In situ stress and pore pressure in the Kumano Forearc Basin, offshore SW Honshu from downhole measurements during riser drilling

Science.gov (United States)

Saffer, D. M.; Flemings, P. B.; Boutt, D.; Doan, M.-L.; Ito, T.; McNeill, L.; Byrne, T.; Conin, M.; Lin, W.; Kano, Y.; Araki, E.; Eguchi, N.; Toczko, S.

2013-05-01

situ stress and pore pressure are key parameters governing rock deformation, yet direct measurements of these quantities are rare. During Integrated Ocean Drilling Program (IODP) Expedition #319, we drilled through a forearc basin at the Nankai subduction zone and into the underlying accretionary prism. We used the Modular Formation Dynamics Tester tool (MDT) for the first time in IODP to measure in situ minimum stress, pore pressure, and permeability at 11 depths between 729.9 and 1533.9 mbsf. Leak-off testing at 708.6 mbsf conducted as part of drilling operations provided a second measurement of minimum stress. The MDT campaign included nine single-probe (SP) tests to measure permeability and in situ pore pressure and two dual-packer (DP) tests to measure minimum principal stress. Permeabilities defined from the SP tests range from 6.53 × 10-17 to 4.23 × 10-14 m2. Pore fluid pressures are near hydrostatic throughout the section despite rapid sedimentation. This is consistent with the measured hydraulic diffusivity of the sediments and suggests that the forearc basin should not trap overpressures within the upper plate of the subduction zone. Minimum principal stresses are consistently lower than the vertical stress. We estimate the maximum horizontal stress from wellbore failures at the leak-off test and shallow MDT DP test depths. The results indicate a normal or strike-slip stress regime, consistent with the observation of abundant active normal faults in the seaward-most part of the basin, and a general decrease in fault activity in the vicinity of Site C0009.

Application of hydraulic fracturing to determine virgin in situ stress state around Waste Isolation Pilot Plant - in situ measurements

International Nuclear Information System (INIS)

Wawersik, W.R.; Stone, C.M.

1985-10-01

Hydraulic fracturing tests were carried out in horizontal drillholes in rock salt in the Waste Isolation Pilot Plant (WIPP) near Carlsbad, NM. It was determined that the virgin in situ stress field is isotropic or nearly isotropic. The inferred magnitude of the isotropic in situ stress falls between bounds of 14.28 MPa and 17.9 MPa for the average breakdown/reopening pressures and driving pressures. The best estimate from instantaneous shut-in pressures is 16.61 MPa. Given some uncertainties about the interpretation of hydraulic fracturing data in salt, all of the foregoing values are in acceptable agreement with an average calculated isotropic in situ stress of 14.9 MPa at an average depth of 657 m below surface. Interpretations of breakdown and reopening pressures are based on finite element analyses of the relaxed stress field around a borehole in salt. This stress field varies little between approximately 50 and 200 days after drilling. The finite element analyses were also used to interpret the observed stable pressure-time signatures with little or no pressure drops during primary breakdown of the salt formation. The conclusion about the isotropic nature of the virgin in situ stress field is supported by observations of the induced fracture patterns. The report includes a comparison of the hydrofrac data in the WIPP with the published results of hydraulic fracturing tests in salt at three other locations. 75 refs., 21 figs., 4 tabs

In-Situ Measurement of Power Loss for Crystalline Silicon Modules Undergoing Thermal Cycling and Mechanical Loading Stress Testing

DEFF Research Database (Denmark)

Spataru, Sergiu; Hacke, Peter; Sera, Dezso

We analyze the degradation of multi-crystalline silicon photovoltaic modules undergoing simultaneous thermal, mechanical, and humidity-freeze stress testing to develop a dark environmental chamber in-situ measurement procedure for determining module power loss. We analyze dark I-V curves measured...

In-situ neutron diffraction measurements of temperature and stresses during friction stir welding of 6061-T6 aluminum alloy

International Nuclear Information System (INIS)

Woo, Wan Chuck; Feng, Zhili; Wang, Xun-Li; Brown, D.W.; Clausen, B.; An, Ke; Choo, Hahn; Hubbard, Camden R.; David, Stan A.

2007-01-01

The evolution of temperature and thermal stresses during friction stir welding of Al6061-T6 was investigated by means of in-situ, time-resolved neutron diffraction technique. A method is developed to deconvolute the temperature and stress from the lattice spacing changes measured by neutron diffraction. The deep penetration capability of neutrons made it possible for the first time to obtain the temperature and thermal stresses inside a friction stir weld

In situ subsoil stress-strain behaviour in relation to soil precompression stress

DEFF Research Database (Denmark)

Keller, T; Arvidsson, J; Schjønning, Per

2012-01-01

is assumed to be elastic and reversible as long as [sigma] work examined soil stress-strain behavior as measured in situ during wheeling experiments and related it to the stress-strain behavior and [sigma]pc measured on soil cores in uniaxial compression tests in the laboratory. The data......Soil compaction negatively influences many important soil functions, including crop growth. Compaction occurs when the applied stress, [sigma], overcomes the soil strength. Soil strength in relation to compaction is typically expressed by the soil precompression stress, [sigma]pc. Deformation...... analyzed were from a large number of wheeling experiments carried out in Sweden and Denmark on soils with a wide range of texture. Contradicting the concept of precompression stress, we observed residual strain, [Latin Small Letter Open E]res, at [sigma

Operational Review of the First Wireline In Situ Stress Test in Scientific Ocean Drilling

Directory of Open Access Journals (Sweden)

Casey Moore

2012-04-01

Full Text Available Scientific ocean drilling’s first in situ stress measurement was made at Site C0009A during Integrated Ocean Drilling Program (IODP Expedition 319 as part of Nankai Trough Seismogenic Zone Experiment (NanTroSEIZE Stage 2. The Modular Formation Dynamics Tester (MDT, Schlumbergerwireline logging tool was deployed in riser Hole C0009A to measure in situ formation pore pressure, formation permeability (often reported as mobility=permeability/viscosity, and the least principal stress (S3 at several isolated depths (Saffer et al., 2009; Expedition 319 Scientists, 2010. The importance of in situ stress measurements is not only for scientific interests in active tectonic drilling, but also for geomechanical and well bore stability analyses. Certain in situ tools were not previously available for scientific ocean drilling due to the borehole diameter and open hole limits of riserless drilling. The riser-capable drillship, D/V Chikyu,now in service for IODP expeditions, allows all of the techniques available to estimate the magnitudes and orientations of 3-D stresses to be used. These techniques include downhole density logging for vertical stress, breakout and caliper log analyses for maximum horizontal stress, core-based anelastic strain recovery (ASR, used in the NanTroSEIZE expeditions in 2007–2008, and leak-off test (Lin et al., 2008 and minifrac/hydraulic fracturing (NanTroSEIZE Expedition319 in 2009. In this report, the whole operational planning process related to in situ measurements is reviewed, and lessons learned from Expedition 319 are summarized for efficient planning and testing in the future.

In situ measurements of Merensky pillar behaviour at Impala Platinum

CSIR Research Space (South Africa)

Watson, BP

2009-12-01

Full Text Available to stabilize the stoping excavations. This paper describes the in situ measurement, of stress within a Merensky pillar from Impala Platinum. These measurements were used to derive a stress-strain curve that includes pre and post failure behaviour. 2D FLAC...

In-situ X-ray residual stress measurement on a peened alloy 600 weld metal at elevated temperature under tensile load

International Nuclear Information System (INIS)

Yunomura, Tomoaki; Maeguchi, Takaharu; Kurimura, Takayuki

2014-01-01

In order to verify stability of residual stress improvement effect of peeing for mitigation of stress corrosion cracking in components of PWR plant, relaxation behavior of residual stress induced by water jet peening (WJP) on surface of alloy 600 weld metal (alloy 132) was investigated by in-situ X-ray residual stress measurement under thermal aging and stress condition considered for actual plant operation. Surface residual stress change was observed at the early stage of thermal aging at 360°C, but no significant further stress relaxation was observed after that. Applied stress below yield stress does not significantly affect stress relaxation behavior of surface residual stress. For the X-ray residual stress measurement, X-ray stress constant at room temperature for alloy 600 was determined experimentally with several surface treatment and existence of applied strain. The X-ray stress constant at elevated temperatures were extrapolated theoretically based on the X-ray stress constant at room temperature for alloy 600. (author)

Review of current capabilities for the measurement of stress, displacement, and in situ deformation modulus

International Nuclear Information System (INIS)

Schrauf, T.W.; Pratt, H.R.

1979-12-01

Current capabilities for the measurement of stress, displacement, and in situ deformation modulus in rock masses are reviewed as to their accuracy, sensitivity, advantages, and limitations. Consideration is given to both the instruments themselves and the measurement technique. Recommendations concerning adaptation of existing measurement techniques to repository monitoring are also discussed. These recommendations include: (1) development of a modified borehole deformation gage with improved long-term stability and reliability and reduced thermal sensitivity; (2) development of a downhole transducer type of extensometer; (3) development of a rigid inclusion type gage; (4) development of an improved vibrating wire stressmeter with greater accuracy and simplified calibration and installation requirements; and (5) modification of standard rod extensometers to improve their sensitivity

Comparison Between Stress Obtained by Numerical Analysis and In-Situ Measurements on a Flexible Pipe Subjected to In-Plane Bending Test

DEFF Research Database (Denmark)

Vestergaard Lukassen, Troels; Glejbøl, Kristian; Lyckegaard, Anders

2016-01-01

to stress patterns obtained during in-situ OMS measurements carried out during an actual experimental inplane bending test. The study showed a good correlation between the stress variation predicted with the finite element model and the measured stress variation.......To predict the lifetime and long-term properties of tensile armour wires in a dynamically loaded pipe, it is essential to have a tool which allows detailed prediction of the stress variations in the tensile armour wires during global pipe loading. Furthermore, detailed understanding of the stress...... variations will allow for performance optimization of the armour layers. To study the detailed stress variations in flexible pipes during dynamic loading, a comprehensive three-dimensional implicit nonlinear finite element model has been developed. The predicted numerical stress variations will be compared...

Numerical study on core damage and interpretation of in situ state of stress

Energy Technology Data Exchange (ETDEWEB)

Hakala, M. [Gridpoint Finland Oy (Finland)

1999-06-01

Core disking is a phenomenon where a diamond cored core sample will be sliced when released from a stressed host rock. Ring disking is a similar phenomenon which takes place during overcoring with a pilot hole. Because of the uniform shape and spacing of disk fracturing, it has the potential to be used for estimating the in situ state of stress. If this is feasible, it could be used in high stress states where the traditional stress measuring techniques are not valid or even possible. In this work the both the core disking and ring disking phenomena were studied based on the elastic bottom hole stress application developed and a series of fracture growth stability simulations. The results-showed that both phenomena are very complicated and site specific, but the spacing, shape, extent and initiation point are clearly stress state dependent. Throughout the work, guidelines for the in situ stress field interpretation method were developed and implemented for the borehole aligned orthogonal stress field and Poisson`s ratio of 0.25. Based on this study, the in situ state of stress can be estimated with acceptable accuracy if information on both core disking and ring disking is available. On the other hand, as an indirect method, there are no reasons to use it if direct measurements can be used. (orig.) 35 refs.

Numerical study on core damage and interpretation of in situ state of stress

International Nuclear Information System (INIS)

Hakala, M.

1999-06-01

Core disking is a phenomenon where a diamond cored core sample will be sliced when released from a stressed host rock. Ring disking is a similar phenomenon which takes place during overcoring with a pilot hole. Because of the uniform shape and spacing of disk fracturing, it has the potential to be used for estimating the in situ state of stress. If this is feasible, it could be used in high stress states where the traditional stress measuring techniques are not valid or even possible. In this work the both the core disking and ring disking phenomena were studied based on the elastic bottom hole stress application developed and a series of fracture growth stability simulations. The results-showed that both phenomena are very complicated and site specific, but the spacing, shape, extent and initiation point are clearly stress state dependent. Throughout the work, guidelines for the in situ stress field interpretation method were developed and implemented for the borehole aligned orthogonal stress field and Poisson's ratio of 0.25. Based on this study, the in situ state of stress can be estimated with acceptable accuracy if information on both core disking and ring disking is available. On the other hand, as an indirect method, there are no reasons to use it if direct measurements can be used. (orig.)

Four-point bend apparatus for in situ micro-Raman stress measurements

Science.gov (United States)

Ward, Shawn H.; Mann, Adrian B.

2018-06-01

A device for in situ use with a micro-Raman microscope to determine stress from the Raman peak position was designed and validated. The device is a four-point bend machine with a micro-stepping motor and load cell, allowing for fine movement and accurate readings of the applied force. The machine has a small footprint and easily fits on most optical microscope stages. The results obtained from silicon are in good agreement with published literature values for the linear relationship between stress and peak position for the 520.8 cm‑1 Raman peak. The device was used to examine 4H–SiC and a good linear relationship was found between the 798 cm‑1 Raman peak position and stress, with the proportionality coefficient being close to the theoretical value of 0.0025. The 777 cm‑1 Raman peak also showed a linear dependence on stress, but the dependence was not as strong. The device examines both the tensile and compressive sides of the beam in bending, granting the potential for many materials and crystal orientations to be examined.

Influence of fracture extension on in-situ stress in tight reservoir

Science.gov (United States)

Zhang, Yongping; Wei, Xu; Zhang, Ye; Xing, Libo; Xu, Jianjun

2018-01-01

Currently, hydraulic fracturing is an important way to develop low permeability reservoirs. The fractures produced during the fracturing process are the main influencing factors of changing in-situ stress. In this paper, the influence of fracture extension on in-situ stress is studied by establishing a mathematical model to describe the relationship between fracture length and in-situ stress. The results show that the growth rate gradually decreases after the fracture reaches a certain length with the increase of fracturing time; the continuous extension of the fracture is the main factor to change the in-situ stress. In order to reduce the impact on the subsequent fracture extension due to the changing of in-situ stress, controlling fracturing time and fracture length without affecting the stimulated reservoir effect is an important way. The results presented in this study can effectively reduce the impact of changing of in-situ stress on subsequent fracturing construction.

Lithology-dependent In Situ Stress in Heterogeneous Carbonate Reservoirs

Science.gov (United States)

Pham, C. N.; Chang, C.

2017-12-01

Characterization of in situ stress state for various geomechanical aspects in petroleum development may be particularly difficult in carbonate reservoirs in which rock properties are generally heterogeneous. We demonstrate that the variation of in situ stress in highly heterogeneous carbonate reservoirs is closely related to the heterogeneity in rock mechanical property. The carbonate reservoir studied consists of numerous sequential layers gently folded, exhibiting wide ranges of porosity (0.01 - 0.29) and Young's modulus (25 - 85 GPa) depending on lithology. Wellbore breakouts and drilling-induced tensile fractures (DITFs) observed in the image logs obtained from several wells indicate that the in situ state of stress orientation changes dramatically with depth and location. Even in a wellbore, the azimuth of the maximum horizontal stress changes by as much as 60° within a depth interval of 500 m. This dramatic change in stress orientation is inferred to be due to the contrast in elastic properties between different rock layers which are bent by folding in the reservoir. The horizontal principal stress magnitudes are constrained by back-calculating stress conditions necessary to induce the observed wellbore failures using breakout width and the presence of DITFs. The horizontal stresses vary widely, which cannot be represented by a constant stress gradient with depth. The horizontal principal stress gradient increases with Young's modulus of layer monotonically, indicating that a stiffer layer conveys a higher horizontal stress. This phenomenon can be simulated using a numerical modelling, in which the horizontal stress magnitudes depend on stiffness of individual layers although the applied far-field stress conditions are constant. The numerical results also suggest that the stress concentration at the wellbore wall is essentially higher in a stiffer layer, promoting the possibility of wellbore breakout formation. These results are in agreement with our

Test design requirements for overcoring stress measurements

International Nuclear Information System (INIS)

Stickney, R.G.

1985-12-01

This document establishes the test design requirements for a series of overcoring stress measurements to be performed in the Exploratory Shaft Facility. The stress measurements will be made to determine the in situ state of stress within the candidate repository horizon and to determine the magnitude and distribution of the stresses induced by the mined openings of the facility. The overcoring technique involves the measurement of strain (or deformation) in a volume of rock as the stress acting on the rock volume is relieved. This document presents an overview of the measurements, including objectives and rationale for the measurements. A description of the measurements is included. The support requirements are identified as are constraints for the design of the measurements. Discussions on Quality Assurance and Safety are also included in the document. 13 refs

The measurement of in-situ stress in near surface environments

International Nuclear Information System (INIS)

Garritty, P.; Irvin, R.A.

1984-04-01

One of the major unknowns affecting aspects of underground construction and the geohydrology of rock masses is the magnitude and direction of the geostatic principal stresses in the earth's crust. This is particularly the case in near surface rocks where there are indications that high horizontal stresses may exist. The measurement of stress in near surface environments is particularly difficult. The techniques, experience and results of a geostatic stress measurement programme using four commercially available devices at shallow depth in the Carnmenellis Granite are critically discussed and compared. This report also brings together some of the conclusions of two previous reports in the series, Garritty (1983) and Garritty and Irvin (1983), and emphasises the fundamental relationship between the state of stress in the earth's crust and the geohydrology of rock masses. (author)

Examining the validity of Stoney-equation for in-situ stress measurements in thin film electrodes using a large-deformation finite-element procedure

Science.gov (United States)

Wen, Jici; Wei, Yujie; Cheng, Yang-Tse

2018-05-01

During the lithiation and delithiation of a thin film electrode, stress in the electrode is deduced from the curvature change of the film using the Stoney equation. The accuracy of such a measurement is conditioned on the assumptions that (a) the mechanical properties of the electrode remain unchanged during lithiation and (b) small deformation holds. Here, we demonstrate that the change in elastic properties can influence the measurement of the stress in thin film electrodes. We consider the coupling between diffusion and deformation during lithiation and delithiation of thin film electrodes and implement the constitutive behavior in a finite-deformation finite element procedure. We demonstrate that both the variation in elastic properties in thin film electrodes and finite-deformation during lithiation and delithiation would challenge the applicability of the Stoney-equation for in-situ stress measurements of thin film electrodes.

Intrinsic stress in ZrN thin films: Evaluation of grain boundary contribution from in situ wafer curvature and ex situ x-ray diffraction techniques

International Nuclear Information System (INIS)

Koutsokeras, L. E.; Abadias, G.

2012-01-01

Low-mobility materials, like transition metal nitrides, usually undergo large residual stress when sputter-deposited as thin films. While the origin of stress development has been an active area of research for high-mobility materials, atomistic processes are less understood for low-mobility systems. In the present work, the contribution of grain boundary to intrinsic stress in reactively magnetron-sputtered ZrN films is evaluated by combining in situ wafer curvature measurements, providing information on the overall biaxial stress, and ex situ x-ray diffraction, giving information on elastic strain (and related stress) inside crystallites. The thermal stress contribution was also determined from the in situ stress evolution during cooling down, after deposition was stopped. The stress data are correlated with variations in film microstructure and growth energetics, in the 0.13-0.42 Pa working pressure range investigated, and discussed based on existing stress models. At low pressure (high energetic bombardment conditions), a large compressive stress is observed due to atomic peening, which induces defects inside crystallites but also promotes incorporation of excess atoms in the grain boundary. Above 0.3-0.4 Pa, the adatom surface mobility is reduced, leading to the build-up of tensile stress resulting from attractive forces between under-dense neighbouring column boundary and possible void formation, while crystallites can still remain under compressive stress.

In-situ observations of stress-induced thin film failures

Energy Technology Data Exchange (ETDEWEB)

Zhao, Z.B., E-mail: zzhao@firstsolar.co [Delphi Research Labs, 51786 Shelby Parkway, Shelby Twp., MI 48315 (United States); Hershberger, J. [Laird Technologies, 4707 Detroit Avenue, Cleveland, Ohio, 44102 (United States); Bilello, J.C. [Department of Materials Science and Engineering, University of Michigan, Ann Arbor, MI 48109-2136 (United States)

2010-02-01

In this work, the failure modes of thin films under thermo-mechanical treatments were observed via in-situ white beam X-ray topography. The in-situ experiments were carried out using an experimental setup on Beamline 2-2 at the Stanford Synchrotron Radiation Laboratory. Magnetron sputtered polycrystalline thin films of Ta and CrN on Si substrates were selected for the present study due to their disparate states of intrinsic residual stresses: the Ta film was anisotropically compressive and the CrN film was isotropically tensile. Under a similar heating-cooling cycle in air, the two types of films exhibited distinct failure modes, which were observed in-situ and in a quasi-real-time fashion. The failures of the samples have been interpreted based on their distinctive growth stress states, superimposed on the additional stress development associated with different forms of thermal instabilities upon heating. These included the formation of oxide for the Ta/Si sample, which led to an increase in compressive stress, and a phase change for the CrN/Si sample, which caused the isotropic stress in the film to become increasingly tensile.

In-situ observations of stress-induced thin film failures

International Nuclear Information System (INIS)

Zhao, Z.B.; Hershberger, J.; Bilello, J.C.

2010-01-01

In this work, the failure modes of thin films under thermo-mechanical treatments were observed via in-situ white beam X-ray topography. The in-situ experiments were carried out using an experimental setup on Beamline 2-2 at the Stanford Synchrotron Radiation Laboratory. Magnetron sputtered polycrystalline thin films of Ta and CrN on Si substrates were selected for the present study due to their disparate states of intrinsic residual stresses: the Ta film was anisotropically compressive and the CrN film was isotropically tensile. Under a similar heating-cooling cycle in air, the two types of films exhibited distinct failure modes, which were observed in-situ and in a quasi-real-time fashion. The failures of the samples have been interpreted based on their distinctive growth stress states, superimposed on the additional stress development associated with different forms of thermal instabilities upon heating. These included the formation of oxide for the Ta/Si sample, which led to an increase in compressive stress, and a phase change for the CrN/Si sample, which caused the isotropic stress in the film to become increasingly tensile.

Evaluation and upgrading of records of stress measurement data in the mining industry.

CSIR Research Space (South Africa)

Stacey, TR

1998-06-01

Full Text Available to tectonic inversion, Proc. Centennial Geocongress (1995), ed J.M.Barton Jnr and Y.E.Copperthwaite, Geological Society of South Africa, pp 452- 455. Gay, N.C. 1972. Virgin rock stresses at Doornfontein Gold Mine, Carletonville, South Africa, Journal... of Geology, Vol 80, pp 61-80. Gay, N.C. 1975. In-situ stress measurements in Southern Africa, Tectonophysics, Vol 29, pp 447-459. Handley, M.F. 1996. In-situ stress measurements taken near SVC raisebore on 109 level at Western Deep Levels Limited South...

In Situ Investigation of the Evolution of Lattice Strain and Stresses in Austenite and Martensite During Quenching and Tempering of Steel

DEFF Research Database (Denmark)

Villa, M.; Niessen, F.; Somers, M. A. J.

2018-01-01

Energy dispersive synchrotron X-ray diffraction was applied to investigate in situ the evolution of lattice strains and stresses in austenite and martensite during quenching and tempering of a soft martensitic stainless steel. In one experiment, lattice strains in austenite and martensite were...... measured in situ in the direction perpendicular to the sample surface during an austenitization, quenching, and tempering cycle. In a second experiment, the sin2ψ method was applied in situ during the austenite-to-martensite transformation to distinguish between macro- and phase-specific micro......-stresses and to follow the evolution of these stresses during transformation. Martensite formation evokes compressive stress in austenite that is balanced by tensile stress in martensite. Tempering to 748 K (475 °C) leads to partial relaxation of these stresses. Additionally, data reveal that (elastic) lattice strain...

Model and calculation of in situ stresses in anisotropic formations

Energy Technology Data Exchange (ETDEWEB)

Yuezhi, W.; Zijun, L.; Lixin, H. [Jianghan Petroleum Institute, (China)

1997-08-01

In situ stresses in transversely isotropic material in relation to wellbore stability have been investigated. Equations for three horizontal in- situ stresses and a new formation fracture pressure model were described, and the methodology for determining the elastic parameters of anisotropic rocks in the laboratory was outlined. Results indicate significantly smaller differences between theoretically calculated pressures and actual formation pressures than results obtained by using the isotropic method. Implications for improvements in drilling efficiency were reviewed. 13 refs., 6 figs.

Quantifying in situ stress magnitudes and orientations for Forsmark. Forsmark stage 2.2

International Nuclear Information System (INIS)

Martin, C. Derek

2007-11-01

Stephansson et al. concluded that in the Fennoscandia shield: (1) there is a large horizontal stress component in the uppermost 1,000 m of bedrock, and (2) the maximum and minimum horizontal stresses exceed the vertical stress assuming the vertical stress is estimated from the weight of the overburden. Several stress campaigns involving both overcoring and hydraulic fracturing, including the hydraulic testing of pre-existing fractures (HTPF), have been carried out at Forsmark to establish the in situ stress state. The results from the initial campaigns were summarised by Sjoeberg et al. which formed the bases for the stresses provided in the Site Descriptive Model version 1.2. Since then additional stress measurement campaigns have been completed. The results from these stress measurement campaigns support the conclusions from Stephansson et al. In addition to these in situ stress measurements the following additional studies were undertaken to aid in assessing the stress state at Forsmark. 1. A detailed televiewer survey of approximately 6,900 m of borehole walls to depths of 1,000 m was carried out to assess borehole wall damage, i.e. borehole breakouts. 2. Evaluation of nonlinear strains in laboratory samples to depths of approximately 800 m to assess if stress magnitudes were sufficient to create stress-induced microcracking. 3. Assessment of the magnitudes required to cause core disking and survey of core disking observed at Forsmark. The magnitudes and orientations from the stress measurement campaigns were analysed to establish the most likely stress magnitudes and orientations for Design Step D2 within the Target Area of the Complete Site Investigations. The maximum and minimum horizontal stress components are essentially the same as the maximum and intermediate principal stresses, σ1 and σ2, respectively. The minimum principal stress (σ3) is synonymous with the vertical stress. The most likely range in values to be used in the design is also shown. The

Quantifying in situ stress magnitudes and orientations for Forsmark. Forsmark stage 2.2

Energy Technology Data Exchange (ETDEWEB)

Martin, C. Derek (Univ. of Alberta (Canada))

2007-11-15

Stephansson et al. concluded that in the Fennoscandia shield: (1) there is a large horizontal stress component in the uppermost 1,000 m of bedrock, and (2) the maximum and minimum horizontal stresses exceed the vertical stress assuming the vertical stress is estimated from the weight of the overburden. Several stress campaigns involving both overcoring and hydraulic fracturing, including the hydraulic testing of pre-existing fractures (HTPF), have been carried out at Forsmark to establish the in situ stress state. The results from the initial campaigns were summarised by Sjoeberg et al. which formed the bases for the stresses provided in the Site Descriptive Model version 1.2. Since then additional stress measurement campaigns have been completed. The results from these stress measurement campaigns support the conclusions from Stephansson et al. In addition to these in situ stress measurements the following additional studies were undertaken to aid in assessing the stress state at Forsmark. 1. A detailed televiewer survey of approximately 6,900 m of borehole walls to depths of 1,000 m was carried out to assess borehole wall damage, i.e. borehole breakouts. 2. Evaluation of nonlinear strains in laboratory samples to depths of approximately 800 m to assess if stress magnitudes were sufficient to create stress-induced microcracking. 3. Assessment of the magnitudes required to cause core disking and survey of core disking observed at Forsmark. The magnitudes and orientations from the stress measurement campaigns were analysed to establish the most likely stress magnitudes and orientations for Design Step D2 within the Target Area of the Complete Site Investigations. The maximum and minimum horizontal stress components are essentially the same as the maximum and intermediate principal stresses, sigma1 and sigma2, respectively. The minimum principal stress (sigma3) is synonymous with the vertical stress. The most likely range in values to be used in the design is also

Estimation of In Situ Stresses with Hydro-Fracturing Tests and a Statistical Method

Science.gov (United States)

Lee, Hikweon; Ong, See Hong

2018-03-01

At great depths, where borehole-based field stress measurements such as hydraulic fracturing are challenging due to difficult downhole conditions or prohibitive costs, in situ stresses can be indirectly estimated using wellbore failures such as borehole breakouts and/or drilling-induced tensile failures detected by an image log. As part of such efforts, a statistical method has been developed in which borehole breakouts detected on an image log are used for this purpose (Song et al. in Proceedings on the 7th international symposium on in situ rock stress, 2016; Song and Chang in J Geophys Res Solid Earth 122:4033-4052, 2017). The method employs a grid-searching algorithm in which the least and maximum horizontal principal stresses ( S h and S H) are varied, and the corresponding simulated depth-related breakout width distribution as a function of the breakout angle ( θ B = 90° - half of breakout width) is compared to that observed along the borehole to determine a set of S h and S H having the lowest misfit between them. An important advantage of the method is that S h and S H can be estimated simultaneously in vertical wells. To validate the statistical approach, the method is applied to a vertical hole where a set of field hydraulic fracturing tests have been carried out. The stress estimations using the proposed method were found to be in good agreement with the results interpreted from the hydraulic fracturing test measurements.

Estimation of In Situ Stress and Permeability from an Extended Leak-off Test

Science.gov (United States)

Nghiep Quach, Quoc; Jo, Yeonguk; Chang, Chandong; Song, Insun

2016-04-01

stress regime with the information of the maximum principal stress that will be estimated based on borehole breakout geometry analysis. To estimate the in situ permeability from the XLOT data, we derived a theoretical equation that relates the slope of pressure versus injected water volume (P-V) curve to permeability based on the Darcy's law. The equation is expressed in terms of permeability as a function of some key parameters such as open-hole dimensions, flowrate, porosity, pressure change and injected water volume. We applied this equation to the early stage of the P-V curves prior to the leak-off point to prevent the effect of induced fractures on permeability. The estimated in situ permeability was (3.1±0.4)×10-17m2, which turns out to be quite similar to the laboratory measurements in recovered cores.

In situ measurement of electromigration-induced transient stress in Pb-free Sn-Cu solder joints by synchrotron radiation based X-ray polychromatic microdiffraction

Energy Technology Data Exchange (ETDEWEB)

Chen, Kai; Tamura, Nobumichi; Kunz, Martin; Tu, King-Ning; Lai, Yi-Shao

2009-12-01

Electromigration-induced hydrostatic elastic stress in Pb-free SnCu solder joints was studied by in situ synchrotron X-ray white beam microdiffraction. The elastic stresses in two different grains with similar crystallographic orientation, one located at the anode end and the other at the cathode end, were analyzed based on the elastic anisotropy of the Beta-Sn crystal structure. The stress in the grain at the cathode end remained constant except for temperature fluctuations, while the compressive stress in the grain at the anode end was built-up as a function of time during electromigration until a steady state was reached. The measured compressive stress gradient between the cathode and the anode is much larger than what is needed to initiate Sn whisker growth. The effective charge number of Beta-Sn derived from the electromigration data is in good agreement with the calculated value.

In situ measurement of electromigration-induced transient stress in Pb-free Sn-Cu solder joints by synchrotron radiation based X-ray polychromatic microdiffraction

Energy Technology Data Exchange (ETDEWEB)

Chen, Kai; Tamura, Nobumichi; Kunz, Martin; Tu, King-Ning; Lai, Yi-Shao

2009-05-15

Electromigration-induced hydrostatic elastic stress in Pb-free SnCu solder joints was studied by in situ synchrotron X-ray white beam microdiffraction. The elastic stresses in two different grains with similar crystallographic orientation, one located at the anode end and the other at the cathode end, were analyzed based on the elastic anisotropy of the {beta}-Sn crystal structure. The stress in the grain at the cathode end remained constant except for temperature fluctuations, while the compressive stress in the grain at the anode end was built-up as a function of time during electromigration until a steady state was reached. The measured compressive stress gradient between the cathode and the anode is much larger than what is needed to initiate Sn whisker growth. The effective charge number of {beta}-Sn derived from the electromigration data is in good agreement with the calculated value.

Modelling of the in situ stress state at Olkiluoto Site, Western Finland

International Nuclear Information System (INIS)

Valli, J.; Kuula, H.; Hakala, M.

2011-06-01

. Although some correlation to current measured in situ stress orientation and magnitude was found at specific depth levels, discrepancies exist. Glacial simulations demonstrated that viscous residual horizontal stresses can result in slip of BFZ in the top most part of the bedrock. The first 300 m of bedrock experienced heavy stress rotations as a result of glaciation whilst magnitudes were roughly the same, essentially a reset of in situ stress. Below this depth level stress magnitudes and trends were similar to those seen prior to loading. As a result of modelling the stress state at Olkiluoto can be considered to be heterogeneous up to a depth of roughly 300 m which is a result of the affects imposed by brittle deformation zones and glaciation. Below this depth principal stress orientations can be considered to match those expected from regional stress. Further studies may include the re-evaluation of core-logging results with the objective of using such parameters in modelling, if it is found necessary to attempt to simulate as realistic a situation as possible. (orig.)

Interpretation of the Haestholmen in situ state of stress based on core damage observations

International Nuclear Information System (INIS)

Hakala, M.

2000-01-01

At the Haestholmen investigation site, direct in situ stress measurements, overcoring and hydraulic fracturing have been unsuccessful because of ring disking and horizontal hydraulic fracturing. Prior to this study, a detailed study on both core disking and ring disking was made, and based on those results an in situ state of stress interpretation method was developed. In this work this method is applied to the Haestholmen site. The interpretation is based on disk fracture type, spacing and shape. Also, the Hoek-Brown strength envelope and Poisson's ratio of intact rock are needed. The interpretation result is most reliable if both core disking and ring disking information at the same depth levels is available. A detailed core logging showed that ring disking is systematic below the -365 m level in the vertical overcoring stress measurement hole, HH-KR6. On the other hand, no representative core disking exists except for two points in two differently oriented subvertical boreholes HH-KR2 and HHKR7. Because the interpretation has to be based on ring disking only, upper and lower estimates for the vertical stress were set. These were gravitational and 67% of gravitational. Furthermore, the in situ stress state was assumed to be in horizontal and vertical planes, because the disking in vertical borehole HH-KR6 was not inclined. The interpretation resulted in a good estimate for the major horizontal stress but none of the horizontal stress rations ( 0.25, 0.5, 0.75 and 1.0 ) or vertical stress assumptions studied are clearly more probable the others. At the 500 m level the resulting maximum horizontal stress is 41 MPa. If a linear fit through the zero depth and zero stress point is applied, the maximum horizontal stress gradient is 0.0818 z MPa/m with a standard deviation between 5 and 12 per cent. The orientation of the major horizontal stress is 108 with standard deviation of 21 degrees. The interpreted major horizontal stress state also indicated that systematic

A test case of the deformation rate analysis (DRA) stress measurement method

Energy Technology Data Exchange (ETDEWEB)

Dight, P.; Hsieh, A. [Australian Centre for Geomechanics, Univ. of WA, Crawley (Australia); Johansson, E. [Saanio and Riekkola Oy, Helsinki (Finland); Hudson, J.A. [Rock Engineering Consultants (United Kingdom); Kemppainen, K.

2012-01-15

As part of Posiva's site and ONKALO investigations, the in situ rock stress has been measured by a variety of techniques, including hydraulic fracturing, overcoring, and convergence measurements. All these techniques involve direct measurements in a drillhole or at the rock surface. An alternative method is to test drillhole core in a way that enables estimation of the magnitudes and orientations of the in situ rock stress. The Kaiser Effect (KE) and Deformation Rate Analysis (DRA) are two ways to do this. In the work reported here, a 'blind' DRA test was conducted on core obtained from the POSE (Posiva's Olkiluoto Spalling Experiment) niche in the ONKALO. The term 'blind' means that the two first authors of this report, who conducted the tests at the Australian Centre for Geomechanics, did not know the depths below surface at which the cores had been obtained. The results of this DRA Test Case are presented, together with an explanation of the DRA procedure. Also, additional information that would help in such DRA testing and associated analysis is explained. One of the problems in comparing the DRA results with the known Olkiluoto stress field is that the latter is highly variable across the site, as experienced by the previous in situ stress measurements and as predicted by numerical analysis. The variability is mainly caused by the presence of the large brittle deformation zones which perturb the local stress state. However, this variability reduces with depth and the stress field becomes more stable at the {approx} 350 m at which the drillhole cores were obtained. Another compounding difficulty is that the stress quantity, being a second order tensor, requires six independent components for its specification. In other words, comparison of the DRA results and the known stress field requires comparison of six different quantities. In terms of the major principal stress orientation, the DRA results predict an orientation completely

A test case of the deformation rate analysis (DRA) stress measurement method

International Nuclear Information System (INIS)

Dight, P.; Hsieh, A.; Johansson, E.; Hudson, J.A.; Kemppainen, K.

2012-01-01

As part of Posiva's site and ONKALO investigations, the in situ rock stress has been measured by a variety of techniques, including hydraulic fracturing, overcoring, and convergence measurements. All these techniques involve direct measurements in a drillhole or at the rock surface. An alternative method is to test drillhole core in a way that enables estimation of the magnitudes and orientations of the in situ rock stress. The Kaiser Effect (KE) and Deformation Rate Analysis (DRA) are two ways to do this. In the work reported here, a 'blind' DRA test was conducted on core obtained from the POSE (Posiva's Olkiluoto Spalling Experiment) niche in the ONKALO. The term 'blind' means that the two first authors of this report, who conducted the tests at the Australian Centre for Geomechanics, did not know the depths below surface at which the cores had been obtained. The results of this DRA Test Case are presented, together with an explanation of the DRA procedure. Also, additional information that would help in such DRA testing and associated analysis is explained. One of the problems in comparing the DRA results with the known Olkiluoto stress field is that the latter is highly variable across the site, as experienced by the previous in situ stress measurements and as predicted by numerical analysis. The variability is mainly caused by the presence of the large brittle deformation zones which perturb the local stress state. However, this variability reduces with depth and the stress field becomes more stable at the ∼ 350 m at which the drillhole cores were obtained. Another compounding difficulty is that the stress quantity, being a second order tensor, requires six independent components for its specification. In other words, comparison of the DRA results and the known stress field requires comparison of six different quantities. In terms of the major principal stress orientation, the DRA results predict an orientation completely different to the NW-SE regional

Microseism Induced by Transient Release of In Situ Stress During Deep Rock Mass Excavation by Blasting

Science.gov (United States)

Yang, Jianhua; Lu, Wenbo; Chen, Ming; Yan, Peng; Zhou, Chuangbing

2013-07-01

During deep rock mass excavation with the method of drill and blast, accompanying the secession of rock fragments and the formation of a new free surface, in situ stress on this boundary is suddenly released within several milliseconds, which is termed the transient release of in situ stress. In this process, enormous strain energy around the excavation face is instantly released in the form of kinetic energy and it inevitably induces microseismic events in surrounding rock masses. Thus, blasting excavation-induced microseismic vibrations in high-stress rock masses are attributed to the combined action of explosion and the transient release of in situ stress. The intensity of stress release-induced microseisms, which depends mainly on the magnitude of the in situ stress and the dimension of the excavation face, is comparable to that of explosion-induced vibrations. With the methods of time-energy density analysis, amplitude spectrum analysis, and finite impulse response (FIR) digital filter, microseismic vibrations induced by the transient release of in situ stress were identified and separated from recorded microseismic signals during a blast of deep rock masses in the Pubugou Hydropower Station. The results show that the low-frequency component in the microseismic records results mainly from the transient release of in situ stress, while the high-frequency component originates primarily from explosion. In addition, a numerical simulation was conducted to demonstrate the occurrence of microseismic events by the transient release of in situ stress, and the results seem to have confirmed fairly well the separated vibrations from microseismic records.

In Situ Investigation of the Evolution of Lattice Strain and Stresses in Austenite and Martensite During Quenching and Tempering of Steel

Science.gov (United States)

Villa, M.; Niessen, F.; Somers, M. A. J.

2018-01-01

Energy dispersive synchrotron X-ray diffraction was applied to investigate in situ the evolution of lattice strains and stresses in austenite and martensite during quenching and tempering of a soft martensitic stainless steel. In one experiment, lattice strains in austenite and martensite were measured in situ in the direction perpendicular to the sample surface during an austenitization, quenching, and tempering cycle. In a second experiment, the sin2 ψ method was applied in situ during the austenite-to-martensite transformation to distinguish between macro- and phase-specific micro-stresses and to follow the evolution of these stresses during transformation. Martensite formation evokes compressive stress in austenite that is balanced by tensile stress in martensite. Tempering to 748 K (475 °C) leads to partial relaxation of these stresses. Additionally, data reveal that (elastic) lattice strain in austenite is not hydrostatic but hkl dependent, which is ascribed to plastic deformation of this phase during martensite formation and is considered responsible for anomalous behavior of the 200 γ reflection.

Survey of horizontal stresses in coal mines from available measurements and mapping.

CSIR Research Space (South Africa)

Frith, R

2002-09-01

Full Text Available of work for the project was outlined in the proposal submitted to SIMRAC in mid-2000 and is summarised as follows: (i) to undertake a peer review of available in-situ stress measurements relating to the Witbank and Highveld coalfields in South Africa... OF HORIZONTAL STRESS IN THE WITBANK AND HIGHVELD COALFIELDS 21 4.1 Is Horizontal Stress at Work in Roadway Roof Behaviour? 21 4.2 Summary of Measured Horizontal Stresses 24 4.3 Proposed Model for the Origin of Horizontal Stress Within the Coalfields 27 4...

Comparison of residual stress measurement in thin films using surface micromachining method

International Nuclear Information System (INIS)

He, Q.; Luo, Z.X.; Chen, X.Y.

2008-01-01

Conductive, dielectric, semiconducting, piezoelectric and ferroelectric thin films are extensively used for MEMS/NEMS applications. One of the important parameters of thin films is residual stress. The residual stress can seriously affect the properties, performance and long-term stability of the films. Excessive compressive or tensile stress results in buckling, cracking, splintering and sticking problems. Stress measurement techniques are therefore essential for both process development and process monitoring. Many suggestions for stress measurement in thin films have been made over the past several decades. This paper is concentrated on the in situ stress measurement using surface micromachining techniques to determine the residual stress. The authors review and compare several types of stress measurement methods including buckling technique, rotating technique, micro strain gauge and long-short beam strain sensor

Study of the inhomogeneity of critical current under in-situ tensile stress for YBCO tape

Science.gov (United States)

Zhu, Y. P.; Chen, W.; Zhang, H. Y.; Liu, L. Y.; Pan, X. F.; Yang, X. S.; Zhao, Y.

2018-07-01

A Hall sensor system was used to measure the local critical current of YBCO tape with high spatial resolution under in-situ tensile stress. The hot spot generation and minimum quench energy of YBCO tape, which depended on the local critical current, was calculated through the thermoelectric coupling model. With the increase in tensile stress, the cracks which have different dimensions and critical current degradation arose more frequently and lowered the thermal stability of the YBCO tape.

Test with different stress measurement methods in two orthogonal bore holes in Aespoe HRL

Energy Technology Data Exchange (ETDEWEB)

Janson, Thomas; Stigsson, Martin [Golder Associates AB, Stockholm (Sweden)

2002-12-01

Within the scope of work, to provide the necessary rock mechanics support for the site investigations, SKB has studied some available pieces of equipment for in situ stress measurements in deep boreholes. A project with the objective to compare three different pieces of equipment for in situ stress measurements under similar conditions has been carried out. The main objective for the project is to compare the three different pieces of equipment for in situ stress measurements and find a strategy for SKB's Site Investigations to determine the state of stress in the rock mass. Two units of equipment use the overcoring method while the third uses the hydraulic fracturing method. The overcoring was performed by AECL, using Deep Door stopper Gauge System (DDGS), and SwedPower, using their triaxial strain measuring instrument (Borre Probe). MeSy Geo Systeme GmbH performed the hydraulic fracturing. The DDGS system is a new method to SKB while the experience of the SwedPower overcoring and the hydraulic fracturing methods are long. The tests were performed in the same orthogonal boreholes at Aespoe Hard Rock Laboratory (HRL), Oskarshamn, Sweden. The measured results have been verified against known conditions at the Aespoe HRL. The results from the three in situ stress measurement methods rose more questions than answers. Which illustrate the complexity to determine the in situ stresses in a rock mass. To understand the difference in results and answer the questions, it was necessary to do deeper investigations such as laboratory tests and theoretical calculations such as geological structure model, analysis of the influence of a nearby fracture, P-wave measurements, uniaxial tests on small cores from the HQ-3 core, theoretical and numerical analyses of the hole bottom (theoretical strains, stress concentrations and microcracking), auditing of DDGS measurements results and assumptions in the DDGS analyse and microscopy investigations on the cores. The following

Changes in In Situ Stress Across the Nankai and Cascadia Convergent Margins From Borehole Breakout Measurements During Ocean Drilling

Science.gov (United States)

McNeill, L.; Moore, J. C.; Yamada, Y.; Chang, C.; Tobin, H.; Kinoshita, M.; Gulick, S.; Moore, G.; Iodp Exp. 314/315/316 Science Party, &

2008-12-01

Borehole breakouts are commonly observed in borehole images shortly after drilling of continental margin sites. This study aims to compile and compare these results to determine what in situ shallow stress measurements can tell us about the larger scale tectonic regime. Recent Logging While Drilling resistivity images across the Kumano transect of the Nankai subduction zone, during Expedition 314, Stage 1 of the IODP NanTroSEIZE project, add to this dataset. Expedition 314 site data within the prism (C0001, C0004, C0006, including the megasplay fault system which may overlie the seismogenic updip limit) suggest maximum compressive stress (SHmax) is perpendicular to the margin (not parallel to the convergence vector) but is rotated through 90° at the forearc basin site (C0002). These results may point to changes in stress state of the shallow forearc from east to west: compression in the aseismic active prism (with evidence of strain partitioning of oblique convergence); and extension above the updip seismogenic zone suggesting focus of plate coupling at the plate boundary and not in the shallow forearc. Further south, ODP Leg 196 drilled the prism toe (808) with breakouts indicating SHmax parallel to the convergence vector, in contrast to Exp. 314 results. The stress state in the shallow prism at Site 808 may be affected by nearby seamount subduction or may represent differences in strain partitioning. On the Cascadia margin, two drilling legs have collected LWD borehole images (Leg 204 and Exp. 311). Leg 204 drilled 3 sites at hydrate ridge in the C Cascadia outer prism with breakout orientations variable between closely spaced sites. Prism fold axes are parallel to the margin so we might expect SHmax perpendicular to the margin as in Exp. 314. Deviations from this orientation may reflect local and surface effects (Goldberg and Janik, 2006). Exp. 311, N Cascadia, drilled 5 sites across the prism with breakouts in LWD images. Subduction is not oblique here, in

Determination of the in situ modulus of the rockmass by the use of backfill measurements

CSIR Research Space (South Africa)

Gurtunca, RG

1991-03-01

Full Text Available In situ measurements and numerical modelling based on elastic theory showed that backfill stresses are considerably higher than originally thought. This has led to a change in understanding of rockmass behaviour. After describing previous work...

In situ stress determination by the overcoring of large surface strain gauge rosettes on the walls of a raise-bored shaft at the Underground Research Laboratory

International Nuclear Information System (INIS)

Chandler, N.A.

1991-08-01

AECL Research is conducting a series of experiments to examine the influence of scale on measured in situ stresses in granite rock. The ventilation raise rosette overcoring experiment is one such test. This experiment, modelled on a previous test conducted in Australia, consisted of overcoring four 120-mm strain gauge rosettes glued to the surface of a 1.8-m-diameter bored raise. The in situ stresses were calculated from the measured strains using the equations for stresses around a cylindrical excavation in an elastic material. The possibility of excavation disturbance around the ventilation raise was investigated using overcore stress measurements, elastic modulus tests on retrieved core, and visual inspection of thin sections obtained from removed core. The effect of a stress-dependent elastic modulus (referred to as non-linear elastic behaviour) is also addressed. Results from the ventilation raise rosette overcoring experiment suggest that rosette overcoring in a bored raise is an acceptable stress-measurement method. The effects of scale and excavation damage on the stress measurements were not considered to be significant; however, if the elastic modulus of the rock is strongly stress-dependent, non-linear elastic behaviour may have a small effect on the measured stresses

Review of possible correlations between in situ stress and PFL fracture transmissivity data at Forsmark

Energy Technology Data Exchange (ETDEWEB)

Martin, Derek (University of Alberta (United States)); Follin, Sven (SF GeoLogic AB (Sweden))

2011-11-15

In laboratory samples, the fracture transmissivity decreases significantly as the confining stress increases. While these experimental relationships are widely accepted and validated on laboratory samples, it is unknown if such relationships exist in situ or if these relationships can be scaled from the centimetre-scale laboratory tests to the metre-scale of in situ fractures. The purpose of this work is to assess the relationship between the structural-hydraulic data gathered in deep, cored boreholes at Forsmark and the in situ stress state acting on the these fractures. In conclusion, there does not appear to be sufficient evidence from these analyses to support the notion that the magnitude of the flow along the fractures at Forsmark is solely controlled by the in situ stress acting on the fracture. This should not be surprising because the majority of the fractures formed more than 1 billion years ago and the current in situ stress state has only been active for the past 12 million years. It is more likely that the transmissivity values are controlled by fracture roughness, open channels within the fracture, fracture stiffness and fracture infilling material

In Situ TEM Electrical Measurements

DEFF Research Database (Denmark)

Canepa, Silvia; Alam, Sardar Bilal; Ngo, Duc-The

2016-01-01

understanding of complex physical and chemical interactions in the pursuit to optimize nanostructure function and device performance. Recent developments of sample holder technology for TEM have enabled a new field of research in the study of functional nanomaterials and devices via electrical stimulation...... influence the sample by external stimuli, e.g. through electrical connections, the TEM becomes a powerful laboratory for performing quantitative real time in situ experiments. Such TEM setups enable the characterization of nanostructures and nanodevices under working conditions, thereby providing a deeper...... and measurement of the specimen. Recognizing the benefits of electrical measurements for in situ TEM, many research groups have focused their effort in this field and some of these methods have transferred to ETEM. This chapter will describe recent advances in the in situ TEM investigation of nanostructured...

In situ measurement on TSV-Cu deformation with hotplate system based on sheet resistance

Science.gov (United States)

Sun, Yunna; Wang, Bo; Wang, Huiying; Wu, Kaifeng; Yang, Shengyong; Wang, Yan; Ding, Guifu

2017-12-01

The in situ measurement of TSVs deformation at different temperature is meaningful for learning more about the thermal deformation schemes of 3D TSVs in the microelectronic devices. An efficient and smart hotplate based on sheet resistance is designed for offering more heat, producing a uniform temperature distribution, relieving thermal stress and heat concentration issues, and reducing room space, which was optimized by the finite element method (FEM). The fabricated hotplate is efficient and smart (2.5 cm  ×  2.0 cm  ×  0.5 cm) enough to be located in the limited space during measuring. The thermal infrared imager was employed as the temperature sensor for monitoring the temperature distribution of TSVs sample. The 3D profilometry was adopted as the observer for TSVs profiles survey. The in situ 2D top surface profiles and 3D displacement profiles of TSVs sample at the different temperature were measured by 3D profilometer. The in situ average relative deformation and effective plastic deformation of the TSV sample were measured. With optical measurement method, 3D profilometry, the TSV sample can be tested repeatedly.

Local stress modification during in situ transmission electron microscopy straining experiments

Czech Academy of Sciences Publication Activity Database

Zárubová, Niva; Gemperle, Antonín; Gemperlová, Juliana

2007-01-01

Roč. 462, - (2007), s. 407-411 ISSN 0921-5093 R&D Projects: GA ČR GA202/04/2016 Institutional research plan: CEZ:AV0Z10100520 Keywords : in situ TEM straining, Local stress in a strained foil * local stress in a strained foil Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.457, year: 2007

A Hydraulic Stress Measurement System for Deep Borehole Investigations

Science.gov (United States)

Ask, Maria; Ask, Daniel; Cornet, Francois; Nilsson, Tommy

2017-04-01

Luleå University of Technology (LTU) is developing and building a wire-line system for hydraulic rock stress measurements, with funding from the Swedish Research Council and Luleå University of Technology. In this project, LTU is collaborating with University of Strasbourg and Geosigma AB. The stress state influences drilling and drillability, as well as rock mass stability and permeability. Therefore, knowledge about the state of in-situ stress (stress magnitudes, and orientations) and its spatial variation with depth is essential for many underground rock engineering projects, for example for underground storage of hazardous material (e.g. nuclear waste, carbon dioxide), deep geothermal exploration, and underground infrastructure (e.g. tunneling, hydropower dams). The system is designed to conduct hydraulic stress testing in slim boreholes. There are three types of test methods: (1) hydraulic fracturing, (2) sleeve fracturing and (3) hydraulic testing of pre-existing fractures. These are robust methods for determining in situ stresses from boreholes. Integration of the three methods allows determination of the three-dimensional stress tensor and its spatial variation with depth in a scientific unambiguously way. The stress system is composed of a downhole and a surface unit. The downhole unit consists of hydraulic fracturing equipment (straddle packers and downhole imaging tool) and their associated data acquisition systems. The testing system is state of the art in several aspects including: (1) Large depth range (3 km), (2) Ability to test three borehole dimensions (N=76 mm, H=96 mm, and P=122 mm), (3) Resistivity imager maps the orientation of tested fracture; (4) Highly stiff and resistive to corrosion downhole testing equipment; and (5) Very detailed control on the injection flow rate and cumulative volume is obtained by a hydraulic injection pump with variable piston rate, and a highly sensitive flow-meter. At EGU General Assembly 2017, we would like to

Finite Element Optimised Back Analysis of In Situ Stress Field and Stability Analysis of Shaft Wall in the Underground Gas Storage

Directory of Open Access Journals (Sweden)

Yifei Yan

2016-01-01

Full Text Available A novel optimised back analysis method is proposed in this paper. The in situ stress field of an underground gas storage (UGS reservoir in a Turkey salt cavern is analysed by the basic theory of elastic mechanics. A finite element method is implemented to optimise and approximate the objective function by systematically adjusting boundary loads. Optimising calculation is performed based on a novel method to reduce the error between measurement and calculation as much as possible. Compared with common back analysis methods such as regression method, the method proposed can further improve the calculation precision. By constructing a large circular geometric model, the effect of stress concentration is eliminated and a minimum difference between computed and measured stress can be guaranteed in the rectangular objective region. The efficiency of the proposed method is investigated and confirmed by its capability on restoring in situ stress field, which agrees well with experimental results. The characteristics of stress distribution of chosen UGS wells are obtained based on the back analysis results and by applying the corresponding fracture criterion, the shaft walls are proven safe.

Development of in-situ rock shear test under low compressive to tensile normal stress

International Nuclear Information System (INIS)

Nozaki, Takashi; Shin, Koichi

2003-01-01

The purpose of this study is to develop an in-situ rock shear testing method to evaluate the shear strength under low normal stress condition including tensile stress, which is usually ignored in the assessment of safety factor of the foundations for nuclear power plants against sliding. The results are as follows. (1) A new in-situ rock shear testing method is devised, in which tensile normal stress can be applied on the shear plane of a specimen by directly pulling up a steel box bonded to the specimen. By applying the counter shear load to cancel the moment induced by the main shear load, it can obtain shear strength under low normal stress. (2) Some model tests on Oya tuff and diatomaceous mudstone have been performed using the developed test method. The shear strength changed smoothly from low values at tensile normal stresses to higher values at compressive normal stresses. The failure criterion has been found to be bi-linear on the shear stress vs normal stress plane. (author)

Determination of in-situ rock stresses related to petroleum activities on the Norwegian Continental Shelf

Energy Technology Data Exchange (ETDEWEB)

Fejerskov, Morten

1996-12-31

In-situ rock stresses have proved to be important for exploration and production of hydrocarbons. This thesis uses various stress determination techniques to characterize the in-situ stress field on the Norwegian Continental Shelf. Leak off tests and borehole breakouts have been used to determine the in-situ stress in deep well bores. Overcoring and earthquake focal mechanisms data have also been compiled and evaluated together with stress information from petroleum wells. A new test procedure is suggested to improve the quality of leak off tests that emphasises the importance of accurate pressure determination, longer test periods and digital data sampling. Four-arm calliper logs are used to identify borehole breakouts on the Tampen Spur and Horda Platform. However, it proved difficult to distinguish borehole breakouts from other drilling processes since the elongations of the borehole consistently appeared in the direction of hole azimuth; drilling-induced key seats are here observed in vertical wells. This behaviour is discussed but not fully understood. This reduces the number of reliable stress data and their quality enormously and even casts some doubt about the quality of previous breakout studies from the North Sea. A highly compressive horizontal stress field seems to be present onshore and offshore Norway. Different stress determination techniques yield very consistent stress orientation, regional and internal variation. A 1. order stress direction is identified, where the maximum horizontal stress direction is rotating from N-S in the Barents Sea to NW-SE in the Norwegian Sea and WNW-ESE in the northern North Sea. At Tampen Spur, a dominant WNW-ESE maximum horizontal stress direction, normal to the major tectonic structures is identified as well as a minimum stress close to the vertical stress, the latter indicating high horizontal stresses. 250 refs., 91 figs., 14 tabs.

From point-wise stress data to a continuous description of the 3D crustal in situ stress state

Science.gov (United States)

Heidbach, O.; Ziegler, M.; Reiter, K.; Hergert, T.

2017-12-01

The in situ stress is a key parameter for the safe and sustainable management of geo-reservoirs or storage of waste and energy in deep geological repositories. It is also an essential initial condition for thermo-hydro-mechanical (THM) models that investigate man-made induced processes e.g. seismicity due to fluid injection/extraction, reservoir depletion or storage of heat producing high-level radioactive waste. Without a reasonable assumption on the initial stress condition it is not possible to assess if a man-made process is pushing the system into a critical state or not. However, modelling the initial 3D stress state on reservoir scale is challenging since data are hardly available before drilling in the area of interest. This is in particular the case for the stress magnitude data which are a prerequisite for a reliable model calibration. Here, we present a multi-stage 3D geomechani­cal-numerical model approach to estimate for a reservoir-scale volume the 3D in situ stress state. First, we set up a large-scale model which is calibrated by stress data and use the modelled stress field subsequently to calibrate a small-scale model located within the large-scale model. The local model contains a significantly higher resolution representation of the subsurface geometry around boreholes of a projected geothermal power plant. This approach incorporates two models and is an alternative to the required trade-off between resolution, computational cost and calibration data which is inevitable for a single model; an extension to a three-stage approach would be straight forward. We exemplify the two-stage approach for the area around Munich in the German Molasse Basin. The results of the reservoir-scale model are presented in terms of values for slip tendency as a measure for the criticality of fault reactivation. The model results show that variations due to uncertainties in the input data are mainly introduced by the uncertain material properties and missing

Effective X-ray elastic constant measurement for in situ stress measurement of biaxially strained AA5754-O

International Nuclear Information System (INIS)

Iadicola, Mark A.; Gnäupel-Herold, Thomas H.

2012-01-01

Accurate measurement of stresses by X-ray diffraction requires accurate X-ray elastic constants. Calibration experiments are one method to determine these for a specific material in a specific condition. In this paper, uniaxial tension experiments are used to investigate the variation of these constants after uniaxial and equal-biaxial plastic deformation for an aluminum alloy (AA5754-O) of interest to the automotive industry. These data are critical for accurate measurement of the biaxial mechanical properties of the material using a recent experimental method combining specialized sheet metal forming equipment with portable X-ray diffraction equipment. The measured effective X-ray elastic constants show some minor variation with increased plastic deformation, and this behavior was found to be consistent for both uniaxially and equal-biaxially strained samples. The use of two average values for effective X-ray elastic constants, one in the rolling direction and one transverse to the rolling direction of the sheet material, is shown to be of sufficient accuracy for the combined tests of interest. Comparison of uniaxial data measured using X-ray diffraction and standard methods show good agreement, and biaxial stress–strain results show good repeatability. Additionally, the calibration data show some non-linear behavior, which is analyzed in regards to crystallographic texture and intergranular stress effects. The non-linear behavior is found to be the result of intergranular stresses based on comparison with additional measurements using other X-ray diffraction equipment and neutron diffraction.

Intercomparison of MODIS Albedo Retrievals and In Situ Measurements Across the Global FLUXNET Network

Science.gov (United States)

Cescatti, Alessandro; Marcolla, Barbara; Vannan, Suresh K. Santhana; Pan, Jerry Yun; Roman, Miguel O.; Yang, Xiaoyuan; Ciais, Philippe; Cook, Robert B.; Law, Beverly E.; Matteucci, Girogio;

In situ micro Raman spectroscopy for characterization of oxide film formed on the new surface and for measurements of the stress of oxide film formed on 304L stainless steel

Energy Technology Data Exchange (ETDEWEB)

Kai, A.; Takegoshi, M.; Shoji, T. [Fracture Research Inst., Tohoku Univ., Sendai (Japan)

2004-07-01

Environmentally assisted cracking (EAC) consists of two distinct events viz., i) crack initiation and ii) crack propagation. On a smooth surface, the EAC initiates by the rupture or by the degradation of the surface film due to the combined action of stress and an electrochemical reaction of the materials with the environment. The mechanical properties of the surface oxide films are also important considerations when determining the susceptibility to EAC. In this research, Micro Raman Spectroscopy (MRS) was applied for in-situ oxides characterization and for in-situ measurements of the stress in oxide film formed on the surface of 304L stainless steel during the scratching electrode and the slow strain rate test (SSRT), respectively. The passive oxide film growth formed on the bare surface was continuously monitored by MRS as a function of time. For stress measurements, Cr{sub 2}O{sub 3} was focused on and raman shift at Cr{sub 2}O{sub 3} peak of Raman spectrum was measured continuously. The strain rate was 8.2 x 10{sup -7}/sec. In the initial stage of SSRT, the Raman shift of surface film decreased gradually with strain. At 5% strain, the Raman shift of surface film increased rapidly to around the initial value of Raman shift. It is considered that the surface film was ruptured at this time. At 5% strain, the shift value of Raman peak of Cr{sub 2}O{sub 3} reached to 5 cm{sup -1}. This value (5 cm{sup -1}) corresponds to 1.2 GPa which value of tensile stress is calculated from reference data. These characteristics of oxide film will be implemented into the theoretical formulation of EAC and their implication to EAC growth rate will be discussed. (orig.)

Residual stress evaluation in brittle coatings using indentation technique combined with in-situ bending

International Nuclear Information System (INIS)

Futakawa, Masatoshi; Steinbrech, R.W.; Tanabe, Yuji; Hara, Toshiaki

2000-01-01

The indentation crack length approach was adopted and further elaborated to evaluate residual stress and toughness of the brittle coatings: two kinds of glass coatings on steel. The influence of the residual stress on indentation cracking was examined in as-received coating condition and by in-situ superimposing a counteracting tensile stress. For purpose of providing reference toughness values stress-free pieces of separated coating material have also been examined. Thus results of the two complementary sets of experiments were assumed to prove self-consistently toughness and residual stress data of the coating. In particular, the in-situ bending of specimen in combination with the indentation test allowed us to vary deliberately the residual stress situation in glass coating. Thus experiments which utilized the combination of bending test and micro-indentation were introduced as a method to provide unambiguous information about residual compressive stress. Toughness and residual compressive stress of glass coatings used in this study were 0.46-0.50 MPa·m 1/2 and 94-111 MPa, respectively. Furthermore, a thermoelastic calculation of the residual compressive stress was performed and it is found that the value of residual compressive stress at coating surface of specimen was 90-102 MPa. (author)

Study of 3-D stress development in parent and twin pairs of a hexagonal close-packed polycrystal: Part I - In-situ three-dimensional synchrotron X-ray diffraction measurement

DEFF Research Database (Denmark)

Abdolvand, Hamidreza; Majkut, Marta; Oddershede, Jette

2015-01-01

to reconstruct the 3D microstructure and statistically study neighborhood effects on the load sharing. The investigated volume of the sample contained 6132 grains initially, yet as a result of twin formation, 9724 grains were measured in the same volume at the last loading step. It is shown that the most favored......) microscopy. In-situ uniaxial straining was carried out at seven steps up to 2.7% in the macroscopic direction that favors twin formation, while center-of-mass position, crystallographic orientation, elastic strain, stress, and relative volume of each grain were measured. This information was used...

In situ measurement of conductivity during nanocomposite film deposition

International Nuclear Information System (INIS)

Blattmann, Christoph O.; Pratsinis, Sotiris E.

2016-01-01

Highlights: • Flame-made nanosilver dynamics are elucidated in the gas-phase & on substrates. • The resistance of freshly depositing nanosilver layers is monitored. • Low T g polymers facilitate rapid synthesis of conductive films. • Conductive nanosilver films form on top of or within the polymer depending on MW. - Abstract: Flexible and electrically conductive nanocomposite films are essential for small, portable and even implantable electronic devices. Typically, such film synthesis and conductivity measurement are carried out sequentially. As a result, optimization of filler loading and size/morphology characteristics with respect to film conductivity is rather tedious and costly. Here, freshly-made Ag nanoparticles (nanosilver) are made by scalable flame aerosol technology and directly deposited onto polymeric (polystyrene and poly(methyl methacrylate)) films during which the resistance of the resulting nanocomposite is measured in situ. The formation and gas-phase growth of such flame-made nanosilver, just before incorporation onto the polymer film, is measured by thermophoretic sampling and microscopy. Monitoring the nanocomposite resistance in situ reveals the onset of conductive network formation by the deposited nanosilver growth and sinternecking. The in situ measurement is much faster and more accurate than conventional ex situ four-point resistance measurements since an electrically percolating network is detected upon its formation by the in situ technique. Nevertheless, general resistance trends with respect to filler loading and host polymer composition are consistent for both in situ and ex situ measurements. The time lag for the onset of a conductive network (i.e., percolation) depends linearly on the glass transition temperature (T g ) of the host polymer. This is attributed to the increased nanoparticle-polymer interaction with decreasing T g . Proper selection of the host polymer in combination with in situ resistance monitoring

Measurement of lattice rotations and internal stresses in over one hundred individual grains during a stress-induced martensitic transformation

Directory of Open Access Journals (Sweden)

Hachi Younes El

2015-01-01

Full Text Available To better understand the properties of polycrystals at a microscopic scale during cyclic mechanical loading we have measured the relationship between grain orientations, their positions inside the sample and their internal stresses. In this work, in-situ 3DXRD technique was performed on over hundred grains during the stress-induced martensitic transformation in a Cu-Al-Be shape memory alloy. Information about the position, orientation, and stress field was obtained for each austenitic grain. These results have been used to develop a procedure that allows automatic processing for a large number of grains, matching them during loading and leads to a quantitative stress field. A strong heterogeneity of stress state between the grains at the surface and in the volume is evident.

In-situ measurement of texture and elastic strains with HIPPO-CRATES

International Nuclear Information System (INIS)

Hartig, Ch.; Vogel, S.C.; Mecking, H.

2006-01-01

In this paper, the micromechanical interaction between constituents of a metallic material during elastic and plastic deformation are analyzed by comparing experimental results with modeling predictions. This comparison aims at determining the locally acting internal stresses, the spatial distribution of strains and the rules allowing deriving the macroscopic behavior of the material from the behavior of its microscopic constituents. We report the application of a new deformation apparatus CRATES, which allows measuring texture and crystal lattice spacings, and from these crystal lattice strains, using neutron diffraction. From the in-situ measured elastic lattice strains ε hkl the corresponding local stresses can be derived. The deformation apparatus allows uni-axial tensile or compressive deformation up to 100 kN and is specifically designed for use in the HIPPO neutron time-of-flight diffractometer. In this paper, we report initial results on an iron-copper model system (Fe100, Fe33Cu67, Fe67Cu33, vol.%) and commercial magnesium alloys (Mg-AZ31 and Mg-AZ80). Finite element calculations using a crystal-plastic constitutive law, allowing for shear and hardening of crystallographic slip-systems, were used for the interpretation of the measurements

A methodology for interpretation of overcoring stress measurements in anisotropic rock

International Nuclear Information System (INIS)

Hakala, M.; Sjoeberg, J.

2006-11-01

The in situ state of stress is an important parameter for the design of a repository for final disposal of spent nuclear fuel. This report presents work conducted to improve the quality of overcoring stress measurements, focused on the interpretation of overcoring rock stress measurements when accounting for possible anisotropic behavior of the rock. The work comprised: (i) development/upgrading of a computer code for calculating stresses from overcoring strains for anisotropic materials and for a general overcoring probe configuration (up to six strain rosettes with six gauges each), (ii) development of a computer code for determining elastic constants for transversely isotropic rocks from biaxial testing, and (iii) analysis of case studies of selected overcoring measurements in both isotropic and anisotropic rocks from the Posiva and SKB sites in Finland and Sweden, respectively. The work was principally limited to transversely isotropic materials, although the stress calculation code is applicable also to orthotropic materials. The developed computer codes have been geared to work primarily with the Borre and CSIRO HI three-dimensional overcoring measurement probes. Application of the codes to selected case studies, showed that the developed tools were practical and useful for interpreting overcoring stress measurements conducted in anisotropic rock. A quantitative assessment of the effects of anisotropy may thus be obtained, which provides increased reliability in the stress data. Potential gaps in existing data and/or understanding can also be identified. (orig.)

Stress–rupture measurements of cast magnesium strengthened by in-situ production of ceramic particles

Directory of Open Access Journals (Sweden)

Nagaraj M. Chelliah

2017-06-01

Full Text Available We have introduced a polymer precursor into molten magnesium and then in-situ pyrolyzed to produce castings of metal matrix composites (P-MMCs containing silicon-carbonitride (SiCNO ceramic particles. Stress-rupture measurements of as-cast P-MMCs was performed at 350 °C (0.69TM to 450 °C (0.78TM under dead load condition corresponding to tensile stress of 2.5 MPa to 20 MPa. The time-to-fracture data were analyzed using the classical Monkman–Grant equation. The time-to-fracture is thermally activated and follows a power-law stress exponent exhibiting dislocation creep. Fractography analysis revealed that while pure magnesium appears to fracture by dislocation slip, the P-MMCs fail from the nucleation and growth of voids at the grain boundaries.

Test plan for suitability assessment of five overcoring stress measurement techniques

International Nuclear Information System (INIS)

Gregory, E.C.; Rundle, T.A.; McCabe, W.M.; Kim, K.

1982-08-01

Tests are to be conducted at the Near-Surface Test Facility (NSTF) to assess the suitability of five overcoring techniques for in situ stress determination in a jointed basalt. The overcoring methods to be investigated use the following instrumentation to measure strain relief by overcoring a pilot borehole: USBM borehole deformation gage, CSIRO hollow inclusion stress cell, cast epoxy inclusion, the Lulea triaxial strain cell and the ''doorstopper'' biaxial strain cell. The tests are to provide data regarding the state of stress below the NSTF. This information is to be used in the evaluation of each method of overcoring. During the course of field testing, an attempt is to be made to adapt conventional overcoring techniques and analytical methods to the basalt medium. If overcoring stress determination in basalt is shown suitable, then additional studies will be identified to further adapt a technique for use at depth. In addition to the five overcoring techniques to be tested at the NSTF, stress measurements by Hydrofracturing are to be conducted to provide data for direct comparison with overcoring results. 16 refs., 18 figs

Influence of Steel Reinforcement on In-Situ Stress Evaluation in Concrete Structures by the Core-Drilling Method

International Nuclear Information System (INIS)

McGinnis, M. J.; Pessiki, S.

2006-01-01

The core-drilling method is an emerging technique for evaluating in-situ stress in a concrete structure. A small hole is drilled into the structure, and the deformations in the vicinity of the hole are measured and related via elasticity theory to the stress. The method is similar to the ASTM hole-drilling strain-gauge method excepting that displacements rather than strains are the measured quantities. The technique may be considered nondestructive since the ability of the structure to perform its function is unaffected, and the hole is easily repaired. Displacement measurements in the current work are performed using 3D digital image correlation and industrial photogrammetry. The current paper addresses perturbations in the method caused by steel reinforcement within the concrete. The reinforcement is significantly stiffer than the surrounding concrete, altering the expected displacement field. A numerical investigation performed indicates an under-prediction of stress by as much as 18 percent in a heavily reinforced structure, although the effect is significantly smaller for more common amounts of reinforcement

Influence of Steel Reinforcement on In-Situ Stress Evaluation in Concrete Structures by the Core-Drilling Method

Science.gov (United States)

McGinnis, M. J.; Pessiki, S.

2006-03-01

The core-drilling method is an emerging technique for evaluating in-situ stress in a concrete structure. A small hole is drilled into the structure, and the deformations in the vicinity of the hole are measured and related via elasticity theory to the stress. The method is similar to the ASTM hole-drilling strain-gauge method excepting that displacements rather than strains are the measured quantities. The technique may be considered nondestructive since the ability of the structure to perform its function is unaffected, and the hole is easily repaired. Displacement measurements in the current work are performed using 3D digital image correlation and industrial photogrammetry. The current paper addresses perturbations in the method caused by steel reinforcement within the concrete. The reinforcement is significantly stiffer than the surrounding concrete, altering the expected displacement field. A numerical investigation performed indicates an under-prediction of stress by as much as 18 percent in a heavily reinforced structure, although the effect is significantly smaller for more common amounts of reinforcement.

Temperature-dependency analysis and correction methods of in-situ power-loss estimation for crystalline silicon modules undergoing potential-induced degradation stress testing

DEFF Research Database (Denmark)

Spataru, Sergiu; Hacke, Peter; Sera, Dezso

2015-01-01

We propose a method of in-situ characterization of the photovoltaic module power at standard test conditions using superposition of the dark current-voltage (I-V) curve measured at elevated stress temperature during potential-induced degradation (PID) testing. PID chamber studies were performed o...

Steel research using neutron beam techniques. In-situ neutron diffraction, small-angle neutron scattering and residual stress analysis

International Nuclear Information System (INIS)

Sueyoshi, Hitoshi; Ishikawa, Nobuyuki; Yamada, Katsumi; Sato, Kaoru; Nakagaito, Tatsuya; Matsuda, Hiroshi; Arakaki, Yu; Tomota, Yo

2014-01-01

Recently, the neutron beam techniques have been applied for steel researches and industrial applications. In particular, the neutron diffraction is a powerful non-destructive method that can analyze phase transformation and residual stress inside the steel. The small-angle neutron scattering is also an effective method for the quantitative evaluation of microstructures inside the steel. In this study, in-situ neutron diffraction measurements during tensile test and heat treatment were conducted in order to investigate the deformation and transformation behaviors of TRIP steels. The small-angle neutron scattering measurements of TRIP steels were also conducted. Then, the neutron diffraction analysis was conducted on the high strength steel weld joint in order to investigate the effect of the residual stress distribution on the weld cracking. (author)

Model test study on propagation law of plane stress wave in jointed rock mass under different in-situ stresses

Science.gov (United States)

Dong, Qian

2017-12-01

The study of propagation law of plane stress wave in jointed rock mass under in-situ stress has important significance for safety excavation of underground rock mass engineering. A model test of the blasting stress waves propagating in the intact rock and jointed rock mass under different in-situ stresses was carried out, and the influencing factors on the propagation law, such as the scale of static loads and the number of joints were studied respectively. The results show that the transmission coefficient of intact rock is larger than that of jointed rock mass under the same loading condition. With the increase of confining pressure, the transmission coefficients of intact rock and jointed rock mass both show an trend of increasing first and then decreasing, and the variation of transmission coefficients in intact rock is smaller than that of jointed rock mass. Transmission coefficient of jointed rock mass decreases with the increase of the number of joints under the same loading condition, when the confining pressure is relatively small, the reduction of transmission coefficients decreases with the increasing of the number of joints, and the variation law of the reduction of transmission coefficients is contrary when the confining pressure is large.

Stress-dependent crystal structure of lanthanum strontium cobalt ferrite by in situ synchrotron X-ray diffraction

Science.gov (United States)

Geiger, Philipp T.; Khansur, Neamul H.; Riess, Kevin; Martin, Alexander; Hinterstein, Manuel; Webber, Kyle G.

2018-02-01

Lanthanum strontium cobalt ferrite La1-xSrxCo1-yFeyO3-δ (LSCF) is one of the most studied mixed ionic-electronic conductor materials due to electrical and transport properties, which are attractive for intermediate temperature solid oxide fuel cells (SOFCs), oxygen permeation membranes, and catalysis. The integration of such materials, however, depends on the thermal as well as mechanical behavior. LSCF exhibits nonlinear hysteresis during compressive stress-strain measurements, marked by a remanent strain and coercive stress, i.e., ferroelasticity. However, the origin of ferroelastic behavior has not been investigated under high compressive stress. This study, therefore, investigates the microscopic origin of stress-induced mechanical behavior in polycrystalline (La0.6Sr0.4)0.95Co0.2Fe0.8O3-δ using in situ synchrotron x-ray diffraction. The data presented here reveals that the strain response originates from the intrinsic lattice strain as well as the extrinsic domain switching strain without any apparent change in crystallographic symmetry. A comparison of the calculated microscopic strain contribution with that of a macroscopic measurement indicates a significant change in the relative contributions of intrinsic and extrinsic strain depending on the applied stress state, i.e., under maximum stress and after unloading. Direct evidence of the microscopic origin of stress-strain response outlined in this paper may assist in guiding materials design with the improved mechanical reliability of SOFCs.

Internal Stress Distribution Measurement of TIG Welded SUS304 Samples Using Neutron Diffraction Technique

Science.gov (United States)

Muslih, M. Refai; Sumirat, I.; Sairun; Purwanta

2008-03-01

The distribution of residual stress of SUS304 samples that were undergone TIG welding process with four different electric currents has been measured. The welding has been done in the middle part of the samples that was previously grooved by milling machine. Before they were welded the samples were annealed at 650 degree Celsius for one hour. The annealing process was done to eliminate residual stress generated by grooving process so that the residual stress within the samples was merely produced from welding process. The calculation of distribution of residual stress was carried out by measuring the strains within crystal planes of Fe(220) SUS304. Strain, Young modulus, and Poisson ratio of Fe(220) SUS304 were measured using DN1-M neutron diffractometer. Young modulus and Poisson ratio of Fe(220) SUS304 sample were measured in-situ. The result of calculations showed that distribution of residual stress of SUS304 in the vicinity of welded area is influenced both by treatments given at the samples-making process and by the electric current used during welding process.

Micromechanics of deformation of metallic-glass-matrix composites from in situ synchrotron strain measurements and finite element modeling

International Nuclear Information System (INIS)

Ott, R.T.; Sansoz, F.; Molinari, J.F.; Almer, J.; Ramesh, K.T.; Hufunagel, T.C.

2005-01-01

In situ X-ray scattering and finite element modeling (FEM) were used to examine the micromechanics of deformation of in situ formed metallic-glass-matrix composites consisting of Ta-rich particles dispersed in an amorphous matrix. The strain measurements show that under uniaxial compression the second-phase particles yield at an applied stress of approx. 325 MPa. After yielding, the particles do not strain harden significantly; we show that this is due to an increasingly hydrostatic stress state arising from the lateral constraint on deformation of the particles imposed by the elastic matrix. Shear band initiation in the matrix is not due to the difference in elastic properties between the matrix and the particles. Rather, the development of a plastic misfit strain causes stress concentrations around the particles, resulting in localized yielding of the matrix by shear band formation at an applied stress of approx. 1450 MPa, considerably lower than the macroscopic yield stress of the composite (approx. 1725 MPa). Shear bands do not propagate at the lower stress because the yield criterion of the matrix is only satisfied in the region immediately around the particles. At the higher stresses, the yield criterion is satisfied in large regions of the matrix, allowing extensive shear band propagation and significant macroscopic plastic deformation. However, the presence of the particles makes the stress state highly inhomogeneous, which may partially explain why fracture is suppressed in the composite, allowing the development of large plastic strains

Kinematic analysis of in situ measurement during chemical mechanical planarization process

Energy Technology Data Exchange (ETDEWEB)

Li, Hongkai; Wang, Tongqing; Zhao, Qian; Meng, Yonggang; Lu, Xinchun, E-mail: xclu@tsinghua.edu.cn [State Key Laboratory of Tribology, Tsinghua University, Beijing 100084 (China)

2015-10-15

Chemical mechanical planarization (CMP) is the most widely used planarization technique in semiconductor manufacturing presently. With the aid of in situ measurement technology, CMP tools can achieve good performance and stable productivity. However, the in situ measurement has remained unexplored from a kinematic standpoint. The available related resources for the kinematic analysis are very limited due to the complexity and technical secret. In this paper, a comprehensive kinematic analysis of in situ measurement is provided, including the analysis model, the measurement trajectory, and the measurement time of each zone of wafer surface during the practical CMP process. In addition, a lot of numerical calculations are performed to study the influences of main parameters on the measurement trajectory and the measurement velocity variation of the probe during the measurement process. All the efforts are expected to improve the in situ measurement system and promote the advancement in CMP control system.

Feasibility of in situ beta ray measurements in underwater environment.

Science.gov (United States)

Park, Hye Min; Park, Ki Hyun; Kang, Sung Won; Joo, Koan Sik

2017-09-01

We describe an attempt at the development of an in situ detector for beta ray measurements in underwater environment. The prototype of the in situ detector is based on a CaF2: Eu scintillator using crystal light guide and Si photomultiplier. Tests were conducted using various reference sources for evaluating the linearity and stability of the detector in underwater environment. The system is simple and stable for long-term monitoring, and consumes low power. We show here an effective detection distance of 7 mm and a 2.273 MeV end-point energy spectrum of 90 Sr/ 90 Y when using the system underwater. The results demonstrate the feasibility of in situ beta ray measurements in underwater environment and can be applied for designing an in situ detector for radioactivity measurement in underwater environment. The in situ detector can also have other applications such as installation on the marine monitoring platform and quantitative analysis of radionuclides. Copyright © 2017 Elsevier Ltd. All rights reserved.

Impact of In Situ Stress Distribution Characteristics on Jointed Surrounding Rock Mass Stability of an Underground Cavern near a Hillslope Surface

Directory of Open Access Journals (Sweden)

Bangxiang Li

2017-01-01

Full Text Available In this paper, a series of numerical simulations are performed to analyze the in situ stress distribution characteristics of the rock mass near different slope angles hillslope surfaces, which are subjected to the vertical gravity stress and different horizontal lateral stresses and the influence which the in situ stress distribution characteristics of 45° hillslope to the integral stability of surrounding rock mass when an underground cavern is excavated considering three different horizontal distances from the underground cavern to the slope surface. It can be concluded from the numerical results that different slope angles and horizontal lateral stresses have a strong impact on the in situ stress distribution and the integral surrounding rock mass stability of the underground cavern when the horizontal distance from the underground cavern to the slope surface is approximately 100 m to 200 m. The relevant results would provide some important constructive suggestions to the engineering site selection and optimization of large-scale underground caverns in hydropower stations.

Hysteresis in YHx films observed with in situ measurements

International Nuclear Information System (INIS)

Remhof, A.; Kerssemakers, J.W.J.; Molen, S.J. van der; Griessen, R.; Kooij, E.S.

2002-01-01

Giant hysteretic effects in the YH x hydrogen switchable mirror system are observed between x=1.9 and x=3 in pressure composition isotherms, optical and electrical properties, and mechanical stress. Polycrystalline Y films are studied by simultaneous in situ measurements of electrical resistivity, optical transmittance and x-ray diffractometry. These experiments are linked to optical microscopy of the samples. During hydrogen loading above x=1.9 the films stay in the metallic fcc phase until the optical transmittance reaches its minimum and the electrical resistance curve exhibits a characteristic feature at x=2.1. Upon further loading the system crosses the miscibility gap in which the fcc phase coexists with the hcp phase before hydrogen saturation is reached in the pure hcp phase. While the fcc phase stays at a concentration of x=2.1 in the coexistence region during loading, it remains at a concentration of x=1.9 during unloading. The hysteretic effects observed in optical transmission and electrical resistivity result from the different properties of the low concentration fcc phase YH 1.9 and the high concentration fcc phase YH 2.1 . They can be explained on the basis of the bulk phase diagram if the different stress states during loading and unloading are taken into account. These results contradict earlier interpretations of the hysteresis in thin film YH x , based on nonsimultaneous measurements of the optical and structural properties on different films

Literature survey: Relations between stress change, deformation and transmissivity for fractures and deformation zones based on in situ investigations

Energy Technology Data Exchange (ETDEWEB)

Fransson, Aasa (Chalmers Univ. of Technology, Goeteborg (Sweden))

2009-02-15

likely explanations. To conclude, impact of normal stress change and deformation on transmissivity could be described based on data from in situ investigations. The results shown in this compilation present a possibility to estimate normal stiffness, k{sub n} and hydraulic aperture, b{sub h} based on storage coefficient, S, and transmissivity, T, from hydraulic interference tests performed in the area of interest. Concerning the impact of shear stress and displacement on transmissivity, no detailed field data was found. This is in line with the comment by Guglielmi et al. where the authors express an urgent need to develop in situ measurements of both normal and shear displacements. An important future issue is therefore better descriptions of the dependency between shear displacement and transmissivity in the field. Further research within the area of hydromechanical coupling where geology, hydrogeology and geomechanics meet is likely to increase the understanding of all these areas

Identification of natural fractures and in situ stress at Rantau Dedap geothermal field

Science.gov (United States)

Artyanto, Andika; Sapiie, Benyamin; Idham Abdullah, Chalid; Permana Sidik, Ridwan

2017-12-01

Rantau Dedap Area is a geothermal field which is located in Great Sumatra Fault (GSF). The fault and fracture are main factor in the permeability of the geothermal system. However, not all faults and fractures have capability of to flow the fluids. Borehole image log is depiction of the borehole conditions, it is used to identify the natural fractures and drilling induced fracture. Both of them are used to identify the direction of the fracture, direction of maximum horizontal stress (SHmax), and geomechanics parameters. The natural fractures are the results of responses to stress on a rock and permeability which controlling factor in research area. Breakouts is found in this field as a trace of drilling induced fracture due to in situ stress work. Natural fractures are strongly clustered with true strike trending which first, second, and third major direction are N170°E - N180°E (N-S), N60°E - N70°E (NE-SW), and N310°E - N320°E (NW-SE), while the dominant dip is 80° -90°. Based on borehole breakout analysis, maximum horizontal stress orientation is identified in N162°E - N204°E (N-S) and N242°E (NE-SW) direction. It’s constantly similar with regional stress which is affected by GSF. Several parameters have been identified and analyzed are SHmax, SHmin, and Sy. It can be concluded that Rantau Dedap Geothermal Field is affected by strike-slip regime. The determination of in situ stress and natural fractures are important to study the pattern of permeability which is related to the fault in reservoir of this field.

The Interplay of In Situ Stress Ratio and Transverse Isotropy in the Rock Mass on Prestressed Concrete-Lined Pressure Tunnels

Science.gov (United States)

Simanjuntak, T. D. Y. F.; Marence, M.; Schleiss, A. J.; Mynett, A. E.

2016-11-01

This paper presents the mechanical and hydraulic behaviour of passively prestressed concrete-lined pressure tunnels embedded in elastic transversely isotropic rocks subjected to non-uniform in situ stresses. Two cases are distinguished based on whether the in situ vertical stress in the rock mass is higher, or lower than the in situ horizontal stress. A two-dimensional finite element model was used to study the influence of dip angle, α, and horizontal-to-vertical stress ratio, k, on the bearing capacity of prestressed concrete-lined pressure tunnels. The study reveals that the in situ stress ratio and the orientation of stratifications in the rock mass significantly affect the load sharing between the rock mass and the lining. The distribution of stresses and deformations as a result of tunnel construction processes exhibits a symmetrical pattern for tunnels embedded in a rock mass with either horizontal or vertical stratification planes, whereas it demonstrates an unsymmetrical pattern for tunnels embedded in a rock mass with inclined stratification planes. The results obtained for a specific value α with coefficient k are identical to that for α + 90° with coefficient 1/ k by rotating the tunnel axis by 90°. The maximum internal water pressure was determined by offsetting the prestress-induced hoop strains at the final lining intrados against the seepage-induced hoop strains. As well as assessing the internal water pressure, this approach is capable of identifying potential locations where longitudinal cracks may occur in the final lining.

Comparison between ex situ and in situ measurement methods for the assessment of radioactively contaminated land. Comparison between measurement methods for the characterisation of radioactively contaminated land

International Nuclear Information System (INIS)

Rostron, Peter D.; Ramsey, Michael H.; Heathcote, John A.

2012-01-01

In the UK, it is estimated that there may be 20,000,000 cubic metres of contaminated land at Sellafield alone. Harwell and Dounreay are known to have significant amounts of radioactive or nonradioactive contaminated land (NDA, 2006). It is therefore important to devise optimal methods for the characterisation of areas of land for radionuclide content, in order to enable cost-effective decommissioning. With chemical contaminants, ex situ measurements are made on a larger volume of soil than are in situ measurements, such as PXRF. However, the opposite is often true for the characterisation of radioactive contamination, when this involves the detection of penetrating radiation from γ-emitting radionuclides. This means that when investigating for hotspots of radioactive contamination at or near the ground surface, better coverage can be obtained using in situ methods. This leads to the question, what is the optimal strategy (e.g. percentage coverage, counting time) for in situ characterisation of radioactively contaminated land' Surveys on light-moderate contaminated areas of ground were conducted at Dounreay in order to compare the relative effectiveness of in situ and ex situ methods, both for the detection of radioactive hotspots and also for estimating the average radionuclide content of an area of ground. These surveys suggest that continuous coverage by in situ devices is more effective at hotspot detection, with ex situ laboratory measurements being less effective, although in one case elevated activity below 10 cm depth that was identified by ex situ measurement was not located by in situ measurement. The surveys also highlighted that careful choice of an appropriate spatial model is critical to the estimation of activity concentrations over averaging areas. Whereas continuous coverage may be considered necessary for hotspot identification, in the particular case of the detection of hot particles (where the particle is very small compared to the sampling

Dry fracture method for simultaneous measurement of in-situ stress state and material properties

International Nuclear Information System (INIS)

Serata, S.; Oka, S.; Kikuchi, S.

1996-01-01

Based on the dry fracture principle, a computerized borehole probe has been developed to measure stress state and material properties, simultaneously. The probe is designed to obtain a series of measurements in a continuing sequence along a borehole length, without any interruptive measures, such as resetting packers, taking indentation of borehole wall, overcoming, etc. The new dry fracture probe for the single fracture method is designed to overcome the difficulties posed by its ancestor which was based on the double fracture method. The accuracy of the single fracture method is confirmed by a close agreement with the theory, FE modeling and laboratory testing

Natural Fractures Characterization and In Situ Stresses Inference in a Carbonate Reservoir—An Integrated Approach

Directory of Open Access Journals (Sweden)

Ali Shafiei

2018-02-01

Full Text Available In this paper, we characterized the natural fracture systems and inferred the state of in situ stress field through an integrated study in a very complex and heterogeneous fractured carbonate reservoir. Relative magnitudes and orientations of the in-situ principal stresses in a naturally fractured carbonate heavy oil field were estimated with a combination of available data (World Stress Map, geological and geotectonic evidence, outcrop studies and techniques (core analysis, borehole image logs and Side View Seismic Location. The estimates made here using various tools and data including routine core analysis and image logs are confirmatory to estimates made by the World Stress Map and geotectonic facts. NE-SW and NW-SE found to be the dominant orientations for maximum and minimum horizontal stresses in the study area. In addition, three dominant orientations were identified for vertical and sub-vertical fractures atop the crestal region of the anticlinal structure. Image logs found useful in recognition and delineation of natural fractures. The results implemented in a real field development and proved practical in optimal well placement, drilling and production practices. Such integrated studies can be instrumental in any E&P projects and related projects such as geological CO2 sequestration site characterization.

Effect of external stress on deuteride (hydride) precipitation in Zircaloy-4 using in situ neutron diffraction

Energy Technology Data Exchange (ETDEWEB)

Lin, Jun-li [Department of Nuclear, Plasma, and Radiological Engineering, University of Illinois at Urbana-Champaign, Urbana, IL 61801 (United States); An, Ke; Stoica, Alexandru D. [Chemical and Engineering Materials Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States); Heuser, Brent J., E-mail: bheuser@illinois.edu [Department of Nuclear, Plasma, and Radiological Engineering, University of Illinois at Urbana-Champaign, Urbana, IL 61801 (United States)

2017-04-15

In situ neutron diffraction is utilized to study the deuteride (hydride) precipitation behavior in a cold-worked stress-relieved (CWSR) Zircaloy-4 material upon cooling from 420 °C to room temperature with a 78 MPa external stress applied along the rolling direction (RD) of the material. Two banks detector capture the diffraction signal from two principal directions of the specimen, the normal direction (ND) and the rolling direction (RD). The evolution of deuterium concentration in zirconium solid solution along the two specimen directions is measured by studying the δ-(220) peak intensity, applying the Rietveld refinement method to the diffraction data and using the measured zirconium c-axis lattice distortion. The deuterium concentration is observed to be higher for zirconium grains in the ND than the RD. The terminal solid solubility of precipitation (TSSp) for deuterium in the solution is then described using the Arrhenius equation. It is observed that the applied stress reduces the energy term Q in the Arrhenius equation when compared with the unstressed Q values from the work of others. A model by Puls is applied to study the effect of stress on deuterium solubility, with polycrystalline hydride precipitation strain calculated using the Kearns factor representative of the studied material. The experimental result does not agree with the model prediction of Puls.

In-situ measurements of soil-water conductivity

International Nuclear Information System (INIS)

Murphy, C.E.

1978-01-01

Radionuclides and other environmentally important materials often move in association with water. In terrestrial ecosystems, the storage and movement of water in the soil is of prime importance to the hydrologic cycle of the ecosystem. The soil-water conductivity (the rate at which water moves through the soil) is a necessary input to models of soil-water movement. In situ techniques for measurement of soil-water conductivity have the advantage of averaging soil-water properties over larger areas than most laboratory methods. The in situ techniques also cause minimum disturbance of the soil under investigation. Results of measurements using a period of soil-water drainage after initial wetting indicate that soil-water conductivity and its variation with soil-water content can be determined with reasonable accuracy for the plot where the measurements were made. Further investigations are being carried out to look at variability between plots within a soil type

In situ stress measurements during electrochemical cycling of lithium-rich cathodes

Science.gov (United States)

Nation, Leah; Li, Juchuan; James, Christine; Qi, Yue; Dudney, Nancy; Sheldon, Brian W.

2017-10-01

Layered lithium transition metal oxides (Li1+xM1-xO2, M = Ni, Mn, Co) are attractive cathode materials for lithium-ion batteries due to their high reversible capacity. However, they suffer from structural changes that lead to substantial voltage fade. In this study, we use stress as a novel way to track irreversible changes in Li1.2Mn0.55Ni0.125Co0.125O2 (LR-NMC) cathodes. A unique and unpredicted stress signature is observed during the first delithiation. Initially, a tensile stress is observed, consistent with volume contraction from lithium removal, however, the stress reverses and becomes compressive with continued charging beyond 4 V vs Li/Li+, indicating volume expansion; this phenomenon is present in the first cycle only. This irreversible stress during delithiation is likely to be at least partially due to oxygen loss and the resulting cation rearrangement. Raman spectroscopy provides evidence of the layered-to-spinel phase transition after cycling in the LR-NMC films, as well as recovery of the original spectra upon re-annealing in an oxygen environment.

CHARACTERIZATION OF IN-SITU STRESS AND PERMEABILITY IN FRACTURED RESERVOIRS

Energy Technology Data Exchange (ETDEWEB)

Daniel R. Burns; M. Nafi Toksoz

2002-12-31

We have extended a three-dimensional finite difference elastic wave propagation model previously developed at the Massachusetts Institute of Technology (MIT) Earth Resources Laboratory (ERL) for modeling and analyzing the effect of fractures on seismic waves. The code has been translated into C language and parallelized [using message passing interface (MPI)] to allow for larger models to be run on Linux PC computer clusters. We have also obtained another 3-D code from Lawrence Berkeley Laboratory, which we will use for verification of our ERL code results and also to run discrete fracture models. Testing of both codes is underway. We are working on a new finite difference model of borehole wave propagation for stressed formations. This code includes coordinate stretching to provide stable, variable grid sizes that will allow us to model the thin fluid annulus layers in borehole problems, especially for acoustic logging while drilling (LWD) applications. We are also extending our analysis routines for the inversion of flexural wave dispersion measurements for in situ stress estimates. Initial results on synthetic and limited field data are promising for a method to invert cross dipole data for the rotation angle and stress state simultaneously. A meeting is being scheduled between MIT and Shell Oil Company scientists to look at data from a fractured carbonate reservoir that may be made available to the project. The Focus/Disco seismic processing system from Paradigm Geophysical has been installed at ERL for field data analysis and as a platform for new analysis modules. We have begun to evaluate the flow properties of discrete fracture distributions through a simple 2D numerical model. Initial results illustrate how fluid flow pathways are very sensitive to variations in the geometry and apertures of fracture network.

[Characterization of kale (Brassica oberacea var acephala) under thallium stress by in situ attenuated total reflection FTIR].

Science.gov (United States)

Yao, Yan; Zhang, Ping; Wang, Zhen-Chun; Chen, Yong-Heng

2009-01-01

The experiment was designed based on consumption of carbon dioxide through the photosynthesis of Brassica oberacea var acephala leaf, and the photosynthesis of kale leaf under thallium stress was investigated by in situ attenuated total reflection FTIR (in situ ATR-FTIR). The ATR-FTIR showed that the absorption peaks of leaves had no obvious difference between plants growing in thallium stress soil and plants growing in non-thallium pollution soil, and the strong peaks at 3,380 cm(-1) could be assigned to the absorption of water, carbohydrate, protein or amide; the strong peaks at 2,916 and 2,850 cm(-1) assigned to the absorption of carbohydrate or aliphatic compound; the peaks at 1,640 cm(-1) assigned to the absorption of water. However, as detected by the in situ ATR-FTIR, the double peaks (negative peaks) at 2,360 and 2,340 cm(-1) that are assigned to the absorption of CO2 appeared and became high gradually. It was showed that kale was carrying photosynthesis. At the same time, the carbon dioxide consumption speed of leaf under thallium stress was obviously larger than that of the blank It was expressed that photosynthesis under thallium stress was stronger than the blank All these represented that kale had certain tolerance to the heavy metal thallium. Meanwhile, the carbon dioxide consumption of grown-up leaf was more than that of young leaf whether or not under thallium stress. It was also indicated that the intensity of photosynthesis in grown-up leaf is higher than that in young leaf.

Evidence against the nuclear in situ binding of arsenicals-oxidative stress theory of arsenic carcinogenesis

International Nuclear Information System (INIS)

Kitchin, Kirk T.; Wallace, Kathleen

2008-01-01

A large amount of evidence suggests that arsenicals act via oxidative stress in causing cancer in humans and experimental animals. It is possible that arsenicals could bind in situ close to nuclear DNA followed by Haber-Weiss type oxidative DNA damage. Therefore, we tested this hypothesis by using radioactive 73 As labeled arsenite and vacuum filtration methodology to determine the binding affinity and capacity of 73 As arsenite to calf thymus DNA and Type 2A unfractionated histones, histone H3, H4 and horse spleen ferritin. Arsenicals are known to release redox active Fe from ferritin. At concentrations up to about 1 mM, neither DNA nor any of the three proteins studied, Type II-A histones, histone H3, H4 or ferritin, bound radioactive arsenite in a specific manner. Therefore, it appears highly unlikely that initial in situ binding of trivalent arsenicals, followed by in situ oxidative DNA damage, can account for arsenic's carcinogenicity. This experimental evidence (lack of arsenite binding to DNA, histone Type II-A and histone H3, H4) does not rule out other possible oxidative stress modes of action for arsenic such as (a) diffusion of longer lived oxidative stress molecules, such as H 2 O 2 into the nucleus and ensuing oxidative damage, (b) redox chemistry by unbound arsenicals in the nucleus, or (c) arsenical-induced perturbations in Fe, Cu or other metals which are already known to oxidize DNA in vitro and in vivo

The contrasting roles of creep and stress relaxation in the time-dependent deformation during in-situ cooling of a nickel-base single crystal superalloy.

Science.gov (United States)

Panwisawas, Chinnapat; D'Souza, Neil; Collins, David M; Bhowmik, Ayan

2017-09-11

Time dependent plastic deformation in a single crystal nickel-base superalloy during cooling from casting relevant temperatures has been studied using a combination of in-situ neutron diffraction, transmission electron microscopy and modelling. Visco-plastic deformation during cooling was found to be dependent on the stress and constraints imposed to component contraction during cooling, which mechanistically comprises creep and stress relaxation. Creep results in progressive work hardening with dislocations shearing the γ' precipitates, a high dislocation density in the γ channels and near the γ/γ' interface and precipitate shearing. When macroscopic contraction is restricted, relaxation dominates. This leads to work softening from a decreased dislocation density and the presence of long segment stacking faults in γ phase. Changes in lattice strains occur to a similar magnitude in both the γ and γ' phases during stress relaxation, while in creep there is no clear monotonic trend in lattice strain in the γ phase, but only a marginal increase in the γ' precipitates. Using a visco-plastic law derived from in-situ experiments, the experimentally measured and calculated stresses during cooling show a good agreement when creep predominates. However, when stress relaxation dominates accounting for the decrease in dislocation density during cooling is essential.

In situ spectrophotometric measurement of dissolved inorganic carbon in seawater

Science.gov (United States)

Liua, Xuewu; Byrne, Robert H.; Adornato, Lori; Yates, Kimberly K.; Kaltenbacher, Eric; Ding, Xiaoling; Yang, Bo

2013-01-01

Autonomous in situ sensors are needed to document the effects of today’s rapid ocean uptake of atmospheric carbon dioxide (e.g., ocean acidification). General environmental conditions (e.g., biofouling, turbidity) and carbon-specific conditions (e.g., wide diel variations) present significant challenges to acquiring long-term measurements of dissolved inorganic carbon (DIC) with satisfactory accuracy and resolution. SEAS-DIC is a new in situ instrument designed to provide calibrated, high-frequency, long-term measurements of DIC in marine and fresh waters. Sample water is first acidified to convert all DIC to carbon dioxide (CO2). The sample and a known reagent solution are then equilibrated across a gas-permeable membrane. Spectrophotometric measurement of reagent pH can thereby determine the sample DIC over a wide dynamic range, with inherent calibration provided by the pH indicator’s molecular characteristics. Field trials indicate that SEAS-DIC performs well in biofouling and turbid waters, with a DIC accuracy and precision of ∼2 μmol kg–1 and a measurement rate of approximately once per minute. The acidic reagent protects the sensor cell from biofouling, and the gas-permeable membrane excludes particulates from the optical path. This instrument, the first spectrophotometric system capable of automated in situ DIC measurements, positions DIC to become a key parameter for in situ CO2-system characterizations.

In situ high-pressure measurement of crystal solubility by using neutron diffraction

Science.gov (United States)

Chen, Ji; Hu, Qiwei; Fang, Leiming; He, Duanwei; Chen, Xiping; Xie, Lei; Chen, Bo; Li, Xin; Ni, Xiaolin; Fan, Cong; Liang, Akun

2018-05-01

Crystal solubility is one of the most important thermo-physical properties and plays a key role in industrial applications, fundamental science, and geoscientific research. However, high-pressure in situ measurements of crystal solubility remain very challenging. Here, we present a method involving high-pressure neutron diffraction for making high-precision in situ measurements of crystal solubility as a function of pressure over a wide range of pressures. For these experiments, we designed a piston-cylinder cell with a large chamber volume for high-pressure neutron diffraction. The solution pressures are continuously monitored in situ based on the equation of state of the sample crystal. The solubility at a high pressure can be obtained by applying a Rietveld quantitative multiphase analysis. To evaluate the proposed method, we measured the high-pressure solubility of NaCl in water up to 610 MPa. At a low pressure, the results are consistent with the previous results measured ex situ. At a higher pressure, more reliable data could be provided by using an in situ high-pressure neutron diffraction method.

Determination of near surface in-situ stresses

International Nuclear Information System (INIS)

Garritty, P.; Irvin, R.

1983-06-01

One of the major unknowns affecting aspects of underground construction and the geohydrology of rock masses is the magnitude and direction of the geostatic principal stresses in the earth's crust. This is particularly the case in near surface rocks where there are indications that high horizontal stresses may exist. The techniques, experiences and results of a preliminary rock stress measurement programme conducted at shallow depth in the Carnmenellis Granite, Cornwall, using C.S.I.R.O. triaxial hollow inclusion cells are described. (author)

Defining in-situ stress magnitude and the responses of geology to stress anisotropy in heterogeneous lithologies for the United Kingdom

Science.gov (United States)

Kingdon, A.; Fellgett, M. W.; Williams, J. D. O.

2017-12-01

Exploitation of shale gas in the USA has led to interest in similar UK deposits. After tremors at the Preese Hall well in 2011, the process of hydraulic fracturing has become contentious. In-situ stress orientation controls the direction that fractures propagate from a well. World Stress Map (WSM) data coverage for the UK has historically been sparse. Improvements to the stress orientations for the UK are vital for reducing risk levels of induced seismicity. In some offshore basins, maximum horizontal stress (SHMax) is sub-parallel to major inverted Permo-Triassic faults, episodically reactivated during the Cenozoic, indicating a degree of structural control. Understanding for UK stress magnitude has been poor. Data for Northern England has been augmented with new estimates of vertical stress (Sv), minimum horizontal stress (Shmin) and pore pressure, focussed on potentially prospective basins east and west of the Pennines. Calculated values combined with legacy hydraulic fracturing and overcoring data show vertical stress gradients vary from 23 to 26 MPa/Km-1. Cheshire and Scotland show higher Shmin values by 2 MPa/Km-1 compared to Yorkshire and South East England. SHMax values exceeds the Sv which in turn exceeds Shmin indicating a predominantly strike slip environment. Pore pressure appears to be uniformly hydrostatic across the studied regions. There is some evidence above 1200 m depth of reverse faulting in igneous rocks in Cornwall, Leicestershire and Cumbria. Analysis of borehole imaging for the lithologically heterogeneous Carboniferous Coal Measures, highlights variability failure modes over confined vertical intervals. Breakouts are disproportionately located in "seatearths", palaeosols located stratigraphically beneath coal seams. Drilling induced tensile fractures are located within close proximity in overbank silt/clay facies and relatively massive channel sands that typically over and underlie coal deposits. Strength tests show that breakouts occur in

Development of portable HPGe spectrometer for in situ measurements

Directory of Open Access Journals (Sweden)

Kail Artjoms

2015-01-01

Full Text Available In situ applications require a very high level of portability of high-resolution spectrometric equipment. Usage of HPGe detectors for radioactivity measurements in the environment or for nuclear safeguard applications, to combat illicit trafficking of nuclear materials or uranium and plutonium monitoring in nuclear wastes, has become a norm in the recent years. Portable HPGe-based radionuclide spectrometer with electrical cooling has lately appeared on the market for in situ applications. At the same time deterioration of energy resolution associated with vibrations produced by cryocooler or high weight of the instrument, short time of autonomous operation and high price of these spectrometers are limiting their usage in many cases. In this paper we present development results of ultra compact hand held all-in-one spectrometer for in situ measurements based on HPGe detector cooled by liquid nitrogen without listing the above disadvantages.

In situ gamma-ray spectrometric measurements of uranium in phosphates soil

International Nuclear Information System (INIS)

Lavi, N.; Ne'eman, E.; Brenner, S.; Haquin, G.; Nir-El, Y.

1997-01-01

Abstract Radioactivity concentration of 238 U in a phosphate ores quarry was measured in situ. Independently, soil samples collected in the site were measured in the laboratory. It was disclosed that radon emanation from the soil lowers in situ results that are derived from radon daughters. Uranium concentration was found to be 121.6±1.9 mg kg -1 (authors)

In situ measurements reveal extremely low pH in soil

DEFF Research Database (Denmark)

Nielsen, Knud Erik; Loibide, Amaia Irixar; Nielsen, Lars Peter

2017-01-01

We measured pH in situ in the top organic soil horizons in heathland and pine forest and found values between 2.6 and 3.2. This was 0.5e0.8 units lower than concurrent laboratory pH measurements of the same soil, which raises questions about the interpretation of pH measurements. We propose that ...... that the higher pH recorded by standard laboratory methods may be due to buffering ions from soil biota released from drying, grinding and rewetting of soil samples, whereas the in situ pH reflects the correct level of acidification....

Overcoring rock stress measurements in drillholes ONK-PP169 and ONK-PP170 Olkiluoto

International Nuclear Information System (INIS)

Berg, S.; Sjoeberg, J.

2009-03-01

Three-dimensional overcoring rock stress measurements were conducted in drillholes ONK-PP169 and ONK-PP170 at the 230 m depth level in the ONKALO site ramp. The measurements were performed during the spring of 2008. The objective of the measurements was to obtain better understanding of the in situ stress field for the measured depth levels. Another objective was to increase the confidence and reliability and to diminish the uncertainties concerning the state of stress at shallow depth of ONKALO. Due to problems with bonding of strain gauges, which may have been caused by a thin layer/coating of unknown material on the pilot hole wall, stress measurements results were only achieved in drillhole ONK-PP170 at -230 m level. The initial plan was to conduct measurements at three depth levels, -120 m, -180 m and -220 m levels, in the ONKALO ramp. Two (2) of the conducted measurements could be rated as successful (rating a) two (2) measurement were partly successful (rating b). The results from the measurements assuming isotropic condition, the major principal stress is plunging between 18deg and 35deg and trending between S and WSW. Stress magnitudes (for σ 1 ) varied between 12 and 16 MPa except for test 2:3:3 where a much higher value (47 MPa) was obtained. The orientation of the major principal stress are similar for test 2:3:3 and 2:4:3 (WSW), but are different from the orientation of the major principal stress for test 2:5:1 and 2:6:1 (S). Likewise, the horizontal stresses have the highest values for test 2:3:3 but in this case the orientation is similar to test 2:5:1 and 2:4:3. The horizontal stress magnitudes of test 2:4:3, 2:5:1 and 2:6:1 are similar but the orientation for test 2:6:1 are different from the other three tests. The results from two of the measurements assuming transversely isotropic conditions, the major principal stress is 12.3 MPa and 12.7 MPa, trending WSW and S, plunging 30 deg. (orig.)

In situ measurement of tritium permeation through stainless steel

Energy Technology Data Exchange (ETDEWEB)

Luscher, Walter G., E-mail: walter.luscher@pnnl.gov [Pacific Northwest National Laboratory, 902 Battelle Blvd, Richland, WA 99352 (United States); Senor, David J., E-mail: david.senor@pnnl.gov [Pacific Northwest National Laboratory, 902 Battelle Blvd, Richland, WA 99352 (United States); Clayton, Kevin K., E-mail: kevin.clayton@inl.gov [Idaho National Laboratory, 2525 Fremont Ave., Idaho Falls, ID 83415 (United States); Longhurst, Glen R., E-mail: glenlonghurst@suu.edu [Idaho National Laboratory, 2525 Fremont Ave., Idaho Falls, ID 83415 (United States)

2013-06-15

Highlights: ► In situ tritium permeation measurements collected over broad pressure range. ► Test conditions relevant to 316 SS in commercial light water reactors. ► Comparisons between in- and ex-reactor measurements provided. ► Correlation between tritium permeation, temperature, and pressure developed. -- Abstract: The TMIST-2 irradiation experiment was conducted in the Advanced Test Reactor at Idaho National Laboratory to evaluate tritium permeation through Type 316 stainless steel (316 SS). The interior of a 316 SS seamless tube specimen was exposed to a {sup 4}He carrier gas mixed with a specified quantity of tritium (T{sub 2}) to yield partial pressures of 0.1, 5, and 50 Pa at 292 °C and 330 °C. In situ tritium permeation measurements were made by passing a He–Ne sweep gas over the outer surface of the specimen to carry the permeated tritium to a bubbler column for liquid scintillation counting. Results from in situ permeation measurements were compared with predictions based on an ex-reactor permeation correlation in the literature. In situ permeation data were also used to derive an in-reactor permeation correlation as a function of temperature and pressure over the ranges considered in this study. In addition, the triton recoil contribution to tritium permeation, which results from the transmutation of {sup 3}He to T, was also evaluated by introducing a {sup 4}He carrier gas mixed with {sup 3}He at a partial pressure of 1013 Pa at 330 °C. Less than 3% of the tritium resulting from {sup 3}He transmutation contributed to tritium permeation.

Application of the Raman technique to measure stress states in individual Si particles in a cast Al-Si alloy

International Nuclear Information System (INIS)

Harris, Stephen J.; O'Neill, Ann; Boileau, James; Donlon, William; Su, Xuming; Majumdar, B.S.

2007-01-01

While Raman spectroscopy is often used to measure stresses, the analyses are almost always limited to cases with simple stress states (uniaxial, equibiaxial). Recently we provided an experimental methodology to determine the full state of stress in Si wafers. Here we extend that methodology to interrogate stress states in Si particles embedded in an Al-Si alloy. Such determinations will ultimately be valuable for predicting ductility of cast Al, since a primary source of damage is cracking of eutectic Si particles. We combine electron back-scattered diffraction with the frequency shift, polarization and intensity of the Raman light to determine stress states. Stress states are measured both in the as-received residually stressed state and under in situ uniaxial loading. Comparison with finite element calculations shows good agreement. As an application of the technique, we show the determination of strength of an individual Si particle and compare the stress evolution with various models

Residual stress measurement with focused acoustic waves and direct comparison with X-ray diffraction stress measurements

International Nuclear Information System (INIS)

Sathish, Shamachary; Moran, Thomas J.; Martin, Richard W.; Reibel, Richard

2005-01-01

The technique of measuring small changes in acoustic wave velocity due to external or internal stress has been used for quantitative determination of residual stress in materials during the last decade. Application of similar methodology with focused acoustic waves leads to residual stress measurement with spatial resolution of a few millimeters to a few microns. The high spatial resolution residual stress measurement required development of new methodologies in both the design of acoustic lenses and the instrumentation for acoustic wave velocity determination. This paper presents two new methodologies developed for the measurement of residual stress with spatial resolution of a few millimeters. The design of new type of acoustic lens for achieving higher spatial resolution in residual stress measurement is introduced. Development of instrumentation for high precision local surface wave velocity measurement will be presented. Residual stresses measured around a crack tip in a sample of Ti-6A1-4V using a focused beam will be compared with X-ray diffraction measurements performed on the same region of the sample. Results of residual stress measurements along a direction perpendicular to the electron beam weld in a sample of Ti-6A1-4V, determined using focused acoustic waves and X-ray diffraction technique, are also presented. The spatial resolution and penetration depth of X-rays and focused acoustic beams with reference to residual stress measurements are discussed

Background Stress Inventory: Developing a Measure of Understudied Stress.

Science.gov (United States)

Terrill, Alexandra L; Gjerde, Jill M; Garofalo, John P

2015-10-01

Background stress is an understudied source of stress that involves both ambient stress and daily hassles upon which new stressors are superimposed. To date, an accurate measure of the background stress construct has not been available. We developed the Background Stress Inventory, a 25-item self-report measure that asks respondents to indicate how distressed they have felt over the past month and the majority of the past year across five domains: financial, occupation, environment, health and social. Seven hundred seventy-two participants completed the paper-and-pencil measure; the sample was randomly split into two separate subsamples for analyses. Exploratory factor analysis suggested five factors corresponding to these domains, and confirmatory factor analysis showed acceptable global fit (X(2)(255) = 456.47, comparative fit index = 0.94, root mean square error of approximation = 0.045). Cronbach's alpha (0.89) indicated good internal reliability. Construct validity analyses showed significant positive relationships with measures of perceived stressfulness (r = 0.62) and daily hassles (0.41), p's < 0.01. Depressive symptoms (0.62) and basal blood pressure (0.21) were both significantly associated with background stress, p's < 0.01. The importance of the proposed measure is reflected in the limited research base on the impact of background stress. Systematic investigation of this measure will provide insight into this understudied form of chronic stress and its potential influence on both psychological and physical endpoints. Copyright © 2013 John Wiley & Sons, Ltd.

An in situ Raman spectroscopy study of stress transfer between carbon nanotubes and polymer

International Nuclear Information System (INIS)

Mu Minfang; Winey, Karen I; Osswald, Sebastian; Gogotsi, Yury

2009-01-01

The transfer mechanism of applied stress in single-wall carbon nanotube (SWCNT)/poly(methyl methacrylate) (PMMA) nanocomposites was investigated using in situ Raman spectroscopy on composite fibers. These SWCNT/PMMA nanocomposite fibers have no specific SWCNT-polymer interactions and the high degree of nanotube alignment minimizes the contributions from nanotube-nanotube interactions. Although tensile testing found significantly improved overall mechanical properties of the fibers, effective stress transfer to SWCNTs is limited to a small strain regime (ε<0.2%). At higher strains, the stress on the SWCNTs decreases due to the slippage at the nanotube-polymer interface. Slippage was also evident in scanning electron micrographs of fracture surfaces produced by tensile testing of the composite fibers. Above ε = 0.2%, the strain-induced slippage was accompanied by irreversible responses in stress and Raman peak shifts. This paper shows that efficient stress transfer to nanotubes as monitored by Raman spectroscopy is crucial to improving the mechanical properties of polymer nanocomposites and to detecting internal damage in nanocomposites.

Stress and Pore Pressure Measurement in IODP Riser Drilling: An Example from Expedition 319, Kumano Basin offshore SW Honshu, Japan

Science.gov (United States)

Saffer, D. M.; McNeill, L. C.; Byrne, T. B.; Araki, E.; Flemings, P. B.; Conin, M.; Eguchi, N. O.; Takahashi, K.; Toczko, S.; Boutt, D. F.; Doan, M.; Kano, Y.; Ito, T.; Lin, W.

2009-12-01

In summer 2009, Integrated Ocean Drilling Program (IODP) Expedition 319 drilled a 1600 m deep riser borehole (Site C0009) in the Kumano Basin offshore SW Japan, to investigate the properties, structure and state of stress in the hanging wall above the subduction plate boundary. The first riser-based scientific drilling in IODP history allowed us to make several new scientific measurements including in situ stress magnitude, pore pressure and permeability using the Modular Formation Dynamics Tester (MDT) wireline tool, and measurement of minimum stress magnitude from Leak-off Tests (LOT). In addition, continuous monitoring of mud weight, mud gas, annular pressure, and mud losses provided data to constrain formation pore fluid pressure and stress. At Site C0009, we conducted 2 LOTs below a casing shoe at 708.6 m depth and 11 successful MDT measurements, including 9 single probe tests to measure pore pressure and fluid mobility and 2 dual packer tests: 1 to measure permeability by a drawdown test, and 1 to measure in situ stress. Measured pore pressures are approximately hydrostatic to 1463.7 m depth. We observed only minor gas shows when drilling ahead (as in-place methane was liberated from the rock at the bit) but little or no gas during pipe connections. This indicates that the borehole mud pressure exceeded the formation pore pressure, and is consistent with the MDT measurements. Permeabilities range from ~10-16 m2 - 10-14 m2, and the observed variation is consistent with lithologic changes defined in gamma ray logs. The MDT measurement at 874.3 mbsf and the LOT at 708.6 m yield values for the least principal stress of 34.8 MPa and 30.2 MPa, respectively. Both are less than the vertical stress (Sv) computed from density logs. Partial mud circulation losses occurred when the borehole mud pressure exceeded the leak-off stress measured at the base of the casing shoe; this provides an additional indirect constraint on Shmin magnitude. Mud pressure slightly in excess

Effect of Applied Stress and Temperature on Residual Stresses Induced by Peening Surface Treatments in Alloy 600

Science.gov (United States)

Telang, A.; Gnäupel-Herold, T.; Gill, A.; Vasudevan, V. K.

2018-04-01

In this study, the effects of applied tensile stress and temperature on laser shock peening (LSP) and cavitation shotless peening (CSP)-induced compressive residual stresses were investigated using neutron and x-ray diffraction. Residual stresses on the surface, measured in situ, were lower than the applied stress in LSP- and CSP-treated Alloy 600 samples (2 mm thick). The residual stress averaged over the volume was similar to the applied stress. Compressive residual stresses on the surface and balancing tensile stresses in the interior relax differently due to hardening induced by LSP. Ex situ residual stress measurements, using XRD, show that residual stresses relaxed as the applied stress exceeded the yield strength of the LSP- and CSP-treated Alloy 600. Compressive residual stresses induced by CSP and LSP decreased by 15-25% in magnitude, respectively, on exposure to 250-450 °C for more than 500 h with 10-11% of relaxation occurring in the first few hours. Further, 80% of the compressive residual stresses induced by LSP and CSP treatments in Alloy 600 were retained even after long-term aging at 350 °C for 2400 h.

Visualizing and measuring flow in shale matrix using in situ synchrotron X-ray microtomography

Science.gov (United States)

Kohli, A. H.; Kiss, A. M.; Kovscek, A. R.; Bargar, J.

2017-12-01

Natural gas production via hydraulic fracturing of shale has proliferated on a global scale, yet recovery factors remain low because production strategies are not based on the physics of flow in shale reservoirs. In particular, the physical mechanisms and time scales of depletion from the matrix into the simulated fracture network are not well understood, limiting the potential to optimize operations and reduce environmental impacts. Studying matrix flow is challenging because shale is heterogeneous and has porosity from the μm- to nm-scale. Characterizing nm-scale flow paths requires electron microscopy but the limited field of view does not capture the connectivity and heterogeneity observed at the mm-scale. Therefore, pore-scale models must link to larger volumes to simulate flow on the reservoir-scale. Upscaled models must honor the physics of flow, but at present there is a gap between cm-scale experiments and μm-scale simulations based on ex situ image data. To address this gap, we developed a synchrotron X-ray microscope with an in situ cell to simultaneously visualize and measure flow. We perform coupled flow and microtomography experiments on mm-scale samples from the Barnett, Eagle Ford and Marcellus reservoirs. We measure permeability at various pressures via the pulse-decay method to quantify effective stress dependence and the relative contributions of advective and diffusive mechanisms. Images at each pressure step document how microfractures, interparticle pores, and organic matter change with effective stress. Linking changes in the pore network to flow measurements motivates a physical model for depletion. To directly visualize flow, we measure imbibition rates using inert, high atomic number gases and image periodically with monochromatic beam. By imaging above/below X-ray adsorption edges, we magnify the signal of gas saturation in μm-scale porosity and nm-scale, sub-voxel features. Comparing vacuumed and saturated states yields image

Blending Satellite Observed, Model Simulated, and in Situ Measured Soil Moisture over Tibetan Plateau

Directory of Open Access Journals (Sweden)

Yijian Zeng

2016-03-01

Full Text Available The inter-comparison of different soil moisture (SM products over the Tibetan Plateau (TP reveals the inconsistency among different SM products, when compared to in situ measurement. It highlights the need to constrain the model simulated SM with the in situ measured data climatology. In this study, the in situ soil moisture networks, combined with the classification of climate zones over the TP, were used to produce the in situ measured SM climatology at the plateau scale. The generated TP scale in situ SM climatology was then used to scale the model-simulated SM data, which was subsequently used to scale the SM satellite observations. The climatology-scaled satellite and model-simulated SM were then blended objectively, by applying the triple collocation and least squares method. The final blended SM can replicate the SM dynamics across different climatic zones, from sub-humid regions to semi-arid and arid regions over the TP. This demonstrates the need to constrain the model-simulated SM estimates with the in situ measurements before their further applications in scaling climatology of SM satellite products.

Photoacoustic measurements of red blood cell oxygen saturation in blood bags in situ

Science.gov (United States)

Pinto, Ruben N.; Bagga, Karan; Douplik, Alexandre; Acker, Jason P.; Kolios, Michael C.

2017-03-01

Red blood cell (RBC) transfusion is a critical component of the health care services. RBCs are stored in blood bags in hypothermic temperatures for a maximum of 6 weeks post donation. During this in vitro storage period, RBCs have been documented to undergo changes in structure and function due to mechanical and biochemical stress. Currently, there are no assessment methods that monitor the quality of RBCs within blood bags stored for transfusion. Conventional assessment methods require the extraction of samples, consequently voiding the sterility of the blood bags and potentially rendering them unfit for transfusions. It is hypothesized that photoacoustic (PA) technology can provide a rapid and non-invasive indication of RBC quality. In this study, a novel PA setup was developed for the acquisition of oxygen saturation (SO2) of two blood bags in situ. These measurements were taken throughout the lifespan of the blood bags (42 days) and compared against the clinical gold standard method of the blood gas analyzer (BGA). SO2 values of the blood bags increased monotonically throughout the storage period. A strong correlation between PA SO2 and BGA SO2 was found, however, PA values were on average 3.5% lower. Both techniques found the bags to increase by an SO2 of approximately 20%, and measured very similar rates of SO2 change. Future work will be focused on determining the cause of discrepancy between SO2 values acquired from PA versus BGA, as well as establishing links between the measured SO2 increase and other changes in RBC in situ.

BEM-DDM modelling of rock damage and its implications on rock laboratory strength and in-situ stresses

International Nuclear Information System (INIS)

Matsui, Hiroya

2008-03-01

Within the framework of JAEA's Research and Development on deep geological environments for assessing the safety and reliability of the disposal technology for nuclear waste, this study was conducted to determine the effects of sample damage on the strength obtained from laboratory results (uniaxial compression and Brazilian test). Results of testing on samples of Toki granite taken at Shobasama and at the construction site for the Mizunami Underground Research Laboratory (MIU) at Mizunami, Gifu Pref., Japan, were analysed. Some spatial variation of the results along the boreholes suggested the presence of a correlation between the laboratory strength and the in-situ stresses measured by means of the hydro-fracturing method. To confirm this, numerical analyses of the drilling process in brittle rock by means of a BEM-DDM program (FRACOD 2D ) were carried out to study the induced fracture patterns. These fracture patterns were compared with similar results reported by other published studies and were found to be realistic. The correlation between strength and in-situ stresses could then be exploited to estimate the stresses and the location of core discing observed in boreholes where stress measurements were not available. A correction of the laboratory strength results was also proposed to take into account sample damage during drilling. Modelling of Brazilian tests shows that the calculated fracture patterns determine the strength of the models. This is different from the common assumption that failure occurs when the uniform tensile stress in the sample reaches the tensile strength of the rock material. Based on the modelling results, new Brazilian tests were carried out on samples from borehole MIZ-1 that confirmed the failure mechanism numerically observed. A numerical study of the fracture patterns induced by removal of the overburden on a large scale produces fracture patterns and stress distributions corresponding to observations in crystalline hard rock in

In-situ geophysical measurements in marine sediments: Applications in seafloor acoustics and paleoceanography

Science.gov (United States)

Gorgas, Thomas Joerg

Acoustic in-situ sound speeds and attenuation were measured on the Eel River shelf, CA, with the Acoustic Lance between 5 and 15 kHz to 2.0 meters below seafloor (mbsf). A comparison with laboratory ultrasonic geoacoustic data obtained at 400 kHz on cored sediments showed faster in-situ and ultrasonic sound speeds in coarse-grained deposits in water depths to 60 m than in fine-grained deposits below that contour line. Ultrasonic attenuation was often greater than in-situ values and remained almost constant below 0.4 mbsf in these heterogeneous deposits. In-situ attenuation decreased with depth. These observations partly agree with results from other field studies, and with theoretical models that incorporate intergranular friction and dispersion from viscosity as main controls on acoustic wave propagation in marine sediments. Deviations among in-situ and laboratory acoustic data from the Eel Margin with theoretical studies were linked to scattering effects. Acoustic Lance was also deployed in homogeneous, fine-grained sediments on the inner shelf of SE Korea, where free gas was identified in late-September, but not in mid-September 1999. Free gas was evidenced by an abrupt decrease of in-situ sound speed and by characteristic changes in acoustic waveforms. These results suggest the presence of a gassy sediment layer as shallow as 2 mbsf along the 70 m bathymetry line, and was attributed to a variable abundance of free gas on short-term and/or small-regional scales on the SE Korea shelf. Bulk density variations in marine sediments obtained along the Walvis Ridge/Basin, SW Africa, at Ocean Drilling Program (ODP) Sites 1081 to 1084 were spectral-analyzed to compute high-resolution sedimentation rates (SRs) in both the time- and age domains by correctly identifying Milankovitch cycles (MCs). SRs for the ODP sites yielded age-depth models that often correlate positively with biostratigraphic data and with organic mass accumulation rates (MAR Corg), a proxy for

Mesures de contraintes in-situ. Méthode de relaxation des carottes Measuring in-Situ Stresses. Relaxation Method with Core Samples

Directory of Open Access Journals (Sweden)

Perreau P.

2006-11-01

Full Text Available Dans cet article, on se propose de présenter les premiers résultats de l'étude de la méthode d'évaluation des contraintes par mesure de déformations différées d'une carotte après son extraction. Le travail correspondant a été réalisé dans le cadre du projet ARTEP Fracturation hydraulique . Les principes de cette méthode et les quelques éléments d'interprétation récemment publiés dans la littérature sont exposés dans un premier temps. Les résultats de deux campagnes de mesures sur deux puits de la SNEA-P (Soudron, novembre 1985 et Lanot, juillet 1986 sont ensuite présentés. Ces essais ont mis en évidence que les déformations différées d'une carotte dues au relachement des contraintes sont effectivement mesurables. Cependant, une interprétation quantitative de ces mesures nécessite une amélioration des conditions expérimentales (stabilisation thermique, stabilisation de l'état de saturation. This article describes the first results of research on a method of evaluating stresses by measuring the differred deformations of a core sample after it has been extracted. The corresponding research was done within the framework of an ARTEP project on Hydraulic Fracturing . The principles of this method and several interpretation aspects published recently in the literature are described in the first part. Then the results of two measurement campaigns using two SNEA-P wells (Soudron in November 1985 and Lanot in July 1986 are described. These tests revealed that the differed deformations of a core sample due to the relaxing of stresses can effectively be measured. However, a quantitative interpretation of these measurements requires an improvement to be made in the experimental conditions (thermal stabilization, stabilization of the state of saturation.

Application of in-situ measurement to determine 137Cs in the Swiss Alps

International Nuclear Information System (INIS)

Schaub, M.; Konz, N.; Meusburger, K.; Alewell, C.

2010-01-01

Establishment of 137 Cs inventories is often used to gain information on soil stability. The latter is crucial in mountain systems, where ecosystem stability is tightly connected to soil stability. In-situ measurements of 137 Cs in steep alpine environments are scarce. Most studies have been carried out in arable lands and with Germanium (Ge) detectors. Sodium Iodide (NaI) detector system is an inexpensive and easy to handle field instrument, but its validity on steep alpine environments has not been tested yet. In this study, a comparison of laboratory measurements with GeLi detector and in-situ measurements with NaI detector of 137 Cs gamma soil radiation has been done in an alpine catchment with high 137 Cs concentration (Urseren Valley, Switzerland). The aim of this study was to calibrate the in-situ NaI detector system for application on steep alpine slopes. Replicate samples from an altitudinal transect through the Urseren Valley, measured in the laboratory with a GeLi detector, showed a large variability in 137 Cs activities at a meter scale. This small-scale heterogeneity determined with the GeLi detector is smoothed out by uncollimated in-situ measurements with the NaI detector, which provides integrated estimates of 137 Cs within the field of view (3.1 m 2 ) of each measurement. There was no dependency of 137 Cs on pH, clay content and carbon content, but a close relationship was determined between measured 137 Cs activities and soil moisture. Thus, in-situ data must be corrected for soil moisture. Close correlation (R 2 = 0.86, p 137 Cs activities (in Bq kg -1 ) estimated with in-situ (NaI detector) and laboratory (GeLi detector) methods. We thus concluded that the NaI detector system is a suitable tool for in-situ measurements in alpine environments. This paper describes the calibration of the NaI detector system for field application under elevated 137 Cs activities originating from Chernobyl fallout.

In situ stresses in rock masses: methodology for its study in tunnel projects in Spain

International Nuclear Information System (INIS)

Madirolas Perez, G.; Perucho Martinez, A.

2014-01-01

In situ stress is one of the main factors to be taken into account in the design of tunnels, as it can cause inadmissible stresses and strains leading to high deviations in the budgets. For that reason, the stress state is directly introduced into the numerical models used for the design of tunnels. In Spain, although several tunnels have been carried out with an important overburden in tectonically relevant zones, a quantitative determination of the stresses has not been usually included in civil work projects. Therefore, it is considered necessary to implement a routine procedure of study of civil work projects involving tunnels excavated in rock, and a new detailed methodology is proposed. The challenge is that project managers, who face works in which stresses may play a determinant role, may have a practical reference enabling them to optimize available resources and to include the real stress information in the design of underground works. (Author)

In situ measurement of diffusivity

International Nuclear Information System (INIS)

Berne, F.; Pocachard, J.

2004-01-01

The mechanism of molecular diffusion controls the migration of contaminants in very low-permeability porous media, like underground facilities for the storage of hazardous waste. Determining of relevant diffusion coefficients is therefore of prime importance. A few techniques exist for in situ measurement of the quantity, but they suffer from many handicaps (duration, complexity and cost of the experiments). We propose here two innovative methods that have some potential to improve the situation. So far, we have found them feasible on the basis of design calculations and laboratory experiments. This work is presently protected by a patent. (author)

In situ measurement of diffusivity

International Nuclear Information System (INIS)

Berne, Ph.; Pocachard, J.

2005-01-01

The mechanism of molecular diffusion controls the migration of contaminants in very low-permeability porous media, like underground facilities for the storage of hazardous waste. Determining the relevant diffusion coefficients is, therefore, of prime importance. A few techniques exist for the in situ measurement of that quantity, but they suffer from many handicaps (duration, complexity and cost of the experiments). We propose here two innovative methods that have some potential to improve this situation. So far, we have found them feasible on the basis of design calculations and laboratory experiments. This work is presently protected by a patent. (author)

Residual-stress measurements

Energy Technology Data Exchange (ETDEWEB)

Ezeilo, A N; Webster, G A [Imperial College, London (United Kingdom); Webster, P J [Salford Univ. (United Kingdom)

1997-04-01

Because neutrons can penetrate distances of up to 50 mm in most engineering materials, this makes them unique for establishing residual-stress distributions non-destructively. D1A is particularly suited for through-surface measurements as it does not suffer from instrumental surface aberrations commonly found on multidetector instruments, while D20 is best for fast internal-strain scanning. Two examples for residual-stress measurements in a shot-peened material, and in a weld are presented to demonstrate the attractive features of both instruments. (author).

SR-Can. Data and uncertainty assessment. Matrix diffusivity and porosity in situ

International Nuclear Information System (INIS)

Jinsong Liu; Loefgren, Martin; Neretnieks, Ivars

2006-12-01

and show beyond doubt that the electrical conductivity method using AC gives the expected information on transport properties (diffusivities) of the pores of crystalline rocks. The electrical conductivity method is much faster and can be used to measure large samples. It has recently been adopted for use in deep boreholes. Tens of thousands of measurements have been made at Simpevarp, Laxemar and Forsmark (Swedish sites) at depths of more than 1,000 m. The results of these measurements form the basis for our proposed diffusion values to be used in Performance Assessment (PA) for the candidate sites (Performance Assessment (PA) used in this report is synonymous to Safety Assessment (SA) sometimes used by other authors). The in situ data are obtained essentially in undisturbed rock and have not been subject to either stress release or disturbances due to sample preparation. The small disturbance nearest the borehole is negligible because the electrical conductivity method samples rock extending to more than a metre from the borehole. A large number of laboratory measurements have been analysed in order to ensure that other effects that cannot be controlled in the in situ measurements do not influence the down-hole data. No unexpected effects have been found. Rock matrix porosity in situ measurements are extremely scarce. However, it has been possible to use some of the in situ measurements to estimate the increase in porosity when taking up rock from its natural environment to the laboratory. One example of such an investigation is briefly discussed to show how this was done. In one in situ diffusion experiment performed at a depth of 60 m in granitic rock in Sweden the experimental conditions were such that it was ensured that any rock stress changes due to the presence of the drift and the presence of the borehole were avoided. The rock was thus subject to 'virgin stress'. Over-coring after exposure to tracers for three and a half years and detailed sampling and

SR-Can. Data and uncertainty assessment. Matrix diffusivity and porosity in situ

Energy Technology Data Exchange (ETDEWEB)

Jinsong Liu; Loefgren, Martin; Neretnieks, Ivars [Dept. of Chemical Engineering and Technology, Royal Inst. of Technology, Stockholm (Sweden)

2006-12-15

and show beyond doubt that the electrical conductivity method using AC gives the expected information on transport properties (diffusivities) of the pores of crystalline rocks. The electrical conductivity method is much faster and can be used to measure large samples. It has recently been adopted for use in deep boreholes. Tens of thousands of measurements have been made at Simpevarp, Laxemar and Forsmark (Swedish sites) at depths of more than 1,000 m. The results of these measurements form the basis for our proposed diffusion values to be used in Performance Assessment (PA) for the candidate sites (Performance Assessment (PA) used in this report is synonymous to Safety Assessment (SA) sometimes used by other authors). The in situ data are obtained essentially in undisturbed rock and have not been subject to either stress release or disturbances due to sample preparation. The small disturbance nearest the borehole is negligible because the electrical conductivity method samples rock extending to more than a metre from the borehole. A large number of laboratory measurements have been analysed in order to ensure that other effects that cannot be controlled in the in situ measurements do not influence the down-hole data. No unexpected effects have been found. Rock matrix porosity in situ measurements are extremely scarce. However, it has been possible to use some of the in situ measurements to estimate the increase in porosity when taking up rock from its natural environment to the laboratory. One example of such an investigation is briefly discussed to show how this was done. In one in situ diffusion experiment performed at a depth of 60 m in granitic rock in Sweden the experimental conditions were such that it was ensured that any rock stress changes due to the presence of the drift and the presence of the borehole were avoided. The rock was thus subject to 'virgin stress'. Over-coring after exposure to tracers for three and a half years and detailed sampling

Probing Stress States in Silicon Nanowires During Electrochemical Lithiation Using In Situ Synchrotron X-Ray Microdiffraction

Directory of Open Access Journals (Sweden)

Imran Ali

2018-04-01

Full Text Available Silicon is considered as a promising anode material for the next-generation lithium-ion battery (LIB due to its high capacity at nanoscale. However, silicon expands up to 300% during lithiation, which induces high stresses and leads to fractures. To design silicon nanostructures that could minimize fracture, it is important to understand and characterize stress states in the silicon nanostructures during lithiation. Synchrotron X-ray microdiffraction has proven to be effective in revealing insights of mechanical stress and other mechanics considerations in small-scale crystalline structures used in many important technological applications, such as microelectronics, nanotechnology, and energy systems. In the present study, an in situ synchrotron X-ray microdiffraction experiment was conducted to elucidate the mechanical stress states during the first electrochemical cycle of lithiation in single-crystalline silicon nanowires (SiNWs in an LIB test cell. Morphological changes in the SiNWs at different levels of lithiation were also studied using scanning electron microscope (SEM. It was found from SEM observation that lithiation commenced predominantly at the top surface of SiNWs followed by further progression toward the bottom of the SiNWs gradually. The hydrostatic stress of the crystalline core of the SiNWs at different levels of electrochemical lithiation was determined using the in situ synchrotron X-ray microdiffraction technique. We found that the crystalline core of the SiNWs became highly compressive (up to -325.5 MPa once lithiation started. This finding helps unravel insights about mechanical stress states in the SiNWs during the electrochemical lithiation, which could potentially pave the path toward the fracture-free design of silicon nanostructure anode materials in the next-generation LIB.

Stress measurements using the CFDF

International Nuclear Information System (INIS)

Maayouf, R.M.A.; Abdel-Latif, I.A.; Khalil, M.I.

2000-01-01

The present work deals with neutron diffraction measurements performed using the Cairo Fourier Diffractometer Facility (CFDF) for stress analysis.The CFDF has 0.45% resolution and a value l.lxl0 6 neutrons . cm -2 , s -1 of integral neutron flux at the sample position. While one of the two samples used for the present measurements was made from two steel cylindrical rods ( 5.5 mm in diameter) electrically welded together, the second one was a stress free steel rod of the same material. The stress distribution after welding was studied from the measured, by the CFDF, diffraction patterns . It has been found from the present measurements that the strain at the welding point is higher than any point far from it; verifying that the CFDF can be successfully used for stress measurement

Method for in situ carbon deposition measurement for solid oxide fuel cells

Science.gov (United States)

Kuhn, J.; Kesler, O.

2014-01-01

Previous methods to measure carbon deposition in solid oxide fuel cell (SOFC) anodes do not permit simultaneous electrochemical measurements. Electrochemical measurements supplemented with carbon deposition quantities create the opportunity to further understand how carbon affects SOFC performance and electrochemical impedance spectra (EIS). In this work, a method for measuring carbon in situ, named here as the quantification of gasified carbon (QGC), was developed. TGA experiments showed that carbon with a 100 h residence time in the SOFC was >99.8% gasified. Comparison of carbon mass measurements between the TGA and QGC show good agreement. In situ measurements of carbon deposition in SOFCs at varying molar steam/carbon ratios were performed to further validate the QGC method, and suppression of carbon deposition with increasing steam concentration was observed, in agreement with previous studies. The technique can be used to investigate in situ carbon deposition and gasification behavior simultaneously with electrochemical measurements for a variety of fuels and operating conditions, such as determining conditions under which incipient carbon deposition is reversible.

In-situ measurement of mechanical properties of structural components using cyclic ball indentation technique

International Nuclear Information System (INIS)

Chatterjee, S.; Madhusoodanan, K.; Panwar, Sanjay; Rupani, B.B.

2007-01-01

Material properties of components change during service due to environmental conditions. Measurement of mechanical properties of the components is important for assessing their fitness for service. In many instances, it is not possible to remove sizable samples from the component for doing the measurement in laboratory. In-situ technique for measurement of mechanical properties has great significance in such cases. One of the nondestructive methods that can be adopted for in-situ application is based on cyclic ball indentation technique. It involves multiple indentation cycles (at the same penetration location) on a metallic surface by a spherical indenter. Each cycle consists of indentation, partial unload and reload sequences. Presently, commercial systems are available for doing indentation test on structural component for limited applications. But, there is a genuine need of remotely operable compact in-situ property measurement system. Considering the importance of such applications Reactor Engineering Division of BARC has developed an In-situ Property Measurement System (IProMS), which can be used for in-situ measurement of mechanical properties of a flat or tubular component. This paper highlights the basic theory of measurement, qualification tests on IProMS and results from tests done on flat specimens and tubular component. (author)

Neutron-diffraction measurements of stress

International Nuclear Information System (INIS)

Holden, T.M.

1995-01-01

Experiments on bent steam-generator tubing have shown that different diffraction peaks, (1 1 1) or (0 0 2), give different results for the sign and magnitude of the stress and strain. From an engineering standpoint, the macroscopic stress field cannot be both positive and negative in the same volume, so this difference must be due to intergranular effects superposed on the macroscopic stress field. Uniaxial tensile test experiments with applied stresses beyond the 0.2% offset yield stress, help to understand this anomaly, by demonstrating the different strain response to applied stress along different crystallographic axes.When Zr-alloys are cooled from elevated temperatures, thermal stresses always develop, so that it is difficult to obtain a stress-free lattice spacing from which residual strains may be derived. From measurements of the temperature dependence of lattice spacing, the temperature at which the thermal stresses vanish may be found. From the lattice spacing at this temperature the stress-free lattice spacings at room temperature can be obtained readily.To interpret the measured strains in terms of macroscopic stress fields it is necessary to know the diffraction elastic constants. Neutron diffraction measurements of the diffraction elastic constants in a ferritic steel for the [1 1 0], [0 0 2] and [2 2 2] crystallographic axes, in directions parallel and perpendicular to the applied stress are compared with theoretical diffraction elastic constants. (orig.)

In-situ membrane hydration measurement of proton exchange membrane fuel cells

Science.gov (United States)

Lai, Yeh-Hung; Fly, Gerald W.; Clapham, Shawn

2015-01-01

Achieving proper membrane hydration control is one of the most critical aspects of PEM fuel cell development. This article describes the development and application of a novel 50 cm2 fuel cell device to study the in-situ membrane hydration by measuring the through-thickness membrane swelling via an array of linear variable differential transducers. Using this setup either as an air/air (dummy) cell or as a hydrogen/air (operating) cell, we performed a series of hydration and dehydration experiments by cycling the RH of the inlet gas streams at 80 °C. From the linear relationship between the under-the-land swelling and the over-the-channel water content, the mechanical constraint within the fuel cell assembly can suppress the membrane water uptake by 11%-18%. The results from the air/air humidity cycling test show that the membrane can equilibrate within 120 s for all RH conditions and that membrane can reach full hydration at a RH higher than 140% in spite of the use of a liquid water impermeable Carbel MP30Z microporous layer. This result confirms that the U.S. DOE's humidity cycling mechanical durability protocol induces sufficient humidity swings to maximize hygrothermal mechanical stresses. This study shows that the novel experimental technique can provide a robust and accurate means to study the in-situ hydration of thin membranes subject to a wide range of fuel cell conditions.

Comparison of GRACE with in situ hydrological measurement data ...

African Journals Online (AJOL)

Comparison of GRACE with in situ hydrological measurement data shows storage depletion in Hai River basin, Northern China. ... of the world, their application in conjunction with hydrological models could improve hydrological studies.

Stress ratio determination from the core-disking phenomenon

International Nuclear Information System (INIS)

Lehnhoff, T.F.; Stefansson, B.; Thirumalai, K.

1982-08-01

The ability to predict in situ stress conditions from standard core samples offers planning and site-selection advantages for most underground facilities. This paper presents an empirical relation for estimating the horizontal to vertical stress ratio in basalt. The resulting estimates can then be used to help assess the extent to which measurement of in situ stress is required. The core disking phenomenon has long been used as an indicator of high in situ stress. It is concluded that disks form as the result of tensile failure initiation rather than shear failure initiation of the core. It is deduced that the tensile failure begins at the edge of the core and propagates toward the center in shear rather than beginning at the center and propagating outward. An empirical relation for horizontal to vertical stress ratio variation with depth has been developed and is shown to agree substantially with previous measured horizontal to vertical stress ratios for locations in several areas of the world. The stress-ratio predictions are justified based on finite-element studies using linear elastic analysis and also nonlinear (tension cut-off) analysis. Indications of fracture propagation paths were determined from the analyses. The shape of the predicted propagation path agrees well with physical observations

In-situ Observation of Cross-Sectional Microstructural Changes and Stress Distributions in Fracturing TiN Thin Film during Nanoindentation.

Science.gov (United States)

Zeilinger, Angelika; Todt, Juraj; Krywka, Christina; Müller, Martin; Ecker, Werner; Sartory, Bernhard; Meindlhumer, Michael; Stefenelli, Mario; Daniel, Rostislav; Mitterer, Christian; Keckes, Jozef

2016-03-07

Load-displacement curves measured during indentation experiments on thin films depend on non-homogeneous intrinsic film microstructure and residual stress gradients as well as on their changes during indenter penetration into the material. To date, microstructural changes and local stress concentrations resulting in plastic deformation and fracture were quantified exclusively using numerical models which suffer from poor knowledge of size dependent material properties and the unknown intrinsic gradients. Here, we report the first in-situ characterization of microstructural changes and multi-axial stress distributions in a wedge-indented 9 μm thick nanocrystalline TiN film volume performed using synchrotron cross-sectional X-ray nanodiffraction. During the indentation, needle-like TiN crystallites are tilted up to 15 degrees away from the indenter axis in the imprint area and strongly anisotropic diffraction peak broadening indicates strain variation within the X-ray nanoprobe caused by gradients of giant compressive stresses. The morphology of the multiaxial stress distributions with local concentrations up to -16.5 GPa correlate well with the observed fracture modes. The crack growth is influenced decisively by the film microstructure, especially by the micro- and nano-scopic interfaces. This novel experimental approach offers the capability to interpret indentation response and indenter imprint morphology of small graded nanostructured features.

Rock properties and their effect on thermally-induced displacements and stresses

International Nuclear Information System (INIS)

Chan, T.; Hood, M.; Board, M.

1980-02-01

A discussion is given of the importance of material properties in the finite-element calculations for thermally induced displacements and stresses resulting from a heating experiment in an in-situ granitic rock, at Stripa, Sweden. Comparisons are made between field measurements and finite element method calculations using (1) temperature independent, (2) temperature dependent thermal and thermomechanical properties and (3) in-situ and laboratory measurements for Young's modulus. The calculations of rock displacements are influenced predominantly by the temperature dependence of the thermal expansion coefficient, whereas the dominant factor affecting predictions for rock stresses is the in-situ modulus

In situ detection of porosity initiation during aluminum thin film anodizing

Science.gov (United States)

Van Overmeere, Quentin; Nysten, Bernard; Proost, Joris

2009-02-01

High-resolution curvature measurements have been performed in situ during aluminum thin film anodizing in sulfuric acid. A well-defined transition in the rate of internal stress-induced curvature change is shown to allow for the accurate, real-time detection of porosity initiation. The validity of this in situ diagnostic tool was confirmed by a quantitative analysis of the spectral density distributions of the anodized surfaces. These were obtained by analyzing ex situ atomic force microscopy images of surfaces anodized for different times, and allowed to correlate the in situ detected transition in the rate of curvature change with the appearance of porosity.

Application of indirect stress measurement techniques (non strain gauge based technology) to quantify stress environments in mines

CSIR Research Space (South Africa)

Stacey, TR

2002-03-01

Full Text Available Reliable values of in situ stress are essential for the valid modelling of mine layouts. Available non-strain gauge methods are reviewed as potential practical techniques for South African mines. From this review it is concluded that the most...

In-situ measurement of environment radioactivity by mobile nuclear field laboratory (MNFL)

International Nuclear Information System (INIS)

Gopalani, Deepak; Mathur, A.P.; Rawat, D.K.; Barala, S.S.; Singhal, K.P.; Singh, G.P.; Samant, R.P.

2008-01-01

In-situ measurement of environment radioactivity is useful tool for determine the unusual increase of radioactivity at any place due to any nuclear eventuality take place. A mobile nuclear field laboratory has been designed and developed for in-situ measurement of environment radioactivity at any desired location. This vehicle is equipped with different monitoring and analysis instruments. These equipment can be operated while vehicle is moving. The measured data can be stored in computer. This vehicle has the space for storage of various environmental matrices of affected area and these can analysis in laboratory. (author)

Environmental gamma-ray measurements using in situ and core sampling techniques

International Nuclear Information System (INIS)

Dickson, H.W.; Kerr, G.D.; Perdue, P.T.; Abdullah, S.A.

1976-01-01

Dose rates from natural radionuclides and 137 Cs in soils of the Oak Ridge area have been determined from in situ and core sample measurements. In situ γ-ray measurements were made with a transportable spectrometer. A tape of spectral data and a soil core sample from each site were returned to ORNL for further analysis. Information on soil composition, density and moisture content and on the distribution of cesium in the soil was obtained from the core samples. In situ spectra were analyzed by a computer program which identified and assigned energies to peaks, integrated the areas under the peaks, and calculated radionuclide concentrations based on a uniform distribution in the soil. The assumption of a uniform distribution was adequate only for natural radionuclides, but simple corrections can be made to the computer calculations for man-made radionuclides distributed on the surface or exponentially in the soil. For 137 Cs a correction was used based on an exponential function fitted to the distribution measured in core samples. At typical sites in Oak Ridge, the dose rate determined from these measurements was about 5 μrad/hr. (author)

RESEARCH OF THE STRESS STATE OF A MODIFIED IN-SITU CONCRETE

Directory of Open Access Journals (Sweden)

D. V. Rudenko

2016-12-01

Full Text Available Purpose. The article focuses on investigation of the stress state of a modified in-situ concrete of natural hardening. Methodology. To achieve the aim, the research of the microstructure of the modified cement matrix of concrete, as well as the mechanism of structure formation of modified concrete with natural hardening was conducted; the methods for reliable evaluation of concrete strength were defined. Findings. The development of internal stresses affects the properties of concretedifferently. With an increase in temperature-shrinkage deformations in time and, thus, with increasing structural stresses in the cement sheath around the grains of the filler two opposite processes may develop: zone of plastic flow or cracking. Originality. It was established that the structural features complex of the modified concrete when the load transfer leads to the formation of extensive zones of prefracture which is able to absorb a significant amount of elastic strain energy that provides the design deformation properties of the concrete for special purposes. Ideas about the definition of the criteria of cracking modified concrete, hardening under natural conditions had further development. Practical value. The resulting equations allow to solve the problem about the minimum level of structural stress in monolithic concrete in a saturated large placeholder, as well as to assess the influence of structural stresses on the properties of concrete. In normal concrete with a relatively thin cement sheath at temperature-shrinkage deformations, high tangential and low radial tension occur. In vivo, this stress is higher as a result of higher values of Δε(τ, which is not observed in the modified concrete. In the modified concretes only tangential stresses are the greatest danger to structures. The change of shrinkage stress with time is straightforward. The total temperature-shrinkage deformations have a sawtooth graph. For modified concrete the amplitude is 48

Stress measurements in the Naesliden Mine

Energy Technology Data Exchange (ETDEWEB)

Leijon, B. [Univ. of Luleaa, Sweden; Carlsson, H.; Myrvang, A.

1980-05-15

Determinations of virgin stresses were performed at an early stage of the Naesliden Project in order to obtain input data for the finite element models of the mine. The Leeman three-dimensional overcoring technique was used at five locations on levels ranging from 210 m to 460 m below surface. Stress data were obtained at four of these locations. The results show an excess of horizontal stresses whilst the vertical stress is in accordance with the gravitational load from the overburden. The major and intermediate principal stresses are sub-horizontal and directed respectively perpendicular and parallel to the schisotsity of the wall rock and the strike of the tabular ore body. The minor principal stress is directed almost vertically. Stresses were also measured close to a stope on 300 m level in the mine. Biaxial and triaxial overcoring measurements were made at eighteen points between 0.25 m and 7.2 m above the roof of the stope. The stresses were found to have magnitudes of about 70 MPa close to the roof and to decrease rapidly with the distance from the roof. Stress measurements were made in connection with slot blastings in the foot wall, the latter measure being made in an attempt to de-stress the roof of stope 3. Two methods were used for stress monitorings, both showing that expected stress changes did not take place. Long-term stress guages have been installed in the ore body in order to monitor expected re-distributions of stresses due to mining. So far, the recorded stress changes are below 5 MPa.

In situ radiation measurements at the former Soviet Nuclear Test Site

International Nuclear Information System (INIS)

Tipton, W.J.

1996-06-01

A team from the Remote Sensing Laboratory conducted a series of in situ radiological measurements at the former Soviet Nuclear Test Site near Semipalatinsk, Kazakhstan, during the period of July 21-30, 1994. The survey team measured the terrestrial gamma radiation at selected areas on the site to determine the levels of natural and man-made radiation. The survey was part of a cooperative effort between the United States team and teams of radiation scientists from the National Nuclear Center of the Republic of Kazakhstan and the V.G. Khlopin Radium Institute in St. Petersburg, Russia. In addition to in situ radiation measurements made by the United States and Russian teams, soil samples were collected and analyzed by the Russian and Kazakhstani teams. All teams conducted their measurements at ten locations within the test site. The United States team also made a number of additional measurements to locate and verify the positions of three potential fallout plumes containing plutonium contamination from nonnuclear tests. In addition, the United States team made several measurements in Kurchatov City, the housing area used by personnel and their families who work(ed) at the test sites. Comparisons between the United States and Russian in situ measurements and the soil sample results are presented as well as comparisons with a Soviet aerial survey conducted in 1990-1991. The agreement between the different types of measurements made by all three countries was quite good

In situ Measurements of Phytoplankton Fluorescence Using Low Cost Electronics

Directory of Open Access Journals (Sweden)

Dana L. Wright

2013-06-01

Full Text Available Chlorophyll a fluorometry has long been used as a method to study phytoplankton in the ocean. In situ fluorometry is used frequently in oceanography to provide depth-resolved estimates of phytoplankton biomass. However, the high price of commercially manufactured in situ fluorometers has made them unavailable to some individuals and institutions. Presented here is an investigation into building an in situ fluorometer using low cost electronics. The goal was to construct an easily reproducible in situ fluorometer from simple and widely available electronic components. The simplicity and modest cost of the sensor makes it valuable to students and professionals alike. Open source sharing of architecture and software will allow students to reconstruct and customize the sensor on a small budget. Research applications that require numerous in situ fluorometers or expendable fluorometers can also benefit from this study. The sensor costs US$150.00 and can be constructed with little to no previous experience. The sensor uses a blue LED to excite chlorophyll a and measures fluorescence using a silicon photodiode. The sensor is controlled by an Arduino microcontroller that also serves as a data logger.

In situ measurement of tritium permeation through stainless steel

Science.gov (United States)

Luscher, Walter G.; Senor, David J.; Clayton, Kevin K.; Longhurst, Glen R.

2013-06-01

The TMIST-2 irradiation experiment was conducted in the Advanced Test Reactor at Idaho National Laboratory to evaluate tritium permeation through Type 316 stainless steel (316 SS). The interior of a 316 SS seamless tube specimen was exposed to a 4He carrier gas mixed with a specified quantity of tritium (T2) to yield partial pressures of 0.1, 5, and 50 Pa at 292 °C and 330 °C. In situ tritium permeation measurements were made by passing a He-Ne sweep gas over the outer surface of the specimen to carry the permeated tritium to a bubbler column for liquid scintillation counting. Results from in situ permeation measurements were compared with predictions based on an ex-reactor permeation correlation in the literature. In situ permeation data were also used to derive an in-reactor permeation correlation as a function of temperature and pressure over the ranges considered in this study. In addition, the triton recoil contribution to tritium permeation, which results from the transmutation of 3He to T, was also evaluated by introducing a 4He carrier gas mixed with 3He at a partial pressure of 1013 Pa at 330 °C. Less than 3% of the tritium resulting from 3He transmutation contributed to tritium permeation.

Measurement of Localized Corrosion Rates at Inclusion Particles in AA7075 by In Situ Three Dimensional (3D) X-ray Synchrotron Tomography

Energy Technology Data Exchange (ETDEWEB)

Singh, Sudhanshu S.; Williams, Jason J.; Stannard, Tyler J.; Xiao, Xianghui; De Carlo, Francesco; Chawla, Nikhilesh

2016-03-01

In situ X-ray synchrotron tomography was used to measure the localized corrosion rate of Mg2Si particles present in 7075 aluminum alloys in deionized ultra-filtered (DIUF) water. The evolution of hydrogen bubbles was captured as a function of time and the measured volume was used to calculate the local corrosion rate of Mg2Si particles. It was shown that in the absence of chloride ions, stress was needed to create fresh particle surfaces, either by fracture or debonding, to initiate corrosion at the particles.

In-situ measurements in Vesivehmaa air field - STUK team

Energy Technology Data Exchange (ETDEWEB)

Markkanen, M.; Honkamaa, T.; Niskala, P. [Finnish Centre for Radiation and Nuclear Safety, Helsinki (Finland)

1997-12-31

Nineteen in-situ gamma-ray spectrometric measurements were performed in Vesivehmaa air field on 17th August 1995. The results for {sup 137}Cs and natural radionuclides are in good agreement with the results from soil sampling and laboratory analyses. (au).

In-situ measurements in Vesivehmaa air field - STUK team

Energy Technology Data Exchange (ETDEWEB)

Markkanen, M; Honkamaa, T; Niskala, P [Finnish Centre for Radiation and Nuclear Safety, Helsinki (Finland)

1998-12-31

Nineteen in-situ gamma-ray spectrometric measurements were performed in Vesivehmaa air field on 17th August 1995. The results for {sup 137}Cs and natural radionuclides are in good agreement with the results from soil sampling and laboratory analyses. (au).

The measurement of residual stresses in claddings

International Nuclear Information System (INIS)

Hofer, G.; Bender, N.

1978-01-01

The ring core method, a variation of the hole drilling method for the measurement of biaxial residual stresses, has been extended to measure stresses from depths of about 5 to 25mm. It is now possible to measure the stress profiles of clad material. Examples of measured stress profiles are shown and compared with those obtained with a sectioning technique. (author)

A New Method of Stress Measurement Based upon Elastic Deformation of Core Sample with Stress Relief by Drilling

Science.gov (United States)

Ito, T.; Funato, A.; Tamagawa, T.; Tezuka, K.; Yabe, Y.; Abe, S.; Ishida, A.; Ogasawara, H.

2017-12-01

When rock is cored at depth by drilling, anisotropic expansion occurs with the relief of anisotropic rock stresses, resulting in a sinusoidal variation of core diameter with a period of 180 deg. in the core roll angle. The circumferential variation of core diameter is given theoretically as a function of rock stresses. These new findings can lead various ideas to estimate the rock stress from circumferential variation of core diameter measured after the core retrieving. In the simplest case when a single core sample is only available, the difference between the maximum and minimum components of rock stress in a plane perpendicular to the drilled hole can be estimated from the maximum and minimum core diameters (see the detail in, Funato and Ito, IJRMMS, 2017). The advantages of this method include, (i) much easier measurement operation than those in other in-situ or in-lab estimation methods, and (ii) applicability in high stress environment where stress measurements need pressure for packers or pumping system for the hydro-fracturing methods higher than their tolerance levels. We have successfully tested the method at deep seismogenic zones in South African gold mines, and we are going to apply it to boreholes collared at 3 km depth and intersecting a M5.5 rupture plane several hundred meters below the mine workings in the ICDP project of "Drilling into Seismogenic zones of M2.0 - M5.5 earthquakes in deep South African gold mines" (DSeis) (e.g., http://www.icdp-online.org/projects/world/africa/orkney-s-africa/details/). If several core samples with different orientation are available, all of three principal components of 3D rock stress can be estimated. To realize this, we should have several boreholes drilled in different directions in a rock mass where the stress field is considered to be uniform. It is commonly carried out to dill boreholes in different directions from a mine gallery. Even in a deep borehole drilled vertically from the ground surface, the

Thermal stress measurement in continuous welded rails using the hole-drilling method

Science.gov (United States)

Zhu, Xuan; Lanza di Scalea, Francesco; Fateh, Mahmood

2016-04-01

The absence of expansion joints in Continuous Welded Rail (CWR) has created the need for the railroad industry to determine the in-situ level of thermal stresses so as to prevent train accidents caused by rail buckling in hot weather and by rail breakage in cold weather. The development of non-destructive or semi-destructive methods for determining the level of thermal stresses in rails is today a high research priority. This study explores the known hole-drilling method as a possible solution to this problem. A new set of calibration coefficients to compute the relieved stress field with the finer hole depth increments was determined by a 3D Finite Element Analysis that modeled the entire hole geometry, including the mechanics of the hole bottom and walls. To compensate the residual stress components, a linear relationship was experimentally established between the longitudinal and the vertical residual stresses of two common sizes of rails, the 136RE and the 141RE, with statistical significance. This result was then utilized to isolate the longitudinal thermal stress component in hole-drilling tests conducted on the 136RE and 141RE thermally-loaded rails at the Large-scale CWR Test-bed of UCSD's Powell Research Laboratories. The results from the Test-bed showed that the hole-drilling procedure, with the appropriate residual stress compensation, can indeed estimate the in-situ thermal stresses to achieve a +/-5°F accuracy of Neutral Temperature determination with a 90% statistical confidence, which is the desired industry gold standard.

Application of in situ measurement for site remediation and final status survey of decommissioning KRR site

Energy Technology Data Exchange (ETDEWEB)

Hong, Sang Bum; Nam, Jong Soo; Choi, Yong Suk; Seo, Bum Kyoung; Moon, Jei Kwon [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

2016-06-15

In situ gamma spectrometry has been used to measure environmental radiation, assumptions are usually made about the depth distribution of the radionuclides of interest in the soil. The main limitation of in situ gamma spectrometry lies in determining the depth distribution of radionuclides. The objective of this study is to develop a method for subsurface characterization by in situ measurement. The peak to valley method based on the ratio of counting rate between the photoelectric peak and Compton region was applied to identify the depth distribution. The peak to valley method could be applied to establish the relation between the spectrally derived coefficients (Q) with relaxation mass per unit area (β) for various depth distribution in soil. The in situ measurement results were verified by MCNP simulation and calculated correlation equation. In order to compare the depth distributions and contamination levels in decommissioning KRR site, in situ measurement and sampling results were compared. The in situ measurement results and MCNP simulation results show a good correlation for laboratory measurement. The simulation relationship between Q and source burial for the source layers have exponential relationship for a variety depth distributions. We applied the peak to valley method to contaminated decommissioning KRR site to determine a depth distribution and initial activity without sampling. The observed results has a good correlation, relative error between in situ measurement with sampling result is around 7% for depth distribution and 4% for initial activity. In this study, the vertical activity distribution and initial activity of {sup 137}Cs could be identifying directly through in situ measurement. Therefore, the peak to valley method demonstrated good potential for assessment of the residual radioactivity for site remediation in decommissioning and contaminated site.

In situ observation of stress relaxation in epitaxial graphene

International Nuclear Information System (INIS)

N'Diaye, Alpha T; Coraux, Johann; Busse, Carsten; Michely, Thomas; Gastel, Raoul van; Poelsema, Bene; MartInez-Galera, Antonio J; Gomez-RodrIguez, Jose M; Hattab, Hichem; Wall, Dirk; Heringdorf, Frank-J Meyer zu; Hoegen, Michael Horn-von

2009-01-01

Upon cooling, branched line defects develop in epitaxial graphene grown at high temperature on Pt(111) and Ir(111). Using atomically resolved scanning tunneling microscopy, we demonstrate that these defects are wrinkles in the graphene layer, i.e. stripes of partially delaminated graphene. With low energy electron microscopy (LEEM), we investigate the wrinkling phenomenon in situ. Upon temperature cycling, we observe hysteresis in the appearance and disappearance of the wrinkles. Simultaneously with wrinkle formation a change in bright field imaging intensity of adjacent areas and a shift in the moire spot positions for micro diffraction of such areas takes place. The stress relieved by wrinkle formation results from the mismatch in thermal expansion coefficients of graphene and the substrate. A simple one-dimensional model taking into account the energies related to strain, delamination and bending of graphene is in qualitative agreement with our observations.

Stress transmission in soil

DEFF Research Database (Denmark)

Lamandé, Mathieu; Schjønning, Per

We urgently need increased quantitative knowledge on stress transmission in real soils loaded with agricultural machinery. 3D measurements of vertical stresses under tracked wheels were performed in situ in a Stagnic Luvisol (clay content 20 %) continuously cropped with small grain cereals......). Seven load cells were inserted horizontally from a pit with minimal disturbance of soil in each of three depths (0.3, 0.6 and 0.9 m), covering the width of the wheeled area. The position of the wheel relative to the transducers was recorded using a laser sensor. Finally, the vertical stresses near...... the soil-tyre interface were measured in separate tests by 17 stress transducers across the width of the tyres. The results showed that the inflation pressure controlled the level of maximum stresses at 0.3 m depth, while the wheel load was correlated to the measured stresses at 0.9 m depth. This supports...

Field instruments for real time in-situ crude oil concentration measurements

International Nuclear Information System (INIS)

Fuller, C.B.; Bonner, J.S.; Page, C.A.; Arrambide, G.; Sterling, M.C.Jr.; Ojo, T.O.

2003-01-01

Accidental oil spills, contaminant release during resuspension, storms, and harmful algal blooms are all episodic events that can effect coastal margins. It is important to quantitatively describe water and ecological quality evolution and predict the impact to these areas by such events, but traditional sampling methods miss environmental activity during cyclical events. This paper presents a new sampling approach that involves continuous, real-time in-situ monitoring to provide data for development of comprehensive modeling protocols. It gives spill response coordinators greater assurance in making decisions using the latest visualization tools which are based on a good understanding of the physical processes at work in pulsed events. Five sensors for rapid monitoring of crude oil concentrations in aquatic systems were described. The in-situ and ex-situ sensors can measure plume transport and estimate polycyclic aromatic hydrocarbon exposure concentrations to assess risk of toxicity. A brief description and evaluation of the following 5 sensors was provided: the LISST-100 by Sequoia Instrument, a submersible multi-angle laser scattering instrument; the AU-10 field fluorometer by Turner Designs, an ex-situ single wavelength fluorometer; the Flashlamp by WET Labs Inc., an in-situ single wavelength fluorometer; and, the ECO-FL3 and SAFire by WET Labs Inc., two in-situ multiple wavelength fluorometers. These instruments were used to analyze crude oil emissions of various concentrations. All of the instruments followed a linear response within the tested concentration range. At the lowest concentrations the LISST-100 was not as effective as the fluorometers because of limited particle volume for scatter. For the AU-10 field fluorometer, the highest concentrations tested were above the measurement range of the instrument. 6 refs., 5 figs

HSRL-2 aerosol optical measurements and microphysical retrievals vs. airborne in situ measurements during DISCOVER-AQ 2013: an intercomparison study

Directory of Open Access Journals (Sweden)

P. Sawamura

2017-06-01

Full Text Available We present a detailed evaluation of remotely sensed aerosol microphysical properties obtained from an advanced, multi-wavelength high-spectral-resolution lidar (HSRL-2 during the 2013 NASA DISCOVER-AQ field campaign. Vertically resolved retrievals of fine-mode aerosol number, surface-area, and volume concentration as well as aerosol effective radius are compared to 108 collocated, airborne in situ measurement profiles in the wintertime San Joaquin Valley, California, and in summertime Houston, Texas. An algorithm for relating the dry in situ aerosol properties to those obtained by the HSRL at ambient relative humidity is discussed. We show that the HSRL-2 retrievals of ambient fine-mode aerosol surface-area and volume concentrations agree with the in situ measurements to within 25 and 10 %, respectively, once hygroscopic growth adjustments have been applied to the dry in situ data. Despite this excellent agreement for the microphysical properties, extinction and backscatter coefficients at ambient relative humidity derived from the in situ aerosol measurements using Mie theory are consistently smaller than those measured by the HSRL, with average differences of 31 ± 5 % and 53 ± 11 % for California and Texas, respectively. This low bias in the in situ estimates is attributed to the presence of coarse-mode aerosol that are detected by HSRL-2 but that are too large to be well sampled by the in situ instrumentation. Since the retrieval of aerosol volume is most relevant to current regulatory efforts targeting fine particle mass (PM2. 5, these findings highlight the advantages of an advanced 3β + 2α HSRL for constraining the vertical distribution of the aerosol volume or mass loading relevant for air quality.

Stress Measurement by Geometrical Optics

Science.gov (United States)

Robinson, R. S.; Rossnagel, S. M.

1986-01-01

Fast, simple technique measures stresses in thin films. Sample disk bowed by stress into approximately spherical shape. Reflected image of disk magnified by amount related to curvature and, therefore, stress. Method requires sample substrate, such as cheap microscope cover slide, two mirrors, laser light beam, and screen.

Calibration and application of a HPGe gamma spectrometer for in-situ measurements

International Nuclear Information System (INIS)

Xiao Xuefu; Yue Qingyu

1992-02-01

The principle and methods of the calibration for an in-situ γ spectrometer are introduced. The calibration for a portable HPGe γ spectrometer has been completed. The N f /A(peak count rate per unit activity in soil) and N f /D(peak count rate per unit absorbed dose rate in the air) are listed. The uncertainties of the calibration factors are estimated. The in-situ measurements have been carried out in surroundings near the nuclear facilities and the data are compared with those measured by other methods

In situ evaluation of cadmium biomarkers in green algae

Energy Technology Data Exchange (ETDEWEB)

Simon, Dana F.; Davis, Thomas A. [Department of Chemistry, University of Montreal, P.O. Box 6128, Succursale Centre-ville, Montreal, Quebec H3C 3J7 (Canada); Tercier-Waeber, Mary-Lou [Analytical and Biophysical Environmental Chemistry, University of Geneva, Sciences II, 30 Quai Ernest-Ansermet, 1211 Geneva 4 (Switzerland); England, Roxane [Department of Chemistry, University of Montreal, P.O. Box 6128, Succursale Centre-ville, Montreal, Quebec H3C 3J7 (Canada); Wilkinson, Kevin J., E-mail: kj.wilkinson@umontreal.ca [Department of Chemistry, University of Montreal, P.O. Box 6128, Succursale Centre-ville, Montreal, Quebec H3C 3J7 (Canada)

2011-10-15

In situ measurements provide data that are the highly representative of the natural environment. In this paper, laboratory-determined biomarkers of Cd stress that were previously identified for the green alga Chlamydomonas reinhardtii, were tested in two French rivers: a contaminated site on the Riou Mort River and an 'uncontaminated' reference site on the Lot River. Transcript abundance levels were determined by real time qPCR for biomarkers thought to be Cd sensitive. Transcript levels were significantly higher (>5 fold) for organisms exposed to the contaminated site as compared to those exposed at the uncontaminated site. Biomarker mRNA levels were best correlated to free Cd (Cd{sup 2+}) rather than intracellular Cd, suggesting that they may be useful indicators of in situ stress. The paper shows that biomarker expression levels increased with time, were sensitive to metal levels and metal speciation and were higher in the 'contaminated' as opposed to the 'reference' site. - Highlights: > Biomarkers of Cd stress were tested in a contaminated and a reference site. > The organism was viable under exposure conditions and metal accumulation occurred. > Biomarker levels were correlated to Cd{sup 2+} and were higher in the contaminated site. - Algal transcription levels of several biomarkers were studied in two natural waters in situ.

Use of tensiometer for in situ measurement of nitrate leaching

Energy Technology Data Exchange (ETDEWEB)

Li, K.; Reddy, M.R.

1999-07-01

In order to monitor nitrate leaching from non-point source pollution, this study used tensiometers to measure in situ nitrate concentration and soil-moisture potential. Instead of filling the tensiometers with pure water, the study filled the tensiometers with nitrate ionic strength adjuster (ISA, 1 M (NH{sub 4}){sub 2}SO{sub 4}). After the installation of the tensiometers at various depths along soil profiles, a portable pressure transducer was used to measure the soil moisture potential, and a nitrate electrode attached to an ion analyzer was used to measure the nitrate concentration in situ. The measurement was continuous and non-destructive. To test this method in the laboratory, eight bottles filled with pure sand were treated with known nitrate solutions, and a tensiometer was placed in each bottle. Measurements were taken every day for 30 days. Laboratory test showed a linear relationship between the known nitrate concentration and the tensiometer readings (R{sup 2} = 0.9990). Then a field test was conducted in a watermelon field with green manure mulch. Field data indicated a potential of nitrate leaching below the soil depth of 100 cm when crop uptake of nutrients was low.

Quantitative comparison of in situ soil CO2 flux measurement methods

Science.gov (United States)

Jennifer D. Knoepp; James M. Vose

2002-01-01

Development of reliable regional or global carbon budgets requires accurate measurement of soil CO2 flux. We conducted laboratory and field studies to determine the accuracy and comparability of methods commonly used to measure in situ soil CO2 fluxes. Methods compared included CO2...

Paloma: In-Situ Measurement of the Isotopic Composition of Mars Atmosphere

Science.gov (United States)

Jambon, A.; Quemerais, E.; Chassiefiere, E.; Berthelier, J. J.; Agrinier, P.; Cartigny, P.; Javoy, M.; Moreira, M.; Sabroux, J. -C.; Sarda, P.; Pineau, J. -F.

2000-07-01

Scientific objectives for an atmospheric analysis of Mars are presented in the DREAM project. Among the information presently available most are fragmentary or limited in their precision for both major element (H, C, O, N) and noble gas isotopes. These data are necessary for the understanding and modelling of Mars atmospheric formation and evolution, and consequently for other planets, particularly the Earth. To fulfill the above requirements, two approaches can be envisonned: 1) analysis of a returned sample (DREAM project) or 2) in situ analysis, e.g. PALOMA project presented here. Among the advantages of in situ analysis, we notice: the minimal terrestrial contamination, the unlimited availability of gas to be analyzed and the possibility of multiple analyses (replicates, daynight... ). Difficulties specific to in situ analyses are of a very different kind to those of returned samples. In situ analysis could also be viewed as a preparation to future analysis of returned samples. Finally, some of the measurements will not be possible on Earth: for instance, radon and its short lived decay products, will provide complementary information to 4-He analysis and can only be obtained in situ, independently of analytical capabilities.

Matrix diffusion studies by electrical conductivity methods. Comparison between laboratory and in-situ measurements

International Nuclear Information System (INIS)

Ohlsson, Y.; Neretnieks, I.

1998-01-01

Traditional laboratory diffusion experiments in rock material are time consuming, and quite small samples are generally used. Electrical conductivity measurements, on the other hand, provide a fast means for examining transport properties in rock and allow measurements on larger samples as well. Laboratory measurements using electrical conductivity give results that compare well to those from traditional diffusion experiments. The measurement of the electrical resistivity in the rock surrounding a borehole is a standard method for the detection of water conducting fractures. If these data could be correlated to matrix diffusion properties, in-situ diffusion data from large areas could be obtained. This would be valuable because it would make it possible to obtain data very early in future investigations of potentially suitable sites for a repository. This study compares laboratory electrical conductivity measurements with in-situ resistivity measurements from a borehole at Aespoe. The laboratory samples consist mainly of Aespoe diorite and fine-grained granite and the rock surrounding the borehole of Aespoe diorite, Smaaland granite and fine-grained granite. The comparison shows good agreement between laboratory measurements and in-situ data

Investigations of some rock stress measuring techniques and the stress field in Norway

Energy Technology Data Exchange (ETDEWEB)

Hanssen, Tor Harald

1998-12-31

Rock stresses are important to the safe construction and operation of all man-made structures in rock, whether In mining, civil or petroleum engineering. The crucial issue is their relative magnitude and orientation. This thesis develops equipment and methods for further rock stress assessment and reevaluates existing overcoring rock stress measurements, and relates this information to the present geological setting. Both laboratory work and field work are involved. In the field, rock stresses are measured by the overcoring and the hydraulic fracturing technique. An observation technique for assessing likely high stresses is developed. The field data refer to several hydropower projects and to some offshore hydrocarbon fields. The principal sections are: (1) Tectonic setting in the western Fennoscandia, (2) Triaxial rock stress measurements by overcoring using the NTH cell (a strain gauge cell developed at the Norwegian technical university in Trondheim and based on the CSIR cell of the South African Council for Scientific and Industrial Research), (3) Laboratory testing of the NTH cell, (4) Quality ranking of stresses measured by the NTH cell, (4) Recalculated rock stresses and implications to the regional stress field, (5) Hydraulic fracturing stress measurements. 113 refs., 98 figs., 62 tabs.

Investigations of some rock stress measuring techniques and the stress field in Norway

Energy Technology Data Exchange (ETDEWEB)

Hanssen, Tor Harald

1997-12-31

Rock stresses are important to the safe construction and operation of all man-made structures in rock, whether In mining, civil or petroleum engineering. The crucial issue is their relative magnitude and orientation. This thesis develops equipment and methods for further rock stress assessment and reevaluates existing overcoring rock stress measurements, and relates this information to the present geological setting. Both laboratory work and field work are involved. In the field, rock stresses are measured by the overcoring and the hydraulic fracturing technique. An observation technique for assessing likely high stresses is developed. The field data refer to several hydropower projects and to some offshore hydrocarbon fields. The principal sections are: (1) Tectonic setting in the western Fennoscandia, (2) Triaxial rock stress measurements by overcoring using the NTH cell (a strain gauge cell developed at the Norwegian technical university in Trondheim and based on the CSIR cell of the South African Council for Scientific and Industrial Research), (3) Laboratory testing of the NTH cell, (4) Quality ranking of stresses measured by the NTH cell, (4) Recalculated rock stresses and implications to the regional stress field, (5) Hydraulic fracturing stress measurements. 113 refs., 98 figs., 62 tabs.

Savannah River Site Experiences in In Situ Field Measurements of Radioactive Materials

International Nuclear Information System (INIS)

Moore, F.S.

1999-01-01

This paper discusses some of the field gamma-ray measurements made at the Savannah River Site, the equipment used for the measurements, and lessons learned during in situ identification and characterization of radioactive materials

Laser-induced stresses versus mechanical stress power measurements during laser ablation of solids

International Nuclear Information System (INIS)

Shannon, M.A.; Russo, R.E.

1995-01-01

Laser-induced stresses resulting from high-power laser-material interactions have been studied extensively. However, the rate of change in mechanical energy, or stress power, due to laser-induced stresses has only recently been investigated. An unanswered question for monitoring laser-material interactions in the far-field is whether stress power differs from stresses measured, particularly with respect to laser-energy coupling to a solid target. This letter shows experimental acoustic data which demonstrate that stress power measured in the far field of the target shows changes in laser-energy coupling, whereas the stresses measured do not. For the ambient medium above the target, stress power and stress together reflect changes in laser-energy coupling. copyright 1995 American Institute of Physics

Measuring the stress field around an evolving crack in tensile deformed Mg AZ31 using three-dimensional X-ray diffraction

International Nuclear Information System (INIS)

Oddershede, Jette; Camin, Bettina; Schmidt, Søren; Mikkelsen, Lars P.; Sørensen, Henning Osholm; Lienert, Ulrich; Poulsen, Henning Friis; Reimers, Walter

2012-01-01

The stress field around a notch in a coarse grained Mg AZ31 sample has been measured under tensile load using the individual grains as probes in an in situ high energy synchrotron diffraction experiment. The experimental set-up, a variant of three-dimensional X-ray diffraction microscopy, allows the position, orientation and full stress tensor of each illuminated grain to be determined and, hence, enables the study of evolving stress fields in coarse grained materials with a spatial resolution equal to the grain size. Grain resolved information like this is vital for understanding what happens when the traditional continuum mechanics approach breaks down and fracture is governed by local heterogeneities (e.g. phase or stress differences) between grains. As a first approximation the results obtained were averaged through the thickness of the sample and compared with an elastic–plastic continuum finite element simulation. It was found that a full three-dimensional simulation was required to account for the measured transition from the overall plane stress case away from the notch to the essentially plane strain case observed near the notch tip. The measured and simulated stress contours were shown to be in good agreement except at the highest applied load, at which stress relaxation at the notch tip was observed in the experimental data. This stress relaxation is attributed to the initiation and propagation of a crack. Finally, it was demonstrated that the measured lattice rotations could be used as a qualitative measure of the shape and extent of the plastic deformation zone.

Measurements for stresses in machine components

CERN Document Server

Yakovlev, V F

1964-01-01

Measurements for Stresses in Machine Components focuses on the state of stress and strain of components and members, which determines the service life and strength of machines and structures. This book is divided into four chapters. Chapter I describes the physical basis of several methods of measuring strains, which includes strain gauges, photoelasticity, X-ray diffraction, brittle coatings, and dividing grids. The basic concepts of the electric strain gauge method for measuring stresses inside machine components are covered in Chapter II. Chapter III elaborates on the results of experim

In situ Micrometeorological Measurements during RxCADRE

Science.gov (United States)

Clements, C. B.; Hiers, J. K.; Strenfel, S. J.

2009-12-01

The Prescribed Fire Combustion and Atmospheric Dynamics Research Experiment (RxCADRE) was a collaborative research project designed to fully instrument prescribed fires in the Southeastern United States. Data were collected on pre-burn fuel loads, post burn consumption, ambient weather, in situ atmospheric dynamics, plume dynamics, radiant heat release (both from in-situ and remote sensors), in-situ fire behavior, and select fire effects. The sampling was conducted at Eglin Air Force Base, Florida, and the Joseph W. Jones Ecological Research Center in Newton, Georgia, from February 29 to March 6, 2008. Data were collected on 5 prescribed burns, totaling 4458 acres. The largest aerial ignition totaled 2,290 acres and the smallest ground ignition totaled 104 acres. Quantifying fire-atmospheric interactions is critical for understanding wildland fire dynamics and enhancing modeling of smoke plumes. During Rx-CADRE, atmospheric soundings using radiosondes were made at each burn prior to ignition. In situ micrometeorological measurements were made within each burn unit using five portable, 10-m towers equipped with sonic and prop anemometers, fine-wire thermocouples, and a carbon dioxide probes. The towers were arranged within the burn units to capture the wind and temperature fields as the fire front and plume passed the towers. Due to the interaction of fire lines following ignition, several of the fire fronts that passed the towers were backing fires and thus less intense. Preliminary results indicate that the average vertical velocities associated with the fire front passage were on the order of 3-5 m s-1 and average plume temperatures were on the order of 30-50 °C above ambient. During two of the experimental burns, radiosondes were released into the fire plumes to determine the vertical structure of the plume temperature, humidity, and winds. A radiosonde released into the plume during the burn conducted on 3 March 2008 indicated a definite plume boundary in the

Central Japan's Atera Active Fault's Wide-Fractured Zone: An Examination of the Structure and In-situ Crustal Stress

Science.gov (United States)

Ikeda, R.; Omura, K.; Matsuda, T.; Mizuochi, Y.; Uehara, D.; Chiba, A.; Kikuchi, A.; Yamamoto, T.

2001-12-01

In-situ downhole measurements and coring within and around an active fault zone are needed to better understand the structure and material properties of fault rocks as well as the physical state of active faults and intra-plate crust. Particularly, the relationship between the stress concentration state and the heterogeneous strength of an earthquake fault zone is important to estimate earthquake occurrence mechanisms which correspond to the prediction of an earthquake. It is necessary to compare some active faults in different conditions of the chrysalis stage and their relation to subsequent earthquake occurrence. To better understand such conditions, "Active Fault Zone Drilling Project" has been conducted in the central part of Japan by the National Research Institute for Earth Science and Disaster Prevention. The Nojima fault which appeared on the surface by the 1995 Great Kobe earthquake (M=7.2) and the Neodani fault created by the 1981 Nobi earthquake, the greatest inland earthquake M=8.0 in Japan, have been drilled through the fault fracture zones. During these past four years, a similar experiment and research at the Atera fault, of which some parts seem to have been dislocated by the 1586 Tensyo earthquake, has been undertaken. The features of the Atera fault are as follows: (1) total length is about 70 km, (2) general trend is NW45_Kwith a left-lateral strike slip, (3) slip rate is estimated as 3-5 m/1000 yrs. and the average recurrence time as 1700 yrs., (4) seismicity is very low at present, and (5) lithologies around the fault are basically granitic rocks and rhyolite. We have conducted integrated investigations by surface geophysical survey and drilling around the Atera fault. Six boreholes have been drilled from the depth of 400 m to 630 m. Four of these boreholes are located on a line crossing the fracture zone of the Atera fault. Resistivity and gravity structures inferred from surface geophysical surveys were compared with the physical properties

Modular enrichment measurement system for in-situ enrichment assay

International Nuclear Information System (INIS)

Stewart, J.P.

1976-01-01

A modular enrichment measurement system has been designed and is in operation within General Electric's Nuclear Fuel Fabrication Facility for the in-situ enrichment assay of uranium-bearing materials in process containers. This enrichment assay system, which is based on the ''enrichment meter'' concept, is an integral part of the site's enrichment control program and is used in the in-situ assay of the enrichment of uranium dioxide (UO 2 ) powder in process containers (five gallon pails). The assay system utilizes a commercially available modular counting system and a collimnator designed for compatability with process container transport lines and ease of operator access. The system has been upgraded to include a microprocessor-based controller to perform system operation functions and to provide data acquisition and processing functions. Standards have been fabricated and qualified for the enrichment assay of several types of uranium-bearing materials, including UO 2 powders. The assay system has performed in excess of 20,000 enrichment verification measurements annually and has significantly contributed to the facility's enrichment control program

Monitoring groundwater variation by satellite and implications for in-situ gravity measurements

International Nuclear Information System (INIS)

Fukuda, Yoichi; Yamamoto, Keiko; Hasegawa, Takashi; Nakaegawa, Toshiyuki; Nishijima, Jun; Taniguchi, Makoto

2009-01-01

In order to establish a new technique for monitoring groundwater variations in urban areas, the applicability of precise in-situ gravity measurements and extremely high precision satellite gravity data via GRACE (Gravity Recovery and Climate Experiment) was tested. Using the GRACE data, regional scale water mass variations in four major river basins of the Indochina Peninsula were estimated. The estimated variations were compared with Soil-Vegetation-Atmosphere Transfer Scheme (SVATS) models with a river flow model of 1) globally uniform river velocity, 2) river velocity tuned by each river basin, 3) globally uniform river velocity considering groundwater storage, and 4) river velocity tuned by each river basin considering groundwater storage. Model 3) attained the best fit to the GRACE data, and the model 4) yielded almost the same values. This implies that the groundwater plays an important role in estimating the variation of total terrestrial storage. It also indicates that tuning river velocity, which is based on the in-situ measurements, needs further investigations in combination with the GRACE data. The relationships among GRACE data, SVATS models, and in-situ measurements were also discussed briefly.

Estimation of the in situ degradation of the washout fraction of starch by using a modified in situ protocol and in vitro measurements

NARCIS (Netherlands)

Jonge, de L.H.; Laar, van H.; Dijkstra, J.

2015-01-01

The in situ degradation of the washout fraction of starch in six feed ingredients (i.e. barley, faba beans, maize, oats, peas and wheat) was studied by using a modified in situ protocol and in vitro measurements. In comparison with the washing machine method, the modified protocol comprises a milder

Two BASIC computer programs for the determination of in situ stresses using the CSIRO hollow inclusion stress cell and the USBM borehole deformation gage

Science.gov (United States)

Smith, W.K.

1982-01-01

The mathematical method of determining in-situ stresses by overcoring, using either the U.S. Bureau of Mines Borehole Deformation Gage or the Commonwealth Scientific and Industrial Research Organisation Hollow Inclusion Stress Cell, is summarized, and data reduction programs for each type of instrument, written in BASIC, are presented. The BASIC programs offer several advantages over previously available FORTRAN programs. They can be executed on a desk-top microcomputer at or near the field site, allowing the investigator to assess the quality of the data and make decisions on the need for additional testing while the crew is still in the field. Also, data input is much simpler than with currently available FORTRAN programs; either English or SI units can be used; and standard deviations of the principal stresses are computed as well as those of the geographic components.

Neutron stress measurement of W-fiber reinforced Cu composite

International Nuclear Information System (INIS)

Nishida, M.; Hanabusa, T.; Ikeuchi, Y.; Minakawa, N.

2003-01-01

Stress measurement methods using neutron and X-ray diffraction were examined by comparing the surface stresses with internal stresses in the continuous tungsten-fiber reinforced copper-matrix composite. Surface stresses were measured by X-ray stress measurement with the sin 2 ψ method. Furthermore, the sin 2 ψ method and the most common triaxal measurement method using Hooke's equation were employed for internal stress measurement by neutron diffraction. On the other hand, microstress distributions developed by the difference in the thermal expansion coefficients between these two phases were calculated by FEM. The weighted average strains and stresses were compared with the experimental results. The FEM results agreed with the experimental results qualitatively and confirmed the importance of the triaxial stress analysis in the neutron stress measurement. (Abstract Copyright [2003], Wiley Periodicals, Inc.)

In-situ ionic conductivity measurement of lithium ceramics under high energy heavy ion irradiation

International Nuclear Information System (INIS)

Nakazawa, Tetsuya; Noda, Kenji; Ishii, Yoshinobu; Ohno, Hideo; Watanabe, Hitoshi; Matsui, Hisayuki.

1992-01-01

To obtain fundamental information regarding the radiation damage in some lithium ceramics, e.g. Li 2 O, Li 4 SiO 4 etc., candidate of breeder materials exposed to severe irradiation environment, an in-situ experiment technique for the ionic conductivity measurement, which allows the specimen temperature control and the beam current monitoring, have been developed. This paper describes the features of an apparatus to measure in situ the ionic conductivity under the irradiation environment and presents some results of ionic conductivity measured for typical ceramic breeders using this apparatus. (J.P.N.)

Profile measurements and data from the 2011 Optics, Acoustics, and Stress In Situ (OASIS) project at the Martha's Vineyard Coastal Observatory

Science.gov (United States)

Sherwood, Christopher R.; Dickhudt, Patrick J.; Martini, Marinna A.; Montgomery, Ellyn T.; Boss, Emmanuel S.

2012-01-01

This report documents data collected by the U.S. Geological Survey (USGS) for the Coastal Model Applications and Field Measurements project under the auspices of the U.S. Navy Office of Naval Research Optics, Acoustics, and Stress In Situ (OASIS) Project. The objective of the measurements was to relate optical and acoustic properties of suspended particles to changes in particle size, concentration, and vertical distribution in the bottom boundary layer near the seafloor caused by wave- and current-induced stresses. This information on the physics of particle resuspension and aggregation and light penetration and water clarity will help improve models of sediment transport, benthic primary productivity, and underwater visibility. There is well-established technology for acoustic profiling, but optical profiles are more difficult to obtain because of the rapid attenuation of light in water. A specially modified tripod with a moving arm was designed to solve this problem by moving instruments vertically in the bottom boundary layer, between the bottom and about 2 meters above the seafloor. The profiling arm was designed, built, and tested during spring and summer 2011 by a team of USGS scientists, engineers, and technicians. To accommodate power requirements and the large data files recorded by some of the optical instruments, the tripod was connected via underwater cable to the Martha's Vineyard Coastal Observatory, operated by the Woods Hole Oceanographic Institution (WHOI). This afforded real-time Internet communication with the embedded computers aboard the tripod. Instruments were mounted on the profiling arm, and additional instruments were mounted elsewhere on the tripod and nearby on the seafloor. The tripod and a small mooring for a profiling current meter were deployed on September 17, 2011, at the Martha's Vineyard Coastal Observatory 12-meter-deep underwater node about 2 kilometers south of Martha's Vineyard, Massachusetts. Divers assisted in the

In-Situ Neutron Diffraction Under Tensile Loading of Powder-in-Tube Cu/Nb$_{3}$Sn Composite Wires Effect of Reaction Heat Treatment on Texture, Internal Stress State and Load Transfer

CERN Document Server

Scheuerlein, C; Thilly, L

2007-01-01

The strain induced degradation of Nb$_{3}$Sn superconductors can hamper the performance of high field magnets. We report elastic strain measurements in the different phases of entire non-heat treated and fully reacted Nb$_{3}$Sn composite strands as a function of uniaxial stress during in-situ deformation under neutron beam. After the reaction heat treatment the Cu matrix loses entirely its load carrying capability and the applied stress is transferred to the remaining Nb-Ta alloy and to the brittle (Nb-Ta)3Sn phase, which exhibits a preferential grain orientation parallel to the strand axis.

Seeing the light: Applications of in situ optical measurements for understanding DOM dynamics in river systems (Invited)

Science.gov (United States)

Pellerin, B. A.; Bergamaschi, B. A.; Downing, B. D.; Saraceno, J.; Fleck, J.; Shanley, J. B.; Aiken, G.; Boss, E.; Fujii, R.

2009-12-01

A critical challenge for understanding the sources, character and cycling of dissolved organic matter (DOM) is making measurements at the time scales in which changes occur in aquatic systems. Traditional approaches for data collection (daily to monthly discrete sampling) are often limited by analytical and field costs, site access and logistical challenges, particularly for long-term sampling at a large number of sites. The ability to make optical measurements of DOM in situ has been known for more than 50 years, but much of the work on in situ DOM absorbance and fluorescence using commercially-available instruments has taken place in the last few years. Here we present several recent examples that highlight the application of in situ measurements for understanding DOM dynamics in riverine systems at intervals of minutes to hours. Examples illustrate the utility of in situ optical sensors for studies of DOM over short-duration events of days to weeks (diurnal cycles, tidal cycles, storm events and snowmelt periods) as well as longer-term continuous monitoring for months to years. We also highlight the application of in situ optical DOM measurements as proxies for constituents that are significantly more difficult and expensive to measure at high frequencies (e.g. methylmercury, trihalomethanes). Relatively simple DOM absorbance and fluorescence measurements made in situ could be incorporated into short and long-term ecological research and monitoring programs, resulting in advanced understanding of organic matter sources, character and cycling in riverine systems.

In-situ gamma spectroscopic measurement of natural waters in Bulgaria

International Nuclear Information System (INIS)

Manushev, B.; Mandzhukov, I.; Tsankov, L.; Boshkova, T.; Gurev, V.; Mandzhukova, B.; Kozhukharov, I.; Grozev, G.

1983-01-01

In-situ gamma spectrometric measurements are carried out to record differences higher than the errors of measurement in the gamma-field spectra in various basins in Bulgaria - two high mountain lakes, dam and the Black sea. A standard scintillation gamma spectrometer, consisting of a scintillation detector ND-424 type, a channel analyzer NP-424 and a 128 channel Al-128 type analyzer, has been used. The sensitivity of the procedure used is sufficient to detect the transfer of nuclides by dissolution from rocks, forming the bottom and the water-collecting region of the water basin. The advancement of the experimental techniques defines the future use of the procedure. In-situ gamma spectrometric determination may be used in cases of continuous and automated control of the radiation purity of the cooling water in atomic power plants or the water basins located close to such plants and of radioactive contamination of the sea and ocean water

Measuring the stress field around an evolving crack in tensile deformed Mg AZ31 using three-dimensional X-ray diffraction

DEFF Research Database (Denmark)

Oddershede, Jette; Camin, Bettina; Schmidt, Søren

2012-01-01

The stress field around a notch in a coarse grained Mg AZ31 sample has been measured under tensile load using the individual grains as probes in an in situ high energy synchrotron diffraction experiment. The experimental set-up, a variant of three-dimensional X-ray diffraction microscopy, allows...... the position, orientation and full stress tensor of each illuminated grain to be determined and, hence, enables the study of evolving stress fields in coarse grained materials with a spatial resolution equal to the grain size. Grain resolved information like this is vital for understanding what happens when...... the traditional continuum mechanics approach breaks down and fracture is governed by local heterogeneities (e.g. phase or stress differences) between grains. As a first approximation the results obtained were averaged through the thickness of the sample and compared with an elastic–plastic continuum finite...

Stress measurement by x-ray diffractometry

Energy Technology Data Exchange (ETDEWEB)

Mitchell, C M

1985-10-22

This invention relates to x-ray diffractometry and more particularly to apparatus and methods for the measurement of residual stress in polycrystalline, e.g. metallic, specimens. The procedure is based on measurement of the lattice strain of crystals by x-ray diffraction, in which change in the interplanar spacing of a set of crystal lattice planes due to strain causes a change in the diffraction angle of the scattered x-ray beam, from which latter change the magnitude of the strain can be determined. In a polycrystalline specimen, from well know relations for elastic behaviour in isotropic materials, the stress on a plane normal to a given direction in the surface has a component in the given direction which can be calculated from measurement of lattice strain in two directions in a plane containing the given direction and the normal to the specimen surface. In general three such stress components in three directions in the surface are required to determine the principal stresses and thus express the state of stress in the surface. (author). 2 tabs., 9 figs.

Analysis of In Situ Thermal Ion Measurements from the MICA Sounding Rocket

Science.gov (United States)

Fernandes, P. A.; Lynch, K. A.; Zettergren, M. D.; Hampton, D. L.; Fisher, L. E.; Powell, S. P.

2014-12-01

The MICA sounding rocket launched on 19 Feb. 2012 into several discrete, localized arcs in the wake of a westward traveling surge. In situ and ground-based observations provide a measured response of the ionosphere to preflight and localized auroral drivers. Initial analysis of the in situ thermal ion data indicate possible measurement of an ion conic at low altitude (< 325 km). In the low-energy regime, the response of the instrument varies from the ideal because the measured thermal ion population is sensitive to the presence of the instrument. The plasma is accelerated in the frame of the instrument due to flows, ram, and acceleration through the sheath which forms around the spacecraft. The energies associated with these processes are large compared to the thermal energy. Correct interpretation of thermal plasma measurements requires accounting for all of these plasma processes and the non-ideal response of the instrument in the low-energy regime. This is an experimental and modeling project which involves thorough analysis of ionospheric thermal ion data from the MICA campaign. Analysis includes modeling and measuring the instrument response in the low-energy regime as well as accounting for the complex sheath formed around the instrument. This results in a forward model in which plasma parameters of the thermal plasma are propagated through the sheath and instrument models, resulting in an output which matches the in situ measurement. In the case of MICA, we are working toward answering the question of the initiating source processes that result, at higher altitudes, in well-developed conics and outflow on auroral field lines.

Hole Drilling Technique – on site stress measurement

OpenAIRE

Schueremans, Luc

2009-01-01

2. Hole Drilling Technique for onsite stress measurement has been used to validate the stress level at 2 pillars of the Sint-Jacobschurch (Leuven, B). The technique allows estimating the stress in a stone from measuring deformation when a small hole is made. It is a low intrusive technique. The application of it is limited to local stress measurements and is a complement to stress estimate from calculations of from the use of –for example- flat jacks. In addition to the flat-jack technique...

Evaluation of stresses generated in steel finger joint of bridge by X-ray stress measurement

International Nuclear Information System (INIS)

Kohri, Ami; Kawano, Yutaka; Nishido, Takayuki

2017-01-01

In a steel bridge, the evaluation of the stress generated in the finger joint without a gap to absorb temperature change can be an index when evaluating the remaining life. This study chose as the object the finger joint of a diagonal bridge, where the generated stress state is considered to be more complicated, prepared a finger joint test specimen that simulated an actual part, and performed a load test. For judgment, FEM analysis, non-destructive X-ray stress measurement, and measurement of the generated stress using strain gauge were applied. Compared with the FEM analysis results, the difference in the stress value was generated due to the difference in the contact state, but the trends of the stress distribution were equivalent. In addition, the same measurement value as the strain gauge was obtained, and the validity of the X-ray stress measurement method was confirmed. As a result, it was found that the stress measurement method by X-ray is effective for measuring the generated stress including the residual stress of the finger joint without gap at a bridge. (A.O.)

Synchrotron X-ray diffraction measurements of internal stresses during loading of steel-based metal matrix composites reinforced with TiB2 particles

International Nuclear Information System (INIS)

Bacon, D.H.; Edwards, L.; Moffatt, J.E.; Fitzpatrick, M.E.

2011-01-01

Highlights: → Synchrotron X-ray diffraction was used to measure internal stresses in Fe-TiB 2 MMCs. → Samples of the MMCs were loaded to failure in situ in the X-ray beam. → The results show good elastic load transfer from the matrix to the reinforcement. → There is good agreement with the predicted elastic stresses from Eshelby modeling. → During plastic deformation there is increasing load transfer to the reinforcement. - Abstract: High-energy synchrotron X-ray diffraction was used to measure the internal strain evolution in the matrix and reinforcement of steel-based metal matrix composites reinforced with particulate titanium diboride (TiB 2 ). Two systems were studied: a 316L matrix with 25% TiB 2 by volume and a W1.4418 matrix with 10% reinforcement. In situ loading experiments were performed, where the materials were loaded uniaxially in the X-ray beam. The results show the strain partitioning between the phases in the elastic regime, and the evolution of the strain partitioning once plasticity occurs. The results are compared with results from Eshelby modelling, and very good agreement is seen between the measured and modelled response for elastic loading of the material. Heat treatment of the 316-based material did not affect the elastic internal strain response.

A Shortened Stress Measure in Military Nursing Personnel

Science.gov (United States)

2017-10-17

REPORT TYPE 3. DATES COVERED (From- To) 10/17/2017 Abstract 4. TITLE AND SUBTITLE Sa. CONTRACT NUMBER A Shortened Stress Measure in Military...Psychology 14. ABSTRACT A Shortened Stress Measure with Military Nursing Personnel Abstract Stress is a psychological construct with important...consequences for human health. A substantial number of stress measures are available that vary in length and dimensionality. The purpose of this study was to

Enhanced functional connectivity properties of human brains during in-situ nature experience.

Science.gov (United States)

Chen, Zheng; He, Yujia; Yu, Yuguo

2016-01-01

In this study, we investigated the impacts of in-situ nature and urban exposure on human brain activities and their dynamics. We randomly assigned 32 healthy right-handed college students (mean age = 20.6 years, SD = 1.6; 16 males) to a 20 min in-situ sitting exposure in either a nature (n = 16) or urban environment (n = 16) and measured their Electroencephalography (EEG) signals. Analyses revealed that a brief in-situ restorative nature experience may induce more efficient and stronger brain connectivity with enhanced small-world properties compared with a stressful urban experience. The enhanced small-world properties were found to be correlated with "coherent" experience measured by Perceived Restorativeness Scale (PRS). Exposure to nature also induces stronger long-term correlated activity across different brain regions with a right lateralization. These findings may advance our understanding of the functional activities during in-situ environmental exposures and imply that a nature or nature-like environment may potentially benefit cognitive processes and mental well-being.

Recent advances in residual stress measurement

International Nuclear Information System (INIS)

Withers, P.J.; Turski, M.; Edwards, L.; Bouchard, P.J.; Buttle, D.J.

2008-01-01

Until recently residual stresses have been included in structural integrity assessments of nuclear pressure vessels and piping in a very primitive manner due to the lack of reliable residual stress measurement or prediction tools. This situation is changing the capabilities of newly emerging destructive (i.e. the contour method) and non-destructive (i.e. magnetic and high-energy synchrotron X-ray strain mapping) residual stress measurement techniques for evaluating ferritic and austenitic pressure vessel components are contrasted against more well-established methods. These new approaches offer the potential for obtaining area maps of residual stress or strain in welded plants, mock-up components or generic test-pieces. The mapped field may be used directly in structural integrity calculations, or indirectly to validate finite element process/structural models on which safety cases for pressurised nuclear systems are founded. These measurement methods are complementary in terms of application to actual plant, cost effectiveness and measurements in thick sections. In each case an exemplar case study is used to illustrate the method and to highlight its particular capabilities

Neutron residual stress measurements in linepipe

International Nuclear Information System (INIS)

Law, Michael; Gnaepel-Herold, Thomas; Luzin, Vladimir; Bowie, Graham

2006-01-01

Residual stresses in gas pipelines are generated by manufacturing and construction processes and may affect the subsequent pipe integrity. In the present work, the residual stresses in eight samples of linepipe were measured by neutron diffraction. Residual stresses changed with some coating processes. This has special implications in understanding and mitigating stress corrosion cracking, a major safety and economic problem in some gas pipelines

Measurement of residual stresses using fracture mechanics weight functions

International Nuclear Information System (INIS)

Fan, Y.

2000-01-01

A residual stress measurement method has been developed to quantify through-the-thickness residual stresses. Accurate measurement of residual stresses is crucial for many engineering structures. Fabrication processes such as welding and machining generate residual stresses that are difficult to predict. Residual stresses affect the integrity of structures through promoting failures due to brittle fracture, fatigue, stress corrosion cracking, and wear. In this work, the weight function theory of fracture mechanics is used to measure residual stresses. The weight function theory is an important development in computational fracture mechanics. Stress intensity factors for arbitrary stress distribution on the crack faces can be accurately and efficiently computed for predicting crack growth. This paper demonstrates that the weight functions are equally useful in measuring residual stresses. In this method, an artificial crack is created by a thin cut in a structure containing residual stresses. The cut relieves the residual stresses normal to the crack-face and allows the relieved residual stresses to deform the structure. Strain gages placed adjacent to the cut measure the relieved strains corresponding to incrementally increasing depths of the cut. The weight functions of the cracked body relate the measured strains to the residual stresses normal to the cut within the structure. The procedure details, such as numerical integration of the singular functions in applying the weight function method, will be discussed

Measurement of residual stresses using fracture mechanics weight functions

International Nuclear Information System (INIS)

Fan, Y.

2001-01-01

A residual stress measurement method has been developed to quantify through-the-thickness residual stresses. Accurate measurement of residual stresses is crucial for many engineering structures. Fabrication processes such as welding and machining generate residual stresses that are difficult to predict. Residual stresses affect the integrity of structures through promoting failures due to brittle fracture, fatigue, stress corrosion cracking, and wear. In this work, the weight function theory of fracture mechanics is used to measure residual stresses. The weight function theory is an important development in computational fracture mechanics. Stress intensity factors for arbitrary stress distribution on the crack faces can be accurately and efficiently computed for predicting crack growth. This paper demonstrates that the weight functions are equally useful in measuring residual stresses. In this method, an artificial crack is created by a thin cut in a structure containing residual stresses. The cut relieves the residual stresses normal to the crack-face and allows the relieved residual stresses to deform the structure. Strain gages placed adjacent to the cut measure the relieved strains corresponding to incrementally increasing depths of the cut. The weight functions of the cracked body relate the measured strains to the residual stresses normal to the cut within the structure. The procedure details, such as numerical integration of the singular functions in applying the weight function method, will be discussed. (author)

Combining Space-Based and In-Situ Measurements to Track Flooding in Thailand

Science.gov (United States)

Chien, Steve; Doubleday, Joshua; Mclaren, David; Tran, Daniel; Tanpipat, Veerachai; Chitradon, Royal; Boonya-aaroonnet, Surajate; Thanapakpawin, Porranee; Khunboa, Chatchai; Leelapatra, Watis;

Evaluation of Rock Stress Estimation by the Kaiser effect

International Nuclear Information System (INIS)

Lehtonen, A.

2005-11-01

The knowledge of in situ stress is the key input parameter in many rock mechanics analyses. Information on stress allows the definition of boundary conditions for various modelling and engineering tasks. Presently, the estimation of stresses in bedrock is one of the most difficult, time-consuming and high-priced rock mechanical investigations. In addition, the methods used today have not evolved significantly in many years. This brings out a demand for novel, more economical and practical methods for stress estimation. In this study, one such method, Kaiser effect based on acoustic emission of core samples, has been evaluated. It can be described as a 'memory' in rock that is indicated by a change in acoustic emission emitted during uniaxial loading test. The most tempting feature of this method is the ability to estimate the in situ stress state from core specimens in laboratory conditions. This yields considerable cost savings compared to laborious borehole measurements. Kaiser effect has been studied in order to determine in situ stresses for decades without any major success. However, recent studies in Australia and China have been promising and made the estimation of stress tensor possible from differently oriented core samples. The aim of this work has been to develop a similar estimation method in Finland (including both equipment and data reduction), and to test it on samples obtained from Olkiluoto, Eurajoki. The developed measuring system proved to work well. The quality of obtained data varied, but they were still interpretable. The results obtained from these tests were compared with results of previous overcoring measurements, and they showed quite good correlation. Thus, the results were promising, but the method still needs further development and more testing before the final decision on its feasibility can be made. (orig.)

In situ measurement of some gamma-emitting radionuclides in plant communities of the South Carolina coastal plain

International Nuclear Information System (INIS)

Ragsdale, H.L.; Tanner, B.K.; Coleman, R.N.; Palms, J.M.; Wood, R.E.

1978-01-01

In situ and laboratory gamma-ray spectroscopy measurements were taken in nine scrub oak forests and nine old fields to determine the applicability of in situ analysis in the coastal plain. Data collected at each of the 18 sites included a 2-hr count, soil density and moisture estimates, and vegetation measurements. Samples returned to the laboratory for radiometric analysis included litter and herbaceous vegetation and soil cores. Analysis of the gamma-emitter detection frequencies, concentrations, and burdens showed good to excellent agreement between laboratory and in situ methods. Generally, forests were determined to be superior in situ sampling systems. Laboratory analysis of collected samples may be a superior technique for gamma emitters with low energies, low concentrations, or nonuniform distributions in the soil. Three potential uses of in situ Ge(Li) spectrometers were identified and discussed in terms of their limits and of the replicate ecosystems appropriate for in situ analyses. Although the variety and the biogeochemical cycling regimes of southeastern coastal plain ecosystems complicate in situ analyses, it was concluded that comparable and probably accurate results can be achieved using in situ technology

Rock stress investigations

International Nuclear Information System (INIS)

Pahl, A.; Heusermann, St.; Braeuer, V.; Gloeggler, W.

1989-04-01

On the research project 'Rock Stress Mesurements' the BGR has developed and tested several methods for use in boreholes at a depth of 200 m. Indirect stress measurements using overcoring methods with BGR-probes and CSIR-triaxial cells as well as direct stress measurements using the hydraulic-fracturing method were made. To determine in-situ rock deformation behavior borehole deformation tests, using a BGR-dilatometer, were performed. Two types of the BGR-probe were applied: a four-component-probe to determine horizontal stresses and a five-component-probe to determine a quasi three-dimensional stress field. The first time a computer for data processing was installed in the borehole together with the BGR-probe. Laboratory tests on low cylinders were made to study the stress-deformation behavior. To validate and to interprete the measurement results some test methods were modelled using the finite-element method. The dilatometer-tests yielded high values of Young's modulus, whereas laboratory tests showed lower values with a distinct deformation anisotropy. Stress measurements with the BGR-probe yielded horizontal stresses being higher than the theoretical overburden pressure. These results are comparable to the results of the hydraulic fracturing tests, whereas stresses obtained with CSIR-triaxial cells are lower. The detailed geological mapping of the borehole indicated relationships between stress and geology. With regard to borehole depth different zones of rock structure joint frequency, joint orientation, and orientation of microfissures as well as stress magnitude, stress direction, and degree of deformation anisotropy could be distinguished. (author) 4 tabs., 76 figs., 31 refs

Stress strain tensors with their application to x-ray stress measurement

International Nuclear Information System (INIS)

Kurita, Masanori

2015-01-01

This paper describes in detail the method of obtaining the formulas of stress-strain tensor that express the directional dependence of stress-strain, that is, how these values change in response to coordinate transformation, and clarifies the preconditions for supporting both formulas. The two conversion formulas are both the second order of tensor, and the formula of strain tensor not only does not use the relational expression of stress and strain at all, but also is obtained completely independently of the formula of stress tensor. Except for the condition that the strain is very small (elastic deformation) in the conversion formula of strain, both formulas unconditionally come into effect. In other words, both formulas hold true even in the isotropic elastic body or anisotropic elastic body. It was shown that the conversion formula of strain can be derived from the conversion formula of stress using the formula of Hooke for isotropic elastic body. From these three-dimensional expressions, the two-dimensional stress-strain coordinate conversion formula that is used for Mohr's stress-strain circle was derived. It was shown that these formulas hold true for three-dimensional stress condition with stress-strain components in the three-axial direction that are not plane stress nor plane strain condition. In addition, as an application case of this theory, two-dimensional and three-dimensional X-ray stress measurements that are effective for residual stress measurement were shown. (A.O.)

Mechanisms of stress generation and relaxation during pulsed laser deposition of epitaxial Fe-Pd magnetic shape memory alloy films on MgO

International Nuclear Information System (INIS)

Edler, Tobias; Mayr, S G; Buschbeck, Joerg; Mickel, Christine; Faehler, Sebastian

2008-01-01

Mechanical stress generation during epitaxial growth of Fe-Pd thin films on MgO from pulsed laser deposition is a key parameter for the suitability in shape memory applications. By employing in situ substrate curvature measurements, we determine the stress states as a function of film thickness and composition. Depending on composition, different stress states are observed during initial film growth, which can be attributed to different misfits. Compressive stress generation by atomic peening is observed in the later stages of growth. Comparison with ex situ x-ray based strain measurements allows integral and local stress to be distinguished and yields heterogeneities of the stress state between coherent and incoherent regions. In combination with cross-sectional TEM measurements the relevant stress relaxation mechanism is identified to be stress-induced martensite formation with (111) twinning

In situ time-of-flight neutron imaging of NiO-YSZ anode support reduction under influence of stress

DEFF Research Database (Denmark)

Makowska, Malgorzata Grazyna; Strobl, Markus; Lauridsen, Erik M.

2016-01-01

This article reports on in situ macroscopic scale imaging of NiO-YSZ (YSZ is yttria-stabilized zirconia) reduction under applied stress - a phase transition taking place in solid oxide electrochemical cells in a reducing atmosphere of a hydrogen/nitrogen mixture and at operation temperatures of u...... of applying energy-resolved neutron imaging with both approaches to the NiO-YSZ reduction investigation indicate enhancement of the reduction rate due to applied stress, which is consistent with the results of the authors’ previous research....

In-situ measurements of the secondary electron yield in an accelerator environment: Instrumentation and methods

International Nuclear Information System (INIS)

Hartung, W.H.; Asner, D.M.; Conway, J.V.; Dennett, C.A.; Greenwald, S.; Kim, J.-S.; Li, Y.; Moore, T.P.; Omanovic, V.; Palmer, M.A.; Strohman, C.R.

2015-01-01

The performance of a particle accelerator can be limited by the build-up of an electron cloud (EC) in the vacuum chamber. Secondary electron emission from the chamber walls can contribute to EC growth. An apparatus for in-situ measurements of the secondary electron yield (SEY) in the Cornell Electron Storage Ring (CESR) was developed in connection with EC studies for the CESR Test Accelerator program. The CESR in-situ system, in operation since 2010, allows for SEY measurements as a function of incident electron energy and angle on samples that are exposed to the accelerator environment, typically 5.3 GeV counter-rotating beams of electrons and positrons. The system was designed for periodic measurements to observe beam conditioning of the SEY with discrimination between exposure to direct photons from synchrotron radiation versus scattered photons and cloud electrons. The samples can be exchanged without venting the CESR vacuum chamber. Measurements have been done on metal surfaces and EC-mitigation coatings. The in-situ SEY apparatus and improvements to the measurement tools and techniques are described

In-situ measurements of the secondary electron yield in an accelerator environment: Instrumentation and methods

Energy Technology Data Exchange (ETDEWEB)

Hartung, W.H., E-mail: wh29@cornell.edu; Asner, D.M.; Conway, J.V.; Dennett, C.A.; Greenwald, S.; Kim, J.-S.; Li, Y.; Moore, T.P.; Omanovic, V.; Palmer, M.A.; Strohman, C.R.

2015-05-21

The performance of a particle accelerator can be limited by the build-up of an electron cloud (EC) in the vacuum chamber. Secondary electron emission from the chamber walls can contribute to EC growth. An apparatus for in-situ measurements of the secondary electron yield (SEY) in the Cornell Electron Storage Ring (CESR) was developed in connection with EC studies for the CESR Test Accelerator program. The CESR in-situ system, in operation since 2010, allows for SEY measurements as a function of incident electron energy and angle on samples that are exposed to the accelerator environment, typically 5.3 GeV counter-rotating beams of electrons and positrons. The system was designed for periodic measurements to observe beam conditioning of the SEY with discrimination between exposure to direct photons from synchrotron radiation versus scattered photons and cloud electrons. The samples can be exchanged without venting the CESR vacuum chamber. Measurements have been done on metal surfaces and EC-mitigation coatings. The in-situ SEY apparatus and improvements to the measurement tools and techniques are described.

STRESSES AND DEFORMABILITY OF ROCK MASS UPON OPEN PIT EXPLOITATION OF DIMENSION STONE

Directory of Open Access Journals (Sweden)

Siniša Dunda

2003-12-01

Full Text Available The appearance of increased stresses and deformability of rock mass in the quarry of Zečevo (exploitation field of Selca – island of Brač has caused a considerable decrease of usability of mineral raw materials, which put into question the survival of the pit. Therefore the research and measurements of the state of stresses and deformability of rock mass within the pit were carried out. Besides detailed laboratory testings (testings on small samples performed were trial in-situ testings on large samples including the corresponding numerical analyses. The exploitation of dimension stone by sowing regularly shaped rectangular blocks has been proved to be appropriate for in-situ testing of bending strength. The paper presents the results of carried out laboratory testings, in-situ testings of bending strength including measuring of deformations after sowing cuts and numerical analyses by which the possible range of horizontal stresses was determined. Since for the case of massive rocks, for which the continuum concept is applied, there are no specifically defined methods of corrections, presented is a possible relation for correction of input size values based on the carried out laboratory and in-situ testings.

Results and conclusions of stress measurements at Stripa

International Nuclear Information System (INIS)

Doe, T.W.; Hustrulid, W.A.; Leijon, B.; Ingevald, K.; Strindell, L.; Carlsson, Hans

1983-01-01

This paper describes the results of stress measurements at Stripa, compares the results obtained by different techniques, and recommends a stress measurement program for a hard rock repository site. The state of stress at the Stripa Mine has been measured both in a 381m deep hole drilled from the surface and in holes drilled from the drifts underground. The results of overcoring and hydraulic fracturing agree well, particularly for the magnitude and orientation of the greatest stress. A recommended program for stress measurement at a repository site would include hydraulic fracturing and deep-hole overcoring in a deep hole drilled from surface, and ovecoring and hydraulic fracturing from holes drilled from underground openings when access is available. Propagation of the hydraulic fractures should be monitored acoustically to determine their location and orientation

Utilizing In Situ Directional Hyperspectral Measurements to Validate Bio-Indicator Simulations for a Corn Crop Canopy

Science.gov (United States)

Cheng, Yen-Ben; Middleton, Elizabeth M.; Huemmrich, Karl F.; Zhang, Qingyuan; Campbell, Petya K. E.; Corp, Lawrence A.; Russ, Andrew L.; Kustas, William P.

2010-01-01

Two radiative transfer canopy models, SAIL and the two-layer Markov-Chain Canopy Reflectance Model (MCRM), were coupled with in situ leaf optical properties to simulate canopy-level spectral band ratio vegetation indices with the focus on the photochemical reflectance index in a cornfield. In situ hyperspectral measurements were made at both leaf and canopy levels. Leaf optical properties were obtained from both sunlit and shaded leaves. Canopy reflectance was acquired for eight different relative azimuth angles (psi) at three different view zenith angles (Theta (sub v)), and later used to validate model outputs. Field observations of photochemical reflectance index (PRI) for sunlit leaves exhibited lower values than shaded leaves, indicating higher light stress. Canopy PRI expressed obvious sensitivity to viewing geometry, as a function of both Theta (sub v) and psi . Overall, simulations from MCRM exhibited better agreements with in situ values than SAIL. When using only sunlit leaves as input, the MCRM-simulated PRI values showed satisfactory correlation and RMSE, as compared to in situ values. However, the performance of the MCRM model was significantly improved after defining a lower canopy layer comprised of shaded leaves beneath the upper sunlit leaf layer. Four other widely used band ratio vegetation indices were also studied and compared with the PRI results. MCRM simulations were able to generate satisfactory simulations for these other four indices when using only sunlit leaves as input; but unlike PRI, adding shaded leaves did not improve the performance of MCRM. These results support the hypothesis that the PRI is sensitive to physiological dynamics while the others detect static factors related to canopy structure. Sensitivity analysis was performed on MCRM in order to better understand the effects of structure related parameters on the PRI simulations. Leaf area index (LAI) showed the most significant impact on MCRM-simulated PRI among the parameters

Stress evolution in elastic-plastic electrodes during electrochemical processes: A numerical method and its applications

Science.gov (United States)

Wen, Jici; Wei, Yujie; Cheng, Yang-Tse

2018-07-01

Monitoring in real time the stress state in high capacity electrodes during charge-discharge processes is pivotal to the performance assessment and structural optimization of advanced batteries. The wafer curvature measurement technique broadly employed in thin-film industry, together with stress analysis using the Stoney equation, has been successfully adopted to measure in situ the stress in thin film electrodes. How large plastic deformation or interfacial delamination during electrochemical cycles in such electrodes affects the applicability of Stoney equation remains unclear. Here we develop a robust electrochemical-mechanical coupled numerical procedure to investigate the influence of large plastic deformation and interfacial failure on the measured stress in thin film electrodes. We identify how the constitutive behavior of electrode materials and film-substrate interfacial properties affect the measured stress-capacity curves of electrodes, and hence establish the relationship of electrode material parameters with the characteristics of stress-capacity curves. Using Li-ions batteries as examples, we show that plastic deformation and interfacial delamination account for the asymmetric stress-capacity loops seen in in situ stress measurements. The methods used here, along with the finite-element code in the supplementary material, may be used to model the electrode behavior as a function of the state of charge.

3D geomechanical modeling and numerical simulation of in-situ stress fields in shale reservoirs: A case study of the lower Cambrian Niutitang formation in the Cen'gong block, South China

Science.gov (United States)

Liu, Jingshou; Ding, Wenlong; Yang, Haimeng; Wang, Ruyue; Yin, Shuai; Li, Ang; Fu, Fuquan

2017-08-01

An analysis of the in-situ state of stress in a shale reservoir was performed based on comprehensive information about the subsurface properties from wellbores established during the development of an oil and gas field. Industrial-level shale gas production has occurred in the Niutitang formation of the lower Cambrian Cen'gong block, South China. In this study, data obtained from hydraulic fracturing, drilling-induced fractures, borehole breakout, global positioning system (GPS), and well deviation statistics have been used to determine the orientation of the maximum horizontal principal stress. Additionally, hydraulic fracturing and multi-pole array acoustic logging (XMAC) were used to determine the vertical variations in the in-situ stress magnitude. Based on logging interpretation and mechanical experiments, the spatial distributions of mechanical parameters were obtained by seismic inversion, and a 3D heterogeneous geomechanical model was established using a finite element stress analysis approach to simulate the in-situ stress fields. The effects of depth, faults, rock mechanics, and layer variations on the principal stresses, horizontal stress difference (Δσ), horizontal stress difference coefficient (Kh), and stress type coefficient (Sp) were determined. The results show that the direction of the maximum principal stress is ESE 120°. Additionally, the development zones of natural fractures appear to correlate with regions with high principal stress differences. At depths shallower than 375 m, the stress type is mainly a thrust faulting stress regime. At depths ranging from 375 to 950 m, the stress type is mainly a strike-slip faulting stress regime. When the depth is > 950 m, the stress type is mainly a normal faulting stress regime. Depth, fault orientation, and rock mechanics all affect the type of stress. The knowledge regarding the Cen'gong block is reliable and can improve borehole stability, casing set point determination, well deployment

In situ measurements and transmission electron microscopy of carbon nanotube field-effect transistors

International Nuclear Information System (INIS)

Kim, Taekyung; Kim, Seongwon; Olson, Eric; Zuo Jianmin

2008-01-01

We present the design and operation of a transmission electron microscopy (TEM)-compatible carbon nanotube (CNT) field-effect transistor (FET). The device is configured with microfabricated slits, which allows direct observation of CNTs in a FET using TEM and measurement of electrical transport while inside the TEM. As demonstrations of the device architecture, two examples are presented. The first example is an in situ electrical transport measurement of a bundle of carbon nanotubes. The second example is a study of electron beam radiation effect on CNT bundles using a 200 keV electron beam. In situ electrical transport measurement during the beam irradiation shows a signature of wall- or tube-breakdown. Stepwise current drops were observed when a high intensity electron beam was used to cut individual CNT bundles in a device with multiple bundles

In-situ Measurements and Analysis of Naturally Occurring Radioactive Materials

International Nuclear Information System (INIS)

Mueller, W.F.; Ilie, G.; Russ, W.R.; Lange, H.J.; Rotty, M.

2013-06-01

The measurement and quantification of naturally occurring radioactive materials (NORM) is an important element of workplace radioprotection in key industries such as oil and gas production, heavy metals mining and refining, coal burning waste, and water treatment. Monitoring of NORM content in home building materials is another challenge for human safety in the prevention of chronic dose uptake. Materials are classified NORM in case they contain significant amounts of the decay chains of U-238 (Ra-226 as a long lived daughter), U-235 or Th- 232 or the primordial nuclide K-40. Due to the decay of the radionuclides, gamma rays with a signature in the energy range from 45 keV up to 2615 keV are emitted. The most accurate method to measure NORM in a sample is to use a high resolution spectrometric instrument such as a germanium detector in a well-shielded laboratory environment. The shield is used to prevent background with the same signature from the building material of the laboratory. There are occasions in which one is required to assay samples in the field. These in situ field applications may require performing measurements with reduced (or no) background shielding conditions, or involve the use of medium resolution spectrometric instruments such as LaBr 3 or NaI detectors. In-situ analyses such as these have increased complexity. The reduced shielding enforces the subtraction of NORM events produced from the environment but the sample material and container can also shield the detector against this background thus biasing the measured results if not appropriately accounted. The use of medium resolution detectors has additional complications that the multiplicity of gamma-rays from NORM materials is such that most of the gamma-rays are interfering and thus require a very careful quantitative analysis. In this presentation, we will discuss the details of the NORM source term both in the environment and what could potentially be in the sample. We will also discuss

In situ and postradiation analysis of mechanical stress in Al2O3:Cr induced by swift heavy-ion irradiation

International Nuclear Information System (INIS)

Skuratov, V.A.; Bujnarowski, G.; Kovalev, Yu.S.; O'Connell, J.; Havanscak, K.

2010-01-01

Optical spectroscopy and TEM techniques have been applied to study the radiation damage and correlated mechanical stresses in Al 2 O 3 and Al 2 O 3 :Cr single crystals induced by (1-3) MeV/amu Kr, Xe and Bi ion irradiation. Mechanical stresses were evaluated in situ using a piezospectroscopic effect through the shift of the respective lines in ionoluminescence spectra. It was found that dose dependence of the stress level for Xe and Bi ions, when ionization energy loss exceeds the threshold of damage formation via electronic excitations, exhibits several alternate stages showing the build-up and relaxation of stresses. The beginning of relaxation stages is observed at fluences associated with beginning of individual ion track regions overlapping. The residual stress profiles through the ion irradiated layers were deduced from depth-resolved photostimulated spectra using laser confocal scanning microscopy set-up. It was determined that stresses are compressive in basal plane and tensile in perpendicular direction in all samples irradiated with high energy ions.

Methyl mercury dynamics in a tidal wetland quantified using in situ optical measurements

Science.gov (United States)

Bergamaschi, B.A.; Fleck, J.A.; Downing, B.D.; Boss, E.; Pellerin, B.; Ganju, N.K.; Schoellhamer, D.H.; Byington, A.A.; Heim, W.A.; Stephenson, M.; Fujii, R.

2011-01-01

We assessed monomethylmercury (MeHg) dynamics in a tidal wetland over three seasons using a novel method that employs a combination of in situ optical measurements as concentration proxies. MeHg concentrations measured over a single spring tide were extended to a concentration time series using in situ optical measurements. Tidal fluxes were calculated using modeled concentrations and bi-directional velocities obtained acoustically. The magnitude of the flux was the result of complex interactions of tides, geomorphic features, particle sorption, and random episodic events such as wind storms and precipitation. Correlation of dissolved organic matter quality measurements with timing of MeHg release suggests that MeHg is produced in areas of fluctuating redox and not limited by buildup of sulfide. The wetland was a net source of MeHg to the estuary in all seasons, with particulate flux being much higher than dissolved flux, even though dissolved concentrations were commonly higher. Estimated total MeHg yields out of the wetland were approximately 2.5 μg m−2 yr−1—4–40 times previously published yields—representing a potential loading to the estuary of 80 g yr−1, equivalent to 3% of the river loading. Thus, export from tidal wetlands should be included in mass balance estimates for MeHg loading to estuaries. Also, adequate estimation of loads and the interactions between physical and biogeochemical processes in tidal wetlands might not be possible without long-term, high-frequency in situ measurements.

X-ray measurement of residual stress on bolt threads

International Nuclear Information System (INIS)

Hagiwara, Masaya; Nakahara, Kanefumi; Yoshimoto, Isamu.

1989-01-01

This study deals with X-ray measurement of residual stress at the local area around the thread root of a bolt. Residual stress in the 0.5 mm x 5 mm area was measured using a method of stepped scanning and parabolic approximation. The conditions of measurement had been determined and evaluated through the preliminary measurement of compressive stress acting on the cylindrical surface. Furthermore, the fatigue strength estimated by applying the residual stress data to the previously presented hypothesis was compared with the experimental results. The main conclusions obtained were as follows: (1) The residual stress in a relatively small area on the cylindrical surface with large curvature can be measured by X-ray using a method of stepped scanning and parabolic approximation; (2) The compressive residual stress measured at the thread root was larger for the bolt manufactured by thread rolling after heat treatment than for one manufactured by thread rolling before heat treatment; (3) The distribution of residual stress along the axial direction from the thread root to the portion under crest did not represent remarkable change in its value; (4) The residual stress of a bolt was somewhat decreased by fatigue loading on the condition of low mean stress; (5) The fatigue strength estimated using residual stress data showed the tendency of experimental results well. (author)

NPE - close-in stress and motion measurements

Energy Technology Data Exchange (ETDEWEB)

Smith, C.W. [Sandia National Labs., Albuquerque, NM (United States)

1994-12-31

On the Non-Proliferation Experiment we measured stresses and accelerations in the nonlinear regime. Measurements were made in the host rock and in the grout stemming of the access drift. The thrust of the measurements was to provide data for a comparison with waveforms from nuclear events and with calculations of the process. Measured stress waveforms show greater amplitudes than yield-scaled waveforms from nearby nuclear events. Specifically, the five stress peaks suggest an equivalent nuclear yield of more than two kilotons. Material velocity data from NPE also show amplitudes greater than nuclear data. The risetimes of the NPE data are slower than risetimes of scaled nuclear data. The ratio of risetimes is about two; this difference may prove useful in discriminating between nuclear and chemical explosions. Non-radical accelerations show some departure from symmetric wave propagation. Tuff strengths-inferred from differences between radial and hoop stresses-show values that are about twice laboratory determined values.

Analysis of rock stress and rock stress measurements with application to Aespoe HRL

International Nuclear Information System (INIS)

Lundholm, Beatrice

2000-11-01

The process of choosing a site for a nuclear waste repository means that many aspects have to be taken into consideration. One of these is that the repository has to be mechanically stable for a long time. The mechanical stability of the rock is very difficult to determine. One of several factors, which determine the mechanical stability, is the virgin state of stress. The thesis project consists of two parts. In the first part the state of stress at Aespoe Hard Rock Laboratory had to be defined. This was done based on earlier rock stress measurements conducted during the years 1988 to 1997. Two different measurement techniques have been used, hydraulic fracturing and overcoring. During the overcoring two types of cells have been used, CSIRO HI-cell and a cell developed by the Swedish State Power Board (SSPB). In the second part of the project, investigation of the correlation between the stress and geological structures are made using numerical modelling tools such as FLAC, UDEC and 3DEC. The rock stress measurements using the hydraulic fracturing gave orientations of the horizontal stress that coincide with earlier hydraulic fracturing measurements conducted in Scandinavia. The magnitudes of rock stresses are slightly lower than the earlier reported stress magnitudes for the Scandinavian part of the earth crust. The rock stresses obtained from the overcoring resulted in higher stresses than what was predicted by the hydraulic fracturing measurements. However, the orientation of the maximum horizontal stresses coincides well between the two techniques. The orientation is also more or less constant with respect to increasing depth. The state of stress at Aespoe is defined by using the results from the hydraulic fracturing and the measurements conducted by SSPB-cell. The measurements from the SSPB-cell are used since these have a Poisson's ratio that corresponds well with the uniaxial tests of rock samples and since the measurements have been done at a distance from

Enhanced functional connectivity properties of human brains during in-situ nature experience

Directory of Open Access Journals (Sweden)

Zheng Chen

2016-07-01

Full Text Available In this study, we investigated the impacts of in-situ nature and urban exposure on human brain activities and their dynamics. We randomly assigned 32 healthy right-handed college students (mean age = 20.6 years, SD = 1.6; 16 males to a 20 min in-situ sitting exposure in either a nature (n = 16 or urban environment (n = 16 and measured their Electroencephalography (EEG signals. Analyses revealed that a brief in-situ restorative nature experience may induce more efficient and stronger brain connectivity with enhanced small-world properties compared with a stressful urban experience. The enhanced small-world properties were found to be correlated with “coherent” experience measured by Perceived Restorativeness Scale (PRS. Exposure to nature also induces stronger long-term correlated activity across different brain regions with a right lateralization. These findings may advance our understanding of the functional activities during in-situ environmental exposures and imply that a nature or nature-like environment may potentially benefit cognitive processes and mental well-being.

Application of heat stress in situ demonstrates a protective role of irradiation on photosynthetic performance in alpine plants

OpenAIRE

Buchner, Othmar; STOLL, Magdalena; Karadar, Matthias; Kranner, Ilse; Neuner, Gilbert

2014-01-01

The impact of sublethal heat on photosynthetic performance, photosynthetic pigments and free radical scavenging activity was examined in three high mountain species, R hododendron ferrugineum, S enecio incanus and R anunculus glacialis using controlled in situ applications of heat stress, both in darkness and under natural solar irradiation. Heat treatments applied in the dark reversibly reduced photosynthetic performance and the maximum quantum efficiency of photosystem II (Fv/Fm), which rem...

'In situ' straining in the HVEM of neutron irradiated copper crystals

International Nuclear Information System (INIS)

Johnson, E.; Hirsch, P.B.

1976-01-01

High energy neutron irradiated copper single crystals strained 'in situ' in the high voltage electron microscope are observed to yield in relatively few strongly developed slip bands. The deformation in the slip bands is caused by glide of inclined dislocations close to screw orientation belonging to the primary slip system. Radiation induced point defect clusters are swept up by the dislocations whereby superjogs are formed. Some of the jogs will be sessile and act as pinning points for the gliding dislocations, which bow out under the applied stress to form perfect dipoles mainly of edge nature, as well as faulted dipoles, which are finally pinched off. The effective stress measured from the radius of curvature of the bowed-out dislocations is in agreement with resolved flow stress measurements from irradiated bulk crystals. (Auth.)

3D shape measurements with a single interferometric sensor for in-situ lathe monitoring

Science.gov (United States)

Kuschmierz, R.; Huang, Y.; Czarske, J.; Metschke, S.; Löffler, F.; Fischer, A.

2015-05-01

Temperature drifts, tool deterioration, unknown vibrations as well as spindle play are major effects which decrease the achievable precision of computerized numerically controlled (CNC) lathes and lead to shape deviations between the processed work pieces. Since currently no measurement system exist for fast, precise and in-situ 3d shape monitoring with keyhole access, much effort has to be made to simulate and compensate these effects. Therefore we introduce an optical interferometric sensor for absolute 3d shape measurements, which was integrated into a working lathe. According to the spindle rotational speed, a measurement rate of 2,500 Hz was achieved. In-situ absolute shape, surface profile and vibration measurements are presented. While thermal drifts of the sensor led to errors of several mµm for the absolute shape, reference measurements with a coordinate machine show, that the surface profile could be measured with an uncertainty below one micron. Additionally, the spindle play of 0.8 µm was measured with the sensor.

Methods of measuring residual stresses in components

International Nuclear Information System (INIS)

Rossini, N.S.; Dassisti, M.; Benyounis, K.Y.; Olabi, A.G.

2012-01-01

Highlights: ► Defining the different methods of measuring residual stresses in manufactured components. ► Comprehensive study on the hole drilling, neutron diffraction and other techniques. ► Evaluating advantage and disadvantage of each method. ► Advising the reader with the appropriate method to use. -- Abstract: Residual stresses occur in many manufactured structures and components. Large number of investigations have been carried out to study this phenomenon and its effect on the mechanical characteristics of these components. Over the years, different methods have been developed to measure residual stress for different types of components in order to obtain reliable assessment. The various specific methods have evolved over several decades and their practical applications have greatly benefited from the development of complementary technologies, notably in material cutting, full-field deformation measurement techniques, numerical methods and computing power. These complementary technologies have stimulated advances not only in measurement accuracy and reliability, but also in range of application; much greater detail in residual stresses measurement is now available. This paper aims to classify the different residual stresses measurement methods and to provide an overview of some of the recent advances in this area to help researchers on selecting their techniques among destructive, semi destructive and non-destructive techniques depends on their application and the availabilities of those techniques. For each method scope, physical limitation, advantages and disadvantages are summarized. In the end this paper indicates some promising directions for future developments.

Micromachined sensor for stress measurement and micromechanical study of free-standing thin films for MEMS applications

Science.gov (United States)

Zhang, Ping

Microelectromechanical systems (MEMS) have a wide range of applications. In the field of wireless and microwave technology, considerable attention has been given to the development and integration of MEMS-based RF (radio frequency) components. An RF MEMS switch requires low insertion loss, high isolation, and low actuation voltage - electrical aspects that have been extensively studied. The mechanical requirements of the switch, such as low sensitivity to built-in stress and high reliability, greatly depend on the micromechanical properties of the switch materials, and have not been thoroughly explored. RF MEMS switches are typically in the form of a free-standing thin film structure. Large stress gradients and across-wafer stress variations developed during fabrication severely degrade their electrical performance. A micromachined stress measurement sensor has been developed that can potentially be employed for in-situ monitoring of stress evolution and stress variation. The sensors were micromachined using five masks on two wafer levels, each measuring 5x3x1 mm. They function by means of an electron tunneling mechanism, where a 2x2 mm silicon nitride membrane elastically deflects under an applied deflection voltage via an external feedback circuitry. For the current design, the sensors are capable of measuring tensile stresses up to the GPa range under deflection voltages of 50--100 V. Sensor functionality was studied by finite element modeling and a theoretical analysis of square membrane deflection. While the mechanical properties of thin films on substrates have been extensively studied, studies of free-standing thin films have been limited due to the practical difficulties in sample handling and testing. Free-standing Al and Al-Ti thin films specimens have been successfully fabricated and microtensile and stress relaxation tests have been performed using a custom-designed micromechanical testing apparatus. A dedicated TEM (transmission electron microscopy

Results and conclusions of stress measurements at Stripa

International Nuclear Information System (INIS)

Doe, T.W.; Hustrulid, W.A.; Leijon, B.; Ingevald, K.; Strindell, L.; Carlsson, H.

1982-10-01

This paper describes the results of stress measurements at Stripa, compares the results obtained by different techniques, and recommends a stress measurement program for a hard rock repository site. The state of stress at the Stripa Mine has been measured both in a 381-m-deep hole drilled from the surface and in holes drilled from the drifts underground. Hydraulic fracturing and several overcoring methods have been used (Lulea triaxial gauge, CSIRO gauge, USBM gauge, Swedish State Power Board deep-hole Leeman triaxial gauge). The results of overcoring and hydraulic fracturing agree well, particularly for the magnitude and orientation of the greatest stress. A recommended program for stress measurement at a repository site would include hydraulic fracturing and deep-hole overcoring in a deep hole drilled from surface, and overcoring (Lulea gauge and USBM gauge) and hydraulic fracturing from holes drilled from underground openings when access is available. Propagation of the hydraulic fractures should be monitored acoustically to determine their location and orientation

Optical residual stress measurement in TFT-LCD panels

Science.gov (United States)

Wang, Wei-Chung; Sung, Po-Chi

2017-06-01

The residual stress of the glass substrate might be one of causes to produce the non-uniform light distribution defect, i.e. Mura, in thin film transistor-liquid crystal display (TFT-LCD) panels. Glass is a birefringent material with very low birefringence. Furthermore, the thinner and thinner thickness request from the market makes the traditional photoelasticity almost impossible to measure the residual stresses produced in thin glass plates. Recently, a low-level stress measurement method called transmissivity extremities theory of photoelasticity (TEToP) was successfully developed to measure the residual stress in glass plate. Besides, to measure the stress of the glass plate in the TFT-LCD panel whose rear surface may has different kinds of coatings, an advanced reflection photoelasticity was also developed. In this paper, three commercially available glass plates with 0.33mm nominal thickness and three glass circular disks with different coatings were inspected to verify the feasibility of the TEToP and the advanced reflection photoelasticity, respectively.

An in-situ measuring method for planar straightness error

Science.gov (United States)

Chen, Xi; Fu, Luhua; Yang, Tongyu; Sun, Changku; Wang, Zhong; Zhao, Yan; Liu, Changjie

2018-01-01

According to some current problems in the course of measuring the plane shape error of workpiece, an in-situ measuring method based on laser triangulation is presented in this paper. The method avoids the inefficiency of traditional methods like knife straightedge as well as the time and cost requirements of coordinate measuring machine(CMM). A laser-based measuring head is designed and installed on the spindle of a numerical control(NC) machine. The measuring head moves in the path planning to measure measuring points. The spatial coordinates of the measuring points are obtained by the combination of the laser triangulation displacement sensor and the coordinate system of the NC machine, which could make the indicators of measurement come true. The method to evaluate planar straightness error adopts particle swarm optimization(PSO). To verify the feasibility and accuracy of the measuring method, simulation experiments were implemented with a CMM. Comparing the measurement results of measuring head with the corresponding measured values obtained by composite measuring machine, it is verified that the method can realize high-precise and automatic measurement of the planar straightness error of the workpiece.

Early in-situ measurements program for the Waste Isolation Pilot Plant

International Nuclear Information System (INIS)

Wowak, W.E.

1979-06-01

The technical basis and description of measurements for the early in-situ measurements program at the WIPP are described and a proposed organizational structure is presented. Measurements are needed for verification of design predictions and also for a prelude to the main experiment program. The design verification measurements will be concentrated in the first shaft and the underground support and access areas. Early experiments will be concentrated in the test drifts on the storage horizons. Recommendations are made to DOE for appropriate division of responsibility among Bechtel, the technical support contractor, the instrumentation contractor, and Sandia

Retrievals of Cloud Droplet Size from the RSP Data: Validation Using in Situ Measurements

Science.gov (United States)

Alexandrov, Mikhail D.; Cairns, Brian; Sinclair, Kenneth; Wasilewski, Andrzej P.; Ziemba, Luke; Crosbie, Ewan; Hair, John; Hu, Yongxiang; Hostetler, Chris; Stamnes, Snorre

2016-01-01

We present comparisons of cloud droplet size distributions retrieved from the Research Scanning Polarimeter (RSP) data with correlative in situ measurements made during the North Atlantic Aerosols and Marine Ecosystems Study (NAAMES). This field experiment was based at St. Johns airport, Newfoundland, Canada with the latest deployment in May - June 2016. RSP was onboard the NASA C-130 aircraft together with an array of in situ and other remote sensing instrumentation. The RSP is an along-track scanner measuring polarized and total reflectances in9 spectral channels. Its unique high angular resolution allows for characterization of liquid water droplet size using the rainbow structure observed in the polarized reflectances in the scattering angle range between 135 and 165 degrees. A parametric fitting algorithm applied to the polarized reflectances provides retrievals of the droplet effective radius and variance assuming a prescribed size distribution shape (gamma distribution). In addition to this, we use a non-parametric method, Rainbow Fourier Transform (RFT), which allows us to retrieve the droplet size distribution (DSD) itself. The latter is important in the case of clouds with complex structure, which results in multi-modal DSDs. During NAAMES the aircraft performed a number of flight patterns specifically designed for comparison of remote sensing retrievals and in situ measurements. These patterns consisted of two flight segments above the same straight ground track. One of these segments was flown above clouds allowing for remote sensing measurements, while the other was at the cloud top where cloud droplets were sampled. We compare the DSDs retrieved from the RSP data with in situ measurements made by the Cloud Droplet Probe (CDP). The comparisons show generally good agreement with deviations explainable by the position of the aircraft within cloud and by presence of additional cloud layers in RSP view that do not contribute to the in situ DSDs. In the

Stability of silver nanoparticle monolayers determined by in situ streaming potential measurements

International Nuclear Information System (INIS)

Morga, Maria; Adamczyk, Zbigniew; Oćwieja, Magdalena

2013-01-01

A silver particle suspension obtained by a chemical reduction was used in this work. Monolayers of these particles (average size 28 nm) on mica modified by poly(allylamine hydrochloride) were produced under diffusion-controlled transport. Monolayer coverages, quantitatively determined by atomic force microscopy (AFM) and SEM, was regulated by adjusting the nanoparticle deposition time and the suspension concentration. The zeta potential of the monolayers was determined by streaming potential measurements carried out under in situ (wet) conditions. These measurements performed for various ionic strengths and pH were interpreted in terms of the three-dimensional (3D) electrokinetic model. The stability of silver monolayers was also investigated using streaming potential and the AFM methods. The decrease in the surface coverage of particles as a function of time and ionic strength varied between 10 −1 and 10 −4  M was investigated. This allowed one to determine the equilibrium adsorption constant K a and the binding energy of silver particles (energy minima depth). Energy minima depth were calculated that varied between −18 kT for I = 10 −1  M and −19 kT for I = 10 −4 for pH 5.5 and T = 298 K. Our investigations suggest that the interactions between surface and nanoparticles are controlled by the electrostatic interactions among ion pairs. It was also shown that the in situ electrokinetic measurements are in accordance with those obtained by more tedious ex situ AFM measurements. This confirmed the utility of the streaming potential method for direct kinetic studies of nanoparticle deposition/release processes.Graphical Abstract

Role of the misfit stress between grains in the Bauschinger effect for a polycrystalline material

International Nuclear Information System (INIS)

Chen, B.; Hu, J.N.; Wang, Y.Q.; Zhang, S.Y.; Van Petegem, S.; Cocks, A.C.F.; Smith, D.J.; Flewitt, P.E.J.

2015-01-01

The role of misfit stress in kinematic hardening under reversed straining of a Type 316H austenitic stainless steel has been investigated by using neutron diffraction combined with in situ deformation. Initial misfit stresses, often referred to an intergranular internal stresses, were created by the tensile pre-straining at high temperature. The misfit stresses at the length-scale of grain families, measured by neutron diffraction, were shown to be a function of the magnitude of the tensile pre-strain. The pre-strained specimens were further subjected to either continued (tensile) straining or reversed (compressive) straining at room temperature. In situ neutron diffraction measurements were undertaken to monitor the change of the misfit stresses during loading. The macroscopic stress–strain behaviour was used to derive isotropic and kinematic hardening stresses developed in the pre-strained specimens. Results show that the change of the transient softening stress towards a zero value is accompanied by a decrease in the change of the misfit stresses. A multi-scale self-consistent model has been developed to assist in understanding the measured change of the misfit stresses when subjecting the material to strain reversal. An important conclusion is that the origin of the kinematic hardening of Type 316H austenitic stainless steel arises from the misfit stress between grains

Measurement of stress using synchrotron x-rays

International Nuclear Information System (INIS)

Weidner, Donald J; Li Li

2006-01-01

Stress analysis in polycrystalline materials reveals that stress can vary considerably among different subpopulations of grains. Samples of MgO and mixtures of MgO and spinel have been studied. After the onset of plastic flow, stronger grains or orientations will support more stress than the weaker grains. A grain to grain fabric develops that enables this stress partitioning. The stress partitioning and the resulting fabric can invalidate static measurements of elastic moduli. However, high temperature flow mechanisms reveal a more isotropic strength behaviour resulting in a more uniform variation of stress with orientation

Stress-induced martensitic transformations in a Cu-Al-Ni shape memory alloy studied by in situ transmission electron microscopy

Czech Academy of Sciences Publication Activity Database

Zárubová, Niva; Gemperlová, Juliana; Gärtnerová, Viera; Gemperle, Antonín

481-482, č. 5 (2008), s. 457-461 ISSN 0921-5093 R&D Projects: GA ČR GA202/04/2016; GA AV ČR(CZ) IAA200100627 Institutional research plan: CEZ:AV0Z10100520 Keywords : in situ TEM straining * CuAlNi shape memory alloy * stress -induced formation of martensite Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.806, year: 2008

An improved in situ measurement of offset phase shift towards quantitative damping-measurement with AFM

International Nuclear Information System (INIS)

Minary-Jolandan, Majid; Yu Minfeng

2008-01-01

An improved approach is introduced in damping measurement with atomic force microscope (AFM) for the in situ measurement of the offset phase shift needed for determining the intrinsic mechanical damping in nanoscale materials. The offset phase shift is defined and measured at a point of zero contact force according to the deflection part of the AFM force plot. It is shown that such defined offset phase shift is independent of the type of sample material, varied from hard to relatively soft materials in this study. This improved approach allows the self-calibrated and quantitative damping measurement with AFM. The ability of dynamic mechanical analysis for the measurement of damping in isolated one-dimensional nanostructures, e.g. individual multiwalled carbon nanotubes, was demonstrated

Manipulation of Samples at Extreme Temperatures for Fast in-situ Synchrotron Measurements

Energy Technology Data Exchange (ETDEWEB)

Weber, Richard [Materials Development, Inc., Arlington Heights, IL (United States)

2016-04-22

An aerodynamic sample levitation system with laser beam heating was integrated with the APS beamlines 6 ID-D, 11 ID-C and 20 BM-B. The new capability enables in-situ measurements of structure and XANES at extreme temperatures (300-3500 °C) and in conditions that completely avoid contact with container surfaces. In addition to maintaining a high degree of sample purity, the use of aerodynamic levitation enables deep supercooling and greatly enhanced glass formation from a wide variety of melts and liquids. Development and integration of controlled extreme sample environments and new measurement techniques is an important aspect of beamline operations and user support. Processing and solidifying liquids is a critical value-adding step in manufacturing semiconductors, optical materials, metals and in the operation of many energy conversion devices. Understanding structural evolution is of fundamental importance in condensed materials, geology, and biology. The new capability provides unique possibilities for materials research and helps to develop and maintain a competitive materials manufacturing and energy utilization industry. Test samples were used to demonstrate key features of the capability including experiments on hot crystalline materials, liquids at temperatures from about 500 to 3500 °C. The use of controlled atmospheres using redox gas mixtures enabled in-situ changes in the oxidation states of cations in melts. Significant innovations in this work were: (i) Use of redox gas mixtures to adjust the oxidation state of cations in-situ (ii) Operation with a fully enclosed system suitable for work with nuclear fuel materials (iii) Making high quality high energy in-situ x-ray diffraction measurements (iv) Making high quality in-situ XANES measurements (v) Publishing high impact results (vi) Developing independent funding for the research on nuclear materials This SBIR project work led to a commercial instrument product for the niche market of processing and

Underwater in situ measurements of radionuclides in selected submarine groundwater springs, Mediterranean sea

International Nuclear Information System (INIS)

Tsabaris, C.; Scholten, J.; Karageorgis, A. P.; Comanducci, J. F.; Georgopoulos, D.; Liong Wee Kwong, L.; Patiris, D. L.; Papathanassiou, E.

2010-01-01

The application of the in situ measurement system 'KATERINA' for monitoring of radon progenies in submarine groundwater discharge (SGD) was investigated at different locations in the Mediterranean Sea (Chalkida, Stoupa, Korfos and Cabbe). At Chalkida and Stoupa radon progenies concentration exhibited almost constant values of 1.2±0.1 and 2.5±0.2 Bq l -1 , respectively. At Korfos these activities ranged between 1.4±0.1 and 2.3±0.2 Bq l -1 exhibiting inverse relationship with salinity. At Cabbe the in situ measured data were compared with radon measurements obtained by liquid scintillation counter. The system also resolved radon progeny variations of SGD on time scales above 1 h. The radioactivity levels of radon progenies from all sites were found considerably lower (approximately 2 orders of magnitude) than the commonly accepted limits for radon in drinking water. (authors)

Geotechnical site assessment methodologies relevant to potential deep underground disposal facilities: with particular reference to the determination of in situ rock stress by the hydraulic fracturing method

International Nuclear Information System (INIS)

Monaghan, B.G.; Richards, L.R.

1986-10-01

A final report summarizing the research conducted on geotechnical site assessment methodologies relevant to Land 3/4 sites. Two areas of research have been investigated; in situ stress determination by the hydraulic fracturing method in basic volcanics and sediments and the laboratory determination of hydraulic fracture tensile strength. The analysis and interpretation of the hydraulic fracturing test data from a programme of testing in the Vale of Belvoir is discussed in detail particularly in respect of the effects of pore water pressure and fluid diffusion in the rocks being tested. The regional stress regime of the Vale of Belvoir is discussed with respect to the results of the in situ stress determination. A method for determining the hydraulic fracture tensile strength in the laboratory is described. The results of a series of laboratory tests on rock core are reported. (author)

Quantitative analysis of stress-induced martensites by in situ transmission electron microscopy superelastic tests in Cu-Al-Ni shape memory alloys

International Nuclear Information System (INIS)

No, M.L.; Ibarra, A.; Caillard, D.; San Juan, J.

2010-01-01

Stress-induced martensite nucleation and further growing, in Cu-Al-Ni shape memory alloys, have been studied during in situ superelastic tests in the transmission electron microscope. Two kinds of martensite, β 3 ' and γ 3 ' , are induced and can coexist under stress, both exhibiting in a high density of stacking faults. The interface plane and the orientation relationships between the different variants of such martensites have been determined, and the atomic configurations of the lattices across the interface have been described. Finally, in light of the results, selection rules for the stress-induced promoted martensites at the nano-scale have been established, being determined by the shear direction and the basal plane of the martensite lattice.

In-situ optical and acoustical measurements of the buoyant cyanobacterium p. Rubescens: spatial and temporal distribution patterns.

Directory of Open Access Journals (Sweden)

Hilmar Hofmann

Full Text Available Optical (fluorescence and acoustic in-situ techniques were tested in their ability to measure the spatial and temporal distribution of plankton in freshwater ecosystems with special emphasis on the harmful and buoyant cyanobacterium P. rubescens. Fluorescence was measured with the multi-spectral FluoroProbe (Moldaenke FluoroProbe, MFP and a Seapoint Chlorophyll Fluorometer (SCF. In-situ measurements of the acoustic backscatter strength (ABS were conducted with three different acoustic devices covering multiple acoustic frequencies (614 kHz ADCP, 2 MHz ADP, and 6 MHz ADV. The MFP provides a fast and reliable technique to measure fluorescence at different wavelengths in situ, which allows discriminating between P. rubescens and other phytoplankton species. All three acoustic devices are sensitive to P. rubescens even if other scatterers, e.g., zooplankton or suspended sediment, are present in the water column, because P. rubescens containing gas vesicles has a strong density difference and hence acoustic contrast to the ambient water and other scatterers. After calibration, the combination of optical and acoustical measurements not only allows qualitative and quantitative observation of P. rubescens, but also distinction between P. rubescens, other phytoplankton, and zooplankton. As the measuring devices can sample in situ at high rates they enable assessment of plankton distributions at high temporal (minutes and spatial (decimeters resolution or covering large temporal (seasonal and spatial (basin scale scales.

Size effect on compression properties of GaN nanocones examined using in situ transmission electron microscopy

International Nuclear Information System (INIS)

Kang, Shao-Hui; Fang, Te-Hua

2014-01-01

Highlights: • Strain-induced structural variations of GaN nanocones are estimated using in situ TEM. • Young’s modulus of GaN nanocones with a diameter of 100–350 nm are 190–290 GPa. • The E 2 peak was red-shifted, indicated increased compressive stress. - Abstract: Mechanical property measurements of single nanocones are challenging because the small scale of the nanostructures. In this study, critical-stress- and strain-induced structural variations of GaN nanocones are estimated using in situ transmission electron microscopy (TEM) compression experiments. For single GaN nanocones with a diameter of 100–350 nm, the Young’s modulus, plastic deformation energy (W p ), and elastic deformation energy (W e ) values were 190–290 GPa, 0.02–1.65 × 10 −11 J, and 0.04–3.85 × 10 −11 J, respectively. Raman spectra were used to measure GaN indentation. The E 2 peak was red-shifted, indicated increased compressive stress in the indented area

Drag balance Cubesat attitude motion effects on in-situ thermosphere density measurements

Science.gov (United States)

Felicetti, Leonard; Santoni, Fabio

2014-08-01

The dynamics of Cubesats carrying a drag balance instrument (DBI) for in situ atmosphere density measurements is analyzed. Atmospheric drag force is measured by the displacement of two light plates exposed to the incoming particle flow. This system is well suited for a distributed sensor network in orbit, to get simultaneous in situ local (non orbit averaged) measurements in multiple positions and orbit heights, contributing to the development and validation of global atmosphere models. The implementation of the DBI leads to orbit normal pointing spinning two body system. The use of a spin-magnetic attitude control system is suggested, based only on magnetometer readings, contributing to making the system simple, inexpensive, and reliable. It is shown, by an averaging technique, that this system provides for orbit normal spin axis pointing. The effect of the coupling between the attitude dynamics and the DBI is evaluated, analyzing its frequency content and showing that no frequency components arise, affecting the DBI performance. The analysis is confirmed by Monte Carlo numerical simulation results.

In situ stresses in rock masses: methodology for its study in tunnel projects in Spain; Metodologia de estudio y obtencion de las tensiones in situ en los proyectos de obra subterranea realizados en Espana

Energy Technology Data Exchange (ETDEWEB)

Madirolas Perez, G.; Perucho Martinez, A.

2014-07-01

In situ stress is one of the main factors to be taken into account in the design of tunnels, as it can cause inadmissible stresses and strains leading to high deviations in the budgets. For that reason, the stress state is directly introduced into the numerical models used for the design of tunnels. In Spain, although several tunnels have been carried out with an important overburden in tectonically relevant zones, a quantitative determination of the stresses has not been usually included in civil work projects. Therefore, it is considered necessary to implement a routine procedure of study of civil work projects involving tunnels excavated in rock, and a new detailed methodology is proposed. The challenge is that project managers, who face works in which stresses may play a determinant role, may have a practical reference enabling them to optimize available resources and to include the real stress information in the design of underground works. (Author)

Characterizing Suspension Plasma Spray Coating Formation Dynamics through Curvature Measurements

Science.gov (United States)

Chidambaram Seshadri, Ramachandran; Dwivedi, Gopal; Viswanathan, Vaishak; Sampath, Sanjay

2016-12-01

Suspension plasma spraying (SPS) enables the production of variety of microstructures with unique mechanical and thermal properties. In SPS, a liquid carrier (ethanol/water) is used to transport the sub-micrometric feedstock into the plasma jet. Considering complex deposition dynamics of SPS technique, there is a need to better understand the relationships among spray conditions, ensuing particle behavior, deposition stress evolution and resultant properties. In this study, submicron yttria-stabilized zirconia particles suspended in ethanol were sprayed using a cascaded arc plasma torch. The stresses generated during the deposition of the layers (termed evolving stress) were monitored via the change in curvature of the substrate measured using an in situ measurement apparatus. Depending on the deposition conditions, coating microstructures ranged from feathery porous to dense/cracked deposits. The evolving stresses and modulus were correlated with the observed microstructures and visualized via process maps. Post-deposition bi-layer curvature measurement via low temperature thermal cycling was carried out to quantify the thermo-elastic response of different coatings. Lastly, preliminary data on furnace cycle durability of different coating microstructures were evaluated. This integrated study involving in situ diagnostics and ex situ characterization along with process maps provides a framework to describe coating formation mechanisms, process parametrics and microstructure description.

History Dependence of the Microstructure on Time-Dependent Deformation During In-Situ Cooling of a Nickel-Based Single-Crystal Superalloy

Science.gov (United States)

Panwisawas, Chinnapat; D'Souza, Neil; Collins, David M.; Bhowmik, Ayan; Roebuck, Bryan

2018-05-01

Time-dependent plastic deformation through stress relaxation and creep deformation during in-situ cooling of the as-cast single-crystal superalloy CMSX-4® has been studied via neutron diffraction, transmission electron microscopy, electro-thermal miniature testing, and analytical modeling across two temperature regimes. Between 1000 °C and 900 °C, stress relaxation prevails and gives rise to softening as evidenced by a decreased dislocation density and the presence of long segment stacking faults in γ phase. Lattice strains decrease in both the γ matrix and γ' precipitate phases. A constitutive viscoplastic law derived from in-situ isothermal relaxation test under-estimates the equivalent plastic strain in the prediction of the stress and strain evolution during cooling in this case. It is thereby shown that the history dependence of the microstructure needs to be taken into account while deriving a constitutive law and which becomes even more relevant at high temperatures approaching the solvus. Higher temperature cooling experiments have also been carried out between 1300 °C and 1150 °C to measure the evolution of stress and plastic strain close to the γ' solvus temperature. In-situ cooling of samples using ETMT shows that creep dominates during high-temperature deformation between 1300 °C and 1220 °C, but below a threshold temperature, typically 1220 °C work hardening begins to prevail from increasing γ' fraction and resulting in a rapid increase in stress. The history dependence of prior accumulated deformation is also confirmed in the flow stress measurements using a single sample while cooling. The saturation stresses in the flow stress experiments show very good agreement with the stresses measured in the cooling experiments when viscoplastic deformation is dominant. This study demonstrates that experimentation during high-temperature deformation as well as the history dependence of the microstructure during cooling plays a key role in deriving

In Situ Stem Psychrometry: toward a Physiologically-Based Drought Monitoring Network

Science.gov (United States)

KOCH, G. W.; Williams, C.; Ambrose, A.

2012-12-01

Plant water potential is a synoptic variable that integrates soil and atmospheric moisture stress and interacts with plant-internal factors to regulate gas exchange and determine vulnerability to drought-induced hydraulic dysfunction. Despite its importance, methods for measuring water potential are labor intensive. This limitation reduces measurement frequency, likely causes important transient events to be overlooked, and restricts development of a richer understanding of the impacts of integrated water stress on plant and ecosystem function. Recent technological advances have enabled in-situ, automated measurement of branch water potential over periods of weeks to months using stem psychrometers. We evaluated this technology through laboratory and field comparisons to standard pressure chamber measurements and with field installations in temperate forest, semi-arid woodland, and chaparral ecosystems. Performance was highly sensitive to installation procedures. With proper sealing, insulation, and radiation shielding, psychrometers typically differed from pressure chamber measurements by less than 0.2 MPa down to water potentials as low as -7 MPa. Measurements in tall trees reaffirmed the influence of gravity on water potential as previously documented with the pressure chamber. Psychrometer performance in situ was stable for periods of several weeks to months, with tissue wound response degrading sensor operation over time. We conclude that stem psychrometer technology is now suitable to serve as the foundation for a physiologically-based drought monitoring network that can anticipate important ecosystem impacts including changes in whole-system fluxes and mortality events.

In-situ neutron diffraction study of Zircaloy 4 subjected to biaxial tension

Energy Technology Data Exchange (ETDEWEB)

Gharghouri, M.A. [Canadian Neutron Beam Centre, Chalk River Laboratories, Chalk River, ON (Canada); McDonald, D.; Xiao, L. [Atomic Energy of Canada Limited, Chalk River, ON (Canada)

2014-07-01

Zircaloy-4 is widely used as fuel element cladding in nuclear reactors. Pellet-clad interaction (PCI) failure is a concern for many water reactor fuel designs. Extensive work on the mechanism of PCI failure has led to the conclusion that stress corrosion cracking (SCC) induced by iodine vapour in the temperature range relevant to fuel operation is the most probable cause of PCI failure in zirconium alloy fuel element cladding. In-situ neutron diffraction measurements performed on tubular Zircaloy-4 specimens simultaneously pulled in tension and pressurized internally will provide information on the effects of stress biaxiality on the distribution of stresses at the crystal level during loading. (author)

Measuring depth profiles of residual stress with Raman spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Enloe, W.S.; Sparks, R.G.; Paesler, M.A.

1988-12-01

Knowledge of the variation of residual stress is a very important factor in understanding the properties of machined surfaces. The nature of the residual stress can determine a part`s susceptibility to wear deformation, and cracking. Raman spectroscopy is known to be a very useful technique for measuring residual stress in many materials. These measurements are routinely made with a lateral resolution of 1{mu}m and an accuracy of 0.1 kbar. The variation of stress with depth; however, has not received much attention in the past. A novel technique has been developed that allows quantitative measurement of the variation of the residual stress with depth with an accuracy of 10nm in the z direction. Qualitative techniques for determining whether the stress is varying with depth are presented. It is also demonstrated that when the stress is changing over the volume sampled, errors can be introduced if the variation of the stress with depth is ignored. Computer aided data analysis is used to determine the depth dependence of the residual stress.

Comparison of AOD, AAOD and column single scattering albedo from AERONET retrievals and in situ profiling measurements

Science.gov (United States)

Andrews, Elisabeth; Ogren, John A.; Kinne, Stefan; Samset, Bjorn

2017-05-01

Here we present new results comparing aerosol optical depth (AOD), aerosol absorption optical depth (AAOD) and column single scattering albedo (SSA) obtained from in situ vertical profile measurements with AERONET ground-based remote sensing from two rural, continental sites in the US. The profiles are closely matched in time (within ±3 h) and space (within 15 km) with the AERONET retrievals. We have used Level 1.5 inversion retrievals when there was a valid Level 2 almucantar retrieval in order to be able to compare AAOD and column SSA below AERONET's recommended loading constraint (AOD > 0.4 at 440 nm). While there is reasonable agreement for the AOD comparisons, the direct comparisons of in situ-derived to AERONET-retrieved AAOD (or SSA) reveal that AERONET retrievals yield higher aerosol absorption than obtained from the in situ profiles for the low aerosol optical depth conditions prevalent at the two study sites. However, it should be noted that the majority of SSA comparisons for AOD440 > 0.2 are, nonetheless, within the reported SSA uncertainty bounds. The observation that, relative to in situ measurements, AERONET inversions exhibit increased absorption potential at low AOD values is generally consistent with other published AERONET-in situ comparisons across a range of locations, atmospheric conditions and AOD values. This systematic difference in the comparisons suggests a bias in one or both of the methods, but we cannot assess whether the AERONET retrievals are biased towards high absorption or the in situ measurements are biased low. Based on the discrepancy between the AERONET and in situ values, we conclude that scaling modeled black carbon concentrations upwards to match AERONET retrievals of AAOD should be approached with caution as it may lead to aerosol absorption overestimates in regions of low AOD. Both AERONET retrievals and in situ measurements suggest there is a systematic relationship between SSA and aerosol amount (AOD or aerosol light

Investigation of creep threshold stresses using in situ TEM straining experiment in an Al-5Y2O3-10SiC composite

International Nuclear Information System (INIS)

Deshmukh, S.P.; Mishra, R.S.; Robertson, I.M.

2010-01-01

Creep behavior of metal matrix composites is similar to dispersion strengthen alloys and characterized by the presence of a threshold stress below which the creep rate is negligible. This threshold stress is attributed, at least in dispersion-strengthened alloys, to dislocation particle interactions in which the detachment of the dislocations from the particle is the rate-limiting step. Creep experiments were performed on an Al-5Y 2 O 3 -10SiC composite in the temperature range of 473 and 573 K and the nature of the dislocation-particle interaction was determined by performing in situ straining experiments at elevated temperature in a transmission electron microscope. The threshold stress and the detachment stress are temperature dependent and the detachment stress is less than the threshold stress emphasizing the contribution of load transfer from the matrix to the reinforcement phase.

Applications of synergistic combination of remote sensing and in-situ measurements on urban monitoring of air quality

Science.gov (United States)

Diaz, Adrian; Dominguez, Victor; Campmier, Mark; Wu, Yonghua; Arend, Mark; Vladutescu, Daniela Viviana; Gross, Barry; Moshary, Fred

2017-08-01

In this study, multiple remote sensing and in-situ measurements are combined in order to obtain a comprehensive understanding of the aerosol distribution in New York City. Measurement of the horizontal distribution of aerosols is performed using a scanning eye-safe elastic-backscatter micro-pulse lidar. Vertical distribution of aerosols is measured with a co-located ceilometer. Furthermore, our analysis also includes in-situ measurements of particulate matter and wind speed and direction. These observations combined show boundary layer dynamics as well as transport and inhomogeneous spatial distribution of aerosols, which are of importance for air quality monitoring.

Characterisation of lead-calcium alloys ageing in anisothermal conditions by calorimetric, resistance and hardness in-situ measurements

Energy Technology Data Exchange (ETDEWEB)

Rossi, F.; Lambertin, M. [Arts et Metiers ParisTech, LaBoMaP, Cluny (France); Delfaut-Durut, L. [CEA, Centre de Valduc, (SEMP, LECM), Is-sur-Tille (France); Maitre, A. [SPCTS, UFR Sciences et techniques, Limoges (France); Vilasi, M. [LCSM, Univ. Nancy I, Vandoeuvre les Nancy (France)

2010-02-15

Transformations undergone by lead-calcium alloys are numerous and have different kinetics from a few minutes to a few years. Anisothermal calorimetric measurements were performed to be able to identify these transformations quickly. It was then possible to identify five transformations. Complementary measurements have enabled us to define transformations with an in-situ electrical resistance measurement to follow the evolution of the calcium in solid solution and with an in-situ hardness measurement to characterise the mechanical properties. The aim of these results is to simulate the ageing and overageing of the alloy in isothermal conditions. (orig.)

Nitrogen budget of the northwestern Black Sea shelf inferred from modeling studies and in situ benthic measurements

NARCIS (Netherlands)

Grégoire, M.; Friedrich, J.

2004-01-01

A 3D eddy-resolving coupled biogeochemical-hydrodynamical model and in situ observations are used to investigate benthic processes on the Black Sea's NW shelf. Measurements of benthic fluxes (oxygen, nutrients, redox compounds) with in situ flux chambers are analyzed in regard to sediment dynamics

Monitoring of In-Situ Remediation By Time Lapse 3D Geo-Electric Measurements

Science.gov (United States)

Kanli, A. I.; Tildy, P.; Neducza, B.; Nagy, P.; Hegymegi, C.

2017-12-01

Injection of chemical oxidant solution to degrade the subsurface contaminants can be used for hydrocarbon contamination remediation. In this study, we developed a non-destructive measurement strategy to monitor oxidative in-situ remediation processes. The difficulties of the presented study originate from the small volume of conductive solution that can be used due to environmental considerations. Due to the effect of conductive groundwater and the high clay content of the targeted layer and the small volume of conductive solution that can be used due to environmental considerations, a site specific synthetic modelling is necessary for measurement design involving the results of preliminary 2D ERT measurements, electrical conductivity measurements of different active agents and expected resistivity changes calculated by soil resistivity modelling. Because of chemical biodegradation, the results of soil resistivity modelling have suggested that the reagent have complex effects on contaminated soils. As a result the plume of resistivity changes caused by the injected agent was determined showing strong fracturing effect because of the high pressure of injection. 3D time-lapse geo-electric measurements were proven to provide a usable monitoring tool for in-situ remediation as a result of our sophisticated tests and synthetic modelling.

IN SITU MEASUREMENT OF BEDROCK EROSION

Directory of Open Access Journals (Sweden)

D. H. Rieke-Zapp

2012-07-01

Full Text Available While long term erosion rates of bedrock material may be estimated by dating methods, current day erosion rates are – if at all available – based on rough estimates or on point measurements. Precise quantification of short term erosion rates are required to improve our understanding of short term processes, for input in landscape evolution models, as well as for studying the mechanics and efficiency of different erosion processes in varying geomorphological settings. Typical current day erosion rates in the European Alps range from sub-millimetre to several millimetres per year depending on the dominant erosion processes. The level of surveying accuracy required for recurring sub-millimetre to millimetre measurements in the field is demanding. A novel surveying setup for in-situ measurement of bedrock erosion was tested recently in three different locations in Switzerland. Natural bedrock was investigated in the Gornera gorge close to Zermatt. Further on, bedrock samples were installed in exposed locations in the Erlenbach research watershed close to Einsiedeln, and in the Illgraben debris flow channel, located in the Canton Schwyz and Valais, respectively. A twofold measurement approach was chosen for all locations. For the first setup control points providing an absolute reference frame for recurrent measurements were embedded close to the area of interest. Close range photogrammetry was applied to measure surface changes on the bedrock samples. The precision for surface measurements in the field was 0.1 mm (1 σ and thus suitable for the application. The equipment needed for the surveys can easily be carried to the field. At one field site a structured light scanner was used along with the photogrammetric setup. Although the current generation of structured light scanners appeared less suitable for field application, data acquisition was much faster and checking the data for completeness in the field was straight forward. The latest

In Situ Measurement of Bedrock Erosion

Science.gov (United States)

Rieke-Zapp, D. H.; Beer, A.; Turowski, J. M.; Campana, L.

2012-07-01

While long term erosion rates of bedrock material may be estimated by dating methods, current day erosion rates are - if at all available - based on rough estimates or on point measurements. Precise quantification of short term erosion rates are required to improve our understanding of short term processes, for input in landscape evolution models, as well as for studying the mechanics and efficiency of different erosion processes in varying geomorphological settings. Typical current day erosion rates in the European Alps range from sub-millimetre to several millimetres per year depending on the dominant erosion processes. The level of surveying accuracy required for recurring sub-millimetre to millimetre measurements in the field is demanding. A novel surveying setup for in-situ measurement of bedrock erosion was tested recently in three different locations in Switzerland. Natural bedrock was investigated in the Gornera gorge close to Zermatt. Further on, bedrock samples were installed in exposed locations in the Erlenbach research watershed close to Einsiedeln, and in the Illgraben debris flow channel, located in the Canton Schwyz and Valais, respectively. A twofold measurement approach was chosen for all locations. For the first setup control points providing an absolute reference frame for recurrent measurements were embedded close to the area of interest. Close range photogrammetry was applied to measure surface changes on the bedrock samples. The precision for surface measurements in the field was 0.1 mm (1 σ) and thus suitable for the application. The equipment needed for the surveys can easily be carried to the field. At one field site a structured light scanner was used along with the photogrammetric setup. Although the current generation of structured light scanners appeared less suitable for field application, data acquisition was much faster and checking the data for completeness in the field was straight forward. The latest generation of compact

Application of x-ray residual stress measurement to products

International Nuclear Information System (INIS)

Goto, T.; Iwamura, T.

1975-01-01

The X-ray residual stress measuring method is the only nondestructive method for measuring residual stress in polycrystalline materials. It is capable of obtaining information not only on macroscopic stress but also microscopic stress. The authors are employing this method for the development of pre-service and in-service inspection methods and for the improvement of various manufacturing techniques. In this paper, the results of measurement of some products as examples of its application are described. The examples introduced concern the following: (1) Selection of optimum conditions in heat treatment and stress-relief treatment. (2) Residual stress produced by mechanical processes such as autofrettage and flow form. (3) Check of manufacturing processes of rotary shaft and welded parts. (4) Estimation of fatigue strength of shot-peened part. (5) Detection of fatigue damage of shot-peened part. (auth.)

An automated x-ray stress measurement system using a microcomputer

International Nuclear Information System (INIS)

Kurita, Masanori; Miyagawa, Matsuo; Sato, Fumiyoshi; Sugiharai, Shigeru; Ishii, Masami; Sumiyoshi, Michio.

1985-01-01

An automated system for a rapid and precise X-ray stress measurement using a microcomputer has been developed. A block diagram of the system and a flowchart for the stress measurement method are shown. Of the various methods, the one most suitable for the material to be measured can be programmed in this system. The residual stress in a hardened steel having a broad diffraction profile (half-width of 7.2 deg ) could be measured in six minutes with a small standard deviation of 13 MPa by the Gaussian curve method using the sin 2 ψ method. Both the oscillation and the fixed ψ methods, using the Gaussian curve method, allow the X-ray stress measurement of coarse-grained steels; the sin 2 ψ diagram obtained by these methods had a good linearity. The residual stress measurement of an annealed chromium powder gave almost zero stress values, -3.2 to 2.9 MPa depending on the method used, showing a high accuracy of the system. (author)

The method for measuring residual stress in stainless steel pipes

International Nuclear Information System (INIS)

Shimov, Georgy; Rozenbaum, Mikhail; Serebryakov, Alexandr; Serebryakov, Andrey

2016-01-01

The main reason of appearance and growth of corrosion damages of the nuclear steam generator heat exchanger tubes is the process of stress-corrosion cracking of metal under the influence of residual tensile stress. Methods used in the production for estimating residual stresses (such as a method of ring samples) allow measuring only the average tangential stress of the pipe wall. The method of ring samples does not allow to assess the level of residual stress in the surface layer of the pipe. This paper describes an experimental method for measuring the residual stresses on the pipe surface by etching a thin surface layer of the metal. The construction and working principle of a trial installation are described. The residual stresses in the wall of the tubes 16 × 1.5 mm (steel AISI 321) for nuclear steam generators is calculated. Keywords: heat exchange pipes, stress corrosion cracking, residual stresses, stress distribution, stress measurement.

Application of heat stress in situ demonstrates a protective role of irradiation on photosynthetic performance in alpine plants.

Science.gov (United States)

Buchner, Othmar; Stoll, Magdalena; Karadar, Matthias; Kranner, Ilse; Neuner, Gilbert

2015-04-01

The impact of sublethal heat on photosynthetic performance, photosynthetic pigments and free radical scavenging activity was examined in three high mountain species, Rhododendron ferrugineum, Senecio incanus and Ranunculus glacialis using controlled in situ applications of heat stress, both in darkness and under natural solar irradiation. Heat treatments applied in the dark reversibly reduced photosynthetic performance and the maximum quantum efficiency of photosystem II (Fv /Fm), which remained impeded for several days when plants were exposed to natural light conditions subsequently to the heat treatment. In contrast, plants exposed to heat stress under natural irradiation were able to tolerate and recover from heat stress more readily. The critical temperature threshold for chlorophyll fluorescence was higher under illumination (Tc (')) than in the dark (Tc). Heat stress caused a significant de-epoxidation of the xanthophyll cycle pigments both in the light and in the dark conditions. Total free radical scavenging activity was highest when heat stress was applied in the dark. This study demonstrates that, in the European Alps, heat waves can temporarily have a negative impact on photosynthesis and, importantly, that results obtained from experiments performed in darkness and/or on detached plant material may not reliably predict the impact of heat stress under field conditions. © 2014 The Authors. Plant, Cell & Environment published by John Wiley & Sons Ltd.

In-situ failure test in the research tunnel at Olkiluoto

Energy Technology Data Exchange (ETDEWEB)

Autio, J.; Johansson, E.; Kirkkomaeki, T. [Saanio and Riekkola Consulting Engineers, Helsinki (Finland); Hakala, M. [Gridpoint Finland Oy (Finland); Heikkilae, E. [Helsinki Univ. of Technology, Otaniemi (Finland). Lab. of Rock Engineering

2000-05-01

A failure test suitable for execution in the Research Tunnel at Olkiluoto has been planned to study the failure of rock in-situ. The objectives of the in-situ failure test is to assess the applicability of numerical modelling codes and methods to the study of rock failure and associated crack propagation and to develop a novel technique to be used to determine the strength of rock in-situ. The objective of this study was to make a preliminary design of the failure test, assess the technical feasibility of the test and to give input information for further numerical modelling of the test. The design of the failure test is reported and results of preliminary modelling are given. The input information for future modelling includes a study of rock properties, fracture propagation in rock, in-situ stresses and the development of techniques for using the expanding agent to produce artificial stress field. The study showed that mechanical properties such as strength of gneissic tonalite, the main rock type in the Research Tunnel, depends highly on the orientation of schistocity. The in-situ failure test was shown to be technically feasible and a state of stress high enough to cause failure can be created artificially by using a proper expansive agent and design. (orig.)

Janus: Graphical Software for Analyzing In-Situ Measurements of Solar-Wind Ions

Science.gov (United States)

Maruca, B.; Stevens, M. L.; Kasper, J. C.; Korreck, K. E.

2016-12-01

In-situ observations of solar-wind ions provide tremendous insights into the physics of space plasmas. Instrument on spacecraft measure distributions of ion energies, which can be processed into scientifically useful data (e.g., values for ion densities and temperatures). This analysis requires a strong, technical understanding of the instrument, so it has traditionally been carried out by the instrument teams using automated software that they had developed for that purpose. The automated routines are optimized for typical solar-wind conditions, so they can fail to capture the complex (and scientifically interesting) microphysics of transient solar-wind - such as coronal mass ejections (CME's) and co-rotating interaction regions (CIR's) - which are often better analyzed manually.This presentation reports on the ongoing development of Janus, a new software package for processing in-situ measurement of solar-wind ions. Janus will provide user with an easy-to-use graphical user interface (GUI) for carrying out highly customized analyses. Transparent to the user, Janus will automatically handle the most technical tasks (e.g., the retrieval and calibration of measurements). For the first time, users with only limited knowledge about the instruments (e.g., non-instrumentalists and students) will be able to easily process measurements of solar-wind ions. Version 1 of Janus focuses specifically on such measurements from the Wind spacecraft's Faraday Cups and is slated for public release in time for this presentation.

In-situ-gamma ray spectrometry for measurements of environmental radioactivity

Energy Technology Data Exchange (ETDEWEB)

Winkelmann, I

1994-12-31

A detailed description of the method is presented. The range of application is shown. The calibration of the in-situ gamma ray spectrometer with a HPGe semiconductor detector and the evaluation of the spectra are described. A measuring time of about 15-30 min is sufficient to determine the specific natural and man-made radioactivity of the soil of some ten Bq/m{sup 2}. The results of soil contamination measurements in Germany after the Chernobyl accident are reported. A total of 22 nuclides are detected. The measured contamination for the first days after the accident was as follows: {sup 132}Te/{sup 132}I - 100 kBq/m{sup 2}, and {sup 131}I - 70 kBq/m{sup 2}. 6 figs., 4 tabs. (orig.).

Contact sponge water absorption test implemented for in situ measures

Science.gov (United States)

Gaggero, Laura; Scrivano, Simona

2016-04-01

The contact sponge method is a non-destructive in-situ methodology used to estimate a water uptake coefficient. The procedure, unlike other in-situ measurement was proven to be directly comparable to the water uptake laboratory measurements, and was registered as UNI 11432:2011. The UNI Normal procedure requires to use a sponge with known density, soaked in water, weighed, placed on the material for 1 minute (UNI 11432, 2011; Pardini & Tiano, 2004), then weighed again. Difficulties arise in operating on test samples or on materials with porosity varied for decay. While carrying on the test, fluctuations in the bearing of the environmental parameters were negligible, but not the pressure applied to the surface, that induced the release of different water amounts towards the material. For this reason we designed a metal piece of the same diameter of the plate carrying the sponge, to be screwed at the tip of a pocket penetrometer. With this instrument the sponge was kept in contact with the surface for 1 minute applying two different loads, at first pushed with 0.3 kg/cm2 in order to press the sponge, but not its holder, against the surface. Then, a load of 1.1 kg/ cm2 was applied, still avoiding deviating the load to the sponge holder. We applied both the current and our implemented method to determine the water absorption by contact sponge on 5 fresh rock types (4 limestones: Fine - and Coarse grained Pietra di Vicenza, Rosso Verona, Breccia Aurora, and the silicoclastic Macigno sandstone). The results show that 1) the current methodology imply manual skill and experience to produce a coherent set of data; the variable involved are in fact not only the imposed pressure but also the compression mechanics. 2) The control on the applied pressure allowed reproducible measurements. Moreover, 3) the use of a thicker sponge enabled to apply the method even on rougher surfaces, as the device holding the sponge is not in contact with the tested object. Finally, 4) the

Rapid characterization of agglomerate aerosols by in situ mass-mobility measurements.

Science.gov (United States)

Scheckman, Jacob H; McMurry, Peter H; Pratsinis, Sotiris E

2009-07-21

Transport and physical/chemical properties of nanoparticle agglomerates depend on primary particle size and agglomerate structure (size, fractal dimension, and dynamic shape factor). This research reports on in situ techniques for measuring such properties. Nanoparticle agglomerates of silica were generated by oxidizing hexamethyldisiloxane in a methane/oxygen diffusion flame. Upon leaving the flame, agglomerates of known electrical mobility size were selected with a differential mobility analyzer (DMA), and their mass was measured with an aerosol particle mass analyzer (APM), resulting in their mass fractal dimension, D(f), and dynamic shape factor, chi. Scanning and transmission electron microscopy (SEM/TEM) images were used to determine primary particle diameter and to qualitatively investigate agglomerate morphology. The DMA-APM measurements were reproducible within 5%, as determined by multiple measurements on different days under the same flame conditions. The effects of flame process variables (oxygen flow rate and mass production rate) on particle characteristics (D(f), and chi) were determined. All generated particles were fractal-like agglomerates with average primary particle diameters of 12-93 nm and D(f) = 1.7-2.4. Increasing the oxygen flow rate decreased primary particle size and D(f), while it increased chi. Increasing the production rate increased the agglomerate and primary particle sizes, and decreased chi without affecting D(f). The effects of oxygen flow rate and particle production rate on primary particle size reported here are in agreement with ex situ measurements in the literature, while the effect of process variables on agglomerate shape (chi) is demonstrated for the first time to our knowledge.

Residual stress in ceramics and ceramic composites

International Nuclear Information System (INIS)

Oden, M.

1992-01-01

Residual stresses in Si 3 N 4 and SiC have been measured with X-ray diffraction after grinding and thermal shock. The produced surface stresses are compressive after both treatments. The stresses show a strong dependence on the quenching temperature up to a certain temperature when cracks relax the stresses. The influence of the amount of reinforcing phase on the residual stress state in a Al 2 O 3 /SiC whisker composite was investigated and correlated to a modified Eshelby model. The agreement is excellent. The composite was quenched in liquid He (4K) and the stress state measured after show no relaxation of stresses, indicating elastic behaviour. An in situ strain measurement as a function of temperature conducted on a Al 2 O 3 /SiC whisker composite and a SiC/TiB 2 particle composite show very good agreement with the Eshelby model for the Al 2 O 3 /SiC system but not agreement for the SiC/TiB 2 system. The reason is believed to be stress relaxation during sample preparation. (au) (53 refs., 24 figs., 14 tabs.)

Factors influencing in situ gamma-ray measurements

Science.gov (United States)

Loonstra, E. H.; van Egmond, F. M.

2009-04-01

Introduction In situ passive gamma-ray sensors are very well suitable for mapping physical soil properties. In order to make a qualitative sound soil map, high quality input parameters for calibration are required. This paper will focus on the factors that affect the output of in situ passive gamma-ray sensors, the primary source, soil, not taken into account. Factors The gamma-ray spectrum contains information of naturally occurring nuclides 40K, 238U and 232Th and man-made nuclides like 137Cs, as well as the total count rate. Factors that influence the concentration of these nuclides and the count rate can be classified in 3 categories. These are sensor design, environmental conditions and operational circumstances. Sensor design The main elements of an in situ gamma-ray sensor that influence the outcome and quality of the output are the crystal and the spectrum analysis method. Material and size of the crystal determine the energy resolution. Though widely used, NaI crystals are not the most efficient capturer of gamma radiation. Alternatives are BGO and CsI. BGO has a low peak resolution, which prohibits use in cases where man-made nuclides are subject of interest. The material is expensive and prone to temperature instability. CsI is robust compared to NaI and BGO. The density of CsI is higher than NaI, yielding better efficiency, especially for smaller crystal sizes. More volume results in higher energy efficiency. The reduction of the measured spectral information into concentration of radionuclides is mostly done using the Windows analysis method. In Windows, the activities of the nuclides are found by summing the intensities of the spectrum found in a certain interval surrounding a peak. A major flaw of the Windows method is the limited amount of spectral information that is incorporated into the analysis. Another weakness is the inherent use of ‘stripping factors' to account for contributions of radiation from nuclide A into the peak of nuclide B. This

Residual stress measurement in a metal microdevice by micro Raman spectroscopy

International Nuclear Information System (INIS)

Song, Chang; Du, Liqun; Qi, Leijie; Li, Yu; Li, Xiaojun; Li, Yuanqi

2017-01-01

Large residual stress induced during the electroforming process cannot be ignored to fabricate reliable metal microdevices. Accurate measurement is the basis for studying the residual stress. Influenced by the topological feature size of micron scale in the metal microdevice, residual stress in it can hardly be measured by common methods. In this manuscript, a methodology is proposed to measure the residual stress in the metal microdevice using micro Raman spectroscopy (MRS). To estimate the residual stress in metal materials, micron sized β -SiC particles were mixed in the electroforming solution for codeposition. First, the calculated expression relating the Raman shifts to the induced biaxial stress for β -SiC was derived based on the theory of phonon deformation potentials and Hooke’s law. Corresponding micro electroforming experiments were performed and the residual stress in Ni–SiC composite layer was both measured by x-ray diffraction (XRD) and MRS methods. Then, the validity of the MRS measurements was verified by comparing with the residual stress measured by XRD method. The reliability of the MRS method was further validated by the statistical student’s t -test. The MRS measurements were found to have no systematic error in comparison with the XRD measurements, which confirm that the residual stresses measured by the MRS method are reliable. Besides that, the MRS method, by which the residual stress in a micro inertial switch was measured, has been confirmed to be a convincing experiment tool for estimating the residual stress in metal microdevice with micron order topological feature size. (paper)

Residual stress measurement in a metal microdevice by micro Raman spectroscopy

Science.gov (United States)

Song, Chang; Du, Liqun; Qi, Leijie; Li, Yu; Li, Xiaojun; Li, Yuanqi

2017-10-01

Large residual stress induced during the electroforming process cannot be ignored to fabricate reliable metal microdevices. Accurate measurement is the basis for studying the residual stress. Influenced by the topological feature size of micron scale in the metal microdevice, residual stress in it can hardly be measured by common methods. In this manuscript, a methodology is proposed to measure the residual stress in the metal microdevice using micro Raman spectroscopy (MRS). To estimate the residual stress in metal materials, micron sized β-SiC particles were mixed in the electroforming solution for codeposition. First, the calculated expression relating the Raman shifts to the induced biaxial stress for β-SiC was derived based on the theory of phonon deformation potentials and Hooke’s law. Corresponding micro electroforming experiments were performed and the residual stress in Ni-SiC composite layer was both measured by x-ray diffraction (XRD) and MRS methods. Then, the validity of the MRS measurements was verified by comparing with the residual stress measured by XRD method. The reliability of the MRS method was further validated by the statistical student’s t-test. The MRS measurements were found to have no systematic error in comparison with the XRD measurements, which confirm that the residual stresses measured by the MRS method are reliable. Besides that, the MRS method, by which the residual stress in a micro inertial switch was measured, has been confirmed to be a convincing experiment tool for estimating the residual stress in metal microdevice with micron order topological feature size.

Surface mechanical property and residual stress of peened nickel-aluminum bronze determined by in-situ X-ray diffraction

Science.gov (United States)

Wang, Chengxi; Jiang, Chuanhai; Zhao, Yuantao; Chen, Ming; Ji, Vincent

2017-10-01

As one of the most important surface strengthening method, shot peening is widely used to improve the fatigue and stress corrosion crack resistance of components by introducing the refined microstructure and compressive residual stress in the surface layer. However, the mechanical properties of this thin layer are different from the base metal and are difficult to be characterized by conventional techniques. In this work, a micro uniaxial tensile tester equipped with in-situ X-ray stress analyzer was employed to make it achievable on a nickel-aluminum bronze with shot peening treatment. According to the equivalent stress-strain relationship based on Von Mises stress criterion, the Young's modulus and yield strength of the peened layer were calculated. The results showed that the Young's modulus was the same as the bulk material, and the yield strength corresponding to the permanent plastic strain of 0.2% was increased by 21% after SP. But the fractographic analysis showed that the fracture feature of the surface layer was likely to transform from the dimple to the cleavage, indicating the improved strength might be attained at the expense of ductility. The monotonic and cyclic loading were also performed via the same combined set-up. In addition, the specific relaxation behavior of compressive residual stress was quantified by linear logarithm relationship between residual stress and cycle numbers. It was found that the compressive residual stress mainly relaxed in the first few cycles, and then reached steady state with further cycles. The relaxation rate and the stable value were chiefly depended on the stress amplitude and number of cycles. The retained residual stress kept in compressive under all given applied stress levels, suggesting that the shot peening could introduce a more stable surface layer of compressive residual stress other than the elevated strength of nickel-aluminum bronze alloy.

Towards the prediction of pre-mining stresses in the European continent. [Estimates of vertical and probable maximum lateral stress in Europe

Energy Technology Data Exchange (ETDEWEB)

Blackwood, R. L.

1980-05-15

There are now available sufficient data from in-situ, pre-mining stress measurements to allow a first attempt at predicting the maximum stress magnitudes likely to occur in a given mining context. The sub-horizontal (lateral) stress generally dominates the stress field, becoming critical to stope stability in many cases. For cut-and-fill mining in particular, where developed fill pressures are influenced by lateral displacement of pillars or stope backs, extraction maximization planning by mathematical modelling techniques demands the best available estimate of pre-mining stresses. While field measurements are still essential for this purpose, in the present paper it is suggested that the worst stress case can be predicted for preliminary design or feasibility study purposes. In the Eurpoean continent the vertical component of pre-mining stress may be estimated by adding 2 MPa to the pressure due to overburden weight. The maximum lateral stress likely to be encountered is about 57 MPa at depths of some 800m to 1000m below the surface.

Neutron diffraction measurements of residual stress in additively manufactured stainless steel

International Nuclear Information System (INIS)

Brown, D.W.; Bernardin, J.D.; Carpenter, J.S.; Clausen, B.; Spernjak, D.; Thompson, J.M.

2016-01-01

Charpy test specimens were additively manufactured (AM) on a single stainless steel plate from a 17–4 class stainless steel using a powder-bed, laser melting technique on an EOS M280 direct metal laser sintering (DMLS) machine. Cross-hatched mesh support structures for the Charpy test specimens were varied in strut width and density to parametrically study their influence on the build stability and accuracy as the DMLS process has been known to generate parts with large amounts of residual stress. Neutron diffraction was used to profile the residual stresses in several of the AM samples before and after the samples were removed from the support structure for the purpose of determining residual stresses. The residual stresses were found to depend very little on the properties of the support structure over the limited range studied here. The largest stress component was in the long direction of each of the samples studied and was roughly 2/3 of the yield stress of the material. The stress field was altered considerably when the specimen was removed from the support structure. It was noted in this study that a single Charpy specimen developed a significant tear between the growth plate and support structure. The presence of the tear in the support structure strongly affected the observed stress field: the asymmetric tear resulted in a significantly asymmetric stress field that propagated through removal of the sample from the base plate. The altered final residual stress state of the sample as well as its observed final shape indicates that the tear initiated during the build and developed without disrupting the fabrication process, suggesting a need for in-situ monitoring.

Neutron diffraction measurements of residual stress in additively manufactured stainless steel

Energy Technology Data Exchange (ETDEWEB)

Brown, D.W.; Bernardin, J.D.; Carpenter, J.S.; Clausen, B.; Spernjak, D.; Thompson, J.M.

2016-12-15

Charpy test specimens were additively manufactured (AM) on a single stainless steel plate from a 17–4 class stainless steel using a powder-bed, laser melting technique on an EOS M280 direct metal laser sintering (DMLS) machine. Cross-hatched mesh support structures for the Charpy test specimens were varied in strut width and density to parametrically study their influence on the build stability and accuracy as the DMLS process has been known to generate parts with large amounts of residual stress. Neutron diffraction was used to profile the residual stresses in several of the AM samples before and after the samples were removed from the support structure for the purpose of determining residual stresses. The residual stresses were found to depend very little on the properties of the support structure over the limited range studied here. The largest stress component was in the long direction of each of the samples studied and was roughly 2/3 of the yield stress of the material. The stress field was altered considerably when the specimen was removed from the support structure. It was noted in this study that a single Charpy specimen developed a significant tear between the growth plate and support structure. The presence of the tear in the support structure strongly affected the observed stress field: the asymmetric tear resulted in a significantly asymmetric stress field that propagated through removal of the sample from the base plate. The altered final residual stress state of the sample as well as its observed final shape indicates that the tear initiated during the build and developed without disrupting the fabrication process, suggesting a need for in-situ monitoring.

In situ recording of particle network formation in liquids by ion conductivity measurements.

Science.gov (United States)

Pfaffenhuber, Christian; Sörgel, Seniz; Weichert, Katja; Bele, Marjan; Mundinger, Tabea; Göbel, Marcus; Maier, Joachim

2011-09-21

The formation of fractal silica networks from a colloidal initial state was followed in situ by ion conductivity measurements. The underlying effect is a high interfacial lithium ion conductivity arising when silica particles are brought into contact with Li salt-containing liquid electrolytes. The experimental results were modeled using Monte Carlo simulations and tested using confocal fluorescence laser microscopy and ζ-potential measurements.

Analysis on the Initial Cracking Parameters of Cross-Measure Hydraulic Fracture in Underground Coal Mines

Directory of Open Access Journals (Sweden)

Yiyu Lu

2015-07-01

Full Text Available Initial cracking pressure and locations are important parameters in conducting cross-measure hydraulic fracturing to enhance coal seam permeability in underground coalmines, which are significantly influenced by in-situ stress and occurrence of coal seam. In this study, stress state around cross-measure fracturing boreholes was analyzed using in-situ stress coordinate transformation, then a mathematical model was developed to evaluate initial cracking parameters of borehole assuming the maximum tensile stress criterion. Subsequently, the influences of in-situ stress and occurrence of coal seams on initial cracking pressure and locations in underground coalmines were analyzed using the proposed model. Finally, the proposed model was verified with field test data. The results suggest that the initial cracking pressure increases with the depth cover and coal seam dip angle. However, it decreases with the increase in azimuth of major principle stress. The results also indicate that the initial cracking locations concentrated in the second and fourth quadrant in polar coordinate, and shifted direction to the strike of coal seam as coal seam dip angle and azimuth of maximum principle stress increase. Field investigation revealed consistent rule with the developed model that the initial cracking pressure increases with the coal seam dip angle. Therefore, the proposed mathematical model provides theoretical insight to analyze the initial cracking parameters during cross-measure hydraulic fracturing for underground coalmines.

Estimation of co-seismic stress change of the 2008 Wenchuan Ms8.0 earthquake

Energy Technology Data Exchange (ETDEWEB)

Sun Dongsheng; Wang Hongcai; Ma Yinsheng; Zhou Chunjing [Key laboratory of Neotectonic movement and Geohazard, Ministry of Land and Resources, Beijing 100081 (China) and Institute of Geomechanics, Chinese academy of Geological Sciences, Beijing 100081 (China)

2012-09-26

In-situ stress change near the fault before and after a great earthquake is a key issue in the geosciences field. In this work, based on the 2008 Great Wenchuan earthquake fault slip dislocation model, the co-seismic stress tensor change due to the Wenchuan earthquake and the distribution functions around the Longmen Shan fault are given. Our calculated results are almost consistent with the before and after great Wenchuan earthquake in-situ measuring results. The quantitative assessment results provide a reference for the study of the mechanism of earthquakes.

Measurement of thermal conductivity and diffusivity in situ: Literature survey and theoretical modelling of measurements

Energy Technology Data Exchange (ETDEWEB)

Kukkonen, I.; Suppala, I. [Geological Survey of Finland, Espoo (Finland)

1999-01-01

In situ measurements of thermal conductivity and diffusivity of bedrock were investigated with the aid of a literature survey and theoretical simulations of a measurement system. According to the surveyed literature, in situ methods can be divided into `active` drill hole methods, and `passive` indirect methods utilizing other drill hole measurements together with cutting samples and petrophysical relationships. The most common active drill hole method is a cylindrical heat producing probe whose temperature is registered as a function of time. The temperature response can be calculated and interpreted with the aid of analytical solutions of the cylindrical heat conduction equation, particularly the solution for an infinite perfectly conducting cylindrical probe in a homogeneous medium, and the solution for a line source of heat in a medium. Using both forward and inverse modellings, a theoretical measurement system was analysed with an aim at finding the basic parameters for construction of a practical measurement system. The results indicate that thermal conductivity can be relatively well estimated with borehole measurements, whereas thermal diffusivity is much more sensitive to various disturbing factors, such as thermal contact resistance and variations in probe parameters. In addition, the three-dimensional conduction effects were investigated to find out the magnitude of axial `leak` of heat in long-duration experiments. The radius of influence of a drill hole measurement is mainly dependent on the duration of the experiment. Assuming typical conductivity and diffusivity values of crystalline rocks, the measurement yields information within less than a metre from the drill hole, when the experiment lasts about 24 hours. We propose the following factors to be taken as basic parameters in the construction of a practical measurement system: the probe length 1.5-2 m, heating power 5-20 Wm{sup -1}, temperature recording with 5-7 sensors placed along the probe, and

Measurement of thermal conductivity and diffusivity in situ: Literature survey and theoretical modelling of measurements

International Nuclear Information System (INIS)

Kukkonen, I.; Suppala, I.

1999-01-01

In situ measurements of thermal conductivity and diffusivity of bedrock were investigated with the aid of a literature survey and theoretical simulations of a measurement system. According to the surveyed literature, in situ methods can be divided into 'active' drill hole methods, and 'passive' indirect methods utilizing other drill hole measurements together with cutting samples and petrophysical relationships. The most common active drill hole method is a cylindrical heat producing probe whose temperature is registered as a function of time. The temperature response can be calculated and interpreted with the aid of analytical solutions of the cylindrical heat conduction equation, particularly the solution for an infinite perfectly conducting cylindrical probe in a homogeneous medium, and the solution for a line source of heat in a medium. Using both forward and inverse modellings, a theoretical measurement system was analysed with an aim at finding the basic parameters for construction of a practical measurement system. The results indicate that thermal conductivity can be relatively well estimated with borehole measurements, whereas thermal diffusivity is much more sensitive to various disturbing factors, such as thermal contact resistance and variations in probe parameters. In addition, the three-dimensional conduction effects were investigated to find out the magnitude of axial 'leak' of heat in long-duration experiments. The radius of influence of a drill hole measurement is mainly dependent on the duration of the experiment. Assuming typical conductivity and diffusivity values of crystalline rocks, the measurement yields information within less than a metre from the drill hole, when the experiment lasts about 24 hours. We propose the following factors to be taken as basic parameters in the construction of a practical measurement system: the probe length 1.5-2 m, heating power 5-20 Wm -1 , temperature recording with 5-7 sensors placed along the probe, and

Improved design and in-situ measurements of new beam position monitors for Indus-2

Science.gov (United States)

Kumar, M.; Babbar, L. K.; Holikatti, A. C.; Yadav, S.; Tyagi, Y.; Puntambekar, T. A.; Senecha, V. K.

2018-01-01

Beam position monitors (BPM) are important diagnostic devices used in particle accelerators to monitor position of the beam for various applications. Improved version of button electrode BPM has been designed using CST Studio Suite for Indus-2 ring. The new BPMs are designed to replace old BPMs which were designed and installed more than 12 years back. The improved BPMs have higher transfer impedance, resonance free output signal, equal sensitivity in horizontal and vertical planes and fast decaying wakefield as compared to old BPMs. The new BPMs have been calibrated using coaxial wire method. Measurement of transfer impedance and time domain signals has also been performed in-situ with electron beam during Indus-2 operation. The calibration and beam based measurements results showed close agreement with the design parameters. This paper presents design, electromagnetic simulations, calibration result and in-situ beam based measurements of newly designed BPMs.

Residual stress measurement in veneering ceramic by hole-drilling.

Science.gov (United States)

Mainjot, Amélie K; Schajer, Gary S; Vanheusden, Alain J; Sadoun, Michaël J

2011-05-01

Mismatch in thermal expansion properties between veneering ceramic and metallic or high-strength ceramic cores can induce residual stresses and initiate cracks when combined with functional stresses. Knowledge of the stress distribution within the veneering ceramic is a key factor for understanding and predicting chipping failures, which are well-known problems with Yttria-tetragonal-zirconia-polycrystal based fixed partial dentures. The objectives of this study are to develop a method for measuring the stress profile in veneering ceramics and to compare ceramic-fused-to-metal compounds to veneered Yttria-tetragonal-zirconia-polycrystal ceramic. The hole-drilling method, often used for engineering measurements, was adapted for use with veneering ceramic. Because of the high sensitivity needed in comparison with industrial applications, a high sensitivity electrical measurement chain was developed. All samples exhibited the same type of stress vs. depth profile, starting with compressive at the ceramic surface, decreasing with depth and becoming tensile at 0.5-1.0mm from the surface, and then becoming slightly compressive again. The zirconia samples exhibited a stress depth profile of larger magnitude. The hole drilling method was shown be a practical tool for measuring residual stresses in veneering ceramics. Copyright © 2010 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Accuracy of soil stress measurements as affected by transducer dimensions and shape

DEFF Research Database (Denmark)

Lamandé, Mathieu; Keller, Thomas; Berisso, Feto Esimo

2015-01-01

Accurate measurements of soil stress are needed to evaluate the impact of traffic on soil properties and prevent soil compaction. Four types of transducer commonly used to measure vertical stress were calibrated in realistic traffic conditions in the field. The four transducer types differed...... in shape and dimensions, which are important factors influencing stress. Deviation of measured stress from true stress ranged from 15% underestimation to 18% overestimation, with transducer thickness to width ratio being the most important shape factor influencing the stress recorded. Changes in physical...... conditions in the soil above the transducers due to their installation did not influence the accuracy of vertical stress measurements. The results of this calibration are valid for correcting stress measurements in topsoil, but should be used with caution for vertical stress measurements in subsoil. All...

Airborne remote sensing and in situ measurements of atmospheric CO2 to quantify point source emissions

Science.gov (United States)

Krings, Thomas; Neininger, Bruno; Gerilowski, Konstantin; Krautwurst, Sven; Buchwitz, Michael; Burrows, John P.; Lindemann, Carsten; Ruhtz, Thomas; Schüttemeyer, Dirk; Bovensmann, Heinrich

2018-02-01

Reliable techniques to infer greenhouse gas emission rates from localised sources require accurate measurement and inversion approaches. In this study airborne remote sensing observations of CO2 by the MAMAP instrument and airborne in situ measurements are used to infer emission estimates of carbon dioxide released from a cluster of coal-fired power plants. The study area is complex due to sources being located in close proximity and overlapping associated carbon dioxide plumes. For the analysis of in situ data, a mass balance approach is described and applied, whereas for the remote sensing observations an inverse Gaussian plume model is used in addition to a mass balance technique. A comparison between methods shows that results for all methods agree within 10 % or better with uncertainties of 10 to 30 % for cases in which in situ measurements were made for the complete vertical plume extent. The computed emissions for individual power plants are in agreement with results derived from emission factors and energy production data for the time of the overflight.

In Situ Acoustic Monitoring of Thermal Spray Process Using High-Frequency Impulse Measurements

Science.gov (United States)

Tillmann, Wolfgang; Walther, Frank; Luo, Weifeng; Haack, Matthias; Nellesen, Jens; Knyazeva, Marina

2018-01-01

In order to guarantee their protective function, thermal spray coatings must be free from cracks, which expose the substrate surface to, e.g., corrosive media. Cracks in thermal spray coatings are usually formed because of tensile residual stresses. Most commonly, the crack occurrence is determined after the thermal spraying process by examination of metallographic cross sections of the coating. Recent efforts focus on in situ monitoring of crack formation by means of acoustic emission analysis. However, the acoustic signals related to crack propagation can be absorbed by the noise of the thermal spraying process. In this work, a high-frequency impulse measurement technique was applied to separate different acoustic sources by visualizing the characteristic signal of crack formation via quasi-real-time Fourier analysis. The investigations were carried out on a twin wire arc spraying process, utilizing FeCrBSi as a coating material. The impact of the process parameters on the acoustic emission spectrum was studied. Acoustic emission analysis enables to obtain global and integral information on the formed cracks. The coating morphology and coating defects were inspected using light microscopy on metallographic cross sections. Additionally, the resulting crack patterns were imaged in 3D by means of x-ray microtomography.

In situ prompt gamma-ray measurement of river water salinity in northern Taiwan using HPGe-252Cf probe

International Nuclear Information System (INIS)

Jiunnhsing Chao; Chien Chung

1991-01-01

A portable HPGe- 252 Cf probe dedicated to in situ survey of river water salinity was placed on board a fishing boat to survey the Tamsui River in northern Taiwan. The variation of water salinity is surveyed by measuring the 6111 keV chlorine prompt photopeak along the river. Results indicate that the probe can be used as a salinometer for rapid, in situ measurement in polluted rivers or sea. (author)

Utilizing The Synergy of Airborne Backscatter Lidar and In-Situ Measurements for Evaluating CALIPSO

Directory of Open Access Journals (Sweden)

Tsekeri Alexandra

2016-01-01

Full Text Available Airborne campaigns dedicated to satellite validation are crucial for the effective global aerosol monitoring. CALIPSO is currently the only active remote sensing satellite mission, acquiring the vertical profiles of the aerosol backscatter and extinction coefficients. Here we present a method for CALIPSO evaluation from combining lidar and in-situ airborne measurements. The limitations of the method have to do mainly with the in-situ instrumentation capabilities and the hydration modelling. We also discuss the future implementation of our method in the ICE-D campaign (Cape Verde, August 2015.

A study of x-ray microbeam stress measurement for local area

International Nuclear Information System (INIS)

Natsume, Yoshitaka; Miyakawa, Susumu

1987-01-01

A new type X-ray microbeam equipment which is capable of three-dimensional oscillation at an X-ray radiation position was used to measure the residual stress of pure iron powder and bending plate specimens as well as that in the vicinity of fatigue crack tip of 1/2 CT specimen. The results obtained are summerized as follows. (1) Diffraction profiles of pure iron powder with diameter 0.02 ∼ 0.03 μm particle size obtained by the present microbeam technique in the beam area of 80 μm in diamether and measuring time more than 800 sec showed Kα 1 and Kα 2 peaks clearly, so that these profiles are good enough for stress measurement. (2) The measured stress of pure iron powder with diameter 10 ∼ 25 μm particle size in the beam area of 80 μm in diameter was not equal to 0 MPa. The measured stress varied greatly and was independent of measuring time. (3) The measured stress of pure iron powder with diameter 0.02 ∼ 0.03 μm particle size in the beam area of 80 μm in diameter was almost 1 MPa, which shows the good accuracy of this X-ray micro-beam equipment. (4) The relation between the X-ray measured stress and the mechanically applied stress showed good agreement. (5) The distribution of residual stress at the vicinity of fatigue crack tip showed that the residual stress at the fatigue crack tip was compression and the residual stress in front of crack tip was tension. This tensile residual stress in front of crack tip existed in the area from 0.02 mm to 2 mm. (6) The above results show that the present equipment is advantageous in the investigation of local stress, shortening the measuring time without sacrificing the accuracy. (author)

Methods for FEM stress initialization based on stress functions, and application to a reservoir cross-section

OpenAIRE

Aliguer Piferrer, Ignasi; Rafels Ybern, Carles; Jaqués Adell, Irene; Carol, Ignacio; Prat Catalán, Pere; Lakashmikhanta, Ramasesha; Segura Segarra, José María

2013-01-01

An accurate description of the in-situ stress field in a rock mass is crucial in different areas of geo-engineering such as: underground excavations, hydrocarbon extraction, CO2 storage, hydraulic fracture etc. In this paper, a novel methodology to numerically generate the in-situ stress state within the Finite Elements framework is presented. It involves two steps: 1) an estimate of the stress components is given for integration point of the discretization, and 2) global equilibrium is verif...

In situ measurement of erosion/deposition in the DIII-D divertor by colorimetry

International Nuclear Information System (INIS)

Weschenfelder, F.; Wienhold, P.; Winter, J.

1996-01-01

Colorimetry was introduced into the DIII-D tokamak to measure in situ the growth and erosion of transparent wall coatings (a-C:H) on the divertor. The colorimetric measurement system consisting of a halogen light source, a set of three filters and a black/white camera is described together with a first erosion measurement. An insertable graphite sample with a diameter of 4.7 cm was precoated with a 300 nm thick amorphous carbon film and was exposed in the divertor for several discharges with its surface coplanar to the surrounding graphite tiles. For each of the discharges the plasma strike point was moved onto the sample for 1 s to erode the coating. Between the discharges a camera signal with each filter was recorded and the film thickness was evaluated along a radial line across the DIMES sample. Thus it has been possible for the first time to measure erosion and deposition of divertor material in situ and shot-by-shot. The average peak heat flux with the strike point on DIMES was about 110 W cm -2 . The measurement shows a strong decrease in the film thickness almost over the entire sample with an average erosion rate of ∼ 9 nm s -1 . (Author)

Interactions between the phase stress and the grain-orientation-dependent stress in duplex stainless steel during deformation

International Nuclear Information System (INIS)

Jia, N.; Peng, R. Lin; Wang, Y.D.; Chai, G.C.; Johansson, S.; Wang, G.; Liaw, P.K.

2006-01-01

The development of phase stress and grain-orientation-dependent stress under uniaxial compression was investigated in a duplex stainless steel consisting of austenite and ferrite. Using in situ neutron diffraction measurements, the strain response of several h k l planes to the applied compressive stress was mapped as a function of applied stress and sample direction. Analysis based on the experimental results and elastoplastic self-consistent simulations shows that phase stresses of thermal origin further increase during elastic loading but decrease with increased plastic deformation. Grain-orientation-dependent stresses become significant in both austenite and ferrite after loading into the plastic region. After unloading from the plastic regime, a considerable intergranular stress remains in the austenitic phase and dominates over the phase stress. This study provides fundamental experimental inputs for future micromechanical modeling aiming at the evaluation and prediction of the mechanical performance of multiphase materials

Validity and reliability of in-situ air conduction thresholds measured through hearing aids coupled to closed and open instant-fit tips.

Science.gov (United States)

O'Brien, Anna; Keidser, Gitte; Yeend, Ingrid; Hartley, Lisa; Dillon, Harvey

2010-12-01

Audiometric measurements through a hearing aid ('in-situ') may facilitate provision of hearing services where these are limited. This study investigated the validity and reliability of in-situ air conduction hearing thresholds measured with closed and open domes relative to thresholds measured with insert earphones, and explored sources of variability in the measures. Twenty-four adults with sensorineural hearing impairment attended two sessions in which thresholds and real-ear-to-dial-difference (REDD) values were measured. Without correction, significantly higher low-frequency thresholds in dB HL were measured in-situ than with insert earphones. Differences were due predominantly to differences in ear canal SPL, as measured with the REDD, which were attributed to leaking low-frequency energy. Test-retest data yielded higher variability with the closed dome coupling due to inconsistent seals achieved with this tip. For all three conditions, inter-participant variability in the REDD values was greater than intra-participant variability. Overall, in-situ audiometry is as valid and reliable as conventional audiometry provided appropriate REDD corrections are made and ambient sound in the test environment is controlled.

Mean wall-shear stress measurements using the micro-pillar shear-stress sensor MPS3

International Nuclear Information System (INIS)

Große, S; Schröder, W

2008-01-01

A new sensor to measure the mean turbulent wall-shear stress in turbulent flows is described. The wall-shear stress sensor MPS 3 has been tested in a well-defined fully developed turbulent pipe flow at Reynolds numbers Re b based on the bulk velocity U b and the pipe diameter D in the range of Re b = 10 000–20 000. The results demonstrate a convincing agreement of the mean wall-shear stress obtained with the new sensor technique with analytical and experimental results from the literature. The sensor device consists of a flexible micro-pillar that extends from the wall into the viscous sublayer. Bending due to the exerting fluid forces, the pillar-tip deflection serves as a measure for the local wall-shear stress. The sensor concept, calibration techniques, the achievable accuracy and error estimates, the fields of application and the sensor limits will be discussed. Furthermore, a first estimate of the pillar dynamic response will be derived showing the potential of the sensor to also measure the turbulent fluctuating wall-shear stress

Development of a stress sensor based on the piezoelectric lead zirconate titanate for impact stress measurement

Science.gov (United States)

Liu, Yiming; Xu, Bin; Li, Lifei; Li, Bing

2012-04-01

The measurement of stress of concrete structures under impact loading and other strong dynamic loadings is crucial for the monitoring of health and damage detection. Due to its main advantages including availability, extremely high rigidity, high natural frequency, wide measuring range, high stability, high reproducibility, high linearity and wide operating temperature range, piezoelectric (Lead Zirconate Titanate, PZT) ceramic materials has been a widely used smart material for both sensing and actuation for monitoring and control in engineering structures. In this paper, a kind of stress sensor based on piezoelectric ceramics for impact stress measuring of concrete structures is developed. Because the PZT is fragile, in order to employ it for the health monitoring of concrete structures, special handling and treatment should be taken to protect the PZT and to make it survive and work properly in concrete. The commercially available PZT patch with lead wires is first applied with an insulation coating to prevent water and moisture damage, and then is packaged by jacketing it by two small precasted cylinder concrete blocks with enough strength to form a smart aggregate (SA). The employed PZT patch has a dimension of 10mm x 10mm x 0.3mm. In order to calibrate the PZT based stress sensor for impact stress measuring, a dropping hammer was designed and calibration test on the sensitivity of the proposed transducer was carried out with an industry charge amplifier. The voltage output of the stress sensor and the impact force under different free falling heights and impact mass were recorded with a high sampling rate data acquisition system. Based on the test measurements, the sensibility of the PZT based stress sensor was determined. Results show that the output of the PZT based stress sensor is proportional to the stress level and the repeatability of the measurement is very good. The self-made piezoelectric stress sensor can be easily embedded in concrete and provide

Applications of in situ optical measurements in ecological and biogeochemical studies - a framework for a user-driven national network

Science.gov (United States)

Bergamaschi, B. A.; Pellerin, B. A.; Downing, B. D.; Saraceno, J.; Aiken, G.; Stumpner, P.

2010-12-01

A critical challenge for understanding the dynamics between water quality, and ecological processes is obtaining data at time scales in which changes occur. Traditional, discrete sampling, approaches for data collection are often limited by analytical and field costs, site access, and logistical challenges, for long-term sampling at a large number of sites. The timescales of change, however, are often minutes, hours, or years. In situ optical (absorbance and fluorescence) instruments offer opportunities to help overcome these difficulties by directly or indirectly measuring constituents of interest. In situ optical instrumentation have been in use in oceanographic studies for well over 50 years, and as advances in the science, engineering and technology of these sensors have improved, optical sensors have become more commercially viable and available for research. We present several examples that highlight applications of in situ optical measurements for understanding dynamics in stream, river, and estuary systems. Examples illustrate the utility of in situ optical sensors for studies over short-duration events of days to weeks (diurnal cycles, tidal cycles, storm events and snowmelt periods) as well as longer-term continuous monitoring for months to years. We also highlight applied in situ optical measurements as proxies for constituents that are difficult and expensive to measure at high spatiotemporal resolution, for example, dissolved organic carbon, dissolved organic nitrogen, mercury and methylmercury, trihalomethane precursors, harmful algal blooms, and others. We propose that relatively simple absorbance and fluorescence measurements made in situ could be incorporated into short and long-term ecological research and monitoring programs, resulting in advanced understanding of sources that contribute to water quality improvements or degradation, contaminant and carbon cycling, and the occurrence and persistence of harmful algal blooms. Linking these efforts

Horonobe underground research laboratory project. The plan for the in-situ experiments in Phase 2 and Phase 3 in/around URL

International Nuclear Information System (INIS)

Matsui, Hiroya

2005-09-01

This report describes for preliminary research plan in Phase 2 and Phase 3 taken into consideration of expected geological environment at location of URL based on the results of the investigations until FY 2003/2004. Duration of construction phase and total cost are considered as important factors for planning as well. The below items are planned for in-situ experiments in Phase 2 and Phase 3 in/around URL are planning. Phase 2. (In-situ experiments for understanding of geological environment) Geological survey at tunnel. Inflow measurement in shafts. Water pressure monitoring and groundwater sampling around shafts during excavation of URL. Investigation for EDZ around shafts. Stress measurement on support. Detail investigations for geological environment around drifts. Excavation disturbance experiment in a drift. Investigation for desaturation zone and REDOX condition around drifts. (Engineered barrier system) In-situ experiment on low-alkali concrete. In-situ experiment for gas migration in engineering barrier system. Phase 3. (In-situ experiments for understanding of geological environment) EDZ experiment for stress interference. Investigation of long-term behavior of EDZ around drifts. Detail investigation on fault/fault zone. Monitoring for the change of geological environment at earthquake. Backfill test in boreholes. (Engineered barrier system) T-H-M-C experiment. In-situ experiment for corrosion of overpack. Investigation of the influence of a concrete to engineering barrier system and geological environment. In-situ experiment for interference between backfill material and geological environment. Backfill test in a drift. (Safety assessment) Tracer tests in engineering barrier system, natural barrier and fault/fault zone. (author)

Flexible Micropost Arrays for Shear Stress Measurement

Science.gov (United States)

Wohl, Christopher J.; Palmieri, Frank L.; Hopkins, John W.; Jackson, Allen M.; Connell, John W.; Lin, Yi; Cisotto, Alexxandra A.

2015-01-01

Increased fuel costs, heightened environmental protection requirements, and noise abatement continue to place drag reduction at the forefront of aerospace research priorities. Unfortunately, shortfalls still exist in the fundamental understanding of boundary-layer airflow over aerodynamic surfaces, especially regarding drag arising from skin friction. For example, there is insufficient availability of instrumentation to adequately characterize complex flows with strong pressure gradients, heat transfer, wall mass flux, three-dimensionality, separation, shock waves, and transient phenomena. One example is the acoustic liner efficacy on aircraft engine nacelle walls. Active measurement of shear stress in boundary layer airflow would enable a better understanding of how aircraft structure and flight dynamics affect skin friction. Current shear stress measurement techniques suffer from reliability, complexity, and airflow disruption, thereby compromising resultant shear stress data. The state-of-the-art for shear stress sensing uses indirect or direct measurement techniques. Indirect measurements (e.g., hot-wire, heat flux gages, oil interferometry, laser Doppler anemometry, small scale pressure drag surfaces, i.e., fences) require intricate knowledge of the studied flow, restrictive instrument arrangements, large surface areas, flow disruption, or seeding material; with smaller, higher bandwidth probes under development. Direct measurements involve strain displacement of a sensor element and require no prior knowledge of the flow. Unfortunately, conventional "floating" recessed components for direct measurements are mm to cm in size. Whispering gallery mode devices and Fiber Bragg Gratings are examples of recent additions to this type of sensor with much smaller (?m) sensor components. Direct detection techniques are often single point measurements and difficult to calibrate and implement in wind tunnel experiments. In addition, the wiring, packaging, and installation

In-situ measurement of the electrical conductivity of aluminum oxide in HFIR

Energy Technology Data Exchange (ETDEWEB)

Zinkle, S.J.; White, D.P.; Snead, L.L. [Oak Ridge National Lab., TN (United States)] [and others

1996-10-01

A collaborative DOE/Monbusho irradiation experiment has been completed which measured the in-situ electrical resistivity of 12 different grades of aluminum oxide during HFIR neutron irradiation at 450{degrees}C. No evidence for bulk RIED was observed following irradiation to a maximum dose of 3 dpa with an applied dc electric field of 200 V/mm.

Temperature profiles by ground-based remote sensing and in situ measurements

Energy Technology Data Exchange (ETDEWEB)

Argentini, S; Pietroni, I; Conidi, A; Mastrantonio, G; Petenko, I; Viola, A [ISAC-CNR, Via del Fosso del Cavaliere, 100, 00133 Roma (Italy); Gariazzo, C; Pelliccioni, A; Amicarelli, A [ISPESL Dipartimento Insediamenti Produttivi e Interazione con l' Ambiente, Via Fontana Candida, 1, 00040 Monteporzio Catone (RM) (Italy)], E-mail: s.argentini@isac.cnr.it

2008-05-01

This study focuses on the accuracy of the temperature profiles measured with a Doppler Radio-Acoustic Sounding System and a Microwave Temperature Profiler during a period of about 3 months in winter 2007-2008. The experiment was carried on at the experimental facility of the Institute of Atmospheric Sciences and Climate (ISAC) of the Italian National Research Council (CNR). The temperature data measured with remote sensors were verified with in situ measurements on a mast as well as with tethered balloon data. The facsimile echograms obtained with the ISAC Doppler SODAR were analysed to understand to which extent the RASS and Radiometer temperature profiles behaviour can represent the real thermal structure of the atmosphere.

Temperature profiles by ground-based remote sensing and in situ measurements

International Nuclear Information System (INIS)

Argentini, S; Pietroni, I; Conidi, A; Mastrantonio, G; Petenko, I; Viola, A; Gariazzo, C; Pelliccioni, A; Amicarelli, A

2008-01-01

This study focuses on the accuracy of the temperature profiles measured with a Doppler Radio-Acoustic Sounding System and a Microwave Temperature Profiler during a period of about 3 months in winter 2007-2008. The experiment was carried on at the experimental facility of the Institute of Atmospheric Sciences and Climate (ISAC) of the Italian National Research Council (CNR). The temperature data measured with remote sensors were verified with in situ measurements on a mast as well as with tethered balloon data. The facsimile echograms obtained with the ISAC Doppler SODAR were analysed to understand to which extent the RASS and Radiometer temperature profiles behaviour can represent the real thermal structure of the atmosphere

In situ and postradiation analysis of mechanical stress in Al{sub 2}O{sub 3}:Cr induced by swift heavy-ion irradiation

Energy Technology Data Exchange (ETDEWEB)

Skuratov, V.A., E-mail: skuratov@jinr.r [Joint Institute for Nuclear Research, Dubna 141980 (Russian Federation); Bujnarowski, G. [Institute of Physics, Opole University, 45-052 Opole (Poland); Kovalev, Yu.S. [Joint Institute for Nuclear Research, Dubna 141980 (Russian Federation); O' Connell, J. [Nelson Mandela Metropolitan University, Port Elizabeth (South Africa); Havanscak, K. [Eoetvoes University, Pazmany P. setany 1/A, H-1117 Budapest (Hungary)

2010-10-01

Optical spectroscopy and TEM techniques have been applied to study the radiation damage and correlated mechanical stresses in Al{sub 2}O{sub 3} and Al{sub 2}O{sub 3}:Cr single crystals induced by (1-3) MeV/amu Kr, Xe and Bi ion irradiation. Mechanical stresses were evaluated in situ using a piezospectroscopic effect through the shift of the respective lines in ionoluminescence spectra. It was found that dose dependence of the stress level for Xe and Bi ions, when ionization energy loss exceeds the threshold of damage formation via electronic excitations, exhibits several alternate stages showing the build-up and relaxation of stresses. The beginning of relaxation stages is observed at fluences associated with beginning of individual ion track regions overlapping. The residual stress profiles through the ion irradiated layers were deduced from depth-resolved photostimulated spectra using laser confocal scanning microscopy set-up. It was determined that stresses are compressive in basal plane and tensile in perpendicular direction in all samples irradiated with high energy ions.

Comparison of ambient aerosol extinction coefficients obtained from in-situ, MAX-DOAS and LIDAR measurements at Cabauw

Directory of Open Access Journals (Sweden)

P. Zieger

2011-03-01

Full Text Available In the field, aerosol in-situ measurements are often performed under dry conditions (relative humidity RH<30–40%. Since ambient aerosol particles experience hygroscopic growth at enhanced RH, their microphysical and optical properties – especially the aerosol light scattering – are also strongly dependent on RH. The knowledge of this RH effect is of crucial importance for climate forcing calculations or for the comparison of remote sensing with in-situ measurements. Here, we will present results from a four-month campaign which took place in summer 2009 in Cabauw, The Netherlands. The aerosol scattering coefficient σ_sp(λ was measured dry and at various, predefined RH conditions between 20 and 95% with a humidified nephelometer. The scattering enhancement factor f(RH,λ is the key parameter to describe the effect of RH on σ_sp(λ and is defined as σ_sp(RH,λ measured at a certain RH divided by the dry σ_sp(dry,λ. The measurement of f(RH,λ together with the dry absorption measurement (assumed not to change with RH allows the determination of the actual extinction coefficient σ_ep(RH,λ at ambient RH. In addition, a wide range of other aerosol properties were measured in parallel. The measurements were used to characterize the effects of RH on the aerosol optical properties. A closure study showed the consistency of the aerosol in-situ measurements. Due to the large variability of air mass origin (and thus aerosol composition a simple parameterization of f(RH,λ could not be established. If f(RH,λ needs to be predicted, the chemical composition and size distribution need to be known. Measurements of four MAX-DOAS (multi-axis differential optical absorption spectroscopy instruments were used to retrieve vertical profiles of σ_ep(λ. The values of the lowest layer were compared to the in-situ values after conversion of the latter ones to ambient

In situ thermal residual stress evolution in ultrathin ZnO and Ag films studied by synchrotron x-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Renault, P.O., E-mail: Pierre.olivier.renault@univ-poitiers.fr [Institut P' , CNRS, Universite de Poitiers, UPR 3346, 86962 Futuroscope (France); Krauss, C.; Le Bourhis, E.; Geandier, G. [Institut P' , CNRS, Universite de Poitiers, UPR 3346, 86962 Futuroscope (France); Benedetto, A. [Saint-Gobain Recherche (SGR), 93303 Aubervilliers (France); Grachev, S.Y.; Barthel, E. [Lab. Surface du Verre et Interfaces (SVI), UMR-CNRS 125, 93303 Aubervilliers (France)

2011-12-30

Residual-stress evolution in sputtered encapsulated ZnO/Ag/ZnO stack has been studied in-situ by synchrotron x-ray diffraction when heat treated. The ZnO/Ag/ZnO stack encapsulated into Si{sub 3}N{sub 4} layers and deposited on (001) Si substrates was thermally heated from 25 Degree-Sign C to 600 Degree-Sign C and cooled down to 25 Degree-Sign C. X-ray diffraction 2D patterns captured continuously during the heat treatment allowed monitoring the diffraction peak shifts of both Ag (15 nm thick) and ZnO (10 nm and 50 nm thick) sublayers. Due to the mismatch between the coefficients of thermal expansion, the silicon substrate induced compressive thermal stresses in the films during heating. We first observed a linear increase of the compressive stress state in both Ag and ZnO films and then a more complex elastic-stress evolution starts to operate from about 100 Degree-Sign C for Ag and about 250 Degree-Sign C for ZnO. Thermal contraction upon cooling seems to dominate so that the initial compressive film stresses relax by about 300 and 700 MPa after thermal treatment for ZnO and Ag, respectively. The overall behavior is discussed in terms of structural changes induced by the heat treatment.

In situ measurements of dose rates from terrestrial gamma rays

International Nuclear Information System (INIS)

Horng, M.C.; Jiang, S.H.

2002-01-01

A portable, high purity germanium (HPGe) detector was employed for the performance of in situ measurements of radionuclide activity concentrations in the ground in Taiwan, at altitudes ranging from sea level to 3900 m. The absolute peak efficiency of the HPGe detector for a gamma-ray source uniformly distributed in the semi-infinite ground was determined using a semi-empirical method. The gamma-ray dose rates from terrestrial radionuclides were calculated from the measured activity levels using recently published dose rate conversion factors. The absorbed dose rate in air due to cosmic rays was derived by subtracting the terrestrial gamma-ray dose rate from the overall absorbed dose rate in air measured using a high-pressure ionization chamber. The cosmic-ray dose rate calculated as a function of altitude, was found to be in good agreement with the data reported by UNSCEAR. (orig.)

In situ optoacoustic measurement of the pointing stability of femtosecond laser beams

Science.gov (United States)

Pushkarev, D.; Mitina, E.; Uryupina, D.; Volkov, R.; Karabytov, A.; Savel'ev, A.

2018-02-01

A new method for the in situ acoustic measurement of the beam pointing stability (BPS) of powerful pulsed lasers is tested. A broadband (~6 MHz) piezoelectric transducer placed a few millimeters from the laser spark produces an electric pulse. We show that variation in time of the position of this pulse can be used to assess the BPS down to 1 µrad in a few hundred laser shots. The estimated value coincides well with the BPS estimated using standard measurement in the far field.

The Force of Crystallization and Fracture Propagation during In-Situ Carbonation of Peridotite

Directory of Open Access Journals (Sweden)

Reinier van Noort

2017-10-01

Full Text Available Subsurface mineralization of CO2 by injection into (hydro-fractured peridotites has been proposed as a carbon sequestration method. It is envisaged that the expansion in solid volume associated with the mineralization reaction leads to a build-up of stress, resulting in the opening of further fractures. We performed CO2-mineralization experiments on simulated fractures in peridotite materials under confined, hydrothermal conditions, to directly measure the induced stresses. Only one of these experiments resulted in the development of a stress, which was less than 5% of the theoretical maximum. We also performed one method control test in which we measured stress development during the hydration of MgO. Based on microstructural observations, as well as XRD and TGA measurements, we infer that, due to pore clogging and grain boundary healing at growing mineral interfaces, the transport of CO2, water and solutes into these sites inhibited reaction-related stress development. When grain boundary healing was impeded by the precipitation of silica, a small stress did develop. This implies that when applied to in-situ CO2-storage, the mineralization reaction will be limited by transport through clogged fractures, and proceed at a rate that is likely too slow for the process to accommodate the volumes of CO2 expected for sequestration.

Molecular force sensors to measure stress in cells

International Nuclear Information System (INIS)

Prabhune, Meenakshi; Rehfeldt, Florian; Schmidt, Christoph F

2017-01-01

Molecularly generated forces are essential for most activities of biological cells, but also for the maintenance of steady state or homeostasis. To quantitatively understand cellular dynamics in migration, division, or mechanically guided differentiation, it will be important to exactly measure stress fields within the cell and the extracellular matrix. Traction force microscopy and related techniques have been established to determine the stress transmitted from adherent cells to their substrates. However, different approaches are needed to directly assess the stress generated inside the cell. This has recently led to the development of novel molecular force sensors. In this topical review, we briefly mention methods used to measure cell-external forces, and then summarize and explain different designs for the measurement of cell-internal forces with their respective advantages and disadvantages. (topical review)

In situ surface roughness measurement using a laser scattering method

Science.gov (United States)

Tay, C. J.; Wang, S. H.; Quan, C.; Shang, H. M.

2003-03-01

In this paper, the design and development of an optical probe for in situ measurement of surface roughness are discussed. Based on this light scattering principle, the probe which consists of a laser diode, measuring lens and a linear photodiode array, is designed to capture the scattered light from a test surface with a relatively large scattering angle ϕ (=28°). This capability increases the measuring range and enhances repeatability of the results. The coaxial arrangement that incorporates a dual-laser beam and a constant compressed air stream renders the proposed system insensitive to movement or vibration of the test surface as well as surface conditions. Tests were conducted on workpieces which were mounted on a turning machine that operates with different cutting speeds. Test specimens which underwent different machining processes and of different surface finish were also studied. The results obtained demonstrate the feasibility of surface roughness measurement using the proposed method.

Stress/strain characteristics of Cu alloy sheath in situ processed MgB2 superconducting wires

International Nuclear Information System (INIS)

Katagiri, Kazumune; Kasaba, Koichi; Shoji, Yoshitaka

2005-01-01

The mechanical properties of copper and copper alloy (Cu-Zr, Cu-Be and Cu-Cr) sheath in situ PIT-processed MgB 2 superconducting wires were studied at room temperature (RT) and 4.2 K. The effects of stress-strain on the critical current (I c ) of the wires have also been studied at 4.2 K and in magnetic fields up to 5 T. It has been clarified that alloying the Cu sheath significantly increases the yield and flow stresses of the wires at both RT and 4.2 K. The 0.5% flow stresses of the Cu alloy sheath wire were 147-237 MPa, whereas that of Cu was 55 MPa. At RT, serration corresponding to multiple cracking was observed around a strain of 0.4% and the stress-strain curves saturated beyond that point. The strain dependence of I c prior to the critical strain (ε irr ) was different depending on the magnetic field; being almost constant at 2 T and increasing with strain at 5 T. The I c decreased beyond ε irr , which is much larger for Cu alloy sheath wires as compared to Cu sheath wire. This is due to the difference in the residual compressive strain in the MgB 2 core during cooling from the heat-treatment temperature to 4.2 K, which is determined through relaxation by yielding in the sheath materials. The transverse compression tests revealed that the I c of the Cu alloy sheath wire did not degrade up to 314 MPa, which is also higher than that of Cu sheath wire. (author)

In-situ real time measurements of net erosion rates of copper during hydrogen plasma exposure

Science.gov (United States)

Kesler, Leigh; Wright, Graham; Peterson, Ethan; Whyte, Dennis

2013-10-01

In order to properly understand the dynamics of net erosion/deposition in fusion reactors, such as tokamaks, a diagnostic measuring the real time rates of net erosion/deposition during plasma exposure is necessary. The DIONISOS experiment produces real time measurements of net erosion/deposition by using Rutherford backscattering spectroscopy (RBS) ion beam analysis simultaneously with plasma exposure from a helicon plasma source. This in-situ method improves on ex-situ weight loss measurements by allowing measurement of possible synergistic effects of high ion implantation rates and net erosion rate and by giving a real time response to changes in plasma parameters. Previous work has validated this new technique for measuring copper (Cu) erosion from helium (He) plasma ion bombardment. This technique is now extended to measure copper erosion due to deuterium and hydrogen plasma ion exposure. Targets used were a 1.5 μm Cu layer on an aluminum substrate. Cu layer thickness is tracked in real time using 1.2 MeV proton RBS. Measured erosion rates will be compared to results from literature and He erosion rates. Supported by US DoE award DE-SC00-02060.

A microscopy approach for in situ inspection of micro-coordinate measurement machine styli for contamination

Science.gov (United States)

Feng, Xiaobing; Pascal, Jonathan; Lawes, Simon

2017-09-01

During the process of measurement using a micro-coordinate measurement machine (µCMM) contamination gradually builds up on the surface of the stylus tip and affects the dimensional accuracy of the measurement. Regular inspection of the stylus for contamination is essential to determine the appropriate cleaning interval and prevent the dimensional error from becoming significant. However, in situ inspection of a µCMM stylus is challenging due to the size, spherical shape, material and surface properties of a typical stylus. To address this challenge, this study evaluates several non-contact measurement technologies for in situ stylus inspection and, based on those findings, proposes a cost-effective microscopy approach. The operational principle is then demonstrated by an automated prototype, coordinated directly by the CMM software MCOSMOS, with an effective threshold of detection as low as 400 nm and a large field of view and depth of field. The level of contamination on the stylus has been found to increase steadily with the number of measurement contacts made. Once excessive contamination is detected on the stylus, measurement should be stopped and a stylus cleaning procedure should be performed to avoid affecting measurement accuracy.

A microscopy approach for in situ inspection of micro-coordinate measurement machine styli for contamination

International Nuclear Information System (INIS)

Feng, Xiaobing; Lawes, Simon; Pascal, Jonathan

2017-01-01

During the process of measurement using a micro-coordinate measurement machine (µCMM) contamination gradually builds up on the surface of the stylus tip and affects the dimensional accuracy of the measurement. Regular inspection of the stylus for contamination is essential to determine the appropriate cleaning interval and prevent the dimensional error from becoming significant. However, in situ inspection of a µCMM stylus is challenging due to the size, spherical shape, material and surface properties of a typical stylus. To address this challenge, this study evaluates several non-contact measurement technologies for in situ stylus inspection and, based on those findings, proposes a cost-effective microscopy approach. The operational principle is then demonstrated by an automated prototype, coordinated directly by the CMM software MCOSMOS, with an effective threshold of detection as low as 400 nm and a large field of view and depth of field. The level of contamination on the stylus has been found to increase steadily with the number of measurement contacts made. Once excessive contamination is detected on the stylus, measurement should be stopped and a stylus cleaning procedure should be performed to avoid affecting measurement accuracy. (paper)

Determination of three-dimensional stress orientations in the Wenchuan earthquake Fault Scientific Drilling (WFSD) hole-1: A preliminary result by anelastic strain recovery measurements of core samples

Science.gov (United States)

Cui, J.; Lin, W.; Wang, L.; Tang, Z.; Sun, D.; Gao, L.; Wang, W.

2010-12-01

A great and destructive earthquake (Ms 8.0; Mw 7.9), Wunchuan earthquake struck on the Longmen Shan foreland trust zone in Sichuan province, China on 12 May 2008 (Xu et al., 2008; Episodes, Vol.31, pp.291-301). As a rapid response scientific drilling project, Wenchuan earthquake Fault Scientific Drilling (WFSD) started on 6 November 2008 shorter than a half of year from the date of earthquake main shock. The first pilot borehole (hole-1) has been drilled to the target depth (measured depth 1201 m MD, vertical depth 1179 m) at Hongkou, Dujianyan, Sichuan and passed through the main fault of the earthquake around 589 m MD. We are trying to determine three dimensional in-situ stress states in the WFSD boreholes by a core-based method, anelastic strain recovery (ASR) method (Lin et al., 2006; Tectonophysics, Vol4.26, pp.221-238). This method has been applied in several scientific drilling projects (TCDP: Lin et al., 2007; TAO, Vol.18, pp.379-393; NanTtoSEIZE: Byrne et al., 2009; GRL, Vol.36, L23310). These applications confirm the validity of using the ASR technique in determining in situ stresses by using drilled cores. We collected total 15 core samples in a depth range from 340 m MD to 1180 m MD, approximately for ASR measurements. Anelastic normal strains, measured every ten minutes in nine directions, including six independent directions, were used to calculate the anelastic strain tensors. The data of the ASR tests conducted at hole-1 is still undergoing analysis. As a tentative perspective, more than 10 core samples showed coherent strain recovery over one - two weeks. However, 2 or 3 core samples cannot be re-orientated to the global system. It means that we cannot rink the stress orientation determined by the core samples to geological structure. Unfortunately, a few core samples showed irregular strain recovery and were not analyzed further. The preliminary results of ASR tests at hole-1 show the stress orientations and stress regime changes a lot with the

Ultrasonic measurements on residual stress in autofrettged thick walled petroleum pipes

International Nuclear Information System (INIS)

Woias, G.; Mizera, J.

2008-01-01

The residual stresses in a component or structure are caused by incompatible permanent deformation and related gradient of plastic/elastic strains. They may be generated or modified at every stage in the components life cycle, from original material production to final disposal. Residual stresses can be measured by non-destructive techniques, including X-ray and neutron diffraction, magnetic and ultrasonic methods. The selection of the optimum measurement technique should take account volumetric resolution, material, geometry and access to the component. For large metallic components neutron diffraction is of prime importance as it provides quantitative information on stresses in relatively large volume of methods disregarding its shape complexity. Residual stresses can play a significant role in explaining or preventing failure of components of industrial installations. One example of residual stresses preventing failure are the ones generated by shot peening, inducing surface compressive stresses that improve the fatigue life. Petroleum refinery piping is generally characterized by large-diameters, operated at elevated temperature and under high pressure. Pipelines of a polyethylene plant working in one of the Polish refineries are subjected to pressures exceeding 300 MPa at temperatures above 200 o C. The pipes considered here were pressurized with pressure of 600 MPa. The wall thickness of the pipes is 27 mm and pipe dimensions are 46 x 100 mm. The material is steel with Re=580 MPa. Due to pressurizing, the components retain compressive stresses at the internal surface. These stresses increase resistance to cracking of the pipes. Over the period of exploitation these stresses diminish due to temperature activated relaxation or creep. The purpose of the project is to verify kinetics of such a relaxation process and calibrate alternative methods of their measurements. To avoid stress relaxation, numerical analysis from Finite Element Modelling (FEM)gave an

In situ stress determination research study

International Nuclear Information System (INIS)

Austin, W.G.; Thompson, P.M.

1994-01-01

The objectives of this study are to evaluate and implement rock stress determination instruments and techniques developed by Atomic Energy of Canada Limited (AECL) at its Underground Research Laboratory (URL) for use in jointed rock and to continue the development of analytical and interpretation methods for stress determination results including effects of scale, structure and anisotropy. Testing and evaluation of the instruments and methods developed at URL need to be done in a similar rock type prior to underground access at the Yucca Mountain Site Characterization Project

Thermal Stress Behavior of Micro- and Nano-Size Aluminum Films

International Nuclear Information System (INIS)

Hanabusa, T.; Kusaka, K.; Nishida, M.

2008-01-01

In-situ observation of thermal stresses in thin films deposited on silicon substrate was made by X-ray and synchrotron radiation. Specimens prepared in this experiment were micro- and nano-size thin aluminum films with and without passivation film. The thickness of the film was 1 micrometer for micro-size films and 10, 20 and 50 nanometer for nano-size films. The stress measurement in micro-size films was made by X-ray radiation whereas the measurement of nano-size films was made by synchrotron radiation. Residual stress measurement revealed tensile stresses in all as-deposited films. Thermal stresses were measured in a series of heating- and cooling-stage. Thermal stress behavior of micro-size films revealed hysteresis loop during a heating and cooling process. The width of a hysteresis loop was larger in passivated film that unpassivated film. No hysteresis loops were observed in nano-size films with SiO 2 passivation. Strengthning mechanism in thin films was discussed on a passivation film and a film thickness

X-ray diffraction and measurement of residual stresses

International Nuclear Information System (INIS)

Maeder, G.; Lebrun, J.L.; Corcaud, L.

1977-01-01

X-ray diffraction technique is a non destructive method for measuring the residual stresses in mechanical parts. This method, called sin 2 PSI method is investigated. It is applied to the measurement of elastic constants in different directions of crystals of Zr alloy (Zircaloy 4) and Ti alloy (TA6V). Stresses in TA6V sheets welded by TIG and electron beam processes are also studied [fr

Straylight measurements in laser in situ keratomileusis and laser-assisted subepithelial keratectomy for myopia

NARCIS (Netherlands)

Lapid-Gortzak, Ruth; van der Linden, Jan Willem; van der Meulen, Ivanka; Nieuwendaal, Carla; van den Berg, Tom

2010-01-01

PURPOSE: To compare straylight values before and 3 months after laser in situ keratomileusis (LASIK) and laser-assisted subepithelial keratectomy (LASEK) and to analyze the causes of any change. SETTING: Private refractive surgery clinic, Driebergen, The Netherlands. METHODS: Straylight was measured

In-situ measurement of magnetic field gradient in a magnetic shield by a spin-exchange relaxation-free magnetometer

International Nuclear Information System (INIS)

Fang Jian-Cheng; Wang Tao; Li Yang; Cai Hong-Wei; Zhang Hong

2015-01-01

A method of measuring in-situ magnetic field gradient is proposed in this paper. The magnetic shield is widely used in the atomic magnetometer. However, there is magnetic field gradient in the magnetic shield, which would lead to additional gradient broadening. It is impossible to use an ex-situ magnetometer to measure magnetic field gradient in the region of a cell, whose length of side is several centimeters. The method demonstrated in this paper can realize the in-situ measurement of the magnetic field gradient inside the cell, which is significant for the spin relaxation study. The magnetic field gradients along the longitudinal axis of the magnetic shield are measured by a spin-exchange relaxation-free (SERF) magnetometer by adding a magnetic field modulation in the probe beam’s direction. The transmissivity of the cell for the probe beam is always inhomogeneous along the pump beam direction, and the method proposed in this paper is independent of the intensity of the probe beam, which means that the method is independent of the cell’s transmissivity. This feature makes the method more practical experimentally. Moreover, the AC-Stark shift can seriously degrade and affect the precision of the magnetic field gradient measurement. The AC-Stark shift is suppressed by locking the pump beam to the resonance of potassium’s D1 line. Furthermore, the residual magnetic fields are measured with σ + - and σ – -polarized pump beams, which can further suppress the effect of the AC-Stark shift. The method of measuring in-situ magnetic field gradient has achieved a magnetic field gradient precision of better than 30 pT/mm. (paper)

The Community Child Health Network Life Stress Interview: a brief chronic stress measure for community health research.

Science.gov (United States)

Tanner Stapleton, Lynlee R; Dunkel Schetter, Christine; Dooley, Larissa N; Guardino, Christine M; Huynh, Jan; Paek, Cynthia; Clark-Kauffman, Elizabeth; Schafer, Peter; Woolard, Richard; Lanzi, Robin Gaines

2016-07-01

Chronic stress is implicated in many theories as a contributor to a wide range of physical and mental health problems. The current study describes the development of a chronic stress measure that was based on the UCLA Life Stress Interview (LSI) and adapted in collaboration with community partners for use in a large community health study of low-income, ethnically diverse parents of infants in the USA (Community Child Health Network [CCHN]). We describe the instrument, its purpose and adaptations, implementation, and results of a reliability study in a subsample of the larger study cohort. Interviews with 272 mothers were included in the present study. Chronic stress was assessed using the CCHN LSI, an instrument designed for administration by trained community interviewers to assess four domains of chronic stress, each rated by interviewers. Significant correlations ranging from small to moderate in size between chronic stress scores on this measure, other measures of stress, biomarkers of allostatic load, and mental health provide initial evidence of construct and concurrent validity. Reliability data for interviewer ratings are also provided. This relatively brief interview (15 minutes) is available for use and may be a valuable tool for researchers seeking to measure chronic stress reliably and validly in future studies with time constraints.

Measuring occupational stress: development of the pressure management indicator.

Science.gov (United States)

Williams, S; Cooper, C L

1998-10-01

The study of occupational stress is hindered by the lack of compact and comprehensive standardized measurement tools. The Pressure Management Indicator (PMI) is a 120-item self-report questionnaire developed from the Occupational Stress Indicator (OSI). The PMI is more reliable, more comprehensive, and shorter than the OSI. It provides an integrated measure of the major dimensions of occupational stress. The outcome scales measure job satisfaction, organizational satisfaction, organizational security, organizational commitment, anxiety--depression, resilience, worry, physical symptoms, and exhaustion. The stressor scales cover pressure from workload, relationships, career development, managerial responsibility, personal responsibility, home demands, and daily hassles. The moderator variables measure drive, impatience, control, decision latitude, and the coping strategies of problem focus, life work balance, and social support.

In-situ stress analysis with X-Ray diffraction for yield locus characterization of sheet metals

Energy Technology Data Exchange (ETDEWEB)

Güner, A.; Tekkaya, A. E. [Institute of Forming Technology and Lightweight Construction, TU Dortmund University, Baroper Str. 301, 44227 Dortmund (Germany); Zillmann, B.; Lampke, T. [Institute of Materials Science and Engineering, Chemnitz University of Technology, Erfenschlager Strasse 73 D-09125 Chemnitz (Germany)

2013-12-16

A main problem in the field of sheet metal characterization is the inhomogeneous plastic deformation in the gauge regions of specimens which causes the analytically calculated stresses to differ from the sought state of stress acting in the middle of the gauge region. To overcome this problem, application of X-Ray diffraction is analyzed. For that purpose a mobile X-ray diffractometer and an optical strain measurement system are mounted on a universal tensile testing machine. This enables the recording of the whole strain and stress history of a material point. The method is applied to uniaxial tension tests, plane strain tension tests and shear tests to characterize the interstitial free steel alloy DC06. The applicability of the concepts of stress factors is verified by uniaxial tension tests. The experimentally obtained values are compared with the theoretical values calculated with crystal elasticity models utilizing the orientation distribution functions (ODF). The relaxation problem is addressed which shows itself as drops in the stress values with the strain kept at a constant level. This drop is analyzed with elasto-viscoplastic material models to correct the measured stresses. Results show that the XRD is applicable to measure the stresses in sheet metals with preferred orientation. The obtained yield locus is expressed with the Yld2000–2D material model and an industry oriented workpiece is analyzed numerically. The comparison of the strain distribution on the workpiece verifies the identified material parameters.

Applicability study of using in-situ gamma-ray spectrometry technique for 137Cs and 210Pbex inventories measurement in grassland environments

International Nuclear Information System (INIS)

Li Junjie; Li Yong; Wang Yanglin; Wu Jiansheng

2010-01-01

In-situ measurement of fallout radionuclides 137 Cs and 210 Pb ex has the potential to assess soil erosion and sedimentation rapidly. In this study, inventories of 137 Cs and 210 Pb ex in the soil of Inner Mongolia grassland were measured using an In-situ Object Counting System (ISOCS). The results from the field study indicate that in-situ gamma-ray spectrometry has the following advantages over traditional laboratory measurements: no extra time is required for sample collection, no reference inventories are required, more economic, prompt availability of the results, the ability to average radionuclide inventory over a large area, and high precision.

Diffraction measurements of residual stress in titanium matrix composites

International Nuclear Information System (INIS)

James, M.R.; Bourke, M.A.; Goldstone, J.A.; Lawson, A.C.

1993-01-01

Metal matrix composites develop residual strains after consolidation due to the thermal expansion mismatch between the reinforcement fiber and the matrix. X-ray and neutron diffraction measured values for the longitudinal residual stress in the matrix of four titanium MMCs are reported. For thick composites (> 6 plies) the surface stress measured by x-ray diffraction matches that determined by neutron diffraction and therefore represents the stress in the bulk region consisting of the fibers and matrix. For thin sheet composites, the surface values are lower than in the interior and increase as the outer rows of fibers are approached. While a rationale for the behavior in the thin sheet has yet to be developed, accounting for composite thickness is important when using x-ray measured values to validate analytic and finite element calculations of the residual stress state

A Study on Residual Stress Measurements by Using Laser Speckle Interferometry

International Nuclear Information System (INIS)

Rho, Kyung Wan; Kang, Young June; Hong, Seong Jin; Kang, Hyung Soo

1999-01-01

Residual stress is one of the causes which make defects in engineering components and materials. And interest in the measurement of residual stress exists in many industries. There are commonly used methods by which residual stresses are currently measured. But these methods have a little demerits: time consumption and other problems. Therefore we devised a new experimental technique to measure residual stress in materials with a combination of laser speckle pattern interferometry, finite element method and spot heating. The speckle pattern interferometer measures in-plane deformations while the heating provides for very localized stress relief. FEM is used for determining heat temperature and other parameters. The residual stresses are determined by the amount of strain that is measured subsequent to the heating and cool-down of the region being interrogated. A simple model is presented to provide a description of the method. In this paper, the ambiguity problem for the fringe patterns has solved by a phase shifting method

X-ray measurement of residual stress in metals at Chalk River Nuclear Laboratories

International Nuclear Information System (INIS)

Winegar, J.E.

1980-06-01

X-ray diffraction is used at CRNL to measure residual stress in metals. This report summarizes the basic principles of stress measurement, and reviews factors affecting accuracy of measurement. The technique and equipment described were developed at CRNL to give reliable measurements. Accuracy of measurement is achieved by using fixed-count step-scanning and by computer analysis of intensity data using a cubic spline curve smoothing routine. Specific reference is made to the measurement of residual stress in Inconel-600 and Incoloy-800 boiler tubing. Because it measures stress in thin surface layers, the X-ray method can also be used to measure the depth profile of stresses. As there are no standardized procedures for measuring residual stress, this report will be useful both to those unfamiliar with the measurement of residual stress and to those already making such measurements in other laboratories. (auth)

A New Technique for Deep in situ Measurements of the Soil Water Retention Behaviour

DEFF Research Database (Denmark)

Rocchi, Irene; Gragnano, Carmine Gerardo; Govoni, Laura

2018-01-01

In situ measurements of soil suction and water content in deep soil layers still represent an experimental challenge. Mostly developed within agriculture related disciplines, field techniques for the identification of soil retention behaviour have been so far employed in the geotechnical context ...

New developments in measurements technology relevant to the studies of deep geological repositories in bedded salt

International Nuclear Information System (INIS)

Mao, N.; Ramirez, A.L.

1980-01-01

This report presents new developments in measurement technology relevant to the studies of deep geological repositories for nuclear waste disposal during all phases of development, i.e., site selection, site characterization, construction, operation, and decommission. Emphasis has been placed on geophysics and geotechnics with special attention to those techniques applicable to bedded salt. The techniques are grouped into sections as follows: tectonic environment, state of stress, subsurface structures, fractures, stress changes, deformation, thermal properties, fluid transport properties, and other approaches. Several areas that merit further research and developments are identified. These areas are: in situ thermal measurement techniques, fracture detection and characterization, in situ stress measurements, and creep behavior. The available instrumentations should generally be improved to have better resolution and accuracy, enhanced instrument survivability, and reliability for extended time periods in a hostile environment

New developments in measurements technology relevant to the studies of deep geological repositories in bedded salt

Science.gov (United States)

Mao, N. H.; Ramirez, A. L.

1980-10-01

Developments in measurement technology are presented which are relevant to the studies of deep geological repositories for nuclear waste disposal during all phases of development, i.e., site selection, site characterization, construction, operation, and decommission. Emphasis was placed on geophysics and geotechnics with special attention to those techniques applicable to bedded salt. The techniques are grouped into sections as follows: tectonic environment, state of stress, subsurface structures, fractures, stress changes, deformation, thermal properties, fluid transport properties, and other approaches. Several areas that merit further research and developments are identified. These areas are: in situ thermal measurement techniques, fracture detection and characterization, in situ stress measurements, and creep behavior. The available instrumentations should generally be improved to have better resolution and accuracy, enhanced instrument survivability, and reliability for extended time periods in a hostile environment.

High precision stress measurements in semiconductor structures by Raman microscopy

Energy Technology Data Exchange (ETDEWEB)

Uhlig, Benjamin

2009-07-01

Stress in silicon structures plays an essential role in modern semiconductor technology. This stress has to be measured and due to the ongoing miniaturization in today's semiconductor industry, the measuring method has to meet certain requirements. The present thesis deals with the question how Raman spectroscopy can be used to measure the state of stress in semiconductor structures. In the first chapter the relation between Raman peakshift and stress in the material is explained. It is shown that detailed stress maps with a spatial resolution close to the diffraction limit can be obtained in structured semiconductor samples. Furthermore a novel procedure, the so called Stokes-AntiStokes-Difference method is introduced. With this method, topography, tool or drift effects can be distinguished from stress related influences in the sample. In the next chapter Tip-enhanced Raman Scattering (TERS) and its application for an improvement in lateral resolution is discussed. For this, a study is presented, which shows the influence of metal particles on the intensity and localization of the Raman signal. A method to attach metal particles to scannable tips is successfully applied. First TERS scans are shown and their impact on and challenges for high resolution stress measurements on semiconductor structures is explained. (orig.)

Measurements of the state of stress in deep drill holes

International Nuclear Information System (INIS)

Vaeaetaeinen, A.; Saerkkae, P.

1985-05-01

The state of stress in rock is one of the most important parameters in the safe planning of stable underground openings in rock. At the same time, it is very difficult to be determined from a great distance. The common methods for the determination of state of stress in bedrock are usually not able to do this from a distance over 30 m. This work is a survey on rock stress determination methods usable in deep, over 500 m, drill holes. It also contains a recommendation for a method to determine the state of stress in Lavia test hole. The presented recommendation for the measurement of the state of stress contains an estimation on the working time for the measurement as well as the amount and location of the measuring points. The examination of the methods has been concentrated on three methods, hydraulic fracturing, overcoring by Vattenfall and differential strain analysis. Theoretical background of these methods has been analyzed. A special interest has been laid on the fundamental assumptions of different methods and their influence on the reliability of the results and the interpretation of the state of stress. The comparison of the methods has been made by literature and user interviews. Equipment and personnel needed, and way of measurement are described for the methods. The parameters measured and their possible sources of errors are described, too, as well as the fundamental assumptions and potential difficulties in the measurement. The organizations in Scandinavia performing measurements and their abilities to do measurements and interpretation are presented. Readiness to interpretation in Finland is described shortly

Analysis of borehole inclusion stress measurement concepts proposed for use in the Waste Isolation Pilot Plant (WIPP)

International Nuclear Information System (INIS)

Morgan, H.S.

1984-01-01

The Waste Isolation Pilot Plant (WIPP) is being developed in southeastern New Mexico by the United States Department of Energy as a research and development (RandD) facility to demonstrate the safe disposal in salt of radioactive wastes resulting from defense activities. As part of the WIPP RandD program, a series of in situ tests will be performed to determine the behavior of drifts and storage rooms in the creeping salt medium. Data obtained in these tests will be used to evaluate and improve numerical models used to compute the structural response of these drifts and rooms. Stress has been proposed as one of the parameters to be measured in the tests, and borehole inclusion stressmeters have been included in the instrumentation package

In-situ studies of the TGO growth stresses and the martensitic transformation in the B2 phase in commercial Pt-modified NiAl and NiCoCrAlY bond coat alloys

Energy Technology Data Exchange (ETDEWEB)

Hovis, D.; Hu, L.; Reddy, A.; Heuer, A.H. [Dept. of Materials Science and Engineering, Case Western Reserve Univ., Cleveland, OH (United States); Paulikas, A.P.; Veal, B.W. [Materials Science Div., Argonne National Lab., Argonne, IL (United States)

2007-12-15

Oxide growth stresses were measured in situ at 1100 C on commercial Pt-modified NiAl and NiCoCrAlY bond coat alloys using synchrotron X-rays. Measurements were taken on samples that had no preoxidation, as well as on samples that had experienced 24 one-hour thermal exposures at 1150 C, a condition known to induce rumpling in the Pt-modified NiAl alloy, but not in the NiCoCrAlY alloy. The NiCoCrAlY alloy showed continuous stress relaxation under all conditions, whereas the Pt-modified NiAl alloys would typically stabilize at a fixed (often non-zero) stress suggesting a higher creep strength in the 'Thermally Grown Oxide' on the latter alloy, though the precise behavior was dependent on initial surface preparation. The formation of martensite in the Pt-modified NiAl alloys was also observed upon cooling and occurred at temperatures below 200 C for all of the samples observed. Based on existing models, this M{sub s} temperature is too low to account for the rumpling observed in these alloys. (orig.)

Studying the effect of stress relaxation and creep on lattice strain evolution of stainless steel under tension

International Nuclear Information System (INIS)

Wang, H.; Clausen, B.; Tomé, C.N.; Wu, P.D.

2013-01-01

Due to relatively long associated count times, in situ strain measurements using neutron diffraction requires periodic interruption of the test to collect the diffraction data by holding either the stress or the strain constant. As a consequence, stress relaxation or strain creep induced by the interrupts is inevitable, especially at loads which are close to the flow stress of the material. An in situ neutron diffraction technique, which consists in performing the diffraction measurements using continuous event-mode data collection while conducting the mechanical loading monotonically with a very slow loading rate, is proposed here to avoid the effects associated with interrupts. The lattice strains in stainless steel under uniaxial tension are measured using the three techniques, and the experimental results are compared to study the effect of stress relaxation and strain creep on the lattice strain measurements. The experimental results are simulated using both the elastic viscoplastic self-consistent (EVPSC) model and the elastic plastic self-consistent (EPSC) model. Both the EVPSC and EPSC models give reasonable predictions for all the three tests, with EVPSC having the added advantage over EPSC that it allows us to address the relaxation and creep effects in the interrupted tests

Hydraulic fracturing rock stress measurement at Haestholmen, Finland

International Nuclear Information System (INIS)

Ljunggren, C.; Klasson, H.

1992-12-01

This report presents hydraulic fracturing measurements in two boreholes located on the Haestholmen island near Loviisa, Finland. The aim of the measurements was to provide stress data, forming input for the design of an underground facility for disposal of low- and medium-level waste as well as future plant decommissioning radioactive waste from the IVO reactor units situated on Haestholmen. The theoretical background to the hydrofracturing method is summarized, as is the equipment and experimental procedures used in the present case. All results obtained are presented and critically discussed. The final stress parameters presented are magnitudes and directions of the maximum and minimum horizontal stresses. Testing was successfully completed according to schedule in both boreholes.(orig.)

3D Tyre/Road pavement contact stress measurements

CSIR Research Space (South Africa)

De Beer, Morris

2010-10-01

Full Text Available The CSIR’s proprietary Stress-in-Motion (SIM) measurements provide rational descriptions of 1D, 2D and 3D tyre/road pavement stresses for: Road pavement design testing and evaluation, as well as tyre design, testing and evaluation....

[Measurement of unemployment-related psychological stress: Validation of the Unemployment Stress (USS)].

Science.gov (United States)

Szabóné Kapuvári, Virág; Martos, Tamás

2016-01-01

Nowadays the theme of unemployment and the given answers of it are up to date questions in psychology. In spite of this fact, the psychological methods measuring this phenomenon are often missing. That is why the Unemployment Stress Scale (USS) is presented in this article. The aim of our study is to develop a scale called USS and test it's validity and reliability. There were 287 adult unemployed persons asked in this study. Besides the USS we used the Beck Depression Scale, the Spielberger Anxiety Scale (TRAIT), the Sense of Coherence Scale (Hungarian version) and the Rosenberg Self Esteem Scale. According to our results, USS has showed an excellent criterion and construct validity. A useful scale has been formed according to test-retest results. (Cronbach-alfa: 0.88 and 0.86 according to the samples). Moreover our scale has a strong correlation with the Spielberger Anxiety Scale (TRAIT) and the Beck Depression Scale. These chracteristics of the new scale proved that we fond a factor, independent from the self esteem and the sense of coherence, which represents the stress level in the situation of unemployment. This scale is a professional construction to measure stress contributed to unemployment. The USS can be a useful scale in clinical practice because after measuring with this scale we can protect the personality of the unemployed by representing the actual unemployment stress level. That is why professionals can help earlier in a crisis like this.

Canopy Vegetation Indices from In situ Hyperspectral Data to Assess Plant Water Status of Winter Wheat under Powdery Mildew Stress.

Science.gov (United States)

Feng, Wei; Qi, Shuangli; Heng, Yarong; Zhou, Yi; Wu, Yapeng; Liu, Wandai; He, Li; Li, Xiao

2017-01-01

Plant disease and pests influence the physiological state and restricts the healthy growth of crops. Physiological measurements are considered the most accurate way of assessing plant health status. In this paper, we researched the use of an in situ hyperspectral remote sensor to detect plant water status in winter wheat infected with powdery mildew. Using a diseased nursery field and artificially inoculated open field experiments, we detected the canopy spectra of wheat at different developmental stages and under different degrees of disease severity. At the same time, destructive sampling was carried out for physical tests to investigate the change of physiological parameters under the condition of disease. Selected vegetation indices (VIs) were mostly comprised of green bands, and correlation coefficients between these common VIs and plant water content (PWC) were generally 0.784-0.902 ( p powdery mildew stress. The Photochemical Reflectance Index (PRI) was sensitive to physiological response influenced by powdery mildew, and the relationships of PRI with chlorophyll content, the maximum quantum efficiency of PSII photochemistry (Fv/Fm), and the potential activity of PSII photochemistry (Fv/Fo) were good with R 2 = 0.639, 0.833, 0.808, respectively. Linear regressions showed PRI demonstrated a steady relationship with PWC across different growth conditions, with R 2 = 0.817 and RMSE = 2.17. The acquired PRI model of wheat under the powdery mildew stress has a good compatibility to different experimental fields from booting stage to filling stage compared with the traditional water signal vegetation indices, WBI, FWBI 1 , and FWBI 2 . The verification results with independent data showed that PRI still performed better with R 2 = 0.819 between measured and predicted, and corresponding RE = 8.26%. Thus, PRI is recommended as a potentially reliable indicator of PWC in winter wheat with powdery mildew stress. The results will help to understand the physical state of

Convenient measurement of the residual stress using X-ray penetration depth

International Nuclear Information System (INIS)

Ukai, Takayoshi; Shibano, Junichi

1994-01-01

The residual stress measured with a characteristic X-ray is usually evaluated as a surface stress. However, it is a weighted mean value over all penetration depth of X-ray. Thus, the classical sin 2 Ψ method with the characteristic X-ray is difficult to use for measuring the steep gradient of residual stress that occurs along the depth direction in a subsurface layer of the material after cold rolling and grinding. This paper presents a convenient method of the residual stress measurement along the depth direction in a subsurface layer using the penetration depth depending on a characteristic X-ray. The residual stress distribution of JIS SKS51 steel plate was measured as an example of applying this method. As a result, it could be confirmed that a residual stress distribution along the depth direction in a subsurface layer could be evaluated nondestructively by this convenient method. (author)

Quality assurance of in-situ-gammaspectrometry. International comparison measurement at the K-RISK-phantom 2015; Qualitaetssicherung der In-situ-Gammaspektrometrie. Internationale Vergleichsmessung an der K-RISK-Phantomwand 2015

Energy Technology Data Exchange (ETDEWEB)

Haas, G.; Schupfner, R. [Regensburg Univ. (Germany). ZRN-URA-Lab.; Buss, K. [Bayerisches Landesamt fuer Umwelt, Kulmbach (Germany)

2016-07-01

During the last years the collimated in-situ-gammaspectrometry established itself as a powerful mean for free- release of buildings, parts of buildings, walls and ground area. To accomplish a suitable possibility for quality assurance of in-situ-gammaspectrometry, the K-RISK-phantom wall was developed and built at the University of Regensburg on the authority of the state office for environmental protection, Kulmbach. The K-RISK-phantom is a large surface calibration wall made of concrete which allows simulating different realistic three-dimensional wall contaminations. Contrary to many other calibration phantoms the K-RISK phantom permits completely reversible three-dimensional activity distributions. The comparison measurement is a useful tool for quality assurance and allows the participants to review their measurements relating to measurement, calibration or analysis. 19 institutions (industry, surveyor, authorities) from Germany, Austria and Switzerland participated at the comparison measurement.

Quantitative Analysis of Oxygen Gas Exhausted from Anode through In Situ Measurement during Electrolytic Reduction

Directory of Open Access Journals (Sweden)

Eun-Young Choi

2017-01-01

Full Text Available Quantitative analysis by in situ measurement of oxygen gas evolved from an anode was employed to monitor the progress of electrolytic reduction of simulated oxide fuel in a molten Li2O–LiCl salt. The electrolytic reduction of 0.6 kg of simulated oxide fuel was performed in 5 kg of 1.5 wt.% Li2O–LiCl molten salt at 650°C. Porous cylindrical pellets of simulated oxide fuel were used as the cathode by loading a stainless steel wire mesh cathode basket. A platinum plate was employed as the anode. The oxygen gas evolved from the anode was exhausted to the instrumentation for in situ measurement during electrolytic reduction. The instrumentation consisted of a mass flow controller, pump, wet gas meter, and oxygen gas sensor. The oxygen gas was successfully measured using the instrumentation in real time. The measured volume of the oxygen gas was comparable to the theoretically calculated volume generated by the charge applied to the simulated oxide fuel.

Model predictions of metal speciation in freshwaters compared to measurements by in situ techniques.

NARCIS (Netherlands)

Unsworth, Emily R; Warnken, Kent W; Zhang, Hao; Davison, William; Black, Frank; Buffle, Jacques; Cao, Jun; Cleven, Rob; Galceran, Josep; Gunkel, Peggy; Kalis, Erwin; Kistler, David; Leeuwen, Herman P van; Martin, Michel; Noël, Stéphane; Nur, Yusuf; Odzak, Niksa; Puy, Jaume; Riemsdijk, Willem van; Sigg, Laura; Temminghoff, Erwin; Tercier-Waeber, Mary-Lou; Toepperwien, Stefanie; Town, Raewyn M; Weng, Liping; Xue, Hanbin

2006-01-01

Measurements of trace metal species in situ in a softwater river, a hardwater lake, and a hardwater stream were compared to the equilibrium distribution of species calculated using two models, WHAM 6, incorporating humic ion binding model VI and visual MINTEQ incorporating NICA-Donnan. Diffusive

X-ray stress measurement by use of synchrotron radiation source

International Nuclear Information System (INIS)

Yoshioka, Yasuo; Matsui, Hisaaki; Moro-oka, Toshimasa; Hasegawa, Ken-ichi; Nakajima, Tetsuo.

1986-01-01

In the field of X-ray stress measurement of polycrystalline materials, a diffraction plane at higher Bragg angle has to be selected in order to obtain the precise value of stress. However, the stress measurement on an optional (hkl) plane desired is not always possible because the X-ray beam exited from a metal target has a dispersive wave length. Recently, we have been able to use the synchrotron radiation source (SR) as an excellent X-ray source. In Japan, the facility of synchrotron radiation (Photon Factory, PF) was constructed in the National Laboratory for High Energy Physics (KEK) at Tsukuba academic city. The use of this SR enables the stress measurements on many (hkl) planes with high accuracy in the higher Bragg angle region by providing an X-ray beam having an optional wave length. We have started the X-ray stress analysis by use of the synchrotron radiation source. This paper reports the system of measurement and some results of preliminaly experiments. Since a monochromatic X-ray beam is required for the stress measurement, we used a beam line which consists of a double crystal monochrometer and a focusing mirror. X-rays between 4 KeV (λ = 0.31 nm) and 10 KeV (λ = 0.12 nm) are available with this optical system. We adopted a constant Bragg angle of 2θ = 154 deg for all the diffraction planes. A PSPC having a carbon fiber anode is made and used as a detector with the use of a fast digital signal processor. We could observe the diffraction profiles from (200), (211), (220), (310) and (321) crystal plane of alpha iron, respectively, and the residual stresses in these planes except the (200) plane were measured with high accuracy in a short time. Such feature especially suits the stress analysis of the material which has preferred orientation or stress gradient. (author)

Simultaneous measurement of polymerization stress and curing kinetics for photo-polymerized composites with high filler contents.

Science.gov (United States)

Wang, Zhengzhi; Landis, Forrest A; Giuseppetti, Anthony A M; Lin-Gibson, Sheng; Chiang, Martin Y M

2014-12-01

Photopolymerized composites are used in a broad range of applications with their performance largely directed by reaction kinetics and contraction accompanying polymerization. The present study was to demonstrate an instrument capable of simultaneously collecting multiple kinetics parameters for a wide range of photopolymerizable systems: degree of conversion (DC), reaction exotherm, and polymerization stress (PS). Our system consisted of a cantilever beam-based instrument (tensometer) that has been optimized to capture a large range of stress generated by lightly-filled to highly-filled composites. The sample configuration allows the tensometer to be coupled to a fast near infrared (NIR) spectrometer collecting spectra in transmission mode. Using our instrument design, simultaneous measurements of PS and DC are performed, for the first time, on a commercial composite with ≈80% (by mass) silica particle fillers. The in situ NIR spectrometer collects more than 10 spectra per second, allowing for thorough characterization of reaction kinetics. With increased instrument sensitivity coupled with the ability to collect real time reaction kinetics information, we show that the external constraint imposed by the cantilever beam during polymerization could affect the rate of cure and final degree of polymerization. The present simultaneous measurement technique is expected to provide new insights into kinetics and property relationships for photopolymerized composites with high filler content such as dental restorative composites. Published by Elsevier Ltd.

Calibration of HPGe detector for in situ measurements of 137Cs in soil by 'peak to valley' method

International Nuclear Information System (INIS)

Fueloep, M.

2000-01-01

The contamination of soil with gamma-ray emitters can be measured in two ways: soil sampling method and in situ spectrometry of the ambient gamma-ray radiation. The conventional soil sampling method has two disadvantages: samples may not be representative for a large areas and determination of the depth distribution of radionuclide requires the measurement of several samples taken from different depths. In situ measurement of a radionuclide activity in soil is more sensitive and provides more representative data than data obtained by soil sample collection and subsequent laboratory analysis. In emergency situations time to assess the contamination is critical. For rapid assessment of the deposited activity direct measurement of ambient gamma-ray radiation are used. In order to obtain accurate measurements of radionuclides in the soil, the detector should be placed on relatively even and open terrain. It is our customary practice to place the detector 1 m above the soil surface. At this height, a tripod-mounted detector can be handled easily and still provide a radius of view for gamma emitting sources out to about 10 m. The 'field of view' actually varies, being somewhat larger for higher sources. Depending upon source energy, the detector effectively sees down to a depth of 15-30 cm. Commonly used method for field gamma spectrometry is method by Beck (1). The most important disadvantages of in situ spectrometry by Beck are that the accuracy of the analysis depends on a separate knowledge of the radioactivity distribution with soil depth. This information can be obtained by calculations using data from in situ measurements and energy dependence of absorption and scattering of photons in soil and track length distribution of photons in soil (2). A method of in situ measurements of 137 Cs in soil where radionuclide distribution in soil profile is calculated by unfolding of detector responses in the full energy peak net area at 0.662 MeV and in the valley under the

An optode sensor array for long term in situ Oxygen measurements in soil and sediment

DEFF Research Database (Denmark)

Rickelt, Lars F; Jensen, Louise Askær; Walpersdorf, Eva Christine

2013-01-01

Long-term measurements of molecular oxygen (O2) dynamics in wetlands are highly relevant for understanding the eff ects of water level changes on net greenhouse gas budgets in these ecosystems. However, such measurements have been limited due to a lack of suitable measuring equipment. We construc......Long-term measurements of molecular oxygen (O2) dynamics in wetlands are highly relevant for understanding the eff ects of water level changes on net greenhouse gas budgets in these ecosystems. However, such measurements have been limited due to a lack of suitable measuring equipment. We...... constructed an O2 optode sensor array for long-term in situ measurements in soil and sediment. Th e new device consists of a 1.3-m-long, cylindrical, spear-shaped rod equipped with 10 sensor spots along the shaft . Each spot contains a thermocouple fi xed with a robust fi beroptic O2 optode made...... characteristics of the sensor array system are presented along with a novel approach for temperature compensation of O2 optodes. During in situ application over several months in a peat bog, we used the new device to document pronounced variations in O2 distribution aft er marked shift s in water level. Th e...

Husbandry Emissions Estimation: Fusion of Mobile Surface and Airborne Remote Sensing and Mobile Surface In Situ Measurements

Science.gov (United States)

Leifer, I.; Hall, J. L.; Melton, C.; Tratt, D. M.; Chang, C. S.; Buckland, K. N.; Frash, J.; Leen, J. B.; Van Damme, M.; Clarisse, L.

2017-12-01

Emissions of methane and ammonia from intensive animal husbandry are important drivers of climate and photochemical and aerosol pollution. Husbandry emission estimates are somewhat uncertain because of their dependence on practices, temperature, micro-climate, and other factors, leading to variations in emission factors up to an order-of-magnitude. Mobile in situ measurements are increasingly being applied to derive trace gas emissions by Gaussian plume inversion; however, inversion with incomplete information can lead to erroneous emissions and incorrect source location. Mobile in situ concentration and wind data and mobile remote sensing column data from the Chino Dairy Complex in the Los Angeles Basin were collected near simultaneously (within 1-10 s, depending on speed) while transecting plumes, approximately orthogonal to winds. This analysis included airborne remote sensing trace gas information. MISTIR collected vertical column FTIR data simultaneously with in situ concentration data acquired by the AMOG-Surveyor while both vehicles traveled in convoy. The column measurements are insensitive to the turbulence characterization needed in Gaussian plume inversion of concentration data and thus provide a flux reference for evaluating in situ data inversions. Four different approaches were used on inversions for a single dairy, and also for the aggregate dairy complex plume. Approaches were based on differing levels of "knowledge" used in the inversion from solely the in situ platform and a single gas to a combination of information from all platforms and multiple gases. Derived dairy complex fluxes differed significantly from those estimated by other studies of the Chino complex. Analysis of long term satellite data showed that this most likely results from seasonality effects, highlighting the pitfalls of applying annualized extensions of flux measurements to a single campaign instantiation.

Advanced In Situ I-V Measurements Used in the Study of Porous Structures Growth on Silicon

Directory of Open Access Journals (Sweden)

Amare Benor

2017-01-01

Full Text Available The rate of oxide formation during growth of pores structures on silicon was investigated by in situ I-V measurements. The measurements were designed to get two I-V curves in a short time (total time for the two measurements was 300 seconds taking into account the gap (in mA/cm2 for each corresponding voltage. The in situ I-V measurements were made at different pore depth/time, at the electrolyte-pore tip interface, while etching takes place based on p-type Si. The results showed increasing, decreasing, and constant I-V gap in time, for macropores, nanopores, and electropolishing regimes, respectively. This was related to the expected diffusion limitation of oxide forming (H2O molecules reaching the electrolyte-pore tip and the anodizing current, while etching takes place. The method can be developed further and has the potential to be applied in other electrochemically etched porous semiconductor materials.

In-situ neutron diffraction characterization of temperature dependence deformation in α-uranium

Science.gov (United States)

Calhoun, C. A.; Garlea, E.; Sisneros, T. A.; Agnew, S. R.

2018-04-01

In-situ strain neutron diffraction measurements were conducted at temperature on specimens coming from a clock-rolled α-uranium plate, and Elasto-Plastic Self-Consistent (EPSC) modeling was employed to interpret the findings. The modeling revealed that the active slip systems exhibit a thermally activated response, while deformation twinning remains athermal over the temperature ranges explored (25-150 °C). The modeling also allowed assessment of the effects of thermal residual stresses on the mechanical response during compression. These results are consistent with those from a prior study of room-temperature deformation, indicating that the thermal residual stresses strongly influence the internal strain evolution of grain families, as monitored with neutron diffraction, even though accounting for these residual stresses has little effect on the macroscopic flow curve, except in the elasto-plastic transition.

In-situ stress measurements - results of experiments performed at the ASSE salt mine - Federal Republic of Germany

International Nuclear Information System (INIS)

Feddersen, H.K.

1989-01-01

High-level nuclear wastes are heat generating wastes. Heat will be transferred to the surrounding salt formation. This heating of the host rock will result in an increased temperature and in stress changes. From 1983 through 1985 two underground tests were conducted in the Asse Salt Mine (Federal Republic of Germany) in which, among others, thermally induced stress changes were investigated. These tests are discussed in this paper

Transmission of vertical stress in a real soil profile. Part III

DEFF Research Database (Denmark)

Lamandé, Mathieu; Schjønning, Per

2011-01-01

The transmission of stress in soils is extremely sensitive to changes in water content. According to the elasticity theory, for a given load applied to a given soil, an increase in soil water content yields a higher concentration of stresses under the centre of the load and a deeper propagation...... of stresses. We quantified the effect of soil water content of topsoil/subsoil layers (wet/wet, wet/dry, and dry/dry) on stress transmission. 3D measurements of vertical stresses under a towed wheel (800/50R34) were performed in situ in a Stagnic Luvisol. The tyre was loaded with 60 kN, and we used...... were measured in separate tests. Increase of water content in the topsoil by 114% increased the contact area by 149%, decreased the vertical stresses at the tyre–soil interface by 50%, and decreased the maximum vertical stress at 0.3 and 0.6 m depth by 46 and 63%, respectively. Stress attenuation...

Rock stress measurements. Preparatory stage of the equipment development project

International Nuclear Information System (INIS)

Mononen, S.; Hakala, M.; Mikkola, P.

2002-01-01

In recent years the rock stress measurement methods used in Finland have been overcoring and hydraulic fracturing. There have been mainly two companies involved in these measurements, namely Suomen Malmi Oy (Smoy) and SwedPower AB. Smoy has done measurements for mines and for rock engineering projects, whereas SwedPower AB has mainly been involved in nuclear waste disposal investigations and conducted hydraulic fracturing measurements in deep boreholes. Smoy together with its partners started in February 2001 a project named JTM, which was a preliminary stage for a future project, which aims to develop a device most suitable for rock stress measurements in Finland. The partners in the project were HUT Rock Engineering, Posiva Oy, Saanio and Riekkola Oy, Gridpoint Finland Oy and Geopros Oy. Tekes, the National Technology Agency, provided almost half of the project funding. In the management group of the project were Pekka Mikkola (chairman) and Tero Laurila from Smoy, Pekka Saerkkae and Sakari Mononen (full-time researcher) from HUT, Aimo Hautojaervi (Posiva Oy), Erik Johansson (Saanio and Riekkola Oy), Matti Hakala (Gridpoint Finland Oy) and Heikki Haemaelaeinen (Geopros Oy). The aim of the JTM-project was to find out the needs for the development of a device most suitable for rock stress measurements in Finnish mines and rock engineering projects. During the project work was done to find out the range of rock stress measurement devices available, to find out the needs for measurements, and to get acquainted to the measurements done in Scandinavia. Also a report of the most suitable methods for Finnish rock conditions was done based on literature and on interviews of rock stress experts. Based on all the information collected during the project a clear picture of the needs for rock stress measurements in Finland could be formed and a preliminary plan of a future project was done. The aim of the suggested project is to build a device based on hydraulic fracturing

In situ measurement of some soil properties in paddy soil using visible and near-infrared spectroscopy.

Directory of Open Access Journals (Sweden)

Ji Wenjun

Full Text Available In situ measurements with visible and near-infrared spectroscopy (vis-NIR provide an efficient way for acquiring soil information of paddy soils in the short time gap between the harvest and following rotation. The aim of this study was to evaluate its feasibility to predict a series of soil properties including organic matter (OM, organic carbon (OC, total nitrogen (TN, available nitrogen (AN, available phosphorus (AP, available potassium (AK and pH of paddy soils in Zhejiang province, China. Firstly, the linear partial least squares regression (PLSR was performed on the in situ spectra and the predictions were compared to those with laboratory-based recorded spectra. Then, the non-linear least-square support vector machine (LS-SVM algorithm was carried out aiming to extract more useful information from the in situ spectra and improve predictions. Results show that in terms of OC, OM, TN, AN and pH, (i the predictions were worse using in situ spectra compared to laboratory-based spectra with PLSR algorithm (ii the prediction accuracy using LS-SVM (R2>0.75, RPD>1.90 was obviously improved with in situ vis-NIR spectra compared to PLSR algorithm, and comparable or even better than results generated using laboratory-based spectra with PLSR; (iii in terms of AP and AK, poor predictions were obtained with in situ spectra (R2<0.5, RPD<1.50 either using PLSR or LS-SVM. The results highlight the use of LS-SVM for in situ vis-NIR spectroscopic estimation of soil properties of paddy soils.

In situ measurements of HO{sub x} in super- and subsonic aircraft exhaust plumes

Energy Technology Data Exchange (ETDEWEB)

Hanisco, T F; Wennberg, P O; Cohen, R C; Anderson, J G [Harvard Univ., Cambridge, MA (United States). Dept. of Chemistry; Fahey, D W; Keim, E R; Gao, R S; Wamsley, R C; Donnelly, S G; Del Negro, L A [National Oceanic and Atmospheric Administration, Boulder, CO (United States). Aeronomy Lab.; others, and

1998-12-31

Concentrations of HO{sub x} (OH and HO{sub 2}) have been obtained in the exhaust plumes of an Air France Concorde and a NASA ER-2 in the lower stratosphere and the NASA DC-8 in the upper troposphere using instruments aboard the NASA ER-2. These fast-time response in situ measurements are used in conjunction with simultaneous in situ measurements of other key exhaust species (NO, NO{sub 2}, NO{sub y}, H{sub 2}O, and CO) to analyze the emissions of HO{sub x} from each aircraft under a variety of conditions. The data are used to establish a general description of gas phase plume chemistry that is easily implemented in a photochemical model. This model is used to determine the amount of HO{sub x} emitted from the engines and the gas phase oxidation rates of nitrogen and sulfur species in the exhaust plumes. (author) 10 refs.

The retrieval of cloud microphysical properties using satellite measurements and an in situ database

Directory of Open Access Journals (Sweden)

C. Poix

1996-01-01

Full Text Available By combining AVHRR data from the NOAA satellites with information from a database of in situ measurements, large-scale maps can be generated of the microphysical parameters most immediately significant for the modelling of global circulation and climate. From the satellite data, the clouds can be classified into cumuliform, stratiform and cirrus classes and then into further sub-classes by cloud top temperature. At the same time a database of in situ measurements made by research aircraft is classified into the same sub-classes and a statistical analysis is used to derive relationships between the sub-classes and the cloud microphysical properties. These two analyses are then linked to give estimates of the microphysical properties of the satellite observed clouds. Examples are given of the application of this technique to derive maps of the probability of occurrence of precipitating clouds and of precipitating water content derived from a case study within the International Cirrus Experiment (ICE held in 1989 over the North Sea.

The retrieval of cloud microphysical properties using satellite measurements and an in situ database

Directory of Open Access Journals (Sweden)

Christophe Poix

Full Text Available By combining AVHRR data from the NOAA satellites with information from a database of in situ measurements, large-scale maps can be generated of the microphysical parameters most immediately significant for the modelling of global circulation and climate. From the satellite data, the clouds can be classified into cumuliform, stratiform and cirrus classes and then into further sub-classes by cloud top temperature. At the same time a database of in situ measurements made by research aircraft is classified into the same sub-classes and a statistical analysis is used to derive relationships between the sub-classes and the cloud microphysical properties. These two analyses are then linked to give estimates of the microphysical properties of the satellite observed clouds. Examples are given of the application of this technique to derive maps of the probability of occurrence of precipitating clouds and of precipitating water content derived from a case study within the International Cirrus Experiment (ICE held in 1989 over the North Sea.

In situ measurements of HO{sub x} in super- and subsonic aircraft exhaust plumes

Energy Technology Data Exchange (ETDEWEB)

Hanisco, T.F.; Wennberg, P.O.; Cohen, R.C.; Anderson, J.G. [Harvard Univ., Cambridge, MA (United States). Dept. of Chemistry; Fahey, D.W.; Keim, E.R.; Gao, R.S.; Wamsley, R.C.; Donnelly, S.G.; Del Negro, L.A. [National Oceanic and Atmospheric Administration, Boulder, CO (United States). Aeronomy Lab.; and others

1997-12-31

Concentrations of HO{sub x} (OH and HO{sub 2}) have been obtained in the exhaust plumes of an Air France Concorde and a NASA ER-2 in the lower stratosphere and the NASA DC-8 in the upper troposphere using instruments aboard the NASA ER-2. These fast-time response in situ measurements are used in conjunction with simultaneous in situ measurements of other key exhaust species (NO, NO{sub 2}, NO{sub y}, H{sub 2}O, and CO) to analyze the emissions of HO{sub x} from each aircraft under a variety of conditions. The data are used to establish a general description of gas phase plume chemistry that is easily implemented in a photochemical model. This model is used to determine the amount of HO{sub x} emitted from the engines and the gas phase oxidation rates of nitrogen and sulfur species in the exhaust plumes. (author) 10 refs.

Internal strain measurement using pulsed neutron diffraction at LANSCE

International Nuclear Information System (INIS)

Goldstone, J.A.; Bourke, M.A.M.; Shi, N.

1994-01-01

The presence of residual stress in engineering components can effect their mechanical properties and structural integrity. Neutron diffraction in the only technique that can make nondestructive measurements in the interior of components. By recording the change in crystalline lattice spacings, elastic strains can be measured for individual lattice reflections. Using a pulsed neutron source, all lattice reflections are recorded in each measurement, which allows for easy examination of heterogeneous materials such as metal matrix composites. Measurements made at the Manuel Lujan Jr. Neutron Scattering Center (LANSCE) demonstrate the potential at pulsed sources for in-situ stress measurements at ambient and elevated temperatures

Visualizing Stress and Temperature Distribution During Elevated Temperature Deformation of IN-617 Using Nanomechanical Raman Spectroscopy

Science.gov (United States)

Zhang, Yang; Wang, Hao; Tomar, Vikas

2018-04-01

This work presents direct measurements of stress and temperature distribution during the mesoscale microstructural deformation of Inconel-617 (IN-617) during 3-point bending tests as a function of temperature. A novel nanomechanical Raman spectroscopy (NMRS)-based measurement platform was designed for simultaneous in situ temperature and stress mapping as a function of microstructure during deformation. The temperature distribution was found to be directly correlated to stress distribution for the analyzed microstructures. Stress concentration locations are shown to be directly related to higher heat conduction and result in microstructural hot spots with significant local temperature variation.

In situ electrical measurements of polytypic silver nanowires

International Nuclear Information System (INIS)

Liu Xiaohua; Zhu Jing; Jin Chuanhong; Peng Lianmao; Tang Daiming; Cheng Huiming

2008-01-01

Novel 4H structure silver nanowires (4H-AgNWs) have been reported to coexist with the usual face-centered cubic (FCC) ones. Here we report the electrical properties of these polytypic AgNWs for the first time. AgNWs with either 4H or FCC structures in the diameter range of 20-80 nm were measured in situ inside a transmission electron microscope (TEM). Both kinds of AgNW in the diameter range show metallic conductance. The average resistivity of the 4H-AgNWs is 19.9 μΩ cm, comparable to the 11.9 μΩ cm of the FCC-AgNWs. The failure current density can be up to ∼10 8 A cm -2 for both 4H-and FCC-AgNWs. The maximum stable current density (MSCD) is introduced to estimate the AgNWs' current-carrying ability, which shows diameter-dependence with a peak around 34 nm in diameter. It is attributed to fast annihilation of the current-induced vacancies and the enhanced surface scattering. Our investigations also suggest that the magnetic field of the electromagnetic lens may also introduce some influence on the measurements inside the TEM

An in situ test of vibrating wire stressmeters in granitic rock

International Nuclear Information System (INIS)

Spinney, M.H.

1990-02-01

An in situ test was conducted to assess the ability of vibrating-wire stressmeters to measure stress changes in hard, unfractured granitic rock at the Underground Research Laboratory (URL). Twelve vibrating-wire stressmeters installed ahead of the face and below floor grade of Room 205 were monitored during the excavation of Room 205. The results were compared with results from CSIRO hollow inclusion triaxial strain cells, USBM boreholes deformation gauge overcore tests done before and after excavation, and a two-dimensional numerical model

Rock stress measurements using the LUT-Gauge overcoring method