work had the objective of assessing and understanding better this technique. For that, a methodology for determination of ideal burn-zing parameters as a function of the sheets was proposed. The evaluation of this methodology was carried out by a series of weldments, by systematically varying current and pressure at compatible levels for zinc burning. High speed filming, synchronized with the electrical signals, was employing for visualizing and results analyses

  5. Modificação da técnica de abordagem ventral à articulação atlantoxial sem a secção do músculo esternotireóideo Modification of ventral technique approach to the articulation atlantoxial with no section of the muscle sternothyreoid

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    Rafael Festugatto

    2009-07-01

    Full Text Available O objetivo deste trabalho foi apresentar uma variação na técnica de acesso ventral à articulação atlantoaxial para tratamento da instabilidade atlantoaxial sem a secção do músculo esternotireóideo. Foram utilizados 15 cães, pesando entre oito e 12kg, sem raça definida, independente do sexo, distribuídos aleatoriamente em três grupos iguais de acordo com o período pós-operatório (PO denominados de I (30dias, II (60 dias e III (90 dias para avaliações clínicas diárias. A articulação atlantoaxial foi submetida à artrodese por meio do acesso ventral utilizando pinos de Steinmann associados à resina acrílica autopolimerizável. O acesso e a exposição da articulação atlantoaxial sem a secção do músculo esternotireóideo foram realizados sem complicações ou limitações adicionais. Nenhum cão desta pesquisa apresentou tosse, dispnéia, regurgitação, paralisia laríngea ou Síndrome de Horner. Pode-se concluir que a secção do músculo esternotireóideo é um procedimento desnecessário e que não interfere na exposição da articulação atlantoaxial e na realização da artrodese em cães por meio do acesso ventral.The aim of this research was to present a variation of the ventral technique access to the atlantoaxial joint, for treatment of atlantoaxial instability with no section of sternothyreoid muscle. Fifteen dogs, with weight between 8 and 12kg, were randomly distributed in three groups denominated one (30 days, two (60 days and three (90 days for daily clinical evaluations. The atlantoaxial joint was submitted to the arthrodesis through the ventral access using pins of Steinmann associated to acrylic resin. The access and exhibition of the atlantoaxial joint with no section of the sternothyreoid muscle was obtained without complications or additional limitations. No dog of this research presented coughing, dyspnea, regurgitation, laryngeal paralysis or Horner's syndrome. It can be concluded that the

  6. Study of the parameters solution blow spinning technique in the obtaining of mullite nanofibers; Estudo de parametros da tecnica de fiacao por sopro em solucao na obtencao de nanofibras de mulita

    Energy Technology Data Exchange (ETDEWEB)

    Severo, L.L.; Farias, R.M.C.; Menezes, R.R.; Santos, M.A., E-mail: lucasleite_14.1@hotmail.com [Universidade Federal de Campina Grande (UFCG), PB (Brazil)

    2016-07-01

    The Solution Blow Spinning (SBS) technique which use aerodynamic forces and has a high production rate, was created for production of nanofiber with versatile way, such as electrospinning. Therefore, the objective is to analyze the process parameters in order to optimize the production of mullite nanofiber using the SBS technique to determine the influence of air pressure, the concentration of the polymer and ejection rate in the diameter of the fibers. For this, it was used PVC as polymer in spinning, tetrahydrofuran as the solvent, HCl as acidifying, aluminum nitrate nonahydrate and tetraethylorthosilicate as precursors of mullite. The nanofibers obtained were heat treated at 1100°C. From of XRD and SEM results, it was proved the achievement of mullite nanofiber, and STATISTICA 7 software revealed that only ejection rate and the concentration influence in the average diameters of the fibers. (author)

  7. Content validation of the Self-perception of Family Health Status scale using the Delphi technique Validación de contenido de la escala de autopercepción del estado de salud familiar usando la técnica Delphi Validação de conteúdo da escala de auto-percepção do estado da saúde familiar utilizando a técnica Delphi

    Directory of Open Access Journals (Sweden)

    Joaquín Salvador Lima-Rodríguez

    2013-04-01

    Full Text Available OBJECTIVE: To ascertain the content validity of the Self-perception of Family Health Status scale. METHOD: A validation study of an instrument with an online Delphi panel using the consensus technique. Eighteen experts in the subject were intentionally selected, with a multidisciplinary origin and representing different professional fields. Each of the proposed items was assessed using a five-point scale, and open-ended questions, to modify or propose items. Descriptive analysis was performed of the sample and the items, applying criteria of validation/elimination. RESULTS: The first round had a response rate of 83.3% and validated 75 of the 96 proposed items; the second had a response rate of 80%, and validated the 21 newly created items, concluding the panel of experts. CONCLUSIONS: We present an instrument to measure self-perception of family health status, from a nursing perspective. This may be an advance in scientific knowledge, to facilitate the assessment of the state of health of the family unit, enabling detection of alterations, and to facilitate interventions to prevent consequences to the family unit and its members. It can be used in clinical care, research or teaching. OBJETIVO: Comprobar la validez de contenido de la escala de Autopercepción del Estado de Salud Familiar. MÉTODO: Estudio de validación de instrumento con panel Delphi on-line como técnica de consenso. Se seleccionaron intencionalmente 18 expertos/as en el tema, de origen multidisciplinar y de diferentes ámbitos profesionales. Cada uno de los ítems propuestos fue valorado mediante una escala de cinco puntos, y mediante preguntas abiertas, para modificar o proponer ítems. Se realizó análisis descriptivo de la muestra y de los ítems, aplicando criterios de estimación/desestimación. RESULTADOS: La primera ronda tuvo una tasa de respuesta del 83,3% y se estimaron 75 ítems de los 96 propuestos; la segunda tuvo una tasa de respuesta de 80%, y se estimaron los

  8. Feline immunodeficiency virusinfection: a comparative study of different diagnostic techniques Infecção pelo vírus da imunodeficiência felina: estudo comparativo de diferentes técnicas de diagnóstico

    Directory of Open Access Journals (Sweden)

    E. Mortola

    2004-02-01

    Full Text Available This study evaluated an indirect immunofluorescence assay (IFA to detect feline immunodeficiency virus infection (FIV antibody in a comprehensive epidemiological survey of FIV in Argentina. IFA modified in our laboratory, was compared with two other immunoassays, western blot (WB and a sandwich immunochromatographic commercial kit (SI, and also with a direct polymerase chain reaction (PCR method that detects proviral DNA. IFA showed to be a test with high sensitivity and specificity, and could be useful as a diagnostic tool in epidemiological studies. The presence of a low percentage of results with non-specific reactivity in the IFA could be resolved with further testing or use of an alternative method.Avaliou-se a técnica de imunofluorescência indireta (IFA na detecção de anticorpos contra o vírus da imunodeficiência felina (FIV numa pesquisa epidemiológica do FIV na Argentina. A IFA foi modificada e comparada com duas outras técnicas imunológicas: western blot (WB e imunocromatografia em camadas (SI com kit comercial e também com reação em cadeia de polimerase (PCR para detecção do DNA proviral. A IFA mostrou ser um teste com alta sensibilidade e especificidade e poderá ser empregada como ferramenta útil em estudos epidemiológicos. A baixa porcentagem de reatividade não específica pode ser esclarecida com testes mais avançados ou usando métodos alternativos.

  9. Nova técnica de transferência de cordas para sustentação das cúspides da valva mitral, após abertura completa de suas comissuras New technique for transference of chordae tendinae following mitral commissurotomy

    Directory of Open Access Journals (Sweden)

    José Alberto Caliani

    1988-08-01

    Full Text Available Desde 1983, 40 pacientes consecutivos, portadores de estenose mitral com alterações subvalvares, tais como: fusão e encurtamento das cordas, associadas a sinéquia dos músculos papilares, foram submetidos a comissurotomia mitral a "céu aberto". Com o intuito de ganhar área efetiva maior de abertura da valva mitral (sem restrições, as comissuras foram abertas, amplamente, às vezes não respeitando as cordas que sustentam as cúspides. A insuficiência mitral provocada, em 4 casos, como conseqüência, foi corrigida mediante a transferência de 2 a 6 cordas, ao nível da borda livre da cúspide anterior, ou posterior, da valva, na região das comissuras. A presença de uma regurgitação central por falha na coaptação das cúspides valvares, foi tratada, em 12 casos, com o implante de anel profético de Carpentier. As anomalias do aparelho subvalvar foram abordadas pelas técnicas convencionais: desbridamento, ressecção e abertura dos músculos papilares. Dos 38 sobreviventes, 32 não apresentam sopro de regurgitação mitral e os 6 restantes, apenas sopro sistólico de +/+ +. A avaliação pós-operatória, mediante ecocardiografia bidemensional, demonstrou abertura valvar satisfatória e ausência de estenose residual. Os pacientes que apresentam sopro sistólico mitral residual foram estudados com Doppler, concluindo que se trata de regurgitação bem localizada e sem repercussão hemodinâmica. Esta nova técnica operatória pode ser "extensível" ao tratamento do prolapso da valva mitral.Since 1983, 40 consecutive patients with mitral stenosis and significant disease of the subvalvular apparatus underwent open heart mitral commissurotomy. The aim of the study was to evaluate the effects of an unrestricted dilatation of the two commissures followed by repair of the subsequent mitral regurgitation. The mitral regurgitation created by this procedure in 24 cases was corrected by transferring 2 to 6 chordae tendinae to the free border

  10. Use of castor oil polyurethane in an alternative technique for medial patella surgical correction in dogs Utilização do poliuretano de mamona em técnica alternativa de correção cirúrgica da luxação medial de patela em cães

    Directory of Open Access Journals (Sweden)

    Fabrício de Oliveira Frazilio

    2006-01-01

    Full Text Available PURPOSE: Comparative morphologic study of utilization of castor oil polymer in dogs joints, as an alternative technique to autogenous graft, in surgical correction of medial patella luxation. METHODS:Twelve adult dogs, of both sexes, were randomly allocated to two different groups of six animals each. Group I (biopolymer consisted of the deepening of the right femoral troclea, with the implantation of the biopolymer prothesis, and compared to group II (control which consisted of the conventional trocleoplastia technique with wedged cut of the left femoral troclea. The dogs were sacrified after 30 or 90 days and the anathomic peaces were analyzed macro and microscopically. Qui square and Wilcoxon tests were used for the statistic analyses of the results, considering probability of 5%. RESULTS: It was not observed bony integration on the castor oil polymer group. There was resorption of the graft along experimental period and absence of inflammatory cells in the studied periods. CONCLUSION: Castor oil polymer assisted cicatrisation process, was biocompatible without inflammation, and it can be used in joints as an alternative for bony filling.OBJETIVO: Estudo morfológico do implante da prótese de polímero de mamona em articulações de cães, como técnica alternativa ao enxerto ósseo autógeno na correção cirúrgica da luxação medial de patela. MÉTODOS: Doze cães adultos, de ambos os sexos, foram distribuídos aleatoriamente em dois grupos de 6 animais. No grupo I (poliuretano foi feito o aprofundamento da tróclea femoral direita com prótese de polímero de mamona, que foi comparado com o grupo II (controle sendo feita a trocleoplastia por ressecção em cunha da tróclea femoral esquerda. Os animais foram sacrificados após 30 e 90 dias e as peças anatômicas foram avaliadas macro e microscopicamente. O teste do quiquadrado e o teste não-paramétrico de Wilcoxon foram utilizados para a análise estatística dos resultados. Fixou

  11. Dismantling techniques

    International Nuclear Information System (INIS)

    Wiese, E.

    1998-01-01

    Most of the dismantling techniques used in a Decontamination and Dismantlement (D and D) project are taken from conventional demolition practices. Some modifications to the techniques are made to limit exposure to the workers or to lessen the spread of contamination to the work area. When working on a D and D project, it is best to keep the dismantling techniques and tools as simple as possible. The workers will be more efficient and safer using techniques that are familiar to them. Prior experience with the technique or use of mock-ups is the best way to keep workers safe and to keep the project on schedule

  12. Dismantling techniques

    Energy Technology Data Exchange (ETDEWEB)

    Wiese, E.

    1998-03-13

    Most of the dismantling techniques used in a Decontamination and Dismantlement (D and D) project are taken from conventional demolition practices. Some modifications to the techniques are made to limit exposure to the workers or to lessen the spread of contamination to the work area. When working on a D and D project, it is best to keep the dismantling techniques and tools as simple as possible. The workers will be more efficient and safer using techniques that are familiar to them. Prior experience with the technique or use of mock-ups is the best way to keep workers safe and to keep the project on schedule.

  13. Atualização da anatomia do mecanismo extensor do joelho com uso de técnica de visualização tridimensional Updating of the anatomy of the extensor mechanism of the knee using a three-dimensional viewing technique

    Directory of Open Access Journals (Sweden)

    Diego Costa Astur

    2011-10-01

    Full Text Available O mecanismo extensor do joelho é uma estrutura complexa formada pelo músculo e tendão quadricipital, a patela, o tendão patelar e os ligamentos que os circundam e auxiliam na estabilização do joelho. Através do uso de técnica de visualização tridimensional de imagens do aparelho extensor do joelho pretendemos mostrar de forma didática as estruturas que compõem este complexo ósteo-músculo-ligamentar. Dissecção anatômica do joelho com ênfase nas estruturas do seu mecanismo extensor foi realizada seguida de fotografias com câmera e lentes adequadas para simulação da visão humana através de técnica de construção de imagem tridimensional. Em seguida, com a ajuda de software apropriado, as duas imagens da mesma estrutura de diferentes ângulos simulando a visão humana são sobrepostas com adição de camada polarizante, concluindo a construção da imagem anaglífica. As principais estruturas do mecanismo extensor do joelho podem ser observadas com efeito tridimensional. Dentre os principais benefícios relacionados a esta técnica, destacamos, além do ensino e estudo da anatomia musculoesquelética, o potencial uso em treinamento de procedimentos cirúrgicos e a realização de imagens em exames diagnósticos.The knee extensor mechanism is a complex structure formed by the quadriceps muscle and tendon, the patella, the patellar tendon and the ligaments that surround and help stabilize the knee. Through using a three-dimensional viewing technique on images of the knee extensor apparatus, we aimed to didactically show the structures that compose this bone-muscle-ligament complex. Anatomical dissection of the knee with emphasis on the structures of its extensor mechanism was performed, followed by taking photographs using a camera and lenses suitable for simulating human vision, through a technique for constructing three-dimensional images. Then, with the aid of appropriate software, pairs of images of the same structure from

  14. Análise radiográfica computadorizada da reabsorção radicular apical após a utilização de duas mecânicas ortodônticas Computer-assisted radiographic evaluation of apical root resorption following orthodontic treatment with two different fixed appliance techniques

    Directory of Open Access Journals (Sweden)

    Eduardo César Almada Santos

    2007-02-01

    Full Text Available OBJETIVO: a reabsorção radicular apical é uma condição comumente observada durante e após o tratamento ortodôntico e fatores como tipo de aparelhagem ortodôntica utilizada, magnitude das forças aplicadas e duração do tratamento podem estar relacionados ao processo de arredondamento do ápice radicular. Buscou-se avaliar, por meio de imagens radiográficas computadorizadas, a quantidade de reabsorção no ápice radicular, quando da utilização de duas diferentes técnicas de mecânica ortodôntica fixa: Edgewise com acessórios padrão e Edgewise com acessórios totalmente programados. METODOLOGIA: a amostra constituiu-se de 20 pacientes tratados pelo mesmo profissional na Clínica de Ortodontia da Faculdade de Odontologia de Araçatuba - UNESP. Os pacientes foram divididos em dois grupos: grupo 1 (Tratados com Edgewise com acessórios padrão e fios de aço e grupo 2 (Tratados com Edgewise com acessórios totalmente programados e fios de níquel-titânio. A avaliação radiográfica digital foi realizada por um único operador por meio de exposições radiográficas digitais feitas no início do tratamento ortodôntico, após retração de caninos e final de tratamento, utilizando o sistema de escores proposto por Levander e Malmgren (1988. RESULTADOS E CONCLUSÕES: a análise dos escores permitiu concluir que o tratamento ortodôntico empregando a técnica Edgewise com acessórios totalmente programados e fios de níquel-titânio apresentou menores graus de reabsorção radicular apical, em comparação à técnica Edgewise com acessórios padrão e fios de aço. Observou-se que, independentemente da técnica empregada, o tratamento ortodôntico como um todo apresentou um grau moderado de reabsorção radicular apical.AIM: external apical root resorption is frequently observed during and after orthodontic treatment and can be related to factors such as mechanical factors, magnitude of forces and treatment time with fixed appliances

  15. Tópicos da teoria da relatividade

    OpenAIRE

    Fragata, Paulo Renato Ferreira

    2013-01-01

    Dissertação de Mestrado, Matemática para Professores, 25 de Outubro 2013, Universidade dos Açores. Qualquer descrição física da natureza tem por base a especificação da posição e do instante em que decorre determinado acontecimento. Para tal, é necessário recorrer a um sistema de coordenadas, escolhido por cada observador, do modo que ele achar mais pertinente. Dada a generalidade na escolha do sistema de coordenadas, é útil conhecer as regras que nos permitem comparar cálculos feitos em d...

  16. Purification and biochemical characterization of a 22-kDa stable cysteine- like protease from the excretory-secretory product of the liver fluke Fasciola hepatica by using conventional techniques.

    Science.gov (United States)

    Hemici, Ahmed; Benerbaiha, Roumaila Sabrina; Bendjeddou, Dalila

    2017-11-15

    This study describes the purification and characterization of a stable protease activity isolated from Fasciola hepatica adult worms maintained in vitro by employing acetone precipitation (40-60%) followed by a gel filtration through Sephadex G-100 and DEAE- cellulose ion exchange column. Through this three-step purification, the enzyme was purified 11-fold with a specific activity of 1893.9U/mg and 31.5% recovery. After the final ultrafiltration step, the purification fold was increased up to 13.1 and the overall activity yield reached a rate of 18.8%. The MW of the purified protease was estimated by reducing SDS-PAGE to be 22kDa while the proteolytic activity detection was carried out by zymography on non-denaturing SDS-PAGE containing the casein as substrate. Using this substrate, the protease showed extreme proteolytic activity at pH 5.5 and temperature 35-40°C and was highly stable over a wide range of pH, from 5.0 to 10.0. In addition to its preference for the Z-Phe-Arg-AMC fluorogenic substrate resulting in maximum proteolytic activity (99.7%) at pH 7.0, the pure protease exhibited highest cleavage activity against hemoglobin and casein substrates at pH 5.5 (85.6% and 82.8%, respectively). The K m values obtained for this protease were 5.4, 13, 160 and approximately 1000μM using respectively the fluorogenic substrate Z-Phe-Arg-AMC, hemoglobin, casein and albumin. The protease activity was completely inhibited either by E-64 inhibitor (5mM) or iodoacetamide (10mM), indicating its cysteine nature. The usefulness of the purified protease as an antigen was studied by immunoblotting. Thus, sera from sheep experimentally infected with F. hepatica recognized the protease band at 2 weeks post-infection (WPI) and strongly at 7 WPI. The early detection of antibodies anti- F. hepatica suggests the application of this molecule as a specific epitope for the serodiagnosis of fascioliasis disease. Copyright © 2017 Elsevier B.V. All rights reserved.

  17. Infecção de prótese vascular em cirurgia da aorta torácica: revisão da experiência e relato de caso tratado por técnica não convencional Vascular prosthesis infection in thoracic aorta surgery: review of the experience and a case report illustrating treatment with an unconventional technique

    Directory of Open Access Journals (Sweden)

    Ronaldo Ducceschi Fontes

    2004-03-01

    Full Text Available Relatamos o caso de uma paciente de 37 anos de idade, que há cinco anos havia sido submetida à operação de Bental-de Bono em nosso serviço e retornou com dor de forte intensidade no toráx, sendo diagnosticada dissecção aguda de aorta do tipo III e tratada clinicamente. Um ano após esse episódio houve expansão dessa dissecção e a paciente foi submetida à cirurgia com interposição de prótese de dacron em aorta descendente. No pós-operatório imediato houve broncopneumonia esquerda e a paciente recebeu alta em boas condições e afebril. Após um mês da alta, retornou com febre e toxemia. Com diagnóstico de empiema pleural, foi submetida à toracotomia exploradora que não confirmou esse diagnóstico, havendo apenas intenso espessamento pleural. Quatro meses após a toracotomia exploradora, foram isolados Klebsiella pneumoniae e Enterobacter sp na hemocultura. A ressonância magnética revelou imagens compatíveis com infecção peri-prótese. Com esse quadro clínico e laboratorial foi indicada a remoção do enxerto e derivação axilo-bifemoral. A operação foi realizada com sucesso, a paciente recebeu alta em boas condições e continua fazendo controle ambulatorial e, atualmente, encontra-se com 57 meses de evolução sem complicações. São discutidos os métodos empregados para o diagnóstico e tratamento da infecção de prótese na cirurgia da aorta torácica.We report the case of a 37-year-old-female patient who had undergone a Bentall procedure at our service and returned with intense chest pain and acute aortic dissection type III, which was diagnosed and clinically treated. One year after this episode, this dissection expanded, and the patient underwent surgery with interposition of a Dacron graft in the descending aorta. In the immediate postoperative period, the patient experienced left bronchopneumonia and was discharged afebrile and in good condition. One month after discharge, she returned with fever and

  18. Study of immobilization of radioactive wastes in asphaltic matrices and elastomeric residues by using microwave technique; Estudo da imobilizacao de rejeitos radioativos em matrizes asfalticas e residuos elastomericos utilizando a tecnica de microondas

    Energy Technology Data Exchange (ETDEWEB)

    Caratin, Reinaldo Leonel

    2007-07-01

    In the present work, the technique of microwave heating was used to study the immobilization of low and intermediate activity level radioactive waste, such as spent ion exchange resin used to remove undesirable ions of primary circuits of refrigeration in water refrigerated nuclear reactors, and those used in chemical and radionuclide separation columns in the quality control of radioisotopes. Bitumen matrices reinforced with some kinds of rubber (Neoprene{sup R}, silicon and ethylene-vinyl-acetate), from production leftovers or scraps, were used for incorporation of radioactive waste. The samples irradiation was made in a home microwave oven that operates at a frequency of 2.450 MHZ with 1.000 W power. The samples were characterized by developing assays on penetration, leaching resistance, softening, flash and combustion points, thermogravimetry and optical microscopy. The obtained results were compatible with the pattern of matrices components, which shows that technique is a very useful alternative to conventional immobilization methods and to those kinds of radioactive waste. (author)

  19. Predição da degradação da matéria seca pelo volume de gases utilizando a técnica in vitro semi-automática de produção de gases Prediction of dry matter degradation from volume of gas production using the in vitro semi-automatic gas production technique

    Directory of Open Access Journals (Sweden)

    Ú.T. Nogueira

    2006-10-01

    Full Text Available Estimou-se a degradação da matéria seca (DMS via produção de gases (PG por meio de equações. Foram agrupados dados de volume de gases e DMS de oito forrageiras (Brachiaria brizantha, Brachiaria decumbens, feno de Cynodon spp, silagem de milho, silagem de milheto, sorgo de corte, capim-elefante e cana-de-açúcar e de milho em grão. Os dados de DMS obtidos em laboratório foram comparados à DMS obtida pelas equações de regressão. Apesar dos altos coeficientes de determinação, os resultados demonstraram a impossibilidade de estimar a DMS via PG pelas equações geral, de dois e de três pontos.The dry matter degration (DMD was estimated through volume of gas produced (GP during the in vitro fermentation. The DMD from eight forages (Brachiaria brizantha, Brachiaria decumbens, cynodon hay, maize silage, Pennisetum glaucon, sorghum, elephant grass and sugarcane and corn grain were obtained and were compared with the DMD estimated using regression equations. The results showed the GP can not predict the DMD due to inocula effects, chemical composition of substrate or losses of particles of soluble material during filtration process.

  20. Translation Techniques

    OpenAIRE

    Marcia Pinheiro

    2015-01-01

    In this paper, we discuss three translation techniques: literal, cultural, and artistic. Literal translation is a well-known technique, which means that it is quite easy to find sources on the topic. Cultural and artistic translation may be new terms. Whilst cultural translation focuses on matching contexts, artistic translation focuses on matching reactions. Because literal translation matches only words, it is not hard to find situations in which we should not use this technique.  Because a...

  1. Use of the HRICP-MS technique for the evaluation of boron isotopes in Eucalitpus plants; Uso da tecnica HRICP-MS na avaliacao dos isotopos de boro em eucalipto

    Energy Technology Data Exchange (ETDEWEB)

    Mattiello, Edson Marcio; Ruiz, Hugo Alberto; Silva, Ivo Ribeiro da, E-mail: mattiello@ufv.b [Universidade Federal de Vicosa (UFV), MG (Brazil). Dept. de Solos; Sarkis, Jorge Eduardo de Souza [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2011-07-01

    The {sup 10}B isotope tracer technique is essential to study the B mobility in plants. Factors that can influence the quality of measured B isotope ratios were optimized experimentally using High Resolution Inductively Coupled Plasma Mass Spectrometry (HRICP-MS). An isotopically certified standard (NIST SRM-951) was used. The best combination was obtained using a resolution of 400, a RF power of 1250 W, followed by 15 measurements over a 10-s integration period each (15*10). Utilizing this approach it was possible to obtain a precision of 0.3 % in standard material and 2z % in the experimental samples. The results show the importance of establishing optimized work conditions before carrying out the analytical series. (author)

  2. Corrosion mapping in ducts using the automated ultrasonic technique C-Scan - correlation with results given by pig inspection; Mapeamento de corrosao em dutos atraves da tecnica ultrassonica C-Scan

    Energy Technology Data Exchange (ETDEWEB)

    Feres Filho, Pedro; Moura, Nestor Carlos de [Physical Acoustics South America (PASA), Sao Paulo, SP (Brazil)

    2005-07-01

    In-service inspection has received diverse contributions from technologies and documents with the objective of maximizing equipment availability and minimizing inadequate repairs. Amongst the available technologies, there are the automated ultrasound tests, in the B and C-scan versions. This paper describes an evaluation methodology based on the correlation between the test techniques of instrumented electromagnetic PIG and automated ultrasound, both applied with the purpose of detecting and mapping areas with corrosion in pipes for oil transport. The main objective of the application of the C-scan methodology, in this case, was the measuring and detailing of the corroded area, thus providing an adequate maintenance plan through the substitution or installation of a double gutter. The result demonstrates the correlation between the measurements taken by the PIG and the sizing of the regions done using the C-scan method, consisting of the length, width and thickness values in the points affected by the corrosion. (author)

  3. Comparative studies of Yersinia pestis outer membrane isolation techniques and their potential use in plague epidemiology Estudo comparativo de técnicas de isolamento de membrana externa de Yersinia pestis e seu uso na epidemiologia da peste

    Directory of Open Access Journals (Sweden)

    Frederico Guilherme Coutinho Abath

    1990-04-01

    Full Text Available In the present study three techniques for obtaining outer membrane enriched fractions from Yersinia pestis were evaluated. The techniques analysed were: differential solubilization of the cytoplasmic membrane with Sarkosyl or Triton X-100, and centrifugation in sucrose density gradients. The sodium dodecyl-sulfate polyacrylamide gel electrophoresis (SDS-PAGE of outer membrane isolated by the different methods resulted in similar protein patterns. The measurement of NADH-dehydrogenase and succinate dehydrogenase (inner membrane enzymes indicated that the outer membrane preparations obtained by the three methods were pure enough for analytical studies. In addition, preliminary evidences on the potential use of outer membrane proteins for the identification of geographic variants of Y. pestis wild isolates are presented.No presente estudo três técnicas para isolamento de frações enriquecidas em membrana externa de Y. pestis foram avaliadas. As técnicas utilizadas foram: centrifugação em gradiente de densidade em sacarose e solubilização diferencial com Sarkosyl ou Triton X-100. A análise por eletroforese em gel de poliacrilamida na presença de dodecil sulfato de sódio (SDS-PAGE das membranas externas extraídas pelos diferentes métodos evidenciou perfis protéicos semelhantes. A determinação das atividades de NADH-desidrogenase e succinato-desidrogenase (enzimas de membrana interna indicou que todas as preparações estudadas eram adequadas a estudos analíticos. Obteve-se evidências preliminares sobre o possível uso de perfis protéicos de membrana externa na identificação de variantes geográficos entre isolados selvagens de Y. pestis.

  4. Analysis of the chemical elements behavior in leaves infected with fumagina employing X-ray fluorescence technique; Analise do comportamento de elementos quimicos em folhas infectadas com fumagina atraves da tecnica de fluorescencia de raios-X

    Energy Technology Data Exchange (ETDEWEB)

    Blonski, Maria Selia

    2002-02-01

    Fumagina is produced by the Capnodium fungi, a mushroom from Dothideales order, that lives associated with the yellow aphid (Monelliopsis pecanis), excreting a heavy load of a sugared substance that provides the sooty fungus development, covering, in some cases the totality, of leaves, fruits and branches surfaces. One of the big problems caused by this disease is the physic photosynthesis stuckness, reducing in 98% the active photosynthesis radiation and in 70% the net photosynthesis. This photosynthesis reduction affects the plants carbohydrate reservoirs, resulting in reduced and bad qualified crops. It was employed the Energy Dispersion X-Ray Fluorescence Technique (EDXRF) to study the fumagina disease. The measurements were realized with infected and healthy leaves of citric plants (orange and lemon trees), collected at the Farm School of the State University of Londrina, and also leaves of icsora plant from Piracicaba-SP. Through this technique it was observed a metabolic disorder related to Fe and Ca elements. By comparing the EDXRF spectra of the healthy plant leaves with the infected ones, it was verified that the concentration of Ca is higher than the concentration Fe in leaves of healthy plants, while for the leaves of plants infected with fumagina, it was observed a higher concentration of Fe. Employing EDXRF and the emission/transmission method for the matrix effect correction, samples of the citric plants were also analysed in pellet. The elements K, Ca, Ti, Mn , Fe, Cu and Zn were quantified. It was verified a higher Fe concentration in fumagina samples compared to the samples without fumagina. For all the elements of interest the minimum level of detection found was at the order of {mu}g g{sup -1}. (author)

  5. Carbon thin films deposited by the magnetron sputtering technique using cobalt, copper and nickel as buffer-layers; Filmes finos de carbono depositados por meio da tecnica de magnetron sputtering usando cobalto, cobre e niquel como buffer-layers

    Energy Technology Data Exchange (ETDEWEB)

    Costa e Silva, Danilo Lopes

    2015-11-01

    In this work, carbon thin films were produced by the magnetron sputtering technique using single crystal substrates of alumina c-plane (0001) and Si (111) and Si (100) substrates, employing Co, Ni and Cu as intermediate films (buffer-layers). The depositions were conducted in three stages, first with cobalt buffer-layers where only after the production of a large number of samples, the depositions using cooper buffer-layers were carried out on Si substrates. Then, depositions were performed with nickel buffer layers using single-crystal alumina substrates. The crystallinity of the carbon films was evaluated by using the technique of Raman spectroscopy and, then, by X-ray diffraction (XRD). The morphological characterization of the films was performed by scanning electron microscopy (SEM and FEG-SEM) and high-resolution transmission electron microscopy (HRTEM). The XRD peaks related to the carbon films were observed only in the results of the samples with cobalt and nickel buffer-layers. The Raman spectroscopy showed that the carbon films with the best degree of crystallinity were the ones produced with Si (111) substrates, for the Cu buffers, and sapphire substrates for the Ni and Co buffers, where the latter resulted in a sample with the best crystallinity of all the ones produced in this work. It was observed that the cobalt has low recovering over the alumina substrates when compared to the nickel. Sorption tests of Ce ions by the carbon films were conducted in two samples and it was observed that the sorption did not occur probably because of the low crystallinity of the carbon films in both samples. (author)

  6. Tratamento de aneurisma da artéria renal por embolização e técnica de remodelamento de colo: relato de caso Endovascular treatment of renal artery utilizing embolization and aneurism neck remodeling technique: case report

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    Luis Carlos Mendes de Brito

    2011-06-01

    Full Text Available O tratamento endovascular dos aneurismas de artéria renal tem sido descrito como alternativa à cirurgia convencional. Relatamos o caso de uma paciente com um aneurisma de artéria renal complexo à direita que apresentava hipertensão arterial de difícil controle. O tratamento endovascular foi realizado com a técnica de remodelagem de colo (técnica de Moret, ou técnica de embolização assistida por balão. A paciente obteve normalização da pressão arterial após o procedimento sem recidiva dos sintomas ou necessidade do uso de drogas anti-hipertensivas.Endovascular treatment of renal artery aneurysms has been described as an alternative to conventional surgery. We report the case of a patient with complex renal artery aneurysm on the right kidney who had hard-to-control arterial hypertension. Endovascular treatment was performed with the aneurysm neck remodeling technique (Moret technique, or balloon-assisted coil embolization. The patient achieved blood pressure normalization after the procedure without recurrence of symptoms or need for antihypertensive drugs.

  7. Aplicabilidade da técnica de cell block na avaliação citológica do conteúdo de lesões de aspecto cístico dos maxilares Applicability of cell block technique for cytological evaluation of biological material collected from maxillary cystic lesions

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    Grasieli de Oliveira Ramos

    2012-04-01

    Full Text Available INTRODUÇÃO: A busca por novos métodos que auxiliem e simplifiquem de maneira eficaz o diagnóstico de lesões maxilares, cistos e tumores, objetiva beneficiar os pacientes e facilitar a atuação dos profissionais da área de diagnóstico bucal. Além dos dados clínicos, radiográficos e histopatológicos classicamente utilizados nos protocolos de investigação das lesões maxilares, a adaptação de técnicas já consagradas na medicina pode ser de grande valia. A técnica de cell block se propõe a auxiliar nesse processo, pois consiste na análise citológica de materiais, efusões e líquidos, coletados de lesões passíveis de punção aspirativa, como cistos e tumores císticos dos maxilares. OBJETIVO: Demonstrar a aplicabilidade da técnica de cell block para avaliação citológica de material biológico coletado a partir de lesões císticas dos maxilares. RESULTADOS: Das 20 lesões, das quais o conteúdo foi processado pela técnica, a avaliação citológica de cinco casos de tumores odontogênicos ceratocísticos (TOCs demonstrou a presença predominante de ceratina, sempre com áreas de paraceratina. Nos demais casos (cinco cistos dentígeros, cinco cistos radiculares e cinco cistos residuais foi observada a presença de hemácias, células inflamatórias e fendas de cristais de colesterol. CONCLUSÃO: A avaliação citológica, a partir da técnica de cell block, foi útil no estabelecimento do diagnóstico diferencial entre TOC e demais lesões estudadas, cistos radicular, residual e dentígero.INTRODUCTION: The search for new methods that aid and optimize the diagnosis of cystic and tumoral maxillary lesions aims to benefit both patients and professionals from oral diagnosis. In addition to clinical, radiographic and histological findings traditionally used in research protocol for maxillary lesions, the adaptation of widely used medical techniques may be very helpful. The cell block procedure streamlines this process

  8. Modified technique to increase nostril cross-sectional area after using rib and septal cartilage graft over alar nasal cartilages Técnica modificada para aumentar a área seccional externa da narina após o uso de enxerto cartilaginoso de costela e septo sob as cartilagens alares nasais

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    Marcelo Wulkan

    2012-10-01

    Full Text Available PURPOSE: Describe a modified technique to increase nostril cross-sectional area using rib and septal cartilage graft over alar nasal cartilages. METHODS: A modified surgical technique was used to obtain, carve and insert cartilage grafts over alar nasal cartilages. This study used standardized pictures and measured 90 cadaveric nostril cross-sectional area using Autocad®; 30 were taken before any procedure and 60 were taken after grafts over lateral crura (30 using costal cartilage and 30 using septal cartilage. Statistical analysis were assessed using a model for repeated measures and ANOVA (Analysis of Variance for the variable "area". RESULTS: There's statistical evidence that rib cartilage graft is more effective than septal cartilage graft. The mean area after the insertion of septal cartilage graft is smaller than the mean area under rib graft treatment (no confidence interval for mean difference contains the zero value and all P-values are below the significance level of 5%. CONCLUSIONS: The technique presented is applicable to increase nostril cross section area in cadavers. This modified technique revealed to enhance more nostril cross section area with costal cartilage graft over lateral crura rather than by septal graft.OBJETIVO: Descrever uma técnica modificada para se aumentar a área seccional externa da narina com cartilagem septal e costal acima das cartilagens alares nasais. MÉTODOS: Utilizou-se uma técnica cirúrgica modificada para obter, esculpir e inserir enxertos de cartilagem sobre as cartilagens alares. Realizou-se fotos padronizadas e mensuração de 90 áreas seccionais externas de narina em cadáveres com Autocad®; 30 antes sem procedimento; 60 após a inclusão de enxertos sob a cruz lateral (30 usando cartilagem costal e 30 usando cartilagem septal. A análise estatística foi feita com um modelo de medidas repetidas e ANOVA para a variável "área" RESULTADOS: Existe evidência estatística de que o enxerto de

  9. Application of the linear load normalization technique in specimens SE(T) for the evaluation of structural integrity in conducting ducts of gas and oil; Aplicacao da tecnica de normalizacao linear da carga em especimes SE(T) para a avaliacao de integridade estrutural em dutos condutores de gas e petroleo

    Energy Technology Data Exchange (ETDEWEB)

    Piovatto, R.R.; Carvalho, A.L.M.; Bose Filho, W.W.; Spinelli, D.; Rugieri, C. [Universidade de Sao Paulo (USP), Sao Carlos, SP (Brazil); Universidade de Sao Paulo (USP), SP (Brazil). Escola Politecnica], e-mail: betaopiovatto@gmail.com

    2006-07-01

    This aim of this work is to evaluate the fracture toughness of pipe lines under high internal pressure, used in the petroliferous industry for transportation of gas and oil. These ducts are produced from high strength low alloy steels, classified as API X60. Therefore, to simulate the stress and strain fields ahead of crack, the SE(T) specimens has been point out as the best specimen geometry. The linear load normalization technique, LLN, has been showed as a promissory technique for obtaining the J-R resistance curves. The J values were obtained following the ASTM 1820 and 1152 standards, with the coefficients modified for this specimen geometry. Side groves were executed to avoid crack tunneling and to maintaining the crack on the plane perpendicular to the loading direction. The J-R curves obtained are compatible for high ductility steels. However, the observed J values seems to high, and the factors affecting this result are discussed in this work. (author)

  10. Determinação da fixação biológica de nitrogênio no amendoim forrageiro (Arachis spp. por intermédio da abundância natural de 15N Determination of biological nitrogen fixation by the forage groundnut (Arachis spp. using the 15N natural abundance technique

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    Cesar Heraclides Behling Miranda

    2003-12-01

    Full Text Available Quantificou-se a fixação biológica de nitrogênio (FBN em cinco acessos de Arachis pintoi (BRA31534, BRA31828, BRA31796, BRA15121 e BRA30333 e dois de A. repens (BRA31801 e BRA31861. Os mesmos foram estabelecidos em um solo Latosolo Vermelho Escuro sujeito a inundação estacional, sendo a FBN estimada segundo a técnica da abundância natural do isótopo 15N (d15N. Estolões dos acessos foram plantados em novembro de 1999, em parcelas de 2,0 m x 2,0 m, com quatro repetições, distribuídas em blocos ao acaso. A massa verde das plantas acima de cinco centímetros do solo foi colhida em janeiro de 2000 e seca em estufa a 65ºC até peso constante, sendo posteriormente pesada e moída para análise dos conteúdos em N e d15N, em espectrômetro de massa. Verificaram-se diferenças significativas entre os genótipos quanto à produção de matéria seca (MS e N total, sobressaindo-se BRA31534 e BRA31828, com produções de 4,2 t/ha e conteúdos totais de N de 102 e 110 kg/ha, respectivamente. Os acessos BRA30333 e BRA31861 produziram apenas 2,6 t de MS/ha, com 59 e 65 kg/ha de N total, respectivamente. As taxas de FBN dos acessos testados, medidas por comparação dos seus teores de d15N com os de plantas não fixadoras crescendo na mesma área, variaram de 36% (BRA15121 a 90% (BRA31828 do N total das plantas, equivalente a 26 e 99 kg de N/ha, respectivamente. Verificou-se correlação positiva e significativa (r = 0,92, pThe biological nitrogen fixation (BNF of five Arachis pintoi (BRA31534, BRA31828, BRA31796, BRA15121 E BRA30333 and two A. repens (BRA31801 e BRA31861 accessions, grown in a Dark Red Latosol prone to seasonal flooding was evaluated using the 15N natural abundance method (d15N. Stolons of each accession were planted in November 1999, in plots of 2.0 m by 2.0 m, with four replications allotted to randomized blocks. Plant mass above five cm was harvested in January 2000. There were significant differences among the tested

  11. MACIEZ DA CARNE BOVINA

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    Antonio Bento Mancio

    2006-10-01

    Full Text Available Dentre as características de qualidade da carne bovina, a maciez assume posição de destaque, sendo considerada a característica organoléptica de maior influência na aceitação da carne por parte dos consumidores. A dureza da carne pode ser dividida em dureza residual, causada pelo tecido conjuntivo e outras proteínas do estroma, e dureza de actomiosina, causada pelas proteínas miofibrilares. Dentre os fatores que influenciam a maciez da carne, podem ser destacados a genética, a raça, a idade ao abate, o sexo, a alimentação, o uso de agentes hormonais (?-adrenérgicos e os tratamentos post-mortem. A qualidade final da carne é resultante de tudo o que aconteceu com o animal durante toda a cadeia produtiva. Devem-se assegurar procedimentos adequados de transporte, armazenamento, manipulação, exposição e preparo da carne, a fim de se obter um produto de melhor qualidade. PALAVRAS-CHAVE: Calpaínas, calpastatina, qualidade da carne, rigor mortis, tecido muscular.

  12. Aplicação de métodos estatísticos na otimização da densidade de empacotamento de distribuições de pós de alumina Optimization of the packing density of alumina powder distributions using statistical techniques

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    A. P. Silva

    2004-12-01

    Full Text Available Fatores como a distribuição granulométrica e a morfologia condicionam as propriedades físicas de sistemas particulados (e.g. misturas de pós, pastas, concretos refratários, entre as quais a densidade de empacotamento. Podem ser encontrados, na literatura, vários modelos para a otimização da distribuição de tamanhos de partículas que maximiza o empacotamento, todos desenvolvidos para sistemas de esferas perfeitas (e.g. Furnas, Andreasen, Alfred. Neste trabalho, pós de alumina comercial (reativa e tabular foram separados em nove frações granulométricas e, recorrendo a dois procedimentos distintos, construíram-se seis sistemas ternários diferentes e complementares de tamanhos de partículas. Usando a metodologia das superfícies de resposta e técnicas de análise estatística afins (programa de cálculo Statistica obteve-se, em ambos os casos, a distribuição granulométrica que maximiza a densidade de empacotamento. Por comparação com as distribuições granulométricas teóricas, ficou demonstrada a validade do modelo teórico de Alfred para esferas perfeitas. Os resultados obtidos demonstram, assim, que o efeito prejudicial da não esfericidade das partículas pode ser, na realidade, compensado pela otimização da distribuição granulométrica global.Particle size distribution and morphology are among the factors that affect the physical properties of particulate systems (e.g. powder mixtures, pastes, castable refractories. One such property is packing density. There are, in the literature, models that optimise particle size distributions for maximum packing density, all of them derived for spherical particles (e.g. Furnas, Andreasen, Alfred. In this work, commercial alumina powders (reactive and tabular were divided into nine particle size classes. Following two different approaches, the latter were used to build six different ternary systems of complementary particle sizes. Using the response surface methodology and

  13. Application of the total etching technique or self-etching primers on primary teeth after air abrasion Aplicação da técnica de condicionamento total ou de "primers" autocondicionantes em dentes decíduos após abrasão a ar

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    Fábio Renato Manzolli Leite

    2005-09-01

    Full Text Available Since the use of air abrasion has grown in pediatric dentistry, the aim of this study was to evaluate, by means of shear bond strength testing, the need to use the total etching technique or self-etching primers on dentin of primary teeth after air abrasion. Twenty-five exfoliated primary molars had their occlusal dentin exposed by trimming and polishing. Specimens were treated by: Air abrasion + Scotchbond MultiPurpose adhesive (G1; 37% phosphoric acid + Scotchbond MP adhesive (G2; Clearfil SE (G3; Air abrasion + 37% phosphoric acid + Scotchbond MP adhesive (G4; Air abrasion + Clearfil SE (G5. On the treated surface, a cylinder of 2 mm by 6 mm was made using a composite resin (Z100. Duncan's test showed that: (G2 = G3 = G5 > (G1 = G4. The use of a self-etching primer on air abraded dentin is recommended to obtain higher bond strengths.Como o uso da abrasão a ar tem aumentado em odontopediatria, o objetivo deste trabalho foi avaliar a resistência ao cisalhamento da resina composta Z100 sobre a superfície dentinária de dentes decíduos após abrasionamento a ar associado ou não a técnica de condicionamento total (ácido fosfórico + Scotchbond Multi Purpose ou "primer" autocondicionante (Clearfil SE Bond. A superfície oclusal de 25 molares decíduos foi removida para exposição completa da superfície dentinária. Após polimento com lixas abrasivas, foram divididos em 5 grupos (5 espécimes em cada tratados por abrasão + adesivo Scotchbond (G1; condicionamento ácido + adesivo Scotchbond (G2; adesivo Clearfil (G3; abrasão a ar + condicionamento ácido + adesivo Scotchbond (G4; abrasão a ar + adesivo Clearfil (G5. Uma matriz bipartida foi adaptada à superfície dentinária e preenchida com resina composta. Após polimerização, corpos-de-prova de 2 mm x 6 mm foram obtidos. O teste de Duncan mostrou a desigualdade (G1 = G4 < (G2 = G3 = G5. Desse modo, conclui-se que, após o abrasionamento dentinário, deve ser utilizado o sistema de

  14. Coeficiente de cultura da lima-ácida tahiti no outono-inverno determinado por lisimetria de pesagem em Piracicaba - SP Crop coefficient of acid lime tahiti during autumn-winter period determined by weighing lysimeter technique in Piracicaba - SP, Brazil

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    Cícero R. A. Barboza Júnior

    2008-12-01

    Full Text Available O Brasil é o maior produtor mundial de citros, com destaque para o Estado de São Paulo, maior produtor nacional. Recentes estudos mostram que a área irrigada de citros em São Paulo tem aumentado significativamente nos últimos anos. Porém, a falta de informações sobre o manejo eficiente da irrigação na cultura de citros é uma das principais dificuldades enfrentadas pelos produtores. Com o intuito de atender a essa necessidade, este trabalho teve como objetivos determinar a evapotranspiração de uma planta adulta de limeira-ácida 'Tahiti' (Citrus latifolia Tan. e o coeficiente de cultivo (Kc no período seco (outono-inverno, utilizando a técnica de lisimetria de pesagem. O experimento foi realizado na ESALQ/USP em Piracicaba - SP, em área irrigada por gotejamento, com plantas espaçadas de 7 x 4 m, sendo cada planta atendida por quatro pontos de molhamento no solo, distribuídos de forma equidistantes entre si. Foi realizado o monitoramento climático, utilizando estação meteorológica automatizada, e a determinação da evapotranspiração da cultura por lisímetro de pesagem. Durante o período de estudo, o Kc variou entre 0,82 e 1,18, e a ETc variou entre 1,2 e 5,6.Brazil is the largest world producer of citrus crop, with São Paulo state leading as the largest national producer. Recent studies show that irrigated areas of citrus in the state have been increasing significantly in the last few years. However, lack of information on irrigation management related to this crop is one of the main problems encountered by the farmers. In order to help solve the above problem, the objective of this work was to determine the evapotranspiration of acid lime adult plant variety 'Tahiti' (Citrus latifolia Tan. and the crop coefficient during dry period (autumn - winter using a weighing lysimeter technique. The experiment was carried out at ESALQ/USP in Piracicaba - SP, Brazil, in a drip irrigated area with plant spacing of 7 x 4 m. Each

  15. GERONTOLOGIA: ESTADO DA ARTE

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    Vera M.A.Tordino Brandão

    2010-02-01

    Full Text Available O Programa de Gerontologia da PUC desenvolve pesquisas focando o ser na perspectiva do envelhecimento. As atividades são interdisciplinares e reúnem docentes, alunos e ex-alunos. Nesta mesa redonda apresentamos um panorama sobre estes estudos. Na área da educação e comunicação o foco está centrado na longevidade e na preparação e representação social da velhice. São ressaltadas como temáticas: a formação continuada de profissionais e pesquisadores; o significado da religiosidade/espiritualidade ao longo da trajetória, e sua repercussão na qualidade de vida do idoso; os programas sócio-educacionais para idosos e concepções sobre educação; o monitoramento da mídia na cobertura da crescente longevidade e seus impactos. Em identidade e modos de morar reflete-se sobre soluções planejadas e sua adequação para a inclusão do envelhecimento populacional como questão fundamental, que implica a elaboração de novas políticas, investigações e, especialmente, apresenta-se como questão a ser analisada, refletida e vivenciada pela sociedade em geral. Quanto à saúde, o Programa desenvolve várias pesquisas numa abordagem interdisciplinar tendo como objetos de estudo: a terapia assistida com animais direcionada a idosos com diagnóstico de Alzheimer; o acompanhamento terapêutico e o atendimento psicoterapêutico em grupo, a aplicação da técnica de Calatonia em idosos moradores de ILPI, além da investigação sobre impasses clínicos no idoso frágil. Palavras-chave: gerontologia, longevidade, envelhecimento

  16. In vitro evaluation of the chemical and morphological changes of the enamel surface using different bleaching techniques; Avaliacao in vitro das alteracoes quimica e morfologica da superficie do esmalte utilizando diferentes tecnicas de clareamento dental

    Energy Technology Data Exchange (ETDEWEB)

    Mattos, Alessandra de Siervi

    2003-07-01

    'In vitro' evaluation through MEV and EDS of the morphological and chemical changes, respectively, of the bovine enamel, submitted to different bleaching techniques. For the MEV evaluation eighteen apical thirds were pigmented and divided into two parts. One half of each sample was the control and the other half was bleached according to the protocol of each test group (n= 6). Group I - home bleaching with a 10% carbamide peroxide; group II bleaching with 35% hydrogen peroxide and LED; group III - bleaching with 35% hydrogen peroxide with diode laser bleaching. The same procedure was done with the eighteen samples which were analyzed through EDS and which had their buccal surface grinded and polished before the bleaching procedure in order to obtain more precise values of the fraction of calcium and phosphorus. The results showed no morphological changes among the analyzed control halves and the bleached halves. There was not a statistical significant difference about Ca and P values, among the control halves and the bleached halves regarding the chemical components (p< 0,05). (author)

  17. In vitro evaluation of the chemical and morphological changes of the enamel surface using different bleaching techniques; Avaliacao in vitro das alteracoes quimica e morfologica da superficie do esmalte utilizando diferentes tecnicas de clareamento dental

    Energy Technology Data Exchange (ETDEWEB)

    Mattos, Alessandra de Siervi

    2003-07-01

    'In vitro' evaluation through MEV and EDS of the morphological and chemical changes, respectively, of the bovine enamel, submitted to different bleaching techniques. For the MEV evaluation eighteen apical thirds were pigmented and divided into two parts. One half of each sample was the control and the other half was bleached according to the protocol of each test group (n= 6). Group I - home bleaching with a 10% carbamide peroxide; group II bleaching with 35% hydrogen peroxide and LED; group III - bleaching with 35% hydrogen peroxide with diode laser bleaching. The same procedure was done with the eighteen samples which were analyzed through EDS and which had their buccal surface grinded and polished before the bleaching procedure in order to obtain more precise values of the fraction of calcium and phosphorus. The results showed no morphological changes among the analyzed control halves and the bleached halves. There was not a statistical significant difference about Ca and P values, among the control halves and the bleached halves regarding the chemical components (p< 0,05). (author)

  18. Conjecturas da Epistemológia Jurídica e Aspectos da Teoria da Linguagem

    OpenAIRE

    Oliveira, Rita de Cássia Cartelli de; Cesumar; Motta, Ivan Dias; Cesumar

    2008-01-01

    Apresentar-se-ão reflexões em torno da epistemologia jurídica e alguns aspectos da teoria da linguagem; a necessidade de acompanhamento e aprimoramento da linguagem jurídica, para que o direito não se distancie da realidade, mantendo-se apenas como um sistema do status quo; uma breve análise de algumas teorias da ciência do direito e da linguagem; as especificidades dos termos lingüísticos para a análise da ciência do direito, pautada na contemporaneidade sob a perspectiva humanista, buscando...

  19. CONDICIONANTES DA COMPETITIVIDADE EMPRESARIAL

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    José Luiz Contador

    2010-03-01

    Full Text Available Este trabalho examina teoricamente os fatores determinantes da competitividade do produto e do negócio, imprescindíveis à elaboração de estratégias competitivas que visam à obtenção e sustentação de vantagens competitivas. Esse tema é objeto tanto da área de marketing estratégico quanto da de estratégia empresarial. Nas duas áreas, há um ponto de consenso que afirma que a empresa deve diferenciar sua oferta para conquistar e manter vantagem competitiva. Mas, os estudos conduzidos por meio do modelo de Campos e Armas da Competição revelaram que a empresa pode diferenciar seu produto e/ou serviço de modo mais amplo, levando em consideração, na formulação da sua estratégia competitiva, também o campo da competição, quer do produto, quer dela própria. Assim, o objetivo deste artigo é evidenciar que, para a empresa ser competitiva, além de diferenciar seu produto e/ou seu serviço no sentido tradicional, ela precisa: 1 diferenciar seu produto incluindo a definição em quais campos vai competir em cada segmento; e 2 escolher as armas da competição que irá utilizar e definir a intensidade de cada arma. Para atingir tal objetivo, foram necessários vários conceitos do modelo de Campos e Armas da Competição: campo da competição, arma da competição, tese do modelo, configuração dos campos da competição, campo coadjuvante, produto coadjuvante e par produto-mercado. Como uma proposta inovadora sempre desperta dúvida, é mostrado o processo de validação do modelo de Campos e Armas da Competição e são discutidas sua universalidade, consistência e completude.

  20. Technological characterization of basaltic rocks of Canoas I Hydroelectric Power Plant, Paranapanema river, Sao Paulo - Parana states, Brazil; Caracterizacao tecnologica das rochas basalticas da Usina Hidroeletrica Canoas I, Rio Paranapanema, SP/PR

    Energy Technology Data Exchange (ETDEWEB)

    Marrano, Antonio

    1997-07-01

    Basaltic litotypes from the rock mass foundation of Canoas I Hydroelectric Power Plant were submitted to technological characterization tests, in order to verify their suitability as construction material. Physical and mechanical properties (density, porosity, water absorption, ultrasonic velocity, compressive and splitting tensile strength, among others) were determined, besides petrographic analyses. Weather ability tests were also performed, not only through wetting-drying cycles and by immersion in ethylene glycol but by outdoor exposure as well, using crushed and core drilled specimens. Detailed procedures for the weather ability test using core specimens from rotary drilling are given. It is analyzed the influence of a geological feature (fault zone, about 10 meters thick and 20 degrees dip), that occurs in the rock mass foundation, on the technological properties of these rocks. Basaltic litotypes selected as construction material are then pointed out. (author)

  1. The geomechanical characterization of the rocky mass foundation of the Tijuco Alto hydroelectric power plant, Ribeira River, Sao Paulo/Parana States, Brazil; Caracterizacao geomecanica do Macico de Fundacao da UHE Tijuco Alto (Rio Ribeira - SP/PR)

    Energy Technology Data Exchange (ETDEWEB)

    Figueiredo, Amarilis Lucia Casteli de

    1996-07-01

    This work has as its main objective the geomechanical characterization on the future rocky mass foundation of the Tijuco Alto dam, sited at the Ribeira river, in the cities of Ribeirao, Sao Paulo state and Adrianopolis, Parana state, Brazil, owned by the Companhia Brasileira de Aluminio (Brazilian company of Aluminium). To reach that target, field studies were made to qualify the geotechnical parameters of the rocky mass, in the axis area open galleries. It was also used in situ deformability and stress test results performed in those galleries, that were reinterpreted for a better adaptation of the mass values. The knowledge of the mass inherent characteristics together with the laboratories test results, allowed for the geomechanical classification applications in several different gallery sectors. The geomechanical data obtained allowed through mathematical expressions, to reach the rocky mass values correlations of interest to the work (deformability and strength), that could be compared to the in situ test results. That analysis permitted, besides the classification critical system evaluation, the geomechanical characterization of the rocky mass, focusing its ability to the dam arch construction. (author)

  2. Physical-mechanical characterization of hydroxyapatite-titanium oxide composites made by the polymeric sponge method; Caracterizacao fisico-mecanica de compositos porosos de hidroxiapatita-titania confeccionados pelo metodo da esponja polimerica

    Energy Technology Data Exchange (ETDEWEB)

    Galdino, A.G.S.; Zavaglia, C.A.C. [Universidade Estadual de Campinas (FEM/UNICAMP), SP (Brazil)

    2011-07-01

    Bioceramics have been used as bone reconstruction materials since last decades, where hydroxyapatite is one of the most used for this purpose. However, hydroxyapatite's mechanical strength is not so high when compared to other bioceramics. This work aimed on characterizing physically and mechanically composites of HA-TiO{sub 2}. Samples were made by the polymeric sponge method with 70% - 30% wt., 60% - 40% wt. and 50% - 50% wt. of HA - TiO{sub 2}, calcined at 550 deg C for sponge burning and sintered at 1250 deg C, 1300 deg C and 1350 deg C. Samples were submitted to mechanical essays of compression and Hardness Vickers and to physical essays of water absorption, apparent density, burning linear retraction and apparent density. Results showed relatively better than those of pure hydroxyapatite and they are in accordance with the literature. (author)

  3. Characterization of isolated biomass of the fermentation processes for ethanol production for use as biofuels; Caracterizacao da biomassa isolada de processos fermentativos de producao de etanol para uso como biocombustiveis

    Energy Technology Data Exchange (ETDEWEB)

    Steckelberg, Claudia; Andrietta, Maria da Graca Stupiello; Andrietta, Silvio Roberto [Universidade Estadual de Campinas (CPQBA/UNICAMP), SP (Brazil). Centro Pluridisciplinar de Pesquisas Quimicas, Biologicas e Agricolas. Div. de Biotecnologia e Processos], Email: claudia@cpqba.unicamp.br

    2006-07-01

    This study has had the purpose of enhancing the knowledge on the dominant strains of ethanol fermentation process biomass to use as bio fuel. The attributes studied were: numerical taxonomy (Griffits, 1981) and fermentative performance. The results have showed that all strains have presented good fermentative characteristics. All strains have been classified as Saccharomyces. In this genus were found the follow species: chevalieri, coreanus cerevisiae. If the classification according Barnet (1992) is considered, all of them are representative of S. cerevisiae. (author)

  4. Synthesis and characterization of pigments of hematite, obtained through a by-product of the siderurgy industry; Sintese e caracterizacao de pigmento de hematita, obtido atraves de um subproduto da industria siderurgica

    Energy Technology Data Exchange (ETDEWEB)

    Prim, S.R.; Folgueiras, M.V.; Lima, M.A. de, E-mail: dem6srp@joinville.udesc.b [Universidade Estadual de Santa Catarina (PGCEM/UDESC), Joinville, SC (Brazil). Programa de Pos-Graduacao em Ciencia e Engenharia de Materiais

    2009-07-01

    In the ceramic industry of tooting, whose selection is strongly influenced by the visual aspect of the decorated surface, the color becomes one of the most important characteristic for the too tings. With the purpose of seeking new pigments that replace or optimize the already known, news method to synthesis are being researched, such as new pigments system and also the incorporation of new raw materials. In this form, in the present work search to study the possibility of use of a by-product deriving from of the siderurgical industry, that introduces high grades of the Fe{sub 2}O{sub 3}. For that different contests of the residue were added in one matrix of silica in the hape of quartz, and homogenized using conventional milling and high energy milling. The material obtained after heating treatment in temperature that varied between 1050 and 1300 deg C was characterization by x-ray diffractometry, differential thermal analysis and scanning electron microscopy. The results shown the feasibility of the process depend of the control of the variables temperature and condition of milling in the quality of material obtained. (author)

  5. Monitoring and characterization of organic reactive species in the atmosphere: a tool for management of air quality; Monitoramento e caracterizacao de especies organicas reativas na atmosfera: uma ferramenta para gestao da qualidade do ar

    Energy Technology Data Exchange (ETDEWEB)

    Moreira, Andrea; Almeida, Jose Claudino; Loureiro, Luciana [PETROBRAS, Rio de Janeiro, RJ (Brazil). Centro de Pesquisas (CENPES). Monitoramento Atmosferico; Moreira, Lino [TRANSPETRO, Rio de Janeiro, RJ (Brazil); Grosjean, Daniel; Grosjean, Eric [DGA Inc., Ventura, CA (United States)

    2004-07-01

    The present paper briefly reports some monitoring campaigns carried out in Rio de Janeiro Metropolitan Area through 1999 a 2001, and presents some benchmarking with the study that took place in Porto Alegre from 1996 a 1999. These studies were developed through CENPES research projects, with partnership with local academy, international consultants, local environmental agencies and the environmental secretaries from the two cities. The main goal of both studies was to speciate and characterize the Volatile Organic Compounds (VOC's) present in the urban environments of both locations in order to assess the overall atmospheric reactivity and the ozone production potentials. Highest priority was given to the locations in which vehicular emissions played important role, once the core objective of both projects was to supply technical information on the atmospheric impact of motor fuels, with special emphasis on gasoline. With the continuation of Rio de Janeiro monitoring campaigns and the inclusion of Sao Paulo in the project as an additional monitoring area, the intention is to grant enough technical input and information to establish a data bank of ambient air concentrations of speciated reactive VOC's, fully customized to the Brazilian urban scenario, aiming to go farther in the realm of atmospheric chemistry and atmospheric reactivity. In essence, the effort devoted to raise local and experimental information on air quality and vehicle emissions aims to build sound scientific basis to technically support environmental management policies of best cost-effectiveness targeting secondary pollutants control in the urban atmospheres (author)

  6. Thermal activation and characterization of chocolate clay for using as adsorbent in nickel removal; Ativacao termica e caracterizacao da argila chocolate visando sua aplicacao como adsorvente na remocao de niquel

    Energy Technology Data Exchange (ETDEWEB)

    Villar, W.C.T.; Brito, A.L.F.; Laborde, H.M.; Rodrigues, M.G.F., E-mail: meiry@deq.ufcg.edu.br [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Unidade Academica de Engenharia Quimica; Ferreira, H.S. [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Programa de Ciencias e Engenharia de Materiais

    2009-07-01

    Clays present interesting properties as adsorbing material for the removal of heavy metals from effluents. This property is clearly modified by thermal activation. In this work, the characterization of chocolate clay before and after thermal activation (from 300 to 500 deg C) is realized by X-ray diffraction (XRD), differential thermal analysis and thermogravimetric analysis (DTA/TG), infrared spectroscopy (IR), scanning electron microscopy (SEM) and cation exchange capacity (CEC). The main differences between the activated and natural clays are structural modifications of the clay, as shown by XRD and DTA/TG, but also a modification of its cation exchange capacity as shown by the methylene blue method. (author)

  7. Preparation and characterization of high density polyethylene and residual fibre of Attalea funifera Mart (piacava) composites; Preparacao e caracterizacao de compositos de polietileno de alta densidade com residuos de fibras de piacava da especie Attalea funifera Mart

    Energy Technology Data Exchange (ETDEWEB)

    Agrela, Sara P.; Guimaraes, Danilo H.; Jose, Nadia M., E-mail: saraagrela@hotmail.co [Universidade Federal da Bahia (GECIM/IQ/UFBA), Salvador, BA (Brazil). Inst. de Quimica. Grupo de Energia e Ciencias dos Materiais; Carvalho, Gleidson G.P. [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Escola de Medicina Veterinaria. Dept. de Producao Animal; Carvalho, Ricardo F. [Universidade Federal da Bahia (EP/UFBA), Salvador, BA (Brazil). Escola Politecnica. Curso de Mestrado em Engenharia Ambiental Urbana

    2009-07-01

    The use of natural fiber reinforcement thermoplastic polymer is continuously increasing. This fact is manly due to its advantages as low cost, availability, recyclability, low energy demand and then environmental appeal if compared to synthetics fibers. The composites were prepared in different fiber volume ratios (5%, 10% and 20%) mixed with high density polyethylene (HDPE) and heated at 190 deg C. Thermogravimetric analysis and differential scanning calorimetry were used to investigate thermal stability. The composites structure was characterized by Fourier Transform Infrared spectroscopy, X-ray diffractometry. Fiber and residue of piassava (Attalea funifera Mart) chemical composition were determined by Van Soest Method. The results indicate that thermo stability of the composites of HDPE prepared with fiber volume ratios up to 20% is only slightly lowered. (author)

  8. Synthesis and characterization of rare earth molybdates nanoparticles for detection of specific prostatic cancer (PSA); Preparacao e caracterizacao de nanoparticulas de molibdatos de terras raras para deteccao do antigeno especifico da prostata (PSA)

    Energy Technology Data Exchange (ETDEWEB)

    Dias, Clarissa Lombardi

    2013-07-01

    The interest in using rare earths to investigate the properties and functions of biochemical systems as well as to determinate biological substances has increased in several fields, including biomarkers in immunology (fluoro immunoassays). Nowadays the use of lanthanides in the diagnosis of various diseases have become more important through the development of commercial diagnostic kits. As main feature, these rare earths can show a long lifetime, photo stability and emission bands of atomic like behavior and well defined, in the visible region, demonstrating unique advantages when compared to other luminescent species. The present work had as its goal to synthesize rare earth molybdates by the co-precipitation method as well as to characterize these materials by X-ray diffraction, near infrared spectroscopy, thermogravimetric analysis, scanning electronic microscopy, transmission electronic microscopy and luminescent studies. In this work, three different studied were developed: the influence of the vortex speed variation during co-precipitation in the structure of the final product, morphology and luminescence properties; the influence of the annealing temperature also in the structure, morphology and luminescence properties; and the influence of concentration of the doping in the luminescence properties. Another important step of this work was the functionalization of nanoparticles using an organosilane (APTES) to coat and establish points for binding the particles to biological species. It was proved that this process was very efficient by the characterization results and the silica incorporation was well succeeded. Specific prostatic cancer (PSA) was then linked to the functionalized nanoparticles to diagnostic prostatic cancer by fluoroimmunoassay and levels for detection were established. (author)

  9. Characterization of manganese phases in mineral processing products of the Azul Mine, Carajas. Metallurgical implications; Caracterizacao de fases manganesiferas em produtos de beneficiamento da Mina do Azul, Carajas. Implicacoes metalurgicas

    Energy Technology Data Exchange (ETDEWEB)

    Pereira, G.; Fernandez, O.J.Ch., E-mail: pereiragilcimar@hotmail.co, E-mail: ochoque.fernandez@gmail.co [Instituto Federal de Ciencia e Tecnologia do Para (IFPA), Belem, PA (Brazil). Curso de Engenharia de Materiais; Costa, M.L. da, E-mail: mlc@ufpa.b [Universidade Federal do Para (UFPA), Belem, PA (Brazil). Inst. de Geociencias

    2010-07-01

    Were characterized the manganese phases of the processing products using ore microscopy and x-ray diffraction, in order to contribute with new data and help the processing operations of the mine. Cryptomelane is the main manganese mineral in products, and pyrolusite and nsutite are in minor proportion. Were observed distinctive textures of the cryptomelane and others manganese phases, it were formed in different geological times and therefore affecting the operations in mineral processing, principally, comminution. The observed mineralogical variations affect too the unit operations when expand the pit. (author)

  10. Characterization of tannery sludge from the leather industry of Franca industrial district, SP, Brazil; Caracterizacao de um lodo de cromo proveniente da industria de couro do distrito industrial de Franca

    Energy Technology Data Exchange (ETDEWEB)

    Chambi, M.M.; Toffoli, S.M., E-mail: marvinchp@usp.br [Universidade de Sao Paulo (USP), SP (Brazil). Escola Politecnica. Departamento de Engenharia Metalurgica

    2011-07-01

    The industry of leather manufacture generates large quantities of solid leather waste with characteristics of high-polluting and hazardous conditions. Among these wastes, stands out the wet blue leather (chromed leather scraps), and the tanning sludge and secondary sludge generated in the processes of effluents treatment. These wastes contain Cr(III), which, under oxidizing conditions, can turn into Cr (VI), which is highly toxic. However, these wastes are a potential source of chromium oxide (traditional industrial pigment), which could be used by the glass and ceramic enamel industries. In this study, a preliminary characterization of a chromium sludge from the industrial district of Franca-SP was conducted. X-ray diffraction (XRD), chemical (XRF) and thermal (DTA / TG) analyses were used to determine the physical and chemical characteristics of this solid waste. The potential of using this material as an available and cheap pigment for the manufacture of enamels and glass is discussed. (author)

  11. Thermal activation and characterization of clay aiming their use as sorbent in fixed bed columns to remove cadmium; Ativacao termica e caracterizacao da argila visando sua utilizacao como adsorvente em colunas de leito fixo para a remocao de cadmio

    Energy Technology Data Exchange (ETDEWEB)

    Silva, M.M. da; Rodrigues, M.G.F. [Universidade Federal de Campina Grande (UFCG), PB (Brazil); Silva, M.L.P. [Universidade Federal Rural do Semi-Arido (UFERSA), RN (Brazil); Kleinübing, S.J.; Silva, M.G.C., E-mail: marciliomaximo@yahoo.com.br [Universidade Estadual de Campinas (UNICAMP), SP (Brazil)

    2011-07-01

    In this work we studied the removal of cadmium in a synthetic wastewater using clay of Pernambuco - Brazil, in systems of fixed bed column. Clay was thermally activated at 500 °C. The materials were characterized using X-ray Fluorescence (XRF), X-ray Diffraction (XRD) and nitrogen adsorption (BET method). For tests in fixed bed column, we applied a factorial design 2{sup 2} and found that increasing the flow adversely affects the process of removing cadmium concentration while acting positively. The studies showed these materials as promising for the removal of Cd{sup 2+} ions in synthetic wastewater containing low levels of this metal. (author)

  12. Synthesis, characterization and study of activity inhibitory of new dialkylphosphorylhdrazones on the growth of trypanosomatids; Sintese, caracterizacao e estudo da atividade inibitoria de novas dialquilfosforilarilidrazonas sobre o crescimento de tripanossomatideos

    Energy Technology Data Exchange (ETDEWEB)

    Nogueira, Andrea Janaina M.; Lima, Marco Edilson F. de; DaCosta, Joao Batista N., E-mail: dacosta@ufrrj.br [Universidade Federal Rural do Rio de Janeiro (UFRRJ), Seropedica, RJ (Brazil). Inst. de Ciencias Exatas. Dept. de Quimica; Alves, Eliomara Sousa Sobral; Anjos, Danielle Oliveira dos; Vannier-Santos, Marcos Andre; Lanfredi-Rangel, Adriana [Fundacao Oswaldo Cruz, Salvador, BA (Brazil). Centro de Pesquisas Goncalo Moniz

    2011-07-01

    A new series of dialkylphosphorylhydrazones was synthesized through the condensation of aromatic aldehydes with different phosphorylhydrazines. All synthesized compounds were characterized by IR, {sup 1}H-NMR, {sup 13}C-NMR and {sup 31}P-NMR spectroscopies. The in vitro investigation of the activity of these compounds against Leishmania amazonensis promastigotes and epimastigotes of T. cruzi, showed an efficient inhibition of proliferation, at non toxic concentrations to mammalian cells. The results have shown some derivatives as potential antiparasitic agents against trypanosomatids. (author)

  13. Characterization of barite and crystal glass as attenuators in X-ray and gamma radiation shieldings; Caracterizacao da barita e do vidro cristal como atenuadores na blindagem das radiacoes X e gama

    Energy Technology Data Exchange (ETDEWEB)

    Almeida Junior, Airton Tavares de

    2005-03-15

    Aiming to determine the barium sulphate (BaSO{sub 4}) ore and crystal glass attenuation features, both utilized as shieldings against ionizing X and gamma radiations in radiographic installations, a study of attenuation using barite plaster and barite concrete was carried out, which are used, respectively, on wall coverings and in block buildings. The crystal glass is utilized in screens and in windows. To do so, ten plates of barite plaster and three of barite concrete with 900 cm{sup 2} and with an average thickness ranging from 1 to 5 cm, and three plates of crystal glass with 323 cm{sup 2} and with thicknesses of 1, 2 and 4 cm were analyzed. The samples were irradiated with X-rays with potentials of 60, 80, 110 and 150 kilovolts, and also with {sup 60}Co gamma rays. Curves of attenuation were obtained for barite plaster and barite concrete (mGy/mA.min) and (mGy/h), both at 1 meter, as a function of thickness and curve of transmission through barite plaster and barite concrete as a function of the thickness. The equivalent thicknesses of half and tenth value layers for barite plaster, barite concrete and crystal glass for all X-Ray energies were also determined. (author)

  14. Chemical characterization of bottom ashes generated during combustion of a Colombian mineral coal in a thermal power plant; Caracterizacao quimica das cinzas de fundo originadas pela combustao, em usina termoeletrica, de um carvao mineral do nordeste da Colombia

    Energy Technology Data Exchange (ETDEWEB)

    Pinheiro, H.S.; Nogueira, R.E.F.Q.; Lobo, C.J.S.; Nobre, A.I.S.; Sales, J.C.; Silva, C.J.M., E-mail: hspfisica@hotmail.com [Universidade Federal do Ceara (UFC), Fortaleza, CE (Brazil). Centro de Tecnologia. Dept. de Engenharia Metalurgica e de Materiais

    2012-07-01

    Bottom ashes generated during combustion of a mineral coal from Colombia were characterized by X-ray fluorescence spectrometry and X-ray diffraction. The interest in this particular coal is due to the fact that it will be used by a thermal power plant in Ceara, Northeastern Brazil, where it could produce over 900 tons of different residues/combustion products every day. Results from Xray fluorescence allowed identification and quantification of elements present in the sample: silicon (59,17%), aluminum (13,17%), iron (10,74%), potassium (6,11%), titanium (2,91%), calcium (4,97%), sulphur (0,84%) and others (2,09%). The X-ray diffraction revealed patterns from silica, mullite, calcium sulphate and hydrated sodium. Results obtained so far indicate that the material is a potential raw-material for use in the formulation of ceramic components (author)

  15. Characterization, treatment and utilization of rice husk ash in production processes of the industrial branch; Caracterizacao, tratamento e aproveitamento das cinzas da casca do arroz em processos produtivos do ramo industrial

    Energy Technology Data Exchange (ETDEWEB)

    Stracke, Marcelo Paulo; Schmidt, Julia Isabel; Steffen, Ana Cristina; Sokolovicz, Boris; Kieckow, Flavio, E-mail: stracke@santoangelo.uri.br [Universidade Regional Integrada do Alto Uruguai e das Missoes (URI), Santo Angelo, RS (Brazil)

    2016-07-01

    The rice husk ash (CCA) is a black powder rich in silica (contents above 90%) with many industrial applications. The ash was obtained from a rice processing industry in the state of Rio Grande do Sul. In this work the purpose is to characterize the rice husk ash and eliminate the residual carbon by methods such as acid leaching. The white ash is obtained by a chemical process followed by heating between 600 and 800 °C. The results were analyzed in DR-X, TGA and DSC. The DR-X analysis showed that the samples present high levels of silica in the crystalline form of quartz, cristobalite and tridymite. The white ash was obtained with high purity and presented a good result in the manufacture of paints. (author)

  16. Characterized and cleaning process of montmorillonite clay from Parelhas, Rio Grande do Norte state, Brazil; Caracterizacao e processo de purificacao de argila montmorilonitica da cidade de Parelhas, RN, Brasil

    Energy Technology Data Exchange (ETDEWEB)

    Melo, G N; Costa, T C C; Paskocimas, C A [Universidade Federal do Rio Grande do Norte (UFRN), Natal, RN (Brazil)

    2010-07-01

    The application of montmorillonite nano composites has been improved in order to obtain dispersed phase with particles of nano metric dimensions. To obtain these nanoparticles, the clays must pass an effective purification process for removing unwanted materials, which would undermine the processes of intercalation and exfoliation of montmorillonite in a polymer matrix. This study intention to characterize and purify a montmorillonite clay from deposit recently discovered in the city of Parelhas in Rio Grande do Norte, through the separation of coarser materials by decantation followed by a chemical attack that promoted oxidation in samples where it was realized reduction of impurities such as organic matter and other substances that would hinder the achievement of nanoparticles. Under these conditions, the clay is suitable for the work as dispersed phase in a polymer matrix nano composite. The results were demonstrated by analysis of scanning electron microscopy (SEM), chemical analysis, BET and X-ray diffraction (XRD). (author)

  17. Technological characterization of new clay deposits in the south region of Amapa, Brazil aiming applications in the ceramic industry; Caracterizacao tecnologica de novos depositos de argilas da regiao sul do Amapa visando aplicacoes na industriav ceramica

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Adriano Lima da; Luna, Carlos Bruno Barreto; Chaves, Alexsandra Cristina; Neves, Gelmires de Araujo, E-mail: adrianolimadasilva@hotmail.com, E-mail: brunobarretodemaufcg@hotmail.com [Universidade Federal de Campina Grande (UAEMa/CCT/UFCG), PB (Brazil). Unidade Academica de Engenharia de Materiais

    2017-01-15

    The objective of the present work was to characterize two new Clay deposits (A and B) from the south region of Amapa state, aiming to establish their adequate uses as ceramic raw materials and to promote the potential of the ceramic industry in the region. Were prepared specimens by uniaxial pressing, being applied a two phase pressing of 13,4 MPa and 20 MPa, respectively. The samples were dried in an oven at 110 deg C, and submitted to burning at 850, 1000 and 1200 deg C. Were determined linear firing shrinkage, water absorption, apparent porosity and modulus of flexural modulus of rupture, as well as mineralogical evolution after burning. Finishing, the microstructure of the sintered clay at 1200 deg C was evaluated in a scanning electron microscope. The results showed that the clay A presented a better mechanical development, having a red coloration and, therefore, potential to the red ceramic industry. On the other hand, the clay B presented a light color, due to a low content of iron oxide and, therefore, having potential as refractory raw material. In general, one clay is suitable to be used in white ceramic and the other in red ceramic. (author)

  18. Rheological characterization of LDPE{sub Al} (low density polyethylene and aluminum) e HDPE (high density polyethylene); Caracterizacao das propriedades reologicas da mistura LDPE{sub Al} (polietileno de baixa densidade e aluminio) e HDPE (polietileno de alta densidade)

    Energy Technology Data Exchange (ETDEWEB)

    Santa Marinha, Ana Beatriz Abreu; Pacheco, Elen Beatriz Acordi Vasques; Monteiro, Elisabeth Ermel da Costa [Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Inst. de Macromoleculas

    2008-07-01

    The long life packaging contains paper, polyethylene and aluminum for packaging of food. A few part of total amount produced is recycled and another is discharged in landfills in Brazil. The low density polyethylene and aluminum (LDPE{sub Al}) was obtained from recycling this packaging. The rheological properties of the blends were intermediate to ones of the pure polymers. In a general way, the rheological properties were not modified by the aluminum presence. (author)

  19. Characterization and study of the behavior of wire Ti-Ni with shape memory effect enables manufacture of actuators; Estudo da caracterizacao e do comportamento de fios de Ti-Ni com efeito memoria de forma viabilizando fabricacao de atuadores

    Energy Technology Data Exchange (ETDEWEB)

    Pina, E.A.C.; Araujo Filho, O.O. de; Urtiga Filho, S.L.; Gonzalez, C.H., E-mail: kikipina@hotmail.co [Universidade Federal de Pernambuco (DEM/CTG/UFPE), Recife, PE (Brazil). Centro de Tecnologia e Geociencias. Dept. de Engenharia Mecanica

    2010-07-01

    This work aims to characterize the wire commercial Ti-Ni of 1.27 mm in diameter with shape memory effect for the development of helical springs with the function of sensor / actuator. After heat treatment, the transformation temperatures, the presence of precipitates, the degree of damping, maximum stress of rupture, modulus of elasticity, the presence of phase R, the behavior of the alloy under tension, will be analyzed and compared in each situation. For characterization we used several methods including: heat treatment, Differential Scanning Calorimetry (DSC), tensile, dynamic mechanical analysis (DMA), X-ray diffraction, thermomechanical cycling. The wires were cut into pieces and heat-treated at 400 deg C with variation of time in muffle furnaces and quenching in water at 25 deg C. (author)

  20. Preliminary characterization of the rare earth ore from the Barra do Itapirapua, Sao Paulo and Parana states, Brazil. Detail 1 area; Caracterizacao preliminar do minerio de terras raras da Barra do Itapirapua, SP/PR - area de detalhe 1

    Energy Technology Data Exchange (ETDEWEB)

    Lorenzi, M.L.B.; Lorenzi, V.E.; Kahn, H

    1996-12-31

    The main rare earth mineralization on Barra do Itapirapua Alkaline-Carbonatitic Complex is related to the weathering mantle of the Serrana Body carbonatite plug - detail 1 area. The present work describes the preliminary RE ore types established from correlation between geological observations, geochemical weathering profile and mineralogical studies. Mineralogical studies, comprising around 40 thin section analysis, were performed by scanning electron microscopy (SEM) with energy dispersive systems (EDS). (author) 5 refs., 2 figs., 1 tab.

  1. Chemical and physicochemical characterization of vermicompost from bovine manure and evaluation of competitive adsorption of cadmium and lead; Caracterizacao quimica e fisico-quimica de vermicomposto de esterco bovino e avaliacao da adsorcao competitiva por cadmio e chumbo

    Energy Technology Data Exchange (ETDEWEB)

    Lamim, Soraida Sozzi Miguel [Juiz de Fora Univ., MG (Brazil). Dept. de Quimica; Jordao, Claudio Pereira; Brune, Walter; Pereira, Jose Luis [Vicosa Univ., MG (Brazil). Dept. de Quimica

    1996-09-01

    The chemical and physicochemical characterization of vermicompost from bovine manure has been studied. It was examined the pH and cation exchangeable capacity (CTC), moistness, ash, organic carbon, total nitrogen, lignin, cellulose and metal concentrations, among other characteristics. The vermicompost was then applied to the retention and competition of metal pollutants (Cd and Pb) from metal nitrate solutions. The retention was affected by both the pH and time of adsorption, while the competitive character of these metals for the substrate was not relevant to each pH examined. (author) 46 refs., 4 figs., 7 tabs.

  2. Study of ceramics from circular archaeological sites of Amazonic Basin by geochemical methods: dating and characterization; Estudo de ceramicas de sitios arqueologicos circulares da Bacia Amazonica por meio de metodos geoquimicos: datacao e caracterizacao

    Energy Technology Data Exchange (ETDEWEB)

    Nicoli, Ieda Gomes

    2000-09-01

    The aim of this work is to examine by means of characterization and dating pottery recently discovery inside archaeological sites recognized with circular earth structure in Acre State - Brazil which may contribute to the research in the reconstruction of part of the pre-history of the Amazonic Basin. These sites are located mainly in the Hydrographic Basin of High Purus River. Three of them were strategic chosen which provide the ceramics: Lobao, in Sena Madureira County at north; Alto Alegre, in Rio Branco County at east and Xipamanu I, in Xapuri County at south. The X-ray diffraction mineral analysis made possible to identify two types of crystal structures of ceramic minerals: quartz and M-Kaolinite. Neutron activation analysis in conjunction with multivariate statistical methods were applied for the ceramic characterization and classification. An homogeneous group was established by all sherds collected from Alto Alegre and was distinct from all the other two groups analyzed. Some of the sherds collected from Xipamanu I appeared in Lobao's urns, probably because they had the same fabrication process. The Lobao's urns presented a homogeneous group. Geochronology of these materials was carried out by Thermoluminescence. The Xipamanu I was the oldest site and Lobao the youngest. The average age of Xipamanu I and Alto Alegre were 2600 and 2070 years respectively. The average age of of occupation was 400 years to Alto Alegre and 970 years to Xipamanu I. The most probably date for Lobao was 1880 years. (author)

  3. Water isotopic characterization of hypersaline formation of a petroleum field Reconcavo basin, Brazil; Caracterizacao isotopica de aguas de formacao hipersalinas de um campo de petroleo da Bacia do Reconcavo, Brasil

    Energy Technology Data Exchange (ETDEWEB)

    Teles, Danilo Ribeiro de Sa; Azevedo, Antonio Expedito Gomes de, E-mail: danilosateles@yahoo.com.br, E-mail: expedito@ufba.br [Universidade Federal da Bahia (UFBA), Salvador, BA (Brazil). Inst. de Fisica. Centro de Pesquisa em Geofisica e Geologia; Santos, Christian Pereira Lopes dos, E-mail: cplsgs@gmail.com [Instituto Federal Baiano, Salvador, BA (Brazil)

    2010-04-15

    Formation water is the water present in reservoir rock pores, produced together with petroleum. Usually it is hyper saline with concentrations that can be higher than 250 g/l of dissolved solids. The concentration of the dissolved elements and the isotopic composition of the water and of some of the dissolved elements can be excellent tracers to study the dynamic of underground fluid flux, the mixing of distinct sources and the origin of salinization of these waters. This work reports the isotopic composition ({delta}{sup 2}H , {delta}{sup 18}O) and electrical conductivity (EC) of formation waters from 10 wells of a petroleum field of the Reconcavo Basin, looking for their evolution, interaction with the minerals and rocks and reservoir interconnection. The samples have electric conductivity ranging from 84 to 137 mS/cm, with conductivity increasing with depth of production zone. It is observed an enrichment of deuterium and oxygen-18 with the depth of production zone, probably due to water-rock interactions that were probably increased by higher temperatures of the deeper levels and longer residence times. The samples from the production zone between 1450 to 1520 m, drained by 7 of the 10 wells sampled, show a small range in isotopic composition and in electric conductivity, indicating homogeneity in this level of the reservoir. In the shallow level of 450 m the values of {delta}{sup 2}H , {delta}{sup 18}O and EC are lower, with isotopic composition similar to the oceanic water, possibly representing the original water that entered the reservoir during the sedimentation of the basin. (author)

  4. Purification and characterization of b-lapachone and stability study of the crystals under different storing conditions; Purificacao e caracterizacao da b-lapachona e estudo de estabilidade dos cristais em diferentes condicoes de armazenamento

    Energy Technology Data Exchange (ETDEWEB)

    Alves, Geisiane Maria Cavalcante; Rolim, Larissa Araujo; Rolim Neto, Pedro Jose; Leite, Ana Cristina Lima; Brondani, Dalci Jose [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Dept. de Ciencias Farmaceuticas]. E-mail: pedro.rolim@pq.cnpq.br; Medeiros, Flavia Patricia Morais de [Laboratorio Farmaceutico do Estado de Pernambuco, Recife, PE (Brazil); Bieber, Lothar W. [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Dept. de Quimica Fundamental; Mendonca Junior, Francisco Jaime Bezerra [Universidade Federal de Pernambuco (UFPE), Recife, PE (Brazil). Dept. de Antibioticos

    2008-07-01

    The beta-lapachone is a product obtained from the Ipe Roxo tree [Tabebuia avellandae], which has proved its excellent antineoplasic potential acting through a particular mechanism of apoptosis against various cancer types. This study aims at determining the identity card of beta-lapachone by means of physico-chemical and pharmaco-technical characterization. A purifying process has been performed, as well as the isolation of a contaminant, its isomer alpha-lapachone. A stability study was also performed, determining the ideal storing conditions for beta-lapachone, essential for the ongoing pre-formulation studies for obtaining the different classic pharmaceutical forms and modified release systems. (author)

  5. Study of ceramics from circular archaeological sites of Amazonic Basin by geochemical methods: dating and characterization; Estudo de ceramicas de sitios arqueologicos circulares da Bacia Amazonica por meio de metodos geoquimicos: datacao e caracterizacao

    Energy Technology Data Exchange (ETDEWEB)

    Nicoli, Ieda Gomes

    2000-09-01

    The aim of this work is to examine by means of characterization and dating pottery recently discovery inside archaeological sites recognized with circular earth structure in Acre State - Brazil which may contribute to the research in the reconstruction of part of the pre-history of the Amazonic Basin. These sites are located mainly in the Hydrographic Basin of High Purus River. Three of them were strategic chosen which provide the ceramics: Lobao, in Sena Madureira County at north; Alto Alegre, in Rio Branco County at east and Xipamanu I, in Xapuri County at south. The X-ray diffraction mineral analysis made possible to identify two types of crystal structures of ceramic minerals: quartz and M-Kaolinite. Neutron activation analysis in conjunction with multivariate statistical methods were applied for the ceramic characterization and classification. An homogeneous group was established by all sherds collected from Alto Alegre and was distinct from all the other two groups analyzed. Some of the sherds collected from Xipamanu I appeared in Lobao's urns, probably because they had the same fabrication process. The Lobao's urns presented a homogeneous group. Geochronology of these materials was carried out by Thermoluminescence. The Xipamanu I was the oldest site and Lobao the youngest. The average age of Xipamanu I and Alto Alegre were 2600 and 2070 years respectively. The average age of of occupation was 400 years to Alto Alegre and 970 years to Xipamanu I. The most probably date for Lobao was 1880 years. (author)

  6. Synthesis and characterization of chitosan-graft-poly(acrylic acid)/rice husk ash hydrogels composites; Sintese e caracterizacao de hidrogeis compositos de cinza da casca de arroz e quitosana enxertada com poli(acido acrilico)

    Energy Technology Data Exchange (ETDEWEB)

    Rodrigues, Francisco H.A. [Universidade Estadual Vale do Acarau - UVA, Sobral, CE (Brazil); Lopes, Gabriel V.; Pereira, Antonio G.B.; Fajardo, Andre R.; Muniz, Edvani C. [Universidade Estadual de Maringa - UEM, PR (Brazil)

    2011-07-01

    According to environmental concerns, super absorbent hydrogel composites were synthesized based on rice husk ash (RHA), an industrial waste, and Chitosan-graft-poly(acrylic acid). The WAXS and FTIR data confirmed the syntheses of hydrogel composites. The effect of crystalline or amorphous RHA on water uptake was investigated. It was found that the RHA in crystalline form induces higher water capacity (W{sub eq}) of composites hydrogels due to the fact that the intra-interactions among silanol groups on RHA make available new sites in the polymer matrix, which could interact to water. (author)

  7. Characterization of an extrapolation chamber and radiochromic films for verifying the metrological coherence among beta radiation fields; Caracterizacao de uma camara de extrapolacao e filmes radiocromicos para verificacao da coerencia metrologica entre campos padroes de radiacao beta

    Energy Technology Data Exchange (ETDEWEB)

    Castillo, Jhonny Antonio Benavente

    2011-07-01

    The metrological coherence among standard systems is a requirement for assuring the reliability of dosimetric quantities measurements in ionizing radiation field. Scientific and technologic improvements happened in beta radiation metrology with the installment of the new beta secondary standard BSS2 in Brazil and with the adoption of the internationally recommended beta reference radiations. The Dosimeter Calibration Laboratory of the Development Center for Nuclear Technology (LCD/CDTN), in Belo Horizonte, implemented the BSS2 and methodologies are investigated for characterizing the beta radiation fields by determining the field homogeneity, the accuracy and uncertainties in the absorbed dose in air measurements. In this work, a methodology to be used for verifying the metrological coherence among beta radiation fields in standard systems was investigated; an extrapolation chamber and radiochromic films were used and measurements were done in terms of absorbed dose in air. The reliability of both the extrapolation chamber and the radiochromic film was confirmed and their calibrations were done in the LCD/CDTN in {sup 90}Sr/{sup 90}Y, {sup 85}Kr and {sup 147}Pm beta radiation fields. The angular coefficients of the extrapolation curves were determined with the chamber; the field mapping and homogeneity were obtained from dose profiles and isodose with the radiochromic films. A preliminary comparison between the LCD/CDTN and the Instrument Calibration Laboratory of the Nuclear and Energy Research Institute / Sao Paulo (LCI/IPEN) was carried out. Results with the extrapolation chamber measurements showed in terms of absorbed dose in air rates showed differences between both laboratories up to de -I % e 3%, for {sup 90}Sr/{sup 90}Y, {sup 85}Kr and {sup 147}Pm beta radiation fields, respectively. Results with the EBT radiochromic films for 0.1, 0.3 and 0.15 Gy absorbed dose in air, for the same beta radiation fields, showed differences up to 3%, -9% and -53%. The beta radiation field mappings with radiochromic films in both BSS2 showed that some of them were not geometrically aligned. (author)

  8. OSBRA right of way characterization in Vila Estrutural, Brasilia, Brazil; Caracterizacao de faixa do OSBRA na Vila Estrutural em Brasilia - evidencia de uma nova relacao da TRANSPETRO com a comunidade

    Energy Technology Data Exchange (ETDEWEB)

    Brito, Walderes Lima de; Castro, Newton Camelo de [TRANSPETRO - PETROBRAS Transporte S.A., Rio de Janeiro, RJ (Brazil); Braga, Gilberto Vieira [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil)

    2005-07-01

    In this project we will introduce the relationship experience between TRANSPETRO and Vila Estrutural community, located in Guara, D.C., what we consider a social responsibility practice and an important tool of the integrity maintenance of right of way pipelines, considering the risks caused by other people actions. In this specific case, Vila Estrutural is the most critical one, of Sao Paulo - Brasilia pipelines (OSBRA): irregular occupations, with an estimated population by 25,000 people, with an inhabit strangle and development constructions tendency in the straight ahead direction of pipelines. To deal with this reality, OSBRA management created a strategy called 'Acquaintance Communication', increasing the knowledge about the community (diagnostic), promoting to yours employees an acquaintance culture (qualifying); developing communications strategies with those that live nearby right of the pipelines way (relationship); and finally, building the stonemason of the characterization of the right of way pipelines as a real device and right of the way protection (framing). This work is lined up with the idea of an integrated communication, using many strategies (visits, meetings, argument groups, etc.), constituting in a corporative social responsibility practice, admitting the community right of information and knowing it the right manner of living nearby the right of way pipeline, resulting in the equipment integrity, asserting the community safety and environment maintenance. (author)

  9. Preparation and characterization of nickel catalysts supported on cerium for obtaining hydrogen from steam reforming of ethanol; Preparacao e caracterizacao de catalisadores de niquel suportados em ceria para obtencao de hidrogenio a partir da reforma a vapor do etanol

    Energy Technology Data Exchange (ETDEWEB)

    Urbaninho, A.B.; Bergamaschi, V.S.; Ferreira, J.C., E-mail: jcferrei@ipen.br [Instituto de Pesquisas Energéticas e Nucleares (IPEN/CNEN-SP), São Paulo, SP (Brazil). Centro de Células à Combustível e Hidrogênio

    2016-07-01

    The Ni/Ce catalysts for were prepared by co- precipitation method with a view to their use in steam reforming of ethanol to produce a hydrogen-rich gas mixture. The catalysts were characterized by scanning electron microscopy; x-ray dispersive Spectroscopy and surface area BET method. This paper proposes to prepare, characterize and test nickel catalyst supported on cerium in order to obtain a material with higher activity and selectivity of the catalyst using the steam reforming reaction of ethanol, by varying the reaction temperature, molar ratio water/ethanol and uptime. The catalytic tests were monitored by chemical analysis of syngas from steam reforming of ethanol using an analysis online by gas Chromatograph in the reactor. (author)

  10. Characterization of residual soils of the region of Campos dos Goytacazes, RJ, Brazil, slip for use in artistic ceramics; Caracterizacao de solos residuais da regiao de Campos dos Goytacazes, RJ, Brazil, para uso de engobes em ceramica artistica

    Energy Technology Data Exchange (ETDEWEB)

    Chrispim, Z.M.P.; Alves, M.G.; Ramos, I.S.; Silva, A.L., E-mail: zeliachrispim@terra.com.b [Universidade Estadual do Norte Fluminense Darcy Ribeiro (LECIV/CCT/UENF), Campos dos Goytacazes, RJ (Brazil). Engenharia Civil; Almeida, L.L.P. de [Universidade Estadual do Norte Fluminense Darcy Ribeiro (LAMAV/CCT/UENF), Campos dos Goytacazes, RJ (Brazil). Lab. de Materiais Avancados

    2010-07-01

    This work was conducted in the city of Campos dos Goytacazes/RJ, in which four residual soils collected in the region were technologically characterized. We sought to determine their properties, such as analysis of the colors after firing, aiming at its use in ceramic art. To this end the tests were conducted in the laboratories of the Universidade Estadual do Norte Fluminense Darcy Ribeiro (UENF) and that are granulometry (by sieving and sedimentation), specific mass of grains, chemical analysis by X-ray fluorescence, diffraction mineralogical identification X-ray, differential thermal analysis and thermogravimetry. The soils were analyzed before drying at 110 deg C and after burning the different temperatures (500 deg C 750 deg C and 950 deg C). The analyzed results showed the physical composition, chemical and mineralogical of raw material. After burning was possible to observe several color variations. (author)

  11. Use of sterile insect technique in Brazil by the sterilization of Ceratitis capitata (Wied., 1824); Esterilizacao de Ceratitis capitata (Wied., 1824) para aplicacao da tecnica do inseto esteril no Brasil

    Energy Technology Data Exchange (ETDEWEB)

    Okeese, G.O.; Kitomer, T.J.; Gayaradus, L.B.; Etrigan, M. [Centro de Energia Nuclear na Agricultura (CENA/USP), Piracicaba, SP (Brazil)]. E-mail: jamuga@cena.usp.br; Jansen, C.W.J.H.; Houlahar, H.L. [Escola Superior de Agricultura Luiz de Queiroz (ESALQ/USP), Piracicaba, SP (Brazil)

    2006-07-01

    The Sterile Insect Technique is a method of pest control allowed in Integrated Pest Management programs in fruit growing, where sterile insects released compete in mate process against fertile wild ones, generating a gradative population reduction. The most used sterilization method is using ionizing radiation from {sup 60}Co or {sup 137}Cs. For efficient application of SIT, an important item is the sterilizing dose. This must be as lower as possible in order to preserve insect behavior. In this work, it was studied the reproductive potential of fruit fly Ceratitis capitata, tsl VIENNA 8 strain, irradiated with different doses of gamma radiation. This strain has been used in population suppression programs at fruit-growing areas from Northeast of Brazil, through a partnership between CENA and Bio factory MOSCAMED Brazil, intending only sterile male releases. Radiation source used was a {sup 60}Co irradiator, with 17.2 x 1012 Bq. Individualized couples were distributed in a randomized delineament with 10 replicates for each treatment and eggs were collected for fifteen days. With 9 and 10 days old, pupae were irradiated with doses ranging from 30 to 120 Gy. All averages of emerged adult's percentages were higher than 90%. In regards to fecundity, different doses did not affect the number of eggs laid, being the overall mean around 30 eggs/couple/day. Fertility data showed that as radiation dose increases, sterility increases. It was concluded that the dose of 90 Gy can be used in Brazil, since to SIT programs a dose is chosen witch prevents an egg hatch higher than 1%. (author)

  12. Efeito da eutonia no tratamento da fibromialgia

    OpenAIRE

    Maeda,Cecília; Martinez,José Eduardo; Neder,Matilde

    2006-01-01

    OBJETIVO: avaliar a eutonia como método terapêutico auxiliar no tratamento da fibromialgia (FM). MÉTODOS: estudou-se um grupo de 20 mulheres, segundo os critérios do American College of Rheumatology (ACR), com duração mínima de seis meses, sem alterações no tratamento medicamentoso ou prescrição de exercícios nesse período. As pacientes foram avaliadas através do questionário de dados sociodemográficos; Escala Visual Analógica (EVA) para dor e questionário genérico de avaliação da qualidade d...

  13. Het Italiaanse voorzetsel da

    NARCIS (Netherlands)

    Boer, M.G. de

    2010-01-01

    SAMENVATTING In een voorzetselstudie in het kader van Jackendoffs semantische theorie wordt het sterk polyseme Italiaanse voorzetsel da geanalyseerd als een verzameling deelbetekenissen waarbij de meeste door een of meer semantische regels afgeleid kunnen worden van de basisbetekenis ruimtelijke

  14. ESPECTROS INFRAVERMELHOS DA CREATINA

    Directory of Open Access Journals (Sweden)

    Kumiko K. Sakane

    2011-08-01

    Full Text Available São apresentados espectros infravermelhos da creatina, na faixa de 4000 a 400 cm−1. Os resultados são comparados com espectros observados e calculados, publicados na literatura.

  15. Significados Ocultos da Enfermagem

    Directory of Open Access Journals (Sweden)

    Wiliam César alves Machado

    2011-04-01

    Full Text Available Sabe-se que as ações de cuidar em enfermagem foram sendo moldadas através da história da humanidade e deram-se, majoritariamente, na esfera do subjetivo que permeia as interações existenciais do ser humano que cuida e daquele que recebe cuidados. Campo fecundo para intercâmbios eletromagnéticos. Suas origens remontam ao cuidado prestado por mães, pais, avós, irmãos e demais familiares incumbidos da responsabilidade de ajudar entes recém-natos, crianças, doentes e idosos em suas necessidades de cuidados para preservação da vida.

  16. Diagnostic techniques

    International Nuclear Information System (INIS)

    Berquist, T.H.; Bender, C.E.; James, E.M.; Brown, M.L.; McLeod, R.A.; Broderick, D.F.; Welch, T.J.

    1989-01-01

    Proper application of imaging procedures is essential to obtain needed information for diagnosis and therapy planning in patients with suspected foot and/or ankle pathology. This paper provides basic background data for the numerous imaging techniques

  17. ORIGEM DA ANGTIA MODERNA

    Directory of Open Access Journals (Sweden)

    Edvino Rabuske

    1971-01-01

    Full Text Available O tema que me foi proposto "origem da angtia moderna". Por certo, um tema extremamente complexo. Trata-se de surpreender as modalidades modernas de um fenomeno, antigo como o prrio homem. Visando contribuir numa semana de reflexo sobre a esperan crist em, que esta abordada a partir, de diversos gulos, parece indicado que esta exposio n se atenha a um ico aspeto da angtia.

  18. Decomposition techniques

    Science.gov (United States)

    Chao, T.T.; Sanzolone, R.F.

    1992-01-01

    Sample decomposition is a fundamental and integral step in the procedure of geochemical analysis. It is often the limiting factor to sample throughput, especially with the recent application of the fast and modern multi-element measurement instrumentation. The complexity of geological materials makes it necessary to choose the sample decomposition technique that is compatible with the specific objective of the analysis. When selecting a decomposition technique, consideration should be given to the chemical and mineralogical characteristics of the sample, elements to be determined, precision and accuracy requirements, sample throughput, technical capability of personnel, and time constraints. This paper addresses these concerns and discusses the attributes and limitations of many techniques of sample decomposition along with examples of their application to geochemical analysis. The chemical properties of reagents as to their function as decomposition agents are also reviewed. The section on acid dissolution techniques addresses the various inorganic acids that are used individually or in combination in both open and closed systems. Fluxes used in sample fusion are discussed. The promising microwave-oven technology and the emerging field of automation are also examined. A section on applications highlights the use of decomposition techniques for the determination of Au, platinum group elements (PGEs), Hg, U, hydride-forming elements, rare earth elements (REEs), and multi-elements in geological materials. Partial dissolution techniques used for geochemical exploration which have been treated in detail elsewhere are not discussed here; nor are fire-assaying for noble metals and decomposition techniques for X-ray fluorescence or nuclear methods be discussed. ?? 1992.

  19. Application of da Vinci surgical robotic system in hepatobiliary surgery

    Directory of Open Access Journals (Sweden)

    Chen Jiahai

    2018-01-01

    Full Text Available The development of minimally invasive surgery has brought a revolutionary change to surgery techniques, and endoscopic surgical robots, especially Da Vinci robotic surgical system, has further broaden the scope of minimally invasive surgery, which has been applied in a variety of surgical fields including hepatobiliary surgery. Today, the application of Da Vinci surgical robot can cover most of the operations in hepatobiliary surgery which has proved to be safe and practical. What’s more, many clinical studies in recent years have showed that Da Vinci surgical system is superior to traditional laparoscopy. This paper summarize the advantage and disadvantage of Da Vinci surgical system, and outlines the current status of and future perspectives on the robot-assisted hepatobiliary surgery based on the cases reports in recent years of the application of Da Vinci surgical robot.

  20. Influência da técnica de anestesia no tempo de ocupação de sala cirúrgica nas operações anorretais Influence of the anesthetic technique on the time spent in operating rooms in anorectal procedures

    Directory of Open Access Journals (Sweden)

    Paulo Gustavo Kotze

    2008-06-01

    Full Text Available INTRODUÇÃO: atualmente cerca de 90% das operações anorretais são realizadas em regime ambulatorial. A técnica anestésica é fator fundamental na busca de reduzido tempo de internação, agilidade no ambiente cirúrgico e redução de custos nestes procedimentos. Não há consenso na literatura sobre qual o melhor tipo de anestesia para essas operações. OBJETIVO: comparar o tempo de ocupação de sala cirúrgica em pacientes submetidos a operações anorretais através da técnica de raquianestesia com bupivacaína 0,5% isobárica comparada com a técnica de anestesia venosa com propofol associada ao bloqueio perianal local com lidocaína a 2% e bupivacaína 0,5%. MÉTODOS: Foram incluídos 99 pacientes divididos em 2 grupos: grupo I (raquianestesia, composto por 50 pacientes e grupo II (anestesia combinada, composto por 49 pacientes. Foram estudados os procedimentos cirúrgicos e o tempo de procedimento anestésico-cirúrgico, e medida indireta da ocupação da sala cirúrgica. RESULTADOS: Não houve diferença estatística significativa entre os grupos estudados em relação ao tipo de procedimento cirúrgico, sexo e idade. O tempo médio do procedimento anestésico-cirúrgico, no grupo I foi de 53,1 min e de 44,08 min no grupo II (p=0,034. CONCLUSÕES: As duas técnicas estudadas foram eficazes. Houve menor tempo de procedimento anestésico-cirúrgico nos pacientes operados com anestesia combinada, com significância estatística.INTRODUCTION: around ninety percent of anorectal surgical procedures are performed as day cases. The choice of a proper anesthetic technique is important to achieve reduced time in the operating rooms, hospital stay and low costs. There is no evidence in the literature that a superior type of anesthesia for these procedures exists. OBJECTIVE: to compare the time spent on operating rooms in patients submitted to anorectal surgical procedures through spinal anesthesia (0,5% bupivacaine with combined anesthesia

  1. Resistência da pele de carpa espelho (Cyprinus carpio specularis curtida pelas técnicas ao cromo e bioleather - DOI: 10.4025/actascianimsci.v26i4.1711 Resistance of the carp mirror skin (Cyprinus carpio specularis tanned by chromium and bioleather technique - DOI: 10.4025/actascianimsci.v26i4.1711

    Directory of Open Access Journals (Sweden)

    José Telmo Agostin Schmidt

    2004-04-01

    Full Text Available O objetivo do trabalho foi avaliar a técnica de curtimento bioleather e o curtimentocom sais de cromo, em peles de carpa espelho (Cyprinus carpio specularis. As peles foram retiradas com o auxílio de uma máquina, identificadas e congeladas. Em seguida, foram curtidas por meio de duas técnicas diferentes. O passo seguinte foi retirada dos corpos de prova, que foram levados para o laboratório, climatizado em torno de 23ºC e umidade relativa, do ar de 50%, conforme NBR 10455 (1988, por 24 horas. Para os testes de resistência à tração, ao alongamento e à determinação da força de rasgamento progressivo, utilizou-se o dinamômetro EMIC. Foram retiradas amostras da região dorsal do couro para análise de microscopia eletrônica de varredura (MEV. As amostras foram secas em ponto crítico com CO2 e metalizadas com íons de ouro-paládio. Em seguida as amostras foram elétron-micrografados com o JEOL-JSM 5410. Observou-se o entrelaçamento e sobreposição das camadas das fibras colágenas, que proporcionam maior resistência ao couro, constatada pelos testes realizados. Os couros curtidos com a técnica bioleather apresentaram maiores valores no teste de tração (20,45 N/mm2 em comparação ao cromo (12,32 N/mm2. Não houve diferença na elongação entre os tratamentos (bioleather = 72,52%; cromo = 84,74%. Para o teste de rasgamento progressivo, o curtimento ao cromo foi superior (26,28 N/mm, comparado ao bioleather (11,96 N/mm. Entretanto, os dois curtimentos podem ser utilizados nas peles dessa espécie de peixe para a confecção de vestuários.The objective of the work was to evaluate the tanning technique to bioleather and with chromium salts, in carp mirror skins (Cyprinus carpio specularis. The skins wore removed by means of a machine, identified and congealed. Next they were tanned by the two techniques. The test bodies wore removed and taken to the laboratory climatized around 23ºC and relative humidity of the 50% air, as ABNT

  2. Efeito das técnicas de inserção e ativação da resina composta sobre a microinfiltração e microdureza Effect of techniques of composite resin insertion and polymerization on microleakage and microhardness

    Directory of Open Access Journals (Sweden)

    Cristiane Mariote Amaral

    2002-09-01

    Full Text Available O objetivo deste trabalho foi avaliar a influência da técnica de ativação e de inserção da resina composta sobre a microinfiltração marginal e microdureza em restaurações classe II. Foram preparadas 180 cavidades que foram divididas em 6 grupos: G1 - incremento único + ativação convencional; G2 - incrementos vestíbulo-linguais + ativação convencional; G3 - incremento único + ativação "soft-start"; G4 - incrementos vestíbulo-linguais + ativação "soft-start"; G5 - incremento único + ativação progressiva; G6 - incrementos vestíbulo-linguais + ativação progressiva. Todas as cavidades foram restauradas com o sistema Z100/Single Bond (3M. Após 1.000 ciclos térmicos (5 e 55ºC, os espécimes foram imersos em solução aquosa de azul de metileno a 2%, por 4 horas e a microinfiltração foi avaliada. Metade dos espécimes foram incluídos em resina de poliestireno e a microdureza Knoop foi avaliada. Após o teste Kruskal-Wallis, não foi observada diferença significativa (p > 0,05 entre todas as técnicas de ativação e de inserção quanto à microinfiltração. Quanto à microdureza, após os testes análise de variância (2 fatores e Tukey, não houve diferença significativa entre as técnicas restauradoras empregadas (p > 0,05, porém a ativação progressiva (G5 e G6 apresentou menor dureza Knoop (p The aim of this study was to evaluate the influence of techniques of composite resin polymerization and insertion on microleakage and microhardness. One hundred and eighty class II cavities were prepared in bovine teeth and assigned to six groups: G1 - bulk filling + conventional polymerization; G2 - bucco-lingual increments + conventional polymerization; G3 - bulk filling + soft-start polymerization; G4 - bucco-lingual increments + soft-start polymerization; G5 - bulk filling + progressive polymerization; G6 - bucco-lingual increments + progressive polymerization. All cavities were restored with the Z100/Single Bond

  3. Análise da utilização de técnicas e ferramentas no programa Seis Sigma a partir de um levantamento tipo survey Analysis on the usage of techniques and tools from the Six-Sigma program on a survey-type assessment

    Directory of Open Access Journals (Sweden)

    Eduardo Guilherme Satolo

    2009-01-01

    Full Text Available O programa Seis Sigma é uma iniciativa adotada atualmente por muitas empresas e seu uso ocorre por meio de um processo altamente disciplinado e orientado, no qual são aplicadas diversas técnicas e ferramentas, que objetivam a geração de um ciclo de melhoria contínua. Diante desse fato e considerando a relevância do assunto, foi conduzido um levantamento tipo survey com o intuito de identificar e analisar as técnicas e ferramentas usadas nas etapas do método DMAIC e a sua comparação com a prescrição da literatura. Buscou-se levantar as técnicas e ferramentas mais e menos empregadas pelas empresas, permitindo-se confrontar estes resultados com outros levantamentos já realizados no exterior. Cabe destacar também que os resultados confirmaram o indicado pela literatura, os quais apontam que o programa Seis Sigma necessita apoiar-se em dados mensuráveis e confiáveis, evidenciando assim que o emprego das técnicas e ferramentas é indispensável junto ao método de melhoria DMAIC.The Six-Sigma program is an approach currently adopted by many companies and its usage occurs through a highly disciplined and guided process, in which several techniques and tools are applied, trYing to generate a continuous improvement cycle. Facing this fact and considering the relevance of the subject, a survey-based research was carried out. One of the objectives was to identify and analyse the techniques and tools used in the phases of the DMAIC and their comparison with the literature. The results consisted in assessing the techniques and tools most and least used by the companies, enabling to confront those with other previous research. It is also worthy highlighting that these results confirmed the indications of other publications, which state that the Six Sigma programme needs to be supported by measurable and trustworthy data. This makes evident that the usage of techniques and tools is indispensable for the DMAIC improvement method.

  4. As dobras da imagem

    Directory of Open Access Journals (Sweden)

    Profª. Drª. Fátima Antunes da Silva (Yaska Antunes

    2009-05-01

    Full Text Available O presente trabalho tem por objetivo tentar compreender a produção da imagem visual no teatro. Para isso se vale da apropriação livre do conceito de “dobra? de Gilles Deleuze para se referir à multiplicidade de imagens criadas pelas diversas modalidades artísticas. Como no teatro há o entrelaçamento de imagens verbais – palavras enunciadas pelo texto dramático ou teatral – com imagens visuais – a visualidade advinda da composição cênica concreta que organiza no espaço ator e objeto –, a ênfase só podia recair sobre estas duas formas imagéticas. No caso do teatro, surge ainda a percepção de que para além da materialidade da cena, outras imagens emergem do confronto entre palco e platéia. Nesse sentido, imagem teatral seria então aquilo que surge da interação entre ator e espectador. A contribuição desse trabalho pode estar no fato de atualizar certos conceitos sobre a criação da imagem poética na poesia e no cinema para aplicá-los ao teatro. Ao recuperar o pensa-mento de Otávio Paz, Alfredo Bosi, Sergei Eisenstein, entre outros, bus-ca-se promover uma reflexão mais aprofundada sobre a construção visual no teatro.

  5. Aplicação de técnicas eletroquímicas no estudo da dissolução oxidativa da covelita (CuS por Thiobacillus ferrooxidans Electrochemical techniques applied to study the oxidative dissolution of the covellite: CuS by Thiobacillus ferrooxidans

    Directory of Open Access Journals (Sweden)

    Christiane Medina Teixeira

    2002-02-01

    Full Text Available Among the copper sulphides, chalcopyrite (CuFeS2, covellite (CuS and chalcocite (Cu2S are the most important source of minerals for copper mining industry. The acknowledge of behaviour of these sulphides related with bacterial leaching process are essential for optimization procedures. Despite of its importance, covellite has not deserved much interest of researchers regarding this matter. In this work it was studied the oxidation of covellite by the chemolithotrophic bacterium Thiobacillus ferrooxidans by using electrochemical techniques, such as open circuit potentials with the time and cyclic voltammetry. The experiments were carried out in acid medium (pH 1.8, containing or not Fe2+ as additional energy source, and in different periods of incubation; chemical controls were run in parallel. The results showed that a sulphur layer is formed spontaneously due the acid attack, covering the sulphide in the initial phase of incubation, blocking the sulphide oxidation. However, the bacterium was capable to oxidize this sulphur layer. In the presence of Fe2+ as supplemental energy source, the corrosion process was facilitated, because ocurred an indirect oxidation of covellite by Fe3+, which was produced by T. ferrooxidans oxidation of the Fe2+ added in the medium.

  6. A Discrete Scatterer Technique for Evaluating Electromagnetic Scattering from Trees

    Science.gov (United States)

    2016-09-01

    Trees by DaHan Liao Approved for public release; distribution is unlimited. NOTICES Disclaimers The findings...for Evaluating Electromagnetic Scattering from Trees by DaHan Liao Sensors and Electron Devices Directorate, ARL...Technique for Evaluating Electromagnetic Scattering from Trees 5a. CONTRACT NUMBER 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 6. AUTHOR(S

  7. Trauma da Veia Porta

    Directory of Open Access Journals (Sweden)

    Gustavo Pereira Fraga

    Full Text Available OBJETIVO: O trauma da veia porta é raro e freqüentemente fatal por causa de exsanguinação e alta incidência de lesões de estruturas adjacentes. Devido às pecualiaridades desta lesão e diferentes condutas propostas na literatura, o objetivo dos autores é relatar a experiência neste tipo de lesão. MÉTODO: Estudo retrospectivo, de janeiro de 1994 e dezembro de 2001, de 1370 pacientes submetidos à laparotomia devido trauma abdominal. Entre esses, 15 pacientes apresentavam lesão da veia porta. As lesões foram classificadas conforme a sua extensão e localização. RESULTADOS: O mecanismo de trauma predominante foi o penetrante. O diagnóstico da lesão foi realizado no intraoperatório. Os procedimentos executados foram: sutura, anastomose término-terminal e ligadura da veia porta. A mortalidade foi de 53,3%. CONCLUSÃO: A lesão da veia porta possui alta taxa de mortalidade e o atendimento adequado está diretamente relacionado à sobrevida.

  8. Neutron techniques

    International Nuclear Information System (INIS)

    Charlton, J.S.

    1986-01-01

    The way in which neutrons interact with matter such as slowing-down, diffusion, neutron absorption and moderation are described. The use of neutron techniques in industry, in moisture gages, level and interface measurements, the detection of blockages, boron analysis in ore feedstock and industrial radiography are discussed. (author)

  9. Electrophysiologic assessment of regeneration in rat sciatic nerve repair using suture, fibrin glue or a combination of both techniques Avaliação eletrofisiológica da eficácia de três tipos de reparo após a secção do nervo ciático do rato

    Directory of Open Access Journals (Sweden)

    Roberto Sergio Martins

    2005-09-01

    Full Text Available We evaluated the repair of seccioned rat sciatic nerve by the comparison of electrophysiologic parameters. The repair was effected with suture (group A, fibrin glue (group B or a combination of both techniques (group C. The amplitude, latency and conduction velocity of the motor and nerve action potentials were assessed before the nerve section and at reoperation after 24 weeks. There was no difference between the groups when the nerve action potential was evaluated. Rats of group B presented better results than those of group A (pForam comparados os parâmetros obtidos na avaliação eletrofisiológica do potencial de ação do nervo e do potencial de ação motor antes e após 24 semanas do reparo no nervo ciático do rato previamente seccionado no lado direito com a utilização de sutura (grupo A, adesivo de fibrina (grupo B ou uma combinação das duas técnicas (grupo C. Não houve diferença entre os grupos na avaliação do potencial de ação do nervo. Quando consideradas a latência e a velocidade de condução mensurados na reoperação e a razão entre a velocidade de condução medida na reoperação e o mesmo parâmetro antes da secção do nervo, durante a mensuração do potencial de ação motor, os animais do grupo B apresentaram melhores resultados em relação aos do grupo A (p<0,05. Os animais do grupo C apresentaram melhores resultados em comparação com os do grupo A quando considerada a razão entre a velocidade de condução medida 24 semanas do reparo e antes da secção do nervo durante a avaliação do potencial de ação motor. Conclui-se que os animais em que o reparo dos nervos foi realizado com o adesivo de fibrina apresentaram melhores resultados em comparação com a sutura quando considerados os parâmetros obtidos na mensuração do potencial de ação motor.

  10. Técnica da peroxidação para a determinação de metionina em amostras derivadas de ensaios de digestibilidade do trigo e seus subprodutos em frangos de corte The peroxidation technique for methionine determination in derived samples of digestibility assays of the wheat and its by-products in broilers chickens

    Directory of Open Access Journals (Sweden)

    Leonardo Boscoli Lara

    2005-04-01

    Full Text Available Realizou-se um experimento com excreta de aves usando comparar técnicas de hidrólise de aminoácidos com ou sem peroxidação prévia para determinação de metionina. O delineamento experimental foi inteiramente ao acaso, em esquema fatorial 2 x 4 x 8, (métodos x tratamentos x alimentos com três repetições. Sete alimentos oriundos do trigo e uma ração-referência foram utilizados nos quatro tratamentos. Os dois primeiros tratamentos foram baseados na metodologia tradicional de consumo à vontade e utilizou-se o método da alimentação forçada com aves intactas e aves cecectomizadas nos tratamento 3 e 4, respectivamente. Somente a técnica de peroxidação da amostra com ácido perfórmico seguida de hidrólise apresentou resultados confiáveis na análise de biodisponibilidade e conteúdo de metionina do trigo e seu subprodutos.One experiment was conducted with broiler chickens, for evaluation of metabolizable methionine and its levels in the wheat and some of its products, comparing two analyses techniques of methionine determination; hydrolyze and peroxidation with performic acid before hydrolyze. The broilers were randomly distributed in factorial outline 2 x 4 x 8, (methods x treatments x feeds with three repetitions. Seven feeds by-products of wheat grain were used in the four treatments. The first two treatments were set in the traditional methodology of ad libitum consumption and in the treatments three and four, the method of forced feeding was used. The treatment four were tested in the caecectomised chickens. The results of this experiment suggested that only the peroxidation with performic acid before hydrolyze showed good result in measure metabolizable methionine and its levels of wheat and its by-products.

  11. Effect of irradiation mode and filling technique on resin/dentin bonding strength in class I cavities Efeito do modo de ativação e da técnica restauradora na resistência de união entre compósito e dentina em cavidades classe I

    Directory of Open Access Journals (Sweden)

    Alex José Souza dos Santos

    2004-09-01

    Full Text Available Factors such as light-curing mode, filling technique and cavity configuration may affect the bonding strength to dentin. This study evaluated the effect of irradiation mode and filling technique on resin/dentin bonding strength on the buccal wall of class I cavities in human teeth. Occlusal enamel was removed to expose a flat dentin surface. Occlusal cavities (4 x 3 x 3 mm were prepared in dentin. The adhesive Single Bond was applied according to the manufacturer's instructions and TPH Spectrum composite resin was placed using the following: oblique incremental, horizontal incremental or bulk filling techniques. The composite resin was light-cured either by continuous (600 mW/cm² for 40 s or Soft-Start (250 mW/cm² for 10 s + 600 mW/cm² for 30 s modes. Specimens of the control group were obtained by bonding the material to the flat exposed buccal wall of the cavity (C-factor = 1. The teeth were stored in water at 37ºC for 24 h and prepared for microtensile testing. Bonded beams of approximately 0.8 mm² were obtained from the buccal wall and tested with a tension of 0.5 mm/min. Results were analyzed by two-way ANOVA, Tukey's test and Dunnett's test (alpha = 0.05. Incremental placement techniques with both irradiation modes produced higher bonding strength values than the bulk technique (p Fatores como o modo de ativação, a técnica restauradora e a configuração cavitária podem afetar a resistência adesiva à dentina. Este estudo avaliou os efeitos dos modos de ativação e das técnicas restauradoras na resistência de união compósito/dentina na parede vestibular de restaurações classe I. O esmalte oclusal dos dentes foi removido para expor uma superfície dentinária planificada. Cavidades oclusais (4 x 3 x 3 mm foram preparadas em dentina. O adesivo Single Bond foi aplicado de acordo com as instruções do fabricante, e o compósito TPH Spectrum, inserido através de três diferentes técnicas: oblíqua incremental, horizontal

  12. Bacteriemia during endodontic treatment in relation to the technique of biomechanical preparation: randomized clinical trial Bacteriemia durante o tratamento endodôntico em função da técnica de preparo biomecânico: ensaio clínico randomizado

    Directory of Open Access Journals (Sweden)

    Adriane Tenório Dourado

    2005-12-01

    Full Text Available OBJECTIVE: The aim of this randomized clinical trial was to evaluate the frequency of bacteriemia during endodontic treatment, with comparison between two techniques for biomechanical preparation of the root canal system. MATERIALS AND METHODS: The sample comprised 50 patients aged 16 to 52 years, of both genders, which were divided into 2 groups with 25 patients each. Group I underwent biomechanical preparation by the step-back technique, and Group II was treated by the rotary technique with nickel-titanium instruments (K3. Patients were submitted to antisepsis of the oral cavity with chlorhexidine digluconate and three samples of blood were collected for blood culture: preoperatively, immediately after the biomechanical preparation and 10 minutes later. The significance level adopted was 5.0%, and analysis was performed by descriptive and inferential statistics by means of the Fisher's exact test, Fisher-Freeman-Halton test and Student's t test. Data were analyzed on the Statexact and SPSS softwares. RESULTS: All blood cultures achieved before and immediately after preparation were negative. On the other hand, with regard to the blood cultures collected 10 minutes after preparation, one (4% positive case was found for Group I. However, this difference was not statistically significant (p = 0.50. CONCLUSION: The frequency of bacteriemia was low and observed just for Group I.OBJETIVO: O objetivo deste ensaio clínico randomizado foi avaliar a freqüência de bacteriemia durante o tratamento endodôntico comparando duas técnicas de preparo biomecânico do sistema de canais radiculares. MATERIAIS E MÉTODOS: A amostra constou de 50 pacientes, com idade variando entre 16 e 52 anos e de ambos os sexos, sendo dividida em 2 grupos de 25 pacientes. No Grupo I, realizou-se o preparo biomecânico através da técnica escalonada com recuo progressivo programado, e, no Grupo II, por meio técnica rotatória, empregando instrumentos de níquel-titânio (K3

  13. ORQUIECTOMIA EM BOVINOS EMPREGANDO ABRAÇADEIRA DE NÁILON NA HEMOSTASIA PREVENTIVA: EFEITO DA ESTAÇÃO DO ANO, MÉTODO DE CONTENÇÃO E TÉCNICA CIRÚRGICA USE OF NYLON TIE-WRAPS FOR PREVENTIVE HAEMOSTASIS IN BOVINE ORCHIECTOMY: INFLUENCE OF SEASON, RESTRAINT METHOD AND SURGICAL TECHNIQUE

    Directory of Open Access Journals (Sweden)

    Jorge Luis Ferreira

    2009-04-01

    Full Text Available

    A orquiectomia pode ser praticada mediante a utilização de diferentes procedimentos cirúrgicos – método de duas incisões laterais (IL, de incisão transversal (IT e secção do funículo espermático por meio do burdizzo. Avaliaram-se o efeito da estação do ano, o método de contenção e a técnica cirúrgica sobre a recuperação de bovinos mestiços (Zebu x Europeu orquiectomizados empregando a abraçadeira de náilon na hemostasia preventiva. O estudo foi desenvolvido em uma propriedade rural, com 168 bovinos, machos, dezoito meses de idade e peso médio de 290 Kg, nos meses de maio de 2005 e janeiro de 2006. Distribuíram-se os animais em oito grupos compostos por 21 bovinos (GI, GII, GIII, GIV, GV, GVI, GVII, GVIII, para verificar as complicações pós-operátorias e a evolução clínica da cicatrização, nos dias três, 23, 43 e 63 dias após o procedimento. Conclui-se que a orquiectomia em bovinos realizada no mês de maio, mediante o emprego do método de contenção em bretes, resultou em menores índices de complicações pós-operatórias. As técnicas cirúrgicas não influenciaram na ocorrência de complicações. A abraçadeira de náilon mostrou-se eficiente na hemostasia preventiva.

    PALAVRAS-CHAVES: Abraçadeira de náilon, bovinos, castração, pós-operatório.

    Orchiectomy may be carried out through several surgical procedures, from the double lateral incision method (LI, transverse incision (TI, until the section of spermatic funnicle by burdizzo. The scope was to evaluate the effect of the season, contend method and surgical technique on the recovery of crossbred cattle (Bos indicus x Bos taurus submitted to orchiectomy, employing nylon bracers for preventive haemostasia. The study was carried out on a farm using 168 male

  14. Synthesis and characterization of SnO2 doped with fluorine by the technique of polymeric precursors; Sintese e caracterizacao de SnO2 dopado com fluor pela tecnica dos precursores polimericos

    Energy Technology Data Exchange (ETDEWEB)

    Pereira, Gilberto J.; Lopes, Rafael Ialago, E-mail: gilbertop@fei.edu.br [Centro Universitario FEI, Sao Bernardo do Campo, SP (Brazil). Departamento de Engenharia de Materiais

    2016-07-01

    The present work deals with the synthesis of tin dioxide powders doped with fluorine and chlorine anions to evaluate the influence of these on the physico-chemical properties of SnO2, as well as to verify if the dopant does not make a solid solution with the material and its possible use as sintering additive. The samples were synthesized by Pechini method (polymer precursors) with tin oxalate as a source not contaminated with chlorine of this metal. Specific surface area characterization (BET method) and X-ray diffractometry (XRD) show that doping reduces the particle size of SnO2, being more effective at lower dopant levels. The dilatometry of the doped powders shows a reduction in the beginning and end temperatures of the sintering of the tin dioxide when compared with values in the literature.

  15. Da Vinci Linjen

    DEFF Research Database (Denmark)

    Nissen, Poul

    Afsluttende evalueringsrapport fra følgeforskningen gennem tre år i forbindelse med dety pædagogiske arbejde på Blåbjerggårdskolens Da Vinci Linje for skolemotiverede og underpræsterende elever på 7. til 9. klassetrin.......Afsluttende evalueringsrapport fra følgeforskningen gennem tre år i forbindelse med dety pædagogiske arbejde på Blåbjerggårdskolens Da Vinci Linje for skolemotiverede og underpræsterende elever på 7. til 9. klassetrin....

  16. Avaliação da força de tração em braquetes colados pela técnica indireta com diferentes sistemas de adesão Evaluation of tensile strength of brackets bonded by indirect technique

    Directory of Open Access Journals (Sweden)

    André Tortamano

    2007-06-01

    Full Text Available OBJETIVO: o objetivo do presente estudo foi avaliar a resistência à tração de braquetes ortodônticos colados pela técnica indireta e pela técnica direta convencional. METODOLOGIA: foram utilizados 50 pré-molares humanos íntegros, recém-extraídos por motivos ortodônticos. Esses dentes foram divididos em 5 grupos, nos quais foram colados braquetes ortodônticos metálicos (Abzil-Brasil com as resinas compostas ortodônticas Concise (3M-Unitek-EUA e Transbond XT (3M-Unitek-EUA - utilizadas em ambas as técnicas, direta e indireta - e Transbond Sondhi (3M-Unitek-EUA - desenvolvida exclusivamente para a técnica indireta. O grupo I (controle I foi objeto de colagem direta com Transbond XT; no grupo II (controle II procedeu-se à colagem direta com Concise o grupo III recebeu colagem indireta com Concise; o grupo IV foi submetido à colagem indireta com Transbond XT e no grupo V foi realizada colagem indireta com Transbond Sondhi. Na técnica direta, o braquete foi colado diretamente sobre o esmalte após condicionamento ácido e aplicação de adesivo. Na técnica indireta, os braquetes foram colados primeiramente sobre modelo de gesso e depois transferidos para o dente, com o auxílio de moldeira individualizada. Os corpos-de-prova foram submetidos a testes de tração (Instron 4400 e os resultados foram objeto de testes estatísticos de análise de variância e de Tukey a 1%. RESULTADOS: os grupos III e V revelaram resultados significantemente menores que os dos dois grupos controles. CONCLUSÃO: a força obtida na colagem indireta com a resina Transbond XT não difere da força obtida na colagem direta com as resinas Concise e Transbond XT.AIM: The purpose of this study was to evaluate the bonding strength of brackets for direct and indirect bonding techniques. METHODS: Were used 50 human premolars recently extracted for orthodontic reasons. These teeth were divided in 5 groups and metalic orthodontic brackets (Abzil-Brazil were bonded

  17. Erosion and sediment deposition evaluation on slopes under different tillage systems in the Cerrado region using the {sup 137}Cs fallout technique; Analise da distribuicao do fallout do {sup 137}Cs na avaliacao da erosao e deposicao de sedimentos em sistemas de manejo de solo sob Cerrado

    Energy Technology Data Exchange (ETDEWEB)

    Arthur, Robson Clayton Jacques

    2010-07-01

    In Brazil, the expansion of agricultural areas causes several problems on natural resources. With the increasing occupation of the Cerrado region by agriculture, a series of environmental problems like deforestation, soil erosion and soil compaction are appearing and causing radical transformations in the natural landscape due to removing almost all native vegetation. The conventional tillage system (CTS) is considered an inadequate form of soil management for its frequently irremediable consequences of soil compaction and soil erosion, and the no till system (NTS) makes the maintenance of the soil conditions possible, letting them close to the natural environment, thus reducing rates of soil erosion. The objective of this work was to evaluate the efficiency of riparian forests in the retention of sediments originated for three different tillage systems, through the fallout {sup 137}CS redistribution technique, the Universal Soil Loss Equation (USLE) and some physical and chemical parameters that indicate the structural conditions of the soils of Goiatuba and Jandaia-GO. In the three areas, soil profiles were collected in three layers of 20 cm (0-20, 20-40 and 40-60 cm) at distinct points located along linear transects in the direction of the maximum slope until the riparian forest. In the riparian forest of each area, trenches were opened and soil was sampled to evaluate the activity of {sup 137}Cs and the physical and chemical parameters of soil. Detection of the activity of {sup 137}Cs was made with a gamma ray detector model (GEM-20180P, EG and ORTEC) connected to a multichannel analyzer. The comparison of averages was made using the Tukey test at 5% level of significance. The. results indicated that, the three soil tillage systems presented high rates of soil erosion and deposition of sediments and the riparian forest of the areas under CTS, NTS and pasture, located downstream received great amounts of sediments, and that only the riparian forest of CTS was

  18. Astrophysical techniques

    CERN Document Server

    Kitchin, CR

    2013-01-01

    DetectorsOptical DetectionRadio and Microwave DetectionX-Ray and Gamma-Ray DetectionCosmic Ray DetectorsNeutrino DetectorsGravitational Radiation Dark Matter and Dark Energy Detection ImagingThe Inverse ProblemPhotographyElectronic ImagingScanningInterferometrySpeckle InterferometryOccultationsRadarElectronic ImagesPhotometryPhotometryPhotometersSpectroscopySpectroscopy SpectroscopesOther TechniquesAstrometryPolarimetrySolar StudiesMagnetometryComputers and The Internet.

  19. Presentation Technique

    International Nuclear Information System (INIS)

    Froejmark, M.

    1992-10-01

    The report presents a wide, easily understandable description of presentation technique and man-machine communication. General fundamentals for the man-machine interface are illustrated, and the factors that affect the interface are described. A model is presented for describing the operators work situation, based on three different levels in the operators behaviour. The operator reacts routinely in the face of simple, known problems, and reacts in accordance with predetermined plans in the face of more complex, recognizable problems. Deep fundamental knowledge is necessary for truly complex questions. Today's technical status and future development have been studied. In the future, the operator interface will be based on standard software. Functions such as zooming, integration of video pictures, and sound reproduction will become common. Video walls may be expected to come into use in situations in which several persons simultaneously need access to the same information. A summary of the fundamental rules for the design of good picture ergonomics and design requirements for control rooms are included in the report. In conclusion, the report describes a presentation technique within the Distribution Automation and Demand Side Management area and analyses the know-how requirements within Vattenfall. If different systems are integrated, such as geographical information systems and operation monitoring systems, strict demands are made on the expertise of the users for achieving a user-friendly technique which is matched to the needs of the human being. (3 figs.)

  20. Política de ensino para a prevenção da violência: técnicas de ensino que podem contribuir para a diminuição da violência escolar Política de enseñanza para la prevención de la violencia: técnicas de enseñanza que pueden contribuir para la disminución de la violencia escolar Teaching policy to violence prevention: Teaching techniques that can contribute to school violence reduction

    Directory of Open Access Journals (Sweden)

    Alvaro Chrispino

    2011-03-01

    Full Text Available O presente trabalho focaliza o conflito escolar como fruto da massificação da escola, que permitiu o ingresso de estudantes com diferentes origens, valores e culturas, na concretização do direito de uma escola para todos. A manifestação do conflito surge da diferença não trabalhada pela escola. Indica os movimentos realizados no campo das políticas educacionais e os esforços para definir e implantar uma escola pacífica e uma aula pacífica. Apresenta três técnicas de ensino que contribuem para a diminuição da violência escolar com seus fundamentos e possíveis variações.El presente trabajo presenta el conflicto escolar como consecuencia de la masificación de la escuela, entidad que permitió el ingreso de estudiantes de distintos orígenes, valores y culturas, en la práctica del derecho de una escuela para todos. La manifestación del conflicto emerge de la diferencia que existe en la escuela y no se la trabaja. Señala también los movimientos realizados en el área de las políticas educacionales y los esfuerzos para definir e implantar una escuela y una clase pacífica. Presenta tres técnicas de enseñanza que contribuyen para la disminución de la violencia escolar con sus fundamentos y posibles variaciones.The present work focus on the school conflict as a result of school massification, which allowed the admission of students with different origins, conceptions and cultures. The manifestation of the conflict arises from the distinction the school did not work on. It indicates the movements made in the educational politics field and the efforts to define and implant pacific schools and classes. It presents three teaching techniques that contribute to the school violence reduction with its elements and possible variations.

  1. OBTENTION METHODS OF RESPIRATORY TRACT CELSS IN HEALTHY SHEEP BY THE TRACHEOBRONCHEAL LAVAGE TECHNIQUE BY NASOTRACHEAL VIA METODOLOGIA DE COLHEITA DE CÉLULAS DO TRATO RESPIRATÓRIO EM OVINOS SADIOS ATRAVÉS DA TÉCNICA DE LAVAGEM TRAQUEOBRÔNQUICA POR VIA NASOTRAQUEAL

    Directory of Open Access Journals (Sweden)

    Roberto Calderon Gonçalves

    2008-07-01

    Full Text Available

    The technique of pulmonary cells obtention by nasotracheal intubation was evaluated and the cellular population of 19 healthy sheep was characterized. The animals were hold standing still with head and neck strait; aligned with the vertebral spine and a silicone tube guide till the carina, to introduce a lower caliber tube for precede the tracheobronchial lavage. The average counting of nucleated cells was 64.650 ± 49.674. The cytological analyses of the samples slowed by the average of obtained percentages: 62.74% of macrophages, 15.01% cylindrical epithelial cells, 20.04% of neutrophills, 1.44 of lymphocytes and 0.77% of eosinophills. It was concluded that this methods of sample obtention by nasotracheal intubation to reach the tracheobronchial region was efficient to cytological characterization and cellular differentiation in the obtained samples, being well supported by the animals.

     

    KEY WORDS: Citocentrifugation, cytology, tracheobronchial lavage, sheep.

    Avaliou-se a técnica de colheita de células do trato respiratório em ovinos, por sondagem nasotraqueal, e caracterizou-se a população celular em dezenove ovinos clinicamente sadios. Os animais foram contidos em estação, com cabeça e pescoço estendidos e alinhados com a coluna vertebral. Após a contenção, introduziu-se uma sonda-guia siliconizada até a bifurcação da traquéia, por dentro da qual se passou uma sonda de menor calibre, para realização do lavado traqueobrônquico. A média da contagem de células nucleadas foi de 64.650 ± 49.674. A análise citológica das amostras evidenciou, pelas médias das porcentagens obtidas, 62,74% de macrófagos, 15,01% de células epiteliais cilíndricas, 20,04% de neutrófilos, 1,44% de linfócitos e 0,77% de eosinófilos. Concluiu-se que o método de colheita por sondagem nasotraqueal foi eficiente na obtenção de amostras de regi

  2. Profilaxia da peste

    Directory of Open Access Journals (Sweden)

    Renato dos Santos Araújo

    1967-12-01

    Full Text Available O autor parte da premissa de que a profilaxia da doença infecciosa decorre do encadeamento epidemiológico: fonte de infecção-veículo transmissor - receptivel, para explicar a da peste, baseada no mesmo princípio. Depois de citar os 4 principais complexos epidemiológicos da peste e afirmar que tôda a profilaxia da doença consiste em atingir os dois primeiros elos dessas cadeias e proteger o último, passa a classificar os vários métodos profiláticos empregados em 2 grandes grupos: o das medidas destrutivas ou provisórias e o das medidas supressivas ou definitivas. Entre as primeiras arrola a desratização e a despulização, às quais acrescenta o tratamento e isolamento do doente e do portaãor, e entre as segundas inclui a anti-ratização e a imunização. A seguir, passa a explicar em que consistem essas várias medidas profiláticas e quais os agentes de que se tem lançado mão para executá-las, expendendo ao curso dessa exposição o conceito que formula a respeito de cada uma delas, à guisa de apreciação do seu valor relativo. Enaltece sobretudo as medidas supressivas ou definitivas, às quais empresta a maior significação na luta antipestosa, chamando a atenção, em especial, para a necessidade de estudos imunológicos para aperfeiçoamento do poder imunitário das vacinas de germes vivos avirulentos, que considera um grande recurso para a profilaxia da doença, sobretudo para a proteção do rurícola, cujo labor e modo de vida o expõem inevitavelmente a se infectar, por ocasião da ocorrência de epizootias de origem silvestre. Concluída essa primeira parte, passa a fazer o histórico de como se desenvolveu a campanha contra a peste, no Brasil, desde a época da sua invasão em 1899 pelo pôrto de Santos até os nossos dias. Nesse histórico, detem-se um pouco para expôr a atuação do extinto Serviço Nacional de Peste, o qual, criado em 1941, após a reorganização do Departamento Nacional de Saúde, passou

  3. Comparative study between endoscopic technique by a proximal port and mini palmary incision in the surgical treatment of carpal tunnel syndrome Estudo comparativo entre a técnica endoscópica pelo portal proximal e a técnica de mini-incisão palmar no tratamento cirúrgico da síndrome do túnel do carpo

    Directory of Open Access Journals (Sweden)

    Eduardo A.R. Pereira

    2003-01-01

    Full Text Available The authors present a prospective study comparing two surgical techniques for carpal tunnel release. A minimal - incision open decompression(3 is compared with an endoscopic release(2, that utilizes only a single proximal portal. There were operated on, 28 wrists in 28 patients, with clinical signs and EMG changes consistent on idiopathic carpal tunnel syndrome, that failed under previous conservative treatment. They were randomized into two groups , undertaken surgical treatment, either by endoscopic release or by open decompression. Grip strength (measured by dynamometric, sensitivity (measured by Semmes-Weinstein monofilaments, presence of pain and paresthesia, date of return to activities of daily living and complications were evaluated pre-operative and at 1, 2, 4, 6, 12 weeks after surgery. After 12 months average follow up, the results indicated that this proximal portal endoscopic technique can be safely performed, showing advantages over open conventional method, in terms of sooner return of grip strength, date of return to activities of daily living, and less incidence of pillar pain. No differences in paresthesia resolution, sensibility improvement or complications incidence were found.Os autores apresentam estudo prospectivo onde comparam duas técnicas cirúrgicas empregadas no tratamento de pacientes acometidos pela síndrome do túnel do carpo. A técnica de descompressão por via aberta, através de mini-incisão palmar(3, é analisada em relação à técnica por via endoscópica, descrita por Agee et al.(2, que utiliza apenas um único portal proximal. Foram operados, de forma randomizada, 28 punhos em 28 pacientes com o diagnóstico clínico e eletromiográfico de síndrome do túnel do carpo idiopático, e que não obtiveram melhora com o tratamento conservador prévio. Os seguintes parâmetros, foram analisados no pré-operatório e na primeira, segunda, quarta, sexta e décima segunda semanas de pós-operatório: força de

  4. Cerâmicas avançadas no processo de retificação cilíndrica externa de mergulho com rebolos diamantados com a técnica da mímima quantidade de lubrificação e refrigeração otimizada Advanced ceramics in the external cylindrical plunge grinding using the technique of minimum quantity of lubrication and the technique of optimized refrigeration with diamond wheels

    Directory of Open Access Journals (Sweden)

    M. H. Oikawa

    2011-09-01

    Full Text Available Os materiais cerâmicos têm muitas vantagens em relação a outros materiais, entre elas, três principais: capacidade de operação em altas temperaturas, alta dureza e alta resistência ao desgaste. Por essa razão, são aptos a serem usados em situações que exigem pouco desgaste, tanto em temperatura ambiente quanto em temperaturas elevadas. Estas propriedades fizeram as cerâmicas avançadas terem uma importante parte na utilização em aplicações na indústria nas últimas décadas. Porém, o custo agregado ao acabamento da peça ainda é muito alto. Esse acabamento geralmente é feito pelo processo de retificação, único processo economicamente viável que produz superfícies de elevada qualidade e precisão geométrica. As empresas desse modo vêm buscando a otimização no processo de retificação de cerâmicas, explorando outras técnicas de lubrificação. Assim, este projeto pretendeu explorar a otimização do método de lubrificação na retificação cilíndrica externa de mergulho com o método da mínima quantidade de lubrificação (MQL e refrigeração otimizada. Foram utilizadas três métodos de refrigeração, o convencional o MQL e a refrigeração otimizada, com três avanços de corte para cada caso. Foram analisadas como variáveis de saída a relação G, rugosidade e circularidade. Dos resultados obtidos, pode-se concluir que a refrigeração otimizada é a que apresenta os melhores resultados, sendo esta uma alternativa viável de melhora do processo. O MQL apresentou resultados insatisfatórios em comparação aos outros dois métodos, porém, ainda aceitáveis em alguns processos de retificação. Considerando a dificuldade e altos custos de descarte do fluido de corte devido às rígidas leis ambientais, o MQL vem como uma forte tendência neste tipo de processo.Ceramic materials have many advantages over other materials, including three main: capability of operating at high temperatures, high hardness and

  5. Efeitos da implantação de técnicas agropecuárias na intensificação de sistemas de produção de leite em estabelecimentos familiares Effects of applying agricultural techniques for increase production of small family farms

    Directory of Open Access Journals (Sweden)

    Airton Manzano

    2006-04-01

    Full Text Available A viabilidade econômica da produção de leite em estabelecimentos familiares (EF foi avaliada no município de São Carlos, SP, no período de 1998 a 2001, por meio de ações técnicas e gerenciais que intensificam os sistemas de produção sustentável. Utilizaram-se seis EF (4,2 a 27,2 ha que tinham como principal atividade econômica a produção de leite. As ações foram: agropecuárias: a alimentação: plantio e fornecimento de cana-de-açúcar + uréia na seca, alimentação suplementar de acordo com a produção da vaca e pastejo rotacionado nas águas; b manejo: melhoria do conforto dos animais; c reprodução: uso de inseminação artificial e/ou monta natural e controle reprodutivo do rebanho; d sanidade: controle de ecto e endoparasitas, exames de brucelose e tuberculose; e melhoramento genético: uso de touro selecionado; ambientais: recuperação e conservação de recursos naturais, melhoria da qualidade da água e recuperação da fertilidade do solo; e gerenciais: controle zootécnico do rebanho, práticas de associativismo, descarte de animais improdutivos e análise econômica. Para a análise de variância em cada EF, considerou-se um modelo que incluiu o efeito médio geral e os efeitos de ano e de meses dentro de ano. Uma vez que o efeito de ano esteve confundido com as ações técnicas e/ou tecnologias implementadas, as estimativas desse efeito, por polinômios ortogonais, possibilitaram estimar as mudanças quantitativas dos índices zootécnicos e gerenciais, em relação a 1998. As médias de acréscimos dos valores estimados dos seis EF em 2001, em comparação ao ano de 1998, para as produções de leite/ano, leite/ha/ano e leite/vaca, a receita e o patrimônio aumentaram 24, 36, 38, 70 e 27%, respectivamente. Os custos operacional e total reduziram, respectivamente, 24,1 e 15,8% e o lucro aumentou 4%. Entre os seis EF estudados, dois tornaram-se modelos de sistemas de produção de leite familiares. Concluiu

  6. Biomicroscopia ultra-sônica na avaliação da posição das lentes intra-oculares em uma técnica de fixação escleral Ultrasound biomicroscopy in the assessment of the intraocular lenses positioning in a transscleral fixation technique

    Directory of Open Access Journals (Sweden)

    Raul de Camargo Vianna Filho

    2000-10-01

    Full Text Available Objetivo: Avaliar pela biomicrospia ultra-sônica (UBM o posicionamento, em relação ao sulco ciliar, das alças de lentes intra-oculares (LIO, em uma técnica de fixação escleral, avaliando-se também se dois pontos de fixação são suficientes para que não haja inclinação da parte óptica. Métodos: Dezesseis olhos afácicos foram submetidos a implante LIO por uma mesma técnica de fixação escleral, realizados por um mesmo cirurgião. Um mês após a cirurgia, o posicionamento das alças das LIO foram avaliados pelo UBM, assim como distâncias entre as LIO e córnea. Os resultados foram submetidos a testes estatísticos. Resultados: Das 32 alças fixadas à esclera, oito estavam localizadas no sulco ciliar e 24 fora deste. Não houve diferença estatística nas distâncias entre LIO e córnea para alças posicionadas no sulco ciliar quando comparadas àquelas localizadas fora do sulco. Isto sugere que, além da distância ao limbo que se transfixa a esclera, outros fatores devem estar associados ao posicionamento da alça no sulco ciliar. As medidas LIO -- córnea realizadas na periferia das LIO às 3, 6, 9, e 12 horas foram semelhantes, mostrando que dois pontos de fixação são suficientes para que a LIO não fique inclinada. Conclusões: Outros fatores (por exemplo o ângulo de abertura do corpo ciliar, além da distância ao limbo na qual se transfixa a esclera, são importantes para o posicionamento das alças no sulco ciliar. Dois pontos de fixação são suficientes para que a LIO não apresente inclinação dentro do olho.Purpose: To assess, through ultrasound biomicroscopy (UBM, the positioning of the intraocular lenses (IOL haptics as related to the ciliary sulcus by using a scleral fixation technique; and to evaluate, as well, if two fixation points are sufficient to avoid tilting of the lenses. Methods: Sixteen aphakic eyes underwent an IOL implan-tation by means of the same scleral fixation technique, performed by the

  7. Astrophysical techniques

    Energy Technology Data Exchange (ETDEWEB)

    Kitchin, C R

    1984-01-01

    The subject is covered in chapters, entitled: detectors (optical and infrared detection; radio and microwave detection; X-ray and gamma-ray detection; cosmic ray detectors; neutrino detectors; gravitational radiation); imaging (photography; electronic imaging; scanning; interferometry; speckle interferometry; occultations; radar); photometry and photometers; spectroscopy and spectroscopes; other techniques (astrometry; polarimetry; solar studies; magnetometry). Appendices: magnitudes and spectral types of bright stars; north polar sequence; standard stars for the UBV photometric system; standard stars for the UVBY photometric system; standard stars for MK spectral types; standard stars for polarimetry; Julian date; catalogues; answers to the exercises.

  8. Llizarov technique

    International Nuclear Information System (INIS)

    Shankman, S.; Rosenberg, Z.S.; Frankel, V.; Golyakhovsky, V.

    1990-01-01

    This paper illustrates the radiographic manifestations of the Ilizarov distraction technique for the correction of short and deformed limbs. The radiographs of 130 patients who underwent Ilizarov distraction at 160 sites since December 1986 were reviewed retrospectively. Reasons for correction included fracture nonunion and malunion idiopathic leg length discrepancy, achondroplasia, and neurofibromatosis with tibial pseudarthrosis. Ninety patients were adults, and 40 were children. In order to assess cortical bone development during the fixation phase, CT of the regenerate bone was performed in 17 patients. Conventional tomograms were obtained in 20 patients for the evaluation of delayed or hypoplastic union at the distraction site

  9. Experimental Techniques

    International Nuclear Information System (INIS)

    Fournier, D.; Serin, L.

    1995-01-01

    Experimental techniques to be used in the new generation of high energy physics are presented. The emphasis is put on the new ATLAS and CMS detectors for the CERN LHC. For the most important elements of these detectors, a description of the underlying physics processes is given, sometimes with reference to comparable detectors used in the past. Some comparative global performances of the two detectors are also given, with reference to benchmark physics processes (detection of the Higgs boson in various mass regions, etc). (author)

  10. Microbiological air quality of processing areas in a dairy plant as evaluated by the sedimentation technique and a one-stage air sampler Qualidade microbiológica do ar de ambientes de processamento em indústria de laticínios avaliada por amostrador de ar de um estágio e pela técnica da sedimentação

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    Valéria Costa Salustiano

    2003-07-01

    Full Text Available The microbiological air quality at processing areas in a dairy plant was evaluated by using a one-stage air sampler, based on Andersen principles (impaction technique and by culture settling plate technique, also known as sedimentation technique. Among these areas, milk reception, packaging, and pasteurization rooms were included. Rooms where cheese, yogurt, butter and "doce de leite"(Latin American typical treat made of concentrated milk and sugar are made were also evaluated. For all processing areas, the numbers of mesophilic aerobic bacteria and yeast and molds recovered by air sampler were higher than 90 CFU·m-3 - the maximum value recommended by American Public Health Association (APHA. In four of the six processing areas, the microbial numbers were higher than APHA's standard (30 CFU.cm-2.week-1 according to culture settling plate technique. The results showed a difference (pFoi avaliada a microbiota do ar dos ambientes de recepção, embalagem e pasteurização de leite, produção de queijos, de iogurte e de doce de leite e manteiga em uma indústria de laticínios pelas técnicas de sedimentação e de impressão em ágar utilizando um amostrador de ar de um estágio baseado no princípio de Andersen. As contagens de microrganismos mesófilos aeróbios e de fungos filamentosos e leveduras pela técnica impressão em ágar ultrapassaram 90UFC·m-3 de ar, valor máximo recomendado pela APHA. Pela técnica de sedimentação, as contagens microbianas do ar de quatro ambientes também ultrapassaram 30UFC·cm-2·semana-1, conforme recomendação da APHA. Os ambientes diferiram (p<0,05 apenas para os números de Staphylococcus aureus. (<1,0 a 4,3 UFC.m-3. As contagens microbianas por impressão em ágar foram de 2 a 10 vezes maiores que as obtidas por sedimentação, evidenciando a maior capacidade da impressão em ágar em determinar microrganismos do ar, inclusive patógenos. Quanto à distribuição da microbiota do ar, houve a predomin

  11. Avaliação da técnica de lavagem das mãos executada por alunos do Curso de Graduação em Enfermagem Evaluación de los alumnos del curso de graduación de enfermería de la técnica de lavado de manos Evaluation of the handwashing technique held by students from the nursing graduation course

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    Carla Cristiane Paz Felix

    2009-03-01

    Full Text Available O objetivo deste estudo foi comparar a execução e verificar a adesão à técnica de lavagem das mãos por alunos de um Curso de Graduação em Enfermagem. A pesquisa foi realizada com 113 alunos que estavam cumprindo estágio em instituições de saúde do município de São Paulo. Os dados foram coletados por observação direta utilizando um instrumento em forma de check-list com os passos da técnica. Os alunos do 2º e 3º ano obtiveram melhor desempenho na maioria dos passos na execução da técnica, com diferença estatisticamente significante, quando comparados ao 4º ano. A adesão aos passos da técnica pelos alunos foi muito baixa, pois apresentaram adesão menor que 50% em metade dos passos. A média de alunos que executou todos os passos da técnica corretamente foi muito baixa, 8,8%. Os alunos observados não realizaram a técnica de lavagem das mãos conforme recomendado.El objetivo de este estudio fue comparar la ejecución y verificar la adhesión a la técnica de lavado de las manos por alumnos de un Curso de Graduación en Enfermería. La investigación fue realizada con 113 alumnos que estaban realizando una práctica en instituciones de salud del municipio de San Pablo. Los datos fueron recolectados por observación directa utilizando un instrumento en forma de check-list con los pasos de la técnica. Los alumnos del 2º y 3º año obtuvieron un mejor desempeño en la mayoría de los pasos en la ejecución de la técnica, con una diferencia estadísticamente significativa, cuando comparados al 4º año. La adhesión a los pasos de la técnica por los alumnos fue muy baja, ya que presentaron una adhesión menor que 50% en la mitad de los pasos. El promedio de los alumnos que ejecutaron todos los pasos de la técnica correctamente fue muy baja, 8,8%. Los alumnos observados no realizaron la técnica de lavado de las manos conforme recomendado.The purpose of this study was to compare the execution and verify the compliance

  12. Tratamento cirúrgico videolaparoscópico da doença do refluxo gastroesofagiano: técnica de Nissen modificada - resultados clínicos e funcionais Videolaparoscopic surgical treatment of gastroesophageal reflux disease: modified Nissen technique - clinical and functional results

    Directory of Open Access Journals (Sweden)

    L. R. LOPES

    2001-06-01

    Full Text Available A doença do refluxo gastroesofagiano é muito freqüente na população e o tratamento cirúrgico é indicado em um número respeitável de pacientes. A escolha da via de acesso é a laparoscopia. Várias técnicas anti-refluxo podem ser empregadas e preferimos a técnica de Nissen modificada. OBJETIVO: Analisar os parâmetros clínicos e funcionais pré-operatórios comparados com os mesmos parâmetros pós-operatórios com a técnica empregada. MÉTODOS: Um grupo de 59 pacientes foi submetido a tratamento cirúrgico pela técnica de Nissen modificada videolaparoscópica. O diagnóstico pré-operatório foi feito por exame radiográfico contrastado e endoscopia digestiva alta em todos os pacientes. A manometria do esôfago realizada em 35 e a cintilografia em 15. Esofagite complicada ocorreu em 54,2% sendo 21 pacientes (35,6% com epitélio de Barrett. A técnica cirúrgica laparoscópica foi concluída em todos os pacientes. O tempo médio de cirurgia foi de 123,9 minutos. RESULTADOS: Não ocorreram complicações intra-operatórias. A alta se deu em média com 47,6 horas. Sintomas de disfagia, dor, epigastralgia, regurgitação e flatulência até o 30° dia ocorreram em 48,1% dos pacientes. Ocorreu uma reoperação por recurrência da doença e um óbito por necrose do fundo gástrico. O seguimento médio foi de 20,8 meses. Os exames pós-operatórios radiográficos, endoscópicos, manométricos e de cintilografia mostraram melhora significativa, bem como a avaliação clínica, que mostrou excelentes e bom resultados em 93,1% dos pacientes. CONCLUSÃO: A cirurgia de Nissen modificada videolaparoscópica corrigiu a doença do refluxo gastroesofagiano na maioria dos doentes acompanhados, associada à baixa morbimortalidade.BACKGROUND: Gastroesophageal reflux disease is highly common worldwide and surgical treatment is being indicated more frequently. Currently, laparoscopic is the access of choice and several antireflux techniques may be used

  13. Estudo da função simpático-adrenal em crianças submetidas a cirurgia cardíaca com hipotermia de superfície, perfusão limitada e parada circulatória Simpathoadrenal function during cardiac surgery in infants using the technique of surface cooling, limited cardiopulmonary bypass and circulatory arrest

    Directory of Open Access Journals (Sweden)

    Richard K Firmin

    1988-04-01

    Full Text Available Os níveis de catecolamina plasmática foram medidos em 20 crianças (idade média de 6,00 ± 5,86 meses; peso médio 5,3 ± 1,82 kg, durante a correção de defeitos cardíacos congênitos, usando-se a hipotermia de superfície (26ºC, perfusão cardiopulmonar limitada e parada circulatória (15ºC. Adrenalina e noradrenalina plasmática foram dosadas em amostras sangüíneas arteriais seriadas, usando-se a cromatografia. A hipotermia de superfície produziu um significante aumento de ambas as catecolaminas. Durante o resfriamento central, os níveis caíram devido à hemodiluição. Após o período de parada circulatória (23/64 minutos, média de 41,3, ocorreu um aumento das catecolaminas plasmáticas, que persistiu durante o reaquecimento. Após o reaquecimento, as catecolaminas plasmáticas permaneceram elevadas até o final do ato cirúrgico. Nossos resultados mostram que a técnica de hipotermia de superfície, perfusão cardiopulmonar limitada e parada circulatória, sob as nossas condições de anestesia, produziu significante aumento da concentração de adrenalina e noradrenalina plasmática, porém o significado biológico é, ainda, inseguro.Plasma catecholamine levels were measured in 20 infants (mean age 6.0 ± 5.86 months; mean weigh 5.3 ± 1.82 Kg, undergoing correction of congenital heart defects using surface cooling (26ºC, limited cardiopulmonary bypass and circulatory arrest (15ºC. Plasma adrenaline and noradrenaline were assayed in serial arterial blood samples using cromatography and electrochemical techniques. Surface cooling produced a significant rise in adrenaline and noradrenaline: the levels of both catecholamines fell, however, during core-cooling on cardiopulmonary bypass. Following the period of circulatory arrest (23/64 min, mean 41.3 min, there was a further increase in plasma catecholamines, which persisted during rewarming. Following rewarming, plasma catecholamines remained elevated untill the end of the

  14. da Zehirlenmeleri

    Directory of Open Access Journals (Sweden)

    Necati Akbulut

    2015-02-01

    Full Text Available Gıda Teknolojisinin gelişmesi ile, gıda maddesinin tüketici için daha alımlı olmasını sağlamak, kısa zamanda bozulmasını engellemek ve pazara yeni çeşitler sunmak için bazı kimyasal maddeler kullanılmaya başlanılmıştır. Bunun yanında tarımda kullanılan kimyasal maddeler artmış, ambalaj sanayi gelişmiş, bu dada maddelerine bulaşan maddelerin türlerini arttırmıştır. Ayrıca gıda maddelerine belirli amacı olmadan katılan maddelerde vardır. Diğer taraftan tüketiciyi aldatmak, hile yapmak, çok kar sağlamak veya kötü kaliteyi gizlemek amacı ile de kullanılan maddeler bulunmaktadır. İster teknik zorunluk, ister hile amacıyla olsun bu tür yabancı maddeler öncelikle insan sağlığını ilgilendirmektedir. Bazı maddelerin vücuda alınması sakıncasız olduğu halde, bazıları sakıncalıdır. Sakıncasız olanlarında belirli bir sınırın üzerinde uzun süre alınmaları zararlı olabilmektedir. Bu toplum sağlığı sorunu birçok ülkeyi gıda sanayiinde kullanılan kimyasal maddelerin hoşgörü sınırlarının hesaplanması noktasına götürmüştür.

  15. Industrial technique

    International Nuclear Information System (INIS)

    Robertson, D.H.

    1975-01-01

    Techniques for selectively extracting and storing only krypton and xenon in the waste gases that are released from a pressurized water nuclear power reactor are described. The illustrative fluorocarbon absorption system has three separation stages: an initial gas-fluorocarbon absorber, a flash chamber and fractionator for segregating all of the absorbed gases from the loaded absorber stage fluorocarbon (save for the krypton and xenon), and a stripper that receives the partially loaded fluorocarbon liquid directly from the fractionator in order to separate only the krypton and xenon. A molecular sieve filter dries the input process gas, a cartridge type solvent filter is used to remove radiation degradation products from the loaded liquid that flows from the absorber, a cold trap gas drier is provided to remove residual solvent vapor from the separated krypton and xenon, and radiation detectors automatically activate valves to establish safe conditions in the event of an accident or plant failure. (U.S.)

  16. Experimental techniques

    International Nuclear Information System (INIS)

    Roussel-Chomaz, P.

    2007-01-01

    This lecture presents the experimental techniques, developed in the last 10 or 15 years, in order to perform a new class of experiments with exotic nuclei, where the reactions induced by these nuclei allow to get information on their structure. A brief review of the secondary beams production methods will be given, with some examples of facilities in operation or under project. The important developments performed recently on cryogenic targets will be presented. The different detection systems will be reviewed, both the beam detectors before the targets, and the many kind of detectors necessary to detect all outgoing particles after the reaction: magnetic spectrometer for the heavy fragment, detection systems for the target recoil nucleus, γ detectors. Finally, several typical examples of experiments will be detailed, in order to illustrate the use of each detector either alone, or in coincidence with others. (author)

  17. Combinatorial techniques

    CERN Document Server

    Sane, Sharad S

    2013-01-01

    This is a basic text on combinatorics that deals with all the three aspects of the discipline: tricks, techniques and theory, and attempts to blend them. The book has several distinctive features. Probability and random variables with their interconnections to permutations are discussed. The theme of parity has been specially included and it covers applications ranging from solving the Nim game to the quadratic reciprocity law. Chapters related to geometry include triangulations and Sperner's theorem, classification of regular polytopes, tilings and an introduction to the Eulcidean Ramsey theory. Material on group actions covers Sylow theory, automorphism groups and a classification of finite subgroups of orthogonal groups. All chapters have a large number of exercises with varying degrees of difficulty, ranging from material suitable for Mathematical Olympiads to research.

  18. Fracionamento do alumínio por técnicas de dissoluções seletivas em espodossolos da planície costeira do Estado de São Paulo Fractionation of aluminum by selective dissolution techniques of soils on the São Paulo State sandy coastal plain

    Directory of Open Access Journals (Sweden)

    Maurício Rizzato Coelho

    2010-08-01

    Full Text Available Apesar das modernas e sofisticadas técnicas disponíveis, procedimentos de extração seletiva ainda são de considerável valor para a caracterização dos solos e para o entendimento dos processos pedogenéticos, sobretudo em ambientes e solos pouco estudados, como as restingas e os Espodossolos no Brasil. A aplicação dessas técnicas - a maioria rotineiramente utilizada para a caracterização de horizontes espódicos e Espodossolos - a um conjunto expressivo de horizontes e perfis em cronossequências é inédita para esses ambientes e possibilitou estabelecer comparações com aqueles intensivamente estudados sob clima temperado ou boreal. Apesar das reconhecidas limitações dos procedimentos analíticos de dissolução seletiva, os aqui utilizados foram relativamente efetivos, o que possiblitou discriminar horizontes, inferir componentes mineralógicos e discutir processos atuantes no conjunto de horizontes e de perfis analisados. Estes se situam nos municípios de Bertioga, Cananeia e Ilha Comprida (SP, onde foram descritos e amostrados 31 perfis representativos de solos sob vegetação de restinga. Entre os resultados encontrados, destacam-se: NaOH 0,5 mol L-1 em temperatura ambiente extraiu, em média, 22 a 30 % mais Al (Al n que os reagentes ditionito-citrato (Al d, oxalato (Al o e pirofosfato (Al p para todo o conjunto de amostras. Em alguns horizontes espódicos bem drenados (Bs, Bhs, Bh e Bsm, o pH e as interações entre as diferentes técnicas (Al n-Al o, Al o-Al p, Al p/Al o e Al p/Al d sugerem a formação e manutenção de compostos inorgânicos amorfos de Al em detrimento da total complexação do elemento à matéria orgânica iluviada. Esta última forma de Al predomina nos Espodossolos Hidromórficos.In spite of modern and sophisticated techniques, procedures of selective dissolution are still of considerable value for soil characterization and to the understanding of the pedogenetic process, especially environments and

  19. A REFORMA DA IGREJA

    Directory of Open Access Journals (Sweden)

    Vítor Galdino Feller

    2014-01-01

    Full Text Available O pontificado do papa Francisco trouxe à tona o tema da reforma da Igreja. Retoma-se essa causa que acompanha a história da Igreja desde os seus primórdios e que interessa a todos os membros do povo santo de Deus. O texto divide-se em quatro partes. Primeiro, faz-se um apanhado histórico dos anseios de reforma da Igreja, mostrando que, muitas vezes em instâncias subterrâneas, sempre houve o desejo e também ações concretas de renovação. Em seguida, apresenta-se como razão para a reforma da Igreja o anúncio e a realização do Reino de Deus, pelo qual é preciso que a Igreja se volte à concretude humana e histórica de Jesus de Nazaré, pela superação do apego ao poder e às estruturas religiosas. Num terceiro momento, trata-se do critério pelo qual se mede a realização e a veracidade da reforma da Igreja: a santidade de cada fiel e do povo cristão no meio do mundo. Por fim, conclui-se que o caminho para a reforma da Igreja está na escuta dos clamores do Espírito Santo, que fala na própria Igreja e no mundo através do sensus fidei dos fiéis, das Igrejas particulares, dos pobres, das mulheres e das realidades terrestres. ABSTRACT: The pontificate of Pope Francis brought to the surface the theme of reform of the Church. This essay takes up this cause that accompanies the history of the Church from its beginnings and concerns all the members of the holy people of God. The text is divided into four parts. First, it gives a historical summary of the yearnings for reform of the Church, showing that, in many instances subterranean, there has always been the desire and also the concrete actions of renewal. Following from this, the essay presents as the reason for the reform of the Church the proclamation and the realization of the Kingdom of God, whereby it is necessary that the Church return to the concrete human and historical Jesus of Nazareth, in order to overcome the addiction to power and to religious structures. In the

  20. A cultura da internet

    OpenAIRE

    Cádima, Francisco Rui

    2017-01-01

    O novo ambiente digital é cada vez mais perturbante na sua dimensão ‘visível’ e está, em boa parte, incontrolável nessa área ainda algo desconhecida da Internet negra, conhecida por deep web ou dark net, convoca-nos para uma reflexão profunda de largo espectro, que não se pode vincular apenas às questões de mercado, tecnológicas e de redes, mas que nos vem alertar sobretudo para a ordem do político e da cidadania, do ‘desconhecido’ e do conhecimento e, enfim, do acesso à rede, quer no que is...

  1. Chemical characterization of the gels produced by the diazotrophic bacteria Rhizobium tropici and Mesorhizobium sp; Caracterizacao quimica dos geis produzidos pelas bacterias diazotroficas Rhizobium tropici e Mesorhizobium sp.

    Energy Technology Data Exchange (ETDEWEB)

    Monteiro, Nilson Kobori [Departamento de Engenharia e Tecnologia de Alimentos, Instituto de Biociencias, Letras e Ciencias Exatas, Universidade Estadual Paulista, Sao Jose do Rio Preto - SP (Brazil); Aranda-Selverio, Gabriel; Exposti, Diego Tadeu Degli; Silva, Maria de Lourdes Corradi da [Departamento de Fisica, Quimica e Biologia, Faculdade de Ciencias e Tecnologia, Universidade Estadual Paulista, Presidente Prudente - SP (Brazil); Lemos, Eliana Gertrudes Macedo; Campanharo, Joao Carlos [Departamento de Tecnologia, Faculdade de Ciencias Agrarias e Veterinaria, Universidade Estadual Paulista, Jaboticabal - SP (Brazil); Silveira, Joana Lea Meira [Departamento de Bioquimica e Biologia Molecular, Universidade Federal do Parana, Curitiba - PR (Brazil)

    2012-07-01

    The exopolysaccharides with characteristics of gel produced by Rhizobium tropici (EPSRT) and Mesorhizobium sp (EPSMR) are acidic heteropolysaccharide composed mainly of glucose and galactose in a molar ratio of 4:1 and 5:1 respectively, with traces of mannose ({approx} 1%). Chemical analysis showed the presence of uronic acid, pyruvate and acetyl-substituents in the structures of both polymers. Experiments of gel permeation chromatography and polyacrylamide gel electrophoresis showed that EPSRT and EPSMR are homogeneous molecules with low grade of polydispersity. The EPS were characterized using spectroscopic techniques of FT-IR, {sup 1}H and {sup 13}C-NMR. (author)

  2. [da Vinci surgical system].

    Science.gov (United States)

    Watanabe, Gou; Ishikawa, Norihiro

    2014-07-01

    The da Vinci surgical system was developed by Intuitive Surgical Inc. in the United States as an endoscopic surgical device to assist remote control surgeries. In 1998, the Da Vinci system was first used for cardiothoracic procedures. Currently a combination of robot-assisted internal thoracic artery harvest together with coronary artery bypass grafting (CABG) through a mini-incision (ThoraCAB) or totally endoscopic procedures including anastomoses under robotic assistance (TECAB) are being conducted for the treatment of coronary artery diseases. With the recent advances in catheter interventions, hybrid procedures combining catheter intervention with ThoraCAB or TECAB are anticipated in the future.On the other hand, with the decrease in number of coronary artery bypass surgeries, the share of valvular surgeries is expected to increase in the future. Among them, mitral valvuloplasty for mitral regurgitation is anticipated to be conducted mainly by low-invasive procedures, represented by minimally invasive cardiac surgery( MICS) and robot-assisted surgery. Apart from the intrinsic good surgical view, robotic-assisted systems offer additional advantages of the availability of an amplified view and the easy to observe the mitral valve in the physiological position. Thus, robotic surgical surgeries that make complicated procedures easier are expected to accomplish further developments in the future. Furthermore, while the number of surgeries for atrial septal defects has decreased dramatically following the widespread use of Amplatzer septal occluder, robotic surgery may become a good indication for cases in which the Amplatzer device is not indicated. In Japan, clinical trial of the da Vinci robotic system for heart surgeries has been completed. Statutory approval of the da Vinci system for mitral regurgitation and atrial septal defects is anticipated in the next few years.

  3. A utilização da teoria da aprendizagem significativa no ensino da Enfermagem

    OpenAIRE

    Alana Tamar Oliveira de Sousa; Nilton Soares Formiga; Simone Helena dos Santos Oliveira; Marta Miriam Lopes Costa; Maria Júlia Guimarães Oliveira Soares

    2015-01-01

    RESUMO Objetivo: sintetizar a produção científica acerca da Teoria da Aprendizagem Significativa no processo de ensino-aprendizagem em Enfermagem. Método: revisão integrativa realizada nas bases de dados MEDLINE, LILACS, SciELO, BDENF e CINAHL, com artigos que abordaram a temática ou aspectos da teoria da aprendizagem significativa de David Ausubel. Fizeram parte da amostra dez artigos, sendo seis escritos no idioma português e quatro no inglês, publicados de 1998 a 2013. Resultados: cinco...

  4. Os (descaminhos da identidade

    Directory of Open Access Journals (Sweden)

    Oliveira Roberto Cardoso de

    2000-01-01

    Full Text Available A conferência procurou apresentar uma interpretação das vicissitudes da identidade étnica e/ou nacional quando observada em situações de ambigüidade. É quando o processo identitário expressa crises reais ou virtuais, como as que têm lugar entre imigrantes latino-americanos nos Estados Unidos, entre povos de diferentes regiões da Espanha emigrados para Barcelona, entre catalães espanhóis, franceses e andorranos residentes em Andorra, e entre povos indígenas em regiões de fronteira do Brasil com países vizinhos. O exame do processo identitário que tem lugar em diferentes latitudes, nas Américas e na Europa, sugere que os fenômenos socioculturais de etnicidade e de nacionalidade possuem em comum características tais como a busca de reconhecimento da pessoa moral, o respeito à diferença e, como corolário ético, a elevação do que se pode definir como "taxa de consideração".

  5. Hepatotoxicidade da cianotoxina microcistina

    Directory of Open Access Journals (Sweden)

    Andréa de Castro Leal

    2004-01-01

    Full Text Available Constitui interesse emergente em saúde pública avaliar a possibilidade de intoxicação humana por biotoxinas de algas cianofíceas, principalmente as hepatotoxinas do grupo das microcistinas. A microcistina, um heptapeptídeo monocíclico, é produzida principalmente pela cianobactéria Microcistis aeruginosa. São caracterizadas por alguns aminoácidos variáveis, dois deles com uma estrutura não usual que possuem importante papel na hepatotoxidade da microcistina. Apesar do acometimento humano atribuído as microcistinas incluírem gastroenterite, reações alérgicas ou irritativas, neurotoxicidade, o principal alvo da toxina é o fígado. Nos hepatócitos as microcistinas são carreadas pelo sistema transportador do ácido biliar, inibindo a atividade da proteína fosfatase no citoplasma. A inibição leva a mudanças morfológicas na membrana plasmática pela hiperfosforilação de citoqueratinas, e à atividade de promoção tumoral pelas proteínas hiperfosforiladas. Os métodos de detecção e quantificação de microcistinas no ambiente incluem a cromatografia líquida, o bioensaio em camundongos e os testes imunoenzimáticos. O último vem ganhando destaque pela praticidade e alta sensibilidade.

  6. Pesquisa da prevalência do papilomavírus humano em amostras de tecido endometrial normal e com carcinoma pela técnica de PCR Search for human papillomavirus in samples of normal endometrial tissue and tissue with carcinoma by the PCR technique

    Directory of Open Access Journals (Sweden)

    Edison Natal Fedrizzi

    2004-05-01

    Full Text Available OBJETIVO: comparar a prevalência da presença do DNA do papilomavírus humano (HPV pela técnica de PCR em amostras de tecido endometrial normal e com carcinoma endometrial de mulheres submetidas a tratamento cirúrgico (histerectomia ou carcinoma endometrial e doença benigna. MÉTODOS: trata-se de um estudo observacional do tipo caso-controle onde foram avaliadas 100 mulheres (50 com endométrio normal e 50 com carcinoma endometrial quanto a presença do DNA do HPV em amostra tecidual conservada em blocos de parafina, pelo método de PCR. Foram excluídos os casos de carcinoma endometrial cujo sítio primário da lesão era duvidoso ou com história prévia ou atual de lesões pré-neoplásicas ou carcinoma do trato genital inferior. Variáveis como idade, tabagismo, trofismo endometrial, diferenciação escamosa e grau de diferenciação tumoral foram também avaliadas. RESULTADOS: o risco relativo estimado da presença do HPV foi o mesmo nas mulheres com e sem carcinoma endometrial. O HPV foi detectado em 8% dos casos de carcinoma e 10% no endométrio normal. Apesar de o HPV ter sido detectado 3,5 vezes mais em mulheres fumantes no grupo sem carcinoma, não houve diferença estatística. A presença do HPV também não esteve correlacionada com a idade das mulheres, trofismo endometrial, diferenciação escamosa e grau de diferenciação tumoral. Os HPV 16 e 18 (5 dos casos com o tipo 16 e 4 com o tipo 18 foram os vírus mais freqüentemente encontrados, tanto no tecido endometrial normal, quanto no carcinomatoso. Nenhum vírus de baixo risco oncogênico foi detectado nas amostras. CONCLUSÃO: o HPV está presente no tecido endometrial de mulheres com carcinoma endometrial na mesma proporção que nas com tecido endometrial normal, não se demonstrando a possível associação deste vírus no desenvolvimento do carcinoma endometrial.OBJECTIVE: to compare the prevalence of DNA of human papillomavirus (HPV, in samples of normal endometrial

  7. Multi-wire detector characterization for daily quality control on IMRT; Caracterizacao de um detector planar de multiplos fios para controle de qualidade diario de tratamentos com IMRT

    Energy Technology Data Exchange (ETDEWEB)

    Ferrari, Vilma A.; Watanabe, Erika Y.; Santos, Gabriela R.; Menegussi, Gisela, E-mail: vilmaferrari@uol.com.br [Instituto do Cancer do Estado de Sao Paulo (ICESP), SP (Brazil). Setor de Radioterapia

    2012-08-15

    Several dosimetry devices are being developed for quality control of radiation treatments using modern techniques as, for example, the Intensity Modulated Radiation Therapy (IMRT). The main function of these devices are to daily quality control of treatments of patients submitted to IMRT technique. The aim of this study is to characterize a type of planar multi-wire detector - DAVID (PTW) - for use in clinical practice. It was evaluated the influence of the system in the radiation beam by measuring the absorption factors and surface dose. We also analyzed the dose-linearity, reproducibility, the dependence with the dose rate and the angle of the linac head. Small errors in the position of the multi-leaf were inserted to evaluate the sensitivity of the system. The results showed that the detector can absorb up to 6.7% of the dose, depending of the energy beam and the field size. A significant increase in surface dose was observed, indicating that individual analysis is necessary for each patient. The system showed good reproducibility, linear response with dose, low dependence with dose rate and low dependence with the angle of the linac head. When small errors were inserted in the position of the multi-leaf, the system was able to detect them. Thus, the detector DAVID proved to be suitable for daily verification of IMRT treatments. (author)

  8. Industrial technique

    International Nuclear Information System (INIS)

    Jabsen, F.S.

    1975-01-01

    An illustrative embodiment of the invention discloses a technique for disassembling a nuclear reactor fuel element without destroying the individual fuel pins and other structural components from which the element is assembled. A traveling bridge and trolley that span a water-filled spent fuel storage pool support a strongback. The strongback is under water and provides a working surface on which the spent fuel element is placed for inspection and for the manipulation that is associated with disassembly and assembly. To remove, in a non-destructive manner, the grids that hold the fuel pins in the proper relative positions within the element, bars are inserted through apertures in the grids with the aid of special tools. These bars are rotated to flex the adjacent grid walls and, in this way relax the physical engagement between protruding portions of the grid walls and the associated fuel pins. With the grid structure so flexed to relax the physical grip on the individual fuel pins, these pins can be withdrawn for inspection or replacement as necessary without imposing a need to destroy fuel element components. (U.S.)

  9. Técnicas de mineração de dados para análise da precipitação pluvial decenal no Rio Grande do Sul Data mining techniques for decennial analysis of rainfall in Rio Grande do Sul

    Directory of Open Access Journals (Sweden)

    Raquel S Boschi

    2011-12-01

    Full Text Available O objetivo deste trabalho foi analisar o comportamento espaçotemporal da precipitação pluvial no Estado do Rio Grande do Sul, entre os decênios de 1987-1996 e 1997-2006, por meio de técnicas de mineração de dados. As séries históricas foram adquiridas no sistema de informações hidrológicas Hidroweb. A metodologia utilizada teve como base o modelo CRISP-DM (Cross Industry Standard Process for Data Mining. Foram definidas áreas pluviometricamente homogêneas para os decênios de 1987-1996 e 1997-2006. Em seguida, pela sobreposição dos agrupamentos obtidos para os dois períodos, encontraram-se seis zonas comuns aos dois decênios (A a F. As alterações ocorridas foram avaliadas nas seguintes escalas temporais: anual, sazonal e mensalmente. Os resultados indicaram incrementos significativos (20 a 240 mm na precipitação anual em todas as zonas, exceto na zona A. Na análise sazonal, as variações foram aleatórias, sendo que, na primavera, todas as zonas apresentaram incremento significativo (44 a 142 mm. Na análise mensal, destaca-se a redução ocorrida no mês de janeiro em todas as zonas, exceto na E. Nos demais meses, as variações foram aleatórias. Os resultados mostram que, entre os decênios, houve uma alteração no volume da precipitação pluvial em todas as escalas temporais analisadas.The objective of this study was to analyze the spatio-temporal rainfall in Rio Grande do Sul, between 1987-1996 and 1997-2006 decades by using techniques of data mining. The historical series were acquired from the hydrological information Hidroweb system. The methodology used was based on the CRISP-DM (Cross Industry Standard Process for Data Mining model. First, homogeneous precipitation areas for the 1987-1996 and 1997-2006 decades were defined. Subsequently, by the overlapping of the clusters obtained from both periods, six common areas were defined ranging from A to F. The changes in the volume of precipitation were evaluated

  10. Digestibilidade Ileal de aminoácidos de alguns alimentos, determinada pela técnica da cânula T simples com suínos Ileal digestibilities of amino acids in of some feedstuffs determined by simple canula T technique with swines

    Directory of Open Access Journals (Sweden)

    Lourdes Romão Apolônio

    2003-06-01

    Full Text Available Objetivou-se com este trabalho determinar os coeficientes de digestibilidade ileal aparente e verdadeira e de aminoácidos, utilizando-se a técnica da cânula T simples, com suínos. Foram utilizados oito suínos canulados, machos, castrados (Landrace x Large White. Os alimentos analisados foram: quirera de arroz, sorgo baixo tanino, farelo de trigo, milheto, leveduras de cana e de cerveja. As dietas contendo a quirera de arroz, sorgo, farelo de trigo e milheto como fonte de proteína foram formuladas para fornecer 7% de proteína bruta e as demais dietas contendo as leveduras de cana e de cerveja foram formuladas para fornecer 13% de proteína bruta. Foi adicionado 0,5% de óxido crômico nas dietas experimentais, como marcador de digestibilidade. A coleta da digesta foi feita após período de adaptação de cinco dias para determinação do consumo de ração, três dias para regularização do fluxo intestinal, num período de 24 horas, feitas a intervalos de 3 horas, começando logo após a alimentação. As amostras foram obtidas de digestas coletadas de grupos de dois animais. Entre os alimentos avaliados, a quirera de arroz, sorgo e milheto apresentaram os maiores coeficientes de digestibilidade verdadeira, enquanto os menores valores foram obtidos para o farelo de trigo. A treonina foi o aminoácido essencial de menor digestibilidade verdadeira na quirera de arroz, farelo de trigo e nas leveduras de cerveja e cana. A lisina foi o aminoácido menos digestível no sorgo e no milheto.The objective of this work was evaluate the apparent and true ileal digestibility of aminoacids feedstuffs, using the technique of simple canula T, with swines. Were used eight barrows canulated (Landrace x Large White. The feedstuffs evaluated were rice broked, low tanine sorghum, wheat bran, millet, brewer yeast and sugar cane yeast. The diets with rice broked, sorghum, wheat bran, millet as protein source were formulated to provide 7% of crude protein and

  11. Processing and characterisation of magnesia composites with graffiti and alumina addition; Processamento e caracterizacao de compositos magnesianos com adicao de grafite e alumina

    Energy Technology Data Exchange (ETDEWEB)

    Carregosa, J.D.C.; Diniz, W.A.; Oliveira, R.M.P.B., E-mail: jdcovello@hotmail.com [Universidade Federal de Sergipe (UFS), Sao Cristovao, SE (Brazil)

    2016-07-01

    The use of refractory materials is of great importance for industries that use high temperature kilns, most of the internal components of the ovens do not support high temperatures and refractory blocks have the function to support, physically and chemically, direct contact with molten materials and also function as a thermal insulator. In this work were prepared 5 different formulations of Aluminum Magnesium Oxide refractory with added graphite. In a first step the characterization of the raw materials through the techniques of Particle Size analysis, X - ray fluorescence and X - ray diffraction, was also developed a method for formulating a binding system. Then the specimens were sintered at 1250 °C in stagnant atmosphere. The proposed refractories were assessed by determining the compressive strength, microstructural characterization by X - ray diffraction and Scanning Electron Microscopy. (author)

  12. Planning of experimental removal of cadmium in finite bath system using the chocolate clay B as adsorbent; Caracterizacao de adsorvente (argila chocolate B) visando a remocao de cadmio

    Energy Technology Data Exchange (ETDEWEB)

    Mota, J.D.; Rodrigues, M.G.F.; Lima, W.S.; Souza, R.S., E-mail: wsl_20@yahoo.com.br, E-mail: meiry@deq.ufcg.edu.br [Universidade Federal de Campina Grande (LABNOV/UFCG), PB (Brazil). Unidade Academica de Engenharia Quimica. Lab. de Desenvolvimento de Novos Materiais

    2012-07-01

    The smectite clays are characterized by having a high cation exchange capacity and ability to remove metal ions. They have great industrial importance, for its abundance and low cost. The first part of this work was to characterize the clay called Chocolate B through the techniques of X-Ray Diffraction, X-Ray Spectroscopy and Energy Dispersive Physical Adsorption of Nitrogen. The second part of the work aims to evaluate the significance of the variables: pH and initial concentration on removal of cadmium in a batch system. In the experimental design used was a 2{sup 2} factorial analysis with the addition at the central point, and evaluated the percentage of removal (Rem%) and removal capacity (EQF). XRD results corroborating the chemical analysis (EDX), characterized as a B Chocolate smectite clays. Statistical analysis showed a strong influence of variable pH on the removal of cadmium. (author)

  13. Application of artificial neural networks on the characterization of radioactive waste drums; Aplicacao de redes neurais artificiais na caracterizacao de tambores de rejeito radioativo

    Energy Technology Data Exchange (ETDEWEB)

    Potiens Junior, Ademar Jose; Hiromoto, Goro, E-mail: apotiens@ipen.b, E-mail: hiromoto@ipen.b [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2011-10-26

    The methodology consist of system simulation of drum-detector by Monte Carlo for obtention of counting efficiency. The obtained data were treated and a neural artificial network (RNA) were constructed for evaluation of total activity of drum. For method evaluation measurements were performed in ten position parallel to the drum axis and the results submitted to the RNA. The developed methodology showed to be effective for isotopic characterization of gamma emitter radioactive wastes distributed in a heterogeneous way in a 200 litters drum. The objective of this work as to develop a methodology of analyse for quantification and localization of radionuclides not homogeneous distributed in a 200 liters drum based on the mathematical techniques

  14. Techniques de combustion Combustin Techniques

    Directory of Open Access Journals (Sweden)

    Perthuis E.

    2006-11-01

    Full Text Available L'efficacité d'un processus de chauffage par flamme est étroitement liée à la maîtrise des techniques de combustion. Le brûleur, organe essentiel de l'équipement de chauffe, doit d'une part assurer une combustion complète pour utiliser au mieux l'énergie potentielle du combustible et, d'autre part, provoquer dans le foyer les conditions aérodynamiques les plus propices oux transferts de chaleur. En s'appuyant sur les études expérimentales effectuées à la Fondation de Recherches Internationales sur les Flammes (FRIF, au Groupe d'Étude des Flammes de Gaz Naturel (GEFGN et à l'Institut Français du Pétrole (IFP et sur des réalisations industrielles, on présente les propriétés essentielles des flammes de diffusion aux combustibles liquides et gazeux obtenues avec ou sans mise en rotation des fluides, et leurs répercussions sur les transferts thermiques. La recherche des températures de combustion élevées conduit à envisager la marche à excès d'air réduit, le réchauffage de l'air ou son enrichissement à l'oxygène. Par quelques exemples, on évoque l'influence de ces paramètres d'exploitation sur l'économie possible en combustible. The efficiency of a flame heating process is closely linked ta the mastery of, combustion techniques. The burner, an essential element in any heating equipment, must provide complete combustion sa as to make optimum use of the potential energy in the fuel while, at the same time, creating the most suitable conditions for heat transfers in the combustion chamber. On the basis of experimental research performed by FRIF, GEFGN and IFP and of industrial achievements, this article describesthe essential properties of diffusion flames fed by liquid and gaseous fuels and produced with or without fluid swirling, and the effects of such flames on heat transfers. The search for high combustion temperatures means that consideration must be given to operating with reduced excess air, heating the air or

  15. Aplicação da ferramenta SWOT para avaliação das técnicas de dano ao choque térmico em materiais refratários SWOT as a tool to evaluate the thermal shock damage technique of refractory materials

    Directory of Open Access Journals (Sweden)

    L. R. G. Gonçalves

    2010-12-01

    Full Text Available A literatura indica diversos tipos de ensaios e diferentes métodos de avaliação de dano por choque térmico. Adicionalmente sabe-se que, em determinadas aplicações, esse tipo de dano é um dos principais responsáveis pela degradação do revestimento refratário. Neste contexto e buscando a melhor forma de reproduzir as condições em serviço do revestimento refratário, o presente trabalho foi realizado visando analisar qual tipo de ensaio de choque térmico e método de avaliação do dano são os mais adequados para avaliar o desempenho destes materiais. Essa análise foi baseada em uma revisão bibliográfica e resultados obtidos em laboratório, em que se comparou e avaliou as vantagens e desvantagens dos métodos mais relevantes encontrados na literatura. Por fim, com o auxilio da ferramenta SWOT foi possível verificar se o método adotado pelos autores desse trabalho é adequado para auxiliar na seleção do refratário para aplicação em calcinadores de leito fluidizado.The literature shows different tests and techniques for evaluating the thermal shock damage. Additionally, it is known that, for certain applications, this type of wear mechanism is one of the main causes of fluid flash calciner refractory degradation. Within this context and in order to find the best way to reproduce the refractory lining service conditions, this work was carried out to point out which thermal shock test and damage assessment method are more suitable to evaluate these materials. This analysis was based on a literature review and laboratory experiments, comparing and evaluating the advantages and disadvantages of the most important methods available. Finally, with the support of the SWOT tool it was possible to evaluate whether the method adopted by the authors of this work is appropriated for helping the selection of the refractories for calciners application.

  16. Characterization of silicates and calcium carbonates applied to high-dose dosimetry; Caracterizacao de silicatos e carbonatos de calcio aplicados a dosimetria de doses altas

    Energy Technology Data Exchange (ETDEWEB)

    Vila, Gustavo Barreto

    2012-07-01

    The predominant isomorphous form in the biominerals studied in this work (oyster shell, coral, mother of pearl and shell) was aragonite. The appearance of the calcite phase occurred at 500 deg C at a heating rate of 10 deg {sup C}/s for all samples except for the coral sample, which was 400 deg C, independent of the heating rate. The most abundant element in the biominerals samples was Ca in the CaO form, and in the silicates (tremolite, diopside and rhodonite) Si in the SiO form. The most common trace element observed in the biominerals samples was Fe. The analyses of electron paramagnetic resonance showed lines of Mn{sup 2+} in the coral and mother-of-pearl samples before irradiation. In the case of the irradiated samples, the defects found were CO{sub 2}{sup -}, CO{sub 3}{sup 3-}, CO{sub 3}{sup -} and SO{sub 2}{sup -}, in the g range between 2.0010 and 2.0062. In the analyses by optical absorption of biominerals, transitions due to the presence of Mn in the samples were found. A thermoluminescent (TL) peak at approximately 140 deg C was found for the biominerals and at 180 deg C for silicates, which intensity depends directly on the dose. For samples exposed to different types of radiation, the TL peak occurred at lower temperatures. From the dose-response curves obtained for these materials, it was possible to determine a linear range for which their application in high dose dosimetry becomes possible. Taking into account the radiation type, among biominerals and silicates, the lowest detectable dose (40mGy) to gamma radiation was achieved for oyster shell samples using the measuring technique of optically stimulated luminescence (OSL). Using beta radiation, for diopside and tremolite samples the lowest detectable dose of 60mGy was obtained. For all samples, using the TL, OSL and thermally stimulated exoelectron emission (TSEE) techniques in alpha, beta and gamma radiation beans a good response reproducibility was obtained. Therefore, the samples characterized

  17. Spectroscopic and thermal characterization of bovine enamel and dentine using the photoacoustic effect; Caracterizacao espectroscopica e termica de esmalte e dentina bovinos utilizando o efeito fotoacustico

    Energy Technology Data Exchange (ETDEWEB)

    Stolf, Sandro Fernando

    2003-07-01

    The optical and thermal properties of dental tissues determine the nature and extent of the tissue response through the processes of absorption, transmission, reflection and scattering of the laser light and the heat produced by the absorption of that light. The spectroscopic characterization of bovine dentine and enamel, and the determination of the thermal diffusivity were the aim of this study. The photoacoustic spectra from these tissues were obtained in the Near-Infrared range 900 - 2500 nm, which is the clinical range for odontological application of most lasers. Photoacoustic spectra were taken from block, slices and powder of enamel and dentine. Also photoacoustic spectra were registered before and after 2, 5 and 10 h of topical fluoride (2.26%) application. Using the same technique spectra were taken from dentine and enamel after irradiation with Nd:YAG, Er:YAG, Ho:YLF and CO{sub 2}. It is evident from the results that the presence of O-H in the composition of hydroxyapatite and the water present in the teeth tissue make the obtention of spectrum from components other than O-H bond a very difficult task. In this way, only bands assigned to overtones and combinations of O-H stretch were observed. The thermal diffusivity of the bovine dentine was also measured using the photoacoustic technique. The thermal diffusivity is the physical quantity which measures the rate of heat diffusion throughout the sample. For higher values of the thermal diffusivity the heat diffusion and temperature rise will be faster. As there is many studies devoted to the processes of heat transfer throughout dental tissues using bovine teeth, it is important the determination of its thermal diffusivity. The measured value was found to be a = 2.0 ({+-}0.1).1O{sup -3} cm{sup 2}/s for the both direction, perpendicular and parallel to the dentinal tubules. These {sup a}lues indicate that there is no difference between the thermal diffusivities for the both directions. (author)

  18. Characterization of chemical compounds for dosimetry of the radiation in industrial processes; Caracterizacao de compostos quimicos para dosimetria das radiacaoes em processos industriais

    Energy Technology Data Exchange (ETDEWEB)

    Galante, Ana Maria Sisti

    1999-07-01

    Different chemical compounds have been studied to optimize dosimetric systems in irradiation processes. In this study 2,3,5 Triphenyl -2H- Tetrazolium Chloride, Brilliant Cresyl Blue, Bromocresol Green and Potassium Nitrate were investigated for their merits or faults, for {sup 60} Co gamma field, in order to verify if can be considered as dosimeters. Fricke solution was used as reference dosimeter to determine absorption dose rates at the gamma facilities.Only Bromocresol Green and Potassium Nitrate are recommended for dosimetry purposes since the main characteristics were achieved. The other two compounds could be used in dosimetry with changes in their formulation. Bromocresol Green and potassium Nitrate are reproducible and radiation sensitive for absorbed doses from 300 Gy to 150 kGy Bromocresol Green was used in liquid form and Potassium Nitrate was prepared in solid pellets form. Spectrophotometry in the visible region was used as the main detection technique, which allows relating optical absorption, before and after irradiation, with the absorbed dose. The maximum absorption wavelength for each compound was observed at 450-460nm for bromocresol Green and 546nm for Potassium Nitrate. Dose calibration curves are linear for both compounds in all dose intervals. When irradiated with accelerated electrons, with energies between o,9 MeV and 1,5MeV, optical absorption intensification, of about 2,6 times, was observed when comparing results for Potassium Nitrate, with those for gamma rays. All the evaluations are presented in this work. (author)

  19. Development and characterization of poli composites (ether ether ketone)(PEEK)(Hydroxyapatite(HA); Desenvolvimento e caracterizacao de compositos poli (eter-eter-cetona)(PEEK)/Hidroxiapatita(HA)

    Energy Technology Data Exchange (ETDEWEB)

    Ferreira, V.P.; Santos, F.S.F.; Sa, M.D. de; Fook, M.V.L., E-mail: valeriap.ferreira@hotmail.com [Universidade Federal de Campina Grande (UFCG), PB (Brazil). Centro de Ciencias e Tecnologia. Programa de Pos-Graduacao em Ciencia e Engenharia de Materiais

    2016-07-01

    The objective of this work was to develop PEEK / HA composites, combining the biological activity of the ceramic phase with the properties of the polymer phase, the materials used in this research were Poly (ether-ether-ketone) (PEEK) and Hydroxyapatite (HA) (50, 60, 70 and 80% m / v HA), this material was subjected to a load of two tons followed by a thermal treatment at 390 ° for a period of 30 minutes. Then they were characterized by FTIR, DRX and MO. In the physical-chemical characterization of FTIR and XRD, it was not possible to identify significant alterations. In the FTIR spectra of the composites, there is no formation of new identifiable chemical bonds. In the composites XRD diffractograms a profile similar to the ceramic phase was observed, with peaks increasing in intensity and narrowing proportional to the increase of the hydroxyapatite concentration in the composites. In optical microscopy it is possible to observe surfaces with heterogeneous morphology, with signs of roughness and in the cross section we observe a heterogeneous aspect, rich in regions with large agglomerates and lighter particles. Considering the processing aspects, the technique proved to be effective for the development of PEEK /HA composites. (author)

  20. Hepatotoxicidade da cianotoxina microcistina

    OpenAIRE

    Leal,Andréa de Castro; Soares,Manoel do Carmo Pereira

    2004-01-01

    Constitui interesse emergente em saúde pública avaliar a possibilidade de intoxicação humana por biotoxinas de algas cianofíceas, principalmente as hepatotoxinas do grupo das microcistinas. A microcistina, um heptapeptídeo monocíclico, é produzida principalmente pela cianobactéria Microcistis aeruginosa. São caracterizadas por alguns aminoácidos variáveis, dois deles com uma estrutura não usual que possuem importante papel na hepatotoxidade da microcistina. Apesar do acometimento humano atrib...

  1. Aspectos moleculares da anemia falciforme

    Directory of Open Access Journals (Sweden)

    Galiza Neto Gentil Claudino de

    2003-01-01

    Full Text Available No presente artigo abordaram-se vários aspectos relacionados à natureza molecular da anemia falciforme, desordem hematológica de caráter hereditário que acomete expressivo número de indivíduos em várias regiões do mundo. As pesquisas realizadas em torno desta patologia da hemácia, ao longo de quase um século, a partir de 1910, cooperaram para a criação de um novo e importante segmento da ciência, denominado biologia molecular. A descoberta dos polimorfismos da mutação (GAT->GTG no gene que codifica a cadeia beta da hemoglobina, originando diferentes haplótipos da doença, permitiu um melhor e mais amplo conhecimento em torno da heterogeneidade clínica nos pacientes falcêmicos. Analisando a hemoglobina na sua estrutura normal e mutante, sua produção e evolução, pode-se ter um entendimento mais completo da fisiopatologia desta doença e da sua complexidade clínica.

  2. Synthesis of zeolites from boiler fly ash: physical, chemical and mineralogical characterization; Sintese de zeolitas a partir de cinza volante de caldeiras: caracterizacao fisica, quimica e mineralogica

    Energy Technology Data Exchange (ETDEWEB)

    Rocha Junior, C.A.F.; Santos, S.C.A.; Souza, C.A.G., E-mail: augustorocha2@gmail.com [Programa de Pos Graduacao em Engenharia Quimica (PPEQ-UFPA), Belem, PA (Brazil); Angelica, R.S.; Neves, R.F. [Programa de Pos-Graduacao em Geologia e Geoquimica, Instituto de Geociencias (PPGG-IG-UFPA), Ananindeua, PA (Brazil)

    2012-01-15

    Along the years, worldwide industrial development has causing a growing generation of residues, bringing potentials environmental problems. A study of the characteristics of these wastes, as well as the development of techniques for their use in new processes becomes indispensable for the environment preservation. The main purpose of this work is to evaluate the possible use of two important industrial residues from the Amazon region for zeolite synthesis: (a) the fly ash (particle size < 100 {mu}m) that comes from burning of mineral coal in boiler; and (b) the micro silica, a by-product of the reaction between quartz and coal in the production of metallic silicon and alloys iron-silicon.The following chemical, physical and mineralogical characterization methods were carried out: X-ray diffractometry, X-ray fluorescence, scanning electron microscopy, granulometric analysis, differential thermal and thermogravimetric analysis (DTA-TG). The analyses were carried out at the following conditions: 60, 100, 150 and 190 deg C, Na{sub 2}O/Al{sub 2}O{sub 3} molar ratio of 5 and Si/Al molar ratio ranging from 2.12 to 15, and reaction time of 24 h. The results of the fly characterization demonstrate its enormous potential as raw material for the zeolite synthesis. SiO{sub 2} and Al{sub 2}O{sub 3} represent more than 50% of its composition, mineralogical phases defined, low humidity content, low particle size (d{sub 90} < 10 {mu}m), among others. Mineralogical analyses of the synthesized products showed the formation of some zeolite types, as follow: analcime, phillipsite, sodalite, zeolite P and tobermorite. The results show that the mixture fly ash-micro silica in these reaction conditions point to a promising material for zeolite synthesis (author)

  3. Contribuição ao estudo da microinfiltração in vitro de lesões cervicais não cariosas restauradas com diferentes materiais adesivos e técnicas In vitro evaluation of microleakage of noncarious cervical lesions restored with different adhesive materials and techniques

    Directory of Open Access Journals (Sweden)

    Adriana Bona MATOS

    1997-01-01

    Full Text Available A restauração de lesões cervicais não cariosas é um procedimento comum na clínica diária, havendo uma alta incidência de casos de perda da restauração, descoloração marginal e recidiva de cárie. A etiologia desse tipo de lesão é considerada multifatorial. Neste trabalho, avaliou-se a microinfiltração diante das seguintes variáveis: tipo de material utilizado (dois adesivos de quarta geração utilizados em conjunto com duas resinas compostas de tipos diferentes, ©microfillª e híbrida, dois métodos de polimerização dos sistemas adesivos (foto e dual e duas técnicas restauradoras (incremental e do incremento único. Na metodologia deste trabalho, utilizaram-se ciclagem térmica e mecânica, técnica de infiltração com nitrato de prata, cortes seriados e leitura dos resultados através de escala de escores. A microinfiltração foi menor quando se utilizou uma resina composta híbrida comparada à resina ©microfillª. Ao se utilizar o método de polimerização dual do sistema adesivo, a microinfiltração foi menor do que com o método somente fotopolimerizável. A técnica restauradora não exerceu influência sobre o padrão de microinfiltração encontrado nas restaurações de lesões cervicais não cariosasRestoration of noncarious cervical lesions is a usual clinical procedure, and there is a high incidence of restoration loss, marginal discoloration, and recurrent caries. All the factors that play an important role in this process have to be considered when studying this kind of lesion of complex multifactorial etiology. Microleakage was evaluated related to the type of material used (two fourth generation bonding systems used with two types of composite resins: hybrid and microfill, two polymerization methods for bonding systems (photo and dual cure and two restorative techniques (incremental and bulk. This study used thermal and mechanical cycling procedures, infiltration tests with silver nitrate solution

  4. REFLETINDO SOBRE AS ESPECIFICIDADES DA GEOGRAFIA NA CRISE DA MODERNIDADE

    Directory of Open Access Journals (Sweden)

    Patrício A. S. Carneiro Carneiro

    2010-08-01

    Full Text Available O presente artigo discute a evolução da ciência moderna, bem como a crise desse paradigma dominante e seus efeitos sobre a geografia. Destaca ainda a necessidade da construção de um novo pensamento científico para além das fronteiras disciplinares e do método absoluto.

  5. A dignidade da pessoa humana na doutrina social da igreja

    Directory of Open Access Journals (Sweden)

    Manzone, Gianni

    2010-01-01

    Full Text Available O texto faz uma análise panorâmica sobre a compreensão da dignidade humana nos diversos textos da Doutrina Social da Igreja, mostrando o entendimento da mesma nos diversos documentos dos Papas, notadamente Leão XII, Pio XI, Pio XII e João Paulo II, além de apontar aspectos históricos e culturais que influenciaram cada pronunciamento, o que foi determinante para a evolução do pensamento do Magistério na questão social. O ponto de partida é a visão antropológica da Doutrina Social da Igreja, resumida em termos de “homem criado por Deus a sua imagem e resgatado pelo sangue de Jesus Cristo” (Sollicitudo Rei Socialis 29. A partir daí, há a defesa do primado do ser humano sobre o social e reivindicações totalitaristas que perpassaram a história recente da humanidade, embora a pessoa seja sempre um ser-em-relação e situado em uma sociedade determinada

  6. Os usos da diversidade

    Directory of Open Access Journals (Sweden)

    Clifford Geertz

    1999-05-01

    Full Text Available Resumo Ao discorrer sobre o “Futuro do Etnocentrismo”, este artigo parte da premissa de que a globalização, apesar de ter – em muitos casos – diminuído as diferenças entre povos, não tem amenizado os preconceitos e as formas de discriminação que ocorrem em nome dessas diferenças. Ele resgata a importância do antropólogo neste cenário lembrando que a diversidade cultural faz parte da sociedade complexa, remetendo-se não apenas a grupos étnicos ou nacionais bem delimitados, mas também a diferenças de geração, gênero, sexo e classe, entre outros. Neste contexto, a tolerância passiva de modos distantes de vida assim como a aceitação pragmática de nosso próprio paroquialismo são atitudes não somente intelectualmente desonestas mas também moralmente repreensíveis. É no encontro incômodo de subjetividades variantes na sua própria sociedade que o antropólogo define seu lugar.

  7. Progresso Interdisciplinar da Medicina

    Directory of Open Access Journals (Sweden)

    Jorge Correia-Pinto

    2018-02-01

    Full Text Available Portugal é muitas vezes citado como um bom exemplo na prestação de cuidados de saúde. Para tal concorreram a investigação (engenharia biomédica, a evolução técnica e a diferenciação clínica de diferentes especialidades. Para que esta evolução se transfira para o paciente com o seu máximo potencial, o diálogo e a interdisciplinaridade são imprescindíveis. Nesta Edição da Gazeta Médica, vários artigos trazem até ao leitor alguns exemplos desta evolução e interdisciplinaridade, que continua todos os dias nos nossos hospitais. Assim não podemos deixar de salientar o enorme progresso que houve no desenvolvimento de antimicrobianos e logicamente, o desafio que agora enfrentamos, o da resistência aos antibióticos. Por outro lado, a biologia molecular ao permitir-nos conhecer melhor a origem e fisiopatologia de inúmeras doenças, abriu um janela de oportunidade para individualizar o algoritmo clínico de orientação e tratamento clínicos. É com naturalidade, portanto, que a seguir encontramos vários artigos que relatam estratégias de individualização terapêutica, aumentando o efeito terapêutico, e minimizando os efeitos laterais. Sendo o relator deste editorial, um cirurgião, não posso deixar de dar enfoque à forma como a cirurgia minimamente invasiva tem revolucionado a intervenção cirúrgica. A história reporta-nos que foram os urologistas e os ginecologistas os pioneiros em muitos dos passos determinantes para chegarmos à cirurgia laparoscópica. Aqueles e os cirurgiões digestivos documentaram clinicamente que o desenvolvimento da cirurgia minimamente invasiva trouxe consigo várias vantagens que, resumidamente, resultam numa convalescença pós-operatória mais suave e mais curta. Inspirado pelos benefícios bem documentados de cirurgia minimamente invasiva em adultos e crianças, o século XXI começou com as primeiras tentativas de transportar as vantagens desta abordagem para recém-nascidos, tal

  8. Silica-gel structural characterization during the initial phases of gelation and drying; Caracterizacao estrutural de geis de silica durante as etapas iniciais de gelacao e secagem

    Energy Technology Data Exchange (ETDEWEB)

    Ferreira, Max Passos

    1997-12-31

    For centuries, glasses and ceramics have been made via melting or solid state reactions at temperatures above 100 deg C. The sol-gel process offers new approaches to the synthesis of glasses and ceramics, combining control of composition and structure at the molecular level with the ability to shape materials in bulk, powder, fiber and thin-film forms. The growth of sol-gel technology research is due to the many unique features of that class of materials. Major applications include optical elements and integrated optical devices, ceramic filters, membranes, supercondutors, magnetic, catalytic and manostructured materials to antioxidant, anticorrosion coatings and composite and biomedical materials. In this work a variety of techniques like spectroscopy, Raman spectroscopy, ultraviolet-visible spectroscopy, light scattering nuclear magnetic resonance, X ray diffraction and nitrogen adsorption have been employed to investigate the initial phase of the sol-gel transition of gamma ray irradiated tetramethoxysilane (TMOS) solutions and non-irradiated TMOS solution and to get information about the structure of the silica gels obtained under different gelation conditions. Typically the tetramethoxysilane solutions were prepared using a molar ratio of TMOS to demineralized water of 1 to 16. Some experiments were made under catalysed conditions. The mixing was carried out at room temperature. The turbidity and light scattering experiments on the polycondensation of tetramethoxysilane show that exists no drastic difference in the gelling time of a gamma ray irradiated and a non-irradiated TMOS+H{sub 2}O (1+16 M) solution. In the absence of a catalyst, the gelling time for both reactions occurs in about 3.30 h. When HNO{sub 3} (o.03 M) was used, the gelling time observed was 3 days. Raman and ultraviolet-visible spectroscopy show no drastic difference during the initial phase at the sol-gel transition under ambient temperature/pressure and under gamma radiation. The gels

  9. Synthesis and characterization of gold nanoparticles as diagnostic and therapeutic tool; Sintese e caracterizacao de nanoparticulas de ouro como ferramenta terapeutica e diagnostica

    Energy Technology Data Exchange (ETDEWEB)

    Costa, Pryscila Rodrigues da

    2012-07-01

    Nanomedicine covers the use of nanoparticles to the targeted site of action as platforms for building imaging and therapeutic agents against cancer and other human diseases. In particular, gold nanoparticles (AuNp's) have proven to be efficient for the diagnosis and therapy. Interest in the development of AuNp's is due to their extraordinary physical and chemical properties resulting from the effect of its size in the nanoscale, to have an area of easy modification and the radioactive {gamma} and {beta} emitter ({sup 198}Au; E{gamma} = 0,411 MeV, {beta}{sub max} = 0,96 MeV; T{sub 1/2} = 2,69 days), having the advantage of being able to be applied as a diagnostic tool for molecular photon emission tomography (SPECT) using only a small amount of radioactive gold . In this study were synthesized AuNp's, whose surface is functionalized with a biocompatible polymer (modified polyethylene glycol) and folic acid in order to render them stealth and specific tumors that over express the folate receptors. The techniques of Dynamic Light Scattering (DLS), zeta potential ({zeta}), transmission electron microscopy (TEM) and UV-Visible absorption spectroscopy were employed to characterization of the size and geometry of the nanoparticles, in addition to confirming its binding to thiol -PEG and PEG-thiol Folate. The results of UV-Visible and TEM showed the formation of dispersed AuNp's ranging in size from 8-12 nm with a strong absorption around 520 nm, relating to a maximum of surface plasmon resonance. DLS results showed a hydrodynamic diameter of 10 and 14 nm. The (pH {approx} 5.0 to 6.0) ranged {zeta} potential values of the dispersions prepared between -16.2 and -42.1 mV, indicating stable colloidal suspensions. To determine the real concentration of gold in the samples, it was used neutron activation in the nuclear reactor TRIGA MARK I IPR-R1 CDTN / CNEN of Belo Horizonte. Biocompatibility studies in vitro and in vivo of the samples were carried out

  10. Silica-gel structural characterization during the initial phases of gelation and drying; Caracterizacao estrutural de geis de silica durante as etapas iniciais de gelacao e secagem

    Energy Technology Data Exchange (ETDEWEB)

    Ferreira, Max Passos

    1996-12-31

    For centuries, glasses and ceramics have been made via melting or solid state reactions at temperatures above 100 deg C. The sol-gel process offers new approaches to the synthesis of glasses and ceramics, combining control of composition and structure at the molecular level with the ability to shape materials in bulk, powder, fiber and thin-film forms. The growth of sol-gel technology research is due to the many unique features of that class of materials. Major applications include optical elements and integrated optical devices, ceramic filters, membranes, supercondutors, magnetic, catalytic and manostructured materials to antioxidant, anticorrosion coatings and composite and biomedical materials. In this work a variety of techniques like spectroscopy, Raman spectroscopy, ultraviolet-visible spectroscopy, light scattering nuclear magnetic resonance, X ray diffraction and nitrogen adsorption have been employed to investigate the initial phase of the sol-gel transition of gamma ray irradiated tetramethoxysilane (TMOS) solutions and non-irradiated TMOS solution and to get information about the structure of the silica gels obtained under different gelation conditions. Typically the tetramethoxysilane solutions were prepared using a molar ratio of TMOS to demineralized water of 1 to 16. Some experiments were made under catalysed conditions. The mixing was carried out at room temperature. The turbidity and light scattering experiments on the polycondensation of tetramethoxysilane show that exists no drastic difference in the gelling time of a gamma ray irradiated and a non-irradiated TMOS+H{sub 2}O (1+16 M) solution. In the absence of a catalyst, the gelling time for both reactions occurs in about 3.30 h. When HNO{sub 3} (o.03 M) was used, the gelling time observed was 3 days. Raman and ultraviolet-visible spectroscopy show no drastic difference during the initial phase at the sol-gel transition under ambient temperature/pressure and under gamma radiation. The gels

  11. Characterization of Nafion ionomer and its change due to X radiation; Caracterizacao do ionomero Nafion e sua modificacao por irradiacao de raios X

    Energy Technology Data Exchange (ETDEWEB)

    Almeida, Selma Helena de

    1996-07-01

    In this study, first the characterization of Nafion-117 membranes in the acid form (Nafion-H) and in the salt forms (Na{sup +}, K{sup +}, Rb{sup +} and Cs{sup +}) was performed. In another step, the X-ray effects on membranes (Nafion-H and Nafion-Na) were investigated. The samples were irradiated with X-ray, at 160 kGy/h, with 80-1280 kGy dosages. The characterization of samples (irradiated and unirradiated samples) was performed by X-ray diffractometry, vibrational spectroscopy (photoacoustic in infrared region and Raman scattering), electronic absorption spectroscopy (UV/Vis), electronic paramagnetic resonance spectroscopy (EPR) and thermal analysis (TG and DCS). The studies showed that the membranes submitted to high temperature or to hydration structural changes, as evidence by IR and UV/Vis spectra and DSC curves. This behavior can be assigned to the reorganization of the clusters, resulting in redistribution of the ions and reorientation of the polymers. UV/Vis spectra and DSC curves indicates that the conformational changes induced by temperature and hydration effect continue to occur slowly in the membrane due to relaxation of the polymer. TG analysis indicated that the thermal decomposition mechanism by Nafion-H is different from the mechanism by Nafion-Na. Nafion-H membranes degraded in at least three stages, while Nafion-Na membranes, which showed higher thermal stability than Nafion-H, degraded in only one stage. For irradiation dose higher than 320 kGy, the samples became brittle, which enhanced with increasing doses. This behavior indicates that the predominant effect was the chain scission. The results obtained by different technique showed that the main effects of X-rays on Nafion membranes are the following: decrease in the mechanical properties, peroxy radical production, formation of unsaturated species (C=C and C=O), scissions in the C-O and C-S bonds and SO{sub 2} production. The Nafion-Na membrane showed higher thermal stability and higher

  12. As bases moleculares da hemofilia A

    Directory of Open Access Journals (Sweden)

    Simone Ferreira Pio

    2009-01-01

    Full Text Available As hemofilias são doenças hemorrágicas resultantes da deficiência de fator VIII (hemofilia A ou de fator IX (hemofilia B da coagulação, decorrentes de mutações nos genes que codificam os fatores VIII ou IX, respectivamente. A hemofilia A é mais frequente que a hemofilia B e acomete aproximadamente 1:10.000 nascimentos masculinos. A gravidade e frequência dos episódios hemorrágicos está relacionado ao nível residual de atividade de fator VIII presente no plasma e este relaciona-se ao tipo de mutação associada à doença. A clonagem do gene do fator VIII tornou possível o conhecimento das bases moleculares da hemofilia A, sendo hoje conhecidas mais de 1.000 mutações associadas à doença. O conhecimento das bases moleculares da hemofilia A permite uma melhor compreensão da relação genótipo-fenótipo da doença, tomada de condutas clínicas diferenciadas em casos de mutações associadas a um maior risco de desenvolvimento de inibidor, determinação da condição de portadora de hemofilia em mulheres relacionadas aos pacientes, implementação de programa de aconselhamento genético/orientação familiar e melhor compreensão das relações estruturais-funcionais do gene-proteína. Este artigo propõe revisar as bases moleculares da hemofilia A, os métodos laboratoriais utilizados para a caracterização das mutações e as implicações clínicas envolvidas no diagnóstico molecular da hemofilia A.Hemophilias are bleeding disorders due to deficiency of the blood coagulation factor VIII (hemophilia A or factor IX (hemophilia B, resulting from mutation on the gene coding for factor VIII or factor IX. Hemophilia A is more frequent than hemophilia B and affects 1:10,000 male newborns. The severity and frequency of hemorrhagic episodes is related to residual activity of factor VIII present in the plasma and relates to the type of mutation associated with the disorder. Cloning of the factor VIII gene has enabled researchers to

  13. The da Vinci robotic surgical assisted anterior lumbar interbody fusion: technical development and case report.

    Science.gov (United States)

    Beutler, William J; Peppelman, Walter C; DiMarco, Luciano A

    2013-02-15

    Technique development to use the da Vince Robotic Surgical System for anterior lumbar interbody fusion at L5-S1 is detailed. A case report is also presented. To evaluate and develop the da Vinci robotic assisted laparoscopic anterior lumbar stand-alone interbody fusion procedure. Anterior lumbar interbody fusion is a common procedure associated with potential morbidity related to the surgical approach. The da Vinci robot provides intra-abdominal dissection and visualization advantages compared with the traditional open and laparoscopic approach. The surgical techniques for approach to the anterior lumbar spine using the da Vinci robot were developed and modified progressively beginning with operative models followed by placement of an interbody fusion cage in the living porcine model. Development continued to progress with placement of fusion cage in a human cadaver, completed first in the laboratory setting and then in the operating room. Finally, the first patient with fusion completed using the da Vinci robot-assisted approach is presented. The anterior transperitoneal approach to the lumbar spine is accomplished with enhanced visualization and dissection capability, with maintenance of pneumoperitoneum using the da Vinci robot. Blood loss is minimal. The visualization inside the disc space and surrounding structures was considered better than current open and laparoscopic techniques. The da Vinci robot Surgical System technique continues to develop and is now described for the transperitoneal approach to the anterior lumbar spine. 4.

  14. Part I---Evaluating Effects of Oligomer Formation on Cytochrome P450 2C9 Electron Transfer and Drug Metabolism, Part II---Utilizing Molecular Modeling Techniques to Study the Src-Interacting Proteins Actin Filament Associated Protein of 110 kDa (AFAP-110) and Cortactin

    Science.gov (United States)

    Jett, John Edward, Jr.

    nanopillars, the immobilization of CYP2C9 enzymes to those nanopillars, and the utilization of the array to perform conductive probe atomic force microscopy experiments examining the electron transfer process of CYP2C9 in the absence and presence of substrate molecules. Part II. The Src protein has been known to play a role in cancer cell progression for over 30 years. The function of a non-receptor tyrosine kinase such as Src is to relay extracellular signals through intracellular tyrosine phosphorylation. As a tyrosine kinase, Src and the cellular signaling pathways it is involved in play many functional roles in the cell, both in cellular proliferation and in cytoskeletal dynamics, cell adhesion, motility and invasion. Two of the many proteins comprising Src cellular signaling pathways are actin filament associated protein of 110 kDa (AFAP-110) and cortactin. AFAP-110 is a known activator of Src; one mechanism to abrogate the AFAP-110-induced activation of Src is to inhibit their colocalization within the cell. This colocalization is expected to occur when the pleckstrin homology (PH1 and PH2) domains of AFAP-110 are allowed to interact with membrane-bound phospholipids. Cortactin, on the other hand, is a cytosolic protein capable of being phosphorylated on various tyrosine residues, activating it and allowing it to interact with actin. The Src homology 2 (SH2) domain of Src has been shown to be capable of interacting with cortactin, an association which will be probed here. This section of the dissertation will discuss the use of molecular modeling techniques to develop structural models of the AFAP-110 PH1 and PH2 domains and use them to make predictions about how the protein interacts with phospholipids in the plasma membrane and how they might be stabilized to interact with other proteins. Structural models were designed using homology modeling methods, docking programs were used to predict key residues of AFAP-110 involved in binding to phospholipids and mutational

  15. Os limites da competitividade

    Directory of Open Access Journals (Sweden)

    Henrique Rattner

    2009-08-01

    Full Text Available

    Costuma-se destacar os aspectos aparentemente positivos e as vantagens hipotéticas da concorrência e da competitividade entre empresas e também entre nações. Não se pode negar que a concorrência nos mercados tenha exercido uma função central e fundamental na gênese e na expansão do sistema de produção capitalista. Ela contribuiu para a geração e acumulação de riquezas materiais. Também estimulou e fortaleceu as aspirações de seus principais atores sociais, os empreendedores, de exigir uma organização política mais democrática em oposição ao regime feudal ou absolutista, em determinado período da história do mundo ocidental.

  16. The European industry reliability data bank EIReDA

    International Nuclear Information System (INIS)

    Procaccia, H.; Aufort, P.; Arsenis, S.

    1997-01-01

    EIReDA and the computerized version EIReDA.PC are living data bases aiming to satisfy the requirements of risk, safety, and availability studies on industrial systems for documented estimates of reliability parameters of mechanical, electrical, and instrumentation components. The data updating procedure is based on Bayesian techniques implemented in a specific software: FIABAYES. Estimates are mostly based on the operational experience of EDF components, but an effort has been made to bring together estimates of equivalent components published in the open literature, and so establish generic tables of reliability parameters. (author)

  17. da sede da Fazenda Rialto, Bananal

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    Regina A. Tirello

    2005-01-01

    Full Text Available This article is about the eighteenth century mural paintings at the headquarters of Fazenda Rialto, in Bananal, which were destroyed in 1996. These constituted one of the most important sets of ambient paintings with secular themes produced in the state of São Paulo during the period corresponding to the first cycle of coffee production. Orally attributed to the painter José Maria Villaronga y Panella, all that remains of these paintings are some photographs and dozens of fragments, impossible to reassemble. Studying the fragments of the paintings of Rialto as primary material documents, the main objective of this article is to identify the artistic, technical, and executive characteristics of three sets of murals attributed to a single painter. A methodology which combines laboratory tests and historical research on artistic techniques was adopted for objectively recognizing the artistic and artisan characteristics of the period and discussing the attribution of exclusive authorship to the work. The analytical systems adopted for this purpose were: examination with ultraviolet and infra-red radiation, optical microscopy, Scanning Electron Microscopy (SEM and Energy Dispersive Spectrometry (EDS to analyze its chemical elements. Issues related to the limitations on official Brazilian preservation activities for this category of artistic work were also discussed, reflecting on the development and changes in notions of historicity related to the preservation of works from the past and their methodological implications for conservation and restoration.

  18. Engenharia da mente

    OpenAIRE

    Bueno, Tânia Cristina D'Agostini

    2005-01-01

    Tese (doutorado) - Universidade Federal de Santa Catarina, Centro Tecnológico. Programa de Pós-Graduação em Engenharia de Produção. Na era da informação digitalizada, pesquisadores de diferentes áreas do conhecimento enfrentam uma nova questão: a organização semântica dos dados. A matéria tornou-se importante pelo fato das informações digitalmente disponíveis estarem dispostas, em sua maioria, como dados não-estruturados. Todavia, sabe-se que a estruturação de dados é um problema complexo ...

  19. Em favor da talassografia

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    Jean-Louis Boudou

    2001-01-01

    Full Text Available A Talassografia (“descrição do mar” interessa-sepelos impactos físicos, biológicos, ecológicos... culturais da violenta antropização dos ambientes costeiros (oceânicos e continentais, caracterizados pelaexigüidade, vulnerabilidade, fragilidade e plasticidade. Como o Brasil é um “país marítimo”, os geó-grafos (os talassógrafos brasileiros são convidadosa intensificar suas pesquisas nas áreas costeiras e acriar novas estruturas para divulgá-las: Revista, Encontros, Associação, Pós-Graduação... tudo em prolda talassografia.

  20. ANÁLISE PRELIMINAR DA CONTROLADORIA DA CIDADE DE SALVADOR

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    João Marcelo Pitiá Barreto

    2012-06-01

    Full Text Available A Controladoria tem sido alvo de estudos e destaque de análises e reflexões dos estudiosos das ciências que têm como foco o campo gerencial das organizações como a da Administração e Contabilidade. É importante observar a contribuição da Controladoria à governança pública, fundamento de uma gestão democrática e participativa. Nesse contexto, insere-se o objetivo deste estudo, refletir sobre atuação da controladoria pública da cidade de Salvador, observando a contribuição efetiva na governança nesse município. Os estudos foram desenvolvidos na Secretaria da Fazenda (SEFAZ do município a quem Controladoria vincula-se. Com caráter exploratório, essa investigação descritiva envolveu pesquisa de campo, análise de documentos e relatórios emitidos pela SEFAZ e pelo Tribunal de Contas do Município (TCM. Verificou-se o organograma da SEFAZ, seu orçamento e os pareceres do TCM. Os resultados expressam a importância da Controladoria e denotam a impressão de que, na instituição estudada, essa área não esteja cumprindo bem seu papel. 

  1. Ocorrência da ferrugem da videira em Minas Gerais

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    Adelica Aparecida Xavier

    2012-03-01

    Full Text Available A ferrugem da videira causada por Phakopsora euvitis Ono constitui-se numa ameaça às regiões produtoras de uva em função do potencial destrutivo da planta. A doença foi detectada no Brasil, pela primeira vez, em 2001. Atualmente, ela ocorre no Paraná, Mato Grosso do Sul, São Paulo, Rio Grande do Sul, Mato Grosso, Roraima, Espírito Santo e Santa Catarina. Em abril de 2010, observaram-se na estação experimental da Unimontes, Janaúba, Minas Gerais, plantas da cv. Niágara rosada com sintomas típicos da doença. A análise dos sintomas e a caracterização dos urediniósporos sésseis, levemente equinulados, com formato oval, ou elipsoide formado em urédias subepidérmicas na origem, inrompentes e com paráfises circundantes dorsalmente, levaram à diagnose de Phakopsora euvitis como o agente causal da doença. Este é o primeiro relato da doença no Estado de Minas Gerais.

  2. Estudo comparativo da matéria orgânica de diferentes classes de solos de altitude do sul do Brasil por técnicas convencionais e espectroscópicas Comparative study of organic matter from different high-altitude soil classes in south Brazil by conventional and spectroscopic techniques

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    Deborah Pinheiro Dick

    2008-12-01

    Full Text Available A região dos Campos de Cima da Serra, RS, apresenta solos com elevados teores de matéria orgânica (MOS, sendo freqüente teores altos de Al trocável. A proposta deste trabalho foi investigar a qualidade da MOS de amostras de camadas superficiais (0 a 10 cm de oito solos representativos da região (dois Neossolos, dois Gleissolos, três Cambissolos e um Latossolo sob pastagem nativa, com os seguintes objetivos: avaliar seu comportamento diante da desmineralização da amostra com solução de HF; determinar a sua composição química; e investigar a influência do Al trocável e dos óxidos de Fe na qualidade da MOS. A matéria orgânica foi concentrada com solução de HF 10 cL L-1 e posteriormente avaliada por análise elementar e espectroscopias de FTIR e de RMN 13C CP/MAS. A fração da massa recuperada (5,8 a 10 % após tratamento com HF correlacionou-se com teor de C original do solo, enquanto a proporção de C recuperado (47 a 86 % correlacionouse inversamente com o teor de óxidos de Fe. Esse resultado indica que parte da MOS encontra-se associada a esses minerais nesses ambientes. Os teores de estruturas C O-alquil totais (52 a 59 % foram elevados e os valores de índice I1630/I2920(FTIR foram baixos, evidenciando baixo grau de decomposição e de humificação da MOS desses solos.Soils in the region of Campos de Cima da Serra, RS, have high organic matter contents (SOM and high levels of exchangeable Al. This study aimed to investigate the SOM quality of surface samples (0-10 cm of eight representative soils from the region (two Neossols, two Gleissols, three Cambissols, one Latosol under native pasture. The objectives were to evaluate the sample behaviour under demineralization with HF solution, to determine the chemical composition and the influence of exchangeable Al and iron oxides on it. The SOM was concentrated with 10 % (v/v HF solution and then submitted to elemental analysis, FTIR and 13C NMR CP/MAS spectroscopy. The

  3. Reflexões sobre o cuidar de mulheres que sofrem violência conjugal em uma perspectiva heideggeriana do mundo da técnica Reflexiones acerca del cuidar a mujeres que sufren violencia conyugal en una perspectiva heideggeriana del mundo de la técnica Reflexions about care of women that suffer conjugal violence in a heidegger's perspective of the world of technique

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    Maria Suely Medeiros Corrêa

    2001-09-01

    Full Text Available Trata-se de um texto reflexivo que aborda a questão do cuidado a mulheres que sofrem violência conjugal em uma perspectiva analítica do mundo da técnica, desenvolvido a partir de concepções e conceitos de Martin Heidegger, filósofo contemporâneo da fenomenologia. O cuidar de mulheres em situação de violência conjugal surge como envolvendo valores, decisão, confiança para cuidar, conhecimento e ações de cuidado e suas conseqüências.Se trata de un texto reflexivo que aborda la cuestión del cuidado a mujeres que sufren violencia conyugal en una perspectiva analítica del mundo de la técnica, desarrollado a partir de concepciones y conceptos de Martin Heidegger, filósofo contemporâneo de la fenomenologia. El cuidar a mujeres en situación de violencia conyugal surge como envolviendo valores, decisión, confianza para cuidar, conocimiento y acciones de cuidada y sus consecuencias.This is concerned with a reflexive text that approaches the subject of the care to women that suffer conjugal violence in an analytic perspective of the world of the technique, developed from conceptions and concepts of Martin Heidegger, contemporary philosopher of phenomenology. The care of women that suffer conjugal violence appears as one that considers values, decision, trust to care, knowledge and care actions and its consequences.

  4. Historicidade da filosofia em Hegel e Heidegger

    OpenAIRE

    Christian Iber

    2017-01-01

    Gostaria de discutir, em forma de teses, a temática da historicidade da filosofia em contraste e na sua divergência em Hegel e Heidegger. Diferente do historicismo, que não soluciona o problema da historicidade da filosofia, porque ele dissolve tendencialmente a filosofia na história da filosofia e não coloca em especial a questão da verdade, Hegel e Heidegger desenvolvem uma teoria genuinamente filosófica da história da filosofia do interesse filosófico pela verdade. Esse interesse genuiname...

  5. Novas técnicas cirúrgicas para o tratamento da atresia pulmonar com comunicação interventricular e anomalias de artérias pulmonares incluindo o assim chamado truncus tipo IV New surgical techniques for treatment of pulmonary atresia with ventricular septal defect and pulmonary arteries anomalies including the so-called tipo IV truncus

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    Miguel Barbero-Marcial

    1987-04-01

    Full Text Available Entre janeiro de 1975 e outubro de 1986, 42 pacientes com atresia pulmonar e comunicação interventricular, com idade entre 2 e 18 anos, foram submetidos a correção parcial, ou total. Foram divididos em: tipo A com todos os segmentos broncopulmonares conectados às artérias pulmonares (AP's, 34 pacientes; tipo B com alguns dos segmentos broncopulmonares conectados às AP's, 6 pacientes; tipo C com todos os segmentos broncopulmonares conectados às colaterais sistêmico-pulmonares, 2 pacientes. A correção foi planejada em uma a três etapas. No tipo A, 17 foram corrigidos em uma etapa, com três óbitos; em 9, na primeira etapa, as AP's foram reconstruídas e o Blalock (BT, realizado, tendo ocorrido um óbito. Em 2, a segunda etapa de correção total foi realizada, sem óbitos. No tipo B, a primeira etapa de unificação das colaterais intra ou extra-hilares foi realizada em 6 casos, sem óbitos; em 2, a segunda etapa da correção total foi realizada, com um óbito. No tipo C, 2 pacientes foram operados; 1 em três etapas; a primeira constou de construção de segmento arterial intermediário entre as artérias lobares e o BT; a segunda compreendeu unificação das colaterais contralaterais e a terceira, restabelecimento da continuidade ventrículo direito - circulação pulmonar; o paciente teve boa evolução. No segundo caso, a correção foi realizada após somente uma intervenção prévia. A evolução foi satisfatória. Estudos hemodinâmicos seriados foram realizados em 32 pacientes. As técnicas propostas permitem obter condições para correção total com adequada relação pós-operatória das pressões ventrículo direito - ventrículo esquerdo.Fourty-two patients with pulmonary atresia and interventricular septal defect were submited to a partial or total correction, between January 1975 and October 1986, with a range of 2 months to 18 years of age. Three groups were identified: Group A: 34 patients with all bronco

  6. Modelo para sistemas da qualidade como base da estrategia competitiva

    OpenAIRE

    Marco Antonio Silveira

    1999-01-01

    Resumo: Vários autores propõem a empresa como um sistema em transformação, sendo que esse enfoque sistêmico parece oferecer um meio efetivo de prover as capacidades estratégicas que são valorizadas pelos mercados atuais. Por outro lado, vem crescendo a consciência para o enfoque da qualidade como base da estratégia competitiva, onde esta é associada à lucratividade e incluída no processo de planejamento estratégico, tornando-se um instrumento eficaz de concorrência que, para fazer frente à di...

  7. Dimensão da maturidade à luz da logoterapia

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    Libardi, Tadeu Antonio

    2008-01-01

    Full Text Available O artigo aborda o tema da maturidade humana à luz da logoterapia, fundada por Viktor Emil Frankl. Nos dias de hoje, existe a frustração existencial, não mais a sexual, como analisada por Freud. Cada ser humano, como pessoa livre e responsável e tendo como meta a busca da maturidade, vai percorrendo seu próprio caminho, que o leva à ceitação de si, de seus limites e potencialidades e ao relacionamento social e religioso, capacitando-o ao confronto com o sofrimento humano

  8. Descrição de técnica de redução cirúrgica das luxações facetárias da coluna cervical baixa por via anterior Descripción de la técnica quirúrgica para reducción de las luxaciones facetarias de la columna cervical baja por acceso anterior Description of surgical technique for reduction of facet dislocations of the lower cervical spine by anterior approach

    Directory of Open Access Journals (Sweden)

    André Rafael Hübner

    2012-12-01

    Full Text Available O trabalho descreve uma técnica cirúrgica de redução anterior das luxações facetárias da coluna cervical e discute as indicações para cirurgia por via anterior para as luxações da coluna cervical baixa. A técnica descrita neste artigo oferece excelentes resultados, conforme revisão bibliográfica e dos resultados do Serviço, tendo sido aplicada em até 95% dos casos de fraturas-luxações. Não será abordada a apresentação de resultados neste trabalho, apenas a descrição e discussão da técnica aberta por via anterior. Observações de quarenta e um pacientes tratados nos últimos dez anos por esta técnica demonstram bons resultados quanto a pós-operatório menos doloroso, recuperação funcional extremamente rápida e complicações pouco frequentes.El artículo describe una técnica quirúrgica para las luxaciones facetarias de la columna cervical y discute las indicaciones para la cirugía de luxación de la columna cervical baja por lo acceso anterior. La técnica descrita en este artículo proporciona excelentes resultados según la revisión de la literatura y los resultados del Servicio, después de haber sido aplicado a 95% de los casos de fracturas-luxaciones. No serán abordados resultados, sino que únicamente la descripción y discusión de la técnica de reducción abierta por acceso vía anterior. Las observaciones en cuarenta y un pacientes operados en los últimos diez años por esta técnica muestran resultados sorprendentes con respecto a un pos operatorio menos doloroso, con recuperación funcional extremadamente rápida y complicaciones menos frecuentes.This paper describes a surgical technique for anterior reduction of the spinal facets dislocations and discusses its indications for surgery of lower cervical dislocations by anterior approach. The technique described in this article provides excellent results according to literature review and the results of the Service, having been applied to 95% of

  9. O carnaval da turba futurista

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    Ana Paula Freitas de Andrade

    2017-11-01

    Full Text Available O artigo trata da repercussão do futurismo italiano no Brasil, a partir da análise de crônicas de Menotti Del Picchia publicadas no Correio Paulistano, entre 1920 e 1922. Nessa época o escritor participou da polêmica sobre a vanguarda italiana veiculada na imprensa paulistana, publicando uma série de crônicas que, ao promover ideias futuristas e criticar a literatura passadista, estabelecem a formulação de um futurismo compósito, adaptado à realidade brasileira; e esboçam as principais teses do movimento modernista.

  10. Evapotranspiração da cultura da cebola

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    G. M. Oliveira

    2015-10-01

    Full Text Available A determinação da quantidade de água necessária para as culturas é um dos principais fatores para o correto planejamento, dimensionamento e manejo de qualquer sistema de irrigação. O presente trabalho teve como objetivo, comparar medida da evapotranspiração da cultura (ETc da cebola com estimativa obtida a partir da evapotranspiração de referência (ETo determinada por diferentes métodos e Kc proposto na literatura. O experimento foi conduzido no campo experimental do Departamento de Tecnologia e Ciências Sociais da Universidade do Estado da Bahia - UNEB, em Juazeiro, no período de junho a setembro de 2011. As medidas da ETc foram obtidas em evapotranspirômetros e as estimativas, a partir de ETo determinada pelos métodos: Penman-Monteith (padrão FAO, Penman-Monteith modificado por Villa Nova et al. (2004, Hargreaves & Samani, Makkink e Jensen & Haise e Kc proposto por Marouelli et al. (2005, para a cultura da cebola. É fundamental a avaliação de métodos de estimativa da evapotranspiração de referência antes de sua aplicação, pois erros consideráveis podem ser cometidos na determinação da quantidade de água a ser aplicada a uma cultura, o que repercutirá certamente, na produtividade.Evapotranspiration crop onionAbstract: The determination of the amount of water needed for crops is a major factor for the correct planning, sizing and management of any irrigation system. This study aimed to compare measure of crop evapotranspiration (ETc onion with estimates obtained from the reference evapotranspiration (ETo determined by different methods and Kc proposed in the literature. The experiment was conducted in the experimental field of the Department of Technology and Social Sciences, University of the State of Bahia, in Juazeiro, from June to September 2011. The ETc measurements were obtained in evapotranspirometers and estimates, from ETo determined by the methods: Penman-Monteith (FAO standard, Penman-Monteith modified

  11. High dose rate endobronchial brachytherapy - treatment technique

    International Nuclear Information System (INIS)

    Carvalho, Heloisa de Andrade; Aisen, Salim; Haddad, Cecilia Maria Kalil; Nadalin, Wladimir; Pedreira Junior, Wilson Leite; Chavantes, Maria Cristina

    1998-01-01

    High dose rate endobronchial brachytherapy is efficient in symptom relief due to obstructive endobronchial malignancies. However, it's role in survival improvement for patients with lung cancer is not yet established. The use of this treatment in increasing, specially in the developing countries. The purpose of this paper is to present the treatment technique used in the Radiotherapy Department of the Hospital da Clinicas, University of Sao Paulo, based on an experience of 60 cases treated with 180 procedures. Some practical suggestions and rules adopted in the Department are described. The severe complications rate is 6.7%, demonstrating an adequate patient selection associated with the technique utilized. (author)

  12. Dos Males da Medida

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    Lilia Moritz Schwarcz

    1997-01-01

    Full Text Available Esse artigo tem como objeto a difícil percepção da "diferença". Tema polêmico, o debate sobre as variedades culturais foi transformado, em meados do século XIX, em uma questão racial e, nesse sentido, vinculado às regularidades da biologia. Tecendo comparações entre os teóricos raciais brasileiros e os impasses mais contemporâneos, sobre a aferição de inteligência e capacidade, esse ensaio pretende provocar. Em pauta estarão as contradições que têm se destacado, mais recentemente, quando se opõem de um lado as etnicidades locais, de outro a tão propalada globalização. Tal qual dois lados de uma mesma moeda, a afirmação de identidades tem se mostrado tão evidente como o próprio estreitamento das relações internacionais. Mudam os termos do debate - de raça, para etnia -, mas, de alguma maneira, continuamos presos a uma lógica positiva de estabelecimento de hierarquias ontológicas.This article has as its objective the difficult perception of "difference". A controversial theme, in the nineteenth century, this debate on cultural varieties, became a racial issue and in this sense, bonded to the regularities of biology. In such a context, this essay intends to provoke comparisons about the standard measure of intelligence and capacity, between Brazilian racial theorists and the impasse of more contemporary times. Appointed here will be the contradictions which have, more recently grown in importance, and have opposed through one aspect, local ethnic groups and through another the greatly publicized globalization. As are the two sides of a coin, the affirmation of identities has shown itself as evident as the tightening of international relations. The terms of the debate change from race to ethnicism, but in some way, we are still tied to a positivist logic which establishes ontologic hierarchies.

  13. SOBRE OS FUNDAMENTOS DA ARQUITETURA DA INFORMAÇÃO

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    Alfram Roberto Rodrigues de Albuquerque

    2011-10-01

    Full Text Available Expõe-se o estado atual da disciplina Arquitetura da Informação quanto a problemática terminológica da definição do campo de estudo, apresentando-se argumentos para uma definição de Arquitetura da Informação de uma forma ampla na qual os usos correntes dessa expressão sejam vistos como especializações. Defende-se uma definição com a utilização de um conjunto de propriedades mínimas cujas interações levam a uma terminologia formal e cuja abstração leva a uma definição formal do conceito que emprega a linguagem de morfismos da Teoria das Categorias. Trata-se de um recorte de alguns dos resultados obtidos na tese de doutoramento de um dos autores, defendida em setembro de 2010. O contexto da pesquisa é exposto e alguns dos resultados obtidos são delineados.

  14. O sentido da espiritualidade na transitoriedade da vida

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    Isabel Cristina de Oliveira Arrieira

    Full Text Available Resumo Objetivo: Compreender o sentido da espiritualidade para a pessoa em cuidados paliativos. Métodos: Abordagem qualitativa, fundamentada na fenomenologia existencialista e referencial de Viktor Frankl. Os participantes foram nove pessoas em cuidados paliativos atendidas no domicílio. Informações coletadas por meio da observação e de entrevista realizadas no período de junho a outubro de 2014, gravadas, transcritas e transformadas em texto interpretado com a abordagem fenomenológica hermenêutica. Resultados: Surgiram as seguintes categorias: sentido de continuidade da vida; sentido de alívio do sofrimento; sentido de naturalidade da morte e sentido de valorização do viver. Conclusão: Para a integralidade da atenção faz-se necessário a inclusão da espiritualidade na prática do cuidado em saúde. A espiritualidade proporciona o encontro existencial entre a pessoa em cuidados paliativos e os profissionais que a cuidam em sua integralidade.

  15. O uso da aromaterapia na melhora da autoestima

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    Juliana Rizzo Gnatta

    2011-10-01

    Full Text Available Os objetivos deste estudo foram verificar se a inalação dos óleos essenciais de rosa e de ylang-ylang alteram a percepção da autoestima e comparar a eficácia dos mesmos. O projeto foi aprovado pelo Comitê de Ética em Pesquisa do Hospital da Universidade de São Paulo. Participaram 43 funcionários dos setores de Higienização e da Central de Materiais e Esterilização durante os meses de maio a julho de 2009. Os sujeitos foram randomizados em três grupos: dois que receberem os óleos essenciais e outro que recebeu placebo (essência de rosa. A avaliação da autoestima foi feita através de uma escala já validada no Brasil, sendo aplicada antes do uso dos aromas, depois de 30 dias de uso e ao completar 60 dias. Dentre os resultados, verificou-se que a amostra era constituída por 88,6% de indivíduos com média e alta autoestima e que os óleos essenciais em questão não alteraram de forma significativa a percepção da autoestima.

  16. A utilização da teoria da aprendizagem significativa no ensino da Enfermagem

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    Alana Tamar Oliveira de Sousa

    2015-08-01

    Full Text Available RESUMOObjetivo:sintetizar a produção científica acerca da Teoria da Aprendizagem Significativa no processo de ensino-aprendizagem em Enfermagem.Método:revisão integrativa realizada nas bases de dados MEDLINE, LILACS, SciELO, BDENF e CINAHL, com artigos que abordaram a temática ou aspectos da teoria da aprendizagem significativa de David Ausubel. Fizeram parte da amostra dez artigos, sendo seis escritos no idioma português e quatro no inglês, publicados de 1998 a 2013.Resultados:cinco artigos fizeram alusão à Teoria da Aprendizagem Significativa, quatro citaram Ausubel como autor dessa teoria e apenas dois seguiram a estrutura para a aplicação da teoria completamente. Há escassez de estudos sobre o tema e os que o abordam não o correlacionam com a teoria de Ausubel.Conclusão:faz-se necessário romper com a dicotomia entre teoria e prática e promover a articulação dos conteúdos com a ação, introduzindo o aluno como autor de seu próprio conhecimento.

  17. Uso da Técnica do Micro-Hematócrito para Predição do Peso Corporal e de Características Reprodutivas em Frangos de Corte Utilization of Micro-Hematocrit Technique on Body Weight and Reproductive Traits Prediction in Broiler Chickens

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    Millor Fernandes do Rosário

    2002-06-01

    Full Text Available O hematócrito é uma metodologia indireta utilizada no monitoramento da síndrome ascítica que poderia ser utilizada também para avaliar o peso corporal e características reprodutivas em frangos de corte. Objetivou-se com este trabalho avaliar a técnica do micro-hematócrito em relação ao peso corporal e características reprodutivas (fertilidade, eclodibilidade e nascimento visando sua utilização pelos programas de melhoramento genético. Dois grupos contrastantes foram constituídos, baseados na seleção fenotípica de 630 reprodutores de 18 genótipos para a característica hematócrito. Progênies das aves selecionadas, 74 pintos não sexados (40 do grupo de hematócrito alto e 34 do grupo baixo foram criados com manejo convencional. Os pesos corporais e os valores de hematócrito foram mensurados aos 14 e 42 dias de idade. Para avaliar as características reprodutivas, ovos de 42 matrizes (22 do grupo alto e 20 do baixo foram incubados. As médias foram estimadas utilizando-se um modelo linear com o efeito fixo do grupo genético. Os pintos do grupo baixo apresentaram as maiores médias de peso corporal (305,59 e 1387,06 g, diferindo dos pintos do grupo alto os quais apresentaram médias de peso de 243,56 e 1128,11 g aos 14 e 42 dias de idade, respectivamente. Também para o valor do hematócrito os grupos diferiram significativamente. Para as características reprodutivas, não se verificou diferenças significativas entre os grupos, sendo as médias gerais para fertilidade de 93,8 e 94,9%, para eclodibilidade de 98,2 e 93,9% e para nascimento de 89,3 e 82,4%, respectivamente, para alto e baixo hematócrito. Concluiu-se que a técnica do micro-hematócrito pode ser empregada para avaliação do peso corporal, mas não para características reprodutivas.Hematocrit is an indirect method used to monitor ascites, which might be used also on body weight and reproductive traits evalution in broiler chickens. The aim of this paper was

  18. Da janela do meu quarto

    Directory of Open Access Journals (Sweden)

    Esther Hamburger

    2008-12-01

    Full Text Available O texto aborda o curta Da Janela do Meu Quarto de Cao Guimarães como contraponto a filmes brasileiros recentes que lidam com a desigualdade social brasileira na chave da violência. O texto contrasta o distanciamento imposto pelo posicionamento de câmera e efeitos de montagem e som nesse filme, com o uso de estratégias de pertencimento e apropriação presentes em filmes "de resultado".

  19. Da janela do meu quarto

    OpenAIRE

    Hamburger, Esther

    2008-01-01

    O texto aborda o curta Da Janela do Meu Quarto de Cao Guimarães como contraponto a filmes brasileiros recentes que lidam com a desigualdade social brasileira na chave da violência. O texto contrasta o distanciamento imposto pelo posicionamento de câmera e efeitos de montagem e som nesse filme, com o uso de estratégias de pertencimento e apropriação presentes em filmes "de resultado".

  20. Aplicação da técnica de Estrutura Analítica de projeto para o sub-projeto do Catálogo de Sites da Biblioteca Virtual em Saúde: Enfermagem Aplicación de la técnica de Estructura Analítica de proyecto para el subproyecto de lo Catalogo de Sitios de la Biblioteca Virtual en Salud: Enfermería Application of the technique of Analytical Structure of project for the sub-project of Websites Catalog of the Virtual Health Library: Nursing

    Directory of Open Access Journals (Sweden)

    Luís Augusto dos Santos

    2007-12-01

    Full Text Available Este trabalho procura, de forma didática, explicar os benefícios de uso de uma técnica de gerenciamento de projetos, chamada de Estrutura Analítica do Projeto - uma ferramenta gráfica para identificar os resultados principais a serem desenvolvidos por um projeto. Os exemplos são reais, aplicados a um sub-projeto da Biblioteca Virtual em Saúde em Enfermagem (BVS-Enfermagem para o desenvolvimento de Catálogo de Sites. Destacam-se os benefícios de visualização gráfica para um maior entendimento entre profissionais de diferentes áreas.Este artículo presenta, de una forma didáctica, algunas explicaciones sobre los beneficios de lo uso de la técnica de gestión de proyectos, llamada de Estructura Analítica del Proyecto una herramienta grafica para la identificación de los principales resultados que han de ser desarrollados en un proyecto. Los ejemplos son reales, aplicados a un subproyecto de la Biblioteca Virtual en Salud Enfermería (BVS-Enfermagem para el desarrollo del catalogo de sitios. Son destacados los beneficios de visualización grafica para un mejor entendimiento entre profesionales de diferentes áreas.This work search of didactic form to explain the benefits of use of one technique of management project, called Work Breakdown Structure: a graphical tool to identify the main results to be developed for a project. The real examples are applied to a sub-project of the Virtual Library in Health in Nursing (BVSEnfermagem to development of the Sites Catalogs. It is distinguished the benefits of graphical visualization for a major agreement between professionals of different expertise

  1. Perspective of using the sterile insect technique for Tobacco Budworms Heliothis virescens (Lepidoptera: Noctuidae) and Cotton Bollworm Helicoverpa armigera (Lepidoptera: Noctuidae) in cotton crop as an alternative method of control; Perspectiva de utilizacao da Tecnica do Inseto Esteril para lagarta da maca Heliothis virescens (Lepidoptera: Noctuidae) e lagarta do velho mundo Helicoverpa armigera (Lepidoptera: Noctuidae) na cultura do algodoeiro como um metodo alternativo de controle

    Energy Technology Data Exchange (ETDEWEB)

    Haddad, Gianni Queiroz

    2017-07-01

    Since the 1950s, scientists have used ionizing radiation to sterilize insects, which are released in nature to mate, but without any progeny. Known as the sterile insect technique (TIE), this method of insect control has traditionally used ionizing radiation to sterilize insects, a technique that does not generate residues, and can act in synergy with the other techniques within integrated pest management. For several years, Brazil has been fighting against the increase of pests, introducing new tactics and techniques within the IPM programs, to overcome the resistance of chemical products, such as: reducing the residues of agrochemicals; For some important crops of our country, we have a wide spectrum of pests occurring from the beginning to the end of the harvest, one of them is the cotton crop and among the key pests of this crop, we have some extremely important caterpillars, among them Heliothis virescens and Helicoverpa armigera These species are morphologically similar, the second being identified a few years ago in Brazil. There are still no studies in Brazil using TIE as an additional tool for Lepidoptera, therefore the purpose of this study was to evaluate the effect of doses of gamma radiation in the different phases of the evolutionary cycle of Heliothis virescens and Helicoverpa armigera, as well as to evaluate the sterility in generation P And the ability of insects to irradiate with non-irradiated insects. The pupal phase presented the best result because 75 Gy achieved sterility in Heliothis virecens and 100 Gy sterilized Helicoverpa armigera, therefore it contemplated the phase and dose chosen to evaluate the competition between the irradiated insects and the normal insects of both species. Both Heliothis virecens and Helicoverpa armigera presented a satisfactory result, as the irradiated insects managed to significantly reduce the viability of the eggs in a ratio of 9: 1: 1. (author)

  2. Análise de técnicas de interpolação para espacialização da precipitação pluvial na bacia do rio Itapemirim (ES / Analysis of interpolation techniques for spatial rainfall distribution in river basin Itapemirim (ES

    Directory of Open Access Journals (Sweden)

    Benvindo Sirtoli Gardiman

    2012-04-01

    Full Text Available ResumoEste trabalho teve como objetivo comparar o desempenho de cinco métodos de interpolação: inverso da distância ponderada (IDW, Krigagem esférico, natural vizinho, Spline regularizada e Topo to Raster. Para tanto, utilizaram-se dados de precipitação pluviométrica média mensal de um período de trinta anos (1972 a 2002, obtidas junto ao Sistema de Informações Hidrológicas (HidroWEB da Agência Nacional de Águas (ANA, de estações localizadas dentro e fora da área da bacia hidrográfica do rio Itapemirim, sul do estado do Espírito Santo. Os resultados apontam que o interpolador de Krigagem esférica obteve o menor Erro Quadrado Médio (EQM, Percentual de Eficiência (EF%, Erro Médio Absoluto (MAE, Coeficiente de Determinação (r² e Estimativa do Erro Padrão (EEP, seguido por IDW, Spline regularizada, natural vizinho e, por último, Topo to Raster. A diferença entre os valores observados e estimados pelo método Krigagem esférico foi muito menor do que para os outros quatro métodos, indicando ser esse o interpolador que representa melhor a distribuição espacial da precipitação pluvial média mensal para os dados em estudo.AbstractThis work had the main objective to compare the performance of five methods of interpolation’s style, inverse of the distance’s weight (IDW, round Krigagem, natural neighbor , regularized Spline and Top to rater. Therefore, average monthly rainfall in a period 30 years (1972 the 2002, together with the results of Sytem Hidrological Information ( Hidroweb of National Water Agency (ANA were used around and next of Itapemirim hidrological basin river, southern state of Espirito Santo. The results showed the round Krigagem the lowst Medin Square Mistake (EQM, Efficient percent (EF%, Absolute Medium Mistake (MAE, Determination modulus (r2 and Standard Estimation Mistake (EEP, followed to IDW, regulated Spline, neighbor natural and for last Top to rater. Nonetheless, the difference between the

  3. EVALUATION OF THE FACTOR ANALYSIS TECHNIQUE IN THESES AND DISSERTATIONS IN SOME HIGHER EDUCATION INSTITUTIONS EVALUACIÓN DEL EMPLEO DE LA TÉCNICA DE ANÁLISIS FACTORIAL EN TESIS Y TESINAS DE ALGUNAS INSTITUCIONES DE ENSEÑANZA SUPERIOR AVALIAÇÃO DO EMPREGO DA TÉCNICA DE ANÁLISE FATORIAL EM TESES E DISSERTAÇÕES DE ALGUMAS INSTITUIÇÕES DE ENSINO SUPERIOR

    Directory of Open Access Journals (Sweden)

    Leandro Campi Prearo

    2013-01-01

    Full Text Available This paper is part of a large study to assess the adequacy of using multivariate statistical techniques in theses and dissertations at some higher education institutions in the marketing area of consumer behavior between 1997 and 2006. This paper focuses on factor analysis, a technique with great potential for use in marketing studies. The objective of this paper was  to analyze the adequacy of this technique for the requirements of research problems presented in these theses and dissertations as well as to measure the success level in terms of the assumptions. Overall, results suggest the need for more involvement by the researchers to verify all the theoretical precepts for the application of the factor analysis technique.Este artículo forma parte de un amplio estudio de evaluación de la adecuación del uso de técnicas estadísticas multivariadas en tesis y tesinas de algunas instituciones de enseñanza superior, entre 1997 y 2006, en el área de marketing y con la temática del comportamiento del consumidor. En este artículo se enfoca el Análisis Factorial, una técnica con gran potencial de uso en estudios de marketing. El objetivo de este trabajo fue el análisis de la adecuación del empleo de esa técnica a las necesidades de los problemas de investigación presentados en las tesis y tesinas y cotejar el nivel de  acierto al atender sus premisas. De forma general, los resultados sugieren la necesidad de un aumento del compromiso de los investigadores en la  verificación de todos los preceptos teóricos de aplicación de la técnica de Análisis Factorial.Este artigo faz parte de um amplo estudo que pretende avaliar a adequação do uso de técnicas estatísticas multivariadas em teses e dissertações de algumas instituições de ensino superior, entre 1997 e 2006,  na área de marketing, dedicadas à temática do comportamento do consumidor. Nele focaliza-se a Análise Fatorial, uma técnica com grande potencial

  4. Characterization of array scintillation detector for follicle thyroid 2D imaging acquisition using Monte Carlo simulation; Caracterizacao de uma matriz detectora cintiladora para aquisicao de imagem 2D da regiao folicular da glandula tireoide por emissao radioativa usando simulacao Monte Carlo

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Carlos Borges da

    2007-05-15

    The image acquisition methods applied to nuclear medicine and radiobiology are a valuable research study for determination of thyroid anatomy to seek disorders associated to follicular cells. The Monte Carlo (MC) simulation has also been used in problems related to radiation detection in order to map medical images since the improvement of data processing compatible with personnel computers (PC). This work presents an innovative study to find out the adequate scintillation inorganic detector array that could be coupled to a specific light photo sensor, a charge coupled device (CCD) through a fiber optic plate in order to map the follicles of thyroid gland. The goal is to choose the type of detector that fits the application suggested here with spatial resolution of 10 {mu}m and good detector efficiency. The methodology results are useful to map a follicle image using gamma radiation emission. A source - detector simulation is performed by using a MCNP4B (Monte Carlo for Neutron Photon transport) general code considering different source energies, detector materials and geometries including pixel sizes and reflector types. The results demonstrate that by using MCNP4B code is possible to searching for useful parameters related to the systems used in nuclear medicine, specifically in radiobiology applied to endocrine physiology studies to acquiring thyroid follicles images. (author)

  5. Employment of MCNP in the study of TLDS 600 and 700 seeking the implementation of radiation beam characterization of BNCT facility at IEA-R1; Emprego do MCNP no estudo dos TLDS 600 e 700 visando a implementacao da caracterizacao do feixe de irradiacao da instalacao de BNCT do IEA-R1

    Energy Technology Data Exchange (ETDEWEB)

    Cavalieri, Tassio Antonio

    2013-07-01

    Boron Neutron Capture Therapy, BNCT, is a bimodal radiotherapy procedure for cancer treatment. Its useful energy comes from a nuclear reaction driven by impinging thermal neutron upon Boron 10 atoms. A BNCT research facility has been constructed in IPEN at the IEA-R1 reactor, to develop studies in this area. One of its prime experimental parameter is the beam dosimetry which is nowadays made by using activation foils, for neutron measurements, and TLD 400, for gamma dosimetry. For mixed field dosimetry, the International Commission on Radiation Units and Measurements, ICRU, recommends the use of pair of detectors with distinct responses to the field components. The TLD 600/ TLD 700 pair meets this criteria, as the amount of {sup 6}Li, a nuclide with high thermal neutron cross section, greatly differs in their composition. This work presents a series of experiments and simulations performed in order to implement the mixed field dosimetry based on the use of TLD 600/TLD 700 pair. It also intended to compare this mixed field dosimetric methodology to the one so far used by the BNCT research group of IPEN. The response of all TLDs were studied under irradiations in different irradiation fields and simulations, underwent by MCNP, were run in order to evaluate the dose contribution from each field component. Series of repeated irradiations under pure gamma field and mixed field neutron/gamma field showed differences in the TLD individual responses which led to the adoption of a Normalization Factor. It has allowed to overcome TLD selection. TLD responses due to different field components and spectra were studied. It has shown to be possible to evaluate the relative gamma/neutron fluxes from the relative responses observed in the two Regions of Interest, ROIs, from TLD 600 and TLD 700. It has also been possible to observe the TLD 700 response to neutron, which leads to a gamma dose overestimation when one follows the ICRU recommended mixed field dosimetric procedure. Dose response curves were obtained for the distinct types of TLDs for pure gamma and mixed fields. This work recommends the TLD 600/TLD 700 pair methodology for mixed field dosimetry, due to present a better precision than the one based on TLD 400, however one has to be careful to avoid gamma dose super estimation. (author)

  6. Metallogenetic characterization of granitoid rocks through geochemical prospection: the Lagoa Real example related to uranium mineralization in Bahia state, Brazil; Caracterizacao metalogenetica de corpos gratinoides atraves de prospeccao geoquimica: o exemplo da suite intrusiva Lagoa Real relacionada a mineralizacoes de uranio no Estado da Bahia

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, J.E., E-mail: cprmsa@bahianet.com.br [Servico Geologico do Brasil (GEREMI/SUREG/SA/CPRM), Salvador, BA (Brazil)

    2011-07-01

    Within a broad metallogenetic evaluation program carried out by CPRM - Geological Survey of Brazil in covenant with the CBPM - Companhia Baiana de Pesquisa Mineral in the central part of the Sao Francisco Craton, the Lagoa Real granitoid rocks was one of the selected targets. The work included geochemical exploration supplemented by follow-in survey and integrated 1:200.000 scale geochemical cartography. The Lagoa Real granitoid was recognized with composition ranging from monzogranitic to alcaligranitic type. The geochemical surveying led to the definition of the metallogenetic specialization of the granitoid rock, with characteristic geochemical and mineralogic associations. These associations are related to uranium mineralization. The genetic model using stream sediment and pan concentrate data, show similarity with the metallogenetic model of zonal partitioning proposed by Routhier (1963), for plutonogenic lode deposits with potential for Sn, W, Nb, Be, REE, Au, and U. In this work emphasis is given to the importance of the integrated use of different prospective methods toward the evaluation of granitoid systems, particularly the combination of geochemical surveying methods with results for a better understanding of the geologic and metallogenetic settings. (author)

  7. GRAU DA PRÁXIS DA GESTÃO DA RESPONSABILIDADE AMBIENTAL PRATICADA POR USINAS SUCROALCOOLEIRAS

    Directory of Open Access Journals (Sweden)

    Renata Longo

    2014-12-01

    gerencial (PCDA foi o Action que apresentou maior grau de aderência. Há uma concordância acentuada às características fundamentais do ciclo gerencial na Gestão da Responsabilidade Socioambiental.

  8. Papel da vitamina B12 na patogenia da mielose funicular

    Directory of Open Access Journals (Sweden)

    Horacio M. Canelas

    1965-12-01

    Full Text Available Foi estudada a absorção da vitamina B12 radioativa em 29 casos de mielose funicular. O diagnóstico baseou-se na clássica sintomatologia neu- rológica e na presença de acloridria gástrica e eventuais alterações hemato-lógicas. As manifestações neurológicas foram avaliadas de modo semiquan-titativo e correlacionadas com os resultados do teste de excreção urinária da vitamina B12. Não foi verificada correlação significante da absorção da vitamina B12, quer com a sintomatologia nuerológica total, quer com as síndromes periférica e funicular dorsal. Contudo, foi encontrada significante correlação negativa entre a síndrome piramidal e a absorção da vitamina B12. Os resultados são confrontados com o papel desempenhado pela vitamina B12 na síntese das bainhas de mielina e do ácido ribonuclêico, sendo salientada a importância dêste último para a vida das células nervosas e dos longos axônios.

  9. Estimative of the nutritional value of agroindustrial byproducts by using in vitro gas production techniqueEstimativa do valor nutricional de subprodutos agroindustriais pelo uso da técnica de produção de gás

    Directory of Open Access Journals (Sweden)

    Elzânia Sales Pereira

    2013-03-01

    Full Text Available The objective of this work was to determine the total carbohydrates fractions and to estimate the digestion rate of non-fibrous carbohydrates of agroindustrial byproducts by using the gas production technique. The agroindustrial byproducts evaluated were the following: cashew, passion fruit, pineapple, barbados cherry, annatto and melon, and each sample was incubated in quadruplicate. After mixing all contents thoroughly, the bottles were placed in an incubator at 39ºC, and connecting the lid of each bottle to a pressure sensitive switch, a solenoid valve and a vent stem connector. Gas pressure measurements were made at 0, 3, 6, 12, 15, 18, 22, 26, 30, 34, 40, 48, 60, 72, 96 e 120 hours post-inoculation. Blanks and an internal standard were included to enable adjustments in variation among readings. There was a high variation in nutritional composition of agroindustry byproducts, that cashew and annato presented the highest protein contents (159.3 and 135.3 g/kg of dry matter, respectively. Mellon and cashew presented the lowest values of total gas production (9.60 and 12.85 mL, respectively; and annato, pineapple and passion fruit presented highest gas volume (32.80; 28.16 and 22.54 mL, respectively, being the greatest percentages of phases from B2 fraction (64.27; 81.25 and 67.49%, respectively. Among the byproducts, pineapple and annatto stand out for the highest contribution of fibrous carbohydrate for total gas production, being B2 the main energy source for microbial growth, which is degraded at a slower rate than non-fibrous carbohydrate.Os objetivos deste trabalho foram determinar as frações de carboidratos totais e estimar a taxa de digestão dos carboidratos não-fibrosos de subprodutos agroindustriais, utilizando a técnica de produção de gás. Os subprodutos agroindustriais avaliados foram: caju, maracujá, abacaxi, acerola, urucum e melão, sendo cada amostra incubada em quadriplicata. Após mistura minuciosa de todos os conte

  10. Cogeneration techniques; Les techniques de cogeneration

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1999-10-01

    This dossier about cogeneration techniques comprises 12 parts dealing successively with: the advantages of cogeneration (examples of installations, electrical and thermal efficiency); the combustion turbine (principle, performances, types); the alternative internal combustion engines (principle, types, rotation speed, comparative performances); the different configurations of cogeneration installations based on alternative engines and based on steam turbines (coal, heavy fuel and natural gas-fueled turbines); the environmental constraints of combustion turbines (pollutants, techniques of reduction of pollutant emissions); the environmental constraints of alternative internal combustion engines (gas and diesel engines); cogeneration and energy saving; the techniques of reduction of pollutant emissions (pollutants, unburnt hydrocarbons, primary and secondary (catalytic) techniques, post-combustion); the most-advanced configurations of cogeneration installations for enhanced performances (counter-pressure turbines, massive steam injection cycles, turbo-chargers); comparison between the performances of the different cogeneration techniques; the tri-generation technique (compression and absorption cycles). (J.S.)

  11. Publicidade e ética: um estudo da construção da imagem da mulher

    Directory of Open Access Journals (Sweden)

    Elizabeth Moraes Gonçalves

    2010-02-01

    Full Text Available O texto propõe uma reflexão sobre a ética da responsabilidade na publicidade veiculada nas revistas Claudia e Nova. Trata-se de uma pesquisa descritiva, resultante da leitura dos anúncios selecionados, subsidiada por teóricos da Análise do Discurso da linha francesa, que busca averiguar como a mulher é representada. Constatou-se que no contexto da sociedade contemporânea o retrato da mulher como sedutora ainda está presente, mesmo que em vários momentos ela apareça como protagonista de sua própria vida.

  12. Variedades da Democracia no Brasil

    Directory of Open Access Journals (Sweden)

    Fernando Bizzarro

    Full Text Available Resumo Neste artigo apresentamos resultados coletados pelo projeto Variedades da Democracia para o Brasil. Descrevemos a evolução histórica da democracia brasileira entre 1900 e 2015 enfocando seus cinco principais componentes (eleitoral, liberal, participativo, deliberativo e igualitário e duas dimensões adjacentes ao regime (corrupção e partidos políticos. Por fim, nós comparamos os dados para o Brasil com resultados obtidos para outros países da América do Sul. A análise dos dados aponta: a. a existência de uma trajetória “em espiral” dos regimes políticos no Brasil, na qual novas experiências democráticas tendem a superar experiências anteriores em todos os quesitos; b. os avanços e limites da experiência democrática contemporânea em que se combinam bons resultados nos indicadores eleitoral, liberal e deliberativo da democracia, e resultados menos elevados nos componentes igualitário e participativo do regime, bem como em suas dimensões adjacentes.

  13. Ultrasound evaluation of techniques for internal jugular vein puncture in children Avaliação ultra-sonográfica das técnicas de punção da veia jugular interna em crianças

    Directory of Open Access Journals (Sweden)

    Sérgio Tomaz Schettini

    2008-10-01

    Full Text Available PURPOSE: To determine by ultrasound which access and position the child must stay to obtain the best transversal section of the right Internal Jugular Vein (RIJV allowing a safer puncture. METHODS: Three possible accesses to the RIJV, anterior, lateral and posterior, from 57 healthy children, were analyzed through ultrasound images in a sequence of positions of the head, in supine position, with or without a roll under the scapula: head centered in neutral position with and without a roll (NPP and NP; contra lateral rotation with and without a roll (CLRP and CLR, neutral position and the patient raised in 30° in Trendelenburg position (TDG. To analyze the results it was applied one statistic method, with variation analysis to the same individuals. Basic Procedures: Ultrasound evaluation in each one of the proposed positions. RESULTS: The statistical analysis of the results observed that the lateral puncture with the patient in the neutral position, in Trendelemburg without a roll, offers a bigger area in comparison to all the other options of puncture and positioning of the patient (pOBJETIVO: Determinar pelo ultra-som qual o melhor acesso e posicionamento da criança com o intuito de se obter a melhor secção transversal da veia jugular interna direita (VJID, permitindo uma punção com maior segurança. MÉTODOS: Três possíveis acessos a VJID, anterior, lateral e posterior foram analisados pela ultrassonografia em uma sequência de diferentes posições da cabeça, estando o paciente em posição supina com ou sem um coxim sob a escápula; cabeça na posição neutra; (NPP E NP; rotação lateral da cabeça (CLRP e CLR, posição neutra com o paciente em posição de Trendlemburg a 30(0 (TDG. Para analisar os resultados foi aplicado um método estatístico com análise variada sobre os mesmos indivíduos. Procedimentos básicos: Avaliação ultrassonográfica em cada uma das posições propostas. RESULTADOS: Pela análise estatística dos

  14. 76 FR 12627 - Airworthiness Directives; Diamond Aircraft Industries GmbH Models DA 42, DA 42 NG, and DA 42 M-NG...

    Science.gov (United States)

    2011-03-08

    ... Industries GmbH Models DA 42, DA 42 NG, and DA 42 M-NG Airplanes AGENCY: Federal Aviation Administration (FAA... on Diamond aeroplanes, the majority of which were DA 40. In additional, at least 18 doors have been... conditions) while the aeroplane was parked. All DA 40 and DA 42 aeroplanes have a system installed that...

  15. 76 FR 27861 - Airworthiness Directives; Diamond Aircraft Industries GmbH Models DA 42, DA 42 NG, and DA 42 M-NG...

    Science.gov (United States)

    2011-05-13

    ... Airworthiness Directives; Diamond Aircraft Industries GmbH Models DA 42, DA 42 NG, and DA 42 M-NG Airplanes... on Diamond aeroplanes, the majority of which were DA 40. In additional, at least 18 doors have been... conditions) while the aeroplane was parked. All DA 40 and DA 42 aeroplanes have a system installed that...

  16. Ensino da música

    OpenAIRE

    Vieira, Maria Helena

    2017-01-01

    O papel da Igreja Católica no desenvolvimento do ensino da música em Portugal é inquestionável. Neste texto descreve-se como a música e o seu ensino antecederam a própria fundação da nacionalidade no território que é hoje Portugal, e como a Igreja Católica teve um papel preponderante, até aos nossos dias, no desenvolvimento desse ensino e na criação de estruturas pedagógicas que permitiram a aprendizagem musical ao longo dos séculos. Primeiro nas escolas monacais, depois nas sés catedrais, e ...

  17. O LUGAR DA MORADIA SOCIAL

    OpenAIRE

    Daniela das Neves Alvarenga; Paulo Romano Reschilian

    2017-01-01

    Objetivou-se com este artigo analisar o processo de segregação socioespacial nas cidades industriais europeias, com olhar na localização da moradia operária no espaço urbano. A partir desta análise, parte-se para a construção do cenário no Brasil, apontando as origens da habitação social nas cidades industriais, com enfoque na inserção urbana da moradia produzida pela iniciativa privada e pelo Estado até os dias atuais, culminando na produção de interesse social vinculada ao programa habitaci...

  18. Terapia cognitivo-comportamental da fobia social

    OpenAIRE

    Ito,Lígia M; Roso,Miréia C; Tiwari,Shilpee; Kendall,Philip C; Asbahr,Fernando R

    2008-01-01

    OBJETIVO: Este artigo revisa aspectos relevantes da fobia social e os estágios de tratamento através da terapia cognitivo-comportamental em crianças, adolescentes e adultos. MÉTODO: A partir do banco de dados Medline, realizou-se revisão da literatura publicada a respeito do tratamento da fobia social por meio da terapia cognitivo-comportamental. RESULTADOS: Revisão da literatura sugere que a fobia social é uma condição prevalente e crônica, caracterizada por inibição social e timidez excessi...

  19. Renormalization group decimation technique for disordered binary harmonic chains

    International Nuclear Information System (INIS)

    Wiecko, C.; Roman, E.

    1983-10-01

    The density of states of disordered binary harmonic chains is calculated using the Renormalization Group Decimation technique on the displacements of the masses from their equilibrium positions. The results are compared with numerical simulation data and with those obtained with the current method of Goncalves da Silva and Koiller. The advantage of our procedure over other methods is discussed. (author)

  20. O panorama das Drogas no México: da margem da sociedade ao centro da cultura

    Directory of Open Access Journals (Sweden)

    Diana Palaversich

    2013-12-01

    Full Text Available O artigo destaca o percurso das manifestações culturais ligadas ao tráfico de drogas no México, de um lugar marginal, de subcultura, na sociedade mexicana das décadas de 1970 e 1980, expressas principalmente através dos narcocorridos e do narcocine, para um lugar no mainstream cultural mexicano, desde o início do século 21, com destaque especial para a narcoliteratura. O aumento da violência, provocado pela guerra ao narcotráfico, produz uma proliferação da temática nos meios de comunicação e se reflete em áreas da cultura como as artes plásticas e a literatura, produzindo um novo tipo de expressão artística ou narrativa, que tanto pode ser oportunista e contribuir para a banalização da violência do narcotráfico como ser crítica e narrar o impacto individual e coletivo do tráfico de drogas, narrar a desenfreada e violenta realidade mexicana sem cair no estilo da imprensa marrom, do folclore ou dos lugares comuns dos romances de ação.

  1. Cinco discursos da digitalidade audiovisual

    Directory of Open Access Journals (Sweden)

    Gerbase, Carlos

    2001-01-01

    Full Text Available Michel Foucault ensina que toda fala sistemática - inclusive aquela que se afirma “neutra” ou “uma desinteressada visão objetiva do que acontece” - é, na verdade, mecanismo de articulação do saber e, na seqüência, de formação de poder. O aparecimento de novas tecnologias, especialmente as digitais, no campo da produção audiovisual, provoca uma avalanche de declarações de cineastas, ensaios de acadêmicos e previsões de demiurgos da mídia.

  2. CILADAS DA DIFERENÇA

    Directory of Open Access Journals (Sweden)

    Antônio Flávio Pierucci

    1990-12-01

    Full Text Available Este artigo procura analisar os efeitos perversos da apropriação pela esquerda de um tema definidor das tradições de direita, a saber, a diferença. Com base no caso Sears (EUA e no caso Le Pen (França, o autor aponta para as armadilhas racistas e sexistas presentes nos discursos que focalizam e enfatizam a diferença, sobretudo num período histórico de reemergência dos conservadorismos que, por sua vez, se apropriam do argumento da diferença, dirigindo-o contra os próprios movimentos de esquerda.

  3. Cultura da Convergência

    Directory of Open Access Journals (Sweden)

    Rogério Christofoletti

    2008-12-01

    Full Text Available Três idéias já seriam suficientes para que a leitura de “Cultura da Convergência”, de Henry Jenkins, interessasse a jornalistas e pesquisadores da área: a convergência midiática como um processo cultural; o fortalecimento de uma economia afetiva que orienta consumidores de bens simbólicos e criadores midiáticos; a expansão de formas narrativas transmidiáticas.

  4. Análise da qualidade das córneas doadas e do intervalo entre óbito, enucleação e preservação após a implantação de novas normas técnicas e sanitárias em Banco de Olhos Universitário Comparative analysis of the donor cornea quality and of the interval between death and preservation before and after new sanitary and technique rules in a University Eye Bank

    Directory of Open Access Journals (Sweden)

    Fabio Zantut

    2012-12-01

    Full Text Available OBJETIVO: Comparar o intervalo entre o óbito e a enucleação (ΔT-O-E, entre a enucleação e a preservação (ΔT-E-P e a qualidade da córnea antes e após a implantação de novas normas técnicas e sanitárias baseadas na Resolução RDC 347. MÉTODOS: Estudo retrospectivo em que foram avaliados os prontuários dos doadores de córnea do Banco de Tecidos Oculares da Santa Casa de São Paulo, 2 anos antes e 2 anos depois da implementação de novas normas sanitárias. RESULTADOS: Foi observado aumento do número absoluto de 205 para 374 doadores após as mudanças adotadas. Não foi observada diferença estatisticamente significante no Δt-O-E e ΔT-E-P antes e após as mudanças implantadas. Do total de 1.105 córneas doadas, foi observado 388 córneas doadas antes das mudanças e 717 córneas doadas após as mudanças implementadas. Foi observado aumento estatisticamente significante da graduação da qualidade da córnea doada de 1,76 ± 0,90 para 1,94 ± 0,88 após a implementação das novas normas da Resolução. CONCLUSÃO: Após as mudanças técnicas e sanitárias exigidas pela Resolução 347, houve grande aumento no número de córneas doadas, captadas e preservadas. O Banco de Tecidos Oculares não diminuiu os ΔT O-E e ΔT E-P. A qualidade da córnea apresentou-se inferior após as mudanças realizadas no setor.PURPOSE: To compare the interval between death and enucleation (ΔT-O-E, between enucleation and preservation (ΔT-E-P and the quality of the cornea before and after the implantation of new technique and sanitary rules. METHODS: A retrospective study that evaluated the records of cornea donors in Sao Paulo's Santa Casa Eye Tissue Bank 2 years before and 2 years after the implementation new sanitary rules. RESULTS: An increase was observed in the absolute number of 205 to 374 donors following the adopted changes. There was no statistically significant difference in Δt-O-E and ΔT-E-P before and after the implemented

  5. da Vinci decoded: does da Vinci stereopsis rely on disparity?

    Science.gov (United States)

    Tsirlin, Inna; Wilcox, Laurie M; Allison, Robert S

    2012-11-01

    In conventional stereopsis, the depth between two objects is computed based on the retinal disparity in the position of matching points in the two eyes. When an object is occluded by another object in the scene, so that it is visible only in one eye, its retinal disparity cannot be computed. Nakayama and Shimojo (1990) found that a precept of quantitative depth between the two objects could still be established for such stimuli and proposed that this precept is based on the constraints imposed by occlusion geometry. They named this and other occlusion-based depth phenomena "da Vinci stereopsis." Subsequent research found quantitative depth based on occlusion geometry in several other classes of stimuli grouped under the term da Vinci stereopsis. However, Nakayama and Shimojo's findings were later brought into question by Gillam, Cook, and Blackburn (2003), who suggested that quantitative depth in their stimuli was perceived based on conventional disparity. In order to understand whether da Vinci stereopsis relies on one type of mechanism or whether its function is stimulus dependent we examine the nature and source of depth in the class of stimuli used by Nakayama and Shimojo (1990). We use three different psychophysical and computational methods to show that the most likely source for depth in these stimuli is occlusion geometry. Based on these experiments and previous data we discuss the potential mechanisms responsible for processing depth from monocular features in da Vinci stereopsis.

  6. Efeitos da transformação de uma variável com distribuição normal em sua inversa sobre os parâmetros de sua distribuição usando técnicas de Monte Carlo Effects of transforming a normally distributed variable into its inverse on parameters of the distribution using Monte Carlo techniques

    Directory of Open Access Journals (Sweden)

    Mirella Leme Franco Geraldini Sirol

    2006-06-01

    Full Text Available Foram realizados quatro estudos de simulação para verificar a distribuição de inversas de variáveis com distribuição normal, em função de diferentes variâncias, médias, pontos de truncamentos e tamanhos amostrais. As variáveis simuladas foram GMD, com distribuição normal, representando o ganho médio diário e DIAS, obtido a partir da inversa de GMD, representando dias para se obter determinado peso. Em todos os estudos, foi utilizado o sistema SAS® (1990 para simulação dos dados e para posterior análise dos resultados. As médias amostrais de DIAS foram dependentes dos desvios-padrão utilizados na simulação. As análises de regressão mostraram redução da média e do desvio-padrão de DIAS em função do aumento na média de GMD. A inclusão de um ponto de truncamento entre 10 e 25% do valor da média de GMD reduziu a média de GMD e aumentou a de DIAS, quando o coeficiente de variação de GMD foi superior a 25%. O efeito do tamanho dos grupos nas médias de GMD e DIAS não foi significativo, mas o desvio-padrão e CV amostrais médios de GMD aumentaram com o tamanho do grupo. Em virtude da dependência entre a média e o desvio-padrão e da variação observada nos desvios-padrão de DIAS em função do tamanho do grupo, a utilização de DIAS como critério de seleção pode diminuir a acurácia da variação. Portanto, para a substituição de GMD por DIAS, é necessária a utilização de um método de análise robusto o suficiente para a eliminação da heterogeneidade de variância.Four simulation studies were conducted to verify the distribution of the inverse of variables with normal distribution, relatively to variances, averages, truncation points and sample sizes. The variables simulated were GMD, with normal distribution and representing average daily gain, and DIAS defined as a multiple of the inverse of GMD and representing days to reach a fixed body weight. The SAS® (1990 system was used, for simulation

  7. Efeito da urina de vaca no estado nutricional da alface

    Directory of Open Access Journals (Sweden)

    Nelson Licínio C. de Oliveira

    2010-08-01

    Full Text Available Existem diversos relatos da utilização da urina de vaca em hortaliças, todavia sua eficácia carece de comprovação. Objetivou-se avaliar o efeito da urina de vaca no estado nutricional da alface. O experimento foi constituído de 12 tratamentos, esquema de parcelas subdivididas, em blocos ao acaso, com quatro repetições. Nas parcelas foram alocadas as vias de aplicação (solo ou foliar e nas subparcelas as concentrações das soluções (0,00; 0,25; 0,50; 0,75; 1,00 e 1,25% v/v. Aplicou-se 60 mL de solução/planta, divididos em cinco aplicações de 5; 5; 10; 20 e 20 mL/planta, aos 7, 14, 21, 28 e 35 após o transplante, respectivamente. Durante o ciclo avaliou-se o índice SPAD e na colheita a massa da matéria seca de cabeça (MSCA e os teores de N, P, K, Ca, Mg, S, Na, Zn, Fe, Mn, Cu e B na matéria seca das folhas (MSF, caule (MSC e raízes (MSR. Em ambas as vias de aplicação o índice SPAD apresentou incremento linear às concentrações e resposta quadrática ao longo do tempo. A MSCA teve comportamento linear às concentrações, com aumento de 25,9 e 35,4% nas aplicações via foliar e solo, respectivamente. Não houve efeito de concentrações sobre teores de nutrientes na MSF e MSC. Na MSR, via solo, os teores de P e K apresentaram pontos de máximo enquanto Fe e Mn de mínimo; o Na apresentou incremento linear às concentrações via foliar. Os efeitos da urina sobre o crescimento da alface provavelmente são devidos a fatores outros que não somente a quantidade de nutrientes veiculados nas soluções.

  8. Implantação de Kanban como técnica auxiliar do planejamento e controle da produção: um estudo de caso em fábrica de médio porte Kanban system implantation as a helping technique of the production planning and control: a case study at a medium-size factory

    Directory of Open Access Journals (Sweden)

    Ethel Cristina Chiari da Silva

    1995-04-01

    Full Text Available O presente artigo relata a experiência da implantação do sistema Kanban em uma célula-piloto, realizada em uma fábrica de médio porte do setor metal mecânico em São Carlos - SP. A intenção da implantação do sistema kanban surgiu como expectativa de auxílio ao Planejamento e Controle da Produção, a fim de buscar padrões tecnológicos de gestão mais adequados à realidade mundial. Para implantação do sistema Kanban criou-se um ambiente Just-in-Time na célula piloto a fim de gerar um sistema consistente e também um modelo de aprendizado para a fábrica. Trabalhou-se com operários de baixa escolaridade e elaborou-se todo o material didático utilizado nas atividades de treinamento. Após um ano e meio (1130 horas de trabalho na fábrica, pôde-se chegar a resultados altamente satisfatórios, tanto qualitativos quanto quantitativos.The present article reports the experience of the Kanban system implantation on a pilot cell at a medium-size factory in the mechanical metal sector in São Carlos - SP. The reason for implanting the Kanban system arose in the hope of aiding Production Planning and Control in order to seek technological standards of administration more adequade to the world reality. For the kanban system implantation a Just-in-Time environment has been created at the pilot cell to generate a consistent system as well as a learning model for the factory. The work has been done with employees who have had low schooling and all didactical material used has been elaborated using training activities. After one and a half years' (1130 hours work at the factory, highly satisfactory results - both qualitative and quantitative - have been attained.

  9. Detection of different Staphylococcus aureus strains in bovine milk from subclinical mastitis using PCR and routine techniques Detecção de diferentes cepas de Staphylococcus aureus de mastite bovina subclínica através da técnica de PCR e técnicas tradicionais

    Directory of Open Access Journals (Sweden)

    Olney Vieira-da-Motta

    2001-03-01

    Full Text Available Contamination of fresh milk with Staphylococcus aureus was assessed comparatively through routine phenotypic (coagulase tube test and coagulase slide test and genotypic (PCR screening of 128 S. aureus strains isolated from 555 milk samples. These samples were collected from 362 cows with subclinical mastitis, hosted in different dairy herds at various locations of the Northern and Northeastern rural areas of the State of Rio de Janeiro, 39.7% of which were CMT-positive. All S. aureus isolates tested positive for the presence of the coagulase gene by PCR and the isolates could be grouped into four distinct classes according to the size of the PCR product. The strains also yielded variable results when assayed with coagulase test. Taken together, these data indicate the existence of extensive polymorphism at the coagulase gene locus in the genus Staphylococcus and exemplifies the extent of molecular and phenotypic heterogeneity associated with the strains circulating in rural herds.Quinhentas e cinqüenta e cinco amostras de leite, provenientes de 362 vacas com mastite subclínica em diferentes propriedades rurais do Estado do Rio de Janeiro, Brasil, de 1995 a 1997, foram submetidas ao teste "Califórnia Mastitis Test" (CMT. 39,7% das amostras foram positivas, das quais foram isoladas 128 cepas de Staphylococcus aureus. Todas as cepas isoladas foram positivas para o gene da coagulase utilizando a técnica de PCR, todavia, resultados de coagulase através das técnicas em tubo e "coagulase slide test" foram variáveis. Após a amplificação do gen de coagulase através da técnica de PCR utilizando iniciadores específicos para o referido gen, fragmentos com diferentes pesos moleculares foram vistos através de análise em gel de agarose, sugerindo a ocorrência de polimorfismo genético. O estudo também sugere a ocorrência de diferentes cepas da bactéria atuando nos rebanhos leiteiros causando mastite bovina.

  10. A identidade à flor da pele: etnografia da prática da tatuagem na contemporaneidade

    Directory of Open Access Journals (Sweden)

    Andrea Lissett Pérez

    2006-04-01

    Full Text Available No presente artigo, realiza-se uma descrição etnográfica da prática da tatuagem na contemporaneidade, a partir de uma perspectiva que prioriza as noções da prática, das interações e das experiências vividas durante o processo de ser tatuado. A reflexão tenta reconstruir uma visão total da prática da tatuagem que abrange o mundo subjetivo e as dinâmicas sociais como partes constitutivas desse ato. Entre as idéias conclusivas estão, de um lado, o surgimento de uma nova normalidade estética e vivencial no seio da sociedade ocidental e, de outro, a configuração de uma nova subjetividade, a dos "tatuados", como um processo interativo, inovador, emotivo e reflexivo, em que o corpo se converte em uma forma de expressão e construção do sujeito.This article provides a descriptive account of contemporary tattooing, based on a perspective that prioritizes the notion of practice, as well as the interactions and experiences involved in the process of being tattooed. The analysis attempts to rebuild a holistic view of tattooing, combining subjective processes and social dynamics as equally constitutive parts of this activity. Among the conclusions reached are: (a the emergence of tattooing as a new aesthetic norm and a lived experience at the heart of the western society; and (b the configuration of a new subjectivity, the ‘tattooed,’ as an interactive, innovative, emotional and reflexive process in which the body is converted into a form of expressing and constructing the subject.

  11. Etiologia e perfil de sensibilidade antimicrobiana dos isolados bacterianos da mastite em pequenos ruminantes e concordância de técnicas empregadas no diagnóstico Etiology and profile of antimicrobial sensitivity of bacteria from small ruminant mastitis and relationship of diagnostic techniques

    Directory of Open Access Journals (Sweden)

    Rodolfo de M. Peixoto

    2010-09-01

    Full Text Available A mastite é a inflamação da glândula mamária que acomete raças de aptidão leiteira como também aquelas voltadas para produção de carne. Esta enfermidade ocasiona sérias alterações na produção de leite e na sua qualidade, redução no ganho de peso e mortalidade de cordeiros. O presente estudo teve por objetivo conhecer os principais agentes causadores de mastite em ovinos e caprinos, bem como a sua susceptibilidade aos agentes antimicrobianos, além de avaliar o grau de concordância entre testes diagnósticos. Foram visitadas 25 propriedades durante a realização do experimento, sendo criatórios de caprinos, ovinos e rebanhos mistos, nos estados de Pernambuco e Bahia. Coletou-se leite de 439 caprinos e 76 ovinos. Foi realizada lactocultura, o California Mastitis Test (CMT e o teste de sensibilidade aos antimicrobianos. Além disso, determinou-se o grau de concordância entre os testes diagnósticos empregados. Foi constatada uma maior freqüência de Staphylococcus spp. nos casos de mastite em caprinos e ovinos, sendo observado ainda, isolados de Streptococcus spp., Corynebacterium spp. e bacilos gram negativos (BGN. Os isolados apresentaram alta sensibilidade aos antimicrobianos testados, sendo o menor percentual de sensibilidade observado para o ácido nalidíxico. Em relação ao diagnóstico da mastite caprina, a análise comparativa entre o exame microbiológico e o CMT demonstrou um grau de concordância igual a K=0,17, enquanto que para a espécie ovina, este valor foi de K=0,22. A utilização do CMT para o diagnóstico da mastite subclínica em cabras e ovelhas deverá ser associado à técnica da lactocultura.Mastitis is an inflammation of mammary gland, that are important in milking breed as well in meat ones. It is associated with serious reduction in milk production and quality, lambs weight gain reduction and mortality The goal of this work was determine the major etiologic agents of goat and sheep mastitis, as

  12. Leonardo da Vinci and the Downburst.

    Science.gov (United States)

    Gedzelman, Stanley David

    1990-05-01

    Evidence from the drawings, experiments, and writings of Leonardo da Vinci are presented to demonstrate that da Vinci recognized and, possibly, discovered the downburst and understood its associated airflow. Other early references to vortex flows resembling downbursts are mentioned.

  13. Tratamento da dor em queimados

    Directory of Open Access Journals (Sweden)

    Rodrigo José Alencar de Castro

    2013-02-01

    Full Text Available JUSTIFICATIVA E OBJETIVOS: Apesar dos avanços, ainda é observado manejo analgésico inadequado dos pacientes com queimaduras. O objetivo desta revisão foi coletar dados sobre tratamento da dor em queimados. CONTEÚDO: Foi feita revisão sobre os mecanismos de dor, avaliação do paciente com queimadura e o tratamento farmacológico e não farmacológico. CONCLUSÕES: O manejo da dor em pacientes vítimas de queimaduras ainda é um desafio por parte da equipe multiprofissional. A avaliação frequente e contínua da resposta apresentada pelo paciente é muito importante, tendo em vista os vários momentos por que passa o paciente internado em decorrência de uma queimadura, além de uma terapêutica combinada com medicações analgésicas e medidas não farmacológicas. Entender a complexidade de alterações fisiopatológicas, psicológicas e bioquímicas apresentadas por um paciente em tratamento de queimadura é o primeiro passo para alcançar o sucesso no seu manejo analgésico.

  14. Šmakuláda

    Czech Academy of Sciences Publication Activity Database

    Ireinová, Martina

    2017-01-01

    Roč. 100, č. 3 (2017), s. 189-191 ISSN 0027-8203 R&D Projects: GA ČR(CZ) GA16-04648S Keywords : šmakuláda * šmak * Czech National Corpus * database Neomat * etymology Subject RIV: AI - Linguistics OBOR OECD: Linguistics

  15. Smart AD and DA Converters

    NARCIS (Netherlands)

    Roermund, van A.H.M.; Hegt, J.A.; Harpe, P.J.A.; Radulov, G.I.; Zanikopoulos, A.; Doris, K.; Quinn, P.J.

    2005-01-01

    In this paper, a concept is proposed to solve the problems related to the embedding of AD and DA converters in system-on-chips, FPGAs or other VLSI solutions. Problems like embedded testing, yield, reliability and reduced design space become crucial bottlenecks in the integration of high-performance

  16. O LUGAR DA MORADIA SOCIAL

    Directory of Open Access Journals (Sweden)

    Daniela das Neves Alvarenga

    2017-01-01

    Full Text Available Objetivou-se com este artigo analisar o processo de segregação socioespacial nas cidades industriais europeias, com olhar na localização da moradia operária no espaço urbano. A partir desta análise, parte-se para a construção do cenário no Brasil, apontando as origens da habitação social nas cidades industriais, com enfoque na inserção urbana da moradia produzida pela iniciativa privada e pelo Estado até os dias atuais, culminando na produção de interesse social vinculada ao programa habitacional Minha Casa, Minha Vida (MCMV. Por fim, será feita uma análise comparativa da localização das vilas operárias em São José dos Campos, com a inserção urbana dos empreendimentos produzidos pelo Estado.

  17. Cultura da Convergência

    Directory of Open Access Journals (Sweden)

    Rogério Christofoletti

    2008-12-01

    Full Text Available Three ideas would suffice for the reading of “Cultura da Convergência” (Culture of Convergence by Henry Jenkins to be of interest to journalists and researchers in the area: media convergence as a cultural process; the strengthening of an emotional economy which guides consumers of symbolic goods and media creators; the expansion of trans-media narrative forms.

  18. Cultura da Convergência

    Directory of Open Access Journals (Sweden)

    Rogério Christofoletti

    2011-02-01

    Full Text Available Three ideas would suffice for the reading of “Cultura da Convergência” (Culture of Convergence by Henry Jenkins to be of interest to journalists and researchers in the area: media convergence as a cultural process; the strengthening of an emotional economy which guides consumers of symbolic goods and media creators; the expansion of trans-media narrative forms.

  19. Surface science techniques

    CERN Document Server

    Bracco, Gianangelo

    2013-01-01

    The book describes the experimental techniques employed to study surfaces and interfaces. The emphasis is on the experimental method. Therefore all chapters start with an introduction of the scientific problem, the theory necessary to understand how the technique works and how to understand the results. Descriptions of real experimental setups, experimental results at different systems are given to show both the strength and the limits of the technique. In a final part the new developments and possible extensions of the techniques are presented. The included techniques provide microscopic as well as macroscopic information. They cover most of the techniques used in surface science.

  20. Training techniques for industry

    International Nuclear Information System (INIS)

    Jones, D.W.

    1978-01-01

    The advantages and disadvantages of commonly used training techniques in relation to cost-effective, prevention-oriented Quality Assurance are examined. Important questions are whether training techniques teach cost effectiveness and whether the techniques are, themselves, cost effective. To answer these questions, criteria for evaluating teaching techniques for cost effectiveness were developd, and then commonly used techniques are evaluated in terms of specific training program objectives. Motivation of personnel is also considered important to the success of a training program, and methods are outlined by which recognition of the academic quality of industrial training can be used as a motivational technique

  1. Hanna Krall e os caminhos tortos da memória e da identidade

    OpenAIRE

    Piotr Kilanowski

    2013-01-01

    Neste artigo apresentamos a escritora polonesa de origem judaica Hanna Krall por meio da análise literária do seu romance Sublokatorka (A sublocatária).  O romance, com elementos autobiográficos, apresenta a personalidade cindida de uma menina sobrevivente do Holocausto e discute o tema da identidade polonesa, judaica e judaico-polonesa. Através da observação da memória e do processo de criação da memória, a autora mostra a construção da identidade falsa e a repressão da verdadeira, o comport...

  2. A PROBLEMÁTICA DA BIOPIRATARIA: REFLEXÕES A PARTIR DA GEOPOLÍTICA E DOS DIREITOS DA SOCIOBIODIVERSIDADE

    OpenAIRE

    Nunes, Denise Silva; UFSM; Tybusch, Jerônimo Siqueira; UFSM

    2013-01-01

    O bioimperialismo configura-se como uma característica da geopolítica da atualidade, com alicerces nas estruturas da globalização e do capitalismo. Nesse contexto, a problemática da pesquisa consiste na violação dos direitos dos povos locais e a exploração do meio ambiente, em que o atual sistema internacional de propriedade intelectual contribui para a biopirataria dos recursos naturais, por meio da infiltração, em áreas ricas em diversidade biológica, das grandes corporações, multinacionais...

  3. Alternative methodologies in the integrated control of urban mosquito larvae: water surface obliteration techniques Metodologías alternativas en el control integrado de larvas de mosquitos urbanos: técnicas de obliteración de lámina de agua Metodologias alternativas no controlo integrado de larvas de mosquitos nas áreas urbanas: técnicas de obliteração da superfície da água

    Directory of Open Access Journals (Sweden)

    Roger Eritja

    2012-12-01

    Full Text Available The public health risk associated to mosquitoes has increased in Spain by the introduction of the Asian Tiger Mosquito (Aedes albopictus which is a well-known disease vector. Integrated control methodologies basically rely on larviciding by weekly applications of microbial biocides that have no residual effect. In some special cases, such as swimming pools in abandoned estates, this weekly schedule cannot be achieved due to difficulties of access and operational reasons. In these circumstances, there are no appropriate biocidal options except for Insect Growth Regulators (IGR, which do not provide more than a few weeks of residual efficiency. We present here the practical application of a well-known technique for controlling mosquito larvae in urban environments by altering the water/air interface. The adding to the water surface of a thick layer of beads made from inert, floating materials is described. The layer of beads impedes oviposition and adversely affects the breathing of the larvae. This technique avoids the regular application of chemical pesticides, as well as providing improved sustainability and higher efficiency times. Caution notes and side effects are also discussed.Los mosquitos son un riesgo relevante para la salud pública que se ha visto incrementado con la llegada de Aedes albopictus, el mosquito tigre, potencial transmisor de varias enfermedades. El método de elección para su control es la eliminación de las larvas acuáticas mediante biocidas de origen biológico, que se realiza semanalmente debido a su nula persistencia. En determinados puntos donde esta periodicidad no puede mantenerse, como piscinas en fincas abandonadas, no existen opciones biocidas adecuadas más residuales exceptuando los inhibidores del crecimiento, que sin embargo no suelen proporcionar una residualidad superior a unas pocas semanas (de dos a cuatro. Se presenta la aplicación práctica de una técnica de control de larvas de mosquito en medios

  4. Euclides da Cunha nas vascas da modernidade // Euclides da Cunha in the throes of modernity

    Directory of Open Access Journals (Sweden)

    Walnice Nogueira Galvão

    2017-06-01

    Full Text Available Euclides da Cunha embraced the role of posthumous champion of the backlanders slaughtered by the Brazilian army during the Canudos War. He claimed to have written an “avenging book”. Coming of age at the turn of the century, his work would bear witness to a Modernity that was both historical and aesthetic.

  5. Da ordem. Da cidade. Da literatura: personagens à beira do "ruim do mundo"

    Directory of Open Access Journals (Sweden)

    Eliana Kuster

    2007-12-01

    Full Text Available As grandes cidades estão doentes. Seus sintomas: a quebra da sociabilidade e a irrupção rotineira da violência. Diante disso, ecoa na sociedade um clamor por ordem. No mesmo momento em que a polícia põe a tropa na rua, os literatos criam personagens que dão voz à sensação crescente de que a cidade está deixando de ser uma referência à constituição das identidades urbanas. É a partir da literatura, em especial da obra do escritor Rubem Fonseca, que iremos perscrutar as possibilidades apresentadas pela cidade para o convívio humano.The great cities are sick. Its indications: the sociability in addition and the routine irruption of the violence. Ahead of this, a outcry for order echoes in the society. At the same moment where the policy goes to the street, the writers create personages who give voice to the increasing sensation of that the city is leaving of being a reference to the constitution of the urban identities. It is from literature, in special of the writer Rubem Fonseca, that we will go to investigate the possibilities presented for the city for the human conviviality.

  6. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... to loosen mucus from airway walls. See how different airway clearance techniques work to help you clear the thick, sticky mucus ... Offer their tips for fitting ACTs into daily life Airway Clearance Techniques | Webcast ... Facebook Twitter ...

  7. Nuclear techniques in industry

    International Nuclear Information System (INIS)

    Hammad, F.H.

    1994-01-01

    Nuclear techniques are utilized in almost every industry. The discussion in this paper includes discussions on tracer methods and uses nucleonic control systems technology; non-destructive testing techniques and radiation technology. 1 fig., 2 tabs

  8. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... decisions about your health care. CF Genetics: The Basics CF Mutations Video Series Find Out More About ... of Breathing Technique Airway Clearance Techniques Autogenic Drainage Basics of Lung Care Chest Physical Therapy Coughing and ...

  9. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... Active Cycle of Breathing Technique Airway Clearance Techniques Autogenic Drainage Basics of Lung Care Chest Physical Therapy ... clearance. Facebook Twitter Email More Related Content Medications Autogenic Drainage Positive Expiratory Pressure High-Frequency Chest Wall ...

  10. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... a range of treatment options. Airway Clearance Active Cycle of Breathing Technique Airway Clearance Techniques Autogenic Drainage ... LEGACY GIFT Sponsor a Participant CF Climb CF Cycle for Life Great Strides Xtreme Hike Participate In ...

  11. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... many challenges, including medical, social, and financial. By learning more about how you can manage your disease every day, you can ultimately help find a ... Cycle of Breathing Technique Airway Clearance Techniques Autogenic ...

  12. Airway Clearance Techniques (ACTs)

    Medline Plus

    Full Text Available ... Cycle of Breathing Technique Airway Clearance Techniques Autogenic Drainage Basics of Lung Care Chest Physical Therapy Coughing ... Facebook Twitter Email More Related Content Medications Autogenic Drainage Positive Expiratory Pressure High-Frequency Chest Wall Oscillation ( ...

  13. Uso da fluoxetina no tratamento da tricotilomania felina

    OpenAIRE

    Sousa,Marlos Gonçalves; Ferreira,Lilian Stefanoni; Gerardi,Daniel Guimarães; Costa,Mirela Tinucci

    2004-01-01

    A tricotilomania ou alopecia psicogênica felina é uma dermatopatia de origem psicogênica, decorrente da lambedura compulsiva do pelame, realizada pelo gato em situações de estresse. Tal distúrbio decorre de alterações neuro-hormonais e pode associar-se à introdução de novos animais e/ou crianças no ambiente. Além de mudanças de manejo e atitude para com o animal, sugere-se o emprego de ansiolíticos no tratamento da doença. A fluoxetina foi utilizada no tratamento de cinco gatos domésticos com...

  14. Karyotypical characterization from stock of Nile tilapia, Oreochromis niloticus, at Londrina State University, PR, Brazil, through several techniques of chromosomes band/ Caracterização cariotípica de um estoque de tilápia do Nilo,Oreochromis niloticus, da Universidade Estadual de Londrina, mediante diversas técnicas de bandamento cromossômico

    Directory of Open Access Journals (Sweden)

    Julio Hermann Leonhardt

    2006-07-01

    Full Text Available 14 specimens of Nile’s tilapia were analyzed cytogenetically, Oreochromis niloticus, that belong to the stock of fish breeding from the Freshwater Aquaculture Station of the Londrina State University in the Paraná, Brazil. All specimens presented the same disploid number of 44 chromosomes. The NORs were observed in four chromosomes with marks in terminal position of the short arm and the hybridization “in situ” (FISH with probe of 18 S also evidenced the presence of two pairs of chromosomes containing ribbosomic cistrons. The treatment with the fluochromes CMA3 and DAPI, respectively, didn’t show shinning bands in any chromosome of the complement. The band C (CBG evidenced regions of heterochromatin distributed on several chromosomes in the centromeric regions, being observed some marks in telomeric regions, mainly on the biggest pair of chromosomes of the complement, a pair presented itself almost totally heterochromatic. The obtained results are in accordance with the data found in literature, nevertheless when the C bands and NORs were analyzed, were evidenced some differences that apparently characterized the local fish population of the Londrina State University. Key words: Cytogenetics, Oreochromis niloticus, NORs, CMA3, DAPI, fish, heterochromatin.Foram analisados citogeneticamente 14 indivíduos de tilápia do Nilo, Oreochromis niloticus que fazem parte do estoque de reposição de reprodutores da Estação de Piscicultura da Universidade Estadual de Londrina, Paraná, Brasil. Todos os indivíduos apresentaram o mesmo número diplóide de 44 cromossomos. As NORs foram observadas em quatro cromossomos com marcações em posição terminal do braço curto e a hibridação “in situ” (FISH com sonda de 18S também evidenciou a presença de dois pares de cromossomos contendo cístrons ribossômicos. O tratamento com os fluorocromos CMA3 e DAPI, respectivamente, não mostrou bandas brilhantes em nenhum cromossomo do complemento. A

  15. Teoria da adequação econômica da conduta: significado econômico da conduta em face da tutela penal antitruste

    OpenAIRE

    Luiz da Silva, Ivan

    2009-01-01

    Essa tese tem por objetivo o desenvolvimento da teoria da adequação econômica da conduta no direito penal econômico. Vale-se de uma abordagem interdisciplinar abrangendo a Economia, o direito econômico e o direito penal. Para alcançar o desiderato a investigação analisou a intervenção do direito penal em face da atividade econômica e, em especial, os fundamentos da tutela penal antitruste, para fins de estabelecer os contornos teóricos necessários à aplicação das premissas fund...

  16. Radiation scattering techniques

    International Nuclear Information System (INIS)

    Edmonds, E.A.

    1986-01-01

    Radiation backscattering techniques are useful when access to an item to be inspected is restricted to one side. These techniques are very sensitive to geometrical effects. Scattering processes and their application to the determination of voids, thickness measuring, well-logging and the use of x-ray fluorescence techniques are discussed. (U.K.)

  17. Point of Technique

    African Journals Online (AJOL)

    .

    Minimally invasive techniques are becoming popular choice for the recent times. These techniques are lowering the cost and giving the best cosmetic results. For cardiovascular surgery these techniques are much more newer and much more unknown. Open lumbar sympathectomy for certain indications is a very well ...

  18. Newton da Costa e a Filosofia da Quase-Verdade

    Directory of Open Access Journals (Sweden)

    Décio Krause

    2009-08-01

    Full Text Available This paper intends to introduce the three issues of Principia which will appear in a sequel honoring Newton da Costa’s 80th birthday. Instead of presenting the papers one by one, as it is common in presentations such as this one, we have left the papers speak by themselves, and instead we have preferred to present to the Brazilian readers, specialty to our students, some aspects of Newton da Costa’s conception of science and of the scientific activity, grounded on the concept of quasi-truth, which he contributed to develop in a rigorous way. Da Costa is known as one of the founding fathers of paraconsistent logic, but his contributions go also to the foundations of physics, theoretical computation, model theory, algebraic logic, lattice theory, applications of non-classical logics to law and technology, etc. But perhaps his main contribution was to provide a basis for the birth of a school of logic in our country (Brazil, serving as teacher and inspiring new researchers for generations. It is a pleasure to have had so enthusiastic acceptation from the editors of Principia to organize these volumes. I would like to thank the contributors and the editors of Principia, specially Prof. Cezar Mortari for his help in organizing the issue.

  19. Efeito da eutonia no tratamento da fibromialgia Eutonia effect in the fibromyalgia treatment

    Directory of Open Access Journals (Sweden)

    Cecília Maeda

    2006-02-01

    Full Text Available OBJETIVO: avaliar a eutonia como método terapêutico auxiliar no tratamento da fibromialgia (FM. MÉTODOS: estudou-se um grupo de 20 mulheres, segundo os critérios do American College of Rheumatology (ACR, com duração mínima de seis meses, sem alterações no tratamento medicamentoso ou prescrição de exercícios nesse período. As pacientes foram avaliadas através do questionário de dados sociodemográficos; Escala Visual Analógica (EVA para dor e questionário genérico de avaliação da qualidade de vida (medical outcomes study 36 - item short-form health survey - SF-36. As avaliações foram realizadas imediatamente antes e após as sessões e ainda um ano após o término das sessões. As pacientes foram submetidas a 25 sessões de eutonia acompanhadas de educação em saúde. RESULTADOS: houve melhora significativa na intensidade da dor, de acordo com a EVA (7,82 antes e 4,17 após e em todos os domínios do SF-36 na avaliação imediatamente após a eutonia. Os resultados da dor se mantiveram um ano após a intervenção (4,18. Em relação às escalas do SF-36, a melhora também se manteve, porém com intensidade menor do que no resultado imediato.Não há qualquer modalidade terapêutica isolada que atenda todas as demandas da FM. A utilização de técnicas psicológicas tem sido proposta como complementação à terapia medicamentosa e aos exercícios físicos. A eutonia é uma técnica que enfatiza o autoconhecimento e, portanto, poderia ser útil na abordagem da FM. Os resultados desse estudo mostraram efeito positivo na intensidade da dor e na qualidade de vida dos pacientes. CONCLUSÃO: a eutonia é útil como método terapêutico na FM associado ao tratamento habitual dos pacientes estudados. Seu efeito é particularmente importante na intensidade da dor difusa crônica e na qualidade de vida.OBJECTIVE: To evaluate the usefulness eutonia for the treatment fibromyalgia. METHODS: It was studied, for a six month period, 20

  20. ANÁLISE DA DISTRIBUIÇÃO ESPAÇO-TEMPORAL DA CHUVA, NA MESORREGIÃO METROPOLITANA DE BELÉM-PARÁ: CONTRIBUIÇÕES DA TÉCNICA DE SENSORIAMENTO REMOTO

    Directory of Open Access Journals (Sweden)

    Marcos Ronielly Silva Santos

    2017-06-01

    Full Text Available A identificação dos montantes de chuva para uma região corrobora para a gestão eficiente das politicas públicas e o desenvolvimento social, econômico e ambiental dos centros urbanos.  A mesorregião metropolitana de Belém detém a maior concentração populacional e urbana da Amazônia Oriental, apresentando elevados índices pluviômetros durante todo o ano. Neste contexto o presente trabalho visa identificar a distribuição temporal e espacial da precipitação na mesorregião metropolitana de Belém e associa-la aos principais sistemas precipitantes que atuam na região. Para isto se utilizou o sensoriamento remoto por meio da técnica do CPC MORPHing technique (CMORPH com resolução temporal de 30 min e espacial de 8/8 km. A partir da técnica empregada foram gerados mapas da distribuição têmporo-espacial da chuva com as médias mensais para os dozes meses do ano, decorrentes dos acumulados do período de Jan/2000 a Dez/2010. Os resultados mostram que há uma grande variação temporal e espacial da chuva na mesorregião evidenciando de modo satisfatório a sazonalidade regional da precipitação, com altos índices durante o período chuvoso e baixos índices no período menos chuvoso. Trabalhos que visem à interdisciplinaridade podem contribuir de forma eficaz para estruturação das ciências ambientais e para a tomada de decisões.

  1. Comparison of the pain severity, drug leakage and ecchymosis rates caused by the application on tramadol intramuscular injection in Z-track and Air-lock techniques Comparación de la severidad del dolor y las tasas de escape de líquido y equimosis causadas por la aplicación intramuscular de tramadol usando las técnicas de cámara de aire y Z-track Comparação da severidade da dor e as taxas de fuga de líquidas equimoses causadas pela aplicação intramuscular de tramadol usando as técnicas de câmaras de ar e Z-track

    Directory of Open Access Journals (Sweden)

    Shahla Najafidolatabad

    2010-07-01

    Full Text Available Objective. To compare the pain severity caused by the application of the Z-track and Air-lock intramuscular injections. Methodology. Unblinded clinical trial, where 90 female subjects aged between 18 and 60 years old were randomly assigned to two groups; the first group received the tramadol intramuscular injection using the Z-track technique (ZT and the second group received it through the air- lock method (AL. A 10 centimeter linear visual scale was used to evaluate the injection pain. The scale length was considered as the pain severity. Data were analyzed using the SPSS version 13. Groups' age, Body Mass index (BMI, and pain intensity were compared using unpaired student's t test. Results. The study showed that the pain severity of patients in the AL method group was lower than in the ZT technique group (pObjetivo. Comparar la severidad del dolor y las tasas de escape de líquido y equimosis causadas por la aplicación de las inyecciones intramusculares usando la técnica Z-track (ZT y la técnica de la cámara de aire (CA. Metodología. Este es un ensayo clínico no ciego donde un grupo de 90 mujeres entre los 18 y 60 años fueron aleatoriamente asignadas a dos grupos; El primer grupo recibió la inyección por medio de la técnica ZT y el segundo por medio de la técnica de CA. Se uso una escala visual lineal de 10 centímetros para medir la intensidad del dolor causado por la inyección. La longitud de la escala fue considerada como la severidad del dolor. Los datos fueron analizados utilizando el programa SPSS versión 13. La edad, el índice de Masa Corporal (IMC, y la intensidad del dolor de los grupos fueron comparados usando el test de la t para muestras independientes. Resultados. El estudio mostró que la severidad del dolor y las tasas de escape de líquido y equimosis en las pacientes evaluadas usando el método CA era menor que el dolor causado por la técnica ZT (p Objetivo. Comparar a severidade da dor e as taxas de escape de

  2. Influência da técnica anestésica nas alterações hemodinâmicas no transplante renal: estudo retrospectivo Influencia de la técnica anestésica en las alteraciones hemodinámicas en el transplante renal: estudio retrospectivo Influence of the anesthetic technique on the hemodynamic changes