Low Cost, Low Power, High Sensitivity Magnetometer

Science.gov (United States)

2008-12-01

which are used to measure the small magnetic signals from brain. Other types of vector magnetometers are fluxgate , coil based, and magnetoresistance...concentrator with the magnetometer currently used in Army multimodal sensor systems, the Brown fluxgate . One sees the MEMS fluxgate magnetometer is...Guedes, A.; et al., 2008: Hybrid - LOW COST, LOW POWER, HIGH SENSITIVITY MAGNETOMETER A.S. Edelstein*, James E. Burnette, Greg A. Fischer, M.G

Scanning Quantum Cryogenic Atom Microscope

Science.gov (United States)

Yang, Fan; Kollár, Alicia J.; Taylor, Stephen F.; Turner, Richard W.; Lev, Benjamin L.

2017-03-01

Microscopic imaging of local magnetic fields provides a window into the organizing principles of complex and technologically relevant condensed-matter materials. However, a wide variety of intriguing strongly correlated and topologically nontrivial materials exhibit poorly understood phenomena outside the detection capability of state-of-the-art high-sensitivity high-resolution scanning probe magnetometers. We introduce a quantum-noise-limited scanning probe magnetometer that can operate from room-to-cryogenic temperatures with unprecedented dc-field sensitivity and micron-scale resolution. The Scanning Quantum Cryogenic Atom Microscope (SQCRAMscope) employs a magnetically levitated atomic Bose-Einstein condensate (BEC), thereby providing immunity to conductive and blackbody radiative heating. The SQCRAMscope has a field sensitivity of 1.4 nT per resolution-limited point (approximately 2 μ m ) or 6 nT /√{Hz } per point at its duty cycle. Compared to point-by-point sensors, the long length of the BEC provides a naturally parallel measurement, allowing one to measure nearly 100 points with an effective field sensitivity of 600 pT /√{Hz } for each point during the same time as a point-by-point scanner measures these points sequentially. Moreover, it has a noise floor of 300 pT and provides nearly 2 orders of magnitude improvement in magnetic flux sensitivity (down to 10-6 Φ0/√{Hz } ) over previous atomic probe magnetometers capable of scanning near samples. These capabilities are carefully benchmarked by imaging magnetic fields arising from microfabricated wire patterns in a system where samples may be scanned, cryogenically cooled, and easily exchanged. We anticipate the SQCRAMscope will provide charge-transport images at temperatures from room temperature to 4 K in unconventional superconductors and topologically nontrivial materials.

Scalar magnetometers for space applications

DEFF Research Database (Denmark)

Primdahl, Fritz

A survey of existing instrumentation and developments is presented emphasizing instrumentation for in-flight calibration of vector magnetometers on magnetic mapping missions. Proton free or forced precession magnetometers are at the focus as calibration references, because the proton gyromagnetic...

The Magnetospheric Multiscale Magnetometers

Science.gov (United States)

Russell, C. T.; Anderson, B. J.; Baumjohann, W.; Bromund, K. R.; Dearborn, D.; Fischer, D.; Le, G.; Leinweber, H. K.; Leneman, D.; Magnes, W.;

Scalar Calibration of Vector Magnetometers

DEFF Research Database (Denmark)

Merayo, José M.G.; Brauer, Peter; Primdahl, Fritz

2000-01-01

The calibration parameters of a vector magnetometer are estimated only by the use of a scalar reference magnetometer. The method presented in this paper differs from those previously reported in its linearized parametrization. This allows the determination of three offsets or signals in the absence...

Performances and place of magnetometers based on amorphous wires compared to conventional magnetometers

International Nuclear Information System (INIS)

Robbes, D.; Dolabdjian, C.; Monfort, Y.

2002-01-01

We discuss and compare performances of various room temperature magnetometers. The work is directed towards the search of those magnetometers having a high sensitivity (>1000 V/T), a very low noise level (>1 pT/√Hz at white noise) attainable in a volume typically smaller than 1 cm 3 . The choice of this set of parameters is related to the useful comparison of room temperature magnetometers versus cryogenic ones, such as Superconducting Quantum Interferometer Devices (SQUIDs). The latter have highly degraded performances when their working operations needs an open unshielded environment as required for example in industrial application (non-destructive evaluation). SQUIDs have also a rather poor spatial resolution, and could be replaced by room temperature sensors in some magnetic imaging systems, which require a high spatial resolution. The paper is 'highlighted' in the field of magnetic sensors based on amorphous magnetic wires that were used to carry out wide bandwidth (>100 kHz), very low noise flux gate (∼pT/√Hz at white noise) and highly sensitive, low noise magnetometers (∼pT/√Hz at white noise) Colpitts oscillator configuration use by K. Bushida's

Man-Portable Simultaneous Magnetometer and EM System (MSEMS)

Science.gov (United States)

2008-12-01

limited to cesium vapor magnetometers outputting a Larmor signal. It cannot, as presently configured, be used with less expensive fluxgate magnetometers ...pulses to convert the frequency-based Larmor signal into nT. A fluxgate magnetometer does not employ the resonance mechanism of an alkali vapor...Simultaneous Magnetometer and EM System (MSEMS) December 2008 Report Documentation Page Form ApprovedOMB No. 0704-0188 Public reporting burden for the

Equipment for automatic measurement of gamma activity distribution in a column

International Nuclear Information System (INIS)

Kalincak, M.; Machan, V.; Vilcek, S.; Balkovsky, K.

1978-01-01

The design of a device for stepwise scanning of gamma activity distributions along chromatographic columns is described. In connection with a single-channel gamma spectrometer and a counting ratemeter with a recorder this device permits the resolution of a number of gamma emitters on the column, the determination of the gamma nuclide content in different chemical forms in the sample by means of column separation methods - Gel Chromatography Columns Scanning Method - and the determination of gamma nuclide distribution along the columns. The device permits the scanning of columns of up to 20 mm in diameter and 700 mm in length and continual scanning over a 450 mm column length with one clamping. With minor adaptations it is possible to scan columns up to 30 mm in diameter. The length of the scanned sections is 5 or 10 mm, the scanning time setting is arbitrary and variable activity levels and radiation energies may be measured. (author)

Magnetogama: an open schematic magnetometer

Science.gov (United States)

Wahyudi; Khakhim, Nurul; Kuntoro, Tri; Mardiatno, Djati; Rakhman, Afif; Setyo Handaru, Anas; Akhmad Mufaqih, Adien; Marwan Irnaka, Theodosius

2017-09-01

Magnetogama is an open schematic hand-assembled fluxgate magnetometer. Compared to another magnetometer, Magnetogama has more benefit concerning its price and its ease of use. Practically Magnetogama can be utilized either in land or attached to an unmanned aerial vehicle (UAV). Magnetogama was designed to give open access to a cheap and accurate alternative to magnetometer sensor. Therefore it can be used as a standard design which is directly applicable to the low-budget company or education purposes. Schematic, code and several verification tests were presented in this article ensuring its reproducibility. Magnetogama has been tested with two kind of tests: a comparison with two nearest observatories at Learmonth (LRM) and Kakadu (KDU) and the response of magnetic substance.

The Pioneer XI high field fluxgate magnetometer

Science.gov (United States)

Acuna, M. A.; Ness, N. F.

1975-01-01

The high field fluxgate magnetometer experiment flown aboard the Pioneer XI spacecraft is described. This extremely simple instrument was used to extend the spacecraft's upper-limit measurement capability by approximately an order of magnitude (from 0.14 mT to 1.00 mT) with minimum power and volume requirements. This magnetometer was designed to complement the low-field measurements provided by a helium vector magnetometer and utilizes magnetic ring core sensors with biaxial orthogonal sense coils. The instrument is a single-range, triaxial-fluxgate magnetometer capable of measuring fields of up to 1 mT along each orthogonal axis, with a maximum resolution of 1 microT.

Development of a nuclear precession magnetometer

International Nuclear Information System (INIS)

Virgens Alves, J.G. das.

1983-12-01

The objective of this thesis was to develop a proton precession magnetometer for geophysical prospecting and base stations. The proton procession magnetometer measures the total magnetic fields intensity. It operates on the basis of nuclear magnetic resonance by determining the processing frequency of protons of a non viscous liquid in the terrestrial magnetic fields. The instrument was tested in field to evaluate signal/noise ratio, supportable gradient and battery consumption. Application test was carried out to take diurnal variation data and, reconnaissance and detail surveys data on an archaeological site in the Marajo Island-Pa. The test results were confronted with two commercial magnetometers-GP-70, McPhar e G-816, Geometric - and, with data from Observatorio Magnetico Ilha de Tatuoca as well. For all cases, the data comparison showed a good performance of the magnetometer tested. (author)

High transition-temperature SQUID magnetometers and practical applications

International Nuclear Information System (INIS)

Dantsker, E.; Lawrence Berkeley National Lab., CA

1997-05-01

The design, fabrication and performance of SQUID magnetometers based on thin films of the high-transition temperature superconductor YBa 2 Cu 3 O 7-x (YBCO) are described. Essential to the achieving high magnetic field resolution at low frequencies is the elimination of 1/f flux noise due to thermally activated hopping of flux vortices between pinning sites in the superconducting films. Through improvements in processing, 1/f noise in single layer YBCO thin films and YBCO-SrTiO 3 -YBCO trilayers was systematically reduced to allow fabrication of sensitive SQUID magnetometers. Both single-layer directly coupled SQUID magnetometers and multilayer magnetometers were fabricated, based on the dc SQUID with bicrystal grain boundary Josephson junctions. Multilayer magnetometers had a lower magnetic field noise for a given physical size due to greater effective sensing areas. A magnetometer consisting of a SQUID inductively coupled to the multiturn input coil of a flux transformer in a flip-chip arrangement had a field noise of 27 fT Hz -1/2 at 1 Hz and 8.5 fT Hz -1/2 at 1 kHz. A multiloop multilayer SQUID magnetometer had a field noise of 37 fT Hz -1/2 at 1 Hz and 18 fT Hz -1/2 at 1 kHz. A three-axis SQUID magnetometer for geophysical applications was constructed and operated in the field in the presence of 60 Hz and radiofrequency noise. Clinical quality magnetocardiograms were measured using multilayer SQUID magnetometers in a magnetically shielded room

Magnetometer and Gyroscope Calibration Method with Level Rotation

Directory of Open Access Journals (Sweden)

Zongkai Wu

2018-03-01

Full Text Available Micro electro mechanical system (MEMS gyroscopes and magnetometers are usually integrated into a sensor module or chip and widely used in a variety of applications. In existing integrated gyroscope and magnetometer calibration methods, rotation in all possible orientations is a necessary condition for a good calibration result. However, rotation around two or more axes is difficult to attain, as it is limited by the range of movement of vehicles such as cars, ships, or planes. To solve this problem, this paper proposes an integrated magnetometer and gyroscope calibration method with level rotation. The proposed method presents a redefined magnetometer output model using level attitude. New gyroscope and magnetometer calibration models are then deduced. In addition, a simplified cubature Kalman filter (CKF is established to estimate calibration parameters. This method possesses important value for application in actual systems, as it only needs level rotation for real-time calibration of gyroscopes and magnetometers. Theoretical analysis and test results verify the validity and feasibility of this method.

Magnetogama: an open schematic magnetometer

Directory of Open Access Journals (Sweden)

Wahyudi

2017-09-01

Full Text Available Magnetogama is an open schematic hand-assembled fluxgate magnetometer. Compared to another magnetometer, Magnetogama has more benefit concerning its price and its ease of use. Practically Magnetogama can be utilized either in land or attached to an unmanned aerial vehicle (UAV. Magnetogama was designed to give open access to a cheap and accurate alternative to magnetometer sensor. Therefore it can be used as a standard design which is directly applicable to the low-budget company or education purposes. Schematic, code and several verification tests were presented in this article ensuring its reproducibility. Magnetogama has been tested with two kind of tests: a comparison with two nearest observatories at Learmonth (LRM and Kakadu (KDU and the response of magnetic substance.

A Scanning Quantum Cryogenic Atom Microscope

Science.gov (United States)

Lev, Benjamin

Microscopic imaging of local magnetic fields provides a window into the organizing principles of complex and technologically relevant condensed matter materials. However, a wide variety of intriguing strongly correlated and topologically nontrivial materials exhibit poorly understood phenomena outside the detection capability of state-of-the-art high-sensitivity, high-resolution scanning probe magnetometers. We introduce a quantum-noise-limited scanning probe magnetometer that can operate from room-to-cryogenic temperatures with unprecedented DC-field sensitivity and micron-scale resolution. The Scanning Quantum Cryogenic Atom Microscope (SQCRAMscope) employs a magnetically levitated atomic Bose-Einstein condensate (BEC), thereby providing immunity to conductive and blackbody radiative heating. The SQCRAMscope has a field sensitivity of 1.4 nT per resolution-limited point (2 um), or 6 nT / Hz1 / 2 per point at its duty cycle. Compared to point-by-point sensors, the long length of the BEC provides a naturally parallel measurement, allowing one to measure nearly one-hundred points with an effective field sensitivity of 600 pT / Hz1 / 2 each point during the same time as a point-by-point scanner would measure these points sequentially. Moreover, it has a noise floor of 300 pT and provides nearly two orders of magnitude improvement in magnetic flux sensitivity (down to 10- 6 Phi0 / Hz1 / 2) over previous atomic probe magnetometers capable of scanning near samples. These capabilities are for the first time carefully benchmarked by imaging magnetic fields arising from microfabricated wire patterns and done so using samples that may be scanned, cryogenically cooled, and easily exchanged. We anticipate the SQCRAMscope will provide charge transport images at temperatures from room to \\x9D4K in unconventional superconductors and topologically nontrivial materials.

Vector Fluxgate Magnetometer (VMAG) Development for DSX

Science.gov (United States)

2010-06-03

AFRL-RV-HA-TR-2010-1056 Vector Fluxgate Magnetometer (VMAG) Development for DSX Mark B. Moldwin UCLA Institute of Geophysics... Fluxgate Magnetometer (VMAG) Development for DSX 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 62601F 6. AUTHOR(S) Mark B. Moldwin 5d. PROJECT...axis fluxgate magnetometer for the AFRL-mission. The instrument is designed to measure the medium-Earth orbit geomagnetic field with precision of 0.1

High transition-temperature SQUID magnetometers and practical applications

Energy Technology Data Exchange (ETDEWEB)

Dantsker, Eugene [Univ. of California, Berkeley, CA (United States). Dept. of Physics

1997-05-01

The design, fabrication and performance of SQUID magnetometers based on thin films of the high-transition temperature superconductor YBa₂Cu₃O_7-x (YBCO) are described. Essential to the achieving high magnetic field resolution at low frequencies is the elimination of 1/f flux noise due to thermally activated hopping of flux vortices between pinning sites in the superconducting films. Through improvements in processing, 1/f noise in single layer YBCO thin films and YBCO-SrTiO₃-YBCO trilayers was systematically reduced to allow fabrication of sensitive SQUID magnetometers. Both single-layer directly coupled SQUID magnetometers and multilayer magnetometers were fabricated, based on the dc SQUID with bicrystal grain boundary Josephson junctions. Multilayer magnetometers had a lower magnetic field noise for a given physical size due to greater effective sensing areas. A magnetometer consisting of a SQUID inductively coupled to the multiturn input coil of a flux transformer in a flip-chip arrangement had a field noise of 27 fT Hz^-1/2 at 1 Hz and 8.5 fT Hz^-1/2 at 1 kHz. A multiloop multilayer SQUID magnetometer had a field noise of 37 fT Hz^-1/2 at 1 Hz and 18 fT Hz^-1/2 at 1 kHz. A three-axis SQUID magnetometer for geophysical applications was constructed and operated in the field in the presence of 60 Hz and radiofrequency noise. Clinical quality magnetocardiograms were measured using multilayer SQUID magnetometers in a magnetically shielded room.

Directly coupled YBCO dc SQUID magnetometers

International Nuclear Information System (INIS)

Petersen, P.R.E.; Shen, Y.Q.; Holst, T.; Larsen, B.H.; Sager, M.P.; Bindslev Hansen, J.

1999-01-01

YBa 2 Cu 3 O 7- x magnetometers have been made on 10mmx10mm MgO substrates by directly coupling the magnetometer pick-up loop to a dc SQUID with narrow strip lines. The dc SQUIDs were made with YBa 2 Cu 3 O 7-x step-edge Josephson junctions. The layout of the magnetometer pick-up loop was chosen as a compromise between maximizing the loop effective area and minimizing the loop inductance. The SQUID was designed to have L S ∼100 pH in order to obtain β L =2I 0 L S /Φ 0 approx.= 1 with the single-junction critical current I 0 ∼10 μA. We have made magnetometers with white noise levels down to 55 fT Hz -1/2 and a 1/f knee at 1 Hz (ac biased). Noise measurements were made on a field-cooled magnetometer. The noise measured at 1 Hz when cooled in 'zero field' was 175 fT Hz -1/2 . When cooled in magnetic fields of B = 50 μT and B = 100 μT we measured the noise at 1 Hz to be 430 fT Hz -1 2 and 1.3 pT Hz -1/2 , respectively. (author)

Choice of Magnetometers and Gradiometers after Signal Space Separation.

Science.gov (United States)

Garcés, Pilar; López-Sanz, David; Maestú, Fernando; Pereda, Ernesto

2017-12-16

Modern Elekta Neuromag MEG devices include 102 sensor triplets containing one magnetometer and two planar gradiometers. The first processing step is often a signal space separation (SSS), which provides a powerful noise reduction. A question commonly raised by researchers and reviewers relates to which data should be employed in analyses: (1) magnetometers only, (2) gradiometers only, (3) magnetometers and gradiometers together. The MEG community is currently divided with regard to the proper answer. First, we provide theoretical evidence that both gradiometers and magnetometers result from the backprojection of the same SSS components. Then, we compare resting state and task-related sensor and source estimations from magnetometers and gradiometers in real MEG recordings before and after SSS. SSS introduced a strong increase in the similarity between source time series derived from magnetometers and gradiometers (r² = 0.3-0.8 before SSS and r² > 0.80 after SSS). After SSS, resting state power spectrum and functional connectivity, as well as visual evoked responses, derived from both magnetometers and gradiometers were highly similar (Intraclass Correlation Coefficient > 0.8, r² > 0.8). After SSS, magnetometer and gradiometer data are estimated from a single set of SSS components (usually ≤ 80). Equivalent results can be obtained with both sensor types in typical MEG experiments.

Observatory Magnetometer In-Situ Calibration

Directory of Open Access Journals (Sweden)

A Marusenkov

2011-07-01

Full Text Available An experimental validation of the in-situ calibration procedure, which allows estimating parameters of observatory magnetometers (scale factors, sensor misalignment without its operation interruption, is presented. In order to control the validity of the procedure, the records provided by two magnetometers calibrated independently in a coil system have been processed. The in-situ estimations of the parameters are in very good agreement with the values provided by the coil system calibration.

Tuned optical cavity magnetometer

Science.gov (United States)

Okandan, Murat; Schwindt, Peter

2010-11-02

An atomic magnetometer is disclosed which utilizes an optical cavity formed from a grating and a mirror, with a vapor cell containing an alkali metal vapor located inside the optical cavity. Lasers are used to magnetically polarize the alkali metal vapor and to probe the vapor and generate a diffracted laser beam which can be used to sense a magnetic field. Electrostatic actuators can be used in the magnetometer for positioning of the mirror, or for modulation thereof. Another optical cavity can also be formed from the mirror and a second grating for sensing, adjusting, or stabilizing the position of the mirror.

Development of a Micro-Fabricated Total-Field Magnetometer

Science.gov (United States)

2011-03-01

are made with fluxgate technologies. Fluxgates have lower sensitivity than Cs magnetometers , yet they continue to be used in small wands simply...extraction process by providing the sensitivity of a Cs magnetometer with the convenience and low cost of a fluxgate wand. Extremely small and low cost...FINAL REPORT Development of a Micro-Fabricated Total-Field Magnetometer SERDP Project MR-1512 MARCH 2011 Mark Prouty Geometrics, Inc

Optical Magnetometer Incorporating Photonic Crystals

Science.gov (United States)

Kulikov, Igor; Florescu, Lucia

2007-01-01

According to a proposal, photonic crystals would be used to greatly increase the sensitivities of optical magnetometers that are already regarded as ultrasensitive. The proposal applies, more specifically, to a state-of-the-art type of quantum coherent magnetometer that exploits the electromagnetically-induced-transparency (EIT) method for determining a small change in a magnetic field indirectly via measurement of the shift, induced by that change, in the hyperfine levels of resonant atoms exposed to the field.

THOR Fluxgate Magnetometer (MAG)

Science.gov (United States)

Nakamura, Rumi; Eastwood, Jonathan; Magnes, Werner; Carr, Christopher, M.; O'Brien, Helen, L.; Narita, Yasuhito; K, Chen, Christopher H.; Berghofer, Gerhard; Valavanoglou, Aris; Delva, Magda; Plaschke, Ferdinand; Cupido, Emanuele; Soucek, Jan

2017-04-01

Turbulence Heating ObserveR (THOR) is the first mission ever flown in space dedicated to plasma turbulence. The fluxgate Magnetometer (MAG) measures the background to low frequency magnetic field. The high sensitivity measurements of MAG enable to characterize the nature of turbulent fluctuations as well as the large-scale context. MAG will provide the reference system for determining anisotropy of field fluctuations, pitch-angle and gyro-phase of particles. The design of the magnetometer consists of two tri-axial sensors and the related magnetometer electronics; the electronics are hosted on printed circuit boards in the common electronics box of the fields and wave processor (FWP). A fully redundant two- sensor system mounted on a common boom and the new miniaturized low noise design based on MMS and Solar Orbiter instruments enable accurate measurement throughout the region of interest for THOR science. The usage of the common electronics hosted by FWP guarantees to fulfill the required timing accuracy with other fields measurements. These improvements are important to obtain precise measurements of magnetic field, which is essential to estimate basic plasma parameters and correctly identify the spatial and temporal scales of the turbulence. Furthermore, THOR MAG provides high quality data with sufficient overlap with the Search Coil Magnetometer (SCM) in frequency space to obtain full coverage of the wave forms over all the frequencies necessary to obtain the full solar wind turbulence spectrum from MHD to kinetic range with sufficient accuracy. We discuss the role of MAG in THOR key science questions and present the new developments during Phase A such as the finalised instrument design, MAG relevant requirement, and new calibraion schemes.

Atomic magnetometer for human magnetoencephalograpy.

Energy Technology Data Exchange (ETDEWEB)

Schwindt, Peter; Johnson, Cort N.

2010-12-01

We have developed a high sensitivity (<5 fTesla/{radical}Hz), fiber-optically coupled magnetometer to detect magnetic fields produced by the human brain. This is the first demonstration of a noncryogenic sensor that could replace cryogenic superconducting quantum interference device (SQUID) magnetometers in magnetoencephalography (MEG) and is an important advance in realizing cost-effective MEG. Within the sensor, a rubidium vapor is optically pumped with 795 laser light while field-induced optical rotations are measured with 780 nm laser light. Both beams share a single optical axis to maximize simplicity and compactness. In collaboration with neuroscientists at The Mind Research Network in Albuquerque, NM, the evoked responses resulting from median nerve and auditory stimulation were recorded with the atomic magnetometer and a commercial SQUID-based MEG system with signals comparing favorably. Multi-sensor operation has been demonstrated with two AMs placed on opposite sides of the head. Straightforward miniaturization would enable high-density sensor arrays for whole-head magnetoencephalography.

Evaluating Detection and Estimation Capabilities of Magnetometer-Based Vehicle Sensors

Science.gov (United States)

2012-05-01

fluxgate magnetometers whose operating characteristics are well documented [1, 2]. Such magnetometers measure two perpendicular magnetic components of...of surveillance scenarios. As part of that work, this analysis focuses on UGS utilizing of two-axis fluxgate magnetometers . Two MOPs are 12 -60 -40 -20...Proceedings of the IEEE, 78(6):973–989, June 1990. [2] E. M. Billingsley and S. W. Billingsley. Fluxgate magnetometers . Proceedings of the IEEE, 5090(194

Comparative investigation of the gel chromatography column scanning method for quality control of /sup 99/sup(m)Tc-methylenediphosphonate

Energy Technology Data Exchange (ETDEWEB)

Darte, L

1981-04-01

Gel chromatography column scanning (GCS) is the method of choice for quality control of sup(99m)Tc-MDP preparations. Using this method all the labelled components are obtained rapidly in one simple test procedure. The influence of various parameters such as gel type, column size, prehistory of column, equilibration, eluent, elution volume and flow rate upon the results have been investigated. Test results for sup(99 m)Tc-MDP have been compared for several different GCS systems, a few TLC systems and column chromatography with fraction collection. The GCS technique, optimized for testing sup(99m)Tc-MDP preparations has been applied in a few experiments in which very good reproducibility is required: Labelling kinetics and stability when stored at room temperature or in a refrigerator and influence of the sup(99m)Te/(sup(99m)Tc + /sup 99/Tc) atomic ratio and of the amount of radioactivity on the sup(99m)Tc-MDP labelling yield, covering parameter ranges of clinical interest, have been studied.

Development and application of gamma scanning technology for on-line investigation of industrial process columns and vessels

International Nuclear Information System (INIS)

Jaafar Abdullah

1999-01-01

Plant Assessment Technology (PAT) group, in association with Intelligent System (IS) Group and Engineering Services Department of Malaysian Institute for Nuclear Technology Research (MINT) has developed gamma scanning facilities for on-line investigation of industrial process columns and vessels. The technology, based on the principle of gamma-ray absorption, has been successfully applied for troubleshooting of a number of distillation columns and process vessels in petroleum refineries, gas processing plants and chemical plants in the country and the region. This paper outlines basic characteristics of the system and describes the inspection procedures, and in addition, case studies are also presented. The case studies are purposely chosen to illustrate the versatility of the technology, and furthermore to demonstrate the economic benefits which can be realised from the application of this technology. (author)

Vector Magnetometer Application with Moving Carriers

Directory of Open Access Journals (Sweden)

Andrii Prystai

2016-12-01

Full Text Available In magnetic prospecting the aeromagnetic survey is a widespread method used for research in large territories or in the areas with difficult access (forests, swamps, shallow waters. At present, a new type of mobile carriers – remotely piloted vehicles or drones – is becoming very common. The drones supplied by magnetometer can be also used for underground utility location (for example, steel and concrete constructions, buried power cables, to name a few. For aeromagnetic survey, obtaining of 3-component magnetic field data gives higher processing precision, so the fluxgate magnetometers (FGM seem to be the most preferable by reason of low weight, noise, power consumption and costs. During movement of FGM fixed to a drone practically permanent attitude changes in the Earth’s magnetic field arises with corresponding changes of its projection at FGM axes. Also the electromagnetic interference from the drone motor and uncontrolled oscillations of drone and suspension are the factors which limit the magnetometer sensitivity level. Aroused because of this, signals significantly exceed the expected signals from a studied object and so should be removed by proper interference filtration and use of stabilized towed construction, as well as at data processing. To find the necessary resolution threshold of a drone-portable FGM, the modeling was made to estimate magnetic field value from a small sphere about 1 cm radius at the minimal altitude of drone flight and it was shown that such a small object can be reliably detected if the FGM noise level is less than 0.15 nT. Next requirement is the necessity to decrease as much as possible the FGM power consumption with retention of low noise level. Finally, because of drone movement, the broadening of a frequency range should be done. The LEMI-026 magnetometer was developed satisfying all requirements to the drone-mounted device. The field tests were successfully performed using two of LEMI-026

Magnetometer calibration and test procedure

International Nuclear Information System (INIS)

Squier, D.M.

1997-01-01

Nuclear waste has been sluiced and pumped from storage tank 241-AX-104, leaving a contaminated heel volume. These operations did not include measurements of the removed waste volume leaving an unknown heel volume in the tank. A magnetometer transducer will be lowered through tank riser ports to rest on the heel's surface. The heel thickness will control the distance between the transducer and the tank's bottom The instrument's output varies with the distance from a magnetic mass, such as the tank's steel bottom, thereby enabling a measurement of the heel depth. Measurements at several tank locations will permit an estimate of the tank's heel volume. The magnetometer's output is influenced by adjacent magnetic materials, such as the tank walls, air lift circulators or other equipment installed in the tank. An adjacent vertical steel surface produces a voltage offset in the instrument's output. Measurements near a tank wall or other tank components may be corrected by noting the offset before the instrument's output is influenced by the tank bottom. An unlevel or uneven heel surface could orient the magnetometer transducer so that it is not vertically level. The magnetometer readings are influenced by these skewed transducer orientations. The magnitude of these errors and offsets must be characterized to bound the heel volume estimate range. The data collected by this activity will be statistically analyzed by SESC to state the confidence level of the heel volume estimates. A test report will document the results of the measurements

The MAGSAT vector magnetometer: A precision fluxgate magnetometer for the measurement of the geomagnetic field

Science.gov (United States)

Acuna, M. H.; Scearce, C. S.; Seek, J.; Scheifele, J.

1978-01-01

A description of the precision triaxial fluxgate magnetometer to be flown aboard the MAGSAT spacecraft is presented. The instrument covers the range of + or - 64,000 nT with a resolution of + or - 0.5 nT, an intrinsic accuracy of + or - 0.001% of full scale and an angular alignment stability of the order of 2 seconds of arc. It was developed at NASA's Goddard Space Flight Center and represents the state-of-the-art in precision vector magnetometers developed for spaceflight use.

A simple fluxgate magnetometer using amorphous alloys

International Nuclear Information System (INIS)

Ghatak, S.K.; Mitra, A.

1992-01-01

A simple fluxgate magnetometer is developed using low magnetostrictive ferromagnetic amorphous alloy acting as a sensing element. It uses the fact that the magnetization of sensing element symmetrically magnetized by a sinusoidal field contains even harmonic components in presence of dc signal field H and the amplitude of the second harmonic component of magnetization is proportional to H. The sensitivity and linearity of the magnetometer with signal field are studied for parallel configuration and the field ranging from 10 nT to 10 μT can be measured. The functioning of the magnetometer is demonstrated by studying the shielding and flux-trapping phenomena in high-Tc superconductor. (orig.)

Gamma-ray scanning for troubleshooting and optimisation of distillation columns in petroleum refineries and chemical plants

International Nuclear Information System (INIS)

Jaafar Abdullah

2001-01-01

The technique and facilities for gamma-ray scanning have been developed by the Plant Assessment Technology (PAT) Group at the Malaysian Institute for Nuclear Technology Research (MINT). The technology has been successfully used for on-line troubleshooting and investigation of various types of distillation columns in petroleum refineries, gas processing installations and chemical plants in the country and the region. This paper outlines the basic principle of the technology and describes the inspection procedures, and in addition, a few case studies are presented. (Author)

Silent Localization of Underwater Sensors Using Magnetometers

Directory of Open Access Journals (Sweden)

Jonas Callmer

2010-01-01

Full Text Available Sensor localization is a central problem for sensor networks. If the sensor positions are uncertain, the target tracking ability of the sensor network is reduced. Sensor localization in underwater environments is traditionally addressed using acoustic range measurements involving known anchor or surface nodes. We explore the usage of triaxial magnetometers and a friendly vessel with known magnetic dipole to silently localize the sensors. The ferromagnetic field created by the dipole is measured by the magnetometers and is used to localize the sensors. The trajectory of the vessel and the sensor positions are estimated simultaneously using an Extended Kalman Filter (EKF. Simulations show that the sensors can be accurately positioned using magnetometers.

Battlefield Applications for the Polatomic 2000 Magnetometer/Gradiometer

National Research Council Canada - National Science Library

Kuhlman, G

2002-01-01

... He(4) scalar magnetometer/gradiometer. A major innovation in the P-2000 helium magnetometer is the introduction of a laser pump source to replace the conventional RF discharge helium lamp used in the Navy AN/ASQ-81/208 MAD Set...

Digital fluxgate magnetometer: design notes

International Nuclear Information System (INIS)

Belyayev, Serhiy; Ivchenko, Nickolay

2015-01-01

We presented an approach to understanding the performance of a fully digital fluxgate magnetometer. All elements of the design are important for the performance of the instrument, and the presence of the digital feed-back loop introduces certain peculiarities affecting the noise and dynamic performance of the instrument. Ultimately, the quantisation noise of the digital to analogue converter is found to dominate the noise of the current design, although noise shaping alleviates its effect to some extent. An example of magnetometer measurements on board a sounding rocket is presented, and ways to further improve the performance of the instrument are discussed. (paper)

Digital fluxgate magnetometer: design notes

Science.gov (United States)

Belyayev, Serhiy; Ivchenko, Nickolay

2015-12-01

We presented an approach to understanding the performance of a fully digital fluxgate magnetometer. All elements of the design are important for the performance of the instrument, and the presence of the digital feed-back loop introduces certain peculiarities affecting the noise and dynamic performance of the instrument. Ultimately, the quantisation noise of the digital to analogue converter is found to dominate the noise of the current design, although noise shaping alleviates its effect to some extent. An example of magnetometer measurements on board a sounding rocket is presented, and ways to further improve the performance of the instrument are discussed.

Digital fluxgate magnetometer for the "Astrid-2" satellite

DEFF Research Database (Denmark)

Pedersen, Erik Bøje; Primdahl, Fritz; Petersen, Jan Raagaard

1999-01-01

The design and performance of the Astrid-2 magnetometer are described. The magnetometer uses mathematical routines implemented by software for commercially available digital dignal processors to determine the magnetic field from the fluxgate sensor. The sensor is from the latest generation of amo...

Research on Intelligent Control System of DC SQUID Magnetometer Parameters for Multi-channel System

Science.gov (United States)

Chen, Hua; Yang, Kang; Lu, Li; Kong, Xiangyan; Wang, Hai; Wu, Jun; Wang, Yongliang

2018-03-01

In a multi-channel SQUID measurement system, adjusting device parameters to optimal condition for all channels is time-consuming. In this paper, an intelligent control system is presented to determine the optimal working point of devices which is automatic and more efficient comparing to the manual one. An optimal working point searching algorithm is introduced as the core component of the control system. In this algorithm, the bias voltage V_bias is step scanned to obtain the maximal value of the peak-to-peak current value I_pp of the SQUID magnetometer modulation curve. We choose this point as the optimal one. Using the above control system, more than 30 weakly damped SQUID magnetometers with area of 5 × 5 mm^2 or 10 × 10 mm^2 are adjusted and a 36-channel magnetocardiography system perfectly worked in a magnetically shielded room. The average white flux noise is 15 μΦ_0/Hz^{1/2}.

On the control of magnetic perturbing field onboard landers: the Magnetometer Protection program for the ESA ExoMars/Humboldt MSMO magnetometer experiment

DEFF Research Database (Denmark)

Menvielle, M.; Primdahl, Fritz; Brauer, Peter

to planetary research. The major difficulty in implementing a magnetometer experiment onboard a lander is to achieve at acceptable costs a good Magnetometer Protection, namely to control the perturbing magnetic field generated by the lander during operations at the planetary surfa ce, so as to achieve...... scientific payload in the frame of the ESA ExoMars mission. Experience from previous missions constitutes the background for the MSMO Magnetometer Protection strategy. DC and AC lander generated magnetic perturbations are discussed, with particular attention to those related to solar generators. Emphasis...... and very resource consuming....

Development of the data logging and graphical presentation for gamma scanning, trouble shooting and process evaluation in the petroleum refinery column

International Nuclear Information System (INIS)

Saengchantr, Dhanaj; Chueinta Siripone

2009-07-01

Full text: Software of data logging and graphical presentation on gamma scanning for trouble shooting and process evaluation of the petroleum refinery column was developed. While setting the gamma source and gamma detector at the opposite orientation along side the column and recording the transmitted radiation through the column at several elevations, the relative density gamma intensity vs. vertical elevation could be obtained in the graphical mode. In comparison with engineering drawing, the physical and process abnormalities could be clearly evaluated during field investigation. The program could also accumulate up to 8 data sets, each of 1,000 points allowing with convenience, the comparison of different operational parameters adjustment during remedy of the problem and/or process optimization. Incorporated with this development and other factors, the technology capability of the TINT Service Center to the petroleum refinery was also enhanced

A development of super computed tomography scanner for industrial column investigation

International Nuclear Information System (INIS)

Abdul Quddoos Abu Bakar; Jaafar Abdullah; Ismail Mustapha

2004-01-01

Computed Tomography (CT) scanner is a desired devices on create images of internal structure of unrecognized object. The formation of a CT images is a distinct three phase process. The scanning phase produces data, but not an image. Then, reconstruction phase processes the acquired data and forms a digital image. The visible and displayed analog image is produced by the digital to analog conversation phase. In this case, there are adjustable factors associated with each of these phases that can have an effect on the characteristics and quantity of the image. In term on this project of column scanning, during the scanning phase a fan-shaped gamma ray beam is scanned around the column. The amount of gamma radiation that penetrates the column along each individual ray (pathway) through the column is measured by the detectors that intercept the gamma ray beam after it passes through the column.This project of Super Computed Tomography (CT) is develop to reconstruct and redesign the mechanical parts and equipment to suits the purpose of the industrial column investigation in the region. (Author)

Modeling a Miniaturized Scanning Electron Microscope Focusing Column - Lessons Learned in Electron Optics Simulation

Science.gov (United States)

Loyd, Jody; Gregory, Don; Gaskin, Jessica

2016-01-01

This presentation discusses work done to assess the design of a focusing column in a miniaturized Scanning Electron Microscope (SEM) developed at the NASA Marshall Space Flight Center (MSFC) for use in-situ on the Moon-in particular for mineralogical analysis. The MSFC beam column design uses purely electrostatic fields for focusing, because of the severe constraints on mass and electrical power consumption imposed by the goals of lunar exploration and of spaceflight in general. The resolution of an SEM ultimately depends on the size of the focused spot of the scanning beam probe, for which the stated goal here is a diameter of 10 nanometers. Optical aberrations are the main challenge to this performance goal, because they blur the ideal geometrical optical image of the electron source, effectively widening the ideal spot size of the beam probe. In the present work the optical aberrations of the mini SEM focusing column were assessed using direct tracing of non-paraxial rays, as opposed to mathematical estimates of aberrations based on paraxial ray-traces. The geometrical ray-tracing employed here is completely analogous to ray-tracing as conventionally understood in the realm of photon optics, with the major difference being that in electron optics the lens is simply a smoothly varying electric field in vacuum, formed by precisely machined electrodes. Ray-tracing in this context, therefore, relies upon a model of the electrostatic field inside the focusing column to provide the mathematical description of the "lens" being traced. This work relied fundamentally on the boundary element method (BEM) for this electric field model. In carrying out this research the authors discovered that higher accuracy in the field model was essential if aberrations were to be reliably assessed using direct ray-tracing. This led to some work in testing alternative techniques for modeling the electrostatic field. Ultimately, the necessary accuracy was attained using a BEM

Self-Compensating Excitation of Fluxgate Sensors for Space Magnetometers

DEFF Research Database (Denmark)

Cerman, Alec; Merayo, José M.G.; Brauer, Peter

2008-01-01

The paper presents design and implementation of the new self-compensating excitation circuitry to the new generation of high-precise space vector magnetometers. The application starts with complex study including design of new robust model of the non-linear inductor leading to investigation...... of the most crucial points, continuous by design of the self-compensating excitation unit and concludes with unit complex testing and application to the magnetometer. The application of the self-compensation of the excitation decreases temperature drift of the magnetometer offset caused by the temperature...

Analysing Harmonic Motions with an iPhone's Magnetometer

Science.gov (United States)

Yavuz, Ahmet; Temiz, Burak Kagan

2016-01-01

In this paper, we propose an experiment for analysing harmonic motion using an iPhone's (or iPad's) magnetometer. This experiment consists of the detection of magnetic field variations obtained from an iPhone's magnetometer sensor. A graph of harmonic motion is directly displayed on the iPhone's screen using the "Sensor Kinetics"…

High-sensitivity dc field magnetometer using nonlinear resonance magnetoelectric effect

International Nuclear Information System (INIS)

Burdin, D.A.; Chashin, D.V.; Ekonomov, N.A.; Fetisov, Y.K.; Stashkevich, A.A.

2016-01-01

The design and operation principle of dc field magnetometer using nonlinear resonance magnetoelectric effect in a ferromagnetic–piezoelectric structure are described. It is shown that under action of ac pumping magnetic field the structure generates the output voltage containing higher harmonics whose amplitudes depend on the dc magnetic field. Best performance of the device is obtained if the signal of the third harmonics is used for the dc field measurement. The sensitivity can be considerably (by approximately three orders of magnitude) increased if advantage is taken of the acoustic resonance of the structure at this frequency. There exists the optimal pumping field ensuring the highest sensitivity. Further increasing of this field expands the range of measurable dc fields at the expense of deteriorated sensitivity. The magnetometer fabricated on the basis of a planar langatate-Metglas structure had sensitivity up to ~1 V/Oe and allowed detection of the fields as low as ~10"−"5 Oe. - Highlights: • Operational principle and design of new type dc field magnetometer is described. • Magnetometer uses nonlinear magnetoelectric effect in a langatate-Metglas structure. • Magnetometer has sensitivity of ~1 V/Oe and detects fields as low as 10"−"5 Oe. • The proposed magnetometer can compete with well known fluxgate sensors.

High-sensitivity dc field magnetometer using nonlinear resonance magnetoelectric effect

Energy Technology Data Exchange (ETDEWEB)

Burdin, D.A.; Chashin, D.V.; Ekonomov, N.A. [Moscow State University of Information Technologies, Radio Engineering and Electronics, Moscow (Russian Federation); Fetisov, Y.K., E-mail: fetisov@mirea.ru [Moscow State University of Information Technologies, Radio Engineering and Electronics, Moscow (Russian Federation); Stashkevich, A.A. [LSPM (CNRS-UPR 3407), Université Paris 13, Sorbonne Paris Cité, 93430 Villetaneuse (France)

2016-05-01

The design and operation principle of dc field magnetometer using nonlinear resonance magnetoelectric effect in a ferromagnetic–piezoelectric structure are described. It is shown that under action of ac pumping magnetic field the structure generates the output voltage containing higher harmonics whose amplitudes depend on the dc magnetic field. Best performance of the device is obtained if the signal of the third harmonics is used for the dc field measurement. The sensitivity can be considerably (by approximately three orders of magnitude) increased if advantage is taken of the acoustic resonance of the structure at this frequency. There exists the optimal pumping field ensuring the highest sensitivity. Further increasing of this field expands the range of measurable dc fields at the expense of deteriorated sensitivity. The magnetometer fabricated on the basis of a planar langatate-Metglas structure had sensitivity up to ~1 V/Oe and allowed detection of the fields as low as ~10{sup −5} Oe. - Highlights: • Operational principle and design of new type dc field magnetometer is described. • Magnetometer uses nonlinear magnetoelectric effect in a langatate-Metglas structure. • Magnetometer has sensitivity of ~1 V/Oe and detects fields as low as 10{sup −5} Oe. • The proposed magnetometer can compete with well known fluxgate sensors.

High Accuracy Vector Helium Magnetometer

Data.gov (United States)

National Aeronautics and Space Administration — The proposed HAVHM instrument is a laser-pumped helium magnetometer with both triaxial vector and omnidirectional scalar measurement capabilities in a single...

Design of a Low-Cost 2-Axes Fluxgate Magnetometer for Small Satellite Applications

Directory of Open Access Journals (Sweden)

Su-Jeoung Kim

2005-03-01

Full Text Available This paper addresses the design and analysis results of a 2-axes magnetometer for attitude determination of small satellite. A low-cost and efficient 2-axes fluxgate magnetometer was selected as the most suitable attitude sensor for LEO microsatellites which require a low-to-medium level pointing accuracy. An optimization trade-off study has been performed for the development of 2-axes fluxgate magnetometer. All the relevant parameters such as permeability, demagnetization factor, coil diameter, core thickness, and number of coil turns were considered for the sizing of a small satellite magnetometer. The magnetometer which is designed, manufactured, and tested in-house as described in this paper satisfies linearity requirement for determining attitude position of small satellites. On the basis of magnetometer which is designed in Space System Research Lab. (SSRL, commercial magnetometer will be developed.

Development of autonomous magnetometer rotorcraft for wide area assessment

Energy Technology Data Exchange (ETDEWEB)

Roelof Versteeg; Matt Anderson; Les Beard; Eric Corban; Darryl Curley; Jeff Gamey; Ross Johnson; Dwight Junkin; Mark McKay; Jared Salzmann; Mikhail Tchernychev; Suraj Unnikrishnan; Scott Vinson

2010-04-01

Large areas across the United States are potentially contaminated with UXO, with some ranges encompassing tens to hundreds of thousands of acres. Technologies are needed which will allow for cost effective wide area scanning with 1) near 100 % coverage and 2) near 100 % detection of subsurface ordnance or features indicative of subsurface ordnance. The current approach to wide area assessment is a multi-level one, in which medium - altitude fixed wing optical imaging is used for an initial site assessment. This assessment is followed with low altitude manned helicopter based magnetometry. Subsequent to this wide area assessment targeted surface investigations are performed using either towed geophysical sensor arrays or man portable sensors. In order to be an effective tool for small UXO detection, the sensing altitude for magnetic site investigations needs to be on the order of 1 – 3 meters. These altitude requirements mean that manned helicopter surveys will generally only be feasible in large, open and relatively flat terrains. While such surveys are effective in mapping large areas relatively fast there are substantial mobilization/demobilization, staffing and equipment costs associated with these surveys (resulting in costs of approximately $100-$150/acre). In addition, due to the low altitude there are substantial risks to pilots and equipment. Surface towed arrays provide high resolution maps but have other limitations, e.g. in their ability to navigate rough terrain effectively. There is thus a need for other systems which can be used for effective data collection. An UAV (Unmanned Aerial Vehicle) magnetometer platform is an obvious alternative. The motivation behind such a system is that it reduces risk to operators, is lower in initial and Operational and Maintenance (O&M) costs (and can thus potentially be applied to smaller sites) and has the potential of being more effective in terms of detection and possibly characterization (through the use of

Search Coil vs. Fluxgate Magnetometer Measurements at Interplanetary Shocks

Science.gov (United States)

Wilson, L.B., III

2012-01-01

We present magnetic field observations at interplanetary shocks comparing two different sample rates showing significantly different results. Fluxgate magnetometer measurements show relatively laminar supercritical shock transitions at roughly 11 samples/s. Search coil magnetometer measurements at 1875 samples/s, however, show large amplitude (dB/B as large as 2) fluctuations that are not resolved by the fluxgate magnetometer. We show that these fluctuations, identified as whistler mode waves, would produce a significant perturbation to the shock transition region changing the interpretation from laminar to turbulent. Thus, previous observations of supercritical interplanetary shocks classified as laminar may have been under sampled.

Induction Magnetometers – Design Peculiarities

Directory of Open Access Journals (Sweden)

Valeriy KOREPANOV

2010-09-01

Full Text Available Induction or search-coil magnetometers (IM are widely used in many branches of science and industry. The frequency range and dynamic range of IMs are probably the widest of all existing magnetometers: they are used for the measurement of magnetic field variations in the frequency band from ~10-4 till ~106 Hz with the intensities from fractions of femtotesla till tens of tesla. This explains the permanent interest to IM design and the attempts to construct the IMs with best possible parameters. The present paper deals with the peculiarities of IM design. An attempt to re-establish the correctness of priorities in the field is made and the approaches to the IM optimization and their quality estimation are described.

Preliminary Report: DESiGN and Test Result of KSR-3 Rocket Magnetometers

Directory of Open Access Journals (Sweden)

Hyo-Min Kim

2000-12-01

Full Text Available The solar wind contributes to the formation of unique space environment called the Earth's magnetosphere by various interactions with the Earth's magnetic field. Thus the solar-terrestrial environment affects the Earth's magnetic field, which can be observed with an instrument for the magnetic field measurement, the magnetometer usually mounted on the rocket and the satellite and based on the ground observatory. The magnetometer is a useful instrument for the spacecraft attitude control as well as the Earth's magnetic field measurements for a scientific purpose. In this paper, we present the preliminary design and test results of the two onboard magnetometers of KARI's (Korea Aerospace Research Institute sounding rocket, KSR-3, which will be launched four times during the period of 2001-02. The KSR-3 magnetometers consist of the fluxgate magnetometer, MAG/AIM (Attitude Information Magnetometer for acquiring the rocket flight attitude information, and of the search-coil magnetometer, MAG/SIM (Scientific Investigation Magnetometer for the observation of the Earth's magnetic field fluctuations. With the MAG/AIM, the 3-axis attitude information can be acquired by the comparison of the resulting dc magnetic vector field with the IGRF (International Geomagnetic Reference Field. The Earth's magnetic field fluctuations ranging from 10 to 1,000 Hz can also be observed with the MAG/SIM measurement.

Calibration of three-axis magnetometers with differential evolution algorithm

International Nuclear Information System (INIS)

Pang, Hongfeng; Zhang, Qi; Wang, Wei; Wang, Junya; Li, Ji; Luo, Shitu; Wan, Chengbiao; Chen, Dixiang; Pan, Mengchun; Luo, Feilu

2013-01-01

The accuracy of three-axis magnetometers is influenced by different scale and bias of each axis and nonorthogonality between axes. One limitation of traditional iteration methods is that initial parameters influence the calibration, thus leading to the local optimal or wrong results. In this paper, a new method is proposed to calibrate three-axis magnetometers. To employ this method, a nonmagnetic rotation platform, a proton magnetometer, a DM-050 three-axis magnetometer and the differential evolution (DE) algorithm are used. The performance of this calibration method is analyzed with simulation and experiment. In simulation, the calibration results of DE, unscented Kalman filter (UKF), recursive least squares (RLS) and genetic algorithm (GA) are compared. RMS error using DE is least, which is reduced from 81.233 nT to 1.567 nT. Experimental results show that comparing with UKF, RLS and GA, the DE algorithm has not only the least calibration error but also the best robustness. After calibration, RMS error is reduced from 68.914 nT to 2.919 nT. In addition, the DE algorithm is not sensitive to initial parameters, which is an important advantage compared with traditional iteration algorithms. The proposed algorithm can avoid the troublesome procedure to select suitable initial parameters, thus it can improve the calibration performance of three-axis magnetometers. - Highlights: • The calibration results and robustness of UKF, GA, RLS and DE algorithm are analyzed. • Calibration error of DE is the least in simulation and experiment. • Comparing with traditional calibration algorithms, DE is not sensitive to initial parameters. • It can improve the calibration performance of three-axis magnetometers

Ultra-sensitive Magnetic Microscopy with an Atomic Magnetometer

Energy Technology Data Exchange (ETDEWEB)

Kim, Young Jin [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2015-08-19

The PowerPoint presentation focused on research goals, specific information about the atomic magnetometer, response and resolution factors of the SERF magnetometer, FC+AM systems, tests of field transfer and resolution on FC, gradient cancellation, testing of AM performance, ideas for a multi-channel AM, including preliminary sensitivity testing, and a description of a 6 channel DAQ system. A few ideas for future work ended the presentation.

Analysing harmonic motions with an iPhone’s magnetometer

Science.gov (United States)

Yavuz, Ahmet; Kağan Temiz, Burak

2016-05-01

In this paper, we propose an experiment for analysing harmonic motion using an iPhone’s (or iPad’s) magnetometer. This experiment consists of the detection of magnetic field variations obtained from an iPhone’s magnetometer sensor. A graph of harmonic motion is directly displayed on the iPhone’s screen using the Sensor Kinetics application. Data from this application was analysed with Eureqa software to establish the equation of the harmonic motion. Analyses show that the use of an iPhone’s magnetometer to analyse harmonic motion is a practical and effective method for small oscillations and frequencies less than 15-20 Hz.

Correlation between fluxgate and SQUID magnetometer data sets for geomagnetic storms

Directory of Open Access Journals (Sweden)

Matladi Thabang

2014-01-01

Full Text Available There has always been a need to monitor the near Earth's magnetic field, as this monitoring provides understanding and possible predictions of Space Weather events such as geomagnetic storms. Conventional magnetometers such as fluxgates have been used for decades for Space Weather research. The use of highly sensitive magnetometers such as Superconducting QUantum Interference Devices (SQUIDs, promise to give more insight into Space Weather. SQUIDs are relatively recent types of magnetometers that exploit the superconductive effects of flux quantization and Josephson tunneling to measure magnetic flux. SQUIDs have a very broad bandwidth compared to most conventional magnetometers and can measure magnetic flux as low as a few femtotesla. Since SQUIDs have never been used in Space Weather research, unshielded, it is necessary to investigate if they can be reliable Space Weather instruments. The validation is performed by comparing the frequency content of the SQUID and fluxgate magnetometers, as reported by Phiri.

Calibration of a fluxgate magnetometer array and its application in magnetic object localization

International Nuclear Information System (INIS)

Pang, Hongfeng; Luo, Shitu; Zhang, Qi; Li, Ji; Chen, Dixiang; Pan, Mengchun; Luo, Feilu

2013-01-01

The magnetometer array is effective for magnetic object detection and localization. Calibration is important to improve the accuracy of the magnetometer array. A magnetic sensor array built with four three-axis DM-050 fluxgate magnetometers is designed, which is connected by a cross aluminum frame. In order to improve the accuracy of the magnetometer array, a calibration process is presented. The calibration process includes magnetometer calibration, coordinate transformation and misalignment calibration. The calibration system consists of a magnetic sensor array, a GSM-19T proton magnetometer, a two-dimensional nonmagnetic rotation platform, a 12 V-dc portable power device and two portable computers. After magnetometer calibration, the RMS error has been decreased from an original value of 125.559 nT to a final value of 1.711 nT (a factor of 74). After alignment, the RMS error of misalignment has been decreased from 1322.3 to 6.0 nT (a factor of 220). Then, the calibrated array deployed on the nonmagnetic rotation platform is used for ferromagnetic object localization. Experimental results show that the estimated errors of X, Y and Z axes are −0.049 m, 0.008 m and 0.025 m, respectively. Thus, the magnetometer array is effective for magnetic object detection and localization in three dimensions. (paper)

Calibration of a fluxgate magnetometer array and its application in magnetic object localization

Science.gov (United States)

Pang, Hongfeng; Luo, Shitu; Zhang, Qi; Li, Ji; Chen, Dixiang; Pan, Mengchun; Luo, Feilu

2013-07-01

The magnetometer array is effective for magnetic object detection and localization. Calibration is important to improve the accuracy of the magnetometer array. A magnetic sensor array built with four three-axis DM-050 fluxgate magnetometers is designed, which is connected by a cross aluminum frame. In order to improve the accuracy of the magnetometer array, a calibration process is presented. The calibration process includes magnetometer calibration, coordinate transformation and misalignment calibration. The calibration system consists of a magnetic sensor array, a GSM-19T proton magnetometer, a two-dimensional nonmagnetic rotation platform, a 12 V-dc portable power device and two portable computers. After magnetometer calibration, the RMS error has been decreased from an original value of 125.559 nT to a final value of 1.711 nT (a factor of 74). After alignment, the RMS error of misalignment has been decreased from 1322.3 to 6.0 nT (a factor of 220). Then, the calibrated array deployed on the nonmagnetic rotation platform is used for ferromagnetic object localization. Experimental results show that the estimated errors of X, Y and Z axes are -0.049 m, 0.008 m and 0.025 m, respectively. Thus, the magnetometer array is effective for magnetic object detection and localization in three dimensions.

Calibration of the Ørsted vector magnetometer

DEFF Research Database (Denmark)

Olsen, Nils; Tøffner-Clausen, Lars; Sabaka, T.J.

2003-01-01

The vector fluxgate magnetometer of the Orsted satellite is routinely calibrated by comparing its output with measurements of the absolute magnetic intensity from the Overhauser instrument, which is the second magnetometer of the satellite. We describe the method used for and the result obtained...... coordinate system and the reference system of the star imager. This is done by comparing the magnetic and attitude measurements with a model of Earth's magnetic field. The Euler angles describing this rotation are determined in this way with an accuracy of better than 4 arcsec....

Analysis of packing microstructure and wall effects in a narrow-bore ultrahigh pressure liquid chromatography column using focused ion-beam scanning electron microscopy.

Science.gov (United States)

Reising, Arved E; Schlabach, Sabine; Baranau, Vasili; Stoeckel, Daniela; Tallarek, Ulrich

2017-09-01

Column wall effects are well recognized as major limiting factor in achieving high separation efficiency in HPLC. This is especially important for modern analytical columns packed with small particles, where wall effects dominate the band broadening. Detailed knowledge about the packing microstructure of packed analytical columns has so far not been acquired. Here, we present the first three-dimensional reconstruction protocol for these columns utilizing focused ion-beam scanning electron microscopy (FIB-SEM) on a commercial 2.1mm inner diameter×50mm length narrow-bore analytical column packed with 1.7μm bridged-ethyl hybrid silica particles. Two sections from the packed bed are chosen for reconstruction by FIB-SEM: one from the bulk packing region of the column and one from its critical wall region. This allows quantification of structural differences between the wall region and the center of the bed due to effects induced by the hard, confining column wall. Consequences of these effects on local flow velocity in the column are analyzed with flow simulations utilizing the lattice-Boltzmann method. The reconstructions of the bed structures reveal significant structural differences in the wall region (extending radially over approximately 62 particle diameters) compared to the center of the column. It includes the local reduction of the external porosity by up to 10% and an increase of the mean particle diameter by up to 3%, resulting in a decrease of the local flow velocity by up to 23%. In addition, four (more ordered) layers of particles in the direct vicinity of the column wall induce local velocity fluctuations by up to a factor of three regarding the involved velocity amplitudes. These observations highlight the impact of radial variations in packing microstructure on band migration and column performance. This knowledge on morphological peculiarities of column wall effects helps guiding us towards further optimization of the packing process for analytical

NetPICOmag: A low-cost networked magnetometer and its applications

Science.gov (United States)

Schofield, I.; Connors, M.; Russell, C. T.

2012-03-01

NetPICOmag (NPM) is the culmination of a design effort to build a compact, low-cost, laboratory-grade, networked magnetometer designed for remote autonomous operation, suited for research and education. NPM allows wide placement of magnetometers sensitive enough to detect auroral activity and the daily variation, and is suitable for education projects and a range of geophysical applications. The use of networked microcontrollers and GPS timing is applicable to other small instruments for field or local deployment, and an onboard data logging capability has also been demonstrated. We illustrate the value of the placement of low-cost magnetometers to increase coverage in an area through the study of a Pc 5 pulsation event which took place on September 4, 2010. By combining results with those from auroral zone magnetometers supporting the THEMIS project, we find that the phase velocity of these morning sector pulsations was northward on the ground. The event took place under very quiet solar wind conditions, and credible mapping associates it with the inner magnetosphere. Another aspect beyond increasing areal coverage is increasing density of coverage, which becomes feasible with instruments of very low cost. We examine aspects of the April 5, 2010 space weather event which are possible to deduce from closely spaced magnetometers.

Radiation tolerance of a spin-dependent tunnelling magnetometer for space applications

International Nuclear Information System (INIS)

Persson, Anders; Thornell, Greger; Nguyen, Hugo

2011-01-01

To meet the increasing demand for miniaturized space instruments, efforts have been made to miniaturize traditional magnetometers, e.g. fluxgate and spin-exchange relaxation-free magnetometers. These have, for different reasons, turned out to be difficult. New technologies are needed, and promising in this respect are tunnelling magnetoresistive (TMR) magnetometers, which are based on thin film technology. However, all new space devices first have to be qualified, particularly in terms of radiation resistance. A study on TMR magnetometers' vulnerability to radiation is crucial, considering the fact that they employ a dielectric barrier, which can be susceptible to charge trapping from ionizing radiation. Here, a TMR-based magnetometer, called the spin-dependent tunnelling magnetometer (SDTM), is presented. A magnetometer chip consisting of three Wheatstone bridges, with an angular pitch of 120°, was fabricated using microstructure technology. Each branch of the Wheatstone bridges consists of eight pairs of magnetic tunnel junctions (MTJs) connected in series. Two such chips are used to measure the three-dimensional magnetic field vector. To investigate the SDTM's resistance to radiation, one branch of a Wheatstone bridge was irradiated with gamma rays from a Co 60 source with a dose rate of 10.9 rad min −1 to a total dose of 100 krad. The TMR of the branch was monitored in situ, and the easy axis TMR loop and low-frequency noise characteristics of a single MTJ were acquired before and after irradiation with the total dose. It was concluded that radiation did not influence the MTJs in any noticeable way in terms of the TMR ratio, coercivity, magnetostatic coupling or low-frequency noise

Developement of a Fluxgate Magnetometer for the KITSAT-3 Satellite

Directory of Open Access Journals (Sweden)

S. H. Hwang

1997-12-01

Full Text Available The magnetometer is one of the most important payloads of scientific satellites to monitor the near-earth space environment. The electromagnetic variations of the space environment can be observed with the electric and magnetic field measurements. In practice, it is well known that the measurement of magnetic fields needs less technical complexities than that of electric fields in space. Therefore the magnetometer has long been recognized as one of the basic payloads for the scientific satellites. In this paper, we discuss the scientific fluxgate magnetometer which will be on board the KITSAT-3. The main circuit design of the present magnetometer is based on that of KISAT-1 and -2 but its facilities have been re-designed to improve the resolution to about 5nT for scientific purpose. The calibration and noise level test of this circuit have been performed at the laboratory of the Tierra Tecnica company in Japan.

Differential Search Coils Based Magnetometers: Conditioning, Magnetic Sensitivity, Spatial Resolution

Directory of Open Access Journals (Sweden)

Timofeeva Maria

2012-03-01

Full Text Available A theoretical and experimental comparison of optimized search coils based magnetometers, operating either in the Flux mode or in the classical Lenz-Faraday mode, is presented. The improvements provided by the Flux mode in terms of bandwidth and measuring range of the sensor are detailed. Theory, SPICE model and measurements are in good agreement. The spatial resolution of the sensor is studied which is an important parameter for applications in non destructive evaluation. A general expression of the magnetic sensitivity of search coils sensors is derived. Solutions are proposed to design magnetometers with reduced weight and volume without degrading the magnetic sensitivity. An original differential search coil based magnetometer, made of coupled coils, operating in flux mode and connected to a differential transimpedance amplifier is proposed. It is shown that this structure is better in terms of volume occupancy than magnetometers using two separated coils without any degradation in magnetic sensitivity. Experimental results are in good agreement with calculations.

Design and analysis of miniature tri-axial fluxgate magnetometer

Science.gov (United States)

Zhi, Menghui; Tang, Liang; Qiao, Donghai

2017-02-01

The detection technology of weak magnetic field is widely used in Earth resource survey and geomagnetic navigation. Useful magnetic field information can be obtained by processing and analyzing the measurement data from magnetic sensors. A miniature tri-axial fluxgate magnetometer is proposed in this paper. This miniature tri-axial fluxgate magnetometer with ring-core structure has a dynamic range of the Earth’s field ±65,000 nT, resolution of several nT. It has three independent parts placed in three perpendicular planes for measuring three orthogonal magnetic field components, respectively. A field-programmable gate array (FPGA) is used to generate stimulation signal, analog-to-digital (A/D) convertor control signal, and feedback digital-to-analog (D/A) control signal. Design and analysis details are given to improve the dynamic range, sensitivity, resolution, and linearity. Our prototype was measured and compared with a commercial standard Magson fluxgate magnetometer as a reference. The results show that our miniature fluxgate magnetometer can follow the Magson’s change trend well. When used as a magnetic compass, our prototype only has ± 0.3∘ deviation compared with standard magnetic compass.

All optical vector magnetometer, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — This Phase I research project will investigate a novel method of operating an atomic magnetometer to simultaneously measure total magnetic fields and vector magnetic...

Huffman and linear scanning methods with statistical language models.

Science.gov (United States)

Roark, Brian; Fried-Oken, Melanie; Gibbons, Chris

2015-03-01

Current scanning access methods for text generation in AAC devices are limited to relatively few options, most notably row/column variations within a matrix. We present Huffman scanning, a new method for applying statistical language models to binary-switch, static-grid typing AAC interfaces, and compare it to other scanning options under a variety of conditions. We present results for 16 adults without disabilities and one 36-year-old man with locked-in syndrome who presents with complex communication needs and uses AAC scanning devices for writing. Huffman scanning with a statistical language model yielded significant typing speedups for the 16 participants without disabilities versus any of the other methods tested, including two row/column scanning methods. A similar pattern of results was found with the individual with locked-in syndrome. Interestingly, faster typing speeds were obtained with Huffman scanning using a more leisurely scan rate than relatively fast individually calibrated scan rates. Overall, the results reported here demonstrate great promise for the usability of Huffman scanning as a faster alternative to row/column scanning.

Sensitivity optimization of Bell-Bloom magnetometers by manipulation of atomic spin synchronization

Science.gov (United States)

Ranjbaran, M.; Tehranchi, M. M.; Hamidi, S. M.; Khalkhali, S. M. H.

2018-05-01

Many efforts have been devoted to the developments of atomic magnetometers for achieving the high sensitivity required in biomagnetic applications. To reach the high sensitivity, many types of atomic magnetometers have been introduced for optimization of the creation and relaxation rates of atomic spin polarization. In this paper, regards to sensitivity optimization techniques in the Mx configuration, we have proposed a novelty approach for synchronization of the spin precession in the Bell-Bloom magnetometers. We have utilized the phenomenological Bloch equations to simulate the spin dynamics when modulation of pumping light and radio frequency magnetic field were both used for atomic spin synchronization. Our results showed that the synchronization process, improved the magnetometer sensitivity respect to the classical configurations.

New Magneto-Inductive DC Magnetometer for Space Missions

Science.gov (United States)

Moldwin, M.; Bronner, B.; Regoli, L.; Thoma, J.; Shen, A.; Jenkins, G.; Cutler, J.

2017-12-01

A new magneto-inductive DC magnetometer is being developed at the University of Michigan that provides fluxgate quality measurements in a low mass, volume, power and cost package. The magnetometer enables constellation-class missions not only due to its low-resource requirements, but also its potential for commercial integrated circuit fabrication. The magneto-inductive operating principle is based on a simple resistance-inductor (RL) circuit and involves measurement of the time it takes to charge and discharge the inductor between an upper and lower threshold by means of a Schmitt trigger oscillator. This time is proportional to the inductance that in turn is proportional to the field strength. We have modeled the operating principle in the circuit simulator SPICE and have built a proto-type using modified commercial sensors. The performance specifications include a dynamic range over the full-Earth's field, sampling rates up to 80 Hz, sensor and electronics mass of about 30 g, circuit board and sensor housing volume of magnetometer.

A spinner magnetometer for large Apollo lunar samples

Science.gov (United States)

Uehara, M.; Gattacceca, J.; Quesnel, Y.; Lepaulard, C.; Lima, E. A.; Manfredi, M.; Rochette, P.

2017-10-01

We developed a spinner magnetometer to measure the natural remanent magnetization of large Apollo lunar rocks in the storage vault of the Lunar Sample Laboratory Facility (LSLF) of NASA. The magnetometer mainly consists of a commercially available three-axial fluxgate sensor and a hand-rotating sample table with an optical encoder recording the rotation angles. The distance between the sample and the sensor is adjustable according to the sample size and magnetization intensity. The sensor and the sample are placed in a two-layer mu-metal shield to measure the sample natural remanent magnetization. The magnetic signals are acquired together with the rotation angle to obtain stacking of the measured signals over multiple revolutions. The developed magnetometer has a sensitivity of 5 × 10-7 Am2 at the standard sensor-to-sample distance of 15 cm. This sensitivity is sufficient to measure the natural remanent magnetization of almost all the lunar basalt and breccia samples with mass above 10 g in the LSLF vault.

A spinner magnetometer for large Apollo lunar samples.

Science.gov (United States)

Uehara, M; Gattacceca, J; Quesnel, Y; Lepaulard, C; Lima, E A; Manfredi, M; Rochette, P

2017-10-01

We developed a spinner magnetometer to measure the natural remanent magnetization of large Apollo lunar rocks in the storage vault of the Lunar Sample Laboratory Facility (LSLF) of NASA. The magnetometer mainly consists of a commercially available three-axial fluxgate sensor and a hand-rotating sample table with an optical encoder recording the rotation angles. The distance between the sample and the sensor is adjustable according to the sample size and magnetization intensity. The sensor and the sample are placed in a two-layer mu-metal shield to measure the sample natural remanent magnetization. The magnetic signals are acquired together with the rotation angle to obtain stacking of the measured signals over multiple revolutions. The developed magnetometer has a sensitivity of 5 × 10 -7 Am 2 at the standard sensor-to-sample distance of 15 cm. This sensitivity is sufficient to measure the natural remanent magnetization of almost all the lunar basalt and breccia samples with mass above 10 g in the LSLF vault.

A portable Hall magnetometer probe for characterization of magnetic iron oxide nanoparticles

Energy Technology Data Exchange (ETDEWEB)

Araujo, Jefferson F.D.F.; Costa, Mateus C.; Louro, Sonia R.W.; Bruno, Antonio C., E-mail: acbruno@puc-rio.br

2017-03-15

We have built a portable Hall magnetometer probe, for measuring magnetic properties of iron oxide nanoparticles, that can be used for bulk materials and liquid samples as well. The magnetometer probe consists of four voltage-programmable commercial Hall sensors and a thin acrylic plate for positioning the sensors. In order to operate, it needs to be attached to a pole of an electromagnet and connected to an AD converter and a computer. It acquires a complete magnetization curve in a couple of minutes and has a magnetic moment sensitivity of 3.5×10{sup −7} Am{sup 2}. We tested its performance with magnetic nanoparticles containing an iron oxide core and having coating layers with different sizes. The magnetization results obtained were compared with measurements performed on commercial stand-alone magnetometers, and exhibited errors of about ±0.2 Am{sup 2}/kg (i.e 0.4%) at saturation and below 0.5 Am{sup 2}/kg (i.e. 10%) at remanence. - Highlights: • A low-cost portable Hall magnetometer probe has been built. • The Hall magnetometer probe can be attached to any electromagnet. • The Hall probe was calibrated and successfully compared to industry standard magnetometers. • The Hall probe was able to measure iron oxide nanoparticles with different coatings.

A portable Hall magnetometer probe for characterization of magnetic iron oxide nanoparticles

International Nuclear Information System (INIS)

Araujo, Jefferson F.D.F.; Costa, Mateus C.; Louro, Sonia R.W.; Bruno, Antonio C.

2017-01-01

We have built a portable Hall magnetometer probe, for measuring magnetic properties of iron oxide nanoparticles, that can be used for bulk materials and liquid samples as well. The magnetometer probe consists of four voltage-programmable commercial Hall sensors and a thin acrylic plate for positioning the sensors. In order to operate, it needs to be attached to a pole of an electromagnet and connected to an AD converter and a computer. It acquires a complete magnetization curve in a couple of minutes and has a magnetic moment sensitivity of 3.5×10 −7 Am 2 . We tested its performance with magnetic nanoparticles containing an iron oxide core and having coating layers with different sizes. The magnetization results obtained were compared with measurements performed on commercial stand-alone magnetometers, and exhibited errors of about ±0.2 Am 2 /kg (i.e 0.4%) at saturation and below 0.5 Am 2 /kg (i.e. 10%) at remanence. - Highlights: • A low-cost portable Hall magnetometer probe has been built. • The Hall magnetometer probe can be attached to any electromagnet. • The Hall probe was calibrated and successfully compared to industry standard magnetometers. • The Hall probe was able to measure iron oxide nanoparticles with different coatings.

An Arduino-Based Magnetometer

Science.gov (United States)

McCaughey, Mike

2017-01-01

An Arduino-based system with a triple axis magnetometer chip may be used to plot both the strength and direction of the magnetic field of a magnet directly on a sheet of paper. Before taking measurements, it is necessary either to correct for or to eliminate soft and hard iron effects. The same sensor may be used to determine the presence of soft…

Feasibility Study for an Autonomous UAV -Magnetometer System -- Final Report on SERDP SEED 1509:2206

Energy Technology Data Exchange (ETDEWEB)

Roelof Versteeg; Mark McKay; Matt Anderson; Ross Johnson; Bob Selfridge; Jay Bennett

2007-09-01

Large areas across the United States are potentially contaminated with UXO, with some ranges encompassing tens to hundreds of thousands of acres. Technologies are needed which will allow for cost effective wide area scanning with 1) near 100 % coverage and 2) near 100 % detection of subsurface ordnance or features indicative of subsurface ordnance. The current approach to wide area scanning is a multi-level one, in which medium altitude fixed wing optical imaging is used for an initial site assessment. This assessment is followed with low altitude manned helicopter based magnetometry followed by surface investigations using either towed geophysical sensor arrays or man portable sensors. In order to be effective for small UXO detection, the sensing altitude for magnetic site investigations needs to be on the order of 1 – 3 meters. These altitude requirements means that manned helicopter surveys will generally only be feasible in large, open and relatively flat terrains. While such surveys are effective in mapping large areas relatively fast there are substantial mobilization/demobilization, staffing and equipment costs associated with these surveys (resulting in costs of approximately $100-$150/acre). Surface towed arrays provide high resolution maps but have other limitations, e.g. in their ability to navigate rough terrain effectively. Thus, other systems are needed allowing for effective data collection. An UAV (Unmanned Aerial Vehicle) magnetometer platform is an obvious alternative. The motivation behind such a system is that it would be safer for the operators, cheaper in initial and O&M costs, and more effective in terms of site characterization. However, while UAV data acquisition from fixed wing platforms for large (> 200 feet) stand off distances is relatively straight forward, a host of challenges exist for low stand-off distance (~ 6 feet) UAV geophysical data acquisition. The objective of SERDP SEED 1509:2006 was to identify the primary challenges

Midlatitude magnetometer chains during the IMS

International Nuclear Information System (INIS)

Mcpherron, R.L.

1982-01-01

The International Magnetospheric Study (IMS) is an international program to study global problems of magnetospheric dynamics. A key element of the U.S. participation in this program was the establishment of a ground magnetometer network. This network included a number of arrays at high and low latitudes. This report describes three chains established at midlatitudes, including the IMS Midlatitude Chain, the AFGL Magnetometer Network, and the Bell Lab Conjugate Array. Descriptions of the type of equipment, station locations, types of data display, and availability of data for each chain are presented in this report. A major problem of the data analysis phase of the IMS will be reducing selected subsets of these data to a common format. Currently, there are no plans to do this in a systematic manner

Design Principles of A Sigma-delta Flux-gate Magnetometer

Science.gov (United States)

Magnes, W.; Valavanoglou, A.; Pierce, D.; Frank, A.; Schwingenschuh, K.

A state-of-the-art flux-gate magnetometer is characterised by magnetic field resolution of several pT in a wide frequency range, low power consumption, low weight and high robustness. Therefore, flux-gate magnetometers are frequently used for ground-based Earth's field observation as well as for measurements aboard scientific space missions. But both traditional analogue and recently developed digital flux-gate magnetometers need low power and high-resolution analogue-to-digital converters for signal quan- tization. The disadvantage of such converters is the low radiation hardness. This fact has led to the idea of combining a traditional analogue flux-gate regulation circuit with that of a discretely realized sigma-delta converter in order to get a radiation hard and further miniaturized magnetometer. The name sigma-delta converter is derived from putting an integrator in front of a 1-bit delta modulator which forms the sigma-delta loop. It is followed by a digital decimation filter realized in a field-programmable gate array (FPGA). The flux-gate regulation and the sigma-delta loop are quite similar in the way of realizing the integrator and feedback circuit, which makes it easy to com- bine these two systems. The presented talk deals with the design principles and the results of a first bread board model.

Microfabricated optically pumped magnetometer arrays for biomedical imaging

Science.gov (United States)

Perry, A. R.; Sheng, D.; Krzyzewski, S. P.; Geller, S.; Knappe, S.

2017-02-01

Optically-pumped magnetometers have demonstrated magnetic field measurements as precise as the best superconducting quantum interference device magnetometers. Our group develops miniature alkali atom-based magnetic sensors using microfabrication technology. Our sensors do not require cryogenic cooling, and can be positioned very close to the sample, making these sensors an attractive option for development in the medical community. We will present our latest chip-scale optically-pumped gradiometer developed for array applications to image magnetic fields from the brain noninvasively. These developments should lead to improved spatial resolution, and potentially sensitive measurements in unshielded environments.

A dumbbell-shaped hybrid magnetometer operating in DC-10 kHz

Science.gov (United States)

Shi, Hongyu; Wang, Yanzhang; Chen, Siyu; Lin, Jun

2017-12-01

This study is motivated by the need to design a hybrid magnetometer operating in a wide-frequency band from DC to 10 kHz. To achieve this objective, a residence times difference fluxgate magnetometer (RTDFM) and an induction magnetometer (IM) have been integrated into a compact form. The hybrid magnetometer has a dumbbell-shaped structure in which the RTDFM transducer is partially inserted into the tube cores of the IM. Thus, the sensitivity of the RTDFM is significantly improved due to the flux amplification. The optimal structure, which has maximum sensitivity enhancement, was obtained through FEM analysis. To validate the theoretical analysis, the optimal hybrid magnetometer was manufactured, and its performance was evaluated. The device has a sensitivity of 45 mV/nT at 1 kHz in IM mode and 0.38 μs/nT in RTDFM mode, which is approximately 3.45 times as large as that of the single RTDFM structure. Furthermore, to obtain a lower noise performance in the entire frequency band, two operation modes switch at the cross frequency (0.16 Hz) of their noise levels. The noise level is 30 pT/√Hz in RTDFM mode and 0.07 pT/√Hz at 1 kHz in IM mode.

Long-term vacuum tests of single-mode vertical cavity surface emitting laser diodes used for a scalar magnetometer

Science.gov (United States)

Hagen, C.; Ellmeier, M.; Piris, J.; Lammegger, R.; Jernej, I.; Magnes, W.; Murphy, E.; Pollinger, A.; Erd, C.; Baumjohann, W.

2017-11-01

Scalar magnetometers measure the magnitude of the magnetic field, while vector magnetometers (mostly fluxgate magnetometers) produce three-component outputs proportional to the magnitude and the direction of the magnetic field. While scalar magnetometers have a high accuracy, vector magnetometers suffer from parameter drifts and need to be calibrated during flight. In some cases, full science return can only be achieved by a combination of vector and scalar magnetometers.

DSCOVR Magnetometer Level 2 One Minute Averages

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — Interplanetary magnetic field observations collected from magnetometer on DSCOVR satellite - 1-minute average of Level 1 data

DSCOVR Magnetometer Level 2 One Second Averages

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — Interplanetary magnetic field observations collected from magnetometer on DSCOVR satellite - 1-second average of Level 1 data

Determination of the Overhauser magnetometer uncertainty

Czech Academy of Sciences Publication Activity Database

Ulvr, M.; Zikmund, A.; Kupec, J.; Janošek, M.; Vlk, Michal; Bayer, Tomáš

2015-01-01

Roč. 66, 7/s (2015), s. 26-29 ISSN 1335-3632 Institutional support: RVO:67985530 Keywords : Overhauser magnetometer * Earth `s magnetic field * comparison * uncertainty Subject RIV: DE - Earth Magnetism, Geodesy, Geography Impact factor: 0.407, year: 2015

A theoretical and experimental investigation of the proton magnetometer

International Nuclear Information System (INIS)

Hancke, G.P.

1987-01-01

This study comprises the investigation of the properties of the proton magnetometer based on the free precession of protons. The basic principle of the free precession of protons in the earth's magnetic field is described and the most important factors affecting this free precession are examined. It is shown that very important parameters to keep in mind are the polarization time and the magnitude of the polarization field. A discussion of the errors of a proton magnetometer built on the periodometer principles is given and it is shown that the error in counting of the number of precession periods during the time of measurement contributes most to the total error. The magnitude of this error depends on the signal-to-noise ratio, the instability of the operating threshold of the discriminator of the period counter, it's operating time and the tuning accuracy of the sensor to the precession frequency. The penetration to a magnetometer input of variable magnetic and electric interferences, their influence on the phase of the useful signal, and the resulting measurement errors are examined and methods of reducing the effects of interferences are discussed. The optimization of sensor design is very important in the development of proton magnetometers. The coil geometry, physical size, the working substance and the polarization design are important parameters. The selection of a method for processing the precession signal of a proton magnetometer is examined, given a sensor and signal amplifier with fixed parameters. A method is proposed and compared with known methods. Measurement errors are computed for various signal-to-noise ratios and times of observation of the precession signal, and it is shown that the proposed method is superior to conventional methods found in commercial instruments

Cryostats for SQUID magnetometers

International Nuclear Information System (INIS)

Testard, O.A.; Locatelli, M.

1982-05-01

A non metallic and non magnetic cryostat, with a very low thermal budget and a container type autonomy was developed, to condition S.Q.U.I.D. magnetometers which maximum sensitivity reaches 10 -14 Tesla Hertzsup(-1/2). This instrumentation puts in hand new concepts of composite materials, thermal shock and vibration resistant, multilayer thermal radiative insulation also to the prouve of vibrations with thermal equivalent emissivity lower than 10 -3

Design and implementation of JOM-3 Overhauser magnetometer analog circuit

Science.gov (United States)

Zhang, Xiao; Jiang, Xue; Zhao, Jianchang; Zhang, Shuang; Guo, Xin; Zhou, Tingting

2017-09-01

Overhauser magnetometer, a kind of static-magnetic measurement system based on the Overhauser effect, has been widely used in archaeological exploration, mineral resources exploration, oil and gas basin structure detection, prediction of engineering exploration environment, earthquakes and volcanic eruotions, object magnetic measurement and underground buried booty exploration. Overhauser magnetometer plays an important role in the application of magnetic field measurement for its characteristics of small size, low power consumption and high sensitivity. This paper researches the design and the application of the analog circuit of JOM-3 Overhauser magnetometer. First, the Larmor signal output by the probe is very weak. In order to obtain the signal with high signal to noise rstio(SNR), the design of pre-amplifier circuit is the key to improve the quality of the system signal. Second, in this paper, the effectual step which could improve the frequency characters of bandpass filter amplifier circuit were put forward, and theoretical analysis was made for it. Third, the shaping circuit shapes the amplified sine signal into a square wave signal which is suitable for detecting the rising edge. Fourth, this design elaborated the optimized choice of tuning circuit, so the measurement range of the magnetic field can be covered. Last, integrated analog circuit testing system was formed to detect waveform of each module. By calculating the standard deviation, the sensitivity of the improved Overhauser magnetometer is 0.047nT for Earth's magnetic field observation. Experimental results show that the new magnetometer is sensitive to earth field measurement.

Field-Programmable Gate Array-based fluxgate magnetometer with digital integration

Science.gov (United States)

Butta, Mattia; Janosek, Michal; Ripka, Pavel

2010-05-01

In this paper, a digital magnetometer based on printed circuit board fluxgate is presented. The fluxgate is pulse excited and the signal is extracted by gate integration. We investigate the possibility to perform integration on very narrow gates (typically 500 ns) by using digital techniques. The magnetometer is based on field-programmable gate array (FPGA) card: we will show all the advantages and disadvantages, given by digitalization of fluxgate output voltage by means of analog-to-digital converter on FPGA card, as well as digitalization performed by external digitizer. Due to very narrow gate, it is shown that a magnetometer entirely based on a FPGA card is preferable, because it avoids noise due to trigger instability. Both open loop and feedback operative mode are described and achieved results are presented.

A Web Server for MACCS Magnetometer Data

Science.gov (United States)

Engebretson, Mark J.

1998-01-01

NASA Grant NAG5-3719 was provided to Augsburg College to support the development of a web server for the Magnetometer Array for Cusp and Cleft Studies (MACCS), a two-dimensional array of fluxgate magnetometers located at cusp latitudes in Arctic Canada. MACCS was developed as part of the National Science Foundation's GEM (Geospace Environment Modeling) Program, which was designed in part to complement NASA's Global Geospace Science programs during the decade of the 1990s. This report describes the successful use of these grant funds to support a working web page that provides both daily plots and file access to any user accessing the worldwide web. The MACCS home page can be accessed at http://space.augsburg.edu/space/MaccsHome.html.

Nonlinear temperature compensation of fluxgate magnetometers with a least-squares support vector machine

International Nuclear Information System (INIS)

Pang, Hongfeng; Chen, Dixiang; Pan, Mengchun; Luo, Shitu; Zhang, Qi; Luo, Feilu

2012-01-01

Fluxgate magnetometers are widely used for magnetic field measurement. However, their accuracy is influenced by temperature. In this paper, a new method was proposed to compensate the temperature drift of fluxgate magnetometers, in which a least-squares support vector machine (LSSVM) is utilized. The compensation performance was analyzed by simulation, which shows that the LSSVM has better performance and less training time than backpropagation and radical basis function neural networks. The temperature characteristics of a DM fluxgate magnetometer were measured with a temperature experiment box. Forty-five measured data under different magnetic fields and temperatures were obtained and divided into 36 training data and nine test data. The training data were used to obtain the parameters of the LSSVM model, and the compensation performance of the LSSVM model was verified by the test data. Experimental results show that the temperature drift of magnetometer is reduced from 109.3 to 3.3 nT after compensation, which suggests that this compensation method is effective for the accuracy improvement of fluxgate magnetometers. (paper)

Nonlinear temperature compensation of fluxgate magnetometers with a least-squares support vector machine

Science.gov (United States)

Pang, Hongfeng; Chen, Dixiang; Pan, Mengchun; Luo, Shitu; Zhang, Qi; Luo, Feilu

2012-02-01

Fluxgate magnetometers are widely used for magnetic field measurement. However, their accuracy is influenced by temperature. In this paper, a new method was proposed to compensate the temperature drift of fluxgate magnetometers, in which a least-squares support vector machine (LSSVM) is utilized. The compensation performance was analyzed by simulation, which shows that the LSSVM has better performance and less training time than backpropagation and radical basis function neural networks. The temperature characteristics of a DM fluxgate magnetometer were measured with a temperature experiment box. Forty-five measured data under different magnetic fields and temperatures were obtained and divided into 36 training data and nine test data. The training data were used to obtain the parameters of the LSSVM model, and the compensation performance of the LSSVM model was verified by the test data. Experimental results show that the temperature drift of magnetometer is reduced from 109.3 to 3.3 nT after compensation, which suggests that this compensation method is effective for the accuracy improvement of fluxgate magnetometers.

Magnetometer Data recovered from 35mm film

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — The L57 CDMP recovery project takes magnetometer data on 35mm film stored at the archive's climate controlled warehouse and digitizes them.

3D Scan of Ornamental Column (huabiao Using Terrestrial LiDAR and Hand-held Imager

Directory of Open Access Journals (Sweden)

W. Zhang

2015-08-01

Full Text Available In ancient China, Huabiao was a type of ornamental column used to decorate important buildings. We carried out 3D scan of a Huabiao located in Peking University, China. This Huabiao was built no later than 1742. It is carved by white marble, 8 meters in height. Clouds and various postures of dragons are carved on its body. Two instruments were used to acquire the point cloud of this Huabiao, a terrestrial LiDAR (Riegl VZ-1000 and a hand-held imager (Mantis Vision F5. In this paper, the details of the experiment were described, including the differences between these two instruments, such as working principle, spatial resolution, accuracy, instrument dimension and working flow. The point clouds obtained respectively by these two instruments were compared, and the registered point cloud of Huabiao was also presented. These should be of interest and helpful for the research communities of archaeology and heritage.

A broadband two axis flux-gate magnetometer

Directory of Open Access Journals (Sweden)

P. Palangio

1998-06-01

Full Text Available A broadband two axis flux-gate magnetometer was developed to obtain high sensitivity in magnetotelluric measurements. In magnetotelluric sounding, natural low frequency electromagnetic fields are used to estimate the conductivity of the Earth's interior. Because variations in the natural magnetic field have small amplitude(10-100 pT in the frequency range 1 Hz to 100 Hz, highly sensitive magnetic sensors are required. In magnetotelluric measurements two long and heavy solenoids, which must be installed, in the field station, perpendicular to each other (north-south and east-west and levelled in the horizontal plane are used. The coil is a critical component in magnetotelluric measurements because very slight motions create noise voltages, particularly troublesome in wooded areas; generally the installation takes place in a shallow trench. Moreover the coil records the derivative of the variations rather than the magnetic field variations, consequently the transfer function (amplitude and phase of this sensor is not constant throughout the frequency range 0.001-100 Hz. The instrument, developed at L'Aquila Geomagnetic Observatory, has a flat response in both amplitude and phase in the frequency band DC-100 Hz, in addition it has low weight, low power, small volume and it is easier to install in the field than induction magnetometers. The sensivity of this magnetometer is 10 pT rms.

Fluxgate Magnetometer Array for Geomagnetic Abnormal Phenomena Tracking

Directory of Open Access Journals (Sweden)

Xiaomei Wang

2011-06-01

Full Text Available The objective of this project is to develop a flexible observation mode for a geomagnetic abnormal phenomena tracking system. The instrument, based on ring core fluxgate magnetometer technology, improves the field environment performance. Using wireless technology provides on-the-spot mobile networking for the observational data, with efficient access to the earthquake precursor observation network. It provides a powerful detection method for earthquake short-term prediction through installation of a low-noise fluxgate magnetometer array, intensely observing the phenomenon of geomagnetic disturbances and abnormal low-frequency electromagnetic signals in different latitudes, then carrying out observational data processing and exploring the relationship between earthquake activity and geomagnetic field changes.

Miniature scientific-grade induction magnetometer for cubesats

Science.gov (United States)

Pronenko, Vira

2017-04-01

One of the main areas of space research is the study and forecasting of space weather. The society is more and more depending nowadays on satellite technology and communications, so it is vital to understand the physical process in the solar-terrestrial system which may disturb them. Besides the solar radiation and Space Weather effects, the Earth's ionosphere is also modified by the ever increasing industrial activity. There have been also multiple reports relating VLF and ELF wave activity to atmospheric storms and geological processes, such as earthquakes and volcanic activity. For advancing in these fields, the AC magnetic field permanent monitoring is crucial. Using the cubesat technology would allow increasing the number of measuring points dramatically. It is necessary to mention that the cubesats use for scientific research requires the miniaturization of scientific sensors what is a serious problem because the reduction of their dimensions leads, as a rule, to the parameters degradation, especially of sensitivity threshold. Today, there is no basic model of a sensitive miniature induction magnetometer. Even the smallest one of the known - for the Bepi-Colombo mission to Mercury - is too big for cubesats. The goal of the present report is to introduce the new design of miniature three-component sensor for measurement of alternative vector magnetic fields - induction magnetometer (IM). The study directions were concentrated on the ways and possibilities to create the miniature magnetometer with best combination of parameters. For this a set of scientific and technological problems, mostly aimed at the sensor construction improvement, was solved. The most important parameter characterizing magnetometer quality is its own magnetic noise level (NL). The analysis of the NL influencing factors is made and the ways to decrease it are discussed in the report. Finally, the LEMI-151 IM was developed for the SEAM cubesat mission with optimal performances within the

The Fluxgate Magnetometer Simulation in Comsol Multiphysics

OpenAIRE

Kolomeytsev Andrey; Baranov Pavel; Zatonov Ivan

2018-01-01

This article describes the fluxgate magnetometer simulation in Comsol Multiphysics software package. The simulation results coincide with the experiment described earlier. Decomposition of the output signal by the Fourier coefficients shows a frequency doubling.

Swarm's absolute magnetometer experimental vector mode, an innovative capability for space magnetometry

DEFF Research Database (Denmark)

Hulot, Gauthier; Vigneron, Pierre; Leger, Jean-Michel

2015-01-01

, combining ASM scalar data with independent uxgate magnetometer vector data. The high level of agreement between these models demonstrates the potential of the ASM's vector mode for data quality control and as a stand alone magnetometer, and illustrates the way the evolution of key eld features can easily...

Column-by-column compositional mapping by Z-contrast imaging

Energy Technology Data Exchange (ETDEWEB)

Molina, S.I. [Departamento de Ciencia de los Materiales e I.M. y Q.I., Facultad de Ciencias, Universidad de Cadiz, Campus Rio San Pedro, s/n, 11510 Puerto Real, Cadiz (Spain)], E-mail: sergio.molina@uca.es; Sales, D.L. [Departamento de Ciencia de los Materiales e I.M. y Q.I., Facultad de Ciencias, Universidad de Cadiz, Campus Rio San Pedro, s/n, 11510 Puerto Real, Cadiz (Spain); Galindo, P.L. [Departamento de Lenguajes y Sistemas Informaticos, CASEM, Universidad de Cadiz, Campus Rio San Pedro, s/n, 11510 Puerto Real, Cadiz (Spain); Fuster, D.; Gonzalez, Y.; Alen, B.; Gonzalez, L. [Instituto de Microelectronica de Madrid (CNM, CSIC), Isaac Newton 8, 28760 Tres Cantos, Madrid (Spain); Varela, M.; Pennycook, S.J. [Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States)

2009-01-15

A phenomenological method is developed to determine the composition of materials, with atomic column resolution, by analysis of integrated intensities of aberration-corrected Z-contrast scanning transmission electron microscopy images. The method is exemplified for InAs{sub x}P{sub 1-x} alloys using epitaxial thin films with calibrated compositions as standards. Using this approach we have determined the composition of the two-dimensional wetting layer formed between self-assembled InAs quantum wires on InP(0 0 1) substrates.

The low cost Proton Precession Magnetometer developed at the Indian Institute of Geomagnetism

International Nuclear Information System (INIS)

Mahavarkar, P.; Singh, S.; Labde, S.; Dongre, V.; Patil, A.

2017-01-01

Proton magnetometers are the oldest scalar magnetometers. The first commercial units were produced in early 1960s as portable instruments. In continuation airborne instruments appeared with optimized speed of readings and sensitivity, large sensors etc. Later development of Overhauser and optically pumped magnetometers has eliminated Proton magnetometers from airborne surveys. However they remain very popular in various ground surveys and observatories. With this primary purpose of generating the ground based magnetic data, the Indian Institute of Geomagnetism (IIG) for the last 3 decades have been developing low cost Proton Precession Magnetometers (PPM). Beginning with the 1 nT PPM which has undergone several changes in design, the successor PM7 the advanced version has been successfully developed by the institute and is installed at various observatories of the institute. PM7 records the total field 'F' with accuracy of 0.1 nT and a sampling rate of 10 seconds/sample. This article briefly discusses the design and development of this IIG make PM7 and compares the data recorded by this instrument with one of the commercially available Overhauser magnetometer in the world market. The quality of data recorded by PM7 is in excellent agreement with the Overhauser. With the available quality of data generated by this instrument, PM7 is an affordable PPM for scientific institutions, schools and colleges intending to carry out geomagnetic studies. The commercial cost of PM7 is ≈ 20% of the cost of Overhauser available in market.

The low cost Proton Precession Magnetometer developed at the Indian Institute of Geomagnetism

Science.gov (United States)

Mahavarkar, P.; Singh, S.; Labde, S.; Dongre, V.; Patil, A.

2017-05-01

Proton magnetometers are the oldest scalar magnetometers. The first commercial units were produced in early 1960s as portable instruments. In continuation airborne instruments appeared with optimized speed of readings and sensitivity, large sensors etc. Later development of Overhauser and optically pumped magnetometers has eliminated Proton magnetometers from airborne surveys. However they remain very popular in various ground surveys and observatories. With this primary purpose of generating the ground based magnetic data, the Indian Institute of Geomagnetism (IIG) for the last 3 decades have been developing low cost Proton Precession Magnetometers (PPM). Beginning with the 1 nT PPM which has undergone several changes in design, the successor PM7 the advanced version has been successfully developed by the institute and is installed at various observatories of the institute. PM7 records the total field `F' with accuracy of 0.1 nT and a sampling rate of 10 seconds/sample. This article briefly discusses the design and development of this IIG make PM7 and compares the data recorded by this instrument with one of the commercially available Overhauser magnetometer in the world market. The quality of data recorded by PM7 is in excellent agreement with the Overhauser. With the available quality of data generated by this instrument, PM7 is an affordable PPM for scientific institutions, schools and colleges intending to carry out geomagnetic studies. The commercial cost of PM7 is ≈ 20% of the cost of Overhauser available in market.

Integrated de SQUID magnetometer with high dV/dB

International Nuclear Information System (INIS)

Drung, D.; Cantor, R.; Peters, M.; Ryhanen, T.; Kochi, H.

1991-01-01

This paper presents a directly coupled dc SQUID magnetometer with very simple feedback electronics. The magnetometer has been integrated on a 7.2 x 7.2 mm 2 chip and fabricated using a four-level Nb/Si x N v /Nb process. Eight pick-up loops are connected in parallel to directly form the SQUID inductance of about 0.4 nH which leads to a high sensitivity B/Φ = 0.47 nT/Φ. An Additional Positive Feedback (APF) circuit on the magnetometer chip has been used to increase the gradient of the V-μ characteristic to dV/dΦ ≅ 300 μV/Φ 0 at the SQUID operating point. The resulting gradient of the transfer function of dV/dB ≅ 640 μV/nT makes it possible to directly read out the SQUID without helium temperature impedance matching circuits or flux modulation techniques

Swarm Optimization-Based Magnetometer Calibration for Personal Handheld Devices

Directory of Open Access Journals (Sweden)

Naser El-Sheimy

2012-09-01

Full Text Available Inertial Navigation Systems (INS consist of accelerometers, gyroscopes and a processor that generates position and orientation solutions by integrating the specific forces and rotation rates. In addition to the accelerometers and gyroscopes, magnetometers can be used to derive the user heading based on Earth’s magnetic field. Unfortunately, the measurements of the magnetic field obtained with low cost sensors are usually corrupted by several errors, including manufacturing defects and external electro-magnetic fields. Consequently, proper calibration of the magnetometer is required to achieve high accuracy heading measurements. In this paper, a Particle Swarm Optimization (PSO-based calibration algorithm is presented to estimate the values of the bias and scale factor of low cost magnetometers. The main advantage of this technique is the use of the artificial intelligence which does not need any error modeling or awareness of the nonlinearity. Furthermore, the proposed algorithm can help in the development of Pedestrian Navigation Devices (PNDs when combined with inertial sensors and GPS/Wi-Fi for indoor navigation and Location Based Services (LBS applications.

A novel HTS magnetometer, exploiting the low jc of bulk YBCO

International Nuclear Information System (INIS)

Gallop, J.C.; Lilleyman, S.; Langham, C.D.; Radcliffe, W.J.; Stewart, M.

1989-01-01

The authors report here a novel of magnetometer which is based on the low critical magnetic field H/sub cl/ of sintered samples of the high temperature ceramic superconductor YBa/sub 2/Cu/sub 3/O/sub y/. By driving a sample of the superconductor around a magnetization hysteresis loop, at a frequency of --100 kHz, and detecting the induced voltage in a coil coupled to the sample, at the second harmonic of the drive frequency, the authors find that this voltage is linearly dependent on the aplied d.c. magnetic field in which the sample is situated. They present a model which explains the operation of this magnetometer. This device, while not as sensitive as a SQUID, has the advantage of a wider dynamic range and direct measurement of flux density, unlike a SQUID which is only capable of sensing flux density changes. When operated at 77K the prototype magnetometer has already demonstrated a sensitivity at least 10 times better than that of a commercial fluxgate magnetometer. The system also appears to provide a simple method for investigation of flux flow in these materials

The IRM fluxgate magnetometer

Science.gov (United States)

Luehr, H.; Kloecker, N.; Oelschlaegel, W.; Haeusler, B.; Acuna, M.

1985-01-01

This report describes the three-axis fluxgate magnetometer instrument on board the AMPTE IRM spacecraft. Important features of the instrument are its wide dynamic range (0.1-60,000 nT), a high resolution (16-bit analog to digital conversion) and the capability to operate automatically or via telecommand in two gain states. In addition, the wave activity is monitored in all three components up to 50 Hz. Inflight checkout proved the nominal functioning of the instrument in all modes.

The Fluxgate Magnetometer Simulation in Comsol Multiphysics

Directory of Open Access Journals (Sweden)

Kolomeytsev Andrey

2018-01-01

Full Text Available This article describes the fluxgate magnetometer simulation in Comsol Multiphysics software package. The simulation results coincide with the experiment described earlier. Decomposition of the output signal by the Fourier coefficients shows a frequency doubling.

Closed-cycle gas flow system for cooling a HTc dc-SQUID magnetometer

NARCIS (Netherlands)

Bosch, van den P.J.; Holland, H.J.; Brake, ter H.J.M.; Rogalla, H.

1994-01-01

A closed-cycle gas flow system for cooling a high-crit. temp. d.c.-superconducting quantum interference device (SQUID) magnetometer by means of a cryocooler has been designed, constructed and tested. The magnetometer is aimed to measure heart signals with a sensitivity of 0.1 pT/Hz1/2. The required

Electromagnetic induction imaging with a radio-frequency atomic magnetometer

Energy Technology Data Exchange (ETDEWEB)

Deans, Cameron; Marmugi, Luca, E-mail: l.marmugi@ucl.ac.uk; Hussain, Sarah; Renzoni, Ferruccio [Department of Physics and Astronomy, University College London, Gower Street, London WC1E 6BT (United Kingdom)

2016-03-07

We report on a compact, tunable, and scalable to large arrays imaging device, based on a radio-frequency optically pumped atomic magnetometer operating in magnetic induction tomography modality. Imaging of conductive objects is performed at room temperature, in an unshielded environment and without background subtraction. Conductivity maps of target objects exhibit not only excellent performance in terms of shape reconstruction but also demonstrate detection of sub-millimetric cracks and penetration of conductive barriers. The results presented here demonstrate the potential of a future generation of imaging instruments, which combine magnetic induction tomography and the unmatched performance of atomic magnetometers.

Novel field emission SEM column with beam deceleration technology

International Nuclear Information System (INIS)

Jiruše, Jaroslav; Havelka, Miloslav; Lopour, Filip

2014-01-01

A novel field-emission SEM column has been developed that features Beam Deceleration Mode, high-probe current and ultra-fast scanning. New detection system in the column is introduced to detect true secondary electron signal. The resolution power at low energy was doubled for conventional SEM optics and moderately improved for immersion optics. Application examples at low landing energies include change of contrast, imaging of non-conductive samples and thin layers. - Highlights: • A novel field-emission SEM column has been developed. • Implemented beam deceleration improves the SEM resolution at 1 keV two times. • New column maintains high analytical potential and wide field of view. • Detectors integrated in the column allow gaining true SE and BE signal separately. • Performance of the column is demonstrated on low energy applications

Novel field emission SEM column with beam deceleration technology

Energy Technology Data Exchange (ETDEWEB)

Jiruše, Jaroslav; Havelka, Miloslav; Lopour, Filip

2014-11-15

A novel field-emission SEM column has been developed that features Beam Deceleration Mode, high-probe current and ultra-fast scanning. New detection system in the column is introduced to detect true secondary electron signal. The resolution power at low energy was doubled for conventional SEM optics and moderately improved for immersion optics. Application examples at low landing energies include change of contrast, imaging of non-conductive samples and thin layers. - Highlights: • A novel field-emission SEM column has been developed. • Implemented beam deceleration improves the SEM resolution at 1 keV two times. • New column maintains high analytical potential and wide field of view. • Detectors integrated in the column allow gaining true SE and BE signal separately. • Performance of the column is demonstrated on low energy applications.

Harmonic detection of magnetic resonance for sensitivity improvement of optical atomic magnetometers

Energy Technology Data Exchange (ETDEWEB)

Ranjbaran, M. [Laser and Plasma Research Institute, Shahid Beheshti University, Tehran (Iran, Islamic Republic of); Tehranchi, M.M., E-mail: teranchi@sbu.ac.ir [Laser and Plasma Research Institute, Shahid Beheshti University, Tehran (Iran, Islamic Republic of); Physics Department, Shahid Beheshti University, Tehran (Iran, Islamic Republic of); Hamidi, S.M. [Laser and Plasma Research Institute, Shahid Beheshti University, Tehran (Iran, Islamic Republic of); Khalkhali, S.M.H. [Physics Department, Kharazmi University, Tehran (Iran, Islamic Republic of)

2017-02-15

Highly sensitive atomic magnetometers use optically detected magnetic resonance of atomic spins to measure extremely weak magnetic field changes. The magnetometer sensitivity is directly proportional to the ratio of intensity to line-shape of the resonance signal. To obtain narrower resonance signal, we implemented harmonic detection of magnetic resonance method in M{sub x} configuration. The nonlinear spin polarization dynamics in detection of the higher harmonics were employed in phenomenological Bloch equations. The measured and simulated harmonic components of the resonance signals in frequency domain yielded significantly narrower line-width accompanying much improved sensitivity. Our results confirm the sensitivity improvement by a factor of two in optical atomic magnetometer via second harmonic signal which can open a new insight in the weak magnetic field measurement system design. - Highlights: • Highly sensitive atomic magnetometers have been used to measure weak magentic filed. • To obtain narrower resonance signal, we impalnted harmonic detection of magnetic resonance. • The nonlinear spin polarization dynamics in detetion of the higher harmonics were imployed.

Self-Calibrating Vector Helium Magnetometer (SVHM), Phase I

Data.gov (United States)

National Aeronautics and Space Administration — This Phase I SBIR proposal describes proposed development of a conceptual design for a Self-Calibrating Vector Helium Magnetometer (SVHM) for design and fabrication...

In-Flight Calibration Processes for the MMS Fluxgate Magnetometers

Science.gov (United States)

Bromund, K. R.; Leinweber, H. K.; Plaschke, F.; Strangeway, R. J.; Magnes, W.; Fischer, D.; Nakamura, R.; Anderson, B. J.; Russell, C. T.; Baumjohann, W.;

Particle swarm optimization algorithm based low cost magnetometer calibration

Science.gov (United States)

Ali, A. S.; Siddharth, S., Syed, Z., El-Sheimy, N.

2011-12-01

Inertial Navigation Systems (INS) consist of accelerometers, gyroscopes and a microprocessor provide inertial digital data from which position and orientation is obtained by integrating the specific forces and rotation rates. In addition to the accelerometers and gyroscopes, magnetometers can be used to derive the absolute user heading based on Earth's magnetic field. Unfortunately, the measurements of the magnetic field obtained with low cost sensors are corrupted by several errors including manufacturing defects and external electro-magnetic fields. Consequently, proper calibration of the magnetometer is required to achieve high accuracy heading measurements. In this paper, a Particle Swarm Optimization (PSO) based calibration algorithm is presented to estimate the values of the bias and scale factor of low cost magnetometer. The main advantage of this technique is the use of the artificial intelligence which does not need any error modeling or awareness of the nonlinearity. The estimated bias and scale factor errors from the proposed algorithm improve the heading accuracy and the results are also statistically significant. Also, it can help in the development of the Pedestrian Navigation Devices (PNDs) when combined with the INS and GPS/Wi-Fi especially in the indoor environments

In-Flight Calibration Processes for the MMS Fluxgate Magnetometers

Science.gov (United States)

Bromund, K. R.; Leinweber, H. K.; Plaschke, F.; Strangeway, R. J.; Magnes, W.; Fischer, D.; Nakamura, R.; Anderson, B. J.; Russell, C. T.; Baumjohann, W.; Chutter, M.; Torbert, R. B.; Le, G.; Slavin, J. A.; Kepko, L.

2015-12-01

The calibration effort for the Magnetospheric Multiscale Mission (MMS) Analog Fluxgate (AFG) and Digital Fluxgate (DFG) magnetometers is a coordinated effort between three primary institutions: University of California, Los Angeles (UCLA); Space Research Institute, Graz, Austria (IWF); and Goddard Space Flight Center (GSFC). Since the successful deployment of all 8 magnetometers on 17 March 2015, the effort to confirm and update the ground calibrations has been underway during the MMS commissioning phase. The in-flight calibration processes evaluate twelve parameters that determine the alignment, orthogonalization, offsets, and gains for all 8 magnetometers using algorithms originally developed by UCLA and the Technical University of Braunschweig and tailored to MMS by IWF, UCLA, and GSFC. We focus on the processes run at GSFC to determine the eight parameters associated with spin tones and harmonics. We will also discuss the processing flow and interchange of parameters between GSFC, IWF, and UCLA. IWF determines the low range spin axis offsets using the Electron Drift Instrument (EDI). UCLA determines the absolute gains and sensor azimuth orientation using Earth field comparisons. We evaluate the performance achieved for MMS and give examples of the quality of the resulting calibrations.

The Pioneer 11 high-field fluxgate magnetometer

Science.gov (United States)

Acuna, M. H.; Ness, N. F.

1973-01-01

The High Field Fluxgate Magnetometer Experiment flow aboard the Pioneer 11 spacecraft to investigate Jupiter's magnetic field is described. The instrument extends the spacecraft's upper limit measurement capability by more than an order of magnitude to 17.3 gauss with minimum power and volume requirements.

Development of Geomagnetic Monitoring System Using a Magnetometer for the Field

Science.gov (United States)

Lee, Young-Cheol; Kim, Sung-Wook; Choi, Eun-Kyeong; Kim, In-Soo

2014-05-01

Three institutes including KMA (Korea Meteorological Administration), KSWC (Korean Space Weather Center) of NRRA (National Radio Research Agency) and KIGAM (Korea Institute of Geoscience and Mineral Resources) are now operating magnetic observatories. Those observatories observe the total intensity and three components of geomagnetic element. This paper comes up with a magnetic monitoring system now under development that uses a magnetometer for field survey. In monitoring magnetic variations in areas (active faults or volcanic regions), more reliable results can be obtained when an array of several magnetometers are used rather than a single magnetometer. In order to establish and operate a magnetometer array, such factors as expenses, convenience of the establishment and operation of the array should be taken into account. This study has come up with a magnetic monitoring system complete with a magnetometer for the field survey of our own designing. A magnetic monitoring system, which is composed of two parts. The one is a field part and the other a data part. The field part is composed of a magnetometer, an external memory module, a power supply and a set of data transmission equipment. The data part is a data server which can store the data transmitted from the field part, analyze the data and provide service to the web. This study has developed an external memory module for ENVI-MAG (Scintrex Ltd.) using an embedded Cortex-M3 board, which can be programmed, attach other functional devices (SD memory cards, GPS antennas for time synchronization, ethernet cards and so forth). The board thus developed can store magnetic measurements up to 8 Gbytes, synchronize with the GPS time and transmit the magnetic measurements to the data server which is now under development. A monitoring system of our own developing was installed in Jeju island, taking measurements throughout Korea. Other parts including a data transfer module, a server and a power supply using solar

Obtaining 'images' from iron objects using a 3-axis fluxgate magnetometer

International Nuclear Information System (INIS)

Chilo, Jose; Jabor, Abbas; Lizska, Ludwik; Eide, Age J.; Lindblad, Thomas

2007-01-01

Magnetic objects can cause local variations in the Earth's magnetic field that can be measured with a magnetometer. Here we used tri-axial magnetometer measurements and an analysis method employing wavelet techniques to determine the 'signature' or 'fingerprint' of different iron objects. Clear distinctions among the iron samples were observed. The time-dependent changes in the frequency powers were extracted by use of the Morlet wavelet corresponding to frequency bands from 0.1 to 100 Hz

Empirical Determination of Efficient Sensing Frequencies for Magnetometer-Based Continuous Human Contact Monitoring

Directory of Open Access Journals (Sweden)

Seungho Kuk

2018-04-01

Full Text Available The high linear correlation between the smartphone magnetometer readings in close proximity can be exploited for physical human contact detection, which could be useful for such applications as infectious disease contact tracing or social behavior monitoring. Alternative approaches using other capabilities in smartphones have aspects that do not fit well with the human contact detection. Using Wi-Fi or cellular fingerprints have larger localization errors than close human contact distances. Bluetooth beacons could reveal the identity of the transmitter, threatening the privacy of the user. Also, using sensors such as GPS does not work for indoor contacts. However, the magnetometer correlation check works best in human contact distances that matter in infectious disease transmissions or social interactions. The omni-present geomagnetism makes it work both indoors and outdoors, and the measured magnetometer values do not easily reveal the identity and the location of the smartphone. One issue with the magnetometer-based contact detection, however, is the energy consumption. Since the contacts can take place anytime, the magnetometer sensing and recording should be running continuously. Therefore, how we address the energy requirement for the extended and continuous operation can decide the viability of the whole idea. However, then, we note that almost all existing magnetometer-based applications such as indoor location and navigation have used high sensing frequencies, ranging from 10 Hz to 200 Hz. At these frequencies, we measure that the time to complete battery drain in a typical smartphone is shortened by three to twelve hours. The heavy toll raises the question as to whether the magnetometer-based contact detection can avoid such high sensing rates while not losing the contact detection accuracy. In order to answer the question, we conduct a measurement-based study using independently produced magnetometer traces from three different

Empirical Determination of Efficient Sensing Frequencies for Magnetometer-Based Continuous Human Contact Monitoring.

Science.gov (United States)

Kuk, Seungho; Kim, Junha; Park, Yongtae; Kim, Hyogon

2018-04-27

The high linear correlation between the smartphone magnetometer readings in close proximity can be exploited for physical human contact detection, which could be useful for such applications as infectious disease contact tracing or social behavior monitoring. Alternative approaches using other capabilities in smartphones have aspects that do not fit well with the human contact detection. Using Wi-Fi or cellular fingerprints have larger localization errors than close human contact distances. Bluetooth beacons could reveal the identity of the transmitter, threatening the privacy of the user. Also, using sensors such as GPS does not work for indoor contacts. However, the magnetometer correlation check works best in human contact distances that matter in infectious disease transmissions or social interactions. The omni-present geomagnetism makes it work both indoors and outdoors, and the measured magnetometer values do not easily reveal the identity and the location of the smartphone. One issue with the magnetometer-based contact detection, however, is the energy consumption. Since the contacts can take place anytime, the magnetometer sensing and recording should be running continuously. Therefore, how we address the energy requirement for the extended and continuous operation can decide the viability of the whole idea. However, then, we note that almost all existing magnetometer-based applications such as indoor location and navigation have used high sensing frequencies, ranging from 10 Hz to 200 Hz. At these frequencies, we measure that the time to complete battery drain in a typical smartphone is shortened by three to twelve hours. The heavy toll raises the question as to whether the magnetometer-based contact detection can avoid such high sensing rates while not losing the contact detection accuracy. In order to answer the question, we conduct a measurement-based study using independently produced magnetometer traces from three different countries. Specifically, we

GIOTTO MAGNETOMETER 8 SECOND DATA V1.0

Data.gov (United States)

National Aeronautics and Space Administration — The main objective of the Giotto Magnetometer Experiment is the investigation of the interaction between Comet Halley and the solar wind at a distance of 0.9 AU from...

Machine Learning Based Localization and Classification with Atomic Magnetometers

Science.gov (United States)

Deans, Cameron; Griffin, Lewis D.; Marmugi, Luca; Renzoni, Ferruccio

2018-01-01

We demonstrate identification of position, material, orientation, and shape of objects imaged by a Rb 85 atomic magnetometer performing electromagnetic induction imaging supported by machine learning. Machine learning maximizes the information extracted from the images created by the magnetometer, demonstrating the use of hidden data. Localization 2.6 times better than the spatial resolution of the imaging system and successful classification up to 97% are obtained. This circumvents the need of solving the inverse problem and demonstrates the extension of machine learning to diffusive systems, such as low-frequency electrodynamics in media. Automated collection of task-relevant information from quantum-based electromagnetic imaging will have a relevant impact from biomedicine to security.

Athermal fiber laser for the SWARM absolute scalar magnetometer

Science.gov (United States)

Fourcault, W.; Léger, J.-M.; Costes, V.; Fratter, I.; Mondin, L.

2017-11-01

The Absolute Scalar Magnetometer (ASM) developed by CEA-LETI/CNES is an optically pumped 4He magnetic field sensor based on the Zeeman effect and an electronic magnetic resonance whose effects are amplified by a laser pumping process [1-2]. Consequently, the role of the laser is to pump the 4He atoms at the D0 transition as well as to allow the magnetic resonance signal detection. The ASM will be the scalar magnetic reference instrument of the three ESA Swarm satellites to be launched in 2012 in order to carry out the best ever survey of the Earth magnetic field and its temporal evolution. The sensitivity and accuracy of this magnetometer based on 4He optical pumping depend directly on the characteristics of its light source, which is the key sub-system of the sensor. We describe in this paper the selected fiber laser architecture and its wavelength stabilization scheme. Its main performance in terms of spectral emission, optical power at 1083 nm and intensity noise characteristics in the frequency bands used for the operation of the magnetometer, are then presented. Environmental testing results (thermal vacuum cycling, vibrations, shocks and ageing) are also reported at the end of this paper.

High Tc Josephson Junctions, SQUIDs and magnetometers

International Nuclear Information System (INIS)

Clarke, J.

1991-01-01

There has recently been considerable progress in the state-of-the-art of high-T c magnetometers based on dc SQUIDs (Superconducting Quantum Interference Devices). This progress is due partly to the development of more manufacturable Josephson junctions, making SQUIDs easier to fabricate, and partly to the development of multiturn flux transformers that convert the high sensitivity of SQUIDs to magnetic flux to a correspondingly high sensitivity to magnetic field. Needless to say, today's high-T c SQUIDs are still considerably less sensitive than their low-T c counterparts, particularly at low frequencies (f) where their level of 1/f noise remains high. Nonetheless, the performance of the high-T c devices has now reached the point where they are adequate for a number of the less demanding applications; furthermore, as we shall see, at least modest improvements in performance are expected in the near future. In this article, the author outlines these various developments. This is far from a comprehensive review of the field, however, and, apart from Sec. 2, he describes largely his own work. He begins in Sec. 2 with an overview of the various types of Josephson junctions that have been investigated, and in Sec. 3, he describes some of the SQUIDs that have been tested, and assess their performance. Section 4 discuss the development of the multilayer structures essential for an interconnect technology, and, in particular, for crossovers and vias. Section 5 shows how this technology enables one to fabricate multiturn flux transformers which, in turn, can be coupled to SQUIDs to make magnetometers. The performance and possible future improvements in these magnetometers are assessed, and some applications mentioned

MgB2 magnetometer with a directly coupled pick-up loop

Science.gov (United States)

Portesi, C.; Mijatovic, D.; Veldhuis, D.; Brinkman, A.; Monticone, E.; Gonnelli, R. S.

2006-05-01

In this work, we show the results obtained in the fabrication and characterization of an MgB2 magnetometer with a directly coupled pick-up loop. We used an all in situ technique for fabricating magnesium diboride films, which consists of the co-evaporation of B and Mg by means of an e-gun and a resistive heater respectively. Consequently, we realized the superconducting device, which incorporates two nanobridges as weak links in a superconducting loop. The nanobridges were realized by focused ion beam milling; they were 240 nm wide and had a critical current density of 107 A cm-2. The magnetometer was characterized at different temperatures and also measurements of the noise levels have been performed. The device shows Josephson quantum interference up to 20 K and the calculated effective area at low temperatures was 0.24 mm2. The transport properties of the magnetometer allow determining fundamental materials properties of the MgB2 thin films, such as the penetration depth.

Choice of optimal parameters for the superconductive quantum magnetometer

Energy Technology Data Exchange (ETDEWEB)

Vasiliev, B V; Ivanenko, A I; Trofimov, V N

1974-12-31

The problem of choosing the optimal coupling coefficient and optimal working frequency for superconductive quantum magnetometer is considered. The present experimental signalnoise dependence confirms the drawn conclusions. (auth)

Mathematical model of a fluxgate magnetometer

OpenAIRE

Baranov Pavel F.; Baranova Vitalia E.; Nesterenko Tamara G.

2018-01-01

In paper analytical equations for calculate the electromotive force in the measuring coil of the fluxgate magnetometer independent of the drive signal frequency content are presented. Also, the equations for es-timation of the fluxgate sensitivity at any harmonic and for study fluxgates operation with a glance to the waveform and the polynomial approximation of the mean magnetization curve of the core are provided.

Mathematical model of a fluxgate magnetometer

Directory of Open Access Journals (Sweden)

Baranov Pavel F.

2018-01-01

Full Text Available In paper analytical equations for calculate the electromotive force in the measuring coil of the fluxgate magnetometer independent of the drive signal frequency content are presented. Also, the equations for es-timation of the fluxgate sensitivity at any harmonic and for study fluxgates operation with a glance to the waveform and the polynomial approximation of the mean magnetization curve of the core are provided.

Fluxgate magnetometers for outer planets exploration

Science.gov (United States)

Acuna, M. H.

1974-01-01

The exploration of the interplanetary medium and the magnetospheres of the outer planets requires the implementation of magnetic field measuring instrumentation with wide dynamic range, high stability, and reliability. The fluxgate magnetometers developed for the Pioneer 11 and Mariner-Jupiter-Saturn missions are presented. These instruments cover the range of .01 nT to 2 million nT with optimum performance characteristics and low power consumption.

Digital Detection and feedback Fluxgate Magnetometer

DEFF Research Database (Denmark)

Piil-Henriksen, J.; Merayo, José M.G.; Nielsen, Otto V

1996-01-01

A new full Earth's field dynamic feedback fluxgate magnetometer is described. It is based entirely on digital signal processing and digital feedback control, thereby replacing the classical second harmonic tuned analogue electronics by processor algorithms. Discrete mathematical cross......-correlation routines and substantial oversampling reduce the noise to 71 pT root-mean-square in a 0.25-10 Hz bandwidth for a full Earth's field range instrument....

Optimizations of spin-exchange relaxation-free magnetometer based on potassium and rubidium hybrid optical pumping

International Nuclear Information System (INIS)

Fang, Jiancheng; Wang, Tao; Li, Yang; Zhang, Hong; Zou, Sheng

2014-01-01

The hybrid optical pumping atomic magnetometers have not realized its theoretical sensitivity, the optimization is critical for optimal performance. The optimizations proposed in this paper are suitable for hybrid optical pumping atomic magnetometer, which contains two alkali species. To optimize the parameters, the dynamic equations of spin evolution with two alkali species were solved, whose steady-state solution is used to optimize the parameters. The demand of the power of the pump beam is large for hybrid optical pumping. Moreover, the sensitivity of the hybrid optical pumping magnetometer increases with the increase of the power density of the pump beam. The density ratio between the two alkali species is especially important for hybrid optical pumping magnetometer. A simple expression for optimizing the density ratio is proposed in this paper, which can help to determine the mole faction of the alkali atoms in fabricating the hybrid cell before the cell is sealed. The spin-exchange rate between the two alkali species is proportional to the saturated density of the alkali vapor, which is highly dependent on the temperature of the cell. Consequently, the sensitivity of the hybrid optical pumping magnetometer is dependent on the temperature of the cell. We proposed the thermal optimization of the hybrid cell for a hybrid optical pumping magnetometer, which can improve the sensitivity especially when the power of the pump beam is low. With these optimizations, a sensitivity of approximately 5 fT/Hz 1/2 is achieved with gradiometer arrangement

Aspartic acid incorporated monolithic columns for affinity glycoprotein purification.

Science.gov (United States)

Armutcu, Canan; Bereli, Nilay; Bayram, Engin; Uzun, Lokman; Say, Rıdvan; Denizli, Adil

2014-02-01

Novel aspartic acid incorporated monolithic columns were prepared to efficiently affinity purify immunoglobulin G (IgG) from human plasma. The monolithic columns were synthesised in a stainless steel HPLC column (20 cm × 5 mm id) by in situ bulk polymerisation of N-methacryloyl-L-aspartic acid (MAAsp), a polymerisable derivative of L-aspartic acid, and 2-hydroxyethyl methacrylate (HEMA). Monolithic columns [poly(2-hydroxyethyl methacrylate-N-methacryloyl-L-aspartic acid) (PHEMAsp)] were characterised by swelling studies, Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). The monolithic columns were used for IgG adsorption/desorption from aqueous solutions and human plasma. The IgG adsorption depended on the buffer type, and the maximum IgG adsorption from aqueous solution in phosphate buffer was 0.085 mg/g at pH 6.0. The monolithic columns allowed for one-step IgG purification with a negligible capacity decrease after ten adsorption-desorption cycles. Copyright © 2013 Elsevier B.V. All rights reserved.

Development of Magnetometer Digital Circuit for KSR-3 Rocket and Analytical Study on Calibration Result

Directory of Open Access Journals (Sweden)

Eun-Seok Lee

2002-12-01

Full Text Available This paper describes the re-design and the calibration results of the MAG digital circuit onboard the KSR-3. We enhanced the sampling rate of magnetometer data. Also, we reduced noise and increased authoritativeness of data. We could confirm that AIM resolution was decreased less than 1nT of analog calibration by a digital calibration of magnetometer. Therefore, we used numerical-program to correct this problem. As a result, we could calculate correction and error of data. These corrections will be applied to magnetometer data after the launch of KSR-3.

Dopamine-imprinted monolithic column for capillary electrochromatography.

Science.gov (United States)

Aşır, Süleyman; Sarı, Duygu; Derazshamshir, Ali; Yılmaz, Fatma; Şarkaya, Koray; Denizli, Adil

2017-11-01

A dopamine-imprinted monolithic column was prepared and used in capillary electrochromatography as stationary phase for the first time. Dopamine was selectively separated from aqueous solution containing the competitor molecule norepinephrine, which is similar in size and shape to the template molecule. Morphology of the dopamine-imprinted column was observed by scanning electron microscopy. The influence of the organic solvent content of mobile phase, applied pressure and pH of the mobile phase on the recognition of dopamine by the imprinted monolithic column has been evaluated, and the imprinting effect in the dopamine-imprinted monolithic polymer was verified. Developed dopamine-imprinted monolithic column resulted in excellent separation of dopamine from structurally related competitor molecule, norepinephrine. Separation was achieved in a short period of 10 min, with the electrophoretic mobility of 5.81 × 10 -5  m 2 V -1 s -1 at pH 5.0 and 500 mbar pressure. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Attitude-independent magnetometer calibration for marine magnetic surveys: regularization issue

International Nuclear Information System (INIS)

Wu, Zhitian; Hu, Xiaoping; Wu, Meiping; Cao, Juliang

2013-01-01

We have developed an attitude-independent calibration method for a shipboard magnetometer to estimate the absolute strength of the geomagnetic field from a marine vessel. The three-axis magnetometer to be calibrated is fixed on a rigid aluminium boom ahead of the vessel to reduce the magnetic effect of the vessel. Due to the constrained manoeuvres of the vessel, a linear observational equation system for calibration parameter estimation is severely ill-posed. Consequently, if the issue is not mitigated, traditional calibration methods may result in unreliable or unsuccessful solutions. In this paper, the ill-posed problem is solved by using the truncated total least squares (TTLS) technique. This method takes advantage of simultaneously considering errors on both sides of the observation equation. Furthermore, the TTLS method suits strongly ill-posed problems. Simulations and experiments have been performed to assess the performance of the TTLS method and to compare it with the performance of conventional regularization approaches such as the Tikhonov method and truncated single value decomposition. The results show that the proposed algorithm can effectively mitigate the ill-posed problem and is more stable than the compared regularization methods for magnetometer calibration applications. (paper)

Coherent population trapping magnetometer by differential detecting magneto–optic rotation effect

International Nuclear Information System (INIS)

Zhang Fan; Tian Yuan; Zhang Yi; Gu Si-Hong

2016-01-01

A pocket coherent population trapping (CPT) atomic magnetometer scheme that uses a vertical cavity surface emitting laser as a light source is proposed and experimentally investigated. Using the differential detecting magneto–optic rotation effect, a CPT spectrum with the background canceled and a high signal-to-noise ratio is obtained. The experimental results reveal that the sensitivity of the proposed scheme can be improved by half an order, and the ability to detect weak magnetic fields is extended one-fold. Therefore, the proposed scheme is suited to realize a pocket-size CPT magnetometer. (paper)

Comparison of a triaxial fluxgate magnetometer and Toftness sensometer for body surface EMF measurement.

Science.gov (United States)

Zhang, John; Toftness, Dave; Snyder, Brian; Nosco, Dennis; Balcavage, Walter; Nindl, Gabi

2004-12-01

The use of magnetic fields to treat disease has intrigued mankind since the time of the ancient Greeks. More recently it has been shown that electromagnetic field (EMF) treatment aids bone healing, and repetitive transcranial magnetic stimulation (rTMS) appears to be beneficial in treating schizophrenia and depression. Since external EMFs influence internal body processes, we hypothesized that measurement of body surface EMFs might be used to detect disease states and direct the course of subsequent therapy. However, measurement of minute body surface EMFs requires use of a sensitive and well documented magnetometer. In this study we evaluated the sensitivity and frequency response of a fluxgate magnetometer with a triaxial probe for use in detecting body surface EMF and we compared the magnetometer readings with a signal from a Toftness Sensometer, operated by an experienced clinician, in the laboratory and in a clinical setting. A Peavy Audio Amplifier and variable power output Telulex signal generator were used to develop 50 microT EMFs in a three coil Merritt coil system. A calibrated magnetometer was used to set a 60 Hz 50 microT field in the coil and an ammeter was used to measure the current required to develop the 50 microT field. At frequencies other than 60 Hz, the field strength was maintained at 50 microT by adjusting the Telulex signal output to keep the current constant. The field generated was monitored using a 10 turn coil connected to an oscilloscope. The oscilloscope reading indicated that the field strength was the same at all frequencies tested. To determine if there was a correspondence between the signals detected by a fluxgate magnetometer (FGM1) and the Toftness Sensometer both devices were placed in the Merritt coil and readings were recorded from the FGM1 and compared with the ability of a highly experienced Toftness operator to detect the 50 microT field. Subsequently, in a clinical setting, FGM1 readings made by an FGM1 technician and

Integrated high-transition temperature magnetometer with only two superconducting layers

DEFF Research Database (Denmark)

Kromann, R.; Kingston, J.J.; Miklich, A.H.

1993-01-01

We describe the fabrication and testing of an integrated YBa2Cu3O7-x thin-film magnetometer consisting of a dc superconducting quantum interference device (SQUID), with biepitaxial grain boundary junctions, integrated with a flux transformer on a single substrate. Only two superconducting layers...... are required, the SQUID body serving as the crossunder that completes the multiturn flux transformer. The highest temperature at which any of the magnetometers functioned was 76 K. At 60 K the magnetic field gain of this device was 63, and the magnetic field noise was 160 fT Hz-1/2 at 2 kHz, increasing to 3...

The simple procedure for the fluxgate magnetometers calibration

Science.gov (United States)

Marusenkov, Andriy

2014-05-01

The fluxgate magnetometers are widely used in geophysics investigations including the geomagnetic field monitoring at the global network of geomagnetic observatories as well as for electromagnetic sounding of the Earth's crust conductivity. For solving these tasks the magnetometers have to be calibrated with an appropriate level of accuracy. As a particular case, the ways to satisfy the recent requirements to the scaling and orientation errors of 1-second INTERNAGNET magnetometers are considered in the work. The goal of the present study was to choose a simple and reliable calibration method for estimation of scale factors and angular errors of the three-axis magnetometers in the field. There are a large number of the scalar calibration methods, which use a free rotation of the sensor in the calibration field followed by complicated data processing procedures for numerical solution of the high-order equations set. The chosen approach also exploits the Earth's magnetic field as a calibrating signal, but, in contrast to other methods, the sensor has to be oriented in some particular positions in respect to the total field vector, instead of the sensor free rotation. This allows to use very simple and straightforward linear computation formulas and, as a result, to achieve more reliable estimations of the calibrated parameters. The estimation of the scale factors is performed by the sequential aligning of each component of the sensor in two positions: parallel and anti-parallel to the Earth's magnetic field vector. The estimation of non-orthogonality angles between each pair of components is performed after sequential aligning of the components at the angles +/- 45 and +/- 135 degrees of arc in respect to the total field vector. Due to such four positions approach the estimations of the non-orthogonality angles are invariant to the zero offsets and non-linearity of transfer functions of the components. The experimental justifying of the proposed method by means of the

Validation of the GOES-16 magnetometer using multipoint measurements and magnetic field models

Science.gov (United States)

Califf, S.; Loto'aniu, P. T. M.; Redmon, R. J.; Sarris, T. E.; Brito, T.

2017-12-01

The Geostationary Operational Environmental Satellites (GOES) have been providing continuous geomagnetic field measurements for over 40 years. While the primary purpose of GOES is operational, the magnetometer data are also widely used in the scientific community. In an effort to validate the recently launched GOES-16 magnetometer, we compare the measurements to existing magnetic field models and other GOES spacecraft currently on orbit. There are four concurrent measurements from GOES-13, 14, 15 and 16 spanning 75W to 135W longitude. Also, GOES-13 is being replaced by GOES-16 in the GOES-East location, and during the transition, GOES-13 and GOES-16 will be parked nearby in order to assist with calibration of the new operational satellite. This work explores techniques to quantify the performance of the GOES-16 magnetometer by comparison to data from nearby spacecraft. We also build on previous work to assimilate in situ measurements with existing magnetic field models to assist in comparing data from different spatial locations. Finally, we use this unique dataset from four simultaneous geosynchronous magnetometer measurements and the close separation between GOES-13 and GOES-16 to study the spatial characteristics of ULF waves and other magnetospheric processes.

Automated system for the calibration of magnetometers

International Nuclear Information System (INIS)

Petrucha, Vojtech; Kaspar, Petr; Ripka, Pavel; Merayo, Jose M. G.

2009-01-01

A completely nonmagnetic calibration platform has been developed and constructed at DTU Space (Technical University of Denmark). It is intended for on-site scalar calibration of high-precise fluxgate magnetometers. An enhanced version of the same platform is being built at the Czech Technical University. There are three axes of rotation in this design (compared to two axes in the previous version). The addition of the third axis allows us to calibrate more complex devices. An electronic compass based on a vector fluxgate magnetometer and micro electro mechanical systems (MEMS) accelerometer is one example. The new platform can also be used to evaluate the parameters of the compass in all possible variations in azimuth, pitch, and roll. The system is based on piezoelectric motors, which are placed on a platform made of aluminum, brass, plastic, and glass. Position sensing is accomplished through custom-made optical incremental sensors. The system is controlled by a microcontroller, which executes commands from a computer. The properties of the system as well as calibration and measurement results will be presented

Detection Range of Airborne Magnetometers in Magnetic Anomaly Detection

Directory of Open Access Journals (Sweden)

Chengjing Li

2015-11-01

Full Text Available Airborne magnetometers are utilized for the small-range search, precise positioning, and identification of the ferromagnetic properties of underwater targets. As an important performance parameter of sensors, the detection range of airborne magnetometers is commonly set as a fixed value in references regardless of the influences of environment noise, target magnetic properties, and platform features in a classical model to detect airborne magnetic anomalies. As a consequence, deviation in detection ability analysis is observed. In this study, a novel detection range model is proposed on the basis of classic detection range models of airborne magnetometers. In this model, probability distribution is applied, and the magnetic properties of targets and the environment noise properties of a moving submarine are considered. The detection range model is also constructed by considering the distribution of the moving submarine during detection. A cell-averaging greatest-of-constant false alarm rate test method is also used to calculate the detection range of the model at a desired false alarm rate. The detection range model is then used to establish typical submarine search probabilistic models. Results show that the model can be used to evaluate not only the effects of ambient magnetic noise but also the moving and geomagnetic features of the target and airborne detection platform. The model can also be utilized to display the actual operating range of sensor systems.

The Future of Ground Magnetometer Arrays in Support of Space Weather Monitoring and Research

Science.gov (United States)

Engebretson, Mark; Zesta, Eftyhia

2017-11-01

A community workshop was held in Greenbelt, Maryland, on 5-6 May 2016 to discuss recommendations for the future of ground magnetometer array research in space physics. The community reviewed findings contained in the 2016 Geospace Portfolio Review of the Geospace Section of the Division of Atmospheric and Geospace Science of the National Science Foundation and discussed the present state of ground magnetometer arrays and possible pathways for a more optimal, robust, and effective organization and scientific use of these ground arrays. This paper summarizes the report of that workshop to the National Science Foundation (Engebretson & Zesta, as well as conclusions from two follow-up meetings. It describes the current state of U.S.-funded ground magnetometer arrays and summarizes community recommendations for changes in both organizational and funding structures. It also outlines a variety of new and/or augmented regional and global data products and visualizations that can be facilitated by increased collaboration among arrays. Such products will enhance the value of ground-based magnetometer data to the community's effort for understanding of Earth's space environment and space weather effects.

Mid-latitude Geomagnetic Field Analysis Using BOH Magnetometer: Preliminary Results

Directory of Open Access Journals (Sweden)

Junga Hwang

2011-09-01

Full Text Available Korea Astronomy and Space Science Institute researchers have installed and operated magnetometers at Mt. Bohyun Observatory to measure the Earth's magnetic field variations in South Korea. We, in 2007, installed a fluxgate magnetometer (RFP-523C to measure H, D, and Z components of the geomagnetic field. In addition, in 2009, we installed a Overhauser proton sensor to measure the absolute total magnetic field F and a three-axis magneto-impedance sensor for spectrum analysis. Currently three types of magnetometer data have been accumulated. In this paper, we provide the preliminary and the first statistical analysis using the BOH magnetometer installed at Mt. Bohyun Observatory. By superposed analysis, we find that daily variations of H, D, and Z shows similar tendency, that is, about 30 minutes before the meridian (11:28 a minimum appears and the time after about 3 hours and 30 minutes (15:28 a maximum appears. Also, a quiet interval start time (19:06 is near the sunset time, and a quiet interval end time (06:40 is near the sunrise time. From the sunset to the sunrise, the value of H has a nearly constant interval, that is, the sun affects the changes in H values. Seasonal variations show similar dependences to the sun. Local time variations show that noon region has the biggest variations and midnight region has the smallest variations. We compare the correlations between geomagnetic variations and activity indices as we expect the geomagnetic variation would contain the effects of geomagnetic activity variations. As a result, the correlation coefficient between H and Dst is the highest (r = 0.947, and other AL, AE, AU index and showed a high correlation. Therefore, the effects of geomagnetic storms and geomagnetic substorms might contribute to the geomagnetic changes significantly.

Z3 model of Saturns magnetic field and the Pioneer 11 vector helium magnetometer observations

International Nuclear Information System (INIS)

Connerney, J.E.P.; Acuna, M.H.; Ness, N.F.

1984-05-01

Magnetic field observations obtained by the Pioneer 11 vector helium magnetometer are compared with the Z(sub 3) model magnetic field. These Pioneer 11 observations, obtained at close-in radial distances, constitute an important and independent test of the Z(sub 3) zonal harmonic model, which was derived from Voyager 1 and Voyager 2 fluxgate magnetometer observations. Differences between the Pioneer 11 magnetometer and the Z(sub 3) model field are found to be small (approximately 1%) and quantitatively consistent with the expected instrumental accuracy. A detailed examination of these differences in spacecraft payload coordinates shows that they are uniquely associated with the instrument frame of reference and operation. A much improved fit to the Pioneer 11 observations is obtained by rotation of the instrument coordinate system about the spacecraft spin axis by 1.4 degree. With this adjustment, possibly associated with an instrumental phase lag or roll attitude error, the Pioneer 11 vector helium magnetometer observations are fully consistent with the Voyager Z(sub 3) model

High temperature superconductive flux gate magnetometer

International Nuclear Information System (INIS)

Gershenson, M.

1991-01-01

This paper proposes a different type of HTS superconducting magnetometer based on the non-linear magnetic behavior of bulk HTS materials. The device design is based on the generation of second harmonics which arise as a result of non-linear magnetization observed in Type-II superconductors. Even harmonics are generated from the non-linear interaction of an ac excitation signal with an external DC magnetic field which acts as a bias signal

Automatic torque magnetometer for vacuum-to-high-pressure hydrogen environments

International Nuclear Information System (INIS)

Larsen, J.W.; Livesay, B.R.

1979-01-01

An automatic torque magnetometer has been developed for use in high-pressure hydrogen. It will contain pressures ranging from vacuum to 200 atm of hydrogen gas at sample temperatures greater than 400 0 C. This magnetometer, which uses an optical lever postion sensor and a restoring force technique has an operating range of 2.0 x 10 3 dyn cm to l.6 x 10 -4 dyn cm. An accompanying digital data collection system extends the sensitivity to 1 x 10 -5 dyn cm as well as increasing the data handling capacity of the system. The magnetic properties of thin films in high-temperature and high-pressure hydrogen environments can be studied using this instruments

The absolute magnetometers on board Swarm, lessons learned from more than two years in space

DEFF Research Database (Denmark)

Hulot, Gauthier; Leger, Jean-Michel; Vigneron, Pierre

ESA's Swarm satellites carry 4He absolute magnetometers (ASM), designed by CEA-Léti and developed in partnership with CNES. These instruments are the first-ever space-borne magnetometers to use a common sensor to simultaneously deliver 1Hz independent absolute scalar and vector readings of the ma...

A game-theoretic approach for calibration of low-cost magnetometers under noise uncertainty

Science.gov (United States)

Siddharth, S.; Ali, A. S.; El-Sheimy, N.; Goodall, C. L.; Syed, Z. F.

2012-02-01

Pedestrian heading estimation is a fundamental challenge in Global Navigation Satellite System (GNSS)-denied environments. Additionally, the heading observability considerably degrades in low-speed mode of operation (e.g. walking), making this problem even more challenging. The goal of this work is to improve the heading solution when hand-held personal/portable devices, such as cell phones, are used for positioning and to improve the heading estimation in GNSS-denied signal environments. Most smart phones are now equipped with self-contained, low cost, small size and power-efficient sensors, such as magnetometers, gyroscopes and accelerometers. A magnetometer needs calibration before it can be properly employed for navigation purposes. Magnetometers play an important role in absolute heading estimation and are embedded in many smart phones. Before the users navigate with the phone, a calibration is invoked to ensure an improved signal quality. This signal is used later in the heading estimation. In most of the magnetometer-calibration approaches, the motion modes are seldom described to achieve a robust calibration. Also, suitable calibration approaches fail to discuss the stopping criteria for calibration. In this paper, the following three topics are discussed in detail that are important to achieve proper magnetometer-calibration results and in turn the most robust heading solution for the user while taking care of the device misalignment with respect to the user: (a) game-theoretic concepts to attain better filter parameter tuning and robustness in noise uncertainty, (b) best maneuvers with focus on 3D and 2D motion modes and related challenges and (c) investigation of the calibration termination criteria leveraging the calibration robustness and efficiency.

A game-theoretic approach for calibration of low-cost magnetometers under noise uncertainty

International Nuclear Information System (INIS)

Siddharth, S; Ali, A S; El-Sheimy, N; Goodall, C L; Syed, Z F

2012-01-01

Pedestrian heading estimation is a fundamental challenge in Global Navigation Satellite System (GNSS)-denied environments. Additionally, the heading observability considerably degrades in low-speed mode of operation (e.g. walking), making this problem even more challenging. The goal of this work is to improve the heading solution when hand-held personal/portable devices, such as cell phones, are used for positioning and to improve the heading estimation in GNSS-denied signal environments. Most smart phones are now equipped with self-contained, low cost, small size and power-efficient sensors, such as magnetometers, gyroscopes and accelerometers. A magnetometer needs calibration before it can be properly employed for navigation purposes. Magnetometers play an important role in absolute heading estimation and are embedded in many smart phones. Before the users navigate with the phone, a calibration is invoked to ensure an improved signal quality. This signal is used later in the heading estimation. In most of the magnetometer-calibration approaches, the motion modes are seldom described to achieve a robust calibration. Also, suitable calibration approaches fail to discuss the stopping criteria for calibration. In this paper, the following three topics are discussed in detail that are important to achieve proper magnetometer-calibration results and in turn the most robust heading solution for the user while taking care of the device misalignment with respect to the user: (a) game-theoretic concepts to attain better filter parameter tuning and robustness in noise uncertainty, (b) best maneuvers with focus on 3D and 2D motion modes and related challenges and (c) investigation of the calibration termination criteria leveraging the calibration robustness and efficiency. (paper)

Performance Improvement of Inertial Navigation System by Using Magnetometer with Vehicle Dynamic Constraints

Directory of Open Access Journals (Sweden)

Daehee Won

2015-01-01

Full Text Available A navigation algorithm is proposed to increase the inertial navigation performance of a ground vehicle using magnetic measurements and dynamic constraints. The navigation solutions are estimated based on inertial measurements such as acceleration and angular velocity measurements. To improve the inertial navigation performance, a three-axis magnetometer is used to provide the heading angle, and nonholonomic constraints (NHCs are introduced to increase the correlation between the velocity and the attitude equation. The NHCs provide a velocity feedback to the attitude, which makes the navigation solution more robust. Additionally, an acceleration-based roll and pitch estimation is applied to decrease the drift when the acceleration is within certain boundaries. The magnetometer and NHCs are combined with an extended Kalman filter. An experimental test was conducted to verify the proposed method, and a comprehensive analysis of the performance in terms of the position, velocity, and attitude showed that the navigation performance could be improved by using the magnetometer and NHCs. Moreover, the proposed method could improve the estimation performance for the position, velocity, and attitude without any additional hardware except an inertial sensor and magnetometer. Therefore, this method would be effective for ground vehicles, indoor navigation, mobile robots, vehicle navigation in urban canyons, or navigation in any global navigation satellite system-denied environment.

Construction and calibration of a low cost and fully automated vibrating sample magnetometer

International Nuclear Information System (INIS)

El-Alaily, T.M.; El-Nimr, M.K.; Saafan, S.A.; Kamel, M.M.; Meaz, T.M.; Assar, S.T.

2015-01-01

A low cost vibrating sample magnetometer (VSM) has been constructed by using an electromagnet and an audio loud speaker; where both are controlled by a data acquisition device. The constructed VSM records the magnetic hysteresis loop up to 8.3 KG at room temperature. The apparatus has been calibrated and tested by using magnetic hysteresis data of some ferrite samples measured by two scientifically calibrated magnetometers; model (Lake Shore 7410) and model (LDJ Electronics Inc. Troy, MI). Our VSM lab-built new design proved success and reliability. - Highlights: • A low cost automated vibrating sample magnetometer VSM has been constructed. • The VSM records the magnetic hysteresis loop up to 8.3 KG at room temperature. • The VSM has been calibrated and tested by using some measured ferrite samples. • Our VSM lab-built new design proved success and reliability

Construction and calibration of a low cost and fully automated vibrating sample magnetometer

Energy Technology Data Exchange (ETDEWEB)

El-Alaily, T.M., E-mail: toson_alaily@yahoo.com [Physics Department, Faculty of Science, Tanta University, Tanta (Egypt); El-Nimr, M.K.; Saafan, S.A.; Kamel, M.M.; Meaz, T.M. [Physics Department, Faculty of Science, Tanta University, Tanta (Egypt); Assar, S.T. [Engineering Physics and Mathematics Department, Faculty of Engineering, Tanta University, Tanta (Egypt)

2015-07-15

A low cost vibrating sample magnetometer (VSM) has been constructed by using an electromagnet and an audio loud speaker; where both are controlled by a data acquisition device. The constructed VSM records the magnetic hysteresis loop up to 8.3 KG at room temperature. The apparatus has been calibrated and tested by using magnetic hysteresis data of some ferrite samples measured by two scientifically calibrated magnetometers; model (Lake Shore 7410) and model (LDJ Electronics Inc. Troy, MI). Our VSM lab-built new design proved success and reliability. - Highlights: • A low cost automated vibrating sample magnetometer VSM has been constructed. • The VSM records the magnetic hysteresis loop up to 8.3 KG at room temperature. • The VSM has been calibrated and tested by using some measured ferrite samples. • Our VSM lab-built new design proved success and reliability.

Automation of scanning technique by gamma radiation

International Nuclear Information System (INIS)

Aamira, Yahya

2011-01-01

The gamma scan technique is a nuclear test allowing the analysis of the internal mechanical properties of distillation columns used in petrochemical industries. Such technique is performed manually. So we propose in this work to automate the gamma scan procedure test by using a PLC. In addition, supervision and data acquisition interfaces are proposed.

Magnetoresistive magnetometer for space science applications

International Nuclear Information System (INIS)

Brown, P; Beek, T; Carr, C; O’Brien, H; Cupido, E; Oddy, T; Horbury, T S

2012-01-01

Measurement of the in situ dc magnetic field on space science missions is most commonly achieved using instruments based on fluxgate sensors. Fluxgates are robust, reliable and have considerable space heritage; however, their mass and volume are not optimized for deployment on nano or picosats. We describe a new magnetometer design demonstrating science measurement capability featuring significantly lower mass, volume and to a lesser extent power than a typical fluxgate. The instrument employs a sensor based on anisotropic magnetoresistance (AMR) achieving a noise floor of less than 50 pT Hz −1/2 above 1 Hz on a 5 V bridge bias. The instrument range is scalable up to ±50 000 nT and the three-axis sensor mass and volume are less than 10 g and 10 cm 3 , respectively. The ability to switch the polarization of the sensor's easy axis and apply magnetic feedback is used to build a driven first harmonic closed loop system featuring improved linearity, gain stability and compensation of the sensor offset. A number of potential geospace applications based on the initial instrument results are discussed including attitude control systems and scientific measurement of waves and structures in the terrestrial magnetosphere. A flight version of the AMR magnetometer will fly on the TRIO-CINEMA mission due to be launched in 2012. (paper)

Column-to-column packing variation of disposable pre-packed columns for protein chromatography.

Science.gov (United States)

Schweiger, Susanne; Hinterberger, Stephan; Jungbauer, Alois

2017-12-08

In the biopharmaceutical industry, pre-packed columns are the standard for process development, but they must be qualified before use in experimental studies to confirm the required performance of the packed bed. Column qualification is commonly done by pulse response experiments and depends highly on the experimental testing conditions. Additionally, the peak analysis method, the variation in the 3D packing structure of the bed, and the measurement precision of the workstation influence the outcome of qualification runs. While a full body of literature on these factors is available for HPLC columns, no comparable studies exist for preparative columns for protein chromatography. We quantified the influence of these parameters for commercially available pre-packed and self-packed columns of disposable and non-disposable design. Pulse response experiments were performed on 105 preparative chromatography columns with volumes of 0.2-20ml. The analyte acetone was studied at six different superficial velocities (30, 60, 100, 150, 250 and 500cm/h). The column-to-column packing variation between disposable pre-packed columns of different diameter-length combinations varied by 10-15%, which was acceptable for the intended use. The column-to-column variation cannot be explained by the packing density, but is interpreted as a difference in particle arrangement in the column. Since it was possible to determine differences in the column-to-column performance, we concluded that the columns were well-packed. The measurement precision of the chromatography workstation was independent of the column volume and was in a range of±0.01ml for the first peak moment and±0.007 ml 2 for the second moment. The measurement precision must be considered for small columns in the range of 2ml or less. The efficiency of disposable pre-packed columns was equal or better than that of self-packed columns. Copyright © 2017 The Author(s). Published by Elsevier B.V. All rights reserved.

Simplified High-Performance Roll Out Composite Magnetometer Boom, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — In response to NASA's need for compact, low-cost deployable magnetometer booms for CubeSats, Roccor proposes to develop a Simple High-performance Roll-Out Composite...

MgB{sub 2} magnetometer with a directly coupled pick-up loop

Energy Technology Data Exchange (ETDEWEB)

Portesi, C [Istituto Elettrotecnico Nazionale Galileo Ferraris, Strada delle Cacce 91, I-10135 Turin (Italy); Mijatovic, D [Low Temperature Division and Mesa Research Institute, University of Twente, PO Box 217, 7500 AE Enschede (Netherlands); Veldhuis, D [Low Temperature Division and Mesa Research Institute, University of Twente, PO Box 217, 7500 AE Enschede (Netherlands); Brinkman, A [Low Temperature Division and Mesa Research Institute, University of Twente, PO Box 217, 7500 AE Enschede (Netherlands); Monticone, E [Istituto Elettrotecnico Nazionale Galileo Ferraris, Strada delle Cacce 91, I-10135 Turin (Italy); Gonnelli, R S [INFM, Dipartimento di Fisica, Politecnico di Torino, Corso Duca degli Abruzzi 24, I-10129 Turin (Italy)

2006-05-15

In this work, we show the results obtained in the fabrication and characterization of an MgB{sub 2} magnetometer with a directly coupled pick-up loop. We used an all in situ technique for fabricating magnesium diboride films, which consists of the co-evaporation of B and Mg by means of an e-gun and a resistive heater respectively. Consequently, we realized the superconducting device, which incorporates two nanobridges as weak links in a superconducting loop. The nanobridges were realized by focused ion beam milling; they were 240 nm wide and had a critical current density of 10{sup 7} A cm{sup -2}. The magnetometer was characterized at different temperatures and also measurements of the noise levels have been performed. The device shows Josephson quantum interference up to 20 K and the calculated effective area at low temperatures was 0.24 mm{sup 2}. The transport properties of the magnetometer allow determining fundamental materials properties of the MgB{sub 2} thin films, such as the penetration depth.

Obtaining 'images' from iron objects using a 3-axis fluxgate magnetometer

Energy Technology Data Exchange (ETDEWEB)

Chilo, Jose [University of Gaevle, S-80176 Gaevle (Sweden); Jabor, Abbas [Royal Institute of Technology, Department of Physics, S-106 91 Stockholm (Sweden); Lizska, Ludwik [Swedish Institute of Space Physics in Umea (Sweden); Eide, Age J. [Ostfold University College, N-1757 Halden (Norway); Lindblad, Thomas [Royal Institute of Technology, Department of Physics, S-106 91 Stockholm (Sweden)], E-mail: lindblad@particle.kth.se

2007-10-01

Magnetic objects can cause local variations in the Earth's magnetic field that can be measured with a magnetometer. Here we used tri-axial magnetometer measurements and an analysis method employing wavelet techniques to determine the 'signature' or 'fingerprint' of different iron objects. Clear distinctions among the iron samples were observed. The time-dependent changes in the frequency powers were extracted by use of the Morlet wavelet corresponding to frequency bands from 0.1 to 100 Hz.

Intense auroral field-aligned currents and electrojets detected by rocket-borne fluxgate magnetometer

International Nuclear Information System (INIS)

Tohyama, Fumio; Fukunishi, Hiroshi; Takahashi, Takao; Kokubun, Susumu; Fujii, Ryoichi; Yamagishi, Hisao.

1988-01-01

The S-310JA-11 and S-310JA-12 rockets, having a vector magnetometer with high sensitivity (1.8 nT) and high sampling frequency (100 Hz), were launched into the aurora on May 29 and July 12, 1985, from Syowa Station, Antarctica. The S-310JA-11 rocket penetrated twice quiet arcs, while the S-310JA-12 rocket traversed across intense and active auroral arcs during a large magnetic substorm. In the S-310JA-12 rocket experiment, intense field-aligned currents of 400 - 600 nT were observed when the rocket penetrated an active arc during the descending flight. The magnetometer on board the S-310JA-12 rocket also detected intense electrojet currents with a center at 110 km on the upward leg and at 108 km on the downward leg. The magnetometer data of the S-310JA-11 rocket showed no distinguished magnetic field variation due to field-aligned current and electrojet. (author)

Characterization and demonstration results of a SQUID magnetometer system developed for geomagnetic field measurements

Science.gov (United States)

Kawai, J.; Miyamoto, M.; Kawabata, M.; Nosé, M.; Haruta, Y.; Uehara, G.

2017-08-01

We characterized a low temperature superconducting quantum interference device (SQUID) magnetometer system developed for high-sensitivity geomagnetic field measurement, and demonstrated the detection of weak geomagnetic signals. The SQUID magnetometer system is comprised of three-axis SQUID magnetometers housed in a glass fiber reinforced plastic cryostat, readout electronics with flux locked loop (FLL), a 24-bit data logger with a global positioning system and batteries. The system noise was approximately 0.2 pT √Hz- 1/2 in the 1-50 Hz frequency range. This performance was determined by including the thermal noise and the shielding effect of the copper shield, which covered the SQUID magnetometers to eliminate high-frequency interference. The temperature drift of the system was ˜0.8 pT °C- 1 in an FLL operation. The system operated for a month using 33 l liquid helium. Using this system, we performed the measurements of geomagnetic field in the open-air, far away from the city. The system could detect weak geomagnetic signals such as the Schumann resonance with sixth harmonics, and the ionospheric Alfvén resonance appearing at night, for the north-south and east-west components of the geomagnetic field. We confirm that the system was capable of high-sensitivity measurement of the weak geomagnetic activities.

Probabilistic resident space object detection using archival THEMIS fluxgate magnetometer data

Science.gov (United States)

Brew, Julian; Holzinger, Marcus J.

2018-05-01

Recent progress in the detection of small space objects, at geosynchronous altitudes, through ground-based optical and radar measurements is demonstrated as a viable method. However, in general, these methods are limited to detection of objects greater than 10 cm. This paper examines the use of magnetometers to detect plausible flyby encounters with charged space objects using a matched filter signal existence binary hypothesis test approach. Relevant data-set processing and reduction of archival fluxgate magnetometer data from the NASA THEMIS mission is discussed in detail. Using the proposed methodology and a false alarm rate of 10%, 285 plausible detections with probability of detection greater than 80% are claimed and several are reviewed in detail.

Measuring In-Flight Angular Motion With a Low-Cost Magnetometer

National Research Council Canada - National Science Library

Harkins, Thomas E; Wilson, Michael J

2007-01-01

A technique for obtaining pitch, yaw, and roll rates of a projectile from a single, low-cost, commercial off-the-shelf magnetometer has been developed at the Advanced Munitions Concepts Branch of the U.S...

Construction and calibration of a low cost and fully automated vibrating sample magnetometer

Science.gov (United States)

El-Alaily, T. M.; El-Nimr, M. K.; Saafan, S. A.; Kamel, M. M.; Meaz, T. M.; Assar, S. T.

2015-07-01

A low cost vibrating sample magnetometer (VSM) has been constructed by using an electromagnet and an audio loud speaker; where both are controlled by a data acquisition device. The constructed VSM records the magnetic hysteresis loop up to 8.3 KG at room temperature. The apparatus has been calibrated and tested by using magnetic hysteresis data of some ferrite samples measured by two scientifically calibrated magnetometers; model (Lake Shore 7410) and model (LDJ Electronics Inc. Troy, MI). Our VSM lab-built new design proved success and reliability.

Membrane-based torque magnetometer: Enhanced sensitivity by optical readout of the membrane displacement

Science.gov (United States)

Blankenhorn, M.; Heintze, E.; Slota, M.; van Slageren, J.; Moores, B. A.; Degen, C. L.; Bogani, L.; Dressel, M.

2017-09-01

The design and realization of a torque magnetometer is reported that reads the deflection of a membrane by optical interferometry. The compact instrument allows for low-temperature measurements of tiny crystals less than a microgram with a significant improvement in sensitivity, signal-to-noise ratio as well as data acquisition time compared with conventional magnetometry and offers an enormous potential for further improvements and future applications in different fields. Magnetic measurements on single-molecule magnets demonstrate the applicability of the membrane-based torque magnetometer.

An expert system for improving the gamma-ray scanning technique

International Nuclear Information System (INIS)

Laraki, K.; Alami, R.; Cherkaoui El Moursli, R.; Bensitel, A.; El Badri, L.

2007-01-01

The gamma-ray scanning technique is widely used in the diagnosis and identification of industrial installations, in general and, in particular, of distillation columns considered as the most critical components in petrochemical plants. It provides essential data to optimise the performance of columns and identify maintenance requirements. Due to the various difficulties that can arise while analysing a scanning profile and in order to benefit from the continuous advent of new technologies in the field of electronics and data processing, the team of the Division of Instrumentation and Industrial Applications of CNESTEN have conducted a project aiming the elaboration of an expert system for acquisition, processing and interpretation of the scanning results. This system consists of two main modules: the first one is devoted to the preparation and control of the scanning operation conditions, while the second module has been developed to carry out easily and effectively the automatic (on-line) analysis and interpretation of the scan profiles

Attitude Determination with Magnetometers and Accelerometers to Use in Satellite Simulator

Directory of Open Access Journals (Sweden)

Helio Koiti Kuga

2013-01-01

Full Text Available Attitude control of artificial satellites is dependent on information provided by its attitude determination process. This paper presents the implementation and tests of a fully self-contained algorithm for the attitude determination using magnetometers and accelerometers, for application on a satellite simulator based on frictionless air bearing tables. However, it is known that magnetometers and accelerometers need to be calibrated so as to allow that measurements are used to their ultimate accuracy. A calibration method is implemented which proves to be essential for improving attitude determination accuracy. For the stepwise real-time attitude determination, it was used the well-known QUEST algorithm which yields quick response with reduced computer resources. The algorithms are tested and qualified with actual data collected on the streets under controlled situations. For such street runaways, the experiment employs a solid-state magnetoresistive magnetometer and an IMU navigation block consisting of triads of accelerometers and gyros, with MEMS technology. A GPS receiver is used to record positional information. The collected measurements are processed through the developed algorithms, and comparisons are made for attitude determination using calibrated and noncalibrated data. The results show that the attitude accuracy reaches the requirements for real-time operation for satellite simulator platforms.

Digital Fluxgate Magnetometer for Detection of Microvibration

Directory of Open Access Journals (Sweden)

Menghui Zhi

2017-01-01

Full Text Available In engineering practice, instruments, such as accelerometer and laser interferometer, are widely used in vibration measurement of structural parts. A method for using a triaxial fluxgate magnetometer as a microvibration sensor to measure low-frequency pendulum microvibration (not translational vibration is proposed in this paper, so as to detect vibration from low-frequency vibration sources, such as large rotating machine, large engineering structure, earthquake, and microtremor. This method provides vibration detection based on the environmental magnetic field signal to avoid increased measurement difficulty and error due to different relative positions of permanent magnet and magnetometer on the device under test (DUT when using the original magnetic measurement method. After fixedly connecting the fluxgate probe with the DUT during the test, the angular displacement due to vibration can be deduced by measuring the geomagnetic field’s magnetic induction intensity change on the orthogonal three components during the vibration. The test shows that the microvibration sensor has angular resolution of over 0.05° and maximum measuring frequency of 64 Hz. As an exploring test aimed to detect the microvibration of earth-orbiting satellite in the in-orbit process, the simulation experiment successfully provides the real-time microvibration information for attitude and orbit control subsystem.

Results from the GSFC fluxgate magnetometer on Pioneer 11

Science.gov (United States)

Acuna, M. H.; Ness, N. F.

1976-01-01

A high-field triaxial fluxgate magnetometer was mounted on Pioneer 11 to measure the main magnetic field of Jupiter. It is found that this planetary magnetic field is more complex than that indicated by the results of the Pioneer 10 vector helium magnetometer. At distances less than 3 Jupiter radii, the magnetic field is observed to increase more rapidly than an inverse-cubed distance law associated with any simple dipole model. Contributions from higher-order multipoles are significant, with the quadrupole and octupole being 24 and 21 percent of the dipole moment, respectively. Implications of the results for the study of trapped particles, planetary radio emission, and planetary interiors are discussed. Major conclusions are that the deviation of the main planetary magnetic field from a simple dipole leads to distortion of the L shells of the charged particles and to warping of the magnetic equator. Enhanced absorption effects associated with Amalthea and Io are predicted.

Mapping of Ambient Magnetic Fields within Liquid Helium Dewar for Testing of a DC SQUID Magnetometer

International Nuclear Information System (INIS)

Newhouse, Randal

2003-01-01

In an effort to explore the cavity lights phenomenon, Experimental Facilities Department at SLAC is testing a DC SQUID magnetometer. Due to the nature of the SQUID magnetometer and the intended tests, the earth's magnetic field must be negated. It is proposed to reduce ambient fields using bucking coils. First, however, an accurate map of the magnetic field inside the liquid helium Dewar where the experiment is going to take place needed to be made. This map was made using a three-axis fluxgate magnetometer mounted on a 3D positioning device made for this purpose. A ten inch tall volume within the Dewar was measured at data points approximately an inch from each other in all three axes. A LabVEIW program took readings from the magnetometer at 2 ms intervals for 1000 readings in such a way as to eliminate any ambient 60 Hz signals that may be present in the data. This data was stored in spreadsheet format and was analyzed to determine how the magnetic field within the Dewar was changing as a function of position

A stochastic view on column efficiency.

Science.gov (United States)

Gritti, Fabrice

2018-03-09

A stochastic model of transcolumn eddy dispersion along packed beds was derived. It was based on the calculation of the mean travel time of a single analyte molecule from one radial position to another. The exchange mechanism between two radial positions was governed by the transverse dispersion of the analyte across the column. The radial velocity distribution was obtained by flow simulations in a focused-ion-beam scanning electron microscopy (FIB-SEM) based 3D reconstruction from a 2.1 mm × 50 mm column packed with 2 μm BEH-C 18 particles. Accordingly, the packed bed was divided into three coaxial and uniform zones: (1) a 1.4 particle diameter wide, ordered, and loose packing at the column wall (velocity u w ), (2) an intermediate 130 μm wide, random, and dense packing (velocity u i ), and (3) the bulk packing in the center of the column (velocity u c ). First, the validity of this proposed stochastic model was tested by adjusting the predicted to the observed reduced van Deemter plots of a 2.1 mm × 50 mm column packed with 2 μm BEH-C 18 fully porous particles (FPPs). An excellent agreement was found for u i  = 0.93u c , a result fully consistent with the FIB-SEM observation (u i  = 0.95u c ). Next, the model was used to measure u i  = 0.94u c for 2.1 mm × 100 mm column packed with 1.6 μm Cortecs-C 18 superficially porous particles (SPPs). The relative velocity bias across columns packed with SPPs is then barely smaller than that observed in columns packed with FPPs (+6% versus + 7%). u w =1.8u i is measured for a 75 μm × 1 m capillary column packed with 2 μm BEH-C 18 particles. Despite this large wall-to-center velocity bias (+80%), the presence of the thin and ordered wall packing layer has no negative impact on the kinetic performance of capillary columns. Finally, the stochastic model of long-range eddy dispersion explains why analytical (2.1-4.6 mm i.d.) and capillary (columns can all be

Small fluxgate magnetometers: development and future trends in Spain.

Science.gov (United States)

Ciudad, David; Díaz-Michelena, Marina; Pérez, Lucas; Aroca, Claudio

2010-01-01

In this paper, we give an overview of the research on fluxgate magnetometers carried out in Spain. In particular we focus in the development of the planar-type instruments. We summarize the fabrication processes and signal processing developments as well as their use in complex systems and space.

Small Fluxgate Magnetometers: Development and Future Trends in Spain

OpenAIRE

Lucas Pérez; Claudio Aroca; Marina Díaz-Michelena; David Ciudad

2010-01-01

In this paper, we give an overview of the research on fluxgate magnetometers carried out in Spain. In particular we focus in the development of the planar-type instruments. We summarize the fabrication processes and signal processing developments as well as their use in complex systems and space.

Corrosion measurement using flux gate magnetometer

International Nuclear Information System (INIS)

Rashdi Shah Ahmad; Chong Cheong Wei

2001-01-01

The ability of fluxgate magnetometer to detect and measure quantitatively the magnetic field generated by electrochemical corrosion is presented. In this study, each sample (iron plate) was exposed to a range of increasingly corrosive environment. During the exposure, we measured the magnetic field above the sample for specific duration of time. The result shows that there is a clear relationship between corrosivity of the environment and the change in magnitude of magnetic field that was generated by the corrosion reaction. Therefore, the measurement of magnetic field might be used to determine the corrosion rates. (Author)

Small Fluxgate Magnetometers: Development and Future Trends in Spain

Science.gov (United States)

Ciudad, David; Díaz-Michelena, Marina; Pérez, Lucas; Aroca, Claudio

2010-01-01

In this paper, we give an overview of the research on fluxgate magnetometers carried out in Spain. In particular we focus in the development of the planar-type instruments. We summarize the fabrication processes and signal processing developments as well as their use in complex systems and space. PMID:22294904

Small Fluxgate Magnetometers: Development and Future Trends in Spain

Directory of Open Access Journals (Sweden)

Lucas Pérez

2010-03-01

Full Text Available In this paper, we give an overview of the research on fluxgate magnetometers carried out in Spain. In particular we focus in the development of the planar-type instruments. We summarize the fabrication processes and signal processing developments as well as their use in complex systems and space.

Development of a {sup 3}He magnetometer for a neutron electric dipole moment experiment

Energy Technology Data Exchange (ETDEWEB)

Kraft, Andreas; Heil, Werner; Lauer, Thorsten; Neumann, Daniel [Johannes Gutenberg University, Institute of Physics, Mainz (Germany); Koch, Hans-Christian [Johannes Gutenberg University, Institute of Physics, Mainz (Germany); University of Fribourg, Physics Department, Fribourg (Switzerland); Daum, Manfred [Paul Scherrer Institute, Villigen (Switzerland); Pazgalev, Anatoly [Ioffe Institute, St Petersburg (Russian Federation); Sobolev, Yuri [Johannes Gutenberg University, Institute of Nuclear Chemistry, Mainz (Germany); Petersburg Nuclear Physics Institute, Gatchina (Russian Federation); Weis, Antoine [University of Fribourg, Physics Department, Fribourg (Switzerland)

2014-01-01

We have developed a highly sensitive {sup 3}He magnetometer for the accurate measurement of the magnetic field in an experiment searching for an electric dipole moment of the neutron. By measuring the Larmor frequency of nuclear spin polarized {sup 3}He atoms a sensitivity on the femto-Tesla scale can be achieved. A {sup 3}He/Cs-test facility was established at the Institute of Physics of the Johannes Gutenberg University in Mainz to investigate the readout of {sup 3}He free induction decay with a lamp-pumped Cs magnetometer. For this we designed and built an ultra-compact and transportable polarizer unit which polarizes {sup 3}He gas up to 55% by metastability exchange optical pumping. The polarized {sup 3}He was successfully transfered from the polarizer into a glass cell mounted in a magnetic shield and the {sup 3}He free induction decay was detected by a lamp-pumped Cs magnetometer. (orig.)

Ionospheric travelling convection vortices observed by the Greenland magnetometer chain

DEFF Research Database (Denmark)

Kotsiaros, Stavros; Stolle, Claudia; Friis-Christensen, Eigil

2013-01-01

The Greenland magnetometer array continuously provides geomagnetic variometer data since the early eighties. With the polar cusp passing over it almost every day, the array is suitable to detect ionospheric traveling convection vortices (TCVs), which were rst detected by Friis-Christensen et al...

Multi-flux-transformer MRI detection with an atomic magnetometer.

Science.gov (United States)

Savukov, Igor; Karaulanov, Todor

2014-12-01

Recently, anatomical ultra-low field (ULF) MRI has been demonstrated with an atomic magnetometer (AM). A flux-transformer (FT) has been used for decoupling MRI fields and gradients to avoid their negative effects on AM performance. The field of view (FOV) was limited because of the need to compromise between the size of the FT input coil and MRI sensitivity per voxel. Multi-channel acquisition is a well-known solution to increase FOV without significantly reducing sensitivity. In this paper, we demonstrate twofold FOV increase with the use of three FT input coils. We also show that it is possible to use a single atomic magnetometer and single acquisition channel to acquire three independent MRI signals by applying a frequency-encoding gradient along the direction of the detection array span. The approach can be generalized to more channels and can be critical for imaging applications of non-cryogenic ULF MRI where FOV needs to be large, including head, hand, spine, and whole-body imaging. Copyright © 2014 Elsevier Inc. All rights reserved.

Magnetometer-inferred, Equatorial, Daytime Vertical ExB Drift Velocities Observed in the African Longitude Sector

Science.gov (United States)

Anderson, D. N.; Yizengaw, E.

2011-12-01

A recent paper has investigated the sharp longitude gradients in the dayside ExB drift velocities associated with the 4-cell, non-migrating structures thought to be connected with the eastward propagating, diurnal, non-migrating (DE3) tides. Observations of vertical ExB drift velocities obtained from the Ion Velocity Meter (IVM) on the Communication/Navigation Outage Forecast System (C/NOFS) satellite were obtained in the Western Pacific, Eastern Pacific, Peruvian and Atlantic sectors for a few days during the months of October, March and December, 2009. Respective ExB drift velocity gradients at the cell boundaries for these 4 longitude sectors were a.) -1.3m/sec/degree, b.) 3m/sec/degree, c.) -4m/sec/degree and d.) 1m/sec/degree and were observed on a day-to-day basis. In this talk, we estimate the longitude gradients in the dayside, vertical ExB drift velocities from magnetometer H-component observations in the African sector. We briefly describe the technique for obtaining realistic ExB drift velocities associated with the difference in the H-component values between a magnetometer on the magnetic equator and one off the magnetic equator at 6 to 9 degrees dip latitude (delta H). We present magnetometer-inferred, dayside ExB drift velocities obtained from the AMBER (African Meridian B-field Education and Research) magnetometer chain in the East Africa (Ethiopian) longitude sector and the West African (Nigerian) longitude sector. We compare the longitude gradients in ExB drift velocities in the African sector with the C/NOFS- observed longitude gradients mentioned above. We also discuss the advantages of using ground-based magnetometer observations to infer ExB drift velocities compared with the C/NOFS satellite observations.

Observations of interplanetary dust by the Juno magnetometer investigation

DEFF Research Database (Denmark)

Benn, Mathias; Jørgensen, John Leif; Denver, Troelz

2017-01-01

One of the Juno magnetometer investigation's star cameras was configured to search for unidentified objects during Juno's transit en route to Jupiter. This camera detects and registers luminous objects to magnitude 8. Objects persisting in more than five consecutive images and moving with an appa...... on the distribution and motion of interplanetary (>μm sized) dust....

The QuakeFinder Magnetometer Network - a Platform for Earth and Space Science Research

Science.gov (United States)

Bleier, T.; Kappler, K. N.; Schneider, D.

2016-12-01

QuakeFinder (QF) is a humanitarian research and development project attempting to characterize earth-emitting electromagnetic (EM) signals as potential precursors to earthquakes. Beginning in 2005, QF designed, built, deployed and now maintains an array of 165 remote monitoring stations in 6 countries (US/California, Taiwan, Greece, Indonesia, Peru and Chile). Having amassed approximately 70 TB of data and greater than 140 earthquakes (M4+), QF is focused on the data analysis and signal processing algorithms in our effort to enable a forecasting capability. QF's autonomous stations, located along major fault lines, collect and transmit electromagnetic readings from 3-axis induction magnetometers and positive/negative ion sensors, a geophone, as well as various station health status and local conditions. The induction magnetometers, oriented N-S,E-W and vertically, have a 40 nT range and 1 pT sensitivity. Data is continuously collected at 50 samples/sec (sps), GPS time-stamped and transmitted, primarily through cell phone networks, to our data center in Palo Alto, California. The induction magnetometers routinely detect subtle geomagnetic and ionospheric disturbances as observed worldwide. QF seeks to make available both historic data and the array platform to strategic partners in the EM-related research and operation fields. The QF system will be described in detail with examples of local and regional geomagnetic activity. The stations are robust and will be undergoing a system-level upgrade in the near future. Domestically, QF maintains a 98% `up time' among the 120 stations in California while internationally our metric is typically near 80%. Irregular cell phone reception is chief among the reasons for outages although little data has been lost as the stations can store up to 90 days of data. These data are retrieved by QF personnel or, when communication is reestablished, the QF data ingest process automatically updates the database. Planned station upgrades

Identification of Mobile Phones Using the Built-In Magnetometers Stimulated by Motion Patterns

Directory of Open Access Journals (Sweden)

Gianmarco Baldini

2017-04-01

Full Text Available We investigate the identification of mobile phones through their built-in magnetometers. These electronic components have started to be widely deployed in mass market phones in recent years, and they can be exploited to uniquely identify mobile phones due their physical differences, which appear in the digital output generated by them. This is similar to approaches reported in the literature for other components of the mobile phone, including the digital camera, the microphones or their RF transmission components. In this paper, the identification is performed through an inexpensive device made up of a platform that rotates the mobile phone under test and a fixed magnet positioned on the edge of the rotating platform. When the mobile phone passes in front of the fixed magnet, the built-in magnetometer is stimulated, and its digital output is recorded and analyzed. For each mobile phone, the experiment is repeated over six different days to ensure consistency in the results. A total of 10 phones of different brands and models or of the same model were used in our experiment. The digital output from the magnetometers is synchronized and correlated, and statistical features are extracted to generate a fingerprint of the built-in magnetometer and, consequently, of the mobile phone. A SVM machine learning algorithm is used to classify the mobile phones on the basis of the extracted statistical features. Our results show that inter-model classification (i.e., different models and brands classification is possible with great accuracy, but intra-model (i.e., phones with different serial numbers and same model classification is more challenging, the resulting accuracy being just slightly above random choice.

Exhaust properties of centre-column-limited plasmas on MAST

International Nuclear Information System (INIS)

Maddison, G.P.; Akers, R.J.; Brickley, C.; Gryaznevich, M.P.; Lott, F.C.; Patel, A.; Sykes, A.; Turner, A.; Valovic, M.

2007-01-01

The lowest aspect ratio possible in a spherical tokamak is defined by limiting the plasma on its centre column, which might therefore maximize many physics benefits of this fusion approach. A key issue for such discharges is whether loads exhausted onto the small surface area of the column remain acceptable. A first series of centre-column-limited pulses has been examined on MAST using fast infra-red thermography to infer incident power densities as neutral-beam heating was scanned from 0 to 2.5 MW. Simple mapping shows that efflux distributions on the column armour are governed mostly by magnetic geometry, which moreover spreads them advantageously over almost the whole vertical length. Hence steady peak power densities between sawteeth remained low, -2 , comparable with the target strike-point value in a reference diverted plasma at lower power. Plasma purity and normalized thermal energy confinement through the centre-column-limited (CCL) series were also similar to properties of MAST diverted cases. A major bonus of CCL geometry is a propensity for exhaust to penetrate through its inner scrape-off layer connecting to the column into an expanding outer plume, which forms a 'natural divertor'. Effectiveness of this process may even increase with plasma heating, owing to rising Shafranov shift and/or toroidal rotation. A larger CCL device could potentially offer a simpler, more economic next-step design

The fluxgate magnetometer of the BepiColombo Mercury Planetary Orbiter

Science.gov (United States)

Glassmeier, K.-H.; Auster, H.-U.; Heyner, D.; Okrafka, K.; Carr, C.; Berghofer, G.; Anderson, B. J.; Balogh, A.; Baumjohann, W.; Cargill, P.; Christensen, U.; Delva, M.; Dougherty, M.; Fornaçon, K.-H.; Horbury, T. S.; Lucek, E. A.; Magnes, W.; Mandea, M.; Matsuoka, A.; Matsushima, M.; Motschmann, U.; Nakamura, R.; Narita, Y.; O'Brien, H.; Richter, I.; Schwingenschuh, K.; Shibuya, H.; Slavin, J. A.; Sotin, C.; Stoll, B.; Tsunakawa, H.; Vennerstrom, S.; Vogt, J.; Zhang, T.

2010-01-01

The magnetometer (MAG) on the Mercury Planetary Orbiter (MPO) of the joint European-Japanese BepiColombo mission to planet Mercury is a low-noise, tri-axial, dual-sensor, digital fluxgate instrument with its sensors mounted on a 2.8-m-long boom. The primary MPO/MAG science objectives are to determine the spatial and temporal structure of the magnetic field in the Hermean system, in particular the structure and origin of the intrinsic magnetic field of Mercury. MPO/MAG has a dynamic measurement range of ±2000nT with a resolution of 2 pT during operation along the near-polar orbit of the MPO spacecraft around Mercury. MPO/MAG is designed to provide measurements with rates between 0.5 and 128 vectors/s. In cooperation with its sister magnetometer instrument, MMO/MGF on board the BepiColombo Mercury Magnetospheric Orbiter (MMO), MPO/MAG will be able to distinguish between temporal and spatial magnetic field variations in the magnetically closely coupled Hermean system.

Space Weather Magnetometer Set with Automated AC Spacecraft Field Correction for GEO-KOMPSAT-2A

Science.gov (United States)

Auster, U.; Magnes, W.; Delva, M.; Valavanoglou, A.; Leitner, S.; Hillenmaier, O.; Strauch, C.; Brown, P.; Whiteside, B.; Bendyk, M.; Hilgers, A.; Kraft, S.; Luntama, J. P.; Seon, J.

2016-05-01

Monitoring the solar wind conditions, in particular its magnetic field (interplanetary magnetic field) ahead of the Earth is essential in performing accurate and reliable space weather forecasting. The magnetic condition of the spacecraft itself is a key parameter for the successful performance of the magnetometer onboard. In practice a condition with negligible magnetic field of the spacecraft cannot always be fulfilled and magnetic sources on the spacecraft interfere with the natural magnetic field measured by the space magnetometer. The presented "ready-to-use" Service Oriented Spacecraft Magnetometer (SOSMAG) is developed for use on any satellite implemented without magnetic cleanliness programme. It enables detection of the spacecraft field AC variations on a proper time scale suitable to distinguish the magnetic field variations relevant to space weather phenomena, such as sudden increase in the interplanetary field or southward turning. This is achieved through the use of dual fluxgate magnetometers on a short boom (1m) and two additional AMR sensors on the spacecraft body, which monitor potential AC disturbers. The measurements of the latter sensors enable an automated correction of the AC signal contributions from the spacecraft in the final magnetic vector. After successful development and test of the EQM prototype, a flight model (FM) is being built for the Korean satellite Geo-Kompsat 2A, with launch foreseen in 2018.

The polarization and the fundamental sensitivity of 39K (133Cs)-85Rb-4He hybrid optical pumping spin exchange relaxation free atomic magnetometers.

Science.gov (United States)

Liu, Jian-Hua; Jing, Dong-Yang; Wang, Liang-Liang; Li, Yang; Quan, Wei; Fang, Jian-Cheng; Liu, Wu-Ming

2017-07-28

The hybrid optical pumping spin exchange relaxation free (SERF) atomic magnetometers can realize ultrahigh sensitivity measurement of magnetic field and inertia. We have studied the 85 Rb polarization of two types of hybrid optical pumping SERF magnetometers based on 39 K- 85 Rb- 4 He and 133 Cs- 85 Rb- 4 He respectively. Then we found that 85 Rb polarization varies with the number density of buffer gas 4 He and quench gas N 2 , pumping rate of pump beam and cell temperature respectively, which will provide an experimental guide for the design of the magnetometer. We obtain a general formula on the fundamental sensitivity of the hybrid optical pumping SERF magnetometer due to shot-noise. The formula describes that the fundamental sensitivity of the magnetometer varies with the number density of buffer gas and quench gas, the pumping rate of pump beam, external magnetic field, cell effective radius, measurement volume, cell temperature and measurement time. We obtain a highest fundamental sensitivity of 1.5073 aT/Hz 1/2 (1 aT = 10 -18 T) with 39 K- 85 Rb- 4 He magnetometer between above two types of magnetometers when 85 Rb polarization is 0.1116. We estimate the fundamental sensitivity limit of the hybrid optical pumping SERF magnetometer to be superior to 1.8359 × 10 -2 aT/Hz 1/2 , which is higher than the shot-noise-limited sensitivity of 1 aT/Hz 1/2 of K SERF atomic magnetometer.

Vector magnetometer design study: Analysis of a triaxial fluxgate sensor design demonstrates that all MAGSAT Vector Magnetometer specifications can be met

Science.gov (United States)

Adams, D. F.; Hartmann, U. G.; Lazarow, L. L.; Maloy, J. O.; Mohler, G. W.

1976-01-01

The design of the vector magnetometer selected for analysis is capable of exceeding the required accuracy of 5 gamma per vector field component. The principal elements that assure this performance level are very low power dissipation triaxial feedback coils surrounding ring core flux-gates and temperature control of the critical components of two-loop feedback electronics. An analysis of the calibration problem points to the need for improved test facilities.

Automated system for the calibration of magnetometers

DEFF Research Database (Denmark)

Petrucha, Vojtech; Kaspar, Petr; Ripka, Pavel

2009-01-01

A completely nonmagnetic calibration platform has been developed and constructed at DTU Space (Technical University of Denmark). It is intended for on-site scalar calibration of high-precise fluxgate magnetometers. An enhanced version of the same platform is being built at the Czech Technical Uni...... through custom-made optical incremental sensors. The system is controlled by a microcontroller, which executes commands from a computer. The properties of the system as well as calibration and measurement results will be presented. ©2009 American Institute of Physics...

Rad-Hard Sigma-Delta 3-Channel ADC for Fluxgate Magnetometers, Phase II

Data.gov (United States)

National Aeronautics and Space Administration — The measurement of the magnetic field vector is of fundamental importance to space physics missions. The fluxgate magnetometer is a device developed for precise...

Rad-Hard Sigma-Delta 3-channel ADC for Fluxgate Magnetometers, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — The proposed project aims to develop a multi-channel analog to digital converter (ADC) required for a fluxgate magnetometer (EPD) employed on NASA's planetary...

Scanning Hall probe microscopy of a diluted magnetic semiconductor

International Nuclear Information System (INIS)

Kweon, Seongsoo; Samarth, Nitin; Lozanne, Alex de

2009-01-01

We have measured the micromagnetic properties of a diluted magnetic semiconductor as a function of temperature and applied field with a scanning Hall probe microscope built in our laboratory. The design philosophy for this microscope and some details are described. The samples analyzed in this work are Ga 0.94 Mn 0.06 As films grown by molecular beam epitaxy. We find that the magnetic domains are 2-4 μm wide and fairly stable with temperature. Magnetic clusters are observed above T C , which we ascribe to MnAs defects too small and sparse to be detected by a superconducting quantum interference device magnetometer.

Scanning Hall probe microscopy of a diluted magnetic semiconductor

Science.gov (United States)

Kweon, Seongsoo; Samarth, Nitin; de Lozanne, Alex

2009-05-01

We have measured the micromagnetic properties of a diluted magnetic semiconductor as a function of temperature and applied field with a scanning Hall probe microscope built in our laboratory. The design philosophy for this microscope and some details are described. The samples analyzed in this work are Ga0.94Mn0.06As films grown by molecular beam epitaxy. We find that the magnetic domains are 2-4 μm wide and fairly stable with temperature. Magnetic clusters are observed above TC, which we ascribe to MnAs defects too small and sparse to be detected by a superconducting quantum interference device magnetometer.

MgB2 magnetometer with directly coupled pick-up loop

NARCIS (Netherlands)

Portesi, C.; Mijatovic, D.; Veldhuis, Dick; Brinkman, Alexander; Monticone, E.; Gonnelli, R.S.

2006-01-01

magnetometer with a directly coupled pick-up loop. We used an all in situ technique for fabricating magnesium diboride films, which consists of the co-evaporation of B and Mg by means of an e-gun and a resistive heater respectively. Consequently, we realized the superconducting device, which

A scanning bi-static SODAR

Energy Technology Data Exchange (ETDEWEB)

Behrens, P; Bradley, S [Physics Department, Auckland University, 38 Princes Street, Auckland (New Zealand); Hunerbein, S von [Acoustics Department, Newton Building, University of Salford, Greater Manchester M5 4WT (United Kingdom)

2008-05-01

Field results are given from a bi-static SODAR which uses a single central vertical transmission and three distributed microphone array receivers. Fourier transform delay methods are applied to data sampled from each microphone to retrospectively scan in angle and follow the transmitted pulse. Advantages of sampling a narrow atmospheric column, rather than distributed volumes are discussed.

A scanning bi-static SODAR

International Nuclear Information System (INIS)

Behrens, P; Bradley, S; Hunerbein, S von

2008-01-01

Field results are given from a bi-static SODAR which uses a single central vertical transmission and three distributed microphone array receivers. Fourier transform delay methods are applied to data sampled from each microphone to retrospectively scan in angle and follow the transmitted pulse. Advantages of sampling a narrow atmospheric column, rather than distributed volumes are discussed

Effect of second harmonic in pulse-width-modulation-based DAC for feedback of digital fluxgate magnetometer

Science.gov (United States)

Belyayev, Serhiy; Ivchenko, Nickolay

2018-04-01

Digital fluxgate magnetometers employ processing of the measured pickup signal to produce the value of the compensation current. Using pulse-width modulation with filtering for digital to analog conversion is a convenient approach, but it can introduce an intrinsic source of nonlinearity, which we discuss in this design note. A code shift of one least significant bit changes the second harmonic content of the pulse train, which feeds into the pick-up signal chain despite the heavy filtering. This effect produces a code-dependent nonlinearity. This nonlinearity can be overcome by the specific design of the timing of the pulse train signal. The second harmonic is suppressed if the first and third quarters of the excitation period pulse train are repeated in the second and fourth quarters. We demonstrate this principle on a digital magnetometer, achieving a magnetometer noise level corresponding to that of the sensor itself.

Micromechanical ``Trampoline'' Magnetometers for Use in Pulsed Magnetic Fields Exceeding 60 Tesla

Science.gov (United States)

Balakirev, F. F.; Boebinger, G. S.; Aksyuk, V.; Gammel, P. L.; Haddon, R. C.; Bishop, D. J.

1998-03-01

We present the design, construction, and operation of a novel magnetometer for use in intense pulsed magnetic fields. The magnetometer consists of a silicon micromachined "trampoline" to which the sample is attached. The small size of the device (typically 400 microns on a side) gives a fast mechanical response (10,000 to 50,000 Hz) and extremely high sensitivity (10-11 Am^2, corresponding to 10-13 Am^2/Hz^(1/2)). The device is robust against electrical and mechanical noise and requires no special vibration isolation from the pulsed magnet. As a demonstration, we present data taken in a 60 tesla pulsed magnetic field which show clear de Haas-van Alphen oscillations in a one microgram sample of the organic superconductor K-(BEDT-TTF)_2Cu(NCS)_2.

Atomic column resolved electron energy-loss spectroscopy

International Nuclear Information System (INIS)

Duscher, G.; Pennycook, S.J.; Browning, N.D.

1998-01-01

Spatially resolved electron energy-loss spectroscopy (EELS) is rapidly developing into a unique and powerful tool to characterize internal interfaces. Because atomic column resolved Z-contrast imaging can be performed simultaneously with EELS in the scanning transmission electron microscope, this combination allows the atomic structure to be correlated with the electronic structure, and thus the local properties of interfaces or defects can be determined directly. However, the ability to characterize interfaces and defects at that level requires not only high spatial resolution but also the exact knowledge of the beam location, from where the spectrum is obtained. Here we discuss several examples progressing from cases where the limitation in spatial resolution is given by the microscopes or the nature of the sample, to one example of impurity atoms at a grain boundary, which show intensity and fine structure changes from atomic column to atomic column. Such data can be interpreted as changes in valence of the impurity, depending on its exact site in the boundary plane. Analysis ofthis nature is a valuable first step in understanding the microscopic structural, optical and electronic properties of materials. (orig.)

Temperature-dependent performance of all-NbN DC-SQUID magnetometers

Science.gov (United States)

Liu, Quansheng; Wang, Huiwu; Zhang, Qiyu; Wang, Hai; Peng, Wei; Wang, Zhen

2017-05-01

Integrated NbN direct current superconducting quantum interference device (DC-SQUID) magnetometers were developed based on high-quality epitaxial NbN/AlN/NbN Josephson junctions for SQUID applications operating at high temperatures. We report the current-voltage and voltage-flux characteristics and the noise performance of the NbN DC-SQUIDs for temperatures ranging from 4.2 to 9 K. The critical current and voltage swing of the DC-SQUIDs decreased by 15% and 25%, respectively, as the temperature was increased from 4.2 to 9 K. The white flux noise of the DC-SQUID magnetometer at 1 kHz increased from 3.9 μΦ0/Hz1/2 at 4.2 K to 4.8 μΦ0/Hz1/2 at 9 K with 23% increase, corresponding to the magnetic field noise of 6.6 and 8.1 fT/Hz1/2, respectively. The results show that NbN DC-SQUIDs improve the tolerance of the operating temperatures and temperature fluctuations in SQUID applications.

New vector/scalar Overhauser DNP magnetometers POS-4 for magnetic observatories and directional oil drilling support

Directory of Open Access Journals (Sweden)

Sapunov V.A., Denisov A.Y., Saveliev D.V., Soloviev A.A., Khomutov S.Y., Borodin P.B., Narkhov E.D., Sergeev A.V., Shirokov A.N.

2016-12-01

Full Text Available This paper covers same results of the research directed at developing an absolute vector proton magnetometer POS-4 based on the switching bias magnetic fields methods. Due to the high absolute precision and stability magnetometer POS-4 found application not only for observatories and to directional drilling support of oi and gas well. Also we discuss the some basic errors of measurements and discuss the long-term experience in the testing of magnetic observatories ART and PARATUNKA.

The MAGIC of CINEMA: first in-flight science results from a miniaturised anisotropic magnetoresistive magnetometer

Science.gov (United States)

Archer, M. O.; Horbury, T. S.; Brown, P.; Eastwood, J. P.; Oddy, T. M.; Whiteside, B. J.; Sample, J. G.

2015-06-01

We present the first in-flight results from a novel miniaturised anisotropic magnetoresistive space magnetometer, MAGIC (MAGnetometer from Imperial College), aboard the first CINEMA (CubeSat for Ions, Neutrals, Electrons and MAgnetic fields) spacecraft in low Earth orbit. An attitude-independent calibration technique is detailed using the International Geomagnetic Reference Field (IGRF), which is temperature dependent in the case of the outboard sensor. We show that the sensors accurately measure the expected absolute field to within 2% in attitude mode and 1% in science mode. Using a simple method we are able to estimate the spacecraft's attitude using the magnetometer only, thus characterising CINEMA's spin, precession and nutation. Finally, we show that the outboard sensor is capable of detecting transient physical signals with amplitudes of ~ 20-60 nT. These include field-aligned currents at the auroral oval, qualitatively similar to previous observations, which agree in location with measurements from the DMSP (Defense Meteorological Satellite Program) and POES (Polar-orbiting Operational Environmental Satellites) spacecraft. Thus, we demonstrate and discuss the potential science capabilities of the MAGIC instrument onboard a CubeSat platform.

Suppression of the Nonlinear Zeeman Effect and Heading Error in Earth-Field-Range Alkali-Vapor Magnetometers.

Science.gov (United States)

Bao, Guzhi; Wickenbrock, Arne; Rochester, Simon; Zhang, Weiping; Budker, Dmitry

2018-01-19

The nonlinear Zeeman effect can induce splitting and asymmetries of magnetic-resonance lines in the geophysical magnetic-field range. This is a major source of "heading error" for scalar atomic magnetometers. We demonstrate a method to suppress the nonlinear Zeeman effect and heading error based on spin locking. In an all-optical synchronously pumped magnetometer with separate pump and probe beams, we apply a radio-frequency field which is in phase with the precessing magnetization. This results in the collapse of the multicomponent asymmetric magnetic-resonance line with ∼100  Hz width in the Earth-field range into a single peak with a width of 22 Hz, whose position is largely independent of the orientation of the sensor within a range of orientation angles. The technique is expected to be broadly applicable in practical magnetometry, potentially boosting the sensitivity and accuracy of Earth-surveying magnetometers by increasing the magnetic-resonance amplitude, decreasing its width, and removing the important and limiting heading-error systematic.

Suppression of the Nonlinear Zeeman Effect and Heading Error in Earth-Field-Range Alkali-Vapor Magnetometers

Science.gov (United States)

Bao, Guzhi; Wickenbrock, Arne; Rochester, Simon; Zhang, Weiping; Budker, Dmitry

2018-01-01

The nonlinear Zeeman effect can induce splitting and asymmetries of magnetic-resonance lines in the geophysical magnetic-field range. This is a major source of "heading error" for scalar atomic magnetometers. We demonstrate a method to suppress the nonlinear Zeeman effect and heading error based on spin locking. In an all-optical synchronously pumped magnetometer with separate pump and probe beams, we apply a radio-frequency field which is in phase with the precessing magnetization. This results in the collapse of the multicomponent asymmetric magnetic-resonance line with ˜100 Hz width in the Earth-field range into a single peak with a width of 22 Hz, whose position is largely independent of the orientation of the sensor within a range of orientation angles. The technique is expected to be broadly applicable in practical magnetometry, potentially boosting the sensitivity and accuracy of Earth-surveying magnetometers by increasing the magnetic-resonance amplitude, decreasing its width, and removing the important and limiting heading-error systematic.

Fluxgate magnetometer offset vector determination by the 3D mirror mode method

Science.gov (United States)

Plaschke, F.; Goetz, C.; Volwerk, M.; Richter, I.; Frühauff, D.; Narita, Y.; Glassmeier, K.-H.; Dougherty, M. K.

2017-07-01

Fluxgate magnetometers on-board spacecraft need to be regularly calibrated in flight. In low fields, the most important calibration parameters are the three offset vector components, which represent the magnetometer measurements in vanishing ambient magnetic fields. In case of three-axis stabilized spacecraft, a few methods exist to determine offsets: (I) by analysis of Alfvénic fluctuations present in the pristine interplanetary magnetic field, (II) by rolling the spacecraft around at least two axes, (III) by cross-calibration against measurements from electron drift instruments or absolute magnetometers, and (IV) by taking measurements in regions of well-known magnetic fields, e.g. cometary diamagnetic cavities. In this paper, we introduce a fifth option, the 3-dimensional (3D) mirror mode method, by which 3D offset vectors can be determined using magnetic field measurements of highly compressional waves, e.g. mirror modes in the Earth's magnetosheath. We test the method by applying it to magnetic field data measured by the following: the Time History of Events and Macroscale Interactions during Substorms-C spacecraft in the terrestrial magnetosheath, the Cassini spacecraft in the Jovian magnetosheath and the Rosetta spacecraft in the vicinity of comet 67P/Churyumov-Gerasimenko. The tests reveal that the achievable offset accuracies depend on the ambient magnetic field strength (lower strength meaning higher accuracy), on the length of the underlying data interval (more data meaning higher accuracy) and on the stability of the offset that is to be determined.

On-orbit real-time magnetometer bias determination for micro-satellites without attitude information

Directory of Open Access Journals (Sweden)

Zhang Zhen

2015-10-01

Full Text Available Due to the disadvantages such as complex calculation, low accuracy of estimation, and being non real time in present methods, a new real-time algorithm is developed for on-orbit magnetometer bias determination of micro-satellites without attitude knowledge in this paper. This method uses the differential value approach. It avoids the impact of quartic nature and uses the iterative method to satisfy real-time applications. Simulation results indicate that the new real-time algorithm is more accurate compared with other methods, which are also tested by an experiment system using real noise data. With the new real-time algorithm, a magnetometer calibration can be taken on-orbit and will reduce the demand for computing power effectively.

Searching for axion stars and Q-balls with a terrestrial magnetometer network

Energy Technology Data Exchange (ETDEWEB)

Jackson Kimball, D. F. [Cal State, East Bay; Budker, D. [UC, Berkeley; Eby, J. [Fermilab; Pospelov, M. [Perimeter Inst. Theor. Phys.; Pustelny, S. [Jagiellonian U.; Scholtes, T. [Fribourg U.; Stadnik, Y. V. [Helmholtz Inst., Mainz; Weis, A. [Fribourg U.; Wickenbrock, A. [Mainz U.

2017-10-11

Light (pseudo-)scalar fields are promising candidates to be the dark matter in the Universe. Under certain initial conditions in the early Universe and/or with certain types of self-interactions, they can form compact dark-matter objects such as axion stars or Q-balls. Direct encounters with such objects can be searched for by using a global network of atomic magnetometers. It is shown that for a range of masses and radii not ruled out by existing observations, the terrestrial encounter rate with axion stars or Q-balls can be sufficiently high (at least once per year) for a detection. Furthermore, it is shown that a global network of atomic magnetometers is sufficiently sensitive to pseudoscalar couplings to atomic spins so that a transit through an axion star or Q-ball could be detected over a broad range of unexplored parameter space.

Modeling Stone Columns.

Science.gov (United States)

Castro, Jorge

2017-07-11

This paper reviews the main modeling techniques for stone columns, both ordinary stone columns and geosynthetic-encased stone columns. The paper tries to encompass the more recent advances and recommendations in the topic. Regarding the geometrical model, the main options are the "unit cell", longitudinal gravel trenches in plane strain conditions, cylindrical rings of gravel in axial symmetry conditions, equivalent homogeneous soil with improved properties and three-dimensional models, either a full three-dimensional model or just a three-dimensional row or slice of columns. Some guidelines for obtaining these simplified geometrical models are provided and the particular case of groups of columns under footings is also analyzed. For the latter case, there is a column critical length that is around twice the footing width for non-encased columns in a homogeneous soft soil. In the literature, the column critical length is sometimes given as a function of the column length, which leads to some disparities in its value. Here it is shown that the column critical length mainly depends on the footing dimensions. Some other features related with column modeling are also briefly presented, such as the influence of column installation. Finally, some guidance and recommendations are provided on parameter selection for the study of stone columns.

Post column derivatisation analyses review. Is post-column derivatisation incompatible with modern HPLC columns?

Science.gov (United States)

Jones, Andrew; Pravadali-Cekic, Sercan; Dennis, Gary R; Shalliker, R Andrew

2015-08-19

Post Column derivatisation (PCD) coupled with high performance liquid chromatography or ultra-high performance liquid chromatography is a powerful tool in the modern analytical laboratory, or at least it should be. One drawback with PCD techniques is the extra post-column dead volume due to reaction coils used to enable adequate reaction time and the mixing of reagents which causes peak broadening, hence a loss of separation power. This loss of efficiency is counter-productive to modern HPLC technologies, -such as UHPLC. We reviewed 87 PCD methods published from 2009 to 2014. We restricted our review to methods published between 2009 and 2014, because we were interested in the uptake of PCD methods in UHPLC environments. Our review focused on a range of system parameters including: column dimensions, stationary phase and particle size, as well as the geometry of the reaction loop. The most commonly used column in the methods investigated was not in fact a modern UHPLC version with sub-2-micron, (or even sub-3-micron) particles, but rather, work-house columns, such as, 250 × 4.6 mm i.d. columns packed with 5 μm C18 particles. Reaction loops were varied, even within the same type of analysis, but the majority of methods employed loop systems with volumes greater than 500 μL. A second part of this review illustrated briefly the effect of dead volume on column performance. The experiment evaluated the change in resolution and separation efficiency of some weak to moderately retained solutes on a 250 × 4.6 mm i.d. column packed with 5 μm particles. The data showed that reaction loops beyond 100 μL resulted in a very serious loss of performance. Our study concluded that practitioners of PCD methods largely avoid the use of UHPLC-type column formats, so yes, very much, PCD is incompatible with the modern HPLC column. Copyright © 2015. Published by Elsevier B.V.

Venus Lightning: What We Have Learned from the Venus Express Fluxgate Magnetometer

Science.gov (United States)

Russell, C. T.; Strangeway, R. J.; Wei, H. Y.; Zhang, T. L.

2010-03-01

The Venus Express magnetometer sees short (tens of milliseconds) pulses of EM waves in the Venus ionosphere as predicted by the lightning model for the PVO electric pulses. These waves are stronger than similar terrestrial signals produced by lightning.

Studies of Polar Current Systems Using the IMS Scandinavian Magnetometer Array

Science.gov (United States)

Untiedt, J.; Baumjohann, W.

1993-09-01

As a contribution to the International Magnetospheric Study (IMS, 1976 1979) a two-dimensional array of 42 temporary magnetometer stations was run in Scandinavia, supplementary to the permanent observatories and concentrated in the northern part of the region. This effort aimed at the time-dependent (periods above about 100 s) determination of the two-dimensional structure of substorm-related magnetic fields at the Earth's surface with highest reasonable spatial resolution (about 100 km, corresponding to the height of the ionosphere) near the footpoints of field-aligned electric currents that couple the disturbed magnetosphere to the ionosphere at auroral latitudes. It has been of particular advantage for cooperative studies that not only simultaneous data were available from all-sky cameras, riometers, balloons, rockets, and satellites, but also from the STARE radar facility yielding colocated two-dimensional ionospheric electric field distributions. In many cases it therefore was possible to infer the three-dimensional regional structure of substorm-related ionospheric current systems. The first part of this review outlines the basic relationships and methods that have been used or have been developed for such studies. The second short part presents typical equivalent current patterns observed by the magnetometer array in the course of substorms. Finally we review main results of studies that have been based on the magnetometer array observations and on additional data, omitting studies on geomagnetic pulsations. These studies contributed to a clarification of the nature of auroral electrojets including the Harang discontinuity and of ionospheric current systems related to auroral features such as the break-up at midnight, the westward traveling surge, eastward drifting omega bands, and spirals.

Exploiting nonlinear dynamics in a coupled-core fluxgate magnetometer

International Nuclear Information System (INIS)

Bulsara, Adi R; In, Visarath; Kho, Andy; Longhini, Patrick; Neff, Joe; Anderson, Gregory; Obra, Christopher; Palacios, Antonio; Baglio, Salvatore; Ando, Bruno

2008-01-01

Unforced bistable dynamical systems having dynamics of the general form τ F x-dot (t)=-∇ x U(x) cannot oscillate (i.e. switch between their stable attractors). However, a number of such systems subject to carefully crafted coupling schemes have been shown to exhibit oscillatory behavior under carefully chosen operating conditions. This behavior, in turn, affords a new mechanism for the detection and quantification of target signals having magnitude far smaller than the energy barrier height in the potential energy function U(x) for a single (uncoupled) element. The coupling-induced oscillations are a feature that appears to be universal in systems described by bi- or multi-stable potential energy functions U(x), and are being exploited in a new class of dynamical sensors being developed by us. In this work we describe one of these devices, a coupled-core fluxgate magnetometer (CCFM), whose operation is underpinned by this dynamic behavior. We provide an overview of the underlying dynamics and, also, quantify the performance of our test device; in particular, we provide a quantitative performance comparison to a conventional (single-core) fluxgate magnetometer via a 'resolution' parameter that embodies the device sensitivity (the slope of its input–output transfer characteristic) as well as the noise floor

Spatial regression analysis on 32 years of total column ozone data

NARCIS (Netherlands)

Knibbe, J.S.; van der A, J.R.; de Laat, A.T.J.

2014-01-01

Multiple-regression analyses have been performed on 32 years of total ozone column data that was spatially gridded with a 1 × 1.5° resolution. The total ozone data consist of the MSR (Multi Sensor Reanalysis; 1979-2008) and 2 years of assimilated SCIAMACHY (SCanning Imaging Absorption spectroMeter

Magnetogate: Using an iPhone Magnetometer for Measuring Kinematic Variables

Science.gov (United States)

Temiz, Burak Kagan; Yavuz, Ahmet

2016-01-01

This paper presents a method to measure the movement of an object from specific locations on a straight line using an iPhone's magnetometer. In this method, called "magnetogate," an iPhone is placed on a moving object (in this case a toy car) and small neodymium magnets are arranged at equal intervals on one side of a straight line. The…

Quantum critical environment assisted quantum magnetometer

Science.gov (United States)

Jaseem, Noufal; Omkar, S.; Shaji, Anil

2018-04-01

A central qubit coupled to an Ising ring of N qubits, operating close to a critical point is investigated as a potential precision quantum magnetometer for estimating an applied transverse magnetic field. We compute the quantum Fisher information for the central, probe qubit with the Ising chain initialized in its ground state or in a thermal state. The non-unitary evolution of the central qubit due to its interaction with the surrounding Ising ring enhances the accuracy of the magnetic field measurement. Near the critical point of the ring, Heisenberg-like scaling of the precision in estimating the magnetic field is obtained when the ring is initialized in its ground state. However, for finite temperatures, the Heisenberg scaling is limited to lower ranges of N values.

Comparison of Vertical Drifts of ISR and Magnetometer Data Measurements at the Magnetic Equator

Science.gov (United States)

Condor P, P. J.

2014-12-01

We compare vertical drifts measured with the Jicamarca incoherent scatter radar (ISR) and drifts estimated from magnetometer data applying a Neural Network data processing technique. For the application of the Neural Network (NN) method, we use the magnitude of the horizontal (H) component of the magnetic field measured with magnetometers at Jicamarca and Piura (Peru). The data was collected between the years 2002 and 2013. In training the NN we use the difference between the magnitudes of the horizontal components (dH) measured at JRO (placed at the magnetic equator) and Piura (displaced 5° away). Additional parameters used are F10.7 and Ap indexes. The estimates obtained with the NN procedure are very good. We have an RMS error of 3.7 m/s using dH as an input of the NN while the error is 3.9 m/s when we use the component H of JRO as an input. The results are validated using the set of vertical drifts observations collected with the Jicamarca incoherent scatter radar. The estimated drifts can be accessed using the following website: http://jro.igp.gob.pe/driftnn. In the poster, we show the comparison of vertical drifts from 2002 to 2013 where we discuss the agreement between magnetometer and ISR data.

Loop-locked coherent population trapping magnetometer based on a fiber electro-optic modulator.

Science.gov (United States)

Hu, Yong; Feng, Y Y; Xu, Chi; Xue, H B; Sun, Li

2014-04-01

We have set up a coherent population trapping (CPT)-based magnetometer prototype with the D1 line of ⁸⁷Rb atoms. The dichromatic light field is derived from a fiber electro-optic modulator (FEOM) connected to an external cavity laser diode. A CPT resonance signal with a 516 Hz linewidth is observed. By feeding back the derivative of the resonance curve to the FEOM with a proportional integral controller, of which the voltage output is directly converted to the measured magnetic field intensity, the resonance peak is locked to the environmental magnetic field. The measurement data we have achieved are well matched with the data measured by a commercial fluxgate magnetometer within 2 nT, and the sensitivity is better than 8 pT/√Hz in a parallel B field.

New type of fluxgate magnetometer for the heart’s magnetic fields detection

Directory of Open Access Journals (Sweden)

Rybalko Ruslan

2015-09-01

Full Text Available The application area of fluxgate sensors is limited by their sensitivity. Medical researches create high demand on the magnetometers with the characteristics of high accuracy and sensibility for measuring weak magnetic fields produced by the human body, such as the heart‘s magnetic field. Due to the insufficient sensitivity of fluxgate sensors, superconducting magnetometers (SQUID take the dominant position for the cardiomagnetic measurements. They have to be cooled by liquefied gases and it leads to high service costs. Therefore an idea of creating a high sensitive sensor based on fluxgate principles and known methods of measurement is attractive and up to date. This paper is dedicated to the modified flux-gate sensors based on Racetrack technology with a new approach of signal demodulation. The improved fluxgate sensor system provides detection of the heart‘s magnetic field without additional expenditures for use.

Miniaturized digital fluxgate magnetometer for small spacecraft applications

International Nuclear Information System (INIS)

Forslund, Åke; Ivchenko, Nickolay; Olsson, Göran; Edberg, Terry; Belyayev, Serhiy; Marusenkov, Andriy

2008-01-01

A novel design of an Earth field digital fluxgate magnetometer is presented, the small magnetometer in low-mass experiment (SMILE). The combination of a number of new techniques results in significant miniaturization of both sensor and electronics. The design uses a sensor with volume compensation, combining three dual rod cores in a Macor® cube with the side dimension of 20 mm. Use of volume compensation provides high geometrical stability of the axes and improved performance compared to component compensated sensors. The sensor is operated at an excitation frequency of 8 kHz. Most of the instrument functionality is combined in a digital signal processing core, implemented in a field programmable gate array (FPGA). The pick-up signal is digitized after amplification and filtering, and values of compensation currents for each of the axes are determined by a digital correlation algorithm, equivalent to a matched filter, and are fed to a hybrid pulse-width modulation/delta-sigma digital-to-analogue converter driving the currents through the compensation coils. Using digital design makes the instrument very flexible, reduces power consumption and opens possibilities for the customization of the operation modes. The current implementation of the design is based on commercial off-the-shelf components. A calibration of the SMILE instrument was carried out at the Nurmijärvi Geophysical Observatory, showing high linearity (within 6 nT on the whole ±50 µT scale), good orthogonality (22 arcmin) and very good temperature stability of the axes

Diurnal and Seasonal Variations in Mid-Latitude Geomagnetic Field During International Quiet Days: BOH Magnetometer

Directory of Open Access Journals (Sweden)

Junga Hwang

2012-12-01

Full Text Available Korea Astronomy and Space Science Institute researchers have installed and operated magnetometers at Bohyunsan Observatory to measure the Earth's magnetic field variations in South Korea. In 2007, we installed a fluxgate magnetometer (RFP-523C to measure H, D, and Z components of the geomagnetic field. In addition, in 2009, we installed a Overhauser proton sensor to measure the absolute total magnetic field F and a three-axis magneto-impedance sensor for spectrum analysis. Currently three types of magnetometer data have been accumulated. In this paper, we use the H, D, Z components of fluxgate magnetometer data to investigate the characteristics of mid-latitude geomagnetic field variation. To remove the temporary changes in Earth’s geomagnetic filed by space weather, we use the international quiet days’ data only. In other words, we performed a superposed epoch analysis using five days per each month during 2008-2011. We find that daily variations of H, D, and Z shows similar tendency compared to previous results using all days. That is, H, D, Z all three components’ quiet intervals terminate near the sunrise and shows maximum 2-3 hours after the culmination and the quiet interval start from near the sunset. Seasonal variations show similar dependences to the Sun. As it becomes hot season, the geomagnetic field variation’s amplitude becomes large and the quiet interval becomes shortened. It is well-known that these variations are effects of Sq current system in the Earth’s atmosphere. We confirm that the typical mid-latitude geomagnetic field variations due to the Sq current system by excluding all possible association with the space weather.

Magnetic shield effect simulation of superconducting film shield covering directly coupled HTS dc-SQUID magnetometer

International Nuclear Information System (INIS)

Terauchi, N.; Noguchi, S.; Igarashi, H.

2011-01-01

A superconducting film shield over a SQUID ring improves the robustness of the SQUID with respect to magnetic noise. Supercurrent in the SQUID magnetometer and the superconducting film shield were simulated. The superconducting film shield reduces the influence of the external magnetic field on the SQUID ring. An HTS SQUID is a high sensitive magnetic sensor. In recent years, the HTS SQUID is widely used in various applications. In some applications, high robustness with respect to magnetic noise is required to realize stable operation at outside of a magnetic shielding room. The target of this paper is a directly coupled HTS dc-SQUID magnetometer. To enhance the robustness of the SQUID magnetometer, use of a superconducting thin film shield has been proposed. The magnetic field directly penetrating the SQUID ring causes the change of the critical current of Josephson junction, and then the SQUID magnetometer transitions into inoperative state. In order to confirm the magnetic shield effect of the superconducting film shield, electromagnetic field simulation with 3D edge finite element method was performed. To simulate the high temperature superconductor, E-J characteristics and c-axis anisotropy are considered. To evaluate the effect of the superconducting film shield, an external magnetic field which is supposed to be a magnetic noise is applied. From the simulation results, the time transition of the magnetic flux penetrating the SQUID ring is investigated and the effect of the superconducting film shield is confirmed. The amplitude of the magnetic flux penetrating the SQUID ring can be reduced to about one-sixth since the superconducting film shield prevents the magnetic noise from directly penetrating the SQUID ring.

Employing anatomical knowledge in vertebral column labeling

Science.gov (United States)

Yao, Jianhua; Summers, Ronald M.

2009-02-01

The spinal column constitutes the central axis of human torso and is often used by radiologists to reference the location of organs in the chest and abdomen. However, visually identifying and labeling vertebrae is not trivial and can be timeconsuming. This paper presents an approach to automatically label vertebrae based on two pieces of anatomical knowledge: one vertebra has at most two attached ribs, and ribs are attached only to thoracic vertebrae. The spinal column is first extracted by a hybrid method using the watershed algorithm, directed acyclic graph search and a four-part vertebra model. Then curved reformations in sagittal and coronal directions are computed and aggregated intensity profiles along the spinal cord are analyzed to partition the spinal column into vertebrae. After that, candidates for rib bones are detected using features such as location, orientation, shape, size and density. Then a correspondence matrix is established to match ribs and vertebrae. The last vertebra (from thoracic to lumbar) with attached ribs is identified and labeled as T12. The rest of vertebrae are labeled accordingly. The method was tested on 50 CT scans and successfully labeled 48 of them. The two failed cases were mainly due to rudimentary ribs.

Fluxgate vector magnetometers: Compensated multi-sensor devices for ground, UAV and airborne magnetic survey for various application in near surface geophysics

Science.gov (United States)

Gavazzi, Bruno; Le Maire, Pauline; Munschy, Marc; Dechamp, Aline

2017-04-01

Fluxgate 3-components magnetometer is the kind of magnetometer which offers the lightest weight and lowest power consumption for the measurement of the intensity of the magnetic field. Moreover, vector measurements make it the only kind of magnetometer allowing compensation of magnetic perturbations due to the equipment carried with it. Unfortunately, Fluxgate magnetometers are quite uncommon in near surface geophysics due to the difficulty to calibrate them precisely. The recent advances in calibration of the sensors and magnetic compensation of the devices from a simple process on the field led Institut de Physique du Globe de Strasbourg to develop instruments for georeferenced magnetic measurements at different scales - from submetric measurements on the ground to aircraft-conducted acquisition through the wide range offered by unmanned aerial vehicles (UAVs) - with a precision in the order of 1 nT. Such equipment is used for different kind of application: structural geology, pipes and UXO detection, archaeology.

The MAGIC of CINEMA: first in-flight science results from a miniaturised anisotropic magnetoresistive magnetometer

Directory of Open Access Journals (Sweden)

M. O. Archer

2015-06-01

Full Text Available We present the first in-flight results from a novel miniaturised anisotropic magnetoresistive space magnetometer, MAGIC (MAGnetometer from Imperial College, aboard the first CINEMA (CubeSat for Ions, Neutrals, Electrons and MAgnetic fields spacecraft in low Earth orbit. An attitude-independent calibration technique is detailed using the International Geomagnetic Reference Field (IGRF, which is temperature dependent in the case of the outboard sensor. We show that the sensors accurately measure the expected absolute field to within 2% in attitude mode and 1% in science mode. Using a simple method we are able to estimate the spacecraft's attitude using the magnetometer only, thus characterising CINEMA's spin, precession and nutation. Finally, we show that the outboard sensor is capable of detecting transient physical signals with amplitudes of ~ 20–60 nT. These include field-aligned currents at the auroral oval, qualitatively similar to previous observations, which agree in location with measurements from the DMSP (Defense Meteorological Satellite Program and POES (Polar-orbiting Operational Environmental Satellites spacecraft. Thus, we demonstrate and discuss the potential science capabilities of the MAGIC instrument onboard a CubeSat platform.

Assembly for connecting the column ends of two capillary columns

International Nuclear Information System (INIS)

Kolb, B.; Auer, M.; Pospisil, P.

1984-01-01

In gas chromatography, the column ends of two capillary columns are inserted into a straight capillary from both sides forming annular gaps. The capillary is located in a tee out of which the capillary columns are sealingly guided, and to which carrier gas is supplied by means of a flushing flow conduit. A ''straight-forward operation'' having capillary columns connected in series and a ''flush-back operation'' are possible. The dead volume between the capillary columns can be kept small

A simple vibrating sample magnetometer for macroscopic samples

Science.gov (United States)

Lopez-Dominguez, V.; Quesada, A.; Guzmán-Mínguez, J. C.; Moreno, L.; Lere, M.; Spottorno, J.; Giacomone, F.; Fernández, J. F.; Hernando, A.; García, M. A.

2018-03-01

We here present a simple model of a vibrating sample magnetometer (VSM). The system allows recording magnetization curves at room temperature with a resolution of the order of 0.01 emu and is appropriated for macroscopic samples. The setup can be mounted with different configurations depending on the requirements of the sample to be measured (mass, saturation magnetization, saturation field, etc.). We also include here examples of curves obtained with our setup and comparison curves measured with a standard commercial VSM that confirms the reliability of our device.

In-flight calibration of the spin axis offset of a fluxgate magnetometer with an electron drift instrument

Science.gov (United States)

Leinweber, H. K.; Russell, C. T.; Torkar, K.

2012-10-01

We show that the spin axis offset of a fluxgate magnetometer can be calibrated with an electron drift instrument (EDI) and that the required input time interval is relatively short. For missions such as Cluster or the upcoming Magnetospheric Multiscale (MMS) mission the spin axis offset of a fluxgate magnetometer could be determined on an orbital basis. An improvement of existing methods for finding spin axis offsets via comparison of accurate measurements of the field magnitude is presented, that additionally matches the gains of the two instruments that are being compared. The technique has been applied to EDI data from the Cluster Active Archive and fluxgate magnetometer data processed with calibration files also from the Cluster Active Archive. The method could prove to be valuable for the MMS mission because the four MMS spacecraft will only be inside the interplanetary field (where spin axis offsets can be calculated from Alfvénic fluctuations) for short periods of time and during unusual solar wind conditions.

In-flight calibration of the spin axis offset of a fluxgate magnetometer with an electron drift instrument

International Nuclear Information System (INIS)

Leinweber, H K; Russell, C T; Torkar, K

2012-01-01

We show that the spin axis offset of a fluxgate magnetometer can be calibrated with an electron drift instrument (EDI) and that the required input time interval is relatively short. For missions such as Cluster or the upcoming Magnetospheric Multiscale (MMS) mission the spin axis offset of a fluxgate magnetometer could be determined on an orbital basis. An improvement of existing methods for finding spin axis offsets via comparison of accurate measurements of the field magnitude is presented, that additionally matches the gains of the two instruments that are being compared. The technique has been applied to EDI data from the Cluster Active Archive and fluxgate magnetometer data processed with calibration files also from the Cluster Active Archive. The method could prove to be valuable for the MMS mission because the four MMS spacecraft will only be inside the interplanetary field (where spin axis offsets can be calculated from Alfvénic fluctuations) for short periods of time and during unusual solar wind conditions. (paper)

A nitrogen triple-point thermal storage unit for cooling a SQUID magnetometer

NARCIS (Netherlands)

Rijpma, A.P.; Meenderink, D.J.; Reincke, H.A.; Venhorst, G.C.F.; Holland, H.J.; Brake, ter H.J.M.

2005-01-01

In order to achieve turnkey operation, the use is planned of cryocoolers to cool a SQUID magnetometer system. To minimize the magnetical and mech. interference from the coolers, they are switched off during the actual measurements. Consequently, a thermal storage unit (TSU) is required with

Combined spacecraft orbit and attitude control through extended Kalman filtering of magnetometer, gyro, and GPS measurements

Directory of Open Access Journals (Sweden)

Tamer Mekky Ahmed Habib

2014-06-01

Full Text Available The main goal of this research is to establish spacecraft orbit and attitude control algorithms based on extended Kalman filter which provides estimates of spacecraft orbital and attitude states. The control and estimation algorithms must be capable of dealing with the spacecraft conditions during the detumbling and attitude acquisition modes of operation. These conditions are characterized by nonlinearities represented by large initial attitude angles, large initial angular velocities, large initial attitude estimation error, and large initial position estimation error. All of the developed estimation and control algorithms are suitable for application to the next Egyptian scientific satellite, EGYPTSAT-2. The parameters of the case-study spacecraft are similar but not identical to the former Egyptian satellite EGYPTSAT-1. This is done because the parameters of EGYPTSAT-2 satellite have not been consolidated yet. The sensors utilized are gyro, magnetometer, and GPS. Gyro and magnetometer are utilized to provide measurements for the estimates of spacecraft attitude state vector where as magnetometer and GPS are utilized to provide measurements for the estimates of spacecraft orbital state vector.

Development of fluxgate magnetometers and applications to the space science missions

Science.gov (United States)

Matsuoka, A.; Shinohara, M.; Tanaka, Y.-M.; Fujimoto, A.; Iguchi, K.

2013-11-01

Magnetic field is one of the essential physical parameters to study the space physics and evolution of the solar system. There are several methods to measure the magnetic field in the space by spacecraft and rockets. Fluxgate magnetometer has been most generally used out of them because it measures the vector field accurately and does not need much weight and power budgets. When we try more difficult missions such as multi-satellite observation, landing on the celestial body and exploration in the area of severe environment, we have to modify the magnetometer or develop new techniques to make the instrument adequate for those projects. For example, we developed a 20-bit delta-sigma analogue-to-digital converter for MGF-I on the BepiColombo MMO satellite, to achieve the wide-range (±2000 nT) measurement with good resolution in the high radiation environment. For further future missions, we have examined the digitalizing of the circuit, which has much potential to drastically reduce the instrument weight, power consumption and performance dependence on the temperature.

A nitrogen triple-point thermal storage unit for cooling a SQUID magnetometer

NARCIS (Netherlands)

Rijpma, A.P.; Meenderink, D.J.; Reincke, H.A.; Venhorst, G.C.F.; Venhorst, G.C.F.; Holland, Herman J.; ter Brake, Hermanus J.M.

2005-01-01

In order to achieve turnkey operation, we plan to use cryocoolers to cool a SQUID magnetometer system. To minimize the magnetical and mechanical interference from the coolers, we intend to switch them off during the actual measurements. Consequently, a thermal storage unit (TSU) is required with

A radiation hardened digital fluxgate magnetometer for space applications

Science.gov (United States)

Miles, D. M.; Bennest, J. R.; Mann, I. R.; Millling, D. K.

2013-09-01

Space-based measurements of Earth's magnetic field are required to understand the plasma processes responsible for energising particles in the Van Allen radiation belts and influencing space weather. This paper describes a prototype fluxgate magnetometer instrument developed for the proposed Canadian Space Agency's (CSA) Outer Radiation Belt Injection, Transport, Acceleration and Loss Satellite (ORBITALS) mission and which has applications in other space and suborbital applications. The magnetometer is designed to survive and operate in the harsh environment of Earth's radiation belts and measure low-frequency magnetic waves, the magnetic signatures of current systems, and the static background magnetic field. The new instrument offers improved science data compared to its predecessors through two key design changes: direct digitisation of the sensor and digital feedback from two cascaded pulse-width modulators combined with analog temperature compensation. These provide an increase in measurement bandwidth up to 450 Hz with the potential to extend to at least 1500 Hz. The instrument can resolve 8 pT on a 65 000 nT field with a magnetic noise of less than 10 pT/√Hz at 1 Hz. This performance is comparable with other recent digital fluxgates for space applications, most of which use some form of sigma-delta (ΣΔ) modulation for feedback and omit analog temperature compensation. The prototype instrument was successfully tested and calibrated at the Natural Resources Canada Geomagnetics Laboratory.

IceBridge Scintrex CS-3 Cesium Magnetometer L0 Raw Magnetic Field, Version 1

Data.gov (United States)

National Aeronautics and Space Administration — The NASA IceBridge Scintrex CS-3 Cesium Magnetometer L0 Raw Magnetic Field data set contains magnetic field readings and fluxgate values taken over Greenland using...

Multilayer Based Technology to Build RTD Fluxgate Magnetometer

Directory of Open Access Journals (Sweden)

B. ANDO

2006-03-01

Full Text Available In this paper we discuss the main features of the Residence Times Difference Fluxgate Magnetometer. A low-cost technology, negligible onboard power requirements and the intrinsic digital form of the readout signal are the main advantages of the proposed strategy. Results obtained show the possibility to realise low-cost devices exploiting Printed Circuit Board (PCB technology for applications requiring resolution in the nanotesla range as the ferrous object (or particles detection, being the performance obtained suitable to detect the presence or the transit of ferrous materials via their interaction with the geomagnetic field.

Polydopamine-coated open tubular column for the separation of proteins by capillary electrochromatography.

Science.gov (United States)

Xiao, Xing; Wang, Wentao; Chen, Jia; Jia, Li

2015-08-01

The separation and determination of proteins in food is an important aspect in food industry. Inspired by the self-polymerization of dopamine under alkaline conditions and the natural adhesive properties of polydopamine, in this paper, a simple and economical method was developed for the preparation of polydopamine-coated open tubular column, in which ammonium persulfate was used as the source of oxygen to induce and facilitate the polymerization of dopamine to form polydopamine. In comparison with a naked fused-silica capillary, the direction and magnitude of the electro-osmotic flow of the as-prepared polydopamine-coated open tubular column could be manipulated by varying the pH values of background solutions due to the existence of amine and phenolic hydroxyl groups on polydopamine coating. The surface morphology of the polydopamine-coated open tubular column was studied by scanning electron microscopy, and the thickness of polydopamine coating was 106 nm. The performance of the polydopamine-coated open tubular column was validated by analysis of proteins. The relative standard deviations of migration times of proteins representing run-to-run, day-to-day, and column-to-column were less than 3.5%. In addition, the feasibility of the polydopamine-coated open tubular column for real samples was verified by the separation of proteins in chicken egg white and pure milk. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

A novel ionic liquid monolithic column and its separation properties in capillary electrochromatography.

Science.gov (United States)

Wang, Yu; Deng, Qi-Liang; Fang, Guo-Zhen; Pan, Ming-Fei; Yu, Yang; Wang, Shuo

2012-01-27

A novel ionic liquid (IL) monolithic capillary column was successfully prepared by thermal free radical copolymerization of IL (1-vinyl-3-octylimidazolium chloride, ViOcIm(+)Cl(-)) together with lauryl methacrylate (LMA) as the binary functional monomers and ethylene dimethacrylate (EDMA) as the cross-linker in binary porogen. The proportion of monomers, porogens and cross-linker in the polymerization mixture was optimized in detail. The resulting IL-monolithic column could not only generate a stable reversed electroosmotic flow (EOF) in a wide pH range (2.0-12.0), but also effectively eliminate the wall adsorption of the basic analytes. The obtained IL-monolithic columns were examined by scanning electron microscopy (SEM) and Fourier transform infrared (FT-IR). These results indicated that the IL-monolithic capillary column possessed good pore properties, mechanical stability and permeability. The column performance was also evaluated by separating different kinds of compounds, such as alkylbenzenes, thiourea and its analogues, and amino acids. The lowest plate height of ~6.8 μm was obtained, which corresponded to column efficiency (theoretical plates, N) of ~147,000 plates m(-1) for thiourea. ILs, as a new type of functional monomer, present a promising option in the fabrication of the organic polymer-based monolithic columns in CEC. Copyright © 2011 Elsevier B.V. All rights reserved.

Magnetometer Data in the Classroom as a part of the NASA THEMIS Satellite Mission

Science.gov (United States)

Peticolas, L. M.; Bean, J.; Walker, A.

2011-12-01

The NASA-funded THEMIS mission was designed to determine the onset time and location of magnetic substorms of Earth's space environment, a prerequisite to understanding space weather. THEMIS is an acronym for Time History of Events and Macroscale Interactions during Substorms. he Geomagnetic Event Observation Network by Students (GEONS) project was the flagship, formal education component of the E/PO program. With the placement of magnetometers in the proximity of rural schools throughout the country, middle and high school teachers along with their students benefited from the opportunity to work with 'real-time' data and participated in hands-on space science activities. Particular attention was paid to placing the magnetometer stations at schools in rural communities whose students were traditionally underserved and underrepresented in the sciences. The project offered to the teachers of these students long-term professional development opportunities that centered around THEMIS-related space science and the magnetometer data. The THEMIS E/PO final evaluation report for the main phase of the THEMIS mission covered the period from 2003-2009, describing the impact of this program such as this program placed magnetometers sites at 13 rural, underserved schools/communities, two-fifths of which are on tribal lands; and provided intensive professional development for 20 teachers from 2004 through 2009. A core group of eight teachers estimated reaching more than 2,720 students with THEMIS-related materials/ideas. 75% of these students are minorities in science. Core teachers provided evidence of the project's positive impact on students' attitudes toward science and their choices for courses that position them for STEM-related careers. Core teachers reported sharing THEMIS-related materials/ideas with 275 colleagues. The NewsHour with Jim Lehrer featured the Petersburg, Alaska site potentially reaching more than 5 million viewers in two airings, according to Nielsen

Contributions to reversed-phase column selectivity: III. Column hydrogen-bond basicity.

Science.gov (United States)

Carr, P W; Dolan, J W; Dorsey, J G; Snyder, L R; Kirkland, J J

2015-05-22

Column selectivity in reversed-phase chromatography (RPC) can be described in terms of the hydrophobic-subtraction model, which recognizes five solute-column interactions that together determine solute retention and column selectivity: hydrophobic, steric, hydrogen bonding of an acceptor solute (i.e., a hydrogen-bond base) by a stationary-phase donor group (i.e., a silanol), hydrogen bonding of a donor solute (e.g., a carboxylic acid) by a stationary-phase acceptor group, and ionic. Of these five interactions, hydrogen bonding between donor solutes (acids) and stationary-phase acceptor groups is the least well understood; the present study aims at resolving this uncertainty, so far as possible. Previous work suggests that there are three distinct stationary-phase sites for hydrogen-bond interaction with carboxylic acids, which we will refer to as column basicity I, II, and III. All RPC columns exhibit a selective retention of carboxylic acids (column basicity I) in varying degree. This now appears to involve an interaction of the solute with a pair of vicinal silanols in the stationary phase. For some type-A columns, an additional basic site (column basicity II) is similar to that for column basicity I in primarily affecting the retention of carboxylic acids. The latter site appears to be associated with metal contamination of the silica. Finally, for embedded-polar-group (EPG) columns, the polar group can serve as a proton acceptor (column basicity III) for acids, phenols, and other donor solutes. Copyright © 2015 Elsevier B.V. All rights reserved.

Two-channel recoder for magnetometer with energy-independent mass memory device

International Nuclear Information System (INIS)

Korzinin, V.N.; Selivanov, A.M.

1993-01-01

The paper describes a two-channel digit-to-analog recorder designed for converting the sequence of pulses from proton magnetometer (MMH-203) outlet; the device enables processing of the pulses and their recording in RAM and on the tape of the analog recorder. The availability of nonvolotile RAM allows to transmit digit information to a computer (BK-0010) for its further processing

Preparation of β-cyclodextrin-gold nanoparticles modified open tubular column for capillary electrochromatographic separation of chiral drugs.

Science.gov (United States)

Zhou, Li; Jiang, Shenmeng; Zhang, Xue; Fang, Linlin; Guo, Xingjie

2018-04-01

In this paper, β-cyclodextrin (β-CD) modified gold nanoparticles (AuNPs) coated open tubular column (OT column) was prepared for capillary electrochromatography. The open tubular column was constructed through self-assembly of gold nanoparticles on 3-mercaptopropyl-trimethoxysilane (MPTMS) prederivatized capillary and subsequent modification of thiols β-cyclodextrin (SH-β-CD). Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and ultraviolet visible spectroscopy were carried out to characterize the prepared open tubular column and synthesized gold nanoparticles. By comparing different coating times of gold nanoparticles and thiols β-cyclodextrin, we got the optimal conditions for preparing the open tubular column. Also, the separation parameters were optimized including buffer pH, buffer concentration and applied voltage. Separation effectiveness of open tubular column was verified by the separation of four pairs of drug enantiomers including bifonazole, fexofenadine, omeprazole and lansoprazole, and satisfactory separation results were achieved for these analytes studied. In addition, the column showed good stability and repeatability. The relative standard deviation values less than 5% were obtained through intra-day, inter-day, and column-to-column investigations. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

JCE Feature Columns

Science.gov (United States)

Holmes, Jon L.

1999-05-01

The Features area of JCE Online is now readily accessible through a single click from our home page. In the Features area each column is linked to its own home page. These column home pages also have links to them from the online Journal Table of Contents pages or from any article published as part of that feature column. Using these links you can easily find abstracts of additional articles that are related by topic. Of course, JCE Online+ subscribers are then just one click away from the entire article. Finding related articles is easy because each feature column "site" contains links to the online abstracts of all the articles that have appeared in the column. In addition, you can find the mission statement for the column and the email link to the column editor that I mentioned above. At the discretion of its editor, a feature column site may contain additional resources. As an example, the Chemical Information Instructor column edited by Arleen Somerville will have a periodically updated bibliography of resources for teaching and using chemical information. Due to the increase in the number of these resources available on the WWW, it only makes sense to publish this information online so that you can get to these resources with a simple click of the mouse. We expect that there will soon be additional information and resources at several other feature column sites. Following in the footsteps of the Chemical Information Instructor, up-to-date bibliographies and links to related online resources can be made available. We hope to extend the online component of our feature columns with moderated online discussion forums. If you have a suggestion for an online resource you would like to see included, let the feature editor or JCE Online (jceonline@chem.wisc.edu) know about it. JCE Internet Features JCE Internet also has several feature columns: Chemical Education Resource Shelf, Conceptual Questions and Challenge Problems, Equipment Buyers Guide, Hal's Picks, Mathcad

Basic technical parameters of magnetometers with ferromagnetic transducers and a method to define them

International Nuclear Information System (INIS)

Nagiello, Z.

1980-01-01

The basic technical parameters of magnetometers with ferromagnetic transducers and measuring methods to define these parameters have been discussed. Special attention was paid to factors which essentially affect the inaccuracy of these measuring instruments. (author)

A novel ionic liquid monolithic column and its separation properties in capillary electrochromatography

International Nuclear Information System (INIS)

Wang Yu; Deng Qiliang; Fang Guozhen; Pan Mingfei; Yu Yang; Wang Shuo

2012-01-01

Highlights: ► ILs as functional monomer for capillary monolithic column. ► Separation of alkylbenzenes, thiourea analogues, and amino acids. ► The column generate a stable reversed EOF from pH 2.0 to 12.0. ► The column efficiency of 147,000 plates m −1 was obtained for thiourea. - Abstract: A novel ionic liquid (IL) monolithic capillary column was successfully prepared by thermal free radical copolymerization of IL (1-vinyl-3-octylimidazolium chloride, ViOcIm + Cl − ) together with lauryl methacrylate (LMA) as the binary functional monomers and ethylene dimethacrylate (EDMA) as the cross-linker in binary porogen. The proportion of monomers, porogens and cross-linker in the polymerization mixture was optimized in detail. The resulting IL-monolithic column could not only generate a stable reversed electroosmotic flow (EOF) in a wide pH range (2.0–12.0), but also effectively eliminate the wall adsorption of the basic analytes. The obtained IL-monolithic columns were examined by scanning electron microscopy (SEM) and Fourier transform infrared (FT-IR). These results indicated that the IL-monolithic capillary column possessed good pore properties, mechanical stability and permeability. The column performance was also evaluated by separating different kinds of compounds, such as alkylbenzenes, thiourea and its analogues, and amino acids. The lowest plate height of ∼6.8 μm was obtained, which corresponded to column efficiency (theoretical plates, N) of ∼147,000 plates m −1 for thiourea. ILs, as a new type of functional monomer, present a promising option in the fabrication of the organic polymer-based monolithic columns in CEC.

Scanning electron microscope facility for examination of radioactive materials

International Nuclear Information System (INIS)

Gibson, J.R.; Braski, D.N.

1985-02-01

An AMRAY model 1200B scanning electron microscope was modified to permit remote examination of radioactive specimens. Features of the modification include pneumatic vibration isolation of the column, motorized stage controls, improvements for monitoring vacuum, and a system for changing filaments without entering the hot cell

General theory of detection of signal induced in vibrating magnetometer

International Nuclear Information System (INIS)

Pacyna, A.W.

1980-01-01

Assuming the point dipole approximation only and making use of the vectorial notation, signal (EMF) induced in a single-turn pick-up coil of the vibrating magnetometer are calculated for the case of any orientation of the coil, of vibration axis and of the magnetic moment of the sample. On the basis of formula obtained, three types of measurement geometries have been distinquished and for these the qualitative analysis is made. (author)

Improved focusing-and-deflection columns

International Nuclear Information System (INIS)

Mui, P.H.; Szilagyi, M.

1995-01-01

Our earlier design procedures for constructing quadrupole columns are further expanded to include octupole corrector units and ''octupole'' deflectors with no third-order harmonics. The additional complications are finer partitioning of the plates and increased number of voltage controllers. Two sample designs, one having only the additional octupole deflectors and one having both the deflectors and the correctors, are presented and compared to our previous quadrupole system. The additional octupole components are shown to be capable of increasing the current density from 30% to more than 300% for a four-plate system, designed to focus and scan the electron beam over a circular area of 0.25 mm radius. The electron beam is assumed to have an initial divergence of ±2.3 mrad, an initial energy of 6 kV, a total energy spread of 1 eV, and a final acceleration of 30 keV. These systems are then slightly reoptimized for a superficial comparison with the commercially available column by Micrion Corporation. The numerical results indicate a potential for substantial improvements, demonstrating the power of this design procedure. Finally, a discussion is presented on how the individual components can interact with each other to reduce the various aberrations. copyright 1995 American Vacuum Society

On determining fluxgate magnetometer spin axis offsets from mirror mode observations

Science.gov (United States)

Plaschke, Ferdinand; Narita, Yasuhito

2016-09-01

In-flight calibration of fluxgate magnetometers that are mounted on spacecraft involves finding their outputs in vanishing ambient fields, the so-called magnetometer offsets. If the spacecraft is spin-stabilized, then the spin plane components of these offsets can be relatively easily determined, as they modify the spin tone content in the de-spun magnetic field data. The spin axis offset, however, is more difficult to determine. Therefore, usually Alfvénic fluctuations in the solar wind are used. We propose a novel method to determine the spin axis offset: the mirror mode method. The method is based on the assumption that mirror mode fluctuations are nearly compressible such that the maximum variance direction is aligned to the mean magnetic field. Mirror mode fluctuations are typically found in the Earth's magnetosheath region. We introduce the method and provide a first estimate of its accuracy based on magnetosheath observations by the THEMIS-C spacecraft. We find that 20 h of magnetosheath measurements may already be sufficient to obtain high-accuracy spin axis offsets with uncertainties on the order of a few tenths of a nanotesla, if offset stability can be assumed.

On determining fluxgate magnetometer spin axis offsets from mirror mode observations

Directory of Open Access Journals (Sweden)

F. Plaschke

2016-09-01

Full Text Available In-flight calibration of fluxgate magnetometers that are mounted on spacecraft involves finding their outputs in vanishing ambient fields, the so-called magnetometer offsets. If the spacecraft is spin-stabilized, then the spin plane components of these offsets can be relatively easily determined, as they modify the spin tone content in the de-spun magnetic field data. The spin axis offset, however, is more difficult to determine. Therefore, usually Alfvénic fluctuations in the solar wind are used. We propose a novel method to determine the spin axis offset: the mirror mode method. The method is based on the assumption that mirror mode fluctuations are nearly compressible such that the maximum variance direction is aligned to the mean magnetic field. Mirror mode fluctuations are typically found in the Earth's magnetosheath region. We introduce the method and provide a first estimate of its accuracy based on magnetosheath observations by the THEMIS-C spacecraft. We find that 20 h of magnetosheath measurements may already be sufficient to obtain high-accuracy spin axis offsets with uncertainties on the order of a few tenths of a nanotesla, if offset stability can be assumed.

Preparation of Affinity Column Based on Zr4+ Ion for Phosphoproteins Isolation

International Nuclear Information System (INIS)

Lee, Seon Mi; Bae, In Ae; Park, Jung Hyen; Kim, Tae Dong; Choi, Seong Ho

2009-01-01

This paper has described about preparation of Zr 4+ affinity column based on the poly(styreneco- glycidyl methacrylate) prepared by emulsion polymerization of styrene and glycidyl methacrylate in order to isolate phosphopeptide. The Zr 4+ ions were introduced after the phophonation of an epoxy group on polymeric microspheres. The successful preparation of Zr 4+ -immobilized polymeric microsphere stationary phase was confirmed through Fourier transform infrared spectra, optical microscopy, scanning electron microscopy, X-ray photoelectron spectra and inductively coupled plasma-atomic emission spectrometer. The separation efficiency for Zr 4+ affinity column prepared by slurry packing was tested to phosphonated casein and dephosphonated casein. The resolution time (min) of the phosphonated casein was higher than that of dephosphated casein for Zr 4+ affinity polymeric microsphere by liquid chromatography. This Zr 4+ affinity column can be used for isolation of phosphonated casein from casein using liquid chromatography

Study on modulation amplitude stabilization method for PEM based on FPGA in atomic magnetometer

Science.gov (United States)

Wang, Qinghua; Quan, Wei; Duan, Lihong

2017-10-01

Atomic magnetometer which uses atoms as sensitive elements have ultra-high precision and has wide applications in scientific researches. The photoelastic modulation method based on photoelastic modulator (PEM) is used in the atomic magnetometer to detect the small optical rotation angle of a linearly polarized light. However, the modulation amplitude of the PEM will drift due to the environmental factors, which reduces the precision and long-term stability of the atomic magnetometer. Consequently, stabilizing the PEM's modulation amplitude is essential to precision measurement. In this paper, a modulation amplitude stabilization method for PEM based on Field Programmable Gate Array (FPGA) is proposed. The designed control system contains an optical setup and an electrical part. The optical setup is used to measure the PEM's modulation amplitude. The FPGA chip, with the PID control algorithm implemented in it, is used as the electrical part's micro controller. The closed loop control method based on the photoelastic modulation detection system can directly measure the PEM's modulation amplitude in real time, without increasing the additional optical devices. In addition, the operating speed of the modulation amplitude stabilization control system can be greatly improved because of the FPGA's parallel computing feature, and the PID control algorithm ensures flexibility to meet different needs of the PEM's modulation amplitude set values. The Modelsim simulation results show the correctness of the PID control algorithm, and the long-term stability of the PEM's modulation amplitude reaches 0.35% in a 3-hour continuous measurement.

Reversed preparation of low-density poly(divinylbenzene/styrene) foam columns coated with gold films

Energy Technology Data Exchange (ETDEWEB)

Dai, Yinhai; Wang, Ni; Li, Yaling; Yao, Mengqi; Gan, Haibo; Hu, Wencheng, E-mail: huwc@uestc.edu.cn

2016-06-15

Highlights: • A reversed fabrication of low density foam columns coated with gold films was proposed. • The uniformity in thickness and purity of gold film are easy to be controlled. • A compact layer is prepared through an electrophoretic deposition method. • A low density (12 mg/cc) foam column coated with gold film is obtained. - Abstract: This work aims to fabricate low-density, porous, non-conductive, structural poly(divinylbenzene/styrene) foam columns by high-internal-phase emulsion templating. We prepare these non-conductive foam columns coated with a thin gold layer by electrochemical deposition and the reversed preparation technique. As expected, the density of the foam obtained through this novel method was about 12 mg cm{sup −3}, and the thickness of the gold coating was about 3 μm. We performed field emission scanning electron microscopy to morphologically and microstructurally characterize the products and X-ray diffraction and energy dispersive spectroscopy to determine the composition of the gold coating.

Column Liquid Chromatography.

Science.gov (United States)

Majors, Ronald E.; And Others

1984-01-01

Reviews literature covering developments of column liquid chromatography during 1982-83. Areas considered include: books and reviews; general theory; columns; instrumentation; detectors; automation and data handling; multidimensional chromatographic and column switching techniques; liquid-solid chromatography; normal bonded-phase, reversed-phase,…

The Global Network of Optical Magnetometers for Exotic physics (GNOME): A novel scheme to search for physics beyond the Standard Model

International Nuclear Information System (INIS)

Pustelny, Szymon; Jackson Kimball, Derek F.; Pankow, Chris; Ledbetter, Micah P.; Wlodarczyk, Przemyslaw; Wcislo, Piotr; Pospelov, Maxim; Smith, Joshua R.; Read, Jocelyn; Gawlik, Wojciech; Budker, Dmitry

2013-01-01

A novel experimental scheme enabling the investigation of transient exotic spin couplings is discussed. The scheme is based on synchronous measurements of optical-magnetometer signals from several devices operating in magnetically shielded environments in distant locations (>or similar 100 km). Although signatures of such exotic couplings may be present in the signal from a single magnetometer, it would be challenging to distinguish them from noise. By analyzing the correlation between signals from multiple, geographically separated magnetometers, it is not only possible to identify the exotic transient but also to investigate its nature. The ability of the network to probe presently unconstrained physics beyond the Standard Model is examined by considering the spin coupling to stable topological defects (e.g., domain walls) of axion-like fields. In the spirit of this research, a brief (∝2 hours) demonstration experiment involving two magnetometers located in Krakow and Berkeley (∝9000 km separation) is presented and discussion of the data-analysis approaches that may allow identification of transient signals is provided. The prospects of the network are outlined in the last part of the paper. (copyright 2013 by WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

Three axis vector atomic magnetometer utilizing polarimetric technique

Energy Technology Data Exchange (ETDEWEB)

Pradhan, Swarupananda, E-mail: spradhan@barc.gov.in, E-mail: pradhans75@gmail.com [Laser and Plasma Technology Division, Bhabha Atomic Research Centre, Mumbai 400085, India and Homi Bhabha National Institute, Department of Atomic Energy, Mumbai 400094 (India)

2016-09-15

The three axis vector magnetic field measurement based on the interaction of a single elliptically polarized light beam with an atomic system is described. The magnetic field direction dependent atomic responses are extracted by the polarimetric detection in combination with laser frequency modulation and magnetic field modulation techniques. The magnetometer geometry offers additional critical requirements like compact size and large dynamic range for space application. Further, the three axis magnetic field is measured using only the reflected signal (one polarization component) from the polarimeter and thus can be easily expanded to make spatial array of detectors and/or high sensitivity field gradient measurement as required for biomedical application.

Controlled crosslinking of trimethylolpropane trimethacrylate for preparation of organic monolithic columns for capillary liquid chromatography.

Science.gov (United States)

Gama, Mariana R; Aggarwal, Pankaj; Lee, Milton L; Bottoli, Carla B G

2017-11-01

Organic monolithic columns based on single crosslinking of trimethylolpropane trimethacrylate (TRIM) monomer were prepared in a single step by living/controlled free-radical polymerization. Full optimization of the preparation, such as using different percentages of TRIM and different amounts of radical promoter as well as various porogen solvents were explored. The resulting monolithic columns were characterized by scanning electronic microscopy and nitrogen sorption for structure morphology studies and surface area measurements, respectively. Using capillary liquid chromatography, 150 μm i.d. columns were applied to separate a mixture of small hydrophobic molecules. The results indicated that column performance is highly sensitive to the type and the amount of porogen solvents used in the polymerization mixture composition. Good resolution factors and methylene selectivity were obtained, indicating the promising potential of this material for capillary liquid chromatography separations. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Simultaneous Scanning Electron Microscope Imaging of Topographical and Chemical Contrast Using In-Lens, In-Column, and Everhart-Thornley Detector Systems.

Science.gov (United States)

Zhang, Xinming; Cen, Xi; Ravichandran, Rijuta; Hughes, Lauren A; van Benthem, Klaus

2016-06-01

The scanning electron microscope provides a platform for subnanometer resolution characterization of material morphology with excellent topographic and chemical contrast dependent on the used detectors. For imaging applications, the predominantly utilized signals are secondary electrons (SEs) and backscattered electrons (BSEs) that are emitted from the sample surface. Recent advances in detector technology beyond the traditional Everhart-Thornley geometry have enabled the simultaneous acquisition and discrimination of SE and BSE signals. This study demonstrates the imaging capabilities of a recently introduced new detector system that consists of the combination of two in-lens (I-L) detectors and one in-column (I-C) detector. Coupled with biasing the sample stage to reduce electron-specimen interaction volumes, this trinity of detector geometry allows simultaneous acquisition of signals to distinguish chemical contrast from topographical changes of the sample, including the identification of surface contamination. The I-C detector provides 4× improved topography, whereas the I-L detector closest to the sample offers excellent simultaneous chemical contrast imaging while not limiting the minimization of working distance to obtain optimal lateral resolution. Imaging capabilities and contrast mechanisms for all three detectors are discussed quantitatively in direct comparison to each other and the conventional Everhart-Thornley detector.

ATS-6 - UCLA fluxgate magnetometer

Science.gov (United States)

Mcpherron, R. L.; Coleman, P. J., Jr.; Snare, R. C.

1975-01-01

A summary of the design of the University of California at Los Angeles' fluxgate magnetometer is presented. Instrument noise in the bandwidth 0.001 to 1.0 Hz is of order 85 m gamma. The DC field of the spacecraft transverse to the earth-pointing axis is 1.0 + or - 21 gamma in the X direction and -2.4 + or - 1.3 gamma in the Y direction. The spacecraft field parallel to this axis is less than 5 gamma. The small spacecraft field has made possible studies of the macroscopic field not previously possible at synchronous orbit. At the 96 W longitude of Applications Technology Satellite-6 (ATS-6), the earth's field is typically inclined 30 deg to the dipole axis at local noon. Most perturbations of the field are due to substorms. These consist of a rotation in the meridian to a more radial field followed by a subsequent rotation back. The rotation back is normally accompanied by transient variations in the azimuthal field. The exact timing of these perturbations is a function of satellite location and the details of substorm development.

A wide-frequency range AC magnetometer to measure the specific absorption rate in nanoparticles for magnetic hyperthermia

International Nuclear Information System (INIS)

Garaio, E.; Collantes, J.M.; Garcia, J.A.; Plazaola, F.; Mornet, S.; Couillaud, F.; Sandre, O.

2014-01-01

Measurement of specific absorption rate (SAR) of magnetic nanoparticles is crucial to assert their potential for magnetic hyperthermia. To perform this task, calorimetric methods are widely used. However, those methods are not very accurate and are difficult to standardize. In this paper, we present AC magnetometry results performed with a lab-made magnetometer that is able to obtain dynamic hysteresis-loops in the AC magnetic field frequency range from 50 kHz to 1 MHz and intensities up to 24 kA m −1 . In this work, SAR values of maghemite nanoparticles dispersed in water are measured by AC magnetometry. The so-obtained values are compared with the SAR measured by calorimetric methods. Both measurements, by calorimetry and magnetometry, are in good agreement. Therefore, the presented AC magnetometer is a suitable way to obtain SAR values of magnetic nanoparticles. - Highlights: • We propose AC magnetometry as a method to measure the specific absorption rate (SAR) of magnetic nanoparticles suitable for magnetic hyperthermia therapy. • We have built a lab-made AC magnetometer, which is able to measure magnetic dynamic hysteresis-loops of nanoparticle dispersions. • The device works with AC magnetic field intensities up to 24 kA m −1 in a frequency range from 75 kHz to 1 MHz. • The SAR values of maghemite nanoparticles around 12 nm in magnetic diameter dispersed in water are measured by the lab-made magnetometer and different calorimetric methods. • Although all methods are in good agreement, several factors (probe location, thermal inertia, losses, etc.) make calorimetric method less accurate than AC magnetometry

CalMagNet – an array of search coil magnetometers monitoring ultra low frequency activity in California

Directory of Open Access Journals (Sweden)

C. Dunson

2008-04-01

Full Text Available The California Magnetometer Network (CalMagNet consists of sixty-eight triaxial search-coil magnetometer systems measuring Ultra Low Frequency (ULF, 0.001–16 Hz, magnetic field fluctuations in California. CalMagNet provides data for comprehensive multi-point measurements of specific events in the Pc 1–Pc 5 range at mid-latitudes as well as a systematic, long-term study of ULF signals in active fault regions in California. Typical events include geomagnetic micropulsations and spectral resonant structures associated with the ionospheric Alfvén resonator. This paper provides a technical overview of the CalMagNet sensors and data processing systems. The network is composed of ten reference stations and fifty-eight local monitoring stations. The primary instruments at each site are three orthogonal induction coil magnetometers. A geophone monitors local site vibration. The systems are designed for future sensor expansion and include resources for monitoring four additional channels. Data is currently sampled at 32 samples per second with a 24-bit converter and time tagged with a GPS-based timing system. Several examples of representative magnetic fluctuations and signals as measured by the array are given.

IceBridge Scintrex CS-3 Cesium Magnetometer L1B Geolocated Magnetic Anomalies, Version 1

Data.gov (United States)

National Aeronautics and Space Administration — The NASA IceBridge Scintrex CS-3 Cesium Magnetometer L1B Geolocated Magnetic Anomalies (IMCS31B) data set contains magnetic field readings taken over Greenland using...

Preparation of Affinity Column Based on Zr{sup 4+} Ion for Phosphoproteins Isolation

Energy Technology Data Exchange (ETDEWEB)

Lee, Seon Mi; Bae, In Ae; Park, Jung Hyen; Kim, Tae Dong; Choi, Seong Ho [Hannam University, Daejeon (Korea, Republic of)

2009-06-15

This paper has described about preparation of Zr{sup 4+} affinity column based on the poly(styreneco- glycidyl methacrylate) prepared by emulsion polymerization of styrene and glycidyl methacrylate in order to isolate phosphopeptide. The Zr{sup 4+} ions were introduced after the phophonation of an epoxy group on polymeric microspheres. The successful preparation of Zr{sup 4+}-immobilized polymeric microsphere stationary phase was confirmed through Fourier transform infrared spectra, optical microscopy, scanning electron microscopy, X-ray photoelectron spectra and inductively coupled plasma-atomic emission spectrometer. The separation efficiency for Zr{sup 4+} affinity column prepared by slurry packing was tested to phosphonated casein and dephosphonated casein. The resolution time (min) of the phosphonated casein was higher than that of dephosphated casein for Zr{sup 4+} affinity polymeric microsphere by liquid chromatography. This Zr{sup 4+} affinity column can be used for isolation of phosphonated casein from casein using liquid chromatography.

Real-space imaging of non-collinear antiferromagnetic order with a single-spin magnetometer

Science.gov (United States)

Gross, I.; Akhtar, W.; Garcia, V.; Martínez, L. J.; Chouaieb, S.; Garcia, K.; Carrétéro, C.; Barthélémy, A.; Appel, P.; Maletinsky, P.; Kim, J.-V.; Chauleau, J. Y.; Jaouen, N.; Viret, M.; Bibes, M.; Fusil, S.; Jacques, V.

2017-09-01

Although ferromagnets have many applications, their large magnetization and the resulting energy cost for switching magnetic moments bring into question their suitability for reliable low-power spintronic devices. Non-collinear antiferromagnetic systems do not suffer from this problem, and often have extra functionalities: non-collinear spin order may break space-inversion symmetry and thus allow electric-field control of magnetism, or may produce emergent spin-orbit effects that enable efficient spin-charge interconversion. To harness these traits for next-generation spintronics, the nanoscale control and imaging capabilities that are now routine for ferromagnets must be developed for antiferromagnetic systems. Here, using a non-invasive, scanning single-spin magnetometer based on a nitrogen-vacancy defect in diamond, we demonstrate real-space visualization of non-collinear antiferromagnetic order in a magnetic thin film at room temperature. We image the spin cycloid of a multiferroic bismuth ferrite (BiFeO3) thin film and extract a period of about 70 nanometres, consistent with values determined by macroscopic diffraction. In addition, we take advantage of the magnetoelectric coupling present in BiFeO3 to manipulate the cycloid propagation direction by an electric field. Besides highlighting the potential of nitrogen-vacancy magnetometry for imaging complex antiferromagnetic orders at the nanoscale, these results demonstrate how BiFeO3 can be used in the design of reconfigurable nanoscale spin textures.

Evaluation of {sup 99}Mo/{sup 99m}Tc generator columns after irradiation with different absorbed doses

Energy Technology Data Exchange (ETDEWEB)

Fukumori, Neuza T.O.; Mengatti, Jair; Matsuda, Margareth M.N., E-mail: ntfukumo@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNE-SP), Sao Paulo, SP (Brazil)

2017-07-01

The {sup 99}Mo/{sup 99m}Tc generator is widely used in nuclear medicine and it consists of a glass column containing Teflon® strips and alumina in which {sup 99}Mo produced by {sup 235}U fission is adsorbed. The {sup 99}mTcO4- eluate shall meet the sterile and pyrogen free conditions for injectable radiopharmaceuticals as determined by the Good Manufacturing Practices. The purpose of this study was to evaluate the feasibility of using gamma radiation in the sterilization of the {sup 99}Mo/{sup 99m}Tc generator column and the influence on the elution efficiency. Alumina-containing columns were irradiated with 10, 15, 25 and 50 kGy absorbed doses. Alumina samples and control (non-irradiated) were submitted to X-ray diffraction and the combined use of scanning electron microscopy and elemental analysis. Teflon® samples were evaluated by thermogravimetry (TGA) and differential scanning calorimetry (DSC). X-ray diffractograms and micrographies with elemental analysis showed no significant changes in the crystalline structure of the alumina because it was stable α-Al{sub 2}O{sub 3}. TGA demonstrated that higher doses showed changes in lower temperatures and times than the control material. For DSC the higher the absorbed dose, the greater the polymer chain breakage and crosslinking in the material. The generator system without radioactivity was set up with the irradiated columns and the eluates demonstrated to be sterile and pyrogen free. The effects of different absorbed doses on the generator column, although some reported changes in the materials, demonstrated that the sterilization of the columns by irradiation with gamma rays as an alternative to wet heat sterilization is feasible from a technical and financial point of view. (author)

Air column in esophagus and symptoms of gastroesophageal reflux disease

International Nuclear Information System (INIS)

Moosavi, Alijavad; Raji, Hanieh; Teimoori, Mojtaba; Ghourchian, Shadi

2012-01-01

During imaging of the normal esophagus, air is often detected. The purpose of this study was to determine the correlation between the appearance of air bubbles on imaging and Gastroesophageal Reflux Disease (GERD) symptoms. The cross-sectional imaging study was conducted at Rasole Akram Hospital, Tehran, Iran. A total of 44 patients underwent X-ray computed tomography (CT) scanning; the presence of air in the esophagus and visible on CT imaging was scrutinized. The average age of the subjects was 59 and the male to female ratio was 0.83. We found a significant relationship between the presence of GERD symptoms, the size of air bubbles and esophageal dilation (ED) on the CT scan. Air bubbles in the esophagus may be seen frequently in CT scans, but their size and location can vary. The GERD symptoms can arise when a small diameter air column is present within the esophagus, especially in the middle and lower parts

Detecting molecules and cells labeled with magnetic particles using an atomic magnetometer

International Nuclear Information System (INIS)

Yu Dindi; Ruangchaithaweesuk, Songtham; Yao Li; Xu Shoujun

2012-01-01

The detection of magnetically labeled molecules and cells involves three essential parameters: sensitivity, spatial resolution, and molecular specificity. We report on the use of atomic magnetometry and its derivative techniques to achieve high performance in terms of all these parameters. With a sensitivity of 80 fT/√Hz for dc magnetic fields, we show that 7,000 streptavidin-conjugated magnetic microparticles magnetized by a permanent magnet produce a magnetic field of 650 pT; this result predicts that a single such particle can be detected during one second of signal averaging. Spatial information is obtained using a scanning magnetic imaging scheme. The spatial resolution is 20 μm with a detection distance of more than 1 cm; this distance is much longer than that in previous reports. The molecular specificity is achieved using force-induced remnant magnetization spectroscopy, which currently uses an atomic magnetometer for detection. As an example, we perform measurement of magnetically labeled human CD4+ T cells, whose count in the blood is the diagnostic criterion for human immunodeficiency virus infection. Magnetic particles that are specifically bound to the cells are resolved from nonspecifically bound particles and quantitatively correlate with the number of cells. The magnetic particles have an overall size of 2.8 μm, with a magnetic core in nanometer regime. The combination of our techniques is predicted to be useful in molecular and cellular imaging.

Detecting molecules and cells labeled with magnetic particles using an atomic magnetometer

Energy Technology Data Exchange (ETDEWEB)

Yu Dindi; Ruangchaithaweesuk, Songtham; Yao Li; Xu Shoujun, E-mail: sxu7@uh.edu [University of Houston, Department of Chemistry (United States)

2012-09-15

The detection of magnetically labeled molecules and cells involves three essential parameters: sensitivity, spatial resolution, and molecular specificity. We report on the use of atomic magnetometry and its derivative techniques to achieve high performance in terms of all these parameters. With a sensitivity of 80 fT/{radical}Hz for dc magnetic fields, we show that 7,000 streptavidin-conjugated magnetic microparticles magnetized by a permanent magnet produce a magnetic field of 650 pT; this result predicts that a single such particle can be detected during one second of signal averaging. Spatial information is obtained using a scanning magnetic imaging scheme. The spatial resolution is 20 {mu}m with a detection distance of more than 1 cm; this distance is much longer than that in previous reports. The molecular specificity is achieved using force-induced remnant magnetization spectroscopy, which currently uses an atomic magnetometer for detection. As an example, we perform measurement of magnetically labeled human CD4+ T cells, whose count in the blood is the diagnostic criterion for human immunodeficiency virus infection. Magnetic particles that are specifically bound to the cells are resolved from nonspecifically bound particles and quantitatively correlate with the number of cells. The magnetic particles have an overall size of 2.8 {mu}m, with a magnetic core in nanometer regime. The combination of our techniques is predicted to be useful in molecular and cellular imaging.

Feasibility study of a sup 3 He-magnetometer for neutron electric dipole moment experiments

CERN Document Server

Borisov, Y; Leduc, M; Lobashev, V; Otten, E W; Sobolev, Y

2000-01-01

We report on a sup 3 He-magnetometer capable of detecting tiny magnetic field fluctuations of less than 10 sup - sup 1 sup 4 T in experiments for measuring the electric dipole moment (EDM) of the neutron. It is based on the Ramsey technique of separated oscillating fields and uses nuclear spin-polarized sup 3 He gas which is stored in two vessels of V approx =10 l in a sandwich-type arrangement around the storage bottle for ultra-cold neutrons (UCN). The gas is polarized by means of optical pumping in a separate, small discharge cell at pressures around 0.5 mbar and is then expanded into the actual magnetometer volume. To detect the polarization of sup 3 He gas at the end of the storage cycle the gas is pumped out by means of an oil-diffusion pump and compressed again into the discharge cell where optical detection of nuclear polarization is used.

Setup and taking into operation of a highly sensitive {sup 3}He magnetometer for a future experiment for the determination of an electric dipole moment of the free neutron; Aufbau und Inbetriebnahme eines hochsensitiven {sup 3}He-Magnetometers fuer ein zukuenftiges Experiment zur Bestimmung eines elektrischen Dipolmoments des freien Neutrons

Energy Technology Data Exchange (ETDEWEB)

Kraft, Andreas

2012-12-20

The measurement of the electric dipole moment of the free neutron is directly linked to the question on the accurate determination of the magnetic field conditions inside the nEDM spectrometer. Using in-situ the spin-precession of polarized {sup 3}He, monitored by optically pumped Cs-magnetometers a sensitivity on the femto-tesla-scale can be obtained. At the institute of physics of the University Mainz a {sup 3}He/Cs-test facility was built to investigate the readout of {sup 3}He-spin-precession with a lamp-pumped Cs-magnetometer. Additionally, an ultra-compact and transportable polarizer unit was developed and installed in Mainz, which polarizes {sup 3}He gas up to 55 % of polarization before the compressed gas is delivered to two sandwich magnetometer cells inside the EDM chamber. This theses will present some results of the first successful test of the polarizer unit in January 2012. {sup 3}He was polarized in the ultra compact polarizer unit and transferred via guiding fields into a 4 layer mu-metal shield, where the free spin precession was detected with a lamp pumped Cs-magnetometer.

Column-Oriented Database Systems (Tutorial)

NARCIS (Netherlands)

D. Abadi; P.A. Boncz (Peter); S. Harizopoulos

2009-01-01

textabstractColumn-oriented database systems (column-stores) have attracted a lot of attention in the past few years. Column-stores, in a nutshell, store each database table column separately, with attribute values belonging to the same column stored contiguously, compressed, and densely packed, as

A method for combining search coil and fluxgate magnetometer data to reveal finer structures in reconnection physics

Science.gov (United States)

Argall, M. R.; Caide, A.; Chen, L.; Torbert, R. B.

2012-12-01

Magnetometers have been used to measure terrestrial and extraterrestrial magnetic fields in space exploration ever since Sputnik 3. Modern space missions, such as Cluster, RBSP, and MMS incorporate both search coil magnetometers (SCMs) and fluxgate magnetometers (FGMs) in their instrument suites: FGMs work well at low frequencies while SCMs perform better at high frequencies. In analyzing the noise floor of these instruments, a cross-over region is apparent around 0.3-1.5Hz. The satellite separation of MMS and average speeds of field convection and plasma flows at the subsolar magnetopause make this a crucial range for the upcoming MMS mission. The method presented here combines the signals from SCM and FGM by taking a weighted average of both in this frequency range in order to draw out key features, such as narrow current sheet structures, that would otherwise not be visible. The technique is applied to burst mode Cluster data for reported magnetopause and magnetotail reconnection events to demonstrate the power of the combined data. This technique is also applied to data from the the EMFISIS instrument on the RBSP mission. The authors acknowledge and thank the FGM and STAFF team for the use of their data from the CLUSTER Active Archive.

Integrated induction coil and fluxgate magnetometers for EM analysis and monitoring

Science.gov (United States)

Hanstein, T.; Strack, K.; Jiang, J.

2013-12-01

The concept of a full field array electromagnetic system is an ideal tool to support hydrocarbon and geothermal E & P as well as various engineering monitoring applications. Some of the key questions are defining the reservoir, mapping of the fractures and reservoir depletion monitoring. The reservoirs are all too often relative thin and give an anomalous electromagnetic (EM) response, which is often small in amplitude and challenging for the EM measuring system. A digital fluxgate magnetometer (32-bit) is connected to the KMS magnetotelluric acquisition system with analogue induction coils and electrodes to extend the range of application of a single recording site. Since the noise level is above that of the induction coil for periods shorter than 20 s, the apparent resistivity is biased. For longer periods the apparent resistivity is consistent and eventually better than the induction coil. However, phase and tipper are not biased and agree well with the induction data even for shorter periods. This allows us to develop algorithms that significantly extend the range of application of the fluxgate beyond what was done in the past. The highest frequency of the fluxgate magnetometer is about 180 Hz and the hightest sampling of the FG-board is 4 kHz.The different induction coils and fluxgate magnetometer have intensively been tested in the magnetic chamber and at the field test site near Houston for noise performance by parallel recordings. They show that even in an environment with high cultural noise, the specification can be met. In Northeast China, a 30-day monitoring test with MT was carried out for seismologic applications. Acquisitition schedule included different recordings times and sampling rates. Daily, the data was collected and processed via the internet from either Europe or the US. Even with long recording, we still had to select the time windows for data averaging and coherences are not a good threshhold criteria in this case. During another MT

Magnetorelaxometry of magnetic nanoparticles with fluxgate magnetometers for the analysis of biological targets

International Nuclear Information System (INIS)

Ludwig, Frank; Heim, Erik; Maeuselein, Sascha; Eberbeck, Dietmar; Schilling, Meinhard

2005-01-01

A magnetorelaxometry system based on sensitive fluxgate magnetometers for the analysis of the relaxation behavior of magnetic nanoparticles is presented. The system is tested with a dilution series of magnetite. The results are directly compared with data obtained with a SQUID magnetorelaxometry system measured on the same samples. Advantages of using fluxgates rather than SQUIDs for magnetorelaxometry are discussed

Family of columns isospectral to gravity-loaded columns with tip force: A discrete approach

Science.gov (United States)

Ramachandran, Nirmal; Ganguli, Ranjan

2018-06-01

A discrete model is introduced to analyze transverse vibration of straight, clamped-free (CF) columns of variable cross-sectional geometry under the influence of gravity and a constant axial force at the tip. The discrete model is used to determine critical combinations of loading parameters - a gravity parameter and a tip force parameter - that cause onset of dynamic instability in the CF column. A methodology, based on matrix-factorization, is described to transform the discrete model into a family of models corresponding to weightless and unloaded clamped-free (WUCF) columns, each with a transverse vibration spectrum isospectral to the original model. Characteristics of models in this isospectral family are dependent on three transformation parameters. A procedure is discussed to convert the isospectral discrete model description into geometric description of realistic columns i.e. from the discrete model, we construct isospectral WUCF columns with rectangular cross-sections varying in width and depth. As part of numerical studies to demonstrate efficacy of techniques presented, frequency parameters of a uniform column and three types of tapered CF columns under different combinations of loading parameters are obtained from the discrete model. Critical combinations of these parameters for a typical tapered column are derived. These results match with published results. Example CF columns, under arbitrarily-chosen combinations of loading parameters are considered and for each combination, isospectral WUCF columns are constructed. Role of transformation parameters in determining characteristics of isospectral columns is discussed and optimum values are deduced. Natural frequencies of these WUCF columns computed using Finite Element Method (FEM) match well with those of the given gravity-loaded CF column with tip force, hence confirming isospectrality.

Poly(norepinephrine)-coated open tubular column for the separation of proteins and recombination human erythropoietin by capillary electrochromatography.

Science.gov (United States)

Xiao, Xue; Zhang, Yamin; Wu, Jia; Jia, Li

2017-12-01

Recombinant human erythropoietin is an important therapeutic protein with high economic interest due to the benefits provided by its clinical use for the treatment of anemias associated with chronic renal failure and chemotherapy. In this work, a poly(norepinephrine)-coated open tubular column was successfully prepared based on the self-polymerization of norepinephrine under mild alkaline condition, the favorable film forming and easy adhesive properties of poly(norepinephrine). The poly(norepinephrine) coating was characterized by scanning electron microscopy and measurement of the electro-osmotic flow. The thickness of the coating was about 431 nm. The electrochromatographic performance of the poly(norepinephrine)-coated open tubular column was evaluated by separation of proteins. Some basic and acidic proteins including two variants of bovine serum albumin and two variants of β-lactoglobulin achieved separation in the poly(norepinephrine)-coated open tubular column. More importantly, the column demonstrated separation ability for the glycoforms of recombinant human erythropoietin. In addition, the column demonstrated good repeatability with the run-to-run, day-to-day, and column-to-column relative standard deviations of migration times of proteins less than 3.40%. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Distillation Column Flooding Predictor

Energy Technology Data Exchange (ETDEWEB)

George E. Dzyacky

2010-11-23

The Flooding Predictor™ is a patented advanced control technology proven in research at the Separations Research Program, University of Texas at Austin, to increase distillation column throughput by over 6%, while also increasing energy efficiency by 10%. The research was conducted under a U. S. Department of Energy Cooperative Agreement awarded to George Dzyacky of 2ndpoint, LLC. The Flooding Predictor™ works by detecting the incipient flood point and controlling the column closer to its actual hydraulic limit than historical practices have allowed. Further, the technology uses existing column instrumentation, meaning no additional refining infrastructure is required. Refiners often push distillation columns to maximize throughput, improve separation, or simply to achieve day-to-day optimization. Attempting to achieve such operating objectives is a tricky undertaking that can result in flooding. Operators and advanced control strategies alike rely on the conventional use of delta-pressure instrumentation to approximate the column’s approach to flood. But column delta-pressure is more an inference of the column’s approach to flood than it is an actual measurement of it. As a consequence, delta pressure limits are established conservatively in order to operate in a regime where the column is never expected to flood. As a result, there is much “left on the table” when operating in such a regime, i.e. the capacity difference between controlling the column to an upper delta-pressure limit and controlling it to the actual hydraulic limit. The Flooding Predictor™, an innovative pattern recognition technology, controls columns at their actual hydraulic limit, which research shows leads to a throughput increase of over 6%. Controlling closer to the hydraulic limit also permits operation in a sweet spot of increased energy-efficiency. In this region of increased column loading, the Flooding Predictor is able to exploit the benefits of higher liquid

Annular pulse column development studies

International Nuclear Information System (INIS)

Benedict, G.E.

1980-01-01

The capacity of critically safe cylindrical pulse columns limits the size of nuclear fuel solvent extraction plants because of the limited cross-sectional area of plutonium, U-235, or U-233 processing columns. Thus, there is a need to increase the cross-sectional area of these columns. This can be accomplished through the use of a column having an annular cross section. The preliminary testing of a pilot-plant-scale annular column has been completed and is reported herein. The column is made from 152.4-mm (6-in.) glass pipe sections with an 89-mm (3.5-in.) o.d. internal tube, giving an annular width of 32-mm (1.25-in.). Louver plates are used to swirl the column contents to prevent channeling of the phases. The data from this testing indicate that this approach can successfully provide larger-cross-section critically safe pulse columns. While the capacity is only 70% of that of a cylindrical column of similar cross section, the efficiency is almost identical to that of a cylindrical column. No evidence was seen of any non-uniform pulsing action from one side of the column to the other

Column ratio mapping: a processing technique for atomic resolution high-angle annular dark-field (HAADF) images.

Science.gov (United States)

Robb, Paul D; Craven, Alan J

2008-12-01

An image processing technique is presented for atomic resolution high-angle annular dark-field (HAADF) images that have been acquired using scanning transmission electron microscopy (STEM). This technique is termed column ratio mapping and involves the automated process of measuring atomic column intensity ratios in high-resolution HAADF images. This technique was developed to provide a fuller analysis of HAADF images than the usual method of drawing single intensity line profiles across a few areas of interest. For instance, column ratio mapping reveals the compositional distribution across the whole HAADF image and allows a statistical analysis and an estimation of errors. This has proven to be a very valuable technique as it can provide a more detailed assessment of the sharpness of interfacial structures from HAADF images. The technique of column ratio mapping is described in terms of a [110]-oriented zinc-blende structured AlAs/GaAs superlattice using the 1 angstroms-scale resolution capability of the aberration-corrected SuperSTEM 1 instrument.

Column ratio mapping: A processing technique for atomic resolution high-angle annular dark-field (HAADF) images

International Nuclear Information System (INIS)

Robb, Paul D.; Craven, Alan J.

2008-01-01

An image processing technique is presented for atomic resolution high-angle annular dark-field (HAADF) images that have been acquired using scanning transmission electron microscopy (STEM). This technique is termed column ratio mapping and involves the automated process of measuring atomic column intensity ratios in high-resolution HAADF images. This technique was developed to provide a fuller analysis of HAADF images than the usual method of drawing single intensity line profiles across a few areas of interest. For instance, column ratio mapping reveals the compositional distribution across the whole HAADF image and allows a statistical analysis and an estimation of errors. This has proven to be a very valuable technique as it can provide a more detailed assessment of the sharpness of interfacial structures from HAADF images. The technique of column ratio mapping is described in terms of a [1 1 0]-oriented zinc-blende structured AlAs/GaAs superlattice using the 1 A-scale resolution capability of the aberration-corrected SuperSTEM 1 instrument.

Column-Oriented Database Systems (Tutorial)

OpenAIRE

Abadi, D.; Boncz, Peter; Harizopoulos, S.

2009-01-01

textabstractColumn-oriented database systems (column-stores) have attracted a lot of attention in the past few years. Column-stores, in a nutshell, store each database table column separately, with attribute values belonging to the same column stored contiguously, compressed, and densely packed, as opposed to traditional database systems that store entire records (rows) one after the other. Reading a subset of a table’s columns becomes faster, at the potential expense of excessive disk-head s...

Nuclear reactor control column

International Nuclear Information System (INIS)

Bachovchin, D.M.

1982-01-01

The nuclear reactor control column comprises a column disposed within the nuclear reactor core having a variable cross-section hollow channel and containing balls whose vertical location is determined by the flow of the reactor coolant through the column. The control column is divided into three basic sections wherein each of the sections has a different cross-sectional area. The uppermost section of the control column has the greatest crosssectional area, the intermediate section of the control column has the smallest cross-sectional area, and the lowermost section of the control column has the intermediate cross-sectional area. In this manner, the area of the uppermost section can be established such that when the reactor coolant is flowing under normal conditions therethrough, the absorber balls will be lifted and suspended in a fluidized bed manner in the upper section. However, when the reactor coolant flow falls below a predetermined value, the absorber balls will fall through the intermediate section and into the lowermost section, thereby reducing the reactivity of the reactor core and shutting down the reactor

Column Selection for Biomedical Analysis Supported by Column Classification Based on Four Test Parameters.

Science.gov (United States)

Plenis, Alina; Rekowska, Natalia; Bączek, Tomasz

2016-01-21

This article focuses on correlating the column classification obtained from the method created at the Katholieke Universiteit Leuven (KUL), with the chromatographic resolution attained in biomedical separation. In the KUL system, each column is described with four parameters, which enables estimation of the FKUL value characterising similarity of those parameters to the selected reference stationary phase. Thus, a ranking list based on the FKUL value can be calculated for the chosen reference column, then correlated with the results of the column performance test. In this study, the column performance test was based on analysis of moclobemide and its two metabolites in human plasma by liquid chromatography (LC), using 18 columns. The comparative study was performed using traditional correlation of the FKUL values with the retention parameters of the analytes describing the column performance test. In order to deepen the comparative assessment of both data sets, factor analysis (FA) was also used. The obtained results indicated that the stationary phase classes, closely related according to the KUL method, yielded comparable separation for the target substances. Therefore, the column ranking system based on the FKUL-values could be considered supportive in the choice of the appropriate column for biomedical analysis.

Improvements in solvent extraction columns

International Nuclear Information System (INIS)

Aughwane, K.R.

1987-01-01

Solvent extraction columns are used in the reprocessing of irradiated nuclear fuel. For an effective reprocessing operation a solvent extraction column is required which is capable of distributing the feed over most of the column. The patent describes improvements in solvent extractions columns which allows the feed to be distributed over an increased length of column than was previously possible. (U.K.)

Preparation and evaluation of a novel hybrid monolithic column based on pentafluorobenzyl imidazolium bromide ionic liquid.

Science.gov (United States)

Shan, Yuanhong; Qiao, Lizhen; Shi, Xianzhe; Xu, Guowang

2015-01-02

To develop a novel hybrid monolithic column based on pentafluorobenzyl imidazolium bromide ionic liquid, a new ionic liquid monomer was synthesized from 1-vinylimidazole and pentafluorobenzyl bromide. By employing a facile one-step copolymerization of polyhedral-oligomeric-silsesquioxane-type (POSS) cross-linking agent and the home-made ionic liquid monomer, the hybrid monolithic columns were in situ fabricated in fused-silica capillary. The morphology of monolithic column was characterized by scanning electron microscope (SEM) and the chemical composition was confirmed by Fourier-transform infrared spectroscopy (FT-IR) and elemental analysis. Excellent mechanical stability and slight swelling propensity were exhibited which was ascribed to the rigid hybrid monolithic skeleton. Reproducibility results of run-to-run, column-to-column, batch-to-batch and day-to-day were investigated and the RSDs were less than 0.46%, 1.84%, 3.96% and 3.17%, respectively. The mixed-mode retention mechanism with hydrophobic interaction, π-π stacking, ion-exchange, electrostatic interaction and dipole-dipole interaction was explored systematically using analytes with different structure types. Satisfied separation capability and column efficiency were achieved for the analysis of small molecular compounds such as alkylbenzenes, polycyclic aromatic hydrocarbons, nucleosides and halogenated compounds. Copyright © 2014 Elsevier B.V. All rights reserved.

Coupled-core fluxgate magnetometer: Novel configuration scheme and the effects of a noise-contaminated external signal

International Nuclear Information System (INIS)

Palacios, Antonio; Aven, John; In, Visarath; Longhini, Patrick; Kho, Andy; Neff, Joseph D.; Bulsara, Adi

2007-01-01

Recent theoretical and experimental work has shown that unidirectional coupling can induce oscillations in overdamped and undriven nonlinear dynamical systems that are non-oscillatory when uncoupled; in turn, this has been shown to lead to new mechanisms for weak (compared to the energy barrier height) signal detection and amplification. The potential applications include fluxgate magnetometers, electric field sensors, and arrays of Superconducting Quantum Interference Device (SQUID) rings. In the particular case of the fluxgate magnetometer, we have developed a ''coupled-core fluxgate magnetometer'' (CCFM); this device has been realized in the laboratory and its dynamics used to quantify many properties that are generic to this class of systems and coupling. The CCFM operation is underpinned by the emergent oscillatory behavior in a unidirectionally coupled ring of wound ferromagnetic cores, each of which can be treated as an overdamped bistable dynamic system when uncoupled. In particular, one can determine the regimes of existence and stability of the (coupling-induced) oscillations, and the scaling behavior of the oscillation frequency. More recently, we studied the effects of a (Gaussian) magnetic noise floor on a CCFM system realized with N=3 coupled ferromagnetic cores. In this Letter, we first introduce a variation on the basic CCFM configuration that affords a path to enhanced device sensitivity, particularly for N>=3 coupled elements. We then analyze the response of the basic CCFM configuration as well as the new setup to a dc target signal that has a small noisy component (or ''contamination'')

( Anogeissus leiocarpus ) timber columns

African Journals Online (AJOL)

A procedure for designing axially loaded Ayin (Anogeissus leiocarpus) wood column or strut has been investigated. Instead of the usual categorization of columns into short, intermediate and slender according to the value of slenderness ratio, a continuous column formula representing the three categories was derived.

Calibration of Helmholtz Coils for the characterization of MEMS magnetic sensor using fluxgate magnetometer with DAS1 magnetic range data acquisition system

Science.gov (United States)

Ahmad, Farooq; Dennis, John Ojur; Md Khir, Mohd Haris; Hamid, Nor Hisham

2012-09-01

This paper presents the calibration of Helmholtz coils for the characterization of MEMS Magnetic sensor using Fluxgate magnetometer with DAS1 Magnetic Range Data Acquisition System. The Helmholtz coils arrangement is often used to generate a uniform magnetic field in space. In the past, standard magnets were used to calibrate the Helmholtz coils. A method is presented here for calibrating these coils using a Fluxgate magnetometer and known current source, which is easier and results in greater accuracy.

LIQUID-LIQUID EXTRACTION COLUMNS

Science.gov (United States)

Thornton, J.D.

1957-12-31

This patent relates to liquid-liquid extraction columns having a means for pulsing the liquid in the column to give it an oscillatory up and down movement, and consists of a packed column, an inlet pipe for the dispersed liquid phase and an outlet pipe for the continuous liquid phase located in the direct communication with the liquid in the lower part of said column, an inlet pipe for the continuous liquid phase and an outlet pipe for the dispersed liquid phase located in direct communication with the liquid in the upper part of said column, a tube having one end communicating with liquid in the lower part of said column and having its upper end located above the level of said outlet pipe for the dispersed phase, and a piston and cylinder connected to the upper end of said tube for applying a pulsating pneumatic pressure to the surface of the liquid in said tube so that said surface rises and falls in said tube.

Miniaturized Laser Heterodyne Radiometer for Measurements of CO2 in the Atmospheric Column

Science.gov (United States)

Wilson, E. L.; Mclinden, M. L.; Miller, J. H.; Allan, G. R.; Lott, L. E.; Melroy, H. R.; Clarke, G. B.

2013-01-01

We have developed a low-cost, miniaturized laser heterodyne radiometer for highly sensitive measurements of carbon dioxide (CO2) in the atmospheric column. In this passive design, sunlight that has undergone absorption by CO2 in the atmosphere is collected and mixed with continuous wave laser light that is step-scanned across the absorption feature centered at 1,573.6 nm. The resulting radio frequency beat signal is collected as a function of laser wavelength, from which the total column mole fraction can be de-convolved. We are expanding this technique to include methane (CH4) and carbon monoxide (CO), and with minor modifications, this technique can be expanded to include species such as water vapor (H2O) and nitrous oxide (N2O).

Synthesis of focusing-and-deflection columns

International Nuclear Information System (INIS)

Szilagyi, M.; Mui, P.H.

1995-01-01

Szilagyi and Szep have demonstrated that focusing lenses of high performances can be constructed from a column of circular plate electrodes. Later, Szilagyi modified that system to include dipole, quadrupole, and octupole components by partitioning each plate into eight equal sectors. It has already been shown that the additional quadrupole components can indeed bring about substantial improvements in the focusing of charged particle beams. In this article, that design procedure is expanded to construct columns capable of both focusing and deflecting particle beams by just introducing additional dipole components. In this new design, the geometry of the system remains unchanged. The only extra complication is the demand for more individual controls of the sector voltages. Two sample designs, one for negative ions and one for electrons, are presented showing that in both cases a ±2.3 mrad diverging beam can be focused down to a spot of less than 50 nm in radius over a scanning circular area of radius 0.25 mm. The details of the two systems are given in Sec. IV along with the source conditions. The performance of the negative ion system is found to be comparable to the published data. For the relativistic electron system, the interaction of individual components to reduce various aberrations is investigated. copyright 1995 American Vacuum Society

Scalability of pre-packed preparative chromatography columns with different diameters and lengths taking into account extra column effects.

Science.gov (United States)

Schweiger, Susanne; Jungbauer, Alois

2018-02-16

Small pre-packed columns are commonly used to estimate the optimum run parameters for pilot and production scale. The question arises if the experiments obtained with these columns are scalable, because there are substantial changes in extra column volume when going from a very small scale to a benchtop column. In this study we demonstrate the scalability of pre-packed disposable and non-disposable columns of volumes in the range of 0.2-20 ml packed with various media using superficial velocities in the range of 30-500 cm/h. We found that the relative contribution of extra column band broadening to total band broadening was not only high for columns with small diameters, but also for columns with a larger volume due to their wider diameter. The extra column band broadening can be more than 50% for columns with volumes larger than 10 ml. An increase in column diameter leads to high additional extra column band broadening in the filter, frits, and adapters of the columns. We found a linear relationship between intra column band broadening and column length, which increased stepwise with increases in column diameter. This effect was also corroborated by CFD simulation. The intra column band broadening was the same for columns packed with different media. An empirical engineering equation and the data gained from the extra column effects allowed us to predict the intra, extra, and total column band broadening just from column length, diameter, and flow rate. Copyright © 2018 The Author(s). Published by Elsevier B.V. All rights reserved.

Rapid determination of 18 glucocorticoids in serum using reusable on-line SPE polymeric monolithic column coupled with LC-quadrupole/orbitrap high-resolution mass spectrometer.

Science.gov (United States)

Li, Hui; Ai, Lianfeng; Fan, Sufang; Wang, Yan; Sun, Dianxing

2017-10-15

A simple, rapid and sensitive method for the simultaneous determination of 18 glucocorticoids in serum was developed by coupling on-line solid-phase extraction (SPE) polymeric monolithic column to a liquid chromatography-quadrupole/orbitrap high-resolution mass spectrometer. A simple poly(ethylene glycol dimethacrylate) monolith column (10mm×2.1mm i.d.) was fabricated, and the morphology, surface area and extraction performance of the monolithic column were characterized. Serum samples were extracted by acetonitrile (ACN). Then, online SPE was achieved on the synthesized monolithic column using a 10mmol/L ammonium acetate solution as the loading solvent. After the transfer from the monolith into analytical column (Capcell Pak ADME column) using ACN, the adsorbed analytes were separated on the analytical column and detected with a high-resolution hybrid quadrupole/orbitrap mass spectrometer with full scan/ddMS 2 scan mode Under optimized conditions, the method was linear with target linear correlation coefficient (R 2 ) higher than 0.995. Detection limits were in range of 0.1-0.6ng/mL, and the quantification limits were 0.3-1.5ng/mL. The recovery was between 71.9% and 89.2% in three spike levels with precision (n=5) of 5.40-12.1%. The serum sample was directly analyzed after a simple extraction procedure, and the on-line SPE and determination were achieved within only 16min. The method was used to analyze the dynamic contents variation of cortisone and hydrocortisone in serum before and after the surgery. Copyright © 2017 Elsevier B.V. All rights reserved.

Geospace Science from Ground-based Magnetometer Arrays: Advances in Sensors, Data Collection, and Data Integration

Science.gov (United States)

Mann, Ian; Chi, Peter

2016-07-01

Networks of ground-based magnetometers now provide the basis for the diagnosis of magnetic disturbances associated with solar wind-magnetosphere-ionosphere coupling on a truly global scale. Advances in sensor and digitisation technologies offer increases in sensitivity in fluxgate, induction coil, and new micro-sensor technologies - including the promise of hybrid sensors. Similarly, advances in remote connectivity provide the capacity for truly real-time monitoring of global dynamics at cadences sufficient for monitoring and in many cases resolving system level spatio-temporal ambiguities especially in combination with conjugate satellite measurements. A wide variety of the plasmaphysical processes active in driving geospace dynamics can be monitored based on the response of the electrical current system, including those associated with changes in global convection, magnetospheric substorms and nightside tail flows, as well as due to solar wind changes in both dynamic pressure and in response to rotations of the direction of the IMF. Significantly, any changes to the dynamical system must be communicated by the propagation of long-period Alfven and/or compressional waves. These wave populations hence provide diagnostics for not only the energy transport by the wave fields themselves, but also provide a mechanism for diagnosing the structure of the background plasma medium through which the waves propagate. Ultra-low frequency (ULF) waves are especially significant in offering a monitor for mass density profiles, often invisible to particle detectors because of their very low energy, through the application of a variety of magneto-seismology and cross-phase techniques. Renewed scientific interest in the plasma waves associated with near-Earth substorm dynamics, including magnetosphere-ionosphere coupling at substorm onset and their relation to magnetotail flows, as well the importance of global scale ultra-low frequency waves for the energisation, transport

Development of Next-Generation Borehole Magnetometer and Its Potential Application in Constraining the Magnetic Declination of Oman Samail Ophiolite at ICDP Drill Sites

Science.gov (United States)

Lee, S. M.; Parq, J. H.; Kim, H.; Moe, K.; Lee, C. S.; Kanamatsu, T.; Kim, K. J.; Bahk, K. S.

2017-12-01

Determining the azimuthal orientation of core samples obtained from deep drilling is extremely difficult because the core itself could have rotated during drilling operations. Several indirect methods have been devised to address this issue, but have certain limitations. Thus it is still a challenge to determine the azimuthal orientation consistently over the entire length of the hole. Provided that the recovery rate is high and thus all the other magnetic properties such as magnetization intensity and inclination are measured from the recovered cores, one possible method for ascertaining magnetic declination information is to measure the magnetic field inside the empty borehole and invert for the best fitting declination. However, there are two major problems: one is that present-day borehole magnetometers are not precise enough to resolve changes in direction of magnetization, and the other is that in most rock drilling experiments the rate of recovery is low. To overcome the first major problem which is technical, scientists from Korea and Japan jointly conducted the development for the next-generation borehole magnetometer, namely 3GBM (3rd Generation Borehole Magnetometer). The borehole magnetometer which uses fiber-optic laser gyro promises to provide accurate information on not only the magnetic field itself but also the orientation of the instrument inside the borehole. Our goal is to deploy this borehole magnetometer in the ICDP Oman Drilling Project Phase 2 drilling experiment early 2018. The site may be suitable for the investigation because, as recent Phase 1 of the Oman Samail Ophiolite drilling has demonstrated, the recovery rate was very high. Also the post-drilling measurements onboard DV Chikyu have shown that much of the recovered samples has moderate magnetization intensity on the order of 0.1 and 1 A/m. Here, we present the results of numerical simulation of magnetic field inside the borehole using finite element method to show that magnetic

Thermodynamics of a closed-cycle gas flow system for cooling a HTc dc-SQUID magnetometer

NARCIS (Netherlands)

van den Bosch, P.J.; van den Bosch, P.J.; ter Brake, Hermanus J.M.; van den Eijkel, G.C.; Boelens, J.P.; Holland, Herman J.; Verberne, J.F.C.; Rogalla, Horst

1994-01-01

A multichannel high-Tc dc-SQUID based heart-magnetometer is currently under development in our laboratory. The system is cooled by a cooler that, due to its magnetic interference, has to be separated from the SQUID unit. In the present prototype system a closed-cycle gas flow was chosen as the

Ultrasensitive magnetometers based on rotational magnetic excitation

International Nuclear Information System (INIS)

Hristoforou, E.; Svec, P. Sr.

2014-01-01

Three new types of fluxgate magnetometers are presented in this paper, able to monitor the three components of the ambient field, all of them based on the principle of rotational excitation field. The first type is based on Yttrium- Iron Garnet (YIG) single crystal film, magnetized with rotational field on its plane, where the 2"n"d, 4"t"h and 6"t"h harmonics offer the three components of the ambient field with sensitivity better than 1 pT at 0.2 Hz, its size being 25 cm"3. The second type is based on permalloy film, where the rotational excitation field on its plane offers change of magnetoresistance with sensitivity better than 10 pT at 1 Hz, uncertainty of 1 ppm and size ∼ 8 cm"3. The third type, is based on amorphous film, where the rotation field mode offer sensitivity better than 100 pT at 1 Hz, uncertainty of 10 ppm and size ∼ 10 mm"3. (authors)

Hall probe magnetometer for SSC magnet cables

International Nuclear Information System (INIS)

Cross, R.W.; Goldfarb, R.B.

1991-01-01

The authors of this paper constructed a Hall probe magnetometer to measure the magnetization hysteresis loops of Superconducting Super Collider magnet cables. The instrument uses two Hall-effect field sensors to measure the applied field H and the magnetic induction B. Magnetization M is calculated from the difference of the two quantities. The Hall probes are centered coaxially in the bore of a superconducting solenoid with the B probe against the sample's broad surface. An alternative probe arrangement, in which M is measured directly, aligns the sample probe parallel to the field. The authors measured M as a function of H and field cycle rate both with and without a dc transport current. Flux creep as a function of current was measured from the dependence of ac loss on the cycling rate and from the decay of magnetization with time. Transport currents up to 20% of the critical current have minimal effect on magnetization and flux creep

Magnetometer-Augmented IMU Simulator: In-Depth Elaboration

Directory of Open Access Journals (Sweden)

Thomas Brunner

2015-03-01

Full Text Available The location of objects is a growing research topic due, for instance, to the expansion of civil drones or intelligent vehicles. This expansion was made possible through the development of microelectromechanical systems (MEMS, inexpensive and miniaturized inertial sensors. In this context, this article describes the development of a new simulator which generates sensor measurements, giving a specific input trajectory. This will allow the comparison of pose estimation algorithms. To develop this simulator, the measurement equations of every type of sensor have to be analytically determined. To achieve this objective, classical kinematic equations are used for the more common sensors, i.e., accelerometers and rate gyroscopes. As nowadays, the MEMS inertial measurement units (IMUs are generally magnetometer-augmented, an absolute world magnetic model is implemented. After the determination of the perfect measurement (through the error-free sensor models, realistic error models are developed to simulate real IMU behavior. Finally, the developed simulator is subjected to different validation tests.

Development of Autonomous Magnetometer Rotorcraft For Wide Area Assessment

Energy Technology Data Exchange (ETDEWEB)

Mark D. McKay; Matthew O. Anderson

2011-08-01

Large areas across the United States and internationally are potentially contaminated with unexploded ordinance (UXO), with some ranges encompassing tens to hundreds of thousands of acres. Technologies are needed which will allow for cost effective wide area scanning with (1) near 100% coverage and (2) near 100% detection of subsurface ordnance or features indicative of subsurface ordnance. The current approach to wide area assessment is a multi-level one, in which medium - altitude fixed wing optical imaging is used for an initial site assessment. This assessment is followed with low altitude manned helicopter based magnetometry. Subsequent to this wide area assessment targeted surface investigations are performed using either towed geophysical sensor arrays or man portable sensors. In order to be an effective tool for small UXO detection, the sensing altitude for magnetic site investigations needs to be on the order of 1 to 3 meters. These altitude requirements mean that manned helicopter surveys will generally only be feasible in large, open and relatively flat terrains. While such surveys are effective in mapping large areas relatively fast there are substantial mobilization/demobilization, staffing and equipment costs associated with these surveys, resulting in costs of approximately $100-$150/acre. In addition, due to the low altitude there are substantial risks to pilots and equipment. Surface towed arrays provide highresolution maps but have other limitations, e.g. in their ability to navigate rough terrain effectively. Thus there is a need for other systems, which can be used for effective data collection. An Unmanned Aerial Vehicle (UAV) magnetometer platform is an obvious alternative. The motivation behind such a system is that it reduces risk to operators, is lower in initial and Operational and Maintenance (O&M) costs (and can thus potentially be applied to smaller sites) and has the potential of being more effective in terms of detection and possibly

Coupled-core fluxgate magnetometer: Novel configuration scheme and the effects of a noise-contaminated external signal

Energy Technology Data Exchange (ETDEWEB)

Palacios, Antonio [San Diego State University, Nonlinear Dynamical Systems Group, Department of Mathematics and Statistics, San Diego, CA 92182-7720 (United States)]. E-mail: palacios@euler.sdsu.edu; Aven, John [San Diego State University, Nonlinear Dynamical Systems Group, Department of Mathematics and Statistics, San Diego, CA 92182-7720 (United States); In, Visarath [Space and Naval Warfare Systems Center San Diego, Code 2363, 53560 Hull St, San Diego, CA 92152-5001 (United States)]. E-mail: visarath@spawar.navy.mil; Longhini, Patrick [Space and Naval Warfare Systems Center San Diego, Code 2363, 53560 Hull St, San Diego, CA 92152-5001 (United States); Kho, Andy [Space and Naval Warfare Systems Center San Diego, Code 2363, 53560 Hull St, San Diego, CA 92152-5001 (United States); Neff, Joseph D. [Space and Naval Warfare Systems Center San Diego, Code 2363, 53560 Hull St, San Diego, CA 92152-5001 (United States); Bulsara, Adi [Space and Naval Warfare Systems Center San Diego, Code 2363, 53560 Hull St, San Diego, CA 92152-5001 (United States)]. E-mail: bulsara@spawar.navy.mil

2007-07-16

Recent theoretical and experimental work has shown that unidirectional coupling can induce oscillations in overdamped and undriven nonlinear dynamical systems that are non-oscillatory when uncoupled; in turn, this has been shown to lead to new mechanisms for weak (compared to the energy barrier height) signal detection and amplification. The potential applications include fluxgate magnetometers, electric field sensors, and arrays of Superconducting Quantum Interference Device (SQUID) rings. In the particular case of the fluxgate magnetometer, we have developed a ''coupled-core fluxgate magnetometer'' (CCFM); this device has been realized in the laboratory and its dynamics used to quantify many properties that are generic to this class of systems and coupling. The CCFM operation is underpinned by the emergent oscillatory behavior in a unidirectionally coupled ring of wound ferromagnetic cores, each of which can be treated as an overdamped bistable dynamic system when uncoupled. In particular, one can determine the regimes of existence and stability of the (coupling-induced) oscillations, and the scaling behavior of the oscillation frequency. More recently, we studied the effects of a (Gaussian) magnetic noise floor on a CCFM system realized with N=3 coupled ferromagnetic cores. In this Letter, we first introduce a variation on the basic CCFM configuration that affords a path to enhanced device sensitivity, particularly for N>=3 coupled elements. We then analyze the response of the basic CCFM configuration as well as the new setup to a dc target signal that has a small noisy component (or ''contamination'')

Optimization and simulation of tandem column supercritical fluid chromatography separations using column back pressure as a unique parameter.

Science.gov (United States)

Wang, Chunlei; Tymiak, Adrienne A; Zhang, Yingru

2014-04-15

Tandem column supercritical fluid chromatography (SFC) has demonstrated to be a useful technique to resolve complex mixtures by serially coupling two columns of different selectivity. The overall selectivity of a tandem column separation is the retention time weighted average of selectivity from each coupled column. Currently, the method development merely relies on extensive screenings and is often a hit-or-miss process. No attention is paid to independently adjust retention and selectivity contributions from individual columns. In this study, we show how tandem column SFC selectivity can be optimized by changing relative dimensions (length or inner diameter) of the coupled columns. Moreover, we apply column back pressure as a unique parameter for SFC optimization. Continuous tuning of tandem column SFC selectivity is illustrated through column back pressure adjustments of the upstream column, for the first time. In addition, we show how and why changing coupling order of the columns can produce dramatically different separations. Using the empirical mathematical equation derived in our previous study, we also demonstrate a simulation of tandem column separations based on a single retention time measurement on each column. The simulation compares well with experimental results and correctly predicts column order and back pressure effects on the separations. Finally, considerations on instrument and column hardware requirements are discussed.

Note: Readout of a micromechanical magnetometer for the ITER fusion reactor

International Nuclear Information System (INIS)

Rimminen, H.; Kyynäräinen, J.

2013-01-01

We present readout instrumentation for a MEMS magnetometer, placed 30 m away from the MEMS element. This is particularly useful when sensing is performed in high-radiation environment, where the semiconductors in the readout cannot survive. High bandwidth transimpedance amplifiers are used to cancel the cable capacitances of several nanofarads. A frequency doubling readout scheme is used for crosstalk elimination. Signal-to-noise ratio in the range of 60 dB was achieved and with sub-percent nonlinearity. The presented instrument is intended for the steady-state magnetic field measurements in the ITER fusion reactor.

Gas Chromatograph Method Optimization Trade Study for RESOLVE: 20-meter Column v. 8-meter Column

Science.gov (United States)

Huz, Kateryna

2014-01-01

RESOLVE is the payload on a Class D mission, Resource Prospector, which will prospect for water and other volatile resources at a lunar pole. The RESOLVE payload's primary scientific purpose includes determining the presence of water on the moon in the lunar regolith. In order to detect the water, a gas chromatograph (GC) will be used in conjunction with a mass spectrometer (MS). The goal of the experiment was to compare two GC column lengths and recommend which would be best for RESOLVE's purposes. Throughout the experiment, an Inficon Fusion GC and an Inficon Micro GC 3000 were used. The Fusion had a 20m long column with 0.25mm internal diameter (Id). The Micro GC 3000 had an 8m long column with a 0.32mm Id. By varying the column temperature and column pressure while holding all other parameters constant, the ideal conditions for testing with each column length in their individual instrument configurations were determined. The criteria used for determining the optimal method parameters included (in no particular order) (1) quickest run time, (2) peak sharpness, and (3) peak separation. After testing numerous combinations of temperature and pressure, the parameters for each column length that resulted in the most optimal data given my three criteria were selected. The ideal temperature and pressure for the 20m column were 95 C and 50psig. At this temperature and pressure, the peaks were separated and the retention times were shorter compared to other combinations. The Inficon Micro GC 3000 operated better at lower temperature mainly due to the shorter 8m column. The optimal column temperature and pressure were 70 C and 30psig. The Inficon Micro GC 3000 8m column had worse separation than the Inficon Fusion 20m column, but was able to separate water within a shorter run time. Therefore, the most significant tradeoff between the two column lengths was peak separation of the sample versus run time. After performing several tests, it was concluded that better

Small Column Ion Exchange

International Nuclear Information System (INIS)

Huff, Thomas

2010-01-01

Small Column Ion Exchange (SCIX) leverages a suite of technologies developed by DOE across the complex to achieve lifecycle savings. Technologies are applicable to multiple sites. Early testing supported multiple sites. Balance of SRS SCIX testing supports SRS deployment. A forma Systems Engineering Evaluation (SEE) was performed and selected Small Column Ion Exchange columns containing Crystalline Silicotitanate (CST) in a 2-column lead/lag configuration. SEE considered use of Spherical Resorcinol-Formaldehyde (sRF). Advantages of approach at SRS include: (1) no new buildings, (2) low volume of Cs waste in solid form compared to aqueous strip effluent; and availability of downstream processing facilities for immediate processing of spent resin.

Mass transfer model liquid phase catalytic exchange column simulation applicable to any column composition profile

Energy Technology Data Exchange (ETDEWEB)

Busigin, A. [NITEK USA Inc., Ocala, FL (United States)

2015-03-15

Liquid Phase Catalytic Exchange (LPCE) is a key technology used in water detritiation systems. Rigorous simulation of LPCE is complicated when a column may have both hydrogen and deuterium present in significant concentrations in different sections of the column. This paper presents a general mass transfer model for a homogenous packed bed LPCE column as a set of differential equations describing composition change, and equilibrium equations to define the mass transfer driving force within the column. The model is used to show the effect of deuterium buildup in the bottom of an LPCE column from non-negligible D atom fraction in the bottom feed gas to the column. These types of calculations are important in the design of CECE (Combined Electrolysis and Catalytic Exchange) water detritiation systems.

A three-axis SQUID-based absolute vector magnetometer

Energy Technology Data Exchange (ETDEWEB)

Schönau, T.; Schmelz, M.; Stolz, R.; Anders, S.; Linzen, S.; Meyer, H.-G. [Department of Quantum Detection, Leibniz Institute of Photonic Technology, Jena 07745 (Germany); Zakosarenko, V.; Meyer, M. [Supracon AG, An der Lehmgrube 11, Jena 07751 (Germany)

2015-10-15

We report on the development of a three-axis absolute vector magnetometer suited for mobile operation in the Earth’s magnetic field. It is based on low critical temperature dc superconducting quantum interference devices (LTS dc SQUIDs) with sub-micrometer sized cross-type Josephson junctions and exhibits a white noise level of about 10 fT/Hz{sup 1/2}. The width of superconducting strip lines is restricted to less than 6 μm in order to avoid flux trapping during cool-down in magnetically unshielded environment. The long-term stability of the flux-to-voltage transfer coefficients of the SQUID electronics is investigated in detail and a method is presented to significantly increase their reproducibility. We further demonstrate the long-term operation of the setup in a magnetic field varying by about 200 μT amplitude without the need for recalibration.

Hypervelocity dust particle impacts observed by the Giotto Magnetometer and Plasma Experiments

OpenAIRE

Neubauer, F. M.; Glassmeier, K. H.; Coates, A. J.; Goldstein, R.; Acuña, M. H.; Musmann, G.

1990-01-01

We report thirteen very short events in the magnetic field of the inner magnetic pile‐up region of comet Halley observed by the Giotto magnetometer experiment together with simultaneous plasma data obtained by the Johnstone plasma analyzer and the ion mass spectrometer experiments. The events are due to dust impacts in the milligram range on the spacecraft at the relative velocity between the cemetery dust and the spacecraft of 68 km/sec. They are generally consistent with dust impact events ...

Fractionation separation of human plasma proteins using HPLC with a homemade iron porphyrin based monolithic column.

Science.gov (United States)

Zhang, Doudou; Zhao, Yu; Lan, Dandan; Pang, Xiaomin; Bai, Ligai; Liu, Haiyan; Yan, Hongyuan

2017-11-15

In this work a polymer monolithic column was fabricated within the confines of a stainless steel column (50×4.6mm i.d.) via radical polymerization by using iron porphyrin and butyl methacrylate as co-monomers, ethylene glycol dimethacrylate as crosslinking agent, ethylene glycol, isopropyl alcohol and N, N-dimethylformamide as tri-porogens, benzoyl peroxide and N,N-dimethylaniline as initiators. The resulting monolithic column was characterized by elemental analysis, scanning electron microscopy, nitrogen adsorption BET surface area, and mercury intrusion porosimetry, respectively. Results showed that the homemade monolith occupied relatively uniform pore structure, low back pressure, and enhanced selectivity for proteins in complex bio-samples. The present work described a simple and efficient method for "fractionation separation" of human plasma proteins, and it is a promising separation method for complex bio-samples in proteomic research. Copyright © 2017 Elsevier B.V. All rights reserved.

Associating ground magnetometer observations with current or voltage generators

DEFF Research Database (Denmark)

Hartinger, M. D.; Xu, Z.; Clauer, C. R.

2017-01-01

A circuit analogy for magnetosphere-ionosphere current systems has two extremes for driversof ionospheric currents: ionospheric elec tric fields/voltages constant while current/conductivity vary—the“voltage generator”—and current constant while electric field/conductivity vary—the “current generator.......”Statistical studies of ground magnetometer observations associated with dayside Transient High LatitudeCurrent Systems (THLCS) driven by similar mechanisms find contradictory results using this paradigm:some studies associate THLCS with voltage generators, others with current generators. We argue that mostof...... these two assumptions substantially alter expectations for magnetic perturbations associatedwith either a current or a voltage generator. Our results demonstrate that before interpreting groundmagnetometer observations of THLCS in the context of current/voltage generators, the location...

Magnetic profiling of the San Andreas Fault using a dual magnetometer UAV aerial survey system.

Science.gov (United States)

Abbate, J. A.; Angelopoulos, V.; Masongsong, E. V.; Yang, J.; Medina, H. R.; Moon, S.; Davis, P. M.

2017-12-01

Aeromagnetic survey methods using planes are more time-effective than hand-held methods, but can be far more expensive per unit area unless large areas are covered. The availability of low cost UAVs and low cost, lightweight fluxgate magnetometers (FGMs) allows, with proper offset determination and stray fields correction, for low-cost magnetic surveys. Towards that end, we have developed a custom multicopter UAV for magnetic mapping using a dual 3-axis fluxgate magnetometer system: the GEOphysical Drone Enhanced Survey Instrument (GEODESI). A high precision sensor measures the UAV's position and attitude (roll, pitch, and yaw) and is recorded using a custom Arduino data processing system. The two FGMs (in-board and out-board) are placed on two ends of a vertical 1m boom attached to the base of the UAV. The in-board FGM is most sensitive to stray fields from the UAV and its signal is used, after scaling, to clean the signal of the out-board FGM from the vehicle noise. The FGMs record three orthogonal components of the magnetic field in the UAV body coordinates which are then transformed into a north-east-down coordinate system using a rotation matrix determined from the roll-pitch-yaw attitude data. This ensures knowledge of the direction of all three field components enabling us to perform inverse modeling of magnetic anomalies with greater accuracy than total or vertical field measurements used in the past. Field tests were performed at Dragon's Back Pressure Ridge in the Carrizo Plain of California, where there is a known crossing of the San Andreas Fault. Our data and models were compared to previously acquired LiDAR and hand-held magnetometer measurements. Further tests will be carried out to solidify our results and streamline our processing for educational use in the classroom and student field training.

Testing the three axis magnetometer and gradiometer MOURA and data comparison on San Pablo de los Montes Observatory.

Science.gov (United States)

Belen Fernandez, Ana; Sanz, Ruy; Covisa, Pablo; Tordesillas, Jose Manuel; Diaz-Michelena, Marina

2013-04-01

A magnetometer and gradiometer named MOURA has been developed with the objective to measure the magnetic field on Mars in the frame of Mars MetNet Precursor Mission (MMPM) [1]. MOURA is a compact, miniaturized, intelligent and low cost instrument, based on two sets of triaxial magnetometers separated one centimeter from each other to do gradiometry studies. It has a resolution of 2.2 nT, and a field range of + 65μT, which can be extended to +130 μT when sensors are saturated. [2] These sensor heads are Anisotropic MagnetoResistances (AMR) Commercial-Off-The-Shelf (COTS) by Honeywell, specifically HMC1043, which has been selected due to their relative low consumption, weight and size, factors very important for the mission with very limited mass and power budget (shared 150 g for three full payloads). Also, this technology has been previously successfully employed on board Unmanned Aerial Vehicles (UAV) to perform geomagnetic surveys in extreme conditions areas [3], and in several space missions for different applications. [4] After the development of the MOURA Engineering Qualification Model (EQM) in November 2011, an exhaustive set of tests have been performed to validate and fully characterize the instrument. Compensation equations have been derived for the temperature corrections in the operation range (between -135 °C and 30 °C) in controlled environments. These compensation equations have been applied to field data, which have shown to follow the daily Earth's magnetic field variations as registered by San Pablo Geomagnetic Observatory (IAGA code: SPT) (available at www.ign.es and www.intermagnet.org) with deviations lower than 40 nT. These deviations were attributed to several error factors as the different locations between MOURA and SPT and other possible different geomagnetic conditions. Due to the above, a measurement campaign on SPT installations are been done. The main objective is to compare MOURA measurements on a relevant environment, with data

Fluxgate vector magnetometers: A multisensor device for ground, UAV, and airborne magnetic surveys

OpenAIRE

Gavazzi , Bruno; Le Maire , Pauline; Munschy , Marc; Dechamp , Aline

2016-01-01

International audience; Fluxgate magnetometers are quite uncommon in geophysics. Recent advances in calibration of the devices and their magnetic compensation ability led Institut de Physique du Globe de Stras-bourg to develop instruments for magnetic measurements at different scales for a wide range of applications — from submetric measurements on the ground to aircraft-conducted acquisition by unmanned aerial vehicles (UAVs). A case study on the aerial military base BA112 shows the usefulne...

Two generalizations of column-convex polygons

International Nuclear Information System (INIS)

Feretic, Svjetlan; Guttmann, Anthony J

2009-01-01

Column-convex polygons were first counted by area several decades ago, and the result was found to be a simple, rational, generating function. In this work we generalize that result. Let a p-column polyomino be a polyomino whose columns can have 1, 2, ..., p connected components. Then column-convex polygons are equivalent to 1-convex polyominoes. The area generating function of even the simplest generalization, namely 2-column polyominoes, is unlikely to be solvable. We therefore define two classes of polyominoes which interpolate between column-convex polygons and 2-column polyominoes. We derive the area generating functions of those two classes, using extensions of existing algorithms. The growth constants of both classes are greater than the growth constant of column-convex polyominoes. Rather tight lower bounds on the growth constants complement a comprehensive asymptotic analysis.

Backside illuminated CMOS-TDI line scan sensor for space applications

Science.gov (United States)

Cohen, Omer; Ofer, Oren; Abramovich, Gil; Ben-Ari, Nimrod; Gershon, Gal; Brumer, Maya; Shay, Adi; Shamay, Yaron

2018-05-01

A multi-spectral backside illuminated Time Delayed Integration Radiation Hardened line scan sensor utilizing CMOS technology was designed for continuous scanning Low Earth Orbit small satellite applications. The sensor comprises a single silicon chip with 4 independent arrays of pixels where each array is arranged in 2600 columns with 64 TDI levels. A multispectral optical filter whose spectral responses per array are adjustable per system requirement is assembled at the package level. A custom 4T Pixel design provides the required readout speed, low-noise, very low dark current, and high conversion gains. A 2-phase internally controlled exposure mechanism improves the sensor's dynamic MTF. The sensor high level of integration includes on-chip 12 bit per pixel analog to digital converters, on-chip controller, and CMOS compatible voltage levels. Thus, the power consumption and the weight of the supporting electronics are reduced, and a simple electrical interface is provided. An adjustable gain provides a Full Well Capacity ranging from 150,000 electrons up to 500,000 electrons per column and an overall readout noise per column of less than 120 electrons. The imager supports line rates ranging from 50 to 10,000 lines/sec, with power consumption of less than 0.5W per array. Thus, the sensor is characterized by a high pixel rate, a high dynamic range and a very low power. To meet a Latch-up free requirement RadHard architecture and design rules were utilized. In this paper recent electrical and electro-optical measurements of the sensor's Flight Models will be presented for the first time.

Quantifying the In-Flight Yaw, Pitch, and Roll of a Semi-Rigidly Mounted Potassium Vapour Magnetometer Suspended Under a Heavy-Lift Multi-Rotor UAV and its Impact on Data Quality

Science.gov (United States)

Walter, C. A.; Braun, A.; Fotopoulos, G.

2017-12-01

Research is being conducted to develop an Unmanned Aerial System (UAS) that is capable of reliably and efficiently collecting high resolution, industry standard magnetic data (magnetic data with a fourth difference of +/- 0.05 nT) via an optically pumped vapour magnetometer. The benefits of developing a UAS with these capabilities include improvements in the resolution of localized airborne surveys (2.5 km by 2.5 km) and the ability to conduct 3D magnetic gradiometry surveys in the observation gap evident between traditional terrestrial and manned airborne magnetic surveys (surface elevation up to 120 m). Quantifying the extent of an optically pumped vapour magnetometer's 3D orientation variations, while in-flight and suspended under a UAS, is a significant advancement to existing knowledge as optically pumped magnetometers have an orientation-dependent (to the primary magnetic field vector) process for measuring the magnetic field. This study investigates the orientation characteristics of a GEM Systems potassium vapour magnetometer, GSMP-35U, while semi-rigidly suspended 3 m under a DJI S900, heavy-lift multi-rotor UAV (Unmanned Aerial Vehicle) during an airborne surveying campaign conducted Northeast of Thunder Bay, Ontario, Canada. A nine degrees of freedom IMU (Inertial Measurement Unit), the Adafruit GY-80, was used to quantify the 3D orientation variations (yaw, pitch and roll) of the magnetic sensor during flight. The orientation and magnetic datasets were indexed and linked with a date and time stamp (within 1 ms) via a Raspberry Pi 2, acting as an on-board computer and data storage system. Analysing the two datasets allowed for the in-flight orientation variations of the potassium vapour magnetometer to be directly compared with the gathered magnetic and signal quality data of the magnetometer. The in-flight orientation characteristics of the magnetometer were also quantified for a range of air-speeds and flight maneuvers throughout the survey. Overall

Setup and taking into operation of a highly sensitive 3He magnetometer for a future experiment for the determination of an electric dipole moment of the free neutron

International Nuclear Information System (INIS)

Kraft, Andreas

2012-01-01

The measurement of the electric dipole moment of the free neutron is directly linked to the question on the accurate determination of the magnetic field conditions inside the nEDM spectrometer. Using in-situ the spin-precession of polarized 3 He, monitored by optically pumped Cs-magnetometers a sensitivity on the femto-tesla-scale can be obtained. At the institute of physics of the University Mainz a 3 He/Cs-test facility was built to investigate the readout of 3 He-spin-precession with a lamp-pumped Cs-magnetometer. Additionally, an ultra-compact and transportable polarizer unit was developed and installed in Mainz, which polarizes 3 He gas up to 55 % of polarization before the compressed gas is delivered to two sandwich magnetometer cells inside the EDM chamber. This theses will present some results of the first successful test of the polarizer unit in January 2012. 3 He was polarized in the ultra compact polarizer unit and transferred via guiding fields into a 4 layer mu-metal shield, where the free spin precession was detected with a lamp pumped Cs-magnetometer.

Gamma Ray Absorption Technique For Scannig Process Column In Up-IV Pertamina Cilacap

International Nuclear Information System (INIS)

Santoso, Sigit Budi; Kushartono; Bisana; Mulyanto, Eko; Adi, Soecipto

2000-01-01

A demonstration using gamma ray absorption technique was carried out to diagnose malfunction such as tray missing, flooding, and weeping occurred in 2 3C-5 Extraction Vacuum Flash Strip Tower . The scan was conducted from the bottom until the top of the orientation of the director-source are (122 o -308 o ) dan (122 o - 270 o ). The results indicate that the tray number 1 and 3 were missing while weeping occurred in the space between tray 4,5,6,and 7. The results show that this technique can be used to diagnose malfunction occurred in the column on-line so it can help maintenance personnel in planning, the time scheduled and spare part for shutdown. Beside of that this technique can be developed to help column personnel's in adjusting the operation parameter to achieve optimum operation

Scanning magnetic tunnel junction microscope for high-resolution imaging of remanent magnetization fields

Science.gov (United States)

Lima, E. A.; Bruno, A. C.; Carvalho, H. R.; Weiss, B. P.

2014-10-01

Scanning magnetic microscopy is a new methodology for mapping magnetic fields with high spatial resolution and field sensitivity. An important goal has been to develop high-performance instruments that do not require cryogenic technology due to its high cost, complexity, and limitation on sensor-to-sample distance. Here we report the development of a low-cost scanning magnetic microscope based on commercial room-temperature magnetic tunnel junction (MTJ) sensors that typically achieves spatial resolution better than 7 µm. By comparing different bias and detection schemes, optimal performance was obtained when biasing the MTJ sensor with a modulated current at 1.0 kHz in a Wheatstone bridge configuration while using a lock-in amplifier in conjunction with a low-noise custom-made preamplifier. A precision horizontal (x-y) scanning stage comprising two coupled nanopositioners controls the position of the sample and a linear actuator adjusts the sensor-to-sample distance. We obtained magnetic field sensitivities better than 150 nT/Hz1/2 between 0.1 and 10 Hz, which is a critical frequency range for scanning magnetic microscopy. This corresponds to a magnetic moment sensitivity of 10-14 A m2, a factor of 100 better than achievable with typical commercial superconducting moment magnetometers. It also represents an improvement in sensitivity by a factor between 10 and 30 compared to similar scanning MTJ microscopes based on conventional bias-detection schemes. To demonstrate the capabilities of the instrument, two polished thin sections of representative geological samples were scanned along with a synthetic sample containing magnetic microparticles. The instrument is usable for a diversity of applications that require mapping of samples at room temperature to preserve magnetic properties or viability, including paleomagnetism and rock magnetism, nondestructive evaluation of materials, and biological assays.

Scanning magnetic tunnel junction microscope for high-resolution imaging of remanent magnetization fields

International Nuclear Information System (INIS)

Lima, E A; Weiss, B P; Bruno, A C; Carvalho, H R

2014-01-01

Scanning magnetic microscopy is a new methodology for mapping magnetic fields with high spatial resolution and field sensitivity. An important goal has been to develop high-performance instruments that do not require cryogenic technology due to its high cost, complexity, and limitation on sensor-to-sample distance. Here we report the development of a low-cost scanning magnetic microscope based on commercial room-temperature magnetic tunnel junction (MTJ) sensors that typically achieves spatial resolution better than 7 µm. By comparing different bias and detection schemes, optimal performance was obtained when biasing the MTJ sensor with a modulated current at 1.0 kHz in a Wheatstone bridge configuration while using a lock-in amplifier in conjunction with a low-noise custom-made preamplifier. A precision horizontal (x–y) scanning stage comprising two coupled nanopositioners controls the position of the sample and a linear actuator adjusts the sensor-to-sample distance. We obtained magnetic field sensitivities better than 150 nT/Hz 1/2 between 0.1 and 10 Hz, which is a critical frequency range for scanning magnetic microscopy. This corresponds to a magnetic moment sensitivity of 10 –14  A m 2 , a factor of 100 better than achievable with typical commercial superconducting moment magnetometers. It also represents an improvement in sensitivity by a factor between 10 and 30 compared to similar scanning MTJ microscopes based on conventional bias-detection schemes. To demonstrate the capabilities of the instrument, two polished thin sections of representative geological samples were scanned along with a synthetic sample containing magnetic microparticles. The instrument is usable for a diversity of applications that require mapping of samples at room temperature to preserve magnetic properties or viability, including paleomagnetism and rock magnetism, nondestructive evaluation of materials, and biological assays. (paper)

Development, construction and analysis of the "Ørsted" fluxgate magnetometer

DEFF Research Database (Denmark)

Nielsen, Otto V; Petersen, Jan Raagaard; Primdahl, Fritz

1995-01-01

glass ribbons as core materials. It is shown that very simple physical models can be used to explain the fluxgate mode of operation, thereby making it easy to calculate the overall sensor performance from first principles. Special attention is drawn to the core excitation current which is analysed...... in the instrument (±65 536 nT with 0.5 nT resolution). The maximum attainablebandwidth is half the sensor excitation frequency (½ x 15 kHz) but the Ørsted magnetometer bandwidth is limited to 250 Hz. The thermal stability of the sensor has been measured to be better than 1 nT in the temperature range -20 to +60°C....

Development of spent salt treatment technology by zeolite column system. Performance evaluation of zeolite column

International Nuclear Information System (INIS)

Miura, Hidenori; Uozumi, Koichi

2009-01-01

At electrorefining process, fission products(FPs) accumulate in molten salt. To avoid influence on heating control by decay heat and enlargement of FP amount in the recovered fuel, FP elements must be removed from the spent salt of the electrorefining process. For the removal of the FPs from the spent salt, we are investigating the availability of zeolite column system. For obtaining the basic data of the column system, such as flow property and ion-exchange performance while high temperature molten salt is passing through the column, and experimental apparatus equipped with fraction collector was developed. By using this apparatus, following results were obtained. 1) We cleared up the flow parameter of column system with zeolite powder, such as flow rate control by argon pressure. 2) Zeolite 4A in the column can absorb cesium that is one of the FP elements in molten salt. From these results, we got perspective on availability of the zeolite column system. (author)

X-ray CT Scanning Reveals Long-Term Copper Pollution Effects on Functional Soil Structure

DEFF Research Database (Denmark)

Naveed, Muhammad; Møldrup, Per; Homstrup, Martin

Soil structure plays the main role in the ability of the soil to fulfill essential soil functions such as the root growth, rate of water infiltration and retention, transport of gaseous and chemicals/pollutants through the soil. Soil structure is a dynamic soil property and affected by various...... factors such as soil type, land use, and soil contamination. In this study, we quantified the soil structure using X-ray CT scanning and revealed the effect of a long history of Copper (Cu) pollution on it. A fallow field at Hygum Denmark provides this opportunity as it had a long history of Copper...... sulphate contamination in a gradient with Cu content varies from 21 mg kg-1 to 3837 mg kg-1. Total 20 intact soil columns (diameter of 10 cm and height of 8 cm) were sampled at five locations along the Cu-gradient from a depth of 5 to 15 cm below surface level. The soil columns were scanned at a voxel...

Elimination of the induced current error in magnetometers using superconducting flux transformers

International Nuclear Information System (INIS)

Dummer, D.; Weyhmann, W.

1987-01-01

The changing magnetization of a sample in a superconducting flux transformer coupled magnetometer induces a current in the transformer which in turn changes the field at the sample. This ''image'' field and the error caused by it can be eliminated by sensing the current in the loop and nulling it by feedback through a mutual inductance. We have tested the technique on the superconducting transition of indium in an applied magnetic field and shown that the observed width of the transition is greatly reduced by maintaining zero current in the flux transformer

The Search-Coil Magnetometer for MMS

Science.gov (United States)

Le Contel, O.; Leroy, P.; Roux, A.; Coillot, C.; Alison, D.; Bouabdellah, A.; Mirioni, L.; Meslier, L.; Galic, A.; Vassal, M. C.; Torbert, R. B.; Needell, J.; Rau, D.; Dors, I.; Ergun, R. E.; Westfall, J.; Summers, D.; Wallace, J.; Magnes, W.; Valavanoglou, A.; Olsson, G.; Chutter, M.; Macri, J.; Myers, S.; Turco, S.; Nolin, J.; Bodet, D.; Rowe, K.; Tanguy, M.; de la Porte, B.

2016-03-01

The tri-axial search-coil magnetometer (SCM) belongs to the FIELDS instrumentation suite on the Magnetospheric Multiscale (MMS) mission (Torbert et al. in Space Sci. Rev. (2014), this issue). It provides the three magnetic components of the waves from 1 Hz to 6 kHz in particular in the key regions of the Earth's magnetosphere namely the subsolar region and the magnetotail. Magnetospheric plasmas being collisionless, such a measurement is crucial as the electromagnetic waves are thought to provide a way to ensure the conversion from magnetic to thermal and kinetic energies allowing local or global reconfigurations of the Earth's magnetic field. The analog waveforms provided by the SCM are digitized and processed inside the digital signal processor (DSP), within the Central Electronics Box (CEB), together with the electric field data provided by the spin-plane double probe (SDP) and the axial double probe (ADP). On-board calibration signal provided by DSP allows the verification of the SCM transfer function once per orbit. Magnetic waveforms and on-board spectra computed by DSP are available at different time resolution depending on the selected mode. The SCM design is described in details as well as the different steps of the ground and in-flight calibrations.

Self-assembled GaN nano-column grown on Si(111) substrate using Au+Ga alloy seeding method by metalorganic chemical vapor deposition

International Nuclear Information System (INIS)

Shim, Byung-Young; Ko, Eun-A; Song, Jae-Chul; Kang, Dong-Hun; Kim, Dong-Wook; Lee, In-Hwan; Kannappan, Santhakumar; Lee, Cheul-Ro

2007-01-01

Single-crystal GaN nano-column arrays were grown on Au-coated silicon (111) substrate by Au-Ga alloy seeding method using metalorganic chemical vapor deposition (MOCVD). The nano-column arrays were studied as a function of growth parameters and Au thin film thickness. The diameter and length of the as-grown nano-column vary from 100 to 500 nm and 4 to 6 μm, respectively. The surface morphology and optical properties of the nano-columns were investigated using scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), cathodoluminescence (CL) and photoluminescence (PL). The Au+Ga alloy droplets were found to be uniformly distributed on silicon surface. Further, SEM image reveals a vertical growth and cylindrical in shape GaN nano-column. The chemical composition of the nano-column, which composed of gallium and nitrogen ions, was estimated by EDX. CL reveals a strong band edge emission from the GaN nano-column. PL spectra show a peak at 365.7 nm with a full-width half maximum (FWHM) of 65 meV which indicates good optical quality GaN nano-column with low dislocation density. Our results suggest that single crystal GaN nano-column can be grown on Au+Ga alloy on silicon substrate with a low dislocation density for better device performances. (author)

High temperature superconductor micro-superconducting-quantum-interference-device magnetometer for magnetization measurement of a microscale magnet.

Science.gov (United States)

Takeda, Keiji; Mori, Hatsumi; Yamaguchi, Akira; Ishimoto, Hidehiko; Nakamura, Takayoshi; Kuriki, Shinya; Hozumi, Toshiya; Ohkoshi, Shin-ichi

2008-03-01

We have developed a high temperature superconductor (HTS) micrometer-sized dc superconducting quantum interference device (SQUID) magnetometer for high field and high temperature operation. It was fabricated from YBa2Cu3O7-delta of 92 nm in thickness with photolithography techniques to have a hole of 4x9 microm2 and 2 microm wide grain boundary Josephson junctions. Combined with a three dimensional magnetic field coil system, the modulation patterns of critical current Ic were observed for three different field directions. They were successfully used to measure the magnetic properties of a molecular ferrimagnetic microcrystal (23x17x13 microm3), [Mn2(H2O)2(CH3COO)][W(CN)8]2H2O. The magnetization curve was obtained in magnetic field up to 0.12 T between 30 and 70 K. This is the first to measure the anisotropy of hysteresis curve in the field above 0.1 T with an accuracy of 10(-12) J T(-1) (10(-9) emu) with a HTS micro-SQUID magnetometer.

High-Sensitivity Low-Noise Miniature Fluxgate Magnetometers Using a Flip Chip Conceptual Design

OpenAIRE

Lu, Chih-Cheng; Huang, Jeff; Chiu, Po-Kai; Chiu, Shih-Liang; Jeng, Jen-Tzong

2014-01-01

This paper presents a novel class of miniature fluxgate magnetometers fabricated on a print circuit board (PCB) substrate and electrically connected to each other similar to the current “flip chip” concept in semiconductor package. This sensor is soldered together by reversely flipping a 5 cm × 3 cm PCB substrate to the other identical one which includes dual magnetic cores, planar pick-up coils, and 3-D excitation coils constructed by planar Cu interconnections patterned on PCB substrates. P...

Demonstration of the SeptiStrand benthic microbial fuel cell powering a magnetometer for ship detection

Science.gov (United States)

Arias-Thode, Y. Meriah; Hsu, Lewis; Anderson, Greg; Babauta, Jerome; Fransham, Roy; Obraztsova, Anna; Tukeman, Gabriel; Chadwick, D. Bart

2017-07-01

The Navy has a need for monitoring conditions and gathering information in marine environments. Sensors can monitor and report environmental parameters and potential activities such as animal movements, ships, or personnel. However, there has to be a means to power these sensors. One promising enabling technology that has been shown to provide long-term power production in underwater environments is the benthic microbial fuel cells (BMFC). BMFCs are devices that generate energy by coupling bioanodes and biocathodes through an external energy harvester. Recent studies have demonstrated success for usage of BMFCs in powering small instruments and other devices on the seafloor over limited periods of time. In this effort, a seven-stranded BMFC linear array of 30 m was designed to power a seafloor magnetometer to detect passing ship movements through Pearl Harbor, Hawaii. The BMFC system was connected to a flyback energy harvesting circuit that charged the battery powering the magnetometer. The deployment was demonstrated the BMFC supplied power to the battery for approximately 38 days. This is the first large-scale demonstration system for usage of the SeptiStrand BMFC technology to power a relevant sensor.

Counter electrojet features in the Brazilian sector: simultaneous observation by radar, digital sounder and magnetometers

Directory of Open Access Journals (Sweden)

C. M. Denardini

2009-04-01

Full Text Available In the present work we show new results regarding equatorial counter electrojet (CEJ events in the Brazilian sector, based on the RESCO radar, two set of fluxgate magnetometer systems and a digital sounder. RESCO radar is a 50 MHz backscatter coherent radar installed in 1998 at São Luís (SLZ, 2.33° S, 44.60° W, an equatorial site. The Digital sounder routinely monitors the electron density profile at the radar site. The magnetometer systems are fluxgate-type installed at SLZ and Eusébio (EUS, 03.89° S, 38.44° W. From the difference between the horizontal component of magnetic field at SLZ station and the same component at EUS (EEJ ground strength several cases of westward morning electrojet and its normal inversion to the eastward equatorial electrojet (EEJ have been observed. Also, the EEJ ground strength has shown some cases of CEJ events, which been detected with the RESCO radar too. Detection of these events were investigated with respect to their time and height of occurrence, correlation with sporadic E (Es layers at the same time, and their spectral characteristics as well as the radar echo power intensity.

Wall modified photonic crystal fibre capillaries as porous layer open tubular columns for in-capillary micro-extraction and capillary chromatography

International Nuclear Information System (INIS)

Kazarian, Artaches A.; Sanz Rodriguez, Estrella; Deverell, Jeremy A.; McCord, James; Muddiman, David C.; Paull, Brett

2016-01-01

Wall modified photonic crystal fibre capillary columns for in-capillary micro-extraction and liquid chromatographic separations is presented. Columns contained 126 internal parallel 4 μm channels, each containing a wall bonded porous monolithic type polystyrene-divinylbenzene layer in open tubular column format (PLOT). Modification longitudinal homogeneity was monitored using scanning contactless conductivity detection and scanning electron microscopy. The multichannel open tubular capillary column showed channel diameter and polymer layer consistency of 4.2 ± 0.1 μm and 0.26 ± 0.02 μm respectively, and modification of 100% of the parallel channels with the monolithic polymer. The modified multi-channel capillaries were applied to the in-capillary micro-extraction of water samples. 500 μL of water samples containing single μg L"−"1 levels of polyaromatic hydrocarbons were extracted at a flow rate of 10 μL min"−"1, and eluted in 50 μL of acetonitrile for analysis using HPLC with fluorescence detection. HPLC LODs were 0.08, 0.02 and 0.05 μg L"−"1 for acenaphthene, anthracene and pyrene, respectively, with extraction recoveries of between 77 and 103%. The modified capillaries were also investigated briefly for direct application to liquid chromatographic separations, with the retention and elution of a standard protein (cytochrome c) under isocratic conditions demonstrated, proving chromatographic potential of the new column format, with run-to-run retention time reproducibility of below 1%. - Highlights: • Novel PS-DVB modified photonic crystal fibres for in-capillary micro-extraction. • New method for micro-extraction of PAHs and HPLC-FL detection at sub-ppb levels. • Demonstration of PS-DVB modified photonic crystal fibres for capillary bioseparations.

Wall modified photonic crystal fibre capillaries as porous layer open tubular columns for in-capillary micro-extraction and capillary chromatography

Energy Technology Data Exchange (ETDEWEB)

Kazarian, Artaches A. [Australian Centre for Research on Separation Science, School of Physical Sciences, University of Tasmania, Private Bag 75, Hobart, Tasmania 7001 (Australia); W.M. Keck FT-ICR-MS Laboratory, Department of Chemistry, North Carolina State University, Raleigh, NC (United States); Sanz Rodriguez, Estrella; Deverell, Jeremy A. [Australian Centre for Research on Separation Science, School of Physical Sciences, University of Tasmania, Private Bag 75, Hobart, Tasmania 7001 (Australia); McCord, James; Muddiman, David C. [W.M. Keck FT-ICR-MS Laboratory, Department of Chemistry, North Carolina State University, Raleigh, NC (United States); Paull, Brett, E-mail: Brett.Paull@utas.edu.au [Australian Centre for Research on Separation Science, School of Physical Sciences, University of Tasmania, Private Bag 75, Hobart, Tasmania 7001 (Australia); ARC Centre of Excellence for Electromaterials Science, School of Physical Sciences, University of Tasmania, Private Bag 75, Hobart, Tasmania 7001 (Australia)

2016-01-28

Wall modified photonic crystal fibre capillary columns for in-capillary micro-extraction and liquid chromatographic separations is presented. Columns contained 126 internal parallel 4 μm channels, each containing a wall bonded porous monolithic type polystyrene-divinylbenzene layer in open tubular column format (PLOT). Modification longitudinal homogeneity was monitored using scanning contactless conductivity detection and scanning electron microscopy. The multichannel open tubular capillary column showed channel diameter and polymer layer consistency of 4.2 ± 0.1 μm and 0.26 ± 0.02 μm respectively, and modification of 100% of the parallel channels with the monolithic polymer. The modified multi-channel capillaries were applied to the in-capillary micro-extraction of water samples. 500 μL of water samples containing single μg L{sup −1} levels of polyaromatic hydrocarbons were extracted at a flow rate of 10 μL min{sup −1}, and eluted in 50 μL of acetonitrile for analysis using HPLC with fluorescence detection. HPLC LODs were 0.08, 0.02 and 0.05 μg L{sup −1} for acenaphthene, anthracene and pyrene, respectively, with extraction recoveries of between 77 and 103%. The modified capillaries were also investigated briefly for direct application to liquid chromatographic separations, with the retention and elution of a standard protein (cytochrome c) under isocratic conditions demonstrated, proving chromatographic potential of the new column format, with run-to-run retention time reproducibility of below 1%. - Highlights: • Novel PS-DVB modified photonic crystal fibres for in-capillary micro-extraction. • New method for micro-extraction of PAHs and HPLC-FL detection at sub-ppb levels. • Demonstration of PS-DVB modified photonic crystal fibres for capillary bioseparations.

Single column and two-column H-D-T distillation experiments at TSTA

International Nuclear Information System (INIS)

Yamanishi, T.; Yoshida, H.; Hirata, S.; Naito, T.; Naruse, Y.; Sherman, R.H.; Bartlit, J.R.; Anderson, J.L.

1988-01-01

Cryogenic distillation experiments were peformed at TSTA with H-D-T system by using a single column and a two-column cascade. In the single column experiment, fundamental engineering data such as the liquid holdup and the HETP were measured under a variety of operational condtions. The liquid holdup in the packed section was about 10 /approximately/ 15% of its superficial volume. The HETP values were from 4 to 6 cm, and increased slightly with the vapor velocity. The reflux ratio had no effect on the HETP. For the wo-colunn experiemnt, dynamic behavior of the cascade was observed. 8 refs., 7 figs., 2 tabs

ON THE ORIGIN OF THE HIGH COLUMN DENSITY TURNOVER IN THE H I COLUMN DENSITY DISTRIBUTION

International Nuclear Information System (INIS)

Erkal, Denis; Gnedin, Nickolay Y.; Kravtsov, Andrey V.

2012-01-01

We study the high column density regime of the H I column density distribution function and argue that there are two distinct features: a turnover at N H I ≈ 10 21 cm –2 , which is present at both z = 0 and z ≈ 3, and a lack of systems above N H I ≈ 10 22 cm –2 at z = 0. Using observations of the column density distribution, we argue that the H I-H 2 transition does not cause the turnover at N H I ≈ 10 21 cm –2 but can plausibly explain the turnover at N H I ∼> 10 22 cm –2 . We compute the H I column density distribution of individual galaxies in the THINGS sample and show that the turnover column density depends only weakly on metallicity. Furthermore, we show that the column density distribution of galaxies, corrected for inclination, is insensitive to the resolution of the H I map or to averaging in radial shells. Our results indicate that the similarity of H I column density distributions at z = 3 and 0 is due to the similarity of the maximum H I surface densities of high-z and low-z disks, set presumably by universal processes that shape properties of the gaseous disks of galaxies. Using fully cosmological simulations, we explore other candidate physical mechanisms that could produce a turnover in the column density distribution. We show that while turbulence within giant molecular clouds cannot affect the damped Lyα column density distribution, stellar feedback can affect it significantly if the feedback is sufficiently effective in removing gas from the central 2-3 kpc of high-redshift galaxies. Finally, we argue that it is meaningful to compare column densities averaged over ∼ kpc scales with those estimated from quasar spectra that probe sub-pc scales due to the steep power spectrum of H I column density fluctuations observed in nearby galaxies.

Adiabatic packed column supercritical fluid chromatography using a dual-zone still-air column heater.

Science.gov (United States)

Helmueller, Shawn C; Poe, Donald P; Kaczmarski, Krzysztof

2018-02-02

An approach to conducting SFC separations under pseudo-adiabatic condition utilizing a dual-zone column heater is described. The heater allows for efficient separations at low pressures above the critical temperature by imposing a temperature profile along the column wall that closely matches that for isenthalpic expansion of the fluid inside the column. As a result, the efficiency loss associated with the formation of radial temperature gradients in this difficult region can be largely avoided in packed analytical scale columns. For elution of n-octadecylbenzene at 60 °C with 5% methanol modifier and a flow rate of 3 mL/min, a 250 × 4.6-mm column packed with 5-micron Kinetex C18 particles began to lose efficiency (8% decrease in the number of theoretical plates) at outlet pressures below 142 bar in a traditional forced air oven. The corresponding outlet pressure for onset of excess efficiency loss was decreased to 121 bar when the column was operated in a commercial HPLC column heater, and to 104 bar in the new dual-zone heater operated in adiabatic mode, with corresponding increases in the retention factor for n-octadecylbenzene from 2.9 to 6.8 and 14, respectively. This approach allows for increased retention and efficient separations of otherwise weakly retained analytes. Applications are described for rapid SFC separation of an alkylbenzene mixture using a pressure ramp, and isobaric separation of a cannabinoid mixture. Copyright © 2018 Elsevier B.V. All rights reserved.

Influence of pressure on the properties of chromatographic columns. II. The column hold-up volume.

Science.gov (United States)

Gritti, Fabrice; Martin, Michel; Guiochon, Georges

2005-04-08

The effect of the local pressure and of the average column pressure on the hold-up column volume was investigated between 1 and 400 bar, from a theoretical and an experimental point of view. Calculations based upon the elasticity of the solids involved (column wall and packing material) and the compressibility of the liquid phase show that the increase of the column hold-up volume with increasing pressure that is observed is correlated with (in order of decreasing importance): (1) the compressibility of the mobile phase (+1 to 5%); (2) in RPLC, the compressibility of the C18-bonded layer on the surface of the silica (+0.5 to 1%); and (3) the expansion of the column tube (columns packed with the pure Resolve silica (0% carbon), the derivatized Resolve-C18 (10% carbon) and the Symmetry-C18 (20% carbon) adsorbents, using water, methanol, or n-pentane as the mobile phase. These solvents have different compressibilities. However, 1% of the relative increase of the column hold-up volume that was observed when the pressure was raised is not accounted for by the compressibilities of either the solvent or the C18-bonded phase. It is due to the influence of the pressure on the retention behavior of thiourea, the compound used as tracer to measure the hold-up volume.

Fluxgate Magnetometer system mounted on UAS system: First field test at Dominga IOCG deposit, Chile

Science.gov (United States)

Yanez, G. A.; Banchero, L.; Marco, A.; Figueroa, R.

2016-12-01

With the support of Fundacion Chile (FCH) grant, we developed an airborne magnetic system (GeoMagDrone GFDAS) mounted on a UAS octodrone platform (DJI, S1000), based on a low cost/light-weight fluxgate magnetometer (FGM-301) and a robust/light-weight data logger for position, temperature, radar altimeter and 3 magnetic components at 16 Hz recording. Fluxgate magnetometer is hanging from the UAS platform at a distance of 2.5m where the EM noise is reduced to less than 2 nT. The whole geophysical system, including batteries, weights 650 gr., with an autonomy of 2 hours. Magnetometer calibration includes the 9 coefficients of amplitude, offset, and orthogonality, and temperature correction. We test the system over the IOCG deposit of Dominga-Chile, a magnetite ore (40%) (a block of 2x3 km with NS lines separated every 50m and a clearance of 40m, the mineral deposit buried 50-100m from the surface, where a ground magnetic survey was conducted previously. Ground conditions includes relatively rough topography with slopes of 10-20%, and some windy days. We use the digital terrain model SRTM30 to define the drape flight shape Average flight performance includes a mean speed of 35-40 km/hour, and an UAS battery consumption of 18-12 minutes depending on the wind conditions. A good correspondence was found between plan deployment and survey results in terms of line direction/separation/clearance. Line path were flown with errors less than 5 meters, whereas clearance of 40m was kept depending on the amount of control points used. The comparison between ground survey and GeoMagDrone results show a perfect match (anomaly amplitude/shape and noise envelope), validating in this way the system developed. Main concern for the productive application of this technology in unmanned geophysical platforms is the battery performance and the quality of digital terrain models to follow the topography.

Compact electron beam focusing column

Science.gov (United States)

Persaud, Arun; Leung, Ka-Ngo; Reijonen, Jani

2001-12-01

A novel design for an electron beam focusing column has been developed at LBNL. The design is based on a low-energy spread multicusp plasma source which is used as a cathode for electron beam production. The focusing column is 10 mm in length. The electron beam is focused by means of electrostatic fields. The column is designed for a maximum voltage of 50 kV. Simulations of the electron trajectories have been performed by using the 2D simulation code IGUN and EGUN. The electron temperature has also been incorporated into the simulations. The electron beam simulations, column design and fabrication will be discussed in this presentation.

Experimental 3-D Vector Velocity Estimation with Row-Column Addressed Arrays

DEFF Research Database (Denmark)

Holbek, Simon; Stuart, Matthias Bo; Jensen, Jørgen Arendt

2016-01-01

Experimental 3-D vector flow estimates obtained with a 62+62 2-D row-column (RC) array with integrated apodization are presented. A transverse oscillation (TO) velocity estimator is implemented on a 3.0 MHz RC array, to yield realtime 3-D vector flow in a cross-sectional scan plane at 750 frames...... per second. The method is validated in a straight-vessel phantom (Ø = 8 mm) connected to a flow pump capable of generating timevarying carotid waveforms. The out-of-plane velocity component perpendicular to the cross section of the vessel and the crosssectional area is used to estimate volumetric flow...

Airborne gamma-ray spectrometer and magnetometer survey, Meade River Quadrangle, Alaska. Final report

International Nuclear Information System (INIS)

1981-02-01

The results obtained from an airborne high sensitivity gamma-ray spectrometer and magnetometer survey over the Meade River map area of Alaska are presented. Based on the criteria outlined in the general section on interpretation, a total of eight uranium anomalies have been outlined on the interpretation map. Most of these are only weakly to moderately anomalous. Zones 3 and 7 are relatively better than the others though none of the anomalies are thought to be of any economic significance. No follow-up work is recommended

Synthesis and characterization of organic–inorganic core–shell structure nanocomposite and application for Zn ions removal from aqueous solution in a fixed-bed column

Energy Technology Data Exchange (ETDEWEB)

Ghasemi, Shokoofeh [Faculty of Chemical, Gas and Petroleum Engineering, Semnan University, Semnan 35131-19111 (Iran, Islamic Republic of); Ghorbani, Mohsen, E-mail: M.ghorbani@nit.ac.ir [Faculty of Chemical Engineering, Babol University of Technology, P.O. Box 484, Babol (Iran, Islamic Republic of); Ghazi, Mohsen Mehdipour [Faculty of Chemical, Gas and Petroleum Engineering, Semnan University, Semnan 35131-19111 (Iran, Islamic Republic of)

2015-12-30

Graphical abstract: - Highlights: • The γ-Fe{sub 2}O{sub 3} nanoparticles were prepared in one step using ultrasonic radiation and coated by polyrhodanine. • Nanocomposite synthesized with core average diameter of 15 nm and polyrhodanine as shell with thickness of 1.5 nm • Application of products was investigated to separate zinc ions from aqueous solution in a fixed-bed column. • The Adams–Bohart, BDST, Thomas and Yoon–Nelson models used to predict model parameters. • The models were nearly in good agreement with the experimental data. - Abstract: An organic–inorganic core/shell structure, γ-Fe{sub 2}O{sub 3}/polyrhodanine nanocomposite with γ-Fe{sub 2}O{sub 3} nanoparticle as core with average diameter of 15 nm and polyrhodanine as shell with thickness of 1.5 nm, has been synthesized via chemical oxidation polymerization and applied for adsorption of Zn ions from aqueous solution in a fixed-bed column. The properties of nanocomposite were characterized with transmission electron microscope (TEM), Fourier transform infrared (FT-IR) spectroscopy and vibrating sample magnetometer (VSM). The performance of the column was assessed under variable bed heights (10, 15 and 20 cm) and influent Zn concentrations (50, 100 and 150 ppm) at a constant flow rate (0.5 mL/min). The results demonstrated that the breakthrough curves are S-shaped and the breakthrough time increases with increasing bed height and decreases with increasing influent concentration. Moreover, the dynamics of the adsorption process were evaluated by using Adams–Bohart, bed depth service time (BDST), Thomas and Yoon–Nelson kinetic models. The models were nearly in good agreement with the experimental data.

The effects of carbide column to swelling potential and Atterberg limit on expansive soil with column to soil drainage

Science.gov (United States)

Muamar Rifa'i, Alfian; Setiawan, Bambang; Djarwanti, Noegroho

2017-12-01

The expansive soil is soil that has a potential for swelling-shrinking due to changes in water content. Such behavior can exert enough force on building above to cause damage. The use of columns filled with additives such as Calcium Carbide is done to reduce the negative impact of expansive soil behavior. This study aims to determine the effect of carbide columns on expansive soil. Observations were made on swelling and spreading of carbides in the soil. 7 Carbide columns with 5 cm diameter and 20 cm height were installed into the soil with an inter-column spacing of 8.75 cm. Wetting is done through a pipe at the center of the carbide column for 20 days. Observations were conducted on expansive soil without carbide columns and expansive soil with carbide columns. The results showed that the addition of carbide column could reduce the percentage of swelling by 4.42%. Wetting through the center of the carbide column can help spread the carbide into the soil. The use of carbide columns can also decrease the rate of soil expansivity. After the addition of carbide column, the plasticity index value decreased from 71.76% to 4.3% and the shrinkage index decreased from 95.72% to 9.2%.

Airborne gamma-ray spectrometer and magnetometer survey: north/south tieline. Final report

International Nuclear Information System (INIS)

1981-05-01

An airborne high sensitivity gamma-ray spectrometer and magnetometer survey was conducted along the 99 0 longitude meridian from the Canadian border southward to the Mexican border. A total of 1555 line miles of geophysical data were acquired and, subsequently, compiled. The north-south tieline was flown as part of the National Uranium Resources Evaluation. NURE is a program of the US Department of Energy's Grand Junction, Colorado, office to acquire and compile geologic and other information with which to assess the magnitude and distribution of uranium resources and to determine areas favorable for the occurrence of uranium in the United States

Thermal process of an air column

International Nuclear Information System (INIS)

Lee, F.T.

1994-01-01

Thermal process of a hot air column is discussed based on laws of thermodynamics. The kinetic motion of the air mass in the column can be used as a power generator. Alternatively, the column can also function as a exhaust/cooler

Airborne gamma-ray spectrometer and magnetometer survey, Sagavanirktok Quadrangle, Alaska. Volume I. Final report

International Nuclear Information System (INIS)

1981-03-01

The results obtained from an airborne high sensitivity gamma-ray spectrometer and magnetometer survey over the Sagavanirktok map area of Alaska are presented. Based on the criteria outlined in the general section on interpretation, a total of eight uranium anomalies have been outlined on the interpretation map. However, all of these zones are only weakly to moderately anomalous. None are thought to be indicative of local enrichment of uranium to economically significant levels. No follow-up work is recommended

Heat storage in the Hettangian aquifer in Berlin - results from a column experiment

Science.gov (United States)

Milkus, Chri(Sch)augott

2015-04-01

Aquifer Thermal Energy Storage (ATES) is a sustainable alternative for storage and seasonal availability of thermal energy. However, its impact on the subsurface flow regime is not well known. In Berlin (Germany), the Jurassic (Hettangian) sandstone aquifer with highly mineralized groundwater (TDS 27 g/L) is currently used for heat storage. The aim of this study was to examine the hydrogeochemical changes that are caused by the induced temperature shift and its effects on the hydraulic permeability of the aquifer. Column experiments were conducted, in which stainless steel columns were filled with sediment from the aquifer and flushed with native groundwater for several weeks. The initial temperature of the experiment was 20°C, comparable to the in-situ conditions within the aquifer. After reaching equilibrium between sediment and water, the temperature was increased to simulate heating of the aquifer. During the experiment, physical and chemical parameters (pH, ORP, dissolved oxygen and dissolved carbon dioxide) were measured at the outflow of the column and the effluent water was sampled. Using a Scanning Electron Microscope, the deposition of precipitated minerals and biofilm on sediment grains was analyzed. Changes in hydraulic properties of the sediment were studied by the use of tracer tests with Uranin.

Atmospheric scanning electron microscope for correlative microscopy.

Science.gov (United States)

Morrison, Ian E G; Dennison, Clare L; Nishiyama, Hidetoshi; Suga, Mitsuo; Sato, Chikara; Yarwood, Andrew; O'Toole, Peter J

2012-01-01

The JEOL ClairScope is the first truly correlative scanning electron and optical microscope. An inverted scanning electron microscope (SEM) column allows electron images of wet samples to be obtained in ambient conditions in a biological culture dish, via a silicon nitride film window in the base. A standard inverted optical microscope positioned above the dish holder can be used to take reflected light and epifluorescence images of the same sample, under atmospheric conditions that permit biochemical modifications. For SEM, the open dish allows successive staining operations to be performed without moving the holder. The standard optical color camera used for fluorescence imaging can be exchanged for a high-sensitivity monochrome camera to detect low-intensity fluorescence signals, and also cathodoluminescence emission from nanophosphor particles. If these particles are applied to the sample at a suitable density, they can greatly assist the task of perfecting the correlation between the optical and electron images. Copyright © 2012 Elsevier Inc. All rights reserved.

Solvent extraction columns

International Nuclear Information System (INIS)

Middleton, P.; Smith, J.R.

1979-01-01

In pulsed columns for use in solvent extraction processes, e.g. the reprocessing of nuclear fuel, the horizontal perforated plates inside the column are separated by interplate spacers manufactured from metallic neutron absorbing material. The spacer may be in the form of a spiral or concentric circles separated by radial limbs, or may be of egg-box construction. Suitable neutron absorbing materials include stainless steel containing boron or gadolinium, hafnium metal or alloys of hafnium. (UK)

Sensitivity of proposed search for axion-induced magnetic field using optically pumped magnetometers

Science.gov (United States)

Chu, P.-H.; Duffy, L. D.; Kim, Y. J.; Savukov, I. M.

2018-04-01

We investigate the sensitivity of a search for the oscillating current induced by axion dark matter in an external magnetic field using optically pumped magnetometers. This experiment is based upon the LC circuit (circuit with inductor and capacitor) axion detection concept of Sikivie et al. [Phys. Rev. Lett. 112, 131301 (2014), 10.1103/PhysRevLett.112.131301]. The modification of Maxwell's equations caused by the axion-photon coupling results in a minute magnetic field oscillating at a frequency equal to the axion mass, in the presence of an external magnetic field. The axion-induced magnetic field could be searched for using a LC circuit amplifier with an optically pumped magnetometer, the most sensitive cryogen-free magnetic-field sensor, in a room-temperature experiment, avoiding the need for a complicated and expensive cryogenic system. We discuss how an existing magnetic resonance imaging experiment can be modified to search for axions in a previously unexplored part of the parameter space. Our existing detection setup, optimized for magnetic resonance imagining, is already sensitive to an axion-photon coupling of 10-7 GeV-1 for an axion mass near 3 ×10-10 eV , which is already limited by astrophysical processes and solar axion searches. We show that realistic modifications, and optimization of the experiment for axion detection, can probe the axion-photon coupling up to 4 orders of magnitude beyond the current best limit, for axion masses between 10-11 and 10-7 eV .

Simulation and measurement of ferromagnetic impurities in non-magnetic aeroengine turbine disks using fluxgate magnetometers

OpenAIRE

Sebastian Hantscher; Ruixin Zhou; Albert Seidl; Johann Hinken; Christian Ziep

2015-01-01

In this paper, ferromagnetic impurities in paramagnetic aeroengine turbine disks are investigated. Because such inclusions represent a significant threat in aviation, a detailed analysis is required for impured turbine disks. For this purpose, sensitive fluxgate magnetometers are used. After a premagnetisation, this sensor is able to detect small ferromagnetic particles by recording the variation of the magnetic flux density while the disk rotates below the sensor head. This trajectory create...

Geophysical Surveying of Shallow Magnetic Anomalies Using the iPhone Magnetometer

Science.gov (United States)

Opdyke, P.; Dudley, C.; Louie, J. N.

2012-12-01

This investigation examined whether the 3-axis Hall-effect magnetometer in the Apple iPhone 3GS can function as an effective shallow magnetic survey instrument. The xSensor Pro app from Crossbow Systems allows recoding of all three sensor components along with the GPS location, at a frequency of 1.0, 4.0, 16.0, and 32.0 Hz. If the iPhone proves successful in collecting useful magnetic data, then geophysicists and especially educators would have a new tool for high-density geophysical mapping. No-contract iPhones that can connect with WiFi can be obtained for about $400, allowing deployment of large numbers of instruments. iPhones with the xSensor Pro app surveyed in parallel with an Overhauser GEM system magnetometer (1 nT sensitivity) to test this idea. Anderson Bay, located on the Pyramid Lake Paiute Reservation, provided a rural survey location free from cultural interference. xSensor Pro, logged each component's intensity and the GPS location at a frequency of four measurements per second. Two Overhauser units functioned as a base unit and a roving unit. The roving unit collected total field at set points located with a handheld GPS. Comparing the total field computed from the iPhone components against that collected by the Overhauser establishes the level of anomalies that the iPhone can detect. iPhone total-field measurements commonly vary by 200 nT from point to point, so a spatial-temporal average over 25 seconds produces a smoothed signal for comparison. Preliminary analysis of the iPhone results show that the data do not accurately correlate to the total field collected by the Overhauser for any anomaly of less than 200 nT.

Preparation of organic monolithic columns in polytetrafluoroethylene tubes for reversed-phase liquid chromatography

International Nuclear Information System (INIS)

Catalá-Icardo, M.; Torres-Cartas, S.; Meseguer-Lloret, S.; Gómez-Benito, C.; Carrasco-Correa, E.; Simó-Alfonso, E.F.; Ramis-Ramos, G.; Herrero-Martínez, J.M.

2017-01-01

In this work, a method for the preparation and anchoring of polymeric monoliths in a polytetrafluoroethylene (PTFE) tubing as a column housing for microbore HPLC is described. In order to assure a covalent attachment of the monolith to the inner wall of the PTFE tube, a two-step procedure was developed. Two surface etching reagents, a commercial sodium naphthalene solution (Fluoroetch"®), or mixtures of H_2O_2 and H_2SO_4, were tried and compared. Then, the obtained hydroxyl groups on the PTFE surface were modified by methacryloylation. Attenuated total reflectance Fourier-transform infrared (ATR-FTIR) spectroscopy and scanning electron microscopy (SEM) confirmed the successful modification of the tubing wall and the stable anchorage of monolith to the wall, respectively. Special emphasis was also put on the reduction of the unwanted effects of shrinking of monolith during polymerization, by using an external proper mold and by selecting the adequate monomers in order to increase the flexibility of the polymer. Poly(glycidyl methacrylate-co-divinylbenzene) monoliths were in situ synthesized by thermal polymerization within the confines of surface-vinylized PTFE tubes. The modified PTFE tubing tightly held the monolith, and the monolithic column exhibited good pressure resistance up to 20 MPa. The column performance was also evaluated via the isocratic separation of a series of alkylbenzenes in the reversed-phase mode. The optimized monolithic columns gave plate heights ranged between 70 and 80 μm. The resulting monoliths were also satisfactorily applied to the separation of proteins. - Highlights: • Successful surface etching of PTFE inner wall tubing was done. • The modified PTFE support was next methacryloylated with GMA. • Organic polymeric monolith was in situ prepared in the functionalized PTFE tube. • The monolithic columns gave suitable pressure resistance and separation of proteins.

Preparation of organic monolithic columns in polytetrafluoroethylene tubes for reversed-phase liquid chromatography

Energy Technology Data Exchange (ETDEWEB)

Catalá-Icardo, M., E-mail: mocaic@qim.upv.es [Research Institute for Integrated Management of Coastal Areas, Universitat Politècnica de València, Paranimf 1, 46730, Grao de Gandía, Valencia (Spain); Torres-Cartas, S.; Meseguer-Lloret, S.; Gómez-Benito, C. [Research Institute for Integrated Management of Coastal Areas, Universitat Politècnica de València, Paranimf 1, 46730, Grao de Gandía, Valencia (Spain); Carrasco-Correa, E.; Simó-Alfonso, E.F.; Ramis-Ramos, G. [Department of Analytical Chemistry, Universitat de València, Dr. Moliner 50, 46100, Burjassot, Valencia (Spain); Herrero-Martínez, J.M., E-mail: jmherrer@uv.es [Department of Analytical Chemistry, Universitat de València, Dr. Moliner 50, 46100, Burjassot, Valencia (Spain)

2017-04-01

In this work, a method for the preparation and anchoring of polymeric monoliths in a polytetrafluoroethylene (PTFE) tubing as a column housing for microbore HPLC is described. In order to assure a covalent attachment of the monolith to the inner wall of the PTFE tube, a two-step procedure was developed. Two surface etching reagents, a commercial sodium naphthalene solution (Fluoroetch{sup ®}), or mixtures of H{sub 2}O{sub 2} and H{sub 2}SO{sub 4}, were tried and compared. Then, the obtained hydroxyl groups on the PTFE surface were modified by methacryloylation. Attenuated total reflectance Fourier-transform infrared (ATR-FTIR) spectroscopy and scanning electron microscopy (SEM) confirmed the successful modification of the tubing wall and the stable anchorage of monolith to the wall, respectively. Special emphasis was also put on the reduction of the unwanted effects of shrinking of monolith during polymerization, by using an external proper mold and by selecting the adequate monomers in order to increase the flexibility of the polymer. Poly(glycidyl methacrylate-co-divinylbenzene) monoliths were in situ synthesized by thermal polymerization within the confines of surface-vinylized PTFE tubes. The modified PTFE tubing tightly held the monolith, and the monolithic column exhibited good pressure resistance up to 20 MPa. The column performance was also evaluated via the isocratic separation of a series of alkylbenzenes in the reversed-phase mode. The optimized monolithic columns gave plate heights ranged between 70 and 80 μm. The resulting monoliths were also satisfactorily applied to the separation of proteins. - Highlights: • Successful surface etching of PTFE inner wall tubing was done. • The modified PTFE support was next methacryloylated with GMA. • Organic polymeric monolith was in situ prepared in the functionalized PTFE tube. • The monolithic columns gave suitable pressure resistance and separation of proteins.

Growth and Brilliant Photo-Emission of Crystalline Hexagonal Column of Alq3 Microwires

Directory of Open Access Journals (Sweden)

Seokho Kim

2018-03-01

Full Text Available We report the growth and nanoscale luminescence characteristics of 8-hydroxyquinolinato aluminum (Alq3 with a crystalline hexagonal column morphology. Pristine Alq3 nanoparticles (NPs were prepared using a conventional reprecipitation method. Crystal hexagonal columns of Alq3 were grown by using a surfactant-assisted self-assembly technique as an adjunct to the aforementioned reprecipitation method. The formation and structural properties of the crystalline and non-crystalline Alq3 NPs were analyzed with scanning electron microscopy and X-ray diffraction. The nanoscale photoluminescence (PL characteristics and the luminescence color of the Alq3 single NPs and their crystal microwires (MWs were evaluated from color charge-coupled device images acquired using a high-resolution laser confocal microscope. In comparison with the Alq3 NPs, the crystalline MWs exhibited a very bright and sharp emission. This enhanced and sharp emission from the crystalline Alq3 single MWs originated from effective π-π stacking of the Alq3 molecules due to strong interactions in the crystalline structure.

Is light narrowing possible with dense-vapor paraffin coated cells for atomic magnetometers?

Science.gov (United States)

Han, Runqi; Balabas, Mikhail; Hovde, Chris; Li, Wenhao; Roig, Hector Masia; Wang, Tao; Wickenbrock, Arne; Zhivun, Elena; You, Zheng; Budker, Dmitry

2017-12-01

We investigated the operation of an all-optical rubidium-87 atomic magnetometer with amplitude-modulated light. To study the suppression of spin-exchange relaxation, three schemes of pumping were implemented with room-temperature and heated paraffin coated vacuum cells. Efficient pumping and accumulation of atoms in the F=2 ground state were obtained. However, the sought-for narrowing of the resonance lines has not been achieved. A theoretical analysis of the polarization degree is presented to illustrate the absence of light narrowing due to radiation trapping at high temperature.

PULSE COLUMN

Science.gov (United States)

Grimmett, E.S.

1964-01-01

This patent covers a continuous countercurrent liquidsolids contactor column having a number of contactor states each comprising a perforated plate, a layer of balls, and a downcomer tube; a liquid-pulsing piston; and a solids discharger formed of a conical section at the bottom of the column, and a tubular extension on the lowest downcomer terminating in the conical section. Between the conical section and the downcomer extension is formed a small annular opening, through which solids fall coming through the perforated plate of the lowest contactor stage. This annular opening is small enough that the pressure drop thereacross is greater than the pressure drop upward through the lowest contactor stage. (AEC)

Treatment of Copper Contaminated Municipal Wastewater by Using UASB Reactor and Sand-Chemically Carbonized Rubber Wood Sawdust Column

Directory of Open Access Journals (Sweden)

Swarup Biswas

2016-01-01

Full Text Available The performance of a laboratory scale upflow anaerobic sludge blanket (UASB reactor and its posttreatment unit of sand-chemically carbonized rubber wood sawdust (CCRWSD column system for the treatment of a metal contaminated municipal wastewater was investigated. Copper ion contaminated municipal wastewater was introduced to a laboratory scale UASB reactor and the effluent from UASB reactor was then followed by treatment with sand-CCRWSD column system. The laboratory scale UASB reactor and column system were observed for a period of 121 days. After the posttreatment column the average removal of monitoring parameters such as copper ion concentration (91.37%, biochemical oxygen demand (BODT (93.98%, chemical oxygen demand (COD (95.59%, total suspended solid (TSS (95.98%, ammonia (80.68%, nitrite (79.71%, nitrate (71.16%, phosphorous (44.77%, total coliform (TC (99.9%, and fecal coliform (FC (99.9% was measured. The characterization of the chemically carbonized rubber wood sawdust was done by scanning electron microscope (SEM, X-ray fluorescence spectrum (XRF, and Fourier transforms infrared spectroscopy (FTIR. Overall the system was found to be an efficient and economical process for the treatment of copper contaminated municipal wastewater.

Treatment of Copper Contaminated Municipal Wastewater by Using UASB Reactor and Sand-Chemically Carbonized Rubber Wood Sawdust Column.

Science.gov (United States)

Biswas, Swarup; Mishra, Umesh

2016-01-01

The performance of a laboratory scale upflow anaerobic sludge blanket (UASB) reactor and its posttreatment unit of sand-chemically carbonized rubber wood sawdust (CCRWSD) column system for the treatment of a metal contaminated municipal wastewater was investigated. Copper ion contaminated municipal wastewater was introduced to a laboratory scale UASB reactor and the effluent from UASB reactor was then followed by treatment with sand-CCRWSD column system. The laboratory scale UASB reactor and column system were observed for a period of 121 days. After the posttreatment column the average removal of monitoring parameters such as copper ion concentration (91.37%), biochemical oxygen demand (BODT) (93.98%), chemical oxygen demand (COD) (95.59%), total suspended solid (TSS) (95.98%), ammonia (80.68%), nitrite (79.71%), nitrate (71.16%), phosphorous (44.77%), total coliform (TC) (99.9%), and fecal coliform (FC) (99.9%) was measured. The characterization of the chemically carbonized rubber wood sawdust was done by scanning electron microscope (SEM), X-ray fluorescence spectrum (XRF), and Fourier transforms infrared spectroscopy (FTIR). Overall the system was found to be an efficient and economical process for the treatment of copper contaminated municipal wastewater.

Performance of RC columns with partial length corrosion

International Nuclear Information System (INIS)

Wang Xiaohui; Liang Fayun

2008-01-01

Experimental and analytical studies on the load capacity of reinforced concrete (RC) columns with partial length corrosion are presented, where only a fraction of the column length was corroded. Twelve simply supported columns were eccentrically loaded. The primary variables were partial length corrosion in tensile or compressive zone and the corrosion level within this length. The failure of the corroded column occurs in the partial length, mainly developed from or located nearby or merged with the longitudinal corrosion cracks. For RC column with large eccentricity, load capacity of the column is mainly influenced by the partial length corrosion in tensile zone; while for RC column with small eccentricity, load capacity of the column greatly decreases due to the partial length corrosion in compressive zone. The destruction of the longitudinally mechanical integrality of the column in the partial length leads to this great reduction of the load capacity of the RC column

In-situ measurement of magnetic field gradient in a magnetic shield by a spin-exchange relaxation-free magnetometer

International Nuclear Information System (INIS)

Fang Jian-Cheng; Wang Tao; Li Yang; Cai Hong-Wei; Zhang Hong

2015-01-01

A method of measuring in-situ magnetic field gradient is proposed in this paper. The magnetic shield is widely used in the atomic magnetometer. However, there is magnetic field gradient in the magnetic shield, which would lead to additional gradient broadening. It is impossible to use an ex-situ magnetometer to measure magnetic field gradient in the region of a cell, whose length of side is several centimeters. The method demonstrated in this paper can realize the in-situ measurement of the magnetic field gradient inside the cell, which is significant for the spin relaxation study. The magnetic field gradients along the longitudinal axis of the magnetic shield are measured by a spin-exchange relaxation-free (SERF) magnetometer by adding a magnetic field modulation in the probe beam’s direction. The transmissivity of the cell for the probe beam is always inhomogeneous along the pump beam direction, and the method proposed in this paper is independent of the intensity of the probe beam, which means that the method is independent of the cell’s transmissivity. This feature makes the method more practical experimentally. Moreover, the AC-Stark shift can seriously degrade and affect the precision of the magnetic field gradient measurement. The AC-Stark shift is suppressed by locking the pump beam to the resonance of potassium’s D1 line. Furthermore, the residual magnetic fields are measured with σ + - and σ – -polarized pump beams, which can further suppress the effect of the AC-Stark shift. The method of measuring in-situ magnetic field gradient has achieved a magnetic field gradient precision of better than 30 pT/mm. (paper)

29 CFR 1926.755 - Column anchorage.

Science.gov (United States)

2010-07-01

... 29 Labor 8 2010-07-01 2010-07-01 false Column anchorage. 1926.755 Section 1926.755 Labor... (CONTINUED) SAFETY AND HEALTH REGULATIONS FOR CONSTRUCTION Steel Erection § 1926.755 Column anchorage. (a) General requirements for erection stability. (1) All columns shall be anchored by a minimum of 4 anchor...

Adsorption columns for use in radioimmunoassays

International Nuclear Information System (INIS)

1976-01-01

Adsorption columns are provided which can be utilized in radioimmunoassay systems such as those involving the separation of antibody-antigen complexes from free antigens. The preparation of the columns includes the treatment of retaining substrate material to render it hydrophilic, preparation and degassing of the separation material and loading the column

Development and applications of radiotracers technologies and gamma scanning

International Nuclear Information System (INIS)

Conejo, Mario; Chaverri, Oscar; Chine, Bruno; Vargas, Celso

2008-01-01

The radiotracers and gamma scanning technologies are very consolidated tools for studying, analyzing and evaluating of industrial processes. The development and the results of radiotracers and gamma scanning technologies applied in laboratory and more complex systems, are reported. The radiotracers technology was used to study boron diffusion during the curing process of the wood, to evaluate a lagoon of sewage treatment with aquatic iris plants and to carry out experimental work with controlled variables in a laboratory hydraulic circuit (flow rig). The gamma scanning technique was used to analyze a pilot tower in the laboratories. The main results achieved with the experiments were the following: 1) the boron absorption as a wood curing agent depends on the section of wood exposed to the curing solution; 2) during the tests effectuated with Iodine 131, the aquatic iris plants situated in the water treatment lagoon absorb part of the radiotracer, making difficult the residence time determination; 3) the sensibility of the system Cesium 137 source and detector is sufficiently high and can detect low radioactive absorption materials, situated inside columns with steel walls. (author) [es

NMFS Water Column Sonar Database

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — Water column sonar data are an important component of fishery independent surveys, habitat studies and other research. NMFS water column sonar data are archived here.

A novel in situ strategy for the preparation of a β-cyclodextrin/polydopamine-coated capillary column for capillary electrochromatography enantioseparations.

Science.gov (United States)

Guo, Heying; Niu, Xiaoying; Pan, Congjie; Yi, Tao; Chen, Hongli; Chen, Xingguo

2017-06-01

Inspired by the chiral recognition ability of β-cyclodextrin and the natural adhesive properties of polydopamine under alkaline conditions, in this study, a rapid and in situ modification strategy was developed to fabricate β-cyclodextrin/polydopamine composite material coated-capillary columns for open tubular capillary electrochromatography. The results of scanning electron microscopy, FTIR spectroscopy, streaming potential, and electro-osmotic flow studies indicated that β-cyclodextrin/polydopamine was successfully fixed on the inner wall of the capillary column. This coating can be achieved within 1 h affording a greatly reduced capillary preparation time. The performance of the β-cyclodextrin/polydopamine-coated capillary was validated by the analysis of seven pairs of chiral analytes, namely epinephrine, norepinephrine, isoprenaline, terbutaline, verapamil, tryptophane, carvedilol. Good enantioseparation efficiencies were achieved for all. For three consecutive runs, the relative standard deviations for the migration times of the analytes for intraday, interday, and column-to-column repeatability were in the range of 0.41-1.74, 1.03-4.18, and 1.66-8.24%, respectively. Moreover, the separation efficiency of the β-cyclodextrin/polydopamine-coated capillary column did not decrease obviously over 90 runs. The strategy should also be feasible to introduce and immobilize other chiral selectors on the inner walls surface of capillary columns. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Investigating the Effect of Column Geometry on Separation Efficiency using 3D Printed Liquid Chromatographic Columns Containing Polymer Monolithic Phases.

Science.gov (United States)

Gupta, Vipul; Beirne, Stephen; Nesterenko, Pavel N; Paull, Brett

2018-01-16

Effect of column geometry on the liquid chromatographic separations using 3D printed liquid chromatographic columns with in-column polymerized monoliths has been studied. Three different liquid chromatographic columns were designed and 3D printed in titanium as 2D serpentine, 3D spiral, and 3D serpentine columns, of equal length and i.d. Successful in-column thermal polymerization of mechanically stable poly(BuMA-co-EDMA) monoliths was achieved within each design without any significant structural differences between phases. Van Deemter plots indicated higher efficiencies for the 3D serpentine chromatographic columns with higher aspect ratio turns at higher linear velocities and smaller analysis times as compared to their counterpart columns with lower aspect ratio turns. Computational fluid dynamic simulations of a basic monolithic structure indicated 44%, 90%, 100%, and 118% higher flow through narrow channels in the curved monolithic configuration as compared to the straight monolithic configuration at linear velocities of 1, 2.5, 5, and 10 mm s -1 , respectively. Isocratic RPLC separations with the 3D serpentine column resulted in an average 23% and 245% (8 solutes) increase in the number of theoretical plates as compared to the 3D spiral and 2D serpentine columns, respectively. Gradient RPLC separations with the 3D serpentine column resulted in an average 15% and 82% (8 solutes) increase in the peak capacity as compared to the 3D spiral and 2D serpentine columns, respectively. Use of the 3D serpentine column at a higher flow rate, as compared to the 3D spiral column, provided a 58% reduction in the analysis time and 74% increase in the peak capacity for the isocratic separations of the small molecules and the gradient separations of proteins, respectively.

Scanning SQUID microscope with an in-situ magnetization/demagnetization field for geological samples

Science.gov (United States)

Du, Junwei; Liu, Xiaohong; Qin, Huafeng; Wei, Zhao; Kong, Xiangyang; Liu, Qingsong; Song, Tao

2018-04-01

Magnetic properties of rocks are crucial for paleo-, rock-, environmental-magnetism, and magnetic material sciences. Conventional rock magnetometers deal with bulk properties of samples, whereas scanning microscope can map the distribution of remanent magnetization. In this study, a new scanning microscope based on a low-temperature DC superconducting quantum interference device (SQUID) equipped with an in-situ magnetization/demagnetization device was developed. To realize the combination of sensitive instrument as SQUID with high magnetizing/demagnetizing fields, the pick-up coil, the magnetization/demagnetization coils and the measurement mode of the system were optimized. The new microscope has a field sensitivity of 250 pT/√Hz at a coil-to-sample spacing of ∼350 μm, and high magnetization (0-1 T)/ demagnetization (0-300 mT, 400 Hz) functions. With this microscope, isothermal remanent magnetization (IRM) acquisition and the according alternating field (AF) demagnetization curves can be obtained for each point without transferring samples between different procedures, which could result in position deviation, waste of time, and other interferences. The newly-designed SQUID microscope, thus, can be used to investigate the rock magnetic properties of samples at a micro-area scale, and has a great potential to be an efficient tool in paleomagnetism, rock magnetism, and magnetic material studies.

High-resolution, high-throughput imaging with a multibeam scanning electron microscope.

Science.gov (United States)

Eberle, A L; Mikula, S; Schalek, R; Lichtman, J; Knothe Tate, M L; Zeidler, D

2015-08-01

Electron-electron interactions and detector bandwidth limit the maximal imaging speed of single-beam scanning electron microscopes. We use multiple electron beams in a single column and detect secondary electrons in parallel to increase the imaging speed by close to two orders of magnitude and demonstrate imaging for a variety of samples ranging from biological brain tissue to semiconductor wafers. © 2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.

Evaluation of Packed Distillation Columns I - Atmospheric Pressure

National Research Council Canada - National Science Library

Reynolds, Thaine

1951-01-01

.... Four column-packing combinations of the glass columns and four column-packing combinations of the steel columns were investigated at atmospheric pressure using a test mixture of methylcyclohexane...

Center column design of the PLT

International Nuclear Information System (INIS)

Citrolo, J.; Frankenberg, J.

1975-01-01

The center column of the PLT machine is a secondary support member for the toroidal field coils. Its purpose is to decrease the bending moment at the nose of the coils. The center column design was to have been a stainless steel casting with the toroidal field coils grouped around the casting at installation, trapping it in place. However, the castings developed cracks during fabrication and were unsuitable for use. Installation of the coils proceeded without the center column. It then became necessary to redesign a center column which would be capable of installation with the toroidal field coils in place. The final design consists of three A-286 forgings. This paper discusses the final center column design and the influence that new knowledge, obtained during the power tests, had on the new design

The handedness of historiated spiral columns.

Science.gov (United States)

Couzin, Robert

2017-09-01

Trajan's Column in Rome (AD 113) was the model for a modest number of other spiral columns decorated with figural, narrative imagery from antiquity to the present day. Most of these wind upwards to the right, often with a congruent spiral staircase within. A brief introductory consideration of antique screw direction in mechanical devices and fluted columns suggests that the former may have been affected by the handedness of designers and the latter by a preference for symmetry. However, for the historiated columns that are the main focus of this article, the determining factor was likely script direction. The manner in which this operated is considered, as well as competing mechanisms that might explain exceptions. A related phenomenon is the reversal of the spiral in a non-trivial number of reproductions of the antique columns, from Roman coinage to Renaissance and baroque drawings and engravings. Finally, the consistent inattention in academic literature to the spiral direction of historiated columns and the repeated publication of erroneous earlier reproductions warrants further consideration.

Column-oriented database management systems

OpenAIRE

Možina, David

2013-01-01

In the following thesis I will present column-oriented database. Among other things, I will answer on a question why there is a need for a column-oriented database. In recent years there have been a lot of attention regarding a column-oriented database, even if the existence of a columnar database management systems dates back in the early seventies of the last century. I will compare both systems for a database management – a colum-oriented database system and a row-oriented database system ...

A summary of the results from the UCLA OGO-5 fluxgate magnetometer

Science.gov (United States)

Coleman, P. J., Jr.; Russell, C. T.

1973-01-01

The OGO-5 fluxgate magnetometer experiment (E-14) was designed to measure the vector magnetic field over the full range of the OGO-5 orbit. Thus, it had a dynamic range of + or - 64,000 gamma yet it maintained a precision of + or - 1/16 gamma at all times. This enabled a broad spectrum of problems to be attached. Studies of the magnetospheric waves, currents, waves-particle interactions, pitch angle distributions and wave normal directions were made. The structure of the magnetopause, the magnetotail, and bow shock were probed, waves and discontinuities in the solar wind were examined and the various phases of substorms were examined in depth.

Airborne gamma-ray spectrometer and magnetometer survey, Wainwright Quadrangle, Alaska. Final report

International Nuclear Information System (INIS)

1981-03-01

The results obtained from a gamma-ray spectrometer and magnetometer survey over the Wainwright map area of Alaska are presented. Based on the criteria outlined in the general section of interpretation, a total of seven uranium anomalies have been outlined on the interpretation map. With the exception of Anomaly 1, all are located over the higher terrain of the foothills in the southern portion of the quadrangle. All seven anomalies are only weakly to moderately anomalous. There are no indications anywhere within the area of any significant preferential accumulations of uranium. None of the anomalies are thought to be of any economic importance. No follow-up work is recommended

Radiotracer Imaging of Sediment Columns

Science.gov (United States)

Moses, W. W.; O'Neil, J. P.; Boutchko, R.; Nico, P. S.; Druhan, J. L.; Vandehey, N. T.

2010-12-01

Nuclear medical PET and SPECT cameras routinely image radioactivity concentration of gamma ray emitting isotopes (PET - 511 keV; SPECT - 75-300 keV). We have used nuclear medical imaging technology to study contaminant transport in sediment columns. Specifically, we use Tc-99m (T1/2 = 6 h, Eγ = 140 keV) and a SPECT camera to image the bacteria mediated reduction of pertechnetate, [Tc(VII)O4]- + Fe(II) → Tc(IV)O2 + Fe(III). A 45 mL bolus of Tc-99m (32 mCi) labeled sodium pertechnetate was infused into a column (35cm x 10cm Ø) containing uranium-contaminated subsurface sediment from the Rifle, CO site. A flow rate of 1.25 ml/min of artificial groundwater was maintained in the column. Using a GE Millennium VG camera, we imaged the column for 12 hours, acquiring 44 frames. As the microbes in the sediment were inactive, we expected most of the iron to be Fe(III). The images were consistent with this hypothesis, and the Tc-99m pertechnetate acted like a conservative tracer. Virtually no binding of the Tc-99m was observed, and while the bolus of activity propagated fairly uniformly through the column, some inhomogeneity attributed to sediment packing was observed. We expect that after augmentation by acetate, the bacteria will metabolically reduce Fe(III) to Fe(II), leading to significant Tc-99m binding. Imaging sediment columns using nuclear medicine techniques has many attractive features. Trace quantities of the radiolabeled compounds are used (micro- to nano- molar) and the half-lives of many of these tracers are short (Image of Tc-99m distribution in a column containing Rifle sediment at four times.

Physical properties and structure of fine core-shell particles used as packing materials for chromatography Relationships between particle characteristics and column performance.

Science.gov (United States)

Gritti, Fabrice; Leonardis, Irene; Abia, Jude; Guiochon, Georges

2010-06-11

The recent development of new brands of packing materials made of fine porous-shell particles, e.g., Halo and Kinetex, has brought great improvements in potential column efficiency, demanding considerable progress in the design of chromatographic instruments. Columns packed with Halo and Kinetex particles provide minimum values of their reduced plate heights of nearly 1.5 and 1.2, respectively. These packing materials have physical properties that set them apart from conventional porous particles. The kinetic performance of 4.6mm I.D. columns packed with these two new materials is analyzed based on the results of a series of nine independent and complementary experiments: low-temperature nitrogen adsorption (LTNA), scanning electron microscopy (SEM), inverse size-exclusion chromatography (ISEC), Coulter counter particle size distributions, pycnometry, height equivalent to a theoretical plate (HETP), peak parking method (PP), total pore blocking method (TPB), and local electrochemical detection across the column exit section (LED). The results of this work establish links between the physical properties of these superficially porous particles and the excellent kinetic performance of columns packed with them. It clarifies the fundamental origin of the difference in the chromatographic performances of the Halo and the Kinetex columns. Copyright 2010 Elsevier B.V. All rights reserved.

Carbon monoxide column retrieval for clear-sky and cloudy atmospheres : A full-mission data set from SCIAMACHY 2.3 μm reflectance measurements

NARCIS (Netherlands)

Borsdorff, Tobias; De Brugh, Joost Aan; Hu, Haili; Nédélec, Philippe; Aben, Ilse; Landgraf, Jochen

2017-01-01

We discuss the retrieval of carbon monoxide (CO) vertical column densities from clear-sky and cloud contaminated 2311-2338 nm reflectance spectra measured by the Scanning Imaging Absorption Spectrometer for Atmospheric Chartography (SCIAMACHY) from January 2003 until the end of the mission in April

Thermally stable dexsil-400 glass capillary columns

International Nuclear Information System (INIS)

Maskarinec, M.P.; Olerich, G.

1980-01-01

The factors affecting efficiency, thermal stability, and reproducibility of Dexsil-400 glass capillary columns for gas chromatography in general, and for polycyclic aromatic hydrocarbons (PAHs) in particular were investigated. Columns were drawn from Kimble KG-6 (soda-lime) glass or Kimox (borosilicate) glass. All silylation was carried out at 200 0 C. Columns were coated according to the static method. Freshly prepared, degassed solutions of Dexsil-400 in pentane or methylene chloride were used. Thermal stability of the Dexsil 400 columns with respect to gas chromatography/mass spectrometry (GC/MS) were tested. Column-to-column variability is a function of each step in the fabrication of the columns. The degree of etching, extent of silylation, and stationary phase film thickness must be carefully controlled. The variability in two Dexsil-400 capillary column prepared by etching, silylation with solution of hexa methyl disilazone (HMDS), and static coating is shown and also indicates the excellent selectivity of Dexsil-400 for the separation of alkylated aromatic compounds. The wide temperature range of Dexsil-400 and the high efficiency of the capillary columns also allow the analysis of complex mixtures with minimal prefractionation. Direct injection of a coal liquefaction product is given. Analysis by GC/MS indicated the presence of parent PAHs, alkylated PAHs, nitrogen and sulfur heterocycles, and their alkylated derivatives. 4 figures

Safety barriers and lighting columns.

NARCIS (Netherlands)

Schreuder, D.A.

1972-01-01

Problems arising from the sitting of lighting columns on the central reserve are reviewed, and remedial measures such as break-away lighting supports and installation of safety fences on the central reserve on both sides of the lighting columns are examined.

Computed Tomography Based Three-dimensional Measurements of Spine Shortening Distance After Posterior Three-column Osteotomies for the Treatment of Severe and Stiff Scoliosis.

Science.gov (United States)

Li, Xue-Shi; Huang, Zi-Fang; Deng, Yao-Long; Fan, Heng-Wei; Sui, Wen-Yuan; Wang, Chong-Wen; Yang, Jun-Lin

2017-07-15

Retrospective study. This study is to measure and analyze the changes of three-dimensional (3D) distances of spinal column and spinal canal at the three-column osteotomy sites and address their clinical and neurologic significance. Three-column osteotomies were developed to treat severe and stiff spine deformities with insufficient understanding on the safe limit of spine shortening and the relationship between the shortening distance of the spinal column and that of the spinal canal. Records of 52 continuous patients with severe and stiff scoliosis treated with three-column spine osteotomies at our institution from July 2013 to June 2015 were reviewed. The preoperative spinal cord function classification were type A in 31 cases, type B in 10 cases, and type C in 11 cases. The types of osteotomies carried out were extended pedicle subtraction osteotomy in nine patients and posterior vertebral column resection in 43 patients. Multimodality neuromonitoring strategies were adopted intraoperatively. 3D pre- and postoperative spine models were reconstructed from the computed tomography (CT) scans. The distances of convex and concave spinal column and the spinal canal shortening were measured and analyzed. The spinal column shortening distance (SCSD) measured on the 3D models (27.8 mm) were statistically shorter than those measured intraoperatively (32.8 mm) (P column strut graft than in those with bone-on-bone fusion (P column cannot represent that of the central spinal canal in patients with severe scoliosis. The spinal column shortening procedure in appropriately selected patient groups with bone-on-bone fusion is a viable option with the CCSD being significantly shorter than the convex SCSD. 4.

Preparation and evaluation of open-tubular capillary column combining a metal-organic framework and a brush-shaped polymer for liquid chromatography.

Science.gov (United States)

Chen, Kai; Zhang, Lingyi; Zhang, Weibing

2018-03-30

In this work, an open-tubular capillary liquid-phase column was prepared by modifying chain polymer on the inner surface of capillary and chemical bonding of metal organic frameworks, NH 2 -UiO-66, to the brushes of chain polymer (poly(glycidyl methacrylate)). Besides advantages of facial preparation and good permeability, the chain polymer effectively increases the modification amount of NH 2 -UiO-66 nanoparticles to increase the phase ratio of open-tubular capillary column and enhance the interactions with analytes. The results of scanning electron microscope energy-dispersive X-ray spectra indicated that NH 2 -UiO-66 nanoparticles were successfully bonded to the chain polymer. Because of the hydrophobic interaction and hydrogen bonding interaction between the analytes and the ligand of NH 2 -UiO-66, different analytes were well separated on the NH 2 -UiO-66-modified poly(glycidyl methacrylate) capillary (1.12 m × 25 μm id × 365 μm od) with the high absolute column efficiency reaching 121 477 plates, benefiting from an open-tubular column and low mass transfer resistance provided by polymer brush and metal-organic framework crystal. The relative standard deviations of the retention time for run-to-run, day-to-day, and column-to-column (n = 3) runs are below 4.28%, exhibiting good repeatability. Finally, the column was successfully applied to separation of flavonoids in licorice. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Temperature-assisted On-column Solute Focusing: A General Method to Reduce Pre-column Dispersion in Capillary High Performance Liquid Chromatography

Science.gov (United States)

Groskreutz, Stephen R.; Weber, Stephen G.

2014-01-01

Solvent-based on-column focusing is a powerful and well known approach for reducingthe impact of pre-column dispersion in liquid chromatography. Here we describe an orthogonal temperature-based approach to focusing called temperature-assisted on-column solute focusing (TASF). TASF is founded on the same principles as the more commonly used solvent-based method wherein transient conditions are created thatlead to high solute retention at the column inlet. Combining the low thermal mass of capillary columns and the temperature dependence of solute retentionTASF is used effectivelyto compress injection bands at the head of the column through the transient reduction in column temperature to 5 °C for a defined 7 mm segment of a 6 cm long 150 μm I.D. column. Following the 30 second focusing time, the column temperature is increased rapidly to the separation temperature of 60 °C releasing the focused band of analytes. We developed a model tosimulate TASF separations based on solute retention enthalpies, focusing temperature, focusing time, and column parameters. This model guides the systematic study of the influence of sample injection volume on column performance.All samples have solvent compositions matching the mobile phase. Over the 45 to 1050 nL injection volume range evaluated, TASF reducesthe peak width for all soluteswith k’ greater than or equal to 2.5, relative to controls. Peak widths resulting from injection volumes up to 1.3 times the column fluid volume with TASF are less than 5% larger than peak widths from a 45 nL injection without TASF (0.07 times the column liquid volume). The TASF approach reduced concentration detection limits by a factor of 12.5 relative to a small volume injection for low concentration samples. TASF is orthogonal to the solvent focusing method. Thus, it canbe used where on-column focusing is required, but where implementation of solvent-based focusing is difficult. PMID:24973805

Heat Transfer Analysis for a Fixed CST Column

International Nuclear Information System (INIS)

Lee, S.Y.

2004-01-01

In support of a small column ion exchange (SCIX) process for the Savannah River Site waste processing program, a transient two-dimensional heat transfer model that includes the conduction process neglecting the convection cooling mechanism inside the crystalline silicotitanate (CST) column has been constructed and heat transfer calculations made for the present design configurations. For this situation, a no process flow condition through the column was assumed as one of the reference conditions for the simulation of a loss-of-flow accident. A series of the modeling calculations has been performed using a computational heat transfer approach. Results for the baseline model indicate that transit times to reach 130 degrees Celsius maximum temperature of the CST-salt solution column are about 96 hours when the 20-in CST column with 300 Ci/liter heat generation source and 25 degrees Celsius initial column temperature is cooled by natural convection of external air as a primary heat transfer mechanism. The modeling results for the 28-in column equipped with water jacket systems on the external wall surface of the column and water coolant pipe at the center of the CST column demonstrate that the column loaded with 300 Ci/liter heat source can be maintained non-boiling indefinitely. Sensitivity calculations for several alternate column sizes, heat loads of the packed column, engineered cooling systems, and various ambient conditions at the exterior wall of the column have been performed under the reference conditions of the CST-salt solution to assess the impact of those parameters on the peak temperatures of the packed column for a given transient time. The results indicate that a water-coolant pipe at the center of the CST column filled with salt solution is the most effective one among the potential design parameters related to the thermal energy dissipation of decay heat load. It is noted that the cooling mechanism at the wall boundary of the column has significant

NON-LINEAR ANALYSIS OF AN EXPERIMENTAL JOINT OF COLUMN AND BEAMS OF ARMED CONCRETE-STEEL COLUMN FOR FRAME

Directory of Open Access Journals (Sweden)

Nelson López

2017-12-01

Full Text Available In this research, the nonlinear behavior of a real-scale experimental joint (node is studied, consisting of three reinforced concrete elements, one column and two beams joined to a structural steel column at the upper level. In the numerical analysis the model of the union was analyzed in the inelastic range, this model was elaborated with the finite element program based on fibers, SeismoStruct to analyze as a function of time, the traction and compression efforts in the confined area and not confined area of the concrete column and in the longitudinal reinforcement steel, as well as verification of the design of the base plate that joins the two columns. The results showed that tensile stresses in the unconfined zone surpassed the concrete breaking point, with cracking occurring just below the lower edge of the beams; in the confined area the traction efforts were much lower, with cracks occurring later than in the non-confined area. The concrete column-steel column joint behaved as a rigid node, so the elastic design was consistent with the calculation methodology of base plates for steel columns.

Measurements of Nitrogen Dioxide Total Column Amounts using a Brewer Double Spectrophotometer in Direct Sun Mode

Science.gov (United States)

Cede, Alexander; Herman, Jay; Richter, Andreas; Krotkov, Nickolay; Burrows, John

2006-01-01

NO2 column amounts were measured for the past 2 years at Goddard Space Flight Center, Greenbelt, Maryland, using a Brewer spectrometer in direct Sun mode. A new bootstrap method to calibrate the instrument is introduced and described. This technique selects the cleanest days from the database to obtain the solar reference spectrum. The main advantage for direct Sun measurements is that the conversion uncertainty from slant column to vertical column is negligible compared to the standard scattered light observations where it is typically on the order of 100% (2sigma) at polluted sites. The total 2sigma errors of the direct Sun retrieved column amounts decrease with solar zenith angle and are estimated at 0.2 to 0.6 Dobson units (DU, 1 DU approx. equal to 2.7 10(exp 16) molecules cm(exp -2)), which is more accurate than scattered light measurements for high NO2 amounts. Measured NO2 column amounts, ranging from 0 to 3 DU with a mean of 0.7 DU, show a pronounced daily course and a strong variability from day to day. The NO2 concentration typically increases from sunrise to noon. In the afternoon it decreases in summer and stays constant in winter. As expected from the anthropogenic nature of its source, NO2 amounts on weekends are significantly reduced. The measurements were compared to satellite retrievals from Scanning Image Absorption Spectrometer for Atmospheric Chartography (SCIAMACHY). Satellite data give the same average NO2 column and show a seasonal cycle that is similar to the ground data in the afternoon. We show that NO2 must be considered when retrieving aerosol absorption properties, especially for situations with low aerosol optical depth.

Fabrication of a micrometer Ni–Cu alloy column coupled with a Cu micro-column for thermal measurement

International Nuclear Information System (INIS)

Lin, J C; Chang, T K; Yang, J H; Jeng, J H; Lee, D L; Jiang, S B

2009-01-01

Micrometer Ni–Cu alloy columns have been fabricated by the micro-anode-guided electroplating (MAGE) process in the citrate bath. The surface morphology and chemical composition of the micro-columns were determined by copper concentration in the bath and by the electrical bias of MAGE. When fabricated in a bath of dilute copper (i.e. 4 mM) at lower voltages (e.g. 3.8 and 4.0 V), the alloy micro-columns revealed uniform diameter and smooth appearance. The alloy composition demonstrated an increase in the wt% ratio of Ni/Cu from 75/25, 80/20, 83/17 to 87/13 with increasing electrical bias from 3.8, 4.0, 4.2 to 4.4 V. However, it decreases from 75/25, 57/43 to 47/53 with increasing copper concentration from 4, 8 to 12 mM in the bath. Citrate plays a role in forming complexes with nickel and copper at similar reduction potentials, thus reducing simultaneously to Ni–Cu alloy. The mechanism for fabricating alloy micro-columns could be delineated on the basis of cathodic polarization of the complexes. A couple of micro-columns were fabricated using MAGE in constructing a pure copper micro-column on the top of a Ni/Cu (at 47/53) alloy micro-column. This micro-thermocouple provides a satisfactory measurement with good sensitivity and precision

Fabrication of a novel hemin-based monolithic column and its application in separation of protein from complex bio-matrix.

Science.gov (United States)

Jiang, Xiaoya; Zhang, Doudou; Li, Xueying; Wang, Xixi; Bai, Ligai; Liu, Haiyan; Yan, Hongyuan

2017-05-10

A novel polymer-based monolithic column was prepared via redox initiation system within the confines of a stainless steel column with 4.6mm i.d. In the processes, hemin and lauryl methacrylate were used as co-monomers; ethylene dimethacrylate as crosslinking agent; n-butyl alcohol, ethanediol, and N, N-dimethylformamide as tri-porogens; benzoyl peroxide and N, N-dimethyl aniline as redox initiation system. The resulting polymer-based monolithic columns were characterized by scanning electron microscopy, nitrogen adsorption-desorption instrument, and mercury intrusion porosimeter, respectively. The results illustrated that the improved monolith had relative uniform porous structure, good permeability, and low back pressure. Aromatic compounds were used to test the chromatographic behavior of the monolith, resulting in highest column efficiency of 19 880 plates per meter with reversed-phase mechanism. Furthermore, the homemade monolith was used as the stationary phase of high performance liquid chromatography to separate proteins from complex bio-matrix, including human plasma, egg white, and snailase. The results showed that the monolithic column occupied good separation ability with these complex bio-samples. Excellent specific character of the homemade hemin-based monolith was that it could simultaneously remove high-abundance proteins (including human serum albumin, immunoglobulin G, and human fibrinogen) from human plasma and separate other proteins to different fractions. Copyright © 2017 Elsevier B.V. All rights reserved.

Behavior of reinforced concrete columns strenghtened by partial jacketing

Directory of Open Access Journals (Sweden)

D. B. FERREIRA

Full Text Available This article presents the study of reinforced concrete columns strengthened using a partial jacket consisting of a 35mm self-compacting concrete layer added to its most compressed face and tested in combined compression and uniaxial bending until rupture. Wedge bolt connectors were used to increase bond at the interface between the two concrete layers of different ages. Seven 2000 mm long columns were tested. Two columns were cast monolithically and named PO (original column e PR (reference column. The other five columns were strengthened using a new 35 mm thick self-compacting concrete layer attached to the column face subjected to highest compressive stresses. Column PO had a 120mm by 250 mm rectangular cross section and other columns had a 155 mm by 250mm cross section after the strengthening procedure. Results show that the ultimate resistance of the strengthened columns was more than three times the ultimate resistance of the original column PO, indicating the effectiveness of the strengthening procedure. Detachment of the new concrete layer with concrete crushing and steel yielding occurred in the strengthened columns.

Plasma Distribution in Mercury's Magnetosphere Derived from MESSENGER Magnetometer and Fast Imaging Plasma Spectrometer Observations

Science.gov (United States)

Korth, Haje; Anderson, Brian J.; Gershman, Daniel J.; Raines, Jim M.; Slavin, James A.; Zurbuchen, Thomas H.; Solomon, Sean C.; McNutt, Ralph L.

2014-01-01

We assess the statistical spatial distribution of plasma in Mercury's magnetosphere from observations of magnetic pressure deficits and plasma characteristics by the MErcury Surface, Space ENvironment, GEochemistry, and Ranging (MESSENGER) spacecraft. The statistical distributions of proton flux and pressure were derived from 10months of Fast Imaging Plasma Spectrometer (FIPS) observations obtained during the orbital phase of the MESSENGER mission. The Magnetometer-derived pressure distributions compare favorably with those deduced from the FIPS observations at locations where depressions in the magnetic field associated with the presence of enhanced plasma pressures are discernible in the Magnetometer data. The magnitudes of the magnetic pressure deficit and the plasma pressure agree on average, although the two measures of plasma pressure may deviate for individual events by as much as a factor of approximately 3. The FIPS distributions provide better statistics in regions where the plasma is more tenuous and reveal an enhanced plasma population near the magnetopause flanks resulting from direct entry of magnetosheath plasma into the low-latitude boundary layer of the magnetosphere. The plasma observations also exhibit a pronounced north-south asymmetry on the nightside, with markedly lower fluxes at low altitudes in the northern hemisphere than at higher altitudes in the south on the same field line. This asymmetry is consistent with particle loss to the southern hemisphere surface during bounce motion in Mercury's offset dipole magnetic field.

Quantitative atomic resolution mapping using high-angle annular dark field scanning transmission electron microscopy

International Nuclear Information System (INIS)

Van Aert, S.; Verbeeck, J.; Erni, R.; Bals, S.; Luysberg, M.; Dyck, D. Van; Tendeloo, G. Van

2009-01-01

A model-based method is proposed to relatively quantify the chemical composition of atomic columns using high angle annular dark field (HAADF) scanning transmission electron microscopy (STEM) images. The method is based on a quantification of the total intensity of the scattered electrons for the individual atomic columns using statistical parameter estimation theory. In order to apply this theory, a model is required describing the image contrast of the HAADF STEM images. Therefore, a simple, effective incoherent model has been assumed which takes the probe intensity profile into account. The scattered intensities can then be estimated by fitting this model to an experimental HAADF STEM image. These estimates are used as a performance measure to distinguish between different atomic column types and to identify the nature of unknown columns with good accuracy and precision using statistical hypothesis testing. The reliability of the method is supported by means of simulated HAADF STEM images as well as a combination of experimental images and electron energy-loss spectra. It is experimentally shown that statistically meaningful information on the composition of individual columns can be obtained even if the difference in averaged atomic number Z is only 3. Using this method, quantitative mapping at atomic resolution using HAADF STEM images only has become possible without the need of simultaneously recorded electron energy loss spectra.

Recent advances in column switching sample preparation in bioanalysis.

Science.gov (United States)

Kataoka, Hiroyuki; Saito, Keita

2012-04-01

Column switching techniques, using two or more stationary phase columns, are useful for trace enrichment and online automated sample preparation. Target fractions from the first column are transferred online to a second column with different properties for further separation. Column switching techniques can be used to determine the analytes in a complex matrix by direct sample injection or by simple sample treatment. Online column switching sample preparation is usually performed in combination with HPLC or capillary electrophoresis. SPE or turbulent flow chromatography using a cartridge column and in-tube solid-phase microextraction using a capillary column have been developed for convenient column switching sample preparation. Furthermore, various micro-/nano-sample preparation devices using new polymer-coating materials have been developed to improve extraction efficiency. This review describes current developments and future trends in novel column switching sample preparation in bioanalysis, focusing on innovative column switching techniques using new extraction devices and materials.

Chromatographic properties PLOT multicapillary columns.

Science.gov (United States)

Nikolaeva, O A; Patrushev, Y V; Sidelnikov, V N

2017-03-10

Multicapillary columns (MCCs) for gas chromatography make it possible to perform high-speed analysis of the mixtures of gaseous and volatile substances at a relatively large amount of the loaded sample. The study was performed using PLOT MCCs for gas-solid chromatography (GSC) with different stationary phases (SP) based on alumina, silica and poly-(1-trimethylsilyl-1-propyne) (PTMSP) polymer as well as porous polymers divinylbenzene-styrene (DVB-St), divinylbenzene-vinylimidazole (DVB-VIm) and divinylbenzene-ethylene glycol dimethacrylate (DVB-EGD). These MCCs have the efficiency of 4000-10000 theoretical plates per meter (TP/m) and at a column length of 25-30cm can separate within 10-20s multicomponent mixtures of substances belonging to different classes of chemical compounds. The sample amount not overloading the column is 0.03-1μg and depends on the features of a porous layer. Examples of separations on some of the studied columns are considered. Copyright © 2017 Elsevier B.V. All rights reserved.

Apparatus for measurement of the electric dipole moment of the neutron using a cohabiting atomic-mercury magnetometer

Energy Technology Data Exchange (ETDEWEB)

Baker, C.A. [Rutherford Appleton Laboratory, Chilton, Didcot, Oxon OX11 0QX (United Kingdom); Chibane, Y.; Chouder, M. [University of Sussex, Falmer, Brighton BN1 9QH (United Kingdom); Geltenbort, P. [Institut Laue-Langevin, BP 156, F-38042 Grenoble Cedex 9 (France); Green, K. [Rutherford Appleton Laboratory, Chilton, Didcot, Oxon OX11 0QX (United Kingdom); Harris, P.G., E-mail: p.g.harris@sussex.ac.uk [University of Sussex, Falmer, Brighton BN1 9QH (United Kingdom); Heckel, B.R. [Department of Physics, University of Washington, Seattle, WA 98195 (United States); Iaydjiev, P.; Ivanov, S.N.; Kilvington, I. [Rutherford Appleton Laboratory, Chilton, Didcot, Oxon OX11 0QX (United Kingdom); Lamoreaux, S.K. [Department of Physics, University of Washington, Seattle, WA 98195 (United States); May, D.J.; Pendlebury, J.M.; Richardson, J.D.; Shiers, D.B.; Smith, K.F. [University of Sussex, Falmer, Brighton BN1 9QH (United Kingdom); Grinten, M. van der [Rutherford Appleton Laboratory, Chilton, Didcot, Oxon OX11 0QX (United Kingdom)

2014-02-01

A description is presented of apparatus used to carry out an experimental search for an electric dipole moment of the neutron, at the Institut Laue-Langevin (ILL), Grenoble. The experiment incorporated a cohabiting atomic-mercury magnetometer in order to reduce spurious signals from magnetic field fluctuations. The result has been published in an earlier letter [1]; here, the methods and equipment used are discussed in detail.

Column study of enhanced Cr(VI) removal and longevity by coupled abiotic and biotic processes using Fe0 and mixed anaerobic culture.

Science.gov (United States)

Zhong, Jiawei; Yin, Weizhao; Li, Yongtao; Li, Ping; Wu, Jinhua; Jiang, Gangbiao; Gu, Jingjing; Liang, Hao

2017-10-01

In this study, Fe 0 and mixed anaerobic culture were integrated in one column to investigate the coupled abiotic and biotic effects on hexa-valent chromium (Cr(VI)) removal and column longevity with an abiotic Fe 0 column in the control experiments. According to the breakthrough study, a slower Cr(VI) breakthrough rate of 0.19 cm/PV was observed in the biotic Fe 0 column whereas the value in the abiotic Fe 0 column was 0.30 cm/PV, resulting in 64% longer life-span and 62% higher Cr(VI) removal capacity in the biotic Fe 0 column than the abiotic one. The solid phase characterization by scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and X-ray diffraction (XRD) confirmed that this enhancement was attributed to the higher consumption of iron and greater production of diverse reactive minerals (e.g., green rust, magnetite and lepidocrocite) induced by the synergistic interaction of Fe 0 and anaerobic culture, providing more reactive sites for Cr(VI) adsorption, reduction and co-precipitation. Furthermore, the decreasing breakthrough rates and growing iron corrosion along the biotic Fe 0 column demonstrated an inhomogeneous distribution of reactive zones in the column and its latter 3/5 section was considered to be the most reactive area for Cr(VI) removal. These results indicate that the inoculation of microorganisms in Fe 0 -based permeable reactive barriers will enable this technology a higher removal capacity and longer life-span for the remediation of Cr(VI)-contaminated groundwater. Copyright © 2017 Elsevier Ltd. All rights reserved.

Continued Development of Meandering Winding Magnetometer (MWM (Register Trademark)) Eddy Current Sensors for the Health Monitoring, Modeling and Damage Detection of Composite Overwrapped Pressure Vessels

Science.gov (United States)

Russell, Richard; Wincheski, Russell; Jablonski, David; Washabaugh, Andy; Sheiretov, Yanko; Martin, Christopher; Goldfine, Neil

2011-01-01

Composite Overwrapped Pressure Vessels (COPVs) are used in essentially all NASA spacecraft, launch. vehicles and payloads to contain high-pressure fluids for propulsion, life support systems and science experiments. Failure of any COPV either in flight or during ground processing would result in catastrophic damage to the spacecraft or payload, and could lead to loss of life. Therefore, NASA continues to investigate new methods to non-destructively inspect (NDE) COPVs for structural anomalies and to provide a means for in-situ structural health monitoring (SHM) during operational service. Partnering with JENTEK Sensors, engineers at NASA, Kennedy Space Center have successfully conducted a proof-of-concept study to develop Meandering Winding Magnetometer (MWM) eddy current sensors designed to make direct measurements of the stresses of the internal layers of a carbon fiber composite wrapped COPV. During this study three different MWM sensors were tested at three orientations to demonstrate the ability of the technology to measure stresses at various fiber orientations and depths. These results showed good correlation with actual surface strain gage measurements. MWM-Array technology for scanning COPVs can reliably be used to image and detect mechanical damage. To validate this conclusion, several COPVs were scanned to obtain a baseline, and then each COPV was impacted at varying energy levels and then rescanned. The baseline subtracted images were used to demonstrate damage detection. These scans were performed with two different MWM-Arrays. with different geometries for near-surface and deeper penetration imaging at multiple frequencies and in multiple orientations of the linear MWM drive. This presentation will include a review of micromechanical models that relate measured sensor responses to composite material constituent properties, validated by the proof of concept study, as the basis for SHM and NDE data analysis as well as potential improvements including

High-sensitivity low-noise miniature fluxgate magnetometers using a flip chip conceptual design.

Science.gov (United States)

Lu, Chih-Cheng; Huang, Jeff; Chiu, Po-Kai; Chiu, Shih-Liang; Jeng, Jen-Tzong

2014-07-30

This paper presents a novel class of miniature fluxgate magnetometers fabricated on a print circuit board (PCB) substrate and electrically connected to each other similar to the current "flip chip" concept in semiconductor package. This sensor is soldered together by reversely flipping a 5 cm × 3 cm PCB substrate to the other identical one which includes dual magnetic cores, planar pick-up coils, and 3-D excitation coils constructed by planar Cu interconnections patterned on PCB substrates. Principles and analysis of the fluxgate sensor are introduced first, and followed by FEA electromagnetic modeling and simulation for the proposed sensor. Comprehensive characteristic experiments of the miniature fluxgate device exhibit favorable results in terms of sensitivity (or "responsivity" for magnetometers) and field noise spectrum. The sensor is driven and characterized by employing the improved second-harmonic detection technique that enables linear V-B correlation and responsivity verification. In addition, the double magnitude of responsivity measured under very low frequency (1 Hz) magnetic fields is experimentally demonstrated. As a result, the maximum responsivity of 593 V/T occurs at 50 kHz of excitation frequency with the second harmonic wave of excitation; however, the minimum magnetic field noise is found to be 0.05 nT/Hz(1/2) at 1 Hz under the same excitation. In comparison with other miniature planar fluxgates published to date, the fluxgate magnetic sensor with flip chip configuration offers advances in both device functionality and fabrication simplicity. More importantly, the novel design can be further extended to a silicon-based micro-fluxgate chip manufactured by emerging CMOS-MEMS technologies, thus enriching its potential range of applications in modern engineering and the consumer electronics market.

PRTR ion exchange vault column sampling

International Nuclear Information System (INIS)

Cornwell, B.C.

1995-01-01

This report documents ion exchange column sampling and Non Destructive Assay (NDA) results from activities in 1994, for the Plutonium Recycle Test Reactor (PRTR) ion exchange vault. The objective was to obtain sufficient information to prepare disposal documentation for the ion exchange columns found in the PRTR Ion exchange vault. This activity also allowed for the monitoring of the liquid level in the lower vault. The sampling activity contained five separate activities: (1) Sampling an ion exchange column and analyzing the ion exchange media for purpose of waste disposal; (2) Gamma and neutron NDA testing on ion exchange columns located in the upper vault; (3) Lower vault liquid level measurement; (4) Radiological survey of the upper vault; and (5) Secure the vault pending waste disposal

Use of CT scanning for the study of posterior lumbar intervertebral articulations

Energy Technology Data Exchange (ETDEWEB)

Hermanus, N.; de Becker, D.; Baleriaux, D.; Hauzeur, J.P.

1983-01-01

CT scan is peculiarly effective in the study of architectural pathologies of the column; it appears that a number of etiological factors of low back pain are involved and they are often related. Indeed, dis herniation, for instance, is frequently associated with facetal asymmetry, the first signs of arthroses and ligamentous calcification after treatment. The three vertebral axes must be evaluated, one discal and two facetal, the slightest defect in one of which can affect the two others. Moreover, in view of the complexity of the innervation, the entire lumbar column from L1 to L5 S1 must be investigated: it is not uncommonly that low sciatica is caused by a more cranial lumbar pathology. This systematic study promotes better understanding of the etiology of low back pain and suggests a stet judicious therapeutic attitude.

Airborne gamma-ray spectrometer and magnetometer survey: Aberdeen quadrangle, South Dakota. Final report

International Nuclear Information System (INIS)

1981-04-01

During the months of June through October, 1980, Aero Service Division Western Geophysical Company of America conducted an airborne high sensitivity gamma-ray spectrometer and magnetometer survey over eleven (11) 2 0 x 1 0 NTMS quadrangles located in the states of Minnesota and Wisconsin and seven (7) 2 0 x 1 0 NTMS quadrangles in North and South Dakota. This report discusses the results obtained over the Aberdeen, South Dakota map area. The final data are presented in four different forms: on magnetic tape; on microfiche; in graphic form as profiles and histograms; and in map form as anomaly maps, flight path maps, and computer printer maps

Laser surface wakefield in a plasma column

International Nuclear Information System (INIS)

Gorbunov, L.M.; Mora, P.; Ramazashvili, R.R.

2003-01-01

The structure of the wakefield in a plasma column, produced by a short intense laser pulse, propagating through a gas affected by tunneling ionization is investigated. It is shown that besides the usual plasma waves in the bulk part of the plasma column [see Andreev et al., Phys. Plasmas 9, 3999 (2002)], the laser pulse also generates electromagnetic surface waves propagating along the column boundary. The length of the surface wake wave substantially exceeds the length of the plasma wake wave and its electromagnetic field extends far outside the plasma column

Airborne gamma-ray spectrometer and magnetometer survey, Point Lay Quadrangle, Alaska. Volume I. Final report

International Nuclear Information System (INIS)

1981-02-01

The results obtained from an airborne high sensitivity gamma-ray spectrometer and magnetometer survey over the Point Lay map area of Alaska are presented. Based on the criteria outlined in the general section on interpretation, a total of six uranium anomalies have been indicated on the interpretation map. All six are only weakly to moderately anomalous in either uranium or the uranium ratios. None of these are thought to be of any economic significance. No follow-up work is recommended for the Point Lay Quadrangle

Airborne gamma-ray spectrometer and magnetometer survey: Harrison Bay Quadrangle, Alaska. Final report, Volume 1

International Nuclear Information System (INIS)

1981-02-01

During the months of July and August of 1980, Aero Service Division Western Geophysical Company of America conducted an airborne high sensitivity gamma-ray spectrometer and magnetometer survey over eleven (11) 3 0 x 1 0 and one (1) 4 0 x 1 0 NTMS quadrangles of the Alaska North Slope. These include the Barrow, Wainwright, Meade River, Teshekpuk, Harrison Bay, Beechey Point, Point Lay, Utukok River, Lookout Ridge, Ikpikpuk River, Umiat, and Sagavanirktok quadrangles. This report discusses the results obtained over the Harrison Bay map area

TSI Model 3936 Scanning Mobility Particle Spectrometer Instrument Handbook

Energy Technology Data Exchange (ETDEWEB)

Kuang, C. [Brookhaven National Lab. (BNL), Upton, NY (United States)

2016-02-01

The Model 3936 Scanning Mobility Particle Spectrometer (SMPS) measures the size distribution of aerosols ranging from 10 nm up to 1000 nm. The SMPS uses a bipolar aerosol charger to keep particles within a known charge distribution. Charged particles are classified according to their electrical mobility, using a long-column differential mobility analyzer (DMA). Particle concentration is measured with a condensation particle counter (CPC). The SMPS is well-suited for applications including: nanoparticle research, atmospheric aerosol studies, pollution studies, smog chamber evaluations, engine exhaust and combustion studies, materials synthesis, filter efficiency testing, nucleation/condensation studies, and rapidly changing aerosol systems.

Digitally controlled high-performance dc SQUID readout electronics for a 304-channel vector magnetometer

Science.gov (United States)

Bechstein, S.; Petsche, F.; Scheiner, M.; Drung, D.; Thiel, F.; Schnabel, A.; Schurig, Th

2006-06-01

Recently, we have developed a family of dc superconducting quantum interference device (SQUID) readout electronics for several applications. These electronics comprise a low-noise preamplifier followed by an integrator, and an analog SQUID bias circuit. A highly-compact low-power version with a flux-locked loop bandwidth of 0.3 MHz and a white noise level of 1 nV/√Hz was specially designed for a 304-channel low-Tc dc SQUID vector magnetometer, intended to operate in the new Berlin Magnetically Shielded Room (BMSR-2). In order to minimize the space needed to mount the electronics on top of the dewar and to minimize the power consumption, we have integrated four electronics channels on one 3 cm × 10 cm sized board. Furthermore we embedded the analog components of these four channels into a digitally controlled system including an in-system programmable microcontroller. Four of these integrated boards were combined to one module with a size of 4 cm × 4 cm × 16 cm. 19 of these modules were implemented, resulting in a total power consumption of about 61 W. To initialize the 304 channels and to service the system we have developed software tools running on a laptop computer. By means of these software tools the microcontrollers are fed with all required data such as the working points, the characteristic parameters of the sensors (noise, voltage swing), or the sensor position inside of the vector magnetometer system. In this paper, the developed electronics including the software tools are described, and first results are presented.

Digitally controlled high-performance dc SQUID readout electronics for a 304-channel vector magnetometer

International Nuclear Information System (INIS)

Bechstein, S; Petsche, F; Scheiner, M; Drung, D; Thiel, F; Schnabel, A; Schurig, Th

2006-01-01

Recently, we have developed a family of dc superconducting quantum interference device (SQUID) readout electronics for several applications. These electronics comprise a low-noise preamplifier followed by an integrator, and an analog SQUID bias circuit. A highly-compact low-power version with a flux-locked loop bandwidth of 0.3 MHz and a white noise level of 1 nV/√Hz was specially designed for a 304-channel low-T c dc SQUID vector magnetometer, intended to operate in the new Berlin Magnetically Shielded Room (BMSR-2). In order to minimize the space needed to mount the electronics on top of the dewar and to minimize the power consumption, we have integrated four electronics channels on one 3 cm x 10 cm sized board. Furthermore we embedded the analog components of these four channels into a digitally controlled system including an in-system programmable microcontroller. Four of these integrated boards were combined to one module with a size of 4 cm x 4 cm x 16 cm. 19 of these modules were implemented, resulting in a total power consumption of about 61 W. To initialize the 304 channels and to service the system we have developed software tools running on a laptop computer. By means of these software tools the microcontrollers are fed with all required data such as the working points, the characteristic parameters of the sensors (noise, voltage swing), or the sensor position inside of the vector magnetometer system. In this paper, the developed electronics including the software tools are described, and first results are presented

Digitally controlled high-performance dc SQUID readout electronics for a 304-channel vector magnetometer

Energy Technology Data Exchange (ETDEWEB)

Bechstein, S [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany); Petsche, F [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany); Scheiner, M [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany); Drung, D [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany); Thiel, F [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany); Schnabel, A [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany); Schurig, Th [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany)

2006-06-01

Recently, we have developed a family of dc superconducting quantum interference device (SQUID) readout electronics for several applications. These electronics comprise a low-noise preamplifier followed by an integrator, and an analog SQUID bias circuit. A highly-compact low-power version with a flux-locked loop bandwidth of 0.3 MHz and a white noise level of 1 nV/{radical}Hz was specially designed for a 304-channel low-T{sub c} dc SQUID vector magnetometer, intended to operate in the new Berlin Magnetically Shielded Room (BMSR-2). In order to minimize the space needed to mount the electronics on top of the dewar and to minimize the power consumption, we have integrated four electronics channels on one 3 cm x 10 cm sized board. Furthermore we embedded the analog components of these four channels into a digitally controlled system including an in-system programmable microcontroller. Four of these integrated boards were combined to one module with a size of 4 cm x 4 cm x 16 cm. 19 of these modules were implemented, resulting in a total power consumption of about 61 W. To initialize the 304 channels and to service the system we have developed software tools running on a laptop computer. By means of these software tools the microcontrollers are fed with all required data such as the working points, the characteristic parameters of the sensors (noise, voltage swing), or the sensor position inside of the vector magnetometer system. In this paper, the developed electronics including the software tools are described, and first results are presented.

The Two-Column Aerosol Project (TCAP) Science Plan

Energy Technology Data Exchange (ETDEWEB)

Berkowitz, CM; Berg, LK; Cziczo, DJ; Flynn, CJ; Kassianov, EI; Fast, JD; Rasch, PJ; Shilling, JE; Zaveri, RA; Zelenyuk, A; Ferrare, RA; Hostetler, CA; Cairns, B; Russell, PB; Ervens, B

2011-07-27

The Two-Column Aerosol Project (TCAP) field campaign will provide a detailed set of observations with which to (1) perform radiative and cloud condensation nuclei (CCN) closure studies, (2) evaluate a new retrieval algorithm for aerosol optical depth (AOD) in the presence of clouds using passive remote sensing, (3) extend a previously developed technique to investigate aerosol indirect effects, and (4) evaluate the performance of a detailed regional-scale model and a more parameterized global-scale model in simulating particle activation and AOD associated with the aging of anthropogenic aerosols. To meet these science objectives, the Atmospheric Radiation Measurement (ARM) Climate Research Facility will deploy the ARM Mobile Facility (AMF) and the Mobile Aerosol Observing System (MAOS) on Cape Cod, Massachusetts, for a 12-month period starting in the summer of 2012 in order to quantify aerosol properties, radiation, and cloud characteristics at a location subject to both clear and cloudy conditions, and clean and polluted conditions. These observations will be supplemented by two aircraft intensive observation periods (IOPs), one in the summer and a second in the winter. Each IOP will deploy one, and possibly two, aircraft depending on available resources. The first aircraft will be equipped with a suite of in situ instrumentation to provide measurements of aerosol optical properties, particle composition and direct-beam irradiance. The second aircraft will fly directly over the first and use a multi-wavelength high spectral resolution lidar (HSRL) and scanning polarimeter to provide continuous optical and cloud properties in the column below.

MOURA magnetometer for Mars MetNet Precursor Mission. Its potential for an in situ magnetic environment and surface characterization

Energy Technology Data Exchange (ETDEWEB)

Diaz Michelena, M.; Sanz, R.; Fernandez, A.B.; Manuel, V. de; Cerdan, M.F.; Apestigue, V.; Arruego, I.; Azcue, J.; Dominguez, J.A.; Gonzalez, M.; Guerrero, H.; Sabau, M.; Kilian, R.; Baeza, O.; Ros, F.; Vazquez, M.; Tordesillas, J.M.; Covisa, P.; Aguado, J.

2016-07-01

MOURA magnetometer and gradiometer is part of the scientific instrumentation for Mars MetNet Precursor mission. This work describes the objective of the investigation, summarizes the work done in the design and development of the sensor as well as its calibration, and shows the demonstration campaigns to show the potential of such instrument for planetary landers and rovers. (Author)

Picobubble enhanced column flotation of fine coal

Energy Technology Data Exchange (ETDEWEB)

Tao, D.; Yu, S.; Parekh, B.K. [University of Kentucky, Lexington, KY (United States). Mining Engineering

2006-07-01

The purpose is to study the effectiveness of picobubbles in the column flotation of -28 mesh fine coal particles. A flotation column with a picobubble generator was developed and tested for enhancing the recovery of ultrafine coal particles. The picobubble generator was designed using the hydrodynamic cavitation principle. A metallurgical and a steam coal were tested in the apparatus. The results show that the use of picobubbles in a 2in. flotation column increased the recovery of fine coal by 10 to 30%. The recovery rate varied with feed rate, collector dosage, and other column conditions. 40 refs., 8 figs., 2 tabs.

Exploring the effect of mesopore size reduction on the column performance of silica-based open tubular capillary columns.

Science.gov (United States)

Hara, Takeshi; Futagami, Shunta; De Malsche, Wim; Baron, Gino V; Desmet, Gert

2018-06-01

We report on a modification in the hydrothermal treatment process of monolithic silica layers used in porous-layered open tubular (PLOT) columns. Lowering the temperature from the customary 95 °C to 80 °C, the size of the mesopores reduced by approximately about 35% from 12-13.5 nm to 7.5-9 nm, while the specific pore volume essentially remains unaltered. This led to an increase of the specific surface area (SA) of about 40%, quasi-independent of the porous layer thickness. The increased surface area provided a corresponding increase in retention, somewhat more (48%) than expected based on the increase in SA for the thin layer columns, and somewhat less than expected (34%) for the thick layer columns. The recipes were applied in 5 μm i.d.-capillaries with a length of 60 cm. Efficiencies under retained conditions amounted up to N = 137,000 for the PLOT column with a layer thickness (d f ) of 300 nm and to N = 109,000 for the PLOT column with d f  = 550 nm. Working under conditions of similar retention, the narrow pore/high SA columns produced with the new 80 °C recipe generated the same number of theoretical plates as the wide pore size/low SA columns produced with the 95 °C recipe. This shows the 80 °C-hydrothermal treatment process allows for an increase in the phase ratio of the PLOT columns without affecting their intrinsic mass transfer properties and separation kinetics. This is further corroborated by the fact that the plate height curves generated with the new and former recipe can both be well-fitted with the Golay-Aris equation without having to change the intra-layer diffusion coefficient. Copyright © 2018 Elsevier B.V. All rights reserved.

Magnetic field `flyby' measurement using a smartphone's magnetometer and accelerometer simultaneously

Science.gov (United States)

Monteiro, Martín; Stari, Cecilia; Cabeza, Cecilia; Marti, Arturo C.

2017-12-01

The spatial dependence of magnetic fields in simple configurations is a common topic in introductory electromagnetism lessons, both in high school and in university courses. In typical experiments, magnetic fields and distances are obtained taking point-by-point values using a Hall sensor and a ruler, respectively. Here, we show how to take advantage of the smartphone capabilities to get simultaneous measures with the built-in accelerometer and magnetometer and to obtain the spatial dependence of magnetic fields. We consider a simple setup consisting of a smartphone mounted on a track whose direction coincides with the axis of a coil. While the smartphone is moving on the track, both the magnetic field and the distance from the center of the coil (integrated numerically from the acceleration values) are simultaneously obtained. This methodology can easily be extended to more complicated setups.

[Online enrichment ability of restricted-access column coupled with high performance liquid chromatography by column switching technique for benazepril hydrochloride].

Science.gov (United States)

Zhang, Xiaohui; Wang, Rong; Xie, Hua; Yin, Qiang; Li, Xiaoyun; Jia, Zhengping; Wu, Xiaoyu; Zhang, Juanhong; Li, Wenbin

2013-05-01

The online enrichment ability of the restricted-access media (RAM) column coupled with high performance liquid chromatography by column switching technique for benazepril hydrochloride in plasma was studied. The RAM-HPLC system consisted of an RAM column as enrichment column and a C18 column as analytical column coupled via the column switching technique. The effects of the injection volume on the peak area and the systematic pressure were studied. When the injection volume was less than 100 microL, the peak area increased with the increase of the injection volume. However, when the injection volume was more than 80 microL, the pressure of whole system increased obviously. In order to protect the whole system, 80 microL was chosen as the maximum injection volume. The peak areas of ordinary injection and the large volume injection showed a good linear relationship. The enrichment ability of RAM-HPLC system was satisfactory. The system was successfully used for the separation and detection of the trace benazepril hydrochloride in rat plasma after its administration. The sensitivity of HPLC can be improved by RAM pre-enrichment. It is a simple and economic measurement method.

Response of steel box columns in fire conditions

Directory of Open Access Journals (Sweden)

Mahmood Yahyai

2017-05-01

Full Text Available Effect of elevated temperatures on the mechanical properties of steel, brings the importance of investigating the effect of fire on the steel structures anxiously. Columns, as the main load-carrying part of a structure, can be highly vulnerable to the fire. In this study, the behavior of steel gravity columns with box cross section exposed to fire has been investigated. These kinds of columns are widely used in common steel structures design in Iran. In current study, the behavior of such columns in fire conditions is investigated through the finite element method. To perform this, the finite element model of a steel column which has been previously tested under fire condition, was prepared. Experimental loading and boundary conditions were considered in the model and was analyzed. Results were validated by experimental data and various specimens of gravity box columns were designed according to the Iran’s steel buildings code, and modeled and analyzed using Abaqus software. The effect of width to thickness ratio of column plates, the load ratio and slenderness on the ultimate strength of the column was investigated, and the endurance time was estimated under ISO 834 standard fire curve. The results revealed that an increase in width to thickness ratio and load ratio leads to reduction of endurance time and the effect of width to thickness ratio on the ultimate strength of the column decreases with temperature increase.

Ductility of reinforced concrete columns confined with stapled strips

International Nuclear Information System (INIS)

Tahir, M.F.; Khan, Q.U.Z.; Shabbir, F.; Sharif, M.B.; Ijaz, N.

2015-01-01

Response of three 150x150x450mm short reinforced concrete (RC) columns confined with different types of confining steel was investigated. Standard stirrups, strips and stapled strips, each having same cross-sectional area, were employed as confining steel around four comer column bars. Experimental work was aimed at probing into the affect of stapled strip confinement on post elastic behavior and ductility level under cyclic axial load. Ductility ratios, strength enhancement factor and core concrete strengths were compared to study the affect of confinement. Results indicate that strength enhancement in RC columns due to strip and stapled strip confinement was not remarkable as compared to stirrup confined column. It was found that as compared to stirrup confined column, stapled strip confinement enhanced the ductility of RC column by 183% and observed axial capacity of stapled strip confined columns was 41 % higher than the strip confined columns. (author)

Retrofit of distillation columns in biodiesel production plants

International Nuclear Information System (INIS)

Nguyen, Nghi; Demirel, Yasar

2010-01-01

Column grand composite curves and the exergy loss profiles produced by the Column-Targeting Tool of the Aspen Plus simulator are used to assess the performance of the existing distillation columns, and reduce the costs of operation by appropriate retrofits in a biodiesel production plant. Effectiveness of the retrofits is assessed by means of thermodynamics and economic improvements. We have considered a biodiesel plant utilizing three distillation columns to purify biodiesel (fatty acid methyl ester) and byproduct glycerol as well as reduce the waste. The assessments of the base case simulation have indicated the need for modifications for the distillation columns. For column T202, the retrofits consisting of a feed preheating and reflux ratio modification have reduced the total exergy loss by 47%, while T301 and T302 columns exergy losses decreased by 61% and 52%, respectively. After the retrofits, the overall exergy loss for the three columns has decreased from 7491.86 kW to 3627.97 kW. The retrofits required a fixed capital cost of approximately $239,900 and saved approximately $1,900,000/year worth of electricity. The retrofits have reduced the consumption of energy considerably, and leaded to a more environmentally friendly operation for the biodiesel plant considered.

Interpretation of the lime column penetration test

International Nuclear Information System (INIS)

Liyanapathirana, D S; Kelly, R B

2010-01-01

Dry soil mix (DSM) columns are used to reduce the settlement and to improve the stability of embankments constructed on soft clays. During construction the shear strength of the columns needs to be confirmed for compliance with technical assumptions. A specialized blade shaped penetrometer known as the lime column probe, has been developed for testing DSM columns. This test can be carried out as a pull out resistance test (PORT) or a push in resistance test (PIRT). The test is considered to be more representative of average column shear strength than methods that test only a limited area of the column. Both PORT and PIRT tests require empirical correlations of measured resistance to an absolute measure of shear strength, in a similar manner to the cone penetration test. In this paper, finite element method is used to assess the probe factor, N, for the PORT test. Due to the large soil deformations around the probe, an Arbitrary Lagrangian Eulerian (ALE) based finite element formulation has been used. Variation of N with rigidity index and the friction at the probe-soil interface are investigated to establish a range for the probe factor.

High-Sensitivity Low-Noise Miniature Fluxgate Magnetometers Using a Flip Chip Conceptual Design

Directory of Open Access Journals (Sweden)

Chih-Cheng Lu

2014-07-01

Full Text Available This paper presents a novel class of miniature fluxgate magnetometers fabricated on a print circuit board (PCB substrate and electrically connected to each other similar to the current “flip chip” concept in semiconductor package. This sensor is soldered together by reversely flipping a 5 cm × 3 cm PCB substrate to the other identical one which includes dual magnetic cores, planar pick-up coils, and 3-D excitation coils constructed by planar Cu interconnections patterned on PCB substrates. Principles and analysis of the fluxgate sensor are introduced first, and followed by FEA electromagnetic modeling and simulation for the proposed sensor. Comprehensive characteristic experiments of the miniature fluxgate device exhibit favorable results in terms of sensitivity (or “responsivity” for magnetometers and field noise spectrum. The sensor is driven and characterized by employing the improved second-harmonic detection technique that enables linear V-B correlation and responsivity verification. In addition, the double magnitude of responsivity measured under very low frequency (1 Hz magnetic fields is experimentally demonstrated. As a result, the maximum responsivity of 593 V/T occurs at 50 kHz of excitation frequency with the second harmonic wave of excitation; however, the minimum magnetic field noise is found to be 0.05 nT/Hz1/2 at 1 Hz under the same excitation. In comparison with other miniature planar fluxgates published to date, the fluxgate magnetic sensor with flip chip configuration offers advances in both device functionality and fabrication simplicity. More importantly, the novel design can be further extended to a silicon-based micro-fluxgate chip manufactured by emerging CMOS-MEMS technologies, thus enriching its potential range of applications in modern engineering and the consumer electronics market.

High-Sensitivity Low-Noise Miniature Fluxgate Magnetometers Using a Flip Chip Conceptual Design

Science.gov (United States)

Lu, Chih-Cheng; Huang, Jeff; Chiu, Po-Kai; Chiu, Shih-Liang; Jeng, Jen-Tzong

2014-01-01

This paper presents a novel class of miniature fluxgate magnetometers fabricated on a print circuit board (PCB) substrate and electrically connected to each other similar to the current “flip chip” concept in semiconductor package. This sensor is soldered together by reversely flipping a 5 cm × 3 cm PCB substrate to the other identical one which includes dual magnetic cores, planar pick-up coils, and 3-D excitation coils constructed by planar Cu interconnections patterned on PCB substrates. Principles and analysis of the fluxgate sensor are introduced first, and followed by FEA electromagnetic modeling and simulation for the proposed sensor. Comprehensive characteristic experiments of the miniature fluxgate device exhibit favorable results in terms of sensitivity (or “responsivity” for magnetometers) and field noise spectrum. The sensor is driven and characterized by employing the improved second-harmonic detection technique that enables linear V-B correlation and responsivity verification. In addition, the double magnitude of responsivity measured under very low frequency (1 Hz) magnetic fields is experimentally demonstrated. As a result, the maximum responsivity of 593 V/T occurs at 50 kHz of excitation frequency with the second harmonic wave of excitation; however, the minimum magnetic field noise is found to be 0.05 nT/Hz1/2 at 1 Hz under the same excitation. In comparison with other miniature planar fluxgates published to date, the fluxgate magnetic sensor with flip chip configuration offers advances in both device functionality and fabrication simplicity. More importantly, the novel design can be further extended to a silicon-based micro-fluxgate chip manufactured by emerging CMOS-MEMS technologies, thus enriching its potential range of applications in modern engineering and the consumer electronics market. PMID:25196107

Behaviour of FRP confined concrete in square columns

OpenAIRE

Diego Villalón, Ana de; Arteaga Iriarte, Ángel; Fernandez Gomez, Jaime Antonio; Perera Velamazán, Ricardo; Cisneros, Daniel

2015-01-01

A significant amount of research has been conducted on FRP-confined circular columns, but much less is known about rectangular/square columns in which the effectiveness of confinement is much reduced. This paper presents the results of experimental investigations on low strength square concrete columns confined with FRP. Axial compression tests were performed on ten intermediate size columns. The tests results indicate that FRP composites can significantly improve the bearing capacity and duc...

Numerical Simulations of Settlement of Jet Grouting Columns

Directory of Open Access Journals (Sweden)

Juzwa Anna

2016-03-01

Full Text Available The paper presents the comparison of results of numerical analyses of interaction between group of jet grouting columns and subsoil. The analyses were conducted for single column and groups of three, seven and nine columns. The simulations are based on experimental research in real scale which were carried out by authors. The final goal for the research is an estimation of an influence of interaction between columns working in a group.

Strengthening of Steel Columns under Load: Torsional-Flexural Buckling

Directory of Open Access Journals (Sweden)

Martin Vild

2016-01-01

Full Text Available The paper presents experimental and numerical research into the strengthening of steel columns under load using welded plates. So far, the experimental research in this field has been limited mostly to flexural buckling of columns and the preload had low effect on the column load resistance. This paper focuses on the local buckling and torsional-flexural buckling of columns. Three sets of three columns each were tested. Two sets corresponding to the base section (D and strengthened section (E were tested without preloading and were used for comparison. Columns from set (F were first preloaded to the load corresponding to the half of the load resistance of the base section (D. Then the columns were strengthened and after they cooled, they were loaded to failure. The columns strengthened under load (F had similar average resistance as the columns welded without preloading (E, meaning the preload affects even members susceptible to local buckling and torsional-flexural buckling only slightly. This is the same behaviour as of the tested columns from previous research into flexural buckling. The study includes results gained from finite element models of the problem created in ANSYS software. The results obtained from the experiments and numerical simulations were compared.

Study on two phase flow characteristics in annular pulsed extraction column with different ratio of annular width to column diameter

International Nuclear Information System (INIS)

Qin Wei; Dai Youyuan; Wang Jiading

1994-01-01

Annular pulsed extraction column can successfully provide large throughput and can be made critically safe for fuel reprocessing. This investigation is to study the two phase flow characteristics in annular pulsed extraction column with four different annular width. 30% TBP (in kerosene)-water is used (water as continuous phase). Results show that modified Pratt correlation is valid under the experimental operation conditions for the annular pulsed extraction column. The characteristic velocity U K decreased with the increase of energy input and increased with the increase of the ratio of annular width to column diameter. Flooding velocity correlation is suggested. The deviation of the calculated values from the experimental data is within +20% for four annular width in a pulsed extraction column

The use of CT scanning for the study of posterior lumbar intervertebral articulations

International Nuclear Information System (INIS)

Hermanus, N.; Becker, D. de; Baleriaux, D.; Hauzeur, J.P.

1983-01-01

CT scan is peculiarly effective in the study of architectural pathologies of the column; it appears that a number of etiological factors of low back pain are involved and they are often related. Indeed, dis herniation, for instance, is frequently associated with facetal asymmetry, the first signs of arthroses and ligamentous calcification after treatment. The three vertebral axes must be evaluated, one discal and two facetal, the slightest defect in one of which can affect the two others. Moreover, in view of the complexity of the innervation, the entire lumbar column from L1 to L5 S1 must be investigated: it is not uncommonly that low sciatica is caused by a more cranial lumbar pathology. This systematic study promotes better understanding of the etiology of low back pain and suggests a stet judicious therapeutic attitude. (orig.)

Collapse of tall granular columns in fluid

Science.gov (United States)

Kumar, Krishna; Soga, Kenichi; Delenne, Jean-Yves

2017-06-01

Avalanches, landslides, and debris flows are geophysical hazards, which involve rapid mass movement of granular solids, water, and air as a multi-phase system. In order to describe the mechanism of immersed granular flows, it is important to consider both the dynamics of the solid phase and the role of the ambient fluid. In the present study, the collapse of a granular column in fluid is studied using 2D LBM - DEM. The flow kinematics are compared with the dry and buoyant granular collapse to understand the influence of hydrodynamic forces and lubrication on the run-out. In the case of tall columns, the amount of material destabilised above the failure plane is larger than that of short columns. Therefore, the surface area of the mobilised mass that interacts with the surrounding fluid in tall columns is significantly higher than the short columns. This increase in the area of soil - fluid interaction results in an increase in the formation of turbulent vortices thereby altering the deposit morphology. It is observed that the vortices result in the formation of heaps that significantly affects the distribution of mass in the flow. In order to understand the behaviour of tall columns, the run-out behaviour of a dense granular column with an initial aspect ratio of 6 is studied. The collapse behaviour is analysed for different slope angles: 0°, 2.5°, 5° and 7.5°.

Nitrogen dioxide column content measurements made from an aircraft between 5 deg and 82 deg N

Energy Technology Data Exchange (ETDEWEB)

Matthews, W A

1984-01-01

In the first two weeks of May 1981, the research jet of the German Aerospace Research Estlablishment (DFVLR) was charted to fly a meridional section between 5 deg and 82 deg N. A scanning filter photometer, developed at the Max-Planck-Institut fuer Aeronomie to measure column content values of atmospheric ozone and nitrogen dioxide, using ultraviolet and visible absorption techniques, constituted part of the experimental payload for this campaign that was called SIMOC. The vertical NO2 column content above the aircraft, flying at approximately 10 km, was found to decrease rapidly from 6.9 x 10 to the 15th molecules/sq cm to 2.5 x 10 to the 15th molecules/sq cm around 50 deg N and then to increase again north of 75 deg N. A sharp rise in the NO2 content was observed south of the subtropical jet but this could possibly be due to the increased depth of the troposphere above the aircraft in these regions. 8 references.

CUB DI (Deionization) column control system

International Nuclear Information System (INIS)

Seino, K.C.

1999-01-01

For the old MR (Main Ring), deionization was done with two columns in CUB, using an ion exchange process. Typically 65 GPM of LCW flew through a column, and the resistivity was raised from 3 Mohm-cm to over 12 Mohm-cm. After a few weeks, columns lost their effectiveness and had to be regenerated in a process involving backwashing and adding hydrochloric acid and sodium hydroxide. For normal MR operations, LCW returned from the ring and passed through the two columns in parallel for deionization, although the system could have been operated satisfactorily with only one in use. A 3000 gallon reservoir (the Spheres) provided a reserve of LCW for allowing water leaks and expansions in the MR. During the MI (Main Injector) construction period, the third DI column was added to satisfy requirements for the MI. When the third column was added, the old regeneration controller was replaced with a new controller based on an Allen-Bradley PLC (i.e., SLC-5/04). The PLC is widely used and well documented, and therefore it may allow us to modify the regeneration programs in the future. In addition to the above regeneration controller, the old control panels (which were used to manipulate pumps and valves to supply LCW in Normal mode and to do Int. Recir. (Internal Recirculation) and Makeup) were replaced with a new control system based on Sixtrak Gateway and I/O modules. For simplicity, the new regeneration controller is called as the US Filter system, and the new control system is called as the Fermilab system in this writing

NOx retention in scrubbing column

International Nuclear Information System (INIS)

Nakazone, A.K.; Costa, R.E.; Lobao, A.S.T.; Matsuda, H.T.; Araujo, B.F.

1988-07-01

During the UO 2 dissolution in nitric acid, some different species of NO x are released. The off gas can either be refluxed to the dissolver or be released and retained on special columns. The final composition of the solution is the main parameter to take in account. A process for nitrous gases retention using scubber columns containing H 2 O or diluted HNO 3 is presented. Chemiluminescence measurement was employed to NO x evalution before and after scrubbing. Gas flow, temperature, residence time are the main parameters considered in this paper. For the dissolution of 100g UO 2 in 8M nitric acid, a 6NL/h O 2 flow was the best condition for the NO/NO 2 oxidation with maximum adsorption in the scrubber columns. (author) [pt

Deconvolution of continuous paleomagnetic data from pass-through magnetometer: A new algorithm to restore geomagnetic and environmental information based on realistic optimization

Science.gov (United States)

Oda, Hirokuni; Xuan, Chuang

2014-10-01

development of pass-through superconducting rock magnetometers (SRM) has greatly promoted collection of paleomagnetic data from continuous long-core samples. The output of pass-through measurement is smoothed and distorted due to convolution of magnetization with the magnetometer sensor response. Although several studies could restore high-resolution paleomagnetic signal through deconvolution of pass-through measurement, difficulties in accurately measuring the magnetometer sensor response have hindered the application of deconvolution. We acquired reliable sensor response of an SRM at the Oregon State University based on repeated measurements of a precisely fabricated magnetic point source. In addition, we present an improved deconvolution algorithm based on Akaike's Bayesian Information Criterion (ABIC) minimization, incorporating new parameters to account for errors in sample measurement position and length. The new algorithm was tested using synthetic data constructed by convolving "true" paleomagnetic signal containing an "excursion" with the sensor response. Realistic noise was added to the synthetic measurement using Monte Carlo method based on measurement noise distribution acquired from 200 repeated measurements of a u-channel sample. Deconvolution of 1000 synthetic measurements with realistic noise closely resembles the "true" magnetization, and successfully restored fine-scale magnetization variations including the "excursion." Our analyses show that inaccuracy in sample measurement position and length significantly affects deconvolution estimation, and can be resolved using the new deconvolution algorithm. Optimized deconvolution of 20 repeated measurements of a u-channel sample yielded highly consistent deconvolution results and estimates of error in sample measurement position and length, demonstrating the reliability of the new deconvolution algorithm for real pass-through measurements.

Electrodynamics of an omega-band as deduced from optical and magnetometer data

Directory of Open Access Journals (Sweden)

H. Vanhamäki

2009-09-01

Full Text Available We investigate an omega-band event that took place above northern Scandinavia around 02:00–02:30 UT on 9 March 1999. In our analysis we use ground based magnetometer, optical and riometer measurements together with satellite based optical images. The optical and riometer data are used to estimate the ionospheric Hall and Pedersen conductances, while ionospheric equivalent currents are obtained from the magnetometer measurements. These data sets are used as input in a local KRM calculation, which gives the ionospheric potential electric field as output, thus giving us a complete picture of the ionospheric electrodynamic state during the omega-band event. The overall structure of the electric field and field-aligned current (FAC provided by the local KRM method are in good agreement with previous studies. Also the E×B drift velocity calculated from the local KRM solution is in good qualitative agreement with the plasma velocity measured by the Finnish CUTLASS radar, giving further support for the new local KRM method. The high-resolution conductance estimates allow us to discern the detailed structure of the omega-band current system. The highest Hall and Pedersen conductances, ~50 and ~25 S, respectively, are found at the edges of the bright auroral tongue. Inside the tongue, conductances are somewhat smaller, but still significantly higher than typical background values. The electric field shows a converging pattern around the tongues, and the field strength drops from ~40 mV/m found at optically dark regions to ~10 mV/m inside the areas of enhanced conductivity. Downward FAC flow in the dark regions, while upward currents flow inside the auroral tongue. Additionally, sharp conductance gradients at the edge of an auroral tongue are associated with narrow strips of intense FACs, so that a strip of downward current flows at the eastern (leading edge and a similar strip of upward current is present at the western (trailing edge. The Joule

A large-scale view of Space Technology 5 magnetometer response to solar wind drivers.

Science.gov (United States)

Knipp, D J; Kilcommons, L M; Gjerloev, J; Redmon, R J; Slavin, J; Le, G

2015-04-01

In this data report we discuss reprocessing of the Space Technology 5 (ST5) magnetometer database for inclusion in NASA's Coordinated Data Analysis Web (CDAWeb) virtual observatory. The mission consisted of three spacecraft flying in elliptical orbits, from 27 March to 27 June 2006. Reprocessing includes (1) transforming the data into the Modified Apex Coordinate System for projection to a common reference altitude of 110 km, (2) correcting gain jumps, and (3) validating the results. We display the averaged magnetic perturbations as a keogram, which allows direct comparison of the full-mission data with the solar wind values and geomagnetic indices. With the data referenced to a common altitude, we find the following: (1) Magnetic perturbations that track the passage of corotating interaction regions and high-speed solar wind; (2) unexpectedly strong dayside perturbations during a solstice magnetospheric sawtooth oscillation interval characterized by a radial interplanetary magnetic field (IMF) component that may have enhanced the accompanying modest southward IMF; and (3) intervals of reduced magnetic perturbations or "calms," associated with periods of slow solar wind, interspersed among variable-length episodic enhancements. These calms are most evident when the IMF is northward or projects with a northward component onto the geomagnetic dipole. The reprocessed ST5 data are in very good agreement with magnetic perturbations from the Defense Meteorological Satellite Program (DMSP) spacecraft, which we also map to 110 km. We briefly discuss the methods used to remap the ST5 data and the means of validating the results against DMSP. Our methods form the basis for future intermission comparisons of space-based magnetometer data.

Modalization in the Political Column of Tempo Magazine

OpenAIRE

Rahmah, Maria Betti Sinaga and

2017-01-01

The study focuses on analyzing the use of modalization in the Political Column of Tempo Magazine. The objectives were to find out the type of modalization and to describe the use of modalization in the Political Column of Tempo magazine. The data were taken from Political Column of Tempo magazine published in June and July 2017. The source of data was Political Column in Tempo magazine. The data analysis applied descriptive qualitative research. There were 135 clauses which contained Modaliza...

Column, particularly extraction column, for fission and/or breeder materials

International Nuclear Information System (INIS)

Vietzke, H.; Pirk, H.

1980-01-01

An absorber rod with a B 4 C insert is situated in the long extraction column for a uranyl nitrate solution or a plutonium nitrate solution. The geometrical dimensions are designed for a high throughput with little corrosion. (DG) [de

Posterior column reconstruction improves fusion rates at the level of osteotomy in three-column posterior-based osteotomies.

Science.gov (United States)

Lewis, Stephen J; Mohanty, Chandan; Gazendam, Aaron M; Kato, So; Keshen, Sam G; Lewis, Noah D; Magana, Sofia P; Perlmutter, David; Cape, Jennifer

2018-03-01

To determine the incidence of pseudarthrosis at the osteotomy site after three-column spinal osteotomies (3-COs) with posterior column reconstruction. 82 consecutive adult 3-COs (66 patients) with a minimum of 2-year follow-up were retrospectively reviewed. All cases underwent posterior 3-COs with two-rod constructs. The inferior facets of the proximal level were reduced to the superior facets of the distal level. If that was not possible, a structural piece of bone graft either from the local resection or a local rib was slotted in the posterior column defect to re-establish continual structural posterior bone across the lateral margins of the resection. No interbody cages were used at the level of the osteotomy. There were 34 thoracic osteotomies, 47 lumbar osteotomies and one sacral osteotomy with a mean follow-up of 52 (24-126) months. All cases underwent posterior column reconstructions described above and the addition of interbody support or additional posterior rods was not performed for fusion at the osteotomy level. Among them, 29 patients underwent one or more revision surgeries. There were three definite cases of pseudarthrosis at the osteotomy site (4%). Six revisions were also performed for pseudarthrosis at other levels. Restoration of the structural integrity of the posterior column in three-column posterior-based osteotomies was associated with > 95% fusion rate at the level of the osteotomy. Pseudarthrosis at other levels was the second most common reason for revision following adjacent segment disease in the long-term follow-up.

Effect of pre- and post-column band broadening on the performance of high-speed chromatography columns under isocratic and gradient conditions.

Science.gov (United States)

Vanderlinden, Kim; Broeckhoven, Ken; Vanderheyden, Yoachim; Desmet, Gert

2016-04-15

We report on the results of an experimental and theoretical study of the effect of the extra-column band broadening (ECBB) on the performance of narrow-bore columns filled with the smallest particles that are currently commercially available. Emphasis is on the difference between the effect of ECBB under gradient and isocratic conditions, as well as on the ability to model and predict the ECBB effects using well-established band broadening expressions available from the theory of chromatography. The fine details and assumptions that need to be taken into account when using these expressions are discussed. The experiments showed that, the steeper the gradient, the more pronounced the extra-column band broadening losses become. Whereas the pre-column band broadening can in both isocratic and gradient elution be avoided by playing on the possibilities to focus the analytes on top of the column (e.g. by using the POISe injection method when running isocratic separations), the post-column extra-column band broadening is inescapable in both cases. Inducing extra-column band broadening by changing the inner diameter of the post-column tubing from 65 to 250 μm, we found that all peaks in the chromatogram are strongly affected (around a factor of 1.9 increase in relative peak width) when running steep gradients, while usually only the first eluting peak was affected in the isocratic mode or when running shallow gradients (factor 1.6-1.8 increase in relative peak width for the first eluting analyte). Copyright © 2016 Elsevier B.V. All rights reserved.

Auto-Calibration Methods of Kinematic Parameters and Magnetometer Offset for the Localization of a Tracked Mobile Robot

OpenAIRE

Luciano Cantelli; Samuel Ligama; Giovanni Muscato; Davide Spina

2016-01-01

This paper describes an automatic calibration procedure adopted to improve the localization of an outdoor mobile robot. The proposed algorithm estimates, by using an extended Kalman filter, the main kinematic parameters of the vehicles, such as the wheel radii and the wheelbase as well as the magnetometer offset. Several trials have been performed to validate the proposed strategy on a tracked electrical mobile robot. The mobile robot is aimed to be adopted as a tool to help humanitarian demi...

Airborne gamma-ray spectrometer and magnetometer survey, Devils Lake quadrangle, North Dakota. Final report

International Nuclear Information System (INIS)

1981-05-01

During the months of June through October, 1980, Aero Service Division Western Geophysical Company of America conducted an airborne high sensitivity gamma-ray spectrometer and magnetometer survey over eleven (11) 2 0 x 1 0 NTMS quadrangles located in the states of Minnesota and Wisconsin and seven (7) 2 0 x 1 0 NTMS quadrangles in North and South Dakota. This report discusses the results obtained over the Devil's Lake map area of North Dakota. The final data are presented in four different forms: on magnetic tape; on microfiche; in graphic form as profiles and histograms; and in map form as anomaly maps, flight path maps, and computer printer maps

A miniature, low-power scientific fluxgate magnetometer: A stepping-stone to cube-satellite constellation missions

Science.gov (United States)

Miles, D. M.; Mann, I. R.; Ciurzynski, M.; Barona, D.; Narod, B. B.; Bennest, J. R.; Pakhotin, I. P.; Kale, A.; Bruner, B.; Nokes, C. D. A.; Cupido, C.; Haluza-DeLay, T.; Elliott, D. G.; Milling, D. K.

2016-12-01

Difficulty in making low noise magnetic measurements is a significant challenge to the use of cube-satellite (CubeSat) platforms for scientific constellation class missions to study the magnetosphere. Sufficient resolution is required to resolve three-dimensional spatiotemporal structures of the magnetic field variations accompanying both waves and current systems of the nonuniform plasmas controlling dynamic magnetosphere-ionosphere coupling. This paper describes the design, validation, and test of a flight-ready, miniature, low-mass, low-power, and low-magnetic noise boom-mounted fluxgate magnetometer for CubeSat applications. The miniature instrument achieves a magnetic noise floor of 150-200 pT/√Hz at 1 Hz, consumes 400 mW of power, has a mass of 121 g (sensor and boom), stows on the hull, and deploys on a 60 cm boom from a three-unit CubeSat reducing the noise from the onboard reaction wheel to less than 1.5 nT at the sensor. The instrument's capabilities will be demonstrated and validated in space in late 2016 following the launch of the University of Alberta Ex-Alta 1 CubeSat, part of the QB50 constellation mission. We illustrate the potential scientific returns and utility of using a CubeSats carrying such fluxgate magnetometers to constitute a magnetospheric constellation using example data from the low-Earth orbit European Space Agency Swarm mission. Swarm data reveal significant changes in the spatiotemporal characteristics of the magnetic fields in the coupled magnetosphere-ionosphere system, even when the spacecraft are separated by only approximately 10 s along track and approximately 1.4° in longitude.

Water hammer with column separation : a historical review

NARCIS (Netherlands)

Bergant, A.; Simpson, A.R.; Tijsseling, A.S.

2006-01-01

Column separation refers to the breaking of liquid columns in fully filled pipelines. This may occur in a water-hammer event when the pressure in a pipeline drops to the vapor pressure at specific locations such as closed ends, high points or knees (changes in pipe slope). The liquid columns are

Continuous Fixed-Bed Column Study and Adsorption Modeling: Removal of Lead Ion from Aqueous Solution by Charcoal Originated from Chemical Carbonization of Rubber Wood Sawdust

Directory of Open Access Journals (Sweden)

Swarup Biswas

2015-01-01

Full Text Available The efficiency of chemically carbonized rubber wood sawdust for the removal of lead ion from the aqueous stream was investigated by column process. Chemically carbonized rubber wood sawdust was prepared by treating the sawdust with H2SO4 and HNO3. Maximum removal of lead ion in column process was found as 38.56 mg/g. The effects of operating parameters such as flow rate, bed depth, concentration, and pH were studied in column mode. Experimental data confirmed that the adsorption capacity increased with the increasing inlet concentration and bed depth and decreased with increasing flow rate. Thomas, Yoon-Nelson, and Adams-Bohart models were used to analyze the column experimental data and the relationship between operating parameters. Chemically carbonized rubber wood sawdust was characterized by using Fourier transform infrared spectroscopy. Scanning electron microscope was also utilized for morphological analysis of the adsorbent. Furthermore X-ray fluorescence spectrum analysis and energy dispersive X-ray spectroscopy were also used for the confirmation of lead adsorption process.

Quantitative composition determination at the atomic level using model-based high-angle annular dark field scanning transmission electron microscopy

International Nuclear Information System (INIS)

Martinez, G.T.; Rosenauer, A.; De Backer, A.; Verbeeck, J.; Van Aert, S.

2014-01-01

High angle annular dark field scanning transmission electron microscopy (HAADF STEM) images provide sample information which is sensitive to the chemical composition. The image intensities indeed scale with the mean atomic number Z. To some extent, chemically different atomic column types can therefore be visually distinguished. However, in order to quantify the atomic column composition with high accuracy and precision, model-based methods are necessary. Therefore, an empirical incoherent parametric imaging model can be used of which the unknown parameters are determined using statistical parameter estimation theory (Van Aert et al., 2009, [1]). In this paper, it will be shown how this method can be combined with frozen lattice multislice simulations in order to evolve from a relative toward an absolute quantification of the composition of single atomic columns with mixed atom types. Furthermore, the validity of the model assumptions are explored and discussed. - Highlights: • A model-based method is extended from a relative toward an absolute quantification of chemical composition of single atomic columns from HAADF HRSTEM images. • The methodology combines statistical parameter estimation theory with frozen lattice multislice simulations to quantify chemical composition atomic column by atomic column. • Validity and limitations of this model-based method are explored and discussed. • Quantification results obtained for a complex structure show agreement with EDX refinement

HPLC-CUPRAC post-column derivatization method for the determination of antioxidants: a performance comparison between porous silica and core-shell column packing.

Science.gov (United States)

Haque, Syed A; Cañete, Socrates Jose P

2018-01-01

An HPLC method employing a post-column derivatization strategy using the cupric reducing antioxidant capacity reagent (CUPRAC reagent) for the determining antioxidants in plant-based materials leverages the separation capability of regular HPLC approaches while allowing for detection specificity for antioxidants. Three different column types, namely core-shell and porous silica including two chemically different core-shell materials (namely phenyl-hexyl and C18), were evaluated to assess potential improvements that could be attained by changing from a porous silica matrix to a core-shell matrix. Tea extracts were used as sample matrices for the evaluation specifically looking at catechin and epigallocatechin gallate (EGCG). Both the C18 and phenyl-hexyl core-shell columns showed better performance compared to the C18 porous silica one in terms of separation, peak shape, and retention time. Among the two core-shell materials, the phenyl-hexyl column showed better resolving power compared to the C18 column. The CUPRAC post-column derivatization method can be improved using core-shell columns and suitable for quantifying antioxidants, exemplified by catechin and EGCG, in tea samples.

Prospecting For Magnetite Ore Deposits With A Innovative Sensor's of Unique Fundamentally New Magnetometer.

Science.gov (United States)

Emelianenko, T. I.; Tachaytdinov, R. S.; Sarichev, V. F.; Kotov, B. V.; Susoeva, G. N.

After careful study of principles and abilities of all existing magnetmeters of all three revolutions in magnetic prospecting we have come to the conclusion that they cannot solve local guestions of the magnetic prospecting or determine centre coordinates of magnetite ore body before drilling Electromagnetism lows and achievents magnetprospectings and radioelectronics of all 20th century serve as a theoretical base of the "locator". While creating this cardinally new magnetmeter , we borrowed different things from radio-prospectors, magnetprospectors, wireless operators and combined all of them while creating the "locators''. The "locators' construction is bas ed on the "magnetic intensification" principle ,owing to which this "locators" are characterised by hight sensitiveness and ability to determine centers of even little commercial magnetite ore deposits with relatively weak magnetic anomalies. The main advantage of the "locators" over existing ones is that it can solve local questions determine centre coordinates. A remarkably simple locator construction determine direction of the on-surface measurings towards the ore body centre and gives approximate prognosis resourses before/withour/ drilling. The "locators" were worked out for the first time in history , they have 2 licences. The fundamental design and drawbacks of the existing magnetometers have been inherited from the original magnetometre dating back two or three hundred years. The developers of the existing magnetometres have all gone along the same well- beaten track of replacing the primitive sensor in the form of a piece of ore hung on a string at first by an arrow sensor and later by magnetically oriented protons and quanta, with amplification of the sensors' OUTPUT signal. Furthermore, all the existing magnetometres are imperfect in that they, lacking the directivity of the ground-level magnetic measurements, only record the overall magnetic vector field generated by all the ore bodies around the

Directly coupled direct current superconducting quantum interference device magnetometers based on ramp-edge Ag:YBa2Cu3O7-x/PrBa2Cu3O7-x/Ag:YBa2Cu3O7-x junctions

International Nuclear Information System (INIS)

Jia, Q.X.; Yan, F.; Mombourquette, C.; Reagor, D.

1998-01-01

Directly coupled dc superconducting quantum interference device (SQUID) magnetometers on LaAlO 3 substrates were fabricated using ramp-edge superconductor/normal-metal/superconductor junctions, where Ag-doped YBa 2 Cu 3 O 7-x was used for the electrode and PrBa 2 Cu 3 O 7-x for the normal-metal barrier. A flux noise of 8x10 -6 Φ 0 Hz -1/2 at 10 kHz measured with a dc bias current was achieved at 75 K, which corresponded to a field sensitivity of 400fTHz -1/2 for a magnetometer with a pick-up loop area of 8.5mmx7.5mm. Most significantly, the noise floor increased at lower frequencies with a frequency dependence slightly less than 1/f. The field noise of the SQUID magnetometers increased by only 25% after cycling the devices from zero field to 500 mG. In a static earth close-quote s magnetic field background, the field noise of the SQUID magnetometers increased by less than a factor of 2. copyright 1998 American Institute of Physics

Graphene oxide sheets immobilized polystyrene for column preconcentration and sensitive determination of lead by flame atomic absorption spectrometry.

Science.gov (United States)

Islam, Aminul; Ahmad, Hilal; Zaidi, Noushi; Kumar, Suneel

2014-08-13

A novel solid-phase extractant was synthesized by coupling graphene oxide (GO) on chloromethylated polystyrene through an ethylenediamine spacer unit to develop a column method for the preconcentration/separation of lead prior to its determination by flame atomic absorption spectrometry. It was characterized by Fourier transform infrared spectroscopy, far-infrared spectroscopy, thermogravimetric analysis/differential thermal analysis, scanning electron microscopy, energy-dispersive spectrometry, and transmission electron microscopy. The abundant oxygen-containing surface functional groups form a strong complex with lead, resulting in higher sorption capacity (227.92 mg g(-1)) than other nanosorbents used for sorption studies of the column method. Using the column procedure here is an alternative to the direct use of GO, which restricts irreversible aggregation of GO and its escape into the ecosystem, making it an environmentally sustainable method. The column method was optimized by varying experimental variables such as pH, flow rate for sorption/desorption, and elution condition and was observed to exhibit a high preconcentration factor (400) with a low preconcentration limit (2.5 ppb) and a high degree of tolerance for matrix ions. The accuracy of the proposed method was verified by determining the Pb content in the standard reference materials and by recovery experiments. The method showed good precision with a relative standard deviation <5%. The proposed method was successfully applied for the determination of lead in tap water, electroplating wastewater, river water, and food samples after preconcentration.

Application of a Fast Separation Method for Anti-diabetics in Pharmaceuticals Using Monolithic Column: Comparative Study With Silica Based C-18 Particle Packed Column.

Science.gov (United States)

Hemdan, A; Abdel-Aziz, Omar

2018-04-01

Run time is a predominant factor in HPLC for quality control laboratories especially if there is large number of samples have to be analyzed. Working at high flow rates cannot be attained with silica based particle packed column due to elevated backpressure issues. The use of monolithic column as an alternative to traditional C-18 column was tested for fast separation of pharmaceuticals, where the results were very competitive. The performance comparison of both columns was tested for separation of anti-diabetic combination containing Metformin, Pioglitazone and Glimepiride using Gliclazide as an internal standard. Working at high flow rates with less significant backpressure was obtained with the monolithic column where the run time was reduced from 6 min in traditional column to only 1 min in monolithic column with accepted resolution. The structure of the monolith contains many pores which can adapt the high flow rate of the mobile phase. Moreover, peak symmetry and equilibration time were more efficient with monolithic column.

Determination of physical and dynamic properties of suspended particles in water column with ultrasonic scanning in between the water surface and stable sediment layer.

Science.gov (United States)

Acar, Dursun; Alpar, Bedri; Ozeren, Sinan; Cagatay, Namık; Sari, Erol; Vardar, Denizhan; Eris, Kadir

2015-04-01

The behavior of seafloor sediment with its water column should be known against any occurrences of anoxic or oxic conditions. The most important ones of these conditions are possible leakage of natural gas or escape of liquids from sediment. On the basis of combined solid/liquid flow dynamics in sedimentation, such kind of events can change, even in an effective manner, the dynamic movements of molecules and their cumulative mass of particules, i.e. the suspended materials. The deployment of suitable sediment traps or ultrasonic transducers somewhere in the water column are not easy attempts in order to obtain useful information about the state of suspended materials during sedimentation. These are usually bulky instruments; therefore they may behave like an anti-move suppresser on the particles moving in the float direction, in oxic and anoxic manner. These instruments, on the other hand, may cover the effects of diffusive flow or bubble formed gas and fluid escape from the sediment surface into the water column. Ultrasonic scanners, however, are able to make observations in a remote manner, without affecting such artificial events. Our field trials were successfully completed at the historical estuary called Halic of Marmara sea . The physical properties; such as the velocity of particles, their travel directions, their dimensions and the ability to observe anti-compositor crushes of shock waves of the bubbles are only a few of these observations in natural ambience. The most important problem solved about water pressure during 3 atmosphere . The sensor has been tested successfully few times. We used the ''High voltage electric isolator oil filling'' to the inside of the scanner for pressure equalization between outer side and inner body of probe at a depth of (20 meters) beneath the sea surface . The transmitted signals by the planar crystal of the transducer become weaker under the pressure of overlying water column in depths. Our efforts are now focused on the

Preparation and evaluation of 400μm I.D. polymer-based hydrophilic interaction chromatography monolithic columns with high column efficiency.

Science.gov (United States)

Liu, Chusheng; Li, Haibin; Wang, Qiqin; Crommen, Jacques; Zhou, Haibo; Jiang, Zhengjin

2017-08-04

The quest for higher column efficiency is one of the major research areas in polymer-based monolithic column fabrication. In this research, two novel polymer-based HILIC monolithic columns with 400μm I.D.×800μm O.D. were prepared based on the thermally initiated co-polymerization of N,N-dimethyl-N-(3-methacrylamidopropyl)-N-(3-sulfopropyl) ammonium betaine (SPP) and ethylene glycol dimethacrylate (EDMA) or N,N'-methylenebisacrylamide (MBA). In order to obtain a satisfactory performance in terms of column permeability, mechanical stability, efficiency and selectivity, the polymerization parameters were systematically optimized. Column efficiencies as high as 142, 000 plates/m and 120, 000 plates/m were observed for the analysis of neutral compounds at 0.6mm/s on the poly(SPP-co-MBA) and poly(SPP-co-EDMA) monoliths, respectively. Furthermore, the Van Deemter plots for thiourea on the two monoliths were compared with that on a commercial silica based ZIC-HILIC column (3.5μm, 200Å, 150mm×300μm I.D.) using ACN/H 2 O (90/10, v/v) as the mobile phase at room temperature. It was noticeable that the Van Deemter curves for both monoliths, particularly the poly(SPP-co-MBA) monolith, are significantly flatter than that obtained for the ZIC-HILIC column, which indicates that in spite of their larger internal diameters, they yield better overall efficiency, with less peak dispersion, across a much wider range of usable linear velocities. A clearly better separation performance was also observed for nucleobases, nucleosides, nucleotides and small peptides on the poly(SPP-co-MBA) monolith compared to the ZIC-HILIC column. It is particularly worth mentioning that these 400μm I.D. polymer-based HILIC monolithic columns exhibit enhanced mechanical strength owing to the thicker capillary wall of the fused-silica capillaries. Copyright © 2017 Elsevier B.V. All rights reserved.

Auto-Calibration Methods of Kinematic Parameters and Magnetometer Offset for the Localization of a Tracked Mobile Robot

Directory of Open Access Journals (Sweden)

Luciano Cantelli

2016-11-01

Full Text Available This paper describes an automatic calibration procedure adopted to improve the localization of an outdoor mobile robot. The proposed algorithm estimates, by using an extended Kalman filter, the main kinematic parameters of the vehicles, such as the wheel radii and the wheelbase as well as the magnetometer offset. Several trials have been performed to validate the proposed strategy on a tracked electrical mobile robot. The mobile robot is aimed to be adopted as a tool to help humanitarian demining operations.

HEAT TRANSFER ANALYSIS FOR FIXED CST AND RF COLUMNS

International Nuclear Information System (INIS)

Lee, S

2007-01-01

In support of a small column ion exchange (SCIX) process for the Savannah River Site waste processing program, transient and steady state two-dimensional heat transfer models have been constructed for columns loaded with cesium-saturated crystalline silicotitanate (CST) or spherical Resorcinol-Formaldehyde (RF) beads and 6 molar sodium tank waste supernate. Radiolytic decay of sorbed cesium results in heat generation within the columns. The models consider conductive heat transfer only with no convective cooling and no process flow within the columns (assumed column geometry: 27.375 in ID with a 6.625 in OD center-line cooling pipe). Heat transfer at the column walls was assumed to occur by natural convection cooling with 35 C air. A number of modeling calculations were performed using this computational heat transfer approach. Minimal additional calculations were also conducted to predict temperature increases expected for salt solution processed through columns of various heights at the slowest expected operational flow rate of 5 gpm. Results for the bounding model with no process flow and no active cooling indicate that the time required to reach the boiling point of ∼130 C for a CST-salt solution mixture containing 257 Ci/liter of Cs-137 heat source (maximum expected loading for SCIX applications) at 35 C initial temperature is about 6 days. Modeling results for a column actively cooled with external wall jackets and the internal coolant pipe (inlet coolant water temperature: 25 C) indicate that the CST column can be maintained non-boiling under these conditions indefinitely. The results also show that the maximum temperature of an RF-salt solution column containing 133 Ci/liter of Cs-137 (maximum expected loading) will never reach boiling under any conditions (maximum predicted temperature without cooling: 88 C). The results indicate that a 6-in cooling pipe at the center of the column provides the most effective cooling mechanism for reducing the maximum

Preparation of a β-Cyclodextrin-Based Open-Tubular Capillary Electrochromatography Column and Application for Enantioseparations of Ten Basic Drugs.

Directory of Open Access Journals (Sweden)

Linlin Fang

Full Text Available An open-tubular capillary electrochromatography column was prepared by chemically immobilized β-cyclodextrin modified gold nanoparticles onto new surface with the prederivatization of (3-mercaptopropyl-trimethoxysilane. The synthesized nanoparticles and the prepared column were characterized by transmission electron microscopy, scanning electron microscopy, infrared spectroscopy and ultraviolet visible spectroscopy. When the column was employed as the chiral stationary phase, no enantioselectivity was observed for ten model basic drugs. So β-cyclodextrin was added to the background electrolyte as chiral additive to expect a possible synergistic effect occurring and resulting in a better separation. Fortunately, significant improvement in enantioselectivity was obtained for ten pairs of drug enantiomers. Then, the effects of β-cyclodextrin concentration and background electrolyte pH on the chiral separation were investigated. With the developed separation mode, all the enantiomers (except for venlafaxine were baseline separated in resolutions of 4.49, 1.68, 1.88, 1.57, 2.52, 2.33, 3.24, 1.63 and 3.90 for zopiclone, chlorphenamine maleate, brompheniramine maleate, dioxopromethazine hydrochloride, carvedilol, homatropine hydrobromide, homatropine methylbromide, venlafaxine, sibutramine hydrochloride and terbutaline sulfate, respectively. Further, the possible separation mechanism involved was discussed.

Daytime, low latitude, vertical ExB drift velocities, inferred from ground-based magnetometer observations in the Peruvian, Philippine and Indian longitude sectors under quiet and disturbed conditions

CERN Document Server

Anderson, D; Chau, J; Yumoto, K; Bhattacharya, A; Alex, S

2006-01-01

Daytime, low latitude, vertical ExB drift velocities, inferred from ground-based magnetometer observations in the Peruvian, Philippine and Indian longitude sectors under quiet and disturbed conditions

The design of a new concept chromatography column.

Science.gov (United States)

Camenzuli, Michelle; Ritchie, Harald J; Ladine, James R; Shalliker, R Andrew

2011-12-21

Active Flow Management is a new separation technique whereby the flow of mobile phase and the injection of sample are introduced to the column in a manner that allows migration according to the principles of the infinite diameter column. A segmented flow outlet fitting allows for the separation of solvent or solute that elutes along the central radial section of the column from that of the sample or solvent that elutes along the wall region of the column. Separation efficiency on the analytical scale is increased by 25% with an increase in sensitivity by as much as 52% compared to conventional separations.

Inert carriers for column extraction chromatography

International Nuclear Information System (INIS)

Katykhin, G.S.

1978-01-01

Inert carriers used in column extraction chromatography are reviewed. Such carriers are devided into two large groups: hydrophilic carriers which possess high surface energy and are well wetted only with strongly polar liquids (kieselguhrs, silica gels, glasses, cellulose, Al 2 O 3 ) and water-repellent carriers which possess low surface energy and are well wetted with various organic solvents (polyethylene, polytetrafluorethylene polytrifluorochlorethylene). Properties of various carriers are presented: structure, chemical and radiation stability, adsorption properties, extracting agent capacity. The effect of structure and sizes of particles on the efficiency of chromatography columns is considered. Ways of immovable phase deposition on the carrier and the latter's regeneration. Peculiarities of column packing for preparative and continuous chromatography are discussed

Feasibility study on measurement of magnetocardiography (MCG) using fluxgate magnetometer

Science.gov (United States)

Sengottuvel, S.; Sharma, Akash; Biswal, Deepak; Khan, Pathan Fayaz; Swain, Pragyna Parimita; Patel, Rajesh; Gireesan, K.

2018-04-01

This paper reports the feasibility of measuring weak magnetic fields generated by the electrical activity of the heart using a portable tri-axial fluxgate magnetometer inside a magnetically shielded room. Measurement of Magnetocardiogram (MCG) signals could be successfully demonstrated from a healthy subject using a novel set-up involving a reference fluxgate sensor which simultaneously measures the magnetic fields associated with the ECG waveform measured on the same subject. The timing information provided by R wave peaks of ECG recorded by the reference sensor is utilized to generate trigger locked average of the sensor output of the measurement fluxgate, and extract MCG signals in all the three orthogonal directions (X, Y and Z) on the anterior thorax. It is expected that such portable room temperature measurements using fluxgate sensor could assist in validating the direction of the equivalent current dipole associated with the electrical activity of the human heart. This is somewhat difficult in conventional MCG measurements using SQUID sensors, which usually furnish only the z component of the magnetic field and its spatial derivatives.

Dynamic effects of diabatization in distillation columns

DEFF Research Database (Denmark)

Bisgaard, Thomas; Huusom, Jakob Kjøbsted; Abildskov, Jens

2013-01-01

The dynamic effects of diabatization in distillation columns are investigated in simulation emphasizing the heat-integrated distillation column (HIDiC). A generic, dynamic, first-principle model has been formulated, which is flexible enough to describe various diabatic distillation configurations....... Dynamic Relative Gain Array and Singular Value Analysis have been applied in a comparative study of a conventional distillation column and a HIDiC. The study showed increased input-output coupling due to diabatization. Feasible SISO control structures for the HIDiC were also found and control...

Dynamic Effects of Diabatization in Distillation Columns

DEFF Research Database (Denmark)

Bisgaard, Thomas; Huusom, Jakob Kjøbsted; Abildskov, Jens

2012-01-01

The dynamic eects of diabatization in distillation columns are investigated in simulation with primary focus on the heat-integrated distillation column (HIDiC). A generic, dynamic, rst-principle model has been formulated, which is exible to describe various diabatic distillation congurations....... Dynamic Relative Gain Array and Singular Value Analysis have been applied in a comparative study of a conventional distillation column and a HIDiC. The study showed increased input-output coupling due to diabatization. Feasible SISO control structures for the HIDiC were also found. Control...

Fringing-field effects in acceleration columns

International Nuclear Information System (INIS)

Yavor, M.I.; Weick, H.; Wollnik, H.

1999-01-01

Fringing-field effects in acceleration columns are investigated, based on the fringing-field integral method. Transfer matrices at the effective boundaries of the acceleration column are obtained, as well as the general transfer matrix of the region separating two homogeneous electrostatic fields with different field strengths. The accuracy of the fringing-field integral method is investigated

Column properties and flow profiles of a flat, wide column for high-pressure liquid chromatography.

Science.gov (United States)

Mriziq, Khaled S; Guiochon, Georges

2008-04-11

The design and the construction of a pressurized, flat, wide column for high-performance liquid chromatography (HPLC) are described. This apparatus, which is derived from instruments that implement over-pressured thin layer chromatography, can carry out only uni-dimensional chromatographic separations. However, it is intended to be the first step in the development of more powerful instruments that will be able to carry out two-dimensional chromatographic separations, in which case, the first separation would be a space-based separation, LC(x), taking place along one side of the bed and the second separation would be a time-based separation, LC(t), as in classical HPLC but proceeding along the flat column, not along a tube. The apparatus described consists of a pressurization chamber made of a Plexiglas block and a column chamber made of stainless steel. These two chambers are separated by a thin Mylar membrane. The column chamber is a cavity which is filled with a thick layer (ca. 1mm) of the stationary phase. Suitable solvent inlet and outlet ports are located on two opposite sides of the sorbent layer. The design allows the preparation of a homogenous sorbent layer suitable to be used as a chromatographic column, the achievement of effective seals of the stationary phase layer against the chamber edges, and the homogenous flow of the mobile phase along the chamber. The entire width of the sorbent layer area can be used to develop separations or elute samples. The reproducible performance of the apparatus is demonstrated by the chromatographic separations of different dyes. This instrument is essentially designed for testing detector arrays to be used in a two-dimensional LC(x) x LC(t) instrument. The further development of two-dimension separation chromatographs based on the apparatus described is sketched.

Real-time Geomagnetic Data from a Raspberry Pi Magnetometer Network in the United Kingdom

Science.gov (United States)

Case, N.; Beggan, C.; Marple, S. R.

2017-12-01

In 2014, BGS and the University of Lancaster won an STFC Public Engagement grant to build and deploy 10 Raspberry Pi magnetometers to secondary schools across the UK to enable citizen science. The system uses a Raspberry Pi computer as a logging and data transfer device, connected to a set of three orthogonal miniature fluxgate magnetometers. The system has a nominal sensitivity of around 1 nanoTesla (nT), in each component direction (North, East and Down). This is around twenty times less sensitive than a current scientific-level instrument, but given its relatively low-cost, at about £250 ($325) per unit, this is an excellent price-to-performance ratio given we could not improve the sensitivity unless we spent a lot more money. The magnetic data are sampled at a 5 second cadence and sent to the AuroraWatch website at Lancaster University every 2 minutes. The data are freely available to view and download. The primary aim of the project is to encourage students from 14-18 years old to look at how sensors can be used to collect geophysical data and integrate it together to give a wider understanding of physical phenomena. A second aim is to provide useful data on the spatial variation of the magnetic field for analysis of geomagnetic storms, alongside data from the BGS observatory and University of Lancaster's SAMNET variometer network. We show results from the build, testing and running of the sensors including some recent storms and we reflect on our experiences in engaging schools and the general public with information about the magnetic field. The information to build the system and logging and analysis software for the Raspberry Pi is all freely available, allowing those interested to participate in the project as citizen scientists.

Cesium ion exchange using actual waste: Column size considerations

International Nuclear Information System (INIS)

Brooks, K.P.

1996-04-01

It is presently planned to remove cesium from Hanford tank waste supernates and sludge wash solutions using ion exchange. To support the development of a cesium ion exchange process, laboratory experiments produced column breakthrough curves using wastes simulants in 200 mL columns. To verify the validity of the simulant tests, column runs with actual supernatants are being planned. The purpose of these actual waste tests is two-fold. First, the tests will verify that use of the simulant accurately reflects the equilibrium and rate behavior of the resin compared to actual wastes. Batch tests and column tests will be used to compare equilibrium behaviors and rate behaviors, respectively. Second, the tests will assist in clarifying the negative interactions between the actual waste and the ion exchange resin, which cannot be effectively tested with simulant. Such interactions include organic fouling of the resin and salt precipitation in the column. These effects may affect the shape of the column breakthrough curve. The reduction in column size also may change the shape of the curve, making the individual effects even more difficult to sort out. To simplify the evaluation, the changes due to column size must be either understood or eliminated. This report describes the determination of the column size for actual waste testing that best minimizes the effect of scale-down. This evaluation will provide a theoretical basis for the dimensions of the column. Experimental testing is still required before the final decision can be made. This evaluation will be confined to the study of CS-100 and R-F resins with NCAW simulant and to a limited extent DSSF waste simulant. Only the cesium loading phase has been considered

A xylophone bar magnetometer for micro/pico satellites

Science.gov (United States)

Lamy, Hervé; Niyonzima, Innocent; Rochus, Pierre; Rochus, Véronique

2010-10-01

The Belgian Institute of Space Aeronomy (BIRA-IASB), "Centre Spatial de Liège" (CSL), "Laboratoire de Techniques Aéronautiques et Spatiales" (LTAS) of University of Liège, and the Microwave Laboratory of University of Louvain-La-Neuve (UCL) are collaborating in order to develop a miniature version of a xylophone bar magnetometer (XBM) using Microelectromechanical Systems (MEMS) technology. The device is based on a classical resonating xylophone bar. A sinusoidal current is supplied to the bar oscillating at the fundamental transverse resonant mode of the bar. When an external magnetic field is present, the resulting Lorentz force causes the bar to vibrate at its fundamental frequency with an amplitude directly proportional to the vertical component of the ambient magnetic field. In this paper we illustrate the working principles of the XBM and the challenges to reach the required sensitivity in space applications (measuring magnetic fields with an accuracy of approximately of 0.1 nT). The optimal dimensions of the MEMS XBM are discussed as well as the constraints on the current flowing through the bar. Analytical calculations as well as simulations with finite element methods have been used. Prototypes have been built in the Microwave Laboratory using silicon on insulator (SOI) and bulk micromachining processes. Several methods to accurately measure the displacement of the bar are proposed.

Stability of embankments over cement deep soil mixing columns

International Nuclear Information System (INIS)

Morilla Moar, P.; Melentijevic, S.

2014-01-01

The deep soil mixing (DSM) is one of the ground improvement methods used for the construction of embankments over soft soils. DSM column-supported embankments are constructed over soft soils to accelerate its construction, improve embankment stability, increase bearing capacity and control of total and differential settlements. There are two traditional design methods, the Japanese (rigid columns) and the scandinavian (soft and semi-rigid columns). Based on Laboratory analysis and numerical analysis these traditional approaches have been questioned by several authors due to its overestimation of the embankment stability considering that the most common failures types are not assumed. This paper presents a brief review of traditional design methods for embankments on DSM columns constructed in soft soils, studies carried out determine the most likely failure types of DSM columns, methods to decrease the overestimation when using limit equilibrium methods and numerical analysis methods that permit detect appropriate failure modes in DSM columns. Finally a case study was assessed using both limited equilibrium and finite element methods which confirmed the overestimation in the factors of safety on embankment stability over DSM columns. (Author)

Vertebral Column Resection for Rigid Spinal Deformity.

Science.gov (United States)

Saifi, Comron; Laratta, Joseph L; Petridis, Petros; Shillingford, Jamal N; Lehman, Ronald A; Lenke, Lawrence G

2017-05-01

Broad narrative review. To review the evolution, operative technique, outcomes, and complications associated with posterior vertebral column resection. A literature review of posterior vertebral column resection was performed. The authors' surgical technique is outlined in detail. The authors' experience and the literature regarding vertebral column resection are discussed at length. Treatment of severe, rigid coronal and/or sagittal malalignment with posterior vertebral column resection results in approximately 50-70% correction depending on the type of deformity. Surgical site infection rates range from 2.9% to 9.7%. Transient and permanent neurologic injury rates range from 0% to 13.8% and 0% to 6.3%, respectively. Although there are significant variations in EBL throughout the literature, it can be minimized by utilizing tranexamic acid intraoperatively. The ability to correct a rigid deformity in the spine relies on osteotomies. Each osteotomy is associated with a particular magnitude of correction at a single level. Posterior vertebral column resection is the most powerful posterior osteotomy method providing a successful correction of fixed complex deformities. Despite meticulous surgical technique and precision, this robust osteotomy technique can be associated with significant morbidity even in the most experienced hands.

Effect of backmixing on pulse column performance

International Nuclear Information System (INIS)

Miao, Y.W.

1979-05-01

A critical survey of the published literature concerning dispersed phase holdup and longitudinal mixing in pulsed sieve-plate extraction columns has been made to assess the present state-of-the-art in predicting these two parameters, both of which are of critical importance in the development of an accurate mathematical model of the pulse column. Although there are many conflicting correlations of these variables as a function of column geometry, operating conditions, and physical properties of the liquid systems involved it has been possible to develop new correlations which appear to be useful and which are consistent with much of the available data over the limited range of variables most likely to be encountered in plant sized equipment. The correlations developed were used in a stagewise model of the pulse column to predict product concentrations, solute inventory, and concentration profiles in a column for which limited experimental data were available. Reasonable agreement was obtained between the mathematical model and the experimental data. Complete agreement, however, can only be obtained after a correlation for the extraction efficiency has been developed. The correlation of extraction efficiency was beyond the scope of this work

Adaption of the Magnetometer Towed Array geophysical system to meet Department of Energy needs for hazardous waste site characterization

International Nuclear Information System (INIS)

Cochran, J.R.; McDonald, J.R.; Russell, R.J.; Robertson, R.; Hensel, E.

1995-10-01

This report documents US Department of Energy (DOE)-funded activities that have adapted the US Navy's Surface Towed Ordnance Locator System (STOLS) to meet DOE needs for a ''... better, faster, safer and cheaper ...'' system for characterizing inactive hazardous waste sites. These activities were undertaken by Sandia National Laboratories (Sandia), the Naval Research Laboratory, Geo-Centers Inc., New Mexico State University and others under the title of the Magnetometer Towed Array (MTA)

Aberration-corrected scanning transmission electron microscopy of semiconductors

International Nuclear Information System (INIS)

Krivanek, O L; Dellby, N; Murfitt, M F

2011-01-01

The scanning transmission electron microscope (STEM) has been able to image individual heavy atoms in a light matrix for some time. It is now able to do much more: it can resolve individual atoms as light as boron in monolayer materials; image atomic columns as light as hydrogen, identify the chemical type of individual isolated atoms from the intensity of their annular dark field (ADF) image and by electron energy loss spectroscopy (EELS); and map elemental composition at atomic resolution by EELS and energy-dispersive X-ray spectroscopy (EDXS). It can even map electronic states, also by EELS, at atomic resolution. The instrumentation developments that have made this level of performance possible are reviewed, and examples of applications to semiconductors and oxides are shown.

The effect of winding and core support material on the thermal gain dependence of a fluxgate magnetometer sensor

Science.gov (United States)

Miles, David M.; Mann, Ian R.; Kale, Andy; Milling, David K.; Narod, Barry B.; Bennest, John R.; Barona, David; Unsworth, Martyn J.

2017-10-01

Fluxgate magnetometers are an important tool in geophysics and space physics but are typically sensitive to variations in sensor temperature. Changes in instrumental gain with temperature, thermal gain dependence, are thought to be predominantly due to changes in the geometry of the wire coils that sense the magnetic field and/or provide magnetic feedback. Scientific fluxgate magnetometers typically employ some form of temperature compensation and support and constrain wire sense coils with bobbins constructed from materials such as MACOR machinable ceramic (Corning Inc.) which are selected for their ultra-low thermal deformation rather than for robustness, cost, or ease of manufacturing. We present laboratory results comparing the performance of six geometrically and electrically matched fluxgate sensors in which the material used to support the windings and for the base of the sensor is varied. We use a novel, low-cost thermal calibration procedure based on a controlled sinusoidal magnetic source and quantitative spectral analysis to measure the thermal gain dependence of fluxgate magnetometer sensors at the ppm°C-1 level in a typical magnetically noisy university laboratory environment. We compare the thermal gain dependence of sensors built from MACOR, polyetheretherketone (PEEK) engineering plastic (virgin, 30 % glass filled and 30 % carbon filled), and acetal to examine the trade between the thermal properties of the material, the impact on the thermal gain dependence of the fluxgate, and the cost and ease of manufacture. We find that thermal gain dependence of the sensor varies as one half of the material properties of the bobbin supporting the wire sense coils rather than being directly related as has been historically thought. An experimental sensor constructed from 30 % glass-filled PEEK (21.6 ppm°C-1) had a thermal gain dependence within 5 ppm°C-1 of a traditional sensor constructed from MACOR ceramic (8.1 ppm°C-1). If a modest increase in thermal

Interaction diagrams for composite columns exposed to fire

Directory of Open Access Journals (Sweden)

Milanović Milivoje

2014-01-01

Full Text Available The bearing capacity of the cross section of composite column in fire conditions through changes in the interaction diagram 'bending moment-axialforce' were analyzed in this paper. The M-N interaction diagram presents the relationship between the intensities of the bending moment and the axial force as actions on the column cross section, or the relationship between the design value of the plastic resistance to axial compression of the total cross-section Npl, Rd and the design value of the bending moment resistance Mpl, Rd. It is well known that the temperature increase causes decrease of the load-bearing characteristics of the constitutive materials. This effect directly reflects on the reduction of the axial force and the bending moment that could be accepted by the column cross section. Interaction diagrams for three different types of column cross sections for five different maximal temperatures developed during the fire action were defined. For that purpose the software package SAFIR was used. The columns, materials and load characteristics, as well as all other terms and conditions, were taken in accordance with the relevant Eurocodes and the theory of composite columns.

Recovery of deuterium from H-D gas mixture by thermal diffusion in a multi-concentric-tube column device of fixed total sum of column heights with transverse sampling streams

International Nuclear Information System (INIS)

Yeh, H.-M.

2010-01-01

The effect of the increment in the number of concentric-tube thermal diffusion columns on the recovery of deuterium from H 2 -HD-D 2 system with fixed total sum of column heights, has been investigated. The equations for predicting the degrees of separation in single-column, double-column and triple-column devices have been derived. Considerable improvement in recovery can be achieved if a multi-column device with larger number of column is employed, instead of a single-column device with column height equal to the same total sum of column heights, especially for the case of higher flow-rate operation and larger total sum of column heights.

Dynamics of annular bright field imaging in scanning transmission electron microscopy

International Nuclear Information System (INIS)

Findlay, S.D.; Shibata, N.; Sawada, H.; Okunishi, E.; Kondo, Y.; Ikuhara, Y.

2010-01-01

We explore the dynamics of image formation in the so-called annular bright field mode in scanning transmission electron microscopy, whereby an annular detector is used with detector collection range lying within the cone of illumination, i.e. the bright field region. We show that this imaging mode allows us to reliably image both light and heavy columns over a range of thickness and defocus values, and we explain the contrast mechanisms involved. The role of probe and detector aperture sizes is considered, as is the sensitivity of the method to intercolumn spacing and local disorder.

Enrichment of heavy water in thermal-diffusion columns connected in series

International Nuclear Information System (INIS)

Yeh, Ho-Ming; Chen, Liu Yi

2009-01-01

The separation equations for enrichment of heavy water from water isotope mixture by thermal diffusion in multiple columns connected in series, have been derived based on one column design developed in previous work. The improvement in separation is achievable by operating in a double-column device, instead of in a single-column device, with the same total column length. It is also found that further improvement in separation is obtainable if a triple-column device is employed, except for operating under small total column length and low flow rate.

Multi-Column Experimental Test Bed for Xe/Kr Separation

International Nuclear Information System (INIS)

Greenhalgh, Mitchell Randy; Garn, Troy Gerry; Welty, Amy Keil; Lyon, Kevin Lawrence; Watson, Tony Leroy

2015-01-01

Previous research studies have shown that INL-developed engineered form sorbents are capable of capturing both Kr and Xe from various composite gas streams. The previous experimental test bed provided single column testing for capacity evaluations over a broad temperature range. To advance research capabilities, the employment of an additional column to study selective capture of target species to provide a defined final gas composition for waste storage was warranted. The second column addition also allows for compositional analyses of the final gas product to provide for final storage determinations. The INL krypton capture system was modified by adding an additional adsorption column in order to create a multi-column test bed. The purpose of this modification was to investigate the separation of xenon from krypton supplied as a mixed gas feed. The extra column was placed in a Stirling Ultra-low Temperature Cooler, capable of controlling temperatures between 190 and 253K. Additional piping and valves were incorporated into the system to allow for a variety of flow path configurations. The new column was filled with the AgZ-PAN sorbent which was utilized as the capture medium for xenon while allowing the krypton to pass through. The xenon-free gas stream was then routed to the cryostat filled with the HZ-PAN sorbent to capture the krypton at 191K. Selectivities of xenon over krypton were determined using the new column to verify the system performance and to establish the operating conditions required for multi-column testing. Results of these evaluations verified that the system was operating as designed and also demonstrated that AgZ-PAN exhibits excellent selectivity for xenon over krypton in air at or near room temperature. Two separation tests were performed utilizing a feed gas consisting of 1000 ppmv xenon and 150 ppmv krypton with the balance being made up of air. The AgZ-PAN temperature was held at 295 or 253K while the HZ-PAN was held at 191K for both

Convolutional Codes with Maximum Column Sum Rank for Network Streaming

OpenAIRE

Mahmood, Rafid; Badr, Ahmed; Khisti, Ashish

2015-01-01

The column Hamming distance of a convolutional code determines the error correction capability when streaming over a class of packet erasure channels. We introduce a metric known as the column sum rank, that parallels column Hamming distance when streaming over a network with link failures. We prove rank analogues of several known column Hamming distance properties and introduce a new family of convolutional codes that maximize the column sum rank up to the code memory. Our construction invol...

Microbially induced carbonate precipitation (MICP) by denitrification as ground improvement method - Process control in sand column experiments

Science.gov (United States)

Pham, Vinh; van Paassen, Leon; Nakano, Akiko; Kanayama, Motohei; Heimovaara, Timo

2013-04-01

Calcite precipitation induced by microbes has been proven to be efficient in stabilizing granular soils, especially with urea hydrolysis, as it has been successfully demonstrated in a pilot application 2010. However, as a byproduct highly concentrated ammonium chloride (NH4Cl) solution is produced, which has to be removed and disposed and forms a significant disadvantage of the technique that makes an alternative process like denitrification preferred. The proof of principle of microbially induced calcite precipitation (MICP) by denitrification has been demonstrated by Van Paassen et al (2010) who suggested that instead of producing waste as a byproduct, different pre-treated waste streams could be used as substrates for in situ growth of denitrifying bacteria and simultaneous cementation without producing waste to be removed. In this study sand column experiments are performed in which calcium carbonate was successfully precipitated by indigenous denitrifying micro-organisms, which were supplied weekly with a pulse of a substrate solution containing calcium acetate and calcium nitrate. Besides the production of calcite and the growth of bacteria in biofilms, the reduction of nitrate resulted in the production of (nitrogen) gas. It was observed that this gas partly fills up the pore space and consequently contributed to a reduction of the permeability of the treated sand. The presence of gas in the pore space affected the flow of the injected substrates and influenced to the distribution of calcium carbonate. The effect of the mean particle size (D50) on the flow and transport of solutes and gas in the porous media has been evaluated by treating several columns with varying grain size distribution and comparing the change in permeability after each incubation period and analyzing the distribution of the gas throughout the columns using X-ray computed tomography (CT) scanning. The present results show that there is a considerable decrease of permeability - a

Acute cervical cord injury without fracture or dislocation of the spinal column.