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Sample records for scan particle spectrometer

  1. TSI Model 3936 Scanning Mobility Particle Spectrometer Instrument Handbook

    Energy Technology Data Exchange (ETDEWEB)

    Kuang, C. [Brookhaven National Lab. (BNL), Upton, NY (United States)

    2016-02-01

    The Model 3936 Scanning Mobility Particle Spectrometer (SMPS) measures the size distribution of aerosols ranging from 10 nm up to 1000 nm. The SMPS uses a bipolar aerosol charger to keep particles within a known charge distribution. Charged particles are classified according to their electrical mobility, using a long-column differential mobility analyzer (DMA). Particle concentration is measured with a condensation particle counter (CPC). The SMPS is well-suited for applications including: nanoparticle research, atmospheric aerosol studies, pollution studies, smog chamber evaluations, engine exhaust and combustion studies, materials synthesis, filter efficiency testing, nucleation/condensation studies, and rapidly changing aerosol systems.

  2. Creation of the precision magnetic spectrometer SCAN-3

    Directory of Open Access Journals (Sweden)

    Afanasiev S.V.

    2017-01-01

    Full Text Available The new JINR project [1] is aimed at studies of highly excited nuclear matter created in nuclei by a high-energy deuteron beam. The matter is studied through observation of its particular decay products - pairs of energetic particles with a wide opening angle, close to 180°. The new precision hybrid magnetic spectrometer SCAN-3 is to be built for detecting charged (π±, K±, p and neutral (n particles produced at the JINR Nuclotron internal target in dA collisions. One of the main and complex tasks is a study of low-energy ηA interaction and a search for η-bound states (η-mesic nuclei. Basic elements of the spectrometer and its characteristics are discussed in the article.

  3. Creation of the precision magnetic spectrometer SCAN-3

    Science.gov (United States)

    Afanasiev, S. V.; Anisimov, Yu. S.; Baldin, A. A.; Berlev, A. I.; Dryablov, D. K.; Dubinchik, B. V.; Elishev, A. F.; Fateev, O. V.; Igamkulov, Z. A.; Krechetov, Yu. F.; Kudashkin, I. V.; Kuznechov, S. N.; Malakhov, A. I.; Smirnov, V. A.; Shimansky, S. S.; Kliman, J.; Matousek, V.; Gmutsa, S.; Turzo, I.; Cruceru, I.; Cruceru, M.; Constantin, F.; Niolescu, G.; Ciolacu, L.; Paraipan, M.; Vokál, S.; Vrláková, J.; Baskov, V. A.; Lebedev, A. I.; L'vov, A. I.; Pavlyuchenko, L. N.; Polyansky, V. V.; Rzhanov, E. V.; Sidorin, S. S.; Sokol, G. A.; Glavanakov, I. V.; Tabachenko, A. N.; Jomurodov, D. M.; Bekmirzaev, R. N.; Ibadov, R. M.; Sultanov, M. U.

    2017-03-01

    The new JINR project [1] is aimed at studies of highly excited nuclear matter created in nuclei by a high-energy deuteron beam. The matter is studied through observation of its particular decay products - pairs of energetic particles with a wide opening angle, close to 180°. The new precision hybrid magnetic spectrometer SCAN-3 is to be built for detecting charged (π±, K±, p) and neutral (n) particles produced at the JINR Nuclotron internal target in dA collisions. One of the main and complex tasks is a study of low-energy ηA interaction and a search for η-bound states (η-mesic nuclei). Basic elements of the spectrometer and its characteristics are discussed in the article.

  4. Charged particle scintillation mass spectrometer

    International Nuclear Information System (INIS)

    Baranov, P.S.; Zhuravlev, E.E.; Nafikov, A.A.; Osadchi , A.I.; Raevskij, V.G.; Smirnov, P.A.; Cherepnya, S.N.; Yanulis, Yu.P.

    1982-01-01

    A scintillation mass-spectrometer for charged particle identification by the measured values of time-of-flight and energy operating on line with the D-116 computer is described. Original time detectors with 100x100x2 mm 3 and 200x2 mm 2 scintillators located on the 1- or 2 m path length are used in the spectrometer. The 200x200x200 mm 3 scintillation unit is used as a E-counter. Time-of-flight spectra of the detected particles on the 2 m path length obtained in spectrometer test in the beam of charged particles escaping from the carbon target at the angle of 130 deg under 1.2 GeV bremsstrahlung beam of the ''Pakhra'' PIAS synchrotron are presented. Proton and deuteron energy spectra as well as mass spectrum of all the particles detected by the spectrometer are given. Mass resolution obtained on the 2 m path length for π-mesons is +-25%, for protons is +-5%, for deuterons is +-3%

  5. Scanning electron microscopy-energy dispersive X-ray spectrometer ...

    African Journals Online (AJOL)

    The distribution of arsenic (As) and cadmium (Cd) in himematsutake was analyzed using scanning electron microscopy-energy dispersive X-ray spectrometer (SEM-EDX). The atomic percentage of the metals was confirmed by inductively coupled plasma-mass spectrometer (ICP-MS). Results show that the accumulation of ...

  6. A spectrometer for submicron particles

    International Nuclear Information System (INIS)

    Pourprix, M.

    1995-01-01

    The electrostatic spectrometer for aerosol particles, is composed of two coaxial parallel conductive disks between which an electric field is established; an annular slot in the first disk allows for the atmosphere air intake. Suction and injection systems, and a third intermediate conductive disk are used to carry out a dynamic confinement that allows for the separation of particles having various electronic mobility and the determination of the suspended particle size distribution. Application to aerosol size spectrum determination and air quality monitoring

  7. Associated Particle Tagging (APT) in Magnetic Spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Jordan, David V.; Baciak, James E.; Stave, Sean C.; Chichester, David; Dale, Daniel; Kim, Yujong; Harmon, Frank

    2012-10-16

    Summary In Brief The Associated Particle Tagging (APT) project, a collaboration of Pacific Northwest National Laboratory (PNNL), Idaho National Laboratory (INL) and the Idaho State University (ISU)/Idaho Accelerator Center (IAC), has completed an exploratory study to assess the role of magnetic spectrometers as the linchpin technology in next-generation tagged-neutron and tagged-photon active interrogation (AI). The computational study considered two principle concepts: (1) the application of a solenoidal alpha-particle spectrometer to a next-generation, large-emittance neutron generator for use in the associated particle imaging technique, and (2) the application of tagged photon beams to the detection of fissile material via active interrogation. In both cases, a magnetic spectrometer momentum-analyzes charged particles (in the neutron case, alpha particles accompanying neutron generation in the D-T reaction; in the tagged photon case, post-bremsstrahlung electrons) to define kinematic properties of the relevant neutral interrogation probe particle (i.e. neutron or photon). The main conclusions of the study can be briefly summarized as follows: Neutron generator: • For the solenoidal spectrometer concept, magnetic field strengths of order 1 Tesla or greater are required to keep the transverse size of the spectrometer smaller than 1 meter. The notional magnetic spectrometer design evaluated in this feasibility study uses a 5-T magnetic field and a borehole radius of 18 cm. • The design shows a potential for 4.5 Sr tagged neutron solid angle, a factor of 4.5 larger than achievable with current API neutron-generator designs. • The potential angular resolution for such a tagged neutron beam can be less than 0.5o for modest Si-detector position resolution (3 mm). Further improvement in angular resolution can be made by using Si-detectors with better position resolution. • The report documents several features of a notional generator design incorporating the

  8. Charged-particle magnetic-quadrupole spectrometer for neutron induced reactions

    International Nuclear Information System (INIS)

    Haight, R.C.; Grimes, S.M.; Tuckey, B.J.; Anderson, J.D.

    1975-01-01

    A spectrometer has been developed for measuring the charged particle production cross sections and spectra in neutron-induced reactions. The spectrometer consists of a magnetic quadrupole doublet which focuses the charged particles onto a silicon surface barrier detector telescope which is 2 meters or more from the irradiated sample. Collimators, shielding, and the large source-to-detector distance reduce the background enough to use the spectrometer with a 14-MeV neutron source producing 4 . 10 12 n/s. The spectrometer has been used in investigations of proton, deuteron, and alpha particle production by 14-MeV neutrons incident on various materials. Protons with energies as low as 1.1 MeV have been measured. The good resolution of the detectors has also made possible an improved measurement of the neutron- neutron scattering length from the 0 0 proton spectrum from deuteron breakup by 14-MeV neutrons

  9. Performance of PC-based charged particle multi-channel spectrometer utilising particle identification

    International Nuclear Information System (INIS)

    Palla, G.; Sziklai, J.; Trajber, Cs.

    1993-12-01

    A collaterally expandable charged particle spectrometer based on PC control and particle identification is described. A typical system configuration consisting of two channels are used to test the system performance. (author) 7 refs.; 5 figs

  10. Miniaturized NIR scanning grating spectrometer for use in mobile phones

    Science.gov (United States)

    Knobbe, Jens; Pügner, Tino; Grüger, Heinrich

    2016-05-01

    An extremely miniaturized scanning grating spectrometer at the size of a sugar cube has been developed at Fraunhofer IPMS. To meet the requirements for the integration into a mobile phone a new system approach has been pursued. The key component within the system is a silicon-based deflectable diffraction grating with an integrated driving mechanism. A first sample of the new spectrometer was built and characterized. It was found to have a spectral range from 950 nm to 1900 nm at a resolution of 10 nm. The results show that the performance of the new MEMS spectrometer is in good agreement with the requirements for mobile phone integration.

  11. Quantitative determination of carbonaceous particle mixing state in Paris using single particle mass spectrometer and aerosol mass spectrometer measurements

    Science.gov (United States)

    Healy, R. M.; Sciare, J.; Poulain, L.; Crippa, M.; Wiedensohler, A.; Prévôt, A. S. H.; Baltensperger, U.; Sarda-Estève, R.; McGuire, M. L.; Jeong, C.-H.; McGillicuddy, E.; O'Connor, I. P.; Sodeau, J. R.; Evans, G. J.; Wenger, J. C.

    2013-04-01

    Single particle mixing state information can be a powerful tool for assessing the relative impact of local and regional sources of ambient particulate matter in urban environments. However, quantitative mixing state data are challenging to obtain using single particle mass spectrometers. In this study, the quantitative chemical composition of carbonaceous single particles has been estimated using an aerosol time-of-flight mass spectrometer (ATOFMS) as part of the MEGAPOLI 2010 winter campaign in Paris, France. Relative peak areas of marker ions for elemental carbon (EC), organic aerosol (OA), ammonium, nitrate, sulphate and potassium were compared with concurrent measurements from an Aerodyne high resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS), a thermal/optical OCEC analyser and a particle into liquid sampler coupled with ion chromatography (PILS-IC). ATOFMS-derived mass concentrations reproduced the variability of these species well (R2 = 0.67-0.78), and ten discrete mixing states for carbonaceous particles were identified and quantified. Potassium content was used to identify particles associated with biomass combustion. The chemical mixing state of HR-ToF-AMS organic aerosol factors, resolved using positive matrix factorization, was also investigated through comparison with the ATOFMS dataset. The results indicate that hydrocarbon-like OA (HOA) detected in Paris is associated with two EC-rich mixing states which differ in their relative sulphate content, while fresh biomass burning OA (BBOA) is associated with two mixing states which differ significantly in their OA/EC ratios. Aged biomass burning OA (OOA2-BBOA) was found to be significantly internally mixed with nitrate, while secondary, oxidized OA (OOA) was associated with five particle mixing states, each exhibiting different relative secondary inorganic ion content. Externally mixed secondary organic aerosol was not observed. These findings demonstrate the heterogeneity of primary and

  12. Medium energy charged particle spectrometer

    International Nuclear Information System (INIS)

    Keppler, E.; Wilken, B.; Richer, K.; Umlauft, G.; Fischer, K.; Winterhoff, H.P.

    1976-10-01

    The charged particle spectrometer E8 on HELIOS A and B will be described in some detail. It covers proton energies from 80 keV to 6 MeV, electrons from 20 keV to 2 MeV, and positrons from 150 to 550 keV. Its flight performance will be discussed. From examples of measurements the capability of the instrument will be demonstrated. (orig.) [de

  13. New spectrometer for charged particles

    International Nuclear Information System (INIS)

    Wajsfelner, Rene

    1970-02-01

    This thesis is devoted to the study and development of an electrostatic spectrometer which is not only more accurate for the determination of size distributions of electrically charged radio-active atmospheric aerosols, but which can also be used for measuring the grain-size distribution of any cloud of particles which will previously have been charged according to a known, reproducible law. An experimental study has been made of the development of this precipitator and also of its calibration. The electrical charge on spherical polystyrene latex particles suspended in air by atomization has been studied; a theoretical explanation of these results is put forward. (author) [fr

  14. Quantitative determination of carbonaceous particle mixing state in Paris using single-particle mass spectrometer and aerosol mass spectrometer measurements

    Directory of Open Access Journals (Sweden)

    R. M. Healy

    2013-09-01

    Full Text Available Single-particle mixing state information can be a powerful tool for assessing the relative impact of local and regional sources of ambient particulate matter in urban environments. However, quantitative mixing state data are challenging to obtain using single-particle mass spectrometers. In this study, the quantitative chemical composition of carbonaceous single particles has been determined using an aerosol time-of-flight mass spectrometer (ATOFMS as part of the MEGAPOLI 2010 winter campaign in Paris, France. Relative peak areas of marker ions for elemental carbon (EC, organic aerosol (OA, ammonium, nitrate, sulfate and potassium were compared with concurrent measurements from an Aerodyne high-resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS, a thermal–optical OCEC analyser and a particle into liquid sampler coupled with ion chromatography (PILS-IC. ATOFMS-derived estimated mass concentrations reproduced the variability of these species well (R2 = 0.67–0.78, and 10 discrete mixing states for carbonaceous particles were identified and quantified. The chemical mixing state of HR-ToF-AMS organic aerosol factors, resolved using positive matrix factorisation, was also investigated through comparison with the ATOFMS dataset. The results indicate that hydrocarbon-like OA (HOA detected in Paris is associated with two EC-rich mixing states which differ in their relative sulfate content, while fresh biomass burning OA (BBOA is associated with two mixing states which differ significantly in their OA / EC ratios. Aged biomass burning OA (OOA2-BBOA was found to be significantly internally mixed with nitrate, while secondary, oxidised OA (OOA was associated with five particle mixing states, each exhibiting different relative secondary inorganic ion content. Externally mixed secondary organic aerosol was not observed. These findings demonstrate the range of primary and secondary organic aerosol mixing states in Paris. Examination of the

  15. Quantitative determination of carbonaceous particle mixing state in Paris using single-particle mass spectrometer and aerosol mass spectrometer measurements

    Science.gov (United States)

    Healy, R. M.; Sciare, J.; Poulain, L.; Crippa, M.; Wiedensohler, A.; Prévôt, A. S. H.; Baltensperger, U.; Sarda-Estève, R.; McGuire, M. L.; Jeong, C.-H.; McGillicuddy, E.; O'Connor, I. P.; Sodeau, J. R.; Evans, G. J.; Wenger, J. C.

    2013-09-01

    Single-particle mixing state information can be a powerful tool for assessing the relative impact of local and regional sources of ambient particulate matter in urban environments. However, quantitative mixing state data are challenging to obtain using single-particle mass spectrometers. In this study, the quantitative chemical composition of carbonaceous single particles has been determined using an aerosol time-of-flight mass spectrometer (ATOFMS) as part of the MEGAPOLI 2010 winter campaign in Paris, France. Relative peak areas of marker ions for elemental carbon (EC), organic aerosol (OA), ammonium, nitrate, sulfate and potassium were compared with concurrent measurements from an Aerodyne high-resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS), a thermal-optical OCEC analyser and a particle into liquid sampler coupled with ion chromatography (PILS-IC). ATOFMS-derived estimated mass concentrations reproduced the variability of these species well (R2 = 0.67-0.78), and 10 discrete mixing states for carbonaceous particles were identified and quantified. The chemical mixing state of HR-ToF-AMS organic aerosol factors, resolved using positive matrix factorisation, was also investigated through comparison with the ATOFMS dataset. The results indicate that hydrocarbon-like OA (HOA) detected in Paris is associated with two EC-rich mixing states which differ in their relative sulfate content, while fresh biomass burning OA (BBOA) is associated with two mixing states which differ significantly in their OA / EC ratios. Aged biomass burning OA (OOA2-BBOA) was found to be significantly internally mixed with nitrate, while secondary, oxidised OA (OOA) was associated with five particle mixing states, each exhibiting different relative secondary inorganic ion content. Externally mixed secondary organic aerosol was not observed. These findings demonstrate the range of primary and secondary organic aerosol mixing states in Paris. Examination of the temporal

  16. Mass spectrometer provided with an optical system for separating neutron particles against charged particles

    Energy Technology Data Exchange (ETDEWEB)

    Reeher, J R; Story, M S; Smith, R D

    1977-03-03

    This invention concerns a mass spectrometer with an ion focusing optical system that efficiently separates the charged and neutral particles. It concerns an apparatus that can be used in ionisation areas operating at relatively high pressure (> 10/sup -2/ Torr). The invention relates more particularly to a mass spectrometer with an inlet device for the samples to be identified, a sample ionisation system for forming charged and neutral particles, a mass analyser and an optical system for focusing the ions formed in the mass analyser. The optics include several conducting components of which at least one has sides formed of grids, in the direction of the axis, towards the analyser the optics forming a potential well along the axis. The selected charged particles are focused in the analyser and the remaining particles can escape by the openings in the conducting grids.

  17. Mobility particle size spectrometers: harmonization of technical standards and data structure to facilitate high quality long-term observations of atmospheric particle number size distributions

    Directory of Open Access Journals (Sweden)

    A. Wiedensohler

    2012-03-01

    Full Text Available Mobility particle size spectrometers often referred to as DMPS (Differential Mobility Particle Sizers or SMPS (Scanning Mobility Particle Sizers have found a wide range of applications in atmospheric aerosol research. However, comparability of measurements conducted world-wide is hampered by lack of generally accepted technical standards and guidelines with respect to the instrumental set-up, measurement mode, data evaluation as well as quality control. Technical standards were developed for a minimum requirement of mobility size spectrometry to perform long-term atmospheric aerosol measurements. Technical recommendations include continuous monitoring of flow rates, temperature, pressure, and relative humidity for the sheath and sample air in the differential mobility analyzer.

    We compared commercial and custom-made inversion routines to calculate the particle number size distributions from the measured electrical mobility distribution. All inversion routines are comparable within few per cent uncertainty for a given set of raw data.

    Furthermore, this work summarizes the results from several instrument intercomparison workshops conducted within the European infrastructure project EUSAAR (European Supersites for Atmospheric Aerosol Research and ACTRIS (Aerosols, Clouds, and Trace gases Research InfraStructure Network to determine present uncertainties especially of custom-built mobility particle size spectrometers. Under controlled laboratory conditions, the particle number size distributions from 20 to 200 nm determined by mobility particle size spectrometers of different design are within an uncertainty range of around ±10% after correcting internal particle losses, while below and above this size range the discrepancies increased. For particles larger than 200 nm, the uncertainty range increased to 30%, which could not be explained. The network reference mobility spectrometers with identical design agreed within ±4% in the

  18. [Emulsion spectrometer experiment for B and C particles

    International Nuclear Information System (INIS)

    1981-01-01

    An experiment is proposed which employs a hybrid emulsion spectrometer to measure lifetimes and decay properties of beauty particles and charmed particles produced by interactions of high energy hadrons. The key to the experiment is a position-sensitive silicon detector. The physics motivation of the experiment and the design of the experimental apparatus and treatment of data are discussed

  19. ultra-Stable Spectrometer for Sky-Scanning, Sun-Tracking Atmospheric Research (5STAR)

    Science.gov (United States)

    Dunagan, S. E.; Johnson, R. R.; Redemann, J.; Holben, B. N.; Schmid, B.; Flynn, C. J.; Fahey, L.; LeBlanc, S. E.; Liss, J.; Kacenelenbogen, M. S.; Segal-Rosenhaimer, M.; Shinozuka, Y.; Dahlgren, R. P.; Pistone, K.; Karol, Y.

    2017-12-01

    The Spectrometer for Sky-Scanning, Sun-Tracking Atmospheric Research (4STAR) combines airborne sun tracking and sky scanning with diffraction spectroscopy to improve knowledge of atmospheric constituents and their links to air pollution and climate. Direct beam hyperspectral measurement of optical depth improves retrievals of gas constituents and determination of aerosol properties. Sky scanning enhances retrievals of aerosol type and size distribution. Hyperspectral cloud-transmitted radiance measurements enable the retrieval of cloud properties from below clouds. These measurements tighten the closure between satellite and ground-based measurements. 4STAR incorporates a modular sun-tracking/ sky-scanning optical head with optical fiber signal transmission to rack mounted spectrometers, permitting miniaturization of the external optical tracking head, and future detector evolution. 4STAR has supported a broad range of flight experiments since it was first flown in 2010. This experience provides the basis for a series of improvements directed toward reducing measurement uncertainty and calibration complexity, and expanding future measurement capabilities, to be incorporated into a new 5STAR instrument. A 9-channel photodiode radiometer with AERONET-matched bandpass filters will be incorporated to improve calibration stability. A wide dynamic range tracking camera will provide a high precision solar position tracking signal as well as an image of sky conditions around the solar axis. An ultrasonic window cleaning system design will be tested. A UV spectrometer tailored for formaldehyde and SO2 gas retrievals will be added to the spectrometer enclosure. Finally, expansion capability for a 4 channel polarized radiometer to measure the Stokes polarization vector of sky light will be incorporated. This paper presents initial progress on this next-generation 5STAR instrument. Keywords: atmosphere; climate; pollution; radiometry; technology; hyperspectral; fiber optic

  20. Hygroscopic analysis of individual Beijing haze aerosol particles by environmental scanning electron microscopy

    Science.gov (United States)

    Bai, Zhangpeng; Ji, Yuan; Pi, Yiqun; Yang, Kaixiang; Wang, Li; Zhang, Yinqi; Zhai, Yadi; Yan, Zhengguang; Han, Xiaodong

    2018-01-01

    Investigating the hygroscopic behavior of haze aerosol particles is essential for understanding their physicochemical properties and their impacts on regional weather and visibility. An environmental scanning electron microscope equipped with a home-made transmission-scattering electron imaging setup and an energy dispersive spectrometer was used for in-situ observations of pure water-soluble (WS) salts and Beijing haze particles. This imaging setup showed obvious advantages for improving the resolution and acquiring internal information of mixed particles in hydrated environments. We measured the deliquescence relative humidity of pure NaCl, NH4NO3, and (NH4)2SO4 by deliquescence-crystallization processes with an accuracy of up to 0.3% RH. The mixed haze particles showed hygroscopic activation like water uptake and morphological changes when they included WS components such as nitrates, sulfates, halides, ammoniums, and alkali metal salts. In addition, the hygroscopic behavior provides complementary information for analyzing possible phases in mixed haze particles.

  1. Satellite-borne time-of-flight particle spectrometer and its response to protons

    International Nuclear Information System (INIS)

    Shino, T.

    1994-01-01

    One of the purposes of the high energy particle (HEP) experiment of the GEOTAIL satellite launched in 1992 is the elucidation of plasma dynamics in the tail region of planetary magnetosphere. For that purpose, a low energy particle detector (LD) was on board, which mainly observed relatively low energy particles up to a few MeV. The LD is the particle spectrometer based on time of flight technique. In order to confirm further its sensitivity to high energy protons, the beam experiment was carried out at Waseda University using the engineering model of the LD spectrometer that is exactly the same as the launched one. The LD spectrometer is shown, and its functions are explained. The LD was designed to identify electrons of 30 - 400 keV, protons of 30 - 1500 keV, helium ions of 80 - 4000 keV, and heavy ions (mainly C, N and O) of 160 - 1500 keV. The relation of measured time of flight signals with energy signals is shown. There are several factors that determine the detection efficiency of the spectrometer, which are discussed. The experiment and the results are reported. (K.I.)

  2. A design of a high speed dual spectrometer by single line scan camera

    Science.gov (United States)

    Palawong, Kunakorn; Meemon, Panomsak

    2018-03-01

    A spectrometer that can capture two orthogonal polarization components of s light beam is demanded for polarization sensitive imaging system. Here, we describe the design and implementation of a high speed spectrometer for simultaneous capturing of two orthogonal polarization components, i.e. vertical and horizontal components, of light beam. The design consists of a polarization beam splitter, two polarization-maintain optical fibers, two collimators, a single line-scan camera, a focusing lens, and a reflection blaze grating. The alignment of two beam paths was designed to be symmetrically incident on the blaze side and reverse blaze side of reflection grating, respectively. The two diffracted beams were passed through the same focusing lens and focused on the single line-scan sensors of a CMOS camera. The two spectra of orthogonal polarization were imaged on 1000 pixels per spectrum. With the proposed setup, the amplitude and shape of the two detected spectra can be controlled by rotating the collimators. The technique for optical alignment of spectrometer will be presented and discussed. The two orthogonal polarization spectra can be simultaneously captured at a speed of 70,000 spectra per second. The high speed dual spectrometer can simultaneously detected two orthogonal polarizations, which is an important component for the development of polarization-sensitive optical coherence tomography. The performance of the spectrometer have been measured and analyzed.

  3. A simplified digital lock-in amplifier for the scanning grating spectrometer.

    Science.gov (United States)

    Wang, Jingru; Wang, Zhihong; Ji, Xufei; Liu, Jie; Liu, Guangda

    2017-02-01

    For the common measurement and control system of a scanning grating spectrometer, the use of an analog lock-in amplifier requires complex circuitry and sophisticated debugging, whereas the use of a digital lock-in amplifier places a high demand on the calculation capability and storage space. In this paper, a simplified digital lock-in amplifier based on averaging the absolute values within a complete period is presented and applied to a scanning grating spectrometer. The simplified digital lock-in amplifier was implemented on a low-cost microcontroller without multipliers, and got rid of the reference signal and specific configuration of the sampling frequency. Two positive zero-crossing detections were used to lock the phase of the measured signal. However, measurement method errors were introduced by the following factors: frequency fluctuation, sampling interval, and integer restriction of the sampling number. The theoretical calculation and experimental results of the signal-to-noise ratio of the proposed measurement method were 2055 and 2403, respectively.

  4. High accuracy wavelength calibration for a scanning visible spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Scotti, Filippo; Bell, Ronald E. [Princeton Plasma Physics Laboratory, Princeton, New Jersey 08543 (United States)

    2010-10-15

    Spectroscopic applications for plasma velocity measurements often require wavelength accuracies {<=}0.2 A. An automated calibration, which is stable over time and environmental conditions without the need to recalibrate after each grating movement, was developed for a scanning spectrometer to achieve high wavelength accuracy over the visible spectrum. This method fits all relevant spectrometer parameters using multiple calibration spectra. With a stepping-motor controlled sine drive, an accuracy of {approx}0.25 A has been demonstrated. With the addition of a high resolution (0.075 arc sec) optical encoder on the grating stage, greater precision ({approx}0.005 A) is possible, allowing absolute velocity measurements within {approx}0.3 km/s. This level of precision requires monitoring of atmospheric temperature and pressure and of grating bulk temperature to correct for changes in the refractive index of air and the groove density, respectively.

  5. The case study on elemental analyses of Asian dust particles by using an analytical scanning electron microscope

    International Nuclear Information System (INIS)

    Takeuchi, Jo; Masaki, Kazushige; Emoto, Yuji

    2009-01-01

    The individual particle analyses of suspended particulate matter (SPM: particles less than 10 μm in size) collected on tape filters during April 17-18, 2006, in Kawasaki, Japan, were carried out. The chemical elements present in aerosol particles were investigated by using a scanning electron microscope with an energy-dispersive X-ray spectrometer. The fraction of chemical elements detected in the particles collected on April 18, 2006, except for S, was in good agreement with that in Asian dust particles from the Loess Plateau, China. S was not detected in Asian dust particles but was detected in the particles collected on April 18, 2006. Therefore, it was concluded that the particles collected in April 18, 2006, in Kawasaki were Asian dust particles transported from the Asian continent, and the absorption of SO 2 or the coagulation of sulfate occurred during the transportation of Asian dust particles. (author)

  6. Frequency-scanning MALDI linear ion trap mass spectrometer for large biomolecular ion detection.

    Science.gov (United States)

    Lu, I-Chung; Lin, Jung Lee; Lai, Szu-Hsueh; Chen, Chung-Hsuan

    2011-11-01

    This study presents the first report on the development of a matrix-assisted laser desorption ionization (MALDI) linear ion trap mass spectrometer for large biomolecular ion detection by frequency scan. We designed, installed, and tested this radio frequency (RF) scan linear ion trap mass spectrometer and its associated electronics to dramatically extend the mass region to be detected. The RF circuit can be adjusted from 300 to 10 kHz with a set of operation amplifiers. To trap the ions produced by MALDI, a high pressure of helium buffer gas was employed to quench extra kinetic energy of the heavy ions produced by MALDI. The successful detection of the singly charged secretory immunoglobulin A ions indicates that the detectable mass-to-charge ratio (m/z) of this system can reach ~385 000 or beyond.

  7. Particle transport simulation for spaceborne, NaI gamma-ray spectrometers

    International Nuclear Information System (INIS)

    Dyer, C.S.; Truscott, P.R.; Sims, A.J.; Comber, C.; Hammond, N.D.A.

    1988-11-01

    Radioactivity induced in detectors by protons and secondary neutrons limits the sensitivity of spaceborne gamma-ray spectrometers. Three dimensional Monte Carlo transport codes have been employed to simulate particle transport of cosmic rays and inner-belt protons in various representations of the Gamma Ray Observatory Spacecraft and the Oriented Scintillation Spectrometer Experiment. Results are used to accurately quantify the contributions to the radioactive background, assess shielding options and examine the effect of detector and space-craft orientation in anisotropic trapped proton fluxes. (author)

  8. An off Axis Cavity Enhanced Absorption Spectrometer and a Rapid Scan Spectrometer with a Room-Temperature External Cavity Quantum Cascade Laser

    Science.gov (United States)

    Liu, Xunchen; Kang, Cheolhwa; Xu, Yunjie

    2009-06-01

    Quantum cascade laser (QCL) is a new type of mid-infrared tunable diode lasers with superior output power and mode quality. Recent developments, such as room temperature operation, wide frequency tunability, and narrow line width, make QCLs an ideal light source for high resolution spectroscopy. Two slit jet infrared spectrometers, namely an off-axis cavity enhanced absorption (CEA) spectrometer and a rapid scan spectrometer with an astigmatic multi-pass cell assembly, have been coupled with a newly purchased room temperature tunable mod-hop-free QCL with a frequency coverage from 1592 cm^{-1} to 1698 cm^{-1} and a scan rate of 0.1 cm^{-1}/ms. Our aim is to utilize these two sensitive spectrometers, that are equipped with a molecular jet expansion, to investigate the chiral molecules-(water)_n clusters. To demonstrate the resolution and sensitivity achieved, the rovibrational transitions of the static N_2O gas and the bending rovibrational transitions of the Ar-water complex, a test system, at 1634 cm^{-1} have been measured. D. Hofstetter and J. Faist in High performance quantum cascade lasers and their applications, Vol.89 Springer-Verlag Berlin & Heidelberg, 2003, pp. 61-98. Y. Xu, X. Liu, Z. Su, R. M. Kulkarni, W. S. Tam, C. Kang, I. Leonov and L. D'Agostino, Proc. Spie, 2009, 722208 (1-11). M. J. Weida and D. J. Nesbitt, J. Chem. Phys. 1997, 106, 3078-3089.

  9. A focusing spectrometer for one and two particles

    CERN Multimedia

    The focusing spectrometer is a device based on existing magnets and proven technology that solves the problem of extracting physics in the high-particle-multiplicity environment of high energy heavy-ion collisions (from S on S up to Pb on Pb) as well as in proton-proton collisions. It sweeps a small central acceptance over interesting regions of phase space, thereby dealing with only a few particles at a time. Because of its resulting excellent momentum resolution, ability to identify particles $(\\pi^{\\pm}, K^{\\pm}, p, \\bar{p}, d$ and $\\bar{d})$, and appropriate acceptance for particle pairs, it is well suited to making detailed studies of two of the more promising observables that have come to light as a result of the first two years of SPS and AGS heavy-ion running: two and three particle interferometry and single identified particle inclusive spectra.\\\\\\\\ Two pion interferometry is a technique which allows one to extract, with an appropriate theory, the space-time evolution of the pion source distribution ...

  10. Multiparticle magnetic spectrometer with dE/dx and TRD particle identification

    International Nuclear Information System (INIS)

    Lindenbaum, S.J.; Longacre, R.S.

    1981-01-01

    Recent advances in detector development by BNL, CCNY and other groups have made possible new designs of fast high resolution large effective solid angle magnetic multiparticle spectrometers with excellent particle tracking, momentum measurement, and identification capability. These new spectrometers are relatively compact and relatively low cost electronics have been developed for them. Thus the cost is relatively low. These techniques are applied here primarily for design of spectrometers for low p/sub t/ and other physics (at moderate and even high p/sub t/) in the ISABELLE small angle hall. However, one should keep in mind that these techniques can be utilized in many other applications

  11. LabVIEW control software for scanning micro-beam X-ray fluorescence spectrometer.

    Science.gov (United States)

    Wrobel, Pawel; Czyzycki, Mateusz; Furman, Leszek; Kolasinski, Krzysztof; Lankosz, Marek; Mrenca, Alina; Samek, Lucyna; Wegrzynek, Dariusz

    2012-05-15

    Confocal micro-beam X-ray fluorescence microscope was constructed. The system was assembled from commercially available components - a low power X-ray tube source, polycapillary X-ray optics and silicon drift detector - controlled by an in-house developed LabVIEW software. A video camera coupled to optical microscope was utilized to display the area excited by X-ray beam. The camera image calibration and scan area definition software were also based entirely on LabVIEW code. Presently, the main area of application of the newly constructed spectrometer is 2-dimensional mapping of element distribution in environmental, biological and geological samples with micrometer spatial resolution. The hardware and the developed software can already handle volumetric 3-D confocal scans. In this work, a front panel graphical user interface as well as communication protocols between hardware components were described. Two applications of the spectrometer, to homogeneity testing of titanium layers and to imaging of various types of grains in air particulate matter collected on membrane filters, were presented. Copyright © 2012 Elsevier B.V. All rights reserved.

  12. Studies of porphyrin-containing specimens using an optical spectrometer connected to a confocal scanning laser microscope.

    Science.gov (United States)

    Trepte, O; Rokahr, I; Andersson-Engels, S; Carlsson, K

    1994-12-01

    A spectrometer has been developed for use with a confocal scanning laser microscope. With this unit, spectral information from a single point or a user-defined region within the microscope specimen can be recorded. A glass prism is used to disperse the spectral components of the recorded light over a linear CCD photodiode array with 256 elements. A regulated cooling unit keeps the detector at 277 K, thereby allowing integration times of up to 60 s. The spectral resolving power, lambda/delta lambda, ranges from 350 at lambda = 400 nm to 100 at lambda = 700 nm. Since the entrance aperture of the spectrometer has the same size as the detector pinhole used during normal confocal scanning, the three-dimensional spatial resolution is equivalent to that of normal confocal scanning. Light from the specimen is deflected to the spectrometer by a solenoid controlled mirror, allowing fast and easy switching between normal confocal scanning and spectrometer readings. With this equipment, studies of rodent liver specimens containing porphyrins have been made. The subcellular localization is of interest for the mechanisms of photodynamic therapy (PDT) of malignant tumours. Spectroscopic detection is necessary to distinguish the porphyrin signal from other fluorescent components in the specimen. Two different substances were administered to the tissue, Photofrin, a haematoporphyrin derivative (HPD) and delta-amino levulinic acid (ALA), a precursor to protoporphyrin IX and haem in the haem cycle. Both are substances under clinical trials for PDT of malignant tumours. Following administration of these compounds to the tissue, the potent photosensitizer and fluorescent compound Photofrin, or protoporphyrin IX, respectively, is accumulated.(ABSTRACT TRUNCATED AT 250 WORDS)

  13. Alpha particles spectrometer with photodiode PIN

    International Nuclear Information System (INIS)

    Chacon R, A.; Hernandez V, R.; Hernandez D, V. M.; Vega C, H. R.; Ramirez G, J.

    2009-10-01

    The radiation propagates in form of electromagnetic waves or corpuscular radiation; if the radiation energy causes ionization in environment that crosses it is considered ionizing radiation. To detect radiation several detectors types are used, if the radiation are alpha particles are used detectors proportional type or trace elements. In this work the design results, construction and tests of an alpha particles spectrometer are presented, which was designed starting from a photodiode PIN type. The system design was simulated with a code for electronic circuits. With results of simulation phase was constructed the electronic phase that is coupled to a multichannel analyzer. The resulting electronic is evaluated analyzing the electronic circuit performance before an alphas triple source and alpha radiation that produce two smoke detectors of domestic use. On the tests phase we find that the system allows obtain, in a multichannel, the pulses height spectrum, with which we calibrate the system. (Author)

  14. High Resolution Spectrometer (HRS) particle-identification system

    International Nuclear Information System (INIS)

    Pratt, J.C.; Spencer, J.E.; Whitten, C.A.

    1977-08-01

    The functions of the particle-identification system (PIDS) designed for the High Resolution Spectrometer facility (HRS) at LAMPF are described, together with the mechanical layout, counter hardware, and associated electronics. The system was designed for easy use and to be applicable to currently proposed experiments at HRS. The several strobe signals that can be generated correspond to different event types or characteristics, and logic configuration and timing can be remotely controlled by computer. Concepts of discrete pattern recognition and multidimensional, analog pulse discrimination are used to distinguish between different event types

  15. Large solid-angle spectrometers for studies of double-differential charged-particle and neutron emission cross sections

    International Nuclear Information System (INIS)

    Baba, M.; Matsuyama, S.; Sanami, T.; Soda, D.; Matsuyama, I.; Ohkubo, T.; Iwasaki, S.; Hirakawa, N.

    1995-01-01

    The large solid-angle spectrometer developed for studies of double-differential cross sections of (n, charged particle) and (n, xn') reactions using a gas-filled gridded-ionization chamber and an 80-cm long liquid scintillator is described. The charged particle spectrometer is a twin gas-filled gridded-ionization chamber with solid angle close to 4 π designed to achieve high stopping power and background suppression. The neutron spectrometer is a long NE213 liquid scintillation detector having position sensitivity. It is used as a large single spectrometer or a position sensitive detector covering wide scattering angle. The facility design, performance and examples of application are discussed. The conclusion is made that the facility provides a useful mean for studies in particular for reactions with small cross sections and/or for neutron sources with low intensity. 15 refs., 15 figs

  16. Scanning mass spectrometer setup for spatially resolved reactivity studies on model catalysts

    Energy Technology Data Exchange (ETDEWEB)

    Roos, Matthias; Schirling, Christian; Kielbassa, Stefan; Bansmann, Joachim; Behm, Juergen [Institut fuer Oberflaechenchemie und Katalyse, Universitaet Ulm, D-89069 Ulm (Germany)

    2007-07-01

    A scanning mass spectrometer with micrometer-scale resolution was developed for investigations on the catalytic activity of microstructured planar model catalysts. Products of local surface reactions can be detected via a fine capillary orifice in a differentially pumped quadrupole mass spectrometer. The position of the sample with respect to the capillary is controlled by three piezo-driven translators. The surface reactivity of a resistive heated sample can be depicted in a spatially resolved topogram, taking into account the influence of the distance between sample and capillary on the magnitude of the QMS signal and the lateral resolution. Photolithographic structured reactive patterns on top of an inactive substrate enable investigations of mesoscopic transport effects such as coupling between catalytically active areas and of (reverse) spillover phenomena on one sample by varying the size and the distances of the active areas.

  17. Intercomparison of 15 Aerodynamic Particle Size Spectrometers (APS 3321): Uncertainties in Particle Sizing and Number Size Distribution.

    Czech Academy of Sciences Publication Activity Database

    Pfeifer, S.; Müller, T.; Weinhold, K.; Zíková, Naděžda; dos Santos, S.M.; Marinoni, A.; Bischof, O.F.; Kykal, C.; Ries, L.; Meinhardt, F.; Aalto, P.; Mihalopoulos, N.; Wiedensohler, A.

    2016-01-01

    Roč. 9, č. 4 (2016), s. 1545-1551 ISSN 1867-1381 EU Projects: European Commission(XE) 262254 - ACTRIS Institutional support: RVO:67985858 Keywords : counting efficiency * aerodynamic particle size spectrometers * laboratory study Subject RIV: CF - Physical ; Theoretical Chemistry Impact factor: 3.089, year: 2016

  18. Automated rapid particle investigation using scanning electron microscopy

    Science.gov (United States)

    Wilkins, Jerod Laurence

    The chemical composition of fly ash particles has been known to vary significantly depending on a number of factors. Current bulk methods of investigation including X-Ray Fluorescence and X-Ray Diffraction are thought to be inadequate in determining the performance of fly ash in concrete. It is the goal of this research to develop a method of Automated Rapid Particle Investigation that will not look at fly ash as a bulk material but as individual particles. By examining each particle individually scientists and engineers will have the ability to study the variation in chemical composition by comparing the chemistry present in each particle. The method of investigation developed by this research provides a practical technique that will allow the automated chemical analysis of hundreds, or even thousands, of fly ash particles in a matter of minutes upon completion of sample preparation and automated scanning electron microscope (ASEM) scanning. This research does not examine the significance of the chemical compounds discovered; rather, only the investigation methodology is discussed. Further research will be done to examine the importance of the chemistry discovered with this automated rapid particle investigation technique.

  19. Cryogenic Scan Mechanism for Fourier Transform Spectrometer

    Science.gov (United States)

    Brasunas, John C.; Francis, John L.

    2011-01-01

    A compact and lightweight mechanism has been developed to accurately move a Fourier transform spectrometer (FTS) scan mirror (a cube corner) in a near-linear fashion with near constant speed at cryogenic temperatures. This innovation includes a slide mechanism to restrict motion to one dimension, an actuator to drive the motion, and a linear velocity transducer (LVT) to measure the speed. The cube corner mirror is double-passed in one arm of the FTS; double-passing is required to compensate for optical beam shear resulting from tilting of the moving cube corner. The slide, actuator, and LVT are off-the-shelf components that are capable of cryogenic vacuum operation. The actuator drives the slide for the required travel of 2.5 cm. The LVT measures translation speed. A proportional feedback loop compares the LVT voltage with the set voltage (speed) to derive an error signal to drive the actuator and achieve near constant speed. When the end of the scan is reached, a personal computer reverses the set voltage. The actuator and LVT have no moving parts in contact, and have magnetic properties consistent with cryogenic operation. The unlubricated slide restricts motion to linear travel, using crossed roller bearings consistent with 100-million- stroke operation. The mechanism tilts several arc seconds during transport of the FTS mirror, which would compromise optical fringe efficiency when using a flat mirror. Consequently, a cube corner mirror is used, which converts a tilt into a shear. The sheared beam strikes (at normal incidence) a flat mirror at the end of the FTS arm with the moving mechanism, thereby returning upon itself and compensating for the shear

  20. Intercomparison of air ion spectrometers: an evaluation of results in varying conditions

    Directory of Open Access Journals (Sweden)

    S. Gagné

    2011-05-01

    Full Text Available We evaluated 11 air ion spectrometers from Airel Ltd. after they had spent one year in field measurements as a part of the EUCAARI project: 5 Air Ion Spectrometers (AIS, 5 Neutral cluster and Air Ion Spectrometers (NAIS and one Airborne NAIS (ANAIS. This is the first time that an ANAIS is evaluated and compared so extensively. The ion spectrometers' mobility and concentration accuracy was evaluated. Their measurements of ambient air were compared between themselves and to reference instruments: a Differential Mobility Particle Sizer (DMPS, a Balanced Scanning Mobility Analyzer (BSMA, and an Ion-DMPS. We report on the simultaneous measurement of a new particle formation (NPF event by all 11 instruments and the 3 reference instruments. To our knowledge, it is the first time that the size distribution of ions and particles is measured by so many ion spectrometers during a NPF event. The new particle formation rates (~0.2 cm−3 s−1 for ions and ~2 cm−3 s−1 for particles and growth rates (~25 nm h−1 in the 3–7 nm size range were calculated for all the instruments. The NAISs and the ANAIS gave higher concentrations and formation rates than the AISs. For example, the AISs agreed with the BSMA within 11 % and 28 % for negative and positive ion concentration respectively, whereas the NAISs agreed within 23 % and 29 %. Finally, based on the results presented here, we give guidelines for data evaluation, when data from different individual ion spectrometers are compared.

  1. X-ray analysis of a single aerosol particle with combination of scanning electron microscope and synchrotron radiation X-ray microscope

    International Nuclear Information System (INIS)

    Toyoda, Masatoshi; Kaibuchi, Kazuki; Nagasono, Mitsuru; Terada, Yasuko; Tanabe, Teruo; Hayakawa, Shinjiro; Kawai, Jun

    2004-01-01

    We developed a microscope by a combination of synchrotron radiation X-ray fluorescence (SR-XRF) microscope and scanning electron microscope (SEM) with an energy dispersive X-ray spectrometer (EDX). SR-XRF is appropriate to detect trace and micro amount of elements and sensitive to heavy elements in an analyte but it cannot observe the real time image. SEM-EDX can observe the secondary electron image of a single particle in real time and is appropriate to detect lighter elements. This combination microscope can ensure the identification of the XRF spectrum to the SEM image without transferring the sample. For aerosol analysis, it is important to analyze each particle. The present method makes feasible to analyze not only the average elemental composition as the total particles but also elemental composition of each particle, which is dependent on the particle shape and size. The microscope was applied to an individual aerosol particle study. The X-ray spectra were different among the particles, but also different between SR-XRF and SEM-EDX for the same particle, due to the difference in fluorescence yields between X-ray excitation and electron excitation

  2. Design of a preamplifier for an alpha particles spectrometer

    International Nuclear Information System (INIS)

    Murillo O, R.; Hernandez D, V. M.; Chacon R, A.; Vega C, H. R.

    2010-09-01

    To detect radiation diverse detector types are used, when these are alpha particles proportional type detectors are used, semiconductor, of scintillation or traces. In this work the design results, the construction and the first tests of a spectrometer (preamplifier) are presented for alpha particles that was designed starting from a Pin type photodiode. The system was designed and simulated with a program for electronic circuits. With the results of the simulation phase was constructed the electronics that is coupled to a spectroscopic amplifier and a multichannel analyzer. The total of the system is evaluated analyzing its performance before a triple source of alphas and that they are produced by two smoke detectors of domestic use. Of the tests phase we find that the system allows to obtain in a multichannel, the pulses height spectrum, with which we calibrate the system. (Author)

  3. Spectrometer based on the silicon semiconductor detectors for a study of the two charged particles correlation

    International Nuclear Information System (INIS)

    Krumsztein, Z.W.; Siemiarczuk, T.; Szawlowski, M.

    1974-01-01

    The spectrometer based on the silicon semiconductor detectors for a study of the correlation between two charged particles is described. The results of the time resolution and particles identification measurements are presented. The tests were performed in the proton beam of the JINR synchrocyclotron. (author)

  4. 3D scanning particle tracking velocimetry

    Energy Technology Data Exchange (ETDEWEB)

    Hoyer, Klaus; Holzner, Markus; Guala, Michele; Liberzon, Alexander; Kinzelbach, Wolfgang [Swiss Federal Institut of Technology Zurich, Institut fuer Hydromechanik und Wasserwirtschaft, Zuerich (Switzerland); Luethi, Beat [Risoe National Laboratory, Roskilde (Denmark)

    2005-11-01

    In this article, we present an experimental setup and data processing schemes for 3D scanning particle tracking velocimetry (SPTV), which expands on the classical 3D particle tracking velocimetry (PTV) through changes in the illumination, image acquisition and analysis. 3D PTV is a flexible flow measurement technique based on the processing of stereoscopic images of flow tracer particles. The technique allows obtaining Lagrangian flow information directly from measured 3D trajectories of individual particles. While for a classical PTV the entire region of interest is simultaneously illuminated and recorded, in SPTV the flow field is recorded by sequential tomographic high-speed imaging of the region of interest. The advantage of the presented method is a considerable increase in maximum feasible seeding density. Results are shown for an experiment in homogenous turbulence and compared with PTV. SPTV yielded an average 3,500 tracked particles per time step, which implies a significant enhancement of the spatial resolution for Lagrangian flow measurements. (orig.)

  5. A Control and Detecting System of Micro-Near-Infrared Spectrometer Based on a MOEMS Scanning Grating Mirror

    Directory of Open Access Journals (Sweden)

    Haitao Liu

    2018-03-01

    Full Text Available Based on the scanning grating mirror we developed, this paper presents a method of the precise control of a scanning grating mirror and of high-speed spectrum data detection. In addition, the system circuit of the scanning grating mirror control and spectrum signal detecting is designed and manufactured in this paper. The mirror control system includes a drive generator module, an amplitude detection module, a feedback control module, and a variable gain amplification (VGA module; the detecting system includes a field programmable gate array (FPGA main control module, a synchronous trigger module, an analog-digital conversion (ADC module, and a universal serial bus (USB interface module. The final results of the experiment show that the control system has successfully realized the precision control of the swing of the scanning grating mirror and that the detecting system has successfully realized the high-speed acquisition and transmission of the spectral signal and the angle signals. The spectrum has been reconstructed according to the mathematical relationship between the wavelength λ and the angle β of the mirror. The resolution of the spectrometer reaches 10 nm in the wavelength range of 800–1800 nm, the signal-to-noise ratio (SNR of the spectrometer is 4562 at full scale, the spectrum data drift is 0.9% in 24 h, and the precision of the closed loop control is 0.06%.

  6. Account of magnetic field effects of polarized proton target on charged particle trajectories in experiments with magnetic spectrometers

    International Nuclear Information System (INIS)

    Telegin, Yu.N.; Ranyuk, Yu.N.; Karnaukhov, I.M.; Lukhanin, A.A.; Sporov, E.A.

    1980-01-01

    Some effects of the influence of magnetic field of a polarized proton target (PPT) on trajectories of secondary particles in experiments using magnetic spectrometers are considered. It is shown that these effects can be eliminated by the target shift relatively to the spectrometer rotation axis and variation of the spectrometer installation angle. Numerical calculations of the correction values were performed for emitted particle momenta of 100-800 MeB/s and working intensity of the H 0 magnetic field H 0 =27 kG. The influence of the PPT magnetic field on the functions of angular and energy resolution in the γp→π + n experiment is investigated. The results obtained can be used in experiments with a polarized proton target

  7. Scanning device for a spectrometer

    International Nuclear Information System (INIS)

    Ignat'ev, V.M.

    1982-01-01

    The invention belongs to scanning devices and is intended for spectrum scanning in spectral devices. The purpose of the invention is broadening of spectral scanning range. The device construction ensures the spectrum scanning range determined from revolution fractions to several revolutions of the monochromator drum head, any number of the drum head revolutions determined by integral number with addition of the drum revolution fractions with high degree of accuracy being possible

  8. A Fourier Transform Spectrometer Based on an Electrothermal MEMS Mirror with Improved Linear Scan Range

    Directory of Open Access Journals (Sweden)

    Wei Wang

    2016-09-01

    Full Text Available A Fourier transform spectrometer (FTS that incorporates a closed-loop controlled, electrothermally actuated microelectromechanical systems (MEMS micromirror is proposed and experimentally verified. The scan range and the tilting angle of the mirror plate are the two critical parameters for MEMS-based FTS. In this work, the MEMS mirror with a footprint of 4.3 mm × 3.1 mm is based on a modified lateral-shift-free (LSF bimorph actuator design with large piston and reduced tilting. Combined with a position-sensitive device (PSD for tilt angle sensing, the feedback controlled MEMS mirror generates a 430 µm stable linear piston scan with the mirror plate tilting angle less than ±0.002°. The usable piston scan range is increased to 78% of the MEMS mirror’s full scan capability, and a spectral resolution of 0.55 nm at 531.9 nm wavelength, has been achieved. It is a significant improvement compared to the prior work.

  9. Comprehensive Measurement of Atmospheric Aerosols with a Wide Range Aerosol Spectrometer

    International Nuclear Information System (INIS)

    Keck, L; Pesch, M; Grimm, H

    2011-01-01

    A wide range aerosol spectrometer (WRAS) was used for comprehensive long term measurements of aerosol size distributions. The system combines the results of an optical aerosol spectrometer with the results of a Scanning Mobility Particle Sizer (SMPS) to record essentially the full size range (5 nm - 32 μm) of atmospheric particles in 72 channels. Measurements were carried out over one year (2009) at the Global Atmospheric Watch (GAW)-Station Hohenpeissenberg, Bavaria. Total particle number concentrations obtained from the aerosol size distributions were compared to the total number concentrations measured by a Condensation Particle Counter (CPC). The comparison showed an excellent agreement of the data. The high time resolution of 5 minutes allows the combination of the measured size distributions with meteorological data and correlations to gaseous pollutants (CO, NOx and SO2). A good correlation of particle number and CO concentrations was found for long distance transported small particles, which were probably mainly soot particles. Correlations to NOx were observed for aerosols from local sources such as traffic emissions. The formation of secondary aerosols from gaseous precursors was also observed. Episodes of relatively high concentration of particles in the range of 2-3 μm were probably caused by pollen.

  10. A simple method for detection of gunshot residue particles from hands, hair, face, and clothing using scanning electron microscopy/wavelength dispersive X-ray (SEM/WDX).

    Science.gov (United States)

    Kage, S; Kudo, K; Kaizoji, A; Ryumoto, J; Ikeda, H; Ikeda, N

    2001-07-01

    We devised a simple and rapid method for detection of gunshot residue (GSR) particles, using scanning electron microscopy/wavelength dispersive X-ray (SEM/WDX) analysis. Experiments were done on samples containing GSR particles obtained from hands, hair, face, and clothing, using double-sided adhesive coated aluminum stubs (tape-lift method). SEM/WDX analyses for GSR were carried out in three steps: the first step was map analysis for barium (Ba) to search for GSR particles from lead styphnate primed ammunition, or tin (Sn) to search for GSR particles from mercury fulminate primed ammunition. The second step was determination of the location of GSR particles by X-ray imaging of Ba or Sn at a magnification of x 1000-2000 in the SEM, using data of map analysis, and the third step was identification of GSR particles, using WDX spectrometers. Analysis of samples from each primer of a stub took about 3 h. Practical applications were shown for utility of this method.

  11. Mixing state of particles with secondary species by single particle aerosol mass spectrometer in an atmospheric pollution event

    Science.gov (United States)

    Xu, Lingling; Chen, Jinsheng

    2016-04-01

    Single particle aerosol mass spectrometer (SPAMS) was used to characterize size distribution, chemical composition, and mixing state of particles in an atmospheric pollution event during 20 Oct. - 5 Nov., 2015 in Xiamen, Southeast China. A total of 533,012 particle mass spectra were obtained and clustered into six groups, comprising of industry metal (4.5%), dust particles (2.6%), carbonaceous species (70.7%), K-Rich particles (20.7%), seasalt (0.6%) and other particles (0.9%). Carbonaceous species were further divided into EC (70.6%), OC (28.5%), and mixed ECOC (0.9%). There were 61.7%, 58.3%, 4.0%, and 14.6% of particles internally mixed with sulfate, nitrate, ammonium and C2H3O, respectively, indicating that these particles had undergone significant aging processing. Sulfate was preferentially mixed with carbonaceous particles, while nitrate tended to mix with metal-containing and dust particles. Compared to clear days, the fractions of EC-, metal- and dust particles remarkably increased, while the fraction of OC-containing particles decreased in pollution days. The mixing state of particles, excepted for OC-containing particles with secondary species was much stronger in pollution days than that in clear days, which revealed the significant influence of secondary particles in atmospheric pollution. The different activity of OC-containing particles might be related to their much smaller aerodynamic diameter. These results could improve our understanding of aerosol characteristics and could be helpful to further investigate the atmospheric process of particles.

  12. Single-particle measurements of bouncing particles and in situ collection efficiency from an airborne aerosol mass spectrometer (AMS) with light-scattering detection

    Science.gov (United States)

    Liao, Jin; Brock, Charles A.; Murphy, Daniel M.; Sueper, Donna T.; Welti, André; Middlebrook, Ann M.

    2017-10-01

    A light-scattering module was coupled to an airborne, compact time-of-flight aerosol mass spectrometer (LS-AMS) to investigate collection efficiency (CE) while obtaining nonrefractory aerosol chemical composition measurements during the Southeast Nexus (SENEX) campaign. In this instrument, particles scatter light from an internal laser beam and trigger saving individual particle mass spectra. Nearly all of the single-particle data with mass spectra that were triggered by scattered light signals were from particles larger than ˜ 280 nm in vacuum aerodynamic diameter. Over 33 000 particles are characterized as either prompt (27 %), delayed (15 %), or null (58 %), according to the time and intensity of their total mass spectral signals. The particle mass from single-particle spectra is proportional to that derived from the light-scattering diameter (dva-LS) but not to that from the particle time-of-flight (PToF) diameter (dva-MS) from the time of the maximum mass spectral signal. The total mass spectral signal from delayed particles was about 80 % of that from prompt ones for the same dva-LS. Both field and laboratory data indicate that the relative intensities of various ions in the prompt spectra show more fragmentation compared to the delayed spectra. The particles with a delayed mass spectral signal likely bounced off the vaporizer and vaporized later on another surface within the confines of the ionization source. Because delayed particles are detected by the mass spectrometer later than expected from their dva-LS size, they can affect the interpretation of particle size (PToF) mass distributions, especially at larger sizes. The CE, measured by the average number or mass fractions of particles optically detected that had measurable mass spectra, varied significantly (0.2-0.9) in different air masses. The measured CE agreed well with a previous parameterization when CE > 0.5 for acidic particles but was sometimes lower than the minimum parameterized CE of 0.5.

  13. Amping it up on a small budget: Transforming inexpensive, commercial audio and video components into a useful charged particle spectrometer

    Science.gov (United States)

    Pallone, Arthur

    Necessity often leads to inspiration. Such was the case when a traditional amplifier quit working during the collection of an alpha particle spectrum. I had a 15 battery-powered audio amplifier in my box of project electronics so I connected it between the preamplifier and the multichannel analyzer. The alpha particle spectrum that appeared on the computer screen matched expectations even without correcting for impedance mismatches. Encouraged by this outcome, I have begun to systematically replace each of the parts in a traditional charged particle spectrometer with audio and video components available through consumer electronics stores with the goal of producing an inexpensive charged particle spectrometer for use in education and research. Hopefully my successes, setbacks, and results to date described in this presentation will inform and inspire others.

  14. The Omicron Spectrometer

    CERN Document Server

    Allardyce, B W

    1976-01-01

    It is intended to build a spectrometer with a large solid angle and a large momentum acceptance at the reconstructed synchrocyclotron at CERN. This spectrometer will have an energy resolution of about 1 MeV for particles with momenta up to about 400 MeV/c.

  15. Expanding Single Particle Mass Spectrometer Analyses for the Identification of Microbe Signatures in Sea Spray Aerosol.

    Science.gov (United States)

    Sultana, Camille M; Al-Mashat, Hashim; Prather, Kimberly A

    2017-10-03

    Ocean-derived microbes in sea spray aersosol (SSA) have the potential to influence climate and weather by acting as ice nucleating particles in clouds. Single particle mass spectrometers (SPMSs), which generate in situ single particle composition data, are excellent tools for characterizing aerosols under changing environmental conditions as they can provide high temporal resolution and require no sample preparation. While SPMSs have proven capable of detecting microbes, these instruments have never been utilized to definitively identify aerosolized microbes in ambient sea spray aersosol. In this study, an aerosol time-of-flight mass spectrometer was used to analyze laboratory generated SSA produced from natural seawater in a marine aerosol reference tank. We present the first description of a population of biological SSA mass spectra (BioSS), which closely match the ion signatures observed in previous terrestrial microbe studies. The fraction of BioSS dramatically increased in the largest supermicron particles, consistent with field and laboratory measurements of microbes ejected by bubble bursting, further supporting the assignment of BioSS mass spectra as microbes. Finally, as supported by analysis of inorganic ion signals, we propose that dry BioSS particles have heterogeneous structures, with microbes adhered to sodium chloride nodules surrounded by magnesium-enriched coatings. Consistent with this structure, chlorine-containing ion markers were ubiquitous in BioSS spectra and identified as possible tracers for distinguishing recently aerosolized marine from terrestrial microbes.

  16. A PbWO4-based Neutral Particle Spectrometer in Hall C at 12 GeV JLab

    Energy Technology Data Exchange (ETDEWEB)

    Horn, Tanja [Catholic University of America , Washington, DC

    2015-02-01

    The Neutral Particle Spectrometer is a standalone electromagnetic calorimeter capable of detecting high energy photons from, for instance, DVCS or π0 decay with good energy and spatial resolution in a high rate environment. It can be used together with the Hall C high-momentum spectrometers for a suite of experiments with the underlying scientific objective of studying quark dynamics through exclusive and semi-inclusive reactions.

  17. First results from the RAPID imaging energetic particle spectrometer on board Cluster

    Directory of Open Access Journals (Sweden)

    B. Wilken

    2001-09-01

    Full Text Available The advanced energetic particle spectrometer RAPID on board Cluster can provide a complete description of the relevant particle parameters velocity, V , and atomic mass, A, over an energy range from 30 keV up to 1.5 MeV. We present the first measurements taken by RAPID during the commissioning and the early operating phases. The orbit on 14 January 2001, when Cluster was travelling from a perigee near dawn northward across the pole towards an apogee in the solar wind, is used to demonstrate the capabilities of RAPID in investigating a wide variety of particle populations. RAPID, with its unique capability of measuring the complete angular distribution of energetic particles, allows for the simultaneous measurements of local density gradients, as reflected in the anisotropies of 90° particles and the remote sensing of changes in the distant field line topology, as manifested in the variations of loss cone properties. A detailed discussion of angle-angle plots shows considerable differences in the structure of the boundaries between the open and closed field lines on the nightside fraction of the pass and the magnetopause crossing. The 3 March 2001 encounter of Cluster with an FTE just outside the magnetosphere is used to show the first structural plasma investigations of an FTE by energetic multi-spacecraft observations.Key words. Magnetospheric physics (energetic particles, trapped; magnetopause, cusp and boundary layers; magnetosheath

  18. Mass spectra features of biomass burning boiler and coal burning boiler emitted particles by single particle aerosol mass spectrometer.

    Science.gov (United States)

    Xu, Jiao; Li, Mei; Shi, Guoliang; Wang, Haiting; Ma, Xian; Wu, Jianhui; Shi, Xurong; Feng, Yinchang

    2017-11-15

    In this study, single particle mass spectra signatures of both coal burning boiler and biomass burning boiler emitted particles were studied. Particle samples were suspended in clean Resuspension Chamber, and analyzed by ELPI and SPAMS simultaneously. The size distribution of BBB (biomass burning boiler sample) and CBB (coal burning boiler sample) are different, as BBB peaks at smaller size, and CBB peaks at larger size. Mass spectra signatures of two samples were studied by analyzing the average mass spectrum of each particle cluster extracted by ART-2a in different size ranges. In conclusion, BBB sample mostly consists of OC and EC containing particles, and a small fraction of K-rich particles in the size range of 0.2-0.5μm. In 0.5-1.0μm, BBB sample consists of EC, OC, K-rich and Al_Silicate containing particles; CBB sample consists of EC, ECOC containing particles, while Al_Silicate (including Al_Ca_Ti_Silicate, Al_Ti_Silicate, Al_Silicate) containing particles got higher fractions as size increase. The similarity of single particle mass spectrum signatures between two samples were studied by analyzing the dot product, results indicated that part of the single particle mass spectra of two samples in the same size range are similar, which bring challenge to the future source apportionment activity by using single particle aerosol mass spectrometer. Results of this study will provide physicochemical information of important sources which contribute to particle pollution, and will support source apportionment activities. Copyright © 2017. Published by Elsevier B.V.

  19. Standalone vertex finding in the ATLAS muon spectrometer

    DEFF Research Database (Denmark)

    Aad, A.; Abajyan, T.; Abbott, B.

    2014-01-01

    A dedicated reconstruction algorithm to find decay vertices in the ATLAS muon spectrometer is presented. The algorithm searches the region just upstream of or inside the muon spectrometer volume for multi-particle vertices that originate from the decay of particles with long decay paths. The perf......A dedicated reconstruction algorithm to find decay vertices in the ATLAS muon spectrometer is presented. The algorithm searches the region just upstream of or inside the muon spectrometer volume for multi-particle vertices that originate from the decay of particles with long decay paths....... The performance of the algorithm is evaluated using both a sample of simulated Higgs boson events, in which the Higgs boson decays to long-lived neutral particles that in turn decay to bbar b final states, and pp collision data at √s = 7 TeV collected with the ATLAS detector at the LHC during 2011....

  20. Design of an electronic charged particle spectrometer to measure (ρR), yield, and implosion symmetry on the OMEGA Upgrade

    International Nuclear Information System (INIS)

    Hicks, D.G.; Li, C.K.; Petrasso, R.D.; Wenzel, K.W.; Knauer, J.P.

    1994-11-01

    The preliminary design for a state-of-the-art diagnostic that will measure a broad energy spectrum of charged particles generated in the OMEGA Upgrade facility is investigated. Using a set of photodiodes (∼10) and a 0.8 Tesla permanent magnet, the diagnostic will uniquely determine particle energies and identities from 0.2 MeV up to the maximum charged particle energies (10.6 MeV tritons, 12.5 MeV deuterons and 17.4 MeV protons). With its high density picture elements, each photodiode has 10 6 single-hit detectors, giving the spectrometer a dynamic range of 1 - 10 5 particles/shot. For example, in the case of a DT yield of 10 9 neutrons, about 100 knock-on charged particles will be detected when the spectrometer aperture is 60 cm from the implosion. Furthermore, the measurement of knock-on D and T spectra will allow ρR's up to 0.15 g/cm 2 to be measured (for a 1 keV plasma), or 0.3 g/cm 2 2 if hydrogen doping is used. In addition, the yield and slowing down of secondary protons may be used to determine ρR up to 0.3 g/cm 2 . Significantly, this diagnostic will also directly measure the DD fusion yield and energy degradation of nascent 3 MeV protons. By using two such compact spectrometers to measure the yield and spectra on widely separated ports around the OMEGA Upgrade target chamber, the implosion and bum symmetry can be determined. Furthermore, the ion temperature, and, in principle, even the electron temperature can be measured. The diagnostic and its development will be fully tested at several critical steps, utilizing 0.2-16 MeV protons (and several other charged particles and neutrons) from our absolutely calibrated Cockcroft-Walton facility

  1. Two-arm semiconductor spectrometer for charged particles for the investigation of absorption by nuclei of stopped negative pions

    International Nuclear Information System (INIS)

    Gornov, M.G.; Gurov, Yu.B.; Lukin, A.S.; Morokhov, P.V.; Pechkurov, V.A.; Pichugin, A.P.; Saveliev, V.I.; Shafigullin, R.R.; Sergeev, F.M.; Khomutov, A.A.; Oganesian, K.O.; Osipenko, B.P.; Sandukovsky, V.G.

    1984-01-01

    A two-arm semiconductor spectrometer for the detection of secondary charged particles, such as p, d, t, 3 He, 4 He and of their correlations in the process of stopped pion absorption by nuclei is described. The spectrometer consists of two telescopes of Si-detectors with a sensitive surface of 800 mm 2 , two semiconductor detectors as monitors and the 'live' target, a silicon surface barrier detector. The number of semiconductor detectors is 19. A technique for pion stop selection in thin targets is described. The problem of particle identification and of measurements of their energy with the help of a multicrystal semiconductor telescope is discussed. The technique provides an absolute normalization of spectra. The 'alive' target helps to obtain more information on the process of pion absorption by Si-nuclei. (orig.)

  2. Astrophysics and particle physics in space with the Alpha Magnetic Spectrometer

    CERN Document Server

    Lamanna, G

    2003-01-01

    The Alpha Magnetic Spectrometer is a high energy particle physics experiment in space scheduled to be installed on the International Space Station (ISS) by 2006 for a three-year mission. After a precursor flight of a prototype detector on board of the NASA Space Shuttle in June 1998, the construction of the detector in its final configuration is started and it will be completed by 2004. The purpose of this experiment is to provide a high statistics measurement of charged particles and nuclei in rigidity range 0.5 GV to few TV and to explore the high-energy (>1 GeV) gamma-ray sky. In this paper we describe the detector layout and present an overview of the main scientific goals both in the domain of astrophysics: cosmic- ray origin, age and propagation and the exploration of the most energetic gamma-ray sources; and in the domain of astroparticle: the antimatter and the dark matter searches. (53 refs).

  3. Imaging of the vertical particle tracks without any depth scanning

    International Nuclear Information System (INIS)

    Soroko, L.M.

    2001-01-01

    The principle of a new optical microscope which enables us to get the image of a vertical particle track without any depth scanning is described. This new optical microscope contains a spatial transformer which consists of mirror lamellar elements and which produces a secondary in focus image of the vertical particle track. Properties of such a system are presented. A longitudinal resolution is estimated

  4. Particle size distribution of the radon progeny and ambient aerosols in the Underground Tourist Route "Liczyrzepa" Mine in Kowary Adit

    Science.gov (United States)

    Wołoszczuk, Katarzyna; Skubacz, Krystian

    2018-01-01

    Central Laboratory for Radiological Protection, in cooperation with Central Mining Institute performed measurements of radon concentration in air, potential alpha energy concentration (PAEC), particle size distribution of the radon progeny and ambient aerosols in the Underground Tourist-Educational Route "Liczyrzepa" Mine in Kowary Adit. A research study was developed to investigate the appropriate dose conversion factors for short-lived radon progeny. The particle size distribution of radon progeny was determined using Radon Progeny Particle Size Spectrometer (RPPSS). The device allows to receive the distribution of PAEC in the particle size range from 0.6 nm to 2494 nm, based on their activity measured on 8 stages composed of impaction plates or diffusion screens. The measurements of the ambient airborne particle size distribution were performed in the range from a few nanometres to about 20 micrometres using Aerodynamic Particle Sizer (APS) spectrometer and the Scanning Mobility Particle Sizer Spectrometer (SMPS).

  5. First results from the RAPID imaging energetic particle spectrometer on board Cluster

    Directory of Open Access Journals (Sweden)

    B. Wilken

    Full Text Available The advanced energetic particle spectrometer RAPID on board Cluster can provide a complete description of the relevant particle parameters velocity, V , and atomic mass, A, over an energy range from 30 keV up to 1.5 MeV. We present the first measurements taken by RAPID during the commissioning and the early operating phases. The orbit on 14 January 2001, when Cluster was travelling from a perigee near dawn northward across the pole towards an apogee in the solar wind, is used to demonstrate the capabilities of RAPID in investigating a wide variety of particle populations. RAPID, with its unique capability of measuring the complete angular distribution of energetic particles, allows for the simultaneous measurements of local density gradients, as reflected in the anisotropies of 90° particles and the remote sensing of changes in the distant field line topology, as manifested in the variations of loss cone properties. A detailed discussion of angle-angle plots shows considerable differences in the structure of the boundaries between the open and closed field lines on the nightside fraction of the pass and the magnetopause crossing. The 3 March 2001 encounter of Cluster with an FTE just outside the magnetosphere is used to show the first structural plasma investigations of an FTE by energetic multi-spacecraft observations.

    Key words. Magnetospheric physics (energetic particles, trapped; magnetopause, cusp and boundary layers; magnetosheath

  6. The BTeV main spectrometer

    International Nuclear Information System (INIS)

    Sheldon, P.D.

    2001-01-01

    BTeV is a second generation B-factory experiment that will use a double-arm, forward spectrometer in the C0 experimental hall at the Fermilab Tevatron. I will describe the motivation and design of the 'main spectrometer', consisting of a ring-imaging Cherenkov system for charged particle identification, an electromagnetic calorimeter of lead-tungstate crystals, a proportional tube muon system with magnetized filtering steel, and a straw-tube and silicon strip charged particle tracking system

  7. Gas-dust-impact mass spectrometer

    CERN Document Server

    Semkin, N D; Myasnikov, S V; Pomelnikov, R A

    2002-01-01

    Paper describes design of a mass spectrometer to study element composition of micro meteorite and man-made particles in space. Paper describes a way to improve resolution of mass spectrometer based on variation of parameters of accelerating electric field in time. The advantage of the given design of mass spectrometer in comparison with similar ones is its large operating area and higher resolution at the comparable weight and dimensions. Application of a combined design both for particles and for gas enables to remove space vehicle degassing products from the spectrum and, thus, to improve reliability of the acquired information, as well as, to acquire information on a gas component of the external atmosphere of a space vehicle

  8. Derivation of gravity wave intrinsic parameters and vertical wavelength using a single scanning OH(3-1) airglow spectrometer

    Science.gov (United States)

    Wüst, Sabine; Offenwanger, Thomas; Schmidt, Carsten; Bittner, Michael; Jacobi, Christoph; Stober, Gunter; Yee, Jeng-Hwa; Mlynczak, Martin G.; Russell, James M., III

    2018-05-01

    For the first time, we present an approach to derive zonal, meridional, and vertical wavelengths as well as periods of gravity waves based on only one OH* spectrometer, addressing one vibrational-rotational transition. Knowledge of these parameters is a precondition for the calculation of further information, such as the wave group velocity vector.OH(3-1) spectrometer measurements allow the analysis of gravity wave ground-based periods but spatial information cannot necessarily be deduced. We use a scanning spectrometer and harmonic analysis to derive horizontal wavelengths at the mesopause altitude above Oberpfaffenhofen (48.09° N, 11.28° E), Germany for 22 nights in 2015. Based on the approximation of the dispersion relation for gravity waves of low and medium frequencies and additional horizontal wind information, we calculate vertical wavelengths. The mesopause wind measurements nearest to Oberpfaffenhofen are conducted at Collm (51.30° N, 13.02° E), Germany, ca. 380 km northeast of Oberpfaffenhofen, by a meteor radar.In order to compare our results, vertical temperature profiles of TIMED-SABER (thermosphere ionosphere mesosphere energetics dynamics, sounding of the atmosphere using broadband emission radiometry) overpasses are analysed with respect to the dominating vertical wavelength.

  9. Calculational approach to ionization spectrometer design

    International Nuclear Information System (INIS)

    Gabriel, T.A.

    1974-01-01

    Many factors contribute to the design and overall performance of an ionization spectrometer. These factors include the conditions under which the spectrometer is to be used, the required performance, the development of the hadronic and electromagnetic cascades, leakage and binding energies, saturation effects of densely ionizing particles, nonuniform light collection, sampling fluctuations, etc. The calculational procedures developed at Oak Ridge National Laboratory that have been applied to many spectrometer designs and that include many of the influencing factors in spectrometer design are discussed. The incident-particle types which can be considered with some generality are protons, neutrons, pions, muons, electrons, positrons, and gamma rays. Charged kaons can also be considered but with less generality. The incident-particle energy range can extend into the hundreds of GeV range. The calculations have been verified by comparison with experimental data but only up to approximately 30 GeV. Some comparisons with experimental data are also discussed and presented so that the flexibility of the calculational methods can be demonstrated. (U.S.)

  10. Probing Single Nanometer-scale Particles with Scanning Tunneling Microscopy and Spectroscopies

    International Nuclear Information System (INIS)

    McCarty, G.S.; Love, J.C.; Kushmerick, J.G.; Charles, L.F.; Keating, C.D.; Toleno, B.J.; Lyn, M.E.; Castleman, A.W.; Natan, M.J.; Weiss, P.S.

    1999-01-01

    Scanning tunneling microscopy can be used to isolate single particles on surfaces for further study. Local optical and electronic properties coupled with topographic information collected by the scanning tunneling microscope (STM) give insight into the intrinsic properties of the species under study. Since each spectroscopic measurement is done on a single particle, each sample is 'monodisperse', regardless of the degree of heterogeneity of the original preparation. We illustrate this with three example systems - a metal cluster of known atomic structure, metal nanoparticles dispersed from colloid suspensions, and metallocarbohedrenes (Met-Cars) deposited with other reaction products. Au and Ag nanoparticles were imaged using a photon emission STM. The threshold voltage, the lowest bias voltage at which photons are produced, was determined for Au nanoparticles. Electronic spectra of small clusters of Ni atoms on MoS 2 were recorded. Preliminary images of Zr-based Met-Car-containing soot were obtained on Au and MoS 2 substrates and partial electronic spectra were recorded of these possible Met-Car particles

  11. The instrumental blank of the Mars Science Laboratory alpha particle X-ray spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Campbell, J.L., E-mail: icampbel@uoguelph.ca [Guelph-Waterloo Physics Institute, University of Guelph, Guelph, Ontario, N1G 2W1 (Canada)

    2012-10-01

    The alpha particle X-ray spectrometers on the Mars exploration rovers Spirit and Opportunity accomplished extensive elemental analysis of the Martian surface through a combination of XRF and PIXE. An advanced APXS is now part of the Mars Science Laboratory's Curiosity rover. APXS spectra contain contributions which enhance elemental peak areas but which do not arise from these elements within the sample under study, thereby introducing error into derived concentrations. A detailed examination of these effects in the MSL APXS enables us to test two schemes for making the necessary corrections.

  12. Particle size distribution of the radon progeny and ambient aerosols in the Underground Tourist Route “Liczyrzepa” Mine in Kowary Adit

    Directory of Open Access Journals (Sweden)

    Wołoszczuk Katarzyna

    2018-01-01

    Full Text Available Central Laboratory for Radiological Protection, in cooperation with Central Mining Institute performed measurements of radon concentration in air, potential alpha energy concentration (PAEC, particle size distribution of the radon progeny and ambient aerosols in the Underground Tourist-Educational Route “Liczyrzepa” Mine in Kowary Adit. A research study was developed to investigate the appropriate dose conversion factors for short-lived radon progeny. The particle size distribution of radon progeny was determined using Radon Progeny Particle Size Spectrometer (RPPSS. The device allows to receive the distribution of PAEC in the particle size range from 0.6 nm to 2494 nm, based on their activity measured on 8 stages composed of impaction plates or diffusion screens. The measurements of the ambient airborne particle size distribution were performed in the range from a few nanometres to about 20 micrometres using Aerodynamic Particle Sizer (APS spectrometer and the Scanning Mobility Particle Sizer Spectrometer (SMPS.

  13. Rotating double arm spectrometer to study hard scattering interactions at Serpukhov accelerator

    International Nuclear Information System (INIS)

    Abramov, V.V.; Baldin, B.Yu.; Buzulutskov, A.F.

    1991-01-01

    The double arm magnetic spectrometer designed to study high P T particle production with intense proton and pion beams is described. Particle trajectories are measured by the drift and proportional chambers. Particles are identified by Cherenkov ring spectrometer and muon identifier. The spectrometer can be rotated around the target up to 160 mrad. 2 tabs.; 13 figs

  14. Feasibility study of a SiC sandwich neutron spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Jian, E-mail: caepwujian@163.com [Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, Sichuan Province (China); Lei, Jiarong, E-mail: jiarong_lei@163.com [Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, Sichuan Province (China); Jiang, Yong; Chen, Yu; Rong, Ru; Zou, Dehui; Fan, Xiaoqiang [Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang 621900, Sichuan Province (China); Chen, Gang; Li, Li; Bai, Song [Nanjing Electronic Devices Institute, Nanjing 210016 (China)

    2013-04-21

    Semiconductor sandwich neutron spectrometers are suitable for in-pile measurements of fast reactor spectra thanks to their compact and relatively simple design. We have assembled and tested a sandwich neutron spectrometer based on 4H-silicon carbide (4H-SiC) Schottky diodes. The SiC diodes detect neutrons via neutron-induced charged particles (tritons and alpha particles) produced by {sup 6}Li(n,α){sup 3}H reaction. {sup 6}LiF neutron converter layers are deposited on the front surface of Schottky diodes by magnetron sputtering. The responses of SiC diodes to charged particles were investigated with an {sup 241}Am alpha source. A sandwich neutron spectrometer was assembled with two SiC Schottky diodes selected based on the charged-particle-response experimental results. The low-energy neutron response of the sandwich spectrometer was measured in the neutron field of the Chinese Fast Burst Reactor-II (CFBR-II). Spectra of alpha particles and tritons from {sup 6}Li(n,α){sup 3}H reaction were obtained with two well-resolved peaks. The energy resolution of the sum spectrum was 8.8%. The primary experimental results confirmed the 4H-SiC sandwich neutron spectrometer's feasibility. -- Highlights: ► Sandwich neutron spectrometer employing 4H-SiC as a detecting material has been developed for the first time. ► {sup 6}LiF neutron converter has been deposited on the surface of 4H-SiC Schottky diode. ► Preliminary testing results obtained with the 4H-SiC sandwich neutron spectrometer are presented.

  15. Measurements of double differential charged particle emission cross sections and development of a wide range charged particles spectrometer for ten`s MeV neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Nauchi, Yasushi; Baba, Mamoru; Kiyosumi, Takehide [Tohoku Univ., Sendai (Japan). Faculty of Engineering] [and others

    1997-03-01

    We measured (n,xp), (n,xd) cross sections of C and Al for En=64.3 MeV neutrons at the {sup 7}Li(p,n) neutron sources facility at TIARA (Takasaki Establishment, JAERI) by using a conventional SSD-NaI telescope placed in the air. They show characteristic energy and angular dependence in high energy regions. In order to extend the measurements to low energy protons and {alpha} particles, a new spectrometer consisting of low pressure gas counters and BaF{sub 2} scintillators is now under development. A low threshold for low energy {alpha} particles will be achieved by using the gas counters. The particle identification over a wide energy range will be achieved by combining the {Delta}E-E method for low energy particles with the pulse shape discrimination (PSD) method of BaF{sub 2} for high energy particles. (author)

  16. Charged particle beam scanning using deformed high gradient insulator

    Science.gov (United States)

    Chen, Yu -Jiuan

    2015-10-06

    Devices and methods are provided to allow rapid deflection of a charged particle beam. The disclosed devices can, for example, be used as part of a hadron therapy system to allow scanning of a target area within a patient's body. The disclosed charged particle beam deflectors include a dielectric wall accelerator (DWA) with a hollow center and a dielectric wall that is substantially parallel to a z-axis that runs through the hollow center. The dielectric wall includes one or more deformed high gradient insulators (HGIs) that are configured to produce an electric field with an component in a direction perpendicular to the z-axis. A control component is also provided to establish the electric field component in the direction perpendicular to the z-axis and to control deflection of a charged particle beam in the direction perpendicular to the z-axis as the charged particle beam travels through the hollow center of the DWA.

  17. Contrast and decay of cathodoluminescence from phosphor particles in a scanning electron microscope.

    Science.gov (United States)

    den Engelsen, Daniel; Harris, Paul G; Ireland, Terry G; Fern, George R; Silver, Jack

    2015-10-01

    Cathodoluminescence (CL) studies are reported on phosphors in a field emission scanning electron microscope (FESEM). ZnO: Zn and other luminescent powders manifest a bright ring around the periphery of the particles: this ring enhances the contrast. Additionally, particles resting on top of others are substantially brighter than underlying ones. These phenomena are explained in terms of the combined effects of electrons backscattered out of the particles, together with light absorption by the substrate. The contrast is found to be a function of the particle size and the energy of the primary electrons. Some phosphor materials exhibit a pronounced comet-like structure at high scan rates in a CL-image, because the particle continues to emit light after the electron beam has moved to a position without phosphor material. Image analysis has been used to study the loss of brightness along the tail and hence to determine the decay time of the materials. The effect of phosphor saturation on the determination of decay times by CL-microscopy was also investigated. Copyright © 2015 Elsevier B.V. All rights reserved.

  18. Single spectrometer station for neutrino-tagging

    International Nuclear Information System (INIS)

    Nedyalkov, I.P.

    1984-01-01

    A neutrino tagging station built with respect to the following scheme is proposed. A beam of muons and kaons passes through a magnetic spectrometer, where the energy of each particle is measured. There are coordinate detectors behind the spectrometer in several planes, where the direction of the trajectory of a given particle is determined. Thus, mesons enter the decay point wth the known 4-momentum. Behind the decay point the direction of μ-meson generated by the decay of parent mesons is measured. It is shown that information is sufficient for determining the kind of parent particle (pion or kaon), the energy and the direction of trajectory of the neutrino

  19. The MEDUSA electron and ion spectrometer and the PIA ultraviolet photometers on Astrid-2

    Directory of Open Access Journals (Sweden)

    O. Norberg

    2001-06-01

    Full Text Available The miniature electron and ion spectrometer MEDUSA on Astrid-2 consists of two "top-hat"-type spherical electrostatic analyzers, sharing a common top-hat. Fast energy sweeps (16 electron sweeps and 8 ion sweeps per second allow for very high temporal resolution measurements of a two-dimensional slice of the particle distribution function. The energy range covered, is in the case of electrons, 4 eV to 22 keV and, in the case of ions, 2 eV to 12 keV. MEDUSA is mounted with its aperture close to the spin plane of Astrid-2, which allows for good pitch-angle coverage when the local magnetic field is in the satellite spin plane. The PIA-1/2 spin-scanning ultraviolet photometers measure auroral emissions. Using the spacecraft spin and orbital motion, it is possible to create two-dimensional images from the data. Spin-scanning photometers, such as PIA, are low-cost, low mass alternatives to auroral imagers, but place constraints on the satellite attitude. Data from MEDUSA are used to study processes in the auroral region, in particular, electrodynamics of aurora and "black aurora". MEDUSA is also a technological development, paving the way for highly capable, miniaturized particle spectrometers.Key words. Ionosphere (instruments and techniques – Magnetospheric physics (auroral phenomena; instruments and techniques

  20. Composite particle production in relativistic Au+Au collisions at AGS: First results from the E866 forward spectrometer at sign 2, 4, and 10.8 A·GeV

    International Nuclear Information System (INIS)

    Ashktorab, K.

    1996-01-01

    Particle spectra were measured for Au + Au collisions at 2, 4, and 10. 8 A·GeV using the E866 spectrometers. Recent results on proton emission and composite particle production form the E866 forward spectrometer data taken in 1994 together with the first results from the 1995/6 AGS running period are presented. Preliminary results indicate a decrease in the coalescence scaling coefficient with increasing projectile energy and centrality

  1. Alpha particles spectrometer with photodiode PIN; Espectrometro de particulas alfa con fotodiodo PIN

    Energy Technology Data Exchange (ETDEWEB)

    Chacon R, A.; Hernandez V, R.; Hernandez D, V. M.; Vega C, H. R. [Universidad Autonoma de Zacatecas, Unidades Academicas de Estudios Nucleares e Ingenieria Electrica, Calle Cipres No. 10, Fracc. La Penuela, 09869 Zacatecas (Mexico); Ramirez G, J. [Instituto Nacional de Estadistica Geografia e Informatica, Direccion General de Innovacion y Tecnologia de Informacion, Av. Heroes de Nacozari Sur 2301, Fracc. Jardines del Parque, 20276 Aguascalientes (Mexico)], e-mail: achruiz@hotmail.com

    2009-10-15

    The radiation propagates in form of electromagnetic waves or corpuscular radiation; if the radiation energy causes ionization in environment that crosses it is considered ionizing radiation. To detect radiation several detectors types are used, if the radiation are alpha particles are used detectors proportional type or trace elements. In this work the design results, construction and tests of an alpha particles spectrometer are presented, which was designed starting from a photodiode PIN type. The system design was simulated with a code for electronic circuits. With results of simulation phase was constructed the electronic phase that is coupled to a multichannel analyzer. The resulting electronic is evaluated analyzing the electronic circuit performance before an alphas triple source and alpha radiation that produce two smoke detectors of domestic use. On the tests phase we find that the system allows obtain, in a multichannel, the pulses height spectrum, with which we calibrate the system. (Author)

  2. A particle identification technique for large acceptance spectrometers

    International Nuclear Information System (INIS)

    Cappuzzello, F.; Cavallaro, M.; Cunsolo, A.; Foti, A.; Carbone, D.; Orrigo, S.E.A.; Rodrigues, M.R.D.

    2010-01-01

    A technique to identify the heavy ions produced in nuclear reactions is presented. It is based on the use of a hybrid detector, which measures the energy loss, the residual energy, the position and angle of the ions at the focal plane of a magnetic spectrometer. The key point is the use of a powerful algorithm for the reconstruction of the ion trajectory, which makes the technique reliable even with large acceptance optical devices. Experimental results with the MAGNEX spectrometer show a remarkable resolution of about 1/160 in the mass parameter.

  3. Step-scan Fourier transform infrared (FTIR) spectrometer for investigating chemical reactions of energy-related materials. Final report, April 1, 1995--March 31, 1997

    Energy Technology Data Exchange (ETDEWEB)

    Eyring, E.M.

    1997-11-04

    Two step-scan Fourier transform infrared (FTIR) spectrometers were purchased with URI-DOE funds by the University of Utah. These infrared spectrometers have been used to carry out the following investigations: the determination of strength of adsorption of organic molecules at the liquid-solid interface of coated attenuated total reflectance (ATR) elements, the kinetic study of the photoinitiated polymerization of a dental resin, the exploration of the kinetics of photochemical reactions of organic molecules in solution, and the development of a stopped-flow FTIR interface for measuring rates and mechanisms of reactions in solution that are not photoinitiated and do not have convenient ultraviolet-visible spectral features.

  4. Local secondary-electron emission spectra of graphite and gold surfaces obtained using the Scanning Probe Energy Loss Spectrometer (SPELS)

    International Nuclear Information System (INIS)

    Lawton, J J; Pulisciano, A; Palmer, R E

    2009-01-01

    Secondary-electron emission (SEE) spectra have been obtained with the Scanning Probe Energy Loss Spectrometer at a tip-sample distance of only 50 nm. Such short working distances are required for the best theoretical spatial resolution (<10 nm). The SEE spectra of graphite, obtained as a function of tip bias voltage, are shown to correspond to unoccupied states in the electronic band structure. The SEE spectra of thin gold films demonstrate the capability of identifying (carbonaceous) surface contamination with this technique.

  5. Local secondary-electron emission spectra of graphite and gold surfaces obtained using the Scanning Probe Energy Loss Spectrometer (SPELS)

    Energy Technology Data Exchange (ETDEWEB)

    Lawton, J J; Pulisciano, A; Palmer, R E, E-mail: R.E.Palmer@bham.ac.u [Nanoscale Physics Research Laboratory, School of Physics and Astronomy, University of Birmingham, Birmingham B15 2TT (United Kingdom)

    2009-11-25

    Secondary-electron emission (SEE) spectra have been obtained with the Scanning Probe Energy Loss Spectrometer at a tip-sample distance of only 50 nm. Such short working distances are required for the best theoretical spatial resolution (<10 nm). The SEE spectra of graphite, obtained as a function of tip bias voltage, are shown to correspond to unoccupied states in the electronic band structure. The SEE spectra of thin gold films demonstrate the capability of identifying (carbonaceous) surface contamination with this technique.

  6. Scintillation forward spectrometer of the SPHERE setup

    International Nuclear Information System (INIS)

    Anisimov, Yu.S.; Afanas'ev, S.V.; Bondarev, V.K.

    1991-01-01

    The construction of the forward spectrometer for the 4π SPHERE setup to study multiple production of particles in nucleus-nucleus interactions is described. The measured parameters of the spectrometer detectors are presented. 7 refs.; 14 figs.; 1 tab

  7. Visible and infrared mapping spectrometer (VIMS) - a facility instrument for planetary missions

    International Nuclear Information System (INIS)

    Wellman, J.B.; Duval, J.; Juergens, D.; Voss, J.

    1988-01-01

    A second-generation visible and IR mapping spectrometer (VIMS), selected for both the Mars Observer and Comet Rendezvous Asteroid Flyby (CRAF) missions, is described. VIMS is a scanning spectrometer with a focal plane consisting of linear arrays of visible and IR detectors, cooled by a radiative cooler. It is noted that a wide-angle scan using a full-aperture scan mirror was implemented for the Mars Observer; a narrow-angle scan using a scanning secondary mirror within a Cassegrain foreoptic was achieved for the CRAF mission. 11 references

  8. EUCAARI ion spectrometer measurements at 12 European sites – analysis of new particle formation events

    Directory of Open Access Journals (Sweden)

    H. E. Manninen

    2010-08-01

    Full Text Available We present comprehensive results on continuous atmospheric cluster and particle measurements in the size range ~1–42 nm within the European Integrated project on Aerosol Cloud Climate and Air Quality interactions (EUCAARI project. We focused on characterizing the spatial and temporal variation of new particle formation events and relevant particle formation parameters across Europe. Different types of air ion and cluster mobility spectrometers were deployed at 12 field sites across Europe from March 2008 to May 2009. The measurements were conducted in a wide variety of environments, including coastal and continental locations as well as sites at different altitudes (both in the boundary layer and the free troposphere. New particle formation events were detected at all of the 12 field sites during the year-long measurement period. From the data, nucleation and growth rates of newly formed particles were determined for each environment. In a case of parallel ion and neutral cluster measurements, we could also estimate the relative contribution of ion-induced and neutral nucleation to the total particle formation. The formation rates of charged particles at 2 nm accounted for 1–30% of the corresponding total particle formation rates. As a significant new result, we found out that the total particle formation rate varied much more between the different sites than the formation rate of charged particles. This work presents, so far, the most comprehensive effort to experimentally characterize nucleation and growth of atmospheric molecular clusters and nanoparticles at ground-based observation sites on a continental scale.

  9. Characterization of particle deformation during compression measured by confocal laser scanning microscopy.

    Science.gov (United States)

    Guo, H X; Heinämäki, J; Yliruusi, J

    1999-09-20

    Direct compression of riboflavin sodium phosphate tablets was studied by confocal laser scanning microscopy (CLSM). The technique is non-invasive and generates three-dimensional (3D) images. Tablets of 1% riboflavin sodium phosphate with two grades of microcrystalline cellulose (MCC) were individually compressed at compression forces of 1.0 and 26.8 kN. The behaviour and deformation of drug particles on the upper and lower surfaces of the tablets were studied under compression forces. Even at the lower compression force, distinct recrystallized areas in the riboflavin sodium phosphate particles were observed in both Avicel PH-101 and Avicel PH-102 tablets. At the higher compression force, the recrystallization of riboflavin sodium phosphate was more extensive on the upper surface of the Avicel PH-102 tablet than the Avicel PH-101 tablet. The plastic deformation properties of both MCC grades reduced the fragmentation of riboflavin sodium phosphate particles. When compressed with MCC, riboflavin sodium phosphate behaved as a plastic material. The riboflavin sodium phosphate particles were more tightly bound on the upper surface of the tablet than on the lower surface, and this could also be clearly distinguished by CLSM. Drug deformation could not be visualized by other techniques. Confocal laser scanning microscopy provides valuable information on the internal mechanisms of direct compression of tablets.

  10. Contrast and decay of cathodoluminescence from phosphor particles in a scanning electron microscope

    Energy Technology Data Exchange (ETDEWEB)

    Engelsen, Daniel den; Harris, Paul G.; Ireland, Terry G., E-mail: terry.ireland@brunel.ac.uk; Fern, George R.; Silver, Jack

    2015-10-15

    Cathodoluminescence (CL) studies are reported on phosphors in a field emission scanning electron microscope (FESEM). ZnO: Zn and other luminescent powders manifest a bright ring around the periphery of the particles: this ring enhances the contrast. Additionally, particles resting on top of others are substantially brighter than underlying ones. These phenomena are explained in terms of the combined effects of electrons backscattered out of the particles, together with light absorption by the substrate. The contrast is found to be a function of the particle size and the energy of the primary electrons. Some phosphor materials exhibit a pronounced comet-like structure at high scan rates in a CL-image, because the particle continues to emit light after the electron beam has moved to a position without phosphor material. Image analysis has been used to study the loss of brightness along the tail and hence to determine the decay time of the materials. The effect of phosphor saturation on the determination of decay times by CL-microscopy was also investigated. - Highlights: • Contrast enhancement are observed in secondary electron and cathodoluminescent images of phosphor particles sitting on top of others. • Backscattered electrons largely explain the observed contrast enhancement. • After glow effects in CL-micrographs of phosphors enable the determination of decay times. • Phosphor saturation can be used to determine the decay time of individual spectral transitions.

  11. The LASS [Larger Aperture Superconducting Solenoid] spectrometer

    International Nuclear Information System (INIS)

    Aston, D.; Awaji, N.; Barnett, B.

    1986-04-01

    LASS is the acronym for the Large Aperture Superconducting Solenoid spectrometer which is located in an rf-separated hadron beam at the Stanford Linear Accelerator Center. This spectrometer was constructed in order to perform high statistics studies of multiparticle final states produced in hadron reactions. Such reactions are frequently characterized by events having complicated topologies and/or relatively high particle multiplicity. Their detailed study requires a spectrometer which can provide good resolution in momentum and position over almost the entire solid angle subtended by the production point. In addition, good final state particle identification must be available so that separation of the many kinematically-overlapping final states can be achieved. Precise analyses of the individual reaction channels require high statistics, so that the spectrometer must be capable of high data-taking rates in order that such samples can be acquired in a reasonable running time. Finally, the spectrometer must be complemented by a sophisticated off-line analysis package which efficiently finds tracks, recognizes and fits event topologies and correctly associates the available particle identification information. This, together with complicated programs which perform specific analysis tasks such as partial wave analysis, requires a great deal of software effort allied to a very large computing capacity. This paper describes the construction and performance of the LASS spectrometer, which is an attempt to realize the features just discussed. The configuration of the spectrometer corresponds to the data-taking on K + and K - interactions in hydrogen at 11 GeV/c which took place in 1981 and 1982. This constitutes a major upgrade of the configuration used to acquire lower statistics data on 11 GeV/c K - p interactions during 1977 and 1978, which is also described briefly

  12. The LASS (Larger Aperture Superconducting Solenoid) spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Aston, D.; Awaji, N.; Barnett, B.; Bienz, T.; Bierce, R.; Bird, F.; Bird, L.; Blockus, D.; Carnegie, R.K.; Chien, C.Y.

    1986-04-01

    LASS is the acronym for the Large Aperture Superconducting Solenoid spectrometer which is located in an rf-separated hadron beam at the Stanford Linear Accelerator Center. This spectrometer was constructed in order to perform high statistics studies of multiparticle final states produced in hadron reactions. Such reactions are frequently characterized by events having complicated topologies and/or relatively high particle multiplicity. Their detailed study requires a spectrometer which can provide good resolution in momentum and position over almost the entire solid angle subtended by the production point. In addition, good final state particle identification must be available so that separation of the many kinematically-overlapping final states can be achieved. Precise analyses of the individual reaction channels require high statistics, so that the spectrometer must be capable of high data-taking rates in order that such samples can be acquired in a reasonable running time. Finally, the spectrometer must be complemented by a sophisticated off-line analysis package which efficiently finds tracks, recognizes and fits event topologies and correctly associates the available particle identification information. This, together with complicated programs which perform specific analysis tasks such as partial wave analysis, requires a great deal of software effort allied to a very large computing capacity. This paper describes the construction and performance of the LASS spectrometer, which is an attempt to realize the features just discussed. The configuration of the spectrometer corresponds to the data-taking on K and K interactions in hydrogen at 11 GeV/c which took place in 1981 and 1982. This constitutes a major upgrade of the configuration used to acquire lower statistics data on 11 GeV/c K p interactions during 1977 and 1978, which is also described briefly.

  13. HISS spectrometer

    International Nuclear Information System (INIS)

    Greiner, D.E.

    1984-11-01

    This talk describes the Heavy Ion Spectrometer System (HISS) facility at the Lawrence Berkeley Laboratory's Bevalac. Three completed experiments and their results are illustrated. The second half of the talk is a detailed discussion of the response of drift chambers to heavy ions. The limitations of trajectory measurement over a large range in incident particle charge are presented

  14. Evaluation of the ROTAX spectrometer

    International Nuclear Information System (INIS)

    Tietze-Jaensch, H.; Schmidt, W.; Geick, R.

    1997-01-01

    After installation of the new-type rotating crystal analyser spectrometer ROTAX at ISIS, we report on practical experience and describe its current status. The rotating analyser technique works feasibly and reliably and provides an ultimate scan flexibility on a pulsed time-of-flight neutron spectrometer. The spinning analyser achieves a mulitplex advantage factor of ca. 50 without compromising the resolution of the instrument. Despite these instrument merits its individual beam position at ISIS has only an unsatisfactorily weak flux, thus hindering this instrument yet to become fully competitive with other high-performance neutron spectrometers based at high-flux reactors. However, we strongly recommend a ROTAX-type instrument to be emphasized when the instrumentation suite of the future European spallation source ESS will come under scrutiny. (orig.)

  15. Theory and optical design of x-ray echo spectrometers

    Science.gov (United States)

    Shvyd'ko, Yuri

    2017-08-01

    X-ray echo spectroscopy, a space-domain counterpart of neutron spin echo, is a recently proposed inelastic x-ray scattering (IXS) technique. X-ray echo spectroscopy relies on imaging IXS spectra and does not require x-ray monochromatization. Due to this, the echo-type IXS spectrometers are broadband, and thus have a potential to simultaneously provide dramatically increased signal strength, reduced measurement times, and higher resolution compared to the traditional narrow-band scanning-type IXS spectrometers. The theory of x-ray echo spectrometers presented earlier [Yu. Shvyd'ko, Phys. Rev. Lett. 116, 080801 (2016), 10.1103/PhysRevLett.116.080801] is developed here further with a focus on questions of practical importance, which could facilitate optical design and assessment of the feasibility and performance of the echo spectrometers. Among others, the following questions are addressed: spectral resolution, refocusing condition, echo spectrometer tolerances, refocusing condition adjustment, effective beam size on the sample, spectral window of imaging and scanning range, impact of the secondary source size on the spectral resolution, angular dispersive optics, focusing and collimating optics, and detector's spatial resolution. Examples of optical designs and characteristics of echo spectrometers with 1-meV and 0.1-meV resolutions are presented.

  16. Qualitative analysis of barium particles coated in small intestinal mucosa of rabbit by using scanning electron microscopy

    International Nuclear Information System (INIS)

    Lee, Yong Suk; Ha, Hyun Kwon; Lee, Yang Seob; Kim, Jae Kyun; Yoon, Seong Eon; Kim, Jung Hoon; Chung, Dong Jin; Auh, Yong Ho

    1998-01-01

    To qualitatively analysed barium coating status in the intestinal mucosa, we used scanning electron microscopy to observe barium particles coated in the small intestinal mucosa of rabbit, and we attempted to assess the relationship between electron microscopic findings and radiographic densities. Six different combination of barium and methylcellulose suspensions were infused into the resected small intestines of 15 rabbits. Barium powders were mixed with water to make 40% and 70% w/v barium solutions, and also mixed with 0.5% methylcellulose solutions were used as a double contrast agent. After the infusion of barium suspensions, a mammography unit was used to obtain radiographs of the small intestine, and their optical densities were measured by a densitometer. Thereafter, photographs of barium-coated small intestinal mucosa were obtained using a scanning electron microscope (x 8,000), and the number of barium particles in the unit area were measured. To compare the relationship between the electron microscopic findings and optical densities, statistical analysis using Spearman correlation was performed. This study shows that by using scanning electron microscopy, barium particles coated on the small intestinal mucosa can be qualitatively analysed. It also shows that the number of small barium particles measured by scanning electron microscopy is related to optical densities. (author). 14 refs., 2 figs

  17. Principle and analysis of a rotational motion Fourier transform infrared spectrometer

    Science.gov (United States)

    Cai, Qisheng; Min, Huang; Han, Wei; Liu, Yixuan; Qian, Lulu; Lu, Xiangning

    2017-09-01

    Fourier transform infrared spectroscopy is an important technique in studying molecular energy levels, analyzing material compositions, and environmental pollutants detection. A novel rotational motion Fourier transform infrared spectrometer with high stability and ultra-rapid scanning characteristics is proposed in this paper. The basic principle, the optical path difference (OPD) calculations, and some tolerance analysis are elaborated. The OPD of this spectrometer is obtained by the continuously rotational motion of a pair of parallel mirrors instead of the translational motion in traditional Michelson interferometer. Because of the rotational motion, it avoids the tilt problems occurred in the translational motion Michelson interferometer. There is a cosine function relationship between the OPD and the rotating angle of the parallel mirrors. An optical model is setup in non-sequential mode of the ZEMAX software, and the interferogram of a monochromatic light is simulated using ray tracing method. The simulated interferogram is consistent with the theoretically calculated interferogram. As the rotating mirrors are the only moving elements in this spectrometer, the parallelism of the rotating mirrors and the vibration during the scan are analyzed. The vibration of the parallel mirrors is the main error during the rotation. This high stability and ultra-rapid scanning Fourier transform infrared spectrometer is a suitable candidate for airborne and space-borne remote sensing spectrometer.

  18. Calibration of a Thomson parabola ion spectrometer and Fujifilm imaging plate detectors for protons, deuterons, and alpha particles.

    Science.gov (United States)

    Freeman, C G; Fiksel, G; Stoeckl, C; Sinenian, N; Canfield, M J; Graeper, G B; Lombardo, A T; Stillman, C R; Padalino, S J; Mileham, C; Sangster, T C; Frenje, J A

    2011-07-01

    A Thomson parabola ion spectrometer has been designed for use at the Multiterawatt (MTW) laser facility at the Laboratory for Laser Energetics (LLE) at the University of Rochester. This device uses parallel electric and magnetic fields to deflect particles of a given mass-to-charge ratio onto parabolic curves on the detector plane. Once calibrated, the position of the ions on the detector plane can be used to determine the particle energy. The position dispersion of both the electric and magnetic fields of the Thomson parabola was measured using monoenergetic proton and alpha particle beams from the SUNY Geneseo 1.7 MV tandem Pelletron accelerator. The sensitivity of Fujifilm BAS-TR imaging plates, used as a detector in the Thomson parabola, was also measured as a function of the incident particle energy over the range from 0.6 MeV to 3.4 MeV for protons and deuterons and from 0.9 MeV to 5.4 MeV for alpha particles. The device was used to measure the energy spectrum of laser-produced protons at MTW.

  19. Calibration of a Thomson parabola ion spectrometer and Fujifilm imaging plate detectors for protons, deuterons, and alpha particles

    Energy Technology Data Exchange (ETDEWEB)

    Freeman, C. G.; Canfield, M. J.; Graeper, G. B.; Lombardo, A. T.; Stillman, C. R.; Padalino, S. J. [Physics Department, SUNY Geneseo, Geneseo, New York 14454 (United States); Fiksel, G.; Stoeckl, C.; Mileham, C.; Sangster, T. C. [Laboratory for Laser Energetics, University of Rochester, Rochester, New York 14623 (United States); Sinenian, N.; Frenje, J. A. [Plasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States)

    2011-07-15

    A Thomson parabola ion spectrometer has been designed for use at the Multiterawatt (MTW) laser facility at the Laboratory for Laser Energetics (LLE) at University of Rochester. This device uses parallel electric and magnetic fields to deflect particles of a given mass-to-charge ratio onto parabolic curves on the detector plane. Once calibrated, the position of the ions on the detector plane can be used to determine the particle energy. The position dispersion of both the electric and magnetic fields of the Thomson parabola was measured using monoenergetic proton and alpha particle beams from the SUNY Geneseo 1.7 MV tandem Pelletron accelerator. The sensitivity of Fujifilm BAS-TR imaging plates, used as a detector in the Thomson parabola, was also measured as a function of the incident particle energy over the range from 0.6 MeV to 3.4 MeV for protons and deuterons and from 0.9 MeV to 5.4 MeV for alpha particles. The device was used to measure the energy spectrum of laser-produced protons at MTW.

  20. Small angle single arm spectrometer

    International Nuclear Information System (INIS)

    Chien, C.Y.

    1976-01-01

    A study is given of an experiment described in the 1975 Summer Study to review the adequacy of the apparatus for its physics goals, equipment needs, logistic needs, vacuum chambers, compatibility with other experiments and to summarize its impacts on ISABELLE. The spectrometer is designed to study single particle inclusive spectra near x = 1 with particle identification and good momentum resolution

  1. Advances in 4D treatment planning for scanned particle beam therapy - report of dedicated workshops

    NARCIS (Netherlands)

    Bert, Christoph; Graeff, Christian; Riboldi, Marco; Nill, Simeon; Baroni, Guido; Knopf, Antje-Christin

    2014-01-01

    We report on recent progress in the field of mobile tumor treatment with scanned particle beams, as discussed in the latest editions of the 4D treatment planning workshop. The workshop series started in 2009, with about 20 people from 4 research institutes involved, all actively working on particle

  2. A prototype experiment to study charmed particle production and decay using a Holographic High Resolution Hydrogen Chamber (HOLEBC) and the European Hybrid Spectrometer

    CERN Multimedia

    2002-01-01

    The high resolution hydrogen bubble chamber LEBC has already been used in experiments at the SPS to detect particles with lifetime $\\geq 5 \\times 10^{-13}$s (NA13 & NA16). \\\\\\\\For this experiment, a new version of LEBC called HOLEBC, has been constructed. This chamber and the NA26 version of the spectrometer have been used with classical optics in the NA27 experiment. A significant improvement in resolution was achieved ($\\simeq$ 20 microns compared with $\\simeq$ 40 $\\mu$m in LEBC) and hence a good sensitivity to all (known) charmed particle decays. The development of holographic recording techniques with HOLEBC is in progress. \\\\\\\\The prototype NA26 experiment is designed to evaluate the feasibility of the high sensitivity, high resolution holographic hydrogen bubble chamber technique and evaluate various possible charm selective triggers using the information from the spectrometer.

  3. 13C-TRIPLY Labeled Ethyl Cyanide Submillimeterwave Study with Lille's Fast Scan Dds-Based Spectrometer

    Science.gov (United States)

    Pienkina, A.; Motiyenko, R. A.; Margulès, L.; Müller, Holger S. P.; Guillemin, J.-C.

    2016-06-01

    This study of the 13C-triply labeled species of ethyl cyanide (CH_3CH_2CN) follows our recent work on the three 13C-doubly-labeled that allowed their detection in the line survey recently obtained with ALMA (EMoCA). The detection of isotopologues could improve the knowledge of the astrochemistry. The other goal is to clean the surveys from the lines of known molecules in order to detect new ones, this is especially important for the abundant complex organic molecules like ethyl cyanide. As in the case of the doubly substitued species, no spectroscopic studies exist up to now for 13CH_313CH_213CN, the first predictions were thus obtained from scaled ab initio calculations. The spectra were recorded and analyzed up to 1 THz. More than 5500 lines were fitted with quantum numbers J and K_a up to 95 and 25 respectively. The spectra were obtained with the new version of the Lille's solid state spectrometers. This new version used Direct Digital Synthesizer in order to speed up acquisition time. We constructed a spectrometer covering a decade, from 150 to 1500 GHz, it scans the full range in 24 hours with high sensitivity and accuracy. This work was supported by the CNES and the Action sur Projets de l'INSU, PCMI. This work was also done under ANR-13-BS05-0008-02 IMOLABS Margules, L.; et al. 2015, 69th International Symposium on Molecular Spectroscopy, RI06 Belloche, A.; et al. 2014, Science, 345, 1584

  4. Dark-field scanning confocal microscope for vertical particle tracks in nuclear emulsion

    International Nuclear Information System (INIS)

    Astakhov, A.Ya.; Batusov, Yu.A.; Soroko, L.M.; Tereshchenko, S.V.; Tereshchenko, V.V.

    1999-01-01

    The principle of the DArk-FIeld Scanning CONfocal (DAFISCON) microscope for selective observation of the vertical particle tracks in nuclear emulsion is described. The construction of the DAFISCON microscope, built on the basis of the 2D measurement microscope, is described. The results of the experimental testing of the DAFISCON microscope, accomplished at high density of the vertical particle tracks, are presented. The 2D plot and the 1D plot of the CCD dark-field image are given. The spatial resolution of our microscope can be increased by using the objective with higher aperture

  5. In-line monitoring of effluents from HTGR fuel particle preparation processes using a time-of-flight mass spectrometer

    International Nuclear Information System (INIS)

    Lee, D.A.; Costanzo, D.A.; Stinton, D.P.; Carpenter, J.A.; Rainey, W.T. Jr.; Canada, D.C.; Carter, J.A.

    1976-08-01

    The carbonization, conversion, and coating processes in the manufacture of HTGR fuel particles have been studied with the use of a time-of-flight mass spectrometer. Non-condensable effluents from these fluidized-bed processes have been monitored continuously from the beginning to the end of the process. The processes which have been monitored are these: uranium-loaded ion exchange resin carbonization, the carbothermic reduction of UO 2 to UC 2 , buffer and low temperature isotropic pyrocarbon coatings of fuel kernels, SiC coating of the kernels, and high-temperature particle annealing. Changes in concentrations of significant molecules with time and temperature have been useful in the interpretation of reaction mechanisms and optimization of process procedures

  6. Forensic Scanning Electron Microscope

    Science.gov (United States)

    Keeley, R. H.

    1983-03-01

    The scanning electron microscope equipped with an x-ray spectrometer is a versatile instrument which has many uses in the investigation of crime and preparation of scientific evidence for the courts. Major applications include microscopy and analysis of very small fragments of paint, glass and other materials which may link an individual with a scene of crime, identification of firearms residues and examination of questioned documents. Although simultaneous observation and chemical analysis of the sample is the most important feature of the instrument, other modes of operation such as cathodoluminescence spectrometry, backscattered electron imaging and direct x-ray excitation are also exploited. Marks on two bullets or cartridge cases can be compared directly by sequential scanning with a single beam or electronic linkage of two instruments. Particles of primer residue deposited on the skin and clothing when a gun is fired can be collected on adhesive tape and identified by their morphology and elemental composition. It is also possible to differentiate between the primer residues of different types of ammunition. Bullets may be identified from the small fragments left behind as they pass through the body tissues. In the examination of questioned documents the scanning electron microscope is used to establish the order in which two intersecting ink lines were written and to detect traces of chemical markers added to the security inks on official documents.

  7. Automation of a thermal ionisation mass spectrometer

    International Nuclear Information System (INIS)

    Pamula, A.; Leuca, M.; Albert, S.; Benta, Adriana

    2001-01-01

    A thermal ionization mass spectrometer was upgraded in order to be monitored by a PC. A PC-LMP-16 National Instruments data acquisition board was used for the ion current channel and the Hall signal channel. A dedicated interface was built to allow commands from the computer to the current supply of the analyzing magnet and to the high voltage unit of the mass spectrometer. A software application was worked out to perform the adjustment of the spectrometer, magnetic scanning and mass spectra acquisition, data processing and isotope ratio determination. The apparatus is used for isotope ratio 235 U/ 238 U determination near the natural abundance. A peak jumping technique is applied to choose between the 235 U and 238 U signal, by switching the high voltage applied to the ion source between two preset values. This avoids the delay between the acquisition of the peaks of interest, a delay that would appear in the case of a 'pure' magnetic scanning. Corrections are applied for the mass discrimination effects and a statistical treatment of the data is achieved. (authors)

  8. AMS, a particle spectrometer in space

    International Nuclear Information System (INIS)

    Buenerd, M.; Ohlsson-Malek, F.; Ren, Z.L.; Santos, D.; Thuillier, T.

    1997-01-01

    The Alpha Magnetic Spectrometer (AMS) is a detector designed for extraterrestrial study of anti-matter, matter and dark matter. A precursor flight and on the STS-91 flight of the shuttle is planned to take place on May 1998. AMS will be installed on the International Space Station in January 2002 where it will be operated next, for three to five years. The contributions of the ISN to the project on the shuttle (aerogel threshold Cherenkov counter) as well as the steps to build a RICH detector for AMS on the ISSA are explained here below. (authors)

  9. Characterizing high-energy-formed particulates with the scanning electron microscope/energy dispersive spectrometer system. Progress report, March--September 1977

    International Nuclear Information System (INIS)

    Casey, A.W.; Biermann, A.H.

    1977-01-01

    A method is being sought that will allow the differentiation between particulates formed in implosions and particulates formed in explosions. The scanning electron microscope (SEM) and energy dispersive x-ray analysis (EDS) were used to measure and compare particle size, shape, surface morphology, and composition. Implosion and explosion detonations yielded spherical, smooth particles within the same size range. Although the particle size, shape, and morphology were the same for comparable samples of different detonation type, there were distinct differences in composition. It is not certain whether differences in composition reflect differences in device components or differences in the nature of the detonation

  10. Three-dimensional three-component particle velocimetry for microscale flows using volumetric scanning

    International Nuclear Information System (INIS)

    Klein, S A; Moran, J L; Posner, J D; Frakes, D H

    2012-01-01

    We present a diagnostic platform for measuring three-dimensional three-component (3D3C) velocity fields in microscopic volumes. The imaging system uses high-speed Nipkow spinning disk confocal microscopy. Confocal microscopy provides optical sectioning using pinhole spatial filtering which rejects light originating from out-of-focus objects. The system accomplishes volumetric scanning by rapid translation of the high numerical aperture objective using a piezo objective positioner. The motion of fluorescent microspheres is quantified using 3D3C super resolution particle-imaging velocimetry with instantaneous spatial resolutions of the order of 5 µm or less in all three dimensions. We examine 3D3C flow in a PDMS microchannel with an expanding section at 3D acquisition rates of 30 Hz, and find strong agreement with a computational model. Equations from the PIV and PTV literature adapted for a scanning objective provide estimates of maximum measurable velocity. The technique allows for isosurface visualization of 3D particle motion and robust high spatial resolution velocity measurements without requiring a calibration step or reconstruction algorithms. (paper)

  11. Mid infrared MEMS FTIR spectrometer

    Science.gov (United States)

    Erfan, Mazen; Sabry, Yasser M.; Mortada, Bassem; Sharaf, Khaled; Khalil, Diaa

    2016-03-01

    In this work we report, for the first time to the best of our knowledge, a bulk-micromachined wideband MEMS-based spectrometer covering both the NIR and the MIR ranges and working from 1200 nm to 4800 nm. The core engine of the spectrometer is a scanning Michelson interferometer micro-fabricated using deep reactive ion etching (DRIE) technology. The spectrum is obtained using the Fourier Transform techniques that allows covering a very wide spectral range limited by the detector responsivity. The moving mirror of the interferometer is driven by a relatively large stroke electrostatic comb-drive actuator. Zirconium fluoride (ZrF4) multimode optical fibers are used to connect light between the white light source and the interferometer input, as well as the interferometer output to a PbSe photoconductive detector. The recorded signal-to-noise ratio is 25 dB at the wavelength of 3350 nm. The spectrometer is successfully used in measuring the absorption spectra of methylene chloride, quartz glass and polystyrene film. The presented solution provides a low cost method for producing miniaturized spectrometers in the near-/mid-infrared.

  12. Scanning tomographic particle image velocimetry applied to a turbulent jet

    KAUST Repository

    Casey, T. A.

    2013-02-21

    We introduce a modified tomographic PIV technique using four high-speed video cameras and a scanning pulsed laser-volume. By rapidly illuminating adjacent subvolumes onto separate video frames, we can resolve a larger total volume of velocity vectors, while retaining good spatial resolution. We demonstrate this technique by performing time-resolved measurements of the turbulent structure of a round jet, using up to 9 adjacent volume slices. In essence this technique resolves more velocity planes in the depth direction by maintaining optimal particle image density and limiting the number of ghost particles. The total measurement volumes contain between 1 ×106 and 3 ×106 velocity vectors calculated from up to 1500 reconstructed depthwise image planes, showing time-resolved evolution of the large-scale vortical structures for a turbulent jet of Re up to 10 000.

  13. Development and characterization of a single particle laser ablation mass spectrometer (SPLAM for organic aerosol studies

    Directory of Open Access Journals (Sweden)

    F. Gaie-Levrel

    2012-01-01

    Full Text Available A single particle instrument was developed for real-time analysis of organic aerosol. This instrument, named Single Particle Laser Ablation Mass Spectrometry (SPLAM, samples particles using an aerodynamic lens system for which the theoretical performances were calculated. At the outlet of this system, particle detection and sizing are realized by using two continuous diode lasers operating at λ = 403 nm. Polystyrene Latex (PSL, sodium chloride (NaCl and dioctylphtalate (DOP particles were used to characterize and calibrate optical detection of SPLAM. The optical detection limit (DL and detection efficiency (DE were determined using size-selected DOP particles. The DE ranges from 0.1 to 90% for 100 and 350 nm DOP particles respectively and the SPLAM instrument is able to detect and size-resolve particles as small as 110–120 nm. During optical detection, particle scattered light from the two diode lasers, is detected by two photomultipliers and the detected signals are used to trigger UV excimer laser (λ = 248 nm used for one-step laser desorption ionization (LDI of individual aerosol particles. The formed ions are analyzed by a 1 m linear time-of-flight mass spectrometer in order to access to the chemical composition of individual particles. The TOF-MS detection limit for gaseous aromatic compounds was determined to be 0.85 × 10−15 kg (∼4 × 103 molecules. DOP particles were also used to test the overall operation of the instrument. The analysis of a secondary organic aerosol, formed in a smog chamber by the ozonolysis of indene, is presented as a first application of the instrument. Single particle mass spectra were obtained with an effective hit rate of 8%. Some of these mass spectra were found to be very different from one particle to another possibly reflecting chemical differences within the investigated indene SOA particles. Our study shows that an exhaustive statistical analysis, over hundreds of particles

  14. Current instrument status of the Airborne Visible/Infrared Imaging Spectrometer (AVIRIS)

    Science.gov (United States)

    Eastwood, Michael L.; Sarture, Charles M.; Chrien, Thomas G.; Green, Robert O.; Porter, Wallace M.

    1991-01-01

    An upgraded version of AVIRIS, an airborne imaging spectrometer based on a whiskbroom-type scanner coupled via optical fibers to four dispersive spectrometers, that has been in operation since 1987 is described. Emphasis is placed on specific AVIRIS subsystems including foreoptics, fiber optics, and an in-flight reference source; spectrometers and detector dewars; a scan drive mechanism; a signal chain; digital electronics; a tape recorder; calibration systems; and ground support requirements.

  15. Multichannel Dynamic Fourier-Transform IR Spectrometer

    Science.gov (United States)

    Balashov, A. A.; Vaguine, V. A.; Golyak, Il. S.; Morozov, A. N.; Khorokhorin, A. I.

    2017-09-01

    A design of a multichannel continuous scan Fourier-transform IR spectrometer for simultaneous recording and analysis of the spectral characteristics of several objects is proposed. For implementing the design, a multi-probe fiber is used, constructed from several optical fibers connected into a single optical connector and attached at the output of the interferometer. The Fourier-transform spectrometer is used as a signal modulator. Each fiber is individually mated with an investigated sample and a dedicated radiation detector. For the developed system, the radiation intensity of the spectrometer is calculated from the condition of the minimum spectral resolution and parameters of the optical fibers. Using the proposed design, emission spectra of a gas-discharge neon lamp have been recorded using a single fiber 1 mm in diameter with a numerical aperture NA = 0.22.

  16. Real-Time Measurements of Gas/Particle Partitioning of Semivolatile Organic Compounds into Different Probe Particles in a Teflon Chamber

    Science.gov (United States)

    Liu, X.; Day, D. A.; Ziemann, P. J.; Krechmer, J. E.; Jimenez, J. L.

    2017-12-01

    The partitioning of semivolatile organic compounds (SVOCs) into and out of particles plays an essential role in secondary organic aerosol (SOA) formation and evolution. Most atmospheric models treat the gas/particle partitioning as an equilibrium between bulk gas and particle phases, despite potential kinetic limitations and differences in thermodynamics as a function of SOA and pre-existing OA composition. This study directly measures the partitioning of oxidized compounds in a Teflon chamber in the presence of single component seeds of different phases and polarities, including oleic acid, squalane, dioctyl sebacate, pentaethylene glycol, dry/wet ammonium sulfate, and dry/wet sucrose. The oxidized compounds are generated by a fast OH oxidation of a series of alkanols under high nitric oxide conditions. The observed SOA mass enhancements are highest with oleic acid, and lowest with wet ammonium sulfate and sucrose. A chemical ionization mass spectrometer (CIMS) was used to measure the decay of gas-phase organic nitrates, which reflects uptake by particles and chamber walls. We observed clear changes in equilibrium timescales with varying seed concentrations and in equilibrium gas-phase concentrations across different seeds. In general, the gas evolution can be reproduced by a kinetic box model that considers partitioning and evaporation with particles and chamber walls, except for the wet sucrose system. The accommodation coefficient and saturation mass concentration of each species in the presence of each seed are derived using the model. The changes in particle size distributions and composition monitored by a scanning mobility particle sizer (SMPS) and a high-resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS) are investigated to probe the SOA formation mechanism. Based on these results, the applicability of partitioning theory to these systems and the relevant quantitative parameters, including the dependencies on seed particle composition, will

  17. Characterization of particulate matter emissions from on-road gasoline and diesel vehicles using a soot particle aerosol mass spectrometer

    OpenAIRE

    Dallmann, T. R.; Onasch, T. B.; Kirchstetter, T. W.; Worton, D. R.; Fortner, E. C.; Herndon, S. C.; Wood, E. C.; Franklin, J. P.; Worsnop, D. R.; Goldstein, A. H.; Harley, R. A.

    2014-01-01

    Particulate matter (PM) emissions were measured in July 2010 from on-road motor vehicles driving through a highway tunnel in the San Francisco Bay area. A soot particle aerosol mass spectrometer (SP-AMS) was used to measure the chemical composition of PM emitted by gasoline and diesel vehicles at high time resolution. Organic aerosol (OA) and black carbon (BC) concentrations were measured during various time periods that had different levels of diesel influence, as well as d...

  18. Scanned beams of high-energy charged particles and features of their collimation

    International Nuclear Information System (INIS)

    Zor'ko, K.I.; Kudoyarov, M.F.; Matyukov, A.V.; Mukhin, S.A.; Patrova, M.Ya.

    2007-01-01

    The coordinate distributions of the accelerated charged particle flux density that are simultaneously formed by sinusoidal scanning and collimation are analyzed. Under certain formation conditions, the edge portions of these distributions are shown to take a two-humped shape. The experimental data obtained are in good agreement with the calculation. Recommendations are made about practical use of these beams in view of the above effects [ru

  19. Spectrometer of Cherenkov radiation rings with hodoscopic photomultipliers

    International Nuclear Information System (INIS)

    Abramov, V.V.; Alekseev, A.V.; Baldin, B.Yu.

    1983-01-01

    Characteristics of SKOCH Cherenkov radiation ring spectrometer intended for identification of π- and K-mesons and protons in a wide divergent beam in the pulse range of 5.5-30 GeV/s are investigated. The spectrometer detecting system is based on using the hodoscopic photoelectron multipliers (HPEM). The HPEM specific feature is that they have an extended cathode and permit to determine the coordinate of an incident photon by measuring the time of photoelectron drift to a dinode system. The spectrometer has been tested at the FODS facility in the secondary particle beam with angular divergence equal to 16x6 mrad and aperture of 400x200 mm in the pulse range of 6-20 GeV/s. The range of Cherenkov radiation angle detection is 40-100 mrad which corresponds to the particle velocity range of 0.996-1. The angular and radial aperture is 30 mrad, the diameter is 420 mm. The obtained velocity resolution is 6x10 -5

  20. Laser ablation aerosol particle time-of-flight mass spectrometer (LAAPTOF): performance, reference spectra and classification of atmospheric samples

    Science.gov (United States)

    Shen, Xiaoli; Ramisetty, Ramakrishna; Mohr, Claudia; Huang, Wei; Leisner, Thomas; Saathoff, Harald

    2018-04-01

    The laser ablation aerosol particle time-of-flight mass spectrometer (LAAPTOF, AeroMegt GmbH) is able to identify the chemical composition and mixing state of individual aerosol particles, and thus is a tool for elucidating their impacts on human health, visibility, ecosystem, and climate. The overall detection efficiency (ODE) of the instrument we use was determined to range from ˜ (0.01 ± 0.01) to ˜ (4.23 ± 2.36) % for polystyrene latex (PSL) in the size range of 200 to 2000 nm, ˜ (0.44 ± 0.19) to ˜ (6.57 ± 2.38) % for ammonium nitrate (NH4NO3), and ˜ (0.14 ± 0.02) to ˜ (1.46 ± 0.08) % for sodium chloride (NaCl) particles in the size range of 300 to 1000 nm. Reference mass spectra of 32 different particle types relevant for atmospheric aerosol (e.g. pure compounds NH4NO3, K2SO4, NaCl, oxalic acid, pinic acid, and pinonic acid; internal mixtures of e.g. salts, secondary organic aerosol, and metallic core-organic shell particles; more complex particles such as soot and dust particles) were determined. Our results show that internally mixed aerosol particles can result in spectra with new clusters of ions, rather than simply a combination of the spectra from the single components. An exemplary 1-day ambient data set was analysed by both classical fuzzy clustering and a reference-spectra-based classification method. Resulting identified particle types were generally well correlated. We show how a combination of both methods can greatly improve the interpretation of single-particle data in field measurements.

  1. The new Athena alpha particle X-ray spectrometer for the Mars Exploration Rovers

    Science.gov (United States)

    Rieder, R.; Gellert, R.; Brückner, J.; Klingelhöfer, G.; Dreibus, G.; Yen, A.; Squyres, S. W.

    2003-11-01

    The new alpha particle X-ray spectrometer (APXS) is part of the Athena payload of the two Mars Exploration Rovers (MER). The APXS sensor head is attached to the turret of the instrument deployment device (IDD) of the rover. The APXS is a very light-weight instrument for determining the major and minor elemental composition of Martian soils, rocks, and other geological materials at the MER landing sites. The sensor head has simply to be docked by the IDD on the surface of the selected sample. X-ray radiation, excited by alpha particles and X rays of the radioactive sources, is recorded by a high-resolution X-ray detector. The X-ray spectra show elements starting from sodium up to yttrium, depending on their concentrations. The backscattered alpha spectra, measured by a ring of detectors, provide additional data on carbon and oxygen. By means of a proper calibration, the elemental concentrations are derived. Together with data from the two other Athena instruments mounted on the IDD, the samples under investigation can be fully characterized. Key APXS objectives are the determination of the chemistry of crustal rocks and soils and the examination of water-related deposits, sediments, or evaporates. Using the rock abrasion tool attached to the IDD, issues of weathering can be addressed by measuring natural and abraded surfaces of rocks.

  2. Project and construction of a spectrometer for alpha particles using surface barrier detectors

    International Nuclear Information System (INIS)

    Terini, R.A.

    1986-01-01

    The project, construction, tests and some applications of a system for alpha and beta spectrometry, using surface barrier detector are described. The device includes a solid state detector ORTEC-Series F coupled to a system for amplifying the charges produced by passage of an ionizing particle through the detector. The amplifying system is composed by a charge sensitive pre-amplifier, which employs an operational amplifier CA 3140, and a low noise linear amplifier, which is based on the operational amplifiers CA 3140 and LM 301. The pre-amplifier stage input impedance is on the order of TΩ and produces output pulses which heights are proportional to total charge produced by passage of particle through the detector sensitive volume. The main advantage to use charge sensitive system lies in obtention of independent pulse heights of the distributed capacity of connecting cable between the detector and the pre-amplifier. The total system amplification ca reach a maximum of 50.000 in the linear region. Pulses are analysed in a multichannel system ORTEC, model 6240. The amplifier system is easily constructed and low cost using components available in the national market, and it can be employed with ionization chambers, proportional counters, scitillation counters and semiconductor detectors. The results of spectrometer application for alpha spectrometry of AM 241 source were compared to systems made with imported stages. (Author) [pt

  3. Development, characterization and application of compact spectrometers based on MEMS with in-plane capacitive drives

    Science.gov (United States)

    Kenda, A.; Kraft, M.; Tortschanoff, A.; Scherf, Werner; Sandner, T.; Schenk, Harald; Luettjohann, Stephan; Simon, A.

    2014-05-01

    With a trend towards the use of spectroscopic systems in various fields of science and industry, there is an increasing demand for compact spectrometers. For UV/VIS to the shortwave near-infrared spectral range, compact hand-held polychromator type devices are widely used and have replaced larger conventional instruments in many applications. Still, for longer wavelengths this type of compact spectrometers is lacking suitable and affordable detector arrays. In perennial development Carinthian Tech Research AG together with the Fraunhofer Institute for Photonic Microsystems endeavor to close this gap by developing spectrometer systems based on photonic MEMS. Here, we review on two different spectrometer developments, a scanning grating spectrometer working in the NIR and a FT-spectrometer accessing the mid-IR range up to 14 μm. Both systems are using photonic MEMS devices actuated by in-plane comb drive structures. This principle allows for high mechanical amplitudes at low driving voltages but results in gratings respectively mirrors oscillating harmonically. Both systems feature special MEMS structures as well as aspects in terms of system integration which shall tease out the best possible overall performance on the basis of this technology. However, the advantages of MEMS as enabling technology for high scanning speed, miniaturization, energy efficiency, etc. are pointed out. Whereas the scanning grating spectrometer has already evolved to a product for the point of sale analysis of traditional Chinese medicine products, the purpose of the FT-spectrometer as presented is to demonstrate what is achievable in terms of performance. Current developments topics address MEMS packaging issues towards long term stability, further miniaturization and usability.

  4. A multi-analyzer crystal spectrometer (MAX) for pulsed neutron sources

    International Nuclear Information System (INIS)

    Tajima, K.; Ishikawa, Y.; Kanai, K.; Windsor, C.G.; Tomiyoshi, S.

    1982-03-01

    The paper describes the principle and initial performance of a multi-analyzer crystal spectrometer (MAX) recently installed at the KENS spallation neutron source at Tsukuba. The spectrometer is able to make time of flight scans along a desired direction in reciprocal space, covering a wide range of the energy transfers corresponding to the fifteen analyzer crystals. The constant Q or constant E modes of operation can be performed. The spectrometer is particularly suited for studying collective excitations such as phonons and magnons to high energy transfers using single crystal samples. (author)

  5. Customized altitude-azimuth mount for a raster-scanning Fourier transform spectrometer

    Science.gov (United States)

    Durrenberger, Jed E.; Gutman, William M.; Gammill, Troy D.; Grover, Dennis H.

    1996-10-01

    Applications of the Army Research Laboratory Mobile Atmospheric Spectrometer Remote Sensing Rover required development of a customized computer-controlled mount to satisfy a variety of requirements within a limited budget. The payload was designed to operate atop a military electronics shelter mounted on a 4-wheel drive truck to be above most atmospheric ground turbulence. Pointing orientation in altitude is limited by constraints imposed by use of a liquid nitrogen detector Dewar in the spectrometer. Stepper motor drives and control system are compatible with existing custom software used with other instrumentation for controlled incremental raster stepping. The altitude axis passes close to the center of gravity of the complete payload to minimize load eccentricity and drive torque requirements. Dovetail fixture mounting enables quick service and fine adjustment of balance to minimize stepper/gearbox drive backlash through the limited orientation range in altitude. Initial applications to characterization of remote gas plumes have been successful.

  6. Photoacoustic Soot Spectrometer (PASS) Instrument Handbook

    Energy Technology Data Exchange (ETDEWEB)

    Dubey, M [Los Alamos National Laboratory; Springston, S [Brookhaven National Laboratory; Koontz, A [Pacific Northwest National Laboratory; Aiken, A [Los Alamos National Laboratory

    2013-01-17

    The photoacoustic soot spectrometer (PASS) measures light absorption by aerosol particles. As the particles pass through a laser beam, the absorbed energy heats the particles and in turn the surrounding air, which sets off a pressure wave that can be detected by a microphone. The PASS instruments deployed by ARM can also simultaneously measure the scattered laser light at three wavelengths and therefore provide a direct measure of the single-scattering albedo. The Operator Manual for the PASS-3100 is included here with the permission of Droplet Measurement Technologies, the instrument’s manufacturer.

  7. BIS-2 spectrometer for search and investigation of narrow resonances

    International Nuclear Information System (INIS)

    Aleev, A.N.; Aref'ev, V.A.; Balandin, V.P.

    1989-01-01

    The configuration and main characteristics of the BIS-2 spectrometer are described. The spectrometer was intended to search for and to investigate charmed particles and narrow resonances produced in neutron-nucleus interactions. It was placed on a neutron beam of the Serpukhov accelerator. The Monte-Carlo simulated and experimentally measured characteristics of individual elements and the spectrometer as a whole are described. A brief review of the principal results based on the analysis of more than 10 7 neutron-nucleus interactions registered by means of the BIS-2 spectrometer is given. 34 refs.; 8 figs.; 5 tabs

  8. Chemical characterization of individual particles (PM10) from ambient air in Guiyang City, China

    International Nuclear Information System (INIS)

    Xie, R.K.; Seip, H.M.; Leinum, J.R.; Winje, T.; Xiao, J.S.

    2005-01-01

    PM 10 samples were collected during 5 days in Guiyang, China in July 2003. A total of about 2300 particles was analyzed by an automated Scanning Electron Microscope with Energy-Dispersive Spectrometer (SEM-EDS). Hierarchical cluster analysis (HCA) was used to identify different particle types that occurred in the aerosol. Seventeen particle types were identified and presented in the order of decreasing number abundance as: silicomanganese slag, soil and fly ash, coal burning, silicomanganese, quartz, syngenite, S-bearing iron, calcium rich, gypsum, sphalerite, dolomite, iron, alloy, lead sulfate, zinc rich, sulfur-rich particles and aluminum manufacturing dust. The majority of the particles in the studied size range are of anthropogenic origin, especially from metallurgical industry. The study illustrates the complexity of particle pollution in air of an industrial Chinese city and the results should be useful in planning mitigation measures

  9. Intermediate PT jet spectrometers

    International Nuclear Information System (INIS)

    Gutay, L.J.; Koltick, D.; Hauptman, J.; Stork, D.; Theodosiou, G.

    1988-01-01

    A design is presented for a limited solid angle, high resolution double arm spectrometer at 90 degree to the begin, with a vertex detector and particle identification in both arms. The jet arm is designed to accept a complete jet, and identify its substructure of sub-jets, hadrons, and leptons. The particle arm would measure e,π,K,p ratios for P T 0 to the beam for the purpose of tagging Higgs production by boson fusion, 1 gauge boson (WW, ZZ, and WZ) scattering 2 L, and other processes involving the interactions of virtual gauge bosons

  10. Bragg rotor spectrometer for tokamak diagnostics

    International Nuclear Information System (INIS)

    Barnsley, R.; Evans, K.D.; Peacock, N.J.

    1986-01-01

    This paper discusses high thru'put broad band (1-24 angstrom) x-ray spectrometer having absolute calibration for wavelength and intensity and demonstrated on the DITE tokamak. This instrument has a self-contained vacuum system which allows full spatial scans of the DITE plasma. Data acquisition and drive mechanism for the rotor and filter selection are operated remotely from a SADA. Results are presented of fast spectral surveys and λ-lock time-evolution of impurity emission during neutral beam injection. Spatial scans of the absolute impurity concentrations are derived

  11. Laser ablation aerosol particle time-of-flight mass spectrometer (LAAPTOF: performance, reference spectra and classification of atmospheric samples

    Directory of Open Access Journals (Sweden)

    X. Shen

    2018-04-01

    Full Text Available The laser ablation aerosol particle time-of-flight mass spectrometer (LAAPTOF, AeroMegt GmbH is able to identify the chemical composition and mixing state of individual aerosol particles, and thus is a tool for elucidating their impacts on human health, visibility, ecosystem, and climate. The overall detection efficiency (ODE of the instrument we use was determined to range from  ∼  (0.01 ± 0.01 to  ∼  (4.23 ± 2.36 % for polystyrene latex (PSL in the size range of 200 to 2000 nm,  ∼  (0.44 ± 0.19 to  ∼  (6.57 ± 2.38 % for ammonium nitrate (NH4NO3, and  ∼  (0.14 ± 0.02 to  ∼  (1.46 ± 0.08 % for sodium chloride (NaCl particles in the size range of 300 to 1000 nm. Reference mass spectra of 32 different particle types relevant for atmospheric aerosol (e.g. pure compounds NH4NO3, K2SO4, NaCl, oxalic acid, pinic acid, and pinonic acid; internal mixtures of e.g. salts, secondary organic aerosol, and metallic core–organic shell particles; more complex particles such as soot and dust particles were determined. Our results show that internally mixed aerosol particles can result in spectra with new clusters of ions, rather than simply a combination of the spectra from the single components. An exemplary 1-day ambient data set was analysed by both classical fuzzy clustering and a reference-spectra-based classification method. Resulting identified particle types were generally well correlated. We show how a combination of both methods can greatly improve the interpretation of single-particle data in field measurements.

  12. Correlative scanning-transmission electron microscopy reveals that a chimeric flavivirus is released as individual particles in secretory vesicles.

    Directory of Open Access Journals (Sweden)

    Julien Burlaud-Gaillard

    Full Text Available The intracellular morphogenesis of flaviviruses has been well described, but flavivirus release from the host cell remains poorly documented. We took advantage of the optimized production of an attenuated chimeric yellow fever/dengue virus for vaccine purposes to study this phenomenon by microscopic approaches. Scanning electron microscopy (SEM showed the release of numerous viral particles at the cell surface through a short-lived process. For transmission electron microscopy (TEM studies of the intracellular ultrastructure of the small number of cells releasing viral particles at a given time, we developed a new correlative microscopy method: CSEMTEM (for correlative scanning electron microscopy - transmission electron microscopy. CSEMTEM analysis suggested that chimeric flavivirus particles were released as individual particles, in small exocytosis vesicles, via a regulated secretory pathway. Our morphological findings provide new insight into interactions between flaviviruses and cells and demonstrate that CSEMTEM is a useful new method, complementary to SEM observations of biological events by intracellular TEM investigations.

  13. Conceptual design of the Radial Gamma Ray Spectrometers system for α particle and runaway electron measurements at ITER

    DEFF Research Database (Denmark)

    Nocente, Massimo; Tardocchi, Marco; Barnsley, Robin

    2017-01-01

    We here present the principles and main physics capabilities behind the design of the radial gamma ray spectrometers (RGRS) system for alpha particle and runaway electron measurements at ITER. The diagnostic benefits from recent advances in gamma-ray spectrometry for tokamak plasmas and combines...... the measurements sensitive to α particles at characteristic resonant energies and to possible anisotropies of their slowing down distribution function. An independent assessment of the neutron rate by gamma-ray emission is also feasible. In case of runaway electrons born in disruptions with a typical duration...... of 100ms, a time resolution of at least 10ms for runaway electron studies can be achieved depending on the scenario and down to a current of 40 kA by use of external gas injection. We find that the bremsstrahlung spectrum in the MeV range from confined runaways is sensitive to the electron velocity space...

  14. [Near infrared distance sensing method for Chang'e-3 alpha particle X-ray spectrometer].

    Science.gov (United States)

    Liang, Xiao-Hua; Wu, Ming-Ye; Wang, Huan-Yu; Peng, Wen-Xi; Zhang, Cheng-Mo; Cui, Xing-Zhu; Wang, Jin-Zhou; Zhang, Jia-Yu; Yang, Jia-Wei; Fan, Rui-Rui; Gao, Min; Liu, Ya-Qing; Zhang, Fei; Dong, Yi-Fan; Guo, Dong-Ya

    2013-05-01

    Alpha particle X-ray spectrometer (APXS) is one of the payloads of Chang'E-3 lunar rover, the scientific objective of which is in-situ observation and off-line analysis of lunar regolith and rock. Distance measurement is one of the important functions for APXS to perform effective detection on the moon. The present paper will first give a brief introduction to APXS, and then analyze the specific requirements and constraints to realize distance measurement, at last present a new near infrared distance sensing algorithm by using the inflection point of response curve. The theoretical analysis and the experiment results verify the feasibility of this algorithm. Although the theoretical analysis shows that this method is not sensitive to the operating temperature and reflectance of the lunar surface, the solar infrared radiant intensity may make photosensor saturation. The solutions are reducing the gain of device and avoiding direct exposure to sun light.

  15. Exploratory study for a solid-state charged-particle spectrometer inside the celsius ring: α + 1H reactions at 1.7 and 2.2 GeV/c

    International Nuclear Information System (INIS)

    Bargholtz, C.; Fransson, K.; Holmberg, L.; Lindh, K.; Sandberg, L.; Tegner, P.E.; Thoerngren-Engblom, P.; Vojdani, D.

    1991-08-01

    Charged particles emitted in the extreme forward direction can be detected in a particle telescope mounted inside the CELSIUS ring in one of the dipole magnets following the target. Results of a test with a plastic scintillator telescope are reported for α + H reactions at 1.7 and 2.2 GeV/c. The results are consistent with ray-trace calculations. Contributions in the spectrometer from back-ground reactions and scattering in the beam tube are small. (au)

  16. Design of a preamplifier for an alpha particles spectrometer; Diseno de un preamplificador para un espectrometro de particulas alfa

    Energy Technology Data Exchange (ETDEWEB)

    Murillo O, R.; Hernandez D, V. M.; Chacon R, A.; Vega C, H. R., E-mail: fermineutron@yahoo.co [Universidad Autonoma de Zacatecas, Unidades Academicas de Estudios Nucleares e Ingenieria Electrica, Calle Cipres No. 10, Fracc. La Penuela, 98068 Zacatecas (Mexico)

    2010-09-15

    To detect radiation diverse detector types are used, when these are alpha particles proportional type detectors are used, semiconductor, of scintillation or traces. In this work the design results, the construction and the first tests of a spectrometer (preamplifier) are presented for alpha particles that was designed starting from a Pin type photodiode. The system was designed and simulated with a program for electronic circuits. With the results of the simulation phase was constructed the electronics that is coupled to a spectroscopic amplifier and a multichannel analyzer. The total of the system is evaluated analyzing its performance before a triple source of alphas and that they are produced by two smoke detectors of domestic use. Of the tests phase we find that the system allows to obtain in a multichannel, the pulses height spectrum, with which we calibrate the system. (Author)

  17. Photoelectron spectrometer for attosecond spectroscopy of liquids and gases

    Energy Technology Data Exchange (ETDEWEB)

    Jordan, I.; Huppert, M.; Wörner, H. J., E-mail: hwoerner@ethz.ch [Laboratory of Physical Chemistry, ETH Zurich, Vladimir-Prelog-Weg 2, 8093 Zurich (Switzerland); Brown, M. A. [Laboratory for Surface Science and Technology, Department of Materials, ETH Zurich, Vladimir-Prelog-Weg 5, 8093 Zurich (Switzerland); Bokhoven, J. A. van [Institute for Chemical and Bioengineering, ETH Zurich, Vladimir-Prelog-Weg 1, 8093 Zurich (Switzerland); Laboratory for Catalysis and Sustainable Chemistry, Paul Scherrer Institute, 5232 Villigen (Switzerland)

    2015-12-15

    A new apparatus for attosecond time-resolved photoelectron spectroscopy of liquids and gases is described. It combines a liquid microjet source with a magnetic-bottle photoelectron spectrometer and an actively stabilized attosecond beamline. The photoelectron spectrometer permits venting and pumping of the interaction chamber without affecting the low pressure in the flight tube. This pressure separation has been realized through a sliding skimmer plate, which effectively seals the flight tube in its closed position and functions as a differential pumping stage in its open position. A high-harmonic photon spectrometer, attached to the photoelectron spectrometer, exit port is used to acquire photon spectra for calibration purposes. Attosecond pulse trains have been used to record photoelectron spectra of noble gases, water in the gas and liquid states as well as solvated species. RABBIT scans demonstrate the attosecond resolution of this setup.

  18. Photoelectron spectrometer for attosecond spectroscopy of liquids and gases

    International Nuclear Information System (INIS)

    Jordan, I.; Huppert, M.; Wörner, H. J.; Brown, M. A.; Bokhoven, J. A. van

    2015-01-01

    A new apparatus for attosecond time-resolved photoelectron spectroscopy of liquids and gases is described. It combines a liquid microjet source with a magnetic-bottle photoelectron spectrometer and an actively stabilized attosecond beamline. The photoelectron spectrometer permits venting and pumping of the interaction chamber without affecting the low pressure in the flight tube. This pressure separation has been realized through a sliding skimmer plate, which effectively seals the flight tube in its closed position and functions as a differential pumping stage in its open position. A high-harmonic photon spectrometer, attached to the photoelectron spectrometer, exit port is used to acquire photon spectra for calibration purposes. Attosecond pulse trains have been used to record photoelectron spectra of noble gases, water in the gas and liquid states as well as solvated species. RABBIT scans demonstrate the attosecond resolution of this setup

  19. Photoelectron spectrometer for attosecond spectroscopy of liquids and gases

    Science.gov (United States)

    Jordan, I.; Huppert, M.; Brown, M. A.; van Bokhoven, J. A.; Wörner, H. J.

    2015-12-01

    A new apparatus for attosecond time-resolved photoelectron spectroscopy of liquids and gases is described. It combines a liquid microjet source with a magnetic-bottle photoelectron spectrometer and an actively stabilized attosecond beamline. The photoelectron spectrometer permits venting and pumping of the interaction chamber without affecting the low pressure in the flight tube. This pressure separation has been realized through a sliding skimmer plate, which effectively seals the flight tube in its closed position and functions as a differential pumping stage in its open position. A high-harmonic photon spectrometer, attached to the photoelectron spectrometer, exit port is used to acquire photon spectra for calibration purposes. Attosecond pulse trains have been used to record photoelectron spectra of noble gases, water in the gas and liquid states as well as solvated species. RABBIT scans demonstrate the attosecond resolution of this setup.

  20. Results of the first air ion spectrometer calibration and intercomparison workshop

    Directory of Open Access Journals (Sweden)

    E. Asmi

    2009-01-01

    Full Text Available The Air Ion Spectrometer (AIS measures mobility and size distributions of atmospheric ions. The Neutral cluster and Air Ion Spectrometer (NAIS can additionally measure neutral particles. The number of the (NAIS instruments in the world is only 11. Nevertheless, they are already widely used in atmospheric ion studies, particularly related to the initial steps of new particle formation. There is no standard method applicable for calibrating the ion spectrometers in the sub-3 nm ion range. However, recent development of high resolution DMAs has enabled the size separation of small ions with good mobility resolution. For the first time, the ion spectrometers were intercompared and calibrated in a workshop, held in January–February 2008 in Helsinki, Finland. The overall goal was to experimentally determine the (NAIS transfer functions. Monomobile mobility standards, 241-Am charger ions and silver particles were generated and used as calibration aerosols. High resolution DMAs were used to size-separate the smaller (1–10 nm ions, while at bigger diameters (4–40 nm the size was selected with a HAUKE-type DMA. Negative ion mobilities were detected by (NAISs with slightly better accuracy than positive, nonetheless, both were somewhat overestimated. A linear fit of slope of one to the whole dataset of mobilities suggested that (NAISs measured the negative mobilities 1.36±0.16 times larger compared with the reference instruments. Similarly, positive mobilities were measured 1.39±0.15 times larger compared with the reference instruments. The completely monomobile mobility standards were measured with the best accuracy. The (NAIS concentrations were compared with an aerosol electrometer (AE and a condensation particle counter (CPC. At sizes below 1.5 nm (positive and 3 nm (negative the ion spectrometers detected higher concentrations while at bigger sizes they showed similar concentrations as the reference instruments. The total particle

  1. Advanced mass spectrometers for hydrogen-isotope analyses

    International Nuclear Information System (INIS)

    Chastagner, P.; Daves, H.L.; Hess, W.B.

    1982-01-01

    Two advanced mass spectrometers for the accurate analysis of mixtures of the hydrogen isotopes were evaluated by Du Pont personnel at the Savannah River Laboratory. One is a large double-focusing instrument with a resolution of 2000 at mass 4 and an abundance sensitivity of >100,000 for the HT-D 2 doublet. The second is a smaller, simpler, stigmatic focusing instrument with exceptionally high ion intensities (>1 x 10 - 9 A at 600 resolution and about 1 x 10 - 10 A at 1300 resolution) for high signal-to-noise ratios. Both instruments are computer controlled. Once a scan is started, peak switching, scanning, mass discrimination control, data collection, and data reduction are done without operator intervention. Utility routines control hysteresis effects and instrument calibration. A containment facility, with dual inlet systems and a standard distribution system, permits testing with tritium mixtures. Helium flow standards and tritium activity meters provide independent verification of the mass spectrometer calibrations. A recovery system prevents the release of tritium to the environment. The performance of the mass spectrometers was essentially equal under simulated process control conditions. Precision and accuracy for the D/T ratio was <0.5% (rel 2sigma limits). Performance factors were: sample equilibration <300 ppM; linearity within +-0.3%; and gas interference <0.1%. Mass discrimination was controlled reliably by the computers

  2. ALICE photon spectrometer crystals

    CERN Multimedia

    Maximilien Brice

    2006-01-01

    Members of the mechanical assembly team insert the last few crystals into the first module of ALICE's photon spectrometer. These crystals are made from lead-tungstate, a crystal as clear as glass but with nearly four times the density. When a high-energy particle passes through one of these crystals it will scintillate, emitting a flash of light allowing the energy of photons, electrons and positrons to be measured.

  3. An approximately 4π tracking magnetic spectrometer for RHIC

    International Nuclear Information System (INIS)

    1987-01-01

    A tracking magnetic spectrometer based on large Time Projection Chambers (TPC) is proposed to measure the momentum of charged particles emerging from the RHIC beam pipe at angles larger than four degrees and to identify the particle type for those beyond fifteen degrees with momenta up to 700 MeV/c, which is a large fraction of the final charged particles emitted by a low rapidity quark-gluon plasma

  4. Applicability of a two-step laser desorption-ionization aerosol time-of-flight mass spectrometer for determination of chemical composition of ultrafine aerosol particles

    Energy Technology Data Exchange (ETDEWEB)

    Laitinen, T.

    2013-11-01

    This thesis is based on the construction of a two-step laser desorption-ionization aerosol time-of-flight mass spectrometer (laser AMS), which is capable of measuring 10 to 50 nm aerosol particles collected from urban and rural air at-site and in near real time. The operation and applicability of the instrument was tested with various laboratory measurements, including parallel measurements with filter collection/chromatographic analysis, and then in field experiments in urban environment and boreal forest. Ambient ultrafine aerosol particles are collected on a metal surface by electrostatic precipitation and introduced to the time-of-flight mass spectrometer (TOF-MS) with a sampling valve. Before MS analysis particles are desorbed from the sampling surface with an infrared laser and ionized with a UV laser. The formed ions are guided to the TOF-MS by ion transfer optics, separated according to their m/z ratios, and detected with a micro channel plate detector. The laser AMS was used in urban air studies to quantify the carbon cluster content in 50 nm aerosol particles. Standards for the study were produced from 50 nm graphite particles, suspended in toluene, with 72 hours of high power sonication. The results showed the average amount of carbon clusters (winter 2012, Helsinki, Finland) in 50 nm particles to be 7.2% per sample. Several fullerenes/fullerene fragments were detected during the measurements. In boreal forest measurements, the laser AMS was capable of detecting several different organic species in 10 to 50 nm particles. These included nitrogen-containing compounds, carbon clusters, aromatics, aliphatic hydrocarbons, and oxygenated hydrocarbons. A most interesting event occurred during the boreal forest measurements in spring 2011 when the chemistry of the atmosphere clearly changed during snow melt. On that time concentrations of laser AMS ions m/z 143 and 185 (10 nm particles) increased dramatically. Exactly at the same time, quinoline concentrations

  5. A fundamental parameters approach to calibration of the Mars Exploration Rover Alpha Particle X-ray Spectrometer

    Science.gov (United States)

    Campbell, J. L.; Lee, M.; Jones, B. N.; Andrushenko, S. M.; Holmes, N. G.; Maxwell, J. A.; Taylor, S. M.

    2009-04-01

    The detection sensitivities of the Alpha Particle X-ray Spectrometer (APXS) instruments on the Mars Exploration Rovers for a wide range of elements were experimentally determined in 2002 using spectra of geochemical reference materials. A flight spare instrument was similarly calibrated, and the calibration exercise was then continued for this unit with an extended set of geochemical reference materials together with pure elements and simple chemical compounds. The flight spare instrument data are examined in detail here using a newly developed fundamental parameters approach which takes precise account of all the physics inherent in the two X-ray generation techniques involved, namely, X-ray fluorescence and particle-induced X-ray emission. The objectives are to characterize the instrument as fully as possible, to test this new approach, and to determine the accuracy of calibration for major, minor, and trace elements. For some of the lightest elements the resulting calibration exhibits a dependence upon the mineral assemblage of the geological reference material; explanations are suggested for these observations. The results will assist in designing the overall calibration approach for the APXS on the Mars Science Laboratory mission.

  6. Physicochemical characteristics and occupational exposure to coarse, fine and ultrafine particles during building refurbishment activities

    Energy Technology Data Exchange (ETDEWEB)

    Azarmi, Farhad; Kumar, Prashant, E-mail: p.kumar@surrey.ac.uk, E-mail: prashant.kumar@cantab.net; Mulheron, Mike [University of Surrey, Department of Civil and Environmental Engineering, Faculty of Engineering and Physical Sciences (United Kingdom); Colaux, Julien L.; Jeynes, Chris [University of Surrey, Faculty of Engineering and Physical Sciences, Ion Beam Centre (United Kingdom); Adhami, Siavash; Watts, John F. [University of Surrey, The Surface Analysis Laboratory, Faculty of Engineering and Physical Sciences (United Kingdom)

    2015-08-15

    Understanding of the emissions of coarse (PM{sub 10} ≤10 μm), fine (PM{sub 2.5} ≤2.5 μm) and ultrafine particles (UFP <100 nm) from refurbishment activities and their dispersion into the nearby environment is of primary importance for developing efficient risk assessment and management strategies in the construction and demolition industry. This study investigates the release, occupational exposure and physicochemical properties of particulate matter, including UFPs, from over 20 different refurbishment activities occurring at an operational building site. Particles were measured in the 5–10,000-nm-size range using a fast response differential mobility spectrometer and a GRIMM particle spectrometer for 55 h over 8 days. The UFPs were found to account for >90 % of the total particle number concentrations and <10 % of the total mass concentrations released during the recorded activities. The highest UFP concentrations were 4860, 740, 650 and 500 times above the background value during wall-chasing, drilling, cementing and general demolition activities, respectively. Scanning electron microscopy, X-ray photoelectron spectroscopy and ion beam analysis were used to identify physicochemical characteristics of particles and attribute them to probable sources considering the size and the nature of the particles. The results confirm that refurbishment activities produce significant levels (both number and mass) of airborne particles, indicating a need to develop appropriate regulations for the control of occupational exposure of operatives undertaking building refurbishment.

  7. Progress in commercial TXRF spectrometer for semiconductors

    International Nuclear Information System (INIS)

    Nishihagi, K.

    2000-01-01

    In the scale down of ULSI devices, it is required to reduce contamination of metal or particle due to get higher yield. For the metallic contamination, we are trying to develop to get higher sensitivity in direct-TXRF method, however, VPD-TXRF is the most important method to get 10 7 to 10 8 atoms/cm 2 sensitivity. For the particle contamination, we have developed software to link TXRF spectrometer with particle counter because not only position or size but also composition analysis have got required. In semiconductor industries, there are two important changing for improvement on production management system as COO (Cost Of Ownership) or standardization. One is the size of wafer has changed from 200 mm to 300 mm. Against this, we have redesigned TXRF spectrometer for 300 mm wafer without down of sensitivity. The other is the production system has become completely automated. On this point, we have also redesigned to link TXRF spectrometer with SMIF (Standard Mechanical Interface) or FOUP (Front Opening Unified Pod) as mini-environment, and with SECS 2 (SEMI Equipment Communications Standard 2) or GEM 300 (Generic Equipment Model) as automatically standardization. We shall also introduce some applications about new materials using TXRF such as Ta 2 O 5 , ZrO 2 and HfO 2 for high-k materials, and also Ru, SRO and IrO 2 for electrode materials. Furthermore, we shall introduce our new equipment for thickness and composition analysis such as PZT, BST and MOCVD TiN thin films. (author)

  8. The OVIRS Visible/IR Spectrometer on the OSIRIS-Rex Mission

    Science.gov (United States)

    Reuter, D. C.; Simon-Miller, A. A.

    2012-01-01

    The OSIRIS-REx (Origins Spectral Interpretation Resource Identification Security Regolith Explorer) Mission is a planetary science mission to study, and return a sample from, the carbonaceous asteroid 1999 RQ-36. The third mission selected under NASA's New Frontiers Program, it is scheduled to be launched in 2016. It is led by PI Dante Lauretta at the University of Arizona and managed by NASA's Goddard Space Flight Center. The spacecraft and the asteroid sampling mechanism, TAGSAM (Touch-And-Go Sample Acquisition Mechanism) will be provided by Lockheed Martin Space Systems. Instrumentation for studying the asteroid include: OCAMS (the OSIRIS-REx Camera Suite), OLA (the OSIRIS-REx Laser Altimeter, a scanning LIDAR), OTES (The OSIRIS-REx Thermal Emission Spectrometer, a 4-50 micron point spectrometer) and OVIRS (the OSIRIS-REx Visible and IR Spectrometer, a 0.4 to 4.3 micron point spectrometer). The payload also includes REXIS (the Regolith X-ray Imaging Spectrometer) a student provided experiment. This paper presents a description of the OVIRS instrument.

  9. Implement of a magnetic spectrometer at the CERN intersecting stockage rings (900 spectrometer in the R608 experiment)

    International Nuclear Information System (INIS)

    Reyrolle, M.

    1985-01-01

    By adding a new spectrometer at 90 0 in the R608 experiment at CERN (ISR) we can search correlations between some systems of particles fully measured in the forward and transverse directions. The corresponding new electronic trigger, which selects events with momentum above a chosen threshold, is mixed or not to the forward trigger, in order to record correlated or inclusive data from the collisions p-p, p-anti-p, α-α. In the 90 0 spectrometer, we build drift chambers, set before the dipolar magnet. We studied the spatial resolution and the methods to associate tracks before and after this magnet. We developed the method to determine the momenta, by taking account of the variations of the deflecting power: the accuracy of this method is better than O.3%, and the global resolution is about 0.01 P 2 . We proposed also how to identify the particles from time of flight measurements and aerogel cerenkov counters [fr

  10. Study of preshower in the PANDA target spectrometer

    International Nuclear Information System (INIS)

    Dutta, Kamal; Kalita, Kushal; Suzuki, K.; Steinschaden, D.; Roy, B.J.

    2015-01-01

    PANDA (antiProton ANnihilation at DArmstdt) is one of the major projects at FAIR, GSI, Germany. The main objective of this experiment is to study the fundamental questions of hadron physics and QCD in pp¯ annihilation using high intensity cooled anti-proton beams with momenta between 1.5 GeV/c and 15 GeV/c. To achieve high momentum resolution and full solid angle coverage, the PANDA detector is split in to two parts: target spectrometer and forward spectrometer. The target spectrometer is a complex detector consisting of several subsystems surrounding the interaction point. It is surrounded by a 2 T superconducting solenoid magnet. A Micro Vertex Detector (MVD), close to interaction point, detects secondary vertices of D and Hyperon decays. The Straw Tube Tracker (STT) is the central tracking system around the MVD. A cherenkov counter named DIRC (Detection of Internally Reflected Cherenkov light), provides π/K separation for particle momenta up to 3.5 GeV/c. The barrel Time-of-Flight (TOF) detector, consists of plastic scintillator tiles with a time resolution of 100 ps. It is used to identify particles of momentum below cherenkov threshold

  11. Miniature Raman spectrometer development

    Science.gov (United States)

    Bonvallet, Joseph; Auz, Bryan; Rodriguez, John; Olmstead, Ty

    2018-02-01

    The development of techniques to rapidly identify samples ranging from, molecule and particle imaging to detection of high explosive materials, has surged in recent years. Due to this growing want, Raman spectroscopy gives a molecular fingerprint, with no sample preparation, and can be done remotely. These systems can be small, compact, lightweight, and with a user interface that allows for easy use and sample identification. Ocean Optics Inc. has developed several systems that would meet all these end user requirements. This talk will describe the development of different Ocean Optics Inc miniature Raman spectrometers. The spectrometer on a phone (SOAP) system was designed using commercial off the shelf (COTS) components, in a rapid product development cycle. The footprint of the system measures 40x40x14 mm (LxWxH) and was coupled directly to the cell phone detector camera optics. However, it gets roughly only 40 cm-1 resolution. The Accuman system is the largest (290x220X100 mm) of the three, but uses our QEPro spectrometer and get 7-11 cm-1 resolution. Finally, the HRS-30 measuring 165x85x40 mm is a combination of the other two systems. This system uses a modified EMBED spectrometer and gets 7-12 cm-1 resolution. Each of these units uses a peak matching algorithm that then correlates the results to the pre-loaded and customizable spectral libraries.

  12. Miniature Neutron-Alpha Activation Spectrometer

    Science.gov (United States)

    Rhodes, E.; Goldsten, J.

    2001-01-01

    We are developing a miniature neutron-alpha activation spectrometer for in situ analysis of samples including rocks, fines, ices, and drill cores, suitable for a lander or Rover platform, that would meet the severe mass, power, and environmental constraints of missions to the outer planets. In the neutron-activation mode, a gamma-ray spectrometer will first perform a penetrating scan of soil, ice, and loose material underfoot (depths to 10 cm or more) to identify appropriate samples. Chosen samples will be analyzed in bulk in neutron-activation mode, and then the sample surfaces will be analyzed in alpha-activation mode using Rutherford backscatter and x-ray spectrometers. The instrument will provide sample composition over a wide range of elements, including rock-forming elements (such as Na, Mg, Si, Fe, and Ca), rare earths (Sm and Eu for example), radioactive elements (K, Th, and U), and light elements present in water, ices, and biological materials (mainly H, C, O, and N). The instrument is expected to have a mass of about l kg and to require less than 1 W power. Additional information is contained in the original extended abstract.

  13. SPICA/SAFARI fourier transform spectrometer mechanism evolutionary design

    NARCIS (Netherlands)

    Dool, T.C. van den; Kruizinga, B.; Braam, B.C.; Hamelinck, R.F.M.M.; Loix, N.; Loon, D. van; Dams, J.

    2012-01-01

    TNO, together with its partners, have designed a cryogenic scanning mechanism for use in the SAFARI Fourier Transform Spectrometer (FTS) on board of the SPICA mission. SPICA is one of the M-class missions competing to be launched in ESA's Cosmic Vision Programme in 2022. JAXA leads the development

  14. Modeling of MOEMS electromagnetic scanning grating mirror for NIR micro-spectrometer

    Directory of Open Access Journals (Sweden)

    Ying Zhou

    2016-02-01

    Full Text Available In this paper, the mathematical model is developed for researching the detailed electromagnetic mechanism of MOEMS scanning mirror. We present the relationship between spectral range and optical scanning angle. Furthermore, the variation tendencies of resonant frequency and maximal torsional angle are studied in detail under different aspect ratios of MOEMS scanning mirror and varied dimensions of torsional bar. The numerical results and Finite Element Analysis simulations both indicate that the thickness of torsional bar is the most important factor. The maximal torsional angle appears when the aspect ratio equals to 1. This mathematical model is an effective way for designing the MOEMS electromagnetic scanning grating mirror in actual fabrication.

  15. Cosmic AntiParticle Ring Imaging Cerenkov Experiment

    CERN Multimedia

    2002-01-01

    %RE2A \\\\ \\\\ %title \\\\ \\\\The CAPRICE experiment studies antimatter and light nuclei in the cosmic rays as well as muons in the atmosphere. The experiment is performed with the spectrometer shown in the figure which is lifted by a balloon to an altitude of 35-40 km. At this altitude less than half a percent of the atmosphere is above the 2 ton spectrometer which makes it possible to study the cosmic ray flux without too much background from atmospherically produced particles. The spectrometer includes time-of-flight scintillators, a gaseous RICH counter, a drift chamber tracker and a silicon electromagnetic calorimeter. The important feature of the spectrometer is to discriminate between different particles.\\\\ \\\\ The experiment aims at measuring the flux of the antiparticles (antiprotons and positrons) above about 5 GeV and relate the fluxes to models including exotic production of antiparticles like dark matter supersymmetric particles. The flux of muons is measured during descent of the balloon through the at...

  16. Determination of the Effective Detector Area of an Energy-Dispersive X-Ray Spectrometer at the Scanning Electron Microscope Using Experimental and Theoretical X-Ray Emission Yields.

    Science.gov (United States)

    Procop, Mathias; Hodoroaba, Vasile-Dan; Terborg, Ralf; Berger, Dirk

    2016-12-01

    A method is proposed to determine the effective detector area for energy-dispersive X-ray spectrometers (EDS). Nowadays, detectors are available for a wide range of nominal areas ranging from 10 up to 150 mm2. However, it remains in most cases unknown whether this nominal area coincides with the "net active sensor area" that should be given according to the related standard ISO 15632, or with any other area of the detector device. Moreover, the specific geometry of EDS installation may further reduce a given detector area. The proposed method can be applied to most scanning electron microscope/EDS configurations. The basic idea consists in a comparison of the measured count rate with the count rate resulting from known X-ray yields of copper, titanium, or silicon. The method was successfully tested on three detectors with known effective area and applied further to seven spectrometers from different manufacturers. In most cases the method gave an effective area smaller than the area given in the detector description.

  17. Simulation of the peak efficiency for a stacked NaI(Tl) spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Yoshida, H; Murohka, H; Anami, K; Nohtomi, A; Uozumi, Y; Sakae, T; Matoba, M [Kyushu Univ., Fukuoka (Japan). Faculty of Engineering; Koori, N; Maki, T

    1996-07-01

    A stacked NaI(Tl) spectrometer has been developed to measure proton spectra in wide energy range. In the measurement of charged particles with intermediate energy, the detecting efficiency of the spectrometer decreases considerably due to nuclear reactions or out-scattering in the detector material. A Monte Carlo simulation code has been developed to estimate the peak efficiency (peak-to-total ratio) of the spectrometer. The calculated efficiency for intermediate energy is in good agreement with the experimental one. (author)

  18. Feasibility studies for the Forward Spectrometer

    International Nuclear Information System (INIS)

    Biernat, Jacek

    2015-01-01

    The Forward Spectrometer designed for the P-barANDA detector will consist of many different detector systems allowing for precise track reconstruction and particle identification. Feasibility studies for Forward Spectrometer done by means of specific reactions will be presented. In the first part of the paper, results of simulations focussing on rate estimates of the tracking stations based on straw tubes will be presented. Next, the importance of the Forward Tracker will be demonstrated through the reconstruction of the ψ(4040) → DD-bar decay. Finally, results from the analysis of the experimental data collected with a straw tube prototype designed and constructed at the Research Center in Juelich will be discussed. (paper)

  19. At the European Hybrid Spectrometer (EHS) for the experiment NA27

    CERN Multimedia

    1983-01-01

    The experiment NA27 was intended to measure accurately the lifetime of Charm particles and to study their hadronic production and decay particles. The vertex detector was the hydrogen bubble chamber LEBC. The aim was to collect several hundreths of fully reconstructed D0 and D+-, and several tens of F+- and Lambda_c decays as produced by 360 GeV/c negative pions and 400 GeV/c protons. The photo gives a side view of a section of the spectrometer, with a 12 m long gas Cerenkov counter at the centre. The spectrometer axis enters the photo at bottom, left corner. See photo 8311661, 8311662X, 8311660X.

  20. Special report: workshop on 4D-treatment planning in actively scanned particle therapy--recommendations, technical challenges, and future research directions.

    Science.gov (United States)

    Knopf, Antje; Bert, Christoph; Heath, Emily; Nill, Simeon; Kraus, Kim; Richter, Daniel; Hug, Eugen; Pedroni, Eros; Safai, Sairos; Albertini, Francesca; Zenklusen, Silvan; Boye, Dirk; Söhn, Matthias; Soukup, Martin; Sobotta, Benjamin; Lomax, Antony

    2010-09-01

    This article reports on a 4D-treatment planning workshop (4DTPW), held on 7-8 December 2009 at the Paul Scherrer Institut (PSI) in Villigen, Switzerland. The participants were all members of institutions actively involved in particle therapy delivery and research. The purpose of the 4DTPW was to discuss current approaches, challenges, and future research directions in 4D-treatment planning in the context of actively scanned particle radiotherapy. Key aspects were addressed in plenary sessions, in which leaders of the field summarized the state-of-the-art. Each plenary session was followed by an extensive discussion. As a result, this article presents a summary of recommendations for the treatment of mobile targets (intrafractional changes) with actively scanned particles and a list of requirements to elaborate and apply these guidelines clinically.

  1. Electron volt neutron spectrometers

    International Nuclear Information System (INIS)

    Pietropaolo, A.; Senesi, R.

    2011-01-01

    The advent of pulsed neutron sources has made available intense fluxes of epithermal neutrons (500 meV ≤E≤100 eV ). The possibility to open new investigations on condensed matter with eV neutron scattering techniques, is related to the development of methods, concepts and devices that drive, or are inspired by, emerging studies at this energy scale. Electron volt spectrometers have undergone continuous improvements since the construction of the first prototype instruments, but in the last decade major breakthroughs have been accomplished in terms of resolution and counting statistics, leading, for example, to the direct measurement of the proton 3-D Born–Oppenheimer potential in any material, or to quantitatively probe nuclear quantum effects in hydrogen bonded systems. This paper reports on the most effective methods and concepts for energy analysis and detection, as well as devices for the optimization of electron volt spectrometers for different applications. This is set in the context of the progress made up to date in instrument development. Starting from early stages of development of the technique, particular emphasis will be given to the Vesuvio eV spectrometer at the ISIS neutron source, the first spectrometer where extensive scientific, as well as research and development programmes have been carried out. The potential offered by this type of instrumentation, from single particle excitations to momentum distribution studies, is then put in perspective into the emerging fields of eV spectroscopy applied to cultural heritages and neutron irradiation effects in electronics. - Highlights: ► Neutron spectrometers at eV energies. ► Methods and techniques for eV neutrons counting at spallation sources. ► Scattering, imaging and radiation hardness tests with multi-eV neutrons.

  2. Single particle characterization using a light scattering module coupled to a time-of-flight aerosol mass spectrometer

    Science.gov (United States)

    Cross, E. S.; Onasch, T. B.; Canagaratna, M.; Jayne, J. T.; Kimmel, J.; Yu, X.-Y.; Alexander, M. L.; Worsnop, D. R.; Davidovits, P.

    2008-12-01

    We present the first single particle results obtained using an Aerodyne time-of-flight aerosol mass spectrometer coupled with a light scattering module (LS-ToF-AMS). The instrument was deployed at the T1 ground site approximately 40 km northeast of the Mexico City Metropolitan Area (MCMA) as part of the MILAGRO field study in March of 2006. The instrument was operated as a standard AMS from 12-30 March, acquiring average chemical composition and size distributions for the ambient aerosol, and in single particle mode from 27-30 March. Over a 75-h sampling period, 12 853 single particle mass spectra were optically triggered, saved, and analyzed. The correlated optical and chemical detection allowed detailed examination of single particle collection and quantification within the LS-ToF-AMS. The single particle data enabled the mixing states of the ambient aerosol to be characterized within the context of the size-resolved ensemble chemical information. The particulate mixing states were examined as a function of sampling time and most of the particles were found to be internal mixtures containing many of the organic and inorganic species identified in the ensemble analysis. The single particle mass spectra were deconvolved, using techniques developed for ensemble AMS data analysis, into HOA, OOA, NH4NO3, (NH4)2SO4, and NH4Cl fractions. Average single particle mass and chemistry measurements are shown to be in agreement with ensemble MS and PTOF measurements. While a significant fraction of ambient particles were internal mixtures of varying degrees, single particle measurements of chemical composition allowed the identification of time periods during which the ambient ensemble was externally mixed. In some cases the chemical composition of the particles suggested a likely source. Throughout the full sampling period, the ambient ensemble was an external mixture of combustion-generated HOA particles from local sources (e.g. traffic), with number concentrations peaking

  3. High-energy e- /e+ spectrometer via coherent interaction in a bent crystal

    Science.gov (United States)

    Bagli, Enrico; Guidi, Vincenzo; Howard, Alexander

    2018-01-01

    We propose a novel spectrometer based on the crystal channeling effect capable of discriminating between positive and negative particles well beyond the TeV energy scale. The atomic order of a crystalline structure generates an electrostatic field built up by all the atoms in the crystals, which confines charged particle trajectories between neighbouring atomic planes. Through such an interaction in a tiny curved crystal, the same dynamical action on the highest energy particles as that of a huge superconducting magnet is achieved. Depending on the charge sign, points of equilibrium of the oscillatory motion under channeling lie between or on atomic planes for positive and negative particles, respectively, forcing positive particles to stably oscillate far from the planes, while negative ones repeatedly cross them. The different interaction rate with atomic planes causes a tremendous discrepancy between the deflection efficiency of positive and negative particles under channeling. We suggest the use of interactions between charged particles and oriented bent crystals as a novel non-cryogenic passive charge spectrometer to aid the search for dark matter in the Universe in satellite-borne experiment. The limited angular acceptance makes this technique particularly suited for directional local sources of energetic charged particles.

  4. Scanning electron-microscopic and X-ray-microanalytic observation of diesel-emission particles associated with mutagenicity

    International Nuclear Information System (INIS)

    Nakashima, K.; Yoshitsugu, K.; Tokiwa, H.; Fukuoka Environmental Research Center

    1983-01-01

    The particles formed by diesel combustion, which may contain various mutagenic chemicals like polycyclic aromatic hydrocarbons (PAH), are analyzed in their morphology by scanning electron microscopy; their sulfur content is detected by X-ray microanalysis, and mutagenicity is tested with a Salmonella typhimurium bioassay. The authors find a close correlation between sulfur content and mutagenicity of PAH. (Auth.)

  5. A spectrometer using semi-conductor detectors; study and applications (1963)

    International Nuclear Information System (INIS)

    Roux, G.

    1963-01-01

    The low average energy, 2.5 to 3.5 eV, required to produce one hole-electron pair in a semiconductor allows an accurate measurement of the energy of the ionizing particles. A high resolution spectrometer has been built using semiconductor detectors. The limit of resolution, due to electronics associated to the detector, to the detector itself and to the source of particles is studied here. The present practical limit of resolution of the spectrometer is 1700 elementary electric charges (full width at half maximum of a ray of a spectrum) or 6 keV in terms of energy lost by a particle in a silicon detector. The physical resolution usually obtained is 20 keV (0.33 per cent) with α particles of the 212 Bi (6.087 MeV). It depends a lot of the kind of detector used. Some results, concerning the background of the detectors and limit of measurements for low energies are given. Various applications are presented: spectrometry β, spectrometry γ and X, spectrometry of mixtures of α radioactive elements, collection of α spectra. (author) [fr

  6. Uncertainty propagation using the Monte Carlo method in the measurement of airborne particle size distribution with a scanning mobility particle sizer

    Science.gov (United States)

    Coquelin, L.; Le Brusquet, L.; Fischer, N.; Gensdarmes, F.; Motzkus, C.; Mace, T.; Fleury, G.

    2018-05-01

    A scanning mobility particle sizer (SMPS) is a high resolution nanoparticle sizing system that is widely used as the standard method to measure airborne particle size distributions (PSD) in the size range 1 nm–1 μm. This paper addresses the problem to assess the uncertainty associated with PSD when a differential mobility analyzer (DMA) operates under scanning mode. The sources of uncertainty are described and then modeled either through experiments or knowledge extracted from the literature. Special care is brought to model the physics and to account for competing theories. Indeed, it appears that the modeling errors resulting from approximations of the physics can largely affect the final estimate of this indirect measurement, especially for quantities that are not measured during day-to-day experiments. The Monte Carlo method is used to compute the uncertainty associated with PSD. The method is tested against real data sets that are monosize polystyrene latex spheres (PSL) with nominal diameters of 100 nm, 200 nm and 450 nm. The median diameters and associated standard uncertainty of the aerosol particles are estimated as 101.22 nm  ±  0.18 nm, 204.39 nm  ±  1.71 nm and 443.87 nm  ±  1.52 nm with the new approach. Other statistical parameters, such as the mean diameter, the mode and the geometric mean and associated standard uncertainty, are also computed. These results are then compared with the results obtained by SMPS embedded software.

  7. Scanning table

    CERN Multimedia

    1960-01-01

    Before the invention of wire chambers, particles tracks were analysed on scanning tables like this one. Today, the process is electronic and much faster. Bubble chamber film - currently available - (links can be found below) was used for this analysis of the particle tracks.

  8. Some conceptual designs for a LASSY spectrometer magnet

    International Nuclear Information System (INIS)

    Green, M.A.

    1995-09-01

    The LASSY spectrometer is a gas filled spectrometer (hydrogen or helium at a pressure of about 1 torr). The design bending power for the primary bending magnet for the spectrometer will have an induction bend radius product of 2.5 tesla-meters. In order to increase the acceptance of the spectrometer, the bending magnet system must be located close to the target where the desired nuclei are created. The spectrometer magnet system must consist of both bending and focusing elements so that the wide acceptance of particles can be brought to a focus at the analysis point that is down stream from the last magnet element. In order improve the spectrometer resolution and to catch the shortest lived nuclei, the length of the magnet system must be as short as possible. The length for the LASSY spectrometer magnet system from the target to the analysis point has been set at 2.5 meters or less. To improve the resolution of the spectrometer, the bending angle for bending magnet system must be increased to close to 180 degrees. In order to achieve a large bending angle and a short magnet system length, the bending induction must be above 3 tesla and the focusing elements must be combined with the bending elements. As a result, a LASSY spectrometer will have bending magnet with a bending angle from 140 to 170 degrees. This magnet win be combined with one or more focusing magnets (a straight dipole in some places and a combined function dipole in other places). The result is a single superconducting bending magnet with one or more quadrupoles incorporated within the large angle bending magnet

  9. Soft X-ray scanning transmission X-ray microscopy (STXM) of actinide particles.

    Science.gov (United States)

    Nilsson, Hans J; Tyliszczak, Tolek; Wilson, Richard E; Werme, Lars; Shuh, David K

    2005-09-01

    A descriptive account is given of our most recent research on the actinide dioxides with the Advanced Light Source Molecular Environmental Science (ALS-MES) Beamline 11.0.2 soft X-ray scanning transmission X-ray microscope (STXM) at the Lawrence Berkeley National Laboratory (LBNL). The ALS-MES STXM permits near-edge X-ray absorption fine structure (NEXAFS) and imaging with 30-nm spatial resolution. The first STXM spectromicroscopy NEXAFS spectra at the actinide 4d5/2 edges of the imaged transuranic particles, NpO2 and PuO2, have been obtained. Radiation damage induced by the STXM was observed in the investigation of a mixed oxidation state particle (Np(V,VI)) and was minimized during collection of the actual spectra at the 4d5/2 edge of the Np(V,VI) solid. A plutonium elemental map was obtained from an irregular PuO2 particle with the dimensions of 650 x 650 nm. The Pu 4d5/2 NEXAFS spectra were collected at several different locations from the PuO2 particle and were identical. A representative oxygen K-edge spectrum from UO2 was collected and resembles the oxygen K-edge from the bulk material. The unique and current performance of the ALS-MES STXM at extremely low energies (ca. 100 eV) that may permit the successful measurement of the actinide 5d edge is documented. Finally, the potential of STXM as a tool for actinide investigations is briefly discussed.

  10. In-SEM Raman microspectroscopy coupled with EDX - a case study of uranium reference particles

    International Nuclear Information System (INIS)

    Stefaniak, Elzbieta A.; Pointurier, Fabien; Marie, Olivier; Truyens, Jan; Aregbe, Yetunde

    2014-01-01

    Information about the molecular composition of airborne uranium-bearing particles may be useful as an additional tool for nuclear safeguards. In order to combine the detection of micrometer-sized particles with the analysis of their molecular forms, we used a hybrid system enabling Raman microanalysis in high vacuum inside a SEM chamber (SEM-SCA system). The first step involved an automatic scan of a sample to detect and save coordinates of uranium particles, along with X-ray microanalysis. In the second phase, the detected particles were relocated in a white light image and subjected to Raman microanalysis. The consecutive measurements by the two beams showed exceptional fragility of uranium particles, leading to their ultimate damage and change of uranium oxidation state. We used uranium reference particles prepared by hydrolysis of uranium hexafluoride to test the reliability of the Raman measurements inside the high vacuum. The results achieved by the hybrid system were verified by using a standalone Raman micro spectrometer. When deposited on exceptionally smooth substrates, uranyl fluoride particles smaller than 1000 nm could successfully be analyzed with the SEM-SCA system. (authors)

  11. The OPERA magnetic spectrometer

    CERN Document Server

    Ambrosio, M; Dusini, S; Dulach, B; Fanin, C; Felici, G; Corso, F D; Garfagnini, A; Grianti, F; Gustavino, C; Monacelli, P; Paoloni, A; Stanco, L; Spinetti, M; Terranova, F; Votano, L

    2004-01-01

    The OPERA neutrino oscillation experiment foresees the construction of two magnetized iron spectrometers located after the lead-nuclear emulsion targets. The magnet is made up of two vertical walls of rectangular cross section connected by return yokes. The particle trajectories are measured by high precision drift tubes located before and after the arms of the magnet. Moreover, the magnet steel is instrumented with Resistive Plate Chambers that ease pattern recognition and allow a calorimetric measurement of the hadronic showers. In this paper we review the construction of the spectrometers. In particular, we describe the results obtained from the magnet and RPC prototypes and the installation of the final apparatus at the Gran Sasso laboratories. We discuss the mechanical and magnetic properties of the steel and the techniques employed to calibrate the field in the bulk of the magnet. Moreover, results of the tests and issues concerning the mass production of the Resistive Plate Chambers are reported. Final...

  12. Search for a particle with a long interaction length. [particle mandela to explain anomalous energy spectra at mountain altitude

    Science.gov (United States)

    Barrowes, S. C.; Huggett, R. W.; Jones, W. V.; Levit, L. B.; Porter, L. G.

    1975-01-01

    A search has been carried out for a long-lived particle having an interaction length lambda sub m equals 300 to 2000 gm/sq cm in air. Such a particle, called the mandela, has been proposed to explain an anomalous energy spectrum of particles observed near sea level with a shallow spectrometer. Data taken at mountain altitude with a deep spectrometer has been examined for compatibility with the existence of the mandela. Although data tend to favor the mandela hypothesis the results are not conclusive and appear to be explainable by conventional means.

  13. Laboratory Experiments and Instrument Intercomparison Studies of Carbonaceous Aerosol Particles

    Energy Technology Data Exchange (ETDEWEB)

    Davidovits, Paul [Boston College, Chestnut Hill, MA (United States)

    2015-10-20

    ) two well-characterized source of soot particles and (b) a flow reactor for controlled OH and/or O3 oxidation of relevant gas phase species to produce well-characterized SOA particles. After formation, the aerosol particles are subjected to physical and chemical processes that simulate aerosol growth and aging. A suite of instruments in our laboratory is used to characterize the physical and chemical properties of aerosol particles before and after processing. The Time of Flight Aerosol Mass Spectrometer (ToF-AMS) together with a Scanning Mobility Particle Sizer (SMPS) measures particle mass, volume, density, composition (including black carbon content), dynamic shape factor, and fractal dimension. The–ToF-AMS was developed at ARI with Boston College participation. About 120 AMS instruments are now in service (including 5 built for DOE laboratories) performing field and laboratory studies world-wide. Other major instruments include a thermal denuder, two Differential Mobility Analyzers (DMA), a Cloud Condensation Nuclei Counter (CCN), a Thermal desorption Aerosol GC/MS (TAG) and the new Soot Particle Aerosol Mass Spectrometer (SP-AMS). Optical instrumentation required for the studies have been brought to our laboratory as part of ongoing and planned collaborative projects with colleagues from DOE, NOAA and university laboratories. Optical instruments that will be utilized include a Photoacoustic Spectrometer (PAS), a Cavity Ring Down Aerosol Extinction Spectrometer (CRD-AES), a Photo Thermal Interferometer (PTI), a new 7-wavelength Aethalometer and a Cavity Attenuated Phase Shift Extinction Monitor (CAPS). These instruments are providing aerosol absorption, extinction and scattering coefficients at a range of atmospherically relevant wavelengths. During the past two years our work has continued along the lines of our original proposal. We report on 12 completed and/or continuing projects conducted during the period 08/14 to 0814/2015. These projects are described in

  14. Development of an ion time-of-flight spectrometer for neutron depth profiling

    Science.gov (United States)

    Cetiner, Mustafa Sacit

    signal. Without loss of generality, the secondary signal is obtained by the passage of the ion through a thin carbon foil, which produces ion-induced secondary electron emission (IISEE). The time-of-flight spectrometer physically acts as an ion/electron separator. The electrons that enter the active volume of the spectrometer are transported onto the microchannel plate detector to generate the secondary signal. The electron optics can be designed in variety of ways depending on the nature of the measurement and physical requirements. Two ion time-of-flight spectrometer designs are introduced: the parallel electric and magnetic (PEM) field spectrometer and the cross electric and magnetic (CEM) field spectrometer. The CEM field spectrometers have been extensively used in a wide range of applications where precise mass differentiation is required. The PEM field spectrometers have lately found interest in mass spectroscopy applications. The application of the PEM field spectrometer for energy measurements is a novel approach. The PEM field spectrometer used in the measurements employs axial electric and magnetic fields along the nominal direction of the incident ion. The secondary electrons are created by a thin carbon foil on the entrance disk and transported on the microchannel plate that faces the carbon foil. The initial angular distribution of the secondary electrons has virtually no effect on the transport time of the secondary electrons from the surface of the carbon foil to the electron microchannel plate detector. Therefore, the PEM field spectrometer can offer high-resolution energy measurement for relatively lower electric fields. The measurements with the PEM field spectrometer were made with the Tandem linear particle accelerator at the IBM T. J. Watson Research Center at Yorktown Heights, NY. The CEM field spectrometer developed for the thesis employs axial electric field along the nominal direction of the ion, and has perpendicular magnetic field. As the

  15. Far-ultraviolet imaging spectrograph and scanning grating spectrometers for the Remote Atmospheric and Ionospheric Detection System

    International Nuclear Information System (INIS)

    McCoy, R.P.; Meier, R.R.; Wolfram, K.D.; Picone, J.M.; Thonnard, S.E.; Fritz, G.G.; Morrill, J.S.; Christensen, A.B.; Kayser, D.C.; Pranke, J.B.; Straus, P.R.

    1994-01-01

    The Remote Atmospheric and Ionospheric Detection System (RAIDS) experiment is an optical remote sensing platform consisting of eight sensors, (spectrographs, spectrometers, and photometers) covering the wavelength range 550 to 8744 angstrom. RAIDS employs a mechanical scan platform to view the Earth's limb and measure line-of-sight column emission from tangent altitudes from 50 to 750 km. These measurements provide vertical profiles of atmospheric dayglow and nightglow from the mesosphere to the upper regions of the F-region ionosphere. RAIDS will be flown on the National Oceanographic and Atmospheric Administration (NOAA) J weather satellite through the auspices of the US Air Force Space Test Program. The RAIDS wavelength and altitude coverage allows remote sensing of the major and many minor constituents in the thermosphere and ionosphere. These measurements will be used as part of a proof of concept for remote sensing of ionospheric and neutral density profiles. The RAIDS database will be used to study composition, thermal structure, and couplings between the mesosphere, thermosphere, thermal structure, and couplings between the mesosphere, thermosphere, and ionosphere. RAIDS is a joint venture of the Naval Research Laboratory (NRL) and the Aerospace Corporation. The authors describe the subset of RAIDS instruments developed at NRL covering the far to near UV regions (1,300 to 4,000 angstrom)

  16. Two-lens spectrometer for. beta. polarimetry

    Energy Technology Data Exchange (ETDEWEB)

    Holdsworth, D; Paul, D [Toronto Univ., Ontario (Canada). Dept. of Physics

    1984-06-01

    A test spectrometer has been built having four degrees of freedom which have been varied to optimize the transmission in a configuration in which the image distance is large compared to the object distance. Iron-clad magnets of 15 cm effective inside diameter were used. Within the limits of the primary magnet field, the optimized transmission T (%. of 4..pi.. sr) increases as the source is advanced through the magnet towards the polarimeter, approximately as T=5.1 exp(zsub(s)/10.5), where zsub(s) is in cm, measured from the position of peak axial field. When the source-image distance is 1.8 m the optimum separation of the peak axial fields of the magnets is 67+-1 cm and the spectrometer transmission is the same for parallel or antiparallel fields. When operating in the optimum configuration, the spectrometer accepts particles with initial trajectories from 18/sup 0/ to 42/sup 0/ relative to the axis and delivers them at the target with half-angle of convergence less than 4.1/sup 0/.

  17. The CHAOS spectrometer for pion physics at TRIUMF

    International Nuclear Information System (INIS)

    Smith, G.R.; Amaudruz, P.A.; Brack, J.T.

    1994-12-01

    The Canadian high acceptance orbit spectrometer (CHAOS) is a unique magnetic spectrometer system recently commissioned for studies of pion induced reactions at TRIUMF. It is based on a cylindrical dipole magnet producing vertical magnetic fields up to 1.6 T. The scattering target is located in the center of the magnet. Charged particle tracks produced by pion interactions there are identified using four concentric cylindrical wire chambers surrounding the target. Particle identification and track multiplicity are determined by cylindrical layers of scintillation counters and lead glass Cerenkov counters, which also provide a first level trigger. A sophisticated second level trigger system permits pion fluxes in excess of 5 MHz to be employed. The detector subtends 360 o in the horizontal plane, and ±7 o out of this plane for a solid angle coverage approximately 10% of 4π sr. The momentum resolution delivered by the detector system is 1% (σ). (author). 16 refs., 12 figs

  18. Cherenkov detectors and a new effective-mass spectrometer method

    Czech Academy of Sciences Publication Activity Database

    Hladký, Jan

    2006-01-01

    Roč. 75, - (2006), s. 854-855 ISSN 0969-806X Institutional research plan: CEZ:AV0Z10100502 Keywords : Cherenkov radiation * spectrometer * effective mass method Subject RIV: BF - Elementary Particles and High Energy Physics Impact factor: 0.868, year: 2006

  19. Coherent x-ray diffraction imaging of paint pigment particles by scanning a phase plate modulator

    International Nuclear Information System (INIS)

    Chu, Y.S.; Chen, B.; Zhang, F.; Berenguer, F.; Bean, R.; Kewish, C.; Vila-Comamala, J.; Rodenburg, J.; Robinson, I.

    2011-01-01

    We have implemented a coherent x-ray diffraction imaging technique that scans a phase plate to modulate wave-fronts of the x-ray beam transmitted by samples. The method was applied to measure a decorative alkyd paint containing iron oxide red pigment particles. By employing an iterative algorithm for wave-front modulation phase retrieval, we obtained an image of the paint sample that shows the distribution of the pigment particles and is consistent with the result obtained from a transmission x-ray microscope. The technique has been experimentally proven to be a feasible coherent x-ray imaging method with about 120 nm spatial resolution and was shown to work well with industrially relevant specimens.

  20. Hygroscopic properties of atmospheric particles emitted during wintertime biomass burning episodes in Athens

    Science.gov (United States)

    Psichoudaki, Magda; Nenes, Athanasios; Florou, Kalliopi; Kaltsonoudis, Christos; Pandis, Spyros N.

    2018-04-01

    This study explores the Cloud Condensation Nuclei (CCN) activity of atmospheric particles during intense biomass burning periods in an urban environment. During a one-month campaign in the center of Athens, Greece, a CCN counter coupled with a Scanning Mobility Particle Sizer (SMPS) and a high resolution Aerosol Mass Spectrometer (HR-AMS) were used to measure the size-resolved CCN activity and composition of the atmospheric aerosols. During the day, the organic fraction of the particles was more than 50%, reaching almost 80% at night, when the fireplaces were used. Positive Matrix Factorization (PMF) analysis revealed 4 factors with biomass burning being the dominant source after 18:00 until the early morning. The CCN-based overall hygroscopicity parameter κ ranged from 0.15 to 0.25. During the night, when the biomass burning organic aerosol (bbOA) dominated, the hygroscopicity parameter for the mixed organic/inorganic particles was on average 0.16. The hygroscopicity of the biomass-burning organic particles was 0.09, while the corresponding average value for all organic particulate matter during the campaign was 0.12.

  1. Triple axis spectrometers

    International Nuclear Information System (INIS)

    Clausen, K.N.

    1997-01-01

    Conventional triple-axis neutron spectroscopy was developed by Brockhouse over thirty years ago' and remains today a versatile and powerful tool for probing the dynamics of condensed matter. The original design of the triple axis spectrometer is technically simple and probes momentum and energy space on a point-by-point basis. This ability to systematically probe the scattering function in a way which only requires a few angles to be moved under computer control and where the observed data in general can be analysed using a pencil and graph paper or a simple fitting routine, has been essential for the success of the method. These constraints were quite reasonable at the time the technique was developed. Advances in computer based data acquisition, neutron beam optics, and position sensitive area detectors have been gradually implemented on many triple axis spectrometer spectrometers, but the full potential of this has not been fully exploited yet. Further improvement in terms of efficiency (beyond point by point inspection) and increased sensitivity (use of focusing optics whenever the problem allows it) could easily be up to a factor of 10-20 over present instruments for many problems at a cost which is negligible compared to that of increasing the flux of the source. The real cost will be in complexity - finding the optimal set-up for a given scan and interpreting the data as the they are taken. On-line transformation of the data for an appropriate display in Q, ω space and analysis tools will be equally important for this task, and the success of these new ideas will crucially depend on how well we solve these problems. (author)

  2. The HISS spectrometer at LBL

    International Nuclear Information System (INIS)

    Greiner, D.

    1981-01-01

    The Heavy Ion Spectrometer System at LBL is designed to be a general purpose experimental work bench able to support a wide variety of experiments. Our philosophy is to provide instruments capable of investigating, with multi-particle sensitivity, a large portion of phase space. We have not chosen a particular region such as mid-rapidity or projectile frame, but instead, have made sure that the magnet and the instrumentation allow these choices as well as many others. (orig.)

  3. HISS spectrometer at LBL

    International Nuclear Information System (INIS)

    Greiner, D.

    1980-11-01

    The Heavy Ion Spectrometer System at LBL is designed to be a general purpose experimental work bench able to support a wide variety of experiments. Our philosophy is to provide instruments capable of investigating, with multi-particle sensitivity, a large portion of phase space. We have not chosen a particular region such as mid-rapidity or projectile frame but, instead, have made sure that the magnet and the instrumentation allow these choices as well as many others. The beam can be brought into the magnet at a variable position and the magnet can be rotated

  4. QQDDQ magnet spectrometer 'BIG KARL'

    Energy Technology Data Exchange (ETDEWEB)

    Martin, S A; Hardt, A; Meissburger, J; Berg, G P.A.; Hacker, U; Huerlimann, W; Roemer, J G.M.; Sagefka, T; Retz, A; Schult, O W.B.

    1983-09-01

    A magnet spectrometer consisting of two quadrupoles, two dipole magnets and another larger quadrupole in front of the detector was designed and installed at the nuclear research institute of the KFA Juelich. It has been used for charged-particle spectroscopy at the isochronous cyclotron since early 1979. Special features of the spectrometer are variable and high dispersion, coils for higher order field corrections in the dipole magnets and a focal plane perpendicular to the optical axis. A large mass-energy product of mE/q/sup 2/ < 540 u x MeV, an angular acceptance of d..cap omega..<12.5 msr, a high resolving power of p/..delta..p up to 3 x 10/sup 4/ and the possibility of kinematical corrections up to K=0.8 make the instrument a very versatile tool for many experiments in the fields of nuclear and atomic physics. 51 references.

  5. Effect of re-melting on particle distribution and interface formation in SiC reinforced 2124Al matrix composite

    Energy Technology Data Exchange (ETDEWEB)

    Mandal, Durbadal, E-mail: durbadal73@yahoo.co.in [MEF Division, CSIR-National Metallurgical Laboratory, Jamshedpur 831007 (India); Viswanathan, Srinath [Dept of Metallurgical and Materials Engineering, University of Alabama, Tuscaloosa, AL (United States)

    2013-12-15

    The interface between metal matrix and ceramic reinforcement particles plays an important role in improving properties of the metal matrix composites. Hence, it is important to find out the interface structure of composite after re-melting. In the present investigation, the 2124Al matrix with 10 wt.% SiC particle reinforced composite was re-melted at 800 °C and 900 °C for 10 min followed by pouring into a permanent mould. The microstructures reveal that the SiC particles are distributed throughout the Al-matrix. The volume fraction of SiC particles varies from top to bottom of the composite plate and the difference increases with the decrease of re-melting temperature. The interfacial structure of re-melted 2124Al–10 wt.%SiC composite was investigated using scanning electron microscopy, an electron probe micro-analyzer, a scanning transmission electron detector fitted with scanning electron microscopy and an X-ray energy dispersive spectrometer. It is found that a thick layer of reaction product is formed at the interface of composite after re-melting. The experimental results show that the reaction products at the interface are associated with high concentration of Cu, Mg, Si and C. At re-melting temperature, liquid Al reacts with SiC to form Al{sub 4}C{sub 3} and Al–Si eutectic phase or elemental Si at the interface. High concentration of Si at the interface indicates that SiC is dissociated during re-melting. The X-ray energy dispersive spectrometer analyses confirm that Mg- and Cu-enrich phases are formed at the interface region. The Mg is segregated at the interface region and formed MgAl{sub 2}O{sub 4} in the presence of oxygen. The several elements identified at the interface region indicate that different types of interfaces are formed in between Al matrix and SiC particles. The Al–Si eutectic phase is formed around SiC particles during re-melting which restricts the SiC dissolution. - Highlights: • Re-melted composite shows homogeneous particle

  6. Drift chambers for a large-area, high-precision muon spectrometer

    International Nuclear Information System (INIS)

    Alberini, C.; Bari, G.; Cara Romeo, G.; Cifarelli, L.; Del Papa, C.; Iacobucci, G.; Laurenti, G.; Maccarrone, G.; Massam, T.; Motta, F.; Nania, R.; Perotto, E.; Prisco, G.; Willutsky, M.; Basile, M.; Contin, A.; Palmonari, F.; Sartorelli, G.

    1987-01-01

    We have tested two prototypes of high-precision drift chamber for a magnetic muon spectrometer. Results of the tests are presented, with special emphasis on their efficiency and spatial resolution as a function of particle rate. (orig.)

  7. FATES: a flexible analysis toolkit for the exploration of single-particle mass spectrometer data

    Science.gov (United States)

    Sultana, Camille M.; Cornwell, Gavin C.; Rodriguez, Paul; Prather, Kimberly A.

    2017-04-01

    Single-particle mass spectrometer (SPMS) analysis of aerosols has become increasingly popular since its invention in the 1990s. Today many iterations of commercial and lab-built SPMSs are in use worldwide. However, supporting analysis toolkits for these powerful instruments are outdated, have limited functionality, or are versions that are not available to the scientific community at large. In an effort to advance this field and allow better communication and collaboration between scientists, we have developed FATES (Flexible Analysis Toolkit for the Exploration of SPMS data), a MATLAB toolkit easily extensible to an array of SPMS designs and data formats. FATES was developed to minimize the computational demands of working with large data sets while still allowing easy maintenance, modification, and utilization by novice programmers. FATES permits scientists to explore, without constraint, complex SPMS data with simple scripts in a language popular for scientific numerical analysis. In addition FATES contains an array of data visualization graphic user interfaces (GUIs) which can aid both novice and expert users in calibration of raw data; exploration of the dependence of mass spectral characteristics on size, time, and peak intensity; and investigations of clustered data sets.

  8. Classification of Multiple Types of Organic Carbon Composition in Atmospheric Particles by Scanning Transmission X-Ray Microscopy Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Kilcoyne, Arthur L; Takahama, S.; Gilardoni, S.; Russell, L.M.; Kilcoyne, A.L.D.

    2007-05-16

    A scanning transmission X-ray microscope at the Lawrence Berkeley National Laboratory is used to measure organic functional group abundance and morphology of atmospheric aerosols. We present a summary of spectra, sizes, and shapes observed in 595 particles that were collected and analyzed between 2000 and 2006. These particles ranged between 0.1 and 12 mm and represent aerosols found in a large range of geographical areas, altitudes, and times. They include samples from seven different field campaigns: PELTI, ACE-ASIA, DYCOMS II, Princeton, MILAGRO (urban), MILAGRO (C-130), and INTEX-B. At least 14 different classes of organic particles show different types of spectroscopic signatures. Different particle types are found within the same region while the same particle types are also found in different geographical domains. Particles chemically resembling black carbon, humic-like aerosols, pine ultisol, and secondary or processed aerosol have been identified from functional group abundance and comparison of spectra with those published in the literature.

  9. A study of the effect of non-spherical dust particles on Geostationary Environment Monitoring Spectrometer (GEMS) aerosol optical properties retrievals

    Science.gov (United States)

    Go, S.; Kim, J.; KIM, M.; Choi, M.; Lim, H.

    2017-12-01

    Non-spherical assumption of particle shape has been used to replace the spherical assumption in the Geostationary Environment Monitoring Spectrometer (GEMS) aerosol optical properties retrievals for dust particles. GEMS aerosol retrieval algorithms are based on optimal estimation method to provide aerosol optical depth (AOD), single scattering albedo (SSA) at 443nm, and aerosol loading height (ALH) simultaneously as products. Considering computing time efficiency, the algorithm takes Look-Up Table (LUT) approach using Vector Linearized Discrete Ordinate Radiative Transfer code (VLIDORT), and aerosol optical properties for three aerosol types of absorbing fine aerosol (BC), dust and non-absorbing aerosol (NA) are integrated from AERONET inversion data, and fed into the LUT calculation. In this study, by applying the present algorithm to OMI top-of the atmosphere normalized radiance, retrieved AOD, SSA with both spherical and non-spherical assumptions have been compared to the surface AERONET observations at East Asia sites for 3 years from 2005 to 2007 to evaluate and quantify the effect of non-spherical dust particles on the satellite aerosol retrievals. The root-mean-square error (RMSE) in the satellite retrieved AOD have been slightly reduced as a result of adopting the non-spherical assumption in the GEMS aerosol retrieval algorithm. For SSA, algorithm tested with spheroid models on dust particle shows promising results for the improved SSA. In terms of ALH, the results are qualitatively compared with CALIOP products, and shows consistent variation. This result suggests the importance of taking into account the effects of non-sphericity in the retrieval of dust particles from GEMS measurements.

  10. Sources and atmospheric processing of organic aerosol in the Mediterranean: insights from aerosol mass spectrometer factor analysis

    Directory of Open Access Journals (Sweden)

    L. Hildebrandt

    2011-12-01

    Full Text Available Atmospheric particles were measured in the late winter (25 February–26 March 2009 at a remote coastal site on the island of Crete, Greece during the Finokalia Aerosol Measurement Experiment-2009. A quadrupole aerosol mass spectrometer (Q-AMS was employed to quantify the size-resolved chemical composition of non-refractory submicron aerosol, and a thermodenuder was used to analyze the organic aerosol (OA volatility. Complementary measurements included particle size distributions from a scanning mobility particle sizer, inorganic and organic particle composition from filter analysis, air ion concentrations, O3, NOx and NOy concentrations, and meteorological measurements. Factor analysis was performed on the OA mass spectra, and the variability in OA composition could best be explained with three OA components. The oxygenated organic aerosol (OOA was similar in composition and volatility to the summertime OA previously measured at this site and may represent an effective endpoint in particle-phase oxidation of organics. The two other OA components, one associated with amines (Amine-OA and the other probably associated with the burning of olive branches (OB-OA, had very low volatility but were less oxygenated. Hydrocarbon-like organic aerosol (HOA was not detected. The absence of OB-OA and Amine-OA in the summer data may be due to lower emissions and/or photochemical conversion of these components to OOA.

  11. Conceptual design of the radial gamma ray spectrometers system for α particle and runaway electron measurements at ITER

    Science.gov (United States)

    Nocente, M.; Tardocchi, M.; Barnsley, R.; Bertalot, L.; Brichard, B.; Croci, G.; Brolatti, G.; Di Pace, L.; Fernandes, A.; Giacomelli, L.; Lengar, I.; Moszynski, M.; Krasilnikov, V.; Muraro, A.; Pereira, R. C.; Perelli Cippo, E.; Rigamonti, D.; Rebai, M.; Rzadkiewicz, J.; Salewski, M.; Santosh, P.; Sousa, J.; Zychor, I.; Gorini, G.

    2017-07-01

    We here present the principles and main physics capabilities behind the design of the radial gamma ray spectrometers (RGRS) system for alpha particle and runaway electron measurements at ITER. The diagnostic benefits from recent advances in gamma-ray spectrometry for tokamak plasmas and combines space and high energy resolution in a single device. The RGRS system as designed can provide information on α ~ particles on a time scale of 1/10 of the slowing down time for the ITER 500 MW full power DT scenario. Spectral observations of the 3.21 and 4.44 MeV peaks from the 9\\text{Be}≤ft(α,nγ \\right){{}12}\\text{C} reaction make the measurements sensitive to α ~ particles at characteristic resonant energies and to possible anisotropies of their slowing down distribution function. An independent assessment of the neutron rate by gamma-ray emission is also feasible. In case of runaway electrons born in disruptions with a typical duration of 100 ms, a time resolution of at least 10 ms for runaway electron studies can be achieved depending on the scenario and down to a current of 40 kA by use of external gas injection. We find that the bremsstrahlung spectrum in the MeV range from confined runaways is sensitive to the electron velocity space up to E≈ 30 -40 MeV, which allows for measurements of the energy distribution of the runaway electrons at ITER.

  12. Standalone vertex finding in the ATLAS muon spectrometer

    Czech Academy of Sciences Publication Activity Database

    Aad, G.; Abajyan, T.; Abbott, B.; Böhm, Jan; Chudoba, Jiří; Hejbal, Jiří; Jakoubek, Tomáš; Kepka, Oldřich; Kupčo, Alexander; Kůs, Vlastimil; Lokajíček, Miloš; Lysák, Roman; Marčišovský, Michal; Mikeštíková, Marcela; Myška, Miroslav; Němeček, Stanislav; Dos Santos, D.R.; Růžička, P.; Šícho, Petr; Staroba, Pavel; Svatoš, Michal; Taševský, Marek; Tic, Tomáš; Vrba, Václav

    2014-01-01

    Roč. 9, Feb (2014), s. 1-22 ISSN 1748-0221 R&D Projects: GA MŠk(CZ) LG13009 Institutional support: RVO:68378271 Keywords : muon spectrometers * performance of high energy physics * detectors * ATLAS * CERN LHC Coll Subject RIV: BF - Elementary Particles and High Energy Physics Impact factor: 1.399, year: 2014

  13. Experimental investigation of the effect of inlet particle properties on the capture efficiency in an exhaust particulate filter

    Energy Technology Data Exchange (ETDEWEB)

    Viswanathan, Sandeep; Rothamer, David; Zelenyuk, Alla; Stewart, Mark; Bell, David

    2017-11-01

    The impact of inlet particle properties on the filtration performance of clean and particulate matter (PM) laden cordierite filter samples was evaluated using PM generated by a spark-ignition direct-injection (SIDI) engine fuelled with tier II EEE certification gasoline. Prior to the filtration experiments, a scanning mobility particle spectrometer (SMPS) was used to measure the electrical-mobility based particle size distribution (PSD) in the SIDI exhaust from distinct engine operating conditions. An advanced aerosol characterization system that comprised of a centrifugal particle mass analyser (CPMA), a differential mobility analyser (DMA), and a single particle mass spectrometer (SPLAT II) was used to obtain additional information on the SIDI particulate, including particle composition, mass, and dynamic shape factors (DSFs) in the transition () and free-molecular () flow regimes. During the filtration experiments, real-time measurements of PSDs upstream and downstream of the filter sample were used to estimate the filtration performance and the total trapped mass within the filter using an integrated particle size distribution method. The filter loading process was paused multiple times to evaluate the filtration performance in the partially loaded state. The change in vacuum aerodynamic diameter () distribution of mass-selected particles was examined for flow through the filter to identify whether preferential capture of particles of certain shapes occurred in the filter. The filter was also probed using different inlet PSDs to understand their impact on particle capture within the filter sample. Results from the filtration experiment suggest that pausing the filter loading process and subsequently performing the filter probing experiments did not impact the overall evolution of filtration performance. Within the present distribution of particle sizes, filter efficiency was independent of particle shape potentially due to the diffusion-dominant filtration

  14. Data acquisition and control system for quadrupole mass spectrometer using an add-on card to an IBM PC

    International Nuclear Information System (INIS)

    Paal, A.; Szadai, J.; Szekely, G.

    1991-01-01

    An RF/DC unit, a dedicated interface card and the PCQMS software was designed to upgrade the existing quadrupole mass spectrometer of ATOMKI series Q300C to Q300PC. The new units and the software features are described. Display modes, all in high resolution graphics are provided to include ion monitoring table, ion monitoring analog, intensity vs time or temperature, scan bargraph and scan analog. The quadrupole mass spectrometer performance has been improved by the new modifications for data acquisition and control to be accomplished automatically. (R.P.) 3 refs.; 4 figs

  15. Plasma rotation measurement in small tokamaks using an optical spectrometer and a single photomultiplier as detector.

    Science.gov (United States)

    Severo, J H F; Nascimento, I C; Kuznetov, Yu K; Tsypin, V S; Galvão, R M O; Tendler, M

    2007-04-01

    The method for plasma rotation measurement in the tokamak TCABR is reported in this article. During a discharge, an optical spectrometer is used to scan sequentially spectral lines of plasma impurities and spectral lines of a calibration lamp. Knowing the scanning velocity of the diffraction grating of the spectrometer with adequate precision, the Doppler shifts of impurity lines are determined. The photomultiplier output voltage signals are recorded with adequate sampling rate. With this method the residual poloidal and toroidal plasma rotation velocities were determined, assuming that they are the same as those of the impurity ions. The results show reasonable agreement with the neoclassical theory and with results from similar tokamaks.

  16. On-board aircrew dosimetry using a semiconductor spectrometer

    CERN Document Server

    Spurny, F

    2002-01-01

    Radiation fields on board aircraft contain particles with energies up to a few hundred MeV. Many instruments have been tested to characterise these fields. This paper presents the results of studies on the use of an Si diode spectrometer to characterise these fields. The spectrometer has been in use since spring 2000 on more than 130 return flights to monitor and characterise the on-board field. During a Czech Airlines flight from Prague to New York it was possible to register the effects of an intense solar flare, (ground level event, GLE 60), which occurred on 15 April 2001. It was found that the number of deposition events registered was increased by about 70% and the dose in Si by a factor of 2.0 when compared with the presence of galactic cosmic rays alone. Directly measured data are interpreted with respect to on-earth reference field calibration (photons, CERN high-energy particles); it was found that this approach leads to encouraging results and should be followed up. (7 refs).

  17. Solar maximum ultraviolet spectrometer and polarimeter

    Science.gov (United States)

    Tandberg-Hanssen, E.; Woodgate, B. E.; Brandt, J. C.; Chapman, R. D.; Hyder, C. L.; Michalitsianos, A. G.; Shine, R. A.; Athay, R. G.; Beckers, J. M.; Bruner, E. C.

    1979-01-01

    The objectives of the UVSP experiment are to study solar ultraviolet radiations, particularly from flares and active regions, and to measure constituents in the terrestrial atmosphere by the extinction of sunlight at satellite dawn and dusk. The instrument is designed to observe the Sun at a variety of spectral and spatial resolutions in the range from 1150 to 3600 A. A Gregorian telescope with effective focal length of 1.8 m is used to feed a 1 m Ebert-Fastie spectrometer. A polarimeter containing rotatable magnesium fluoride waveplates is included behind the spectrometer entrance slit and will allow all four Stokes parameters to be determined. Velocities on the Sun can also be measured. The instrument is controlled by a computer which can interact with the data stream to modify the observing program. The observing modes, including rasters, spectral scans, velocity measurements, and polarimetry, are also described along with plans for mission operations, data handling, and analysis of the observations.

  18. Further development of a track detector as the spectrometer of linear energy transfer

    International Nuclear Information System (INIS)

    Spurny, F.; Bednar, J.; Vlcek, B.; Botollier-Depois, J.F.

    1998-01-01

    Track revealing in a track etch detector is a phenomenon related to the linear energy transfer (LET) of the particle registered. The measurements of track parameters permit to determine the LET corresponding to each revealed track, i.e. LET spectrum. We have recently developed a spectrometer of LET based on the chemically etched polyallyldiglycolcarbonate (PADC). In this contribution the results obtained with such spectrometer in some neutron fields are presented, analyzed and discussed. Several radionuclide neutron sources have been used, LET spectrometer has been also exposed in high energy neutron reference fields at CERN and JINR Dubna, and on board aircraft. (author)

  19. Effective mass trigger at the Brookhaven Multi-Particle Spectrometer (MPS)

    International Nuclear Information System (INIS)

    Willen, E.H.

    1980-01-01

    An effective mass trigger for use at the Brookhaven Multiparticle Spectrometer (MPS) is described. It is a microprocessor based device using extensive fast memory attached to proportional wire chambers in the MPS magnetic field. It will select kinematic quantities unique to the reaction being studied, thereby permitting higher sensitivities and a reduction in data-processing cost for MPS experiments. The principles of operation for this trigger, and the results of simulations to assess its performance, are presented

  20. Cylindrical Crystal Imaging Spectrometer (CCIS) for cosmic X-ray spectroscopy

    Science.gov (United States)

    Schnopper, H. W.; Taylor, P. O.

    1981-01-01

    A "stigmatic" focusing, Bragg crystal spectrometer was developed and used for high spectral resolution X-ray emission line diagnostics on hot laboratory plasmas. The concept be applied at the focal plane of an orbiting X-ray telescope where it offers several advantages over conventional spectrometers, i.e., mechanical simplicity, high resolving power and sensitivity, simultaneous measurement of an extended segment of spectrum, and good imaging properties. The instrument features a simple, unambiguous, non-scanning spectrum readout that is not adversely affected by either spacecraft pointing error or source extent. The performance of the instrument is estimated in the context of the Advanced X-Ray Astrophysical Facility mission.

  1. Cross-Sectional Information on Pore Structure and Element Distribution of Sediment Particles by SEM and EDS

    Directory of Open Access Journals (Sweden)

    Minghong Chen

    2017-01-01

    Full Text Available The interaction between pollutants and sediment particles often occurs on the particle surface, so surface properties directly affect surface reaction. The physical and chemical processes occurring on sediment particle surfaces are microscopic processes and as such need to be studied from a microscopic perspective. In this study, field emission scanning electron microscopy (SEM and energy dispersive X-ray spectrometer (EDS were adopted to observe and analyze the pore structure and element distribution of sediment particles. In particular, a special method of sample preparation was used to achieve the corresponding cross-sectional information of sediment particles. Clear images of a particle profile and pore microstructure were obtained by high-resolution SEM, while element distribution maps of sediment particles were obtained by EDS. The results provide an intuitive understanding of the internal microenvironment and external behavior of sediment particles, in addition to revealing a significant role of pore microstructure in the adsorption and desorption of pollutants. Thus, a combination of different experimental instruments and observation methods can provide real images and information on microscopic pore structure and element distribution of sediment particles. These results should help to improve our understanding of sediment dynamics and its environmental effects.

  2. Microprocessor system to recover data from a self-scanning photodiode array

    International Nuclear Information System (INIS)

    Koppel, L.N.; Gadd, T.J.

    1975-01-01

    A microprocessor system developed at Lawrence Livermore Laboratory has expedited the recovery of data describing the low energy x-ray spectra radiated by laser-fusion targets. An Intel microprocessor controls the digitization and scanning of the data stream of an x-ray-sensitive self-scanning photodiode array incorporated in a crystal diffraction spectrometer

  3. A superconducting electron spectrometer

    International Nuclear Information System (INIS)

    Guttormsen, M.; Huebel, H.; Grumbkow, A. von

    1983-03-01

    The set-up and tests of an electron spectrometer for in-beam conversion electron measurements are described. A superconducting solenoid is used to transport the electrons from the target to cooled Si(Li) detectors. The solenoid is designed to produce either a homogeneous axially symmetric field of up to 2 Tesla or a variety of field profiles by powering the inner and outer set of coils of the solenoid separately. The electron trajectories resulting for various field profiles are discussed. In-beam electron spectra taken in coincidence with electrons, gammas and alpha-particles are shown. (Auth.)

  4. Design of magnetic analysis system for magnetic proton recoil spectrometer

    International Nuclear Information System (INIS)

    Qi Jianmin; Jiang Shilun; Zhou Lin; Peng Taiping

    2010-01-01

    Magnetic proton recoil (MPR) spectrometer is a novel diagnostic instrument with high performance for measurements of the neutron spectra from inertial confinement fusion (ICF) experiments and high power fusion devices. The design of the magnetic analysis system, which is a key part of the compact MPR-type spectrometer, has been completed through two-dimensional beam transport simulations and three-dimensional particle transport simulation. The analysis of the system's parameters and performances was performed, as well as system designs based on preferential principles of energy resolution, detection efficiency, and count rate, respectively. The results indicate that the magnetic analysis system can achieve a detection efficiency of 10 -5 ∼ 10 -4 level at the resolution range of 1.5% to 3.0% and fulfill the design goals of the compact MPR spectrometer. (authors)

  5. Effect of secondary organic aerosol coating thickness on the real-time detection and characterization of biomass-burning soot by two particle mass spectrometers

    Directory of Open Access Journals (Sweden)

    A. T. Ahern

    2016-12-01

    Full Text Available Biomass burning is a large source of light-absorbing refractory black carbon (rBC particles with a wide range of morphologies and sizes. The net radiative forcing from these particles is strongly dependent on the amount and composition of non-light-absorbing material internally mixed with the rBC and on the morphology of the mixed particles. Understanding how the mixing state and morphology of biomass-burning aerosol evolves in the atmosphere is critical for constraining the influence of these particles on radiative forcing and climate. We investigated the response of two commercial laser-based particle mass spectrometers, the vacuum ultraviolet (VUV ablation LAAPTOF and the IR vaporization SP-AMS, to monodisperse biomass-burning particles as we sequentially coated the particles with secondary organic aerosol (SOA from α-pinene ozonolysis. We studied three mobility-selected soot core sizes, each with a number of successively thicker coatings of SOA applied. Using IR laser vaporization, the SP-AMS had different changes in sensitivity to rBC compared to potassium as a function of applied SOA coatings. We show that this is due to different effective beam widths for the IR laser vaporization region of potassium versus black carbon. The SP-AMS's sensitivity to black carbon (BC mass was not observed to plateau following successive SOA coatings, despite achieving high OA : BC mass ratios greater than 9. We also measured the ion fragmentation pattern of biomass-burning rBC and found it changed only slightly with increasing SOA mass. The average organic matter ion signal measured by the LAAPTOF demonstrated a positive correlation with the condensed SOA mass on individual particles, despite the inhomogeneity of the particle core compositions. This demonstrates that the LAAPTOF can obtain quantitative mass measurements of aged soot-particle composition from realistic biomass-burning particles with complex morphologies and composition.

  6. Identification and energy measurement of charged particles in the 50-300 MeV energy range by means of a magnet-free hardron spectrometer

    International Nuclear Information System (INIS)

    Bayukov, Yu D.; Bukiej, A.E.; Gavrilov, V.B.

    1980-01-01

    Studied are the main characteristics (efficiency, time delay and amplitude singal distribution) of a magnet-free hadron spectrometer, in which a plastic scintillator block is the main part. The plastic scintillator having the form of a cylinder of the 20 cm diameter and the 20 cm height is examined with a photomultiplier through a 50 cm light guide. The dependencies of the amplitude conversion coefficient and signal time delay on the distance between the scintillation point and the light guide are resented. The analysis of the results obtained has shown that the closer the beam passes to the light guide, the greater is the signal amplitude. The counter signal delay linearly increases with the distance increase between the beam and the light guide. The dependence of the spectrometer efficiency on the proton energy is measured as well. The investigations have proved possible utilization of the scintillation detector described for identification of charged particles in the 50-300 MeV range and measurement of their energy with the 3-8% accuracy

  7. Chemical characterization of individual microparticles using an ion trap: real-time chemical analysis of aerosol particles

    International Nuclear Information System (INIS)

    Yang, Mo; Whitten, W.B.; Reilly, P.T.A.; Gieray, R.; Ramsey, J.M.

    1996-01-01

    This paper describes initial experiments to perform laser ablation mass spectrometry in real time on airborne microparticles. The microparticles are sampled directly from the air by a particle inlet system into the vacuum chamber of a mass spectrometer. An incoming particle is detected as it passes through two CW laser beams and a pulsed laser is triggered to intercept the particle for laser ablation/ionization in the mass spectrometer. The initial studies were made with an existing ion trap mass spectrometer with the particle sampling occurring at the center of the trap electrodes. Performance of the inlet system, particle detection, and preliminary results are described

  8. Utilization of dE/dx approx E sup n /a dependence for DELTA E - E-spectrometer calibration

    CERN Document Server

    Gorpinich, O K; Jachmenov, O O

    2002-01-01

    The method of calibration of DELTA E - E-spectrometers by the use of known empiric form dE/dx approx E sup n /a which describes the specific energy loss of charge particles in the matter for energy calibration of DELTA E - E-spectrometer was designed.

  9. Using rapid-scan EPR to improve the detection limit of quantitative EPR by more than one order of magnitude.

    Science.gov (United States)

    Möser, J; Lips, K; Tseytlin, M; Eaton, G R; Eaton, S S; Schnegg, A

    2017-08-01

    X-band rapid-scan EPR was implemented on a commercially available Bruker ELEXSYS E580 spectrometer. Room temperature rapid-scan and continuous-wave EPR spectra were recorded for amorphous silicon powder samples. By comparing the resulting signal intensities the feasibility of performing quantitative rapid-scan EPR is demonstrated. For different hydrogenated amorphous silicon samples, rapid-scan EPR results in signal-to-noise improvements by factors between 10 and 50. Rapid-scan EPR is thus capable of improving the detection limit of quantitative EPR by at least one order of magnitude. In addition, we provide a recipe for setting up and calibrating a conventional pulsed and continuous-wave EPR spectrometer for rapid-scan EPR. Copyright © 2017 Elsevier Inc. All rights reserved.

  10. The circular electrical mobility spectrometer; theory, performances and applications

    International Nuclear Information System (INIS)

    Mesbah, Boualem

    1995-04-01

    A new type of electrical mobility spectrometer (S.M.E.C.) has been designed in the Service d'Etudes et de Recherches en Aerocontamination et en Confinement (CEA) laboratories. It differs from classical electrical mobility spectrometers in its plan circular geometry and its radial flow. This gives some advantages and the possibility of new applications. The theories that we derive for the different versions of this device are confirmed by experimental results obtained using aerosol particles with known electrical mobility. The S.M.E.C's performances are tested for several applications: - controlled surface contamination, - monodisperse aerosol production, - fine and ultrafine aerosol sizing. (author) [fr

  11. Superconducting RF separator for Omega Spectrometer

    CERN Multimedia

    1977-01-01

    The photo shows an Nb-deflector for the superconducting RF separator ready for installation in its cryostat (visible at the back). Each deflector was about 3 m long. L. Husson and P. Skacel (Karlsruhe) stand on the left, A. Scharding (CERN) stands on the right. This particle separator, the result of a collaboration between the Gesellshaft für Kernforschung, Karlsruhe, and CERN was installed in the S1 beam line to Omega spectrometer. (See Annual Report 1977.)

  12. Cryogenic system for a superconducting spectrometer

    International Nuclear Information System (INIS)

    Porter, J.

    1983-03-01

    The Heavy Ion Spectrometer System (HISS) relies upon superconducting coils of cryostable, pool boiling design to provide a maximum particle bending field of 3 tesla. This paper describes the cryogenic facility including helium refrigeration, gas management, liquid nitrogen system, and the overall control strategy. The system normally operates with a 4 K heat load of 150 watts; the LN 2 circuits absorb an additional 4000 watts. 80K intercept control is by an LSI 11 computer. Total available refrigeration at 4K is 400 watts using reciprocating expanders at the 20K and 4K level. The minicomputer has the capability of optimizing overall utility input cost by varying operating points. A hybrid of pneumatic, analog, and digital control is successful in providing full time unattended operation. The 7m diameter magnet/cryostat assembly is rotatable through 180 degrees to provide a variety of spectrometer orientations

  13. Strangelet search and particle production studies in Pb-Pb collisions at 158·A GeV/c with the H6 beamline spectrometer at CERN

    CERN Document Server

    Lindén, Tomas

    The charged particle beamline simulation program DECAY TURTLE (Trace Unlimited Rays Through Lumped Elements) has been modified to enable simulation of dipole magnet steering effects and simulation of hadronic interactions. These modifications together with the implementation of the measured misalignments of the magnetic elements of the H6 beamline at the CERN North Area and implementation of more accurate magnet apertures have been shown to allow a realistic simulation to be made of the complex 524 m long H6 beamline spectrometer used by NA52. The acceptance of the H6 beamline spectrometer has been computed using this modified version of DECAY TURTLE. Using these results better determined invariant differential production cross sections have been computed from the NA52 1994-1995 data, with improved error estimates. New limits for strangelet production in lead-lead collisions at 158.A GeV/c have been computed from the NA52 measurements from 1994-1995. The methods and results presented in this work can be appli...

  14. GIOVE, a shallow laboratory Ge-spectrometer with 100 μBq/kg sensitivity

    Energy Technology Data Exchange (ETDEWEB)

    Heusser, G.; Weber, M.; Denz, T.; Hakenmueller, J.; Hofacker, R.; Lackner, R.; Lindner, M.; Maneschg, W.; Reisfelder, M.; Simgen, H.; Schreiner, J.; Stolzenburg, D.; Strecker, H.; Westermann, J. [Max-Planck-Institut fuer Kernphysik, Saupfercheckweg 1, D-69117 Heidelberg (Germany)

    2013-08-08

    A new germanium gamma spectrometer called GIOVE (Germanium spectrometer with Inner and Outer Veto) has been set up at the underground/shallow laboratory (15 m w.e.) of MPI-K. Its double plastic scintillator veto system and neutron moderation interlayer lower the background by more than one order of magnitude compared to the other existing spectrometer at this facility. The integral (40-2700 keV) background rate of about 290 counts (day kg){sup −1} is just a factor 4 to 8 above that of the GeMPI spectrometers operated at LNGS (3800 m w.e.) and thus proves that even under shallow overburden sub mBq/kg sensitivities are achievable. Extended material screening and neutron attenuation studies preceded the final design of the spectrometer. The technical realization of the spectrometer is described in detail with special emphasis on the inner veto system. For its optimisation a simulation model was developed for light collection on small low activity PMT’s under various geometrical conditions. Radon suppression is accomplished by employing a gas tight sample container and a nitrogen flushed glove-box system with an airlock. The active volume of the crystal was modelled by absorption scanning measurements and Monte Carlo simulations. The complete shield is implemented in a Geant4 based simulation framework.

  15. Advances in 4D treatment planning for scanned particle beam therapy - report of dedicated workshops.

    Science.gov (United States)

    Bert, Christoph; Graeff, Christian; Riboldi, Marco; Nill, Simeon; Baroni, Guido; Knopf, Antje-Christin

    2014-12-01

    We report on recent progress in the field of mobile tumor treatment with scanned particle beams, as discussed in the latest editions of the 4D treatment planning workshop. The workshop series started in 2009, with about 20 people from 4 research institutes involved, all actively working on particle therapy delivery and development. The first workshop resulted in a summary of recommendations for the treatment of mobile targets, along with a list of requirements to apply these guidelines clinically. The increased interest in the treatment of mobile tumors led to a continuously growing number of attendees: the 2012 edition counted more than 60 participants from 20 institutions and commercial vendors. The focus of research discussions among workshop participants progressively moved from 4D treatment planning to complete 4D treatments, aiming at effective and safe treatment delivery. Current research perspectives on 4D treatments include all critical aspects of time resolved delivery, such as in-room imaging, motion detection, beam application, and quality assurance techniques. This was motivated by the start of first clinical treatments of hepato cellular tumors with a scanned particle beam, relying on gating or abdominal compression for motion mitigation. Up to date research activities emphasize significant efforts in investigating advanced motion mitigation techniques, with a specific interest in the development of dedicated tools for experimental validation. Potential improvements will be made possible in the near future through 4D optimized treatment plans that require upgrades of the currently established therapy control systems for time resolved delivery. But since also these novel optimization techniques rely on the validity of the 4DCT, research focusing on alternative 4D imaging technique, such as MRI based 4DCT generation will continue.

  16. Spherical grating spectrometers

    Science.gov (United States)

    O'Donoghue, Darragh; Clemens, J. Christopher

    2014-07-01

    We describe designs for spectrometers employing convex dispersers. The Offner spectrometer was the first such instrument; it has almost exclusively been employed on satellite platforms, and has had little impact on ground-based instruments. We have learned how to fabricate curved Volume Phase Holographic (VPH) gratings and, in contrast to the planar gratings of traditional spectrometers, describe how such devices can be used in optical/infrared spectrometers designed specifically for curved diffraction gratings. Volume Phase Holographic gratings are highly efficient compared to conventional surface relief gratings; they have become the disperser of choice in optical / NIR spectrometers. The advantage of spectrometers with curved VPH dispersers is the very small number of optical elements used (the simplest comprising a grating and a spherical mirror), as well as illumination of mirrors off axis, resulting in greater efficiency and reduction in size. We describe a "Half Offner" spectrometer, an even simpler version of the Offner spectrometer. We present an entirely novel design, the Spherical Transmission Grating Spectrometer (STGS), and discuss exemplary applications, including a design for a double-beam spectrometer without any requirement for a dichroic. This paradigm change in spectrometer design offers an alternative to all-refractive astronomical spectrometer designs, using expensive, fragile lens elements fabricated from CaF2 or even more exotic materials. The unobscured mirror layout avoids a major drawback of the previous generation of catadioptric spectrometer designs. We describe laboratory measurements of the efficiency and image quality of a curved VPH grating in a STGS design, demonstrating, simultaneously, efficiency comparable to planar VPH gratings along with good image quality. The stage is now set for construction of a prototype instrument with impressive performance.

  17. One module of the ALICE photon spectrometer

    CERN Multimedia

    Maximilien Brice

    2006-01-01

    The first module for the ALICE photon spectrometer has been completed. Each of the five modules will contain 3584 lead-tungstate crystals, a material as transparent as ordinary silica glass but with nearly four times the density. When a high-energy particle passes through one of these crystals it will scintillate, allowing the energy of electrons, positrons and photons to be measured through the 17 920 detection channels.

  18. Search for a particle with a long interaction length

    International Nuclear Information System (INIS)

    Barrowes, S.C.; Huggett, R.W.; Jones, W.V.; Levit, L.B.; Porter, L.G.

    1975-01-01

    A search has been carried out for a long-lived particle having an interaction length lambdasub(m) = 300 to 2,000 cm -2 in air. Such a particle, called the mandela, has been proposed by the Leeds group to explain an anomalous energy spectrum of particles observed near sea level with a shallow spectrometer. Data taken at mountain altitude with a deep spectrometer has been examined for compatibility with the existence of the mandela. Although the data tend to favor the mandela hypothesis the results are not conclusive and appear to be explainable by conventional means. (orig.) [de

  19. An electrostatic beam line for accelerator mass spectroscopy of exotic particles

    International Nuclear Information System (INIS)

    Elmore, D.; Kubik, P.W.; Hemmick, T.; Teng, R.; Kagan, H.; Haas, P.; Boyd, R.N.; Turner, R.; Nitz, D.; Ciampa, D.; Olsen, S.L.; Gentile, T.; Haelen, T.

    1985-01-01

    An all-electrostatic charged particle spectrometer has been constructed to perform high sensitivity searches for exotic states of matter. This spectrometer consists of an electrosatic beam line capable of mass independent charged particle transport and selection together with time-of-flight, energy loss and total energy detectors. This system has been used in conjunction with the tandem electrostatic accelerator at the Nuclear Structure Research Laboratory of the University of Rochester to search for fractionally charged or anomalously heavy particles. (orig.)

  20. Dustbuster: a New Generation Impact-ionization Time-of-flight Mass Spectrometer for in situ Analysis of Cosmic Dust

    Science.gov (United States)

    Austin, D. E.; Ahrens, T. J.; Beauchamp, J. L.

    2000-10-01

    We have developed and tested a small impact-ionization time-of-flight mass spectrometer for analysis of cosmic dust, suitable for use on deep space missions. This mass spectrometer, named Dustbuster, incorporates a large target area and a reflectron, simultaneously optimizing mass resolution, sensitivity, and collection efficiency. Dust particles hitting the 65-cm2 target plate are partially ionized. The resulting ions are accelerated through a modified reflectron that focuses the ions in space and time to produce high-resolution spectra. The instrument, shown below, measures 10 x 10 x 20 cm, has a mass of 500 g, and consumes little power. Laser desorption ionization of metal and mineral samples (embedded in the impact plate) simulates particle impacts for instrument performance tests. Mass resolution in these experiments is near 200, permitting resolution of isotopes. The mass spectrometer can be combined with other instrument components to determine dust particle trajectories and sizes. This project was funded by NASA's Planetary Instrument Definition and Development Program.

  1. Confocal scanning microscope for nuclear photoemulsion

    International Nuclear Information System (INIS)

    Batusov, Yu.A.; Kovalev, Yu.S.; Soroko, L.M.

    2005-01-01

    The application of the confocal scanning microscope to the objects in the nuclear photoemulsion is described. An array of 27 microtomograms of single silver grain is shown. The cross sections of the same particle track of diameter 1 μm, detected by means of the confocal scanning microscope with open and annular apertures, are presented. It was shown that the confocal scanning microscope opens indeed new opportunities for the nuclear photoemulsion technique to get previously inaccessible information for physics of the short-living particles

  2. A 4π tracking magnetic spectrometer for RHIC

    International Nuclear Information System (INIS)

    Lindenbaum, S.J.

    1988-01-01

    A tracking magnetic spectrometer based on large Time Projection Chambers (TPC) was previously proposed to measure the momentum of charged particles emerging from the RHIC beam pipe at angles larger than four degrees and to identify the particle type for those beyond fifteen degrees with momenta up to 700 MeV/c, which is a large fraction of the final charged particles emitted by a low cm rapidity quark-gluon plasma. Experimental progress in the successful performance of a TPC developed for AGS E-810 is reported. We have also included typical results of our event generator which contains an interface of an improved HIJET and a plasma bubble model. Typical plasma signals one can expect from this model are presented. 4 refs., 9 figs

  3. High resolution study of high mass pairs and high transverse momentum particles

    International Nuclear Information System (INIS)

    Smith, S.R.

    1983-01-01

    Preliminary experiments involving the high resolution spectrometer (experiment 605) at Fermilab are described. The spectrometer is designed for the study of pairs of particles at large invariant masses and single particles at large transverse momenta. A number of applications of the apparatus in the study of Drell-Yan processes, e.g. transverse momentum measurement, are discussed

  4. Real-time airborne particle analyzer

    Science.gov (United States)

    Reilly, Peter T.A.

    2012-10-16

    An aerosol particle analyzer includes a laser ablation chamber, a gas-filled conduit, and a mass spectrometer. The laser ablation chamber can be operated at a low pressure, which can be from 0.1 mTorr to 30 mTorr. The ablated ions are transferred into a gas-filled conduit. The gas-filled conduit reduces the electrical charge and the speed of ablated ions as they collide and mix with buffer gases in the gas-filled conduit. Preferably, the gas filled-conduit includes an electromagnetic multipole structure that collimates the nascent ions into a beam, which is guided into the mass spectrometer. Because the gas-filled conduit allows storage of vast quantities of the ions from the ablated particles, the ions from a single ablated particle can be analyzed multiple times and by a variety of techniques to supply statistically meaningful analysis of composition and isotope ratios.

  5. Silicon Microleaks for Inlets of Mass Spectrometers

    Science.gov (United States)

    Harpold, Dan; Hasso, Niemann; Jamieson, Brian G.; Lynch, Bernard A.

    2009-01-01

    Microleaks for inlets of mass spectrometers used to analyze atmospheric gases can be fabricated in silicon wafers by means of photolithography, etching, and other techniques that are commonly used in the manufacture of integrated circuits and microelectromechanical systems. The microleaks serve to limit the flows of the gases into the mass-spectrometer vacuums to specified very small flow rates consistent with the capacities of the spectrometer vacuum pumps. There is a need to be able to precisely tailor the dimensions of each microleak so as to tailor its conductance to a precise low value. (As used here, "conductance" signifies the ratio between the rate of flow in the leak and the pressure drop from the upstream to the downstream end of the leak.) To date, microleaks have been made, variously, of crimped metal tubes, pulled glass tubes, or frits. Crimped-metal and pulled-glass-tube microleaks cannot readily be fabricated repeatably to precise dimensions and are susceptible to clogging with droplets or particles. Frits tend to be differentially chemically reactive with various gas constituents and, hence, to distort the gas mixtures to be analyzed. The present approach involving microfabrication in silicon largely overcomes the disadvantages of the prior approaches.

  6. Calculation of Multisphere Neutron Spectrometer Response Functions in Energy Range up to 20 MeV

    CERN Document Server

    Martinkovic, J

    2005-01-01

    Multisphere neutron spectrometer is a basic instrument of neutron measurements in the scattered radiation field at charged-particles accelerators for radiation protection and dosimetry purposes. The precise calculation of the spectrometer response functions is a necessary condition of the propriety of neutron spectra unfolding. The results of the response functions calculation for the JINR spectrometer with LiI(Eu) detector (a set of 6 homogeneous and 1 heterogeneous moderators, "bare" detector within cadmium cover and without it) at two geometries of the spectrometer irradiation - in uniform monodirectional and uniform isotropic neutron fields - are given. The calculation was carried out by the code MCNP in the neutron energy range 10$^{-8}$-20 MeV.

  7. Source apportionment of aerosol particles using polycapillary slightly focusing X-ray lens

    Energy Technology Data Exchange (ETDEWEB)

    Sun Tianxi [Key Laboratory of Beam Technology and Materials Modification of Ministry of Education, Beijing Normal University, Beijing 100875 (China) and Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing 100875 (China) and Beijing Radiation Center, Beijing 100875 (China)], E-mail: stxbeijing@163.com; Liu Zhiguo [Key Laboratory of Beam Technology and Materials Modification of Ministry of Education, Beijing Normal University, Beijing 100875 (China) and Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing 100875 (China) and Beijing Radiation Center, Beijing 100875 (China)], E-mail: liuzgbeijing@163.com; Zhu Guanghua; Liu Hui [Key Laboratory of Beam Technology and Materials Modification of Ministry of Education, Beijing Normal University, Beijing 100875 (China); Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing 100875 (China); Beijing Radiation Center, Beijing 100875 (China); Ma Yongzhong [Center for Disease Control and Prevention of Beijing, Beijing 100013 (China); Xu Qing [Institute of High Energy Physics, Chinese Academy of Science, Beijing 100039 (China); Li Yude; Wang Guangpu; Luo Ping; Pan Qiuli; Ding Xunliang [Key Laboratory of Beam Technology and Materials Modification of Ministry of Education, Beijing Normal University, Beijing 100875 (China); Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing 100875 (China); Beijing Radiation Center, Beijing 100875 (China)

    2009-06-11

    A micro-X-ray fluorescence (Micro-XRF) spectrometer based on a polycapillary slightly focusing X-ray lens (PSFXRL) and laboratory X-ray source was designed to carry out the source apportionment of aerosol particles. In the distribution curve of the X-ray intensity in the focal spot of PSFXRL, there was a plateau with a diameter of about 65 {mu}m. The uniformity of this plateau was about 3%. This was helpful in measuring the XRF spectrum of a single aerosol particle in which the element distributions are not uniform. The minimum detection limit (MDL) of this Micro-XRF spectrometer was 15 ppm for the Fe-K{sub {alpha}}. The origins of the aerosol particles at the exit of a subway station and a construction site were apportioned. This Micro-XRF spectrometer has potential applications in analysis of single aerosol particles.

  8. First test model of the optical microscope which images the whole vertical particle tracks without any depth scanning

    International Nuclear Information System (INIS)

    Soroko, L.M.

    2001-01-01

    The first test model of the optical microscope which produces the in focus image of the whole vertical particle track without depth scanning is described. The in focus image of the object consisting of the linear array of the point-like elements was obtained. A comparison with primary out of focus image of such an object has been made

  9. The ANTARES recoil time-of-flight spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Martin, J.W.; Russell, G.J. [New South Wales Univ., Kensington, NSW (Australia); Cohen, D.D.; Dytlewski, N. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1996-12-31

    The Australian National Tandem for Applied Research (ANTARES), is a 8MV FN tandem particle accelerator at the Australian Nuclear Science and Technology Organisation. Research on the accelerator is divided between two groups, Accelerator Mass Spectrometry (AMS) and lon Beam Analysis (IBA). The IBA group carries out a range of research projects from nuclear physics to materials characterisation. The major IBA project on the accelerator is a recoil time-of-flight spectrometer which consists of two electrostatic time pulse generators and an ion-implanted surface barrier detector. The spectrometer is ideally suited to the profiling of layered multi-element materials, and has been used to characterise materials such as metal-germanides, optoelectronics, superconductors and catalytic converters. This paper will describe the time-of-flight system as well as some recent materials characterisation results. 1 refs., 3 figs.

  10. The ANTARES recoil time-of-flight spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Martin, J W; Russell, G J [New South Wales Univ., Kensington, NSW (Australia); Cohen, D D; Dytlewski, N [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1997-12-31

    The Australian National Tandem for Applied Research (ANTARES), is a 8MV FN tandem particle accelerator at the Australian Nuclear Science and Technology Organisation. Research on the accelerator is divided between two groups, Accelerator Mass Spectrometry (AMS) and lon Beam Analysis (IBA). The IBA group carries out a range of research projects from nuclear physics to materials characterisation. The major IBA project on the accelerator is a recoil time-of-flight spectrometer which consists of two electrostatic time pulse generators and an ion-implanted surface barrier detector. The spectrometer is ideally suited to the profiling of layered multi-element materials, and has been used to characterise materials such as metal-germanides, optoelectronics, superconductors and catalytic converters. This paper will describe the time-of-flight system as well as some recent materials characterisation results. 1 refs., 3 figs.

  11. Correlation spectrometer

    Science.gov (United States)

    Sinclair, Michael B [Albuquerque, NM; Pfeifer, Kent B [Los Lunas, NM; Flemming, Jeb H [Albuquerque, NM; Jones, Gary D [Tijeras, NM; Tigges, Chris P [Albuquerque, NM

    2010-04-13

    A correlation spectrometer can detect a large number of gaseous compounds, or chemical species, with a species-specific mask wheel. In this mode, the spectrometer is optimized for the direct measurement of individual target compounds. Additionally, the spectrometer can measure the transmission spectrum from a given sample of gas. In this mode, infrared light is passed through a gas sample and the infrared transmission signature of the gasses present is recorded and measured using Hadamard encoding techniques. The spectrometer can detect the transmission or emission spectra in any system where multiple species are present in a generally known volume.

  12. H∞ Robust Control of a Large-Piston MEMS Micromirror for Compact Fourier Transform Spectrometer Systems

    Directory of Open Access Journals (Sweden)

    Huipeng Chen

    2018-02-01

    Full Text Available Incorporating linear-scanning micro-electro-mechanical systems (MEMS micromirrors into Fourier transform spectral acquisition systems can greatly reduce the size of the spectrometer equipment, making portable Fourier transform spectrometers (FTS possible. How to minimize the tilting of the MEMS mirror plate during its large linear scan is a major problem in this application. In this work, an FTS system has been constructed based on a biaxial MEMS micromirror with a large-piston displacement of 180 μm, and a biaxial H∞ robust controller is designed. Compared with open-loop control and proportional-integral-derivative (PID closed-loop control, H∞ robust control has good stability and robustness. The experimental results show that the stable scanning displacement reaches 110.9 μm under the H∞ robust control, and the tilting angle of the MEMS mirror plate in that full scanning range falls within ±0.0014°. Without control, the FTS system cannot generate meaningful spectra. In contrast, the FTS yields a clean spectrum with a full width at half maximum (FWHM spectral linewidth of 96 cm−1 under the H∞ robust control. Moreover, the FTS system can maintain good stability and robustness under various driving conditions.

  13. H∞ Robust Control of a Large-Piston MEMS Micromirror for Compact Fourier Transform Spectrometer Systems.

    Science.gov (United States)

    Chen, Huipeng; Li, Mengyuan; Zhang, Yi; Xie, Huikai; Chen, Chang; Peng, Zhangming; Su, Shaohui

    2018-02-08

    Incorporating linear-scanning micro-electro-mechanical systems (MEMS) micromirrors into Fourier transform spectral acquisition systems can greatly reduce the size of the spectrometer equipment, making portable Fourier transform spectrometers (FTS) possible. How to minimize the tilting of the MEMS mirror plate during its large linear scan is a major problem in this application. In this work, an FTS system has been constructed based on a biaxial MEMS micromirror with a large-piston displacement of 180 μm, and a biaxial H∞ robust controller is designed. Compared with open-loop control and proportional-integral-derivative (PID) closed-loop control, H∞ robust control has good stability and robustness. The experimental results show that the stable scanning displacement reaches 110.9 μm under the H∞ robust control, and the tilting angle of the MEMS mirror plate in that full scanning range falls within ±0.0014°. Without control, the FTS system cannot generate meaningful spectra. In contrast, the FTS yields a clean spectrum with a full width at half maximum (FWHM) spectral linewidth of 96 cm -1 under the H∞ robust control. Moreover, the FTS system can maintain good stability and robustness under various driving conditions.

  14. On the simultaneous deployment of two single-particle mass spectrometers at an urban background and a roadside site during SAPUSS

    Directory of Open Access Journals (Sweden)

    M. Dall'Osto

    2016-08-01

    Full Text Available The aerosol time-of-flight mass spectrometer (ATOFMS provides size-resolved information on the chemical composition of single particles with high time resolution. Within SAPUSS (Solving Aerosol Problems by Using Synergistic Strategies, continuous ATOFMS measurements of ambient particles were made simultaneously at two urban locations: urban background (UB site and roadside (RS site in the city of Barcelona (Spain from 17 September to 18 October 2010. Two different instrumental configurations were used: ATOFMS (TSI 3800 with a converging nozzle inlet (high efficiency at about 800–2000 nm at the UB site and ATOFMS (TSI 3800-100 with an aerodynamic lens inlet (high efficiency at about 300–700 nm at the RS site. This is the first time, to our knowledge, that two ATOFMS instruments have been deployed in the same field study. The different instrument configurations had an impact on the observed particle types at the two sites. Nevertheless, 10 particle types were detected at both locations, including local and regional elemental carbon (22.7–58.9 % of total particles, fresh and aged sea salt (1.0–14.6 %, local and regional nitrate-containing aerosols (3–11.6 %, local lead-containing metallic particles (0.1–0.2 %, and transported Fe-nitrate particles (0.8–2.5 %. The ATOFMS at the UB also characterized four particle types: calcium-containing dust (0.9 %, Saharan dust (1.3 %, vanadium-containing particles (0.9 %, and vegetative debris (1.7 %. By contrast, the high statistical counts of fine particles detected at the RS allowed identification of eight particle types. Four of these contained organic nitrogen of primary and secondary origin, which highlights the complex nature of the sources and processes that contribute to this aerosol chemical component. Aminium salts were found related to coarse sulfate-rich particle types, suggesting heterogeneous reaction mechanisms for their formation. The other four particle

  15. Interfacing an aspiration ion mobility spectrometer to a triple quadrupole mass spectrometer

    International Nuclear Information System (INIS)

    Adamov, Alexey; Viidanoja, Jyrki; Kaerpaenoja, Esko; Paakkanen, Heikki; Ketola, Raimo A.; Kostiainen, Risto; Sysoev, Alexey; Kotiaho, Tapio

    2007-01-01

    This article presents the combination of an aspiration-type ion mobility spectrometer with a mass spectrometer. The interface between the aspiration ion mobility spectrometer and the mass spectrometer was designed to allow for quick mounting of the aspiration ion mobility spectrometer onto a Sciex API-300 triple quadrupole mass spectrometer. The developed instrumentation is used for gathering fundamental information on aspiration ion mobility spectrometry. Performance of the instrument is demonstrated using 2,6-di-tert-butyl pyridine and dimethyl methylphosphonate

  16. Project for a high resolution magnetic spectrometer for heavy ions

    International Nuclear Information System (INIS)

    Birien, P.; Valero, S.

    1981-05-01

    The energy loss spectrometer presented in this report has an energy resolution of 2x10 -4 with the full solid angle of 5 msr. The maximum magnetic rigidity of the particles analysed is 2.88 Tesla-meters on the optical axis and the total acceptance in energy is 14%. Experiments with reaction angles near 0 0 are possible. Kinematic compensation is adapted to heavy ion physics. In this report, we have paid special attention to the simplicity of the construction and of the use of this spectrometer by experimentalists. This report is addressed both to non-specialists and to future users as well [fr

  17. Piotron at SIN - a large superconducting double torus spectrometer

    International Nuclear Information System (INIS)

    Horvath, I.; Vecsey, G.; Zellweger, J.

    1981-01-01

    A test facility for radiation therapy with negative /pi/-mesons was constructed in Switzerland. The facility is a large double torus spectrometer similar to the Stanford design. For variation of stopping depth different momenta are selected by variation of the magnetic field. Superconducting ac magnets are necessary for tumor scanning and represent a major part of such a facility. Main design features and performance are reported. 10 refs

  18. Computation of the magnetic field of a spectrometer in detectors region

    International Nuclear Information System (INIS)

    Zhidkov, E.P.; Yuldasheva, M.B.; Yudin, I.P.; Yuldashev, O.I.

    1995-01-01

    Computed results of the 3D magnetic field of a spectrometer intended for investigation of hadron production of charmed particles and the indication of the narrow resonances in neutron-nucleus interactions are presented. The methods used in computations: finite element method and finite element method with suggested new infinite elements are described. For accuracy control the computations were carried out on a sequence of three-dimensional meshes. Special attention is devoted to behaviour of the magnetic field in the basic detector (proportional chambers) region. The performed results can be used for the field behaviour estimate of similar spectrometer magnets. (orig.)

  19. Dosimetric consequences of pencil beam width variations in scanned beam particle therapy

    International Nuclear Information System (INIS)

    Chanrion, M A; Ammazzalorso, F; Wittig, A; Engenhart-Cabillic, R; Jelen, U

    2013-01-01

    Scanned ion beam delivery enables the highest degree of target dose conformation attainable in external beam radiotherapy. Nominal pencil beam widths (spot sizes) are recorded during treatment planning system commissioning. Due to changes in the beam-line optics, the actual spot sizes may differ from these commissioning values, leading to differences between planned and delivered dose. The purpose of this study was to analyse the dosimetric consequences of spot size variations in particle therapy treatment plans. For 12 patients with skull base tumours and 12 patients with prostate carcinoma, scanned-beam carbon ion and proton treatment plans were prepared and recomputed simulating spot size changes of (1) ±10% to simulate the typical magnitude of fluctuations, (2) ±25% representing the worst-case scenario and (3) ±50% as a part of a risk analysis in case of fault conditions. The primary effect of the spot size variation was a dose deterioration affecting the target edge: loss of target coverage and broadening of the lateral penumbra (increased spot size) or overdosage and contraction of the lateral penumbra (reduced spot size). For changes ⩽25%, the resulting planning target volume mean 95%-isodose line coverage (CI-95%) deterioration was ranging from negligible to moderate. In some cases changes in the dose to adjoining critical structures were observed. (paper)

  20. Magnetic spectrometer of the DEUTERON-2 set-up

    International Nuclear Information System (INIS)

    Ajvazyan, R.V.; Alanakyan, K.V.; Amaryan, M.J.

    1989-01-01

    A magnetic spectrometer of the two-arm DEUTERON-2 set-up of the Erevan Physical Institute is described. It is shown that the rejection factor for electrons and pions is 10 -2 - 10 -3 . The positively charged particles in the momentum range up to 1.5 GeV/c are identified by momentum and time-of-flight measurements. The main characteristics of the spectrometer are: momentum and angular acceptance δp/p = 46%, Δθ = 4 deg, solid angle ΔΩ = 2.75 msr, momentum resolution δp/p = 1.5%, angular resolutions δθ = 0.6 deg, δφ = 2 deg. The intervals of measured momentum and the polar scattering anlge are 0.5-3 GeV/c and 10-30 deg, 68-90 deg respectively. 7 refs.; 11 figs

  1. New approach to determine the angular transmission in zero-degree magnetic spectrometers

    International Nuclear Information System (INIS)

    Benlliure, J.; Pereira-Conca, J.; Schmidt, K.H.

    2000-11-01

    A new method to estimate the angular transmission in zero-degree magnetic spectrometers is presented. This method is based on a parameterisation of the angular aperture of the spectrometer for any possible value of the magnetic rigidity of the transmitted particles. This parameterisation of the angular aperture together with a description of the kinematics of the reaction mechanism allows to determine the angular transmission analytically, avoiding tedious Monte-Carlo calculations. The analytical solutions are implemented for residual nuclei produced in fission, projectile-fragmentation and fusion-evaporation reactions. (orig.)

  2. Possible physics program with a large acceptance hyperon spectrometer at J-PARC

    International Nuclear Information System (INIS)

    Imai, Kenichi

    2013-01-01

    We are going to construct a large acceptance hyperon spectrometer (HypTPC) at J-PARC primarily to search for H-dibaryon. The HypTPC consists of a superconducting Helmholtz magnet and a Time Projection Chamber (TPC). The short-life hyperons can be detected with high precision as well as any charged particles. Here, we discuss possible physics programs other than H-dibaryon which can be done with this spectrometer, such as a nucleon resonance spectroscopy experiment, systematic study of Λ(1405) and spectroscopy of Ξ and Ω - resonances. (author)

  3. Upgrade of the NASA 4STAR (Spectrometer for Sky-Scanning, Sun-Tracking Atmospheric Research) to its Full Science Capability of Sun-Sky-Cloud-Trace Gas Spectrometry in Airborne Science Deployments

    Science.gov (United States)

    Johnson, Roy R.; Russell, P.; Dunagan, S.; Redemann, J.; Shinozuka, Y.; Segal-Rosenheimer, M.; LeBlanc, S.; Flynn, C.; Schmid, B.; Livingston, J.

    2014-01-01

    The objectives of this task in the AITT (Airborne Instrument Technology Transition) Program are to (1) upgrade the NASA 4STAR (Spectrometer for Sky-Scanning, Sun-Tracking Atmospheric Research) instrument to its full science capability of measuring (a) direct-beam sun transmission to derive aerosol optical depth spectra, (b) sky radiance vs scattering angle to retrieve aerosol absorption and type (via complex refractive index spectra, shape, and mode-resolved size distribution), (c) zenith radiance for cloud properties, and (d) hyperspectral signals for trace gas retrievals, and (2) demonstrate its suitability for deployment in challenging NASA airborne multiinstrument campaigns. 4STAR combines airborne sun tracking, sky scanning, and zenith pointing with diffraction spectroscopy to improve knowledge of atmospheric constituents and their links to air pollution, radiant energy budgets (hence climate), and remote measurements of Earth's surfaces. Direct beam hyperspectral measurement of optical depth improves retrievals of gas constituents and determination of aerosol properties. Sky scanning enhances retrievals of aerosol type and size distribution. 4STAR measurements are intended to tighten the closure between satellite and ground-based measurements. 4STAR incorporates a modular sun-tracking/sky-scanning optical head with fiber optic signal transmission to rack mounted spectrometers, permitting miniaturization of the external optical head, and future detector evolution. 4STAR test flights, as well as science flights in the 2012-13 TCAP (Two-Column Aerosol Project) and 2013 SEAC4RS (Studies of Emissions and Atmospheric Composition, Clouds and Climate Coupling by Regional Surveys) have demonstrated that the following are essential for 4STAR to achieve its full science potential: (1) Calibration stability for both direct-beam irradiance and sky radiance, (2) Improved light collection and usage, and (3) Improved flight operability and reliability. A particular challenge

  4. Do it yourself: optical spectrometer for physics undergraduate instruction in nanomaterial characterization

    International Nuclear Information System (INIS)

    Nuryantini, Ade Yeti; Mahen, Ea Cahya Septia; Sawitri, Asti; Nuryadin, Bebeh Wahid

    2017-01-01

    In this paper, we report on a homemade optical spectrometer using diffraction grating and image processing techniques. This device was designed to produce spectral images that could then be processed by measuring signal strength (pixel intensity) to obtain the light source, transmittance, and absorbance spectra of the liquid sample. The homemade optical spectrometer consisted of: (i) a white LED as a light source, (ii) a cuvette or sample holder, (iii) a slit, (iv) a diffraction grating, and (v) a CMOS camera (webcam). In this study, various concentrations of a carbon nanoparticle (CNP) colloid were used in the particle size sample test. Additionally, a commercial optical spectrometer and tunneling electron microscope (TEM) were used to characterize the optical properties and morphology of the CNPs, respectively. The data obtained using the homemade optical spectrometer, commercial optical spectrometer, and TEM showed similar results and trends. Lastly, the calculation and measurement of CNP size were performed using the effective mass approximation (EMA) and TEM. These data showed that the average nanoparticle sizes were approximately 2.4 nm and 2.5 ± 0.3 nm, respectively. This research provides new insights into the development of a portable, simple, and low-cost optical spectrometer that can be used in nanomaterial characterization for physics undergraduate instruction. (paper)

  5. Broadband crystal spectrometer for the non-active and active phases of JET

    International Nuclear Information System (INIS)

    Engelhardt, W.; Fink, J.; Fussmann, G.; Krause, H.; Schilling, H.B.; Schumacher, U.

    1982-03-01

    The design study treats the possibilities of quantitatively measuring the Soft X-ray spectrum of JET with a double crystal spectrometer device in parallel mode. This spectrometer type is much suited for broad band soft X-ray spectroscopy, also - due to its folded optical pathway - during D-T operation of JET; the expected detector count rates are far above the background level. Methods to fulfill the important condition of parallel orientation of the two crystals, to shield the device against neutrons and gamma rays, to obtain spectral resolution sufficient for spectral line profile measurements and to upgrade the device for continuous spatial scanning of the JET plasma are presented. (orig.)

  6. The new double energy-velocity spectrometer VERDI

    Science.gov (United States)

    Jansson, Kaj; Frégeau, Marc Olivier; Al-Adili, Ali; Göök, Alf; Gustavsson, Cecilia; Hambsch, Franz-Josef; Oberstedt, Stephan; Pomp, Stephan

    2017-09-01

    VERDI (VElocity foR Direct particle Identification) is a fission-fragment spectrometer recently put into operation at JRC-Geel. It allows measuring the kinetic energy and velocity of both fission fragments simultaneously. The velocity provides information about the pre-neutron mass of each fission fragment when isotropic prompt-neutron emission from the fragments is assumed. The kinetic energy, in combination with the velocity, provides the post-neutron mass. From the difference between pre- and post-neutron masses, the number of neutrons emitted by each fragment can be determined. Multiplicity as a function of fragment mass and total kinetic energy is one important ingredient, essential for understanding the sharing of excitation energy between fission fragments at scission, and may be used to benchmark nuclear de-excitation models. The VERDI spectrometer design is a compromise between geometrical efficiency and mass resolution. The spectrometer consists of an electron detector located close to the target and two arrays of silicon detectors, each located 50 cm away from the target. In the present configuration pre-neutron and post-neutron mass distributions are in good agreement with reference data were obtained. Our latest measurements performed with spontaneously fissioning 252Cf is presented along with the developed calibration procedure to obtain pulse height defect and plasma delay time corrections.

  7. Pollutants identification of ambient aerosols by two types of aerosol mass spectrometers over southeast coastal area, China.

    Science.gov (United States)

    Yan, Jinpei; Chen, Liqi; Lin, Qi; Zhao, Shuhui; Li, Lei

    2018-02-01

    Two different aerosol mass spectrometers, Aerodyne Aerosol Mass Spectrometer (AMS) and Single Particle Aerosol Mass Spectrometer (SPAMS) were deployed to identify the aerosol pollutants over Xiamen, representing the coastal urban area. Five obvious processes were classified during the whole observation period. Organics and sulfate were the dominant components in ambient aerosols over Xiamen. Most of the particles were in the size range of 0.2-1.0μm, accounting for over 97% of the total particles measured by both instruments. Organics, as well as sulfate, measured by AMS were in good correlation with measured by SPAMS. However, high concentration of NH 4 + was obtained by AMS, while extremely low value of NH 4 + was detected by SPAMS. Contrarily, high particle number counts of NO 3 - and Cl - were given by SPAMS while low concentrations of NO 3 - and Cl - were measured by AMS. The variations of POA and SOA obtained from SPAMS during event 1 and event 2 were in accordance with the analysis of HOA and OOA given by AMS, suggesting that both of AMS and SPAMS can well identify the organic clusters of aerosol particles. Overestimate or underestimate of the aerosol sources and acidity would be present in some circumstances when the measurement results were used to analyze the aerosol properties, because of the detection loss of some species for both instruments. Copyright © 2017. Published by Elsevier B.V.

  8. Possibilities of magnet prism β-spectrometer application in on-line experiments

    International Nuclear Information System (INIS)

    Akhmetov, K.M.; Arynov, S.

    1996-01-01

    The main attention is paid to works with particle beam in up-to-date nuclear investigations. The application of magnet prism β-spectrometer for works in 'on-line' experiments is considered in this article. The source chamber and detector chamber are distanted from each other on great distance (4 m) and are out of operation field of spectrometer. There is a reliable defence of operating field of device from external parasitic fields by the magnetic screens system. The additional advantage is a factor that source (target) and detector could replacing in specific directions about few centimetres during the device operating. The main β-spectroscopic performances of device are compared with Grenoble spectroscopic complex. The liner depression of prism spectrometer account for from 3,6 up to 6 m; light force - from 2·10 -4 up to 6·10 -4 up to 4π; operating resolving power - 0,02-0,05% by impulse. Investigation range is from several keV up to 3 MeV. There are all opportunities for installing of the on-line magnetic prism spectrometer on the U-150 accelerator and the WWR-K reactor. Spectrometer application in 'on-line' experiments gives possibility to obtain more wide information. 4 refs

  9. Fullerene Soot in Eastern China Air: Results from Soot Particle-Aerosol Mass Spectrometer

    Science.gov (United States)

    Wang, J.; Ge, X.; Chen, M.; Zhang, Q.; Yu, H.; Sun, Y.; Worsnop, D. R.; Collier, S.

    2015-12-01

    In this work, we present for the first time, the observation and quantification of fullerenes in ambient airborne particulate using an Aerodyne Soot Particle - Aerosol Mass Spectrometer (SP-AMS) deployed during 2015 winter in suburban Nanjing, a megacity in eastern China. The laser desorption and electron impact ionization techniques employed by the SP-AMS allow us to differentiate various fullerenes from other aerosol components. Mass spectrum of the identified fullerene soot is consisted by a series of high molecular weight carbon clusters (up to m/z of 2000 in this study), almost identical to the spectral features of commercially available fullerene soot, both with C70 and C60 clusters as the first and second most abundant species. This type of soot was observed throughout the entire study period, with an average mass loading of 0.18 μg/m3, accounting for 6.4% of the black carbon mass, 1.2% of the total organic mass. Temporal variation and diurnal pattern of fullerene soot are overall similar to those of black carbon, but are clearly different in some periods. Combining the positive matrix factorization, back-trajectory and analyses of the meteorological parameters, we identified the petrochemical industrial plants situating upwind from the sampling site, as the major source of fullerene soot. In this regard, our findings imply the ubiquitous presence of fullerene soot in ambient air of industry-influenced area, especially the oil and gas production regions. This study also offers new insights into the characterization of fullerenes from other environmental samples via the advanced SP-AMS technique.

  10. A semiconductor beta ray spectrometer

    International Nuclear Information System (INIS)

    Bom, V.R.

    1987-01-01

    Measurement of energy spectra of beta particles emitted from nuclei in beta-decay processes provides information concerning the mass difference of these nuclei between initial and final state. Moreover, experimental beta spectra yield information on the feeding of the levels in the daughter nucleus. Such data are valuable in the construction and checking of the level schemes. This thesis describes the design, construction, testing and usage of a detector for the accurate measurement of the mentioned spectra. In ch. 2 the design and construction of the beta spectrometer, which uses a hyper-pure germanium crystal for energy determination, is described. A simple wire chamber is used to discriminate beta particles from gamma radiation. Disadvantages arise from the large amounts of scattered beta particles deforming the continua. A method is described to minimize the scattering. In ch. 3 some theoretical aspects of data analysis are described and the results of Monte-Carlo simulations of the summation of annihilation radiation are compared with experiments. Ch. 4 comprises the results of the measurements of the beta decay energies of 103-108 In. 87 refs.; 34 figs.; 7 tabs

  11. The design and performance of a velocity map imaging spectrometer for the study of molecular photoionisation dynamics

    Energy Technology Data Exchange (ETDEWEB)

    Holland, D.M.P., E-mail: david.holland@stfc.ac.uk [Daresbury Laboratory, Daresbury, Warrington, Cheshire WA4 4AD (United Kingdom); Shaw, D.A. [Daresbury Laboratory, Daresbury, Warrington, Cheshire WA4 4AD (United Kingdom)

    2012-12-10

    Highlights: Black-Right-Pointing-Pointer Velocity map imaging spectrometer optimised for molecular photoionisation dynamics. Black-Right-Pointing-Pointer Kinetic energy distribution of O{sup +} fragments measured. Black-Right-Pointing-Pointer Effect of autoionisation on photoelectron vibrational populations studied. -- Abstract: The design, construction and performance of a velocity map imaging spectrometer for the study of molecular photoionisation dynamics is described. The spectrometer has been optimised for the efficient collection and detection of particles (electrons or positively charged ions) generated through the interaction of gas phase molecules with synchrotron radiation. A double Einzel lens, incorporated into the flight tube, enhances the collection efficiency of energetic particles. Computer modelling has been used to trace the trajectories of charged particles through the spectrometer and to assess the image quality. A time and position sensitive delay-line detector is used to record the images. Results from two experimental studies are presented to illustrate the capabilities of the spectrometer. In the first, the effect of electronic autoionisation on the vibrationally resolved photoelectron branching ratios of the N{sub 2}{sup +} X {sup 2}{Sigma}{sub g}{sup +} state has been investigated in an excitation range where prominent structure due to Rydberg states occurs in the ion yield curve. The results show that autoionisation leads to rotational branch populations that differ from those observed in direct, non-resonant, photoionisation. In the second, the kinetic energy distribution and the angular distribution of O{sup +} fragments formed in the dissociative photoionisation of molecular oxygen have been measured. The timing properties of the detector have allowed O{sup +} fragments to be separated from O{sub 2}{sup +} parent ions using time-of-flight techniques.

  12. Particles identification using nuclear emulsion in OPERA

    International Nuclear Information System (INIS)

    Manai, K.

    2007-10-01

    The Opera experiment will try to confirm the ν μ → ν τ oscillations by the appearance of the ν τ in a pure ν μ beam. Indeed, a neutrino beam almost pure is produced at CERN (CNGS Beam) and sent to the Opera detector. The detector is composed of two muons spectrometers and a target formed by walls of bricks. Each brick is an alternation of lead plates and emulsions. This modular structure allows to reconstruct the kink topology of the τ lepton decay with a high spatial resolution. The great challenge of the Opera experiment is to detect the ν τ interactions with the less uncertainty. To reduce this uncertainty it is essential to identify with the greatest efficiency any background event not including a tau particle. My work permits to reduce background. My principal contribution concerns the selection development, the reconstruction and the muons identification at low energy. This work is based on the setting of variables related to the deposit energy and the multiple scattering. Previously, only deposit energy was used in the analyses of pion/muon separation. This study allows doubling the muon identification efficiency at low energy. This leads to increase the background events rejection in Opera and to decrease the contamination by 30%. I also studied the nuclear emulsions capacity to identify charged particles through the analysis of a test beam carried out by the Nagoya group. This test contains protons and pions with different energies. My work proves that the European scan system gives comparable results with those obtained by the Japanese scan system. (author)

  13. Synthesis of hydroxyapatite particles in catanionic mixed surfactants template

    International Nuclear Information System (INIS)

    Tari, Nesa Esmaeilian; Kashani Motlagh, Mohammad M.; Sohrabi, Beheshteh

    2011-01-01

    Highlights: ►The mixture of cetyltrimethyl ammonium bromide (CTAB) and sodium dodecyl sulfate (SDS) with different ratio were used as the template for synthesizing HAP particles. ► The overall morphology of the obtained powders at anionic-rich region (SDS:CTAB, 99:1) solution is rod like with high regularity. ► In the presence of cationic rich region (SDS:CTAB, 1:99) the resulted particles was sheet like. ► The resulted HAP nano particles in the presence of SDS were rod like but their morphology was less oriented than anionic-rich region. - Abstract: Different morphologies of nano hydroxyapatite particles, Ca 10 (PO 4 ) 6 (OH) 2 (HAP) are prepared by precipitation method using CaCl 2 and H 3 PO 4 (water phase) and the mixture of cationic surfactant cetyltrimethyl ammonium bromide (CTAB) and anionic one sodium dodecyl sulfate (SDS) as template. The mixture of these surfactants in two regions of cationic-rich and anionic-rich form the various aggregations as template. The results show that by changing the ratio of cationic to anionic surfactant in the mixture the morphology of the nano HAP can be controlled. The nano structure of products is studied by the means of X-ray diffraction (XRD), Fourier transmission infrared spectrometer (FT-IR) and scanning electron microscopy (SEM). With this system we could synthesize nano particles of hydroxyapatite with high crystallinity and least agglomeration.

  14. Synthesis of hydroxyapatite particles in catanionic mixed surfactants template

    Energy Technology Data Exchange (ETDEWEB)

    Tari, Nesa Esmaeilian [Department of Chemistry, Iran University of Science and Technology, Resalat Square, Hengam Street, Tehran (Iran, Islamic Republic of); Kashani Motlagh, Mohammad M., E-mail: M.Kashani@iust.ac.ir [Department of Chemistry, Iran University of Science and Technology, Resalat Square, Hengam Street, Tehran (Iran, Islamic Republic of); Sohrabi, Beheshteh [Department of Chemistry, Iran University of Science and Technology, Resalat Square, Hengam Street, Tehran (Iran, Islamic Republic of)

    2011-12-15

    Highlights: Black-Right-Pointing-Pointer The mixture of cetyltrimethyl ammonium bromide (CTAB) and sodium dodecyl sulfate (SDS) with different ratio were used as the template for synthesizing HAP particles. Black-Right-Pointing-Pointer The overall morphology of the obtained powders at anionic-rich region (SDS:CTAB, 99:1) solution is rod like with high regularity. Black-Right-Pointing-Pointer In the presence of cationic rich region (SDS:CTAB, 1:99) the resulted particles was sheet like. Black-Right-Pointing-Pointer The resulted HAP nano particles in the presence of SDS were rod like but their morphology was less oriented than anionic-rich region. - Abstract: Different morphologies of nano hydroxyapatite particles, Ca{sub 10}(PO{sub 4}){sub 6}(OH){sub 2} (HAP) are prepared by precipitation method using CaCl{sub 2} and H{sub 3}PO{sub 4} (water phase) and the mixture of cationic surfactant cetyltrimethyl ammonium bromide (CTAB) and anionic one sodium dodecyl sulfate (SDS) as template. The mixture of these surfactants in two regions of cationic-rich and anionic-rich form the various aggregations as template. The results show that by changing the ratio of cationic to anionic surfactant in the mixture the morphology of the nano HAP can be controlled. The nano structure of products is studied by the means of X-ray diffraction (XRD), Fourier transmission infrared spectrometer (FT-IR) and scanning electron microscopy (SEM). With this system we could synthesize nano particles of hydroxyapatite with high crystallinity and least agglomeration.

  15. Preparation of Ti-coated diamond particles by microwave heating

    International Nuclear Information System (INIS)

    Gu, Quanchao; Peng, Jinghui; Xu, Lei; Srinivasakannan, C.

    2016-01-01

    Highlights: • The Ti-Coated diamond particles have been prepared using by microwave heating. • The uniform and dense coating can be produced, and the TiC species was formed. • With increases the temperature results in the thickness of coating increased. • The coating/diamond interfacial bonding strength increased with temperature increasing until 760 °C, then decreased. - Abstract: Depositing strong carbide-forming elements on diamond surface can dramatically improve the interfacial bonding strength between diamond grits and metal matrix. In the present work, investigation on the preparation of Ti-coated diamond particles by microwave heating has been conducted. The morphology, microstructure, and the chemical composition of Ti-coated diamond particles were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive x-ray spectrometer (EDX). The thickness of Ti coating was measured and the interfacial binding strength between Ti coating and diamond was analyzed. The results show that the surface of the diamond particles could be successfully coated with Ti, forming a uniform and continuous Ti-coated layer. The TiC was found to form between the surface of diamond particles and Ti-coated layer. The amount of TiC as well as the thickness of coating increased with increasing coating temperature, furthermore, the grain size of the coating also grew gradually. The interfacial bonding strength between coating and diamond was found to be best at the temperature of 760 °C.

  16. Preparation of Ti-coated diamond particles by microwave heating

    Energy Technology Data Exchange (ETDEWEB)

    Gu, Quanchao [National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093 (China); Yunnan Copper Smelting and Processing Complex, Yunnan Copper (Group) CO., LTD., Kunming 650102 (China); International Joint Research Center of Advanced Preparation of Superhard Materials Field, Kunming Academician Workstation of Advanced Preparation of Superhard Materials Field, Kunming 650093 (China); Peng, Jinghui [National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093 (China); International Joint Research Center of Advanced Preparation of Superhard Materials Field, Kunming Academician Workstation of Advanced Preparation of Superhard Materials Field, Kunming 650093 (China); Xu, Lei, E-mail: xulei_kmust@aliyun.com [National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093 (China); Mechanical Engineering, University of Washington, Seattle, WA 98195 (United States); International Joint Research Center of Advanced Preparation of Superhard Materials Field, Kunming Academician Workstation of Advanced Preparation of Superhard Materials Field, Kunming 650093 (China); Srinivasakannan, C. [Chemical Engineering Department, The Petroleum Institute, P.O. Box 2533, Abu Dhabi (United Arab Emirates); and others

    2016-12-30

    Highlights: • The Ti-Coated diamond particles have been prepared using by microwave heating. • The uniform and dense coating can be produced, and the TiC species was formed. • With increases the temperature results in the thickness of coating increased. • The coating/diamond interfacial bonding strength increased with temperature increasing until 760 °C, then decreased. - Abstract: Depositing strong carbide-forming elements on diamond surface can dramatically improve the interfacial bonding strength between diamond grits and metal matrix. In the present work, investigation on the preparation of Ti-coated diamond particles by microwave heating has been conducted. The morphology, microstructure, and the chemical composition of Ti-coated diamond particles were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive x-ray spectrometer (EDX). The thickness of Ti coating was measured and the interfacial binding strength between Ti coating and diamond was analyzed. The results show that the surface of the diamond particles could be successfully coated with Ti, forming a uniform and continuous Ti-coated layer. The TiC was found to form between the surface of diamond particles and Ti-coated layer. The amount of TiC as well as the thickness of coating increased with increasing coating temperature, furthermore, the grain size of the coating also grew gradually. The interfacial bonding strength between coating and diamond was found to be best at the temperature of 760 °C.

  17. Characterization and source term assessments of radioactive particles from Marshall Islands using non-destructive analytical techniques

    Science.gov (United States)

    Jernström, J.; Eriksson, M.; Simon, R.; Tamborini, G.; Bildstein, O.; Marquez, R. Carlos; Kehl, S. R.; Hamilton, T. F.; Ranebo, Y.; Betti, M.

    2006-08-01

    Six plutonium-containing particles stemming from Runit Island soil (Marshall Islands) were characterized by non-destructive analytical and microanalytical methods. Composition and elemental distribution in the particles were studied with synchrotron radiation based micro X-ray fluorescence spectrometry. Scanning electron microscope equipped with energy dispersive X-ray detector and with wavelength dispersive system as well as a secondary ion mass spectrometer were used to examine particle surfaces. Based on the elemental composition the particles were divided into two groups: particles with pure Pu matrix, and particles where the plutonium is included in Si/O-rich matrix being more heterogenously distributed. All of the particles were identified as nuclear fuel fragments of exploded weapon components. As containing plutonium with low 240Pu/ 239Pu atomic ratio, less than 0.065, which corresponds to weapons-grade plutonium or a detonation with low fission yield, the particles were identified to originate from the safety test and low-yield tests conducted in the history of Runit Island. The Si/O-rich particles contained traces of 137Cs ( 239 + 240 Pu/ 137Cs activity ratio higher than 2500), which indicated that a minor fission process occurred during the explosion. The average 241Am/ 239Pu atomic ratio in the six particles was 3.7 × 10 - 3 ± 0.2 × 10 - 3 (February 2006), which indicated that plutonium in the different particles had similar age.

  18. Monolithic spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Rajic, Slobodan (Knoxville, TN); Egert, Charles M. (Oak Ridge, TN); Kahl, William K. (Knoxville, TN); Snyder, Jr., William B. (Knoxville, TN); Evans, III, Boyd M. (Oak Ridge, TN); Marlar, Troy A. (Knoxville, TN); Cunningham, Joseph P. (Oak Ridge, TN)

    1998-01-01

    A monolithic spectrometer is disclosed for use in spectroscopy. The spectrometer is a single body of translucent material with positioned surfaces for the transmission, reflection and spectral analysis of light rays.

  19. Improved Cloud Condensation Nucleus Spectrometer

    Science.gov (United States)

    Leu, Ming-Taun

    2010-01-01

    An improved thermal-gradient cloud condensation nucleus spectrometer (CCNS) has been designed to provide several enhancements over prior thermal- gradient counters, including fast response and high-sensitivity detection covering a wide range of supersaturations. CCNSs are used in laboratory research on the relationships among aerosols, supersaturation of air, and the formation of clouds. The operational characteristics of prior counters are such that it takes long times to determine aerosol critical supersaturations. Hence, there is a need for a CCNS capable of rapid scanning through a wide range of supersaturations. The present improved CCNS satisfies this need. The improved thermal-gradient CCNS (see Figure 1) incorporates the following notable features: a) The main chamber is bounded on the top and bottom by parallel thick copper plates, which are joined by a thermally conductive vertical wall on one side and a thermally nonconductive wall on the opposite side. b) To establish a temperature gradient needed to establish a supersaturation gradient, water at two different regulated temperatures is pumped through tubes along the edges of the copper plates at the thermally-nonconductive-wall side. Figure 2 presents an example of temperature and supersaturation gradients for one combination of regulated temperatures at the thermally-nonconductive-wall edges of the copper plates. c) To enable measurement of the temperature gradient, ten thermocouples are cemented to the external surfaces of the copper plates (five on the top plate and five on the bottom plate), spaced at equal intervals along the width axis of the main chamber near the outlet end. d) Pieces of filter paper or cotton felt are cemented onto the interior surfaces of the copper plates and, prior to each experimental run, are saturated with water to establish a supersaturation field inside the main chamber. e) A flow of monodisperse aerosol and a dilution flow of humid air are introduced into the main

  20. Computation of the Magnetic Field of a Spectrometer in Detectors Region

    International Nuclear Information System (INIS)

    Zhidkov, E.P.; Yuldasheva, M.B.; Yudin, I.P.; Yuldashev, O.I.

    1994-01-01

    Computed results of the 3D magnetic field of a spectrometer intended for investigation of hadron production of charmed particles and the indication of the narrow resonances in neutron-nucleus interaction are presented. The methods, used in computations - finite element method and finite element method with suggested new infinite elements are described. For accuracy control the computations were carried out on a sequence of three-dimensional meshes. Special attention is devoted to the behaviour of the magnetic field in the basic detectors (proportional chambers) region. The performed results can be used for the field behaviour estimate of similar spectrometer magnets. 12 refs., 16 figs

  1. Direct observation of the decay of beauty particles into charm particles

    International Nuclear Information System (INIS)

    Albanese, J.P.; Alpe, V.; Aoki, S.; Arnold, R.; Baroni, G.; Barth, M.; Bartley, J.H.; Bertrand, D.; Bertrand-Coremans, G.; Bisi, V.; Breslin, A.C.; Carboni, G.; Chesi, E.; Chiba, K.; Cook, G.S.; Coupland, M.; Crosetti, G.; Davis, D.H.; Dell'Uomo, S.; Di Liberto, S.; Bonnelly, W.; Duff, B.G.; Esten, M.J.; Gamba, D.; Gerke, C.; Hazama, M.; Heymann, F.F.; Hoshino, K.; Imrie, D.C.; Isokane, Y.; Kazuno, M.; Kodama, Y.; Lush, G.J.; Maeda, Y.; Marzari-Chiesa, A.; Mazzoni, M.A.; Meddi, F.; Miyanishi, M.; Montwill, A.; Muciaccia, M.T.; Musset, P.; Nakamura, M.; Nakazawa, K.; Natali, S.; Niu, K.; Niwa, K.; Nuzzo, S.; Ohashi, M.; Piuz, F.; Poulard, G.; Ramello, L.; Riccati, L.; Romano, G.; Roosen, R.; Rosa, G.; Ruggieri, F.; Sato, Y.; Sasaki, H.; Sgarbi, C.; Shibuya, H.; Simone, S.; Sletten, H.; Tasaka, S.; Tesuka, I.; Tomita, Y.; Tovee, D.N.; Trent, P.; Tsuneoka, Y.; Ushida, N.; Yamakawa, O.; Yanagisawa, Y.; Aichi Women's Coll., Nisshin-Cho; Bari Univ.; Istituto Nazionale di Fisica Nucleare, Bari; Birkbeck Coll., London; Interuniversity Inst. for High Energies, Brussels; European Organization for Nuclear Research, Geneva; University Coll., Dublin; Gifu Univ.; University Coll., London; Nagoya Univ.; Nagoya Inst. of Tech.; Rome Univ.; Istituto Nazionale di Fisica Nucleare, Rome; Toho Univ., Funabashi, Chiba; Istituto Nazionale di Fisica Nucleare, Turin; Turin Univ.; Utsunomiya Univ.; Yokohama National Univ.

    1985-01-01

    The associated production of a pair of beauty particles B - and anti B 0 by a 350 GeV π - interaction has been observed in an emulsion target inserted in an array of silicon microstrip detectors. Both beauty particles decay into charm particles, both of which are also observed to decay in the emulsion. Two negative muons were identified and their momenta measured in a large muon spectrometer. One muon has a psub(T) of 1.9 GeV/c and is associated with a beauty particle decay. The other, with a psub(T) of 0.45 GeV/c is associated with a charm particle decay. The flight times of the two beauty particles are respectively (0.8+-0.1).10 -13 s and (5sub(-1) +2 ).10 -13 s. Alternative interpretations of this event have negligible probability. (orig.)

  2. Monitoring and Quantifying Particles Emissions around Industrial Sites with Scanning Doppler Lidar

    Science.gov (United States)

    Thobois, L.; Royer, P.; Parmentier, R.; Brooks, M.; Knoepfle, A.; Alexander, J.; Stidwell, P.; Kumar, R.

    2018-04-01

    Scanning Coherent Doppler Lidars have been used over the last decade for measuring wind for applications in wind energy [1], meteorology [2] and aviation [3]. They allow for accurate measurements of wind speeds up to a distance of 10 km based on the Doppler shift effect of aerosols. The signal reflectivity (CNR or Carrier-to-Noise Ratio) profiles can also be retrieved from the strength of the Lidar signal. In this study, we will present the developments of algorithm for retrieving aerosol optical properties like the relative attenuated backscatter coefficient and the mass concentration of particles. The use of these algorithms during one operational trial in Point Samson, Western Australia to monitor fugitive emissions over a mine will be presented. This project has been initiated by the Australian Department of Environment Regulations to better determine the impact of the Port on the neighboring town. During the trial in Summer, the strong impact of turbulence refractive index on Lidar performances has been observed. Multiple methodologies have been applied to reduce this impact with more or less success. At the end, a dedicated setup and configuration have been established that allow to properly observe the plumes of the mine with the scanning Lidar. The Lidar data has also been coupled to beta attenuation in-situ sensors for retrieving mass concentration maps. A few case of dispersion of plumes will be presented showing the necessity to combine both the wind and aerosol data.

  3. Removal of stored particle background via the electric dipole method in the KATRIN main spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Hilk, Daniel [Institut fuer Experimentelle Kernphysik, KIT, Karlsruhe (Germany); Collaboration: KATRIN-Collaboration

    2016-07-01

    The goal of the KArlsruhe TRItium Neutrino (KATRIN) experiment is to determine the effective mass of the electron anti neutrino by measuring the electron energy spectrum of tritium beta decay near the endpoint. The goal is to reach a sensitivity on the neutrino mass of 200 meV for which a low background level of 10{sup -2} counts per second is mandatory. Electrons from single radioactive decays of radon and tritium in the KATRIN main spectrometer with energies in the keV range can be magnetically stored for hours. While cooling down via ionization of residual gas molecules, they produce hundreds of secondary electrons, which can reach the detector and contribute to the background signals. In order to suppress this background component, several methods are investigated to remove stored electrons, such as the application of an electric dipole field and the application of magnetic pulses. This talk introduces the mechanism of background production due to stored electrons and their removal by the electric dipole method in the main spectrometer. In context of the spectrometer- and detector-commissioning phase in summer 2015, measurement results of the application of the electric dipole method are presented.

  4. First steps towards geometry optimization for Spectrometer Straw Tracker of SHiP detector

    CERN Document Server

    Solovev, Vladimir

    2017-01-01

    This report contains details of CERN Summer Student project which was performed for SHiP experiment (Search for Hidden Particles). The main aim of the project is optimization of Spectrometer Straw Tracker (SST) geometry implemented in FairSHiP simulation program.

  5. The ALICE Dimuon Spectrometer High Level Trigger

    CERN Document Server

    Becker, B; Cicalo, Corrado; Das, Indranil; de Vaux, Gareth; Fearick, Roger; Lindenstruth, Volker; Marras, Davide; Sanyal, Abhijit; Siddhanta, Sabyasachi; Staley, Florent; Steinbeck, Timm; Szostak, Artur; Usai, Gianluca; Vilakazi, Zeblon

    2009-01-01

    The ALICE Dimuon Spectrometer High Level Trigger (dHLT) is an on-line processing stage whose primary function is to select interesting events that contain distinct physics signals from heavy resonance decays such as J/psi and Gamma particles, amidst unwanted background events. It forms part of the High Level Trigger of the ALICE experiment, whose goal is to reduce the large data rate of about 25 GB/s from the ALICE detectors by an order of magnitude, without loosing interesting physics events. The dHLT has been implemented as a software trigger within a high performance and fault tolerant data transportation framework, which is run on a large cluster of commodity compute nodes. To reach the required processing speeds, the system is built as a concurrent system with a hierarchy of processing steps. The main algorithms perform partial event reconstruction, starting with hit reconstruction on the level of the raw data received from the spectrometer. Then a tracking algorithm finds track candidates from the recon...

  6. Far From ‘Easy’ Spectroscopy with the 8π and GRIFFIN Spectrometers at TRIUMF-ISAC

    Science.gov (United States)

    Garrett, P. E.; Radich, A. J.; Allmond, J. M.; Andreoiu, C.; Ball, G. C.; Bender, P. C.; Bianco, L.; Bildstein, V.; Bidaman, H.; Braid, R.; Burbadge, C.; Chagnon-Lessard, S.; Cross, D. S.; Deng, G.; Demand, G. A.; Diaz Varela, A.; Dunlop, M. R.; Dunlop, R.; Finlay, P.; Garnsworthy, A. B.; Grinyer, G. F.; Hackman, G.; Hadinia, B.; Ilyushkin, S.; Jigmeddorj, B.; Kisliuk, D.; Kuhn, K.; Laffoley, A. T.; Leach, K. G.; MacLean, A. D.; Michetti-Wilson, J.; Miller, D.; Moore, W.; Olaizola, B.; Orce, J. N.; Pearson, C. J.; Pore, J. L.; Rajabali, M. M.; Rand, E. T.; Sarazin, F.; Smith, J. K.; Starosta, K.; Sumithrarachchi, C. S.; Svensson, C. E.; Triambak, S.; Turko, J.; Wang, Z. M.; Wood, J. L.; Wong, J.; Williams, S. J.; Yates, S. W.; Zganjar, E. F.

    2015-09-01

    The 8π spectrometer, installed at the TRIUMF-ISAC facility, was the world's most sensitive γ-ray spectrometer dedicated to β-decay studies. A description is given of the 8π spectrometer and its auxiliary detectors including the plastic scintillator array SCEPTAR used for β-particle tagging and the Si(Li) array PACES for conversion electron measurements, its moving tape collector, and its data acquisition system. The recent investigation of the decay of 124Cs to study the nuclear structure of 124Xe, and how the β-decay measurements complemented previous Coulomb excitation studies, is highlighted, including the extraction of the deformation parameters for the excited 0+ bands in 124Xe. As a by-product, the decay scheme of the (7+) 124Cs isomeric state, for which the data from the PACES detectors were vital, was studied. Finally, a description of the new GRIFFIN spectrometer, which uses the same auxiliary detectors as the 8π spectrometer, is given.

  7. Development and evaluation of the Combined Ion and Neutron Spectrometer (CINS)

    International Nuclear Information System (INIS)

    Zeitlin, C.; Maurer, R.; Roth, D.; Goldsten, J.; Grey, M.

    2009-01-01

    The Combined Ion and Neutron Spectrometer, CINS, is designed to measure the charged and neutral particles that contribute to the radiation dose and dose equivalent received by humans in spaceflight. As the depth of shielding increases, either onboard a spacecraft or in a surface habitat, the relative contribution of neutrons increases significantly, so that obtaining accurate neutron spectra becomes a critical part of any dosimetric measurements. The spectrometer system consists of high- and medium-energy neutron detectors along with a charged-particle detector telescope based on a standard silicon stack concept. The present version of the design is intended for ground-based use at particle accelerators; future iterations of the design can easily be streamlined to reduce volume, mass, and power consumption to create an instrument package suitable for spaceflight. The detector components have been tested separately using high-energy heavy ion beams at the NASA Space Radiation Laboratory at the Brookhaven National Laboratory and neutron beams at the Radiological Research Accelerator Facility operated by Columbia University. Here, we review the progress made in fabricating the hardware, report the results of several test runs, and discuss the remaining steps necessary to combine the separate components into an integrated system. A custom data acquisition system built for CINS is described in an accompanying article.

  8. Evolution of particle composition in CLOUD nucleation experiments

    Directory of Open Access Journals (Sweden)

    H. Keskinen

    2013-06-01

    Full Text Available Sulphuric acid, ammonia, amines, and oxidised organics play a crucial role in nanoparticle formation in the atmosphere. In this study, we investigate the composition of nucleated nanoparticles formed from these compounds in the CLOUD (Cosmics Leaving Outdoor Droplets chamber experiments at CERN (Centre européen pour la recherche nucléaire. The investigation was carried out via analysis of the particle hygroscopicity, ethanol affinity, oxidation state, and ion composition. Hygroscopicity was studied by a hygroscopic tandem differential mobility analyser and a cloud condensation nuclei counter, ethanol affinity by an organic differential mobility analyser and particle oxidation level by a high-resolution time-of-flight aerosol mass spectrometer. The ion composition was studied by an atmospheric pressure interface time-of-flight mass spectrometer. The volume fraction of the organics in the particles during their growth from sizes of a few nanometers to tens of nanometers was derived from measured hygroscopicity assuming the Zdanovskii–Stokes–Robinson relationship, and compared to values gained from the spectrometers. The ZSR-relationship was also applied to obtain the measured ethanol affinities during the particle growth, which were used to derive the volume fractions of sulphuric acid and the other inorganics (e.g. ammonium salts. In the presence of sulphuric acid and ammonia, particles with a mobility diameter of 150 nm were chemically neutralised to ammonium sulphate. In the presence of oxidation products of pinanediol, the organic volume fraction of freshly nucleated particles increased from 0.4 to ~0.9, with an increase in diameter from 2 to 63 nm. Conversely, the sulphuric acid volume fraction decreased from 0.6 to 0.1 when the particle diameter increased from 2 to 50 nm. The results provide information on the composition of nucleated aerosol particles during their growth in the presence of various combinations of sulphuric acid

  9. Hierarchical ZnO particles grafting by fluorocarbon polymer derivative: Preparation and superhydrophobic behavior

    Energy Technology Data Exchange (ETDEWEB)

    Gao, Dahai; Jia, Mengqiu, E-mail: jiamq@mail.buct.edu.cn

    2015-07-15

    Graphical abstract: - Highlights: • The hierarchical particles were prepared by a simple, mild hydrothermal process. • The obtained “chestnut” ZnO particles show dual-scale morphology with high roughness. • FEVE derivative was creatively imported to graft onto hierarchical particles. • Superhydrophobic surfaces were obtained, on which the contact angles surpass 150°. • A special model was proposed to explain the wetting state in this work. - Abstract: Superhydrophobic surfaces on the basis of hierarchical ZnO particles grafted by fluoroethylene-vinylether (FEVE) polymer derivative were prepared using a facile, mild and low-cost method. X-ray diffraction (XRD) and scanning electron microscope (SEM) revealed that the resulting ZnO particles via hydrothermal process exhibit micro–nano dual-scale morphology with high purity under a suitable surfactant amount and alkali concentration. The grafting of FEVE derivative was confirmed by Fourier transform infrared spectroscopy (FTIR) and energy-dispersive X-ray spectrometer (EDS), suggesting that hierarchical surface of ZnO particles was an imported monomolecular layer of fluorocarbon polymer. The obtained surface fabricated by drop-casting shows considerably high contact angle and good resistance to water immersion. The wetting behavior in this work was furthermore analyzed by theoretical wetting model. This work demonstrates that the sufficient low-wettable surface and high roughness both take a vital role in the superhydrophobic behavior.

  10. Low cost, microcontroller based heating device for multi-wavelength differential scanning fluorimetry.

    Science.gov (United States)

    Hoeser, Jo; Gnandt, Emmanuel; Friedrich, Thorsten

    2018-01-23

    Differential scanning fluorimetry is a popular method to estimate the stability of a protein in distinct buffer conditions by determining its 'melting point'. The method requires a temperature controlled fluorescence spectrometer or a RT-PCR machine. Here, we introduce a low-budget version of a microcontroller based heating device implemented into a 96-well plate reader that is connected to a standard fluorescence spectrometer. We demonstrate its potential to determine the 'melting point' of soluble and membranous proteins at various buffer conditions.

  11. Time-of-flight small-angle scattering spectrometers on pulsed neutron sources

    International Nuclear Information System (INIS)

    Ostanevich, Yu.M.

    1987-01-01

    The operation principles, constructions, advantages and shortcomings of known time-of-flight small angle neutron scattering (TOF SANS) spectrometers built up with pulsed neutron sources are reviewed. The most important characteristics of TOF SANS apparatuses are rather a high luminosity and the possibility for the measurement in an extremely wide range of scattering vector at a single exposure. This is achieved by simultaneous employment of white beam, TOF technique for wave length-scan and the commonly known angle-scan. However, the electronic equipment, data-matching programs, and the measurement procedure, necessary for accurate normalization of experimental data and their transformation into absolute cross-section scale, they all become more complex, as compared with those for SANS apparatuses operating on steady-state neutron sources, where only angle-scan is used

  12. Fast neutron spectrometer with pulse shape discrimination

    International Nuclear Information System (INIS)

    Verbitsky, S.S.

    1978-01-01

    A fast neutron spectrometer with a stilbene single crystal designed to operate at high pulsed count rate has been described. Making use of identification and rejection of events, accompanied by pile-up, allowed to increase permissible count rates by an order of magnitude. The results of energy dependence of signal amplitude and shape relative anisotropy in stilbene in the range 4-10 and 2-8 MeV respectively have been presented. Taking into account anisotropy of the detector-scintillation properties allowed to improve particle discrimination. (Auth.)

  13. Towards simultaneous Talbot bands based optical coherence tomography and scanning laser ophthalmoscopy imaging.

    Science.gov (United States)

    Marques, Manuel J; Bradu, Adrian; Podoleanu, Adrian Gh

    2014-05-01

    We report a Talbot bands-based optical coherence tomography (OCT) system capable of producing longitudinal B-scan OCT images and en-face scanning laser ophthalmoscopy (SLO) images of the human retina in-vivo. The OCT channel employs a broadband optical source and a spectrometer. A gap is created between the sample and reference beams while on their way towards the spectrometer's dispersive element to create Talbot bands. The spatial separation of the two beams facilitates collection by an SLO channel of optical power originating exclusively from the retina, deprived from any contribution from the reference beam. Three different modes of operation are presented, constrained by the minimum integration time of the camera used in the spectrometer and by the galvo-scanners' scanning rate: (i) a simultaneous acquisition mode over the two channels, useful for small size imaging, that conserves the pixel-to-pixel correspondence between them; (ii) a hybrid sequential mode, where the system switches itself between the two regimes and (iii) a sequential "on-demand" mode, where the system can be used in either OCT or SLO regimes for as long as required. The two sequential modes present varying degrees of trade-off between pixel-to-pixel correspondence and independent full control of parameters within each channel. Images of the optic nerve and fovea regions obtained in the simultaneous (i) and in the hybrid sequential mode (ii) are presented.

  14. Harmonisation of nanoparticle concentration measurements using GRIMM and TSI scanning mobility particle sizers

    International Nuclear Information System (INIS)

    Joshi, Manish; Sapra, B. K.; Khan, Arshad; Tripathi, S. N.; Shamjad, P. M.; Gupta, Tarun; Mayya, Y. S.

    2012-01-01

    Regional studies focusing on the role of atmospheric nanoparticles in climate change have gained impetus in the last decade. Several multi-institutional studies involving measurement of nanoparticles with several kinds of instruments are on the rise. It is important to harmonize these measurements as the instruments may work on different techniques or principles and are developed by different manufacturers. Scanning mobility particle sizers (SMPS) are often used to measure size distribution of nanoparticles in the airborne phase. Two such commercially available instruments namely, GRIMM and TSI-SMPS have been compared for ambient and laboratory generated conditions. A stand-alone condensation particle counter (CPC) of TSI make was used as a reference for particle concentration measurements. The consistency of the results in terms of mean size and geometric standard deviation was seen to be excellent for both the SMPSs, with GRIMM always showing slightly (approximately 10 %) lower mean size. The integrated number concentration from GRIMM-SMPS was seen to be closer to stand-alone reference CPC compared to TSI-SMPS, for an ambient overnight comparison. However, a concentration-dependent response, i.e. the variations between the two instruments increasing with the concentration, was observed and possible reasons for this have been suggested. A separate experiment was performed for studying the modifying effect of diffusion dryer and sheath air dryer on the measured aerosol size spectra. A significant hygroscopic growth was noted when diffusion dryer was attached to one of the SMPS. The introduction of sheath air dryer in GRIMM-SMPS produced a significant shift towards lower mean size. These results have been compared and discussed with the recent inter-comparison results to strengthen and harmonize the measurement protocols.

  15. Harmonisation of nanoparticle concentration measurements using GRIMM and TSI scanning mobility particle sizers

    Science.gov (United States)

    Joshi, Manish; Sapra, B. K.; Khan, Arshad; Tripathi, S. N.; Shamjad, P. M.; Gupta, Tarun; Mayya, Y. S.

    2012-12-01

    Regional studies focusing on the role of atmospheric nanoparticles in climate change have gained impetus in the last decade. Several multi-institutional studies involving measurement of nanoparticles with several kinds of instruments are on the rise. It is important to harmonize these measurements as the instruments may work on different techniques or principles and are developed by different manufacturers. Scanning mobility particle sizers (SMPS) are often used to measure size distribution of nanoparticles in the airborne phase. Two such commercially available instruments namely, GRIMM and TSI-SMPS have been compared for ambient and laboratory generated conditions. A stand-alone condensation particle counter (CPC) of TSI make was used as a reference for particle concentration measurements. The consistency of the results in terms of mean size and geometric standard deviation was seen to be excellent for both the SMPSs, with GRIMM always showing slightly (approximately 10 %) lower mean size. The integrated number concentration from GRIMM-SMPS was seen to be closer to stand-alone reference CPC compared to TSI-SMPS, for an ambient overnight comparison. However, a concentration-dependent response, i.e. the variations between the two instruments increasing with the concentration, was observed and possible reasons for this have been suggested. A separate experiment was performed for studying the modifying effect of diffusion dryer and sheath air dryer on the measured aerosol size spectra. A significant hygroscopic growth was noted when diffusion dryer was attached to one of the SMPS. The introduction of sheath air dryer in GRIMM-SMPS produced a significant shift towards lower mean size. These results have been compared and discussed with the recent inter-comparison results to strengthen and harmonize the measurement protocols.

  16. Weak Decays of Charmed Particles

    Energy Technology Data Exchange (ETDEWEB)

    Turcotte, Marc Gilles [McGill Univ., Montreal, QC (Canada)

    1986-05-01

    The lifetimes of charmed particles produced in interactions of high energy neutrinos with nucleons have been measured using a combination of a very high resolution emulsion-based vertex detector and a spectrometer allowing full kinematical reconstruction of the decays.

  17. Development of a single-shot-imaging thin film for an online Thomson parabola spectrometer

    International Nuclear Information System (INIS)

    Sakaki, H.; Fukuda, Y.; Nishiuchi, M.; Hori, T.; Yogo, A.; Jinno, S.; Kanasaki, M.; Niita, K.

    2013-01-01

    A single-shot-imaging thin scintillator film was developed for an online Thomson parabola (TP) spectrometer and the first analysis of laser accelerated ions, using the online TP spectrometer, was demonstrated at the JAEA-Kansai Advanced Relativistic Engineering Laser System (J-KAREN). An energy spectrum of ∼4.0 MeV protons is obtained using only this imaging film without the need of a microchannel plate that is typically utilized in online ion analyses. A general-purpose Monte Carlo particle and heavy ion-transport code system, which consists of various quantum dynamics models, was used for the prediction of the luminescent properties of the scintillator. The simulation can reasonably predict not only the ion trajectories detected by the spectrometer, but also luminescence properties.

  18. Direct observation of the decay of beauty particles into charm particles

    Energy Technology Data Exchange (ETDEWEB)

    Albanese, J P; Alpe, V; Aoki, S; Arnold, R; Baroni, G; Barth, M; Bartley, J H; Bertrand, D; Bertrand-Coremans, G; Bisi, V [Aichi Univ. of Education, Kariya (Japan); Aichi Women' s Coll, Nisshin-Cho [Japan; Bari Univ. (Italy). Ist. di Fisica; Istituto Nazionale di Fisica Nucleare, Bari (Italy); Birkbeck Coll, London [UK; Interuniversity Inst. for High Energies, Brussels (Belgium); European Organization for Nuclear Research, Geneva (Switzerland); University Coll., Dublin (Ireland); Gifu Univ. (Japan). Faculty of Education; University Coll., London (UK); Nagoya Univ. (Japan). Dept. of Physics; Nagoya Inst. of Tech. (Japan); Rome Univ. (Italy). Ist. di Fisica; Istituto Nazionale di Fisica Nucleare, Rome (Italy); Toho Univ., Funabashi, Chiba (Japan). Faculty of Science; Istituto Nazionale di Fisica Nucleare, Turin (Italy); Turin Univ. (Italy). Ist. di Fisica; Utsunomiya Univ. (Japan). Faculty of Education; Yokohama National Univ. (Japan). Faculty of Education

    1985-08-08

    The associated production of a pair of beauty particles B/sup -/ and anti B/sup 0/ by a 350 GeV ..pi../sup -/ interaction has been observed in an emulsion target inserted in an array of silicon microstrip detectors. Both beauty particles decay into charm particles, both of which are also observed to decay in the emulsion. Two negative muons were identified and their momenta measured in a large muon spectrometer. One muon has a psub(T) of 1.9 GeV/c and is associated with a beauty particle decay. The other, with a psub(T) of 0.45 GeV/c is associated with a charm particle decay. The flight times of the two beauty particles are respectively (0.8 +- 0.1).10/sup -13/s and (5sub(-1)/sup +2/).10/sup -13/s. Alternative interpretations of this event have negligible probability.

  19. Wide angle spectrometers for intermadiate energy electron accelerators

    International Nuclear Information System (INIS)

    Leconte, P.

    1982-10-01

    It is shown that improvements of the detector acceptances (in solid angle and momentum bite) is as important as increased duty cycle for coincidence experiments. To have a maximum efficiency and thus to reduce the cost of experiments, it is imperative to develop maximum solid angle systems. This implies an axial symmetry with respect to the incoming beam. At Saclay, we have investigated some of the properties of specific detectors covering up to 90% of 4π steradians for a high energy, 100% duty cycle electron accelerator. The techniques of wide angle spectrometers have already been explored on a large scale in high energy physics. However, in the case of charged particles, such detectors, compared to classical iron dipole spectrometers, present a smaller resolving power and a rather low background rejection. The choice of which of these two solutions is to be used depends on the conditions of the specific experiment

  20. IBM-PC based data acquisition system for a laser enhanced ionisation spectrometer using a low cost GPIB card

    International Nuclear Information System (INIS)

    Sampath Kumar, R.; Ravindranath, S.V.G.

    1992-01-01

    An IBM-PC based data acquisition system has been developed for the existing laser enhanced ionisation spectrometer in the Division. Here the boxcar averager (type SR 250) which integrates the spectrometer output is interfaced to an IBM-PC, converted into a GPIB controller with the help of a locally available GPIB card, (Dynalog Micro Systems make PCL 848) through the GPIB port of the computer interface module (SR 245). The menu driven software developed in BASIC, triggers the scan in the dye laser through its control port, collects data from the spectrometer, plots, displays and stores it on the hard disc for further use. (author). 6 refs., 18 figs., 2 appendixes

  1. Ultra-compact MEMS FTIR spectrometer

    Science.gov (United States)

    Sabry, Yasser M.; Hassan, Khaled; Anwar, Momen; Alharon, Mohamed H.; Medhat, Mostafa; Adib, George A.; Dumont, Rich; Saadany, Bassam; Khalil, Diaa

    2017-05-01

    Portable and handheld spectrometers are being developed and commercialized in the late few years leveraging the rapidly-progressing technology and triggering new markets in the field of on-site spectroscopic analysis. Although handheld devices were commercialized for the near-infrared spectroscopy (NIRS), their size and cost stand as an obstacle against the deployment of the spectrometer as spectral sensing components needed for the smart phone industry and the IoT applications. In this work we report a chip-sized microelectromechanical system (MEMS)-based FTIR spectrometer. The core optical engine of the solution is built using a passive-alignment integration technique for a selfaligned MEMS chip; self-aligned microoptics and a single detector in a tiny package sized about 1 cm3. The MEMS chip is a monolithic, high-throughput scanning Michelson interferometer fabricated using deep reactive ion etching technology of silicon-on-insulator substrate. The micro-optical part is used for conditioning the input/output light to/from the MEMS and for further light direction to the detector. Thanks to the all-reflective design of the conditioning microoptics, the performance is free of chromatic aberration. Complemented by the excellent transmission properties of the silicon in the infrared region, the integrated solution allows very wide spectral range of operation. The reported sensor's spectral resolution is about 33 cm-1 and working in the range of 1270 nm to 2700 nm; upper limited by the extended InGaAs detector. The presented solution provides a low cost, low power, tiny size, wide wavelength range NIR spectral sensor that can be manufactured with extremely high volumes. All these features promise the compatibility of this technology with the forthcoming demand of smart portable and IoT devices.

  2. Multidimensional spectrometer

    Science.gov (United States)

    Zanni, Martin Thomas; Damrauer, Niels H.

    2010-07-20

    A multidimensional spectrometer for the infrared, visible, and ultraviolet regions of the electromagnetic spectrum, and a method for making multidimensional spectroscopic measurements in the infrared, visible, and ultraviolet regions of the electromagnetic spectrum. The multidimensional spectrometer facilitates measurements of inter- and intra-molecular interactions.

  3. Small angle spectrometers: Summary

    International Nuclear Information System (INIS)

    Courant, E.; Foley, K.J.; Schlein, P.E.

    1986-01-01

    Aspects of experiments at small angles at the Superconducting Super Collider are considered. Topics summarized include a small angle spectrometer, a high contingency spectrometer, dipole and toroid spectrometers, and magnet choices

  4. Time-averaged probability density functions of soot nanoparticles along the centerline of a piloted turbulent diffusion flame using a scanning mobility particle sizer

    KAUST Repository

    Chowdhury, Snehaunshu; Boyette, Wesley; Roberts, William L.

    2017-01-01

    In this study, we demonstrate the use of a scanning mobility particle sizer (SMPS) as an effective tool to measure the probability density functions (PDFs) of soot nanoparticles in turbulent flames. Time-averaged soot PDFs necessary for validating

  5. Non-linearity issues and multiple ionization satellites in the PIXE portion of spectra from the Mars alpha particle X-ray spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Campbell, John L., E-mail: icampbel@uoguelph.ca; Heirwegh, Christopher M.; Ganly, Brianna

    2016-09-15

    Spectra from the laboratory and flight versions of the Curiosity rover’s alpha particle X-ray spectrometer were fitted with an in-house version of GUPIX, revealing departures from linear behavior of the energy-channel relationships in the low X-ray energy region where alpha particle PIXE is the dominant excitation mechanism. The apparent energy shifts for the lightest elements present were attributed in part to multiple ionization satellites and in part to issues within the detector and/or the pulse processing chain. No specific issue was identified, but the second of these options was considered to be the more probable. Approximate corrections were derived and then applied within the GUAPX code which is designed specifically for quantitative evaluation of APXS spectra. The quality of fit was significantly improved. The peak areas of the light elements Na, Mg, Al and Si were changed by only a few percent in most spectra. The changes for elements with higher atomic number were generally smaller, with a few exceptions. Overall, the percentage peak area changes are much smaller than the overall uncertainties in derived concentrations, which are largely attributable to the effects of rock heterogeneity. The magnitude of the satellite contributions suggests the need to incorporate these routinely in accelerator-based PIXE using helium beams.

  6. Particulate contamination spectrometer. Volume 1: Technical report

    Science.gov (United States)

    Schmitt, R. J.; Boyd, B. A.; Linford, R. M. F.

    1975-01-01

    A laser particulate spectrometer (LPS) system was developed to measure the size and speed distributions of particulate (dusts, aerosols, ice particles, etc.) contaminants. Detection of the particulates was achieved by means of light scattering and extinction effects using a single laser beam to cover a size range of 0.8 to 275 microns diameter and a speed range of 0.2 to 20 meter/second. The LPS system was designed to operate in the high vacuum environment of a space simulation chamber with cold shroud temperatures ranging from 77 to 300 K.

  7. Initial results of the mexican participation in the Alpha Magnetic Spectrometer Project

    International Nuclear Information System (INIS)

    Belmont M, E.; Menchaca R, A.; Sandoval, A.; Alfaro, R.; Martinez D, A.; Grabski, V.

    2007-01-01

    Mexico is part of the AMS (Alpha Magnetic Spectrometer) project, consisting of several radiation detectors integrated in a single telescope to be sent to the outer space in search of antimatter. One of those detectors is a RICH (Ring Imaging Cherenkov), where the cosmic particle's speed is calculated from the Cherenkov light-rings observed. The IF-UNAM group works in characterizing the silica aerogel used as luminous element in this detector. Because the spectrometer will be in orbit for several years, some particular studies are necessary. Our group works on possible ageing mechanisms, showing that the main threat to this material is contamination rather than thermal, or vacuum, shocks. (Author)

  8. Construction and performance of silicon detectors for the small angle spectrometers of the collider detector of Fermilab

    International Nuclear Information System (INIS)

    Apollinari, G.; Bedeschi, F.; Bellettini, G.; Bosi, F.; Bosisio, L.; Cervelli, F.; Del Fabbro, R.; Dell'Orso, M.; Di Virgilio, A.; Focardi, E.; Giannetti, P.; Giorgi, M.; Menzione, A.; Ristori, L.; Scribano, A.; Sestini, P.; Stefanini, A.; Tonelli, G.; Zetti, F.; Bertolucci, S.; Cordelli, M.; Curatolo, M.; Dulach, B.; Esposito, B.; Giromini, P.; Miscetti, S.; Sansoni, A.

    1987-01-01

    The manufacturing process of a series of position sensitive silicon detectors is described together with the tests performed to optimize the performance of the detectors. The detectors are Schottky diodes with strips on the ohmic contact which allow to determine the position of the incoming ionizing particles by charge partition. Four detectors were assembled in a telescope and tested inside the vacuum pipe of the Tevatron Collider at Fermilab. The system is a prototype of the Small Angle Silicon Spectrometer, designed primarily to study p-anti p elastic and diffractive cross sections, and is a part of the Collider Detector of Fermilab (CDF). Several tests were performed to check the efficiency and the linearity of response of various regions of the detectors. Scans of the beam halo were also done in high and low β optics to check how close to the beam the detectors could be operated. Finally, the dependence of the detector response on temperature and integrated radiation dose was investigated. (orig.)

  9. Characterization and source term assessments of radioactive particles from Marshall Islands using non-destructive analytical techniques

    Energy Technology Data Exchange (ETDEWEB)

    Jernstroem, J. [Laboratory of Radiochemistry, Department of Chemistry, P.O. Box 55, FI-00014 University of Helsinki (Finland)]. E-mail: jussi.jernstrom@helsinki.fi; Eriksson, M. [IAEA-MEL, International Atomic Energy Agency - Marine Environment Laboratory, 4 Quai Antoine 1er, MC 98000 Monaco (Monaco); Simon, R. [Institute for Synchrotron Radiation, Forschungszentrum Karlsruhe GmbH, D-76021 Karlsruhe (Germany); Tamborini, G. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Bildstein, O. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Marquez, R. Carlos [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Kehl, S.R. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, CA 94551-0808 (United States); Hamilton, T.F. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, CA 94551-0808 (United States); Ranebo, Y. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Betti, M. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany)]. E-mail: maria.betti@ec.europa.eu

    2006-08-15

    Six plutonium-containing particles stemming from Runit Island soil (Marshall Islands) were characterized by non-destructive analytical and microanalytical methods. Composition and elemental distribution in the particles were studied with synchrotron radiation based micro X-ray fluorescence spectrometry. Scanning electron microscope equipped with energy dispersive X-ray detector and with wavelength dispersive system as well as a secondary ion mass spectrometer were used to examine particle surfaces. Based on the elemental composition the particles were divided into two groups: particles with pure Pu matrix, and particles where the plutonium is included in Si/O-rich matrix being more heterogenously distributed. All of the particles were identified as nuclear fuel fragments of exploded weapon components. As containing plutonium with low {sup 240}Pu/{sup 239}Pu atomic ratio, less than 0.065, which corresponds to weapons-grade plutonium or a detonation with low fission yield, the particles were identified to originate from the safety test and low-yield tests conducted in the history of Runit Island. The Si/O-rich particles contained traces of {sup 137}Cs ({sup 239+240}Pu/{sup 137}Cs activity ratio higher than 2500), which indicated that a minor fission process occurred during the explosion. The average {sup 241}Am/{sup 239}Pu atomic ratio in the six particles was 3.7 x 10{sup -3} {+-} 0.2 x 10{sup -3} (February 2006), which indicated that plutonium in the different particles had similar age.

  10. High-energy resolution Thomson Parabola spectrometer for laser plasma diagnostics

    Energy Technology Data Exchange (ETDEWEB)

    Cirrone, G. A. P.; Schillaci, F. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania, Italy and Institute of Physics of the ASCR, ELI-Beamlines project, Na Slovance 2, Prague (Czech Republic); Carpinelli, M. [INFN Sezione di Cagliari, c/o Dipartimento di Fisica, Università di Cagliari, Cagliari (Italy); Cuttone, G.; Romano, F. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania (Italy); Maggiore, M. [Institute of Physics of the ASCR, ELI-Beamlines project, Na Slovance 2, Prague, Czech Republic and Laboratori Nazionali di Legnaro, INFN, Via Università 2, Legnaro (PD) (Italy); Ter-Avetisyan, S. [Laboratori Nazionali di Legnaro, INFN, Via Università 2, Legnaro (PD) (Italy); Tramontana, A. [Istituto Nazionale di Fisica Nucleare, Laboratori Nazionali del Sud, Via Santa Sofia 62, Catania, Italy and School of Mathematics and Physics, The Queen' s University Belfast, BT7 1NN (United Kingdom); Velyhan, A. [Institute of Physics of the ASCR, ELI-Beamlines project, Na Slovance 2, Prague (Czech Republic)

    2013-07-26

    Thomson Parabola (TP) spectrometers are widely used devices for laser-driven beam diagnostics as they provide a complete set of information on the accelerated particles. A novel TP has been developed at LNS with a design able to detect protons up to 20 MeV. The layout design and some results obtained during the experimental campaign at PALS laboratory will be reported in the following.

  11. Brookhaven National Laboratory's multiparticle spectrometer drift chamber system

    International Nuclear Information System (INIS)

    Etkin, A.; Kramer, M.A.

    1979-01-01

    A system of drift chambers is being built to replace the present spark chambers in the Brookhaven National Laboratory's Multiparticle Spectrometer. This system will handle a beam of approx. 3 million particles per second and have a resolution of 200 μm. A summary of the status of the chambers and the custom integrated circuits is presented. The data acquisition system is described. Prototype chambers have been built and tested with results that are consistent with the expected chamber properties

  12. Miniature, Low-Power, Waveguide Based Infrared Fourier Transform Spectrometer for Spacecraft Remote Sensing

    Science.gov (United States)

    Hewagama, TIlak; Aslam, Shahid; Talabac, Stephen; Allen, John E., Jr.; Annen, John N.; Jennings, Donald E.

    2011-01-01

    Fourier transform spectrometers have a venerable heritage as flight instruments. However, obtaining an accurate spectrum exacts a penalty in instrument mass and power requirements. Recent advances in a broad class of non-scanning Fourier transform spectrometer (FTS) devices, generally called spatial heterodyne spectrometers, offer distinct advantages as flight optimized systems. We are developing a miniaturized system that employs photonics lightwave circuit principles and functions as an FTS operating in the 7-14 micrometer spectral region. The inteferogram is constructed from an ensemble of Mach-Zehnder interferometers with path length differences calibrated to mimic scan mirror sample positions of a classic Michelson type FTS. One potential long-term application of this technology in low cost planetary missions is the concept of a self-contained sensor system. We are developing a systems architecture concept for wide area in situ and remote monitoring of characteristic properties that are of scientific interest. The system will be based on wavelength- and resolution-independent spectroscopic sensors for studying atmospheric and surface chemistry, physics, and mineralogy. The self-contained sensor network is based on our concept of an Addressable Photonics Cube (APC) which has real-time flexibility and broad science applications. It is envisaged that a spatially distributed autonomous sensor web concept that integrates multiple APCs will be reactive and dynamically driven. The network is designed to respond in an event- or model-driven manner or reconfigured as needed.

  13. Pion minus energy measurement by a multilayer semiconductor spectrometer

    International Nuclear Information System (INIS)

    Gornov, M.G.; Gurov, Yu.B.; Lapushkin, S.V.

    1981-01-01

    A technique for determining π - meson energy by a laminated semiconductor spectrometer is described. Results of experimental test of the technique carried out using beams of meson track of the JINR synchrocyclotron and three Si(Li) detectors are given. A specific feature of the technique is that chi 2 criterium with a functional written through exact thicknesses of semiconductor detectors was used for separating events with disturbance of ionization dependence and determining particle energy. It is shown that the absolute resolution can be not worse than 0.5 MeV in a wide energy range. It is concluded that the technique suggested is suitable for measuring energy of any charged particles with indefinite energy release during stoppage [ru

  14. The SPEDE spectrometer

    Science.gov (United States)

    Papadakis, P.; Cox, D. M.; O'Neill, G. G.; Borge, M. J. G.; Butler, P. A.; Gaffney, L. P.; Greenlees, P. T.; Herzberg, R.-D.; Illana, A.; Joss, D. T.; Konki, J.; Kröll, T.; Ojala, J.; Page, R. D.; Rahkila, P.; Ranttila, K.; Thornhill, J.; Tuunanen, J.; Van Duppen, P.; Warr, N.; Pakarinen, J.

    2018-03-01

    The electron spectrometer, SPEDE, has been developed and will be employed in conjunction with the Miniball spectrometer at the HIE-ISOLDE facility, CERN. SPEDE allows for direct measurement of internal conversion electrons emitted in-flight, without employing magnetic fields to transport or momentum filter the electrons. Together with the Miniball spectrometer, it enables simultaneous observation of γ rays and conversion electrons in Coulomb excitation experiments using radioactive ion beams.

  15. Rapid monitoring of gaseous radionuclides using a portable spectrometer

    International Nuclear Information System (INIS)

    Chung, C.; Tsai, C.H.

    1995-01-01

    A field gamma ray spectrometer, consisting of a portable high purity germanium detector, portable multichannel analyser, and a notebook computer, was used to conduct in situ rapid scanning of radioactive Ar, Kr and Xe isotopes in the air around a nuclear facility. The portable gamma ray spectrometer was calibrated using Ar, Kr, and Xe radioisotopes, activated in a research reactor and released in a sealed chamber. The unit was further tested inside the reactor containment to monitor the concentration of 41 Ar. In a typical one hour field measurement, the detection limits for some rare gas radionuclides corresponded to dose rates around 0.1 nSv.h -1 , which is far less than the dose rate induced by derived air concentrations imposed by the authority. The dose rate due to ground level concentrations of gaseous radionuclides dispersed from a source, such a nuclear facility or nuclear test, can be monitored in a short period using the portable unit. (Author)

  16. Versatile mid-infrared frequency-comb referenced sub-Doppler spectrometer

    Science.gov (United States)

    Gambetta, A.; Vicentini, E.; Coluccelli, N.; Wang, Y.; Fernandez, T. T.; Maddaloni, P.; De Natale, P.; Castrillo, A.; Gianfrani, L.; Laporta, P.; Galzerano, G.

    2018-04-01

    We present a mid-IR high-precision spectrometer capable of performing accurate Doppler-free measurements with absolute calibration of the optical axis and high signal-to-noise ratio. The system is based on a widely tunable mid-IR offset-free frequency comb and a Quantum-Cascade-Laser (QCL). The QCL emission frequency is offset locked to one of the comb teeth to provide absolute-frequency calibration, spectral-narrowing, and accurate fine frequency tuning. Both the comb repetition frequency and QCL-comb offset frequency can be modulated to provide, respectively, slow- and fast-frequency-calibrated scanning capabilities. The characterisation of the spectrometer is demonstrated by recording sub-Doppler saturated absorption features of the CHF3 molecule at around 8.6 μm with a maximum signal-to-noise ratio of ˜7 × 103 in 10 s integration time, frequency-resolution of 160 kHz, and accuracy of less than 10 kHz.

  17. Versatile mid-infrared frequency-comb referenced sub-Doppler spectrometer

    Directory of Open Access Journals (Sweden)

    A. Gambetta

    2018-04-01

    Full Text Available We present a mid-IR high-precision spectrometer capable of performing accurate Doppler-free measurements with absolute calibration of the optical axis and high signal-to-noise ratio. The system is based on a widely tunable mid-IR offset-free frequency comb and a Quantum-Cascade-Laser (QCL. The QCL emission frequency is offset locked to one of the comb teeth to provide absolute-frequency calibration, spectral-narrowing, and accurate fine frequency tuning. Both the comb repetition frequency and QCL-comb offset frequency can be modulated to provide, respectively, slow- and fast-frequency-calibrated scanning capabilities. The characterisation of the spectrometer is demonstrated by recording sub-Doppler saturated absorption features of the CHF3 molecule at around 8.6 μm with a maximum signal-to-noise ratio of ∼7 × 103 in 10 s integration time, frequency-resolution of 160 kHz, and accuracy of less than 10 kHz.

  18. Refinement of the Compton–Rayleigh scatter ratio method for use on the Mars Science Laboratory alpha particle X-ray spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Campbell, J.L., E-mail: icampbel@uoguelph.ca [Guelph-Waterloo Physics Institute, University of Guelph, Guelph, Ontario, Canada N1G 2W1 (Canada); Perrett, G.M. [Guelph-Waterloo Physics Institute, University of Guelph, Guelph, Ontario, Canada N1G 2W1 (Canada); Maxwell, J.A. [3A 47 Surrey St. East, Guelph, Ontario, Canada N1H 3P6 (Canada); Nield, E.; Gellert, R. [Guelph-Waterloo Physics Institute, University of Guelph, Guelph, Ontario, Canada N1G 2W1 (Canada); King, P.L. [Research School of Earth Sciences, Australian National University, Canberra, ACT 0200 (Australia); Lee, M.; O’Meara, J.M.; Pradler, I. [Guelph-Waterloo Physics Institute, University of Guelph, Guelph, Ontario, Canada N1G 2W1 (Canada)

    2013-05-01

    Spectra from the Mars rover alpha particle X-ray spectrometers contain the elastic and inelastic scatter peaks of the plutonium L X-rays emitted by the instrument’s {sup 244}Cm source. Various spectrum fitting approaches are tested using the terrestrial twin of the APXS instrument on the Mars Science Laboratory Curiosity rover, in order to provide accurate extraction of the Lα and Lβ Compton/Rayleigh intensity ratios, which can provide information about light “invisible” constituents such as water in geological samples. A well-defined dependence of C/R ratios upon mean sample atomic number is established using a large and varied set of geochemical reference materials, and the accuracy of this calibration is examined. Detailed attention is paid to the influence of the rubidium and strontium peaks which overlap the Lα scatter peaks. Our Monte Carlo simulation code for prediction of C/R ratios from element concentrations is updated. The ratio between measured and simulated C/R ratios provides a second means of calibration.

  19. Airborne Laser Infrared Absorption Spectrometer (ALIAS-II) for in situ Atmospheric Measurements of N(sub 2)0, CH(sub 4), CO, HCl, and NO(sub 2) from Balloon or RPA Platforms

    Science.gov (United States)

    Scott, D.; Herman, R.; Webster, C.; May, R.; Flesch, G.; Moyer, E.

    1998-01-01

    The Airborne Laser Infrared Absorption Spectrometer II (ALIAS-II) is a lightweight, high-resolution (0.0003 cm-1), scanning, mid-infrared absorption spectrometer based on cooled (80 K) lead-salt tunable diode laser sources.

  20. Using rapid scan EPR to improve the detection limit of quantitative EPR by more than one order of magnitude

    OpenAIRE

    Möser, J.; Lips, K.; Tseytlin, M.; Eaton, G.; Eaton, S.; Schnegg, A

    2017-01-01

    X band rapid scan EPR was implemented on a commercially available Bruker ELEXSYS E580 spectrometer. Room temperature rapid scan and continuous wave EPR spectra were recorded for amorphous silicon powder samples. By comparing the resulting signal intensities the feasibility of performing quantitative rapid scan EPR is demonstrated. For different hydrogenated amorphous silicon samples, rapid scan EPR results in signal to noise improvements by factors between 10 and 50. Rapid scan EPR is thus ca...

  1. The data acquisition system used in one-dimension multichannel fast electron energy loss spectrometer

    International Nuclear Information System (INIS)

    Jiang Weichun; Zhu Linfan; Zhang Yijun; Xu Kezuo

    2010-01-01

    It describes a data acquisition system used in one dimension multichannel fast electron energy loss spectrometer, which can work in scan acquisition mode and static acquisition mode. The timing precision of the scan mode is less than 4 μs by utilizing the gated signal generated by data acquisition card DAQ2010 and an AND logic circuit. A timer card PCI8554 is used to synchronize the data acquisition card and the personal computer. The scan voltage supply is controlled by the personal computer through the RS232 interface. The multithreading technology is used in the acquisition software in order to improve the accommodating-err ability of the acquisition system. A satisfactory test result is given. (authors)

  2. Evolution of particle composition in CLOUD nucleation experiments

    CERN Document Server

    Keskinen, H; Joutsensaari, J; Tsagkogeorgas, G; Duplissy, J; Schobesberger, S; Gysel, M; Riccobono, F; Bianchi, F; Yli-Juuti, T; Lehtipalo, K; Rondo, L; Breitenlechner, M; Kupc, A; Almeida, J; Amorim, A; Dunne, E M; Downard, A J; Ehrhart, S; Franchin, A; Kajos, M K; Kirkby, J; Kurten, A; Nieminen, T; Makhmutov, V; Mathot, S; Miettinen, P; Onnela, A; Petaja, T; Praplan, A; Santos, F D; Schallhart, S; Sipila, M; Stozhkov, Y; Tome, A; Vaattovaara, P; Wimmer, D; Prevot, A; Dommen, J; Donahue, N M; Flagan, R C; Weingartner, E; Viisanen, Y; Riipinen, I; Hansel, A; Curtius, J; Kulmala, M; Worsnop, D R; Baltensperger, U; Wex, H; Stratmann, F; Laaksonen, A; Slowik, J G

    2013-01-01

    Sulphuric acid, ammonia, amines, and oxidised organics play a crucial role in nanoparticle formation in the atmosphere. In this study, we investigate the composition of nucleated nanoparticles formed from these compounds in the CLOUD (Cosmics Leaving Outdoor Droplets) chamber experiments at CERN (Centre europ ́ een pour la recherche nucl ́ eaire). The investigation was carried out via analysis of the particle hygroscopicity, ethanol affinity, oxidation state, and ion composition. Hygroscopicity was studied by a hygroscopic tandem differential mobility analyser and a cloud condensation nuclei counter, ethanol affinity by an organic differential mobility analyser and particle oxidation level by a high-resolution time-of-flight aerosol mass spectrometer. The ion composition was studied by an atmospheric pressure interface time-of-flight mass spectrometer. The volume fraction of the organics in the particles during theirgrowth from sizes of a few nanometers to tens of nanometers was derived from measured hygros...

  3. Preparation of hierarchical porous Zn-salt particles and their superhydrophobic performance

    Energy Technology Data Exchange (ETDEWEB)

    Gao, Dahai; Jia, Mengqiu, E-mail: jiamq@mail.buct.edu.cn

    2015-12-30

    Graphical abstract: - Highlights: • Hierarchical particles with high roughness were prepared by modified hydrothermal route. • The high roughness is provided by extremely low thickness of sheet crystals. • FEVE polymer derivative was used for surface treatment of hierarchical surface. • The novel particles via surface treatment were firstly used as superhydrophobic materials. • The product properties were compared with multi-scale ZnO particles via conventional route. - Abstract: Superhydrophobic surfaces arranged by hierarchical porous particles were prepared using modified hydrothermal routes under the effect of sodium citrate. Two particle samples were generated in the medium of hexamethylenetetramine (P1) and urea (P2), respectively. X-ray diffraction, scanning electron microscope, and transmission electron microscope were adopted for the investigation, and results revealed that the P1 and P2 particles are porous microspheres with crosslinked extremely thin (10–30 nm) sheet crystals composed of Zn{sub 5}(OH){sub 8}Ac{sub 2}·2H{sub 2}O and Zn{sub 5}(CO{sub 3}){sub 2}(OH){sub 6}, respectively. The prepared particles were treated with a fluoroethylene vinyl ether derivative and studied using Fourier transform infrared spectroscopy and energy-dispersive X-ray spectrometer. Results showed that the hierarchical surfaces of these particles were combined with low-wettable fluorocarbon layers. Moreover, the fabricated surface composed of the prepared hierarchical particles displayed considerably high contact angles, indicating great superhydrophobicity for the products. The wetting behavior of the particles was analyzed with a theoretical wetting model in comparison with that of chestnut-like ZnO products obtained through a conventional hydrothermal route. Correspondingly, this study provided evidence that high roughness surface plays a great role in superhydrophobic behavior.

  4. An Advanced Neutron Spectrometer for Future Manned Exploration Missions

    Science.gov (United States)

    Christl, Mark; Apple, Jeffrey A.; Cox, Mark D.; Dietz, Kurtis L.; Dobson, Christopher C.; Gibson, Brian F.; Howard, David E.; Jackson, Amanda C.; Kayatin, Mathew J.; Kuznetsov, Evgeny N.; hide

    2014-01-01

    An Advanced Neutron Spectrometer (ANS) is being developed to support future manned exploration missions. This new instrument uses a refined gate and capture technique that significantly improves the identification of neutrons in mixed radiation fields found in spacecraft, habitats and on planetary surfaces. The new instrument is a composite scintillator comprised of PVT loaded with litium-6 glass scintillators. We will describe the detection concept and show preliminary results from laboratory tests and exposures at particle accelerators

  5. VESUVIO--the double difference inverse geometry spectrometer at ISIS

    International Nuclear Information System (INIS)

    Mayers, J.; Tomkinson, J.; Abdul-Redah, T.; Stirling, W.G.; Andreani, C.; Senesi, R.; Nardone, M.; Colognesi, D.; Degiorgi, E.

    2004-01-01

    The VESUVIO spectrometer at the ISIS pulsed neutron source performs inelastic neutron scattering at high-energy and wave vector transfers, employing gold and uranium resonant foils. A factor of two improvement in the instrumental resolution has been achieved by making use of the double filter difference method. Experimental results are presented for measurements on polycrystalline Pb, which indicate that accurate measurements of single-particle momentum distribution n(p) in quantum fluids are now possible at eV energy transfers

  6. VESUVIO--the double difference inverse geometry spectrometer at ISIS

    Energy Technology Data Exchange (ETDEWEB)

    Mayers, J.; Tomkinson, J.; Abdul-Redah, T.; Stirling, W.G.; Andreani, C.; Senesi, R.; Nardone, M.; Colognesi, D.; Degiorgi, E

    2004-07-15

    The VESUVIO spectrometer at the ISIS pulsed neutron source performs inelastic neutron scattering at high-energy and wave vector transfers, employing gold and uranium resonant foils. A factor of two improvement in the instrumental resolution has been achieved by making use of the double filter difference method. Experimental results are presented for measurements on polycrystalline Pb, which indicate that accurate measurements of single-particle momentum distribution n(p) in quantum fluids are now possible at eV energy transfers.

  7. VESUVIO-the double difference inverse geometry spectrometer at ISIS

    Science.gov (United States)

    Mayers, J.; Tomkinson, J.; Abdul-Redah, T.; Stirling, W. G.; Andreani, C.; Senesi, R.; Nardone, M.; Colognesi, D.; Degiorgi, E.

    2004-07-01

    The VESUVIO spectrometer at the ISIS pulsed neutron source performs inelastic neutron scattering at high-energy and wave vector transfers, employing gold and uranium resonant foils. A factor of two improvement in the instrumental resolution has been achieved by making use of the double filter difference method. Experimental results are presented for measurements on polycrystalline Pb, which indicate that accurate measurements of single-particle momentum distribution n(p) in quantum fluids are now possible at eV energy transfers.

  8. Fast neutron scintillation spectrometer in a heavy ion accelerator

    International Nuclear Information System (INIS)

    Blinov, M.V.; Gavrilov, B.P.; Ivannikova, L.L.; Kozulin, Eh.M.; Mozhaev, A.N.; Tyurin, G.P.

    1984-01-01

    Scintillation fast neutron spectrometer in a heavy ion accelerator is described in short. The spectrometer is used to measure characteristics of neutrons emitted in heavy ion interaction with different nuclei. Experiment was performed on the base of particle flight from 0.7 up to 2 m. Within the angle range of 0-150 deg. The technique is based on recording of two-dimensional neutron spectra obtained due to combination of the time-of-flight method and the method of recoil proton energy detection. Two measuring channels were used in the spectrometer. Each channel comprise both amplitude and time tracks. Detector on the base microchannel plates (MCP) generated a signal in passing the next ion bunch was used in order to obtain the time mark. Data from the scintillation block are recorded with respect to three parameters: recoil proton amplitude, time of neutron or γ-quantum arrival in respect of MCP-sensor pulse. Apparatus is carried out within the CAMAC standard. The spectrometer calibration within the 1-20 MeV neutron range was conducted in the Van-de-Graaf accelerator, and for higher energies - with the use of lightguides. Spectrometer time resolution for neutron energies of 0.5-50 MeV constituted 1.5-1.8 ns. The above measuring of neutron spectra from 1 /H2C+ 181 Ta and sup(20, 22)Ne+sup(181)Ta reaction have revealed a possibility of the experiment organization in heavy ion accelerators in the presence of strong neutron and γ-fields. Organization of multi-dimensional analysis combining two methods allows one to separate accelerator cycle, a region of the most reliable information, free of a low-energy gamma background and limited both by a dynamic threshold and a region of permissible energy values

  9. Performance of drift chambers in a magnetic rigidity spectrometer for measuring the cosmic radiation

    International Nuclear Information System (INIS)

    Hof, M.; Bremerich, M.; Menn, W.; Pfeifer, C.; Reimer, O.; Simon, M.; Mitchell, J.W.; Barbier, L.M.; Christian, E.R.; Ormes, J.F.; Streitmatter, R.E.; Golden, R.L.; Stochaj, S.J.

    1994-01-01

    A drift chamber tracking system was developed and flown as part of the IMAX balloon-borne magnetic spectrometer. The drift chamber uses a hexagonal drift-cell structure and is filled with pure CO 2 gas. It operated with high efficiency in the strong and inhomogenous field of a superconducting magnet, demonstrating a spatial resolution of better than 100 μm over most of the drift path for singly charged particles, as well as for helium and lithium nuclei. The drift chamber portion of the spectrometer achieved a maximum detectable rigidity of 175 and 250 GV/c for protons and helium respectively. ((orig.))

  10. Superconducting nano-strip particle detectors

    International Nuclear Information System (INIS)

    Cristiano, R; Ejrnaes, M; Casaburi, A; Zen, N; Ohkubo, M

    2015-01-01

    We review progress in the development and applications of superconducting nano-strip particle detectors. Particle detectors based on superconducting nano-strips stem from the parent devices developed for single photon detection (SSPD) and share with them ultra-fast response times (sub-nanosecond) and the ability to operate at a relatively high temperature (2–5 K) compared with other cryogenic detectors. SSPDs have been used in the detection of electrons, neutral and charged ions, and biological macromolecules; nevertheless, the development of superconducting nano-strip particle detectors has mainly been driven by their use in time-of-flight mass spectrometers (TOF-MSs) where the goal of 100% efficiency at large mass values can be achieved. Special emphasis will be given to this case, reporting on the great progress which has been achieved and which permits us to overcome the limitations of existing mass spectrometers represented by low detection efficiency at large masses and charge/mass ambiguity. Furthermore, such progress could represent a breakthrough in the field. In this review article we will introduce the device concept and detection principle, stressing the peculiarities of the nano-strip particle detector as well as its similarities with photon detectors. The development of parallel strip configuration is introduced and extensively discussed, since it has contributed to the significant progress of TOF-MS applications. (paper)

  11. A possible edge effect in enhanced network. [solar K-line observations by multichannel spectrometer

    Science.gov (United States)

    Jones, H. P.; Brown, D. R.

    1977-01-01

    K-line observations of enhanced network taken with the NASA/SPO Multichannel Spectrometer on September 28, 1975, in support of OSO-8 are discussed. The data show a correlation between core brightness and asymmetry for spatial scans which cross enhanced network boundaries. The implications of this result concerning mass flow in and near supergranule boundaries are discussed.

  12. The Omega spectrometer in the West Hall.

    CERN Multimedia

    CERN PhotoLab

    1976-01-01

    Inside the hut which sits on top of the superconducting magnet are the TV cameras that observe the particle events occurring in the spark chambers in the magnet gap below. On the background the two beam lines feeding the spectrometer target, for separated hadrons up to 40 GeV, on the right, for 80 GeV electrons, on the left, respectively. The latter strikes a radiator thus sending into Omega tagged photons up to 80 GeV. On the foreground, the two sections of the large gas Cerenkov counter working at atmospheric pressure, used for trigger purpose.

  13. Characterization of winter airborne particles at Emperor Qin's Terra-cotta Museum, China

    International Nuclear Information System (INIS)

    Hu, Tafeng; Lee, Shuncheng; Cao, Junji; Chow, Judith C.; Watson, John G.; Ho, Kinfai; Ho, Wingkei; Rong, Bo; An, Zhisheng

    2009-01-01

    Daytime and nighttime total suspended particulate matters (TSP) were collected inside and outside Emperor Qin's Terra-cotta Museum, the most popular on-site museum in China, in winter 2008. The purpose of this study was to investigate the contribution of visitors to indoor airborne particles in two display halls with different architectural and ventilating conditions, including Exhibition Hall and Pit No.1. Morphological and elemental analyses of 7-day individual particle samples were performed with scanning electron microscopy and energy dispersive X-ray spectrometer (SEM-EDX). Particle mass concentrations in Exhibition Hall and Pit No.1 were in a range of 54.7-291.7 μg m -3 and 95.3-285.4 μg m -3 with maximum diameters of 17.5 μm and 26.0 μm, respectively. In most sampling days, daytime/nighttime particle mass ratios in Exhibition Hall (1.30-3.12) were higher than those in Pit No.1 (0.96-2.59), indicating more contribution of the tourist flow in Exhibition Hall than in Pit No. 1. The maximum of particle size distributions were in a range of 0.5-1.0 μm, with the highest abundance (43.4%) occurred in Exhibition Hall at night. The majority of airborne particles at the Museum was composed of soil dust, S-containing particles, and low-Z particles like soot aggregate and biogenic particles. Both size distributions and particle types were found to be associated with visitor numbers in Exhibition Hall and with natural ventilation in Pit No.1. No significant influence of visitors on indoor temperature and relative humidity (RH) was found in either display halls. Those baseline data on the nature of the airborne particles inside the Museum can be incorporated into the maintenance criteria, display management, and ventilation strategy by conservators of the museum.

  14. Light collection and its fluctuation in Cherenkov and scintillation spectrometers

    International Nuclear Information System (INIS)

    Kitaev, D.F.; Samedov, V.V.; Stolyarova, E.L.

    1982-01-01

    The GAMMA program for calculating light collection in the Cherenkov and scintillation counters is described. Together with the shower modelling program the GAMNA program can be used for evaluating the output signal and energy resolution of shower spectrometers. Principle formulae and block diagram of the program are given. Results of test calculations performed on the example of scintillation counters of culindrical and rectangular shapes were considered. Modelling of the radiation polarization envisaged in the program permits to take account of the effect of selective discrimination of photoelectron amplifier photocathode. The program analyzes, for the present situation, calculation errors which permits to plan in advance the calculation with the given accuracy. The program permits to use additional subprograms together with it where it is possible to take account of other peculiarities of light collection, for example, the presence of outer reflectors and focusing elements of light collection systems, particle slowing down in the spectrometer radiator expressed in the change of angle of semiaperture of the Cherenkov radiation cone. It is concluded on the basis of analyzing results of test calculations that the choosen technique and algorithms of light collection coefficient calculation in spectrometer radiators are correct

  15. The SAGE spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Pakarinen, J.; Papadakis, P. [University of Liverpool, Department of Physics, Oliver Lodge Laboratory, Liverpool (United Kingdom); University of Jyvaeskylae, Department of Physics, Jyvaeskylae (Finland); Sorri, J.; Greenlees, P.T.; Jones, P.; Julin, R.; Konki, J.; Rahkila, P.; Sandzelius, M. [University of Jyvaeskylae, Department of Physics, Jyvaeskylae (Finland); Herzberg, R.D.; Butler, P.A.; Cox, D.M.; Cresswell, J.R.; Mistry, A.; Page, R.D.; Parr, E.; Sampson, J.; Seddon, D.A.; Thornhill, J.; Wells, D. [University of Liverpool, Department of Physics, Oliver Lodge Laboratory, Liverpool (United Kingdom); Coleman-Smith, P.J.; Lazarus, I.H.; Letts, S.C.; Pucknell, V.F.E.; Simpson, J. [STFC Daresbury Laboratory, Warrington (United Kingdom)

    2014-03-15

    The SAGE spectrometer has been constructed for in-beam nuclear structure studies. SAGE combines a Ge-detector array and an electron spectrometer for detection of γ-rays and internal conversion electrons, respectively, and allows simultaneous observation of both electrons and γ-rays emitted from excited nuclei. SAGE is set up in the Accelerator Laboratory of the University of Jyvaeskylae and works in conjunction with the RITU gas-filled recoil separator and the GREAT focal-plane spectrometer allowing the use of the recoil-decay tagging method. (orig.)

  16. The SAGE spectrometer

    International Nuclear Information System (INIS)

    Pakarinen, J.; Papadakis, P.; Sorri, J.; Greenlees, P.T.; Jones, P.; Julin, R.; Konki, J.; Rahkila, P.; Sandzelius, M.; Herzberg, R.D.; Butler, P.A.; Cox, D.M.; Cresswell, J.R.; Mistry, A.; Page, R.D.; Parr, E.; Sampson, J.; Seddon, D.A.; Thornhill, J.; Wells, D.; Coleman-Smith, P.J.; Lazarus, I.H.; Letts, S.C.; Pucknell, V.F.E.; Simpson, J.

    2014-01-01

    The SAGE spectrometer has been constructed for in-beam nuclear structure studies. SAGE combines a Ge-detector array and an electron spectrometer for detection of γ-rays and internal conversion electrons, respectively, and allows simultaneous observation of both electrons and γ-rays emitted from excited nuclei. SAGE is set up in the Accelerator Laboratory of the University of Jyvaeskylae and works in conjunction with the RITU gas-filled recoil separator and the GREAT focal-plane spectrometer allowing the use of the recoil-decay tagging method. (orig.)

  17. Characterization of aerosol particles from grass mowing by joint deployment of ToF-AMS and ATOFMS instruments

    Science.gov (United States)

    Drewnick, Frank; Dall'Osto, Manuel; Harrison, Roy

    During a measurement campaign at a semi-urban/industrial site a grass-cutting event was observed, when the lawn in the immediate surrounding of the measurement site was mowed. Using a wide variety of state-of-the-art aerosol measurement technology allowed a broad characterization of the aerosol generated by the lawn mowing. The instrumentation included two on-line aerosol mass spectrometers: an Aerodyne Time-of-Flight Aerosol Mass Spectrometer (ToF-AMS) and a TSI Aerosol Time-of-Flight Mass Spectrometer (ATOFMS); in addition, a selection of on-line aerosol concentration and size distribution instruments (OPC, APS, SMPS, CPC, FDMS-TEOM, MAAP) was deployed. From comparison of background aerosol measurements during most of the day with the aerosol measured during the lawn mowing, the grass cutting was found to generate mainly two different types of aerosol particles: an intense ultrafine particle mode (1 h average: 4 μg m -3) of almost pure hydrocarbon-like organics and a distinct particle mode in the upper sub-micrometer size range containing particles with potassium and nitrogen-organic compounds. The ultrafine particles are probably lubricating oil particles from the lawn mower exhaust; the larger particles are swirled-up plant debris particles from the mowing process. While these particle types were identified in the data from the two mass spectrometers, the on-line aerosol concentration and size distribution data support these findings. The results presented here show that the combination of quantitative aerosol particle ensemble mass spectrometry (ToF-AMS) and single particle mass spectrometry (ATOFMS) provides much deeper insights into the nature of the aerosol properties than each of the instruments could do alone. Therefore a combined deployment of both types of instruments is strongly recommended.

  18. Scientific Payload Of The Emirates Mars Mission: Emirates Mars Infrared Spectrometer (Emirs) Overview.

    Science.gov (United States)

    Altunaiji, E. S.; Edwards, C. S.; Christensen, P. R.; Smith, M. D.; Badri, K. M., Sr.

    2017-12-01

    The Emirates Mars Mission (EMM) will launch in 2020 to explore the dynamics in the atmosphere of Mars on a global scale. EMM has three scientific instruments to an improved understanding of circulation and weather in the Martian lower and middle atmosphere. Two of the EMM's instruments, which are the Emirates eXploration Imager (EXI) and Emirates Mars Infrared Spectrometer (EMIRS) will focus on the lower atmosphere observing dust, ice clouds, water vapor and ozone. On the other hand, the third instrument Emirates Mars Ultraviolet Spectrometer (EMUS) will focus on both the thermosphere of the planet and its exosphere. The EMIRS instrument, shown in Figure 1, is an interferometric thermal infrared spectrometer that is jointly developed by Arizona State University (ASU) and Mohammed Bin Rashid Space Centre (MBRSC). It builds on a long heritage of thermal infrared spectrometers designed, built, and managed, by ASU's Mars Space Flight Facility, including the Thermal Emission Spectrometer (TES), Miniature Thermal Emission Spectrometer (Mini-TES), and the OSIRIS-REx Thermal Emission Spectrometer (OTES). EMIRS operates in the 6-40+ µm range with 5 cm-1 spectral sampling, enabled by a Chemical Vapor-Deposited (CVD) diamond beamsplitter and state of the art electronics. This instrument utilizes a 3×3 detector array and a scan mirror to make high-precision infrared radiance measurements over most of a Martian hemisphere. The EMIRS instrument is optimized to capture the integrated, lower-middle atmosphere dynamics over a Martian hemisphere and will capture 60 global images per week ( 20 images per orbit) at a resolution of 100-300 km/pixel. After processing through an atmospheric retrieval algorithm, EMIRS will determine the vertical temperature profiles to 50km altitude and measure the column integrated global distribution and abundances of key atmospheric parameters (e.g. dust, water ice (clouds) and water vapor) over the Martian day, seasons and year.

  19. Searching for Dark Photons with the SeaQuest Spectrometer

    Science.gov (United States)

    Uemura, Sho; SeaQuest Collaboration

    2017-09-01

    The existence of a dark sector, containing families of particles that do not couple directly to the Standard Model, is motivated as a possible model for dark matter. A ``dark photon'' - a massive vector boson that couples weakly to electric charge - is a common component of dark sector models. The SeaQuest spectrometer at Fermilab is designed to detect dimuon pairs produced by the interaction of a 120 GeV proton beam with a rotating set of thin fixed targets. An iron-filled magnet downstream of the target, 5 meters in length, serves as a beam dump. The SeaQuest spectrometer is sensitive to dark photons that are mostly produced in the beam dump and decay to dimuons, and a SeaQuest search for dark sector particles was approved as Fermilab experiment E1067. As part of E1067, a displaced-vertex trigger was built, installed and commissioned this year. This trigger uses two planes of extruded scintillators to identify dimuons originating far downstream of the target, and is sensitive to dark photons that travel deep inside the beam dump before decaying to dimuons. This trigger will be used to take data parasitically with the primary SeaQuest physics program. In this talk I will present the displaced-vertex trigger and its performance, and projected sensitivity from future running.

  20. Hygroscopicity of internally mixed particles composed of (NH4)2SO4 and citric acid under pulsed RH change.

    Science.gov (United States)

    Shi, Xiao-Min; Wu, Feng-Min; Jing, Bo; Wang, Na; Xu, Lin-Lin; Pang, Shu-Feng; Zhang, Yun-Hong

    2017-12-01

    In this research, we applied a pulsed RH controlling system and a rapid scan vacuum FTIR spectrometer (PRHCS-RSVFTIR) to investigate hygroscopicity of internally mixed (NH 4 ) 2 SO 4 (AS)/citric acid (CA) particles. The water content and efflorescence ratio of AS in the particles and ambient relative humidity (RH) as a function of time were obtained with a subsecond time resolution. The hygroscopic behavior of AS aerosols in two different RH control processes (equilibrium and RH pulsed processes) showed that AS droplets crystallize with RH ranging from 42% to 26.5%. It was found that the half-life time ratio between the water content in the CA particles and the gas phase under RH pulsed change was greater than one under low RH conditions (humidity (ERH) of the mixed particles with AS/CA by molar ratio 3:1 was found between 22.7% and 5.9%, which was much lower than AS particles. No efflorescence process was observed for the 1:1 mixed particles, indicating that CA greatly suppressed nucleation of AS. Our results have shown that the PRHCS-RSVFTIR is effective to simulate hygroscopicity and water transport of aerosols under fast variations in RH in atmosphere. Copyright © 2017 Elsevier Ltd. All rights reserved.

  1. Bent solenoids for spectrometers and emittance exchange sections

    International Nuclear Information System (INIS)

    Norem, J.

    1999-01-01

    Bent solenoids can be used to transport low energy beams as they provide both confinement and dispersion of particle orbits. Solenoids are being considered both as emittance exchange sections and spectrometers in the muon cooling system as part of the study of the muon collider. They present the results of a study of bent solenoids which considers the design of coupling sections between bent solenoids to straight solenoids, drift compensation fields, aberrations, and factors relating to the construction, such as field ripple, stored energy, coil forces and field errors

  2. A search for non-$q\\bar{q}$ mesons at the CERN Omega Spectrometer

    CERN Document Server

    Kirk, A.

    1999-01-01

    The non-Abelian nature of QCD suggests that particles that have a gluon constituent, such as glueballs or hybrids, should exist. Experiments WA76, WA91 and WA102 have performed a dedicated search for these states in central production using the CERN Omega Spectrometer. Several non-qqbar candidates have been observed. This paper presents a study of central meson production as a function of the difference in transverse momentum (dPT) of the exchanged particles which shows that undisputed qqbar mesons are suppressed at small dPT whereas the glueball candidates are enhanced.

  3. Hybrid emulsion spectrometer for the detection of hadronically produced heavy flavor states

    International Nuclear Information System (INIS)

    Kodama, K.; Ushida, N.; Lander, R.L.; Mokhtarani, A.; Paolone, V.S.; Wilcox, J.O.; Yager, P.M.; Edelstein, R.M.; Freyberger, A.P.; Gibaut, D.B.; Lipton, R.J.; Nichols, W.R.; Potter, D.M.; Russ, J.R.; Zhang, Y.; Jang, H.I.; Kim, J.Y.; Pac, M.Y.; Baller, B.R.; Stefanski, R.J.; Nakazawa, K.; Tasaka, S.; Choi, Y.S.; Chung, K.H.; Kim, D.C.; Park, I.G.; Song, J.S.; Yoon, C.S.; Chikawa, M.; Abe, T.; Fujii, T.; Fujioka, G.; Fujiwara, K.; Fukushima, H.; Hara, T.; Takahashi, Y.; Taruma, K.; Tsuzuki, Y.; Yokoyama, C.; Chang, S.D.; Cheon, B.G.; Cho, J.H.; Kang, J.S.; Kim, C.O.; Kim, K.Y.; Kim, T.Y.; Lee, J.C.; Lee, S.B.; Lim, G.Y.; Lim, I.T.; Nam, S.W.; Shin, T.S.; Sim, K.S.; Woo, J.K.; Isokane, Y.; Tsuneoka, Y.; Aoki, S.; Gauthier, A.; Hoshino, K.; Kitamura, H.; Kobayashi, M.; Miyanishi, M.; Nakamura, K.; Nakamura, M.; Nakamura, Y.; Nakanishi, S.; Niu, K.; Niwa, K.; Tajima, H.; Dunlea, J.M.; Frederiksen, S.G.; Kuramata, S.; Lundberg, B.G.; Oleynik, G.A.; Reay, N.W.; Reibel, K.; Rush, C.J.; Sidwell, R.A.; Stanton, N.R.; Moriyama, K.; Shibata, H.; Jaffery, T.S.; Kalbfleisch, G.R.; Skubic, P.L.; Snow, J.M.; Willis, S.E.; Yuan, W.Y.; Kusumoto, O.; Okusawa, T.; Teranaka, M.; Tominaga, T.; Watanabe, T.; Yamato, J.; Okabe, H.; Yokota, J.; Sato, Y.; Tezuka, I.; Bahk, S.Y.; Kim, S.K.

    1990-01-01

    A hybrid apparatus consisting of a movable emulsion target and a magnetic spectrometer was used in a fixed target Fermilab Tevatron experiment to study the production of heavy quarks by high-energy hadron beams. High-resolution silicon microstrip detectors were used for precise tracking in the dense particle environment. Details of the experimental apparatus, including the data acquisition system, are described. (orig.)

  4. Detection Efficiency of a ToF Spectrometer from Heavy-Ion Elastic Recoil Detection

    International Nuclear Information System (INIS)

    Barbara, E. de; Marti, G. V.; Capurro, O. A.; Fimiani, L.; Mingolla, M. G.; Negri, A. E.; Arazi, A.; Figueira, J. M.; Pacheco, A. J.; Martinez Heimann, D.; Carnelli, P. F. F.; Fernandez Niello, J. O.

    2010-01-01

    The detection efficiency of a time-of-flight system based on two micro-channel plates (MCP) time zero detectors plus a conventional silicon surface barrier detector was obtained from heavy ion elastic recoil measurements (this ToF spectrometer is mainly devoted to measurements of total fusion cross section of weakly bound projectiles on different mass-targets systems). In this work we have used beams of 7 Li, 16 O, 32 S and 35 Cl to study the mass region of interest for its application to measurements fusion cross sections in the 6,7 Li+ 27 Al systems at energies around and above the Coulomb barrier (0.8V B ≤E≤2.0V B ). As the efficiency of a ToF spectrometer is strongly dependent on the energy and mass of the detected particles, we have covered a wide range of the scattered particle energies with a high degree of accuracy at the lowest energies. The different experimental efficiency curves obtained in that way were compared with theoretical electronic stopping power curves on carbon foils and were applied.

  5. Large solid angle tracking of Monte Carlo events of heavy ion collisions in TPC magnetic spectrometers

    International Nuclear Information System (INIS)

    Lindenbaum, S.J.; Etkin, A.; Foley, K.J.; Hackenburg, R.W.; Longacre, R.S.; Love, W.A.; Morris, T.W.; Platner, E.D.; Saulys, A.C.; Asoka-Kumar, P.P.V.; Chan, C.S.; Kramer, M.A.

    1987-01-01

    The BNL/CCNY collaboration has for some time had as its goal the development and use of ≅ 4π solid angle magnetic spectrometer tracking of charged particles produced in heavy ion collision experiments at AGS, and eventually RHIC. (orig./HSI)

  6. Main Injector Particle Production Experiment Status

    International Nuclear Information System (INIS)

    Lebedev, Andre

    2007-01-01

    MIPP (FNAL-E907) is a large acceptance spectrometer to measure hadronic particle production - TPC and wire chambers to measure track parameters - TPC dE/dx, ToF, differential Cherenkov and ring imaging Cherenkov give π/K/p separation up to 100 GeV/c

  7. Study of the Production Mechanisms and Decay Properties of Charmed Particles Observed in Nuclear Emulsions Coupled to the NA14 Spectrometer

    CERN Multimedia

    2002-01-01

    The aims of this test experiment are: \\item a)~~~~to check the expected improvement in scanning speed and efficiency, due to the use of the microstrip vertex detector of the NA14 set-up and to the help of automated microscopes; \\item b)~~~~to evaluate the enrichment factor in the charmed event content of the sample to be searched, due to the particle identification power and the vertex detector of NA14; \\item c)~~~~to collect some 100 pairs of charmed particles, produced and decaying in emulsion, which would allow a comparison with the results from the WA58 experiment, in particular about the possible energy dependence of the production mechanism of associated @L^c|+~$\\bar{D}$. \\end{enumerate} The incident beam will consist of tagged photons between 70 and 150-200~GeV.

  8. Aging induced changes on NEXAFS fingerprints in individual combustion particles

    Directory of Open Access Journals (Sweden)

    V. Zelenay

    2011-11-01

    Full Text Available Soot particles can significantly influence the Earth's climate by absorbing and scattering solar radiation as well as by acting as cloud condensation nuclei. However, despite their environmental (as well as economic and political importance, the way these properties are affected by atmospheric processing of the combustion exhaust gases is still a subject of discussion. In this work, individual soot particles emitted from two different vehicles, a EURO 2 transporter, a EURO 3 passenger car, and a wood stove were investigated on a single-particle basis. The emitted exhaust, including the particulate and the gas phase, was processed in a smog chamber with artificial solar radiation. Single particle specimens of both unprocessed and aged soot were characterized using near edge X-ray absorption fine structure spectroscopy (NEXAFS and scanning electron microscopy. Comparison of NEXAFS spectra from the unprocessed particles and those resulting from exhaust photooxidation in the chamber revealed changes in the carbon functional group content. For the wood stove emissions, these changes were minor, related to the relatively mild oxidation conditions. For the EURO 2 transporter emissions, the most apparent change was that of carboxylic carbon from oxidized organic compounds condensing on the primary soot particles. For the EURO 3 car emissions oxidation of primary soot particles upon photochemical aging has likely contributed as well. Overall, the changes in the NEXAFS fingerprints were in qualitative agreement with data from an aerosol mass spectrometer. Furthermore, by taking full advantage of our in situ microreactor concept, we show that the soot particles from all three combustion sources changed their ability to take up water under humid conditions upon photochemical aging of the exhaust. Due to the selectivity and sensitivity of the NEXAFS technique for the water mass, also small amounts of water taken up into the internal voids of agglomerated

  9. Scanning electron microscopy and micro-analyses

    International Nuclear Information System (INIS)

    Brisset, F.; Repoux, L.; Ruste, J.; Grillon, F.; Robaut, F.

    2008-01-01

    Scanning electron microscopy (SEM) and the related micro-analyses are involved in extremely various domains, from the academic environments to the industrial ones. The overall theoretical bases, the main technical characteristics, and some complements of information about practical usage and maintenance are developed in this book. high-vacuum and controlled-vacuum electron microscopes are thoroughly presented, as well as the last generation of EDS (energy dispersive spectrometer) and WDS (wavelength dispersive spectrometer) micro-analysers. Beside these main topics, other analysis or observation techniques are approached, such as EBSD (electron backscattering diffraction), 3-D imaging, FIB (focussed ion beams), Monte-Carlo simulations, in-situ tests etc.. This book, in French language, is the only one which treats of this subject in such an exhaustive way. It represents the actualized and totally updated version of a previous edition of 1979. It gathers the lectures given in 2006 at the summer school of Saint Martin d'Heres (France). Content: 1 - electron-matter interactions; 2 - characteristic X-radiation, Bremsstrahlung; 3 - electron guns in SEM; 4 - elements of electronic optics; 5 - vacuum techniques; 6 - detectors used in SEM; 7 - image formation and optimization in SEM; 7a - SEM practical instructions for use; 8 - controlled pressure microscopy; 8a - applications; 9 - energy selection X-spectrometers (energy dispersive spectrometers - EDS); 9a - EDS analysis; 9b - X-EDS mapping; 10 - technological aspects of WDS; 11 - processing of EDS and WDS spectra; 12 - X-microanalysis quantifying methods; 12a - quantitative WDS microanalysis of very light elements; 13 - statistics: precision and detection limits in microanalysis; 14 - analysis of stratified samples; 15 - crystallography applied to EBSD; 16 - EBSD: history, principle and applications; 16a - EBSD analysis; 17 - Monte Carlo simulation; 18 - insulating samples in SEM and X-ray microanalysis; 18a - insulating

  10. Photon event distribution sampling: an image formation technique for scanning microscopes that permits tracking of sub-diffraction particles with high spatial and temporal resolutions.

    Science.gov (United States)

    Larkin, J D; Publicover, N G; Sutko, J L

    2011-01-01

    In photon event distribution sampling, an image formation technique for scanning microscopes, the maximum likelihood position of origin of each detected photon is acquired as a data set rather than binning photons in pixels. Subsequently, an intensity-related probability density function describing the uncertainty associated with the photon position measurement is applied to each position and individual photon intensity distributions are summed to form an image. Compared to pixel-based images, photon event distribution sampling images exhibit increased signal-to-noise and comparable spatial resolution. Photon event distribution sampling is superior to pixel-based image formation in recognizing the presence of structured (non-random) photon distributions at low photon counts and permits use of non-raster scanning patterns. A photon event distribution sampling based method for localizing single particles derived from a multi-variate normal distribution is more precise than statistical (Gaussian) fitting to pixel-based images. Using the multi-variate normal distribution method, non-raster scanning and a typical confocal microscope, localizations with 8 nm precision were achieved at 10 ms sampling rates with acquisition of ~200 photons per frame. Single nanometre precision was obtained with a greater number of photons per frame. In summary, photon event distribution sampling provides an efficient way to form images when low numbers of photons are involved and permits particle tracking with confocal point-scanning microscopes with nanometre precision deep within specimens. © 2010 The Authors Journal of Microscopy © 2010 The Royal Microscopical Society.

  11. Fabrication and electromagnetic properties of bio-based helical soft-core particles by way of Ni-Fe alloy electroplating

    Energy Technology Data Exchange (ETDEWEB)

    Lan Mingming, E-mail: lan_mingming@163.com [Bionic and Micro/Nano/Bio Manufacturing Technology Research Center, School of Mechanical Engineering and Automation, Beihang University, Beijing 100191 (China); Zhang Deyuan; Cai Jun; Zhang Wenqiang; Yuan Liming [Bionic and Micro/Nano/Bio Manufacturing Technology Research Center, School of Mechanical Engineering and Automation, Beihang University, Beijing 100191 (China)

    2011-12-15

    Ni-Fe alloy electroplating was used as a bio-limited forming process to fabricate bio-based helical soft-core ferromagnetic particles, and a low frequency vibration device was applied to the cathode to avoid microorganism (Spirulina platens) cells adhesion to the copper net during the course of plating. The morphologies and ingredients of the coated Spirulina cells were characterized using scanning electron microscopy and energy dispersive spectrometer. The complex permittivity and permeability of the samples containing the coated Spirulina cells before and after heat treatment were measured and investigated by a vector network analyzer. The results show that the Spirulina cells after plating keep their initial helical shape, and applying low frequency vibration to the copper net cathode in the plating process can effectively prevent agglomeration and intertwinement of the Spirulina cells. The microwave absorbing and electromagnetic properties of the samples containing the coated Spirulina cells particles with heat treatment are superior to those samples containing the coated Spirulina cells particles without heat treatment. - Highlights: > We used the microorganism cells as forming template to fabricate the bio-based helical soft-core ferromagnetic particles. > Microorganism selected as forming templates was Spirulina platens, which are of natural helical shape and have high aspect ratio. > Coated Spirulina cells were a kind lightweight ferromagnetic particle.

  12. Absolute activity measurements with the windowless 4π-CsI(Tl)-sandwich spectrometer

    International Nuclear Information System (INIS)

    Denecke, B.

    1994-01-01

    The windowless 4π-CsI(Tl)-sandwich spectrometer consists of two scintillation crystals sandwiching radioactive sources deposited on thin plastic foils. This configuration has a solid angle very close to 4π sr. The detectors are sensitive to charged particles with energies > 15 keV and measure photons of 15-200 keV with a probability > 98%. Disintegration rates of samples of radionuclides with complex decay modes can be determined directly from the measured count rates with uncertainties below 0.3%. Radionuclide solutions of 57 Co, 109 Cd, 125 I, 152 Eu and 192 Ir were standardised, partly in the framework of international comparisons. A detailed description of the spectrometer and the measurement procedure is given. (orig.)

  13. Absolute activity measurements with the windowless 4π-CsI(Tl)-sandwich spectrometer

    Science.gov (United States)

    Denecke, B.

    1994-01-01

    The windowless 4π-CsI(Tl)-sandwich spectrometer consists of two scintillation crystals sandwiching radioactive sources deposited on thin plastic foils. This configuration has a solid angle very close to 4π sr. The detectors are sensitive to charged particles with energies > 15 keV and measure photons of 15-200 keV with a probability > 98%. Disintegration rates of samples of radionuclides with complex decay modes can be determined directly from the measured count rates with uncertainties below 0.3%. Radionuclide solutions of 57Co, 109Cd, 125I, 152Eu and 192Ir were standardised, partly in the framework of international comparisons. A detailed description of the spectrometer and the measurement procedure is given.

  14. The CEBAF large acceptance spectrometer (CLAS)

    Energy Technology Data Exchange (ETDEWEB)

    Mecking, B.A.; Adams, G.; Ahmad, S.; Anciant, E.; Anghinolfi, M.; Asavapibhop, B.; Asryan, G.; Audit, G.; Auger, T.; Avakian, H.; Ball, J.P.; Barbosa, F.J.; Barrow, S.; Battaglieri, M.; Beard, K.; Berman, B.L.; Bianchi, N.; Boiarinov, S.; Bonneau, P.; Briscoe, W.J.; Brooks, W.K.; Burkert, V.D.; Carman, D.S.; Carstens, T.; Cetina, C.; Christo, S.B.; Cole, P.L.; Coleman, A.; Connelly, J.; Cords, D.; Corvisiero, P.; Crabb, D.; Crannell, H.; Cuevas, R.C.; Degtyarenko, P.V.; Dennis, L.; DeSanctis, E.; DeVita, R.; Distelbrink, J.; Dodge, G.E.; Dodge, W.; Doolittle, G.; Doughty, D.; Dugger, M.; Duncan, W.S.; Dytman, S.; Egiyan, H.; Egiyan, K.S.; Elouadrhiri, L.; Feuerbach, R.J.; Ficenec, J.; Frolov, V.; Funsten, H.; Gilfoyle, G.P.; Giovanetti, K.L.; Golovatch, E.; Gram, J.; Guidal, M.; Gyurjyan, V.; Heddle, D.; Hemler, P.; Hersman, F.W.; Hicks, K.; Hicks, R.S.; Holtrop, M.; Hyde-Wright, C.E.; Insley, D.; Ito, M.M.; Jacobs, G.; Jenkins, D.; Joo, K.; Joyce, D.; Kashy, D.; Khandaker, M.; Kim, W.; Klein, A.; Klein, F.J.; Klusman, M.; Kossov, M.; Kramer, L.; Koubarovski, V.; Kuhn, S.E.; Lake, A.; Lawrence, D.; Longhi, A.; Lukashin, K.; Lachniet, J.; Magahiz, R.A.; Major, W.; Manak, J.J.; Marchand, C.; Martin, C.; Matthews, S.K.; McMullen, M.; McNabb, J.W.C.; Mestayer, M.D.; Minehart, R.; Mirazita, M.; Miskimen, R.; Muccifora, V.; Mueller, J.; Murphy, L.Y.; Mutchler, G.S.; Napolitano, J.; Niculescu, I.; Niczyporuk, B.B.; Nozar, M.; O' Brien, J.T.; Opper, A.K.; O' Meara, J.E.; Pasyuk, E.; Philips, S.A.; Polli, E.; Price, J.W.; Pozdniakov, S.; Qin, L.M.; Raue, B.A.; Riccardi, G.; Ricco, G.; Riggs, C.; Ripani, M.; Ritchie, B.G.; Robb, J.; Ronchetti, F.; Rossi, P.; Roudot, F.; Salgado, C.; Sapunenko, V.; Schumacher, R.A.; Serov, V.S.; Sharabian, Y.G.; Smith, E.E.S. E-mail: elton@jlab.org; Smith, L.C.; Smith, T.; Sober, D.I.; Stavinsky, A.; Stepanyan, S.; Stoler, P.; Taiuti, M.; Taylor, W.M.; Taylor, S.; Tedeschi, D.J.; Thoma, U.; Thompson, R.; Tilles, D.; Todor, L. [and others

    2003-05-11

    The CEBAF large acceptance spectrometer (CLAS) is used to study photo- and electro-induced nuclear and hadronic reactions by providing efficient detection of neutral and charged particles over a good fraction of the full solid angle. A collaboration of about 30 institutions has designed, assembled, and commissioned CLAS in Hall B at the Thomas Jefferson National Accelerator Facility. The CLAS detector is based on a novel six-coil toroidal magnet which provides a largely azimuthal field distribution. Trajectory reconstruction using drift chambers results in a momentum resolution of 0.5% at forward angles. Cherenkov counters, time-of-flight scintillators, and electromagnetic calorimeters provide good particle identification. Fast triggering and high data-acquisition rates allow operation at a luminosity of 10{sup 34} nucleon cm{sup -2} s{sup -1}. These capabilities are being used in a broad experimental program to study the structure and interactions of mesons, nucleons, and nuclei using polarized and unpolarized electron and photon beams and targets. This paper is a comprehensive and general description of the design, construction and performance of CLAS.

  15. Magnetic and electric deflector spectrometers for ion emission analysis from laser generated plasma

    Directory of Open Access Journals (Sweden)

    Torrisi Lorenzo

    2018-01-01

    Full Text Available The pulsed laser-generated plasma in vacuum and at low and high intensities can be characterized using different physical diagnostics. The charge particles emission can be characterized using magnetic, electric and magnet-electrical spectrometers. Such on-line techniques are often based on time-of-flight (TOF measurements. A 90° electric deflection system is employed as ion energy analyzer (IEA acting as a filter of the mass-to-charge ratio of emitted ions towards a secondary electron multiplier. It determines the ion energy and charge state distributions. The measure of the ion and electron currents as a function of the mass-to-charge ratio can be also determined by a magnetic deflector spectrometer, using a magnetic field of the order of 0.35 T, orthogonal to the ion incident direction, and an array of little ion collectors (IC at different angles. A Thomson parabola spectrometer, employing gaf-chromix as detector, permits to be employed for ion mass, energy and charge state recognition. Mass quadrupole spectrometry, based on radiofrequency electric field oscillations, can be employed to characterize the plasma ion emission. Measurements performed on plasma produced by different lasers, irradiation conditions and targets are presented and discussed. Complementary measurements, based on mass and optical spectroscopy, semiconductor detectors, fast CCD camera and Langmuir probes are also employed for the full plasma characterization. Simulation programs, such as SRIM, SREM, and COMSOL are employed for the charge particle recognition.

  16. Magnetic and electric deflector spectrometers for ion emission analysis from laser generated plasma

    Science.gov (United States)

    Torrisi, Lorenzo; Costa, Giuseppe; Ceccio, Giovanni; Cannavò, Antonino; Restuccia, Nancy; Cutroneo, Mariapompea

    2018-01-01

    The pulsed laser-generated plasma in vacuum and at low and high intensities can be characterized using different physical diagnostics. The charge particles emission can be characterized using magnetic, electric and magnet-electrical spectrometers. Such on-line techniques are often based on time-of-flight (TOF) measurements. A 90° electric deflection system is employed as ion energy analyzer (IEA) acting as a filter of the mass-to-charge ratio of emitted ions towards a secondary electron multiplier. It determines the ion energy and charge state distributions. The measure of the ion and electron currents as a function of the mass-to-charge ratio can be also determined by a magnetic deflector spectrometer, using a magnetic field of the order of 0.35 T, orthogonal to the ion incident direction, and an array of little ion collectors (IC) at different angles. A Thomson parabola spectrometer, employing gaf-chromix as detector, permits to be employed for ion mass, energy and charge state recognition. Mass quadrupole spectrometry, based on radiofrequency electric field oscillations, can be employed to characterize the plasma ion emission. Measurements performed on plasma produced by different lasers, irradiation conditions and targets are presented and discussed. Complementary measurements, based on mass and optical spectroscopy, semiconductor detectors, fast CCD camera and Langmuir probes are also employed for the full plasma characterization. Simulation programs, such as SRIM, SREM, and COMSOL are employed for the charge particle recognition.

  17. Mass spectrometric analysis and aerodynamic properties of various types of combustion-related aerosol particles

    Science.gov (United States)

    Schneider, J.; Weimer, S.; Drewnick, F.; Borrmann, S.; Helas, G.; Gwaze, P.; Schmid, O.; Andreae, M. O.; Kirchner, U.

    2006-12-01

    Various types of combustion-related particles in the size range between 100 and 850 nm were analyzed with an aerosol mass spectrometer and a differential mobility analyzer. The measurements were performed with particles originating from biomass burning, diesel engine exhaust, laboratory combustion of diesel fuel and gasoline, as well as from spark soot generation. Physical and morphological parameters like fractal dimension, effective density, bulk density and dynamic shape factor were derived or at least approximated from the measurements of electrical mobility diameter and vacuum aerodynamic diameter. The relative intensities of the mass peaks in the mass spectra obtained from particles generated by a commercial diesel passenger car, by diesel combustion in a laboratory burner, and by evaporating and re-condensing lubrication oil were found to be very similar. The mass spectra from biomass burning particles show signatures identified as organic compounds like levoglucosan but also others which are yet unidentified. The aerodynamic behavior yielded a fractal dimension (Df) of 2.09 +/- 0.06 for biomass burning particles from the combustion of dry beech sticks, but showed values around three, and hence more compact particle morphologies, for particles from combustion of more natural oak. Scanning electron microscope images confirmed the finding that the beech combustion particles were fractal-like aggregates, while the oak combustion particles displayed a much more compact shape. For particles from laboratory combusted diesel fuel, a Df value of 2.35 was found, for spark soot particles, Df [approximate] 2.10. The aerodynamic properties of fractal-like particles from dry beech wood combustion indicate an aerodynamic shape factor [chi] that increases with electrical mobility diameter, and a bulk density of 1.92 g cm-3. An upper limit of [chi] [approximate] 1.2 was inferred for the shape factor of the more compact particles from oak combustion.

  18. Microprocessor based data acquisition system for Moessbauer spectrometer

    International Nuclear Information System (INIS)

    Patwardhan, P.K.; Indurkar, V.S.

    1981-01-01

    A data acquisition system, for Moessbauer spectrometer and other probability distribution spectrum is described. This utilizes the advantages of incorporating a microcomputer for providing a flexible analytical capability and speed of hard wired MCS unit updating channel contents in DMA. Holbourn, Player and Woodhams have recently described a microprocessor controlled Moessbauer spectrometer where microprocessor performs the task of updating channel contents, requiring about 60 micro seconds in interrupt mode. This imposes restrictions on increasing the channel number and on increasing the velocity scan frequency in order to cover higher velocity ranges. The system described in this article performs data acquisition in faster direct memory access. It is a two module system, (1) MCS module (2) Microcomputer module, arranged around a common address, data and control buses. The microcomputer module has an access to the system data during flyback periods and can be programmed for the task of monitor on progess of experiment and as a manipulator of various control operations needed during experiment. The system firmware includes: (1) MONITOR (2) BLOCK-TRANSFER (3) DATA-SMOOTHING (4) DECIMAL-CONVERTER (5) MATH. The scope of this firmware is briefly described. (author)

  19. Dosimetry and LET spectrometry in C 290 MeV/n and Ne 400 MeV/n HIMAC ion beam by different TLD's, TED based LET spectrometers, and Si energy-deposition spectrometer

    International Nuclear Information System (INIS)

    Spurny, F.; Brabcova, K.; Jadrnickova, I.; Uchihori, Y.; Kitamura, H.; Yasuda, N.; Molokanov, A. G.

    2009-01-01

    The sets of track etched detectors based (TED) spectrometer's of the linear energy transfer (LET) have been, together with two types of thermoluminescent detectors (TLD)and MDU- Liulin energy deposition spectrometer exposed in the C 290 MeV/n and Ne 400 MeV/n ion beams at the HlMAC installation at NIRS, Chiba, Japan. The experiment has been performed in the frame of NPI project 20P241 agreed by HlMAC P AC at the beginning of 2008 year. Up to now, moxstle only results obtained in C-ion beam have been treated and analyzed. Sets of TED spectrometer's and TLD detectors have been exposed in 19 depths in the C-ion beam with expected LET values of primary particles from 13 keV/μm in water, through the Bragg peak area up to two depth behind the Bragg peak. The contribution of fragments to total number of events, and to the energy absorbed in Si has been determined, when possible separately for different fragments. In all cases also total contribution of fragments (and other secondary particles) to the total number of energy deposition events and to the absorbed dose has been estimated. LET and energy deposition spectra obtained will be compared together , a good agreement of data has bee stated. Some of results have been also compared with those obtained by calculation by means of PHITS code. (authors)

  20. Short description of BMS/BMF MDT chamber production for the muon spectrometer of the ATLAS experiment

    International Nuclear Information System (INIS)

    Barashkov, A.V.; Glonti, G.L.; Gongadze, A.L.; Gongadze, I.B.; Gostkin, M.I.; Gus'kov, A.V.; Dedovich, D.V.; Demichev, M.A.; Evtukhovich, P.G.; Elagin, A.L.; Zhemchugov, A.S.; Il'yushenko, E.N.; Kotov, S.A.; Kotova, T.I.; Korolevich, Ya.V.; Kruchonok, V.G.; Krumshtejn, Z.V.; Kuznetsov, N.K.; Lomidze, D.D.; Nikolaev, K.V.; Potrap, I.N.; Rudenko, T.O.; Kharchenko, D.V.; Tskhadadze, Eh.G.; Chepurnov, V.F.; Shelkov, G.A.; Shiyakova, M.M.; Shcherbakov, A.A.; Podkladkin, S.Yu.

    2005-01-01

    The method of assembly of the MDT chambers for the muon spectrometer of the ATLAS experiment is described. During 2000-2004 ∼ 25000 drift tubes were produced at the DLNP, JINR. The tubes were assembled into 84 muon chambers of BMS/BMF type, one of the six main types for the barrel part of the ATLAS muon spectrometer. Particle momenta must be measured in the ATLAS spectrometer with very high precision (2% at 100 GeV/c and 10% at 1000 GeV/c), which required to produce the coordinate detectors with very high (∼80 μm) precision. We describe the method of assembly of large-scale 5-10 m 2 muon chambers with the signal wire mean deviation from the nominal position less than 20 μm

  1. Particle identification by nuclear emulsions in the OPERA experiment

    International Nuclear Information System (INIS)

    Manai, Kais

    2007-01-01

    The OPERA experiment will try to confirm the ν μ →ν τ oscillations by the appearance of the ν τ in a pure ν μ beam. Indeed, a neutrino beam almost pure is produced at CERN (CNGS Beam) and sent to the OPERA detector. The detector is composed of two muons spectrometers and a target formed by walls of bricks. Each brick is an alternation of lead plates and emulsions. This modular structure allows to reconstruct the kink topology of the τ lepton decay with a high spatial resolution. The great challenge of the OPERA experiment is to detect the ν τ interactions with the less uncertainty. To reduce this uncertainty it is essential to identify with the greatest efficiency any background event not including a tau particle. My work permits to reduce background. My principal contribution concerns the selection development, the reconstruction and the muons identification at low energy. This work is based on the setting of variables related to the deposit energy and the multiple scattering. Previously, only deposit energy was used in the analyses of pion/muon separation. This study allows doubling the muon identification efficiency at low energy. This leads to increase the background events rejection in OPERA and to decrease the contamination by 30 pour cent. I also studied the nuclear emulsions capacity to identify charged particles through the analysis of a test beam carried out by the Nagoya group. This test contains protons and pions with different energies. My work proves that the European scan system gives comparable results with those obtained by the Japanese scan system. (Author)

  2. A gamma scintillation spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Symbalisty, S

    1952-07-01

    A scintillation type gamma ray spectrometer employing coincidence counting, designed and built at the Physics Department of the University of Western Ontario is described. The spectrometer is composed of two anthracene and photomultiplier radiation detectors, two pulse analyzing channels, a coincidence stage, three scalers and a high voltage stabilized supply. A preliminary experiment to test the operation of the spectrometer was performed and the results of this test are presented. (author)

  3. Simplified monte carlo simulation for Beijing spectrometer

    International Nuclear Information System (INIS)

    Wang Taijie; Wang Shuqin; Yan Wuguang; Huang Yinzhi; Huang Deqiang; Lang Pengfei

    1986-01-01

    The Monte Carlo method based on the functionization of the performance of detectors and the transformation of values of kinematical variables into ''measured'' ones by means of smearing has been used to program the Monte Carlo simulation of the performance of the Beijing Spectrometer (BES) in FORTRAN language named BESMC. It can be used to investigate the multiplicity, the particle type, and the distribution of four-momentum of the final states of electron-positron collision, and also the response of the BES to these final states. Thus, it provides a measure to examine whether the overall design of the BES is reasonable and to decide the physical topics of the BES

  4. A laser sheet self-calibration method for scanning PIV

    Science.gov (United States)

    Knutsen, Anna N.; Lawson, John M.; Dawson, James R.; Worth, Nicholas A.

    2017-10-01

    Knowledge of laser sheet position, orientation, and thickness is a fundamental requirement of scanning PIV and other laser-scanning methods. This paper describes the development and evaluation of a new laser sheet self-calibration method for stereoscopic scanning PIV, which allows the measurement of these properties from particle images themselves. The approach is to fit a laser sheet model by treating particles as randomly distributed probes of the laser sheet profile, whose position is obtained via a triangulation procedure enhanced by matching particle images according to their variation in brightness over a scan. Numerical simulations and tests with experimental data were used to quantify the sensitivity of the method to typical experimental error sources and validate its performance in practice. The numerical simulations demonstrate the accurate recovery of the laser sheet parameters over range of different seeding densities and sheet thicknesses. Furthermore, they show that the method is robust to significant image noise and camera misalignment. Tests with experimental data confirm that the laser sheet model can be accurately reconstructed with no impairment to PIV measurement accuracy. The new method is more efficient and robust in comparison with the standard (self-) calibration approach, which requires an involved, separate calibration step that is sensitive to experimental misalignments. The method significantly improves the practicality of making accurate scanning PIV measurements and broadens its potential applicability to scanning systems with significant vibrations.

  5. Contribution of sulfuric acid and oxidized organic compounds to particle formation and growth

    Directory of Open Access Journals (Sweden)

    F. Riccobono

    2012-10-01

    Full Text Available Lack of knowledge about the mechanisms underlying new particle formation and their subsequent growth is one of the main causes for the large uncertainty in estimating the radiative forcing of atmospheric aerosols in global models. We performed chamber experiments designed to study the contributions of sulfuric acid and organic vapors to the formation and early growth of nucleated particles. Distinct experiments in the presence of two different organic precursors (1,3,5-trimethylbenzene and α-pinene showed the ability of these compounds to reproduce the formation rates observed in the low troposphere. These results were obtained measuring the sulfuric acid concentrations with two chemical ionization mass spectrometers confirming the results of a previous study which modeled the sulfuric acid concentrations in presence of 1,3,5-trimethylbenzene.

    New analysis methods were applied to the data collected with a condensation particle counter battery and a scanning mobility particle sizer, allowing the assessment of the size resolved growth rates of freshly nucleated particles. The effect of organic vapors on particle growth was investigated by means of the growth rate enhancement factor (Γ, defined as the ratio between the measured growth rate in the presence of α-pinene and the kinetically limited growth rate of the sulfuric acid and water system. The observed Γ values indicate that the growth is already dominated by organic compounds at particle diameters of 2 nm. Both the absolute growth rates and Γ showed a strong dependence on particle size, supporting the nano-Köhler theory. Moreover, the separation of the contributions from sulfuric acid and organic compounds to particle growth reveals that the organic contribution seems to be enhanced by the sulfuric acid concentration. Finally, the size resolved growth analysis indicates that both condensation of oxidized organic compounds and reactive uptake contribute to particle growth.

  6. GoAmazon 2014/15 Thermal Desorption Chemical Ionization Mass Spectrometer (TDCIMS) Field Campaign Report

    Energy Technology Data Exchange (ETDEWEB)

    Smith, JN [Univ. of California, Irvine, CA (United States)

    2016-04-01

    The Thermal Desorption Chemical Ionization Mass Spectrometer (TDCIMS) deployment to the U.S. Department of Energy (DOE)’s Atmospheric Radiation Measurement (ARM) Climate Research Facility T3 site in Manacapuru, Brazil, was motivated by two main scientific objectives of the Green Ocean Amazon (GoAmazon) 2014/15 field campaign. 1) Study the interactions between anthropogenic and biogenic emissions by determining important molecular species in ambient nanoparticles. To address this, TDCIMS data will be combined with coincident measurements such as gas-phase sulfuric acid to determine the contribution of sulfuric acid condensation to nucleation and growth. We can then compare that result to TDCIMS-derived nanoparticle composition to determine the fraction of growth that can be attributed to the uptake of organic compounds. The molecular composition of sampled particles will also be used to attribute specific chemical species and mechanisms to growth, such as the condensation of low-volatility species or the oligomerization of α-dicarbonyl compounds. 2) Determine the source of new ambient nanoparticles in the Amazon. The hypothesis prior to measurements was that potassium salts formed from the evaporation of primary particles emitted by fungal spores can provide a unique and important pathway for new particle production in the Amazon basin. To explore this hypothesis, the TDCIMS recorded the mass spectra of sampled ambient particles using a protonated water cluster Chemical Ionization Mass Spectrometer (CIMS). Laboratory tests performed using potassium salts show that the TDCIMS can detect potassium with high sensitivity with this technique.

  7. Development of a Multi-GeV spectrometer for laser-plasma experiment at FLAME

    Science.gov (United States)

    Valente, P.; Anelli, F.; Bacci, A.; Batani, D.; Bellaveglia, M.; Benocci, R.; Benedetti, C.; Cacciotti, L.; Cecchetti, C. A.; Clozza, A.; Cultrera, L.; Di Pirro, G.; Drenska, N.; Faccini, R.; Ferrario, M.; Filippetto, D.; Fioravanti, S.; Gallo, A.; Gamucci, A.; Gatti, G.; Ghigo, A.; Giulietti, A.; Giulietti, D.; Gizzi, L. A.; Koester, P.; Labate, L.; Levato, T.; Lollo, V.; Londrillo, P.; Martellotti, S.; Pace, E.; Pathak, N.; Rossi, A.; Tani, F.; Serafini, L.; Turchetti, G.; Vaccarezza, C.

    2011-10-01

    The advance in laser-plasma acceleration techniques pushes the regime of the resulting accelerated particles to higher energies and intensities. In particular, the upcoming experiments with the 250 TW laser at the FLAME facility of the INFN Laboratori Nazionali di Frascati, will enter the GeV regime with more than 100 pC of electrons. At the current status of understanding of the acceleration mechanism, relatively large angular and energy spreads are expected. There is therefore the need for developing a device capable to measure the energy of electrons over three orders of magnitude (few MeV to few GeV), with still unknown angular divergences. Within the PlasmonX experiment at FLAME, a spectrometer is being constructed to perform these measurements. It is made of an electro-magnet and a screen made of scintillating fibers for the measurement of the trajectories of the particles. The large range of operation, the huge number of particles and the need to focus the divergence, present challenges in the design and construction of such a device. We present the design considerations for this spectrometer that lead to the use of scintillating fibers, multichannel photo-multipliers and a multiplexing electronics, a combination which is innovative in the field. We also present the experimental results obtained with a high intensity electron beam performed on a prototype at the LNF beam test facility.

  8. Development of a Multi-GeV spectrometer for laser-plasma experiment at FLAME

    International Nuclear Information System (INIS)

    Valente, P.; Anelli, F.; Bacci, A.; Batani, D.; Bellaveglia, M.; Benocci, R.; Benedetti, C.; Cacciotti, L.; Cecchetti, C.A.; Clozza, A.; Cultrera, L.; Di Pirro, G.; Drenska, N.; Faccini, R.; Ferrario, M.; Filippetto, D.; Fioravanti, S.; Gallo, A.; Gamucci, A.; Gatti, G.

    2011-01-01

    The advance in laser-plasma acceleration techniques pushes the regime of the resulting accelerated particles to higher energies and intensities. In particular, the upcoming experiments with the 250 TW laser at the FLAME facility of the INFN Laboratori Nazionali di Frascati, will enter the GeV regime with more than 100 pC of electrons. At the current status of understanding of the acceleration mechanism, relatively large angular and energy spreads are expected. There is therefore the need for developing a device capable to measure the energy of electrons over three orders of magnitude (few MeV to few GeV), with still unknown angular divergences. Within the PlasmonX experiment at FLAME, a spectrometer is being constructed to perform these measurements. It is made of an electro-magnet and a screen made of scintillating fibers for the measurement of the trajectories of the particles. The large range of operation, the huge number of particles and the need to focus the divergence, present challenges in the design and construction of such a device. We present the design considerations for this spectrometer that lead to the use of scintillating fibers, multichannel photo-multipliers and a multiplexing electronics, a combination which is innovative in the field. We also present the experimental results obtained with a high intensity electron beam performed on a prototype at the LNF beam test facility.

  9. Emissions from Ethanol-Gasoline Blends: A Single Particle Perspective

    Directory of Open Access Journals (Sweden)

    Peter H. McMurry

    2011-06-01

    Full Text Available Due to its agricultural origin and function as a fuel oxygenate, ethanol is being promoted as an alternative biomass-based fuel for use in spark ignition engines, with mandates for its use at state and regional levels. While it has been established that the addition of ethanol to a fuel reduces the particulate mass concentration in the exhaust, little attention has been paid to changes in the physicochemical properties of the emitted particles. In this work, a dynamometer-mounted GM Quad-4 spark ignition engine run without aftertreatment at 1,500 RPM and 100% load was used with four different fuel blends, containing 0, 20, 40 and 85 percent ethanol in gasoline. This allowed the effects of the fuel composition to be isolated from other effects. Instrumentation employed included two Aerosol Time-of-Flight Mass Spectrometers covering different size ranges for analysis of single particle composition, an Aethalometer for black carbon, a Scanning Mobility Particle Sizer for particle size distributions, a Photoelectric Aerosol Sensor for particle-bound polycyclic aromatic hydrocarbon (PAH species and gravimetric filter measurements for particulate mass concentrations. It was found that, under the conditions investigated here, additional ethanol content in the fuel changes the particle size distribution, especially in the accumulation mode, and decreases the black carbon and total particulate mass concentrations. The molecular weight distribution of the PAHs was found to decrease with added ethanol. However, PAHs produced from higher ethanol-content fuels are associated with NO2− (m/z—46 in the single-particle mass spectra, indicating the presence of nitro-PAHs. Compounds associated with the gasoline (e.g., sulfur-containing species are diminished due to dilution as ethanol is added to the fuel relative to those associated with the lubricating oil (e.g., calcium, zinc, phosphate in the single particle spectra. These changes have potential

  10. TOF spectrometer with improved sensitivity for ERDA of light isotopes

    International Nuclear Information System (INIS)

    Siketic, Z.; Bogdanovic Radovic, I.; Jaksic, M.

    2009-01-01

    Time-of-Flight Elastic Recoil Detection Analysis (TOF ERDA) is a well established and powerful ion beam analytical technique. It is used for simultaneous and quantitative analysis of elemental depth distributions of light and medium mass elements in both light and heavy matrices. Contrary to silicon particle detectors, the efficiency of the carbon-foil MCP time detectors in TOF system depends on energy and electronic stopping power of analyzing recoil atoms in the C foil and it is often less than 100% for light elements (H, He, Li). This is particularly critical for hydrogen isotopes where detection efficiency can be drastically reduced (∼ 10%). Therefore, TOF ERDA spectrometers were so far not the best choice for depth profiling and quantification of light elements. To improve the detection efficiency of TOF ERDA, the electron emission of C foils (∼ 0.3 μg/cm 2 ) has been enhanced by evaporating a thin LiF layer on the foil. That procedure improved significantly detection efficiency of hydrogen and other light elements, making TOF ERDA spectrometer more suitable for multielemental analysis applications. The capabilities of upgraded spectrometer were demonstrated on samples with well known as well as unknown concentration and depth distribution of H and D.(author)

  11. Acquisition of HPLC-Mass Spectrometer

    Science.gov (United States)

    2015-08-18

    31-Jan-2015 Approved for Public Release; Distribution Unlimited Final Report: Acquisition of HPLC -Mass Spectrometer The views, opinions and/or findings...published in peer-reviewed journals: Final Report: Acquisition of HPLC -Mass Spectrometer Report Title The acquisition of the mass spectrometer has been a

  12. Outdoor chamber measurements of biological aerosols with a passive FTIR spectrometer

    Science.gov (United States)

    D'Amico, Francis M.; Emge, Darren K.; Roelant, Geoffrey J.

    2004-02-01

    Outdoor measurements of dry bacillus subtilis (BG) spores were conducted with a passive Fourier transform infrared (FTIR) spectrometer using two types of chambers. One was a large open-ended cell, and the other was a canyon of similar dimensions. The canyon exposes the aerosol plume to downwelling sky radiance, while the open-ended cell does not. The goal of the experiments was to develop a suitable test methodology for evaluation of passive standoff detectors for open-air aerosol measurements. Dry BG aerosol particles were dispersed with a blower through an opening in the side of the chamber to create a pseudo-stationary plume, wind conditions permitting. Numerous trials were performed with the FTIR spectrometer positioned to view mountain, sky and mixed mountain-sky backgrounds. This paper will discuss the results of the FTIR measurements for BG and Kaolin dust releases.

  13. A review on research activities using the SANS spectrometer in transmission geometry at ET-RR-1 reactor

    International Nuclear Information System (INIS)

    Adib, M.

    1999-01-01

    The phased double rotor facility operating at ET-RR-1 reactor (2MW) was rearranged to operate as SANS spectrometer in transmission geometry. The rotors are suspended in magnetic fields and are spinning up to 16,000 rpm producing bursts of polyenergetic neutrons with wavelengths from 0.2 nm to 6.5 nm and beam divergence of 17' on the sample. The review on research activities using the SANS spectrometer and its applications for powder particle size determination and the long wavelength fluctuation of magnetization of the Fe-Ni alloys are discussed. (author)

  14. Simulations for a compact electron-positron spectrometer

    International Nuclear Information System (INIS)

    Filep, T.; Krasznahorkay, A.; Csatlos, M.; Gulyas, J.

    2011-01-01

    Complete text of publication follows. In the frame of the ENSAR (FP7) project, we are constructing a Compact Positron- Electron spectrometer (COPE) using toroidal magnetic field. It will be used for studying the internal pair creation process in nuclear transitions. It will look like a miniaturized model of the ATLAS spectrometer at CERN at a scale of 1:100. The mean design parameters are high efficiency, good energy resolution and precise angle reconstruction. By our plans the size of this spectrometer would be limited to a diameter of about 30 cm and length about 20 cm, having 1 % energy- and 2deg angular resolutions. The solid angle of the planned spectrometer will be 2π. It is necessary to develop a geometry in which the inhomogeneity of the field can be easily handled. Prior to the construction it was necessary to perform computer simulations in order to avoid rough construction mistakes. The better approach of the reality with simulations is very important. The problem what we have to solve is very complicated. We need to simulate the magnetic field and trajectory of the particle moving in that field. We started our simulations using the PerMag software package. >From the result we learned the followings: 1) It has no meaning to cover the magnets with iron coat because it complicates the magnetic field. 2) It is not a good idea to form the magnetic one-segment from a big magnet and 12 smaller magnets. The fringing field of the small magnets significantly modifies the magnetic field distribution around the segment. On the other hand the construction of one segment from pieces is very difficult in reality. 3) The best shape for a segment which can easily be constructed is simple box. The PerMag package could simulate the magnetic field only in 2D, but we wanted to do more precise simulation in 3D. The free package developed by the European Synchrotron Radiation Facility (ESRF) was used for the simulation of the magnetic field applying the finite element method

  15. On the origin of particle fluxes from thunderclouds

    International Nuclear Information System (INIS)

    Chilingarian, A.; Chilingaryan, S.; Karapetyan, T.; Khanikyants, Y.; Pokhsraryan, D.; Soghomonyan, S.

    2017-01-01

    We present the observational data on registration of atmospheric discharges simultaneously with the detection of elementary particles performed during thunderstorms at 3200m altitudes above sea level on Mt. Aragats in Armenia. Throughout the 2016 summer campaign on Aragats we monitored lightning occurrences and signals from NaI spectrometers, plastic scintillators, and Neutron Monitor proportional counters, and analyzed the shape of registered pulses. Particle detector signals were synchronized with lightning occurrences on microsecond time scale. Our measurements prove that all signals registered by particle detectors simultaneously with lightning were Electromagnetic interferences (EMI) and not typical responses of particle detectors on the passage of neutral or charged elementary particles. (author)

  16. A new approach for accurate mass assignment on a multi-turn time-of-flight mass spectrometer.

    Science.gov (United States)

    Hondo, Toshinobu; Jensen, Kirk R; Aoki, Jun; Toyoda, Michisato

    2017-12-01

    A simple, effective accurate mass assignment procedure for a time-of-flight mass spectrometer is desirable. External mass calibration using a mass calibration standard together with an internal mass reference (lock mass) is a common technique for mass assignment, however, using polynomial fitting can result in mass-dependent errors. By using the multi-turn time-of-flight mass spectrometer infiTOF-UHV, we were able to obtain multiple time-of-flight data from an ion monitored under several different numbers of laps that was then used to calculate a mass calibration equation. We have developed a data acquisition system that simultaneously monitors spectra at several different lap conditions with on-the-fly centroid determination and scan law estimation, which is a function of acceleration voltage, flight path, and instrumental time delay. Less than 0.9 mDa mass errors were observed for assigned mass to charge ratios ( m/z) ranging between 4 and 134 using only 40 Ar + as a reference. It was also observed that estimating the scan law on-the-fly provides excellent mass drift compensation.

  17. An Alpha Proton X-Ray Spectrometer for Mars-96 and Mars Pathfinder

    Science.gov (United States)

    Rieder, R.; Wanke, H.; Economou, T.

    1996-09-01

    Mars Pathfinder and the Russian Mars-96 will carry an Alpha Proton X-Ray Spectrometer (APXS) for the determination of the chemical composition of Martian rocks and soil. The instrument will measure the concentration of all major and many minor elements, including C,N and O, at levels above typically 1%. The method employed consist of bombarding a sample of 50 mm diameter with alpha particles from a radioactive source (50 mCi of Cm-244) and measuring: (i) backscattered alpha particles (alpha mode) (ii) protons from (a,p) reactions with some light elements (proton mode) (iii) characteristic X-rays emitted from the sample (X-ray mode). The APXS has a long standing space heritage, going back to Surveyor V,VI and VII (1967/68) and the Soviet Phobos (1988) missions. The present design is the result of an endeavour to reduce mass and power consumption to 600g/ 300mW. It consist of a sensor head containing the alpha sources, a telescope of a silicon detectors for the detection of the alpha particles and protons and a separate X-ray detector with its preamplifier, and an electronics box (80x70x60 mm) containing a microcontroller based multichannel spectrometer. The paper will describe the APXS flight hardware and present results obtained with the flight instrument that will show the instrument capabili- ties and the expected results to be obtained during surface operations on Mars.

  18. Fourier Transform Spectrometer System

    Science.gov (United States)

    Campbell, Joel F. (Inventor)

    2014-01-01

    A Fourier transform spectrometer (FTS) data acquisition system includes an FTS spectrometer that receives a spectral signal and a laser signal. The system further includes a wideband detector, which is in communication with the FTS spectrometer and receives the spectral signal and laser signal from the FTS spectrometer. The wideband detector produces a composite signal comprising the laser signal and the spectral signal. The system further comprises a converter in communication with the wideband detector to receive and digitize the composite signal. The system further includes a signal processing unit that receives the composite signal from the converter. The signal processing unit further filters the laser signal and the spectral signal from the composite signal and demodulates the laser signal, to produce velocity corrected spectral data.

  19. Characterization of winter airborne particles at Emperor Qin's Terra-cotta Museum, China

    Energy Technology Data Exchange (ETDEWEB)

    Hu, Tafeng, E-mail: hutafeng@hotmail.com [Department of Environmental Science and Engineering, Xi' an Jiaotong University, Xi' an, 710049 (China); SKLLQG, Institute of Earth Environment, Chinese Academy of Sciences, Xi' an, 710075 (China); Department of Civil and Structural Engineering, The Hong Kong Polytechnic University, Hong Kong (China); Lee, Shuncheng [Department of Civil and Structural Engineering, The Hong Kong Polytechnic University, Hong Kong (China); Cao, Junji [Department of Environmental Science and Engineering, Xi' an Jiaotong University, Xi' an, 710049 (China); SKLLQG, Institute of Earth Environment, Chinese Academy of Sciences, Xi' an, 710075 (China); Chow, Judith C.; Watson, John G. [SKLLQG, Institute of Earth Environment, Chinese Academy of Sciences, Xi' an, 710075 (China); Division of Atmospheric Sciences, Desert of Research Institute, Reno (United States); Ho, Kinfai; Ho, Wingkei [Department of Civil and Structural Engineering, The Hong Kong Polytechnic University, Hong Kong (China); Rong, Bo [Emperor Qin' s Terra-cotta Warriors and Horses Museum, Xi' an (China); An, Zhisheng [SKLLQG, Institute of Earth Environment, Chinese Academy of Sciences, Xi' an, 710075 (China)

    2009-10-01

    Daytime and nighttime total suspended particulate matters (TSP) were collected inside and outside Emperor Qin's Terra-cotta Museum, the most popular on-site museum in China, in winter 2008. The purpose of this study was to investigate the contribution of visitors to indoor airborne particles in two display halls with different architectural and ventilating conditions, including Exhibition Hall and Pit No.1. Morphological and elemental analyses of 7-day individual particle samples were performed with scanning electron microscopy and energy dispersive X-ray spectrometer (SEM-EDX). Particle mass concentrations in Exhibition Hall and Pit No.1 were in a range of 54.7-291.7 {mu}g m{sup -3} and 95.3-285.4 {mu}g m{sup -3} with maximum diameters of 17.5 {mu}m and 26.0 {mu}m, respectively. In most sampling days, daytime/nighttime particle mass ratios in Exhibition Hall (1.30-3.12) were higher than those in Pit No.1 (0.96-2.59), indicating more contribution of the tourist flow in Exhibition Hall than in Pit No. 1. The maximum of particle size distributions were in a range of 0.5-1.0 {mu}m, with the highest abundance (43.4%) occurred in Exhibition Hall at night. The majority of airborne particles at the Museum was composed of soil dust, S-containing particles, and low-Z particles like soot aggregate and biogenic particles. Both size distributions and particle types were found to be associated with visitor numbers in Exhibition Hall and with natural ventilation in Pit No.1. No significant influence of visitors on indoor temperature and relative humidity (RH) was found in either display halls. Those baseline data on the nature of the airborne particles inside the Museum can be incorporated into the maintenance criteria, display management, and ventilation strategy by conservators of the museum.

  20. The development of a spectrometer for 14 MeV neutrons from fusion

    International Nuclear Information System (INIS)

    Aronsson, D.

    1991-01-01

    A spectrometer for 14 MeV neutrons, to be used for fusion plasma diagnostics at JET, was developed. The spectrometer utilizes neutron scattering in a polyethylene foil with the detection of the scattered neutron and its associated recoil proton. For the detection of 12 MeV protons we have tested silicon surface barrier detectors, lithium-drifted silicon detectors and high purity germanium detectors. The lithium-drifted detectors were finally selected for use in the spectrometer. The lithium-drifted silicon diodes have also been used for direct spectrometry, utilizing the neutron induced charged particle reactions in silicon. The methods used for the energy calibration and the timing calibration of the diodes, both during the installation of the spectrometer and during operation, are described. The detection of 2 MeV neutrons is done by fast plastic scintillators. Since the neutron generator which was used to test the detectors supplies 14 MeV or 2.5 MeV neutrons only, a neutron energy converter has to be constructed to study the detectors at other neutron energies. In the actual spectrometer an array of scintillation neutron detectors is used. A method of calibrating such an array of detectors with a gamma source was elaborated and is also described here. The result of the calibration is a set of parameters than can be used to determine the high voltage settings and the discriminator levels that are needed to achieve homogeneous sensitivity for all the detectors of the array. The energy scale itself was then calibrated by using gamma sources of various energies. To test the spectrometer as a whole at a neutron generator, a test bed was constructed. A lithium-drifted silicon diode was used to measure the neutron flux and the neutron energy resolution in the test bed. (au)

  1. Data processing for elliptical crystal spectrometer used in Z-pinch diagnostic

    International Nuclear Information System (INIS)

    Li Jing; Xie Weiping; Huang Xianbin; Yang Libing; Cai Hongchun; Xiao Shali

    2010-01-01

    Elliptical crystal spectrometers are key instruments to detect the line spectra of soft X-rays in Z-pinch diagnostics. This paper deals with the data processing for an elliptical crystal spectrometer. Taking the diagnostic results obtained in a neon gas-puff Z-pinch experiment as an example, the detailed processes, such as changing the optical density to X-ray intensity according a calibrated film response curve, determining the X-ray energy of the measured spectrum using the energy and the order number of scanned point of identified spectral lines, and correcting the intensity of spectrum using the formula given by Henke are discussed. In the Henke's formula, the effect of nonuniform dispersion, integrated reflectivity of crystals and transmission of X-ray filters are considered. The final unfolding results are presented, including the relative intensities of several neon K-shell lines (H α , He α and He β , etc.) given by Lorentz fitting. The relative errors of the spectral intensities are also briefly discussed. (authors)

  2. Distribution Of Natural Radioactivity On Soil Size Particles

    International Nuclear Information System (INIS)

    Tran Van Luyen; Trinh Hoai Vinh; Thai Khac Dinh

    2008-01-01

    This report presents a distribution of natural radioactivity on different soil size particles, taken from one soil profile. On the results shows a range from 52% to 66% of natural radioisotopes such as 238 U, 232 Th, 226 Ra and 40 K concentrated on the soil particles below 40 micrometers in diameter size. The remained of natural radioisotopes were distributed on a soil particles with higher diameter size. The study is available for soil sample collected to natural radioactive analyze by gamma and alpha spectrometer methods. (author)

  3. Development of a ten inch manipulators-based, flexible, broadband two-crystal spectrometer

    International Nuclear Information System (INIS)

    Steel, A. B.; Dunn, J.; Emig, J.; Beiersdorfer, P.; Brown, G. V.; Shepherd, R.; Marley, E. V.; Hoarty, D. J.

    2014-01-01

    We have developed and implemented a broadband X-ray spectrometer with a variable energy range for use at the Atomic Weapons Establishment's Orion Laser. The spectrometer covers an energy bandwidth of ∼1–2 keV using two independently mounted, movable Bragg diffraction crystals. Using combinations of cesium hydrogen pthlate, ammonium dihydrogen phosphate, and pentaerythritol crystals, spectra covering the 1.4–2.5, 1.85–3.15, or 3.55–5.1 keV energy bands have been measured. Image plate is used for detection owing to its high dynamic range. Background signals caused by high energy X-rays and particles commonly produced in high energy laser experiments are reduced by a series of tantalum baffles and filters installed between the source and crystal and also between the crystals and detector

  4. The Alpha Magnetic Spectrometer Silicon Tracker

    CERN Document Server

    Burger, W J

    1999-01-01

    The Alpha Magnetic Spectrometer (AMS) is designed as a independent module for installation on the International Space Station Alpha (ISSA) in the year 2002 for an operational period of three years. The principal scientific objectives are the searches for antimatter and dark matter in cosmic rays. The AMS uses 5.5 m sup 2 of silicon microstrip sensors to reconstruct charged particle trajectories in the field of a permanent magnet. The detector design and construction covered a 3 yr period which terminated with a test flight on the NASA space shuttle Discovery during June 2-12, 1988. In this contribution, we describe the shuttle version of the AMS silicon tracker, including preliminary results of the tracker performance during the flight. (author)

  5. Primary studies on particle recovery of swipe samples for nuclear safeguards

    International Nuclear Information System (INIS)

    Fan Wang; Yan Chen; Yong-gang Zhao; Yan Zhang; Tong-xing Wang; Jing-huai Li; Zhi-yuan Chang; Hai-ping Cui

    2013-01-01

    Environmental sampling plays a significant role in nuclear safeguards. Isotopic ratio in uranium-bearing particles from swipe samples provides important information for detecting undeclared activities. Particle recovery which is the primary step of particle analysis, would affect the following analysis. The particle recovery efficiency of ultrasoneration recovery and vacuum suction-impact recovery were measured by alpha spectrometer with standard particles produced via aerosol spray pyrolysis method. The conditions of ultrasoneration were optimized and both recovery methods were evaluated. Finally, a procedure of particle recovery for unknown swipe samples was set up. (author)

  6. Modification, calibration, and performance of the Ultra-High Sensitivity Aerosol Spectrometer for particle size distribution and volatility measurements during the Atmospheric Tomography Mission (ATom) airborne campaign

    Science.gov (United States)

    Kupc, Agnieszka; Williamson, Christina; Wagner, Nicholas L.; Richardson, Mathews; Brock, Charles A.

    2018-01-01

    Atmospheric aerosol is a key component of the chemistry and climate of the Earth's atmosphere. Accurate measurement of the concentration of atmospheric particles as a function of their size is fundamental to investigations of particle microphysics, optical characteristics, and chemical processes. We describe the modification, calibration, and performance of two commercially available, Ultra-High Sensitivity Aerosol Spectrometers (UHSASs) as used on the NASA DC-8 aircraft during the Atmospheric Tomography Mission (ATom). To avoid sample flow issues related to pressure variations during aircraft altitude changes, we installed a laminar flow meter on each instrument to measure sample flow directly at the inlet as well as flow controllers to maintain constant volumetric sheath flows. In addition, we added a compact thermodenuder operating at 300 °C to the inlet line of one of the instruments. With these modifications, the instruments are capable of making accurate (ranging from 7 % for Dp 0.13 µm), precise ( 1000 to 225 hPa, while simultaneously providing information on particle volatility.We assessed the effect of uncertainty in the refractive index (n) of ambient particles that are sized by the UHSAS assuming the refractive index of ammonium sulfate (n = 1.52). For calibration particles with n between 1.44 and 1.58, the UHSAS diameter varies by +4/-10 % relative to ammonium sulfate. This diameter uncertainty associated with the range of refractive indices (i.e., particle composition) translates to aerosol surface area and volume uncertainties of +8.4/-17.8 and +12.4/-27.5 %, respectively. In addition to sizing uncertainty, low counting statistics can lead to uncertainties of 1000 cm-3.Examples of thermodenuded and non-thermodenuded aerosol number and volume size distributions as well as propagated uncertainties are shown for several cases encountered during the ATom project. Uncertainties in particle number concentration were limited by counting statistics

  7. Digital positron annihilation spectrometer

    International Nuclear Information System (INIS)

    Cheng Bin; Weng Huimin; Han Rongdian; Ye Bangjiao

    2010-01-01

    With the high speed development of digital signal process, the technique of the digitization and processing of signals was applied in the domain of a broad class of nuclear technique. The development of digital positron lifetime spectrometer (DPLS) is more promising than the conventional positron lifetime spectrometer equipped with nuclear instrument modules. And digital lifetime spectrometer has many advantages, such as low noise, long term stability, flexible online or offline digital processing, simple setup, low expense, easy to setting, and more physical information. Digital constant fraction discrimination is for timing. And a new method of optimizing energy windows setting for digital positron lifetime spectrometer is also developed employing the simulated annealing for the convenient use. The time resolution is 220ps and the count rate is 200cps. (authors)

  8. Spectra of the linear energy transfer measured with a track etch spectrometer in the beam of 1 GeV protons and the contribution of secondary charged particles to the dose

    International Nuclear Information System (INIS)

    Spurny, F.; Vlcek, B.; Bamblevskij, V.P.; Timoshenko, G.N.

    1999-01-01

    A spectrometer of the linear energy transfer (LET) on the base of CR-39 detector was used to establish the spectra of LET in the beam of protons with the primary energy of 1 GeV. It was found out that the LET spectra of secondary charged particles between 100 and 7000 MeV cm 2 g -1 do not depend on the radiator. The average quality factors for the LET region mentioned were obtained about 11.6 with ICRP 26 quality factors and about 14.0 with ICRP 60 quality factors. The spectra obtained permitted to calculate the contributions of these secondary charged particles to the dosimetric quantities. It was observed that these contributions were about 7.0% for the total absorbed dose of protons and close 90% in the case of the equivalent doses. It is more than it was found out for few hundred MeV protons

  9. The Ulysses fast latitude scans: COSPIN/KET results

    Directory of Open Access Journals (Sweden)

    B. Heber

    2003-06-01

    Full Text Available Ulysses, launched in October 1990, began its second out-of-ecliptic orbit in December 1997, and its second fast latitude scan in September 2000. In contrast to the first fast latitude scan in 1994/1995, during the second fast latitude scan solar activity was close to maximum. The solar magnetic field reversed its polarity around July 2000. While the first latitude scan mainly gave a snapshot of the spatial distribution of galactic cosmic rays, the second one is dominated by temporal variations. Solar particle increases are observed at all heliographic latitudes, including events that produce >250 MeV protons and 50 MeV electrons. Using observations from the University of Chicago’s instrument on board IMP8 at Earth, we find that most solar particle events are observed at both high and low latitudes, indicating either acceleration of these particles over a broad latitude range or an efficient latitudinal transport. The latter is supported by "quiet time" variations in the MeV electron background, if interpreted as Jovian electrons. No latitudinal gradient was found for >106 MeV galactic cosmic ray protons, during the solar maximum fast latitude scan. The electron to proton ratio remains constant and has practically the same value as in the previous solar maximum. Both results indicate that drift is of minor importance. It was expected that, with the reversal of the solar magnetic field and in the declining phase of the solar cycle, this ratio should increase. This was, however, not observed, probably because the transition to the new magnetic cycle was not completely terminated within the heliosphere, as indicated by the Ulysses magnetic field and solar wind measurements. We argue that the new A<0-solar magnetic modulation epoch will establish itself once both polar coronal holes have developed.Key words. Interplanetary physics (cosmic rays; energetic particles; interplanetary magnetic fields

  10. Scanning holograms

    International Nuclear Information System (INIS)

    Natali, S.

    1984-01-01

    This chapter reports on the scanning of 1000 holograms taken in HOBC at CERN. Each hologram is triggered by an interaction in the chamber, the primary particles being pions at 340 GeV/c. The aim of the experiment is the study of charm production. The holograms, recorded on 50 mm film with the ''in line'' technique, can be analyzed by shining a parallel expanded laser beam through the film, obtaining immediately above it the real image of the chamber which can then be scanned and measured with a technique half way between emulsions and bubble chambers. The results indicate that holograms can be analyzed as quickly and reliably as in other visual techniques and that to them is open the same order of magnitude of large scale experiments

  11. Ion chemistry and individual particle analysis of atmospheric aerosols over Mt. Bogda of eastern Tianshan Mountains, Central Asia.

    Science.gov (United States)

    Zhao, Shuhui; Li, Zhongqin; Zhou, Ping

    2011-09-01

    Aerosol samples were collected during the scientific expedition to Mt. Bogda in July-August, 2009. The major inorganic ions (Na( + ), NH⁺₄, K( + ), Mg(2 + ), Ca(2 + ), Cl( - ), SO²⁻₄, and NO⁻₃) of the aerosols were determined by ion chromatography. SO²⁻₄, NO⁻₃, and Ca(2 + ) were the dominate ions, with the mean concentrations of 0.86, 0.56, and 0.28 μg m⁻³, respectively. These mean ion concentrations were generally comparable with the background conditions in remote site of Xinjiang, while much lower than those in Ürümqi. Morphology and elemental compositions of 1,500 particles were determined by field emission scanning electron microscopy equipped with an energy dispersive X-ray spectrometer. Based on the morphology and elemental compositions, particles were classed into four major groups: soot (15.1%), fly ash (4.7%), mineral particles (78.9%), and little other matters (0.8% Fe-rich particles and 0.5% unrecognized particles). Presence of soot and fly ash particles indicated the influence of anthropogenic pollutions, while abundance mineral particles suggested that natural processes were the primary source of aerosols over this region, coinciding with the ionic analysis. Backward air mass trajectory analysis suggested that Ürümqi may contribute some anthropogenic pollution to this region, while the arid and semi-arid regions of Central Asia were the primary source.

  12. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions.

    Science.gov (United States)

    Arndt, J; Deboudt, K; Anderson, A; Blondel, A; Eliet, S; Flament, P; Fourmentin, M; Healy, R M; Savary, V; Setyan, A; Wenger, J C

    2016-03-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe-Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. Copyright © 2015 Elsevier Ltd. All rights reserved.

  13. Continuous scanning of the mobility and size distribution of charged clusters and nanometer particles in atmospheric air and the Balanced Scanning Mobility Analyzer BSMA

    Science.gov (United States)

    Tammet, H.

    2006-12-01

    Measuring of charged nanometer particles in atmospheric air is a routine task in research on atmospheric electricity, where these particles are called the atmospheric ions. An aspiration condenser is the most popular instrument for measuring atmospheric ions. Continuous scanning of a mobility distribution is possible when the aspiration condenser is connected as an arm of a balanced bridge. Transfer function of an aspiration condenser is calculated according to the measurements of geometric dimensions, air flow rate, driving voltage, and electric current. The most complicated phase of the calibration is the estimation of the inlet loss of ions due to the Brownian deposition. The available models of ion deposition on the protective inlet screen and the inlet control electrofilter have the uncertainty of about 20%. To keep the uncertainty of measurements low the adsorption should not exceed a few tens of percent. The online conversion of the mobility distribution to the size distribution and a correct reduction of inlet losses are possible when air temperature and pressure are measured simultaneously with the mobility distribution. Two instruments called the Balanced Scanning Mobility Analyzers (BSMA) were manufactured and tested in routine atmospheric measurements. The concentration of atmospheric ions of the size of about a few nanometers is very low and a high air flow rate is required to collect enough of ion current. The air flow of 52 l/s exceeds the air flow in usual aerosol instruments by 2-3 orders of magnitude. The high flow rate reduces the time of ion passage to 60 ms and the heating of air in an analyzer to 0.2 K, which suppresses a possible transformation of ions inside the instrument. The mobility range of the BSMA of 0.032-3.2 cm 2 V - 1 s - 1 is logarithmically uniformly divided into 16 fractions. The size distribution is presented by 12 fractions in the diameter range of 0.4-7.5 nm. The measurement noise of a fraction concentration is typically

  14. Data processing for the Active Particle-induced X-ray Spectrometer and initial scientific results from Chang'e-3 mission

    Science.gov (United States)

    Fu, Xiao-Hui; Li, Chun-Lai; Zhang, Guang-Liang; Zou, Yong-Liao; Liu, Jian-Jun; Ren, Xin; Tan, Xu; Zhang, Xiao-Xia; Zuo, Wei; Wen, Wei-Bin; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Wang, Huan-Yu

    2014-12-01

    The Active Particle-induced X-ray Spectrometer (APXS) is an important payload mounted on the Yutu rover, which is part of the Chang'e-3 mission. The scientific objective of APXS is to perform in-situ analysis of the chemical composition of lunar soil and rock samples. The radioactive sources, 55Fe and 109Cd, decay and produce α-particles and X-rays. When X-rays and α-particles interact with atoms in the surface material, they knock electrons out of their orbits, which release energy by emitting X-rays that can be measured by a silicon drift detector (SDD). The elements and their concentrations can be determined by analyzing their peak energies and intensities. APXS has analyzed both the calibration target and lunar soil once during the first lunar day and again during the second lunar day. The total detection time lasted about 266 min and more than 2000 frames of data records have been acquired. APXS has three operating modes: calibration mode, distance sensing mode and detection mode. In detection mode, work distance can be calculated from the X-ray counting rate collected by SDD. Correction for the effect of temperature has been performed to convert the channel number for each spectrum to X-ray energy. Dead time correction is used to eliminate the systematic error in quantifying the activity of an X-ray pulse in a sample and derive the real count rate. We report APXS data and initial results during the first and second lunar days for the Yutu rover. In this study, we analyze the data from the calibration target and lunar soil on the first lunar day. Seven major elements, including Mg, Al, Si, K, Ca, Ti and Fe, have been identified. Comparing the peak areas and ratios of calibration basalt and lunar soil the landing site was found to be depleted in K, and have lower Mg and Al but higher Ca, Ti, and Fe. In the future, we will obtain the elemental concentrations of lunar soil at the Chang'e-3 landing site using APXS data.

  15. Automation of an X-ray photoelectron spectrometer

    International Nuclear Information System (INIS)

    Ashury, M.R.

    2003-02-01

    The Institute of Solid State Physics of the Vienna University of Technology is established with an X-ray Photoelectron Spectrometer Kratos XSAM 800. In its original state the instrument enables measurements of photoelectron spectra in a semiautomatical mode. After mounting of the specimen an eventual surface cleaning by argon ion sputtering is possible. Next steps are setting of x-ray tube high voltage and current, start energy and energy range of spectrum and time of measurement. Data are obtained by an x-t plotter and evaluations are performed from the registration charts. If necessary, measured spectra have to be digitized by means of a scanner. In the Introduction of this thesis the principle of X-ray photoelectron spectrometry is treated including a number of practical examples. It shows that an automation allows an extension of the performance of the instrument. Details are remote controlled experiments, wider energy ranges with improved energy resolution. Furthermore, the digitized data treatment enables background subtration, determination of line positions and integrated signal strengths, and is the detection of lowlevel of lines (the peak with lowamplitude) possible. A further advantage is the computer assisted documentation and comparison of results from different specimens. After this description of the essential requirements different possible solutions of an automation are discussed. Thus, it is decided to develop a completely new hardware for a perfect control of the spectrometer. A further decision is to be made on the most efficient kind of micro processor. From the considerations follows a completely new control board with a transputer as multi tasking processor. The complete control unit consists of a digital system, an analog system and a power unit. The digital system controls settings and spectra accumulation and includes the transputer board, the pc-link card, the i/o-card and the step scanning control board. The analog system controls the

  16. Scanning tomographic particle image velocimetry applied to a turbulent jet

    KAUST Repository

    Casey, T. A.; Sakakibara, J.; Thoroddsen, Sigurdur T

    2013-01-01

    planes in the depth direction by maintaining optimal particle image density and limiting the number of ghost particles. The total measurement volumes contain between 1 ×106 and 3 ×106 velocity vectors calculated from up to 1500 reconstructed depthwise

  17. Characterization of a time-of-flight mass spectrometer and its applications in the study of solid surfaces; Charakterisierung eines Flugzeitmassenspektrometers und seine Anwendungen in der Festkoerperoberflaechenuntersuchung

    Energy Technology Data Exchange (ETDEWEB)

    Mazarov, P.

    2006-12-21

    The object and the purpose of the present work was to develop, to assemble and to start running a new TOF (time of flight) mass spectrometer for imaging SNMS analytic which is optimized for the analysis of highly molecular secondary ions. The most important purpose was the characterization of the TOF mass spectrometer. The obtained mass spectra of indium, tantalum and silver clusters reflect the excellent properties of the TOF mass spectrometer for the detection of large clusters with good detection efficiency up to masses of 16000 amu. The possibility of the deflection of selected saturated atom and cluster peaks serves for further improvement of the detection efficiency for large molecules. The accessible mass resolution was determined to be of the order of m/{delta}m=1000 in the high mass region. Numerous measurements were carried out to characterize the useful yield of this spectrometer. For a best possible adaptation of the TOF mass spectrometer for the detection of highly molecular particles, a device for post-acceleration of the detected particles by up to 10 keV were inserted directly before the MCP detector. The detection efficiency of positive secondary ions was determined for different post-acceleration voltages for the example of sputtered indium cluster ions. In addition, a new method was developed for the quantitative determination of the spectral ionization probability {alpha}{sup +}({nu}) of sputtered particles as a function of the emission velocity. The next application of the TOF mass spectrometer is the analysis of complicated organic molecules in solid state surfaces. During measurements of the photo-ionization behaviour of neutral tryptophan molecules, it was found out that a stable molecular ion signal is generated in the SNMS spectrum with h{nu}=7.9 eV can only be observed by the use of a continuous ion beam or very long (ms range) ion pulses. (orig.)

  18. Simulation of the SAGE spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Cox, D.M.; Herzberg, R.D. [University of Liverpool, Department of Physics, Oliver Lodge Laboratory, Liverpool (United Kingdom); Konki, J.; Greenlees, P.T.; Pakarinen, J.; Papadakis, P.; Rahkila, P.; Sandzelius, M.; Sorri, J. [University of Jyvaeskylae, Department of Physics, Jyvaeskylae (Finland); Hauschild, K. [Universite Paris-Sud, CSNSM-IN2P3-CNRS, Orsay (France)

    2015-06-15

    The SAGE spectrometer combines a Ge-detector array with a Si detector to allow simultaneous detection of γ-rays and electrons. A comprehensive GEANT4 simulation package of the SAGE spectrometer has been developed with the ability to simulate the expected datasets based on user input files. The measured performance of the spectrometer is compared to the results obtained from the simulations. (orig.)

  19. Simulation of the SAGE spectrometer

    International Nuclear Information System (INIS)

    Cox, D.M.; Herzberg, R.D.; Konki, J.; Greenlees, P.T.; Pakarinen, J.; Papadakis, P.; Rahkila, P.; Sandzelius, M.; Sorri, J.; Hauschild, K.

    2015-01-01

    The SAGE spectrometer combines a Ge-detector array with a Si detector to allow simultaneous detection of γ-rays and electrons. A comprehensive GEANT4 simulation package of the SAGE spectrometer has been developed with the ability to simulate the expected datasets based on user input files. The measured performance of the spectrometer is compared to the results obtained from the simulations. (orig.)

  20. Isotope, scanning electron microscope, and energy dispersive spectrometer studies of heterogeneous zircons from radioactive granites in the Grenville structural province, Quebec and Ontario

    International Nuclear Information System (INIS)

    Rimsaite, J.

    1981-01-01

    Heterogeneous zircons yielded discordant Pb-U, Pb-Th, and 207 Pb- 206 Pb isotopic ages. Most data points fall below the concordia curve, implying losses of daughter elements, bqt they define a discordia line that intersects the concordia at approximately 90 Ma and 1020 Ma. To obtain evidence for mobilization of U and radiogenic Pb, zircon grains were studied using a scanning electron microscope coupled with an energy dispersive spectrometer. High magnification backscattered and secondary electron images of the zircon revealed narrow fractures, zoning and diverse mineral inclusions. Three groups of mineral inclusions observed were: 1) those predating zoned zircon and apparently serving as a nucleus; 2) uraninite, feldspar, and apatite associated with the growth and zoning of the host zircon; and 3) fracture-fillings that postdate crystallization of the host zircon. The U- and Pb-rich inclusions incorporated into the zircon grains during and after its crystallization markedly affect isotopic ages of the host zircon. Migration of Pb and U have occurred along fractures in zircon. Zircon, uraninite, and other associated minerals have decomposed and complex reactions have taken place between the liberated Zr, U, Th and other elements to produce overgrowths on mineral grains and unidentified Zr-bearing material in fractures

  1. Multifrequency scanning probe microscopy study of nanodiamond agglomerates

    Science.gov (United States)

    Aravind, Vasudeva; Lippold, Stephen; Li, Qian; Strelcov, Evgheny; Okatan, Baris; Legum, Benjamin; Kalinin, Sergei; Clarion University Team; Oak Ridge National Laboratory Team

    Due to their rich surface chemistry and excellent mechanical properties and non-toxic nature, nanodiamond particles have found applications such as biomedicine, tribology and lubrication, targeted drug delivery systems, tissue scaffolds and surgical implants. Although single nanodiamond particles have diameters about 4-5nm, they tend to form agglomerates. While these agglomerates can be useful for some purposes, many applications of nanodiamonds require single particle, disaggregated nanodiamonds. This work is oriented towards studying forces and interactions that contribute to agglomeration in nanodiamonds. In this work, using multifrequency scanning probe microscopy techniques, we show that agglomerate sizes can vary between 50-100nm in raw nanodiamonds. Extremeties of particles and Interfaces between agglomerates show dissipative forces with scanning probe microscope tip, indicating agglomerates could act as points of increased adhesion, thus reducing lubricating efficiency when nanodiamonds are used as lubricant additives. This research was conducted at the Center for Nanophase Materials Sciences, which is a DOE Office of Science User Facility.

  2. Development of a ten inch manipulators-based, flexible, broadband two-crystal spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Steel, A. B., E-mail: steel1@llnl.gov; Dunn, J.; Emig, J.; Beiersdorfer, P.; Brown, G. V.; Shepherd, R.; Marley, E. V. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Hoarty, D. J. [Atomic Weapons Establishment, Aldermaston (United Kingdom)

    2014-11-15

    We have developed and implemented a broadband X-ray spectrometer with a variable energy range for use at the Atomic Weapons Establishment's Orion Laser. The spectrometer covers an energy bandwidth of ∼1–2 keV using two independently mounted, movable Bragg diffraction crystals. Using combinations of cesium hydrogen pthlate, ammonium dihydrogen phosphate, and pentaerythritol crystals, spectra covering the 1.4–2.5, 1.85–3.15, or 3.55–5.1 keV energy bands have been measured. Image plate is used for detection owing to its high dynamic range. Background signals caused by high energy X-rays and particles commonly produced in high energy laser experiments are reduced by a series of tantalum baffles and filters installed between the source and crystal and also between the crystals and detector.

  3. Particle mass yield in secondary organic aerosol formed by the dark ozonolysis of α-pinene

    Directory of Open Access Journals (Sweden)

    J. E. Shilling

    2008-04-01

    Full Text Available The yield of particle mass in secondary organic aerosol (SOA formed by dark ozonolysis was measured for 0.3–22.8 ppbv of reacted α-pinene. Most experiments were conducted using a continuous-flow chamber, allowing nearly constant SOA concentration and chemical composition for several days. For comparison, some experiments were also conducted in batch mode. Reaction conditions were 25°C, 40% RH, dry (NH4SO4 seed particles, and excess 1-butanol. The organic particle loading was independently measured by an aerosol mass spectrometer and a scanning mobility particle sizer, and the two measurements agreed well. The observations showed that SOA formation occurred for even the lowest reacted α-pinene concentration of 0.3 ppbv. The particle mass yield was 0.09 at 0.15 μg m−3, increasing to 0.27 at 40 μg m−3. Compared to some results reported in the literature, the yields were 80 to 100% larger for loadings above 2 μg m−3. At lower loadings, the yields had an offset of approximately +0.07 from those reported in the literature. To as low as 0.15 μm−3, the yield curve had no inflection point toward null yield, implying the formation of one or several products having vapor pressures below this value. These observations of increased yields, especially for low loadings, are potentially important for accurate prediction by chemical transport models of organic particle concentrations in the ambient atmosphere.

  4. Laboratory verification of the Active Particle-induced X-ray Spectrometer (APXS) on the Chang'e-3 mission

    International Nuclear Information System (INIS)

    Zhang, Guang-Liang; Li, Chun-Lai; Fu, Xiao-Hui; Zhang, Li-Yan; Ban, Cao; Li, Han; Zou, Yong-Liao; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Wang, Huan-Yu

    2015-01-01

    In the Chang'e-3 mission, the Active Particle-induced X-ray Spectrometer (APXS) on the Yutu rover is used to analyze the chemical composition of lunar soil and rock samples. APXS data are only valid are only if the sensor head gets close to the target and integration time lasts long enough. Therefore, working distance and integration time are the dominant factors that affect APXS results. This study confirms the ability of APXS to detect elements and investigates the effects of distance and time on the measurements. We make use of a backup APXS instrument to determine the chemical composition of both powder and bulk samples under the conditions of different working distances and integration times. The results indicate that APXS can detect seven major elements, including Mg, Al, Si, K, Ca, Ti and Fe under the condition that the working distance is less than 30 mm and having an integration time of 30 min. The statistical deviation is smaller than 15%. This demonstrates the instrument's ability to detect major elements in the sample. Our measurements also indicate the increase of integration time could reduce the measurement error of peak area, which is useful for detecting the elements Mg, Al and Si. However, an increase in working distance can result in larger errors in measurement, which significantly affects the detection of the element Mg. (paper)

  5. Charge state mapping of mixed valent iron and manganese mineral particles using Scanning Transmission X-ray Microscopy (STXM)

    International Nuclear Information System (INIS)

    Pecher, K.; Nealson, K.; Kneedler, E.; Rothe, J.; Meigs, G.; Warwick, T.; Tonner, B.

    2000-01-01

    The interfaces between solid mineral particles and water play a crucial role in partitioning and chemical transformation of many inorganic as well as organic pollutants in environmental systems. Among environmentally significant minerals, mixed-valent oxides and hydroxides of iron (e.g. magnetite, green rusts) and manganese (hausmanite, birnessite) have been recognized as particularly strong sorbents for metal ions. In addition, minerals containing Fe(II) have recently been proven to be powerful reductants for a wide range of pollutants. Chemical properties of these minerals strongly depend on the distribution and availability of reactive sites and little is known quantitatively about the nature of these sites. We have investigated the bulk distribution of charge states of manganese (Mn (II, III, IV)) and iron (Fe(II, III)) in single particles of natural manganese nodules and synthetic green rusts using Scanning Transmission X-ray SpectroMicroscopy (STXM). Pixel resolved spectra (XANES) extracted from stacks of images taken at different wave lengths across the metal absorption edge were fitted to total electron yield (TEY) spectra of single valent reference compounds. Two dimensional maps of bulk charge state distributions clearly reveal domains of different oxidation states within single particles of Mn-nodules and green rust precipitates. Changes of oxidation states of iron were followed as a result of reductive transformation of an environmental contaminant (CCl 4 ) using green rust as the only reductant

  6. Mass spectrometer calibration of Cosmic Dust Analyzer

    Science.gov (United States)

    Ahrens, Thomas J.; Gupta, Satish C.; Jyoti, G.; Beauchamp, J. L.

    2003-02-01

    The time-of-flight (TOF) mass spectrometer (MS) of the Cosmic Dust Analyzer (CDA) instrument aboard the Cassini spacecraft is expected to be placed in orbit about Saturn to sample submicrometer-diameter ring particles and impact ejecta from Saturn's satellites. The CDA measures a mass spectrum of each particle that impacts the chemical analyzer sector of the instrument. Particles impact a Rh target plate at velocities of 1-100 km/s and produce some 10-8 to 10-5 times the particle mass of positive valence, single-charged ions. These are analyzed via a TOF MS. Initial tests employed a pulsed N2 laser acting on samples of kamacite, pyrrhotite, serpentine, olivine, and Murchison meteorite induced bursts of ions which were detected with a microchannel plate and a charge sensitive amplifier (CSA). Pulses from the N2 laser (1011 W/cm2) are assumed to simulate particle impact. Using aluminum alloy as a test sample, each pulse produces a charge of ~4.6 pC (mostly Al+1), whereas irradiation of a stainless steel target produces a ~2.8 pC (Fe+1) charge. Thus the present system yields ~10-5% of the laser energy in resulting ions. A CSA signal indicates that at the position of the microchannel plate, the ion detector geometry is such that some 5% of the laser-induced ions are collected in the CDA geometry. Employing a multichannel plate detector in this MS yields for Al-Mg-Cu alloy and kamacite targets well-defined peaks at 24 (Mg+1), 27(Al+1), and 64 (Cu+1) and 56 (Fe+1), 58 (Ni+1), and 60 (Ni+1) dalton, respectively.

  7. The MEG positron spectrometer

    International Nuclear Information System (INIS)

    Nishiguchi, Hajime

    2007-01-01

    We have been developing an innovative spectrometer for the MEG experiment at the Paul Scherrer Institute (PSI) in Switzerland. This experiment searches for a lepton flavour violating decay μ + →e + γ with a sensitivity of 10 -13 in order to explore the region predicted by supersymmetric extensions of the standard model. The MEG positron spectrometer consists of a specially designed superconducting solenoidal magnet with a highly graded field, an ultimate low-mass drift chamber system, and a precise time measuring counter system. This innovative positron spectrometer is described here focusing on the drift chamber system

  8. VEGAS: VErsatile GBT Astronomical Spectrometer

    Science.gov (United States)

    Bussa, Srikanth; VEGAS Development Team

    2012-01-01

    The National Science Foundation Advanced Technologies and Instrumentation (NSF-ATI) program is funding a new spectrometer backend for the Green Bank Telescope (GBT). This spectrometer is being built by the CICADA collaboration - collaboration between the National Radio Astronomy Observatory (NRAO) and the Center for Astronomy Signal Processing and Electronics Research (CASPER) at the University of California Berkeley.The backend is named as VErsatile GBT Astronomical Spectrometer (VEGAS) and will replace the capabilities of the existing spectrometers. This backend supports data processing from focal plane array systems. The spectrometer will be capable of processing up to 1.25 GHz bandwidth from 8 dual polarized beams or a bandwidth up to 10 GHz from a dual polarized beam.The spectrometer will be using 8-bit analog to digital converters (ADC), which gives a better dynamic range than existing GBT spectrometers. There will be 8 tunable digital sub-bands within the 1.25 GHz bandwidth, which will enhance the capability of simultaneous observation of multiple spectral transitions. The maximum spectral dump rate to disk will be about 0.5 msec. The vastly enhanced backend capabilities will support several science projects with the GBT. The projects include mapping temperature and density structure of molecular clouds; searches for organic molecules in the interstellar medium; determination of the fundamental constants of our evolving Universe; red-shifted spectral features from galaxies across cosmic time and survey for pulsars in the extreme gravitational environment of the Galactic Center.

  9. Electrostatic systems used for the multipassage magnetic mass spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Berger, C; Baril, M

    1987-08-15

    Improvement in the power of resolution is desirable in the multiplication of passages in magnetic fields; our guiding principle is to carry out the operation using a single magnetic prism. In the multipassage process the ions must first turn back after leaving the prism. This turnback is obtained by an electrostatic mirror. We obtain a large enough number of passages by placing two mirrors and two systems with time-varying roles at right angles. These systems are referred to as lens-mirror 1. When they act as mirrors, they enable the particles to circulate in a closed circuit; when they act as lenses, they enable the particles to enter the circuit or leave it. The coupling of two multipassage spectrometers is momentarily possible thanks to lens-mirror 2. The function change results from a change in electrode potential. The requirements for these electrostatic systems and their construction are studied.

  10. Identified particles in Au+Au collisions at S=200 GeV

    Science.gov (United States)

    Phobos Collaboration; Wosiek, Barbara; Back, B. B.; Baker, M. D.; Barton, D. S.; Betts, R. R.; Ballintijn, M.; Bickley, A. A.; Bindel, R.; Budzanowski, A.; Busza, W.; Carroll, A.; Decowski, M. P.; García, E.; George, N.; Gulbrandsen, K.; Gushue, S.; Halliwell, C.; Hamblen, J.; Heintzelman, G. A.; Henderson, C.; Hofman, D. J.; Hollis, R. S.; Hołyński, R.; Holzman, B.; Iordanova, A.; Johnson, E.; Kane, J. L.; Katzy, J.; Khan, N.; Kucewicz, W.; Kulinich, P.; Kuo, C. M.; Manly, S.; McLeod, D.; Michałowski, J.; Mignerey, A. C.; Nouicer, R.; Olszewski, A.; Pak, R.; Park, I. C.; Pernegger, H.; Reed, C.; Remsberg, L. P.; Reuter, M.; Roland, C.; Roland, G.; Rosenberg, L.; Sagerer, J.; Sarin, P.; Sawicki, P.; Skulski, W.; Steadman, S. G.; Steinberg, P.; Stephans, G. S. F.; Stodulski, M.; Sukhanov, A.; Tang, J.-L.; Teng, R.; Trzupek, A.; Vale, C.; van Nieuwenhuizen, G. J.; Verdier, R.; Wadsworth, B.; Wolfs, F. L. H.; Wosiek, B.; Woźniak, K.; Wuosmaa, A. H.; Wysłouch, B.

    2003-03-01

    The yields of identified particles have been measured at RHIC for Au+Au collisions at S=200 GeV using the PHOBOS spectrometer. The ratios of antiparticle to particle yields near mid-rapidity are presented. The first measurements of the invariant yields of charged pions, kaons and protons at very low transverse momenta are also shown.

  11. Double difference method in deep inelastic neutron scattering on the VESUVIO spectrometer

    International Nuclear Information System (INIS)

    Andreani, C.; Colognesi, D.; Degiorgi, E.; Filabozzi, A.; Nardone, M.; Pace, E.; Pietropaolo, A.; Senesi, R.

    2003-01-01

    The principles of the Double Difference (DD) method, applied to the neutron spectrometer VESUVIO, are discussed. VESUVIO, an inverse geometry spectrometer operating at the ISIS pulsed neutron source in the eV energy region, has been specifically designed to measure the single particle dynamical properties in condensed matter. The width of the nuclear resonance of the absorbing filter, used for the neutron energy analysis, provides the most important contribution to the energy resolution of the inverse geometry instruments. In this paper, the DD method, which is based on a linear combination of two measurements recorded with filter foils of the same resonance material but of different thickness, is shown to improve significantly the instrumental energy resolution, as compared with the Single Difference (SD) method. The asymptotic response functions, derived through Monte-Carlo simulations for polycrystalline Pb and ZrH 2 samples, are analysed in both DD and SD methods, and compared with the experimental ones for Pb sample. The response functions have been modelled for two distinct experimental configurations of the VESUVIO spectrometer, employing 6 Li-glass neutron detectors and NaI γ detectors revealing the γ-ray cascade from the (n,γ) reaction, respectively. The DD method appears to be an effective experimental procedure for Deep Inelastic Neutron Scattering measurements on VESUVIO spectrometer, since it reduces the experimental resolution of the instrument in both 6 Li-glass neutron detector and γ detector configurations

  12. Double difference method in deep inelastic neutron scattering on the VESUVIO spectrometer

    Science.gov (United States)

    Andreani, C.; Colognesi, D.; Degiorgi, E.; Filabozzi, A.; Nardone, M.; Pace, E.; Pietropaolo, A.; Senesi, R.

    2003-02-01

    The principles of the Double Difference (DD) method, applied to the neutron spectrometer VESUVIO, are discussed. VESUVIO, an inverse geometry spectrometer operating at the ISIS pulsed neutron source in the eV energy region, has been specifically designed to measure the single particle dynamical properties in condensed matter. The width of the nuclear resonance of the absorbing filter, used for the neutron energy analysis, provides the most important contribution to the energy resolution of the inverse geometry instruments. In this paper, the DD method, which is based on a linear combination of two measurements recorded with filter foils of the same resonance material but of different thickness, is shown to improve significantly the instrumental energy resolution, as compared with the Single Difference (SD) method. The asymptotic response functions, derived through Monte-Carlo simulations for polycrystalline Pb and ZrH 2 samples, are analysed in both DD and SD methods, and compared with the experimental ones for Pb sample. The response functions have been modelled for two distinct experimental configurations of the VESUVIO spectrometer, employing 6Li-glass neutron detectors and NaI γ detectors revealing the γ-ray cascade from the ( n,γ) reaction, respectively. The DD method appears to be an effective experimental procedure for Deep Inelastic Neutron Scattering measurements on VESUVIO spectrometer, since it reduces the experimental resolution of the instrument in both 6Li-glass neutron detector and γ detector configurations.

  13. Double difference method in deep inelastic neutron scattering on the VESUVIO spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Andreani, C.; Colognesi, D.; Degiorgi, E.; Filabozzi, A.; Nardone, M.; Pace, E.; Pietropaolo, A. E-mail: antonino.pietropaolo@roma2.infn.it; Senesi, R

    2003-02-01

    The principles of the Double Difference (DD) method, applied to the neutron spectrometer VESUVIO, are discussed. VESUVIO, an inverse geometry spectrometer operating at the ISIS pulsed neutron source in the eV energy region, has been specifically designed to measure the single particle dynamical properties in condensed matter. The width of the nuclear resonance of the absorbing filter, used for the neutron energy analysis, provides the most important contribution to the energy resolution of the inverse geometry instruments. In this paper, the DD method, which is based on a linear combination of two measurements recorded with filter foils of the same resonance material but of different thickness, is shown to improve significantly the instrumental energy resolution, as compared with the Single Difference (SD) method. The asymptotic response functions, derived through Monte-Carlo simulations for polycrystalline Pb and ZrH{sub 2} samples, are analysed in both DD and SD methods, and compared with the experimental ones for Pb sample. The response functions have been modelled for two distinct experimental configurations of the VESUVIO spectrometer, employing {sup 6}Li-glass neutron detectors and NaI {gamma} detectors revealing the {gamma}-ray cascade from the (n,{gamma}) reaction, respectively. The DD method appears to be an effective experimental procedure for Deep Inelastic Neutron Scattering measurements on VESUVIO spectrometer, since it reduces the experimental resolution of the instrument in both {sup 6}Li-glass neutron detector and {gamma} detector configurations.

  14. Annual report 1977, Particle physics, Institute of Physics, University of Stockholm

    International Nuclear Information System (INIS)

    1978-01-01

    The research in the field of elementary particle physics concerns hadronic processes at high energies, using the facilities offered by CERN and Fermilab, USA. The teams carrying out experiments with bubble chambers are mainly working at the institute, whereas the tems utilizing counter techniques spend long periods at CERN. Experiments at CERN SPS and Fermilab are in progress. The equipment for bubble chamber physics at the institute consists of five scanning tables, one manual measuring machine and the Spiral Reader measuring machine. A computer CD 6400 is available at the institute. The research program comprises study of 100 GeV/c antiproton-deuterium reactions, 12 GeV/c antiproton-deuterium reactions, 9 and 12 GeV/c antiproton-proton reactions studying all annihilation and non-annihilation processes, a detailed study of amplitudes in 4 GeV/c π - p reactions with strange particles, strange particle production in 19 GeV/c pp and study of 19 GeV/c pd. The main emphasis in the future will be on experiments with the European Hybrid Spectrometer system and the Big European Bubble Chamber at SPS. The group participates in the design work and planning for the physics experiments. Research physicists from the group participate in counter experiments at SPS studying elastic scattering at high transverse momenta, elastic scattering of π, K and p sup(+-) at PS energies and study of line reversal invariance in πp and Kp reactions. (author)

  15. Magnetic spectrometer Grand Raiden

    International Nuclear Information System (INIS)

    Fujiwara, M.; Akimune, H.; Daito, I.; Fujimura, H.; Fujita, Y.; Hatanaka, K.; Ikegami, H.; Katayama, I.; Nagayama, K.; Matsuoka, N.; Morinobu, S.; Noro, T.; Yoshimura, M.; Sakaguchi, H.; Sakemi, Y.; Tamii, A.; Yosoi, M.

    1999-01-01

    A high-resolution magnetic spectrometer called 'Grand Raiden' is operated at the RCNP ring cyclotron facility in Osaka for nuclear physics studies at intermediate energies. This magnetic spectrometer has excellent ion-optical properties. In the design of the spectrometer, the second-order dispersion matching condition has been taken into account, and almost all the aberration terms such as (x vertical bar θ 3 ), (x vertical bar θφ 2 ), (x vertical bar θ 2 δ) and (x vertical bar θδ 2 ) in a third-order matrix calculation are optimized. A large magnetic rigidity of the spectrometer (K = 1400 MeV) gives a great advantage to measure the charge-exchange ( 3 He, t) reactions at 450 MeV. The ability of the high-resolution measurement has been demonstrated. Various coincidence measurements are performed to study the nuclear structures of highly excited states through decay properties of nuclear levels following nuclear reactions at intermediate energies

  16. The plastic ball spectrometer - an electronic 4π detector with particle identification

    International Nuclear Information System (INIS)

    Baden, A.; Poskanzer, A.M.; Renner, T.; Riedesel, H.

    1982-04-01

    For the high multiplicity events occuring in relativistic nuclear collisions an electronic 4π detector with particle identification has been built. It consists of 815 ΔE-E telescopes and 176 TOF telescopes covering 97% of 4π. Very good particle identification has been obtained for hydrogen and helium isotopes and also π + have been detected with high efficiency. (orig.)

  17. High-temperature quadrupole mass spectrometer for studying vaporization from materials heated by a CO2 laser

    International Nuclear Information System (INIS)

    Fredin, L.; Hansen, G.P.; Sampson, M.P.; Margrave, J.L.; Behrens, R.G.

    1986-09-01

    To evaluate the effectiveness of mass spectrometry techniques in studying vaporization from selected materials, we designed a mass spectrometer than can be used either with a continuous wave or pulsed laser heating system or with a conventional furnace heating system. Our experimental apparatus, the components of which are described in detail, consisted of a quadrupole mass spectrometer positioned in a crossed-beam configuration, controlling electronics, a data acquisition system, a vacuum system, a cryogenic collimation system, and a laser heating system. Results of mass spectral scans taken during laser pyrolysis of polymeric materials and laser vaporization of graphite were compatible with data reported in other studies. Results of mass spectral studies of laser-induced combustion in the Ti + C system are also presented

  18. Dosimetry and microdosimetry using LET spectrometer based on the track-etch detector: radiotherapy Bremsstrahlung beam, onboard aircraft radiation field

    International Nuclear Information System (INIS)

    Jadrnickova, I.; Spurny, F.

    2006-01-01

    The spectrometer of linear energy transfer (Let) based on the chemically etched poly-allyl-diglycol-carbonate (P.A.D.C.) track-etch detector was developed several years ago in our institute. This Let spectrometer enables determining Let of particles approximately from 10 to 700 keV/μm. From the Let spectra, dose characteristics can be calculated. The contribution presents the Let spectra and other dosimetric characteristics obtained onboard a commercial aircraft during more than 6 months long exposure and in the 18 MV radiotherapy Bremsstrahlung beam. (authors)

  19. RITA-type triple axis spectrometers

    International Nuclear Information System (INIS)

    Roennow, H.M.

    2001-01-01

    The RITA spectrometer at Risoe National Laboratory was the first to incorporate a complete re-thinking of the neutron-path from source, through detector to analysis. Since then, other RITA-type spectrometers such as SPINS at NIST, RITA-II at PSI have been built, and several new spectrometers around the world are adapting the same philosophy. The main novelty of RITA was the introduction of a single back-end tank featuring both an analyser block with multiple individually turnable analyser blades and a 2D position sensitive detector. Several new triple-axis spectrometers are presently being built at existing and future sources, and almost all of them have learnt from the experience with RITA. (R.P.)

  20. Particles and nuclei, letters

    International Nuclear Information System (INIS)

    2000-01-01

    The present collection of letters from JINR, Dubna, contains seven separate records on the integral representation for structure functions and target mass effects, multiscale properties of DNA primary structure including cross-scale correlations, dissipative evolution of the elementary act, the fine structure of the M T =1 Gamow-Teller resonance in 147g Tb→ 147 Gd β + /EC decay, the behaviour of the TVO temperature sensors in the magnetic fields, a fast method for searching for tracks in multilayer drift chambers of HADES spectrometer, a novel approach to particle track etching including surfactant enhanced control of pore morphology, azimuthal correlations of secondary particles in 32 S induced interactions with Ag(Br) nuclei at 4.5 GeV/ c/ nucleon

  1. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions

    International Nuclear Information System (INIS)

    Arndt, J.; Deboudt, K.; Anderson, A.; Blondel, A.; Eliet, S.; Flament, P.; Fourmentin, M.; Healy, R.M.; Savary, V.; Setyan, A.; Wenger, J.C.

    2016-01-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe–Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy–energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. - Highlights: • Similar composition for emitted particles as those collected on the chimney filters. • Emitted particles dominated by Ca-, Mn and/or Al-containing particles. • Identification of specific particle types emitted by the different process units. - The particles emitted by metallurgy activities are fully described by ATOFMS and SEM-EDX, enabling the identification of specific particle types from the different units of the process.

  2. Near-Infrared Mapping Spectrometer for investigation of Jupiter and its satellites

    International Nuclear Information System (INIS)

    Aptaker, I.M.

    1988-01-01

    The Near-Infrared-Mapping Spectrometer (NIMS) is one of the science instruments in the Galileo mission, which will explore Jupiter and its satellites in the mid-1990's. The NIMS experiment will map geological units on the surfaces of the Jovian satellites and characterize their mineral content; and, for the atmosphere of Jupiter, investigate cloud properties and the spatial and temporal variability of molecular abundances. The optics are gold-coated reflective and consist of a telescope and a grating spectrometer. The balance of the instrument includes a 17-detector (silicon and indium antimonide) focal plane array, a tuning fork chopper, microprocessor-controlled electronics, and a passive radiative cooler. A wobbling secondary mirror in the telescope provides 20 pixels in one dimension of spatial scanning in a pushbroom mode with 0.5 mr x 0.5 mr instantaneous field of view. The spectral range is 0.7-5.2 microns; resolution is 0.025 micron. NIMS is the first infrared experiment to combine both spatial and spectral mapping capability in one instrument

  3. Software for mass spectrometer control

    International Nuclear Information System (INIS)

    Curuia, Marian; Culcer, Mihai; Anghel, Mihai; Iliescu, Mariana; Trancota, Dan; Kaucsar, Martin; Oprea, Cristiana

    2004-01-01

    The paper describes a software application for the MAT 250 mass spectrometer control, which was refurbished. The spectrometer was bring-up-to-date using a hardware structure on its support where the software application for mass spectrometer control was developed . The software application is composed of dedicated modules that perform given operations. The instructions that these modules have to perform are generated by a principal module. This module makes possible the change of information between the modules that compose the software application. The use of a modal structure is useful for adding new functions in the future. The developed application in our institute made possible the transformation of the mass spectrometer MAT 250 into a device endowed with other new generation tools. (authors)

  4. 3m vacuum ultraviolet spectrometer with optical multichanel detector

    International Nuclear Information System (INIS)

    Marin, P.; Peraza, C.; Blanco, F.; Campos, J.

    1993-01-01

    This paper, describes the design and the performance of a normal incidence vacuum ultraviolet spectrometer, for the 300-2400 A spectral range. It is provided with a multichannel detection system. The monochromator is original design and it has been built at CIEMAT: It is equipped with a 3 m concave holographic grating with 2400 grooves/mm. The multichannel detector consists of a windowless double microchannel plate/phosphor screen image intensifier, coupled by fiber optic to a 1024 elements self-scanning linear photodiode array. The output from the arrays is digitized by a 12-bit analog to digital converter and stored in a computer for its later analysis. The necessary software to store and display data has been developed. (Author)

  5. Direct mass measurements of light neutron-rich nuclei using fast recoil spectrometers

    International Nuclear Information System (INIS)

    Vieira, D.J.; Wouters, J.M.

    1987-01-01

    Extensive new mass measurement capabilities have evolved with the development of recoil spectrometers. In the Z = 3 to 9 neutron-rich region alone, 12 neutron-rich nuclei have been determined for the first time by the fast-recoil direct mass measurement method. A recent experiment using the TOFI spectrometer illustrates this technique. A systematic investigation of nuclei that lie along or near the neutron-drip line has provided a valuable first glimpse into the nuclear structure of such nuclei. No evidence for a large single-particle energy gap at N = 14 is observed; however, a change in the two-neutron separation model calculations, and is interpreted in terms of the smaller 1s/sub 1/2/ - 1s/sub 1/2/ interaction compared to that of the 0d/sub 5/2/ - 0d/sub 5/2/ neutron-neutron interaction. 18 refs., 7 figs., 1 tab

  6. Resolution of the VESUVIO spectrometer for High-energy Inelastic Neutron Scattering experiments

    Science.gov (United States)

    Imberti, S.; Andreani, C.; Garbuio, V.; Gorini, G.; Pietropaolo, A.; Senesi, R.; Tardocchi, M.

    2005-11-01

    New perspectives for epithermal neutron spectroscopy have been opened up as a result of the development of the Resonance Detector and its use on inverse geometry time-of-flight spectrometers at spallation sources. A special application of the Resonance Detector is the Very Low Angle Detector Bank (VLAD) for the VESUVIO spectrometer at ISIS, operating in the angular range 1∘500 meV, a regime so far inaccessible to experimental studies on condensed matter systems. The HINS measurements complement the Deep Inelastic Neutron Scattering (DINS) measurements performed on VESUVIO in the high wavevector q(20 Å-11 eV), where the short-time single-particle dynamics can be sampled. This paper will revise the main components of the resolution for HINS measurements of VESUVIO. Instrument performances and examples of applications for neutron scattering processes at high energy and at low wavevector transfer are discussed.

  7. Method and apparatus for scanning x-ray tomography

    International Nuclear Information System (INIS)

    Albert, R.D.

    1988-01-01

    In a method of producing a tomographic image of a subject that includes the steps of generating X-rays at a moving origin point by directing a charged particle beam to a target surface, deflecting the charged particle beam to travel the origin point through a predetermined raster scan at the surface, detecting variations of X-ray intensity during the course of the raster scan at spaced apart detection points situated at the opposite side of the subject from the origin point, generating a first sequence of data values that is indicative of variations of X-ray intensity at a first of the detection points at successive times during the course of the raster scan and generating at least a second sequence of data values that is indicative of variations of X-ray intensity at a second of the detection points at successive times during the course of the same raster scan, the improvement is described comprising: combining successive individual data values of the first sequence that are generated by X-rays from successive particular locations in the raster scan with at least individual data values of the second sequence that are generated by X-rays from predetermined successive different locations in the same raster scan in order to produce a composite sequence of data values, and producing an image corresponding to at least a portion of the raster scan which depicts variations of the magnitude of successive data values of the composite sequence

  8. Mass spectrometers in medicine

    International Nuclear Information System (INIS)

    Bushman, J.A.

    1975-01-01

    This paper describes how the mass spectrometer enables true lung function, namely the exchange of gases between the environment and the organism, to be measured. This has greatly improved the understanding of respiratory disease and the latest generation of respiratory mass spectrometers will do much to increase the application of the technique. (author)

  9. Direct observation and analysis of yolk-shell materials using low-voltage high-resolution scanning electron microscopy: Nanometal-particles encapsulated in metal-oxide, carbon, and polymer

    Energy Technology Data Exchange (ETDEWEB)

    Asahina, Shunsuke; Suga, Mitsuo; Takahashi, Hideyuki [JEOL Ltd., SM Business Unit, Tokyo (Japan); Young Jeong, Hu [Graduate School of EEWS, WCU/BK21+, KAIST, Daejeon 305-701 (Korea, Republic of); Galeano, Carolina; Schüth, Ferdi [Department of Heterogeneous Catalysis, Max-Planck-Institut für Kohlenforschung, Mülheim (Germany); Terasaki, Osamu, E-mail: terasaki@mmk.su.se, E-mail: terasaki@kaist.ac.kr [Graduate School of EEWS, WCU/BK21+, KAIST, Daejeon 305-701 (Korea, Republic of); Department of Materials and Environmental Chemistry, Berzelii Centre EXSELENT on Porous Materials, Stockholm University, SE-10691 Stockholm (Sweden)

    2014-11-01

    Nanometal particles show characteristic features in chemical and physical properties depending on their sizes and shapes. For keeping and further enhancing their features, the particles should be protected from coalescence or degradation. One approach is to encapsulate the nanometal particles inside pores with chemically inert or functional materials, such as carbon, polymer, and metal oxides, which contain mesopores to allow permeation of only chemicals not the nanometal particles. Recently developed low-voltage high-resolution scanning electron microscopy was applied to the study of structural, chemical, and electron state of both nanometal particles and encapsulating materials in yolk-shell materials of Au@C, Ru/Pt@C, Au@TiO{sub 2}, and Pt@Polymer. Progresses in the following categories were shown for the yolk-shell materials: (i) resolution of topographic image contrast by secondary electrons, of atomic-number contrast by back-scattered electrons, and of elemental mapping by X-ray energy dispersive spectroscopy; (ii) sample preparation for observing internal structures; and (iii) X-ray spectroscopy such as soft X-ray emission spectroscopy. Transmission electron microscopy was also used for characterization of Au@C.

  10. SPRED: a multichannel grazing-incidence spectrometer for plasma impurity diagnosis

    International Nuclear Information System (INIS)

    Fonck, R.J.; Ramsey, A.T.; Yelle, R.V.

    1982-03-01

    A compact vacuum ultraviolet spectrometer system has been developed to provide time-resolved impurity spectra from tokamak plasmas. Two interchangeable aberration-corrected toroidal diffraction gratings with flat focal fields provide simultaneous coverage over the ranges 100 to 1100 A or 160 to 1700 A. The detector is an intensified self-scanning photodiode array. Spectral resolution is 2 A with the higher dispersion grating. Minimum readout time for a full spectrum is 20 ms, but up to 7 individual spectral lines can be measured with a 1 ms time resolution. The sensitivity of the system is comparable to that of a conventional grazing incidence monochromator

  11. SPRED: a multichannel grazing-incidence spectrometer for plasma impurity diagnosis

    Energy Technology Data Exchange (ETDEWEB)

    Fonck, R.J.; Ramsey, A.T.; Yelle, R.V.

    1982-03-01

    A compact vacuum ultraviolet spectrometer system has been developed to provide time-resolved impurity spectra from tokamak plasmas. Two interchangeable aberration-corrected toroidal diffraction gratings with flat focal fields provide simultaneous coverage over the ranges 100 to 1100 A or 160 to 1700 A. The detector is an intensified self-scanning photodiode array. Spectral resolution is 2 A with the higher dispersion grating. Minimum readout time for a full spectrum is 20 ms, but up to 7 individual spectral lines can be measured with a 1 ms time resolution. The sensitivity of the system is comparable to that of a conventional grazing incidence monochromator.

  12. The measurement of tripartition alpha particle low energy spectrum in 235U fission induced by thermal neutrons

    International Nuclear Information System (INIS)

    El Hage Sleiman, F.

    1980-01-01

    The energy spectrum of the α particles emitted in the thermal neutron induced fission of 235 U was measured from 11.5 MeV down to 2 MeV using the parabola mass spectrometer Lohengrin at the ILL high flux reactor. A Monte Carlo program, that simulates the α particle motion to the spectrometer, has been developed. Numerical results of Monte Carlo calculations for differents values of parameter are reported. The overall energy spectrum is slightly asymmetric at low energy. The possible reasons for the existence of this asymmetry are discussed [fr

  13. spectrometer

    Directory of Open Access Journals (Sweden)

    J. K. Hedelius

    2016-08-01

    Full Text Available Bruker™ EM27/SUN instruments are commercial mobile solar-viewing near-IR spectrometers. They show promise for expanding the global density of atmospheric column measurements of greenhouse gases and are being marketed for such applications. They have been shown to measure the same variations of atmospheric gases within a day as the high-resolution spectrometers of the Total Carbon Column Observing Network (TCCON. However, there is little known about the long-term precision and uncertainty budgets of EM27/SUN measurements. In this study, which includes a comparison of 186 measurement days spanning 11 months, we note that atmospheric variations of Xgas within a single day are well captured by these low-resolution instruments, but over several months, the measurements drift noticeably. We present comparisons between EM27/SUN instruments and the TCCON using GGG as the retrieval algorithm. In addition, we perform several tests to evaluate the robustness of the performance and determine the largest sources of errors from these spectrometers. We include comparisons of XCO2, XCH4, XCO, and XN2O. Specifically we note EM27/SUN biases for January 2015 of 0.03, 0.75, –0.12, and 2.43 % for XCO2, XCH4, XCO, and XN2O respectively, with 1σ running precisions of 0.08 and 0.06 % for XCO2 and XCH4 from measurements in Pasadena. We also identify significant error caused by nonlinear sensitivity when using an extended spectral range detector used to measure CO and N2O.

  14. Real-time analysis of insoluble particles in glacial ice using single-particle mass spectrometry

    Science.gov (United States)

    Osman, Matthew; Zawadowicz, Maria A.; Das, Sarah B.; Cziczo, Daniel J.

    2017-11-01

    Insoluble aerosol particles trapped in glacial ice provide insight into past climates, but analysis requires information on climatically relevant particle properties, such as size, abundance, and internal mixing. We present a new analytical method using a time-of-flight single-particle mass spectrometer (SPMS) to determine the composition and size of insoluble particles in glacial ice over an aerodynamic size range of ˜ 0.2-3.0 µm diameter. Using samples from two Greenland ice cores, we developed a procedure to nebulize insoluble particles suspended in melted ice, evaporate condensed liquid from those particles, and transport them to the SPMS for analysis. We further determined size-dependent extraction and instrument transmission efficiencies to investigate the feasibility of determining particle-class-specific mass concentrations. We find SPMS can be used to provide constraints on the aerodynamic size, composition, and relative abundance of most insoluble particulate classes in ice core samples. We describe the importance of post-aqueous processing to particles, a process which occurs due to nebulization of aerosols from an aqueous suspension of originally soluble and insoluble aerosol components. This study represents an initial attempt to use SPMS as an emerging technique for the study of insoluble particulates in ice cores.

  15. Multilayer Semiconductor Charged-Particle Spectrometers for Accelerator Experiments

    Science.gov (United States)

    Gurov, Yu. B.; Lapushkin, S. V.; Sandukovsky, V. G.; Chernyshev, B. A.

    2018-03-01

    The current state of studies in the field of development of multilayer semiconductor systems (semiconductor detector (SCD) telescopes), which allow the energy to be precisely measured within a large dynamic range (from a few to a few hundred MeV) and the particles to be identified in a wide mass range (from pions to multiply charged nuclear fragments), is presented. The techniques for manufacturing the SCD telescopes from silicon and high-purity germanium are described. The issues of measuring characteristics of the constructed detectors and their impact on the energy resolution of the SCD telescopes and on the quality of the experimental data are considered. Much attention is given to the use of the constructed semiconductor devices in experimental studies at accelerators of PNPI (Gatchina), LANL (Los Alamos) and CELSIUS (Uppsala).

  16. How comparable are size-resolved particle number concentrations from different instruments?

    Science.gov (United States)

    Hornsby, K. E.; Pryor, S. C.

    2012-12-01

    The need for comparability of particle size resolved measurements originates from multiple drivers including: (i) Recent suggestions that air quality standards for particulate matter should migrate from being mass-based to incorporating number concentrations. This move would necessarily be predicated on measurement comparability which is absolutely critical to compliance determination. (ii) The need to quantify and diagnose causes of variability in nucleation and growth rates in nano-particle experiments conducted in different locations. (iii) Epidemiological research designed to identify key parameters in human health responses to fine particle exposure. Here we present results from a detailed controlled laboratory instrument inter-comparison experiment designed to investigate data comparability in the size range of 2.01-523.3 nm across a range of particle composition, modal diameter and absolute concentration. Particle size distributions were generated using a TSI model 3940 Aerosol Generation System (AGS) diluted using zero air, and sampled using four TSI Scanning Mobility Particle Spectrometer (SMPS) configurations and a TSI model 3091 Fast Mobility Particle Sizer (FMPS). The SMPS configurations used two Electrostatic Classifiers (EC) (model 3080) attached to either a Long DMA (LDMA) (model 3081) or a Nano DMA (NDMA) (model 3085) plumbed to either a TSI model 3025A Butanol Condensed Particle Counting (CPC) or a TSI model 3788 Water CPC. All four systems were run using both high and low flow conditions, and were operated with both the internal diffusion loss and multiple charge corrections turned on. The particle compositions tested were sodium chloride, ammonium nitrate and olive oil diluted in ethanol. Particles of all three were generated at three peak concentration levels (spanning the range observed at our experimental site), and three modal particle diameters. Experimental conditions were maintained for a period of 20 minutes to ensure experimental

  17. An Improvement on Space Focusing Resolution in Two-Field Time-of-Flight Mass Spectrometers

    International Nuclear Information System (INIS)

    Yildirim, M.; Aydin, R.; Akin, U.; Kilic, H. S.; Sise, O.; Ulu, M.; Dogan, M.

    2007-01-01

    Time-of-Flight Mass Spectrometer (TOFMS) is a sophisticated device for the mass selective analysis of a variety of samples. The main limitation on TOFMS technique is the obtainable resolution where the two main limiting factors are the initial space and energy spread of particles created in ionization region. Similar charged particles starting at different points will reach the detector at different times. So, this problem makes space focusing is very important subject. We have presented principles of two-fields TOFMS with second-order space focusing both using analytical methods and ray-tracing simulation. This work aims understanding of ion optical system clearly and gives hint of expectation for future developments

  18. Performance Studies of Resistive Micromegas Detectors for the Upgrade of the ATLAS Muon Spectrometer

    CERN Document Server

    AUTHOR|(INSPIRE)INSPIRE-00387450

    2017-01-01

    With the high luminosity upgrade of the LHC the ATLAS Muon spectrometer will face increased particle rates, requiring an upgrade of the innermost end-cap detectors with a high-rate capable technology. Micromegas have been chosen as main tracking technology for this New Small Wheel upgrade. In an intense R$\\&$D and prototype phase the technology has proven to meet the stringent performance requirements of highly efficient particle detection with better than 100$\\rm{\\mu m}$ spatial resolution, independent of the track incidence angle up to 32$^\\circ$, in a magnetic field B $\\leq$ 0.3 T and at background hit rate of up to 15kHz/cm$^2$.

  19. ATLAS Muon Spectrometer Upgrades for the High Luminosity LHC

    CERN Document Server

    Valderanis, Chrysostomos; The ATLAS collaboration

    2015-01-01

    ATLAS Muon Spectrometer Upgrades for the High Luminosity LHC The luminosity of the LHC will increase up to 2x10^34 cm-2s-1 after the long shutdown in 2019 (phase-1 upgrade) and up to 7x10^34 cm-2s-1 after the long shutdown in 2025 (phase-2 upgrade). In order to cope with the increased particle fluxes, upgrades are envisioned for the ATLAS muon spectrometer. At phase-1, the current innermost stations of the ATLAS muon endcap tracking system (the Small Wheels) will be upgraded with 2x4-layer modules of Micromega detectors, sandwiched by two 4 layer modules of small strip Thin Gap Chambers on either side. Each 4-layer module of the so-called New Small Wheels covers a surface area of approximately 2 to 3 m2 for a total active area of 1200 m2 each for the two technologies. On such large area detectors, the mechanical precision (30 \\mu m along the precision coordinate and 80 \\mu m along the beam) is a key point and must be controlled and monitored along the process of construction and integration. The design and re...

  20. HyperCP: A high-rate spectrometer for the study of charged hyperon and kaon decays

    International Nuclear Information System (INIS)

    Burnstein, R.A.; Chakravorty, A.; Chan, A.; Chen, Y.C.; Choong, W.-S.; Clark, K.; Dukes, E.C.; Durandet, C.; Felix, J.; Fuzesy, R.; Gidal, G.; Gu, P.; Gustafson, H.R.; Ho, C.; Holmstrom, T.; Huang, M.; James, C.; Jenkins, C.M.; Jones, T.D.; Kaplan, D.M.; Lederman, L.M.; Leros, N.; Longo, M.J.; Lopez, F.; Lu, L.C.; Luebke, W.; Luk, K.-B.; Nelson, K.S.; Park, H.K.; Perroud, J.-P.; Rajaram, D.; Rubin, H.A.; Teng, P.K.; Turko, B.; Volk, J.; White, C.G.; White, S.L.; Zyla, P.

    2005-01-01

    The HyperCP experiment (Fermilab E871) was designed to search for rare phenomena in the decays of charged strange particles, in particular CP violation in Ξ and Λ hyperon decays with a sensitivity of 10 -4 . Intense charged secondary beams were produced by 800GeV/c protons and momentum selected by a magnetic channel. Decay products were detected in a large-acceptance, high-rate magnetic spectrometer using multiwire proportional chambers, trigger hodoscopes, a hadronic calorimeter, and a muon-detection system. Nearly identical acceptances and efficiencies for hyperons and antihyperons decaying within an evacuated volume were achieved by reversing the polarities of the channel and spectrometer magnets. A high-rate data-acquisition system enabled 231 billion events to be recorded in 12 months of data-taking

  1. Enhanced antioxidation and microwave absorbing properties of SiO2-coated flaky carbonyl iron particles

    Science.gov (United States)

    Zhou, Yingying; Xie, Hui; Zhou, Wancheng; Ren, Zhaowen

    2018-01-01

    SiO2 was successfully coated on the surface of flaky carbonyl iron particles using a chemical bath deposition method in the presence of 3-aminopropyl triethoxysilane (APTES). The morphologies, composition, valence states of elements, as well as antioxidation and electromagnetic properties of the samples were characterized by scanning electron microscope (SEM), energy dispersive spectrometer (EDS), X-ray photoelectron spectroscopy (XPS), thermogravimetric (TG) and microwave network analyzer. TG curve shows the obvious weight gain of carbonyl iron was deferred to 360 °C after SiO2-coated, which can be ascribed to the exits of SiO2 overlayer. Compared with the raw carbonyl iron, SiO2-coated sample shows good wave absorption performance due to its impedance matching. The electromagnetic properties of raw and SiO2-coated carbonyl iron particles were characterized in X band before and after heat treatment at 250 °C for 10 h. It was established that SiO2-coated carbonyl iron demonstrate good thermal stability, indicating SiO2-coating is useful in the usage of microwave absorbers operating at temperature up to 250 °C.

  2. Circumvention of fluorophore photobleaching in fluorescence fluctuation experiments: a beam scanning approach.

    Science.gov (United States)

    Satsoura, Dmitri; Leber, Brian; Andrews, David W; Fradin, Cécile

    2007-04-23

    Photobleaching is a fluorophore-damaging process that commonly afflicts single-molecule fluorescence studies. It becomes an especially severe problem in fluorescence fluctuation experiments when studying slowly diffusing particles. One way to circumvent this problem is to use beam scanning to decrease the residence time of the fluorophores in the excitation volume. We report a systematic study of the effects of circular beam scanning on the photobleaching of fluorescent particles as observed in single-photon excitation fluorescence fluctuation experiments. We start by deriving a simple expression relating the average detected fluorescence to the photobleaching cross section of the fluorophores. We then perform numerical calculations of the spatial distribution of fluorescent particles in order to understand under which conditions beam scanning can prevent the formation of a photobleaching hole. To support these predictions, we show experimental results obtained for large unilamellar vesicles containing a small amount of the fluorescent lipophilic tracer DiD. We establish the required scanning radius and frequency range in order to obtain sufficient reduction of the photobleaching effect for that system. From the detected increase in fluorescence upon increase in scanning speed, we estimate the photobleaching cross section of DiD.

  3. Background reduction of the KATRIN spectrometers. Transmission function of the pre-spectrometer and systematic tests of the main-spectrometer wire electrode

    Energy Technology Data Exchange (ETDEWEB)

    Prall, Matthias

    2011-07-04

    The KArlsruhe TRItium Neutrino experiment, KATRIN will determine the mass of the anti {nu}{sub e} with a sensitivity of 0.2 eV (90% C.L.) via a measurement of the {beta}-spectrum of tritium decaying in a windowless gaseous molecular tritium source near its endpoint of 18.57 keV. This approach relies exclusively on the relativistic kinematics of the decay products rendering the experiment model independent and reducing the systematic uncertainty. An ultra-low background of a few mHz and an energy resolution of 0.93 eV are among the requirements to reach the sensitivity. These demands are fulfilled with the main spectrometer (MS). While the {beta}-decay electrons are guided by a magnetic field through the experiment, the MS acts as a high-pass filter for the {beta}-decay electrons. Only those above an energy barrier, the retarding potential, are transmitted to the detector. The last about 30 eV of the T{sub 2} {beta}-spectrum will be scanned in this way. The MS is equipped with a 650 m{sup 2}, two-layered, UHV compatible and quasi-massless wire electrode suppressing secondary electron background originating at the main-spectrometer walls and caused by residual radioactivity and cosmic muons. Its energy resolution of 0.93 eV is only achieved, if a large part of the 248 wire electrode modules, which determine the electric field inside the MS, has a mechanical precision of 0.2 mm. Not a single of the about 28.000 wires of the electrode must break during the lifetime of KATRIN. A 2-dimensional laser sensor for contact-less position (precision about 0.01 mm) and tension (precision about 0.04 N) measurements was developed and applied, to firstly, verify the mechanical precision of the electrode modules and secondly, to examine their reliability. A 3-dimensional coordinate measurement table was automated to perform these measurements in a clean room. This table was also used to verify the precision of components using a camera system and image recognition methods (0.05 mm

  4. Electrophoretic deposition of PTFE particles on porous anodic aluminum oxide film and its tribological properties

    International Nuclear Information System (INIS)

    Zhang, Dongya; Dong, Guangneng; Chen, Yinjuan; Zeng, Qunfeng

    2014-01-01

    Polytetrafluoroethylene (PTFE) composite film was successfully fabricated by depositing PTFE particles into porous anodic aluminum oxide film using electrophoretic deposition (EPD) process. Firstly, porous anodic aluminum oxide film was synthesized by anodic oxidation process in sulphuric acid electrolyte. Then, PTFE particles in suspension were directionally deposited into the porous substrate. Finally, a heat treatment at 300 °C for 1 h was utilized to enhance PTFE particles adhesion to the substrate. The influence of anodic oxidation parameters on the morphology and micro-hardness of the porous anodic aluminum oxide film was studied and the PTFE particles deposited into the pores were authenticated using energy-dispersive spectrometer (EDS) and scanning electron microscopy (SEM). Tribological properties of the PTFE composite film were investigated under dry sliding. The experimental results showed that the composite film exhibit remarkable low friction. The composite film had friction coefficient of 0.20 which deposited in 15% PTFE emulsion at temperature of 15 °C and current density of 3 A/dm 2 for 35 min. In addition, a control specimen of porous anodic aluminum oxide film and the PTFE composite film were carried out under the same test condition, friction coefficient of the PTFE composite film was reduced by 60% comparing with the control specimen at 380 MPa and 100 mm/s. The lubricating mechanism was that PTFE particles embedded in porous anodic aluminum oxide film smeared a transfer film on the sliding path and the micro-pores could support the supplement of solid lubricant during the sliding, which prolonged the lubrication life of the aluminum alloys.

  5. Note: Electron energy spectroscopy mapping of surface with scanning tunneling microscope.

    Science.gov (United States)

    Li, Meng; Xu, Chunkai; Zhang, Panke; Li, Zhean; Chen, Xiangjun

    2016-08-01

    We report a novel scanning probe electron energy spectrometer (SPEES) which combines a double toroidal analyzer with a scanning tunneling microscope to achieve both topography imaging and electron energy spectroscopy mapping of surface in situ. The spatial resolution of spectroscopy mapping is determined to be better than 0.7 ± 0.2 μm at a tip sample distance of 7 μm. Meanwhile, the size of the field emission electron beam spot on the surface is also measured, and is about 3.6 ± 0.8 μm in diameter. This unambiguously demonstrates that the spatial resolution of SPEES technique can be much better than the size of the incident electron beam.

  6. Note: Electron energy spectroscopy mapping of surface with scanning tunneling microscope

    Energy Technology Data Exchange (ETDEWEB)

    Li, Meng; Xu, Chunkai, E-mail: xuck@ustc.edu.cn, E-mail: xjun@ustc.edu.cn; Zhang, Panke; Li, Zhean; Chen, Xiangjun, E-mail: xuck@ustc.edu.cn, E-mail: xjun@ustc.edu.cn [Hefei National Laboratory for Physical Science at Microscale and Department of Modern Physics, University of Science and Technology of China, Hefei 230026, China and Synergetic Innovation Center of Quantum Information and Quantum Physics, University of Science and Technology of China, Hefei 230026 (China)

    2016-08-15

    We report a novel scanning probe electron energy spectrometer (SPEES) which combines a double toroidal analyzer with a scanning tunneling microscope to achieve both topography imaging and electron energy spectroscopy mapping of surface in situ. The spatial resolution of spectroscopy mapping is determined to be better than 0.7 ± 0.2 μm at a tip sample distance of 7 μm. Meanwhile, the size of the field emission electron beam spot on the surface is also measured, and is about 3.6 ± 0.8 μm in diameter. This unambiguously demonstrates that the spatial resolution of SPEES technique can be much better than the size of the incident electron beam.

  7. Note: Electron energy spectroscopy mapping of surface with scanning tunneling microscope

    International Nuclear Information System (INIS)

    Li, Meng; Xu, Chunkai; Zhang, Panke; Li, Zhean; Chen, Xiangjun

    2016-01-01

    We report a novel scanning probe electron energy spectrometer (SPEES) which combines a double toroidal analyzer with a scanning tunneling microscope to achieve both topography imaging and electron energy spectroscopy mapping of surface in situ. The spatial resolution of spectroscopy mapping is determined to be better than 0.7 ± 0.2 μm at a tip sample distance of 7 μm. Meanwhile, the size of the field emission electron beam spot on the surface is also measured, and is about 3.6 ± 0.8 μm in diameter. This unambiguously demonstrates that the spatial resolution of SPEES technique can be much better than the size of the incident electron beam.

  8. LANL/Green Star spectrometer tests

    International Nuclear Information System (INIS)

    Sampson, T.E.; Cremers, T.L.; Vo, D.T.; Seldiakov, Y.P.; Dorin, A.B.; Kondrashov, M.V.; Timoshin, V.I.

    1997-12-01

    The US and Russia have agreed to the joint development of a nondestructive assay system for use to support the dismantlement of nuclear weapons in Russia. This nondestructive assay system will be used to measure plutonium produced by the conversion of Russian nuclear weapons. The NDA system for Russia will be patterned after the ARIES NDA system being constructed at Los Alamos. One goal of the program is to produce an NDA system for use in Russia that maximizes the use of Russian resources to facilitate maintenance and future upgrades. The Green Star SBS50 Single Board Spectrometer system (Green Star Ltd., Moscow, Russia) has been suggested for use as the data acquisition component for gamma ray instruments in the system. Possible uses are for plutonium isotopic analysis and also segmented gamma scanning. Green Star has also developed analysis software for the SBS50. This software, both plutonium isotopic analysis and uranium enrichment analysis, was developed specifically for customs/border inspection applications (low counting rate applications and identification as opposed to quantification) and was not intended for MC and A applications. Because of the relative immaturity of the Green Star plutonium isotopic analysis software (it has been under development for only one year and is patterned after US development circa 1980), it was tentatively agreed, before the tests, that the Russian NDA system would use the Los Alamos PC/FRAM software for plutonium isotopic analysis. However, it was also decided to include the Green Star plutonium isotopic software in the testing, both to quantify its performance for MC and A applications and also to provide additional data to Green Star for further development of their software. The main purpose of the testing was to evaluate the SBS-50 spectrometer as a data acquisition device for use with LANL software

  9. Electron spectrometer for gas-phase spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Bozek, J.D.; Schlachter, A.S. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

    1997-04-01

    An electron spectrometer for high-resolution spectroscopy of gaseous samples using synchrotron radiation has been designed and constructed. The spectrometer consists of a gas cell, cylindrical electrostatic lens, spherical-sector electron energy analyzer, position-sensitive detector and associated power supplies, electronics and vacuum pumps. Details of the spectrometer design are presented together with some representative spectra.

  10. Solar flare activity in 2006 - 2016 according to PAMELA and ARINA spectrometers

    Science.gov (United States)

    Rodenko, S. A.; Borkut, I. K.; Mayorov, A. G.; Malakhov, V. V.; PAMELA Collaboration

    2018-01-01

    From 2006 to 2016 years on the board of RESURS-DK1 satellite PAMELA and ARINA cosmic rays experiments was carried out. The main goal of experiments is measurement of galactic component of cosmic rays; it also registers solar particles accelerated in powerful explosive processes on the sun (solar flares) in wide energy range. The article includes the list of solar events when PAMELA or ARINA spectrometers have registered increasing of proton flux intensities for energies more than 4 MeV.

  11. Detailed SEM-EPMA investigation of high specific radioactivity particles (hot particles)

    International Nuclear Information System (INIS)

    Burin, K.; Tsacheva, Ts.; Mandjoukov, I.; Mandjoukova, B.

    1993-01-01

    Scanning electron microscope (SEM) images and electron probe microanalysis (EPMA) spectra of a group of hot particles collected in Bulgaria after the Chernobyl accident have been obtained. A technique for hot particle localization is described. The object is irradiated for two days with a β source and the resulting autoradiographs show particles location precisely. High resolution x-ray spectrum of each particle has been obtained using EPMA. The distribution of chemical elements is visualized by colour dot maps representing the regions of interest of the spectrum. It is concluded that apart from reactor fuel the investigated hot particles come from either construction materials or materials used for the covering of the damaged reactor. 7 figs., 2 ref

  12. Spectrometers for compact neutron sources

    Science.gov (United States)

    Voigt, J.; Böhm, S.; Dabruck, J. P.; Rücker, U.; Gutberlet, T.; Brückel, T.

    2018-03-01

    We discuss the potential for neutron spectrometers at novel accelerator driven compact neutron sources. Such a High Brilliance Source (HBS) relies on low energy nuclear reactions, which enable cryogenic moderators in very close proximity to the target and neutron optics at comparably short distances from the moderator compared to existing sources. While the first effect aims at increasing the phase space density of a moderator, the second allows the extraction of a large phase space volume, which is typically requested for spectrometer applications. We find that competitive spectrometers can be realized if (a) the neutron production rate can be synchronized with the experiment repetition rate and (b) the emission characteristics of the moderator can be matched to the phase space requirements of the experiment. MCNP simulations for protons or deuterons on a Beryllium target with a suitable target/moderator design yield a source brightness, from which we calculate the sample fluxes by phase space considerations for different types of spectrometers. These match closely the figures of todays spectrometers at medium flux sources. Hence we conclude that compact neutron sources might be a viable option for next generation neutron sources.

  13. How does a scanning ribosomal particle move along the 5'-untranslated region of eukaryotic mRNA? Brownian Ratchet model.

    Science.gov (United States)

    Spirin, Alexander S

    2009-11-17

    A model of the ATP-dependent unidirectional movement of the 43S ribosomal initiation complex (=40S ribosomal subunit + eIF1 + eIF1A + eIF2.GTP.Met-tRNA(i) + eIF3) during scanning of the 5'-untranslated region of eukaryotic mRNA is proposed. The model is based on the principles of molecular Brownian ratchet machines and explains several enigmatic data concerning the scanning complex. In this model, the one-dimensional diffusion of the ribosomal initiation complex along the mRNA chain is rectified into the net-unidirectional 5'-to-3' movement by the Feynman ratchet-and-pawl mechanism. The proposed mechanism is organized by the heterotrimeric protein eIF4F (=eIF4A + eIF4E + eIF4G), attached to the scanning ribosomal particle via eIF3, and the RNA-binding protein eIF4B that is postulated to play the role of the pawl. The energy for the useful work of the ratchet-and-pawl mechanism is supplied from ATP hydrolysis induced by the eIF4A subunit: ATP binding and its hydrolysis alternately change the affinities of eIF4A for eIF4B and for mRNA, resulting in the restriction of backward diffusional sliding of the 43S ribosomal complex along the mRNA chain, while stochastic movements ahead are allowed.

  14. Lessons learned with the SAGE spectrometer

    International Nuclear Information System (INIS)

    Sorri, J; Greenlees, P T; Jones, P; Julin, R; Konki, J; Pakarinen, J; Rahkila, P; Sandzelius, M; Uusitalo, J; Papadakis, P; Cox, D M; Herzberg, R D

    2012-01-01

    The SAGE spectrometer combines a high-efficiency γ-ray detection system with an electron spectrometer. Some of the design features have been known to be problematic and surprises have come up during the early implementation of the spectrometer. Tests related to bismuth germanate Compton-suppression shields, electron detection efficiency and an improved cooling system are discussed in the paper. (paper)

  15. Peculiarities of taking account of background and spectrometer response function in processing the (n,p) and (n,np) reaction spectra

    International Nuclear Information System (INIS)

    Aleksandrov, D.V.; Kovrigin, B.S.

    1980-01-01

    Problems of taking account of background and spectrometer response function when restoring spectra of the (n, p) and (n, np) reactions at 14 MeV neutron energy are considered. These reaction spectra have been obtained by the (E, ΔE) method by means of a telescope consisting of two proportional gas counters. Main components of the reaction background, which must be taken account of, are background due to irradiation with primary and scattered neutrons of telescope details, background of random coincidences and background from scattered neutrons. The following corrections are introduced to the apparatus spectrum obtained after subtraction of all the spectrum kinds: energy resolution correction for the spectrometer, apparatus line stub correction for the spectrometer, energy loss correction for gas filling the telescope, energy loss and particle absorption corrections for the target [ru

  16. Study of the Production and Decay Properties of using the OMEGA Spectrometer

    CERN Multimedia

    2002-01-01

    The aim of the experiment is to study beauty particles production and decay in a 350~GeV negative pion beam, using a scintillating optical fibre target in conjunction with a silicon microstrip telescope and the Omega spectrometer.\\\\ \\\\ A multiparticle high $p _{T}$ ~trigger together with an impact parameter trigger and muon selection is employed to enrich the $ B \\bar{B} $ ~signal. An automatic system of reconstructing tracks and vertices has been developed to select beauty decay topologies. A 50~day run should yield about 200~ $ B \\bar{B} $ events per nanobarn. \\\\ \\\\ Fast, high resolution micro-tracking has been realized with the scintillating fibre detector, but some technical problems are still under study. \\\\ \\\\ The collaboration is continuing with the R&D programme and at the same time has joined with the WA82 collaboration in a common proposal to study beauty production and decay with the Omega spectrometer using the better-known technique of silicon microstrip (this is approved as WA92).

  17. Resolution of the VESUVIO spectrometer for High-energy Inelastic Neutron Scattering experiments

    International Nuclear Information System (INIS)

    Imberti, S.; Andreani, C.; Garbuio, V.; Gorini, G.; Pietropaolo, A.; Senesi, R.; Tardocchi, M.

    2005-01-01

    New perspectives for epithermal neutron spectroscopy have been opened up as a result of the development of the Resonance Detector and its use on inverse geometry time-of-flight spectrometers at spallation sources. A special application of the Resonance Detector is the Very Low Angle Detector Bank (VLAD) for the VESUVIO spectrometer at ISIS, operating in the angular range 1 deg. -1 ) and high energy (unlimited) transfer -bar ω>500meV, a regime so far inaccessible to experimental studies on condensed matter systems. The HINS measurements complement the Deep Inelastic Neutron Scattering (DINS) measurements performed on VESUVIO in the high wavevector q(20A -1 -1 ) and high energy transfer (-bar ω>1eV), where the short-time single-particle dynamics can be sampled. This paper will revise the main components of the resolution for HINS measurements of VESUVIO. Instrument performances and examples of applications for neutron scattering processes at high energy and at low wavevector transfer are discussed

  18. Study and realization of a detection apparatus for the Grenoble magnetic spectrometer

    International Nuclear Information System (INIS)

    Burel, J.-P.

    1975-01-01

    Two multiwire proportional chambers were studied for a magnetic spectrometer. The first one is constructed for visualization of the attenuated beam at the place of the target. The sensitive area is 4x4cm 2 . The anode wires are 0.020mm diameter, gold plated tungsten, 2mm spaced. Each cathode plane wires are connected to a 20 units-5ns delay line. The planes are 3.2mm spaced. The spatial resolution obtained is better than 0.3mm. The second chamber is placed at the focal plane of the spectrometer. The sensitive area is 50x5cm 2 . The horizontal position detection uses an original charge-division system with four chains of capacitors. The particle position results of the center of gravity calculus of different amplified pulses. An electronic circuit has been constructed and the result is directly stored in a memory unit. The spatial resolution obtained is 0.4mm [fr

  19. Development of the DAQ System of Triple-GEM Detectors for the CMS Muon Spectrometer Upgrade at LHC

    CERN Document Server

    AUTHOR|(INSPIRE)INSPIRE-00387583

    The Gas Electron Multiplier (GEM) upgrade project aims at improving the performance of the muon spectrometer of the Compact Muon Solenoid (CMS) experiment which will suffer from the increase in luminosity of the Large Hadron Collider (LHC). After a long technical stop in 2019-2020, the LHC will restart and run at a luminosity of 2 × 1034 cm−2 s−1, twice its nominal value. This will in turn increase the rate of particles to which detectors in CMS will be exposed and affect their performance. The muon spectrometer in particular will suffer from a degraded detection efficiency due to the lack of redundancy in its most forward region. To solve this issue, the GEM collaboration proposes to instrument the first muon station with Triple-GEM detectors, a technology which has proven to be resistant to high fluxes of particles. Within the GEM collaboration, the Data Acquisition (DAQ) subgroup is in charge of the development of the electronics and software of the DAQ system of the detectors. This thesis presents th...

  20. Construction of an inexpensive molecular iodine spectrometer using a self-developed Pohl wavemeter around 670 nm wavelength

    International Nuclear Information System (INIS)

    Barthwal, Sachin; Vudayagiri, Ashok

    2015-01-01

    We describe the construction of an inexpensive iodine spectrometer with a homemade iodine vapour cell and a self-developed wavemeter based on the Pohl interferometer, around the 670 nm wavelength. This can be easily realized in an undergraduate teaching laboratory to demonstrate the use of a diode laser interferometer using a Pohl interferometer and measurement of the wavelength using image processing techniques. A visible alternative to the infrared diode lasers, the 670 nm diode laser used here gives undergraduate students a chance to perform comprehensive though illustrative atomic physics experiments including the Zeeman effect, the Hanle effect, and the magneto-optic rotation effect with a little tweaking in the present spectrometer. The advantage of the spectrometer is its ease of construction with readily available optics, electronics, evacuation and glass-blowing facilities, and easy analysis algorithm to evaluate the wavelength. The self-developed algorithm of raster scanning and circular averaging gives the researcher insight into the basics of image processing techniques. Resolution approaching 0.5 nm can be easily achieved using such a simple setup. (paper)

  1. High resolution solar soft X-ray spectrometer

    International Nuclear Information System (INIS)

    Zhang Fei; Wang Huanyu; Peng Wenxi; Liang Xiaohua; Zhang Chunlei; Cao Xuelei; Jiang Weichun; Zhang Jiayu; Cui Xingzhu

    2012-01-01

    A high resolution solar soft X-ray spectrometer (SOX) payload onboard a satellite is developed. A silicon drift detector (SDD) is adopted as the detector of the SOX spectrometer. The spectrometer consists of the detectors and their readout electronics, a data acquisition unit and a payload data handling unit. A ground test system is also developed to test SOX. The test results show that the design goals of the spectrometer system have been achieved. (authors)

  2. Heterogeneous oxidation of saturated organic aerosols by hydroxyl radicals: uptake kinetics, condensed-phase products, and particle size change

    Directory of Open Access Journals (Sweden)

    I. J. George

    2007-08-01

    Full Text Available The kinetics and reaction mechanism for the heterogeneous oxidation of saturated organic aerosols by gas-phase OH radicals were investigated under NOx-free conditions. The reaction of 150 nm diameter Bis(2-ethylhexyl sebacate (BES particles with OH was studied as a proxy for chemical aging of atmospheric aerosols containing saturated organic matter. An aerosol reactor flow tube combined with an Aerodyne time-of-flight aerosol mass spectrometer (ToF-AMS and scanning mobility particle sizer (SMPS was used to study this system. Hydroxyl radicals were produced by 254 nm photolysis of O3 in the presence of water vapour. The kinetics of the heterogeneous oxidation of the BES particles was studied by monitoring the loss of a mass fragment of BES with the ToF-AMS as a function of OH exposure. We measured an initial OH uptake coefficient of γ0=1.3 (±0.4, confirming that this reaction is highly efficient. The density of BES particles increased by up to 20% of the original BES particle density at the highest OH exposure studied, consistent with the particle becoming more oxidized. Electrospray ionization mass spectrometry analysis showed that the major particle-phase reaction products are multifunctional carbonyls and alcohols with higher molecular weights than the starting material. Volatilization of oxidation products accounted for a maximum of 17% decrease of the particle volume at the highest OH exposure studied. Tropospheric organic aerosols will become more oxidized from heterogeneous photochemical oxidation, which may affect not only their physical and chemical properties, but also their hygroscopicity and cloud nucleation activity.

  3. Accurate virus quantitation using a Scanning Transmission Electron Microscopy (STEM) detector in a scanning electron microscope.

    Science.gov (United States)

    Blancett, Candace D; Fetterer, David P; Koistinen, Keith A; Morazzani, Elaine M; Monninger, Mitchell K; Piper, Ashley E; Kuehl, Kathleen A; Kearney, Brian J; Norris, Sarah L; Rossi, Cynthia A; Glass, Pamela J; Sun, Mei G

    2017-10-01

    A method for accurate quantitation of virus particles has long been sought, but a perfect method still eludes the scientific community. Electron Microscopy (EM) quantitation is a valuable technique because it provides direct morphology information and counts of all viral particles, whether or not they are infectious. In the past, EM negative stain quantitation methods have been cited as inaccurate, non-reproducible, and with detection limits that were too high to be useful. To improve accuracy and reproducibility, we have developed a method termed Scanning Transmission Electron Microscopy - Virus Quantitation (STEM-VQ), which simplifies sample preparation and uses a high throughput STEM detector in a Scanning Electron Microscope (SEM) coupled with commercially available software. In this paper, we demonstrate STEM-VQ with an alphavirus stock preparation to present the method's accuracy and reproducibility, including a comparison of STEM-VQ to viral plaque assay and the ViroCyt Virus Counter. Copyright © 2017 The Authors. Published by Elsevier B.V. All rights reserved.

  4. Crystal-diffraction spectrometer of increased efficiency

    International Nuclear Information System (INIS)

    Saukov, A.I.; Gornitsyn, G.A.; Morozov, N.A.

    1985-01-01

    The geometry of the spectrometer is illustrated in this paper. An attempt is made to achieve optimal design of the spectrometer by finding the coefficient of reflection of the gamma radiation from the various Ge planes. In these experiments, the Du Mond design was used in the spectrometer. Illustrations are provided to explain dependence of the relative efficiency upon the energy of the gamma quanta

  5. Research in elementary particle physics: Technical progress report, June 1, 1986-May 31, 1987

    International Nuclear Information System (INIS)

    Kirsch, L.E.; Schnitzer, H.J.; Abbott, L.F.; Bensinger, J.R.; Blocker, C.A.

    1987-01-01

    Work is reported in the areas of: design, construction, and testing of components of the CDF, including shower counters, electronics, and electron identification algorithms; contributions to the design and construction of the Brookhaven MultiParticle Spectrometer; search for charm and K*'s and baryonium; measurement of differential cross section and polarization in the Lambda-antiLambda channel; a study of Xi states which measured the Xi asymmetry parameter; and dibaryon searches using the Brookhaven Hypernuclear Spectrometer. Theoretical efforts are reported in the areas of string theory, the Skyrme model applied to elementary particle phenomenology, quantum field theory, cosmology, galaxy formation, supernova 187A, field theory in curved space-times, and spin-glasses

  6. Scanning electron microscopy applied to the study of solid pollution particles deposited on monumental stone; La microscopia electronica de barrido aplicada al estudio de particulas solidas de contaminacion depositadas sobre la piedra momumental

    Energy Technology Data Exchange (ETDEWEB)

    Diaz-Pache, F.; Alonso, F.J.; Esbert, R.M. [Departamento de Geologia, Universidad de Oviedo (Spain)

    1996-06-01

    Solid pollution particles play an important role in the decay of monumental stone. Scanning electron microscopy (SEM) in conjunction with microanalysis (EDX) are a very valuable study tool. In the present paper, particular attention is paid to sample collection and preparation. Examples of particles providing information on the source of decay are submitted. (Author) 9 refs.

  7. MEMS based digital transform spectrometers

    Science.gov (United States)

    Geller, Yariv; Ramani, Mouli

    2005-09-01

    Earlier this year, a new breed of Spectrometers based on Micro-Electro-Mechanical-System (MEMS) engines has been introduced to the commercial market. The use of these engines combined with transform mathematics, produces powerful spectrometers at unprecedented low cost in various spectral regions.

  8. 3m Vacuum Ultraviolet Spectrometer with Optical Multichannel Detector

    International Nuclear Information System (INIS)

    Martin, P.; Peraza, C.; Blanco, F.; Campos, J.

    1993-01-01

    This paper describes the design and the performance of a normal incidence vacuum ultraviolet spectrometer, for the 300-2400 A spectral range. It is provided with a multichannel detection system. The monochromator is original design and it has been built at CIEMAT. It is equipped with a 3 m concave holographic grating with 2400 grooves/mm. The multichannel detector consists of a windowless double microchannel plate / phosphor screen image intensifier, coupled by fiber optic to a 1024 elements self-scanning linear photodiode array. The output from the array is digitized by a 12-bit analog to digital converter and stored in a computer, for its later analysis. The necessary software to store and display data has been developed. (Author) 18 refs

  9. Neutron activation analysis of small particles brought back from the asteroid Itokawa by the space probe Hayabusa

    International Nuclear Information System (INIS)

    Ebihara, Mitsuru

    2013-01-01

    The probe in the title launched in May 2003, landed on the asteroid 25143 (Itokawa) to collect the surface material, and returned to the desert of Australia in June 2010. The material carried in Japan Aerospace Exploration Agency (JAXA) was found to be >1,500 particles of extraterrestrial origin. This paper reports the results of activation analysis of a part of particles for the purpose of characterizing the elemental composition. The size of particles was mostly <100 mc-m and the mass, several 10s mc-g. The experiment was performed preliminarily on Kilabo meteorite using Kyoto University Research Reactor (KURR) as a neutron source, and then on 1 Itokawa particle named RA-QD02-0049, which was activated for 19 hr. The cooled particle was found to be split mainly in 2 parts (0049-1 and -2), which were subjected to analysis of gamma ray with Ge semiconductor detector in the KURR Institute and Kanazawa University. Analysis revealed that the 2 particles contained 8 elements of Na, Sc, Cr, Fe, Co, Ni, Zn and Ir, which were then quantitated with similarly neutron irradiated Allende meteorite, basalt JB-1 and highly purified Fe, and with previous findings by scanning electron microscope with energy dispersive X-ray spectrometer (SEM-EDX) showing the Itokawa particle was an olivine. Finally, 0049-1 and -2 were found to be of mass of 1.6 and 1.5 mc-g, respectively, based on which the calculated contents of the 8 elements revealed that they were homogeneously existed in the Itokawa particle. Comparison of elemental composition of the particle with those of various intra- and extra-terrestrial rocks and meteorites suggested that Itokawa had a feature of elements aggregated at the early stage after formation of the solar system 4.5 billion years ago. (T.T.)

  10. A review of central production experiments at the CERN Omega spectrometer

    CERN Document Server

    Kirk, Andrew

    2014-01-01

    The non-Abelian nature of QCD suggests that particles that have a gluon constituent, such as glueballs or hybrids, should exist. This paper presents a study of central meson production in the fixed target experiments WA76, WA91 and WA102 at the CERN Omega spectrometer at centre-of-mass energies of $\\sqrt{s} = 12.7$, 23.8 and 29~GeV. A study of the resonance production cross section as a function of $\\sqrt{s}$ shows which states are compatible with being produced by Double Pomeron Exchange (DPE). In these DPE processes, the difference in the transverse momentum between the exchange particles ($dP_T)$ can be used to select out known $q\\overline q$ states from non-$q \\overline q$ candidates. The distribution of the azimuthal angle ($\\phi$) between the two exchange particles suggests that the Pomeron transforms like a non-conserved vector current. Finally there is evidence from an analysis of the the decay modes of the scalar states observed, that the lightest scalar glueball manifests itself through the mixing w...

  11. Direct observation and analysis of york-shell materials using low-voltage high-resolution scanning electron microscopy: Nanometal-particles encapsulated in metal-oxide, carbon, and polymer

    Directory of Open Access Journals (Sweden)

    Shunsuke Asahina

    2014-11-01

    Full Text Available Nanometal particles show characteristic features in chemical and physical properties depending on their sizes and shapes. For keeping and further enhancing their features, the particles should be protected from coalescence or degradation. One approach is to encapsulate the nanometal particles inside pores with chemically inert or functional materials, such as carbon, polymer, and metal oxides, which contain mesopores to allow permeation of only chemicals not the nanometal particles. Recently developed low-voltage high-resolution scanning electron microscopy was applied to the study of structural, chemical, and electron state of both nanometal particles and encapsulating materials in york-shell materials of Au@C, Ru/Pt@C, Au@TiO2, and Pt@Polymer. Progresses in the following categories were shown for the york-shell materials: (i resolution of topographic image contrast by secondary electrons, of atomic-number contrast by back-scattered electrons, and of elemental mapping by X-ray energy dispersive spectroscopy; (ii sample preparation for observing internal structures; and (iii X-ray spectroscopy such as soft X-ray emission spectroscopy. Transmission electron microscopy was also used for characterization of Au@C.

  12. Electro-Optical Imaging Fourier-Transform Spectrometer

    Science.gov (United States)

    Chao, Tien-Hsin; Zhou, Hanying

    2006-01-01

    An electro-optical (E-O) imaging Fourier-transform spectrometer (IFTS), now under development, is a prototype of improved imaging spectrometers to be used for hyperspectral imaging, especially in the infrared spectral region. Unlike both imaging and non-imaging traditional Fourier-transform spectrometers, the E-O IFTS does not contain any moving parts. Elimination of the moving parts and the associated actuator mechanisms and supporting structures would increase reliability while enabling reductions in size and mass, relative to traditional Fourier-transform spectrometers that offer equivalent capabilities. Elimination of moving parts would also eliminate the vibrations caused by the motions of those parts. Figure 1 schematically depicts a traditional Fourier-transform spectrometer, wherein a critical time delay is varied by translating one the mirrors of a Michelson interferometer. The time-dependent optical output is a periodic representation of the input spectrum. Data characterizing the input spectrum are generated through fast-Fourier-transform (FFT) post-processing of the output in conjunction with the varying time delay.

  13. Design and construction of a hadron calorimeter for the European hybrid spectrometer

    International Nuclear Information System (INIS)

    Schmiedmayer, H.J.

    1983-01-01

    The Intermedia Neutral Particle Calorimeter is an iron (5 cm)-scintillator (0.8 cm) sampling calorimeter. The read-out is done in three groups comprising 4 scintillators separated by 5 cm of iron. The signal can also be used for triggering. The device has been tested for linearity and long-time stability muon-calibrated and inserted into the spectrometer EHS. Finally a simulation model for hadron showers was developed which fits data from the literature in the 20-200 GeV range. (G.Q.)

  14. Rapid monitoring of gaseous fission products in BWRs using a portable spectrometer

    International Nuclear Information System (INIS)

    Yeh, Wei-Wen; Lee, Cheng-Jong; Chen, Chen-Yi; Chung, Chien

    1996-01-01

    Rapid, quantitative determination of gaseous radionuclides is the most difficult task in the field of environmental monitoring for radiation. Although the identification of each gaseous radionuclide is relatively straightforward using its decayed gamma ray as an index, the quantitative measurement is hampered by the time-consuming sample collection procedures, in particular for the radioactive noble gaseous fission products of krypton and xenon. In this work, a field gamma-ray spectrometer consisting of a high-purity germanium detector, portable multichannel anlayzer, and a notebook computer was used to conduct rapid scanning of radioactive krypton and xenon in the air around a nuclear facility

  15. Upgrading a high-throughput spectrometer for high-frequency (<400 kHz) measurements

    Science.gov (United States)

    Nishizawa, T.; Nornberg, M. D.; Den Hartog, D. J.; Craig, D.

    2016-11-01

    The upgraded spectrometer used for charge exchange recombination spectroscopy on the Madison Symmetric Torus resolves emission fluctuations up to 400 kHz. The transimpedance amplifier's cutoff frequency was increased based upon simulations comparing the change in the measured photon counts for time-dynamic signals. We modeled each signal-processing stage of the diagnostic and scanned the filtering frequency to quantify the uncertainty in the photon counting rate. This modeling showed that uncertainties can be calculated based on assuming each amplification stage is a Poisson process and by calibrating the photon counting rate with a DC light source to address additional variation.

  16. Upgrading a high-throughput spectrometer for high-frequency (<400 kHz) measurements

    International Nuclear Information System (INIS)

    Nishizawa, T.; Nornberg, M. D.; Den Hartog, D. J.; Craig, D.

    2016-01-01

    The upgraded spectrometer used for charge exchange recombination spectroscopy on the Madison Symmetric Torus resolves emission fluctuations up to 400 kHz. The transimpedance amplifier’s cutoff frequency was increased based upon simulations comparing the change in the measured photon counts for time-dynamic signals. We modeled each signal-processing stage of the diagnostic and scanned the filtering frequency to quantify the uncertainty in the photon counting rate. This modeling showed that uncertainties can be calculated based on assuming each amplification stage is a Poisson process and by calibrating the photon counting rate with a DC light source to address additional variation.

  17. Upgrading a high-throughput spectrometer for high-frequency (<400 kHz) measurements

    Energy Technology Data Exchange (ETDEWEB)

    Nishizawa, T., E-mail: nishizawa@wisc.edu; Nornberg, M. D.; Den Hartog, D. J. [University of Wisconsin–Madison, Madison, Wisconsin 53706 (United States); Craig, D. [Wheaton College, Wheaton, Illinois 60187 (United States)

    2016-11-15

    The upgraded spectrometer used for charge exchange recombination spectroscopy on the Madison Symmetric Torus resolves emission fluctuations up to 400 kHz. The transimpedance amplifier’s cutoff frequency was increased based upon simulations comparing the change in the measured photon counts for time-dynamic signals. We modeled each signal-processing stage of the diagnostic and scanned the filtering frequency to quantify the uncertainty in the photon counting rate. This modeling showed that uncertainties can be calculated based on assuming each amplification stage is a Poisson process and by calibrating the photon counting rate with a DC light source to address additional variation.

  18. The RITA spectrometer at Risø - design considerations and recent results

    Science.gov (United States)

    Clausen, K. N.; McMorrow, D. F.; Lefmann, K.; Aeppli, G.; Mason, T. E.; Schröder, A.; Issikii, M.; Nohara, M.; Takagi, H.

    In the new cold triple axis spectrometer RITA at Risø we have improved the front end by extensive use of state of the art optical elements and better shielding material. The analyser system is situated in one large open tank and consists of seven individually orientable PG(002) crystal analyser blades, and a 170 mm by 120 mm 2 areas sensitive micro-strip detector. In comparison to the old TAS6 spectrometer we have obtained a factor 2-5 gain in intensity on the sample, a substantially lower background, much more flexibility for optimising the instrument and the possibility to go beyond simple point-by-point inspection. The excellent performance of RITA in the standard TAS mode is exemplified by a study of the dynamics of ≈ 15 nm hematite (α-Fe 2O 3) nano-particles, and utilisation of horizontal and vertical focusing modes to study two dimensional systems is illustrated by a study of the spin fluctuations in the high Tc superconductor La 1.83Sr 0.17CuO 4.

  19. Synthetic neutron camera and spectrometer in JET based on AFSI-ASCOT simulations

    Science.gov (United States)

    Sirén, P.; Varje, J.; Weisen, H.; Koskela, T.; contributors, JET

    2017-09-01

    The ASCOT Fusion Source Integrator (AFSI) has been used to calculate neutron production rates and spectra corresponding to the JET 19-channel neutron camera (KN3) and the time-of-flight spectrometer (TOFOR) as ideal diagnostics, without detector-related effects. AFSI calculates fusion product distributions in 4D, based on Monte Carlo integration from arbitrary reactant distribution functions. The distribution functions were calculated by the ASCOT Monte Carlo particle orbit following code for thermal, NBI and ICRH particle reactions. Fusion cross-sections were defined based on the Bosch-Hale model and both DD and DT reactions have been included. Neutrons generated by AFSI-ASCOT simulations have already been applied as a neutron source of the Serpent neutron transport code in ITER studies. Additionally, AFSI has been selected to be a main tool as the fusion product generator in the complete analysis calculation chain: ASCOT - AFSI - SERPENT (neutron and gamma transport Monte Carlo code) - APROS (system and power plant modelling code), which encompasses the plasma as an energy source, heat deposition in plant structures as well as cooling and balance-of-plant in DEMO applications and other reactor relevant analyses. This conference paper presents the first results and validation of the AFSI DD fusion model for different auxiliary heating scenarios (NBI, ICRH) with very different fast particle distribution functions. Both calculated quantities (production rates and spectra) have been compared with experimental data from KN3 and synthetic spectrometer data from ControlRoom code. No unexplained differences have been observed. In future work, AFSI will be extended for synthetic gamma diagnostics and additionally, AFSI will be used as part of the neutron transport calculation chain to model real diagnostics instead of ideal synthetic diagnostics for quantitative benchmarking.

  20. Simulation of path delay multiplexing-based Fourier transform spectrometer for fiber Bragg grating interrogation.

    Science.gov (United States)

    Chelliah, Pandian; Sahoo, Trilochan; Singh, Sheela; Sujatha, Annie

    2015-10-20

    A Fourier transform spectrometer (FTS) used for interrogating a fiber Bragg grating (FBG) consists of a scanning-type interferometer. The FTS has a broad wavelength range of operation and good multiplexing capability. However, it has poor wavelength resolution and interrogation speed. We propose a modification to the FTS using path delay multiplexing to improve the same. Using this method, spatial resolution and interrogation time can be improved by n times by using n path delays. In this paper, simulation results for n=2, 5 are shown.

  1. Digital Spectrometers for Interplanetary Science Missions

    Science.gov (United States)

    Jarnot, Robert F.; Padmanabhan, Sharmila; Raffanti, Richard; Richards, Brian; Stek, Paul; Werthimer, Dan; Nikolic, Borivoje

    2010-01-01

    A fully digital polyphase spectrometer recently developed by the University of California Berkeley Wireless Research Center in conjunction with the Jet Propulsion Laboratory provides a low mass, power, and cost implementation of a spectrum channelizer for submillimeter spectrometers for future missions to the Inner and Outer Solar System. The digital polyphase filter bank spectrometer (PFB) offers broad bandwidth with high spectral resolution, minimal channel-to-channel overlap, and high out-of-band rejection.

  2. Conversion electrons from high-statistics β-decay measurements with the 8π spectrometer at TRIUMF-ISAC

    Science.gov (United States)

    Garrett, P. E.; Jigmeddorj, B.; Radich, A. J.; Andreoiu, C.; Ball, G. C.; Bangay, J. C.; Bianco, L.; Bildstein, V.; Chagnon-Lessard, S.; Cross, D. S.; Demand, G. A.; Diaz Varela, A.; Dunlop, R.; Finlay, P.; Garnsworthy, A. B.; Green, K. L.; Hackman, G.; Hadinia, B.; Leach, K. G.; Michetti-Wilson, J.; Orce, J. N.; Rajabali, M. M.; Rand, E. T.; Starosta, K.; Sumithrarachchi, C.; Svensson, C. E.; Triambak, S.; Wang, Z. M.; Williams, S. J.; Wood, J. L.; Wong, J.; Yates, S. W.; Zganjar, E. F.

    2016-09-01

    The 8π spectrometer, located at TRIUMF-ISAC, was the world's most powerful spectrometer dedicated to β-decay studies until its decommissioning in early 2014 for replacement with the GRIFFIN array. An integral part of the 8π spectrometer was the Pentagonal Array for Conversion Electron Spectroscopy (PACES) consisting of 5 Si(Li) detectors used for charged-particle detection. PACES enabled both γ - e- and e- - e- coincidence measurements, which were crucial for increasing the sensitivity for discrete e- lines in the presence of large backgrounds. Examples from a 124Cs decay experiment, where the data were vital for the expansion of the 124Cs decay scheme, are shown. With suffcient statistics, measurements of conversion coeffcients can be used to extract the E0 components of Jπ → Jπ transitions for J ≠ 0, which is demonstrated for data obtained in 110In→110Cd decay. With knowledge of the shapes of the states involved, as obtained, for example, from the use of Kumar-Cline shape invariants, the mixing of the states can be extracted.

  3. Superresolution of a compact neutron spectrometer at energies relevant for fusion diagnostics

    International Nuclear Information System (INIS)

    Reginatto, M.; Zimbal, A.

    2011-01-01

    The ability to achieve resolution that is better than the instrument resolution (i.e., superresolution) is well known in optics, where it has been extensively studied. Unfortunately, there are only a handful of theoretical studies concerning superresolution of particle spectrometers, even though experimentalists are familiar with the enhancement of resolution that is achievable when appropriate methods of data analysis are used, such as maximum entropy and Bayesian methods. Knowledge of the superresolution factor is in many cases important. For example, in applications of neutron spectrometry to fusion diagnostics, the temperature of a burning plasma is an important physical parameter which may be inferred from the width of the peak of the neutron energy spectrum, and the ability to determine this width depends on the superresolution factor. Kosarev has derived an absolute limit for resolution enhancement using arguments based on a well known theorem of Shannon. Most calculations of superresolution factors in the literature, however, are based on the assumption of Gaussian, translationally invariant response functions and therefore not directly applicable to neutron spectrometers which typically have response functions not satisfying these requirements. In this work, we develop a procedure that allows us to overcome these difficulties and we derive estimates of superresolution for liquid scintillator spectrometers of a type commonly used for neutron measurements. Theoretical superresolution factors are compared to experimental results.

  4. A large-acceptance Bragg curve spectrometer with a longitudinal electric field and a segmented anode

    International Nuclear Information System (INIS)

    Farrar, K.A.; Hasan, A.T.; Prosser, F.W.; Sanders, S.J.; Henderson, D.J.

    1994-01-01

    A large-acceptance Bragg curve spectrometer with a longitudinal electron collection field and a segmented anode has been constructed and tested. The effects on the charge resolution of the entrance angle and entrance position of the incident particle have been studied. Simulations have been done in order to isolate the contribution to the overall detector performance of the signal-shaping electronics from that of the intrinsic design of the detector. ((orig.))

  5. Calibration of Solar Radio Spectrometer of the Purple Mountain Observatory

    Science.gov (United States)

    Lei, LU; Si-ming, LIU; Qi-wu, SONG; Zong-jun, NING

    2015-10-01

    Calibration is a basic and important job in solar radio spectral observations. It not only deduces the solar radio flux as an important physical quantity for solar observations, but also deducts the flat field of the radio spectrometer to display the radio spectrogram clearly. In this paper, we first introduce the basic method of calibration based on the data of the solar radio spectrometer of Purple Mountain Observatory. We then analyze the variation of the calibration coefficients, and give the calibrated results for a few flares. These results are compared with those of the Nobeyama solar radio polarimeter and the hard X-ray observations of the RHESSI (Reuven Ramaty High Energy Solar Spectroscopic Imager) satellite, it is shown that these results are consistent with the characteristics of typical solar flare light curves. In particular, the analysis on the correlation between the variation of radio flux and the variation of hard X-ray flux in the pulsing phase of a flare indicates that these observations can be used to study the relevant radiation mechanism, as well as the related energy release and particle acceleration processes.

  6. Escherichia coli pyruvate dehydrogenase complex: particle masses of the complex and component enzymes measured by scanning transmission electron microscopy

    International Nuclear Information System (INIS)

    CaJacob, C.A.; Frey, P.A.; Hainfeld, J.F.; Wall, J.S.; Yang, H.

    1985-01-01

    Particle masses of the Escherichia coli pyruvate dehydrogenase (PDH) complex and its component enzymes have been measured by scanning transmission electron microscopy (STEM). The particle mass of PDH complex measured by STEM is 5.28 X 10(6) with a standard deviation of 0.40 X 10(6). The masses of the component enzymes are 2.06 X 10(5) for the dimeric pyruvate dehydrogenase (E1), 1.15 X 10(5) for dimeric dihydrolipoyl dehydrogenase (E3), and 2.20 X 10(6) for dihydrolipoyl transacetylase (E2), the 24-subunit core enzyme. STEM measurements on PDH complex incubated with excess E3 or E1 failed to detect any additional binding of E3 but showed that the complex would bind additional E1 under forcing conditions. The additional E1 subunits were bound too weakly to represent binding sites in an isolated or isolable complex. The mass measurements by STEM are consistent with the subunit composition 24:24:12 when interpreted in the light of the flavin content of the complex and assuming 24 subunits in the core enzyme (E2)

  7. An active pixels spectrometers for neutronic fields metrology

    International Nuclear Information System (INIS)

    Taforeau, Julien

    2013-01-01

    The fundamental metrology is responsible for the sustainability of the measurement systems and handles to supply the reference standards. Concerning the metrology of ionizing radiations and, in particular the neutron metrology, detectors standards are used to characterize reference fields, in terms of energy and fluence. The dosimeters or particle detectors are calibrated on these reference fields. This thesis presents the development of a neutron spectrometer neutron candidate to the status of primary standard for the characterization of neutron fields in the range from 5 to 20 MeV. The spectrometer uses the recoil proton telescope as detection principle; the CMOS technology, through three sensor positions, is taking advantage to realize the tracking of protons. A Si(Li) detector handles the measure of the residual proton energy. The device simulations, realized under MCNPX, allow to estimate its performances and to validate the neutron energy reconstruction. An essential step of characterization of the telescope elements and in particular of CMOS sensors is also proposed to guarantee the validity of posterior experimental measurements. The tests realized as well in mono-energy fields as in radionuclide source show the very good performances of the system. The quantification of uncertainties indicates an energy estimation with 1.5 % accuracy and a resolution of less than 6 %. The fluence measurement is performed with an uncertainty about 4 to 6%. (author)

  8. Ion mobility spectrometer / mass spectrometer (IMS-MS).

    Energy Technology Data Exchange (ETDEWEB)

    Hunka Deborah Elaine; Austin, Daniel E.

    2005-07-01

    The use of Ion Mobility Spectrometry (IMS) in the Detection of Contraband Sandia researchers use ion mobility spectrometers for trace chemical detection and analysis in a variety of projects and applications. Products developed in recent years based on IMS-technology include explosives detection personnel portals, the Material Area Access (MAA) checkpoint of the future, an explosives detection vehicle portal, hand-held detection systems such as the Hound and Hound II (all 6400), micro-IMS sensors (1700), ordnance detection (2500), and Fourier Transform IMS technology (8700). The emphasis to date has been on explosives detection, but the detection of chemical agents has also been pursued (8100 and 6400). Combining Ion Mobility Spectrometry (IMS) with Mass Spectrometry (MS) is described. The IMS-MS combination overcomes several limitations present in simple IMS systems. Ion mobility alone is insufficient to identify an unknown chemical agent. Collision cross section, upon which mobility is based, is not sufficiently unique or predictable a priori to be able to make a confident peak assignment unless the compounds present are already identified. Molecular mass, on the other hand, is much more readily interpreted and related to compounds. For a given compound, the molecular mass can be determined using a pocket calculator (or in one's head) while a reasonable value of the cross-section might require hours of computation time. Thus a mass spectrum provides chemical specificity and identity not accessible in the mobility spectrum alone. In addition, several advanced mass spectrometric methods, such as tandem MS, have been extensively developed for the purpose of molecular identification. With an appropriate mass spectrometer connected to an ion mobility spectrometer, these advanced identification methods become available, providing greater characterization capability.

  9. Deflection of high energy channeled charged particles by elastically bent silicon single crystals

    International Nuclear Information System (INIS)

    Gibson, W.M.; Kim, I.J.; Pisharodoy, M.; Salman, S.M.; Sun, C.R.; Wang, G.H.; Wijayawardana, R.; Forster, J.S.; Mitchell, I.V.; Baker, S.I.; Carrigan, R.A. Jr.; Toohig, T.E.; Avdeichikov, V.V.; Ellison, J.A.; Siffert, P.

    1984-01-01

    An experiment has been carried out to observe the deflection of charged particles by planar channeling in bent single crystals of silicon for protons with energy up to 180 GeV. Anomolous loss of particles from the center point of a three point bending apparatus was observed at high incident particle energy. This effect has been exploited to fashion a 'dechanneling spectrometer' to study dechanneling effects due to centripital displacement of channeled particle trajectories in a bent crystal. The bending losses generally conform to the predictions of calculations based on a classical model. (orig.)

  10. Combined raman spectrometer/laser-induced breakdown spectrometer design concept

    Science.gov (United States)

    Bazalgette Courrèges-Lacoste, Gregory; Ahlers, Berit; Boslooper, Erik; Rull-Perez, Fernando; Maurice, Sylvestre

    2017-11-01

    Amongst the different instruments that have been preselected to be on-board the Pasteur payload on ExoMars is the Raman/ Laser Induced Breakdown Spectroscopy (LIBS) instrument. Raman spectroscopy and LIBS will be integrated into a single instrument sharing many hardware commonalities. An international team under the lead of TNO has been gathered to produce a design concept for a combined Raman Spectrometer/ LIBS Elegant Bread-Board (EBB). The instrument is based on a specifically designed extremely compact spectrometer with high resolution over a large wavelength range, suitable for both Raman spectroscopy and LIBS measurements. Low mass, size and resources are the main drivers of the instrument's design concept. The proposed design concept, realization and testing programme for the combined Raman/ LIBS EBB is presented as well as background information on Raman and LIBS.

  11. A multiple-orbit time-of-flight mass spectrometer based on a low energy electrostatic storage ring

    Science.gov (United States)

    Sullivan, M. R.; Spanjers, T. L.; Thorn, P. A.; Reddish, T. J.; Hammond, P.

    2012-11-01

    The results are presented for an electrostatic storage ring, consisting of two hemispherical deflector analyzers (HDA) connected by two separate sets of cylindrical lenses, used as a time-of-flight mass spectrometer. Based on the results of charged particle simulations and formal matrix model, the Ion Storage Ring is capable of operating with multiple stable orbits, for both single and multiply charged ions simultaneously.

  12. NQR spectrometer controlled by a computer

    International Nuclear Information System (INIS)

    Stoican, Ovidiu

    2002-01-01

    Nuclear quadrupole resonance (NQR) is one of the sensitive methods for studying physical and chemical properties of a substance, such as chemical composition, molecular structure, molecular motion and electronic environment. The specifications of the research project require the use of a nuclear quadrupole resonance spectrometer. Design and performances of a pulsed nuclear quadrupole resonance spectrometer prototype covering the range 1-10 MHz are presented. The pulsed NQR method offers considerably higher sensitivity than either the marginal oscillator or super-regenerative methods. Strong echoes are often observed directly with an oscilloscope or a simple receiver. The method allows us to observe two signal categories: free induction decay (fid) and echoes. The block diagram of the pulsed nuclear quadrupole resonance spectrometer is shown. All operations performed by the spectrometer are controlled by a computer. The scanning frequency range, amplitude and width of the RF pulse, additional magnetic field and sample temperature can be controlled by the software. Also it is possible to improve the signal-to-noise ratio using digital filtering applied to the data stored. Automatic operation eliminates operator skill and uncertainty of manual operation. The NQR spectrometer control software is a stand alone executable file, runs on Windows 95/98 platform and does not require the existence of another software package. A graphical interface allows to user an easy control over the spectrometer operations. All measured parameters by the control system interface are saved in the standard data files and can be processed further. The design is readily adaptable for other applications. The sample is contained within an aluminum cylindrical case. The upper end cap of the case can be removed and it allows introducing the sample. On the upper end cap RF and main temperature sensor connector are placed. On the internal side of the bottom end cap a thermoelectric cooler (MELCOR

  13. Modification, calibration, and performance of the Ultra-High Sensitivity Aerosol Spectrometer for particle size distribution and volatility measurements during the Atmospheric Tomography Mission (ATom airborne campaign

    Directory of Open Access Journals (Sweden)

    A. Kupc

    2018-01-01

    Full Text Available Atmospheric aerosol is a key component of the chemistry and climate of the Earth's atmosphere. Accurate measurement of the concentration of atmospheric particles as a function of their size is fundamental to investigations of particle microphysics, optical characteristics, and chemical processes. We describe the modification, calibration, and performance of two commercially available, Ultra-High Sensitivity Aerosol Spectrometers (UHSASs as used on the NASA DC-8 aircraft during the Atmospheric Tomography Mission (ATom. To avoid sample flow issues related to pressure variations during aircraft altitude changes, we installed a laminar flow meter on each instrument to measure sample flow directly at the inlet as well as flow controllers to maintain constant volumetric sheath flows. In addition, we added a compact thermodenuder operating at 300 °C to the inlet line of one of the instruments. With these modifications, the instruments are capable of making accurate (ranging from 7 % for Dp < 0.07 µm to 1 % for Dp > 0.13 µm, precise (< ±1.2 %, and continuous (1 Hz measurements of size-resolved particle number concentration over the diameter range of 0.063–1.0 µm at ambient pressures of > 1000 to 225 hPa, while simultaneously providing information on particle volatility.We assessed the effect of uncertainty in the refractive index (n of ambient particles that are sized by the UHSAS assuming the refractive index of ammonium sulfate (n =  1.52. For calibration particles with n between 1.44 and 1.58, the UHSAS diameter varies by +4/−10 % relative to ammonium sulfate. This diameter uncertainty associated with the range of refractive indices (i.e., particle composition translates to aerosol surface area and volume uncertainties of +8.4/−17.8 and +12.4/−27.5 %, respectively. In addition to sizing uncertainty, low counting statistics can lead to uncertainties of < 20 % for aerosol surface area and < 30

  14. A Scanning scheimpflug lidar system developed for urban pollution monitoring

    Science.gov (United States)

    Yang, Yang; Guan, Peng; Mei, Liang

    2018-04-01

    A scanning Scheimpflug lidar system based on the Scheimpflug principle has been developed by employing a high power multimode 808 nm laser diode and a highly integrated CMOS sensor in Dalian University of Technology, Dalian, Northern China. Atmospheric scanning measurements in urban area were performed for the studies of particle emission sources.

  15. Analogue particle identifier and test unit for automatic measuring of errors

    International Nuclear Information System (INIS)

    Boden, A.; Lauch, J.

    1979-04-01

    A high accuracy analogue particle identifier is described. The unit is used for particle identification or data correction of experimental based errors in magnetic spectrometers. Signals which are proportional to the energy, the time-of-flight or the position of absorption of the particles are supplied to an analogue computation circuit (multifunction converter). Three computation functions are available for different applications. The output of the identifier produces correction signals or pulses whose amplitudes are proportional to the mass of the particles. Particle identification and data correction can be optimized by the adjustment of variable parameters. An automatic test unit has been developed for adjustment and routine checking of particle identifiers. The computation functions can be tested by this unit with an accuracy of 1%. (orig.) [de

  16. Recent ion optics and mass spectrometers

    International Nuclear Information System (INIS)

    Matsuda, Hisashi

    1976-01-01

    The establishment of the third order approximation method for computing the orbit of the ion optical system for mass spectrometers and the completion of its computer program are reported. A feature of this orbit computation is in that the effect of the fringing field can be considered with the accuracy of third order approximation. Several new ion optical systems for mass spectrometers have been proposed by using such orbit computing programs. Brief explanation and the description on the future prospect and problems are made on the following items: the vertual image double focusing mass spectrometer, the second order double focusing mass spectrometer, the E x B superposed field mass spectrometer, and the apparatus with a cylindrical electric field and Q-lens. In the E x B superposed field with Matsuda plates, if the magnetic field is generated by an electromagnet instead of a permanent magnet, the dispersion of mass and energy can be changed at will. The Matsuda plates are known as the auxiliary electrodes positioned at the top and bottom of a cylindrical capacitor. Utilizing those characteristics, a zoom spectrometer can be made, with which only a necessary part of mass spectra can be investigated in detail, but the whole spectra are investigated roughly. In addition, the distribution of energy can be investigated simultaneously after the separation of ionic mass similarly to the parabola apparatus. (Iwakiri, K.)

  17. Virtual design of the neutron guide for the TOF spectrometer NEAT

    International Nuclear Information System (INIS)

    Izaola, Zunbeltz; Russina, Margarita

    2010-01-01

    We present the results of a virtual design study based on Monte-Carlo neutron ray tracing techniques for the neutron guide of the time of flight (TOF) spectrometer NEAT. We studied several configurations with linearly or elliptically tapered compressors with different degrees of focusing and different guide coatings. The calculations were performed and crosschecked using two software packages which produced similar results. The geometrical arrangement of selected guide components was optimised with the Particle Swarm Optimisation algorithm. The results of the Monte Carlo simulations confirm an expected intensity gain factor of approximately 5, that can be achieved by the optimal configuration.

  18. Virtual design of the neutron guide for the TOF spectrometer NEAT

    Science.gov (United States)

    Izaola, Zunbeltz; Russina, Margarita

    2010-11-01

    We present the results of a virtual design study based on Monte-Carlo neutron ray tracing techniques for the neutron guide of the time of flight (TOF) spectrometer NEAT. We studied several configurations with linearly or elliptically tapered compressors with different degrees of focusing and different guide coatings. The calculations were performed and crosschecked using two software packages which produced similar results. The geometrical arrangement of selected guide components was optimised with the Particle Swarm Optimisation algorithm. The results of the Monte Carlo simulations confirm an expected intensity gain factor of approximately 5, that can be achieved by the optimal configuration.

  19. Neutron spectra measuring by magnetless hadron spectrometer

    International Nuclear Information System (INIS)

    Bayukov, Yu.D.; Buklej, A.E.; Gavrilov, V.B.

    1980-01-01

    The energy resolution, efficiency and background conditions of neutron recording in inclusive nuclear reactions by a magnetless hadron spectrometer (MHS) in the 8-300 MeV energy range. The scheme of apparatus lay-out for measuring neutron recording efficiency is shown. For recording colliding particles with the 3 GeV/c momentum four beam scintillation counters, the latter of which of 30x40 mm dimensions and 1 mm thickness defines the working beam range in the target centre, are used. Targets of the 80 mm diameter made of C and Pb (2.08 g/cm 2 and 3.04 g/cm 2 thickness, respectively) are located at the 45 deg angle in respect to the beam direction. Secondary particles escaping at the 90 deg angle are recorded by two telescopes of the scintillation counters. For neutron and γ quanta recording the special scintillation detector of the 20 cm thickness encircled by an anticoincidence counter is used. The neutron recording efficiency is determined on the basis of comparison of the neutron production differential cross sections of the π +- 12 C 6 → nX reactions and of proton production in isotopically symmetric reactions π +- 12 C 6 → pX. The experimental data are in good agreement with the calculation data [ru

  20. The TRIUMF low energy pion spectrometer and channel

    International Nuclear Information System (INIS)

    Sobie, R.J.; Drake, T.E.; Barnett, B.M.; Erdman, K.L.; Gyles, W.; Johnson, R.R.; Roser, H.W.; Tacik, R.; Blackmore, E.W.; Gill, D.R.

    1983-08-01

    A low energy pion spectrometer has been developed for use with the TRIUMF M13 pion channel. The combined channel and spectrometer resolution is presently 1.1 MeV at T = 50 MeV. This is limited by the amount of gas and detector material in the spectrometer in addition to the inherent resolution of the channel. Improvements to both the spectrometer and channel are discussed

  1. Contribution to the study of aerosol aerodynamic behaviour - development of a diffusional and inertial spectrometer (SDI 2000)

    International Nuclear Information System (INIS)

    Diouri, M.

    1987-09-01

    A theoretical and experimental study of cascade impactor and particle diffusion on granular beds was carried out. It resulted in the development of a diffusional and inertial spectrometer (SDI 2000) covering a large particle size range (0.0075 - 15 μm). The second part of the study is devoted to an overview on data reduction and to a comparative study of linear, non-linear and simulation inversion methods adapted to cascade impactors. The inversion problem for SDI 2000 was solved. Finally, the particle size distributions of Diesel exhausts was determined. The possibility to characterize a radioactive aerosol with SDI 20000 was demonstrated, and the results of dust sampling with SDI 2000 inside the JET vessel (Joint European Torus) are presented [fr

  2. The gamma ray spectrometer GA.SP

    Energy Technology Data Exchange (ETDEWEB)

    Bazzacco, D [Instituto Nazionale di Fisica Nucleare, Sezione di Padova, Padova (Italy)

    1992-08-01

    GA.SP is a general purpose 4{pi} detector array for advanced {gamma}-spectroscopy and, in the same time, a suitable system for reaction mechanism studies. The detector is sited at the LNL Tandem+Linac accelerator and has been built as a joint project of INFN Padova, LNL, Milano and Firenze. The array consists of 40 Compton suppressed HPGe detectors and of a 4{pi} calorimeter composed of 80 BGO crystals. The detector houses a reaction chamber of 34 cm diameter where a charged particles multiplicity filter composed of 40 Si detectors is going to be installed. Evaporation residues produced in the centre of GA.SP can be injected into the recoil mass spectrometer (RMS, named CAMEL) in use at LNL, without the need to remove any of the gamma detectors. The coupled operation of GA.SP, RMS and Si ball will give a unique instrument for identification and study of weak reaction channels. (author). 6 figs.

  3. The gamma ray spectrometer GA.SP

    International Nuclear Information System (INIS)

    Bazzacco, D.

    1992-01-01

    GA.SP is a general purpose 4π detector array for advanced γ-spectroscopy and, in the same time, a suitable system for reaction mechanism studies. The detector is sited at the LNL Tandem+Linac accelerator and has been built as a joint project of INFN Padova, LNL, Milano and Firenze. The array consists of 40 Compton suppressed HPGe detectors and of a 4π calorimeter composed of 80 BGO crystals. The detector houses a reaction chamber of 34 cm diameter where a charged particles multiplicity filter composed of 40 Si detectors is going to be installed. Evaporation residues produced in the centre of GA.SP can be injected into the recoil mass spectrometer (RMS, named CAMEL) in use at LNL, without the need to remove any of the gamma detectors. The coupled operation of GA.SP, RMS and Si ball will give a unique instrument for identification and study of weak reaction channels. (author). 6 figs

  4. A magnetic-lens - mini-orange coincidence spectrometer

    International Nuclear Information System (INIS)

    Bargholtz, C.; Holmberg, L.; Ruus, N.; Tegner, P.E.; Weiss, G.

    1997-04-01

    A coincidence spectrometer consisting of a Gerholm type magnetic lens and a permanent magnet mini-orange spectrometer is described. Electron-electron or electron-positron coincidences may be registered in various angular settings. The spectrometer has been developed mainly to search for anomalous contributions to Bhabha scattering or positrons and is at present used for such studies. 6 refs

  5. Ultra-Wideband Optical Modulation Spectrometer (OMS) Development

    Science.gov (United States)

    Gardner, Jonathan (Technical Monitor); Tolls, Volker

    2004-01-01

    The optical modulation spectrometer (OMS) is a novel, highly efficient, low mass backend for heterodyne receiver systems. Current and future heterodyne receiver systems operating at frequencies up to a few THz require broadband spectrometer backends to achieve spectral resolutions of R approximately 10(exp 5) to 10(exp 6) to carry out many important astronomical investigations. Among these are observations of broad emission and absorption lines from extra-galactic objects at high redshifts, spectral line surveys, and observations of planetary atmospheres. Many of these lines are pressure or velocity broadened with either large half-widths or line wings extending over several GHz. Current backend systems can cover the needed bandwidth only by combining the output of several spectrometers, each with typically up to 1 GHz bandwidth, or by combining several frequency-shifted spectra taken with a single spectrometer. An ultra-wideband optical modulation spectrometer with 10 - 40 GHz bandwidth will enable broadband ob- servations without the limitations and disadvantages of hybrid spectrometers. Spectrometers like the OMS will be important for both ground-based observatories and future space missions like the Single Aperture Far-Infrared Telescope (SAFIR) which might carry IR/submm array heterodyne receiver systems requiring a spectrometer for each array pixel. Small size, low mass and small power consumption are extremely important for space missions. This report summarizes the specifications developed for the OMS and lists already identified commercial parts. The report starts with a review of the principle of operation, then describes the most important components and their specifications which were derived from theory, and finishes with a conclusion and outlook.

  6. Preliminary testing of the Scanning Laser Environmental Airborne Fluorosensor

    International Nuclear Information System (INIS)

    Brown, C.E.; Marois, R.; Fingas, M.F.; Mullin, J.V.

    2000-01-01

    The installation and testing program of the Scanning Laser Environmental Airborne Fluorosensor (SLEAF) on Environment Canada's DC-3 aircraft was described and the capabilities of the new system were presented. SLEAF is a new generation of laser fluorosensor designed to provide prompt reliable detection and mapping of oil pollution in different marine and terrestrial environments. It consists of a high-power excimer laser, high-resolution range-gated intensified diode-array spectrometer, and a pair of variable speed and angular displacement scanning mirrors. SLEAF is capable of detecting narrow bands of oil that can pile up along the high tide lines of beaches and shorelines, including those that contain ice and snow. It also has the added benefit of providing real-time detection. SLEAF will be declared operational for emergency response personnel when the initial test flight program will be completed in the near future. 9 refs., 2 figs

  7. Online differentiation of mineral phase in aerosol particles by ion formation mechanism using a LAAP-TOF single-particle mass spectrometer

    Science.gov (United States)

    Marsden, Nicholas A.; Flynn, Michael J.; Allan, James D.; Coe, Hugh

    2018-01-01

    Mineralogy of silicate mineral dust has a strong influence on climate and ecosystems due to variation in physiochemical properties that result from differences in composition and crystal structure (mineral phase). Traditional offline methods of analysing mineral phase are labour intensive and the temporal resolution of the data is much longer than many atmospheric processes. Single-particle mass spectrometry (SPMS) is an established technique for the online size-resolved measurement of particle composition by laser desorption ionisation (LDI) followed by time-of-flight mass spectrometry (TOF-MS). Although non-quantitative, the technique is able to identify the presence of silicate minerals in airborne dust particles from markers of alkali metals and silicate molecular ions in the mass spectra. However, the differentiation of mineral phase in silicate particles by traditional mass spectral peak area measurements is not possible. This is because instrument function and matrix effects in the ionisation process result in variations in instrument response that are greater than the differences in composition between common mineral phases.In this study, we introduce a novel technique that enables the differentiation of mineral phase in silicate mineral particles by ion formation mechanism measured from subtle changes in ion arrival times at the TOF-MS detector. Using a combination of peak area and peak centroid measurements, we show that the arrangement of the interstitial alkali metals in the crystal structure, an important property in silicate mineralogy, influences the ion arrival times of elemental and molecular ion species in the negative ion mass spectra. A classification scheme is presented that allowed for the differentiation of illite-smectite, kaolinite and feldspar minerals on a single-particle basis. Online analysis of mineral dust aerosol generated from clay mineral standards produced mineral fractions that are in agreement with bulk measurements reported by

  8. Controlling Charged Particles with Inhomogeneous Electrostatic Fields

    Science.gov (United States)

    Herrero, Federico A. (Inventor)

    2016-01-01

    An energy analyzer for a charged-particle spectrometer may include a top deflection plate and a bottom deflection plate. The top and bottom deflection plates may be non-symmetric and configured to generate an inhomogeneous electrostatic field when a voltage is applied to one of the top or bottom deflection plates. In some instances, the top and bottom deflection plates may be L-shaped deflection plates.

  9. Mass analysis of charged aerosol particles in NLC and PMSE during the ECOMA/MASS campaign

    Directory of Open Access Journals (Sweden)

    S. Robertson

    2009-03-01

    Full Text Available MASS (Mesospheric Aerosol Sampling Spectrometer is a multichannel mass spectrometer for charged aerosol particles, which was flown from the Andøya Rocket Range, Norway, through NLC and PMSE on 3 August 2007 and through PMSE on 6 August 2007. The eight-channel analyzers provided for the first time simultaneous measurements of the charge density residing on aerosol particles in four mass ranges, corresponding to ice particles with radii <0.5 nm (including ions, 0.5–1 nm, 1–2 nm, and >3 nm (approximately. Positive and negative particles were recorded on separate channels. Faraday rotation measurements provided electron density and a means of checking charge density measurements made by the spectrometer. Additional complementary measurements were made by rocket-borne dust impact detectors, electric field booms, a photometer and ground-based radar and lidar. The MASS data from the first flight showed negative charge number densities of 1500–3000 cm−3 for particles with radii >3 nm from 83–88 km approximately coincident with PMSE observed by the ALWIN radar and NLC observed by the ALOMAR lidar. For particles in the 1–2 nm range, number densities of positive and negative charge were similar in magnitude (~2000 cm−3 and for smaller particles, 0.5–1 nm in radius, positive charge was dominant. The occurrence of positive charge on the aerosol particles of the smallest size and predominately negative charge on the particles of largest size suggests that nucleation occurs on positive condensation nuclei and is followed by collection of negative charge during subsequent growth to larger size. Faraday rotation measurements show a bite-out in electron density that increases the time for positive aerosol particles to be neutralized and charged negatively. The larger particles (>3 nm are observed throughout the NLC region, 83–88 km, and the smaller particles are observed primarily at the high end of the range, 86–88 km

  10. Mass analysis of charged aerosol particles in NLC and PMSE during the ECOMA/MASS campaign

    Directory of Open Access Journals (Sweden)

    S. Robertson

    2009-03-01

    Full Text Available MASS (Mesospheric Aerosol Sampling Spectrometer is a multichannel mass spectrometer for charged aerosol particles, which was flown from the Andøya Rocket Range, Norway, through NLC and PMSE on 3 August 2007 and through PMSE on 6 August 2007. The eight-channel analyzers provided for the first time simultaneous measurements of the charge density residing on aerosol particles in four mass ranges, corresponding to ice particles with radii <0.5 nm (including ions, 0.5–1 nm, 1–2 nm, and >3 nm (approximately. Positive and negative particles were recorded on separate channels. Faraday rotation measurements provided electron density and a means of checking charge density measurements made by the spectrometer. Additional complementary measurements were made by rocket-borne dust impact detectors, electric field booms, a photometer and ground-based radar and lidar. The MASS data from the first flight showed negative charge number densities of 1500–3000 cm−3 for particles with radii >3 nm from 83–88 km approximately coincident with PMSE observed by the ALWIN radar and NLC observed by the ALOMAR lidar. For particles in the 1–2 nm range, number densities of positive and negative charge were similar in magnitude (~2000 cm−3 and for smaller particles, 0.5–1 nm in radius, positive charge was dominant. The occurrence of positive charge on the aerosol particles of the smallest size and predominately negative charge on the particles of largest size suggests that nucleation occurs on positive condensation nuclei and is followed by collection of negative charge during subsequent growth to larger size. Faraday rotation measurements show a bite-out in electron density that increases the time for positive aerosol particles to be neutralized and charged negatively. The larger particles (>3 nm are observed throughout the NLC region, 83–88 km, and the smaller particles are observed primarily at the high end of the range, 86–88 km. The second flight into

  11. A facility for low energy charged particle induced reaction studies

    International Nuclear Information System (INIS)

    Vilaithong, T.; Singkarat, S.; Yu, L.D.; Intarasiri, S.; Tippawan, U.

    2000-01-01

    In Chiang Mai, a highly stable low energy ion accelerator (0 - 350 kV) facility is being established. A subnano-second pulsing system will be incorporated into the beam transport line. The detecting system will consist of a time-of-flight charged particle spectrometer and a high resolution gamma-ray system. The new facility will be used in the studies of low energy heavy ion backscattering and charged particle induced cross section measurement in the interests of material characterization and nucleosynthesis. (author)

  12. Influence of synthesis conditions on particle morphology of ...

    Indian Academy of Sciences (India)

    Wintec

    diffraction (XRD), scanning electron microscopy (SEM), and dynamic light scattering (DLS). Cu/ZnO ... Considerable attention has been paid to copper metal nano- particles .... And also energy dispersive scanning (EDS) analyses of sample ...

  13. Charged particle spectra in π-p,π-d and π-C interactions at 38 GeV/c with single-particle high pT trigger

    International Nuclear Information System (INIS)

    Boos, E.G.; Mosienko, A.M.; Baerwolff, H.

    1987-01-01

    Angular momentum distributions of charged secondaries from 38 GeV/c π - p, π - d and π - C interactions triggered on at least one particle with p T >or approx. 1 GeV/c at an 90 deg πN c.m.s angle have been investigated with the spectrometer RISK (a streamer chamber placed into a magnet). Transversal momentum spectra of secondaries in the 0.4-2.4 GeV/c p T -range including triggering particles are quite well fitted with the exponential function for all nuclei studied and for particles of different charges. The azimuthal angle distribution of secondaries (an angle relative to the p T -tilde of the triggering particle) for both trigger-like and trigger-unlike charges is anisotropic, preferring the direction away from the triggering particle. The mean charge distribution of associated particles is discussed. A small fraction of triggering particles is due to neutral strange particle decays. Many Λ 0 -hyperons were detected among those neutral strange triggers

  14. Study of neutron spectrometers for ITER

    Energy Technology Data Exchange (ETDEWEB)

    Kaellne, Jan

    2005-11-15

    A review is presented of the developments in the field of neutron emission spectrometry (NES) which is of relevance for identifying the role of NES diagnostics on ITER and selecting suitable instrumentation. Neutron spectrometers will be part of the ITER neutron diagnostic complement and this study makes a special effort to examine which performance characteristics the spectrometers should possess to provide the best burning plasma diagnostic information together with neutron cameras and neutron yield monitors. The performance of NES diagnostics is coupled to how much interface space can be provided which has lead to an interest to find compact instruments and their NES capabilities. This study assesses all known spectrometer types of potential interest for ITER and makes a ranking of their performance (as demonstrated or projected), which, in turn, are compared with ITER measurement requirements as a reference; the ratio of diagnostic performance to interface cost for different spectrometers is also discussed for different spectrometer types. The overall result of the study is an assessment of which diagnostic functions neutron measurements can provide in burning plasma fusion experiments on ITER and the role that NES can play depending on the category of instrument installed. Of special note is the result that much higher quality diagnostic information can be obtained from neutron measurements with total yield monitors, profile flux cameras and spectrometers when the synergy in the data is considered in the analysis and interpretation.

  15. Occurrence of particle debris field during focused Ga ion beam milling of glassy carbon

    Energy Technology Data Exchange (ETDEWEB)

    Hu Qin [Centre for Industrial Photonics, Institute for Manufacturing, Department of Engineering, University of Cambridge, Alan Reece Building, 17 Charles Babbage Road, Cambridge, CB3 0FS (United Kingdom); O' Neill, William, E-mail: wo207@eng.cam.ac.uk [Centre for Industrial Photonics, Institute for Manufacturing, Department of Engineering, University of Cambridge, Alan Reece Building, 17 Charles Babbage Road, Cambridge, CB3 0FS (United Kingdom)

    2010-08-01

    To explore the machining characteristics of glassy carbon by focused ion beam (FIB), particles induced by FIB milling on glassy carbon have been studied in the current work. Nano-sized particles in the range of tens of nanometers up to 400 nm can often be found around the area subject to FIB milling. Two ion beam scanning modes - slow single scan and fast repetitive scan - have been tested. Fewer particles are found in single patterns milled in fast repetitive scan mode. For a group of test patterns milled in a sequence, it was found that a greater number of particles were deposited around sites machined early in the sequence. In situ EDX analysis of the particles showed that they were composed of C and Ga. The formation of particles is related to the debris generated at the surrounding areas, the low melting point of gallium used as FIB ion source and the high contact angle of gallium on glassy carbon induces de-wetting of Ga and the subsequent formation of Ga particles. Ultrasonic cleaning can remove over 98% of visible particles. The surface roughness (R{sub a}) of FIB milled areas after cleaning is less than 2 nm.

  16. Occurrence of particle debris field during focused Ga ion beam milling of glassy carbon

    International Nuclear Information System (INIS)

    Hu Qin; O'Neill, William

    2010-01-01

    To explore the machining characteristics of glassy carbon by focused ion beam (FIB), particles induced by FIB milling on glassy carbon have been studied in the current work. Nano-sized particles in the range of tens of nanometers up to 400 nm can often be found around the area subject to FIB milling. Two ion beam scanning modes - slow single scan and fast repetitive scan - have been tested. Fewer particles are found in single patterns milled in fast repetitive scan mode. For a group of test patterns milled in a sequence, it was found that a greater number of particles were deposited around sites machined early in the sequence. In situ EDX analysis of the particles showed that they were composed of C and Ga. The formation of particles is related to the debris generated at the surrounding areas, the low melting point of gallium used as FIB ion source and the high contact angle of gallium on glassy carbon induces de-wetting of Ga and the subsequent formation of Ga particles. Ultrasonic cleaning can remove over 98% of visible particles. The surface roughness (R a ) of FIB milled areas after cleaning is less than 2 nm.

  17. Quantification of aggregate grain shape characteristics using 3-D laser scanning technology

    CSIR Research Space (South Africa)

    Mgangira, Martin B

    2013-07-01

    Full Text Available to identify the differences between individual aggregates. It was possible to quantify differences in particle shape characteristics at the small particle scale. The study has demonstrated the advantages of the innovative 3-D laser scanning technology...

  18. Spectrometer for Particle Characterization With a New Multiple-Scattering Theory, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — There are two major commercial types of light-scattering particle size analyzers: Static Light Scattering and Dynamic Light Scattering. They are expensive, delicate,...

  19. Multi-spectrometer calibration transfer based on independent component analysis.

    Science.gov (United States)

    Liu, Yan; Xu, Hao; Xia, Zhenzhen; Gong, Zhiyong

    2018-02-26

    Calibration transfer is indispensable for practical applications of near infrared (NIR) spectroscopy due to the need for precise and consistent measurements across different spectrometers. In this work, a method for multi-spectrometer calibration transfer is described based on independent component analysis (ICA). A spectral matrix is first obtained by aligning the spectra measured on different spectrometers. Then, by using independent component analysis, the aligned spectral matrix is decomposed into the mixing matrix and the independent components of different spectrometers. These differing measurements between spectrometers can then be standardized by correcting the coefficients within the independent components. Two NIR datasets of corn and edible oil samples measured with three and four spectrometers, respectively, were used to test the reliability of this method. The results of both datasets reveal that spectra measurements across different spectrometers can be transferred simultaneously and that the partial least squares (PLS) models built with the measurements on one spectrometer can predict that the spectra can be transferred correctly on another.

  20. [Design of Dual-Beam Spectrometer in Spectrophotometer for Colorimetry].

    Science.gov (United States)

    Liu, Yi-xuan; Yan, Chang-xiang

    2015-07-01

    Spectrophotometers for colorimetry are usually composed of two independent and identical spectrometers. In order to reduce the volume of spectrophotometer for colorimetry, a design method of double-beam spectrometer is put forward. A traditional spectrometer is modified so that a new spectrometer can realize the function of double spectrometers, which is especially suitable for portable instruments. One slit is replaced by the double-slit, than two beams of spectrum can be detected. The working principle and design requirement of double-beam spectrometer are described. A spectrometer of portable spectrophotometer is designed by this method. A toroidal imaging mirror is used for the Czerny-Turner double-beam spectrometer in this paper, which can better correct astigmatism, and prevent the dual-beam spectral crosstalk. The results demonstrate that the double-beam spectrometer designed by this method meets the design specifications, with the spectral resolution less than 10 nm, the spectral length of 9.12 mm, and the volume of 57 mm x 54 mm x 23 mm, and without the dual-beam spectral overlap in the detector either. Comparing with a traditional spectrophotometer, the modified spectrophotometer uses a set of double-beam spectrometer instead of two sets of spectrometers, which can greatly reduce the volume. This design method can be specially applied in portable spectrophotometers, also can be widely applied in other double-beam spectrophotometers, which offers a new idea for the design of dual-beam spectrophotometers.