Sample records for ratio submicron roughness

  1. Light emitting diode with high aspect ratio submicron roughness for light extraction and methods of forming

    Li, Ting


    The surface morphology of an LED light emitting surface is changed by applying a reactive ion etch (RIE) process to the light emitting surface. High aspect ratio, submicron roughness is formed on the light emitting surface by transferring a thin film metal hard-mask having submicron patterns to the surface prior to applying a reactive ion etch process. The submicron patterns in the metal hard-mask can be formed using a low cost, commercially available nano-patterned template which is transferred to the surface with the mask. After subsequently binding the mask to the surface, the template is removed and the RIE process is applied for time duration sufficient to change the morphology of the surface. The modified surface contains non-symmetric, submicron structures having high aspect ratio which increase the efficiency of the device.

  2. Generating Sub-Micron Features On Rough Surfaces Using Optical Trap Assisted Nanopatterning

    Tsai, Yu-Cheng; Fardel, Romain; Arnold, Craig B.


    Near-field intensity enhancement enables laser modification of materials with feature sizes below the classical diffraction limit. However, the need to maintain close distances between the objective element and the substrate typically limit demonstrations of this technology to flat surfaces, even though there are many cases where the ability to produce sub-micron features on rough or structured surfaces are needed. Here, we show the use of a new technique, optical trap assisted nanopatterning (OTAN), for the production of nanoscale features on rippled substrates. The ability to position a microbead near-field objective close to the surface without the need for active feedback and control allows one to continuously move the bead across a rough surface without sticking. Sub-micron patterning of polyimide is demonstrated on surfaces with 1.1 μm steps showing good uniformity. Finally, the enabling technology allows for straightforward parallelization where multiple patterns can be created simultaneously over surface.

  3. Aerodynamic Properties of Rough Surfaces with High Aspect-Ratio Roughness Elements: Effect of Aspect Ratio and Arrangements

    Sadique, Jasim; Yang, Xiang I. A.; Meneveau, Charles; Mittal, Rajat


    We examine the effect of varying roughness-element aspect ratio on the mean velocity distributions of turbulent flow over arrays of rectangular-prism-shaped elements. Large-eddy simulations (LES) in conjunction with a sharp-interface immersed boundary method are used to simulate spatially-growing turbulent boundary layers over these rough surfaces. Arrays of aligned and staggered rectangular roughness elements with aspect ratio >1 are considered. First the temporally- and spatially-averaged velocity profiles are used to illustrate the aspect-ratio effects. For aligned prisms, the roughness length (z_o) and the friction velocity (u_*) increase initially with an increase in the roughness-element aspect ratio, until the values reach a plateau at a particular aspect ratio. The exact value of this aspect ratio depends on the coverage density. Further increase in the aspect ratio changes neither z_o, u_* nor the bulk flow above the roughness elements. For the staggered cases, z_o and u_* continue to increase for the surface coverage density and the aspect ratios investigated. To model the flow response to variations in roughness aspect ratio, we turn to a previously developed phenomenological volumetric sheltering model (Yang et al., in J Fluid Mech 789:127-165, 2016), which was intended for low to moderate aspect-ratio roughness elements. Here, we extend this model to account for high aspect-ratio roughness elements. We find that for aligned cases, the model predicts strong mutual sheltering among the roughness elements, while the effect is much weaker for staggered cases. The model-predicted z_o and u_* agree well with the LES results. Results show that the model, which takes explicit account of the mutual sheltering effects, provides a rapid and reliable prediction method of roughness effects in turbulent boundary-layer flows over arrays of rectangular-prism roughness elements.

  4. Optimization of the crystallinity of polypropylene/submicronic-talc composites: The role of filler ratio and cooling rate

    A. Makhlouf


    Full Text Available Micronic and submicronic mineral fillers recently appeared as efficient reinforcing agents for polyolefins in addition to the benefit of bypassing the exfoliation/dispersion problem encountered in the case of incorporation of nanoscopic fillers such as clay. Submicronic-talc, designated as μ-talc, belongs to this kind of new fillers. This work was aimed at searching to optimize the crystallinity ratio of isotactic polypropylene in the presence of μ-talc in relation to the filler ratio of the composites and the cooling rate from the melt. In order to highlight the efficiency of the μ-talc on the crystallization of polypropylene comparison has been made with PP composites containing conventional talc particles. The study has been carried out on samples having μ-talc weight fractions covering the range 3–30%. In the context of optimizing the crystallinity ratio of the polypropylene matrix in the composites, calorimetric experiments have been planned using a full factorial design. The results were statistically processed by analysis of the variance via mathematical models for predicting the crystallinity ratio in relation to the cooling rate and the filler ratio. Contour graphs have been plotted to determine the effect of each parameter on crystallinity. The cooling rate proved to have a significantly stronger influence on crystallinity than the type and content of filler.

  5. Characterization and analysis of sub-micron surface roughness of injection moulded microfluidic systems using White Light Interferometry

    Tosello, Guido; Marinello, Francesco; Hansen, Hans Nørgaard


    Surface topography is of great importance in polymer micro fluidics, therefore the replication capability of the process and the surface quality of the tool has to be suitably optimized. In this paper, optical profilometry (white light interferometry, WLI) is implemented for topographical...... have been controlled: temperature of the melt, temperature of the mould and injection speed. Hybrid tooling was employed for the tool making process and two different types of surfaces were obtained within the micro cavity: a finely finished flat surface (average roughness Ra...

  6. On the determination of Poisson's ratio of stressed monolayer and bilayer submicron thick films

    Martins, P; Brida, S; Barbier, D


    In this paper, the bulge test is used to determine the mechanical properties of very thin dielectric membranes. Commonly, this experimental method permits to determine the residual stress (s0) and biaxial Young's modulus (E/(1-u)). Associating square and rectangular membranes with different length to width ratios, the Poisson's ratio (u) can also be determined. LPCVD Si3N4 monolayer and Si3N4/SiO2 bilayer membranes, with thicknesses down to 100 nm, have been characterized giving results in agreement with literature for Si3N4, E = 212 $\\pm$ 14 GPa, s0 = 420 $\\pm$ 8 and u = 0.29.

  7. High-speed microprobe for roughness measurements in high-aspect-ratio microstructures

    Doering, Lutz; Brand, Uwe; Bütefisch, Sebastian; Ahbe, Thomas; Weimann, Thomas; Peiner, Erwin; Frank, Thomas


    Cantilever-type silicon microprobes with an integrated tip and a piezoresistive signal read out have successfully proven to bridge the gap between scanning force microscopy and stylus profilometry. Roughness measurements in high-aspect-ratio microstructures (HARMS) with depths down to 5 mm and widths down to 50 µm have been demonstrated. To improve the scanning speed up to 15 mm s‑1, the wear of the tip has to be reduced. The atomic layer deposition (ALD) technique with alumina (Al2O3) has been tested for this purpose. Repeated wear measurements with coated and uncoated microprobe cantilevers have been carried out on a roughness standard at a speed of 15 mm s‑1. The tip shape and the wear have been measured using a new probing tip reference standard containing rectangular silicon grooves with widths from 0.3 µm to 3 µm. The penetration depth of the microprobe allows one to measure the wear of the tip as well as the tip width and the opening angle of the tip. The roughness parameters obtained on the roughness standard during wear experiments agree well with the reference values measured with a calibrated stylus instrument, nevertheless a small amount of wear still is observable. Further research is necessary in order to obtain wear resistant microprobe tips for non-destructive inspection of microstructures in industry and microform measurements, for example in injection nozzles.

  8. Phase-ratio technique as applied to the assessment of lunar surface roughness

    Kaydash, Vadym; Videen, Gorden; Shkuratov, Yuriy

    Regoliths of atmosphereless celestial bodies demonstrate prominent light backscattering that is common for particulate surfaces. This occurs over a wide range of phase angles and can be seen in the phase function [1]. The slope of the function may characterize the complexity of planetary surface structure. Imagery of such a parameter suggests that information can be obtained about the surface, like variations of unresolved surface roughness and microtopography [2]. Phase-ratio imagery allows one to characterize the phase function slope. This imagery requires the ratio of two co-registered images acquired at different phase angles. One important advantage of the procedure is that the inherent albedo variations of the surface are suppressed, and, therefore, the resulting image is sensitive to the surface structure variation [2,3]. The phase-ratio image characterizes surface roughness variation at spatial scales on the order of the incident wavelengths to that of the image resolution. Applying the phase-ratio technique to ground-based telescope data has allowed us to find new lunar surface formations in the southern part of Oceanus Procellarum. These are suggested to be weak swirls [4]. We also combined the phase-ratio technique with the space-derived photometry data acquired from the NASA Lunar Reconnaissance Orbiter with high spatial resolution. Thus we exploited the method to analyze the sites of Apollo landings and Soviet sample-return missions. Phase-ratio imagery has revealed anomalies of the phase-curve slope indicating a smoothing of the surface microstructure at the sites caused by dust uplifted by the engine jets of the descent and ascent modules [5,6]. Analysis of phase-ratios helps to understand how the regolith properties have been affected by robotic and human activity on the Moon [7,8]. We have demonstrated the use of the method to search for fresh natural disturbances of surface structure, e.g., to detect areas of fresh slumps, accumulated material on

  9. Research on the dynamic response of high-contact-ratio spur gears influenced by surface roughness under EHL condition

    Kang, Huang; Xiong, Yangshou; Wang, Tao; Chen, Qi


    Employing high-contact-ratio (HCR) gear is an effective method of decreasing the load on a single tooth, as well as reducing vibration and noise. While the spindlier tooth leads to greater relative sliding, having more teeth participate in contact at the same time makes the HCR gear more sensitive to the surface quality. Available literature regarding HCR gear primarily investigates the geometrical optimization, load distribution, or efficiency calculation. Limited work has been conducted on the effect of rough surfaces on the dynamic performance of HCR gear. For this reason, a multi-degree-of-freedom (MDOF) model is presented mathematically to characterize the static transmission error based on fractal theory, investigate the relative sliding friction using an EHL-based friction coefficient formula, and detail the time-varying friction coefficient suitable for HCR gear. Based on numerical results, the surface roughness has little influence on system response in terms of the dynamic transmission error but has a large effect on the motion in off-line-of-action (OLOA) direction and friction force. The impact of shaft-bearing stiffness and damping ratio is also explored with results revealing that a greater shaft-bearing stiffness is beneficial in obtaining a more stable motion in OLOA direction, and a larger damping ratio results in a smaller effective friction force. The theory presented in this report outlines a new method of analyzing the dynamics of HCR gear in respect of introducing surface roughness into MDOF model directly, as well as establishing an indirect relationship between dynamic responses and surface roughness. This method is expected to guide surface roughness design and manufacturing in the future.

  10. Development of a prediction equation for depth, aspect ratio, and trench roughness pertaining to excimer laser ablation of polymer materials

    McGinty, Sean; O'Connor, Gerard M.; Glynn, Thomas J.


    Excimer based laser ablation of micro-fluidic circuits for micro-total analysis systems (μTAS) is an alternative to more expensive techniques of LIGA or micro-moulding. In the interests of developing a rapid prototyping method for direct writing of micro-fluidic circuits in polymer materials the ablation process was characterised using Design of Experiment techniques and a robust full factorial model was developed. Input factors of pulse energy, repetition rate, scan speed and number of passes were considered. Output responses of trench bottom width, sidewall angle, trench depth and trench roughness were measured. From this a prediction equation was created to forecast the output responses prior to machining and to allow the development of a process prior to machining. The accuracy of the prediction equation is discussed for four materials; Polystyrene, Polycarbonate, Non-CQ grade PMMA and CQ grade PMMA. For the four materials studied the response of Polystyrene and Polycarbonate were similar while the two grades of PMMA behave differently.

  11. Proceedings of submicron multiphase materials

    Baney, R.; Gilliom, L.; Hirano, S.I.; Schmidt, H.


    This book contains the papers presented at Symposium R of the spring 1992 Materials Research Society meeting held in San Francisco, California. The title of the symposium, Submicron Multiphase Materials, was selected by the organizers to encompass the realm of composite materials from those smaller than conventional fiber matrix composites to those with phase separation dimensions approaching molecular dimensions. The development of composite materials is as old as the development of materials. Humans quickly learned that, by combining materials, the best properties of each can be realized and that, in fact, synergistic effects often arise. For example, chopped straw was used by the Israelites to limit cracking in bricks. The famed Japanese samurai swords were multilayers of hard oxide and tough ductile materials. One also finds in nature examples of composite materials. These range form bone to wood, consisting of a hard phase which provides strength and stiffness and a softer phase for toughness. Advanced composites are generally thought of as those which are based on a high modulus, discontinuous, chopped or woven fiber phase and a continuous polymer phase. In multiphase composites, dimensions can range from meters in materials such as steel rod-reinforced concrete structures to angstroms. In macrophase separated composite materials, properties frequently follow the rule of mixtures with the properties approximating the arithmetic mean of the properties of each individual phase, if there is good coupling between the phases. As the phases become smaller, the surface to volume ratio grows in importance with respect to properties. Interfacial and interphase phenomena being to dominate. Surface free energies play an ever increasing role in controlling properties. In recent years, much research in materials science has been directed at multiphase systems where phase separations are submicron in at least some dimension.

  12. Filter-less submicron hydrodynamic size sorting.

    Fouet, M; Mader, M-A; Iraïn, S; Yanha, Z; Naillon, A; Cargou, S; Gué, A-M; Joseph, P


    We propose a simple microfluidic device able to separate submicron particles (critical size ∼0.1 μm) from a complex sample with no filter (minimum channel dimension being 5 μm) by hydrodynamic filtration. A model taking into account the actual velocity profile and hydrodynamic resistances enables prediction of the chip sorting properties for any geometry. Two design families are studied to obtain (i) small sizes within minutes (low-aspect ratio, two-level chip) and (ii) micron-sized sorting with a μL flow rate (3D architecture based on lamination). We obtain quantitative agreement of sorting performances both with experiments and with numerical solving, and determine the limits of the approach. We therefore demonstrate a passive, filter-less sub-micron size sorting with a simple, robust, and easy to fabricate design.

  13. Ultrahigh Aspect Ratio Copper-Nanowire-Based Hybrid Transparent Conductive Electrodes with PEDOT:PSS and Reduced Graphene Oxide Exhibiting Reduced Surface Roughness and Improved Stability.

    Zhu, Zhaozhao; Mankowski, Trent; Balakrishnan, Kaushik; Shikoh, Ali Sehpar; Touati, Farid; Benammar, Mohieddine A; Mansuripur, Masud; Falco, Charles M


    Copper nanowires (CuNWs) with ultrahigh aspect ratio are synthesized with a solution process and spray-coated onto select substrates to fabricate transparent conductive electrodes (TCEs). Different annealing methods are investigated and compared for effectiveness and convenience. The CuNWs are subsequently combined with the conductive polymer poly(3,4-ethylenedioxythiophene) poly(styrenesulfonate) ( PSS) or with reduced graphene oxide (rGO) platelets in order to reduce the surface roughness and improve the durability of the fabricated TCEs. Our best-performing PSS/CuNW films have optical transmittance T550 = 84.2% (at λ = 550 nm) and sheet resistance Rs = 25 Ω/sq, while our best CuNW/rGO films have T550 = 84% and Rs = 21.7 Ω/sq.

  14. Neurotoxicity of low-dose repeatedly intranasal instillation of nano- and submicron-sized ferric oxide particles in mice

    Wang, Bing; Feng, Weiyue; Zhu, Motao; Wang, Yun; Wang, Meng; Gu, Yiqun; Ouyang, Hong; Wang, Huajian; Li, Ming; Zhao, Yuliang; Chai, Zhifang; Wang, Haifang


    Olfactory tract has been demonstrated to be an important portal for inhaled solid nanoparticle transportation into the central nervous system (CNS). We have previously demonstrated that intranasally instilled Fe2O3 nanoparticles could transport into the CNS via olfactory pathway. In this study, we investigated the neurotoxicity and size effect of repeatedly low-dose (130 μg) intranasal exposure of nano- and submicron-sized Fe2O3 particles (21 nm and 280 nm) to mice. The biomarkers of oxidative stress, activity of nitric oxide synthases and release of monoamine neurotransmitter in the brain were studied. Our results showed that significant oxidative stress was induced by the two sizes of Fe2O3 particles. The activities of GSH-Px, Cu,Zn-SOD, and cNOS significantly elevated and the total GSH and GSH/GSSG ratio significantly decreased in the olfactory bulb and hippocampus after the nano- and submicron-sized Fe2O3 particle treatment ( p < 0.05). The nano-sized Fe2O3 generally induced greater alteration and more significant dose-effect response than the submicron-sized particle did. Some slight perturbation of monoamine neurotransmitters were found in the hippocampus after exposure to the two sizes of Fe2O3 particle. The TEM image showed that some ultrastructural alterations in nerve cells, including neurodendron degeneration, membranous structure disruption and lysosome increase in the olfactory bulb, slight dilation in the rough endoplasmic reticulum and lysosome increase in the hippocampus were induced by the nano-sized Fe2O3 treatment. In contrast, in the submicron-sized Fe2O3 treated mice, slightly swollen mitochondria and some vacuoles were observed in the olfactory bulb and hippocampus, respectively. These results indicate that intranasal exposure of Fe2O3 nanoparticles could induce more severe oxidative stress and nerve cell damage in the brain than the larger particle did. This is the first study to compare the neurotoxicity of nano- and submicron-sized Fe2O3

  15. Neurotoxicity of low-dose repeatedly intranasal instillation of nano- and submicron-sized ferric oxide particles in mice

    Wang Bing; Feng Weiyue, E-mail:; Zhu Motao; Wang Yun; Wang Meng [Chinese Academy of Sciences, Laboratory for Bio-Environmental Effects of Nanomaterials and Nanosafety and Key Laboratory of Nuclear Analytical Techniques, Institute of High Energy Physics (China); Gu Yiqun [Maternity Hospital of Haidian District (China); Ouyang Hong; Wang Huajian; Li Ming; Zhao Yuliang, E-mail:; Chai Zhifang [Chinese Academy of Sciences, Laboratory for Bio-Environmental Effects of Nanomaterials and Nanosafety and Key Laboratory of Nuclear Analytical Techniques, Institute of High Energy Physics (China); Wang Haifang [Peking University, College of Chemistry and Molecular Engineering (China)


    Olfactory tract has been demonstrated to be an important portal for inhaled solid nanoparticle transportation into the central nervous system (CNS). We have previously demonstrated that intranasally instilled Fe{sub 2}O{sub 3} nanoparticles could transport into the CNS via olfactory pathway. In this study, we investigated the neurotoxicity and size effect of repeatedly low-dose (130 {mu}g) intranasal exposure of nano- and submicron-sized Fe{sub 2}O{sub 3} particles (21 nm and 280 nm) to mice. The biomarkers of oxidative stress, activity of nitric oxide synthases and release of monoamine neurotransmitter in the brain were studied. Our results showed that significant oxidative stress was induced by the two sizes of Fe{sub 2}O{sub 3} particles. The activities of GSH-Px, Cu,Zn-SOD, and cNOS significantly elevated and the total GSH and GSH/GSSG ratio significantly decreased in the olfactory bulb and hippocampus after the nano- and submicron-sized Fe{sub 2}O{sub 3} particle treatment (p < 0.05). The nano-sized Fe{sub 2}O{sub 3} generally induced greater alteration and more significant dose-effect response than the submicron-sized particle did. Some slight perturbation of monoamine neurotransmitters were found in the hippocampus after exposure to the two sizes of Fe{sub 2}O{sub 3} particle. The TEM image showed that some ultrastructural alterations in nerve cells, including neurodendron degeneration, membranous structure disruption and lysosome increase in the olfactory bulb, slight dilation in the rough endoplasmic reticulum and lysosome increase in the hippocampus were induced by the nano-sized Fe{sub 2}O{sub 3} treatment. In contrast, in the submicron-sized Fe{sub 2}O{sub 3} treated mice, slightly swollen mitochondria and some vacuoles were observed in the olfactory bulb and hippocampus, respectively. These results indicate that intranasal exposure of Fe{sub 2}O{sub 3} nanoparticles could induce more severe oxidative stress and nerve cell damage in the brain than the

  16. Comparative evaluation of dental resin composites based on micron- and submicron-sized monomodal glass filler particles.

    Valente, Lisia L; Peralta, Sonia L; Ogliari, Fabrício A; Cavalcante, Larissa M; Moraes, Rafael R


    A model resin composite containing a novel monomodal inorganic filler system based on submicron-sized Ba-Si-Al glass particles (NanoFine NF180; Schott) was formulated and compared with an experimental composite containing micron-sized particles (UltraFine UF1.0; Schott). The filler particles were characterized using X-ray microanalysis and granulometry, while the composites were characterized in terms of filler-resin morphology, radiopacity, degree of CC conversion, hardness, flexural strength/modulus, work-of-fracture, surface roughness and gloss (before and after simulated toothbrushing abrasion), and bulk compressive creep. The composites were formulated from the same photoactivated dimethacrylate co-monomer, incorporating mass fractions of 75% micron- and 78% submicron-sized particles. Quantitative data were analyzed at a significance level of pcomposites were similar in radiopacity, flexural strength, work-of-fracture, and creep. The submicron composite was harder but had lower flexural modulus and CC conversion. No significant differences in roughness were observed before brushing, although the submicron composite had higher gloss. Brushing increased roughness and decreased gloss on both materials, but the submicron composite retained higher gloss after brushing. The monomodal submicron glass filler system demonstrated potential for use in restorative dental composites, particularly due to improved esthetic properties. Copyright © 2013 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

  17. On the dry deposition of submicron particles

    Wesely, M. L.


    The air-surface exchange of particles can have a strong role in determining the amount, size, and chemical composition of particles in the troposphere. Here the authors consider only dry processes (deposition processes not directly aided by precipitation) and mostly address particles less than about 2 {micro}m in diameter (often referred to as submicron particles because most of such particles are less than 1 {micro}m in diameter). The processes that control the dry exchange of particulate material between the atmosphere and the surface of the Earth are numerous, highly varied, and sometimes poorly understood. As a result, determining which of the surface processes to parameterize or simulate in modeling the tropospheric mass budget of a particulate substance can be a significant challenge. Dry deposition, for example, can be controlled by a combination of Brownian diffusion, impaction, interception, and gravitational settling, depending on the size of the particles, the roughness of the surface on both micrometeorological and microscopic scales, the geometrical structure of vegetative canopies, and other surface characteristics such as wetness. Particles can be added to the lower atmosphere by resuspension from land surfaces and sea spray. The roles of rapid gas-to-particle conversion and growth or shrinkage of particles as a result of water condensation or evaporation in the lower few meters of the atmosphere can also have a significant impact on particle concentrations in the lower atmosphere. Here, a few micrometeorological observations and inferences on particle air-surface exchange are briefly addressed.

  18. Fabrication and electrical characterization of sub-micron diameter through-silicon via for heterogeneous three-dimensional integrated circuits

    Abbaspour, R.; Brown, D. K.; Bakir, M. S.


    This paper presents the fabrication and electrical characterization of high aspect-ratio (AR) sub-micron diameter through silicon vias (TSVs) for densely interconnected three-dimensional (3D) stacked integrated circuits (ICs). The fabricated TSV technology features an AR of 16:1 with 680 nm diameter copper (Cu) core and 920 nm overall diameter. To address the challenges in scaling TSVs, scallop-free low roughness nano-Bosch silicon etching and direct Cu electroplating on a titanium-nitride (TiN) diffusion barrier layer have been developed as key enabling modules. The electrical resistance of the sub-micron TSVs is measured to be on average 1.2 Ω, and the Cu resistivity is extracted to be approximately 2.95 µΩ cm. Furthermore, the maximum achievable current-carrying capacity (CCC) of the scaled TSVs is characterized to be approximately 360 µA for the 680 nm Cu core.

  19. Submicron particle dynamics for different surfaces under quiescent and turbulent conditions

    Vohra, Karn; Ghosh, Kunal; Tripathi, S. N.; Thangamani, I.; Goyal, P.; Dutta, Anu; Verma, V.


    Experiments were conducted using CsI aerosols in a small scale test chamber to simulate behaviour of aerosols in the containment of a nuclear reactor. The primary focus of the study was on submicron particles (14.3 nm-697.8 nm) due to their hazardous effect on human health. Different wall surfaces, viz., plexiglass, concrete and sandpaper were chosen to study the effect of surface roughness on dry deposition velocity under both quiescent and turbulent conditions. An analytical approach to calculate dry deposition velocity of submicron particles for rough surfaces has been proposed with an improvement in the existing parameterization for shift in the velocity boundary layer. The predicted deposition velocity with the improved parameterization was found to have better agreement with published measured data of Lai and Nazaroff (2005) compared to the existing parameterizations (Wood, 1981; Zhao and Wu, 2006b). There was a significant reduction in root mean square error (RMSE) between predicted, using the improved parameterization and measured deposition velocity (upto 100%) compared to earlier ones. The new analytical deposition approach was coupled with volume conserving semi-implicit coagulation model. This aerosol dynamic model was evaluated against explicit particle size distribution for the first time for rough surfaces. Normalized RMSE between simulated and measured particle size distribution varied in the range of 2%-20% at different instances. The model seems to closely predict submicron particle behaviour in indoor environment.

  20. Rough function model and rough membership function

    Wang Yun; Guan Yanyong; Huang Zhiqin


    Two pairs of approximation operators, which are the scale lower and upper approximations as well as the real line lower and upper approximations, are defined. Their properties and antithesis characteristics are analyzed. The rough function model is generalized based on rough set theory, and the scheme of rough function theory is made more distinct and complete. Therefore, the transformation of the real function analysis from real line to scale is achieved. A series of basic concepts in rough function model including rough numbers, rough intervals, and rough membership functions are defined in the new scheme of the rough function model. Operating properties of rough intervals similar to rough sets are obtained. The relationship of rough inclusion and rough equality of rough intervals is defined by two kinds of tools, known as the lower (upper) approximation operator in real numbers domain and rough membership functions. Their relative properties are analyzed and proved strictly, which provides necessary theoretical foundation and technical support for the further discussion of properties and practical application of the rough function model.

  1. Formation of Submicron Copper Sulfide Particles Using Spray Pyrolysis Method

    Lenggoro, I.; Kang, Yun; Komiya, Takafumi; Okuyama, Kikuo; Tohge, Noboru


    The morphology and crystalline phase of submicron copper sulfide particles prepared by spray pyrolysis method have been studied. In a nitrogen gas atmosphere, the covellite phase (CuS) spherical particles could be prepared using the solution with molar ratio of copper nitrate to thiourea and furnace temperatures of 1:2 at 200 300°C, as well as of 1:5 at 200 600°C. The crystalline phase of particles was highly depended on the composition of the precursors and the pyrolysis temperature. The sphericity of particles could be enhanced by increasing the temperature and prolonging the residence time of the droplets or particles in the furnace.

  2. Experimental investigation of submicron and ultrafine soot particle removal by tree leaves

    Hwang, Hee-Jae; Yook, Se-Jin; Ahn, Kang-Ho


    Soot particles emitted from vehicles are one of the major sources of air pollution in urban areas. In this study, five kinds of trees were selected as Pinus densiflora, Taxus cuspidata, Platanus occidentalis, Zelkova serrata, and Ginkgo biloba, and the removal of submicron (densiflora showed the greatest deposition velocity, followed by T. cuspidata, Platanus occidentalis, Zelkova serrata, and Ginkgo biloba. In addition, from the comparison of deposition velocity between two groups of Platanus occidentalis leaves, i.e. one group of leaves with front sides only and the other with back sides only, it was supposed in case of the broadleaf trees that the removal of airborne soot particles of submicron and ultrafine sizes could be affected by the surface roughness of tree leaves, i.e. the veins and other structures on the leaves.

  3. Geo-rough Space


    Rough set is a new approach to uncertainties in spatial analysis.In this paper,rough set symbols are simplified and standardized in terms of rough interpretation and specialized indication.Rough spatial entities and their topological relationships are also proposed in rough space,thus a universal intersected equation is developed,and rough membership function is further extended with the gray scale in our case study.We complete three works.First,a set of simplified rough symbols is advanced on the basis of existing rough symbols.Second,rough spatial entity is put forward to study the real world as it is,without forcing uncertainties into crisp set.Third,rough spatial topological relationships are studied by using rough matrix and their figures.The relationships are divided into three types,crisp entity and crisp entity (CC),rough entity and crisp entity (RC),and rough entity and rough entity (RR).A universal intersected equation is further proposed.Finally,the maximum and minimum maps of river thematic classification are generated via rough membership function and rough relationships in our case study.

  4. Roughness-induced streaming in turbulent wave boundary layers

    Fuhrman, David R.; Sumer, B. Mutlu; Fredsøe, Jørgen


    -averaged streaming characteristics induced by bottom roughness variations are systematically assessed. The effects of variable roughness ratio, gradual roughness transitions, as well as changing flow orientation in plan are all considered. As part of the latter, roughness-induced secondary flows are predicted...

  5. Separation of submicron bioparticles by dielectrophoresis.

    Morgan, H.; Hughes, M P; Green, N G


    Submicron particles such as latex spheres and viruses can be manipulated and characterized using dielectrophoresis. By the use of appropriate microelectrode arrays, particles can be trapped or moved between regions of high or low electric fields. The magnitude and direction of the dielectrophoretic force on the particle depends on its dielectric properties, so that a heterogeneous mixture of particles can be separated to produce a more homogeneous population. In this paper the controlled sepa...

  6. Water condensation for submicronic particles abatement

    Cozzolino, Gennaro


    Control of particulate matter (PM) emissions from industrial processes is important for protection of human health and the environment. A promising technique for submicron PM abatement is by condensing water vapor onto the particles, which enhances particle growth and improves the performance of traditional particle collection devices. This thesis analyzes the flue gases cleaning process by means of activation heterogeneous water nucleation mechanism on particles surface as a function of work...

  7. Submicron Surface-Patterned Fibers and Textiles


    Submitted to 1 DOI: 10.1002/adma.((please add manuscript number)) Article type : Communication Submicron surface-patterned fibers and...we investigate three specific types of physical forming techniques: milling, laser cutting, and molding (Figure S1). Each method has its unique...semi-crystalline Submitted to 4 polymers, such as polyvinylidene fluoride (PVDF). Conventional molding methods for plastics limit the feature

  8. Filling schemes at submicron scale: Development of submicron sized plasmonic colour filters

    Rajasekharan, Ranjith; Balaur, Eugeniu; Minovich, Alexander; Collins, Sean; James, Timothy D.; Djalalian-Assl, Amir; Ganesan, Kumaravelu; Tomljenovic-Hanic, Snjezana; Kandasamy, Sasikaran; Skafidas, Efstratios; Neshev, Dragomir N.; Mulvaney, Paul; Roberts, Ann; Prawer, Steven


    The pixel size imposes a fundamental limit on the amount of information that can be displayed or recorded on a sensor. Thus, there is strong motivation to reduce the pixel size down to the nanometre scale. Nanometre colour pixels cannot be fabricated by simply downscaling current pixels due to colour cross talk and diffraction caused by dyes or pigments used as colour filters. Colour filters based on plasmonic effects can overcome these difficulties. Although different plasmonic colour filters have been demonstrated at the micron scale, there have been no attempts so far to reduce the filter size to the submicron scale. Here, we present for the first time a submicron plasmonic colour filter design together with a new challenge - pixel boundary errors at the submicron scale. We present simple but powerful filling schemes to produce submicron colour filters, which are free from pixel boundary errors and colour cross- talk, are polarization independent and angle insensitive, and based on LCD compatible aluminium technology. These results lay the basis for the development of submicron pixels in displays, RGB-spatial light modulators, liquid crystal over silicon, Google glasses and pico-projectors.

  9. Sub-micronic capsules based on gelatin and poly(maleic anhydride-alt-vinyl acetate) obtained by interfacial condensation with potential biomedical applications.

    Iurea, Delia Mihaela; Peptu, Cătălina Anişoara; Chailan, Jean-François; Carriere, Pascal; Popa, Marcel


    New sub-micronic capsules based on a copolymer of maleic anhydride-alt-vinyl acetate and a natural polymer (gelatin) using an interfacial condensation method were obtained. Sub-micronic capsules were characterized by Fourier Transform infrared spectroscopy (FTIR), dynamic light scattering (DLS) method, zeta-potential, scanning electron microscopy (SEM) and atomic force microscopy (AFM). The thermal properties were investigated by thermogravimetric analysis (TGA). According to some parameters of the synthesis reaction (polymer weight ratio, acetone/water ratio, surfactant concentration), the mean diameter of the sub-micronic capsules can be tuned from 200 to 760 nm. The sub-micronic capsules show a higher agglomeration tendency as the amount of gelatin in their composition increases. The swelling capacity in aqueous solutions is dependent on the composition and size of the sub-micronic capsules, decreasing with their diameter and gelatin composition. The drug loading and release capacity was studied using Penicillin G (sodium salt) (PG), and it has been proved that it is influenced by the sub-micronic capsules morphology induced by preparation parameters. Encapsulation and controlled release of small molecule were successfully carried out, demonstrating the potential biomedical applications of these new easily obtained sub-micronic capsules.

  10. Discovering sub-micron ice particles across Dione' surface

    Scipioni, Francesca; Schenk, Pual; Tosi, Federico; Clark, Roger; Dalle Ore, Cristina; Combe, Jean-Philippe


    Water ice is the most abundant component of Saturn’s mid-sized moons. However, these moons show an albedo asymmetry - their leading sides are bright while their trailing side exhibits dark terrains. Such differences arise from two surface alteration processes: (i) the bombardment of charged particles from the interplanetary medium and driven by Saturn’s magnetosphere on the trailing side, and (ii) the impact of E-ring water ice particles on the satellites’ leading side. As a result, the trailing hemisphere appears to be darker than the leading side. This effect is particularly evident on Dione's surface. A consequence of these surface alteration processes is the formation or the implantation of sub-micron sized ice particles.The presence of such particles influences and modifies the surfaces' spectrum because of Rayleigh scattering by the particles. In the near infrared range of the spectrum, the main sub-micron ice grains spectral indicators are: (i) asymmetry and (ii) long ward minimum shift of the absorption band at 2.02 μm (iii) a decrease in the ratio between the band depths at 1.50 and 2.02 μm (iv) a decrease in the height of the spectral peak at 2.6 μm (v) the suppression of the Fresnel reflection peak at 3.1 μm and (vi) the decrease of the reflection peak at 5 μm relative to those at 3.6 μm.We present results from our ongoing work mapping the variation of sub-micron ice grains spectral indicators across Dione' surface using Cassini-VIMS cubes acquired in the IR range (0.8-5.1 μm). To characterize the global variations of spectral indicators across Dione' surface, we divided it into a 1°x1° grid and then averaged the band depths and peak values inside each square cell.We will investigate if there exist a correspondence with water ice abundance variations by producing water ice' absorption band depths at 1.25, 1.52 and 2.02 μm, and with surface morphology by comparing the results with ISS color maps in the ultraviolet, visible and infrared

  11. Submicron FETs Using Molecular Beam Epitaxy.


    C NISMIMOTO N0001-77-C-0655 UNCLASSIFIED NLIiiII/mlum.. varian SUBMICRON FETs USING MOLECULAR BEAM EPITAXY 00 ANNUAL REPORT NO. 2 (August 1978...Ohmic Contacts to Highly Doped n-type GaAs Layers Grown by Molecular Beam Epitaxy (MBE) for Field-Effect Trans- istors," J. Appl. Phys. 50, 951 (1979...36 ’A, References (Cont.) 8. D. M. Collins, "The Use of SnTe as the Source of Donor Impurities in GaAs Grown by Molecular Beam Epitaxy ," Appl. Phys

  12. Influence of locational states of submicron fibers added into matrix on mechanical properties of plain-woven Carbon Fiber Composite

    Kumamoto, Soichiro; Okubo, Kazuya; Fujii, Toru


    The aim of this study was to show the influence of locational states of submicron fibers added into epoxy matrix on mechanical properties of modified plane-woven carbon fiber reinforced plastic (CFRP). To change the locational states of submicron fibers, two kinds of fabrication processes were applied in preparing specimen by hand lay-up method. Submicron fibers were simply added into epoxy resin with ethanol after they were stirred by a dispersion process using homogenizer to be located far from the interface between reinforcement and matrix. In contrast, submicron fibers were attached onto the carbon fibers by injecting from a spray nozzle accompanying with ethanol to be located near the interface, after they were tentatively contained in ethanol. The plain-woven CFRP plates were fabricated by hand lay-up method and cured at 80 degree-C for 1 hour and then at 150 degree-C for 3 hours. After curing, the plain-woven CFRP plates were cut into the dimension of specimen. Tensile shear strength and Mode-II fracture toughness of CFRP were determined by tensile lap-shear test and End-notched flexure(ENF) test, respectively. When submicron fibers were located far from the interface between carbon fibers and epoxy resin, tensile shear strength and Mode-II fracture toughness of CFRP were improved 30% and 18% compared with those of unmodified case. The improvement ratio in modified case was rather low (about few percentages) in the case where submicron fibers were located near the interface. The result suggested that crack propagation should be prevented when submicron fibers were existed far from the interface due to the effective stress state around the crack tip.

  13. Influence of locational states of submicron fibers added into matrix on mechanical properties of plain-woven Carbon Fiber Composite

    Kumamoto Soichiro


    Full Text Available The aim of this study was to show the influence of locational states of submicron fibers added into epoxy matrix on mechanical properties of modified plane-woven carbon fiber reinforced plastic (CFRP. To change the locational states of submicron fibers, two kinds of fabrication processes were applied in preparing specimen by hand lay-up method. Submicron fibers were simply added into epoxy resin with ethanol after they were stirred by a dispersion process using homogenizer to be located far from the interface between reinforcement and matrix. In contrast, submicron fibers were attached onto the carbon fibers by injecting from a spray nozzle accompanying with ethanol to be located near the interface, after they were tentatively contained in ethanol. The plain-woven CFRP plates were fabricated by hand lay-up method and cured at 80 degree-C for 1 hour and then at 150 degree-C for 3 hours. After curing, the plain-woven CFRP plates were cut into the dimension of specimen. Tensile shear strength and Mode-II fracture toughness of CFRP were determined by tensile lap-shear test and End-notched flexure(ENF test, respectively. When submicron fibers were located far from the interface between carbon fibers and epoxy resin, tensile shear strength and Mode-II fracture toughness of CFRP were improved 30% and 18% compared with those of unmodified case. The improvement ratio in modified case was rather low (about few percentages in the case where submicron fibers were located near the interface. The result suggested that crack propagation should be prevented when submicron fibers were existed far from the interface due to the effective stress state around the crack tip.

  14. Electrospray crystallization for high-quality submicron-sized crystals

    Radacsi, N.; Stankiewicz, A.I.; Creyghton, Y.L.M.; Heijden, A.E.D.M. van der; Horst, J.H. ter


    Nano- and submicron-sized crystals are too small to contain inclusions and are, therefore, expected to have a higher internal quality compared to conventionally sized particles (several tens to hundreds of microns). Using electrospray crystallization, nano- and submicron-sized crystals can be easily

  15. Submicron electrode gaps fabricated by gold electrodeposition at interdigitated electrodes

    Megen, M.J.J; Olthuis, W.; Berg, van den A.


    Electrodes with submicron gaps are desired for achieving high amplification redox cycling sensors. In this contribution we report the use of electrodeposition of gold in order to decrease the inter-electrode spacing at interdigitated electrodes. Using this method submicron spacings can be obtained w

  16. Submicron mineral structures control the stabilization of litter-derived organic matter in soils - A NanoSIMS study

    Vogel, Cordula; Mueller, Carsten W.; Höschen, Carmen; Buegger, Franz; Heister, Katja; Schulz, Stefanie; Schloter, Michael; Kögel-Knabner, Ingrid


    The sequestration of carbon and nitrogen by clay-sized particles in soils is well established. However, in the most cases, the complex structure of the organo-mineral associations remain a black box due to the common measurements of soil fractions as a whole. By combining nano-scale secondary ion mass spectrometry (NanoSIMS) with isotopic tracing it is possible to study the formation and spatial heterogeneity of organo-mineral associations. NanoSIMS enables the detection of up to seven secondary ion species (e.g. 13C-, 12N15N-, 27Al16O-, 56Fe16O-) simultaneously, to generate a submicron-scale image of the elemental and isotopic composition (e.g. 13C, 15N, Al and Fe) down to a lateral resolution of ~150 nm. Therefore this technique can be used to study organo-mineral associations at the relevant scale. The aim of our study was to follow the formation of organo-mineral associations over different time steps and the distribution of C and N by imaging the complex arrangement between soil mineral surfaces and litter-derived organic matter (OM). Parallel to the determination of the isotopic N and C composition of bulk soil and soil fractions (combined density and particle size fractionation) using isotope ratio mass spectrometry (IRMS), the spatial distribution of the OM was investigated by NanoSIMS analysis of the clay-sized fraction. In our study we show that only some of the clay-sized surfaces bind OM. Surprisingly, less than 19% of the mineral areas visible by scanning electron microscopy and NanoSIMS show an OM attachment. We demonstrate that mineral clusters with rough surfaces exhibit the preferential binding spots for OM. By combining NanoSIMS and isotopic tracing, we distinguish between new labelled and pre-existing OM and show that new OM is preferentially attached to already present organo-mineral clusters. Vogel, C., Mueller, C.W., Höschen, C., Buegger, F., Heister, K., Schulz, S., Schloter, M., Kögel-Knabner, I., 2014. Submicron structures provide

  17. Generalization Rough Set Theory

    XIAO Di; ZHANG Jun-feng; HU Shou-song


    In order to avoid the discretization in the classical rough set theory, a generlization rough set theory is proposed.At first, the degree of general importance of an attribute and attribute subsets are presented.Then, depending on the degree of general importance of attribute, the space distance can be measured with weighted method.At last, a generalization rough set theory based on the general near neighborhood relation is proposed.The proposed theory partitions the universe into the tolerant modules, and forms lower approximation and upper approximation of the set under general near neighborhood relationship, which avoids the discretization in Pawlak's rough set theory.

  18. Measurement of surface roughness

    De Chiffre, Leonardo

    This document is used in connection with two 3 hours laboratory exercises that are part of the course GEOMETRICAL METROLOGY AND MACHINE TESTING. The laboratories include a demonstration of the function of roughness measuring instruments plus a series of exercises illustrating roughness measurement...

  19. Rough Neutrosophic Sets

    Said Broumi; Florentin Smarandache; Mamoni Dhar


     Both neutrosophic sets theory and rough sets theory are emerging as powerful tool for managing uncertainty, indeterminate, incomplete and imprecise information. In this paper we develop an hybrid structure called rough neutrosophic sets and studied their properties. 

  20. Electrodeposited submicron thermocouples with microsecond response times.

    Bourg, M E; van der Veer, W E; Güell, A G; Grüell, A G; Penner, R M


    We describe a procedure for preparing submicron scale silver-nickel thermocouples (TCs) using electrochemical step edge decoration on graphite surfaces. Each fabrication operation produced ensembles of 2-20 TCs with diameters in the 1.0 microm to 500 nm range. These "sub-mum TCs" (SMTCs) produced linear voltage versus temperature output over the range from 20 to 100 degrees C characterized by a Seebeck coefficient of 20 +/- 1 microV/degrees C, equal to the 21 microV/degrees C that is theoretically expected for a junction between these two metals. The time response of SMTCs was evaluated using two different laser-heating methods and compared with the smallest mechanically robust commercially available type J TCs. Electrochemical etching of the silver wire introduced constrictions at grain boundaries that reduced the thermal mass of the junction without altering its integrity or its overall diameter, producing a decrease of the measured rise time for SMTCs up to 96%.

  1. Zirconia nanocrystals as submicron level biological label

    Smits, K.; Liepins, J.; Gavare, M.; Patmalnieks, A.; Gruduls, A.; Jankovica, D.


    Inorganic nanocrystals are of increasing interest for their usage in biology and pharmacology research. Our interest was to justify ZrO2 nanocrystal usage as submicron level biological label in baker's yeast Saccharomyces cerevisia culture. For the first time (to our knowledge) images with sub micro up-conversion luminescent particles in biologic media were made. A set of undoped as well as Er and Yb doped ZrO2 samples at different concentrations were prepared by sol-gel method. The up-conversion luminescence for free standing and for nanocrystals with baker's yeast cells was studied and the differences in up-conversion luminescence spectra were analyzed. In vivo toxic effects of ZrO2 nanocrystals were tested by co-cultivation with baker's yeast.

  2. Carbohydrate-Like Composition of Submicron Atmospheric Particles and their Production from Ocean Bubble Bursting

    Russell, L. M.; Hawkins, L. N.; Frossard, A. A.; Quinn, P.; Bates, T. S.


    Oceans cover over two-thirds of the Earth’s surface, and the particles emitted to the atmosphere by waves breaking on sea surfaces provide an important contribution to the planetary albedo. During the ICEALOT cruise on the R/V Knorr in March and April of 2008, organic mass accounted for 15% to 47% of the submicron particle mass in the air masses sampled over the North Atlantic and Arctic Oceans. A majority of this organic component (0.1 to 0.4 μg m-3) consisted of organic hydroxyl (including polyol and other alcohol) groups characteristic of saccharides, similar to biogenic carbohydrates found in seawater. The large fraction of organic hydroxyl groups measured during ICEALOT in submicron atmospheric aerosol exceeded those measured in most previous campaigns but were similar to particles in marine air masses in the open ocean (Southeast Pacific Ocean) and coastal sites at northern Alaska (Barrow) and northeastern North America (Appledore Island and Chebogue Point). The ocean-derived organic hydroxyl mass concentration during ICEALOT correlated strongly to submicron Na concentration and wind speed. The observed submicron particle ratios of marine organic mass to Na were enriched by factors of ~100 to ~1000 over reported sea surface organic to Na ratios, suggesting that the surface-controlled process of film bursting is influenced by the dissolved organic components present in the sea surface micro-layer. Both marine organic components and Na increased with increasing number mean diameter of the accumulation mode, suggesting a possible link between organic components in the ocean surface and aerosol-cloud interactions.

  3. Physical model for turbulent friction on rough surfaces

    Li, Zhuoqun


    We present an analytical expression for turbulent friction on rough surfaces with regularly distributed roughness elements. Wall shear stresses are expressed as functions of physical quantities. Surfaces with varying roughness densities and roughness elements with different aspect ratios are considered. As the drag on each roughness element decreases as roughness density increases, we propose a straight forward method based on momentum conservation to deduce drag on elements by expressing it as a function of the maximum drag on elements and drag reductions ratios. We proposed a drag reduction effect of momentum redistribution and studied the mutual sheltering effect. Reduction ratios for redistribution effect and mutual sheltering effect are deduced, for different rough surfaces. These two drag reduction mechanisms are significant for sparse and dense surfaces, respectively. The shear stress on elements and the total shear stress are obtained as the result of the drag analysis. The estimated wall shear stress...

  4. F-rough law and the discovery of rough law

    Qiu Jinming; Shi Kaiquan


    By using function one direction S-rough sets (function one direction singular rough sets), this article presents the concepts of F-law, F-rough law, and the relation metric of rough law; by using these concepts, this article puts forward the theorem of F-law relation metric, two orders theorem of F-rough law relation metric, the attribute theorem of F-rough law band, the extremum theorem of F-rough law relation metric, the discovery principle of F-rough law and the application of F-rough law.

  5. Modeling and simulation of surface roughness

    Patrikar, Rajendra M


    With the technology advancement, electronic devices are miniaturized at every development node. Physical parameters such as microscopic roughness are affecting these devices because surface to volume ratio is increasing rapidly. On all the real surfaces microscopic roughness appears, which affects many electronic properties of the material, which in turn decides the yield and reliability of the devices. Different type of parameters and simulation methods are used to describe the surface roughness. Classically surface roughness was modeled by methods such as power series and Fast Fourier Transform (FFT). Limitations of this methods lead to use the concept of self-similar fractals to model the rough surface through Mandelbrot-Weierstrass function. It is difficult to express surface roughness as a function of process parameters in the form of analytical functions. Method based on neural networks has been used to model these surfaces to map the process parameters to roughness parameters. Finally, change in electrical parameters such as capacitance, resistance and noise due to surface roughness has been computed by numerical methods.

  6. Automatic Determination of Roughness


    During the second development and the design of AutoCAD, it's necessary for us to choose roughness according to the part's precision grade, it's connecting relationship, and look up the list. In order to make the designer and programmer get the precision grade quickly and accurately, and decide the roughness in the drawing, this article analyze the relationship between the precision and roughness on the basis of analyzing method, and consider the experience in practice, then carry out a set of method formul...

  7. Turbulent boundary layer over roughness transition with variation in spanwise roughness length scale

    Westerweel, Jerry; Tomas, Jasper; Eisma, Jerke; Pourquie, Mathieu; Elsinga, Gerrit; Jonker, Harm


    Both large-eddy simulations (LES) and water-tunnel experiments, using simultaneous stereoscopic PIV and LIF were done to investigate pollutant dispersion in a region where the surface changes from rural to urban roughness. This consists of rectangular obstacles where we vary the spanwise aspect ratio of the obstacles. A line source of passive tracer was placed upstream of the roughness transition. The objectives of the study are: (i) to determine the influence of the aspect ratio on the roughness-transition flow, and (ii) to determine the dominant mechanisms of pollutant removal from street canyons in the transition region. It is found that for a spanwise aspect ratio of 2 the drag induced by the roughness is largest of all considered cases, which is caused by a large-scale secondary flow. In the roughness transition the vertical advective pollutant flux is the main ventilation mechanism in the first three streets. Furthermore, by means of linear stochastic estimation the mean flow structure is identied that is responsible for exchange of the fluid between the roughness obstacles and the outer part of the boundary layer. Furthermore, it is found that the vertical length scale of this structure increases with increasing aspect ratio of the obstacles in the roughness region.

  8. Umatilla - Rough Fish Eradication

    US Fish and Wildlife Service, Department of the Interior — In order to enhance environmental conditions in the McCormack Slough on Umatilla NWR, the population of rough fish, including common carp (Cyprinus carpio) and...

  9. On the Acoustic Properties of Vaporized Submicron Perfluorocarbon Droplets

    Reznik, Nikita; Lajoinie, Guillaume; Shpak, Oleksandr; Gelderblom, Erik C.; Williams, Ross; Jong, de Nico; Versluis, Michel; Burns, Peter N.


    The acoustic characteristics of microbubbles created from vaporized submicron perfluorocarbon droplets with fluorosurfactant coating are examined. Utilizing ultra-high-speed optical imaging, the acoustic response of individual microbubbles to low-intensity diagnostic ultrasound was observed on clini

  10. Resolution enhancement techniques for submicron deep trench processes

    Tong, Lijun; Hsiang, Joyce; Lin, Kuanchih; Newman, Gary


    Due to the rapid advancements in the data storage market, the development of new technologies and mechanisms are needed to support the continued growth of data storage systems. The concept and technology of Micro Electro Mechanical Systems (MEMS) can provide opportunities to meet these demands. Correspondingly, new MEMS devices can be made commercially available by sharing the benefits of developments in data storage systems. The photolithography requirements for thin film head (TFH) processing have grown increasingly challenging. Specifically, the resolution of submicron isolated features is required in thick photoresist; resulting in aspect ratios of nearly 10 to 1. To satisfy these imaging requirements, the use of i-line reduction lithography tools with variable numerical aperture and partial coherence are necessary. This study examines the influence of NA, (sigma) , and reticle bias on critical features in a typical TFH write-layer process. Combinations of NA and (sigma) were investigated for their impact on minimum feature size, process latitude, and sidewall angle. Process latitude was quantified for each illumination condition over a range of focus and exposure conditions.

  11. A fast direct numerical simulation method for characterising hydraulic roughness

    Chung, Daniel; MacDonald, Michael; Hutchins, Nicholas; Ooi, Andrew


    We describe a fast direct numerical simulation (DNS) method that promises to directly characterise the hydraulic roughness of any given rough surface, from the hydraulically smooth to the fully rough regime. The method circumvents the unfavourable computational cost associated with simulating high-Reynolds-number flows by employing minimal-span channels (Jimenez & Moin 1991). Proof-of-concept simulations demonstrate that flows in minimal-span channels are sufficient for capturing the downward velocity shift, that is, the Hama roughness function, predicted by flows in full-span channels. We consider two sets of simulations, first with modelled roughness imposed by body forces, and second with explicit roughness described by roughness-conforming grids. Owing to the minimal cost, we are able to conduct DNSs with increasing roughness Reynolds numbers while maintaining a fixed blockage ratio, as is typical in full-scale applications. The present method promises a practical, fast and accurate tool for character...

  12. Submicron Features in Higher Manganese Silicide

    Yatir Sadia


    Full Text Available The world energy crisis had increased the demand for alternative energy sources and as such is one of the topics at the forefront of research. One way for reducing energy consumption is by thermoelectricity. Thermoelectric effects enable direct conversion of thermal into electrical energy. Higher manganese silicide (HMS, MnSi1.75 is one of the promising materials for applications in the field of thermoelectricity. The abundance and low cost of the elements, combined with good thermoelectric properties and high mechanical and chemical stability at high temperatures, make it very attractive for thermoelectric applications. Recent studies have shown that Si-rich HMS has improved thermoelectric properties. The most interesting of which is the unusual reduction in thermal conductivity. In the current research, transmission (TEM and scanning (SEM electron microscopy as well as X-ray diffraction methods were applied for investigation of the govern mechanisms resulting in very low thermal conductivity values of an Si-rich HMS composition, following arc melting and hot-pressing procedures. In this paper, it is shown that there is a presence of sub-micron dislocations walls, stacking faults, and silicon and HMS precipitates inside each other apparent in the matrix, following a high temperature (0.9 Tm hot pressing for an hour. These are not just responsible for the low thermal conductivity values observed but also indicate the ability to create complicate nano-structures that will last during the production process and possibly during the application.

  13. Low-loss, submicron chalcogenide integrated photonics with chlorine plasma etching

    Chiles, Jeff; Malinowski, Marcin; Rao, Ashutosh [CREOL, The College of Optics and Photonics, University of Central Florida, Orlando, Florida 32816 (United States); Novak, Spencer; Richardson, Kathleen [CREOL, The College of Optics and Photonics, University of Central Florida, Orlando, Florida 32816 (United States); Department of Materials Science and Engineering, COMSET, Clemson University, Clemson, South Carolina 29634 (United States); Fathpour, Sasan, E-mail: [CREOL, The College of Optics and Photonics, University of Central Florida, Orlando, Florida 32816 (United States); Department of Electrical Engineering and Computer Science, University of Central Florida, Orlando, Florida 32816 (United States)


    A chlorine plasma etching-based method for the fabrication of high-performance chalcogenide-based integrated photonics on silicon substrates is presented. By optimizing the etching conditions, chlorine plasma is employed to produce extremely low-roughness etched sidewalls on waveguides with minimal penalty to propagation loss. Using this fabrication method, microring resonators with record-high intrinsic Q-factors as high as 450 000 and a corresponding propagation loss as low as 0.42 dB/cm are demonstrated in submicron chalcogenide waveguides. Furthermore, the developed chlorine plasma etching process is utilized to demonstrate fiber-to-waveguide grating couplers in chalcogenide photonics with high power coupling efficiency of 37% for transverse-electric polarized modes.

  14. Artifacts for Calibration of Submicron Width Measurements

    Grunthaner, Frank; Grunthaner, Paula; Bryson, Charles, III


    Artifacts that are fabricated with the help of molecular-beam epitaxy (MBE) are undergoing development for use as dimensional calibration standards with submicron widths. Such standards are needed for calibrating instruments (principally, scanning electron microscopes and scanning probe microscopes) for measuring the widths of features in advanced integrated circuits. Dimensional calibration standards fabricated by an older process that involves lithography and etching of trenches in (110) surfaces of single-crystal silicon are generally reproducible to within dimensional tolerances of about 15 nm. It is anticipated that when the artifacts of the present type are fully developed, their critical dimensions will be reproducible to within 1 nm. These artifacts are expected to find increasing use in the semiconductor-device and integrated- circuit industries as the width tolerances on semiconductor devices shrink to a few nanometers during the next few years. Unlike in the older process, one does not rely on lithography and etching to define the critical dimensions. Instead, one relies on the inherent smoothness and flatness of MBE layers deposited under controlled conditions and defines the critical dimensions as the thicknesses of such layers. An artifact of the present type is fabricated in two stages (see figure): In the first stage, a multilayer epitaxial wafer is grown on a very flat substrate. In the second stage, the wafer is cleaved to expose the layers, then the exposed layers are differentially etched (taking advantage of large differences between the etch rates of the different epitaxial layer materials). The resulting structure includes narrow and well-defined trenches and a shelf with thicknesses determined by the thicknesses of the epitaxial layers from which they were etched. Eventually, it should be possible to add a third fabrication stage in which durable, electronically inert artifacts could be replicated in diamondlike carbon from a master made by

  15. Submicron R2Fe14B particles

    O. Koylu-Alkan


    Full Text Available Mechanochemical synthesis of submicron R2Fe14B particles with R = Dy, Nd, Pr has been performed successfully via high energy ball milling of rare-earth oxides, iron oxide and boron oxide in the presence of a reducing agent (Ca and a dispersant material (CaO, followed by annealing at 800 - 900 °C. In the R = Nd system, we were able to fabricate particles embedded in a CaO matrix with coercivity (Hc of 10.3 kOe after annealing at 900 °C for 5 min. After washing off the dispersant, the Hc was decreased to below 1 kOe because of hydrogen absorption that leads to the formation of the hydrated R2Fe14BHx phase that has a lower anisotropy. Upon removal of the hydrogen the coercivity was increased to 3.3 kOe. The average size of the Nd2Fe14B particles increases from 100 nm in a sample synthesized at 800 °C to 158 nm at 900 °C. The isotropic Dy2Fe14B particles showed a higher coercivity of 21 kOe in washed samples after annealing at 900 °C for 5 min. An average size of 71 nm is measured in samples synthesized at 800 °C and 107 nm at 900 °C. Fitting the high field M(H measurements in Nd2Fe14B to the law of approach to saturation gave values for the magnetocrystalline anisotropy for the washed sample 2.23 × 107 erg/cm3 and for the vacuum annealed sample 4.15 × 107 erg/cm3, both of which are lower than the bulk values. This would explain the lower values of Hc observed in the particles.

  16. Subcellular fractionation of rough microsomes.

    Sabatini, David D


    When eukaryotic cells are homogenized, the rough endoplasmic reticula are converted into small vesicles, called rough microsomes. Strategies for the isolation of rough microsomes are introduced here, as are methods for evaluating the purity and intactness of an isolated rough microsomal fraction.

  17. Dualities in Covering Rough Operations

    William Zhu


    Rough set theory is a technique of granular computing. In this paper, we study a type of generalized rough sets based on covering. There are several literatures[ 1,40-43 ] exploring covering-based rough sets. Our focus of this paper is on the dualities in rough operations.

  18. Roughing up Beta

    Bollerslev, Tim; Li, Sophia Zhengzi; Todorov, Viktor

    Motivated by the implications from a stylized equilibrium pricing framework, we investigate empirically how individual equity prices respond to continuous, or \\smooth," and jumpy, or \\rough," market price moves, and how these different market price risks, or betas, are priced in the cross-section...

  19. Rough similarity degree and rough close degree in rough fuzzy sets and the applications

    Li Jian; Xu Xiaojing; Shi Kaiquan


    Based on rough similarity degree of rough sets and close degree of fuzzy sets,the definitions of rough similarity degree and rough close degree of rough fuzzy sets are given,which can be used to measure the similar degree between two rough fuzzy sets.The properties and theorems are listed.Using the two new measures,the method of clustering in the rough fuzzy system can be obtained.After clustering,the new fuzzy sample can be recognized by the principle of maximal similarity degree.

  20. Aligned submicron grains in archeological potteries with high TRM anisotropy

    Fukuma, K.; Ooga, M.; Isobe, H.


    Potteries have been often used to obtain archeointensity data because of the extremely high success rates in Thellier experiments. Since high anisotropy of thermoremanent magnetization (TRM) are commonly observed for potteries, anisotropy correction is routinely applied to make archeointensity data reliable. Such a TRM anisotropy is characterized by the foliated structure parallel to the surface and has been interpreted to reflect aligned magnetic minerals during molding. However, the high thermal stability and the higher degrees of TRM anisotropies than those of low-field susceptibility suggest that pottery TRM resides in fine-grained magnetic minerals formed during firing. Molding is not sufficient to explain highly anisotropic TRM of potteries. We measured TRM susceptibility tensors on potteries manufactured from 14th to 17th centuries in Japan. These potteries were fired up to about 1200°C resulting in partial vitrification. The ratios of maximum and minimum eigenvalues of the TRM susceptibility tensors are well distributed and reaches 1.8 for most anisotropic samples. The Curie temperature ranges from 500°C to 550°C implying titanium-poor titanomagnetite as TRM carriers, and the narrow unblocking temperature indicates that the low-titanium titanomagnetites are in or close to the single-domain size range. Submicron titanomagnetite grains were commonly observed on the polished sections under a FE-SEM. Some of the grains occur as inclusions in iron-bearing silicates such as pyroxene or hornblende, and other grains reside in glass matrix. In addition, vesiculated clay minerals contain highly elongated titanomagnetite grains. Such clay minerals seem stretched parallel to the pottery surface and inside titanomagnetite grains are also elongated along the surface. Relative abundance of titanomagnetite inclusions in silicates or glass against in clay minerals should control the degree of TRM anisotropy. Foliated TRM anisotropies originate from both alignment of clay

  1. NATO Advanced Study Institute on Physics of Submicron Semiconductor Devices

    Ferry, David; Jacoboni, C


    The papers contained in the volume represent lectures delivered as a 1983 NATO ASI, held at Urbino, Italy. The lecture series was designed to identify the key submicron and ultrasubmicron device physics, transport, materials and contact issues. Nonequilibrium transport, quantum transport, interfacial and size constraints issues were also highlighted. The ASI was supported by NATO and the European Research Office. H. L. Grubin D. K. Ferry C. Jacoboni v CONTENTS MODELLING OF SUB-MICRON DEVICES.................. .......... 1 E. Constant BOLTZMANN TRANSPORT EQUATION... ... ...... .................... 33 K. Hess TRANSPORT AND MATERIAL CONSIDERATIONS FOR SUBMICRON DEVICES. . .. . . . . .. . . . .. . .. . .... ... .. . . . .. . . . .. . . . . . . . . . . 45 H. L. Grubin EPITAXIAL GROWTH FOR SUB MICRON STRUCTURES.................. 179 C. E. C. Wood INSULATOR/SEMICONDUCTOR INTERFACES.......................... 195 C. W. Wilms en THEORY OF THE ELECTRONIC STRUCTURE OF SEMICONDUCTOR SURFACES AND INTERFACES...................

  2. Thin film coated submicron gratings: theory, design, fabrication and application

    Heine, C.


    The realization of new applications of submicron grating structures requires efficient theoretical methods and elaborate fabrication techniques. In this work rigorous diffraction theory for one-dimensional gratings has been investigated and optimization techniques, based on methods used in thin film optics, have been developed. Submicron gratings embossed in polycarbonate have been fabricated and characterized. This includes transmission measurements which are in good agreement with theoretical calculations. Designs for a wide range of optical filters, which lead to improved optical and mechanical properties, are presented. This has been demonstrated for broadband antireflection structures for solar energy applications, based on MgF{sub 2}-coated gratings. (author) figs., tabs., refs.


    Zhou Yuming; Xu Baowen


    Accuracy and roughness, proposed by Pawlak(1982), might draw a conclusion inconsistent with our intuition in some cases. This letter analyzes the limitations in these measures and proposes improved accuracy and roughness measures based on information theory.

  4. Surface Roughness Effects on Discharge Coefficient of Broad Crested Weir

    Shaker A. Jalil


    Full Text Available The aim of this study is to investigate the effects of surface roughness sizes on the discharge coefficient for a broad crested weirs. For this purpose, three models having different lengths of broad crested weirs were tested in a horizontal flume. In each model, the surface was roughed four times. Experimental results of all models showed that the logical negative effect of roughness increased on the discharge (Q for different values of length. The performance of broad crested weir improved with decrease ratio of roughness to the weir height (Ks/P and with the increase of the total Head to the Length (H/L. An empirical equation was obtained to estimate the variation of discharge coefficient Cd in terms total head to length ratio, with total head to roughness ratio.

  5. Role of free carriers excited by ultrafast Bessel beams for submicron structuring applications

    Velpula, Praveen Kumar; Bhuyan, Manoj Kumar; Mauclair, Cyril; Colombier, Jean-Philippe; Stoian, Razvan


    Ultrafast Bessel beams are ideal sources for high aspect ratio submicron structuring applications because of their nondiffracting nature and higher stability in nonlinear propagation. We report here on the interaction of ultrafast Bessel beams at various laser energies and pulse durations with transparent materials (fused silica) and define their impact on photoinscription regimes, i.e., formation of positive and negative refractive index structures. The laser pulse duration was observed to be key in deciding the type of the structures via excitation efficiency. To understand the relevant mechanisms for forming these different structures, the free carrier behavior as a function of laser pulse duration and energy was studied by capturing instantaneous excitation profiles using time-resolved microscopy. Time-resolved imaging and simulation studies reveal that low carrier densities are generated for ultrashort pulses, leading to soft positive index alterations via presumably nonthermally induced structural transitions involving defects. On the other hand, the high free carrier density generation in the case of longer pulse durations leads to hydrodynamic expansion, resulting in high aspect ratio submicron-size wide voids. Delayed ionization, carrier defocusing, and lower nonlinear effects are responsible for the confinement of energy, resulting in efficient energy deposition on-axis.

  6. Effects of deformation on microstructures and properties of submicron crystalline Cu-5%Cr alloy

    HE Wen-xiong; WANG Er-de; CHEN Hui; YU Yang; LIU Jing-lei


    Warm extrusion of submicron crystalline Cu-5%Cr from 100 ℃ to 600 ℃ was investigated. The effects of different extrusion ratios and different extrusion temperatures on microstructures and properties of submicron crystalline Cu-5%Cr were studied. The microstructures of the extruded Cu-5%Cr were characterized by backscattered electron images(BSE) and transmission electron microscopy(TEM). The mechanical properties of the extruded Cu-5%Cr were measured by means of microhardness and tension test. The results show that, the deformation, dynamic recovery and dynamic recrystallization of the extruded Cu-5%Cr are mainly produced in Cu matrix. The higher extrusion ratio leads to more uniform microstructure and finer Cu grains. When being extruded in the range of 100-600 ℃, dynamic recovery of Cu is the dominant process, and dynamic recrystallization of Cu occurred above 300 ℃ is far from end. The most part of microstructure of as-extruded Cu-5%Cr is subcrystallines produced by dynamic recovery, only a few recrystallines exist, and the average size of these grains is not larger than 400 nm. With extrusion temperature rising, the tensile strength and microhardness of Cu-5%Cr decrease, and elongation increases gradually.

  7. Bloch-Wave Engineered Submicron Diameter Micropillars with Quality Factors Exceeding 10,000

    Hofling, S.; Lermer, M.; Gregersen, Niels;


    Adiabatic design submicron diameter quantum-dot micropillars have been designed and implemented for cavity quantum electrodynamics experiments. Ultra-high experimental quality factors (>10,000) are obtained for submicron diameters and strong light-matter interaction is observed.......Adiabatic design submicron diameter quantum-dot micropillars have been designed and implemented for cavity quantum electrodynamics experiments. Ultra-high experimental quality factors (>10,000) are obtained for submicron diameters and strong light-matter interaction is observed....

  8. Fabrication of pullulan and pectin submicron fibers by electrospinning

    Pullulan (PUL), a food grade polysaccharide, was fabricated into fibrous mats from fibers of submicron size by electrospinning. The effects of inorganic salts and polyanions present in the electrospinning solution on the properties of the resultant fibers was investigated. The inclusion of exogenous...

  9. Analog Circuits in Ultra-Deep-Submicron CMOS

    Annema, Anne-Johan; Nauta, Bram; Langevelde, van Ronald; Tuinhout, Hans


    Modern and future ultra-deep-submicron (UDSM) technologies introduce several new problems in analog design. Nonlinear output conductance in combination with reduced voltage gain pose limits in linearity of (feedback) circuits. Gate-leakage mismatch exceeds conventional matching tolerances. Increasin

  10. Spinning of a submicron sphere by Airy beams.

    Kim, Kyoung-Youm; Kim, Saehwa


    We show that by employing two incoherent counter-propagating Airy beams, we can manipulate a submicron sphere to spin around a transverse axis. We can control not only the spinning speed, but also the direction of the spinning axis by changing the polarization directions of Airy beams.

  11. UV Light–Induced Aggregation of Titania Submicron Particles

    Can Zhou


    Full Text Available In this study, aggregation of TiO2 (rutile and anatase submicron particles in deionized (DI water under ultra-violet (UV light irradiation was investigated. While no aggregation was observed in the dark, rutile and anatase submicron particles started aggregating upon application of UV light and ceased aggregation in about 2 and 8.4 h, respectively. It has been demonstrated that UV light directly mitigated the particle mobility of TiO2, resulting in a neutralization effect of the Zeta potential. It was also observed that rutile particles aggregated much faster than anatase particles under UV radiation, indicating that the Zeta potential of as-prepared rutile is less than that of anatase in deionized (DI water. In addition, the interaction energy of rutile and anatase particles was simulated using the Derjaguin–Landau–Verwey–Overbeek (DLVO model. The results showed a significant reduction of barrier energy from 118.2 kBT to 33.6 kBT for rutile and from 333.5 kBT to 46.1 kBT for anatase, respectively, which further validated the remarkable influence of UV irradiation on the aggregation kinetics of rutile and anatase submicron particles. This work presents a further understanding of the aggregation mechanism of light-controlled submicron particles and has a promising potential application in environmental remediation.

  12. Pharmacokinetic performance of the nitrendipine intravenous submicron emulsion in rats

    Jibin Guan


    Full Text Available To compare pharmacokinetic behaviors of nitrendipine submicron emulsion with nitrendipine solution following intravenous administration in rats. The plasma concentrations were analyzed by ultra-performance liquid chromatography coupled with tandem mass spectrometry detection (UPLC–MS/MS through a new validated method. The pharmacokinetic parameters of the nitrendipine submicron emulsion and nitrendipine solution were as follows: AUC0–t 900.76 ± 186.59 versus 687.08 ± 66.24 ng h/ml, Cmax 854.54 ± 159.48 versus 610.59 ± 235.99 ng/ml, t1/2 2.37 ± 1.99 versus 2.80 ± 2.69 h. The relative bioavailability of nitrendipine submicron emulsion to nitrendipine solution was 131.4 ± 11.3%. The developed methods could meet the requirements of bioanalysis. Compared to the solution injection, intravenous submicron emulsion presents higher systematic exposure which can help to improve the therapeutic efficacy.

  13. Edge effects and submicron tracks in magnetic tape recording

    Hozoi, Adrian


    The scope of the work presented in this thesis was to investigate the recording phenomena at very high track density and understand the requirements for reaching submicron tracks in magnetic tape. A broad study of edge effects is presented with a focus on side writing and erasing, which are critical

  14. Reversal mechanism of submicron patterned CoNi/Pt multilayers

    Haast, M.A.M.; Schuurhuis, J.R.; Abelmann, L.; Lodder, J.C.; Popma, Th.J.A.


    With laser interference lithography Co50Ni50/Pt multilayers with perpendicular magnetic anisotropy have been patterned into regular matrices of submicron sized dots. Their magnetic properties have been studied with Vibrating Sample Magnetometry. Compared to continuous multilayers (Hc=15 kA/m) the co

  15. Pavement roughness and skid properties

    Road roughness and roadway safety as it relates to both surface and air transportation are discussed. The role of road roughness in vehicle ride, the measurement of roughness, the evaluation of riding confort, and the effect of grooving pavements are discussed. The effects of differential pavement friction on the response of cars in skidding maneuvers is discussed.

  16. Modelling dynamic roughness during floods

    Paarlberg, Andries; Dohmen-Janssen, Catarine M.; Hulscher, Suzanne J.M.H.; Termes, A.P.P.


    In this paper, we present a dynamic roughness model to predict water levels during floods. Hysteresis effects of dune development are explicitly included. It is shown that differences between the new dynamic roughness model, and models where the roughness coefficient is calibrated, are most

  17. Rough-Granular Computing

    Andrzej Skowron


    Solving complex problems by multi-agent systems in distributed environments requires new approximate reasoning methods based on new computing paradigms. One such recently emerging computing paradigm is Granular Computing(GC). We discuss the Rough-Granular Computing(RGC) approach to modeling of computations in complex adaptive systems and multiagent systems as well as for approximate reasoning about the behavior of such systems. The RGC methods have been successfully applied for solving complex problems in areas such as identification of objects or behavioral patterns by autonomous systems, web mining, and sensor fusion.

  18. On Random Rough Sets

    Weizhi Wu


    In this paper,the concept of a random rough set which includes the mechanisms of numeric and non-numeric aspects of uncertain knowledge is introduced. It is proved that for any belief structure and its inducing belief and plausibility measures there exists a random approximation space such that the associated lower and upper probabilities are respectively the given belief and plausibility measures, and vice versa. And for a random approximation space generated from a totally random set, its inducing lower and upper probabilities are respectively a pair of necessity and possibility measures.

  19. Atmospheric Chemistry Special Feature: Carbohydrate-like composition of submicron atmospheric particles and their production from ocean bubble bursting

    Russell, Lynn M.; Hawkins, Lelia N.; Frossard, Amanda A.; Quinn, Patricia K.; Bates, Tim S.


    Oceans cover over two-thirds of the Earth's surface, and the particles emitted to the atmosphere by waves breaking on sea surfaces provide an important contribution to the planetary albedo. During the International Chemistry Experiment in the Arctic LOwer Troposphere (ICEALOT) cruise on the R/V Knorr in March and April of 2008, organic mass accounted for 15-47% of the submicron particle mass in the air masses sampled over the North Atlantic and Arctic Oceans. A majority of this organic component (0.1 - 0.4 μ m-3) consisted of organic hydroxyl (including polyol and other alcohol) groups characteristic of saccharides, similar to biogenic carbohydrates found in seawater. The large fraction of organic hydroxyl groups measured during ICEALOT in submicron atmospheric aerosol exceeded those measured in most previous campaigns but were similar to particles in marine air masses in the open ocean (Southeast Pacific Ocean) and coastal sites at northern Alaska (Barrow) and northeastern North America (Appledore Island and Chebogue Point). The ocean-derived organic hydroxyl mass concentration during ICEALOT correlated strongly to submicron Na concentration and wind speed. The observed submicron particle ratios of marine organic mass to Na were enriched by factors of ˜102-˜103 over reported sea surface organic to Na ratios, suggesting that the surface-controlled process of film bursting is influenced by the dissolved organic components present in the sea surface microlayer. Both marine organic components and Na increased with increasing number mean diameter of the accumulation mode, suggesting a possible link between organic components in the ocean surface and aerosol-cloud interactions.

  20. Rough weather rescue



    This report, which was commissioned by the Offshore Division of the Health and Safety Executive, reviews the type of equipment and techniques used to rescue people from the water around offshore platforms in rough weather. It also examines the limitations of the equipment in extreme conditions and reports the views of the various industry sectors (as determined by a questionnaire survey). The type of incidents covered by the report include: man overboard; helicopter ditching; and evacuation from totally enclosed motor propelled survival craft (TEMPSC) and life rafts. The report considers: the approach taken by other oil-producing countries; current escape, evacuation and rescue (EER) practices for the UK Continental Shelf (UKCS); environmental limits; methods for rescue and recovery from the water and TEMPSC; launch and recovery systems; fast rescue craft (FSC) and daughter craft; emergency response and rescue vessels; helicopters; casualty personal protection equipment; claimed versus actual equipment performance; training and practice procedures; attitudes to environmental limits; lessons learnt from incidents; mechanical recovery devices; equipment design and use in rough weather; and recommendations for improvements.

  1. Numerical simulation of pulsatile flow in rough pipes

    Chin, Cheng; Monty, Jason; Ooi, Andrew; Illingworth, Simon; Marusic, Ivan; Skvortsov, Alex


    Direct numerical simulation (DNS) of pulsatile turbulent pipe flow is carried out over three-dimensional sinusoidal surfaces mimicking surface roughness. The simulations are performed at a mean Reynolds number of Reτ 540 (based on friction velocity, uτ, and pipe radii, δ) and at various roughness profiles following the study of Chan et al., where the size of the roughness (roughness semi-amplitude height h+ and wavelength λ+) is increased geometrically while maintaining the height-to-wavelength ratio of the sinusoidal roughness element. Results from the pulsatile simulations are compared with non-pulsatile simulations to investigate the effects of pulsation on the Hama roughness function, ΔU+ . Other turbulence statistics including mean turbulence intensities, Reynolds stresses and energy spectra are analysed. In addition, instantaneous phase (eg. at maximum and minimum flow velocities) and phase-averaged flow structures are presented and discussed.

  2. Development of eco-friendly submicron emulsions stabilized by a bio-derived gum.

    Pérez-Mosqueda, Luis María; Ramírez, Pablo; Trujillo-Cayado, Luis Alfonso; Santos, Jenifer; Muñoz, José


    Many traditional organic solvents are being gradually replaced by ecofriendly alternatives. D-Limonene is a terpenic (bio)-solvent that fulfils the requirements to be considered a green solvent. D-Limonene sub-micron emulsions suffer from Ostwald ripening destabilization. In this study, we examined the influence of the addition of a natural gum (rosin gum) to D-limonene in order to prevent Ostwald ripening. This contribution deals with the study of emulsions formulated with a mixture of D-limonene and rosin gum as dispersed phase and Pluronic PE9400 as emulsifier. The procedure followed for the development of these formulations was based on the application of product design principles. This led to the optimum ratio rosin gum/D-limonene and subsequently to the optimum surfactant concentration. The combination of different techniques (rheology, laser diffraction and multiple light scattering) was demonstrated to be a powerful tool to assist in the prediction of the emulsions destabilization process. Not only did the addition of rosin gum highly increase the stability of these emulsions by inhibiting the Ostwald ripening, but it also reduced the emulsions droplet size. Thus, we found that stable sub-micron D-limonene-in-water emulsions have been obtained in the range 3-6 wt% Pluronic PE-9400 by means of a single-step rotor/stator homogenizing process.

  3. Rough Surface Contact

    T Nguyen


    Full Text Available This paper studies the contact of general rough curved surfaces having nearly identical geometries, assuming the contact at each differential area obeys the model proposed by Greenwood and Williamson. In order to account for the most general gross geometry, principles of differential geometry of surface are applied. This method while requires more rigorous mathematical manipulations, the fact that it preserves the original surface geometries thus makes the modeling procedure much more intuitive. For subsequent use, differential geometry of axis-symmetric surface is considered instead of general surface (although this “general case” can be done as well in Chapter 3.1. The final formulas for contact area, load, and frictional torque are derived in Chapter 3.2.

  4. Experimental demonstration of an on-chip polarization splitter in a submicron asymmetric dielectric-coated metal slit

    Chen, Jianjun, E-mail:; Sun, Chengwei; Gong, Qihuang [State Key Laboratory for Mesoscopic Physics and Department of Physics, Peking University, Beijing 100871 (China); Collaborative Innovation Center of Quantum Matter, Beijing (China); Li, Hongyun [State Key Laboratory for Mesoscopic Physics and Department of Physics, Peking University, Beijing 100871 (China)


    A submicron asymmetric dielectric-coated metal slit with a Fabry–Perot (FP) nano-resonator is experimentally fabricated to realize an ultra-small on-chip polarization splitter. In the hybrid plasmonic structure, both of the transverse-electric (TE) and transverse-magnetic (TM) modes can be efficiently generated on the front metal surface. Based on the quite different resonant conditions and the different field confinements of the two orthogonal polarization modes in the FP resonator, the TM and TE modes are generated to propagate in the opposite directions along the metal surface. In this device, there are no coupling waveguide regions, and the excitation and the splitting of the TE and TM modes are integrated into the same asymmetric nano-slit. This considerably shrinks the device dimension to only about 850 nm (about one wavelength). In such a submicron asymmetric slit, the measured extinction ratios for the two opposite directions can reach up to (η{sub L}/η{sub R}){sup TM} ≈ 1:14 and (η{sub L}/η{sub R}){sup TE} ≈ 11:1 at λ = 820 nm. This on-chip submicron polarization splitter is of importance in highly integrated photonic circuits.

  5. On the acoustic properties of vaporized submicron perfluorocarbon droplets.

    Reznik, Nikita; Lajoinie, Guillaume; Shpak, Oleksandr; Gelderblom, Erik C; Williams, Ross; de Jong, Nico; Versluis, Michel; Burns, Peter N


    The acoustic characteristics of microbubbles created from vaporized submicron perfluorocarbon droplets with fluorosurfactant coating are examined. Utilizing ultra-high-speed optical imaging, the acoustic response of individual microbubbles to low-intensity diagnostic ultrasound was observed on clinically relevant time scales of hundreds of milliseconds after vaporization. It was found that the vaporized droplets oscillate non-linearly and exhibit a resonant bubble size shift and increased damping relative to uncoated gas bubbles due to the presence of coating material. Unlike the commercially available lipid-coated ultrasound contrast agents, which may exhibit compression-only behavior, vaporized droplets may exhibit expansion-dominated oscillations. It was further observed that the non-linearity of the acoustic response of the bubbles was comparable to that of SonoVue microbubbles. These results suggest that vaporized submicron perfluorocarbon droplets possess the acoustic characteristics necessary for their potential use as ultrasound contrast agents in clinical practice.

  6. Laser processing of silicon at submicron scale using photochromic films

    Chen Qiying; Nikumb, Suwas


    Laser fabrication at submicron scale is experimentally demonstrated with the nonlinear optical switching effect of photochromism. The effect, which is a result of change in the optical properties of the photochromic material between the open-ring and closed-ring isomers during the photoisomerization, effectively reduces the laser beam size. The ultrafast response of the molecular photocyclization and cycloreversion reactions at a time scale of a few picoseconds ensures the instantaneous realization of the effect. Utilizing a photochromic film of cis-1,2-dicyano-1,2-bis(2,4,5-trimethyl-3-thienyl) ethane as the mask layer, laser processing of a silicon wafer demonstrated submicron scale feature size with improved surface quality as compared to the smallest features achievable using direct laser ablation without the photochromic film.

  7. Submicron CMOS technologies for high energy physics and space applications

    Anelli, G; Faccio, F; Heijne, Erik H M; Jarron, Pierre; Kloukinas, Kostas C; Marchioro, A; Moreira, P; Snoeys, W


    The radiation environment present in some of today's High-Energy Physics (HEP) experiments and in space has a detrimental influence on the integrated circuits working in these environments. Special technologies, called radiation hardened, have been used in the past to prevent the radiation-induced degradation. In the last decades, the market of these special technologies has undergone a considerable shrinkage, rendering them less reliably available and far more expensive than today's mainstream technologies. An alternative approach is to use a deep submicron CMOS technology. The most sensitive part to radiation effects in a MOS transistor is the gate oxide. One way to reduce the effects of ionizing radiation in the gate oxide is to reduce its thickness, which is a natural trend in modern technologies. Submicron CMOS technologies seem therefore a good candidate for implementing radiation-hardened integrated circuits using a commercial, inexpensive technology. Nevertheless, a certain number of radiation-induced...

  8. Rough Sets and Nuclear Safety


    It is well-known that rough set theory can be applied successfully to rough classification and knowledge discovery. Our work is concerned with finding methods for using rough sets to identify classes in datasets, finding dependencies in relations and discovering rules which are hidden in databases by means of decision tables and algorithm D. We use these methods to analyze and control aspects of nuclear energy generation.

  9. Submicron Resolution Spectral-Domain Optical Coherence Tomography

    Alarousu, Erkki


    Apparatuses and systems for submicron resolution spectral-domain optical coherence tomography (OCT) are disclosed. The system may use white light sources having wavelengths within 400-1000 nanometers, and achieve resolution below 1 .mu.m. The apparatus is aggregated into a unitary piece, and a user can connect the apparatus to a user provided controller and/or light source. The light source may be a supercontinuum source.

  10. Fabrication of submicron proteinaceous structures by direct laser writing

    Serien, Daniela [Center for International Research on Integrative Biomedical Systems, Institute of Industrial Science, The University of Tokyo, 4-6-1 Komaba, Meguro-ku, 153-8505 Tokyo (Japan); Takeuchi, Shoji, E-mail: [Center for International Research on Integrative Biomedical Systems, Institute of Industrial Science, The University of Tokyo, 4-6-1 Komaba, Meguro-ku, 153-8505 Tokyo (Japan); ERATO Takeuchi Biohybrid Innovation Project, Japan Science and Technology Agency, 4-6-1 Komaba, Meguro-ku, 153-8505 Tokyo (Japan)


    In this paper, we provide a characterization of truly free-standing proteinaceous structures with submicron feature sizes depending on the fabrication conditions by model-based analysis. Protein cross-linking of bovine serum albumin is performed by direct laser writing and two-photon excitation of flavin adenine dinucleotide. We analyze the obtainable fabrication resolution and required threshold energy for polymerization. The applied polymerization model allows prediction of fabrication conditions and resulting fabrication size, alleviating the application of proteinaceous structure fabrication.

  11. Roughness Measurement of Dental Materials

    Shulev Assen


    Full Text Available This paper presents a roughness measurement of zirconia ceramics, widely used for dental applications. Surface roughness variations caused by the most commonly used dental instruments for intraoral grinding and polishing are estimated. The applied technique is simple and utilizes the speckle properties of the scattered laser light. It could be easily implemented even in dental clinic environment. The main criteria for roughness estimation is the average speckle size, which varies with the roughness of zirconia. The algorithm used for the speckle size estimation is based on the normalized autocorrelation approach.

  12. Roughness Measurement of Dental Materials

    Shulev, Assen; Roussev, Ilia; Karpuzov, Simeon; Stoilov, Georgi; Ignatova, Detelina; See, Constantin von; Mitov, Gergo


    This paper presents a roughness measurement of zirconia ceramics, widely used for dental applications. Surface roughness variations caused by the most commonly used dental instruments for intraoral grinding and polishing are estimated. The applied technique is simple and utilizes the speckle properties of the scattered laser light. It could be easily implemented even in dental clinic environment. The main criteria for roughness estimation is the average speckle size, which varies with the roughness of zirconia. The algorithm used for the speckle size estimation is based on the normalized autocorrelation approach.

  13. Scanning SQUID susceptometers with sub-micron spatial resolution

    Kirtley, John R., E-mail:; Rosenberg, Aaron J.; Palmstrom, Johanna C.; Holland, Connor M.; Moler, Kathryn A. [Department of Applied Physics, Stanford University, Stanford, California 94305-4045 (United States); Paulius, Lisa [Department of Physics, Western Michigan University, Kalamazoo, Michigan 49008-5252 (United States); Spanton, Eric M. [Department of Physics, Stanford University, Stanford, California 94305-4045 (United States); Schiessl, Daniel [Attocube Systems AG, Königinstraße 11A, 80539 Munich (Germany); Jermain, Colin L.; Gibbons, Jonathan [Department of Physics, Cornell University, Cornell, Ithaca, New York 14853 (United States); Fung, Y.-K.K.; Gibson, Gerald W. [IBM Research Division, T. J. Watson Research Center, Yorktown Heights, New York 10598 (United States); Huber, Martin E. [Department of Physics, University of Colorado Denver, Denver, Colorado 80217-3364 (United States); Ralph, Daniel C. [Department of Physics, Cornell University, Cornell, Ithaca, New York 14853 (United States); Kavli Institute at Cornell, Ithaca, New York 14853 (United States); Ketchen, Mark B. [OcteVue, Hadley, Massachusetts 01035 (United States)


    Superconducting QUantum Interference Device (SQUID) microscopy has excellent magnetic field sensitivity, but suffers from modest spatial resolution when compared with other scanning probes. This spatial resolution is determined by both the size of the field sensitive area and the spacing between this area and the sample surface. In this paper we describe scanning SQUID susceptometers that achieve sub-micron spatial resolution while retaining a white noise floor flux sensitivity of ≈2μΦ{sub 0}/Hz{sup 1/2}. This high spatial resolution is accomplished by deep sub-micron feature sizes, well shielded pickup loops fabricated using a planarized process, and a deep etch step that minimizes the spacing between the sample surface and the SQUID pickup loop. We describe the design, modeling, fabrication, and testing of these sensors. Although sub-micron spatial resolution has been achieved previously in scanning SQUID sensors, our sensors not only achieve high spatial resolution but also have integrated modulation coils for flux feedback, integrated field coils for susceptibility measurements, and batch processing. They are therefore a generally applicable tool for imaging sample magnetization, currents, and susceptibilities with higher spatial resolution than previous susceptometers.


    İsmail Aydın


    Full Text Available Some visual characteristics of wood such as color, pattern and texture determine the quality of manufactured products. Surface properties of wood material are important both in production and marketing after production. Initial studies related to the roughness of wood surface were begun in early 1950’s. However, no general agreed standardization can not have been developed for wood surfaces. Surface roughness of wood is function of the production process, product type and the natural anatomical properties of wood. Contact and non-contact tracing methods are used to measure of wood surface roughness. Surface roughness also affects the gluability and wettability of wood surfaces. The success in finishing also depends on the surface roughness of wood.

  15. The investigation of ferromagnetic resonance linewidth in Ni80Fe20 films with submicron rectangular elements

    D. Zhang


    Full Text Available Patterned magnetic films with nano-scaled dots exhibit some special magnetic properties. In this paper, we investigate the in-plane shape anisotropy and the magnetization dynamic damping in permalloy (Ni80Fe20 arrays of submicron rectangular elements using ferromagnetic resonance (FMR. The FMR linewidth exhibits a dependence on the element size, and mainly comes from the contribution of the intrinsic damping. Also the contribution of two-magnon scattering plays an important role and is reduced with increasing aspect ratio. The damping coefficient decreases from 0.0129 to 0.0118 with the element length increasing from 300 nm to 1200 nm, and the theoretical calculation suggests that the change of damping results from the longitudinal and transverse interlayer spin current due to the spatially inhomogeneous magnetization dynamics.

  16. Insights into Submicron Aerosol Composition and Sources from the WINTER Aircraft Campaign Over the Eastern US.

    Schroder, J. C.; Campuzano Jost, P.; Day, D. A.; Fibiger, D. L.; McDuffie, E. E.; Blake, N. J.; Hills, A. J.; Hornbrook, R. S.; Apel, E. C.; Weinheimer, A. J.; Campos, T. L.; Brown, S. S.; Jimenez, J. L.


    The WINTER aircraft campaign was a recent field experiment to probe the sources and evolution of gas pollutants and aerosols in Northeast US urban and industrial plumes during the winter. A highly customized Aerodyne aerosol mass spectrometer (AMS) was flown on the NCAR C-130 to characterize submicron aerosol composition and evolution. Thirteen research flights were conducted covering a wide range of conditions, including rural, urban, and marine environments during day and night. Organic aerosol (OA) was a large component of the submicron aerosol in the boundary layer. The fraction of OA (fOA) was smaller (35-40%) than in recent US summer campaigns (~60-70%). Biomass burning was observed to be an important source of OA in the boundary layer, which is consistent with recent wintertime studies that show a substantial contribution of residential wood burning to the OA loadings. OA oxygenation (O/C ratio) shows a broad distribution with a substantial fraction of smaller O/C ratios when compared to previous summertime campaigns. Since measurements were rarely made very close to primary sources (i.e. directly above urban areas), this is consistent with oxidative chemistry being slower during winter. SOA formation and aging in the NYC plume was observed during several flights and compared with summertime results from LA (CalNex) and Mexico City (MILAGRO). Additionally, an oxidation flow reactor (OFR) capable of oxidizing ambient air up to several equivalent days of oxidation was deployed for the first time in an aircraft platform. The aerosol outflow of the OFR was sampled with the AMS to provide real-time snapshots of the potential for aerosol formation and aging. For example, a case study of a flight through the Ohio River valley showed evidence of oxidation of SO2 to sulfate. The measured sulfate enhancements were in good agreement with our OFR chemical model. OFR results for SOA will be discussed.

  17. Bankruptcy Prediction with Rough Sets

    J.C. Bioch (Cor); V. Popova (Viara)


    textabstractThe bankruptcy prediction problem can be considered an or dinal classification problem. The classical theory of Rough Sets describes objects by discrete attributes, and does not take into account the order- ing of the attributes values. This paper proposes a modification of the Rough Set

  18. Study of the roughness in a photoresist masked, isotropic, SF6-based ICP silicon etch

    Larsen, Kristian Pontoppidan; Petersen, Dirch Hjorth; Hansen, Ole


    In this paper we study the etching behavior and the resulting roughness in photoresist-masked isotropic silicon plasma etch performed in an inductively coupled plasma (ICP) etcher using SF6. We report detailed observations of the resulting roughness for various etching parameters, covering......: pressure from 2.5 to 70 mTorr, SF6 flow rate from 50 to 300 sccm, platen power from 0 to 16 W, and ICP power from 1000 to 3000 W. Etch processes with a normalized roughness below 0.005 were found at low pressure, p = 10 mTorr, while larger normalized roughness, above 0.02, occurred at higher pressures, p...... = 40 - 70 mTorr. Here the normalized roughness is the ratio of the roughness amplitude to the etch depth. The rough etching processes showed characteristic high-aspect-ratio and crystal-orientation-dependent surface morphology. The temporal evolution of this roughness was studied, and observations...

  19. High Proportions of Sub-micron Particulate Matter in Icelandic Dust Storms in 2015

    Dagsson Waldhauserova, Pavla; Arnalds, Olafur; Olafsson, Haraldur; Magnusdottir, Agnes


    Iceland is extremely active dust region and desert areas of over 44,000 km2 acknowledge Iceland as the largest Arctic and European desert. Frequent dust events, up to 135 dust days annually, transport dust particles far distances towards the Arctic and Europe. Satellite MODIS pictures have revealed dust plumes exceeding 1,000 km. The annual dust deposition was calculated as 40.1 million tons yr-1. Two dust storms were measured in transverse horizontal profile about 90 km far from different dust sources in southwestern Iceland in the summer of 2015. Aerosol monitor DustTrak DRX 8533EP was used to measure PM mass concentrations corresponding to PM1, PM2.5, PM4, PM10 and the total PM15 at several places within the dust plume. Images from camera network operated by the Icelandic Road and Coastal Administration were used to estimate the visibility and spatial extent of measured dust events. A numerical simulation of surface winds was carried out with the numerical model HIRLAM with horizontal resolution of 5 km and used to calculate the total dust flux from the sources. The in situ measurements inside the dust plumes showed that aeolian dust can be very fine. The study highlights that suspended volcanic dust in Iceland causes air pollution with extremely high PM1 concentrations comparable to the polluted urban stations in Europe or Asia rather than reported dust event observations from around the world. The PM1/PM2.5 ratios are generally low during dust storms outside of Iceland, much lower than > 0.9 and PM1/PM10 ratios of 0.34-0.63 found in our study. It shows that Icelandic volcanic dust consists of higher proportion of submicron particles compared to crustal dust. The submicron particles are predicted to travel long distances. Moreover, such submicron particles pose considerable health risk because of high potential for entering the lungs. Icelandic volcanic glass has often fine pipe-vesicular structures known from asbestos and high content of heavy metals. Previous

  20. S-Rough communication and its characteristics

    Hu Haiqing; Wang Yan; Shi Kaiquan


    In view of certain defects of common rough communication, using the S-rough sets, this article presents a S-rough communication model. The S-rough communication model is the extension of the common rough communication model.S-rough communication has two kinds of forms: one-direction S-rough communication and two-direction S-rough communication. The mathematical structure and characteristics of the one-direction S-rough communication and the two-direction S-rough communication, the relationship theorem between the one-direction S-rough communication and the two-direction S-rough communication are also presented. The S-rough communication is a dynamic communication method,and it is a novel research direction in rough sets field.

  1. Radiation tolerant VLSI circuits in standard deep submicron CMOS technologies for the LHC experiments practical design aspects

    Anelli, G; Delmastro, M; Faccio, F; Floria, S; Giraldo, A; Heijne, Erik H M; Jarron, Pierre; Kloukinas, Kostas C; Marchioro, A; Moreira, P; Snoeys, W


    We discuss design issues related to the extensive use of Enclosed Layout Transistors (ELT's) and guard rings in deep submicron CMOS technologies in order to improve radiation tolerance of ASIC's designed for the LHC experiments (the Large Hadron Collider at present under construction at CERN). We present novel aspects related to the use of ELT's: noise measured before and after irradiation up to 100 Mrad (SiO/sub 2/), a model to calculate the W/L ratio and matching properties of these devices. Some conclusions concerning the density and the speed of IC's conceived with this design approach are finally drawn. (16 refs).


    İsmail Aydın; Gürsel Çolakoğlu


    Some visual characteristics of wood such as color, pattern and texture determine the quality of manufactured products. Surface properties of wood material are important both in production and marketing after production. Initial studies related to the roughness of wood surface were begun in early 1950’s. However, no general agreed standardization can not have been developed for wood surfaces. Surface roughness of wood is function of the production process, product type and the natural anatomic...

  3. Characterization and analysis of micro channels and sub-micron surface roughness of injection moulded microfluidic systems using optical metrology

    Tosello, Guido; Marinello, Francesco; Hansen, Hans Nørgaard


    measuring machine and a white light interferometer respectively. The effect of the dimensional scale range on the micro/nano features replication was evaluated and it was found to be the dominant parameter if compared with the effect of the other process-related parameters investigated (melt and mould...... temperature, injection speed)....

  4. Characterization and analysis of micro channels and sub-micron surface roughness of injection moulded microfluidic systems using optical metrology

    Tosello, Guido; Marinello, Francesco; Hansen, Hans Nørgaard


    measuring machine and a white light interferometer respectively. The effect of the dimensional scale range on the micro/nano features replication was evaluated and it was found to be the dominant parameter if compared with the effect of the other process-related parameters investigated (melt and mould...... temperature, injection speed)....

  5. Submicron Defect Detection in Periodic Structures Using Photorefractive Holography

    Uhrich, Craig Edward

    Detection of defects in periodic objects is an important step in the manufacture of integrated circuits, particularly memory chips which are highly repetitive. As feature sizes shrink below 1 mum, automated detection of sub-micron defects becomes necessary. We present a real-time holographic system which allows the detection of sub-micron defects in periodic structures. The inspection technique is a marriage of Fourier spatial filtering and real-time phase conjugate holography. The system output is a near diffraction limited image of any defects in the pattern (defined to be any deviations from periodicity). Real-time holographic recording allows the system to adapt to the orientation and period of the object. The early chapters introduce the photorefractive effect and the generation of the phase conjugate of an optical wavefront using Bi_{12} SiO_{20}. Relevant properties of the optical Fourier transform are also discussed. The following sections present the system design rules and experimental techniques which allow the system to reliably detect sub-micron defects. The most important improvements over previous demonstrations are (1) a novel write/read holographic process which increases phase conjugate reflectivity by orders of magnitude, (2) control of the light polarization to allow efficient object illumination and collection of the diffracted signal, (3) avoidance of noise by moving the crystal away from the origin of the Fourier plane, and (4) compensation for the crystal aberrations with a holographic optical element. The final chapter presents results which clearly show enhancement of sub-micron defects and near perfect suppression of the surrounding periodic patterns. An area larger than 1 mm^2 is inspected in 20-60 seconds. Over 90% of the 0.5 mu m diameter defects on glass masks (viewed in reflection) are detected, and approximately 80% of defects in the 0.2 -0.3 μm range are found. On silicon wafers, the results are even better with over a 95% success

  6. Noise estimation for deep sub-micron integrated circuits

    陈彬; 杨华中; 汪惠


    Noise analysis and avoidance are an increasingly critical step in the design of deep submicron (DSM) integrated circuits (Ics). The crosstalk between neighboring interconnects gradually becomes the main noise sources in DSM Ics. We introduce an efficient and accurate noise-evaluation method for capacitively coupled nets of Ics. The method holds for a victim net with arbitrary number of aggressive nets under ramp input excitation. For common RC nets extracted by electronic design automation (EDA) tools, the deviation between our method and HSPICE is under 10%.

  7. Submicron particle monitoring of paving and related road construction operations.

    Freund, Alice; Zuckerman, Norman; Baum, Lisa; Milek, Debra


    This study identified activities and sources that contribute to ultrafine and other submicron particle exposure that could trigger respiratory symptoms in highway repair workers. Submicron particle monitoring was conducted for paving, milling, and pothole repair operations in a major metropolitan area where several highway repair workers were identified as symptomatic for respiratory illness following exposures at the 2001 World Trade Center disaster site. Exposure assessments were conducted for eight trades involved in road construction using a TSI P-Trak portable condensation particle counter. Direct readings near the workers' breathing zones and observations of activities and potential sources were logged on 7 days on 27 workers using four different models of pavers and two types of millers. Average worker exposure levels ranged from 2 to 3 times background during paving and from 1 to 4 times background during milling. During asphalt paving, average personal exposures to submicron particulates were 25,000-60,000, 28,000-70,000, and 23,000-37,000 particles/ cm(3) for paver operators, screed operators, and rakers, respectively. Average personal exposures during milling were 19,000-111,000, 28,000-81,000, and 19,000 particles/cm(3) for the large miller operators, miller screed operators, and raker, respectively. Personal peak exposures were measured up to 467,000 and 455,000 particles/cm(3) in paving and milling, respectively. Several sources of submicron particles were identified. These included the diesel and electric fired screed heaters; engine exhaust from diesel powered construction vehicles passing by or idling; raking, dumping, and paving of asphalt; exhaust from the hotbox heater; pavement dust or fumes from milling operations, especially when the large miller started and stopped; and secondhand cigarette smoke. To reduce the potential for health effects in workers, over 40 recommendations were made to control exposures, including improved maintenance of

  8. Multiscale Modeling of Red Blood Cells Squeezing through Submicron Slits

    Peng, Zhangli; Lu, Huijie


    A multiscale model is applied to study the dynamics of healthy red blood cells (RBCs), RBCs in hereditary spherocytosis, and sickle cell disease squeezing through submicron slits. This study is motivated by the mechanical filtration of RBCs by inter-endothelial slits in the spleen. First, the model is validated by comparing the simulation results with experiments. Secondly, the deformation of the cytoskeleton in healthy RBCs is investigated. Thirdly, the mechanisms of damage in hereditary spherocytosis are investigated. Finally, the effects of cytoplasm and membrane viscosities, especially in sickle cell disease, are examined. The simulations results provided guidance for future experiments to explore the dynamics of RBCs under extreme deformation.

  9. Bayesian approach to rough set

    Marwala, Tshilidzi


    This paper proposes an approach to training rough set models using Bayesian framework trained using Markov Chain Monte Carlo (MCMC) method. The prior probabilities are constructed from the prior knowledge that good rough set models have fewer rules. Markov Chain Monte Carlo sampling is conducted through sampling in the rough set granule space and Metropolis algorithm is used as an acceptance criteria. The proposed method is tested to estimate the risk of HIV given demographic data. The results obtained shows that the proposed approach is able to achieve an average accuracy of 58% with the accuracy varying up to 66%. In addition the Bayesian rough set give the probabilities of the estimated HIV status as well as the linguistic rules describing how the demographic parameters drive the risk of HIV.

  10. Speciation of atmospheric polycyclic aromatic hydrocarbons (PAHs) present during fog time collected submicron particles.

    Singh, Dharmendra Kumar; Sharma, Swati; Habib, Gazala; Gupta, Tarun


    Airborne submicron particles (PM1) were collected using PM1 sampler during the fog-dominated days (December 2013-January 2014). PM1 values varied between 58.12 μg/m(3) and 198.75 μg/m(3), and average mass concentration was 162.33 ± 38.25 μg/m(3) while total average concentration of particle-associated polycyclic aromatic hydrocarbon (PAHs) determined was 616.31 ± 30.31 ng/m(3). This is a signal for an alarming high pollution level at this site situated in the Indo-Gangetic Plain (IGP). PAHs were extracted from filters using toluene and acetonitrile. Quantitative measurements of polycyclic aromatic hydrocarbons (PAHs) were carried out using the high performance liquid chromatography (HPLC) technique. The extracts were analyzed for 16 target polycyclic aromatic hydrocarbons (PAHs) including carcinogenic compound benzo(a)pyrene (19.86 ± 38.98 ng/m(3)). Fluoranthene, benzo(a)anthracene, anthracene, and fluorene were the predominant compounds found in the samples collected during foggy days. Based on number of rings, four-ring PAH compounds had maximum contribution (43%) in this fog time collected submicron particles followed by three-ring (21%), five-ring (20%), six-ring (13%), and two-ring (3%), respectively. In winter and foggy days, wood and coal combustion and biomass burning also significantly contribute to the PAH levels. However, diagnostic ratio suggests diesel emissions as the prime source of PAHs at this sampling site.

  11. Submicron particle mass concentrations and sources in the Amazonian wet season (AMAZE-08)

    Chen, Q.; Farmer, D. K.; Rizzo, L. V.; Pauliqueivis, T.; Kuwata, Mikinori; Karl, Thomas G.; Guenther, Alex B.; Allan, James D.; Coe, H.; Andreae, M. O.; Poeschl, U.; Jiminez, J. L.; Artaxo, Paulo; Martin, Scot T.


    Real-time mass spectra of non-refractory component of submicron aerosol particles were recorded in a tropical rainforest in the central Amazon basin during the wet season of 2008, as a part of the Amazonian Aerosol Characterization Experiment (AMAZE-08). Organic components accounted on average for more than 80% of the non-refractory submicron particle mass concentrations during the period of measurements. Ammonium was present in sufficient quantities to halfway neutralize sulfate. In this acidic, isoprene-dominated, low-NOx environment the high-resolution mass spectra as well as mass closures with ion chromatography measurements did not provide evidence for significant contributions of organosulfate species, at least at concentrations above uncertainty levels. Positive-matrix factorization of the time series of particle mass spectra identified four statistical factors to account for the variance of the signal intensities of the organic constituents: a factor HOA having a hydrocarbon-like signature and identified as regional emissions of primary organic material, a factor OOA-1 associated with fresh production of secondary organic material by a mechanism of BVOC oxidation followed by gas-to-particle conversion, a factor OOA-2 consistent with reactive uptake of isoprene oxidation products, especially epoxydiols by acidic particles, and a factor OOA-3 associated with long range transport and atmospheric aging. The OOA-1, -2, and -3 factors had progressively more oxidized signatures. Diameter-resolved mass spectral markers also suggested enhanced reactive uptake of isoprene oxidation products to the accumulation mode for the OOA-2 factor, and such size partitioning can be indicative of in-cloud process. The campaign-average factor loadings were in a ratio of 1.1:1.0 for the OOA-1 compared to the OOA-2 pathway, suggesting the comparable importance of gas-phase compared to particle-phase (including cloud waters) production pathways of secondary organic material during

  12. Submicron magnetic core conducting polypyrrole polymer shell: Preparation and characterization.

    Tenório-Neto, Ernandes Taveira; Baraket, Abdoullatif; Kabbaj, Dounia; Zine, Nadia; Errachid, Abdelhamid; Fessi, Hatem; Kunita, Marcos Hiroiuqui; Elaissari, Abdelhamid


    Magnetic particles are of great interest in various biomedical applications, such as, sample preparation, in vitro biomedical diagnosis, and both in vivo diagnosis and therapy. For in vitro applications and especially in labs-on-a-chip, microfluidics, microsystems, or biosensors, the needed magnetic dispersion should answer various criteria, for instance, submicron size in order to avoid a rapid sedimentation rate, fast separations under an applied magnetic field, and appreciable colloidal stability (stable dispersion under shearing process). Then, the aim of this work was to prepare highly magnetic particles with a magnetic core and conducting polymer shell particles in order to be used not only as a carrier, but also for the in vitro detection step. The prepared magnetic seed dispersions were functionalized using pyrrole and pyrrole-2-carboxylic acid. The obtained core-shell particles were characterized in terms of particle size, size distribution, magnetization properties, FTIR analysis, surface morphology, chemical composition, and finally, the conducting property of those particles were evaluated by cyclic voltammetry. The obtained functional submicron highly magnetic particles are found to be conducting material bearing function carboxylic group on the surface. These promising conducting magnetic particles can be used for both transport and lab-on-a-chip detection.

  13. Atmospheric pressure plasma assisted calcination of composite submicron fibers

    Medvecká, Veronika; Kováčik, Dušan; Tučeková, Zlata; Zahoranová, Anna; Černák, Mirko


    The plasma assisted calcination of composite organic/inorganic submicron fibers for the preparation of inorganic fibers in submicron scale was studied. Aluminium butoxide/polyvinylpyrrolidone fibers prepared by electrospinning were treated using low-temperature plasma generated by special type of dielectric barrier discharge, so called diffuse coplanar surface barrier discharge (DCSBD) at atmospheric pressure in ambient air, synthetic air, oxygen and nitrogen. Effect of plasma treatment on base polymer removal was investigated by using Attenuated total reflectance - Fourier transform infrared (ATR-FTIR) spectroscopy. Influence of working gas on the base polymer reduction was studied by energy-dispersive X-ray spectroscopy (EDX) and CHNS elemental analysis. Changes in fibers morphology were observed by scanning electron microscopy (SEM). High efficiency of organic template removal without any degradation of fibers was observed after plasma treatment in ambient air. Due to the low-temperature approach and short exposure time, the plasma assisted calcination is a promising alternative to the conventional thermal calcination. Contribution to the topical issue "6th Central European Symposium on Plasma Chemistry (CESPC-6)", edited by Nicolas Gherardi, Ester Marotta and Cristina Paradisi

  14. Magnetic trapping of superconducting submicron particles produced by laser ablation in superfluid helium

    Takahashi, Yuta; Suzuki, Junpei; Yoneyama, Naoya; Tokawa, Yurina; Suzuki, Nobuaki; Matsushima, Fusakazu; Kumakura, Mitsutaka; Ashida, Masaaki; Moriwaki, Yoshiki


    We produced spherical superconducting submicron particles by laser ablation of their base metal tips in superfluid helium, and trapped them using a quadrupole magnetic field owing to the diamagnetism caused by the Meissner effect. We also measured their critical temperatures of superconductivity, by observing the threshold temperatures for the confinement of superconducting submicron particles in the trap.

  15. Influencing factors of surface roughness of MAO ceramic coating on AZ91D

    DI Shi-chun; PAN Ming-qiang; CHI Guan-xin


    To investigate the treating parameters' influence on the surface roughness of the MAO ceramic coating on AZ91D, experiments were implemented in the alkaline electrolyte by using a pulse power source with positive and negative pulse, and the surface roughness was measured and analyzed by using a Times roughness-meter and an optical microscope. The machining parameters' influencing rule on the coating surface roughness was investigated. The result indicates that the influence of all parameters is interactive, while the positive voltage and the electrolyte concentration, or increasing the frequency and the positive and negative voltage ratio are appropriate, the coating surface roughness will be improved.

  16. Information Measures of Roughness of Knowledge and Rough Sets for Incomplete Information Systems

    LIANG Ji-ye; QU Kai-she


    In this paper we address information measures of roughness of knowledge and rough sets for incomplete information systems. The definition of rough entropy of knowledge and its important properties are given. In particular, the relationship between rough entropy of knowledge and the Hartley measure of uncertainty is established. We show that rough entropy of knowledge decreases monotonously as granularity of information become smaller. This gives an information interpretation for roughness of knowledge. Based on rough entropy of knowledge and roughness of rough set. a definition of rough entropy of rough set is proposed, and we show that rough entropy of rough set decreases monotonously as granularity of information become smaller. This gives more accurate measure for roughness of rough set.

  17. Interaction between submicron COD crystals and renal epithelial cells

    Peng H


    Full Text Available Hua Peng1,2 Jian-Ming Ouyang1,2 Xiu-Qiong Yao1, Ru-E Yang11Department of Chemistry, Jinan University, 2Institute of Biomineralization and Lithiasis Research, Jinan University, Guangzhou, ChinaObjectives: This study aims to investigate the adhesion characteristics between submicron calcium oxalate dihydrate (COD with a size of 150 ± 50 nm and African green monkey kidney epithelial cells (Vero cells before and after damage, and to discuss the mechanism of kidney stone formation.Methods: Vero cells were oxidatively injured by hydrogen peroxide to establish a model of injured cells. Scanning electron microscopy was used to observe Vero–COD adhesion. Inductively coupled plasma emission spectrometry was used to quantitatively measure the amount of adhered COD microcrystals. Nanoparticle size analyzer and laser scanning confocal microscopy were performed to measure the change in the zeta potential on the Vero cell surface and the change in osteopontin expression during the adhesion process, respectively. The level of cell injury was evaluated by measuring the changes in malonaldehyde content, and cell viability during the adhesion process.Results: The adhesion capacity of Vero cells in the injury group to COD microcrystals was obviously stronger than that of Vero cells in the control group. After adhesion to COD, cell viability dropped, both malonaldehyde content and cell surface zeta potential increased, and the fluorescence intensity of osteopontin decreased because the osteopontin molecules were successfully covered by COD. Submicron COD further damaged the cells during the adhesion process, especially for Vero cells in the control group, leading to an elevated amount of attached microcrystals.Conclusion: Submicron COD can further damage injured Vero cells during the adhesion process. The amount of attached microcrystals is proportional to the degree of cell damage. The increased amount of microcrystals that adhered to the injured epithelial

  18. Sensing roughness and polish direction

    Jakobsen, Michael Linde; Olesen, Anders Sig; Larsen, Henning Engelbrecht;


    needs information about the RMS-value of the surface roughness and the current direction of the scratches introduced by the polishing process. The RMS-value indicates to the operator how far he is from the final finish, and the scratch orientation is often specified by the customer in order to avoid...... complications during the casting process. In this work we present a method for measuring the RMS-values of the surface roughness while simultaneously determining the polishing direction. We are mainly interested in the RMS-values in the range from 0 – 100 nm, which corresponds to the finish categories of A1, A2...... and A3 (Finishing guide, Bales). Based on simple intensity measurements, we estimate the RMS-value of the surface roughness, and by using a sectioned annually shaped photo-detector to collect the scattered light, we can determine the direction of polishing and distinguish light scattered from random...

  19. Stochastic control with rough paths

    Diehl, Joscha [University of California San Diego (United States); Friz, Peter K., E-mail: [TU & WIAS Berlin (Germany); Gassiat, Paul [CEREMADE, Université Paris-Dauphine, PSL Research University (France)


    We study a class of controlled differential equations driven by rough paths (or rough path realizations of Brownian motion) in the sense of Lyons. It is shown that the value function satisfies a HJB type equation; we also establish a form of the Pontryagin maximum principle. Deterministic problems of this type arise in the duality theory for controlled diffusion processes and typically involve anticipating stochastic analysis. We make the link to old work of Davis and Burstein (Stoch Stoch Rep 40:203–256, 1992) and then prove a continuous-time generalization of Roger’s duality formula [SIAM J Control Optim 46:1116–1132, 2007]. The generic case of controlled volatility is seen to give trivial duality bounds, and explains the focus in Burstein–Davis’ (and this) work on controlled drift. Our study of controlled rough differential equations also relates to work of Mazliak and Nourdin (Stoch Dyn 08:23, 2008).

  20. Topology theory on rough sets.

    Wu, QingE; Wang, Tuo; Huang, YongXuan; Li, JiSheng


    For further studying the theories and applications of rough sets (RS), this paper proposes a new theory on RS, which mainly includes topological space, topological properties, homeomorphism, and its properties on RS by some new definitions and theorems given. The relationship between partition and countable open covering is discussed, and some applications based on the topological rough space and its topological properties are introduced. Moreover, some perspectives for future research are given. Throughout this paper, the advancements of the new theory on RS and topological algebra not only represent an important theoretical value but also exhibit significant applications of RS and topology.

  1. Fault zone roughness controls slip stability

    Harbord, Christopher; Nielsen, Stefan; De Paola, Nicola


    Fault roughness is an important control factor in the mechanical behaviour of fault zones, in particular the frictional slip stability and subsequent earthquake nucleation. Despite this, there is little experimental quantification as to the effects of varying roughness upon rate- and state-dependant friction (RSF). Utilising a triaxial deformation apparatus and a novel adaptation of the direct shear methodology to simulate initially bare faults in Westerly Granite, we performed a series of velocity step frictional sliding experiments. Initial root mean square roughnesses (Sq) was varied in the range 6x10-7 - 2.4x10-5 m. We also investigated the effects upon slip stability of normal stress variation in the range σn = 30 - 200 MPa, and slip velocity between 0.1 - 10 μm s-1. A transition from stable sliding to unstable slip (manifested by stick-slip and slow slip events) was observed, depending on the parameter combination, thus covering the full spectrum of fault slip behaviours. At low normal stress (σn = 30MPa) smooth faults (Sqstress drops on slow slip events upon velocity increase), with strongly velocity weakening friction. When normal stress is increased to intermediate values (σn = 100 - 150 MPa), smooth faults (Sqstress (σn = 200 MPa) a transition from unstable to stable sliding is observed for smooth faults, which is not expected using RSF stability criteria. At all conditions sliding is stable for rough faults (Sq> 1x10-6 m). We find that instability can develop when the ratio of fault to critical stiffness kf kc > 10, or, alternatively, even when a - b > 0 at σn = 150MPa, suggesting that bare surfaces may not strictly obey the R+S stability condition. Additionally we present white light interferometry and SEM analysis of experimentally deformed samples which provide information about the distribution and physical nature of frictional contact. Significantly we suggest that bare fault surfaces may require a different stability criterion (based on

  2. Microscopic methods in analysis of submicron phospholipid dispersions

    Płaczek Marcin


    Full Text Available Microscopy belongs to the group of tests, used in pharmaceutical technology, that despite the lapse of time and the development of new analytical methods, still remain irreplaceable for the characterization of dispersed drug dosage forms (e.g., suspensions and emulsions. To obtain complete description of a specific drug formulation, such as parenteral colloidal products, a combination of different microscopic techniques is sometimes required. Electron microscopy methods are the most useful ones; however, even such basic methods as optical microscopy may be helpful for determination of some properties of a sample. The publication explicates the most popular microscopical techniques used nowadays for characterization of the morphology of nanoparticles suspended in pharmaceutical formulations; ad vantages and disadvantages of these methods are also discussed. Parenteral submicron formulations containing lecithin or a particular phospholipid were chosen as examples.

  3. Submicron particles of Co, Ni and Co–Ni alloys

    P Saravanan; T A Jose; P John Thomas; G U Kulkarni


    Magnetic sub-micron sized particles (with diameters in the range 100–600 nm) of Co, Ni and Co–Ni alloys, protected with polyvinylpyrrolidone have been prepared in gram quantities using the polyol process. Experiments carried out with different metal precursors and starting compositions have yielded reliable routes to produce particles of the desired diameters in the 100–600 nm range. The particles were characterized with X-ray diffraction, scanning electron microscopy, energy dispersive X-ray analysis, thermogravimetric analysis and magnetic measurements. The particles are found to be stable under ambient conditions indefinitely. The coercivity values of the Co and Ni particles are ∼ 50% higher compared to the corresponding bulk values. The alloy particles follow a trend similar to the bulk alloys.

  4. Submicron cubic boron nitride as hard as diamond

    Liu, Guoduan; Kou, Zili, E-mail:, E-mail:; Lei, Li; Peng, Fang; Wang, Qiming; Wang, Kaixue; Wang, Pei; Li, Liang; Li, Yong; Wang, Yonghua [Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065 (China); Yan, Xiaozhi, E-mail:, E-mail:; Li, Wentao [Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065 (China); Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai 201203 (China); Bi, Yan [Institute of Fluid Physics and National Key Laboratory of Shockwave and Detonation Physic, China Academy of Engineering Physics, Mianyang 621900 (China); Leng, Yang [Department of Mechanical Engineering, Hong Kong University of Science and Technology, Kowloon, Hong Kong (China); He, Duanwei [Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065 (China); Institute of Fluid Physics and National Key Laboratory of Shockwave and Detonation Physic, China Academy of Engineering Physics, Mianyang 621900 (China)


    Here, we report the sintering of aggregated submicron cubic boron nitride (sm-cBN) at a pressure of 8 GPa. The sintered cBN compacts exhibit hardness values comparable to that of single crystal diamond, fracture toughness about 5-fold that of cBN single crystal, in combination with a high oxidization temperature. Thus, another way has been demonstrated to improve the mechanical properties of cBN besides reducing the grain size to nano scale. In contrast to other ultrahard compacts with similar hardness, the sm-cBN aggregates are better placed for potential industrial application, as their relative low pressure manufacturing perhaps be easier and cheaper.

  5. Coherent Magnetic Switching in a Permalloy Submicron Junction

    Wang, Junlin; Lu, Xianyang; Zhang, Jason; Ling, Hua; Wu, Jing; Zhou, Yan; Xu, Yongbing


    This work provides a numerical micromagnetic study of the magnetic switching of a submicron magnetic junction in a Permalloy (Ni80Fe20) cross structure. The simulation results demonstrate that the magnetic domain at the junction can be controlled to switch coherently by the applied magnetic field. This coherent magnetic switching in the cross structure has been found to be reversible and the 2-bit information can be written in the magnetic junction. For information storage, this kind of device can also realize the function of a quaternary arithmetic unit. By varying the direction of the applied magnetic field, we have demonstrated that this magnetic junction could be the building block for a magnetoresistive random access memory (MRAM) or a quaternary magnetic arithmetic unit.

  6. Chemical strategies for die/wafer submicron alignment and bonding.

    Martin, James Ellis; Baca, Alicia I.; Chu, Dahwey; Rohwer, Lauren Elizabeth Shea


    This late-start LDRD explores chemical strategies that will enable sub-micron alignment accuracy of dies and wafers by exploiting the interfacial energies of chemical ligands. We have micropatterned commensurate features, such as 2-d arrays of micron-sized gold lines on the die to be bonded. Each gold line is functionalized with alkanethiol ligands before the die are brought into contact. The ligand interfacial energy is minimized when the lines on the die are brought into registration, due to favorable interactions between the complementary ligand tails. After registration is achieved, standard bonding techniques are used to create precision permanent bonds. We have computed the alignment forces and torque between two surfaces patterned with arrays of lines or square pads to illustrate how best to maximize the tendency to align. We also discuss complex, aperiodic patterns such as rectilinear pad assemblies, concentric circles, and spirals that point the way towards extremely precise alignment.

  7. Short range investigation of sub-micron zirconia particles

    Caracoche, M C; Martinez, J A [Departamento de Fisica, IFLP, Facultad de Ciencias Exactas, CICPBA, Universidad Nacional de La Plata (Argentina); Rivas, P C [IFLP-CONICET, Facultad de Ciencias Agrarias y Forestales, Universidad Nacional de La Plata (Argentina); Bondioli, F; Cannillo, V [Dipartimento di Ingegniria dei Materiali e dell' Ambiente, Facolta di Ingegneria, Universita di Modena e Reggio Emilia (Italy); Ferrari, A M, E-mail: [Dipartimento di Scienza a Metodi dell' Ingegneria, Universita di Modena e Reggio Emilia (Italy)


    The Perturbed Angular Correlations technique was used to determine the configurations around Zirconium ions and their thermal behavior in non-aggregated sub-micron zirconia spherical particles. Three residues containing- Zr surroundings were determined for the non-crystalline starting particles, which were identified under the assumption of a certain chemical reactions sequence during synthesis. While the one made up mainly by hydroxyl groups was common to both samples, the two involving mainly organic residues were particle size dependent. Upon crystallization, both samples stabilized in the t'- and t- tetragonal forms and the Xc-cubic form but their amounts and temperatures of appearance were different. On heating, the structure of the smaller particles became gradually monoclinic achieving total degradation upon the subsequent cooling to RT.

  8. SEMICONDUCTOR DEVICES: Deep submicron PDSOI thermal resistance extraction

    Jianhui, Bu; Jinshun, Bi; Linmao, Xi; Zhengsheng, Han


    Deep submicron partially depleted silicon on insulator (PDSOI) MOSFETs with H-gate were fabricated based on the 0.35 μm SOI process developed by the Institute of Microelectronics of the Chinese Academy of Sciences. Because the self-heating effect (SHE) has a great influence on SOI, extractions of thermal resistance were done for accurate circuit simulation by using the body-source diode as a thermometer. The results show that the thermal resistance in an SOI NMOSFET is lower than that in an SOI PMOSFET; and the thermal resistance in an SOI NMOSFET with a long channel is lower than that with a short channel. This offers a great help to SHE modeling and parameter extraction.

  9. Highly nonlinear sub-micron silicon nitride trench waveguide coated with gold nanoparticles

    Huang, Yuewang; Zhao, Qiancheng; Sharac, Nicholas; Ragan, Regina; Boyraz, Ozdal


    We demonstrate the fabrication of a highly nonlinear sub-micron silicon nitride trench waveguide coated with gold nanoparticles for plasmonic enhancement. The average enhancement effect is evaluated by measuring the spectral broadening effect caused by self-phase-modulation. The nonlinear refractive index n2 was measured to be 7.0917×10-19 m2/W for a waveguide whose Wopen is 5 μm. Several waveguides at different locations on one wafer were measured in order to take the randomness of the nanoparticle distribution into consideration. The largest enhancement is measured to be as high as 10 times. Fabrication of this waveguide started with a MEMS grade photomask. By using conventional optical lithography, the wide linewidth was transferred to a wafer. Then the wafer was etched anisotropically by potassium hydroxide (KOH) to engrave trapezoidal trenches with an angle of 54.7º. Side wall roughness was mitigated by KOH etching and thermal oxidation that was used to generate a buffer layer for silicon nitride waveguide. The guiding material silicon nitride was then deposited by low pressure chemical vapor deposition. The waveguide was then patterned with a chemical template, with 20 nm gold particles being chemically attached to the functionalized poly(methyl methacrylate) domains. Since the particles attached only to the PMMA domains, they were confined to localized regions, therefore forcing the nanoparticles into clusters of various numbers and geometries. Experiments reveal that the waveguide has negligible nonlinear absorption loss, and its nonlinear refractive index can be greatly enhanced by gold nano clusters. The silicon nitride trench waveguide has large nonlinear refractive index, rendering itself promising for nonlinear applications.

  10. Thermophoretic capture of submicron particles by a droplet

    Wang, Ao; Song, Qiang; Yao, Qiang


    Thermophoresis is an important mechanism for submicron particle capture by droplets. The thermophoretic deposition efficiencies under varying Reynolds (Re) numbers and temperature differences are obtained from the direct numerical simulation of the submicron particle flowing around the droplet. Comparison of the results calculated under the same conditions through the classical thermophoretic deposition efficiency formula and by numerical simulation shows that the Davenport formula always returns greater values than the numerical simulation, by a relative deviation of 19.8%-63.8%. The relative deviation decreased first and then increased with increasing difference in temperature, and increased gradually with increasing Re. The deviation resulted from the assumption that the particle concentration on the droplet surface is equal to that of the incoming flow in the formula deduction process. The convection of the gas and the thermophoresis of the particles together determined the migration of the particles in the boundary layer, and so determined the particle concentration distribution on the surface of droplets. Thus, the particle concentrations on the surface of droplets are actually lower than those of the incoming flow and are distributed bimodally on the surface. The dimensionless particle concentration on the surface of droplets decreased with increasing Re, and increased first then decreased later with increasing difference in temperature. The dimensionless thermophoretic driving velocity and Re were adopted to correct the formula. The results calculated by the corrected formula were consistent with the numerical simulation employed in this paper, such that the maximum relative deviation was reduced from the original 66.8% to less than 8%.

  11. Homomorphic Properties of Fuzzy Rough Groups

    QIN Ke-yun; ZHANG Xiao-hua


    This paper is devoted to the discussion of homomorphic properties of fuzzy rough groups.The fuzzy approximation space was generated by fuzzy normal subgroups and the fuzzy rough approximation operators were discussed in the frame of fuzzy rough set model.The basic properties of fuzzy rough approximation operators were obtained.

  12. Fuzzy Rough Ring and Its Prop erties

    REN Bi-jun; FU Yan-ling


    This paper is devoted to the theories of fuzzy rough ring and its properties. The fuzzy approximation space generated by fuzzy ideals and the fuzzy rough approximation operators were proposed in the frame of fuzzy rough set model. The basic properties of fuzzy rough approximation operators were analyzed and the consistency between approximation operators and the binary operation of ring was discussed.

  13. A New Minimal Rough Set Axiom Group

    DAI Jian-hua


    Rough set axiomatization is one aspect of rough set study, and the purpose is to characterize rough set theory using independable and minimal axiom groups. Thus, rough set theory can be studied by logic and axiom system methods. To characterize rough set theory, an axiom group named H consisting of 4 axioms, is proposed. That validity of the axiom group in characterizing rough set theory is reasonable, is proved. Simultaneously, the minimization of the axiom group, which requires that each axiom is an inequality and each is independent, is proved. The axiom group is helpful for researching rough set theory by logic and axiom system methods.

  14. Plant Communities of Rough Rock.

    Jacobs, Linda

    A unit of study on plants grown in the Navajo community of Rough Rock, Arizona, is presented in sketches providing the common Navajo name for the plant, a literal English translation, the English name of the plant, and the Latin name. A brief description of each plant includes where the plant grows, how the Navajos use the plant, and the color and…

  15. Calibration of surface roughness standards

    Thalmann, R.; Nicolet, A.; Meli, F.


    The key comparison EURAMET.L-K8.2013 on roughness was carried out in the framework of a EURAMET project starting in 2013 and ending in 2015. It involved the participation of 17 National Metrology Institutes from Europe, Asia, South America and Africa representing four regional metrology organisat...

  16. Rough Set Theory over Fuzzy Lattices

    Guilong Liu


    Rough set theory, proposed by Pawlak in 1982, is a tool for dealing with uncertainty and vagueness aspects of knowledge model. The main idea of roug h sets corresponds to the lower and upper approximations based on equivalence relations. This paper studies the rough set and its extension. In our talk, we present a linear algebra approach to rough set and its extension, give an equivalent definition of the lower and upper approximations of rough set based on the characteristic function of sets, and then we explain the lower and upper approximations as the colinear map and linear map of sets, respectively. Finally, we define the rough sets over fuzzy lattices, which cover the rough set and fuzzy rough set, and the independent axiomatic systems are constructed to characterize the lower and upper approximations of rough set over fuzzy lattices, respectively, based on inner and outer products. The axiomatic systems unify the axiomization of Pawlak's rough sets and fuzzy rough sets.

  17. Human roughness perception and possible factors effecting roughness sensation.

    Aktar, Tugba; Chen, Jianshe; Ettelaie, Rammile; Holmes, Melvin; Henson, Brian


    Surface texture sensation is significant for business success, in particular for solid surfaces for most of the materials; including foods. Mechanisms of roughness perception are still unknown, especially under different conditions such as lubricants with varying viscosities, different temperatures, or under different force loads during the observation of the surface. This work aims to determine the effect of those unknown factors, with applied sensory tests on 62 healthy participants. Roughness sensation of fingertip was tested under different lubricants including water and diluted syrup solutions at room temperature (25C) and body temperature (37C) by using simple pair-wise comparison to observe the just noticeable difference threshold and perception levels. Additionally, in this research applied force load during roughness observation was tested with pair-wise ranking method to illustrate its possible effect on human sensation. Obtained results showed that human's capability of roughness discrimination reduces with increased viscosity of the lubricant, where the influence of the temperature was not found to be significant. Moreover, the increase in the applied force load showed an increase in the sensitivity of roughness discrimination. Observed effects of the applied factors were also used for estimating the oral sensation of texture during eating. These findings are significant for our fundamental understanding to texture perception, and for the development of new food products with controlled textural features. Texture discrimination ability, more specifically roughness discrimination capability, is a significant factor for preference and appreciation for a wide range of materials, including food, furniture, or fabric. To explore the mechanism of sensation capability through tactile senses, it is necessary to identify the relevant factors and define characteristics that dominate the process involved. The results that will be obtained under these principles

  18. Transformation and entropy for fuzzy rough sets


    A new method for translating a fuzzy rough set to a fuzzy set is introduced and the fuzzy approximation of a fuzzy rough set is given.The properties of the fuzzy approximation of a fuzzy rough set are studied and a fuzzy entropy measure for fuzzy rough sets is proposed.This measure is consistent with similar considerations for ordinary fuzzy sets and is the result of the fuzzy approximation of fuzzy rough sets.

  19. Rough Class on a Completely Distributive Lattice

    陈德刚; 张文修; 宋士吉


    This paper generalizes the Pawlak rough set method to a completely distributive lattice. Theconcept of a rough set has many applications in data mining. The approximation operators on a completelydistributive lattice are studied, the rough class on a completely distributive lattice is defined and theexpressional theorems of the rough class are proven. These expressional theorems are used to prove that thecollection of all rough classes is an atomic completely distributive lattice.

  20. The effect of bottom roughness on scalar transport in aquatic ecosystems: implications for reproduction and recruitment in the benthos.

    Quinn, Noel P; Ackerman, Josef D


    Bottom roughness can influence gamete and larval transport in benthic organisms. For example the ratio of the roughness spacing (λ) and roughness height (k) determines the type of roughness flow regime created in two dimensional (2D) flows: λ/k8 results in isolated roughness flow. Computational fluid dynamic modeling (COMSOL K-ε) was used to examine the effect of roughness geometry (e.g., a gradient in angularity provided by square, triangular and round 2D bottom roughness elements) on the prediction of roughness flow regime using biologically relevant λ/k ratios. In addition, a continuously released scalar (a proxy for gametes and larvae) in a coupled convection-diffusion model was used to determine the relationship among roughness geometry, λ/k ratios, and scalar transport (relative scalar transport, RT=ratio of scalar measured downstream in a series of roughness elements placed in tandem). The modeled roughness flow regimes fit closely with theoretical predictions using the square and triangle geometries, but the round geometry required a lower λ/k ratio than expected for skimming flow. Relative transport of the scalar was consistent with the modeled flow regimes, however significant differences in RT were found among the roughness flows for each geometry, and significantly lower RT values were observed for skimming flow in the round geometry. The λ/k ratio provides an accurate means of classifying flow in and around the roughness elements, whereas RT indicates the nature of scalar transport and retention. These results indicate that the spatial configuration of bottom roughness is an important determinant of gamete/larval transport in terms of whether the scalar will be retained among roughness elements or transported downstream.

  1. Avalanche dynamics on a rough inclined plane.

    Börzsönyi, Tamás; Halsey, Thomas C; Ecke, Robert E


    The avalanche behavior of gravitationally forced granular layers on a rough inclined plane is investigated experimentally for different materials and for a variety of grain shapes ranging from spherical beads to highly anisotropic particles with dendritic shape. We measure the front velocity, area, and height of many avalanches and correlate the motion with the area and height. We also measure the avalanche profiles for several example cases. As the shape irregularity of the grains is increased, there is a dramatic qualitative change in avalanche properties. For rough nonspherical grains, avalanches are faster, bigger, and overturning in the sense that individual particles have down-slope speeds u p that exceed the front speed uf as compared with avalanches of spherical glass beads that are quantitatively slower and smaller and where particles always travel slower than the front speed. There is a linear increase of three quantities: (i) dimensionless avalanche height, (ii) ratio of particle to front speed, and (iii) the growth rate of avalanche speed with increasing avalanche size with increasing tan theta r where theta r is the bulk angle of repose, or with increasing beta P, the slope of the depth averaged flow rule, where both theta r and beta P reflect the grain shape irregularity. These relations provide a tool for predicting important dynamical properties of avalanches as a function of grain shape irregularity. A relatively simple depth-averaged theoretical description captures some important elements of the avalanche motion, notably the existence of two regimes of this motion.

  2. Enhanced Backscattering from Rough Surfaces


    under Referee ..................... 12 3.4 Papers Presented at Professional Conferences ................... 12 4.0 LIST OF ALL PARTICIPATING SCIENTIFIC...60 -30 0 30 60 90 Scattering Angle (deg) Figure 2 (b). The DRC for the Perfectly Conducting Surface whose Profile is shown in Figure 2 (a) when the...Randomly Rough Surfaces", accepted for publication in Applied Optics (1993). I 3.3 Papers Submitted to Journal under Referee 19. E.R. Mendez, H.M

  3. Rough Sets in Quotient Semigroups

    LanShu; JialiYu


    This article is based on the notions of a congruence of a semigroup and the p-lower and p-upper approximations of a nonempty subset of a semigroup, discussing some properties of the product of these two subsets according to the properties of some especial single subsets such as subsemigroups and ideals, then the rigorous proof was given. Thus the rough theory in semigroups are completed and perfected.

  4. Noise of sliding rough contact

    Le Bot, Alain


    This article is a discussion about the origin of friction noise produced when rubbing solids having rough surfaces. We show that noise emerges from numerous impacts into the contact between antagonist asperities of surfaces. Prediction of sound sources reduces to a statistical problem of contact mechanics. On the other hand, contact is also responsible of dissipation of vibration. This leads to the paradoxical result that the noise may not be proportional to the number of sources.

  5. Simulation of hurricane response to suppression of warm rain by sub-micron aerosols

    Rosenfeld, D; Khain, A; Lynn, B; Woodley, W. L


    ...). The possible impact of seeding of clouds with submicron cloud condensation nuclei (CCN) on hurricane structure and intensity as measured by nearly halving of the area covered by hurricane force winds was simulated by "turning...

  6. Sensing roughness and polish direction

    Jakobsen, M. L.; Olesen, A. S.; Larsen, H. E.; Stubager, J.; Hanson, S. G.; Pedersen, T. F.; Pedersen, H. C.


    As a part of the work carried out on a project supported by the Danish council for technology and innovation, we have investigated the option of smoothing standard CNC machined surfaces. In the process of constructing optical prototypes, involving custom-designed optics, the development cost and time consumption can become relatively large numbers in a research budget. Machining the optical surfaces directly is expensive and time consuming. Alternatively, a more standardized and cheaper machining method can be used, but then the object needs to be manually polished. During the polishing process the operator needs information about the RMS-value of the surface roughness and the current direction of the scratches introduces by the polishing process. The RMS-value indicates to the operator how far he is from the final finish, and the scratch orientation is often specified by the customer in order to avoid complications during the casting process. In this work we present a method for measuring the RMS-values of the surface roughness while simultaneously determining the polishing direction. We are mainly interested in the RMS-values in the range from 0 - 100 nm, which corresponds to the finish categories of A1, A2 and A3. Based on simple intensity measurements we estimates the RMS-value of the surface roughness, and by using a sectioned annual photo-detector to collect the scattered light we can determine the direction of polishing and distinguish light scattered from random structures and light scattered from scratches.

  7. Characteristics of Submicron Aerosols in 2013 summer of Beijing

    Guo, Song; Hu, Min; Shang, Dongjie; Zheng, Jing; Du, Zhuofei; Wu, Yusheng; Lu, Sihua; Zeng, Limin; Zhang, Renyi


    To characterize the air pollution of North China Plain of China, CAREBEIJING-2013 field campaign (Campaigns of Air quality REsearch in BEIJING and surrounding region) was conducted in summer of 2013. Submicron aerosols were measured at an urban site PKU (Peking University, 39° 59'21"N, 116° 18'25"E) from July 28th to September 31st 2013. A suite of integrated instruments was used to measure the size distribution, effective density and hygroscopicity of ambient particles. The chemical composition of submicron particles were measured by using an Aerodyne High-Resolution Time-of-Flight Aerosol Mass Spectrometer (HR-ToF-AMS) (Billerica, MA, USA). The average PM2.5 concentration was 73.0±70.7 μg m-3 during the measurement. The particulate pollution showed distinct 4-7 days cycles controlled by the meteorological conditions. Each cycle started with low PM2.5 mass concentrations (air mass was from relatively clean mountainous area. The particle number concentrations were high, but and the sizes were small (60 μg day-1, and the particle mean diameter grew to >100 nm. It is interesting to note that the mean diameters showed similar trend to PM2.5 mass concentrations, indicating the particle pollution attributed to the growth of the newly formed small particles. During the measurement, the average particle densities are between 1.3-1.5 g cm-3, indicating organics and sulfate were dominant in the particles. The densities of smaller particles, i.e. 46 nm, 81nm, showed single peak at 1.3-1.5 g cm-3, indicating the particles are internal mixed sulfate and organics. While the 150nm and 240 nm particle densities exhibited bimodal distribution with an additional small peak at ˜1.1 g cm-3, which is considered as external mixed organic particles or aged soot particles. The particle hygroscopic growth factor for all the measured sizes at RH of 90% showed bimodal distribution, attributing to external mixed organics (or aged soot) and internal mixed organics and sulfate. Both the

  8. Design and Analysis of an Isokinetic Sampling Probe for Submicron Particle Measurements at High Altitude

    Heath, Christopher M.


    An isokinetic dilution probe has been designed with the aid of computational fluid dynamics to sample sub-micron particles emitted from aviation combustion sources. The intended operational range includes standard day atmospheric conditions up to 40,000-ft. With dry nitrogen as the diluent, the probe is intended to minimize losses from particle microphysics and transport while rapidly quenching chemical kinetics. Initial results indicate that the Mach number ratio of the aerosol sample and dilution streams in the mixing region is an important factor for successful operation. Flow rate through the probe tip was found to be highly sensitive to the static pressure at the probe exit. Particle losses through the system were estimated to be on the order of 50% with minimal change in the overall particle size distribution apparent. Following design refinement, experimental testing and validation will be conducted in the Particle Aerosol Laboratory, a research facility located at the NASA Glenn Research Center to study the evolution of aviation emissions at lower stratospheric conditions. Particle size distributions and number densities from various combustion sources will be used to better understand particle-phase microphysics, plume chemistry, evolution to cirrus, and environmental impacts of aviation.

  9. Equilibrium contact angles of liquid droplets on ideal rough solids.

    Kang, Hie Chan; Jacobi, Anthony M


    This work proposes a theoretical model for predicting the apparent equilibrium contact angle of a liquid on an ideal rough surface that is homogeneous and has a negligible body force, line tension, or contact angle hysteresis between solid and liquid. The model is derived from the conservation equations and the free-energy minimization theory for the changes of state of liquid droplets. The work of adhesion is expressed as the contact angles in the wetting process of the liquid droplets. Equilibrium contact angles of liquid droplets for rough surfaces are expressed as functions of the area ratios for the solid, liquid, and surrounding gas and the roughness ratio and wetting ratio of the liquid on the solid for the partially and fully wet states. It is found that the ideal critical angle for accentuating the contact angles by the surface roughness is 48°. The present model is compared with existing experimental data and the classical Wenzel and Cassie-Baxter models and agrees with most of the experimental data for various surfaces and liquids better than does the Wenzel model and accounts for trends that the Wenzel model cannot explain.

  10. Simulation of sub-micron particle formation and growth during combustion processes

    WEI Feng; ZHANG Junying; ZHENG Chuguang


    Sub-micron particle formation and growth during combustion processes is very complex because of its strong uncertainty and randomness. A model to simulate the sub-micron particle formation and growth during the combustion process is developed based on the gas kinetic theory and is expressed by the vapor concentration changes and particle loading changes, which reflects effect characteristics of different mechanism (nucleation, condensation and coagulation) in particle formation processes. The developed characteristic time is used to token the three mechanisms. It is thought that environmental temperature and pressure, vapor temperature and critical pressure are important factors influencing the sub-micron particle formation and growth. The sub-micron particle formation processes under different conditions are studied and the effect characteristics of these mechanisms are analyzed, which show that the nucleation, condensation,and coagulation occur simultaneously during the sub-micron particle formation and growth process. Nucleation contributes to the sub-micron particle formation, while condensation and coagulation is helpful to the growth of the particle size.

  11. Development of microstructure in submicron particles reinforced magnesium matrix composite processed by room temperature deformation

    Nie, K.B., E-mail: [College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024 (China); Deng, K.K., E-mail: [College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024 (China); Xu, F.J. [College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024 (China); Wang, X.J.; Wu, K. [School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001 (China)


    Magnesium matrix composite reinforced with submicron SiC particles was subjected to room temperature deformation. A stepped tensile method was adopted to observe the development of microstructure at different tensile strain state. The microstructure evolution determined by transmission electron microscopy showed that the existence of submicron SiC particles could promote dislocation multiplication as well as impede dislocation motion. Dislocation density around SiC particles increased with the increase of tensile strain. Compared with the matrix alloy, the composite could withstand greater external loads, which can be related to the pinning effect caused by the submicron SiC particles on the movement of grain and twin boundaries. The study of the interface between the submicron SiC particles and matrix in the composite suggested that single submicron SiC particle bonded well with the matrix alloy after tensile process. Initiation of micro-cracks usually generated in the submicron particle dense zone during tensile process, which could lead to the fracture of composite. - Highlights: • Interaction among SiCp, dislocations, grain boundaries and twinning is analyzed. • Microstructures of SiCp/AZ91 during tensile is characterized. • 0.2 μm SiCp has significant pinning effect on dislocation movement. • Interfacial bonding between 0.2 μm SiCp-Mg is analyzed.

  12. Rough Implication%粗糙蕴涵

    薛占熬; 何华灿


    Rough implication operator is the emphasis and difficulty in the study of rough logic. Due to the shortage of rough implication in [3]~[5], we redefine rough set and rough implication operator by Stone algebra, and introduce new rough operators such as rough intersection, rough union, and rough complement. Moreover the characteristics of the proposed rough implication are investigated ,and we also point out that the proposed implication operation is superior to that of three-valued Lukasiewicz logic.

  13. Controlled motion of domain walls in submicron amorphous wires

    Mihai Ţibu


    Full Text Available Results on the control of the domain wall displacement in cylindrical Fe77.5Si7.5B15 amorphous glass-coated submicron wires prepared by rapid quenching from the melt are reported. The control methods have relied on conical notches with various depths, up to a few tens of nm, made in the glass coating and in the metallic nucleus using a focused ion beam (FIB system, and on the use of small nucleation coils at one of the sample ends in order to apply magnetic field pulses aimed to enhance the nucleation of reverse domains. The notch-based method is used for the first time in the case of cylindrical ultrathin wires. The results show that the most efficient technique of controlling the domain wall motion in this type of samples is the simultaneous use of notches and nucleation coils. Their effect depends on wire diameter, notch depth, its position on the wire length, and characteristics of the applied pulse.

  14. NMOS symmetric load ring VCOs modeling for submicron technologies

    Fino, M. Helena


    Voltage Controlled Oscillators (VCOs) are a key element in PLL design. The simulation of VCOs is a time consuming process because transient circuit simulations must run long enough that the steady state is attained. Furthermore, the robustness of design against operating and technological conditions must also be tested by simulating the circuits at several corners, thus making the design methodology based in iterative simulation rather prohibitive for this class of circuits. The development of efficient and reliable VCO models is therefore a very important task, not only for the automation of the circuit design, but for design space exploration as well. Besides accuracy and simplicity, models must easily adapt to the rapid technology evolution. In order to grant such robustness, we must develop models based on transistor level technological parameters. This paper presents an accurate model for submicron Voltage Controlled Oscillators (VCOs). The model obtained is based on the Npower MOS model, yielding quite accurate results for sub micron technologies. An example considering a 1.2V TSMC013 VCO is presented, where the accuracy of the results obtained against Hspice simulation is shown. Results obtained in about 2 seconds have 4% average error, compared to simulations taking over 15 minutes.

  15. An X-Ray Tomographic Microscope with Submicron Resolution

    Stampanoni, M.; Borchert, G. L.; Abela, R.; Patterson, B.; Vermeulen, D.; Rueegsegger, P.; Wyss, P.


    X-ray tomographic microscopy (XTM) is a powerful non-destructive investigation method, that has been applied in many fields of modern research (material science, microelectronics, medicine, biology, archaeology). Sofar the major limitations were imposed by low detection efficiency and low spatial resolution. With the advent of third generation synchrotron facilities excellent high intensity X-ray sources became available that by far counterbalanced low efficiency. On the other hand the resolution of presently used detector systems is restricted by scintillator properties, optical light transfer, and CCD granularity. They impose a practical limit of about one micrometer, while the progressing research demands urgently an advance in the submicron region. A break-through in this respect is being achieved by a novel detector type. It uses the properties of asymmetric Bragg reflection to increase the cross section of the reflected X-ray beam. A suitable combination of correspondingly cut Bragg crystals yields an image magnification that even at higher energies may surpass a factor of 1000. In this way the influence of the detector resolution can be scaled down accordingly. Such a device is being constructed and installed at the SLS which delivers an optimal X-ray beam of about 23 keV. The special properties of this experiment will be presented.

  16. Dynamics of Red Blood Cells through submicronic splenic slits

    Helfer, Emmanuele; Gambhire, Priya; Atwell, Scott; Bedu, Frederic; Ozerov, Igor; Viallat, Annie; Charrier, Anne; Badens, Catherine; Centre de reference Thalassemie, Badens Team; Physics; Engineering of Living Systems Team


    Red Blood Cells (RBCs) are periodically monitored for changes in their deformability by the spleen, and are entrapped and destroyed if unable to pass through the splenic interendothelial slits (IESs). In particular, in sickle cell disease (SCD), where hemoglobin form fibers inside the RBCs, and in hereditary spherocytosis (HS), where RBCs are more spherical and membrane-cytoskekeleton bonds are weakened, the loss of RBC deformability leads to spleen dysfunction. By combining photolithography and anisotropic wet etching techniques, we developed a new on-chip PDMS device with channels replicating the submicronic physiological dimensions of IESs to study the mechanisms of deformation of the RBCs during their passage through these biomimetic slits. For the first time, with HS RBCs, we show the disruption of the links between the RBC membrane and the underlying spectrin network. In the case of SCD RBCs we show the appearance of a tip at the front of the RBC with a longer time relaxation due to the increased cytoplasmic viscosity. This work has been carried out thanks to the support of the A*MIDEX project (n° ANR-11-IDEX-0001-02) funded by the «Investissements d'Avenir». French Government program, managed by ANR.

  17. Tracking Submicron Particles in Microchannel Flow by Microscopic Holography

    罗锐; 刘石


    Three-dimensional tracking of submicron particles in flows in a micro-channel was carried out using in-line holographic microscopy.A fixed single 0.5 μm fluorescent particle was identified and isolated from dust particles or overlapped particle pair using the laser induced fluorescent(LIF) method.Then in-line microscopic holograms of the fixed single particle were obtained at different positions on the optical axis,i.e.the defocus distances.The holograms of the single particle were used as the model templates with the known defocus distances.The particles in the in-line microscopic holograms of flow in the microchannel were then identified and located to obtain their two-dimensional positions.The defocus distances of those particles were determined by matching each hologram pattern to one of the model templates obtained in the single particle test.Finally the three-dimensional position and velocity of each particle were obtained.

  18. Quantitative roughness measurements with iTIRM

    Bijl, R.J.M. van der; Fähnle, O.W.; Brug, H. van; Braat, J.J.M.


    A new method, iTIRM, is used for quantitative surface roughness measurements of ground and polished surfaces and it is shown to be a useful tool for measuring total surface quality instead of individual roughness parameters.


    Reece, Charles E. [JLAB; Kelley, Michael J. [JLAB, W& amp; M College; Xu, Chen [JLAB, W& amp; M College


    Topographic structure on Superconductivity Radio Frequency (SRF) surfaces can contribute additional cavity RF losses describable in terms of surface RF reflectivity and absorption indices of wave scattering theory. At isotropic homogeneous extent, Power Spectrum Density (PSD) of roughness is introduced and quantifies the random surface topographic structure. PSD obtained from different surface treatments of niobium, such Buffered Chemical Polishing (BCP), Electropolishing (EP), Nano-Mechanical Polishing (NMP) and Barrel Centrifugal Polishing (CBP) are compared. A perturbation model is utilized to calculate the additional rough surface RF losses based on PSD statistical analysis. This model will not consider that superconductor becomes normal conducting at fields higher than transition field. One can calculate the RF power dissipation ratio between rough surface and ideal smooth surface within this field range from linear loss mechanisms.

  20. Function S-Rough sets and its applications

    Cui Yuquan; Shi Kaiquan


    Based on S-rough sets(singular rough sets), this paper presents function S-rough sets (function singular rough sets)and its mathematical structures and features. Function S-rough sets has two forms: function one direction S-rough sets (function one direction singular rough sets) and function two direction S-rough sets (function two direction singular rough sets). This paper advances the relationship theorem of function S-rough sets and S-rough sets. Function S-rough sets is the general form of S-rough sets, and S-rough sets is the special case of function Srough sets. In this paper, applications of function S-rough sets in rough law mining-discovery of system are given. Function S-rough sets is a new research direction of rough sets and rough system.

  1. On Wind and Roughness over Land

    Verkaik, J.W.


    The relation between wind, momentum flux, roughness and land-use in disturbed, non-homogeneous boundary layers is studied. Key questions are: ``how is the roughness related to land-use?'', ``how are wind and friction related to the upstream land-use and roughness?'', and ``is Monin-Obukhov theory

  2. Diffusion-induced line-edge roughness

    Stewart, Michael D.; Schmid, Gerard M.; Goldfarb, Dario L.; Angelopoulos, Marie; Willson, C. Grant


    As feature dimensions shrink, line edge roughness has become an increasing concern in semiconductor fabrication. There are numerous potential contributors to line edge roughness throughout the lithographic process and any measured roughness value on a printed device feature is, like the feature itself, a convolved function of every processing step. When the full lithographic process is used to study line edge roughness, it can be difficult to isolate the contribution to final roughness from any individual processing step or factor. To gain a more fundamental understanding of roughness generation that is specifically related to photoresist chemistry and formulation it is necessary to design experiments that separate out exposure related issues like mask dimension variation or local dose variation ("shot noise"). This can be accomplished using previously reported experimental protocols for bilayer film stack creation. The bilayer experimental approach has been used to study the effect of variations in such factors as post exposure bake time, photoacid generator loading, and developer concentration on roughness generation. Surface roughness of the developed film stacks is measured via atomic force microscopy. Surface roughness of developed bilayer film stacks may be considered analogous to sidewall roughness of printed features. An acrylate-based 193nm photoresist resin and an APEX-type resin are used in these experiments. In addition to experimental results, results from mesoscale lithographic simulations are used to gain further insight into diffusion induced roughness and how roughness in the latent image is modified during the development step.

  3. What is the critical height of leading edge roughness for aerodynamics?

    Bak, Christian; Gaunaa, Mac; Olsen, Anders Smærup;


    In this paper the critical leading edge roughness height is analyzed in two cases: 1) leading edge roughness influencing the lift-drag ratio and 2) leading edge roughness influencing the maximum lift. The analysis was based on wind tunnel measurements on the airfoils NACA0015, Risoe-B1-18 and Ris...... with panel code predictions of the boundary layer momentum thickness created the basis for determining the impact of roughness on the aerodynamic performance. The critical heights were related to the Reynolds numbers and thereby the size of the wind turbines....

  4. Dust Diffusion and Settling in the Presence of Collisions: Trapping (sub)micron Grains in the Midplane

    Krijt, Sebastiaan; Ciesla, Fred J.


    In protoplanetary disks, the distribution and abundance of small (sub)micron grains are important for a range of physical and chemical processes. For example, they dominate the optical depth at short wavelengths and their surfaces are the sites of many important chemical reactions, such as the formation of water. Based on their aerodynamical properties (i.e., their strong dynamical coupling with the surrounding gas) it is often assumed that these small grains are well-mixed with the gas. Our goal is to study the vertical (re)distribution of grains taking into account settling, turbulent diffusion, and collisions with other dust grains. Assuming a fragmentation-limited background dust population, we developed a Monte Carlo approach that follows single monomers as they move through a vertical column of gas and become incorporated in different aggregates as they undergo sticking and fragmenting collisions. We find that (sub)micron grains are not necessarily well-mixed vertically, but can become trapped in a thin layer with a scale height that is significantly smaller than that of the gas. This collisional trapping occurs when the timescale for diffusion is comparable to or longer than the collision timescale in the midplane and its effect is strongest when the most massive particles in the size distribution show significant settling. Based on simulations and analytical considerations, we conclude that for typical dust-to-gas ratios and turbulence levels, the collisional trapping of small grains should be a relatively common phenomenon. The absence of trapping could then indicate a low dust-to-gas ratio, possibly because a large portion of the dust mass has been removed through radial drift or is locked up in planetesimals.

  5. (F)-Rough Integrals and Its Measurements%(F)粗积分与它的度量

    于秀清; 徐凤生; 韩忠月


    (F)-rough integrals is defined on the basis of the dual of function one direction S-rough sets, which has dynamic characteristics. Using (F)-rough integrals, the concepts of expansion measurement-expansion degree and expansion ratio are given. By expansion degree and expansion ratio the changing extent can be expressed with numbers, and the recognition principle of attribute effect on function equivalences is got.

  6. Ellipsometry analysis of a-Si:H solar cell structures with submicron-size textures using glass-side illumination

    Yamaguchi, Shinji, E-mail: [Center of Innovative Photovoltaic Systems, Gifu University, 1-1 Yanagido, Gifu 501-1193 (Japan); FPD Equipment Company, DAINIPPON SCREEN MFG. CO., LTD., 480-1 Takamiya-cho, Hikone, Shiga 522-0292 (Japan); Sugimoto, Yoshio [FPD Equipment Company, DAINIPPON SCREEN MFG. CO., LTD., 480-1 Takamiya-cho, Hikone, Shiga 522-0292 (Japan); Fujiwara, Hiroyuki [Center of Innovative Photovoltaic Systems, Gifu University, 1-1 Yanagido, Gifu 501-1193 (Japan)


    Hydrogenated amorphous silicon (a-Si:H) solar cell structures with submicron-size textures have been determined by spectroscopic ellipsometry (SE) measurements, in which the probe light illuminates the glass/SnO{sub 2}:F/a-Si:H/ZnO:Al/Ag structure from the glass-substrate side. To analyze the inhomogeneous solar cell structures due to random textures, we applied an optical model having two regions with different layer thicknesses. The optical response of the rough interface regions in the textured structures is expressed using the multilayer optical structure, in which the variation of the multiphase compositions toward the depth direction is modeled by a power function. Although only the specular reflection has been considered in the SE analysis, the ellipsometry spectra calculated from our optical model show excellent agreement with the measured spectra, as the diffused light induced by the rough textures has not been detected in our measurement configuration. Furthermore, the layer thicknesses deduced from the SE analysis agree quite well with those evaluated by transmission electron microscopy. Using the SE analysis method developed in this study, the non-destructive structural characterization of large-area a-Si:H solar cell modules can be made by illuminating with the SE probe light from the glass-substrate side. - Highlights: • Textured a-Si:H solar cell structures have been characterized by ellipsometry. • In the measurement, the probe light is illuminated from the glass substrate side. • The inhomogeneous and textured structures are expressed by a new optical model. • The film structures deduced from the analysis agree well with those evaluated by TEM.

  7. Terahertz oscillations in an In0.53Ga0.47As submicron planar Gunn diode

    Khalid, Ata; Dunn, G. M.; Macpherson, R. F.; Thoms, S.; Macintyre, D.; Li, C.; Steer, M. J.; Papageorgiou, V.; Thayne, I. G.; Kuball, M.; Oxley, C. H.; Montes Bajo, M.; Stephen, A.; Glover, J.; Cumming, D. R. S.


    The length of the transit region of a Gunn diode determines the natural frequency at which it operates in fundamental mode—the shorter the device, the higher the frequency of operation. The long-held view on Gunn diode design is that for a functioning device the minimum length of the transit region is about 1.5 μm, limiting the devices to fundamental mode operation at frequencies of roughly 60 GHz. Study of these devices by more advanced Monte Carlo techniques that simulate the ballistic transport and electron-phonon interactions that govern device behaviour, offers a new lower bound of 0.5 μm, which is already being approached by the experimental evidence that has shown planar and vertical devices exhibiting Gunn operation at 600 nm and 700 nm, respectively. The paper presents results of the first ever THz submicron planar Gunn diode fabricated in In0.53Ga0.47As on an InP substrate, operating at a fundamental frequency above 300 GHz. Experimentally measured rf power of 28 μW was obtained from a 600 nm long × 120 μm wide device. At this new length, operation in fundamental mode at much higher frequencies becomes possible—the Monte Carlo model used predicts power output at frequencies over 300 GHz.

  8. Cold Spray Coating of Submicronic Ceramic Particles on Poly(vinyl alcohol) in Dry and Hydrogel States

    Moreau, David; Borit, François; Corté, Laurent; Guipont, Vincent


    We report an approach using cold spray technology to coat poly(vinyl alcohol) (PVA) in polymer and hydrogel states with hydroxyapatite (HA). Using porous aggregated HA powder, we hypothesized that fragmentation of the powder upon cold spray could lead to formation of a ceramic coating on the surface of the PVA substrate. However, direct spraying of this powder led to complete destruction of the swollen PVA hydrogel substrate. As an alternative, HA coatings were successfully produced by spraying onto dry PVA substrates prior to swelling in water. Dense homogeneous HA coatings composed of submicron particles were obtained using rather low-energy spraying parameters (temperature 200-250 °C, pressure 1-3 MPa). Coated PVA substrates could swell in water without removal of the ceramic layer to form HA-coated hydrogels. Microscopic observations and in situ measurements were used to explain how local heating and impact of sprayed aggregates induced surface roughening and strong binding of HA particles to the molten PVA substrate. Such an approach could lead to design of ceramic coatings whose roughness and crystallinity can be finely adjusted to improve interfacing with biological tissues.

  9. Experimental Study on Effects of Ground Roughness on Flow Characteristics of Tornado-Like Vortices

    Wang, Jin; Cao, Shuyang; Pang, Weichiang; Cao, Jinxin


    The three-dimensional wind velocity and dynamic pressure for stationary tornado-like vortices that developed over ground of different roughness categories were investigated to clarify the effects of ground roughness. Measurements were performed for various roughness categories and two swirl ratios. Variations of the vertical and horizontal distributions of velocity and pressure with roughness are presented, with the results showing that the tangential, radial, and axial velocity components increase inside the vortex core near the ground under rough surface conditions. Meanwhile, clearly decreased tangential components are found outside the core radius at low elevations. The high axial velocity inside the vortex core over rough ground surface indicates that roughness produces an effect similar to a reduced swirl ratio. In addition, the pressure drop accompanying a tornado is more significant at elevations closer to the ground under rough compared with smooth surface conditions. We show that the variations of the flow characteristics with roughness are dependent on the vortex-generating mechanism, indicating the need for appropriate modelling of tornado-like vortices.

  10. Characterization of base roughness for granular chute flows

    Jing, Lu; Leung, Y F; Sobral, Y D


    Base roughness plays an important role to the dynamics of granular flows but is yet poorly understood due to the difficulty of its quantification. For a bumpy base made by spheres, at least two factors should be considered to characterize its geometric roughness, namely the size ratio of base- to flow-particles and the packing of base particles. In this paper, we propose a definition of base roughness, Ra, which is a function of both the size ratio and the packing arrangement of base particles. The function is generalized for random and regular packing of multi-layered spheres, where the range of possible values of Ra is studied, along with the optimal values to create maximum base roughness. The new definition is applied to granular flows down chute in both two- and three-dimensional configurations. It is proven to be a good indicator of slip condi- tion, and a transition occurs from slip to non-slip condition as Ra increases. Critical values of Ra are identified for the construction of a non-slip base. The ...

  11. Fog-Influenced Submicron Aerosol Number Size Distributions

    Zikova, N.; Zdimal, V.


    The aim of this work is to evaluate the influence of fog on aerosol particle number size distributions (PNSD) in submicron range. Thus, five-year continuous time series of the SMPS (Scanning Mobility Particle Sizer) data giving information on PNSD in five minute time step were compared with detailed meteorological records from the professional meteorological station Kosetice in the Czech Republic. The comparison included total number concentration and PNSD in size ranges between 10 and 800 nm. The meteorological records consist from the exact times of starts and ends of individual meteorological phenomena (with one minute precision). The records longer than 90 minutes were considered, and corresponding SMPS spectra were evaluated. Evaluation of total number distributions showed considerably lower concentration during fog periods compared to the period when no meteorological phenomenon was recorded. It was even lower than average concentration during presence of hydrometeors (not only fog, but rain, drizzle, snow etc. as well). Typical PNSD computed from all the data recorded in the five years is in Figure 1. Not only median and 1st and 3rd quartiles are depicted, but also 5th and 95th percentiles are plotted, to see the variability of the concentrations in individual size bins. The most prevailing feature is the accumulation mode, which seems to be least influenced by the fog presence. On the contrary, the smallest aerosol particles (diameter under 40 nm) are effectively removed, as well as the largest particles (diameter over 500 nm). Acknowledgements: This work was supported by the projects GAUK 62213 and SVV-2013-267308. Figure 1. 5th, 25th, 50th, 75th and 95th percentile of aerosol particle number size distributions recorded during fog events.

  12. Sub-micron parallel laser direct-write

    Othon, Christina M.; Laracuente, Arnaldo; Ladouceur, H. D.; Ringeisen, Bradley R.


    We have developed a modified laser induced forward transfer (LIFT) technique which allows for the parallel deposition of hundreds of sub-micron features. The approach utilizes a self-assembled monolayer of monodisperse polystyrene microspheres as the focusing element. A monolayer of close-packed microspheres is formed on top of an ultra-thin quartz support (25 μm thick), and a metallic thin film is then deposited on the underside of the quartz. This approach is different from previous parallel microsphere-assisted LIFT experiments that required the deposition of metal directly onto the surface of the periodic microsphere structure. For this study, an 800 nm, 130 fs laser pulse was directed toward the microsphere layer to focus the incident laser beam through the thin quartz layer to the quartz-metal interface. At this interface, a portion of the thin metal film was ablated directly below each microsphere, resulting in an array of holes in the thin metal film. The metal removed from the film was patterned onto a receiving substrate to form an array of discrete deposits. In some cases, a two layer thin film was utilized resulting in the forward transfer of bilayer metal features. The holes and deposited features were characterized using scanning electron microscopy, atomic force microscopy, and scanning Auger electron spectroscopy. The diameter of the holes (0.5-5 μm) as well as the diameter (0.9-5 μm) and quality of the deposited metallic features were modulated by varying the sphere size, incident laser energy, and material composition.

  13. Submicron hard X-ray fluorescence imaging of synthetic elements

    Jensen, Mark P., E-mail: [Chemical Sciences and Engineering Division, Argonne National Laboratory, Argonne, IL 60439 (United States); Aryal, Baikuntha P. [Chemical Sciences and Engineering Division, Argonne National Laboratory, Argonne, IL 60439 (United States); Department of Chemistry, University of Chicago, Chicago, IL 60637 (United States); Gorman-Lewis, Drew [Chemical Sciences and Engineering Division, Argonne National Laboratory, Argonne, IL 60439 (United States); Paunesku, Tatjana [Department of Radiation Oncology, Feinberg School of Medicine, Northwestern University, Chicago, IL 60611 (United States); Department of Radiology, Feinberg School of Medicine, Northwestern University, Chicago, IL 60611 (United States); Lai, Barry; Vogt, Stefan [X-ray Science Division, Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439 (United States); Woloschak, Gayle E. [Department of Radiation Oncology, Feinberg School of Medicine, Northwestern University, Chicago, IL 60611 (United States); Department of Radiology, Feinberg School of Medicine, Northwestern University, Chicago, IL 60611 (United States)


    Highlights: Black-Right-Pointing-Pointer Actinide elements are mapped with L-edge X-rays and better than 400 nm resolution. Black-Right-Pointing-Pointer A typical detection limit was 2.9 Multiplication-Sign 10{sup -20} moles Pu {mu}m{sup -2}. Black-Right-Pointing-Pointer XANES measurements provide chemical information in 0.1 {mu}m{sup 2} spots. Black-Right-Pointing-Pointer Selection of materials for encapsulation is important for avoiding interferences. - Abstract: Synchrotron-based X-ray fluorescence microscopy (XFM) using hard X-rays focused into sub-micron spots is a powerful technique for elemental quantification and mapping, as well as microspectroscopic measurements such as {mu}-XANES (X-ray absorption near edge structure). We have used XFM to image and simultaneously quantify the transuranic element plutonium at the L{sub 3} or L{sub 2}-edge as well as Th and lighter biologically essential elements in individual rat pheochromocytoma (PC12) cells after exposure to the long-lived plutonium isotope {sup 242}Pu. Elemental maps demonstrate that plutonium localizes principally in the cytoplasm of the cells and avoids the cell nucleus, which is marked by the highest concentrations of phosphorus and zinc, under the conditions of our experiments. The minimum detection limit under typical acquisition conditions with an incident X-ray energy of 18 keV for an average 202 {mu}m{sup 2} cell is 1.4 fg Pu or 2.9 Multiplication-Sign 10{sup -20} moles Pu {mu}m{sup -2}, which is similar to the detection limit of K-edge XFM of transition metals at 10 keV. Copper electron microscopy grids were used to avoid interference from gold X-ray emissions, but traces of strontium present in naturally occurring calcium can still interfere with plutonium detection using its L{sub {alpha}} X-ray emission.

  14. The role of adsorbed water on the friction of a layer of submicron particles

    Sammis, Charles G.; Lockner, David A.; Reches, Ze’ev


    Anomalously low values of friction observed in layers of submicron particles deformed in simple shear at high slip velocities are explained as the consequence of a one nanometer thick layer of water adsorbed on the particles. The observed transition from normal friction with an apparent coefficient near μ = 0.6 at low slip speeds to a coefficient near μ = 0.3 at higher slip speeds is attributed to competition between the time required to extrude the water layer from between neighboring particles in a force chain and the average lifetime of the chain. At low slip speeds the time required for extrusion is less than the average lifetime of a chain so the particles make contact and lock. As slip speed increases, the average lifetime of a chain decreases until it is less than the extrusion time and the particles in a force chain never come into direct contact. If the adsorbed water layer enables the otherwise rough particles to rotate, the coefficient of friction will drop to μ = 0.3, appropriate for rotating spheres. At the highest slip speeds particle temperatures rise above 100°C, the water layer vaporizes, the particles contact and lock, and the coefficient of friction rises to μ = 0.6. The observed onset of weakening at slip speeds near 0.001 m/s is consistent with the measured viscosity of a 1 nm thick layer of adsorbed water, with a minimum particle radius of approximately 20 nm, and with reasonable assumptions about the distribution of force chains guided by experimental observation. The reduction of friction and the range of velocities over which it occurs decrease with increasing normal stress, as predicted by the model. Moreover, the analysis predicts that this high-speed weakening mechanism should operate only for particles with radii smaller than approximately 1 μm. For larger particles the slip speed required for weakening is so large that frictional heating will evaporate the adsorbed water and weakening will not occur.

  15. Axis Problem of Rough 3-Valued Algebras

    Jianhua Dai; Weidong Chen; Yunhe Pan


    The collection of all the rough sets of an approximation space has been given several algebraic interpretations, including Stone algebras, regular double Stone algebras, semi-simple Nelson algebras, pre-rough algebras and 3-valued Lukasiewicz algebras. A 3-valued Lukasiewicz algebra is a Stone algebra, a regular double Stone algebra, a semi-simple Nelson algebra, a pre-rough algebra. Thus, we call the algebra constructed by the collection of rough sets of an approximation space a rough 3-valued Lukasiewicz algebra. In this paper,the rough 3-valued Lukasiewicz algebras, which are a special kind of 3-valued Lukasiewicz algebras, are studied. Whether the rough 3-valued Lukasiewicz algebra is a axled 3-valued Lukasiewicz algebra is examined.

  16. Rough Sets in Approximate Solution Space

    Hui Sun; Wei Tian; Qing Liu


    As a new mathematical theory, Rough sets have been applied to processing imprecise, uncertain and in complete data. It has been fruitful in finite and non-empty set. Rough sets, however, are only served as the theoretic tool to discretize the real function. As far as the real function research is concerned, the research to define rough sets in the real function is infrequent. In this paper, we exploit a new method to extend the rough set in normed linear space, in which we establish a rough set,put forward an upper and lower approximation definition, and make a preliminary research on the property of the rough set. A new tool is provided to study the approximation solutions of differential equation and functional variation in normed linear space. This research is significant in that it extends the application of rough sets to a new field.

  17. Function S-rough sets and mining-discovery of rough law in systems

    Shi Kaiquan; Xia Jiarong


    Function S-rough sets (function singular rough sets) is defined on -function equivalence class [u]. Function S-rough sets is the extension form of S-rough sets. By using the function S-rough sets, this paper gives rough law generation model of -function equivalence class, discussion on law mining and law discovery in systems, and application of law mining and law discovery in communication system. Function S-rough sets is a new theory and method in law mining research.

  18. Microstructures and properties of cold drawn and annealed submicron crystalline Cu-5%Cr alloy

    HE Wen-xiong; YU Yang; WANG Er-de; SUN Hong-fei; HU Lian-xi; CHEN Hui


    The microstructures and properties after cold drawing and subsequent annealing of submicron crystalline Cu-5%Cr (mass fraction) alloy were investigated. The results show that, the microstructure of submicron crystalline Cu-5%Cr can be further refined by cold drawing. After cold drawing, the grains of Cu-5%Cr alloy with grain size of 400-500 nm can be refined to be cellular structures and subgrains with size of 100-200 nm. Both strength and ductility of Cu-5%Cr alloy can be enhanced by cold drawing, and the optimal mechanical properties can be achieved with drawing deformation increasing. It is suggested that dislocation glide is still the main mechanism in plastic deformation of submicron crystalline Cu-5%Cr, but grain boundary slide and diffusion may play more and more important roles with drawing deformation increasing. When the cold drawn Cu-5%Cr wires are annealed at 550 ℃, fine recrystal grains with grain size of 200-300 nm can be obtained. Furthermore, there are lots of fine Cr particles precipitated during annealing, by which the recrystallization softening temperatures of the cold drawn Cu-5%Cr wires can be increased to 480-560 ℃. Due to the fact that Cr particles have the effect of restricting Cu grains growth, a favorable structural thermal stability of the submicron crystalline Cu-5%Cr can be achieved, and the submicron grained microstructure can be retained at high temperature annealing.

  19. Deciphering sub-micron ice particles on Enceladus surface

    Scipioni, F.; Schenk, P.; Tosi, F.; D'Aversa, E.; Clark, R.; Combe, J.-Ph.; Ore, C. M. Dalle


    The surface of Saturn's moon Enceladus is composed primarily by pure water ice. The Cassini spacecraft has observed present-day geologic activity at the moon's South Polar Region, related with the formation and feeding of Saturn's E-ring. Plumes of micron-sized particles, composed of water ice and other non-ice contaminants (e.g., CO2, NH3, CH4), erupt from four terrain's fractures named Tiger Stripes. Some of this material falls back on Enceladus' surface to form deposits that extend to the North at ∼40°W and ∼220°W, with the highest concentration found at the South Pole. In this work we analyzed VIMS-IR data to identify plumes deposits across Enceladus' surface through the variation in band depth of the main water ice spectral features. To characterize the global variation of water ice band depths across Enceladus, the entire surface was sampled with an angular resolution of 1° in both latitude and longitude, and for each angular bin we averaged the value of all spectral indices as retrieved by VIMS. The position of the plumes' deposits predicted by theoretical models display a good match with water ice band depths' maps on the trailing hemisphere, whereas they diverge significantly on the leading side. Space weathering processes acting on Enceladus' surface ionize and break up water ice molecules, resulting in the formation of particles smaller than one micron. We also mapped the spectral indices for sub-micron particles and we compared the results with the plumes deposits models. Again, a satisfactory match is observed on the trailing hemisphere only. Finally, we investigated the variation of the depth of the water ice absorption bands as a function of the phase angle. In the visible range, some terrains surrounding the Tiger Stripes show a decrease in albedo when the phase angle is smaller than 10°. This unusual effect cannot be confirmed by near infrared data, since observations with a phase angle lower than 10° are not available. For phase angle

  20. Study on the submicron and micron morphology and the properties of poor bituminous coal burnout

    Pei-Fang Fu; Huai-Chun Zhou; Qing-Yan Fang; Hai Yao; Jianrong Qiu; Minghou Xu [Huazhong University of Science and Technology, Wuhan (China). State Key Laboratory of Coal Combustion


    Carbon burnout and its reaction mechanism have been widely focused on in the past decades. The properties of burnout, submicron and micron morphology and the reaction mechanism of poor bituminous coal/char (PBC) in a W-shaped power plant boiler was studied and was compared with those in DTF and in TGA, which showed that the degree of PBC burnout in TGA at 1450{sup o}C was greater than or approximately equal to that in a W-shaped boiler, and that the complexity of the reactions among residual char, oxygen and SiO{sub 2} did not seem to result in mass loss in TGA, although the weight percentage of the residual char in ash decreased from 33% ad (air dry basis) at 900{sup o}C to 9% and at 1450{sup o}C. According to the distribution of pores and the properties of the char burnout, the char can be simply categorized into three classes: char burnout easy, char burnout difficult and char burnout very difficult. The differences of the reaction mechanism must be considered while predicting the burning rate and degree of char burnout in a full-scale boiler by making use of experimental results from TGA and DTF. A different char particle contains markedly different amount of carbons, but for a special char particle, the ratio of carbon to ash is generally constant, and an ash shell does not exist on the char surface. The fusion mineral matter composing of C-O-Si-Al is amorphous, not in the form of Al{sub 2}O{sub 3} and SiO{sub 2} above 1450{sup o}C.

  1. Sources and characteristics of sub-micron aerosols in the San Joaquin Valley, CA

    Bahreini, R.; Middlebrook, A. M.; Brioude, J.; Brock, C. A.; de Gouw, J. A.; Hall, K.; Holloway, J. S.; Neuman, J.; Nowak, J. B.; Pollack, I. B.; Ryerson, T. B.; Warneke, C.; Parrish, D. D.


    The NOAA WP-3D aircraft performed several flights in the San Joaquin Valley (SJV), California during the CalNex-2010 (California Research at the Nexus of Air Quality and Climate Change) field project in May-June 2010. SJV is generally a rural valley, with a high concentration of feedlots and agricultural sites as well as urbanized centers such as Fresno and Bakersfield. Preliminary results on size-resolved chemical composition of sub-micron aerosols measured using a compact time-of-flight aerosol mass spectrometer, measurements of trace gases affecting secondary production of aerosols, and FLEXPART back trajectory analyses are presented in order to identify sources of aerosols transported to or produced in the valley. Observed enhancements in various trace gases and aerosol species indicate a mixed influence from urban, industrial, and animal feedlots in the SJV. Three distinct observations suggest a complex transport pattern of pollutants with different origins to and within the valley: 1) CO and NOx mixing ratios were prominent downwind of the urban areas in the valley; 2) SO2, aerosol organics and sulfate were higher closer to the foothills of the Sierra Nevada Mountains on the east of the valley; 3) high concentration of aerosol phase ammonium and nitrate were observed in NH3-rich air masses, directly downwind of the feedlots in the central part of the valley. Aerosol enhancements in each of these air mass categories relative to the background determine the relative contribution and significance of different sources to aerosol loadings in the valley. Differences in VOC measurements and meteorology will be explored to investigate the observed variation in characteristics of organics on different days.

  2. Microfluidic separation of satellite droplets as the basis of a monodispersed micron and submicron emulsification system.

    Tan, Yung-Chieh; Lee, Abraham Phillip


    Emulsions are widely used to produce sol-gel, drugs, synthetic materials, and food products. Recent advancements in microfluidic droplet emulsion technology has enabled the precise sampling and processing of small volumes of fluids (picoliter to femtoliter) by the controlled viscous shearing in microchannels. However the generation of monodispersed droplets smaller than 1 microm without surfactants has been difficult to achieve. Normally, the generation of satellite droplets along with parent droplets is undesirable and makes it difficult to control volume and purity of samples in droplets. In this paper, however, several methods are presented to passively filter out satellite droplets from the generation of parent droplets and use these satellite droplets as the source for monodispersed production of submicron emulsions. A passive satellite droplet filtration system and a dynamic satellite droplet separation system are demonstrated. Satellite droplets are filtered from parent droplets with a two-layer channel geometry. This design allows the creation and collection of droplets that are less than 100 nm in diameter. In the dynamic separation system, satellite droplets of defined sizes can be selectively separated into different collecting zones. The separation of the satellite droplets into different collecting zones correlates with the cross channel position of the satellite droplets during the breakup of the liquid thread. The delay time for droplets to switch between the different alternating collecting zones is nominally 1 min and is proportional to the ratio of the oil shear flows. With our droplet generation system, monodispersed satellite droplets with an average radius of 2.23 +/- 0.11 microm, and bidispersed secondary and tertiary satellite droplets with radii of 1.55 +/- 0.07 microm and 372 +/- 46 nm respectively, have been dynamically separated and collected.

  3. Relevance of roughness parameters of surface finish in precision hard turning.

    Jouini, Nabil; Revel, Philippe; Bigerelle, Maxence


    Precision hard turning is a process to improve the surface integrity of functional surfaces. Machining experiments are carried out on hardened AISI 52100 bearing steel under dry condition using c-BN cutting tools. A full factorial experimental design is used to characterize the effect of cutting parameters. As surface topography is characterized by numerous roughness parameters, their relative relevance is investigated by statistical indices of performance computed by combining the analysis of variance, discriminant analysis and the bootstrap method. The analysis shows that the profile Length ratio (Lr) and the Roughness average (Ra) are the relevant pair of roughness parameters which best discriminates the effect of cutting parameters and enable the classification of surfaces which cannot be distinguished by one parameter: low profile length ratio Lr (Lr = 100.23%) is clearly distinguished from an irregular surface corresponding to a profile length ratio Lr (Lr = 100.42%), whereas the roughness average Ra values are nearly identical.

  4. Fabrication and characterization of submicron polymer waveguides by micro-transfer molding

    Wu, Te-Wei [Iowa State Univ., Ames, IA (United States)


    Various methods exist for fabrication of micron and submicron sized waveguide structures. However, most of them include expensive and time consuming semiconductor fabrication techniques. An economical method for fabricating waveguide structures is introduced and demonstrated in this thesis. This method is established based on previously well-developed photonic crystal fabrication method called two-polymer microtransfer molding. The waveguide in this work functions by a coupler structure that diffracts the incident light into submicron polymer rods. The light is then guided through the rods. Characterization is done by collecting the light that has been guided through the waveguide and exits the end of these submicron polymer bars. The coupling and waveguiding capabilities are demonstrated using two light sources, a laser and white light.

  5. Air flow through smooth and rough cracks

    Kula, H.-G.; Sharples, S. [Sheffield Univ. (United Kingdom). Dept. of Building Science


    A series of laboratory experiments are described which investigated the effect of surface roughness on the air flow characteristics of simple, straight-through, no-bend cracks with smooth and rough internal surfaces. The crack thicknesses used in the study were 1.0, 1.5 and 2.0mm. The crack lengths, in the direction of flow, were 50.8mm and 76.2mm. For the rough cracks the roughness was simulated with two different grades of commercially available energy-cloth (grade 60 and 100). The experimental results were satisfactorily fitted to a quadratic relationship between {Delta}p and Q of the form {Delta}p = AQ + BQ{sup 2} for both the smooth and rough crack data. The effect of roughness on the reduction of air flowing through a crack is also discussed. (author)

  6. SEM/EDS of Submicron and Coarse PM Using Modified Passive Aerosol Sampler Substrates

    Wagner, J.; Wang, Z.; Willis, B.; Casuccio, G.


    Deployment of multiple UNC Passive Aerosol Samplers is an inexpensive and unobtrusive technique for assessing airborne particulate matter (PM) exposure and spatial variability. Computer-controlled SEM/EDS (Scanning Electron Microscopy / Energy-Dispersive X-ray Spectroscopy) is used to measure the deposited particle mass and chemistry. A deposition velocity model is used to obtain ambient PM and elemental size distributions. Previous results have correlated well with active sampler results in environments dominated by coarse mineral dusts. To accurately measure submicron and carbonaceous aerosols, an improved collection substrate is needed. Previous studies used a double-sided carbon adhesive tab, which was ideal for coarse PM but under-detected submicron PM. One promising alternative is polycarbonate (PC) filter substrates. Another is transmission electron microscope (TEM) grids with formvar films mounted over holes drilled in the samplers. Preliminary tests of PC filters and TEM grid substrates, including tests in areas with smoke aerosols, exhibited substantial submicron aerosol and differing elemental size distributions. Detailed qualitative and quantitative evidence shows that the PC filters retained coarse PM well and yielded improved submicron PM imaging. TEM grids yield the best imaging and chemistry of submicron carbonaceous PM, but potentially the poorest retention of coarse PM. PM and elemental size distributions are presented for collocated passive samplers using the three substrate types, in both indoor and outdoor environments. Several methods are proposed to further optimize passive sampling of both submicron and coarse PM. Although this work was reviewed by EPA and approved for publication, it may not necessarily reflect official Agency policy.

  7. Dissipative Quantum Tunneling of a Single Defect in a Submicron Bismuth Wire Below 1 K

    Chun, Kookjin

    The quantum mechanical problem of a particle tunneling in a double-well potential is of great theoretical and experimental interest. Interaction of the tunneling system with a dissipative environment can have a striking effect on the tunneling dynamics. A very interesting case is that of ohmic dissipation, which occurs when an atom tunnels in a metal in the presence of conduction electrons. We have studied the electrical resistance of submicron Bi wires at low temperature. Due to quantum interference of the conduction electrons, the resistance is highly sensitive to the motion of even a single scattering center. We observe discrete switching of the resistance due to the motion of bistable defects in the sample. We have measured the tunneling rates of a particular defect over the temperature range 0.1-2 K and magnetic field range 0-7 T. The energy asymmetry, varepsilon, of this defect varied over the range 40-420 mK depending on the value of the magnetic field. The temperature dependence of the tunneling rates is qualitatively different for the cases k_{B}T effect of Joule heating on the dynamics of the defect in the same sample. The ratio of the fast and slow transition rates of a defect depends on temperature through the detailed balance relation, gamma_{f}/ gamma_{s} e^ {varepsilon / k_{B}T}. We interpret this ratio as a local thermometer. When varepsilon / k_{B}T > 1, this ratio is sensitive to small changes in the temperature T seen by the defect. Since the defect is strongly coupled to the conduction electrons in the sample below 1 K, we interpret its sensitivity to drive current as an indication of electron heating. As the drive current increases, the defect temperature approaches a power law dependence with the drive current, independent of the nominal lattice temperature. The data are consistent with a simple model of heating, and strong thermal coupling between the defect and the electron bath. We also tried to measure the electron temperature directly

  8. Aerosols in the tropical and subtropical UT/LS: in-situ measurements of submicron particle abundance and volatility

    S. Borrmann


    Full Text Available Processes occurring in the tropical upper troposphere (UT, the Tropical Transition Layer (TTL, and the lower stratosphere (LS are of importance for the global climate, for stratospheric dynamics and air chemistry, and for their influence on the global distribution of water vapour, trace gases and aerosols. In this contribution we present aerosol and trace gas (in-situ measurements from the tropical UT/LS over Southern Brazil, Northern Australia, and West Africa. The instruments were operated on board of the Russian high altitude research aircraft M-55 "Geophysica" and the DLR Falcon-20 during the campaigns TROCCINOX (Araçatuba, Brazil, February 2005, SCOUT-O3 (Darwin, Australia, December 2005, and SCOUT-AMMA (Ouagadougou, Burkina Faso, August 2006. The data cover submicron particle number densities and volatility from the COndensation PArticle counting System (COPAS, as well as relevant trace gases like N2O, ozone, and CO. We use these trace gas measurements to place the aerosol data into a broader atmospheric context. Also a juxtaposition of the submicron particle data with previous measurements over Costa Rica and other tropical locations between 1999 and 2007 (NASA DC-8 and NASA WB-57F is provided. The submicron particle number densities, as a function of altitude, were found to be remarkably constant in the tropical UT/LS altitude band for the two decades after 1987. Thus, a parameterisation suitable for models can be extracted from these measurements. Compared to the average levels in the period between 1987 and 2007 a slight increase of particle abundances was found for 2005/2006 at altitudes with potential temperatures, Θ, above 430 K. The origins of this increase are unknown except for increases measured during SCOUT-AMMA. Here the eruption of the Soufrière Hills volcano in the Caribbean caused elevated particle mixing ratios. The vertical profiles from Northern hemispheric mid-latitudes between 1999 and 2006 also are

  9. Aerosols in the tropical and subtropical UT/LS: in-situ measurements of submicron particle abundance and volatility

    Borrmann, S.; Kunkel, D.; Weigel, R.; Minikin, A.; Deshler, T.; Wilson, J. C.; Curtius, J.; Volk, C. M.; Homan, C. D.; Ulanovsky, A.; Ravegnani, F.; Viciani, S.; Shur, G. N.; Belyaev, G. V.; Law, K. S.; Cairo, F.


    Processes occurring in the tropical upper troposphere (UT), the Tropical Transition Layer (TTL), and the lower stratosphere (LS) are of importance for the global climate, for stratospheric dynamics and air chemistry, and for their influence on the global distribution of water vapour, trace gases and aerosols. In this contribution we present aerosol and trace gas (in-situ) measurements from the tropical UT/LS over Southern Brazil, Northern Australia, and West Africa. The instruments were operated on board of the Russian high altitude research aircraft M-55 "Geophysica" and the DLR Falcon-20 during the campaigns TROCCINOX (Araçatuba, Brazil, February 2005), SCOUT-O3 (Darwin, Australia, December 2005), and SCOUT-AMMA (Ouagadougou, Burkina Faso, August 2006). The data cover submicron particle number densities and volatility from the COndensation PArticle counting System (COPAS), as well as relevant trace gases like N2O, ozone, and CO. We use these trace gas measurements to place the aerosol data into a broader atmospheric context. Also a juxtaposition of the submicron particle data with previous measurements over Costa Rica and other tropical locations between 1999 and 2007 (NASA DC-8 and NASA WB-57F) is provided. The submicron particle number densities, as a function of altitude, were found to be remarkably constant in the tropical UT/LS altitude band for the two decades after 1987. Thus, a parameterisation suitable for models can be extracted from these measurements. Compared to the average levels in the period between 1987 and 2007 a slight increase of particle abundances was found for 2005/2006 at altitudes with potential temperatures, Θ, above 430 K. The origins of this increase are unknown except for increases measured during SCOUT-AMMA. Here the eruption of the Soufrière Hills volcano in the Caribbean caused elevated particle mixing ratios. The vertical profiles from Northern hemispheric mid-latitudes between 1999 and 2006 also are compact enough to derive a

  10. Simplified Approach to Predicting Rough Surface Transition

    Boyle, Robert J.; Stripf, Matthias


    Turbine vane heat transfer predictions are given for smooth and rough vanes where the experimental data show transition moving forward on the vane as the surface roughness physical height increases. Consiste nt with smooth vane heat transfer, the transition moves forward for a fixed roughness height as the Reynolds number increases. Comparison s are presented with published experimental data. Some of the data ar e for a regular roughness geometry with a range of roughness heights, Reynolds numbers, and inlet turbulence intensities. The approach ta ken in this analysis is to treat the roughness in a statistical sense , consistent with what would be obtained from blades measured after e xposure to actual engine environments. An approach is given to determ ine the equivalent sand grain roughness from the statistics of the re gular geometry. This approach is guided by the experimental data. A roughness transition criterion is developed, and comparisons are made with experimental data over the entire range of experimental test co nditions. Additional comparisons are made with experimental heat tran sfer data, where the roughness geometries are both regular as well a s statistical. Using the developed analysis, heat transfer calculatio ns are presented for the second stage vane of a high pressure turbine at hypothetical engine conditions.

  11. Rough set models of Physarum machines

    Pancerz, Krzysztof; Schumann, Andrew


    In this paper, we consider transition system models of behaviour of Physarum machines in terms of rough set theory. A Physarum machine, a biological computing device implemented in the plasmodium of Physarum polycephalum (true slime mould), is a natural transition system. In the behaviour of Physarum machines, one can notice some ambiguity in Physarum motions that influences exact anticipation of states of machines in time. To model this ambiguity, we propose to use rough set models created over transition systems. Rough sets are an appropriate tool to deal with rough (ambiguous, imprecise) concepts in the universe of discourse.


    杨强; 杨卫


    The authors proposed a plausible explanation for the deviation of experimental data for sub-micron polycrystals from the Hall-Petch relation by in troducing the configuration entropy. The present paper extends the previous two dimensional analysis to the three-dimensional case. The statistical distribution of dislocation lengths within a spherical grain and the bow-out of dislocations are con sidered. According to Ashby's model, analyses are pursued for the statistically stored dislocations and geometrically necessary dislocations, respectively. It is confirmed that the configuration entropy model can predict the abnormal Hall-Petch depen dence for grain sizes in the sub-micron range.

  13. Multifractal analysis of atmospheric sub-micron particle data

    Arizabalo, Rubén Darío; González-Ávalos, Eugenio; Korvin, Gabor


    Multifractal analysis was used to describe air pollution by sub-micrometric atmospheric particles. Atmospheric particle concentrations were studied from March 31 to April 21, 2006, as part of the MILAGRO campaign at the Jasso Station by means of an SMPS. Sixteen campaign days were selected to carry out the multifractal analysis of the experimental data through Singularity Spectra f(α). In this work, the roughness/smoothness feature of atmospheric particle distributions was studied by means of the Hölder exponent (α), which can be associated with the intensity of particle emissions through time and the randomness of the external emission sources. Multifractal analysis has been found to be a useful tool to establish intensity fluctuations of atmospheric data.

  14. Rock discontinuity surface roughness variation with scale

    Bitenc, Maja; Kieffer, D. Scott; Khoshelham, Kourosh


    ABSTRACT: Rock discontinuity surface roughness refers to local departures of the discontinuity surface from planarity and is an important factor influencing the shear resistance. In practice, the Joint Roughness Coefficient (JRC) roughness parameter is commonly relied upon and input to a shear strength criterion such as developed by Barton and Choubey [1977]. The estimation of roughness by JRC is hindered firstly by the subjective nature of visually comparing the joint profile to the ten standard profiles. Secondly, when correlating the standard JRC values and other objective measures of roughness, the roughness idealization is limited to a 2D profile of 10 cm length. With the advance of measuring technologies that provide accurate and high resolution 3D data of surface topography on different scales, new 3D roughness parameters have been developed. A desirable parameter is one that describes rock surface geometry as well as the direction and scale dependency of roughness. In this research a 3D roughness parameter developed by Grasselli [2001] and adapted by Tatone and Grasselli [2009] is adopted. It characterizes surface topography as the cumulative distribution of local apparent inclination of asperities with respect to the shear strength (analysis) direction. Thus, the 3D roughness parameter describes the roughness amplitude and anisotropy (direction dependency), but does not capture the scale properties. In different studies the roughness scale-dependency has been attributed to data resolution or size of the surface joint (see a summary of researches in [Tatone and Grasselli, 2012]). Clearly, the lower resolution results in lower roughness. On the other hand, have the investigations of surface size effect produced conflicting results. While some studies have shown a decrease in roughness with increasing discontinuity size (negative scale effect), others have shown the existence of positive scale effects, or both positive and negative scale effects. We

  15. Effect of roughness on imaging and characterizing rough crack-like defect using ultrasonic arrays

    Zhang, J.; Drinkwater, B. W.; Wilcox, P. D.


    All naturally occurring crack-like defects in solid structures are rough to some degree, which can affect defect inspection and characterization. Based on the simulated array data for various rough cracks and the total focusing method imaging algorithm, the effect of roughness on defect imaging and characterization was discussed. The array data was simulated by using the forward model combining with scattering matrices for various rough cracks. The scattering matrix describes the scattering field of a scatterer from all possible incident and scattering directions. It is shown that roughness can be either beneficial or detrimental to the detectability of a crack-like defect, depending on the defect characteristics such as length, roughness, correlation length, orientation angle, and array inspection configuration. It is also shown that roughness can cause the underestimation of length of rough crack-like defects by using the image-based approach.

  16. Wetting properties of molecularly rough surfaces

    Svoboda, Martin; Malijevský, Alexandr; Lísal, Martin


    We employ molecular dynamics simulations to study the wettability of nanoscale rough surfaces in systems governed by Lennard-Jones (LJ) interactions. We consider both smooth and molecularly rough planar surfaces. Solid substrates are modeled as a static collection of LJ particles arranged in a face-centered cubic lattice with the (100) surface exposed to the LJ fluid. Molecularly rough solid surfaces are prepared by removing several strips of LJ atoms from the external layers of the substrate, i.e., forming parallel nanogrooves on the surface. We vary the solid-fluid interactions to investigate strongly and weakly wettable surfaces. We determine the wetting properties by measuring the equilibrium droplet profiles that are in turn used to evaluate the contact angles. Macroscopic arguments, such as those leading to Wenzel's law, suggest that surface roughness always amplifies the wetting properties of a lyophilic surface. However, our results indicate the opposite effect from roughness for microscopically corrugated surfaces, i.e., surface roughness deteriorates the substrate wettability. Adding the roughness to a strongly wettable surface shrinks the surface area wet with the liquid, and it either increases or only marginally affects the contact angle, depending on the degree of liquid adsorption into the nanogrooves. For a weakly wettable surface, the roughness changes the surface character from lyophilic to lyophobic due to a weakening of the solid-fluid interactions by the presence of the nanogrooves and the weaker adsorption of the liquid into the nanogrooves.

  17. Preparation of rough microsomes from rat liver.

    Sabatini, David D


    This protocol describes how to prepare rat liver rough microsomes that contain undegraded membrane-bound polysomes and can function very well in an in vitro translation system. It uses endogenous ribonuclease inhibitor in all steps, avoiding pelleting rough microsomes in all steps and sacrificing good recovery.


    Chen Jiecheng; Wang Silei


    In this survery report, we shall mainly summarize some recent progress, interesting problems and typi cal methods used in the theory related to rough Marcinkiewicz integrals and rough singular integrals on product spaces. In addition, we give new proofs for some known results.

  19. Prediction of Ductile Fracture Surface Roughness Scaling

    Needleman, Alan; Tvergaard, Viggo; Bouchaud, Elisabeth


    Experimental observations have shown that the roughness of fracture surfaces exhibit certain characteristic scaling properties. Here, calculations are carried out to explore the extent to which a ductile damage/fracture constitutive relation can be used to model fracture surface roughness scaling....... The scaling properties of the predicted thickness average fracture surfaces are calculated and the results are discussed in light of experimental observations....

  20. Axiomatic Characterizations of IVF Rough Approximation Operators

    Guangji Yu


    Full Text Available This paper is devoted to the study of axiomatic characterizations of IVF rough approximation operators. IVF approximation spaces are investigated. The fact that different IVF operators satisfy some axioms to guarantee the existence of different types of IVF relations which produce the same operators is proved and then IVF rough approximation operators are characterized by axioms.

  1. Influence of surface roughness on dispersion forces

    Svetovoy, V. B.; Palasantzas, G.

    Surface roughness occurs in a wide variety of processes where it is both difficult to avoid and control. When two bodies are separated by a small distance the roughness starts to play an important role in the interaction between the bodies, their adhesion, and friction. Control of this

  2. Hydrodynamics and Roughness of Irregular Boundaries


    principle component analysis (PCA) similar to that used by Preston (2009) for ship- mounted multibeam data. Several variables derived from the...complex boundaries as well as characterization of acoustic and optical processes. Turbulent processes at the seabed are at the foundation of littoral...nearshore hydrodynamics, turbulence over rough beds influences optical and acoustic properties. Bed roughness also directly affects acoustic propagation in

  3. Bed roughness experiments in supply limited conditions

    Spekkers, Matthieu; Tuijnder, Arjan; Ribberink, Jan S.; Hulscher, Suzanne J.M.H.; Parsons, D.R.; Garlan, T.; Best, J.L.


    Reliable roughness models are of great importance, for example, when predicting water levels in rivers. The currently available roughness models are based on fully mobile bed conditions. However, in rivers where widely graded sediments are present more or less permanent armour layers can develop

  4. Turning rough sleepers into responsible citizens

    E. Tonkens; dr Lia van Doorn


    On the eve of the twenty-first century, it is a scandal that there are still people sleeping rough on our streets. This is not a situation we can continue to tolerate in a modern and civil society. These were the words of Tony Blair in his foreword to the policy document Rough Sleeping, The Governme

  5. Roughness on Dutch railway wheels and rails

    Dings, P.C.; Dittrich, M.G.


    Surface roughness on 150 railway wheels and on the rails of 30 sites in the Netherlands have been measured. Block braked wheels were found to show higher roughnesses than the rail at any site. The smoothest rail is 8 dB smoother than the smoothest wheel. It was concluded that in reducing railway

  6. Computation of surface roughness using optical correlation

    A M hamed; M Saudy


    The laser speckle photography is used to calculate the average surface roughness from the autocorrelation function of the aluminum diffuse objects. The computed results of surface roughness obtained from the profile shapes of the autocorrelation function of the diffuser show good agreement with the results obtained by the stylus profile meter.

  7. Modeling And Analysis Of The Surface Roughness And Geometrical Error Using Taguchi And Response Surface Methodology



    Full Text Available This experimental work presents a technique to determine the better surface quality by controlling the surface roughness and geometrical error. In machining operations, achieving desired surface quality features of the machined product is really a challenging job. Because, these quality features are highly correlated and areexpected to be influenced directly or indirectly by the direct effect of process parameters or their interactive effects. Thus The four input process parameters such as spindle speed, depth of cut, feed rate, and stepover have been selected to minimize the surface roughness and geometrical error simultaneously by using the robustdesign concept of Taguchi L9(34 method coupled with Response surface concept. Mathematical models for surface roughness and geometrical error were obtained from response surface analysis to predict values of surface roughness and geometrical error. S/N ratio and ANOVA analyses were also performed to obtain for significant parameters influencing surface roughness and geometrical error.

  8. New strategies for submicron characterization the carbon binding of reactive minerals in long-term contrasting fertilized soils: implications for soil carbon storage

    Xiao, Jian; He, Xinhua; Hao, Jialong; Zhou, Ying; Zheng, Lirong; Ran, Wei; Shen, Qirong; Yu, Guanghui


    Mineral binding is a major mechanism for soil carbon (C) stabilization. However, the submicron information about the in situ mechanisms of different fertilization practices affecting organo-mineral complexes and associated C preservation remains unclear. Here, we applied nano-scale secondary ion mass spectrometry (NanoSIMS), X-ray photoelectron spectroscopy (XPS), and X-ray absorption fine structure spectroscopy (XAFS) to examine differentiating effects of inorganic versus organic fertilization on interactions between highly reactive minerals and soil C preservation. To examine such interactions, soils and their extracted colloids were collected during a 24-year long-term fertilization period (1990-2014) (no fertilization, control; chemical nitrogen (N), phosphorus (P), and potassium (K) fertilization, NPK; and NPK plus swine manure fertilization, NPKM). The results for different fertilization conditions showed a ranked soil organic matter concentration with NPKM > NPK > control. Meanwhile, oxalate-extracted Al (Alo), Fe (Feo), short-range ordered Al (Alxps), Fe (Fexps), and dissolved organic carbon (DOC) ranked with NPKM > control > NPK, but the ratios of DOC / Alxps and DOC / Fexps ranked with NPKM > NPK > control. Compared with the NPK treatment, the NPKM treatment enhanced the C-binding loadings of Al and Fe minerals in soil colloids at the submicron scale. Furthermore, a greater concentration of highly reactive Al and Fe minerals was presented under NPKM than under NPK. Together, these submicron-scale findings suggest that both the reactive mineral species and their associations with C are differentially affected by 24-year long-term inorganic and organic fertilization.

  9. Identification of characteristic mass spectrometric markers for primary biological aerosol particles and comparison with field data from submicron pristine aerosol particles

    Freutel, F.; Schneider, J.; Zorn, S. R.; Drewnick, F.; Borrmann, S.; Hoffmann, T.; Martin, S. T.


    The contribution of primary biological aerosol (PBA) to the total aerosol particle concentration is estimated to range between 25 and 80%, depending on location and season. Especially in the tropical rain forest it is expected that PBA is a major source of particles in the supermicron range, and is also an important fraction of the submicron aerosol. PBA particles like plant fragments, pollen, spores, fungi, viruses etc. contain chemical compounds as proteins, sugars, amino acids, chlorophyll, and cellular material as cellulose. For this reason we have performed mass spectrometric laboratory measurements (Aerodyne C-ToF and W-ToF AMS, single particle laser ablation instrument SPLAT) on pure submicron aerosol particles containing typical PBA compounds in order to identify typical mass spectral patterns of these compounds and to explain the observed fragmentation patterns on the basis of molecular structures. These laboratory data were compared to submicron particle mass spectra obtained during AMAZE-08 (Amazonian Aerosol CharacteriZation Experiment, Brazil, February/March 2008). The results indicate that characteristic m/z ratios for carbohydrates (e.g., glucose, saccharose, levoglucosan, mannitol) can be identified, for example m/z = 60(C2H4O2+) or m/z = 61(C2H5O2+). Certain characteristic peaks for amino acids were also identified in the laboratory experiments. In the field data from AMAZE-08, these characteristic peaks for carbohydrates and amino acids were found, and their contribution to the total organic mass was estimated to about 5%. Fragment ions from peptides and small proteins were also identified in laboratory experiments. Larger proteins, however, seem to become oxidized to CO2+ to a large extend in the vaporizing process of the AMS. Thus, detection of proteins in atmospheric aerosol particles with the AMS appears to be difficult.

  10. Predicting bed form roughness: the influence of lee side angle

    Lefebvre, Alice; Winter, Christian


    Flow transverse bedforms (ripples and dunes) are ubiquitous in rivers and coastal seas. Local hydrodynamics and transport conditions depend on the size and geometry of these bedforms, as they constitute roughness elements at the bed. Bedform influence on flow energy must be considered for the understanding of flow dynamics, and in the development and application of numerical models. Common estimations or predictors of form roughness (friction factors) are based mostly on data of steep bedforms (with angle-of-repose lee slopes), and described by highly simplified bedform dimensions (heights and lengths). However, natural bedforms often are not steep, and differ in form and hydraulic effect relative to idealised bedforms. Based on systematic numerical model experiments, this study shows how the hydraulic effect of bedforms depends on the flow structure behind bedforms, which is determined by the bedform lee side angle, aspect ratio and relative height. Simulations reveal that flow separation behind bedform crests and, thus, a hydraulic effect is induced at lee side angles steeper than 11 to 18° depending on relative height, and that a fully developed flow separation zone exists only over bedforms with a lee side angle steeper than 24°. Furthermore, the hydraulic effect of bedforms with varying lee side angle is evaluated and a reduction function to common friction factors is proposed. A function is also developed for the Nikuradse roughness (k s), and a new equation is proposed which directly relates k s to bedform relative height, aspect ratio and lee side angle.

  11. Rough sets: the classical and extended views

    ZIARKO Wojciech


    The article is a comprehensive review of two major approaches to rough set theory: the classic rough setmodel introduced by Pawlak and the probabilistic approaches. The classic model is presented as a staging ground to the discussion of two varieties of the probabilistic approach, i.e. of the variable precision and Bayesian rough set models. Both of these models extend the classic model to deal with stochastic interactions while preserving the basicideas of the original rough set theory, such as set approximations, data dependencies, reducts etc. The probabilistic models are able to handle weaker data interactions than the classic model, thus extending the applicability of the rough set paradigm. The extended models are presented in considerable detail with some illustrative examples.


    Ahmed T. Shawky


    Full Text Available Decision models which adopt rough set theory have been used effectively in many real world applications.However, rough decision models suffer the high computational complexity when dealing with datasets ofhuge size. In this research we propose a new rough decision model that allows making decisions based onmodularity mechanism. According to the proposed approach, large-size datasets can be divided intoarbitrary moderate-size datasets, then a group of rough decision models can be built as separate decisionmodules. The overall model decision is computed as the consensus decision of all decision modulesthrough some aggregation technique. This approach provides a flexible and a quick way for extractingdecision rules of large size information tables using rough decision models.

  13. Modular Approach with Rough Decision Models

    Ahmed T. Shawky


    Full Text Available Decision models which adopt rough set theory have been used effectively in many real world applications.However, rough decision models suffer the high computational complexity when dealing with datasets ofhuge size. In this research we propose a new rough decision model that allows making decisions based onmodularity mechanism. According to the proposed approach, large-size datasets can be divided intoarbitrary moderate-size datasets, then a group of rough decision models can be built as separate decisionmodules. The overall model decision is computed as the consensus decision of all decision modulesthrough some aggregation technique. This approach provides a flexible and a quick way for extractingdecision rules of large size information tables using rough decision models.

  14. Modeling surface roughness scattering in metallic nanowires

    Moors, Kristof, E-mail: [KU Leuven, Institute for Theoretical Physics, Celestijnenlaan 200D, B-3001 Leuven (Belgium); IMEC, Kapeldreef 75, B-3001 Leuven (Belgium); Sorée, Bart [IMEC, Kapeldreef 75, B-3001 Leuven (Belgium); Physics Department, University of Antwerp, Groenenborgerlaan 171, B-2020 Antwerpen (Belgium); KU Leuven, Electrical Engineering (ESAT) Department, Kasteelpark Arenberg 10, B-3001 Leuven (Belgium); Magnus, Wim [IMEC, Kapeldreef 75, B-3001 Leuven (Belgium); Physics Department, University of Antwerp, Groenenborgerlaan 171, B-2020 Antwerpen (Belgium)


    Ando's model provides a rigorous quantum-mechanical framework for electron-surface roughness scattering, based on the detailed roughness structure. We apply this method to metallic nanowires and improve the model introducing surface roughness distribution functions on a finite domain with analytical expressions for the average surface roughness matrix elements. This approach is valid for any roughness size and extends beyond the commonly used Prange-Nee approximation. The resistivity scaling is obtained from the self-consistent relaxation time solution of the Boltzmann transport equation and is compared to Prange-Nee's approach and other known methods. The results show that a substantial drop in resistivity can be obtained for certain diameters by achieving a large momentum gap between Fermi level states with positive and negative momentum in the transport direction.

  15. Electrochemically grown rough-textured nanowires

    Tyagi, Pawan; Postetter, David; Saragnese, Daniel [Johns Hopkins University, Department of Chemical and Biomolecular Engineering (United States); Papadakis, Stergios J. [Johns Hopkins University, Applied Physics Laboratory (United States); Gracias, David H., E-mail: dgracias@jhu.ed [Johns Hopkins University, Department of Chemical and Biomolecular Engineering (United States)


    Nanowires with a rough surface texture show unusual electronic, optical, and chemical properties; however, there are only a few existing methods for producing these nanowires. Here, we describe two methods for growing both free standing and lithographically patterned gold (Au) nanowires with a rough surface texture. The first strategy is based on the deposition of nanowires from a silver (Ag)-Au plating solution mixture that precipitates an Ag-Au cyanide complex during electrodeposition at low current densities. This complex disperses in the plating solution, thereby altering the nanowire growth to yield a rough surface texture. These nanowires are mass produced in alumina membranes. The second strategy produces long and rough Au nanowires on lithographically patternable nickel edge templates with corrugations formed by partial etching. These rough nanowires can be easily arrayed and integrated with microscale devices.

  16. Suppression of intrinsic roughness in encapsulated graphene

    Thomsen, Joachim Dahl; Gunst, Tue; Gregersen, Søren Schou


    Roughness in graphene is known to contribute to scattering effects which lower carrier mobility. Encapsulating graphene in hexagonal boron nitride (hBN) leads to a significant reduction in roughness and has become the de facto standard method for producing high-quality graphene devices. We have...... fabricated graphene samples encapsulated by hBN that are suspended over apertures in a substrate and used noncontact electron diffraction measurements in a transmission electron microscope to measure the roughness of encapsulated graphene inside such structures. We furthermore compare the roughness...... of these samples to suspended bare graphene and suspended graphene on hBN. The suspended heterostructures display a root mean square (rms) roughness down to 12 pm, considerably less than that previously reported for both suspended graphene and graphene on any substrate and identical within experimental error...

  17. Numerical Investigation of Evaporation Induced Self-Assembly of Sub-Micron Particles Suspended in Water

    Tayeb, Raihan; Zhang, Yuwen


    Self-assembly of sub-micron particles suspended in a water film is investigated numerically. The liquid medium is allowed to evaporate leaving only the sub-micron particles. A coupled CFD-DEM approach is used for the simulation of fluid-particle interaction. Momentum exchange and heat transfer between particles and fluid and among particles are considered. A history dependent contact model is used to compute the contact force among sub-micron particles. Simulation is done using the open source software package CFDEM which basically comprises of two other open source packages OpenFOAM and LIGGGHTS. OpenFOAM is a widely used solver for CFD related problems. LIGGGHTS, a modification of LAMMPS, is used for DEM simulation of granular materials. The final packing structure of the sub-micron particles is discussed in terms of distribution of coordination number and radial distribution function (RDF). The final packing structure shows that particles form clusters and exhibit a definite pattern as water evaporates awa...

  18. The efficiency and stability of bubble formation by acoustic vaporization of submicron perfluorocarbon droplets

    Reznik, Nikita; Shpak, Oleksandr; Gelderblom, Erik C.; Williams, Ross; Jong, de Nico; Versluis, Michel; Burns, Peter N.


    Submicron droplets of liquid perfluorocarbon converted into microbubbles with applied ultrasound have been studied, for a number of years, as potential next generation extravascular ultrasound contrast agents. In this work, we conduct an initial ultra-high-speed optical imaging study to examine the

  19. Submicron hollow spot generation by solid immersion lens and structured illumination

    Kim, M.S.; Assafrao, A.C.; Scharf, T.; Wachters, A.J.H.; Pereira, S.F.; Urbach, H.P.; Brun, M.; Olivier, S.; Nicoletti, S.; Herzig, H.P.


    We report on the experimental and numerical demonstration of immersed submicron-size hollow focused spots, generated by structuring the polarization state of an incident light beam impinging on a micro-size solid immersion lens (μ-SIL) made of SiO2. Such structured focal spots are characterized by a

  20. Electric and thermal conduction mechanisms of submicron-structured Ni-ZrO2 composites

    范秋林; 胡行方; 郭景坤


    The experimental results indicate that the Ni-ZrO2 composites synthesized with urn-sized Ni powder and nm-sized ZrO2 powder possess submicron structure. Based on the fractal theory, the relationship between the electric and thermal conductance and the chemical composition of the composites has been studied. The results show that with the increase of the nickel content, the electric and thermal conductance of the composites varies. It is proposed that in the submicron structured composites, electrons and phonons have different transport mechanisms. The electric transport in the submicron-structured composites can be attributed to the medium punch-through effect and quantum tunnel punch-through effect of electrons and the low thermal conductance is due to the phonic scattering by the submicron-sized pores, grains and grain boundaries. The reason can also be used to explain why the thermal percolation threshold value lags behind the electric percolation value. The phenomenon has been observed.

  1. Submicron organic nanofiber devices with different anode-cathode materials: A simple approach

    Henrichsen, Henrik Hartmann; Sturm, Heinz; Bøggild, Peter


    The authors present a simple general method for simultaneously producing tens of submicron electrode gaps with different cathode and anode materials on top of nanofibers, nanowires, and nanotubes, with an optional gap size variation. Using this method, an ensemble of para-hexaphenylene (p6P...

  2. Analysis of submicron-sized niflumic acid crystals prepared by electrospray crystallization

    Ambrus, R.; Radacsi, N.; Szunyogh, T.; Heijden, A.E.D.M. van der; Horst, J.H. ter; Szabó-Révész, P.


    Interest in submicron-sized drug particles has emerged from both laboratory and industrial perspectives in the last decade. Production of crystals in the nano size scale offers a novel way to particles for drug formulation solving formulation problems of drugs with low solubility in class II of the

  3. Submicron hollow spot generation by solid immersion lens and structured illumination

    Kim, M.S.; Assafrao, A.C.; Scharf, T.; Wachters, A.J.H.; Pereira, S.F.; Urbach, H.P.; Brun, M.; Olivier, S.; Nicoletti, S.; Herzig, H.P.


    We report on the experimental and numerical demonstration of immersed submicron-size hollow focused spots, generated by structuring the polarization state of an incident light beam impinging on a micro-size solid immersion lens (μ-SIL) made of SiO2. Such structured focal spots are characterized by a

  4. Power management of digital circuits in deep sub-micron CMOS technologies

    Henzler, Stephan


    In the deep sub-micron regime, the power consumption has become one of the most important issues for competitive design of digital circuits. This book mainly deals with circuit design but also addresses the interface between circuit and system level design on the one side and between circuit and physical design on the other side.

  5. Selective epitaxial growth of sub-micron structures of YBaCuO by substrate modification

    Blank, Dave H.A.; Damen, Cas A.J.; Kropman, Boike L.; Rogalla, Horst


    Sub-micron structures of high-Tc thin films have been realized with Selective Epitaxial Growth (SEG). Two different techniques to achieve SEG have been studied. First, narrow trenches down to 100 nm are etched into the substrate with a four-layer E-beam lithography technique. Second, amorphous metal

  6. Partitioning and characterization of high speed adder structures in deep-submicron technologies

    Estrada, Adrián; Sassaw, Gashaw; Jiménez, Carlos J.; Valencia, Manuel


    The availability of higher performance (in area, time and power consumption) and greater precision binary adders is a constant requirement in digital systems. Consequently, the design and characterization of adders and, most of all, their adaptation to the requisites of present-day deep-submicron technologies, are today still issues of concern. The binary adder structures in deep-submicron technologies must be revised to achieve the best balance between the number of bits in the adder and its delay, area and power consumption. It is therefore very important to make an effort to carefully optimize adder structures, thus obtaining improvements in digital systems. This communication presents the optimization of adder structures for implementations in deep-submicron technologies through their partitioning into blocks. This partitioning consists of dividing the number of input bits to the adder into several subsets of bits that will constitute the inputs to several adder structures of the same or of different types. The structures used to accomplish this study range from the more traditional types, such as the carry look ahead adder, the ripple carry adder or the carry select adder, to more innovative kinds, like the parallel prefix adders of the type proposed by Brent-Kung, Han-Carlson, Kogge-Stone or Ladner-Fischer. The analyses carried out allow the characterization of structures implemented in deep-submicron technologies for area, delay and power consumption parameters.

  7. High-Performance Deep SubMicron CMOS Technologies with Polycrystalline-SiGe Gates

    Ponomarev, Youri V.; Stolk, Peter A.; Salm, Cora; Schmitz, Jurriaan; Woerlee, P.H.


    The use of polycrystalline SiGe as the gate material for deep submicron CMOS has been investigated. A complete compatibility to standard CMOS processing is demonstrated when polycrystalline Si is substituted with SiGe (for Ge fractions below 0.5) to form the gate electrode of the transistors. Perfor

  8. A facile route for the synthesis of sub-micron sized hollow and multiporous organosilica spheres

    Segers,M.; Arfsten, N.; Buskens, P.; Möller, M.


    We present a facile route for the synthesis of sub-micron sized hollow and multiporous organosilica spheres, which is based on an oil-in-water emulsion and merely uses one organosilica precursor-phenyl trimethoxysilane-that serves as monomer, precursor for a surface active species and oil phase. Thi

  9. Bloch-wave engineered submicron-diameter quantum-dot micropillars for cavity QED experiments

    Gregersen, Niels; Lermer, Matthias; Reitzenstein, Stephan;


    The semiconductor micropillar is attractive for cavity QED experiments. For strong coupling, the figure of merit is proportional to Q/√V, and a design combining a high Q and a low mode volume V is thus desired. However, for the standard submicron diameter design, poor mode matching between...

  10. Reversal studies on sub-micron Co-Cr thin films by AHE analysis

    Haan, de S.; Lodder, J.C.


    In this study three Co---Cr thin films, prepared under different deposition conditions, are investigated. They have values for the coercivity (Hc) of 11, 90 and 170 kA/m, respectively. The anomalous Hall effect (AHE) has been used to record the hysteresis curves of specially prepared sub-micron Hall

  11. On-chip detection of ferromagnetic resonance of a single submicron Permalloy strip

    Costache, M. V.; Sladkov, M.; van der Wal, C. H.; van Wees, B. J.


    The authors measured ferromagnetic resonance of a single submicron ferromagnetic strip, embedded in an on-chip microwave transmission line device. The method used is based on detection of the oscillating magnetic flux due to the magnetization dynamics, with an inductive pickup loop. The dependence o

  12. Suppression and origin of soft ESD failures in a submicron CMOS process

    Kuper, Fred; Luchies, Jan Marc; Bruines, Joop


    Soft failures occurring after low-level ESD stress of thick and thin oxide NMOSTs in a submicron CMOS process have been studied. Simple drain engineering appears to have a dramatic improving effect. Simulation is used to study the cause for the soft failures.

  13. Large voltage modulation in superconducting quantum interference devices with submicron-scale step-edge junctions

    Lam, Simon K. H.


    A promising direction to improve the sensitivity of a SQUID is to increase its junction's normal resistance value, Rn, as the SQUID modulation voltage scales linearly with Rn. As a first step to develop highly sensitive single layer SQUID, submicron scale YBCO grain boundary step edge junctions and SQUIDs with large Rn were fabricated and studied. The step-edge junctions were reduced to submicron scale to increase their Rn values using focus ion beam, FIB and the measurement of transport properties were performed from 4.3 to 77 K. The FIB induced deposition layer proves to be effective to minimize the Ga ion contamination during the FIB milling process. The critical current-normal resistance value of submicron junction at 4.3 K was found to be 1-3 mV, comparable to the value of the same type of junction in micron scale. The submicron junction Rn value is in the range of 35-100 Ω, resulting a large SQUID modulation voltage in a wide temperature range. This performance promotes further investigation of cryogen-free, high field sensitivity SQUID applications at medium low temperature, e.g. at 40-60 K.

  14. High-Performance Deep SubMicron CMOS Technologies with Polycrystalline-SiGe Gates

    Ponomarev, Youri V.; Stolk, Peter A.; Salm, Cora; Schmitz, Jurriaan; Woerlee, P.H.


    The use of polycrystalline SiGe as the gate material for deep submicron CMOS has been investigated. A complete compatibility to standard CMOS processing is demonstrated when polycrystalline Si is substituted with SiGe (for Ge fractions below 0.5) to form the gate electrode of the transistors.

  15. Effects of soil surface roughness on interrill erosion processes and sediment particle size distribution

    Ding, Wenfeng; Huang, Chihua


    Soil surface roughness significantly impacts runoff and erosion under rainfall. Few previous studies on runoff generation focused on the effects of soil surface roughness on the sediment particle size distribution (PSD), which greatly affects interrill erosion and sedimentation processes. To address this issue, a rainfall-simulation experiment was conducted with treatments that included two different initial soil surface roughnesses and two rainfall intensities. Soil surface roughness was determined by using photogrammetric method. For each simulated event, runoff and sediment samples were collected at different experimental times. The effective (undispersed) PSD of each sediment sample and the ultimate (after dispersion) PSD were used to investigate the detachment and transport mechanisms involved in sediment movement. The results show that soil surface roughness significantly delayed runoff initiation, but had no significant effect on the steady runoff rate. However, a significant difference in the soil loss rate was observed between the smooth and rough soil surfaces. Sediments from smooth soil surfaces were more depleted in clay-size particles, but more enriched in sand-size particles than those from rough soil surfaces, suggesting that erosion was less selective on smooth than on rough soil surfaces. The ratio of different sizes of transported sediment to the soil matrix indicates that most of the clay was eroded in the form of aggregates, silt-size particles were transported mainly as primary particles, and sand-size particles were predominantly aggregates of finer particles. Soil surface roughness has a crucial effect on the sediment size distribution and erosion processes. Significant differences of the enrichment ratios for the effective PSD and the ultimate PSD were observed under the two soil surface roughness treatments. These findings demonstrate that we should consider each particle size separately rather than use only the total sediment discharge in

  16. Development of enteric submicron particle formulation of papain for oral delivery

    Sharma M


    Full Text Available Manu Sharma1, Vinay Sharma2, Amulya K Panda3, Dipak K Majumdar41Department of Pharmacy, Banasthali Vidhyapith, Banasthali, India; 2Department of Bioscience and Biotechnology, Banasthali Vidhyapith, Banasthali, India; 3National Institute of Immunology, Aruna Asaf Ali Marg, New Delhi, India; 4Department of Pharmaceutics, Delhi Institute of Pharmaceutical Sciences and Research, University of Delhi, New Delhi, IndiaBackground: Particulate systems have received increasing attention for oral delivery of biomolecules. The objective of the present study was to prepare submicron particulate formulations of papain for pH-dependent site-specific release using pH-sensitive polymers.Methods: Enteric submicron particle formulations of papain were prepared by w/o/w emulsion solvent evaporation using hydroxypropyl methylcellulose phthalate (HPMCP, Eudragit L100, and Eudragit S100, to avoid gastric inactivation of papain.Results: Smaller internal and external aqueous phase volumes provided maximum encapsulation efficiency (75.58%–82.35%, the smallest particle size (665.6–692.4 nm, and 25%–30% loss of enzyme activity. Release studies in 0.1 N HCl confirmed the gastroresistance of the formulations. The anionic submicron particles aggregated in 0.1 N HCl (ie, gastric pH 1.2 due to protonation of carboxylic groups in the enteric polymer. Aggregates < 500 µm size would not impede gastric emptying. However, at pH > 5.0 (duodenal pH, the submicron particles showed deaggregation due to restoration of surface charge. HPMCP submicron particles facilitated almost complete release of papain within 30 minutes at pH 6.0, while Eudragit L100 and Eudragit S100 particles released 88.82% and 53.00% of papain at pH 6.8 and pH 7.4, respectively, according to the Korsmeyer–Peppas equation. Sodium dodecyl sulfate polyacrylamide gel electrophoresis and fluorescence spectroscopy confirmed that the structural integrity of the enzyme was maintained during encapsulation. Fourier

  17. Flow formed by spanwise gaps between roughness elements

    Logan, E.; Lin, S. H.; Islam, O.


    Measurements of the three mean velocity components and the three Reynolds shear stresses were made in the region downstream of gaps between wall-mounted roughness elements of square cross section and high aspect ratio in a thick turbulent boundary layer. The effect of small and large gaps was studied in a wind tunnel at a Reynolds number of 3600, based on obstacle height and free-stream velocity. The small gap produces retardation of the gap flow as with a two-dimensional roughness element, but a definite interaction between gap and wake flows is observed. The interaction is more intense for the large gap than for the small. Both gaps generate a secondary crossflow which moves fluid away from the centerline in the wall region and toward the centerline in the outer (y greater than 1.5H) region.

  18. Function S-rough sets and law identification

    SHI KaiQuan; YAO BingXue


    By introducing element equivalence class that proposes dynamic characteristic into Pawlak Z rough sets theory, the first author of this paper improved Pawlak Z rough sets and put forward S-rough sets (singular rough sets). S-rough sets are defined by element equivalence class that proposes dynamic characteristic. S-rough sets have dynamic characteristic. By introducing the function equivalence class (law equivalence class) that proposes dynamic characteristic into S-rough sets, the first author improved S-rough sets and put forward function S-rough sets (function singular rough sets). Function S-rough sets have dynamic characteristic and law characteristic, and a function is a law. By using function S-rough sets, this paper presents law identification, law identification theorem, and law identification criterion and applications. Function S-rough sets are a new research direction of rough sets theory, and it is also a new tool to the research of system law identifica-tion.

  19. Effect of Grinding Process Parameters on Surface Area Roughness of Glass fibre Reinforced Composite Laminate under Dry and Coolant Environment

    P. Chockalingam


    Full Text Available This paper presents a comparative study on dry and wet grinding of chopped strand mat glass fibre reinforced polymer laminates using an alumina wheel. Investigations were performed to study the impact of the grinding parameters, namely feed, speed, and depth of cut on grinding force ratio and surface area roughness. Effective grinding parameters were sought in this study to maximize grinding force ratio and minimize surface area roughness. Test results show that coolant helped to decrease surface area roughness, but inevitably reduced the grinding force ratio in some cases. These findings lead to economic machining solution for optimum grinding conditions in grinding composite laminates.

  20. Mathematical model for strip surface roughness of stainless steel in cold rolling process

    Chen, Jinshan; Li, Changsheng; Zhu, Tao; Han, Wenlong; Cao, Yong


    Surface roughness control is one of the most important subjects during producing stainless steel strips. In this paper, under the conditions of introducing to the concepts of transferring ratio and genetic factor and through the further theoretical analysis, a set of theoretical models about strip surface roughness were put forward in stainless steel cold tandem rolling. Meanwhile, the lubrication experiment in cold rolling process of SUS430 stainless steel strip was carried out in order to comprehensively study surface roughness. The effect of main factors on transferring ratio and genetic factor was analyzed quantitatively, such as reduction, initial thickness, deformation resistance, emulsion technological parameters and so on. Attenuation function equations used for describing roll surface roughness were set up, and also strip surface roughness at the entry of last mill was solved approximately. Ultimately, mathematical model on strip surface roughness for cold tandem rolling of stainless steel was built, and then it was used into the practical production. A great number of statistical results show that experimental data is in excellent agreement with the given regression equations, and exactly, the relative deviation on roughness between calculated and measured is less than 6.34%.

  1. On Characterization of Rough Type-2 Fuzzy Sets

    Tao Zhao; Zhenbo Wei


    Rough sets theory and fuzzy sets theory are important mathematical tools to deal with uncertainties. Rough fuzzy sets and fuzzy rough sets as generalizations of rough sets have been introduced. Type-2 fuzzy set provides additional degree of freedom, which makes it possible to directly handle high uncertainties. In this paper, the rough type-2 fuzzy set model is proposed by combining the rough set theory with the type-2 fuzzy set theory. The rough type-2 fuzzy approximation operators induced f...

  2. Surface roughness characterization of cast components using 3D optical methods

    Nwaogu, Ugochukwu Chibuzoh; Tiedje, Niels Skat; Hansen, Hans Nørgaard

    scanning probe image processor (SPIP) software and the results of the surface roughness parameters obtained were subjected to statistical analyses. The bearing area ratio was introduced and applied to the surface roughness analysis. From the results, the surface quality of the standard comparators...... made in green sand moulds and the surface roughness parameter (Sa) values were compared with those of the standards. Sa parameter suffices for the evaluation of casting surface texture. The S series comparators showed a better description of the surface of castings after shot blasting than the A series...

  3. Understanding EUV mask blank surface roughness induced LWR and associated roughness requirement

    Yan, Pei-Yang [Intel Corp., Santa Clara, CA (United States); Zhang, Guojing [Intel Corp., Santa Clara, CA (United States); Gullickson, Eric M. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Goldberg, Kenneth A. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Benk, Markus P. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)


    Extreme ultraviolet lithography (EUVL) mask multi-layer (ML) blank surface roughness specification historically comes from blank defect inspection tool requirement. Later, new concerns on ML surface roughness induced wafer pattern line width roughness (LWR) arise. In this paper, we have studied wafer level pattern LWR as a function of EUVL mask surface roughness via High-NA Actinic Reticle Review Tool. We found that the blank surface roughness induced LWR at current blank roughness level is in the order of 0.5nm 3σ for NA=0.42 at the best focus. At defocus of ±40nm, the corresponding LWR will be 0.2nm higher. Further reducing EUVL mask blank surface roughness will increase the blank cost with limited benefit in improving the pattern LWR, provided that the intrinsic resist LWR is in the order of 1nm and above.

  4. Lungs deposition and pharmacokinetic study of submicron budesonide particles in Wistar rats intended for immediate effect in asthma.

    Rauf, Abdul; Bhatnagar, Aseem; Sisodia, S S; Khar, Roop K; Ahmad, Farhan J


    The purpose of the present investigation was to study the aerosolization, lungs deposition and pharmacokinetic study of inhalable submicron particles of budesonide in male Wistar rats. Submicron particles were prepared by antisolvent nanoprecipitation method and freeze-dried to obtain free flowing powder. The freeze-drying process yielded dry powder with desirable aerodynamic properties for inhalation therapy. An in-house model inhaler was designed to deliver medicine to lungs, optimized at dose level of 10 mg for 30 sec of fluidization. The in vitro aerosolization study demonstrates that submicron particles dissolve faster with improved aerosolization effect as compared to micronized budesonide. Both submicron and micron particles were compared for in vivo lungs deposition. The results showed that relatively high quantity of submicron particles reaches deep into the lungs as compared to micron particles. Most pronounced effect observed with submicron particles from pharmacokinetic parameters was the enhancement in peak plasma concentration (Cmax) by 28.85 %, and increase in area under concentration curve (AUC0-8h) by 30.33 % compared to micron sized particles. The results suggested that developed submicronized formulation of budesonide can be used for pulmonary drug delivery for high deposition to deep lungs tissues.

  5. Synthesis and characterization of submicron-sized mesoporous aluminosilicate spheres

    Gautam Gundiah; M Eswaramoorthy; S Neeraj; Srinivasan Natarajan; C N R Rao


    Me soporous a luminosilicate spheres of 0 3-0 4 m diameter, with different Si/Al ratios, have been prepared by surfactant templating. Surface area of these materials is in the 510-970 m2g-1 range and pore diameter in the 15-20 Å range.

  6. Rough Fuzzy Relation on Two Universal Sets

    Xuan Thao Nguyen


    Full Text Available Fuzzy set theory was introduced by L.A. Zadeh in 1965. Immediately, it has many applications in practice and in building databases, one of which is the construction of a fuzzy relational database based on similar relationship. The study of cases of fuzzy relations in different environments will help us understand its applications. In this paper, the rough fuzzy relation on Cartesian product of two universe sets is defined, and then the algebraic properties of them, such as the max, min, and composition of two rough fuzzy relations are examined. Finally, reflexive, α-reflexive, symmetric and transitive rough fuzzy relations on two universe sets are also defined.

  7. Rough Sets, Their Extensions and Applications

    Qiang Shen; Richard Jensen


    Rough set theory provides a useful mathematical foundation for developing automated computational systems that can help understand and make use of imperfect knowledge. Despite its recency, the theory and its extensions have been widely applied to many problems, including decision analysis, data mining, intelligent control and pattern recognition. This paper presents an outline of the basic concepts of rough sets and their major extensions, covering variable precision, tolerance and fuzzy rough sets. It also shows the diversity of successful applications these theories have entailed, ranging from financial and business, through biological and medicine, to physical, art, and meteorological.

  8. Surface Roughness and Porosity of Hydrated Cement Pastes

    T. Ficker


    Full Text Available . Seventy-eight graphs were plotted to describe and analyze the dependences of the height and roughness irregularities on the water-to-cement ratio and on the porosity of the cement hydrates. The results showed unambiguously that the water-to-cement ratio or equivalently the porosity of the specimens has a decisive influence on the irregularities of the fracture surfaces of this material. The experimental results indicated the possibility that the porosity or the value of the water-to-cement ratio might be inferred from the height irregularities of the fracture surfaces. It was hypothesized that there may be a similarly strong correlation between porosity and surface irregularity, on the one hand, and some other highly porous solids, on the other, and thus the same possibility to infer porosity from the surfaces of their fracture remnants.

  9. Use of roughness maps in visualisation of surfaces

    Seitavuopio, Paulus; Rantanen, Jukka; Yliruusi, Jouko


    In this study we will present a new method to describe surface roughness. This method builds a roughness map of the studied area. The roughness map can give information of localised roughness. The test surfaces used in the evaluation of the method were tablets, which were made of lactose monohydr...... of the heterogeneity of surface roughness of various materials....

  10. Number size distributions and seasonality of submicron particles in Europe 2008–2009

    A. Asmi


    Full Text Available Two years of harmonized aerosol number size distribution data from 24 European field monitoring sites have been analysed. The results give a comprehensive overview of the European near surface aerosol particle number concentrations and number size distributions between 30 and 500 nm of dry particle diameter. Spatial and temporal distribution of aerosols in the particle sizes most important for climate applications are presented. We also analyse the annual, weekly and diurnal cycles of the aerosol number concentrations, provide log-normal fitting parameters for median number size distributions, and give guidance notes for data users. Emphasis is placed on the usability of results within the aerosol modelling community.

    We also show that the aerosol number concentrations of Aitken and accumulation mode particles (with 100 nm dry diameter as a cut-off between modes are related, although there is significant variation in the ratios of the modal number concentrations. Different aerosol and station types are distinguished from this data and this methodology has potential for further categorization of stations aerosol number size distribution types.

    The European submicron aerosol was divided into characteristic types: Central European aerosol, characterized by single mode median size distributions, unimodal number concentration histograms and low variability in CCN-sized aerosol number concentrations; Nordic aerosol with low number concentrations, although showing pronounced seasonal variation of especially Aitken mode particles; Mountain sites (altitude over 1000 m a.s.l. with a strong seasonal cycle in aerosol number concentrations, high variability, and very low median number concentrations. Southern and Western European regions had fewer stations, which decreases the regional coverage of these results. Aerosol number concentrations over the Britain and Ireland had very high variance and there are indications of mixed air masses

  11. Chemical and physical characteristics of long-range transport submicron particles at the central Tibet Plateau

    Xu, J.; Zhang, Q.; Shi, J.; Ge, X.; Xie, C.; Wang, J.


    Tibetan Plateau, the biggest and highest plateau on the Earth, is an ideal location for studying long range transport of air pollution due to the minimum of local emission. Recent studies in this region have revealed a significant influx of air pollution from south Asia during pre-monsoon period because of the favorable atmospheric circulation and less precipitation. In order to characterize the chemical composition of aerosol particles in this pristine area and elucidate the sources and optical properties of transported aerosol pollutants, we conducted an intensive field study during June 2015 at a high elevation station (4730 m a.s.l) on the central Tibetan Plateau by deploying a suite of advanced instruments including an Aerodyne high-resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS), a nephelometer, and a multi-angle absorption photometer (MAAP). The average mass concentration of submicron particular matter (PM1) for the whole campaign period was 1.85 µg m-3, with organics accounting for 64% of the mass, followed by sulfate (16%), black carbon (9%), ammonium (8%), and nitrate (3%). The mass concentrations and chemical properties of PM1 were significantly different between pre-monsoon and monsoon periods. Elevated aerosol pollution episodes were observed during pre-monsoon period, while aerosol concentrations were persistently low during monsoon period. Aerosol composition was generally similar during the whole campaign period. However, organic aerosol was more oxidized during premonsoon period with an average atomic oxygen-to-carbon (O/C) ratio of = 0.7 compared to O/C = 0.52 during monsoon period. HYSPLIT trajectory calculations revealed that most of the arriving air masses traveled long distances (>1,000 km) and went through the northwest of India during premonsoon period. Positive matrix factorization of the HR-ToF-AMS spectra of organic aerosol identified two oxygenated organic aerosol (OOA) factors - a less oxidized OOA (LO-OOA) and a more

  12. Long-term Chemical Characterization of Submicron Aerosol Particles in the Amazon Forest - ATTO Station

    Carbone, S.; Brito, J.; Rizzo, L. V.; Holanda, B. A.; Cirino, G. G.; Saturno, J.; Krüger, M. L.; Pöhlker, C.; Ng, N. L.; Xu, L.; Andreae, M. O.; Artaxo, P.


    The study of the chemical composition of aerosol particles in the Amazon forest represents a step forward to understand the strong coupling between the atmosphere and the forest. For this reason submicron aerosol particles were investigated in the Amazon forest, where biogenic and anthropogenic aerosol particles coexist at the different seasons (wet/dry). The measurements were performed at the ATTO station, which is located about 150 km northeast of Manaus. At ATTO station the Aerosol chemical speciation monitor (ACSM, Aerodyne) and the Multiangle absorption photometer (MAAP, Thermo 5012) have been operated continuously from March 2014 to July 2015. In this study, long-term measurements (near-real-time, ~30 minutes) of PM1 chemical composition were investigated for the first time in this environment.The wet season presented lower concentrations than the dry season (~5 times). In terms of chemical composition, both seasons were dominated by organics (75 and 63%) followed by sulfate (11 and 13%). Nitrate presented different ratio values between the mass-to-charges 30 to 46 (main nitrate fragments) suggesting the presence of nitrate as inorganic and organic nitrate during both seasons. The results indicated that about 75% of the nitrate signal was from organic nitrate during the dry season. In addition, several episodes with elevated amount of chloride, likely in the form of sea-salt from the Atlantic Ocean, were observed during the wet season. During those episodes, chloride comprised up to 7% of the PM1. During the dry season, chloride was also observed; however, with different volatility, which suggested that Chloride was present in different form and source. Moreover, the constant presence of sulfate and BC during the wet season might be related to biomass burning emissions from Africa. BC concentration was 2.5 times higher during the dry season. Further characterization of the organic fraction was accomplished with the positive matrix factorization (PMF), which

  13. Umatilla - Umatilla Slough Rough Fish Eradication

    US Fish and Wildlife Service, Department of the Interior — The purpose of the proposed action is to enhance environmental conditions in the Whitcomb Island Slough by reducing the population of rough fish, including common...

  14. McNary - Rough Fish Control

    US Fish and Wildlife Service, Department of the Interior — The purpose of the action is to enhance environmental conditions in the McNary Slough by reducing the population of rough fish, including common carp (Cyprinus...

  15. Accurate Topological Measures for Rough Sets


    Data granulation is considered a good tool of decision making in various types of real life applications. The basic ideas of data granulation have appeared in many fields, such as interval analysis, quantization, rough set theory, Dempster-Shafer theory of belief functions, divide and conquer, cluster analysis, machine learning, databases, information retrieval, and many others. Some new topological tools for data granulation using rough set approximations are initiated. Moreover, some topolo...

  16. General Regularities of Wood Surface Roughness

    MAGOSS, Endre


    Full Text Available The surface roughness of wood products is depending on many factors related both towood properties and wood working operational parameters. Probably this is the reason why there areno generally valid correlation determining surface roughness parameters as a function of influencingfactors. In particular, the account of wood structure in the surface roughness interpretation proved tobe difficult.In the last years an important progress was made in recognizing the role of the anatomicalstructure of wood species in the attainable surface roughness. The introduction of a structure numbermade it possible to express and characterize the different wood species numerically.The aim of these studies was the separation of roughness components due to the anatomicalstructure and the woodworking operation. Using a special finishing technique, the roughnesscomponent due to woodworking operations was not significant and could be separated. The samespecimens were also subjected to different woodworking operations using cutting velocities between10 and 50 m/s. The processing of experimental data resulted in a chart showing the minimumroughness component due to different woodworking operations. Special experimental investigationwas conducted to clear the influence of edge dullness on the surface roughness, especially on itsAbbott-parameters. The measurements showed that the Rk-parameter is a good indicator to predictedge dullness.

  17. The apparent state of droplets on a rough surface

    CHEN XiaoLing; LU Tian


    The factors influencing the state and wetting transition of droplets on a rough surface are both complex and obscure. The change in wetting is directly reflected by changes under the contact condition of the droplets with the surface. The recent study about the wettability of the superhydrophobic surface under the condensing condition arouses the new understanding about the apparent state of droplets on a rough surface, in this work, to validate the existence of droplets in an intermediate state, a microscale pillar topological polydimethylsiloxane (PDMS) surface was manufactured and its wettability under various conditions was studied. According to the experimental data, it is proposed that the wetting state of a rough surface may be embodied using the contact area ratio of a solid/liquid/gas droplet with the projective plane. A general calculation model for the apparent contact angle of droplets is given and expressed diagrammatically. It is found that the measured apparent contact angles of droplets at dif-ferent states on the surface falls within the range predicted by our proposed equation.

  18. Data fusion for accurate microscopic rough surface metrology.

    Chen, Yuhang


    Data fusion for rough surface measurement and evaluation was analyzed on simulated datasets, one with higher density (HD) but lower accuracy and the other with lower density (LD) but higher accuracy. Experimental verifications were then performed on laser scanning microscopy (LSM) and atomic force microscopy (AFM) characterizations of surface areal roughness artifacts. The results demonstrated that the fusion based on Gaussian process models is effective and robust under different measurement biases and noise strengths. All the amplitude, height distribution, and spatial characteristics of the original sample structure can be precisely recovered, with better metrological performance than any individual measurements. As for the influencing factors, the HD noise has a relatively weaker effect as compared with the LD noise. Furthermore, to enable an accurate fusion, the ratio of LD sampling interval to surface autocorrelation length should be smaller than a critical threshold. In general, data fusion is capable of enhancing the nanometrology of rough surfaces by combining efficient LSM measurement and down-sampled fast AFM scan. The accuracy, resolution, spatial coverage and efficiency can all be significantly improved. It is thus expected to have potential applications in development of hybrid microscopy and in surface metrology.

  19. The apparent state of droplets on a rough surface


    The factors influencing the state and wetting transition of droplets on a rough surface are both complex and obscure. The change in wetting is directly reflected by changes under the contact condition of the droplets with the surface. The recent study about the wettability of the superhydrophobic surface under the condensing condition arouses the new understanding about the apparent state of droplets on a rough surface. In this work, to validate the existence of droplets in an intermediate state, a microscale pillar topological polydimethylsiloxane (PDMS) surface was manufactured and its wettability under various conditions was studied. According to the experimental data, it is proposed that the wetting state of a rough surface may be embodied using the contact area ratio of a solid/liquid/gas droplet with the projective plane. A general calculation model for the apparent contact angle of droplets is given and expressed diagrammatically. It is found that the measured apparent contact angles of droplets at dif- ferent states on the surface falls within the range predicted by our proposed equation.

  20. Incidence of rough and irregular atmospheric ice particles from Small Ice Detector 3 measurements

    Ulanowski, Z.; Kaye, P. H.; Hirst, E.; Greenaway, R. S.; Cotton, R. J.; Hesse, E.; Collier, C. T.


    The knowledge of properties of ice crystals such as size, shape, concavity and roughness is critical in the context of radiative properties of ice and mixed-phase clouds. Limitations of current cloud probes to measure these properties can be circumvented by acquiring two-dimensional light-scattering patterns instead of particle images. Such patterns were obtained in situ for the first time using the Small Ice Detector 3 (SID-3) probe during several flights in a variety of mid-latitude mixed-phase and cirrus clouds. The patterns are analysed using several measures of pattern texture, selected to reveal the magnitude of particle roughness or complexity. The retrieved roughness is compared to values obtained from a range of well-characterized test particles in the laboratory. It is found that typical in situ roughness corresponds to that found in the rougher subset of the test particles, and sometimes even extends beyond the most extreme values found in the laboratory. In this study we do not differentiate between small-scale, fine surface roughness and large-scale crystal complexity. Instead, we argue that both can have similar manifestations in terms of light-scattering properties and also similar causes. Overall, the in situ data are consistent, with ice particles with highly irregular or rough surfaces being dominant. Similar magnitudes of roughness were found in growth and sublimation zones of cirrus. The roughness was found to be negatively correlated with the halo ratio, but not with other thermodynamic or microphysical properties found in situ. Slightly higher roughness was observed in cirrus forming in clean oceanic air masses than in a continental, polluted one. Overall, the roughness and complexity are expected to lead to increased shortwave cloud reflectivity, in comparison with cirrus composed of more regular, smooth ice crystal shapes. These findings put into question suggestions that climate could be modified through aerosol seeding to reduce cirrus

  1. The sub-micron hole array in sapphire produced by inductively-coupled plasma reactive ion etching.

    Shiao, Ming-Hua; Chang, Chun-Ming; Huang, Su-Wei; Lee, Chao-Te; Wu, Tzung-Chen; Hsueh, Wen-Jeng; Ma, Kung-Jeng; Chiang, Donyau


    The sub-micron hole array in a sapphire substrate was fabricated by using nanosphere lithography (NSL) combined with inductively-coupled-plasma reactive ion etching (ICP-RIE) technique. Polystyrene nanospheres of about 600 nm diameter were self-assembled on c-plane sapphire substrates by the spin-coating method. The diameter of polystyrene nanosphere was modified by using oxygen plasma in ICP-RIE system. The size of nanosphere modified by oxygen plasma was varied from 550 to 450 nm with different etching times from 15 to 35 s. The chromium thin film of 100 nm thick was then deposited on the shrunk nanospheres on the substrate by electron-beam evaporation system. The honeycomb type chromium mask can be obtained on the sapphire substrate after the polystyrene nanospheres were removed. The substrate was further etched in two sets of chlorine/Argon and boron trichloride/Argon mixture gases at constant pressure of 50 mTorr in ICP-RIE processes. The 400 nm hole array in diameter can be successfully produced under suitable boron trichloride/Argon gas flow ratio.

  2. Microscopic Characterization of Individual Submicron Bubbles during the Layer-by-Layer Deposition: Towards Creating Smart Agents

    Riku Kato


    Full Text Available We investigated the individual properties of various polyion-coated bubbles with a mean diameter ranging from 300 to 500 nm. Dark field microscopy allows one to track the individual particles of the submicron bubbles (SBs encapsulated by the layer-by-layer (LbL deposition of cationic and anionic polyelectrolytes (PEs. Our focus is on the two-step charge reversals of PE-SB complexes: the first is a reversal from negatively charged bare SBs with no PEs added to positive SBs encapsulated by polycations (monolayer deposition, and the second is overcharging into negatively charged PE-SB complexes due to the subsequent addition of polyanions (double-layer deposition. The details of these phenomena have been clarified through the analysis of a number of trajectories of various PE-SB complexes that experience either Brownian motion or electrophoresis. The contrasted results obtained from the analysis were as follows: an amount in excess of the stoichiometric ratio of the cationic polymers was required for the first charge-reversal, whereas the stoichiometric addition of the polyanions lead to the electrical neutralization of the PE-SB complex particles. The recovery of the stoichiometry in the double-layer deposition paves the way for fabricating multi-layered SBs encapsulated solely with anionic and cationic PEs, which provides a simple protocol to create smart agents for either drug delivery or ultrasound contrast imaging.

  3. Submicron-Scale Heterogeneities in Nickel Sorption of Various Cell-Mineral Aggregates Formed by Fe(II)-Oxidizing Bacteria.

    Schmid, Gregor; Zeitvogel, Fabian; Hao, Likai; Ingino, Pablo; Adaktylou, Irini; Eickhoff, Merle; Obst, Martin


    Fe(II)-oxidizing bacteria form biogenic cell-mineral aggregates (CMAs) composed of microbial cells, extracellular organic compounds, and ferric iron minerals. CMAs are capable of immobilizing large quantities of heavy metals, such as nickel, via sorption processes. CMAs play an important role for the fate of heavy metals in the environment, particularly in systems characterized by elevated concentrations of dissolved metals, such as mine drainage or contaminated sediments. We applied scanning transmission (soft) X-ray microscopy (STXM) spectrotomography for detailed 3D chemical mapping of nickel sorbed to CMAs on the submicron scale. We analyzed different CMAs produced by phototrophic or nitrate-reducing microbial Fe(II) oxidation and, in addition, a twisted stalk structure obtained from an environmental biofilm. Nickel showed a heterogeneous distribution and was found to be preferentially sorbed to biogenically precipitated iron minerals such as Fe(III)-(oxyhydr)oxides and, to a minor extent, associated with organic compounds. Some distinct nickel accumulations were identified on the surfaces of CMAs. Additional information obtained from scatter plots and angular distance maps, showing variations in the nickel-iron and nickel-organic carbon ratios, also revealed a general correlation between nickel and iron. Although a high correlation between nickel and iron was observed in 2D maps, 3D maps revealed this to be partly due to projection artifacts. In summary, by combining different approaches for data analysis, we unambiguously showed the heterogeneous sorption behavior of nickel to CMAs.

  4. Real-time retrieval of submicron aerosol size distributions from multi-wavelength spectral extinction measurements

    CHEN; Jiawei; YANG; Mu; FENG; Haibao; NI; Qijun


    The real-time retrieval of submicron aerosol size distributions is of major interest for applications. Based on the Mie theory,the spectral extinction method offers a simple measurement principle and a convenient optical arrangement. In contrast to the relative simplicity of the experimental measurement the retrieval of the particles size distribution and particle concentration from the spectral extinction method is difficult. Mie scattering Equation is a Fredholm Integral Equation of the First Kind. This paper develops a hybrid iterative model-dependent algorithm for on-line particle sizing from extinction spectra which is both computationally efficient and accurate. Applying the refined Mie diagnostic iterative procedures within some candidate solutions can identify the unique result accurately and rapidly enough for real time measurement. With the addition of added Gaussian noise,an average tolerance up to 5% of noise level is kept for particle size from submicron to micrometer under moderate polydispersity.

  5. Submicron area NbN/MgO/NbN tunnel junctions for SIS mixer applications

    Leduc, H. G.; Judas, A.; Cypher, S. R.; Bumble, B.; Hunt, B. D.


    The development of submicron area mixer elements for operation in the submillimeter wave range is discussed. High-current-density NbN/MgO/NbN tunnel junctions with areas down to 0.1 sq microns have been fabricated in both planar and edge geometries. The planar junctions were fabricated from in situ deposited trilayers using electron-beam lithography to pattern submicron area mesas. Modifications of fabrication techniques used in larger-area NbN tunnel junctions are required and are discussed. The NbN/MgO/NbN edge junction process using sapphire substrates has been transferred to technologically important quartz substrates using MgO buffer layers to minimize substrate interactions. The two junction geometries are compared and contrasted in the context of submillimeter wave mixer applications.

  6. Novel submicronized rebamipide liquid with moderate viscosity: significant effects on oral mucositis in animal models.

    Nakashima, Takako; Sako, Nobutomo; Matsuda, Takakuni; Uematsu, Naoya; Sakurai, Kazushi; Ishida, Tatsuhiro


    This study aimed at developing a novel rebamipide liquid for an effective treatment of oral mucositis. The healing effects of a variety of liquids comprising submicronized rebamipide crystals were investigated using a rat cauterization-induced oral ulcer model. Whereas 2% rebamipide liquid comprising micro-crystals did not exhibit significant curative effect, 2% rebamipide liquids comprising submicronized crystals with moderate viscosities exhibited healing effects following intra-oral administration. The 2% and 4% optimized rebamipide liquids showed significant healing effects in the rat oral ulcer model (prebamipide liquid significantly reduced the percent area of ulcerated injury (prebamipide liquid with moderate viscosity following intra-oral administration showed better both healing effect in the rat oral ulcer model and preventive effect in the rat irradiation-induced glossitis model.

  7. Microstructural and electromagnetic properties of MnO2 coated nickel particles with submicron size

    Tang Bao-Lin; He Jun; Ji Tian-Hao; Wang Xin-Lin


    Nickel particles with submicron size are prepared by using the solvothermal method. These spheres are then coated with a layer of MnO2 using the soft chemical method. The microstructure is characterized by x-ray diffraction,transmission electron microscopy, and scanning electron microscopy. Energy x-ray dispersive spectrometry and high-resolution images show that the granular composites have a classical core/shell structure with an MnO2 superficial layer, no more than 10 nm in thickness. The hysteresis measurements indicate that these submicron-size Ni composite powders have small remanence and moderate coercivity. The electromagnetic properties of the powders measured by a vector network analyzer in a frequency range of 2-18 GHz are also reported in detail.

  8. Fabrication of submicron chalcogenide glass photonic crystal by resist-free nanoimprint lithography

    Zeng, Jianghui; Zhang, Qian; Zhang, Peiqing; Tang, Junzhou; Xu, Yinsheng; Chen, Feifei; Shen, Xiang; Dai, Shixun


    We reported the fabrication of submicron photonic crystal with As40Se40Te20 chalcogenide glass by resist-free thermal nanoimprint using a soft stamp. The As40Se40Te20 glass was prepared with melt-quenching method, and measured to have broad transmission range, high linear and nonlinear refractive index, and good thermal stability. Due to the very low glass transition temperature, the thermal nanoimprint was accomplished directly on the resist-free bulk glass with the soft stamp. By choosing suitable imprint condition, submicron chalcogenide glass photonic crystal with the band gap covering telecom wavelength was obtained. Taking advantage of the high nonlinearity of As40Se40Te20 glass, the imprinted PC structure may have potential applications for all-optical switch in optical communications.

  9. Preparation techniques of the submicron lithium titanate materials by electro-spinning

    Wang, Yudong; Yang, Kai; Gao, Fei; Liu, Hao; Zhang, Mingjie


    Combining sol-gel process and electro-spinning, the submicron lithium titanate materials are prepared with lithium acetate and titanium tetraisopropanolate respectively as the lithium and titanium sources, and polyvinylpyrrolidone (PVP) as the template. It's found by scanning electron microscope(SEM )that, the prepared lithium titanate materials are characterized by the fiber diameter 150~200nm, a large number of irregular indentations in the surface, and the larger specific surface area than that before calcination. The lithium titanate cell receives charge-discharge test and cyclic voltammetry. The capacity of the submicron lithium titanate materials is up to 160mAh·g-1 at the rate of 0.1C, and it's revealed by cyclic voltammetry that the cell in the charge or discharge process undergoes a single redox reaction, but having good reversibility.

  10. Correlation between Surface Roughness Characteristics in CO2 Laser Cutting of Mild Steel

    M. Radovanović


    Full Text Available CO2 laser oxygen cutting of mild steel is widely used industrial application. Cut surface quality is a very important characteristic of laser cutting that ensures an advantage over other contour cutting processes. In this paper mathematical models for estimating characteristics of surface quality such as average surface roughness and ten-point mean roughness in CO2 laser cutting of mild steel based on laser cutting parameters were developed. Empirical models were developed using artificial neural networks and experimental data collected. Taguchi’s orthogonal array was implemented for experimental plan. From the analysis of the developed mathematical models it was observed that functional dependence between laser cutting parameters, their interactions and surface roughness characteristics is complex and non-linear. It was also observed that there exist region of minimal average surface roughness to ten-point mean roughness ratio. The relationship between average surface roughness and ten-point mean roughness was found to be nonlinear and can be expressed with a second degree polynomial.

  11. Impact of Device Architecture on Performance and Reliability of Deep Submicron SOI MOSFETs (invited paper)


    The main electrical properties of advanced Silicon-On-Insulator MOSFETs are addressed. The subthreshold and high field operations are analysed as a function of device architecture. The special SOI parasitic phenomena, such as the floating body potential and temperature, are critically reviewed. The main limitations of submicron MOSFET are comparatively evaluated for various SOI structures. Short channel and hot carrier effects as well as the reliability of the SOI technology are investigated for gate length down to sub-0. 1 micron.

  12. Study of Submicron Particle Size Distribution by Laser Doppler Measurement of Brownian Motion.


    regime considered here, heat transfer from the submicron particles by forced convection and natural convection are negligible due to the extremely small...physical processes begin to influence the Brownian motion characteristics at high laser beam intensity. An analysis of the effects of thermophoresis and...photon pressure was carried out. The effect of thermophoresis due to the uneven heating of the particle by the laser beam was found to be a major

  13. DARPA-URI Consortium Meetings on Submicron Heterostructures of Diluted Magnetic Semiconductors.


    B 35, 7464 (1987). 46. S. Rodriguez, A. Camacho and L. Quiroga, "Electrostatic and Magnetostatic Modes in Semiconductor Superlattices", (to appear in...AD-RI93 499 DARPA-URI CONSORTIUM MEETINGS ON SUSMICRON IETEROSTRUCTURES OF DILUTED MAGNETIC SEMICONDUCTORS (U) PURDUE UNIV LRFRYETTE IN 1987 N91114-86...o FILE COPY (SUBMICRON HETEROSTRUCTURES ,it OF DILUTED MAGNETIC SEMICONDUCTORS ANNUAL REPORT 1986-87 The Principal Investigators along with their co

  14. 1.55 Micrometer Sub-Micron Finger, Interdigitated MSM Photodetector Arrays with Low Dark Current


    morphology is generally smoother. These transparent conducting oxides may also be used as electrodes in solar cells and flat-panel display devices...REPORT Final Report of 1.55 UM Sub-Micron Finger, Interdigitated MSM Photodetector Arrays with Low Dark Current 14. ABSTRACT 16. SECURITY... Interdigitated MSM Photodetector Arrays with Low Dark Current Sponsored by: U. S. Army Research Office Dr. Michael D. Gerhold Contract

  15. Directed assembly of conducting polymers on sub-micron templates by electrical fields

    Shen, Jia; Wei, Ming [National Science Foundation (NSF) Nanoscale Science and Engineering Center for High-Rate Nanomanufacturing, University of Massachusetts Lowell, Lowell, MA 01854 (United States); Busnaina, Ahmed [National Science Foundation (NSF) Nanoscale Science and Engineering Center for High-Rate Nanomanufacturing, Northeastern University, Boston, MA 02115 (United States); Barry, Carol [National Science Foundation (NSF) Nanoscale Science and Engineering Center for High-Rate Nanomanufacturing, University of Massachusetts Lowell, Lowell, MA 01854 (United States); Mead, Joey, E-mail: [National Science Foundation (NSF) Nanoscale Science and Engineering Center for High-Rate Nanomanufacturing, University of Massachusetts Lowell, Lowell, MA 01854 (United States)


    Highlights: Black-Right-Pointing-Pointer Nanoscale patterns with dimensions of assembled PANi down to 100 nm were fabricated. Black-Right-Pointing-Pointer We use electrophoretic and dielectrophoretic assembly to deposit PANi. Black-Right-Pointing-Pointer Electrophoretic and dielectrophoretic assembly of PANi finished in less than 1 min. Black-Right-Pointing-Pointer Effect of process parameters on assembly of PANi onto nanoscale pattern was studied. Black-Right-Pointing-Pointer The assembled PANi can be transferred to other flexible substrates. - Abstract: Patterning of conducting polymer into sub-micron patterns over large areas at high rate and low cost is significant for commercial manufacturing of novel devices. Electrophoretic and dielectrophoretic assembly provide an easily scaled approach with high fabrication rates. In this work, electrophoretic and dielectrophoretic assembly were used to assemble polyaniline (PANi) into multiscale sub-micron size patterns in less than 1 min. The process was controlled by assembly time, amplitude, and frequency of the electric field. Dielectrophoretic assembly is preferable for manufacturing as it reduces damage to the templates used to control the assembly. Using this method, sub-micron patterns with dimensions of the assembled PANi down to 100 nm were fabricated over large areas in short times. The assembled PANi was further transferred to other flexible polymer substrates by a thermoforming process, providing a fast, easily controlled and promising approach for fabrication of nanoscale devices.

  16. Continuous Draw Spinning of Extra-Long Silver Submicron Fibers with Micrometer Patterning Capability.

    Bai, Xiaopeng; Liao, Suiyang; Huang, Ya; Song, Jianan; Liu, Zhenglian; Fang, Minghao; Xu, Chencheng; Cui, Yi; Wu, Hui


    Ultrathin metal fibers can serve as highly conducting and flexible current and heat transport channels, which are essential for numerous applications ranging from flexible electronics to energy conversion. Although industrial production of metal fibers with diameters of down to 2 μm is feasible, continuous production of high-quality and low-cost nanoscale metal wires is still challenging. Herein, we report the continuous draw spinning of highly conductive silver submicron fibers with the minimum diameter of ∼200 nm and length of more than kilometers. We obtained individual AgNO3/polymer fibers by continuous drawing from an aqueous solution at a speed of up to 8 m/s. With subsequent heat treatment, freestanding Ag submicron fibers with high mechanical flexibility and electric conductivity have been obtained. Woven mats of aligned Ag submicron fibers were used as transparent electrodes with high flexibility and high performance with sheet resistance of 7 Ω sq(-1) at a transparency of 96%. Continuous draw spinning opened new avenues for scalable, flexible, and ultralow-cost fabrication of extra-long conductive ultrathin metal fibers.

  17. A new route for the synthesis of submicron-sized LaB{sub 6}

    Lihong, Bao; Wurentuya,; Wei, Wei; Tegus, O., E-mail:


    Submicron crystalline LaB{sub 6} has been successfully synthesized by a solid-state reaction of La{sub 2}O{sub 3} with NaBH{sub 4} at 1200 °C. The effects of reaction temperature on the crystal structure, grain size and morphology were investigated by X-ray diffraction, scanning electron microscope and transmission electron microscope. It is found that when the reaction temperature is in the range of 1000–1100 °C, there are ultrafine nanoparticles and nanocrystals that coexist. When the reaction temperature elevated to 1200 °C, the grain morphology transformed from ultrafine nanoparticle to submicron crystals completely. High resolution transmission electron microscope images fully confirm the formation of LaB{sub 6} cubic structure. - Highlights: • Single-phased LaB{sub 6} have been synthesized by a solid-state reaction in a continuous evacuating process. • The reaction temperature has a important effect on the phase composition. • The grain size increase from nano-size to submicron with increasing reaction temperature.

  18. Ordered YBCO sub-micron array structures induced by pulsed femtosecond laser irradiation.

    Luo, C W; Lee, C C; Li, C H; Shih, H C; Chen, Y-J; Hsieh, C C; Su, C H; Tzeng, W Y; Wu, K H; Juang, J Y; Uen, T M; Chen, S P; Lin, J-Y; Kobayashi, T


    We report on the formation of organized sub-micron YBa(2)Cu(3)O(7) (YBCO) dots induced by irradiating femtosecond laser pulses on YBCO films prepared by pulse laser deposition with fluence in the range of 0.21 approximately 0.53 J/cm(2). The morphology of the YBCO film surface depends strongly on the laser fluences irradiated. At lower laser fluence (approximately 0.21 J/cm(2)) the morphology was pattern of periodic ripples with sub-micrometer spacing. Slightly increasing the laser fluence to 0.26 J/cm(2) changes the pattern into organized sub-micron dots with diameters ranging from 100 nm to 800 nm and height of 150 nm. Further increase of the laser fluence to over 0.32 J/cm(2), however, appeared to result in massive melting and led to irregular morphology. The mechanism and the implications of the current findings will be discussed. Arrays of YBCO sub-micron dots with T(c) = 89.7 K were obtained.

  19. Parametric Deduction Optimization for Surface Roughness

    Tian-Syung Lan


    Full Text Available Problem statement: Surface roughness is a major consideration in modern Computer Numerical Control (CNC turning industry. Most existing optimization researches for CNC finish turning were either accomplished within certain manufacturing circumstances, or achieved through numerous equipment operations. Therefore, a general deduction optimization scheme is deemed to be necessary for the industry. Approach: In this study, four parameters (cutting depth, feed rate, speed, tool nose runoff with three levels (low, medium, high were considered to optimize the surface roughness for Computer Numerical Control (CNC finish turning. Additionally, twenty-seven fuzzy control rules using trapezoid membership function with respective to seventeen linguistic grades for the surface roughness were constructed. Considering thirty input and eighty output intervals, the defuzzification using center of gravity was moreover completed. Through the Taguchi experiment, the optimum general deduction parameters can then be received. Results: The confirmation experiment for optimum deduction parameters was furthermore performed on an ECOCA-3807 CNC lathe. It was shown that the surface roughness from the fuzzy deduction optimization parameters are significantly advanced comparing to those from benchmark. Conclusion: This study not only proposed a parametric deduction optimization scheme using orthogonal array, but also contributed the satisfactory fuzzy approach to the surface roughness for CNC turning with profound insight.

  20. Surface roughness measurement with laser triangulation

    Bai, Fuzhong; Zhang, Xiaoyan; Tian, Chaoping


    A surface roughness measurement method is introduced in the paper, which is based on laser triangulation and digital image processing technique. In the measuring system, we use the line-structured light as light source, microscope lens and high-accuracy CCD sensor as displacement sensor as well. In addition, the working angle corresponding to the optimal sensitivity is considered in the optical structure design to improve the measuring accuracy. Through necessary image processing operation for the light strip image, such as center-line extraction with the barycenter algorithm, Gaussian filtering, the value of roughness is calculated. A standard planing surface is measured experimentally with the proposed method and the stylus method (Mitutoyo SJ-410) respectively. The profilograms of surface appearance are greatly similar in the shape and the amplitude to two methods. Also, the roughness statistics values are close. The results indicate that the laser triangulation with the line-structured light can be applied to measure the surface roughness with the advantages of rapid measurement and visualized display of surface roughness profile.

  1. Investigation of Surface Roughness in High-Speed Milling of Aeronautical Aluminum Alloy

    PAN Yong-zhi; AI Xing; ZHAO Jun; WAN Yi


    An approach is presented to optimize the surface roughness in high-speed finish milling of 7050-T7451 aeronautical aluminum alloy. In view of this, the multi-linear regression model for surface roughness has been developed in terms of slenderness ratio, cutting speed, radial depth-of-cut and feed per tooth by means of orthogonal experimental design. Variance analyses were applied to check the adequacy of the predictive model and the significances of the independent input parameters. Response contours of surface roughness were generated by using response surface methodology (RSM). From these contours, it was possible to select an optimum combination of cutting parameters that improves machining efficiency without increasing the surface roughness.

  2. Lunar polar craters - Icy, rough or just sloping?

    Eke, Vincent R.; Bartram, Sarah A.; Lane, David A.; Smith, David; Teodoro, Luis F. A.


    Circular Polarisation Ratio (CPR) mosaics from Mini-SAR on Chandrayaan-1 and Mini-RF on LRO are used to study craters near to the lunar north pole. The look direction of the detectors strongly affects the appearance of the crater CPR maps. Rectifying the mosaics to account for parallax also significantly changes the CPR maps of the crater interiors. It is shown that the CPRs of crater interiors in unrectified maps are biased to larger values than crater exteriors, because of a combination of the effects of parallax and incidence angle. Using the LOLA Digital Elevation Map (DEM), the variation of CPR with angle of incidence has been studied. For fresh craters, CPR ∼0.7 with only a weak dependence on angle of incidence or position interior or just exterior to the crater, consistent with dihedral scattering from blocky surface roughness. For anomalous craters, the CPR interior to the crater increases with both incidence angle and distance from the crater centre. Central crater CPRs are similar to those in the crater exteriors. CPR does not appear to correlate with temperature within craters. Furthermore, the anomalous polar craters have diameter-to-depth ratios that are lower than those of typical polar craters. These results strongly suggest that the high CPR values in anomalous polar craters are not providing evidence of significant volumes of water ice. Rather, anomalous craters are of intermediate age, and maintain sufficiently steep sides that sufficient regolith does not cover all rough surfaces.

  3. Anisotropic spreading of liquid metal on a rough intermetallic surface

    Liu Wen


    Full Text Available An anisotropic wicking of molten Sn-Pb solder over an intermetallic rough surface has been studied. The phenomenon features preferential spreading and forming of an elliptical spread domain. A theoretically formulated model was established to predict the ratio of the wicking distance along the long axis (rx to that along the short axis (ry of the final wicking pattern. The phenomenon was simultaneously experimentally observed and recorded with a hotstage microscopy technique. The anisotropic wicking is established to be caused by a non-uniform topography of surface micro structures as opposed to an isotropic wicking on an intermetallic surface with uniformly distributed surface micro features. The relative deviation between the theoretically predicted rx/ry ratio and the corresponding average experimental value is 5%. Hence, the small margin of error confirms the validity of the proposed theoretical model of anisotropic wicking.

  4. Radiative transfer model for contaminated rough slabs

    Andrieu, François; Schmidt, Frédéric; Schmitt, Bernard


    We present a semi-analytical model to simulate bidirectional reflectance distribution function (BRDF) spectra of a rough slab layer containing impurities. This model has been optimized for fast computation in order to analyze hyperspectral data. We designed it for planetary surfaces ices studies but it could be used for other purposes. It estimates the bidirectional reflectance of a rough slab of material containing inclusions, overlaying an optically thick media (semi-infinite media or stratified media, for instance granular material). The inclusions are supposed to be close to spherical, and of any type of other material than the ice matrix. It can be any type of other ice, mineral or even bubbles, defined by their optical constants. We suppose a low roughness and we consider the geometrical optics conditions. This model is thus applicable for inclusions larger than the considered wavelength. The scattering on the inclusions is assumed to be isotropic. This model has a fast computation implementation and th...

  5. Probabilistic Approach to Rough Set Theory

    Wojciech Ziarko


    The presentation introduces the basic ideas and investigates the probabilistic approach to rough set theory. The major aspects of the probabilistic approach to rough set theory to be explored during the presentation are: the probabilistic view of the approximation space, the probabilistic approximations of sets, as expressed via variable precision and Bayesian rough set models, and probabilistic dependencies between sets and multi-valued attributes, as expressed by the absolute certainty gain and expected certainty gain measures, respectively. The probabilis-tic dependency measures allow for representation of subtle stochastic associations between attributes. They also allow for more comprehensive evaluation of rules computed from data and for computation of attribute reduct, core and significance factors in probabilistic decision tables. It will be shown that the probabilistic dependency measure-based attribute reduction techniques are also extendible to hierarchies of decision tables. The presentation will include computational examples to illustrate pre-sented concepts and to indicate possible practical applications.

  6. Spin Hall effect by surface roughness

    Zhou, Lingjun


    The spin Hall and its inverse effects, driven by the spin orbit interaction, provide an interconversion mechanism between spin and charge currents. Since the spin Hall effect generates and manipulates spin current electrically, to achieve a large effect is becoming an important topic in both academia and industries. So far, materials with heavy elements carrying a strong spin orbit interaction, provide the only option. We propose here a new mechanism, using the surface roughness in ultrathin films, to enhance the spin Hall effect without heavy elements. Our analysis based on Cu and Al thin films suggests that surface roughness is capable of driving a spin Hall angle that is comparable to that in bulk Au. We also demonstrate that the spin Hall effect induced by surface roughness subscribes only to the side-jump contribution but not the skew scattering. The paradigm proposed in this paper provides the second, not if only, alternative to generate a sizable spin Hall effect.

  7. Radiation pressure on fluffy submicron-sized grains

    Silsbee, Kedron


    We investigate the claim that the ratio {\\beta} of radiation pressure force to gravitational force on a dust grain in our solar system can substantially exceed unity for some grain sizes, provided that grain porosity is high enough. For model grains consisting of random aggregates of silicate spherules, we find that the maximum value of {\\beta} is almost independent of grain porosity, but for small (<0.3 {\\mu}m) grains, {\\beta} actually decreases with increasing porosity. These results affect the interpretation of the grain trajectories estimated from the Stardust mission, which were modeled assuming {\\beta} values exceeding one. We find that radiation pressure effects are not large enough for particles Orion and Hylabrook captured by Stardust to be of interstellar origin given their reported impact velocities. We also investigate the effect of metallic iron inclusions in the dust grains, and find that metallic iron will increase {\\beta}, but at least half the grain (by mass) must be iron in order to raise...

  8. Reducing DRIFT Backgrounds with a Submicron Aluminized-Mylar Cathode

    Battat, James B R; Dorofeev, Alexei; Ezeribe, Anthony C; Fox, Jennifer R; Gauvreau, Jean-Luc; Gold, Michael; Harmon, Lydia; Harton, John; Lafler, Randy; Lauer, Robert J; Lee, Eric R; Loomba, Dinesh; Lumnah, Alexander; Matthews, John; Miller, Eric H; Mouton, Frederic; Murphy, Alexander St J; Phan, Nguyen; Sadler, Stephen W; Scarff, Andrew; Schuckman, Fred; Snowden-Ifft, Daniel; Spooner, Neil J C; Walker, Daniel


    Background events in the DRIFT-IId dark matter detector, mimicking potential WIMP signals, are predominantly caused by alpha decays on the central cathode in which the alpha particle is completely or partially absorbed by the cathode material. We installed a 0.9 micron thick aluminized-mylar cathode as a way to reduce the probability of producing these backgrounds. We study three generations of cathode (wire, thin-film, and radiologically clean thin-film) with a focus on the ratio of background events to alpha decays. Two independent methods of measuring the absolute alpha decay rate are used to ensure an accurate result, and agree to within $10\\%$. Using alpha range spectroscopy, we measure the radiologically cleanest cathode version to have a contamination of $3.3\\pm0.1$ ppt $^{234}$U and $73\\pm2$ ppb $^{238}$U. This cathode reduces the probability of producing an RPR from an alpha decay by a factor of $70\\pm20$ % while reducing the overall background rate by $96.5\\pm0.5\\%$ compared to the original stainles...

  9. Investigating the annual behaviour of submicron secondary inorganic and organic aerosols in London

    D. E. Young


    Full Text Available For the first time, the behaviour of non-refractory inorganic and organic submicron particulate through an entire annual cycle is investigated using measurements from an Aerodyne compact time-of-flight aerosol mass spectrometer (cToF-AMS located at a UK urban background site in North Kensington, London. We show secondary aerosols account for a significant fraction of the submicron aerosol burden and that high concentration events are governed by different factors depending on season. Furthermore, we demonstrate that on an annual basis there is no variability in the extent of secondary organic aerosol (SOA oxidation, as defined by the oxygen content, irrespective of amount. This result is surprising given the changes in precursor emissions and contributions as well as photochemical activity throughout the year; however it may make the characterisation of SOA in urban environments more straightforward than previously supposed. Organic species, nitrate, sulphate, ammonium, and chloride were measured during 2012 with average concentrations (±one standard deviation of 4.32 (±4.42, 2.74 (±5.00, 1.39 (±1.34, 1.30 (±1.52 and 0.15 (±0.24 μg m–3, contributing 43, 28, 14, 13 and 2% to the total submicron mass, respectively. Components of the organic aerosol fraction are determined using positive matrix factorisation (PMF where five factors are identified and attributed as hydrocarbon-like OA (HOA, cooking OA (COA, solid fuel OA (SFOA, type 1 oxygenated OA (OOA1, and type 2 oxygenated OA (OOA2. OOA1 and OOA2 represent more and less oxygenated OA with average concentrations of 1.27 (±1.49 and 0.14 (±0.29 μg m–3, respectively, where OOA1 dominates the SOA fraction (90%. Diurnal, monthly, and seasonal trends are observed in all organic and inorganic species, due to meteorological conditions, specific nature of the aerosols, and availability of precursors. Regional and transboundary pollution as well as other individual pollution events influence

  10. Generation of sub-micron particles and secondary pollutants from building materials by ozone reaction

    Aoki, Taisuke; Tanabe, Shin-ichi

    This study reports results from two different experiments examining reactions between ozone and common building materials that can lead to the formation of secondary products and particulate-phase materials. Monitored species include sub-micron particles and volatile organic compounds (VOCs). In the first set of experiments, various building materials were placed in a 20 L stainless-steel chamber and exposed to ozone. The materials included expanded polystyrene, a natural rubber adhesive, cedar board, Japanese Cyprus board and silver fir board, as well as d-limonene, which is a known constituent of certain woods and cleaning products. The combination of ozone and either d-limonene, cedar board or cypress board produced sub-micron particles, with most of the increase occurring in the size range of 0.01- 0.5μm diameter. This was not observed for the other materials. In the case of cedar board, the consequence of ozone exposure over an extended time interval was monitored. As the exposure time elapsed, the concentration of sub-micron particles moderately decreased. In the second set of experiments, unwaxed or waxed plastic tiles were placed in the 20 L chamber and exposed to ozone. Sub-micron particles and organic compounds were measured during the course of the experiments. In the case of the waxed tile, the number of 0.01- 1.0μm size particles grew about 50×108particlesm-3; particle growth was significantly less for the un-waxed tile. For both the waxed and un-waxed tiles, the emission rates of heptane, nonane, nonanal, and decanal increased after ozone was added to the supply air. (However, it is not clear if some or all of this production was due to ozone reacting with the sorbent used for sampling or with compounds captured by the sorbent.) This study provides further evidence that ozone-initiated reactions with building materials can be a significant source of both sub-micron particles and secondary organic compounds in indoor environments.

  11. Evaluating model parameterizations of submicron aerosol scattering and absorption with in situ data from ARCTAS 2008

    Alvarado, Matthew J.; Lonsdale, Chantelle R.; Macintyre, Helen L.; Bian, Huisheng; Chin, Mian; Ridley, David A.; Heald, Colette L.; Thornhill, Kenneth L.; Anderson, Bruce E.; Cubison, Michael J.; Jimenez, Jose L.; Kondo, Yutaka; Sahu, Lokesh K.; Dibb, Jack E.; Wang, Chien


    Accurate modeling of the scattering and absorption of ultraviolet and visible radiation by aerosols is essential for accurate simulations of atmospheric chemistry and climate. Closure studies using in situ measurements of aerosol scattering and absorption can be used to evaluate and improve models of aerosol optical properties without interference from model errors in aerosol emissions, transport, chemistry, or deposition rates. Here we evaluate the ability of four externally mixed, fixed size distribution parameterizations used in global models to simulate submicron aerosol scattering and absorption at three wavelengths using in situ data gathered during the 2008 Arctic Research of the Composition of the Troposphere from Aircraft and Satellites (ARCTAS) campaign. The four models are the NASA Global Modeling Initiative (GMI) Combo model, GEOS-Chem v9-02, the baseline configuration of a version of GEOS-Chem with online radiative transfer calculations (called GC-RT), and the Optical Properties of Aerosol and Clouds (OPAC v3.1) package. We also use the ARCTAS data to perform the first evaluation of the ability of the Aerosol Simulation Program (ASP v2.1) to simulate submicron aerosol scattering and absorption when in situ data on the aerosol size distribution are used, and examine the impact of different mixing rules for black carbon (BC) on the results. We find that the GMI model tends to overestimate submicron scattering and absorption at shorter wavelengths by 10-23 %, and that GMI has smaller absolute mean biases for submicron absorption than OPAC v3.1, GEOS-Chem v9-02, or GC-RT. However, the changes to the density and refractive index of BC in GC-RT improve the simulation of submicron aerosol absorption at all wavelengths relative to GEOS-Chem v9-02. Adding a variable size distribution, as in ASP v2.1, improves model performance for scattering but not for absorption, likely due to the assumption in ASP v2.1 that BC is present at a constant mass fraction

  12. A Novel Research on Rough Clustering Algorithm

    Tao Qu


    Full Text Available The aim of this study is focusing the issue of traditional clustering algorithm subjects to data space distribution influence, a novel clustering algortihm combined with rough set theory is employed to the normal clustering. The proposed rough clustering algorithm takes the condition attributes and decision attributes displayed in the information table as the consistency principle, meanwhile it takes the data supercubic and information entropy to realize data attribute shortcutting and discretizing. Based on above discussion, by applying assemble feature vector addition principle computiation only one scanning information table can realize clustering for the data subject. Experiments reveal that the proposed algorithm is efficient and feasible.

  13. Fuzzy sets, rough sets, multisets and clustering

    Dahlbom, Anders; Narukawa, Yasuo


    This book is dedicated to Prof. Sadaaki Miyamoto and presents cutting-edge papers in some of the areas in which he contributed. Bringing together contributions by leading researchers in the field, it concretely addresses clustering, multisets, rough sets and fuzzy sets, as well as their applications in areas such as decision-making. The book is divided in four parts, the first of which focuses on clustering and classification. The second part puts the spotlight on multisets, bags, fuzzy bags and other fuzzy extensions, while the third deals with rough sets. Rounding out the coverage, the last part explores fuzzy sets and decision-making.


    Hunter, C.


    Surface roughness values for the areas surrounding the H, D and N-Area meteorological towers were computed from archived 2010 meteorological data. These 15-minute-averaged data were measured with cup anemometers and bidirectional wind vanes (bivanes) 61 m above the surface. The results of the roughness calculation using the standard deviation of elevation angle {sigma}{sub E}, and applying the simple formula based on tree canopy height, gave consistent estimates for roughness around the H-Area tower in the range of 1.76 to 1.86 m (95% confidence interval) with a mean value of 1.81 m. Application of the {sigma}{sub E} method for the 61-m level at D and N-Areas gave mean values of 1.71 and 1.81 with confidence ranges of 1.62-1.81 and 1.73-1.88 meters, respectively. Roughness results are azimuth dependent, and thus are presented as averages over compass sectors spanning 22.5 degrees. Calculated values were compared to other methods of determining roughness, including the standard deviation of the azimuth direction, {sigma}{sub A}, and standard deviation of the wind speed, {sigma}{sub U}. Additional data was obtained from a sonic anemometer at 61-m on the H-Area tower during a period of a few weeks in 2010. Results from the sonic anemometer support our use of {sigma}{sub E} to calculate roughness. Based on the H-Area tower results, a surface roughness of 1.8 m using is recommended for use in dispersion modeling applications that consider the impacts of a contaminant release to individuals along the Site boundary. The canopy surrounding the H-Area tower is relatively uniform (i.e., little variance in roughness by upwind direction), and data supplied by the U.S. Forest Service at Savannah River show that the canopy height and composition surrounding the H-Area tower is reasonably representative of forested areas throughout the SRS reservation. For dispersion modeling analyses requiring assessments of a co-located worker within the respective operations area, recommended

  15. Rough-wall turbulent boundary layers with constant skin friction

    Sridhar, A.


    A semi-empirical model is presented that describes the development of a fully developed turbulent boundary layer in the presence of surface roughness with length scale ks that varies with streamwise distance x . Interest is centred on flows for which all terms of the von Kármán integral relation, including the ratio of outer velocity to friction velocity U+∞≡U∞/uτ , are streamwise constant. For Rex assumed large, use is made of a simple log-wake model of the local turbulent mean-velocity profile that contains a standard mean-velocity correction for the asymptotic fully rough regime and with assumed constant parameter values. It is then shown that, for a general power-law external velocity variation U∞∼xm , all measures of the boundary-layer thickness must be proportional to x and that the surface sand-grain roughness scale variation must be the linear form ks(x)=αx , where x is the distance from the boundary layer of zero thickness and α is a dimensionless constant. This is shown to give a two-parameter (m,α) family of solutions, for which U+∞ (or equivalently Cf ) and boundary-layer thicknesses can be simply calculated. These correspond to perfectly self-similar boundary-layer growth in the streamwise direction with similarity variable z/(αx) , where z is the wall-normal coordinate. Results from this model over a range of α are discussed for several cases, including the zero-pressure-gradient ( m=0 ) and sink-flow ( m=−1 ) boundary layers. Trends observed in the model are supported by wall-modelled large-eddy simulation of the zero-pressure-gradient case for Rex in the range 108−1010 and for four values of α . Linear streamwise growth of the displacement, momentum and nominal boundary-layer thicknesses is confirmed, while, for each α , the mean-velocity profiles and streamwise turbulent variances are found to collapse reasonably well onto z/(αx) . For given α , calculations of U+∞ obtained from large-eddy simulations are streamwise

  16. In situ visualisation and characterisation of the capacity of highly reactive minerals to preserve soil organic matter (SOM) in colloids at submicron scale.

    Xiao, Jian; Wen, Yongli; Li, Huan; Hao, Jialong; Shen, Qirong; Ran, Wei; Mei, Xinlan; He, Xinhua; Yu, Guanghui


    Mineral-organo associations (MOAs) are a mixture of identifiable biopolymers associated with highly reactive minerals and microorganisms. However, the in situ characterization and correlation between soil organic matter (SOM) and highly reactive Al and Fe minerals are still unclear for the lack of technologies, particularly in the long-term agricultural soil colloids at submicron scale. We combined several novel techniques, including nano-scale secondary ion mass spectrometry (NanoSIMS), X-ray absorption near edge structure (XANES) and confocal laser scanning microscopy (CLSM) to characterise the capacity of highly reactive Al and Fe minerals to preserve SOM in Ferralic Cambisol in south China. Our results demonstrated that: (1) highly reactive minerals were strongly related to SOM preservation, while SOM had a more significant line correlation with the highly reactive Al minerals than the highly reactive Fe minerals, according to the regions of interest correlation analyses using NanoSIMS; (2) allophane and ferrihydrite were the potential mineral species to determine the SOM preservation capability, which was evaluated by the X-ray photoelectron spectroscopy (XPS) and Fe K-edge XANES spectroscopy techniques; and (3) soil organic biopolymers with dominant compounds, such as proteins, polysaccharides and lipids, were distributed at the rough and clustered surface of MOAs with high chemical and spatial heterogeneity according to the CLSM observation. Our results also promoted the understanding of the roles played by the highly reactive Al and Fe minerals in the spatial distribution of soil organic biopolymers and SOM sequestration.

  17. Terahertz oscillations in an In{sub 0.53}Ga{sub 0.47}As submicron planar Gunn diode

    Khalid, Ata, E-mail:; Thoms, S.; Macintyre, D.; Li, C.; Steer, M. J.; Papageorgiou, V.; Thayne, I. G.; Cumming, D. R. S. [School of Engineering, University of Glasgow, Glasgow G12 8LT (United Kingdom); Dunn, G. M.; Macpherson, R. F.; Stephen, A. [School of Engineering and Physical Sciences, University of Aberdeen, Aberdeen AB24 SFX (United Kingdom); Kuball, M.; Montes Bajo, M. [H. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue BS8 1TL (United Kingdom); Oxley, C. H.; Glover, J. [Electronic Engineering Department, Faculty of Technology, De Montfort University, Leicester LE1 9BH (United Kingdom)


    The length of the transit region of a Gunn diode determines the natural frequency at which it operates in fundamental mode—the shorter the device, the higher the frequency of operation. The long-held view on Gunn diode design is that for a functioning device the minimum length of the transit region is about 1.5 μm, limiting the devices to fundamental mode operation at frequencies of roughly 60 GHz. Study of these devices by more advanced Monte Carlo techniques that simulate the ballistic transport and electron-phonon interactions that govern device behaviour, offers a new lower bound of 0.5 μm, which is already being approached by the experimental evidence that has shown planar and vertical devices exhibiting Gunn operation at 600 nm and 700 nm, respectively. The paper presents results of the first ever THz submicron planar Gunn diode fabricated in In{sub 0.53}Ga{sub 0.47}As on an InP substrate, operating at a fundamental frequency above 300 GHz. Experimentally measured rf power of 28 μW was obtained from a 600 nm long × 120 μm wide device. At this new length, operation in fundamental mode at much higher frequencies becomes possible—the Monte Carlo model used predicts power output at frequencies over 300 GHz.

  18. Tailoring the electric and magnetic properties of submicron-sized metallic multilayered systems by TVA atomic inter-diffusion engineered processes

    Miculescu, F.; Jepu, I.; Stan, G. E.; Miculescu, M.; Voicu, S. I.; Cotrut, C.; Pisu, T. Machedon; Ciuca, S.


    Thermo-ionic Vacuum Arc evaporation method was selected for the synthesis of Fe/Cu/Ni/Cu multilayer structures on Si (1 0 0) substrates. The aim of the study was the preparation and characterization of structures featuring a giant magnetoresistance effect. This was accomplished by inducing the formation of nanosized ferromagnetic crystallites in multilayer nonmagnetic solutions via atomic inter-diffusion processes by the tuning of deposition parameters. Layer-by-layer and inter-diffused type structures were prepared and comparatively analyzed by scanning electron microscopy, X-ray microanalysis, atomic force microscopy, X-ray diffraction and high-resolution transmission electron microscopy coupled with selected area electron diffraction. We presented the influence of the microstructure on electric and magnetic properties of the submicron-sized multilayers. The dependence of the electric resistance and the magnetoresistance on the composition, structure, morphology and roughness of the layers was established. We obtained an electric resistance value of 1.22 Ω for the layer-by-layer type structure, and 0.46 Ω for the inter-diffusion designed structure. Using the atomic inter-diffusion we succeeded in achieving an improvement of the magnetoresistive effect, from 0.1% to 2.3%.

  19. Self-affine roughness influence on the Casimir effect

    Palasantzas, G


    In this work we investigate the influence of self-affine roughness on the Casimir energy for plate-plate geometry. The plate roughness is characterized by the rms roughness amplitude w, the lateral correlation length xi, and the roughness exponent H. It is shown that the latter has a prominent effec

  20. Self-affine roughness influence on redox reaction charge admittance

    Palasantzas, G


    In this work we investigate the influence of self-affine electrode roughness on the admittance of redox reactions during facile charge transfer kinetics. The self-affine roughness is characterized by the rms roughness amplitude w, the correlation length xi and the roughness exponent H (0

  1. Rough sets selected methods and applications in management and engineering

    Peters, Georg; lzak, Dominik


    Rough Set Theory, introduced by Pawlak in the early 1980s, has become an important part of soft computing within the last 25 years. However, much of the focus has been on the theoretical understanding of Rough Sets, with a survey of Rough Sets and their applications within business and industry much desired. Rough Sets: Selected Methods and Applications in Management and Engineering provides context to Rough Set theory, with each chapter exploring a real-world application of Rough Sets. Rough Sets is relevant to managers striving to improve their businesses, industry researchers looking to imp

  2. More on neutrosophic soft rough sets and its modification

    Emad Marei


    Full Text Available This paper aims to introduce and discuss anew mathematical tool for dealing with uncertainties, which is a combination of neutrosophic sets, soft sets and rough sets, namely neutrosophic soft rough set model. Also, its modification is introduced. Some of their properties are studied and supported with proved propositions and many counter examples. Some of rough relations are redefined as a neutrosophic soft rough relations. Comparisons among traditional rough model, suggested neutrosophic soft rough model and its modification, by using their properties and accuracy measures are introduced. Finally, we illustrate that, classical rough set model can be viewed as a special case of suggested models in this paper.

  3. Surface roughness scattering in multisubband accumulation layers

    Fu, Han; Reich, K. V.; Shklovskii, B. I.


    Accumulation layers with very large concentrations of electrons where many subbands are filled became recently available due to ionic liquid and other new methods of gating. The low-temperature mobility in such layers is limited by the surface roughness scattering. However, theories of roughness scattering so far dealt only with the small-density single subband two-dimensional electron gas (2DEG). Here we develop a theory of roughness-scattering limited mobility for the multisubband large concentration case. We show that with growing 2D electron concentration n the surface dimensionless conductivity σ /(2 e2/h ) first decreases as ∝n-6 /5 and then saturates as ˜(d aB/Δ2)≫1 , where d and Δ are the characteristic length and height of the surface roughness and aB is the effective Bohr radius. This means that in spite of the shrinkage of the 2DEG thickness and the related increase of the scattering rate the 2DEG remains a good metal.

  4. Plasticity under rough surface contact and friction

    Sun, F.


    The ultimate objective of this work is to gain a better understanding of the plastic behavior of rough metal surfaces under contact loading. Attention in this thesis focuses on the study of single and multiple asperities with micrometer scale dimensions, a scale at which plasticity is known to be si

  5. Potential roughness near lithographically fabricated atom chips

    Krüger, Peter; Andersson, L. M.; Wildermuth, Stefan


    Potential roughness has been reported to severely impair experiments in magnetic microtraps. We show that these obstacles can be overcome as we measure disorder potentials that are reduced by two orders of magnitude near lithographically patterned high-quality gold layers on semiconductor atom chip...

  6. Traceability of optical roughness measurements on polymers

    De Chiffre, Leonardo; Gasparin, Stefania; Carli, Lorenzo;


    An experimental investigation on surface roughness measurements on plastics was carried out with the objective of developing a methodology to achieve traceability of optical instruments. A ground steel surface and its replicas were measured using a stylus instrument, an optical auto-focus......% for the auto-focus instrument and 10% for confocal microscope....



    In this note the authors give the weighted Lp-boundedness fora class of maximal singular integral operators with rough kernel.The result in this note is an improvement and extension ofthe result obtained by Chen and Lin in 1990.

  8. Using Modularity with Rough Decision Models

    Ahmed T. Shawky


    Full Text Available Many real world applications need to deal with imprecise data. Therefore, there is a need for new techniques which can manage such imprecision. Computational Intelligence (CI techniques are the most appropriate for dealing with imprecise data to help decision makers. It is well known that soft computing techniques like genetic algorithms, neural networks, and fuzzy logic are effective in dealing with problems without explicit model and characterized by uncertainties Using fuzzy set theory considered as major techniques, which allows decision makers to take a good decision using imprecise inexact data and knowledge. Now using rough set is getting quite necessary to be used for its ability to mining such type of data. In this research, we are looking forward to propose a novel technique, which depends on the integration between fuzzy set concepts and rough set theory in mining relational databases. The proposed model allows introducing modularity mechanism, by building a virtual modular decision tables according to variety of decision makers points of view. And introduce decision grouping mechanism for getting the optimizing decision. This approach provides flexibility in decision making verifies all decision standards and determines decision requirements, through modularizing rough decision table, extraction of rough association rules and developing mechanisms for decision grouping.

  9. Distance upon contact: Determination from roughness profile

    van Zwol, P.J.; Svetovoy, Vitaly; Palasantzas, G.


    The point at which two random rough surfaces make contact takes place at the contact of the highest asperities. The distance upon contact d0 in the limit of zero load has crucial importance for determination of dispersive forces. Using gold films as an example we demonstrate that for two parallel

  10. Automated Grading of Rough Hardwood Lumber

    Richard W. Conners; Tai-Hoon Cho; Philip A. Araman


    Any automatic hardwood grading system must have two components. The first of these is a computer vision system for locating and identifying defects on rough lumber. The second is a system for automatically grading boards based on the output of the computer vision system. This paper presents research results aimed at developing the first of these components. The...

  11. Optical measurement of surface roughness in manufacturing

    Brodmann, R.


    The measuring system described here is based on the light-scattering method, and was developed by Optische Werke G. Rodenstock, Munich. It is especially useful for rapid non-contact monitoring of surface roughness in production-related areas. This paper outlines the differences between this system and the common stylus instrument, including descriptions of some applications in industry.

  12. Radiative Transfer Model for Contaminated Rough Surfaces


    plot of Figure 8 shows three sharp spectral features (in the LWIR region) that were used for calibration . 1000 1500 2000 2500 3000 3500 0 0.1 0.2...transfer, reflectance, rough surface, BRDF, Kramers-Kronig, penetration depth, fill factor, infrared, LWIR , MWIR, absorption coefficient, scattering...and the calibrated α are plotted in red, and green, respectively

  13. Thermal smoothing of rough surfaces in vacuo

    Wahl, G.


    The derivation of equations governing the smoothing of rough surfaces, based on Mullins' (1957, 1960, and 1963) theories of thermal grooving and of capillarity-governed solid surface morphology is presented. As an example, the smoothing of a one-dimensional sine-shaped surface is discussed.

  14. Surface roughness evolution of nanocomposite thin films

    Turkin, A; Pei, Y.T.; Shaha, K.P.; Chen, C.Q.; Vainchtein, David; Hosson, J.Th.M. De


    An analysis of dynamic roughening and smoothening mechanisms of thin films grown with pulsed-dc magnetron sputtering is presented. The roughness evolution has been described by a linear stochastic equation, which contains the second- and fourth-order gradient terms. Dynamic smoothening of the growin

  15. Transitional flow in the wake of a moderate to large height cylindrical roughness element

    Plogmann, B.; Würz, W.; Krämer, E.


    The effect of an isolated, cylindrical roughness on the stability of an airfoil boundary layer has been studied based on particle image velocimetry and hot-wire anemometry. The investigated roughness elements range from a sub-critical to a super-critical behavior with regard to the critical roughness Reynolds number. For the sub-critical case, the nonlinear disturbance growth in the near wake is governed by oblique Tollmien-Schlichting (TS) type modes. Further downstream, these disturbance modes are, however, damped with the mean flow stabilization and no dominant modes persist in the far wake. By contrast, in the transitional configuration the disturbance growth is increased, but still associated with a TS-type instability in the near-wake centerline region of the low-aspect (height-to-diameter) ratio element. That is, the disturbances in the centerline region show a similar behavior as known for 2D elements, whereas in the outer spanwise domain a Kelvin-Helmholtz (KH) type, shear-layer instability is found, as previously reported for larger aspect ratio isolated elements. With increasing height and, thereby, aspect ratio of the roughness, the KH-type instability domain extends toward the centerline and, accordingly, the TS-type instability domain decreases. For high super-critical cases, transition is already triggered in the wall-normal and spanwise shear layers upstream and around the roughness. In the immediate wake, periodic shear-layer disturbances roll up into a—for isolated elements characteristic—shedding of vortices, which was not present at the lower roughness Reynolds number cases due to the decreased aspect ratio and, thereby, different instability mechanism.

  16. Contact angle hysteresis on randomly rough surfaces: a computational study.

    David, Robert; Neumann, A Wilhelm


    Wetting is important in many applications, and the solid surfaces being wet invariably feature some amount of surface roughness. A free energy-based computational simulation is used to study the effect of roughness on wetting and especially contact angle hysteresis. On randomly rough, self-affine surfaces, it is found that hysteresis depends primarily on the value of the Wenzel roughness parameter r, increasing in proportion with r - 1. Micrometer-level roughness causes hysteresis of a few degrees.

  17. Physically-based Ice Thickness and Surface Roughness Retrievals over Rough Deformed Sea Ice

    Li, Li; Gaiser, Peter; Allard, Richard; Posey, Pamela; Hebert, David; Richter-Menge, Jacqueline; Polashenski, Christopher; Claffey, Keran


    The observations of sea ice thickness and ice surface roughness are critical for our understanding of the state of the changing Arctic. Currently, the Radar and/or LiDAR data of sea ice freeboard are used to infer sea ice thickness via isostasy. The underlying assumption is that the LiDAR signal returns at the air/snow interface and radar signal at the snow/ice interface. The elevations of these interfaces are determined based on LiDAR/Radar return waveforms. However, the commonly used threshold-based surface detection techniques are empirical in nature and work well only over level/smooth sea ice. Rough sea ice surfaces can modify the return waveforms, resulting in significant Electromagnetic (EM) bias in the estimated surface elevations, and thus large errors in the ice thickness retrievals. To understand and quantify such sea ice surface roughness effects, a combined EM rough surface and volume scattering model was developed to simulate radar returns from the rough sea ice 'layer cake' structure. A waveform matching technique was also developed to fit observed waveforms to a physically-based waveform model and subsequently correct the roughness induced EM bias in the estimated freeboard. This new EM Bias Corrected (EMBC) algorithm was able to better retrieve surface elevations and estimate the surface roughness parameter simultaneously. Both the ice thickness and surface roughness retrievals are validated using in-situ data. For the surface roughness retrievals, we applied this EMBC algorithm to co-incident LiDAR/Radar measurements collected during a Cryosat-2 under-flight by the NASA IceBridge missions. Results show that not only does the waveform model fit very well to the measured radar waveform, but also the roughness parameters derived independently from the LiDAR and radar data agree very well for both level and deformed sea ice. For sea ice thickness retrievals, validation based on in-situ data from the coordinated CRREL/NRL field campaign demonstrates

  18. Reynolds number and roughness effects on turbulent stresses in sandpaper roughness boundary layers

    Morrill-Winter, C.; Squire, D. T.; Klewicki, J. C.; Hutchins, N.; Schultz, M. P.; Marusic, I.


    Multicomponent turbulence measurements in rough-wall boundary layers are presented and compared to smooth-wall data over a large friction Reynolds number range (δ+). The rough-wall experiments used the same continuous sandpaper sheet as in the study of Squire et al. [J. Fluid Mech. 795, 210 (2016), 10.1017/jfm.2016.196]. To the authors' knowledge, the present measurements are unique in that they cover nearly an order of magnitude in Reynolds number (δ+≃2800 -17 400 ), while spanning the transitionally to fully rough regimes (equivalent sand-grain-roughness range, ks+≃37 -98 ), and in doing so also maintain very good spatial resolution. Distinct from previous studies, the inner-normalized wall-normal velocity variances, w2¯, exhibit clear dependencies on both ks+ and δ+ well into the wake region of the boundary layer, and only for fully rough flows does the outer portion of the profile agree with that in a comparable δ+ smooth-wall flow. Consistent with the mean dynamical constraints, the inner-normalized Reynolds shear stress profiles in the rough-wall flows are qualitatively similar to their smooth-wall counterparts. Quantitatively, however, at matched Reynolds numbers the peaks in the rough-wall Reynolds shear stress profiles are uniformly located at greater inner-normalized wall-normal positions. The Reynolds stress correlation coefficient, Ru w, is also greater in rough-wall flows at a matched Reynolds number. As in smooth-wall flows, Ru w decreases with Reynolds number, but at different rates depending on the roughness condition. Despite the clear variations in the Ru w profiles with roughness, inertial layer u , w cospectra evidence invariance with ks+ when normalized with the distance from the wall. Comparison of the normalized contributions to the Reynolds stress from the second quadrant (Q2) and fourth quadrant (Q4) exhibit noticeable differences between the smooth- and rough-wall flows. The overall time fraction spent in each quadrant is, however

  19. Roughness Length of Water Vapor over Land Surfaces and Its Influence on Latent Heat Flux

    Sang-Jong Park


    Full Text Available Latent heat flux at the surface is largely dependent on the roughness length for water vapor (z0q. The determination of z0q is still uncertain because of its multifaceted characteristics of surface properties, atmospheric conditions and insufficient observations. In this study, observed values from the Fluxes Over Snow Surface II field experiment (FLOSS-II from November 2002 to March 2003 were utilized to estimate z0q over various land surfaces: bare soil, snow, and senescent grass. The present results indicate that the estimated z0q over bare soil is much smaller than the roughness length of momentum (z0m; thus, the ratio z0m/z0q is larger than those of previous studies by a factor of 20 - 150 for the available flow regime of the roughness Reynolds number, Re* > 0.1. On the snow surface, the ratio is comparable to a previous estimation for the rough flow (Re* > 1, but smaller by a factor of 10 - 50 as the flow became smooth (Re* < 1. Using the estimated ratio, an optimal regression equation of z0m/z0q is determined as a function of Re* for each surface type. The present parameterization of the ratio is found to greatly reduce biases of latent heat flux estimation compared with that estimated by the conventional method, suggesting the usefulness of current parameterization for numerical modeling.

  20. The Effect of Surface Roughness on Thermohydrodynamic Performance in Misaligned Journal Bearings

    Mustafa Mohammed K.


    Full Text Available In this work an approach has been developed to investigate the influence of surface roughness on thermohydrodynamic performance in aligned and misaligned journal bearings by considering an average flow model and deriving the shear flow factor for various roughness configurations, similar to the pressure flow factor. An average Reynolds equation for rough surfaces is defined in term of pressure and shear flow factors, which can be obtained by numerical flow simulation, though the use of measured or numerically generated rough surfaces. Reynolds, heat conduction and energy equations are solved simultaneously by using a suitable numerical technique (Finite Difference Method to obtain the pressure and temperature distribution through the oil film thickness of the journal bearing. These equations are obtained for isotropic surfaces and for surfaces with directional patterns. The flow factors for these surfaces are expressed as empirical relations in term of normalized oil film thickness (h/σ and surface characteristic (γ defined as the ratio of x and z correlation lengths . The results of this approach showed increase in load carrying capacity and maximum pressure and decrease in maximum temperature in the case of stationary surface roughness (rough bearing and smooth journal with transverse pattern. The results obtained through this work have been compared with that published by other works and found to be in a good agreement.

  1. Contact ratio and deformation of asperity in nano-partia lubrication


    Partial lubrication or mixed lubrication in the nano-scale is discussed, which is consti-tuted from dry contact, boundary lubrication, thin film lubrication. A dynamic contact ratio has beenused to describe such lubrication, and the relationship between the contact ratio and its influencefactors was investigated. Experimental results indicate that the dynamic contact ratio increaseswith the decrease of film thickness by the exponential function. The decrease of speed and lubri-cant viscosity, and the increase of loads will enlarge the value of the contact ratio. When the polaradditives are added into the basic oil, the contact ratio decreases. In addition, the contact ratio ofthe surfaces with small roughness is larger than that of the surfaces with large roughness at verylow speed. However, the contact ratio of smooth surfaces decreases more quickly with speed thanthat of rough surfaces, and therefore, it will become smaller than that of rough surfaces after speedincreases over a certain degree.

  2. [Nasal submicron emulsion of Scutellariae Radix extract preparation technology research based on phase transfer of solute technology].

    Shi, Ya-jun; Shi, Jun-hui; Chen, Shi-bin; Yang, Ming


    Based on the demand of nasal drug delivery high drug loadings, using the unique phase transfer of solute, integrating the phospholipid complex preparation and submicron emulsion molding process of Scutellariae Radix extract, the study obtained the preparation of the high drug loadings submicron emulsion of Scutellariae Radix extract. In the study of drug solution dispersion method, the uniformity of drug dispersed as the evaluation index, the traditional mixing method, grinding, homogenate and solute phase transfer technology were investigated, and the solute phase transfer technology was adopted in the last. With the adoption of new technology, the drug loading capacity reached 1.33% (phospholipid complex was 4%). The drug loading capacity was improved significantly. The transfer of solute method and timing were studied as follows,join the oil phase when the volume of phospholipid complex anhydrous ethanol solution remaining 30%, the solute phase transfer was completed with the continued recycling of anhydrous ethanol. After drug dissolved away to oil phase, the preparation technology of colostrum was determined with the evaluation index of emulsion droplet form. The particle size of submicron emulsion, PDI and stability parameters were used as evaluation index, orthogonal methodology were adopted to optimize the submicron emulsion ingredient and main influential factors of high pressure homogenization technology. The optimized preparation technology of Scutellariae Radix extract nasal submicron emulsion is practical and stable.

  3. 函数粗集生成的粗积分%Rough Integrals Generated by Function Rough Sets

    于秀清; 徐凤生


    The concepts of the lower approximation integral, the upper approximation integral and rough integrals are given on the basis of function rough sets. Based on these concepts, the relation of the lower approximation integrals, the relation of the upper approximation integrals, the relation of rough integrals, and the double median theorem of rough integrals are discussed. Rough integrals have finite contraction characteristic and finite extension characteristic.

  4. A case study on relation between roughness, lubrication and fatigue life of rolling bearings

    Balan, M. R.; Tufescu, A.; Cretu, S. S.


    A spherical roller bearing under high radial loading, constant speed and imposed roughness for the contacting surfaces was chosen as case study. Different lubrication regimes were obtained by varying oil viscosity through the operating temperature. For bearings with especially machined contacting surfaces, λ-ratio is firstly determined and its value is used to estimate the particular value of the lubrication parameter κ. Using the λ-ratio approach the paper reveals the relationship between roughness amplitude and the modified rating life of rolling bearings. The roughness values corresponding to good manufacturing practice are possible to be determined for each particular case. Three groups of random Gaussian roughness were generated with the same values for the Ra parameter as used in the modified lives investigations. For medium and especially high radial loads, the contacts between rough surfaces develop, inside the shallow layer, von Mises equivalent stresses higher than the fatigue limit stress. For condition of lack of lubricant or starved lubrication, these findings explain the initiation of the rolling contact fatigue in the shallow layer, close to contacting surfaces.

  5. Sub-micron Cu/SSZ-13: Synthesis and application as selective catalytic reduction (SCR) catalysts

    Prodinger, Sebastian; Derewinski, Miroslaw A.; Wang, Yilin; Washton, Nancy M.; Walter, Eric D.; Szanyi, János; Gao, Feng; Wang, Yong; Peden, Charles H. F.


    For the first time, sub-micron Cu/SSZ-13, obtained by modifying an existing synthesis procedure, was shown to be an effective and stable catalyst for selective catalytic reduction reactions, such as NO reduction. Characterization of the materials with X-ray diffraction, N2-physisorption and 27Al MAS NMR shows that hydrothermal aging, simulating SCR reaction conditions, is more destructive in respect to dealumination for smaller particles prior to Cu-exchange. However, the catalytic performance and hydrothermal stability for Cu/SSZ-13 is independent of the particle size. In particular, the stability of tetrahedral framework Al is improved in the sub-micron Cu/SSZ-13 catalysts of comparable Cu loading. This indicates that variations in the Al distribution for different SSZ-13 synthesis procedures have a more critical influence on stabilizing isolated Cu-ions during harsh hydrothermal aging than the particle size. This study is of high interest for applications in vehicular DeNOx technologies where high loadings of active species on wash coats can be achieved by using sub-micron Cu/SSZ-13. The authors would like to thank B. W. Arey and J. J. Ditto for performing electron microscope imaging. The authors gratefully acknowledge the US Department of Energy (DOE), Energy Efficiency and Renewable Energy, Vehicle Technologies Office for the support of this work. S. P and M. A. D also acknowledge support by the Materials Synthesis and Simulation Across Scales (MS3 Initiative) conducted under the Laboratory Directed Research & Development Program at PNNL. The research described in this paper was performed in the Environmental Molecular Sciences Laboratory (EMSL), a national scientific user facility sponsored by the DOE’s Office of Biological and Environmental Research and located at Pacific Northwest National Laboratory (PNNL). PNNL is operated for the US DOE by Battelle.

  6. Velocity overshoot decay mechanisms in compound semiconductor field-effect transistors with a submicron characteristic length

    Jang Jyegal


    Full Text Available Velocity overshoot is a critically important nonstationary effect utilized for the enhanced performance of submicron field-effect devices fabricated with high-electron-mobility compound semiconductors. However, the physical mechanisms of velocity overshoot decay dynamics in the devices are not known in detail. Therefore, a numerical analysis is conducted typically for a submicron GaAs metal-semiconductor field-effect transistor in order to elucidate the physical mechanisms. It is found that there exist three different mechanisms, depending on device bias conditions. Specifically, at large drain biases corresponding to the saturation drain current (dc region, the velocity overshoot suddenly begins to drop very sensitively due to the onset of a rapid decrease of the momentum relaxation time, not the mobility, arising from the effect of velocity-randomizing intervalley scattering. It then continues to drop rapidly and decays completely by severe mobility reduction due to intervalley scattering. On the other hand, at small drain biases corresponding to the linear dc region, the velocity overshoot suddenly begins to drop very sensitively due to the onset of a rapid increase of thermal energy diffusion by electrons in the channel of the gate. It then continues to drop rapidly for a certain channel distance due to the increasing thermal energy diffusion effect, and later completely decays by a sharply decreasing electric field. Moreover, at drain biases close to a dc saturation voltage, the mechanism is a mixture of the above two bias conditions. It is suggested that a large secondary-valley energy separation is essential to increase the performance of submicron devices.

  7. Submicron Schottky-gate field-effect transistors - a new elemental base for microwave integrated microcircuits

    Tolstoi, A.I.; Petrov, G.V.; Batura, V.G.; Bosyi, V.I.


    The authors analyze the present level of development of submicron semiconducting devices in order to systematize the available information, point out existing problems, and provide a foundation for methods for avoiding these problems. The authors specify the following methods: (1) structural - decreasing the dimensions of the active regions should further increase the limiting frequencies, decrease the noise factor, and increase the gain; (2) choice of semiconducting material - the use of semiconductors with higher charge-carrier mobility will improve the limiting frequencies, gain, and noise factor and affect the choice of structure of the semiconducting device.

  8. Two-photon laser fabrication of three-dimensional silver microstructures with submicron scale linewidth

    Tsutsumi, Naoto; Nagata, Kazuya; Sakai, Wataru [Kyoto Institute of Technology, Department of Macromolecular Science and Engineering, Graduate School of Science and Technology, Kyoto (Japan)


    We show three-dimensional silver microstructures with a submicron scale linewidth fabricated via two-photon photoreduction of silver ions in a poly(N-vinylpyrrolidone) (PVP) matrix. Femtosecond laser at 508 nm directly excites the carbonyl group of PVP via two-photon excitation to reduce silver ions. Lone pair electrons in PVP stabilized silver ions and lower molecular weight of PVP prevented silver clusters growing larger. The effect of molecular weight of PVP on linewidth of silver nanowire is investigated. (orig.)

  9. Infiltration techniques for suppressing grain growth during the densification of submicron and nanophase alumina composites

    Vernon, Deborah Marshall

    Grain growth control during the final stages of densification is an issue with extreme technological significance. In the last decade, nanophase ceramic starting powders have become commercially available, and in order to take full advantage of the unique properties nanophase ceramics potentially offer, grain growth control during processing of these materials must be addressed. In this research study the author addresses the topic of suppression of grain growth in submicron and nanophase alumina using novel processing techniques. The approach used to decrease grain boundary motion during processing involves the addition of an intermediate step between initial powder pressing and sintering. During the intermediate step either solute amounts of an infiltrant are incorporated along grain boundary junctions through a vapor-phase technique or, second phase inclusions are formed within the pore structure of the ceramic porous compacts via a liquid-phase technique. Using the vapor-phase technique, silicon nitride was introduced into porous submicron and nanophase alumina compacts. It was determined that silicon nitride in amounts below the solubility limit is an effective grain growth inhibitor. In the submicron pellets studies, three regions of grain growth were observed: abnormal, suppressed, and normal. Using a mathematical model developed for simulating the vapor infiltration process, a range of silicon concentrations (70 to 50 ppm) was determined to correspond to the suppressed grain growth region. In the nanophase silicon nitride infiltrated pellets, suppression of grain growth was observed throughout the infiltrated specimen, however the suppression effects were not great enough to retain the nanosized nature of the alumina grains. Using the liquid-phase technique, zirconia particles were formed within the pore structure of submicron and nanophase alumina compacts. A comparison between suppression effects in compacts created by liquid-phase and by powder

  10. Phase Evolution during the Sintering of Submicron Ti(C,N)-Based Cermets


    The submicron powder mixtures of TiC-TiN-WC-Mo-C-Ni sintered at 1400℃ or below in vacuum were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) analyses. The results showed that Mo2C formed at 800℃ or below. Both WC and Mo2C disappeared at 1200℃, and TiN disappeared at 1250℃. In addition, the variations of lattice constants of the titanium carbonitride and nickel binder phase with sintering temperature were experimentally obtained, and the reason was analyzed.

  11. Infrared Luminescent Properties of a Pr-Doped KBr Submicron Rod

    WEI Feng-Wei; ZHANG Xiao-Song; LI Lan; XU Jian-Ping; ZHOU Yong-Liang; LIU Pei


    KBr:Pr with a submicron rod structure is successfully synthesized by a solid-state reaction using absolute alcohol as the abrasive. X-ray diffraction,scanning electron microscopy,photoluminescence spectra and fluorescence decay curves are used to characterize the resulting materials.The influences of Pr3+ dopant concentration on the luminescence and lifetime are discussed.Furthermore,luminescent measurements show that KBr:Pr has a high emission intensity compared with other Pr-doped matrixes,which is related to the low phonon energy of KBr.The results suggest that the phonon energy of the host is important in determining the luminescent efficiency.

  12. Novel deep—submicron x—ray lithography process for T—shaped gate patterns

    XieChangqing; YiFuting; 等


    The growing interest in the use of Gallium Arsenids semiconductor materials has presented many opportunities for device operational speed improvements but has also presented many problems for the device maker,A novel deep-submicron x-ray lithography process for T-shaped gate patterns useful for high-electron-mobility transistors(HEMT) is introduced in this work.In the fabrication of T-shaped gate a therr layer resists method is used.The x-ray exposure experiments were finished by Beijing Synchrotron Radiation Facility(BSRF) 3B1A beamline,and good result has been obtained.

  13. Measurement of focusing properties for high numerical aperture optics using an automated submicron beamprofiler

    Chapman, J J; Streed, E W; Kielpinski, D


    The focusing properties of three aspheric lenses with numerical aperture (NA) between 0.53 and 0.68 were directly measured using an interferometrically referenced scanning knife-edge beam profiler with sub-micron resolution. The results obtained for two of the three lenses tested were in agreement with paraxial gaussian beam theory. It was also found that the highest NA aspheric lens which was designed for 830nm was not diffraction limited at 633nm. This process was automated using motorized translation stages and provides a direct method for testing the design specifications of high numerical aperture optics.

  14. Diazepam submicron emulsions containing soya-bean oil and intended for oral or rectal delivery.

    Gajewska, M; Sznitowska, M; Janicki, S


    Physically stable diazepam submicron emulsions were prepared using soya-bean oil. Diazepam concentration 4 mg/ml, suitable for rectal or oral delivery, was achieved in 20% emulsions. Mixture of egg lecithin (1.2%) and poloxamer (2.0%) has been chosen as the most suitable emulsifying agent. Composition of the emulsion may be supplemented with alpha-tocopherol and parabens. However, the system was not stable when either phenylethanol or chlorhexidine gluconate was added. Taste masking agents commonly used as food additives decreased stability of the preparation and were not efficient in elimination of a bitter taste of the drug-loaded emulsions.

  15. Analysis and Design of Monolithic Inductors in Sub-micron CMOS

    Fallesen, Carsten; Jørgensen, Allan


    In the last few years the CMOS processes have gone into deep sub-micron channel lengths. This means that it is now possible to make GHz applications in CMOS. In analog GHz applications it is often necessary to have access to inductors. This report describes the development of a physical model...... for optimization. To verify the model more than 40 inductors have been produced and their performance have been measured. The produced inductors sweep a number of design parameters of the inductors, in order to get a realistic dataset. The produced inductors have inductances values of 2 nH to 10 nH, resonance...

  16. Methodology of Efficient Energy Design for Noisy Deep Submicron VLSI Chips



    Power dissipation is becoming increasingly important as technology continues to scale. This paper describes a way to consider the dynamic, static and shortcircuit power dissipation simultaneously for making complete, quantitative prediction on the total power dissipation of noisy VLSI chip. Especially, this new method elucidates the mechanism of power dissipation caused by the intrinsic noise of deep submicron VLSI chip. To capture the noise dependency of efficient energy design strategies for VLSI chip, the simulation of two illustrative cases are observed. Finally, the future works are proposed for the optimum tradeoff among the power, speed and area, which includes the use of floating-body partially depleted silicon-on-insulator CMOS technology.

  17. Suppression of transient enhanced diffusion in sub-micron patterned silicon template by dislocation loops formation

    Hu, Kuan-Kan; Chang, Ruey-Dar; Woon, Wei Yen


    We investigate the evolution of two dimensional transient enhanced diffusion (TED) of phosphorus in sub-micron scale patterned silicon template. Samples doped with low dose phosphorus with and without high dose silicon self-implantation, were annealed for various durations. Dopant diffusion is probed with plane-view scanning capacitance microscopy. The measurement revealed two phases of TED. Significant suppression in the second phase TED is observed for samples with high dose self-implantation. Transmission electron microscopy suggests the suppressed TED is related to the evolution of end of range defect formed around ion implantation sidewalls.

  18. Suppression of transient enhanced diffusion in sub-micron patterned silicon template by dislocation loops formation

    Hu, Kuan-Kan; Woon, Wei Yen [Department of Physics, National Central University, Jungli, 32054, Taiwan (China); Chang, Ruey-Dar [Chang Gung University, Taoyuan, Taiwan 33302 (China)


    We investigate the evolution of two dimensional transient enhanced diffusion (TED) of phosphorus in sub-micron scale patterned silicon template. Samples doped with low dose phosphorus with and without high dose silicon self-implantation, were annealed for various durations. Dopant diffusion is probed with plane-view scanning capacitance microscopy. The measurement revealed two phases of TED. Significant suppression in the second phase TED is observed for samples with high dose self-implantation. Transmission electron microscopy suggests the suppressed TED is related to the evolution of end of range defect formed around ion implantation sidewalls.

  19. Suppression of transient enhanced diffusion in sub-micron patterned silicon template by dislocation loops formation

    Kuan-Kan Hu


    Full Text Available We investigate the evolution of two dimensional transient enhanced diffusion (TED of phosphorus in sub-micron scale patterned silicon template. Samples doped with low dose phosphorus with and without high dose silicon self-implantation, were annealed for various durations. Dopant diffusion is probed with plane-view scanning capacitance microscopy. The measurement revealed two phases of TED. Significant suppression in the second phase TED is observed for samples with high dose self-implantation. Transmission electron microscopy suggests the suppressed TED is related to the evolution of end of range defect formed around ion implantation sidewalls.

  20. Submicron-scale manipulation of phase separation in organic solar cells

    Chen, Fang-Chung; Lin, Yi-Kai; Ko, Chu-Jung


    This paper describes a method for controlling the submicron-scale phase separation of poly(3-hexylthiophene) and (6,6)-phenyl-C61-butyric acid methyl ester in organic solar cells. Using microcontact printing of self-assembled monolayers on the device buffer layer to divide the surface into two regimes having different surface energies, an interdigitated structure aligned vertical to the substrate surface is achieved after spontaneous surface-directed phase separation. The power conversion efficiency increases upon decreasing the grating spacing, reaching 2.47%. The hole mobility increased as a consequence of improved polymer chain ordering, resulting in higher device efficiency, while smaller pattern sizes were used.

  1. IR Drop Analysis and Its Reduction Techniques in Deep Submicron Technology

    Vanpreet Kaur


    Full Text Available This paper presents a detailed conceptual analysis of IR Drop effect in deep submicron technologies and its reduction techniques. The IR Drop effect in power/ground network increases rapidly with technology scaling. This affects the timing of the design and hence the desired speed. It is shown that in present day designs, using well known reduction techniques such as wire sizing and decoupling capacitor insertion, may not be sufficient to limit the voltage fluctuations and hence, two more important methods such as selective glitch reduction technique and IR Drop reduction through combinational circuit partitioning are discussed and the issues related to all the techniques are revised.

  2. Tactile perception of the roughness of the end of a tool: what role does tool handle roughness play?

    Zampini, Massimiliano; Mawhinney, Sara; Spence, Charles


    We investigated whether the perceived roughness of the end of a tool is influenced by the texture of the handle used to hold it. Participants rated the roughness of the ends (caps) of a series of tools by rubbing them along their forearm, and indicated the perceived roughness of the tool's cap by means of an anchored visual scale. The caps of the tools had one of eight different levels of roughness varying from very smooth (sample 1) to very rough (sample 8). The participants held the tool handle in one hand while rubbing the cap of the tool against their contralateral forearm. The tool handle was either smooth (similar in smoothness to sample 1) or else very rough (matched in roughness to sample 8). Overall, participants were remarkably good at ignoring the roughness of the tool's handle when discriminating the roughness of the tool's cap. Nevertheless, the roughness of the tool handle was shown to modulate roughness judgments concerning the tool cap under certain conditions: in particular, tool caps at the rougher end of the scale (6 and 7) were rated as being significantly less rough when the participants held tools with a rough handle than when they held tools with a smooth handle. Our results therefore demonstrate a small but significant effect of the roughness of the handle of a tool on the perceived roughness of its cap.

  3. Minimal axiom group of similarity-based rough set model

    DAI Jian-hua; PAN Yun-he


    Rough set axiomatization is one aspect of rough set study to characterize rough set theory using dependable and minimal axiom groups.Thus,rough set theory can be studied by logic and axiom system methods.The classical rough set theory is based on equivalence relation,but the rough set theory based on similarity relation has wide applications in the real world.To characterize similarity-based rough set theory,an axiom group named S,consisting of 3 axioms,is proposed.The reliability of the axiom group,which shows that characterizing of rough set theory based on similarity relation is rational,is proved.Simultaneously,the minimization of the axiom group,which requests that each axiom is an equation and independent,is proved.The axiom group is helpful to research rough set theory by logic and axiom system methods.

  4. Effects of confinement & surface roughness in electrorheological flows

    Helal, Ahmed; Telleria, Maria J.; Wang, Julie; Strauss, Marc; Murphy, Mike; McKinley, Gareth; Hosoi, A. E.


    Electrorheological (ER) fluids are dielectric suspensions that exhibit a fast, reversible change in rheological properties with the application of an external electric field. Upon the application of the electric field, the material develops a field-dependent yield stress that is typically modeled using a Bingham plastic model. ER fluids are promising for designing small, cheap and rapidly actuated hydraulic devices such as rapidly-switchable valves, where fluid flowing in a microchannel can be arrested by applying an external electric field. In the lubrication limit, for a Bingham plastic fluid, the maximum pressure the channel can hold, before yielding, is a function of the field-dependent yield stress, the length of the channel and the electrode gap. In practice, the finite width of the channel and the surface roughness of the electrodes could affect the maximum yield pressure but a quantitative understanding of these effects is currently lacking. In this study, we experimentally investigate the effects of the channel aspect ratio (width/height) and the effects of electrode roughness on the performance of ER valves. Based on this quantitative analysis, we formulate new performance metrics for ER valves as well as design rules for ER valves that will help guide and optimize future designs.

  5. Deposition of toxic metal particles on rough nanofiltration membranes

    Agboola, Oluranti; Maree, Jannie; Mbaya, Richard; Zvinowanda, Caliphs Musa [Tshwane University of Technology, Pretoria (South Africa); Molelekwa, Gomotsegang Fred; Jullok, Nora; Bruggen, Bart Van der; Volodine, Alexander; Haesendonck, Chris Van [KU Leuven, Heverlee (Belgium)


    Two nanofiltration (NF90 and Nano-Pro-3012) membranes were investigated for their capacity to remove metal ions. This study presents the effect of membrane roughness on the removal of toxic metal ions during dead end membrane filtration. Atomic force microscopy, scanning electron microscopy, WSXM software and ImageJ were used to characterize the roughness of the membranes. Gradual decrease in filtration permeate flux was observed as foulants accumulated at the interface of the membranes; filtration permeate flux varied from 20 L/m{sup 2}/h to 14 L/m{sup 2}/h and 11 L/ m{sup 2}/h to 6 L/m{sup 2}/h for NF90 and Nano-Pro-3012, respectively. NF90 membrane was more prone to fouling than the Nano-Pro-3012 membrane: the percentage flux reduction was higher for NF90 (3.6%) than Nano-Pro-3012 (0.98%). The bearing ratio of the fouled NF90 exhibited a high peak of 7.09 nm than the fouled Nano-Pro-3012 with the peak of 6.8 nm.

  6. Replicated mask surface roughness effects on EUV lithographic pattering and line edge roughness

    George, Simi A.; Naulleau, Patrick P.; Gullikson, Eric M.; Mochi, Iacopo; Salmassi, Farhad; Goldberg, Kenneth A.; Anderson, Erik H.


    To quantify the roughness contributions to speckle, a programmed roughness substrate was fabricated with a number of areas having different roughness magnitudes. The substrate was then multilayer coated. Atomic force microscopy (AFM) surface maps were collected before and after multilayer deposition. At-wavelength reflectance and total integrated scattering measurements were also completed. Angle resolved scattering based power spectral densities are directly compared to the AFM based power spectra. We show that AFM overpredicts the roughness in the picometer measurements range. The mask was then imaged at-wavelength for the direct characterization of the aerial image speckle using the SEMATECH Berkeley Actinic Inspection Tool (AIT). Modeling was used to test the effectiveness of the different metrologies in predicting the measured aerial-image speckle. AIT measured contrast values are 25% or more than the calculated image contrast values obtained using the measured rms roughness input. The extent to which the various metrologies can be utilized for specifying tolerable roughness limits on EUV masks is still to be determined. Further modeling and measurements are being planned.

  7. Rough primes and rough conversations: evidence for a modality-specific basis to mental metaphors.

    Schaefer, Michael; Denke, Claudia; Heinze, Hans-Jochen; Rotte, Michael


    How does our brain organize knowledge? Traditional theories assume that our knowledge is represented abstractly in an amodal conceptual network of formal logic symbols. The theory of embodied cognition challenges this view and argues that conceptual representations that constitute our knowledge are grounded in sensory and motor experiences. We tested this hypothesis by examining how the concept of social coordination is grounded metaphorically in the tactile sensation of roughness. Participants experienced rough or smooth touch before being asked to judge an ambiguous social interaction. Results revealed that rough touch made social interactions appear more difficult and adversarial, consistent with the rough metaphor. This impact of tactile cues on social impressions was accompanied by a network including primary and secondary somatosensory cortices, amygdala, hippocampus and inferior prefrontal cortex. Thus, the roughness of tactile stimulation affected metaphor-relevant (but not metaphor-irrelevant) behavioral and neural responses. Receiving touch from a rough object seems to trigger the application of associated ontological concepts (or scaffolds) even for unrelated people and situations (but not to unrelated or more general feelings). Since this priming was based on somatosensory brain areas, our results provide support for the theory that sensorimotor grounding is intrinsic to cognitive processes.

  8. Comparison of aerodynamically and model-derived roughness lengths (zo) over diverse surfaces, central Mojave Desert, California, USA

    MacKinnon, D.J.; Clow, G.D.; Tigges, R.K.; Reynolds, R.L.; Chavez, P.S.


    The vulnerability of dryland surfaces to wind erosion depends importantly on the absence or the presence and character of surface roughness elements, such as plants, clasts, and topographic irregularities that diminish wind speed near the surface. A model for the friction velocity ratio has been developed to account for wind sheltering by many different types of co-existing roughness elements. Such conditions typify a monitored area in the central Mojave Desert, California, that experiences frequent sand movement and dust emission. Two additional models are used to convert the friction velocity ratio to the surface roughness length (zo) for momentum. To calculate roughness lengths from these models, measurements were made at 11 sites within the monitored area to characterize the surface roughness element. Measurements included (1) the number of roughness species (e.g., plants, small-scale topography, clasts), and their associated heights and widths, (2) spacing among species, and (3) vegetation porosity (a measurement of the spatial distribution of woody elements of a plant). Documented or estimated values of drag coefficients for different species were included in the modeling. At these sites, wind-speed profiles were measured during periods of neutral atmospheric stability using three 9-m towers with three or four calibrated anemometers on each. Modeled roughness lengths show a close correspondence (correlation coefficient, 0.84-0.86) to the aerodynamically determined values at the field sites. The geometric properties of the roughness elements in the model are amenable to measurement at much higher temporal and spatial resolutions using remote-sensing techniques than can be accomplished through laborious ground-based methods. A remote-sensing approach to acquire values of the modeled roughness length is particularly important for the development of linked surface/atmosphere wind-erosion models sensitive to climate variability and land-use changes in areas such

  9. Five-axis rough machining for impellers

    Ruolong QI; Weijun LIU; Hongyou BIAN; Lun LI


    The most important components used in aero-space, ships, and automobiles are designed with free form surfaces. An impeller is one of the most important components that is difficult to machine because of its twisted blades. Rough machining is recognized as the most crucial procedure influencing machining efficiency and is critical for the finishing process. An integrated rough machining course with detailed algorithms is presented in this paper. An algorithm for determining the minimum distance between two surfaces is applied to estimate the tool size. The space between two blades that will be cleared from the roughcast is divided to generate CC points. The tool axis vector is confirmed based on flank milling using a simple method that could eliminate global interference between the tool and the blades. The result proves that the machining methodology presented in this paper is useful and successful.

  10. Generalized rough sets hybrid structure and applications

    Mukherjee, Anjan


    The book introduces the concept of “generalized interval valued intuitionistic fuzzy soft sets”. It presents the basic properties of these sets and also, investigates an application of generalized interval valued intuitionistic fuzzy soft sets in decision making with respect to interval of degree of preference. The concept of “interval valued intuitionistic fuzzy soft rough sets” is discussed and interval valued intuitionistic fuzzy soft rough set based multi criteria group decision making scheme is presented, which refines the primary evaluation of the whole expert group and enables us to select the optimal object in a most reliable manner. The book also details concept of interval valued intuitionistic fuzzy sets of type 2. It presents the basic properties of these sets. The book also introduces the concept of “interval valued intuitionistic fuzzy soft topological space (IVIFS topological space)” together with intuitionistic fuzzy soft open sets (IVIFS open sets) and intuitionistic fuzzy soft cl...

  11. Fractai Estimation of Joint Roughness Coefficients

    谢和平; Willian G.Pariseau


    Based on the triadic Koch curve,a generalized fractal model of joint profiles is establishedto simulate joint roughness.The fractal dimension of a joint profile can be directly obtained from the two pa-rameters,L~* and h~*, the average base length and average height of asperities of the joint,respectively,i,e D=log4/log[2(1+cos tan~1(2h’/L’))]This fractal dimension is strongly correlated with the value of the joint roughness coefficient (JRC). An empirical relationship is found in the form,JRC=85.2671·(D-1)~0.5679 Thus, the fractal analysis proposed provides a new method of estimating JRC values

  12. Roughly isometric minimal immersions into Riemannian manifolds

    Markvorsen, Steen

    A given metric (length-) space $X$ (whether compact or not) is roughly isometric to any one of its Kanai graphs $G$, which in turn can be {\\em{geometrized}} by considering each edge of $G$ as a 1-dimensional manifold with an associated metric $g$ giving the 'correct' length of the edge. In this t......A given metric (length-) space $X$ (whether compact or not) is roughly isometric to any one of its Kanai graphs $G$, which in turn can be {\\em{geometrized}} by considering each edge of $G$ as a 1-dimensional manifold with an associated metric $g$ giving the 'correct' length of the edge....... In this talk we will mainly be concerned with {\\em{minimal}} isometric immersions of such geometrized approximations $(G, g)$ of $X$ into Riemannian manifolds $N$ with bounded curvature. When such an immersion exists, we will call it an $X$-web in $N$. Such webs admit a natural 'geometric' extension...

  13. Anisotropy and roughness of the solid-liquid interface of BCC Fe.

    Sun, Yongli; Wu, Yongquan; Lu, Xiuming; Li, Rong; Xiao, Junjiang


    Melting point T m and kinetic coefficient μ (a proportional constant between the interfacial velocity ν and undercooling ΔT), along with the structural roughness of the solid-liquid interface for body centered cubic (BCC) Fe were calculated by molecular dynamics (MD) simulation. All simulations applied the Sutton-Chen potential, and adopted average bond orientational order (ABOO) parameters together with Voronoi polyhedron method to characterize atomic structure and calculate atomic volume. Anisotropy of T m was found through about 20~40 K decreasing from [100] to [110] and continuously to [111]. Anisotropy of μ with three low index orientations was found as: μ s,[100] > > μ s,[110] > μ s,[111] for solidifying process and μ m,[100] > > μ m,[111] > μ m,[110] for melting process. Slight asymmetry between melting and solidifying was discovered from that the ratios of μ m/μ s are all slightly larger than 1. To explain these, interfacial roughness R int and area ratio S/S 0 (ratio of realistic interfacial area S and the ideal flat cross-sectional area S 0) were defined to verify the anisotropy of interfacial roughness under different supercoolings/superheatings. The results indicated interfacial roughness anisotropies were approximately [100] > [111] > [110]; the interface in melting process is rougher than that in solidifying process; asymmetry of interfacial roughness was larger when temperature deviation ΔT was larger. Anisotropy and asymmetry of interfacial roughness fitted the case of kinetic coefficient μ very well, which could give some explanations to the anisotropies of T m and μ.

  14. Source apportionment of submicron organic aerosols at an urban site by linear unmixing of aerosol mass spectra

    V. A. Lanz


    Full Text Available Submicron ambient aerosol was characterized in summer 2005 at an urban background site in Zurich, Switzerland, during a three-week measurement campaign. Highly time-resolved samples of non-refractory aerosol components were analyzed with an Aerodyne aerosol mass spectrometer (AMS. Positive matrix factorization (PMF was used for the first time for AMS data to identify the main components of the total organic aerosol and their sources. The PMF retrieved factors were compared to measured reference mass spectra and were correlated with tracer species of the aerosol and gas phase measurements from collocated instruments. Six factors were found to explain virtually all variance in the data and could be assigned either to sources or to aerosol components such as oxygenated organic aerosol (OOA. Our analysis suggests that at the measurement site only a small (<10% fraction of organic PM1 originates from freshly emitted fossil fuel combustion. Other primary sources identified to be of similar or even higher importance are charbroiling (10–15% and wood burning (~10%, along with a minor source interpreted to be influenced by food cooking (6%. The fraction of all identified primary sources is considered as primary organic aerosol (POA. This interpretation is supported by calculated ratios of the modelled POA and measured primary pollutants such as elemental carbon (EC, NOx, and CO, which are in good agreement to literature values. A high fraction (60–69% of the measured organic aerosol mass is OOA which is interpreted mostly as secondary organic aerosol (SOA. This oxygenated organic aerosol can be separated into a highly aged fraction, OOA I, (40–50% with low volatility and a mass spectrum similar to fulvic acid, and a more volatile and probably less processed fraction, OOA II (on average 20%. This is the first publication of a multiple component analysis technique to AMS organic spectral data and also the first report of the

  15. Integrability Estimates for Gaussian Rough Differential Equations

    Cass, Thomas; Lyons, Terry


    We derive explicit tail-estimates for the Jacobian of the solution flow of stochastic differential equations driven by Gaussian rough paths. In particular, we deduce that the Jacobian has finite moments of all order for a wide class of Gaussian process including fractional Brownian motion with Hurst parameter H>1/4. We remark on the relevance of such estimates to a number of significant open problems.

  16. Hydrodynamic Noise from Flexible Roughness Elements


    approach. The specialized plumage features believed to be responsible for this noise suppression are a leading-edge comb of evenly spaced feathers, the...turbulent structures of the boundary layer, and control not only the source of roughness noise but Trailing-Edge Fringe Leading-Edge Comb Velvety Down...0=1/2. The mapping relationship between the z- and f-planes is completed by equating the background mean flows far from the fiber, which yields V

  17. Autonomous Clustering Using Rough Set Theory


    This paper proposes a clustering technique that minimizes the need for subjective human intervention and is based on elements of rough set theory (RST). The proposed algorithm is unified in its approach to clustering and makes use of both local and global data properties to obtain clustering solutions. It handles single-type and mixed attribute data sets with ease. The results from three data sets of single and mixed attribute types are used to illustrate the technique and establish its efficiency.

  18. Roughness parameter selection for novel manufacturing processes.

    Ham, M; Powers, B M


    This work proposes a method of roughness parameter (RP) selection for novel manufacturing processes or processes where little knowledge exists about which RPs are important. The method selects a single parameter to represent a group of highly correlated parameters. Single point incremental forming (SPIF) is used as the case study for the manufacturing process. This methodology was successful in reducing the number of RPs investigated from 18 to 8 in the case study. © Wiley Periodicals, Inc.

  19. Roughness preserving filter design to remove spatial noise from stereoscopic skin images for stable haptic rendering.

    Lee, K; Kim, M; Lee, O; Kim, K


    A problem in skin rendering with haptic feedback is the reconstruction of accurate 3D skin surfaces from stereo skin images to be used for touch interactions. This problem also encompasses the issue of how to accurately remove haptic spatial noise caused by the construction of disparity maps from stereo skin images, while minimizing the loss of the original skin roughness for cloning real tough textures without errors. Since the haptic device is very sensitive to high frequencies, even small amounts of noise can cause serious system errors including mechanical oscillations and unexpected exerting forces. Therefore, there is a need to develop a noise removal algorithm that preserves haptic roughness. A new algorithm for a roughness preserving filter (RPF) that adaptively removes spatial noise, is proposed. The algorithm uses the disparity control parameter (λ) and noise control parameter (k), obtained from singular value decomposition of a disparity map. The parameter k determines the amount of noise to be removed, and the optimum value of k is automatically chosen based on a threshold of gradient angles of roughness (Ra ). The RPF algorithm was implemented and verified with three real skin images. Evaluation criteria include preserved roughness quality and removed noise. Mean squared error (MSE), peak signal to noise ratio (PSNR), and objective roughness measures Ra and Rq were used for evaluation, and the results were compared against a median filter. The results show that the proposed RPF algorithm is a promising technology for removing noise and retaining maximized roughness, which guarantees stable haptic rendering for skin roughness. The proposed RPF is a promising technology because it allows for any stereo image to be filtered without the risk of losing the original roughness. In addition, the algorithm runs automatically for any given stereo skin image with relation to the disparity parameter λ, and the roughness parameters Ra or Rq are given priority

  20. Rough – Granular Computing knowledge discovery models

    Mohammed M. Eissa


    Full Text Available Medical domain has become one of the most important areas of research in order to richness huge amounts of medical information about the symptoms of diseases and how to distinguish between them to diagnose it correctly. Knowledge discovery models play vital role in refinement and mining of medical indicators to help medical experts to settle treatment decisions. This paper introduces four hybrid Rough – Granular Computing knowledge discovery models based on Rough Sets Theory, Artificial Neural Networks, Genetic Algorithm and Rough Mereology Theory. A comparative analysis of various knowledge discovery models that use different knowledge discovery techniques for data pre-processing, reduction, and data mining supports medical experts to extract the main medical indicators, to reduce the misdiagnosis rates and to improve decision-making for medical diagnosis and treatment. The proposed models utilized two medical datasets: Coronary Heart Disease dataset and Hepatitis C Virus dataset. The main purpose of this paper was to explore and evaluate the proposed models based on Granular Computing methodology for knowledge extraction according to different evaluation criteria for classification of medical datasets. Another purpose is to make enhancement in the frame of KDD processes for supervised learning using Granular Computing methodology.

  1. Wenzel Wetting on Slippery Rough Surfaces

    Stogin, Birgitt; Dai, Xianming; Wong, Tak-Sing


    Liquid repellency is an important surface property used in a wide range of applications including self-cleaning, anti-icing, anti-biofouling, and condensation heat transfer, and is characterized by apparent contact angle (θ*) and contact angle hysteresis (Δθ*). The Wenzel equation (1936) predicts θ* of liquids in the Wenzel state, and is one of the most fundamental equations in the wetting field. However, droplets in the Wenzel state on conventional rough surfaces exhibit large Δθ* , making it difficult to experimentally verify the model with precision. As a result, precise verification of the Wenzel wetting model has remained an open scientific question for the past 79 years. Here we introduce a new class of liquid-infused surfaces called slippery rough surfaces -- surfaces with significantly reduced Δθ* compared to conventional rough surfaces--and use them to experimentally assess the Wenzel equation with the highest precision to date. We acknowledge the funding support by National Science Foundation (NSF) CAREER Award #: 1351462 and Office of Navy Research MURI Award #: N00014-12-1-0875. Stogin acknowledges the support from the NSF Graduate Research Fellowship (Grant No. DGE1255832).


    Ahmed T. Shawky


    Full Text Available Many real world applications need to deal with imprecise data. Therefore, there is a need for newtechniques which can manage such imprecision. Computational Intelligence (CI techniques are the mostappropriate for dealing with imprecise data to help decision makers. It is well known that soft computingtechniques like genetic algorithms, neural networks, and fuzzy logic are effective in dealing with problemswithout explicit model and characterized by uncertainties Using fuzzy set theory considered as majortechniques, which allows decision makers to take a good decision using imprecise inexact data andknowledge. Now using rough set is getting quite necessary to be used for its ability to mining such type ofdata. In this research, we are looking forward to propose a novel technique, which depends on theintegration between fuzzy set concepts and rough set theory in mining relational databases. The proposedmodel allows introducing modularity mechanism, by building a virtual modular decision tables accordingto variety of decision makers points of view. And introduce decision grouping mechanism for getting theoptimizing decision. This approach provides flexibility in decision making verifies all decision standardsand determines decision requirements, through modularizing rough decision table, extraction of roughassociation rules and developing mechanisms for decision grouping.

  3. A Field Theoretic Approach to Roughness Corrections

    Wu, Hua Yao


    We develop a systematic field theoretic description for the roughness correction to the Casimir free energy of parallel plates. Roughness is modeled by specifying a generating functional for correlation functions of the height profile, the two-point correlation function being characterized by the variance, \\sigma^2, and correlation length, \\ell, of the profile. We obtain the partition function of a massless scalar quantum field interacting with the height profile of the surface via a \\delta-function potential. The partition function of this model is also given by a holographic reduction to three coupled scalar fields on a two-dimensional plane. The original three-dimensional space with a parallel plate at separation 'a' is encoded in the non-local propagators of the surface fields on its boundary. Feynman rules for this equivalent 2+1-dimensional model are derived and its counter terms constructed. The two-loop contribution to the free energy of this model gives the leading roughness correction. The absolute ...

  4. Radiative transfer model for contaminated rough slabs.

    Andrieu, François; Douté, Sylvain; Schmidt, Frédéric; Schmitt, Bernard


    We present a semi-analytical model to simulate the bidirectional reflectance distribution function (BRDF) of a rough slab layer containing impurities. This model has been optimized for fast computation in order to analyze massive hyperspectral data by a Bayesian approach. We designed it for planetary surface ice studies but it could be used for other purposes. It estimates the bidirectional reflectance of a rough slab of material containing inclusions, overlaying an optically thick media (semi-infinite media or stratified media, for instance granular material). The inclusions are assumed to be close to spherical and constituted of any type of material other than the ice matrix. It can be any other type of ice, mineral, or even bubbles defined by their optical constants. We assume a low roughness and we consider the geometrical optics conditions. This model is thus applicable for inclusions larger than the considered wavelength. The scattering on the inclusions is assumed to be isotropic. This model has a fast computation implementation and thus is suitable for high-resolution hyperspectral data analysis.

  5. Soil Albedo in Relation to Soil Color, Moisture and Roughness

    Fontes, Adan Fimbres

    Land surface albedo is the ratio of reflected to incident solar radiation. It is a function of several surface parameters including soil color, moisture, roughness and vegetation cover. A better understanding of albedo and how it changes in relation to variations in these parameters is important in order to help improve our ability to model the effects of land surface modifications on climate. The objectives of this study were (1) To determine empirical relationships between smooth bare soil albedo and soil color, (2) To develop statistical relationships between albedo and ground-based thematic mapper (TM) measurements of spectral reflectances, (3) To determine how increased surface roughness caused by tillage reduces bare soil albedo and (4) To empirically relate albedo with TM data and other physical characteristics of mixed grass/shrubland sites at Walnut Gulch Watershed. Albedos, colors and spectral reflectances were measured by Eppley pyranometer, Chroma Meter CR-200 and a Spectron SE-590, respectively. Measurements were made on two field soils (Gila and Pima) at the Campus Agricultural Center (CAC), Tucson, AZ. Soil surface roughness was measured by a profile meter developed by the USDA/ARS. Additional measurements were made at the Maricopa Agricultural Center (MAC) for statistical model testing. Albedos of the 15 smooth, bare soils (plus silica sand) were determined by linear regression to be highly correlated (r^2 = 0.93, p > 0.01) with color values for both wet and dry soil conditions. Albedos of the same smooth bare soils were also highly correlated (r^2>=q 0.86, p > 0.01) with spectral reflectances. Testing of the linear regression equations relating albedo to soil color and spectral reflectances using the data from MAC showed a high correlation. A general nonlinear relationship given by y = 8.366ln(x) + 37.802 r^2 = 0.71 was determined between percent reduction in albedo (y) and surface roughness index (x) for wet and dry Pima and Gila field soils

  6. Nano/submicron-scale TiO{sub 2} network on titanium surface for dental implant application

    Yang, W.-E. [Institute of Oral Biology, National Yang-Ming University, Taipei, Taiwan (China); Hsu, M.-L.; Lin, M.-C. [Department of Dentistry, National Yang-Ming University, Taipei, Taiwan (China); Chen, Z.-H. [Institute of Oral Biology, National Yang-Ming University, Taipei, Taiwan (China); Chen, L.-K. [Department of Dentistry, Taipei City Hospital, Taipei, Taiwan (China); Huang, H.-H. [Institute of Oral Biology, National Yang-Ming University, Taipei, Taiwan (China); Department of Dentistry, National Yang-Ming University, Taipei, Taiwan (China); Department of Dentistry, Taipei City Hospital, Taipei, Taiwan (China)], E-mail:


    In this study, a fast electrochemical anodization treatment, applying different anodic currents, was used to produce a nano/submicron-scale network oxide layer on Ti metal surface for biomedical implant application. The anodized Ti surface was analyzed using thin film X-ray diffractometer, X-ray photoelectron spectrometer, and field emission scanning electron microscope. The whole blood coagulation and human bone marrow stem cells (hBMSCs) adhesion on the anodized Ti surface were evaluated. Results showed that a nano/submicron-scale TiO{sub 2} network layer with a lateral pore size of 20-160 nm could be rapidly produced on Ti surface through electrochemical anodization treatment. Increasing the applied anodic current led to an increase in pore size of TiO{sub 2} network. The nano/submicron-scale TiO{sub 2} network layer significantly enhanced the whole blood coagulation and hBMSCs adhesion on Ti surface.

  7. An experimental result of surface roughness machining performance in deep hole drilling

    Mohamad Azizah


    Full Text Available This study presents an experimental result of a deep hole drilling process for Steel material at different machining parameters which are feed rate (f, spindle speed (s, the depth of the hole (d and MQL, number of drops (m on surface roughness, Ra. The experiment was designed using two level full factorial design of experiment (DoE with centre points to collect surface roughness, Ra values. The signal to noise (S/N ratio analysis was used to discover the optimum level for each machining parameters in the experiment.

  8. Experimental investigation of surface roughness in electrical discharge turning process

    Gohil, Vikas; Puri, Y. M.


    In the present study the effects of machining parameters on the average surface roughness (Ra) in electrical discharge turning (EDT) is investigated. EDT is a new machining process in which a rotary spindle is added to a conventional die-sinking EDM machine in order to produce cylindrical components. In this method a new process parameter (spindle rotation) along with pulse on time and current is introduced to study its effect on Ra. This has been done by means of full factorial design (21 × 32) of experiments. A mathematical model has been developed for Ra by regression analysis and factor effects were analyzed using analysis of variance (ANOVA). Signal-to-noise ratio analysis is used to find the optimal condition.

  9. The efficiency and stability of bubble formation by acoustic vaporization of submicron perfluorocarbon droplets.

    Reznik, Nikita; Shpak, Oleksandr; Gelderblom, Erik C; Williams, Ross; de Jong, Nico; Versluis, Michel; Burns, Peter N


    Submicron droplets of liquid perfluorocarbon converted into microbubbles with applied ultrasound have been studied, for a number of years, as potential next generation extravascular ultrasound contrast agents. In this work, we conduct an initial ultra-high-speed optical imaging study to examine the vaporization of submicron droplets and observe the newly created microbubbles in the first microseconds after vaporization. It was estimated that single pulses of ultrasound at 10 MHz with pressures within the diagnostic range are able to vaporize on the order of at least 10% of the exposed droplets. However, only part of the newly created microbubbles survives immediately following vaporization - the bubbles may recondense back into the liquid droplet state within microseconds of nucleation. The probability of bubble survival within the first microseconds of vaporization was shown to depend on ultrasound excitation pressure as well as on bubble coalescence during vaporization, a behavior influenced by the presence of coating material on the newly created bubbles. The results of this study show for the first time that although initial vaporization of droplets is necessary to create echogenic bubbles, additional factors, such as coalescence and bubble shell properties, are important and should be carefully considered for the production of microbubbles for use in medical imaging.

  10. Airborne studies of submicron aerosol in the troposphere over West Siberia

    Panchenko, M.V.; Zuev, V.E.; Belan, B.D.; Terpugova, S.A. [Institute of Atmospheric Optics, Tomsk (Russian Federation)


    Submicron fraction particles that have the longest lifespan and are included in almost all atmospheric processes are of special importance among the great variety of sizes of particles present in the atmosphere. Submicron particles mainly determine the opticle state of the atmosphere in the visible spectral range, essentially cause the absorption of infrared radiation and, since they are the products and participants in all aerosol-to-gas transformations, accumulate of a lot of various chemical compounds and transfer them to large distances. Investigation of the processes of the spatial-temporal variability of aerosol particles for different climatic zones of the earth is the experimental base for studying their effect on climatically and ecologically significant factors and estimating their unfavorable tendencies. The increasing anthropogenic loading of the earth`s atmosphere is creating an urgency for aerosol research. Regardless of how perfect the analytical and numerical methods of solving radiation problems may be, success in forecasting climatic change is mainly determined by the reliability of the experimental data on optical parameters of the atmosphere and of the description of their variability under the effect of external factors.

  11. Sub-micron alignment for nuclear emulsion plates using low energy electrons caused by radioactive isotopes

    Miyamoto, S.; Ariga, A.; Fukuda, T.; Kazuyama, M.; Komatsu, M.; Nakano, T.; Niwa, K.; Sato, O.; Takahashi, S.


    Nuclear emulsion plates are employed in three-dimensional charged particle detectors that have sub-micron position resolution over 1 m2 with no dead space and no dead time. These detectors are suitable for the study of short-lived particle decays, and direct detection of neutrino interactions of all flavors. Typically emulsion plates are used in a stacked structure. Precise alignment between plates is required for physics analysis. The most accurate alignment method is to use tracks passing through the emulsion plates. The accuracy is about 0.2 μm. However, in an experiment with low track density alignment accuracy decreases to 20 μm because of plate distortion and it becomes more difficult to perform the analysis. This paper describes a new alignment method between emulsion plates by using trajectories of low energy electrons originating from environmental radioactive isotopes. As a trial emulsion plates were exposed to β-rays and γ-rays from K40. The trajectories which passed through emulsion layers were detected by a fully automated emulsion readout system. Using this method, the alignment between emulsion plates is demonstrated to be sub-micron. This method can be applied to many nuclear emulsion experiments. For example, the location of neutrino interaction vertices in the OPERA experiment can benefit from this new technique.

  12. Hybridization between nanocavities for a polarimetric color sorter at the sub-micron scale.

    Segal, Elad; Weissman, Adam; Gachet, David; Salomon, Adi


    Metallic hole arrays have been recently used for color generation and filtering due to their reliability and color tunability. However, color generation is still limited to several microns. Understanding the interaction between the individual elements of the whole nanostructure may push the resolution to the sub-micron level. Herein, we study the hybridization between silver nanocavities in order to obtain active color generation at the micron scale. To do so, we use five identical triangular cavities which are separated by hundreds of nanometers from each other. By tuning either the distance between the cavities or the optical polarization state of the incoming field, the transmitted light through the cavities is actively enhanced at specific frequencies. Consequently, a rainbow of colors is observed from a sub-micron scale unit. The reason for this is that the metallic surface plays a vital role in the hybridization between the cavities and contributes to higher frequency modes. Cathodoluminescence measurements have confirmed this assumption and have revealed that these five triangular cavities act as a unified entity surrounded by the propagated surface plasmons. In such plasmonic structures, multi-color tuning can be accomplished and may open the possibility to improve color generation and high-quality pixel fabrication.

  13. Low-cost replication of self-organized sub-micron structures into polymer films

    H. Stenberg


    Full Text Available In this paper, the results of exploiting self-organized sub-micron polystyrene (PS wrinkle patterns possessing random orientation, in preparation of a nickel stamp for hot embossing purposes, are presented. Self-organized patterns were prepared employing a method in which a stiff cross-linked capping layer on the topmost part of the soft polystyrene layer was created by using reactive ion etching (RIE device with mild conditions and argon as a process gas, and the wrinkle formation was initiated thermally. Different surface patternings were obtained using silicon and stainless steel (SST wafers as substrates. Prepared Ni-stamps were employed in hot embossing of polycarbonate (PC and cyclo-olefin polymer (COP films, using a nano-imprinting process. The replication quality of the self-organized wrinkle structures in PC and COP films was monitored by comparing the shape and dimensions of the original and final surface structures. The hot embossed sub-micron scale features, originally formed on stainless steel substrate, were found to have influence on the optical properties of the PC and COP films by lowering their reflectances.

  14. Investigations of micron and submicron wear features of diseased human cartilage surfaces.

    Peng, Zhongxiao; Baena, Juan C; Wang, Meiling


    Osteoarthritis is a common disease. However, its causes and morphological features of diseased cartilage surfaces are not well understood. The purposes of this research were (a) to develop quantitative surface characterization techniques to study human cartilages at a micron and submicron scale and (b) to investigate distinctive changes in the surface morphologies and biomechanical properties of the cartilages in different osteoarthritis grades. Diseased cartilage samples collected from osteoarthritis patients were prepared for image acquisition using two different techniques, that is, laser scanning microscopy at a micrometer scale and atomic force microscopy at a nanometer scale. Three-dimensional, digital images of human cartilages were processed and analyzed quantitatively. This study has demonstrated that high-quality three-dimensional images of human cartilage surfaces could be obtained in a hydrated condition using laser scanning microscopy and atomic force microscopy. Based on the numerical data extracted from improved image quality and quantity, it has been found that osteoarthritis evolution can be identified by specific surface features at the micrometer scale, and these features are amplitude and functional property related. At the submicron level, the spatial features of the surfaces were revealed to differ between early and advanced osteoarthritis grades. The effective indentation moduli of human cartilages effectively revealed the cartilage deterioration. The imaging acquisition and numerical analysis methods established allow quantitative studies of distinctive changes in cartilage surface characteristics and better understanding of the cartilage degradation process.

  15. Laser smoothing of sub-micron grooves in hydroxyl-rich fused silica

    Shen, N; Matthews, M J; Fair, J E; Britten, J A; Nguyen, H T; Cooke, D; Elhadj, S; Yang, S T


    Nano- to micrometer-sized surface defects on UV-grade fused silica surfaces are known to be effectively smoothed through the use of high-temperature localized CO{sub 2} laser heating, thereby enhancing optical properties. However, the details of the mass transport and the effect of hydroxyl content on the laser smoothing of defective silica at submicron length scales is still not completely understood. In this study, we examine the morphological evolution of sub-micron, dry-etched periodic surface structures on type II and type III SiO{sub 2} substrates under 10.6 {micro}m CO{sub 2} laser irradiation using atomic force microscopy (AFM). In-situ thermal imaging was used to map the transient temperature field across the heated region, allowing assessment of the T-dependent mass transport mechanisms under different laser-heating conditions. Computational fluid dynamics simulations correlated well with experimental results, and showed that for large effective capillary numbers (N{sub c} > 2), surface diffusion is negligible and smoothing is dictated by capillary action, despite the relatively small spatial scales studied here. Extracted viscosity values over 1700-2000K were higher than the predicted bulk values, but were consistent with the surface depletion of OH groups, which was confirmed using confocal Raman microscopy.

  16. Fluidization of nano and sub-micron powders using mechanical vibration

    Souresh Kaliyaperumal; Shahzad Barghi; Lauren Briens; Sohrab Rohani; Jesse Zhu


    The fluidization behavior of nano and sub-micron powders belonging to group C of Geldart's classification was studied in a mechanically vibrated fluidized bed (vibro-fluidized bed) at room temperature.Pretreated air was used as the fluidizing gas whereas SiO2, Al2O3, TiO2, ZrSi, BaSO4 were solid particles.Mechanical vibration amplitudes were 0.1, 0.25, 0.35, 0.45 mm, while the frequencies were 5, 20, 30,40 Hz to investigate the effects of frequency and amplitude of mechanical vibration on minimum fluidization velocity, bed pressure drop, bed expansion, and the agglomerate size and size distribution. A novel technique was employed to determine the apparent minimum fluidization velocity from pressure drop signals. Richardson-Zaki equation was employed as nano-particles showed fluid like behavior when fluidized. The average size of agglomerates formed on top of the bed was smaller than those at the bottom.Size distribution of agglomerates on top was also more uniform compared to those near the distributor.Larger agglomerates at the bottom of the bed formed a small fraction of the bed particles. Average size of submicron agglomerates decreased with increasing the frequency of vibration, however nano particles were less sensitive to change in vibration frequency. Mechanical vibration enhanced the quality of fluidization by reducing channeling and rat-holing phenomena caused by interparticle cohesive forces.

  17. Dynamics of submicron aerosol droplets in a robust optical trap formed by multiple Bessel beams

    Thanopulos, Ioannis [Laboratory of Physical Chemistry, Vladimir-Prelog-Weg 2, ETH Zurich, CH-8093 Zurich (Switzerland); Theoretical and Physical Chemistry Institute, National Hellenic Research Foundation, Athens 11635 (Greece); Luckhaus, David; Signorell, Ruth, E-mail: [Laboratory of Physical Chemistry, Vladimir-Prelog-Weg 2, ETH Zurich, CH-8093 Zurich (Switzerland); Preston, Thomas C. [School of Chemistry, University of Bristol, Cantock' s Close, Clifton, Bristol BS8 1TS (United Kingdom)


    In this paper, we model the three-dimensional escape dynamics of single submicron-sized aerosol droplets in optical multiple Bessel beam traps. Trapping in counter-propagating Bessel beams (CPBBs) is compared with a newly proposed quadruple Bessel beam (QBB) trap, which consists of two perpendicularly arranged CPBB traps. Calculations are performed for perfectly and imperfectly aligned traps. Mie-theory and finite-difference time-domain methods are used to calculate the optical forces. The droplet escape kinetics are obtained from the solution of the Langevin equation using a Verlet algorithm. Provided the traps are perfectly aligned, the calculations indicate very long lifetimes for droplets trapped either in the CPBB or in the QBB trap. However, minor misalignments that are hard to control experimentally already severely diminish the stability of the CPBB trap. By contrast, such minor misalignments hardly affect the extended droplet lifetimes in a QBB trap. The QBB trap is found to be a stable, robust optical trap, which should enable the experimental investigation of submicron droplets with radii down to 100 nm. Optical binding between two droplets and its potential role in preventing coagulation when loading a CPBB trap is briefly addressed.

  18. Mechanisms of submicron inclusion re-equilibration during host mineral deformation

    Griffiths, Thomas; Habler, Gerlinde; Abart, Rainer; Rhede, Dieter; Wirth, Richard


    Both brittle and ductile deformation can facilitate re-equilibration of mineral inclusions. The presence of inclusions also influences stress and strain distribution in the host. The processes governing feedbacks between brittle deformation, ductile deformation, and inclusion re-equilibration have been studied using unique microstructures in Permian meta-pegmatite garnets from the Koralpe, Eastern Alps, Austria. Sampled almandine-spessartine garnets contain highly abundant submicron-sized inclusions, which originated during or subsequent to magmatic garnet growth. The Permian magmatic assemblages were affected by eclogite facies metamorphism during the Cretaceous tectono-metamorphic event. The meta-pegmatite garnet deformed crystal-plastically at this metamorphic stage (Bestmann et al. 2008) and the host-inclusion system was affected by partial recrystallization. Trails of coarser inclusions (1-10µm diameter) crosscut the magmatic submicron inclusion density zoning in the garnet, defining curviplanar geometrical surfaces in 3D. In 10-40µm broad 'bleaching zones' flanking inclusion trails, the original ≤1µm sized inclusions are not seen in the optical microscope or SEM, however inclusions crystal axes is observed in connection with some already coarsened inclusions. Strain concentrations are widespread in some trails, but rare in others. A TEM foil transecting a garnet domain with concentrated lattice rotation in association with inclusions reveals well developed polygonal subgrain walls with few free dislocations. Where dislocation density is greatest, almost no Journal of Structural Geology 30: 777-790

  19. The effect of continuous natural roughness onhydraulic jump characteristics on the stone ramps

    M. F. Maghrebi


    the flume. Water contraction usually occurs after the sluice gate is avoided by a steel plate welded on the sluice gate. So, the initial depth equals the gate opening. According to the experimental procedure, after placing theuniform roughness heights on channel bed, the pump runs and water flows slowly into the flume. Then, discharge increases to reach the desired value and the sluice gate opening is set up to have the hydraulic jump formed at a distance of ahead of the gate. These circumstances maintain enough for data recording. The parameter of gravel particles considered as the most sensible characteristic. The subcritical depth y2 was measured from the profile survey, where the water surface began to be essentially level. Results and discussions: In the smooth and rough beds experiments show that variation in initial depth does not have any effect on decreasing the conjugate depths ratio. The conjugate depths ratio decreases as the roughness increases. The difference between conjugate depths ratio of rough beds with middle diameter 3.5mm (B and 11mm (C appears when the Froude number exceeds 7.5 and for Froude numbers greater than 10, a significant drop can be observed in the conjugate depths ratio diagrams from rough bed B to C. The horizontal distance between the beginning and end point of a hydraulic jump is considered as the length of the hydraulic jump. Dimensionless length of the hydraulic jump is presented as which is usually considered as a function of . For Froude number greater than 10, the dimensionless length of the hydraulic jump is nearly constant. Then, the ratio of for Froude numbers greater than 10 seems to be independent of supercritical Froude number and is just a function of roughness. In all experiments the length of the hydraulic jump decreases compared with the smooth bed under conditions that bed roughness is not subjected to water jet. Conclusions: Experiments demonstrated that in the rough bed by increasing roughness, the conjugated

  20. Estimating small-scale roughness of a rock joint using TLS data

    Bitenc, Maja; Kieffer, D. Scott; Khoshelham, Kourosh


    ) is approximately normal. Standard deviation of differences on average slightly increases with the noise level, but is strongly dependent on the analysis direction. As proved by different researches within the field of signal, image and also TLS data processing, noise can be, to a certain extent, removed by a post-processing step called denoising. In this research, four denoising methods, namely discrete WT (DWT) and stationary WT (SWT), and classic NLM (NLM) and probabilistic NLM (PNLM), were used on noisy ATOS data. Results were compared based on the (i) height and (ii) roughness differences between denoised surfaces and reference ATOS surface, (iii) the peak signal-to-noise ratio (PSNR) and (iv) the visual check of denoised surface. Increased PSNRs and reduced roughness differences prove the importance of the TLS data denoising procedure. In case of SWT, NLM and PNLM the surface is mostly over smoothed, whereas in case of DWT some noise remains. References: - Grasselli, G. (2001). Shear strength of rock joints based on quantified surface description. École Polytechnique Fédérale de Lausanne. Lausanne, EPFL. - Sturzenegger, M. and D. Stead (2009). "Close-range terrestrial digital photogrammetry and terrestrial laser scanning for discontinuity characterization on rock cuts." Engineering Geology 106(3-4): 163-182.

  1. Combined AFM nano-machining and reactive ion etching to fabricate high aspect ratio structures.

    Peng, Ping; Shi, Tielin; Liao, Guanglan; Tang, Zirong


    In this paper, a new combined method of sub-micron high aspect ratio structure fabrication is developed which can be used for production of nano imprint template. The process includes atomic force microscope (AFM) scratch nano-machining and reactive ion etching (RIE) fabrication. First, 40 nm aluminum film was deposited on the silicon substrate by magnetron sputtering, and then sub-micron grooves were fabricated on the aluminum film by nano scratch using AFM diamond tip. As aluminum film is a good mask for etching silicon, high aspect ratio structures were finally fabricated by RIE process. The fabricated structures were studied by SEM, which shows that the grooves are about 400 nm in width and 5 microm in depth. To obtain sub-micron scale groove structures on the aluminum film, experiments of nanomachining on aluminum films under various machining conditions were conducted. The depths of the grooves fabricated using different scratch loads were also studied by the AFM. The result shows that the material properties of the film/substrate are elastic-plastic following nearly a bilinear law with isotropic strain hardening. Combined AFM nanomachining and RIE process provides a relative lower cost nano fabrication technique than traditional e-beam lithography, and it has a good prospect in nano imprint template fabrication.


    Lan Jiacheng


    In this paper, the author gives the weighted weak Lipschitz boundedness with power weight for rough multilinear integral operators. A simple way is obtained that is closely linked with a class of rough fractional integral operators.

  3. Rough communication of crisp concept in fuzzy approximation spaces

    Wang Hongkai; Guan Yanyong; Yu Zhaoxia


    To study the problem of knowledge translation in fuzzy approximation spaces, the concept of rough communication of crisp set in fuzzy approximation spaces is proposed. In a rough communication of crisp set in fuzzy approximation spares, the problem of uncertainty exists, for each agent has a different language and cannot provide precise communication to each other. By means of some concepts, such as CF rough communication cut, which is a bridge between fuzzy concept and crisp concept, cut analysis of CF rough communication is made, and the relation theorem between CF rough communication and rough communication of crisp concept is obtained. Finally, in order to give an intuitive analysis of the relation between CF rough communication and rough communication of crisp concept, an example is given.

  4. A sparse scattering model for nanoparticles on rough substrates

    Karamehmedovic, Mirza; Hansen, Poul-Erik; Wriedt, Thomas


    We present and validate an efficient forward scattering model for nanoparticles on rough contaminated substrates.......We present and validate an efficient forward scattering model for nanoparticles on rough contaminated substrates....

  5. Surface Roughness Effects on Vortex Torque of Air Supported Gyroscope

    LIANG Yingchun; LIU Jingshi; SUN Yazhou; LU Lihua


    In order to improve the drift precision of air supported gyroscope, effects of surface roughness magnitude and direction on vortex torque of air supported gyroscope are studied. Based on Christensen's rough surface stochastic model and consistency transformation method, Reynolds equation of air supported gyroscope containing surface roughness information is established.Also effects of mathematical models of main machining errors on vortex torque are established. By using finite element method,the Reynolds equation is solved numerically and the vortex torque in the presence of machining errors and surface roughness is calculated. The results show that surface roughness of slit has a significant effect on vortex torque. Transverse surface roughness makes vortex torque greater, while longitudinal surface roughness makes vortex torque smaller. The maximal difference approaches 11.4% during the range analyzed in this article. However surface roughness of journal influences vortex torque insignificantly. The research is of great significance for designing and manufacturing air supported gyroscope and predicting its performance.

  6. Effect of enamel etching time on roughness and bond strength

    Barkmeier, Wayne W; Erickson, Robert L; Kimmes, Nicole S; Latta, Mark A; Wilwerding, Terry M


    The current study examined the effect of different enamel conditioning times on surface roughness and bond strength using an etch-and-rinse system and four self-etch adhesives. Surface roughness (Ra...

  7. Interferometric microscopy study of the surface roughness of Portland cement under the action of different irrigants.

    Ballester-Palacios, Maria L; Berástegui-Jimeno, Esther M; Parellada-Esquius, Neus; Canalda-Sahli, Carlos


    Some investigations suggested common Portland cement (PC) as a substitute material for MTA for endodontic use; both MTA and PC have a similar composition. The aim of this study was to determine the surface roughness of common PC before and after the exposition to different endodontic irrigating solutions: 10% and 20% citric acid, 17% ethylenediaminetetraacetic (EDTA) and 5% sodium hypochlorite. Fifty PC samples in the form of cubes were prepared. PC was mixed with distilled water (powder/liquid ratio 3:1 by weight). The samples were immersed for one minute in 10% and 20% citric acid, 17% EDTA and 5% sodium hypochlorite. After gold coating, PC samples were examined using the New View 100 Zygo interferometric microscope. It was used to examine and register the surface roughness and the profile of two different areas of each sample. Analysis of variance (ANOVA) was carried out, and as the requirements were not met, use was made of the Kruskal-Wallis test for analysis of the results obtained, followed by contrasts using Tukey's contrast tests. Sodium hypochlorite at a concentration of 5% significantly reduced the surface roughness of PC, while 20% citric acid significantly increased surface roughness. The other evaluated citric acid concentration (10%) slightly increased the surface roughness of PC, though statistical significance was not reached. EDTA at a concentration of 17% failed to modify PC surface roughness. Irrigation with 5% sodium hypochlorite and 20% citric acid lowered and raised the roughness values, respectively. The surface texture of PC is modified as the result of treatment with different irrigating solutions commonly used in endodontics, depending on their chemical composition and concentration.

  8. Effects of surface roughness on magnetic flux leakage testing of micro-cracks

    Deng, Zhiyang; Sun, Yanhua; Yang, Yun; Kang, Yihua


    Magnetic flux leakage (MFL) testing owns the advantages of high inspection sensitivity and stability, but its testing results are always affected by surface roughness. The relationship between the surface roughness ({{R}a} ) and detection signals for surface-breaking cracks is mainly discussed. The existence of roughness magnetic compression effect (RMCE) in present MFL testing is specially pointed out and its relevant theory is also analyzed, which manifest themselves in the compression of MFL signal in its peak value and the baseline drifts mixed with noise. An experimental investigation on surface comparators with different arithmetic average height ({{R}a} ) and artificial notch size, is performed to analyze the effects of surface roughness on detection signals of cracks. The detection limit (DL) of micro-crack is analyzed by comparing the {{B}y} noise-signal ratio ({{S}y} ) and peak-peak signals of the cracks. Meanwhile, {{S}y} increases with the {{R}a} and R{{S}m} , in this case, relatively shallow defects cannot be clearly distinguished at determined rough surface. Afterwards, a series of simulations are designed and performed to verify the effects of surface roughness on characteristic {{B}y} of the electromagnetic field, and a theoretical DL of micro-crack is presented as: DL=2.88{{R}a}+7.00 . Furthermore, the optimal lift-off value is selected for the micro-cracks’ detection to weaken the negative magnetic compression effect. MFL signals cannot reflect the accurate sizes of the cracks on rough surface due to the RMCE and its relevant phenomenon. The discovery and results will benefit the quantitative evaluation of the MFL testing.

  9. 14 CFR 25.1517 - Rough air speed, VRA.


    ... 14 Aeronautics and Space 1 2010-01-01 2010-01-01 false Rough air speed, VRA. 25.1517 Section 25... Limitations § 25.1517 Rough air speed, VRA. A rough air speed, VRA, for use as the recommended turbulence... specified in § 25.335(d); and (3) Is sufficiently less than VMO to ensure that likely speed variation...

  10. ROMI 4.0: Updated Rough Mill Simulator

    Timo Grueneberg; R. Edward Thomas; Urs. Buehlmann


    In the secondary hardwood industry, rough mills convert hardwood lumber into dimension parts for furniture, cabinets, and other wood products. ROMI 4.0, the US Department of Agriculture Forest Service's ROugh-MIll simulator, is a software package designed to simulate the cut-up of hardwood lumber in rough mills in such a way that a maximum possible component yield...

  11. 7 CFR 868.201 - Definition of rough rice.


    ... 7 Agriculture 7 2010-01-01 2010-01-01 false Definition of rough rice. 868.201 Section 868.201... FOR CERTAIN AGRICULTURAL COMMODITIES United States Standards for Rough Rice Terms Defined § 868.201 Definition of rough rice. Rice (Oryza sativa L.) which consists of 50 percent or more of paddy kernels...

  12. On Characterization of Rough Type-2 Fuzzy Sets

    Tao Zhao


    Full Text Available Rough sets theory and fuzzy sets theory are important mathematical tools to deal with uncertainties. Rough fuzzy sets and fuzzy rough sets as generalizations of rough sets have been introduced. Type-2 fuzzy set provides additional degree of freedom, which makes it possible to directly handle high uncertainties. In this paper, the rough type-2 fuzzy set model is proposed by combining the rough set theory with the type-2 fuzzy set theory. The rough type-2 fuzzy approximation operators induced from the Pawlak approximation space are defined. The rough approximations of a type-2 fuzzy set in the generalized Pawlak approximation space are also introduced. Some basic properties of the rough type-2 fuzzy approximation operators and the generalized rough type-2 fuzzy approximation operators are discussed. The connections between special crisp binary relations and generalized rough type-2 fuzzy approximation operators are further examined. The axiomatic characterization of generalized rough type-2 fuzzy approximation operators is also presented. Finally, the attribute reduction of type-2 fuzzy information systems is investigated.

  13. Procedure and applications of combined wheel/rail roughness measurement

    Dittrich, M.G.


    Wheel-rail roughness is known to be the main excitation source of railway rolling noise. Besides the already standardised method for direct roughness measurement, it is also possible to measure combined wheel-rail roughness from vertical railhead vibration during a train pass-by. This is a different

  14. Rough sets selected methods and applications in management and engineering

    Peters, Georg; Ślęzak, Dominik; Yao, Yiyu


    Introduced in the early 1980s, Rough Set Theory has become an important part of soft computing in the last 25 years. This book provides a practical, context-based analysis of rough set theory, with each chapter exploring a real-world application of Rough Sets.

  15. A note on rough set and non-measurable set


    It is proved that rough set is equivalent to non-measurable set in measure theory. Hence, rough set is not a new concept in some sense. At the same time, we defined the measurable degree of a set by inner measure and outer measure. Its special case is the accuracy measure of rough set.

  16. Robust surface roughness indices and morphological interpretation

    Trevisani, Sebastiano; Rocca, Michele


    Geostatistical-based image/surface texture indices based on variogram (Atkison and Lewis, 2000; Herzfeld and Higginson, 1996; Trevisani et al., 2012) and on its robust variant MAD (median absolute differences, Trevisani and Rocca, 2015) offer powerful tools for the analysis and interpretation of surface morphology (potentially not limited to solid earth). In particular, the proposed robust index (Trevisani and Rocca, 2015) with its implementation based on local kernels permits the derivation of a wide set of robust and customizable geomorphometric indices capable to outline specific aspects of surface texture. The stability of MAD in presence of signal noise and abrupt changes in spatial variability is well suited for the analysis of high-resolution digital terrain models. Moreover, the implementation of MAD by means of a pixel-centered perspective based on local kernels, with some analogies to the local binary pattern approach (Lucieer and Stein, 2005; Ojala et al., 2002), permits to create custom roughness indices capable to outline different aspects of surface roughness (Grohmann et al., 2011; Smith, 2015). In the proposed poster, some potentialities of the new indices in the context of geomorphometry and landscape analysis will be presented. At same time, challenges and future developments related to the proposed indices will be outlined. Atkinson, P.M., Lewis, P., 2000. Geostatistical classification for remote sensing: an introduction. Computers & Geosciences 26, 361-371. Grohmann, C.H., Smith, M.J., Riccomini, C., 2011. Multiscale Analysis of Topographic Surface Roughness in the Midland Valley, Scotland. IEEE Transactions on Geoscience and Remote Sensing 49, 1220-1213. Herzfeld, U.C., Higginson, C.A., 1996. Automated geostatistical seafloor classification - Principles, parameters, feature vectors, and discrimination criteria. Computers and Geosciences, 22 (1), pp. 35-52. Lucieer, A., Stein, A., 2005. Texture-based landform segmentation of LiDAR imagery

  17. Offshore Wind Power at Rough Sea

    Petersen, Kristian Rasmus; Madsen, Erik Skov; Bilberg, Arne


    This study compare the current operations and maintenance issues of one offshore wind park at very rough sea conditions and two onshore wind parks. Through a detailed data analysis and case studies this study identifies how improvements have been made in maintenance of large wind turbines. However......, the study has also revealed the need for new maintenance models including a shift from breakdown and preventive maintenances and towards more predictive maintenance to reduce the cost of energy for offshore wind energy installations in the future....

  18. Bounds for convection between rough boundaries

    Goluskin, David


    We consider Rayleigh-B\\'enard convection in a layer of fluid between no-slip rough boundaries, where the top and bottom boundary heights are functions of the horizontal coordinates with bounded gradients. We use the background method to derive an upper bound on mean heat flux across the layer for all admissible boundary geometries. This flux, normalized by the temperature difference between the boundaries, can grow with the Rayleigh number ($Ra$) no faster than $Ra^{1/2}$ as $Ra \\rightarrow \\infty$. Coefficients of the bound are given explicitly in terms of the geometry, and evaluation of the coefficients is illustrated for sinusoidal boundaries.

  19. On $\\alpha$-roughly weighted games

    Freixas, Josep


    Very recently Gvozdeva, Hemaspaandra, and Slinko (2011) have introduced three hierarchies for simple games in order to measure the distance of a given simple game to the class of weighted voting games or roughly weighted voting games. Their third class $\\mathcal{C}_\\alpha$ consists of all simple games permitting a weighted representation such that each winning coalition has a weight of at least 1 and each losing coalition a weight of at most $\\alpha$. We continue their work and contribute some new results on the possible values of $\\alpha$ for a given number of voters.

  20. Wave scattering from statistically rough surfaces

    Bass, F G; ter Haar, D


    Wave Scattering from Statistically Rough Surfaces discusses the complications in radio physics and hydro-acoustics in relation to wave transmission under settings seen in nature. Some of the topics that are covered include radar and sonar, the effect of variations in topographic relief or ocean waves on the transmission of radio and sound waves, the reproduction of radio waves from the lower layers of the ionosphere, and the oscillations of signals within the earth-ionosphere waveguide. The book begins with some fundamental idea of wave transmission theory and the theory of random processes a

  1. Turbulent flow structure response to a varying wall-roughness arrangement: a modelling study

    Jakirlic, Suad; Krumbein, Benjamin; Fooroghi, Pourya; Magagnato, Franco; Frohnapfel, Bettina; Darmstadt Collaboration; Karlsruhe Collaboration


    Presently adopted approach to the modelling of rough surfaces relies on introducing an additional drag term in the appropriately 'filtered' Navier-Stokes equations, accounting for the form drag and blockage effects, the roughness elements exert on the flow. A non-dimensional drag function D(y) accounting for the shape of roughness elements is introduced. It is evaluated by applying a reference DNS of an open channel flow over a wall characterized by varying arrangement (aligned/staggered) of differently-shaped/sized roughness elements at a bulk Reynolds number Re =6500 by Fooroghi et al.. The prime objective of the present work is to assess the roughness model capability to predict mean velocities and turbulent intensities in conjunction with a recently formulated hybrid LES/RANS (Reynolds-Averaged Navier-Stokes) model, based on the Very Large Eddy Simulation (VLES) concept of Speziale. A seamless transition from RANS to LES is enabled depending on the ratio of the turbulent viscosities associated with the unresolved scales corresponding to the LES cut-off and those related to the turbulent properties of the VLES residual motion.

  2. Optical scattering simulation of ice particles with surface roughness modeled using the Edwards-Wilkinson equation

    Zhang, Jianing; Bi, Lei; Liu, Jianping; Panetta, R. Lee; Yang, Ping; Kattawar, George W.


    Constructing an appropriate particle morphology model is essential for realistic simulation of optical properties of atmospheric particles. This paper presents a model for generating surface roughness based on a combination of methods from discrete differential geometry combined with a stochastic partial differential equation for surface evolution introduced by Edwards and Wilkinson. Scattering of light by roughened particles is simulated using the Invariant Imbedding T-Matrix (II-TM) method. The effects of surface roughness on the single-scattering properties, namely, the phase matrix, asymmetry factor, and extinction efficiency, are investigated for a single wavelength in the visible range and for a range of size parameters up to x=50. Three different smooth shapes are considered: spherical, spheroidal, and hexagonal, the latter two in just the "compact particle" case of unit aspect ratio. It is shown that roughness has negligible effects on the optical scattering properties for size parameters less than 20. For size parameters ranging from 20 to 50, the phase matrix elements are more sensitive to the surface roughness than are two important integral optical properties, the extinction efficiency and asymmetry factor. As has been seen in studies using other forms of roughening, the phase function is progressively smoothed as roughness increases. The effect on extinction efficiency is to increase it, and on asymmetry factor is to decrease it. Each of these effects is relatively modest in the size range considered, but the trend of results suggests that greater effects will be seen for size parameters larger than ones considered here.

  3. Experimental characterization of roughness-induced crack closure in Al-Li 2090 alloy

    Jung, H.Y. [Georgia Inst. of Technology, Atlanta, GA (United States). School of Civil Engineering; Antolovich, S.D. [Washington State Univ., Pullman, WA (United States). Dept. of Mechanical and Material Engineering


    Fatigue crack propagation testing and a fractographic analysis for Al-Li 2090 alloy specimens were performed to experimentally characterize roughness-induced crack closure. The effects of fracture surface roughness on crack closure were quite significant. It was found that asperity contact inside of Al-Li alloy specimens can occur via different mechanisms which depend on the magnitude of load or crack length. In addition, sterelogical techniques were used to provide additional input required to characterize the three-dimensional nature of the fracture surface and to represent the most salient measurable features of the actual fracture surface in two-dimensional form. From this, relations between the roughness parameter and the nominal range of stress intensity factors were rationalized for different load ratios and load ranges. The degree of mixed mode fracture was characterized. Based on these studies, it was concluded that asperity contact can involve two components: (1) mechanical contact of asperities due to the roughness on the fracture surface and, (2) mixed mode crack tip displacements when the load is applied. Crack closure due to out-of--plane mixed mode fracture (i.e., Mode III) appeared to be more prominent compared to in-plane mixed mode fracture (i.e., Mode II) since the roughness dimension (mean height) is large in the thickness section and the angle between asperity slip band facets is large (50{degree}).

  4. Functionalized PDMS with versatile and scalable surface roughness gradients for cell culture

    Zhou, Bingpu


    This manuscript describes a simple and versatile approach to engineering surface roughness gradients via combination of microfluidics and photo-polymerization. Through UV-mediated polymerization, N-isopropylacrylamide with concentration gradients are successfully grafted onto PDMS surface, leading to diverse roughness degrees on the obtained PDMS substrate. Furthermore, the extent of surface roughness can be controllably regulated via tuning the flow rate ratio between the monomer solution and deionized water. Average roughness ranging from 8.050 nm to 151.68 nm has well been achieved in this work. Such PDMS samples are also demonstrated to be capable of working as supporting substrates for controlling cell adhesion or detachment. Due to the different degrees of surface roughness on a single substrate, our method provides an effective approach for designing advanced surafecs for cell culture. Finally, the thermosensitive property of N-isopropylacrylamide makes our sample furnish as another means for controlling the cell detachment from the substrates with correspondence to the surrounding temperature.

  5. Acoustic imaging in application to reconstruction of rough rigid surface with airborne ultrasound waves

    Krynkin, A.; Dolcetti, G.; Hunting, S.


    Accurate reconstruction of the surface roughness is of high importance to various areas of science and engineering. One important application of this technology is for remote monitoring of open channel flows through observing its dynamic surface roughness. In this paper a novel airborne acoustic method of roughness reconstruction is proposed and tested with a static rigid rough surface. This method is based on the acoustic holography principle and Kirchhoff approximation which make use of acoustic pressure data collected at multiple receiver points spread along an arch. The Tikhonov regularisation and generalised cross validation technique are used to solve the underdetermined system of equations for the acoustic pressures. The experimental data are collected above a roughness created with a 3D printer. For the given surface, it is shown that the proposed method works well with the various number of receiver positions. In this paper, the tested ratios between the number of surface points at which the surface elevation can be reconstructed and number of receiver positions are 2.5, 5, and 7.5. It is shown that, in a region comparable with the projected size of the main directivity lobe, the method is able to reconstruct the spatial spectrum density of the actual surface elevation with the accuracy of 20%.

  6. Turbulent transfer coefficient and roughness length in a high-altitude lake, Tibetan Plateau

    Li, Zhaoguo; Lyu, Shihua; Zhao, Lin; Wen, Lijuan; Ao, Yinhuan; Wang, Shaoying


    A persistent unstable atmospheric boundary layer was observed over Lake Ngoring, caused by higher temperature on the water surface compared with the overlying air. Against this background, the eddy covariance flux data collected from Lake Ngoring were used to analyse the variation of transfer coefficients and roughness lengths for momentum, heat and moisture. Results are discussed and compared with parameterization schemes in a lake model. The drag coefficient and momentum roughness length rapidly decreased with increasing wind velocity, reached a minimum value in the moderate wind velocity and then increased slowly as wind velocity increased further. Under weak wind conditions, the surface tension or small scale capillary wave becomes more important and increases the surface roughness. The scalar roughness length ratio was much larger than unity under weak wind conditions, and it decreased to values near unity as wind velocity exceeded 4.0 m s-1. The lake model could not reproduce well the variation of drag coefficient, or momentum roughness length, versus wind velocity in Lake Ngoring, but it did simulate well the sensible heat and latent heat fluxes, as a result of complementary opposite errors.

  7. Bacterial Adhesion and Surface Roughness for Different Clinical Techniques for Acrylic Polymethyl Methacrylate


    This study sought to assess the effect of different surface finishing and polishing protocols on the surface roughness and bacterial adhesion (S. sanguinis) to polymethyl methacrylates (PMMA). Fifty specimens were divided into 5 groups (n = 10) according to their fabrication method and surface finishing protocol: LP (3 : 1 ratio and laboratory polishing), NF (Nealon technique and finishing), NP (Nealon technique and manual polishing), MF (3 : 1 ratio and manual finishing), and MP (3 : 1 ratio...

  8. Analysis of a Rough Elliptic Bore Journal Bearing using Expectancy Model of Roughness Characterization

    P.C. Mishra


    Full Text Available Performance characteristics of a rough elliptic bore journal bearing are studied. The bearing bore of isotropic roughness orientation is characterized by stochastic function and the film geometry is quantified to elliptic shape. There after the Reynolds equation and energy equation are descretized for pressure and temperature respectively. A finite difference model is developed to evaluate hydrodynamic pressure and oil temperature. Solution to this model is done using effective influence Newton-Raphson method. Performance parameters such as load bearing ability, friction, flow-in and side leakages are computed and discussed.

  9. The effect of inductively-coupled-plasma reactive ion etching power on the etching rate and the surface roughness of a sapphire substrate.

    Chang, Chun-Ming; Shiao, Ming-Hua; Yang, Chin-Tien; Cheng, Chung-Ta; Hsueh, Wen-Jeng


    In this study, patterned sapphire substrates are fabricated using nanosphere lithography (NSL) and inductively-coupled-plasma reactive ion etching (ICP-RIE). Polystyrene nanospheres of approximately 600 nm diameter are self-assembled on c-plane sapphire substrates by spin-coating. The diameter of the polystyrene nanospheres is modified to adjust the etching mask pitch cycle using oxygen plasma in the ICP-RIE system. A nickel thin film mask of 100 nm thickness is deposited by electron-beam evaporation on a substrate covered with treated nanospheres. The sapphire substrate is then etched in an inductively coupled plasma system using BCl3/Ar gas, to fabricate a structure with a periodic sub-micron hole array with different sidewall intervals. The DC bias voltage, the sapphire etching rate, the surface roughness, are studied as a function of the ICP and the RF power. Different sub-micron hole arrays with spacing cycles of 89 nm, 139 nm and 167 nm are successfully fabricated on the sapphire substrate, using suitable etching parameters.

  10. Submicron InP DHBT technology for high-speed high-swing mixed-signal ICs

    Godin, Jean; Nodjiadjim, V.; Riet, Muriel;


    We report on the development of a submicron InP DHBT technology, optimized for the fabrication of 50-GHz-clock mixed signal ICs. In-depth study of device geometry and structure has allowed to get the needed performances and yield. Special attention has been paid to critical thermal behavior. Vari...

  11. The role of jet and film drops in controlling the mixing state of submicron sea spray aerosol particles

    Wang, Xiaofei; Deane, Grant B.; Moore, Kathryn A.; Ryder, Olivia S.; Stokes, M. Dale; Beall, Charlotte M.; Collins, Douglas B.; Santander, Mitchell V.; Burrows, Susannah M.; Sultana, Camille M.; Prather, Kimberly


    Covering 71% of the Earth’s surface, oceans represent a significant global source of atmospheric aerosols. The size and composition of sea spray aerosols (SSA) affect their ability to serve as cloud seeds and thus understanding the factors controlling their composition is critical to predicting their impact on clouds and climate. SSA particles have been shown to be an external mixture of particles with different compositions. Film and jet drop production mechanisms ultimately determine the individual particle compositions which are comprised of an array of salt/organic mixtures ranging from pure sea salt to nearly pure organic particles. It is often assumed that the majority of submicron SSA are formed by film drops produced from bursting hydrophobic organic-rich bubble film caps at the sea surface, and in contrast, jet drops are postulated to produce larger supermicron particles from underlying seawater comprised largely of salts and water soluble organic species. However, here we show that jet drops produced by bursting sub-100 m bubbles account for up to 40 % of all submicron particles. They have distinct chemical compositions, organic volume fractions and ice nucleating activities from submicron film drops. Thus a substantial fraction of submicron particles will not necessarily be controlled by the composition of the sea surface microlayer as has been assumed in many studies. This finding has significant ramifications for the size-resolved mixing states of SSA particles which must be taken into consideration when accessing SSA impacts on clouds.

  12. Do nanofill or submicron composites show improved smoothness and gloss? A systematic review of in vitro studies

    Kaizer, M.R.; Oliveira-Ogliari, A. de; Cenci, M.S.; Opdam, N.J.M.; Moraes, R.R.


    OBJECTIVES: Despite nanofill and submicron composites' aim to provide high initial polishing combined with superior smoothness and gloss retention, the question still remains whether clinicians should consider using these new materials over traditional microhybrids. The aim of this paper was to syst

  13. Hemodynamics and the parameters of the heart mass in the dog after inhalation of submicron /sup 239/Pu dioxide

    Kalmykova, Z.I.; Buldakov, Z.I.; Kharunzhin, V.V.

    The growth of the right heart mass was mainly registered in dogs after inhalation of different quantities of /sup 239/Pu submicron dioxide. This was correlated with the value of /sup 239/Pu deposited in the lungs and associated with the systemic hemodynamic disorders.

  14. A Nordic project on high speed low power design in sub-micron CMOS technology for mobile phones

    Olesen, Ole

    This paper is a survey paper presenting the Nordic CONFRONT project and reporting some results from the group at CIE/DTU, Denmark. The objective of the project is to demonstrate the feasibility of sub-micron CMOS for the realisation of RF front-end circuits operating at frequencies in the 1...

  15. A Novel Leakage-tolerant Domino Logic Circuit With Feedback From Footer Transistor In Ultra Deep Submicron CMOS

    Moradi, Farshad; Peiravi, Ali; Mahmoodi, Hamid

    As the CMOS manufacturing process scales down into the ultra deep sub-micron regime, the leakage current becomes an increasingly more important consideration in VLSI circuit design. In this paper, a high speed and noise immune domino logic circuit is presented which uses the property of the footer...

  16. A Nordic project on high speed low power design in sub-micron CMOS technology for mobile phones

    Olesen, Ole

    This paper is a survey paper presenting the Nordic CONFRONT project and reporting some results from the group at CIE/DTU, Denmark. The objective of the project is to demonstrate the feasibility of sub-micron CMOS for the realisation of RF front-end circuits operating at frequencies in the 1.8-2.0...

  17. Inspecting wood surface roughness using computer vision

    Zhao, Xuezeng


    Wood surface roughness is one of the important indexes of manufactured wood products. This paper presents an attempt to develop a new method to evaluate manufactured wood surface roughness through the utilization of imaging processing and pattern recognition techniques. In this paper a collimated plane of light or a laser is directed onto the inspected wood surface at a sharp angle of incidence. An optics system that consists of lens focuses the image of the surface onto the objective of a CCD camera, the CCD camera captures the image of the surface and using a CA6300 board digitizes the image. The digitized image is transmitted into a microcomputer. Through the use of the methodology presented in this paper, the computer filters the noise and wood anatomical grain and gives an evaluation of the nature of the manufactured wood surface. The preliminary results indicated that the method has the advantages of non-contact, 3D, high-speed. This method can be used in classification and in- time measurement of manufactured wood products.

  18. Ordered roughness effects on NACA 0026 airfoil

    Harun, Z.; Abbas, A. A.; Dheyaa, R. Mohammed; Ghazali, M. I.


    The effects of highly-ordered rough surface - riblets, applied onto the surface of a NACA 0026 airfoil, are investigated experimentally using wind tunnel. The riblets are arranged in directionally converging - diverging pattern with dimensions of height, h = 1 mm, pitch or spacing, s = 1 mm, yaw angle α = 0o and 10o The airfoil with external geometry of 500 mm span, 600 mm chord and 156 mm thickness has been built using mostly woods and aluminium. Turbulence quantities are collected using hotwire anemometry. Hotwire measurements show that flows past converging and diverging pattern inherit similar patterns in the near-wall region for both mean velocity and turbulence intensities profiles. The mean velocity profiles in logarithmic regions for both flows past converging and diverging riblet pattern are lower than that with yaw angle α = 0o. Converging riblets cause the boundary layer to thicken and the flow with yaw angle α = 0o produces the thinnest boundary layer. Both the converging and diverging riblets cause pronounced outer peaks in the turbulence intensities profiles. Most importantly, flows past converging and diverging pattern experience 30% skin friction reductions. Higher order statistics show that riblet surfaces produce similar effects due to adverse pressure gradient. It is concluded that a small strip of different ordered roughness features applied at a leading edge of an airfoil can change the turbulence characteristics dramatically.

  19. On mathematical structures of fuzzy rough set algebras

    WU Wei-zhi


    In rough set theory, the lower and upper approximation operators are important notions defined by a binary rela-tion. In this paper, we introduce a general type of relation-based fuzzy rough model determined by a triangular norm. Prop-erties of fuzzy rough approximation operators are examined. The fuzzy rough approximation operators are also characterized by axioms. A comparative study of the fuzzy rough set algebra with other mathematical structures such as fuzzy topological spaces, fuzzy measurable spaces, and fuzzy belief structures is investigated.

  20. Bacterial Adhesion and Surface Roughness for Different Clinical Techniques for Acrylic Polymethyl Methacrylate

    Lucas Costa de Medeiros Dantas


    Full Text Available This study sought to assess the effect of different surface finishing and polishing protocols on the surface roughness and bacterial adhesion (S. sanguinis to polymethyl methacrylates (PMMA. Fifty specimens were divided into 5 groups (n=10 according to their fabrication method and surface finishing protocol: LP (3 : 1 ratio and laboratory polishing, NF (Nealon technique and finishing, NP (Nealon technique and manual polishing, MF (3 : 1 ratio and manual finishing, and MP (3 : 1 ratio and manual polishing. For each group, five specimens were submitted to bacterial adhesion tests and analyzed by scanning electron microscopy (SEM. Two additional specimens were subjected to surface topography analysis by SEM and the remaining three specimens were subjected to surface roughness measurements. Data were compared by one-way ANOVA. The mean bacterial counts were as follows: NF, 19.6±3.05; MP, 5.36±2.08; NP, 4.96±1.93; MF, 7.36±2.45; and LP, 1.56±0.62 (CFU. The mean surface roughness values were as follows: NF, 3.23±0.15; MP, 0.52±0.05; NP, 0.60±0.08; MF, 2.69±0.12; and LP, 0.07±0.02 (μm. A reduction in the surface roughness was observed to be directly related to a decrease in bacterial adhesion. It was verified that the laboratory processing of PMMA might decrease the surface roughness and consequently the adhesion of S. sanguinis to this material.

  1. Bacterial Adhesion and Surface Roughness for Different Clinical Techniques for Acrylic Polymethyl Methacrylate.

    Dantas, Lucas Costa de Medeiros; da Silva-Neto, João Paulo; Dantas, Talita Souza; Naves, Lucas Zago; das Neves, Flávio Domingues; da Mota, Adérito Soares


    This study sought to assess the effect of different surface finishing and polishing protocols on the surface roughness and bacterial adhesion (S. sanguinis) to polymethyl methacrylates (PMMA). Fifty specimens were divided into 5 groups (n = 10) according to their fabrication method and surface finishing protocol: LP (3 : 1 ratio and laboratory polishing), NF (Nealon technique and finishing), NP (Nealon technique and manual polishing), MF (3 : 1 ratio and manual finishing), and MP (3 : 1 ratio and manual polishing). For each group, five specimens were submitted to bacterial adhesion tests and analyzed by scanning electron microscopy (SEM). Two additional specimens were subjected to surface topography analysis by SEM and the remaining three specimens were subjected to surface roughness measurements. Data were compared by one-way ANOVA. The mean bacterial counts were as follows: NF, 19.6 ± 3.05; MP, 5.36 ± 2.08; NP, 4.96 ± 1.93; MF, 7.36 ± 2.45; and LP, 1.56 ± 0.62 (CFU). The mean surface roughness values were as follows: NF, 3.23 ± 0.15; MP, 0.52 ± 0.05; NP, 0.60 ± 0.08; MF, 2.69 ± 0.12; and LP, 0.07 ± 0.02 (μm). A reduction in the surface roughness was observed to be directly related to a decrease in bacterial adhesion. It was verified that the laboratory processing of PMMA might decrease the surface roughness and consequently the adhesion of S. sanguinis to this material.

  2. Relationship between subsurface damage and surface roughness of ground optical materials

    LI Sheng-yi; WANG Zhuo; WU Yu-lie


    A theoretical model of relationship between subsurface damage and surface roughness was established to realize rapid and non-destructive measurement of subsurface damage of ground optical materials. Postulated condition of the model was that subsurface damage depth and peak-to-valley surface roughness are equal to depth of radial and lateral cracks in brittle surface induced by small-radius (radius≤200 μm) spherical indenter, respectively. And contribution of elastic stress field to the radial cracks propagation was also considered in the loading cycle. Subsurface damage depth of ground BK7 glasses was measured by magnetorheological finishing spot technique to validate theoretical ratio of subsurface damage to surface roughness. The results show that the ratio is directly proportional to load of abrasive grains and hardness of optical materials, while inversely proportional to granularity of abrasive grains and fracture toughness of optical materials. Moreover, the influence of the load and fracture toughness on the ratio is more significant than the granularity and hardness, respectively. The measured ratios of 80 grit and 120 grit fixed abrasive grinding of BK7 glasses are 5.8 and 5.4, respectively.

  3. Indomethacin submicron particle capsules provide effective pain relief in patients with acute pain: a phase 3 study.

    Altman, Roy; Daniels, Stephen; Young, Clarence L


    Although frequently prescribed to relieve acute pain in patients, non-steroidal anti-inflammatory drugs (NSAIDs) are associated with dose-related gastrointestinal, cardiovascular, and renal complications. Investigational, submicron particle NSAIDs are being developed that could provide effective pain relief at lower doses than currently available oral NSAIDs. This is the first phase 3 study evaluating the analgesic efficacy and safety of lower-dose indomethacin submicron particle capsules in patients following elective surgery. This multicenter, double-blind study enrolled patients aged 18 to 68 years who underwent bunionectomy under regional anesthesia. Patients with a pain intensity rating of ≥40 mm on a 100-mm Visual Analog Scale were randomized to receive indomethacin submicron particle capsules (40 mg 3 times daily [TID], 40 mg twice daily [BID], or 20 mg TID), celecoxib (400 mg loading dose, then 200 mg BID), or placebo. The primary efficacy parameter was the overall (summed) pain intensity difference measured by a Visual Analog Scale during a period of 48 hours. Scheduled assessments measured secondary efficacy parameters such as patient pain intensity differences. Indomethacin submicron particle capsules 40 mg 3 times daily (509.6 ± 91.9 overall [summed] pain intensity difference), 40 mg twice daily (328.0 ± 92.9 overall [summed] pain intensity difference), and 20 mg 3 times daily (380.5 ± 92.9 overall [summed] pain intensity difference) reduced pain intensity from 0 to 48 hours (P ≤ 0.046 for all 3 groups) compared with placebo (67.8 ± 91.4 overall [summed] pain intensity difference). There was some evidence of patient analgesia for celecoxib (279.4 ± 91.9 overall [summed] pain intensity difference; P = 0.103). Some evidence of pain control was observed in patients as early as 2 hours following administration of indomethacin submicron particle capsules and was sustained throughout the treatment period. Indomethacin submicron particle capsules were

  4. Vectors and submicron precision: redundancy and 3D stacking in silicon pixel detectors

    Heijne, E H M; Wong, W; Idarraga, J; Visser, J; Jakubek, J; Leroy, C; Turecek, D; Visschers, J; Pospisil, S; Ballabriga, R; Vykydal, Z; Vermeulen, J; Plackett, R; Heijne, E H M; Llopart, X; Boltje, D; Campbell, M


    Measurements are shown of GeV pions and muons in two 300 mu m thick, Si Medipix pixel detector assemblies that are stacked on top of each other, with a 25 mu m thick brass foil in between. In such a radiation imaging semiconductor matrix with a large number of pixels along the particle trail, one can determine local space vectors for the particle trajectory instead of points. This improves pattern recognition and track reconstruction, especially in a crowded environment. Stacking of sensor planes is essential for resolving directional ambiguities. Signal charge sharing can be employed for measuring positions with submicron precision. In the measurements one notices accompanying `delta' electrons that emerge outside the particle trail, far beyond the boundaries of the 55 mu m pixel cells. The frequency of such corrupted position measurements is similar to one per 2.5mm of traversed Si.

  5. Fabrication of high-quality submicron Nb/Al-AlOx/Nb tunnel junctions

    Yu Hai-Feng; Cao Wen-Hui; Zhu Xiao-Bo; Yang Hai-Fang; Yu Hong-Wei; Ren Yu-Feng; Gu Chang-Zhi; Chen Geng-Hua; Zhao Shi-Ping


    Nb/Al-AlOx/Nb tunnel junctions are often used in the studies of macroscopic quantum phenomena and supercon-ducting qubit applications of the Josepheon devices. In this work, we describe a convenient and reliable process using electron beam lithography for the fabrication of high-quality, submicron-sized Nb/Al-AlOx/Nb Josephson junctions.The technique follows the well-known selective Nb etching process and produces high-quality junctions with Vm=100 mV at 2.3 K for the typical critical current density of 2.2 kA/cm2, which can be adjusted by controlling the oxygen pressure and oxidation time during the formation of the tunnelling barrier. We present the results of the temperature depen-dence of the sub-gap current and in-plane magnetic-field dependence of the critical current, and compare them with the theoretical predictions.

  6. Occurrence of weak, sub-micron, tropospheric aerosol events at high Arctic latitudes

    O'Neill, N. T.; Pancrati, O.; Baibakov, K.; Eloranta, E.; Batchelor, R. L.; Freemantle, J.; McArthur, L. J. B.; Strong, K.; Lindenmaier, R.


    Numerous fine mode (sub-micron) aerosol optical events were observed during the summer of 2007 at the High Arctic atmospheric observatory (PEARL) located at Eureka, Nunavut, Canada. Half of these events could be traced to forest fires in southern and eastern Russia and the Northwest Territories of Canada. The most notable findings were that (a) a combination of ground-based measurements (passive sunphotometry, high spectral resolution lidar) could be employed to determine that weak (near sub-visual) fine mode events had occurred, and (b) this data combined with remote sensing imagery products (MODIS, OMI-AI, FLAMBE fire sources), Fourier transform spectroscopy and back trajectories could be employed to identify the smoke events.

  7. Experimental studies of the noise properties of a deep submicron CMOS process

    Manghisoni, M.; Re, V. E-mail:; Speziali, V.; Svelto, F


    Deep submicron CMOS technologies are presently very attractive for front-end electronics design, because of their features in terms of low power consumption, high integration density and radiation tolerance. A full understanding of the noise parameters of the devices belonging to these technologies is needed to confirm that they can be used to implement low-noise analog blocks. This paper describes a noise test system, which was purposely developed to measure the noise voltage spectrum of CMOS devices in a frequency range extending up to 100 MHz. As an application example, the results of the experimental characterization of the noise properties of a 0.35 {mu}m CMOS process are presented.

  8. Analysis of submicron-sized niflumic acid crystals prepared by electrospray crystallization.

    Ambrus, Rita; Radacsi, Norbert; Szunyogh, Tímea; van der Heijden, Antoine E D M; Ter Horst, Joop H; Szabó-Révész, Piroska


    Interest in submicron-sized drug particles has emerged from both laboratory and industrial perspectives in the last decade. Production of crystals in the nano size scale offers a novel way to particles for drug formulation solving formulation problems of drugs with low solubility in class II of the Biopharmaceutical Classification System. In this work niflumic acid nanoparticles with a size range of 200-800nm were produced by the novel crystallization method, electrospray crystallization. Their properties were compared to those from evaporative and anti-solvent crystallizations, using the same organic solvent, acetone. There is a remarkable difference in the product crystal size depending on the applied methods. The size and morphology were analyzed by scanning electron microscopy and laser diffraction. The structure of the samples was investigated using differential scanning calorimetry, Fourier-transformed infrared spectroscopy and X-ray powder diffraction. The particles produced using electrospray crystallization process were probably changing from amorphous to crystalline state after the procedure.


    V. I. Timoshenko


    Full Text Available The features of deposition of highly dispersed particles of smoke on nanoscale biological airway surface on the example of tobacco smoke are considering. A model of particle deposition of the nicotine gum along the way through the smoke inhaled. Obtain a solution of the equation for the diffusion flux changes deposited nano- and submicron particles through hydrodynamic boundary layer.The particle deposition of nicotine gum on the airways by scanning the distribution of nanoparticles deposited using an atomic force microscope SobverPRO was experimentally studied. Patterns of distribution of nanoparticles dispersed smoke 4 species of tobacco in different parts of the respiratory tract were obtained. That allowed to talk about the absence of the effect of coagulation of the airway. It was established that the child as a passive smoker particle deposition diffusive flux of nicotine is proportionally higher than adult because the channel width is less than the airways than in adults.

  10. Essential features of optical processes in neon-buffered submicron-thin Rb vapor cell.

    Hakhumyan, Grant; Sargsyan, Armen; Leroy, Claude; Pashayan-Leroy, Yevgenya; Papoyan, Aram; Sarkisyan, David


    A new submicron thin cell (STC) filled with Rb and neon gas is developed and comparison of resonant absorption with STC containing pure Rb is provided. The effect of collapse and revival of Dicke-type narrowing is still observable for the thickness L = lambda /2 and L = lambda , where lambda is a resonant laser wavelength 794 nm (D(1) line). For an ordinary Rb cm-size cell with addition of buffer gas, the velocity selective optical pumping/saturation (VSOP) resonances in saturated absorption spectra are fully suppressed if neon pressure > 0.5 Torr. A spectacular difference is that for L = lambda , VSOP resonances are still observable even when neon pressure is > or = 6 Torr. Narrow fluorescence spectra at L = lambda /2 allow one to realize online buffer gas pressure monitoring. A good agreement with theoretical model is observed.

  11. Instabilities in the current-voltage characteristics of submicron BSCCO bridges

    Zybtsev, S G [Institute of Radioengineering and Electronics RAS Moscow 125009 (Russian Federation); Pokrovskii, V Ya [Institute of Radioengineering and Electronics RAS Moscow 125009 (Russian Federation); Gorlova, I G [Institute of Radioengineering and Electronics RAS Moscow 125009 (Russian Federation); Latyshev, Yu I [Institute of Radioengineering and Electronics RAS Moscow 125009 (Russian Federation); Timofeev, V N [A.A. Baikov Institute of Metallurgy RAS Moscow (Russian Federation)


    The influence of magnetic field and microwave irradiation on dynamical phase separation in submicron Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+x} bridges has been studied. Strong effect on the shape and metastable character of the step-like I-V characteristics are found. Under a weak field H < 2 Oe and low level microwave irradiation the step-like structure of the I-V characteristics smears out and disappears completely. The average frequency of switching between metastable states grows by 5 orders under increase of magnetic field by only 1 Oe. This behavior is explained in terms of the model of dynamical vortex lines.

  12. Size-selective separation of submicron particles in suspensions with ultrasonic atomization.

    Nii, Susumu; Oka, Naoyoshi


    Aqueous suspensions containing silica or polystyrene latex were ultrasonically atomized for separating particles of a specific size. With the help of a fog involving fine liquid droplets with a narrow size distribution, submicron particles in a limited size-range were successfully separated from suspensions. Performance of the separation was characterized by analyzing the size and the concentration of collected particles with a high resolution method. Irradiation of 2.4MHz ultrasound to sample suspensions allowed the separation of particles of specific size from 90 to 320nm without regarding the type of material. Addition of a small amount of nonionic surfactant, PONPE20 to SiO2 suspensions enhanced the collection of finer particles, and achieved a remarkable increase in the number of collected particles. Degassing of the sample suspension resulted in eliminating the separation performance. Dissolved air in suspensions plays an important role in this separation.

  13. Ubiquity of organic nitrates from nighttime chemistry in the European submicron aerosol

    Kiendler-Scharr, A.; Mensah, A. A.; Friese, E.; Topping, D.; Nemitz, E.; Prevot, A. S. H.; ńijälä, M.; Allan, J.; Canonaco, F.; Canagaratna, M.; Carbone, S.; Crippa, M.; Dall Osto, M.; Day, D. A.; De Carlo, P.; Di Marco, C. F.; Elbern, H.; Eriksson, A.; Freney, E.; Hao, L.; Herrmann, H.; Hildebrandt, L.; Hillamo, R.; Jimenez, J. L.; Laaksonen, A.; McFiggans, G.; Mohr, C.; O'Dowd, C.; Otjes, R.; Ovadnevaite, J.; Pandis, S. N.; Poulain, L.; Schlag, P.; Sellegri, K.; Swietlicki, E.; Tiitta, P.; Vermeulen, A.; Wahner, A.; Worsnop, D.; Wu, H.-C.


    In the atmosphere nighttime removal of volatile organic compounds is initiated to a large extent by reaction with the nitrate radical (NO3) forming organic nitrates which partition between gas and particulate phase. Here we show based on particle phase measurements performed at a suburban site in the Netherlands that organic nitrates contribute substantially to particulate nitrate and organic mass. Comparisons with a chemistry transport model indicate that most of the measured particulate organic nitrates are formed by NO3 oxidation. Using aerosol composition data from three intensive observation periods at numerous measurement sites across Europe, we conclude that organic nitrates are a considerable fraction of fine particulate matter (PM1) at the continental scale. Organic nitrates represent 34% to 44% of measured submicron aerosol nitrate and are found at all urban and rural sites, implying a substantial potential of PM reduction by NOx emission control.

  14. Stochastic process variation in deep-submicron CMOS circuits and algorithms

    Zjajo, Amir


    One of the most notable features of nanometer scale CMOS technology is the increasing magnitude of variability of the key device parameters affecting performance of integrated circuits. The growth of variability can be attributed to multiple factors, including the difficulty of manufacturing control, the emergence of new systematic variation-generating mechanisms, and most importantly, the increase in atomic-scale randomness, where device operation must be described as a stochastic process. In addition to wide-sense stationary stochastic device variability and temperature variation, existence of non-stationary stochastic electrical noise associated with fundamental processes in integrated-circuit devices represents an elementary limit on the performance of electronic circuits. In an attempt to address these issues, Stochastic Process Variation in Deep-Submicron CMOS: Circuits and Algorithms offers unique combination of mathematical treatment of random process variation, electrical noise and temperature and ne...

  15. Formation of stable submicron peptide or protein particles by thin film freezing

    Johnston, Keith P.; Engstrom, Joshua; Williams, III, Robert O.


    The present invention includes compositions and methods for preparing micron-sized or submicron-sized particles by dissolving a water soluble effective ingredient in one or more solvents; spraying or dripping droplets solvent such that the effective ingredient is exposed to a vapor-liquid interface of less than 50, 100, 150, 200, 250, 200, 400 or 500 cm.sup.-1 area/volume to, e.g., increase protein stability; and contacting the droplet with a freezing surface that has a temperature differential of at least C. between the droplet and the surface, wherein the surface freezes the droplet into a thin film with a thickness of less than 500 micrometers and a surface area to volume between 25 to 500 cm.sup.-1.

  16. Differential Equations driven by \\Pi-rough paths

    Gyurkó, Lajos Gergely


    This paper revisits the concept of rough paths of inhomogeneous degree of smoothness (geometric \\Pi-rough paths in our terminology) sketched by Lyons ("Differential equations driven by rough signals", Revista Mathematica Iber. Vol 14, Nr. 2,215-310, 1998). Although geometric \\Pi-rough paths can be treated as p-rough paths for a sufficiently large p and the theory of integration of Lip-\\gamma one-forms (\\gamma>p-1) along geometric p-rough paths applies, we prove the existence of integrals of one-forms under weaker conditions. Moreover, we consider differential equations driven by geometric \\Pi-rough paths and give sufficient conditions for existence and uniqueness of solution.

  17. Bio-inspired canopies for the reduction of roughness noise

    Clark, Ian A.; Daly, Conor A.; Devenport, William; Alexander, W. Nathan; Peake, Nigel; Jaworski, Justin W.; Glegg, Stewart


    This work takes inspiration from the structure of the down covering the flight feathers of larger species of owls, which contributes to their ability to fly almost silently at frequencies above 1.6 kHz. Microscope photographs of the down show that it consists of hairs that form a structure similar to that of a forest. The hairs initially rise almost perpendicular to the feather surface but then bend over in the flow direction to form a canopy with an open area ratio of about 70 percent. Experiments have been performed to examine the noise radiated by a large open area ratio canopy suspended above a surface. The canopy is found to dramatically reduce pressure fluctuations on the underlying surface. While the canopy can produce its own sound, particularly at high frequencies, the reduction in surface pressure fluctuations can reduce the noise scattered from an underlying rough surface at lower frequencies. A theoretical model is developed which characterizes the mechanism of surface pressure reduction as a result of the mixing layer instability of flow over forest canopies.

  18. A phase 2 study of lower-dose, indomethacin submicron particle capsules demonstrates early onset of acute pain relief.

    Manvelian, Garen; Hochberg, Marc C; Daniels, Stephen E; Altman, Roy D; Young, Clarence L


    Nonsteroidal anti-inflammatory drugs are efficacious for the treatment of acute and chronic pain; however, they have the potential for serious adverse events (AEs). The objective of this study was to evaluate the efficacy and safety of investigational, lower-dose, indomethacin submicron particle capsules compared with placebo in a study of patients with postsurgical pain. This phase 2, multicenter, randomized, double-blind, single-dose, and placebo-controlled study enrolled 203 patients (18 to 50 y old) following extraction of ≥ 2 third molars who experienced moderate-to-severe pain intensity ≤ 6 hours after surgery. Patients received indomethacin submicron particle capsules (20 or 40 mg), celecoxib 400 mg, or placebo. The primary efficacy endpoint was the sum of total pain relief over 0 to 8 hours (TOTPAR-8) determined from the area under the curve for pain relief over 0 to 8 hours following administration of the study drug, where pain relief was measured on a 0 to 4 scale. Safety and tolerability were also assessed. Mean ± SE TOTPAR-8 scores were 10.8 ± 1.4 (indomethacin submicron particle capsules 20 mg), 12.6 ± 1.3 (indomethacin submicron particle capsules 40 mg), 14.8 ± 1.3 (celecoxib), and 3.0 ± 1.3 (placebo; Pcapsules treatment groups demonstrated better mean TOTPAR over 4 hours than placebo (Pcapsules provide good overall pain relief in patients with postsurgical pain and are generally well tolerated. Indomethacin submicron particle capsules are a potentially promising option for treatment of acute pain and warrant further study.

  19. Influence of surface roughness on nonlinear flow behaviors in 3D self-affine rough fractures: Lattice Boltzmann simulations

    Wang, Min; Chen, Yi-Feng; Ma, Guo-Wei; Zhou, Jia-Qing; Zhou, Chuang-Bing


    This study investigates the impacts of surface roughness on the nonlinear fluid flow through three-dimensional (3D) self-affine rock fractures, whose original surface roughness is decomposed into primary roughness (i.e. the large-scale waviness of the fracture morphology) and secondary roughness (i.e. the small-scale unevenness) with a wavelet analysis technique. A 3D Lattice Boltzmann method (LBM) is adopted to predict the flow physics in rock fractures numerically created with and without consideration of the secondary roughness, respectively. The simulation results show that the primary roughness mostly controls the pressure distribution and fracture flow paths at a large scale, whereas the secondary roughness determines the nonlinear properties of the fluid flow at a local scale. As the pressure gradient increases, the secondary roughness enhances the local complexity of velocity distribution by generating and expanding the eddy flow and back flow regions in the vicinity of asperities. It was found that the Forchheimer's law characterizes well the nonlinear flow behavior in fractures of varying roughness. The inertial effects induced by the primary roughness differ only marginally in fractures with the roughness exponent varying from 0.5 to 0.8, and it is the secondary roughness that significantly enhances the nonlinear flow and leads to earlier onset of nonlinearity. Further examined were the effects of surface roughness on the transmissivity, hydraulic aperture and the tortuosity of flow paths, demonstrating again the dominant role of the secondary roughness, especially for the apparent transmissivity and the equivalent hydraulic aperture at high pressure gradient or high Reynolds number. The results may enhance our understanding of the role of surface roughness in the nonlinear flow behaviors in natural rock fractures.

  20. Numerical modeling of multiphase flow in rough and propped fractures

    Dabrowski, Marcin; Dzikowski, Michał; Jasinski, Lukasz; Olkiewicz, Piotr


    crystalline rocks. The detailed pattern of flow paths and effective fracture conductivity are largely dependent on the level of confining stresses and fracture wall roughness, which both determine the shape and distribution of fracture apertures and contact areas. The distribution of proppant grains, which are used to maintain apertures of hydraulic fractures, is a key factor governing fracture flow in industrial applications. The flow of multiphase fluids in narrow apertures of rock fractures may substantially differ from the flow of a single-phase fluid. For example, multiphase flow effects play an important role during all stages of unconventional reservoir life cycle. Multiphase flow conditions are also expected to prevail in high temperature geothermal fields and during the transport of non aqueous phase liquid contaminants in groundwaters. We use direct numerical simulations to study single- and multiphase flow in rough and propped fractures. We compute the fluid flow using either the finite element or the lattice Boltzmann method. Body-fitting, unstructured computational meshes are used to improve the numerical accuracy. The fluid-fluid and fluid-solid interfaces are directly resolved and an implicit approach to surface tension is used to alleviate restrictions due to capillary CFL condition. In FEM simulations, the Beltrami-Laplace operator is integrated by parts to avoid interface curvature computation during evaluation of the surface tension term. We derive and validate an upscaled approach to Stokes flow in propped and rough fractures. Our upscaled 2.5D fracture flow model features a Brinkman term and is capable of treating no-slip boundary conditions on the rims of proppant grains and fracture wall contact areas. The Stokes-Brinkman fracture flow model provides an improvement over the Reynolds model, both in terms of the effective fracture permeability and the local flow pattern. We present numerical and analytical models for the propped fracture

  1. Skin friction measurements of mathematically generated roughness in the transitionally- to fully-rough regimes

    Barros, Julio; Schultz, Michael; Flack, Karen


    Engineering systems are affected by surface roughness which cause an increase in drag leading to significant performance penalties. One important question is how to predict frictional drag purely based upon surface topography. Although significant progress has been made in recent years, this has proven to be challenging. The present work takes a systematic approach by generating surface roughness in which surfaces parameters, such as rms , skewness, can be controlled. Surfaces were produced using the random Fourier modes method with enforced power-law spectral slopes. The surfaces were manufactured using high resolution 3D-printing. In this study three surfaces with constant amplitude and varying slope, P, were investigated (P = - 0 . 5 , - 1 . 0 , - 1 . 5). Skin-friction measurements were conducted in a high Reynolds number turbulent channel flow facility, covering a wide range of Reynolds numbers, from hydraulic-smooth to fully-rough regimes. Results show that some long wavelength roughness scales do not contribute significantly to the frictional drag, thus highlighting the need for filtering in the calculation of surface statistics. Upon high-pass filtering, it was found that krms is highly correlated with the measured ks.

  2. Simulation and Modeling of Submicron Semiconductor Devices by a New Hydrodynamic Method.

    Lin, Qi.

    Robust numerical methods for the solution of the hydrodynamic model are developed and implemented for the simulation of submicron semiconductor devices. The hydrodynamic equations are reformulated into readily solvable self-adjoint forms with the aid of newly defined HD-Slotboom state variables. A new discretization strategy is developed to resolve the rapid variation in the carrier densities and carrier temperatures. The approach also yields a coefficient matrix for each discretized hydrodynamic equation, which is guaranteed to be diagonally dominant. The hydrodynamic equations are decoupled by using a Gummel block iteration method. A fixed-point iteration technique is employed to solve the discretized equations, which guarantees that each decoupled equation converges for any starting value. Furthermore, the decoupling of equations and use of the fixed-point iteration scheme obviate the need for direct solutions of large matrix equations, and thereby eliminate the need for large memory allocations. The algorithm is inherently parallel, so it can be readily implemented on parallel machines to increase computation speed. Using these methods, several simulation packages are developed for the analysis of one-dimensional (1-D) n^+-n-n^+ devices, and square electric fields, two-dimensional (2-D) & three-dimensional (3-D) MOSFET's, and two-dimensional SOI MOSFET's. Various simulation results for these devices are presented. Some one-dimensional simulation results are compared with Monte Carlo calculations, and a good agreement is observed. Also convergence, stability, and efficiency of the methods are examined by a set of numerical experiments. The device simulators are applied to investigate the hot-electron induced degradation in submicron SOI devices and EPROM's. The impact of localized interface charge on device characteristics is studied. Some measured results are used to calibrate the process parameters in the simulators so that the simulators can predict device

  3. Analysis of major air pollutants and submicron particles in New York City and Long Island

    Masiol, M.; Hopke, P. K.; Felton, H. D.; Frank, B. P.; Rattigan, O. V.; Wurth, M. J.; LaDuke, G. H.


    A year-long sampling campaign of major air pollutants and submicron particle number size distributions was conducted at two sites taken as representative of city-wide air quality in New York City and Long Island, respectively. A number of species were quantified with hourly time resolution, including particle number concentrations in 6 size ranges (20-30 nm, 30-50 nm, 50-70 nm, 70-100 nm, 100-200 nm, and >200 nm), nitrogen oxides, sulfur dioxide, ozone, carbon monoxide, methane, non-methane hydrocarbons, PM2.5 mass concentration and some PM major components (sulfate, organic and elemental carbon). Hourly concentrations of primary and secondary organic carbon were estimated using the EC tracer method. Data were matched with weather parameters and air parcel back-trajectories. A series of tools were thus applied to: (i) study the seasonal, weekly, diurnal cycles of pollutants; (ii) investigate the relationships amongst pollutants through correlation and lagged correlation analyses; (iii) depict the role of atmospheric photochemical processes; (iv) examine the location of the potential sources by mean of conditional bivariate probability function analysis and (v) investigate the role of regional transport of air masses to the concentrations of analyzed species. Results indicate that concentrations of NOx, SO2, CO, non-methane hydrocarbons, primary OC and EC are predominantly determined by local sources, but are also affected by regional transports of polluted air masses. On the contrary, the transport of continental polluted air masses has a main effect in raising the concentrations of secondary PM2.5 (sulfate and secondary organic carbon). By providing direct information on the concentrations and trends of key pollutants and submicron particle number concentrations, this study finally enables some general considerations about air quality status and atmospheric processes over the New York City metropolitan area.

  4. Bacterial characterization in ambient submicron particles during severe haze episodes at Ji'nan, China.

    Xu, Caihong; Wei, Min; Chen, Jianmin; Wang, Xinfeng; Zhu, Chao; Li, Jiarong; Zheng, Lulu; Sui, Guodong; Li, Weijun; Wang, Wenxing; Zhang, Qingzhu; Mellouki, Abdelwahid


    In January 2014, severe haze episodes which sweep across Chinese cities have attracted public concern and interest at home and abroad. In addition to the physicochemical properties of air pollutants, bacteria are thought to be responsible for the spread of respiratory diseases and various allergies. We attempted the bacterial characterization of submicron particles (PM0.18-0.32, PM0.32-0.56, and PM0.56-1) under severe haze episodes using high-throughput sequencing and real-time quantitative PCR detecting system based on 21 samples collected from January to March 2014 at Ji'nan, China. The high bacterial concentration in PM0.32-0.56 (7314cells m(-3)), PM0.18-0.32 (7212cells m(-3)), and PM0.56-1 (6982cells m(-3)) showed significant negative correlations with SO2, NO2, and O3. Under sufficient sequencing depth, 37 phyla, 71 classes, 137 orders, 236 families, and 378 genera were classified, and the bacterial community structure varied significantly in different size fractions. For example, Holophagaceae (Acidobacteria) in PM0.32-0.56 showed 6-fold higher abundance than that in PM0.18-0.32. Moreover, functional categories and bacterial species (Lactococcus piscium, Pseudomonas fragi, Streptococcus agalactiae, and Pseudomonas cichorii) that may potentially be responsible for infections and allergies were also discovered. Source track analysis showed that the ambient bacteria mainly originated from soils, leaf surfaces, and feces. Our results highlighted the importance of airborne microbial communities by understanding the concentration, structure, ecological and health effects, especially those in submicron particles during haze episodes.

  5. Adjustment of roughness sublayer in turbulent flows over two-dimensional idealised roughness elements

    HO, Yat-Kiu; LIU, Chun-Ho


    The atmospheric boundary layer (ABL) immediately above the urban canopy is the roughness sublayer (RSL). In this layer, flows and turbulence are strongly affected by the roughness elements beneath, e.g. building obstacles. The wind flows over urban areas could be represented by conventional logarithmic law of the wall (log-law) in the neutrally stratified ABL. However, in the RSL region, the vertical wind profile deviates from that predicted from log-law and the effect could be extended from ground level up to several canopy heights. As a result, the Monin-Obukhov similarity theory (MOST) fails and an additional length scale is required to describe the flows. The key aim of this study is to introduce a simple wind profile model which accounts for the effect of the RSL in neutral stratification using wind tunnel experiments. Profile measurements of wind speeds and turbulence quantities over various two-dimensional (2D) idealised roughness elements are carried out in an open-circuit wind tunnel with test section of size 560 mm (width) × 560 mm (height) × 6 m (length). The separation between the roughness elements is varied systematically so that ten different types of surface forms are adopted. The velocity measurements are obtained by hot-wire anemometry using X-probe design (for UW- measurements) with a constant temperature anemometer. For each configuration, eight vertical profiles are collected over the canopy, including solid boundaries and cavities of the roughness elements. Firstly, we compute the measurement results using conventional MOST to determine different roughness parameters. Afterwards, we derive the RSL height from the Reynolds stress profiles. Since the profiles taken from different locations of the canopy are eventually converged with increasing height, we use this 'congregated height' to define the RSL height. Next, we introduce an alternative function, i.e. power-law function, instead of MOST, to describe the velocity profile in attempt to

  6. Phase transformation and intense 2.7 μm emission from Er3+ doped YF3/YOF submicron-crystals.

    Chai, Guanqi; Dong, Guoping; Qiu, Jianrong; Zhang, Qinyuan; Yang, Zhongmin


    Yttrium fluoride YF3:Er(3+) and yttrium oxyfluoride YOF:Er(3+) submicron-crystals with mid-infrared fluorescent emissions were synthesized for the first time. The rhombohedral phase YOF submicron-crystals were synthesized by the crystalline phase transformation from pure orthorhombic YF3 submicron-crystals, which were prepared by co-precipitation method. The composition and morphology were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscopy (TEM), which showed that submicron-crystals were quasi-spherical with the particle size of ~400 nm. A novel formation mechanism of YOF submicron-crystals was proposed. Photoluminescence (PL) spectra indicated the 2.7 μm emission of Er(3+) has remarkably enhanced with the increase of Er(3+) doping concentration, and a novel dynamic circulatory energy transfer mechanism was proposed. Fourier transform infrared spectra (FTIR) were used to demonstrate the change of hydroxyl content. These oxyfluoride submicron-crystals provide a new material for nano/submicron-crystals-glass composites, and open a brand new field for the realization of mid-infrared micro/nano-lasers.

  7. Plume Dispersion over Idealized Urban-liked Roughness with Height Variation: an LES Approach

    Wong, Colman Ching Chi; Liu, Chun-Ho


    Human activities (e.g. vehicular emission) are the primary pollutant sources affecting the health and living quality of stakeholders in modern compact cities. Gaussian plume dispersion model is commonly used for pollutant distribution estimate that works well over rural areas with flat terrain. However, its major parameters, dispersion coefficients, exclude the effect of surface roughness that unavoidably prone to error handling the pollutant transport in the urban boundary layer (UBL) over building roughness. Our recent large-eddy simulation (LES) has shown that urban surfaces affect significantly the pollutant dispersion over idealized, identical two-dimensional (2D) street canyons of uniform height. As an extension to our on-going effort, this study is conceived to investigate how rough urban surfaces, which are constructed by 2D street canyons of non-uniform height, modify the UBL pollutant dispersion . A series of LESs with idealized roughness elements of non-uniform heights were performed in neutral stratification. Building models with two different heights were placed alternatively in the computational domain to construct 2D street canyons in cross flows. The plume dispersion from a ground-level passive pollutant source over more realistic urban areas was then examined. Along with the existing building-height-to-street-width (aspect) ratio (AR), a new parameter, building-height variability (BHV), is used to measure the building height unevenness. Four ARs (1, 0.5, 0.25 and 0.125) and three BHVs (20%, 40% and 60%) were considered in this study. Preliminary results show that BHV greatly increases the aerodynamic roughness of the hypothetical urban surfaces for narrow street canyons. Analogous to our previous findings, the air exchange rate (ACH) of street canyons increases with increasing friction factor, implying that street-level ventilation could be improved by increasing building roughness via BHV. In addition, the parameters used in dispersion coefficient



    The characteristics of the roughness coefficient are very important for practical application. Some experiments are conducted to study the variation of Manning's n with flow depth, mean velocity, and density of vegetation,. An assumed velocity distribution to describe the vegetative flow of submerged vegetation is confirmed by experimental results. The measured velocities in this study seem to have little effect on the curve of n ~ h, and a new linear relationship between Manning's n and flow depths is observed clearly. According to the arguments that the flow resistance of densely unsubmerged vegetation is dominated by the resistance exerted on vegetations, the influence of the density of vegetation on Manning's n is estimated. On the basis of the velocity distribution, the n ~ h curve under submerged condition is theoretically obtained from the n ~ h curve under unsubmerged condition. These results are also well confirmed by experimental results and very significant for practical applications.

  9. Rough differential equations with unbounded drift term

    Riedel, S.; Scheutzow, M.


    We study controlled differential equations driven by a rough path (in the sense of T. Lyons) with an additional, possibly unbounded drift term. We show that the equation induces a solution flow if the drift grows at most linearly. Furthermore, we show that the semiflow exists assuming only appropriate one-sided growth conditions. We provide bounds for both the flow and the semiflow. Applied to stochastic analysis, our results imply strong completeness and the existence of a stochastic (semi)flow for a large class of stochastic differential equations. If the driving process is Gaussian, we can further deduce (essentially) sharp tail estimates for the (semi)flow and a Freidlin-Wentzell-type large deviation result.

  10. Quantitative Characterization of Boundary Roughness in Metals

    Sun, Jun

    structural aspects into account, a detailed characterization is essential of partly recrystallized microstructures focusing on the local shapes of the boundaries, in particular on whether protrusions and retrusions are formed or not. Quantification of the “amount” of boundary roughness in the form......The boundary migration during recrystallization is by nature a heterogeneous process and local structural variations form on recrystallization boundaries, as revealed from modern techniques such as synchrotron X-rays and advanced electron microscopy. The local structural variations, in the form...... variable to obtain information of local structural variations such as protrusions and retrusions formed on recrystallization boundaries. The AII value is directionindependent allowing unbiased characterization of morphological irregularities with both closed and non-closed boundary profiles. The length...

  11. Reproducibility of surface roughness in reaming

    Müller, Pavel; De Chiffre, Leonardo

    concentration of the oil in water-based cutting fluid (or when using a straight mineral oil) results in surface profiles that are more reproducible at higher cutting speed. Moreover, it can be seen that three cutting fluids (two water-based cutting fluids with different oil concentration and a straight mineral......An investigation on the reproducibility of surface roughness in reaming was performed to document the applicability of this approach for testing cutting fluids. Austenitic stainless steel was used as a workpiece material and HSS reamers as cutting tools. Reproducibility of the results was evaluated...... oil) used in connection with a low cutting speed result in "identical" surface profiles. Biggest uncertainty contributors were due to the process repeatability and repeatability around the hole circumference. This was however only in the case of high cutting speeds and low degree of oil concentration...

  12. Rough set-based feature selection method

    ZHAN Yanmei; ZENG Xiangyang; SUN Jincai


    A new feature selection method is proposed based on the discern matrix in rough set in this paper. The main idea of this method is that the most effective feature, if used for classification, can distinguish the most number of samples belonging to different classes. Experiments are performed using this method to select relevant features for artificial datasets and real-world datasets. Results show that the selection method proposed can correctly select all the relevant features of artificial datasets and drastically reduce the number of features at the same time. In addition, when this method is used for the selection of classification features of real-world underwater targets,the number of classification features after selection drops to 20% of the original feature set, and the classification accuracy increases about 6% using dataset after feature selection.

  13. Comparison among sea surface roughness schemes


    Based on the measurements from the US National Data Buoy Center 3-m discus buoy site No.44004 (38.5°N, 70.47°W) from January 1 to March 31 of 2003, with the COARE algorithm (Version 3.0), the results from four parameterization schemes developed recently for sea surface aerodynamic roughness length were compared with each other. Calculations of frictional speed u*, drag coefficient Cd and wind stress τ indicate that the calculated frictional velocities from the four schemes (8.50%-16.20%, the normalized standard error estimate, or NSEE), the computed drag coefficients and wind stress (respectively 15.08%-28.67% and 17.26%-50.59% NSEE) are reasonable. Schemes YT96 and GW03 are consistent. The O02 scheme gives overestimated values for u* and Cd. Schemes TY01 and GW03 display discontinuous characteristics in handling young wave data.

  14. Surface roughness evolution on experimentally simulated faults

    Renard, François; Mair, Karen; Gundersen, Olav


    To investigate the physical processes operating in active fault zones, we conduct analogue laboratory experiments where we track the morphological and mechanical evolution of an interface during slip. Our laboratory friction experiments consist of a halite (NaCl) slider held under constant normal load that is dragged across a coarse sandpaper substrate. This set-up is a surrogate for a fault surface, where brittle and plastic deformation mechanisms operate simultaneously during sliding. Surface morphology evolution, frictional resistance and infra-red emission are recorded with cumulative slip. After experiments, we characterize the roughness developed on slid surfaces, to nanometer resolution, using white light interferometry. We directly observe the formation of deformation features, such as slip parallel linear striations, as well as deformation products or gouge. The striations are often associated with marginal ridges of positive relief suggesting sideways transport of gouge products in the plane of the slip surface in a snow-plough-like fashion. Deeper striations are commonly bounded by triangular brittle fractures that fragment the salt surface and efficiently generate a breccia or gouge. Experiments with an abundance of gouge at the sliding interface have reduced shear resistance compared to bare surfaces and we show that friction is reduced with cumulative slip as gouge accumulates from initially bare surfaces. The relative importance of these deformation mechanisms may influence gouge production rate, fault surface roughness evolution, as well as mechanical behavior. Finally, our experimental results are linked to Nature by comparing the experimental surfaces to an actual fault surface, whose striated morphology has been characterized to centimeter resolution using a laser scanner. It is observed that both the stress field and the energy dissipation are heterogeneous at all scales during the maturation of the interface with cumulative slip. Importantly

  15. Enhanced thermoelectric performance of rough silicon nanowires.

    Hochbaum, Allon I; Chen, Renkun; Delgado, Raul Diaz; Liang, Wenjie; Garnett, Erik C; Najarian, Mark; Majumdar, Arun; Yang, Peidong


    Approximately 90 per cent of the world's power is generated by heat engines that use fossil fuel combustion as a heat source and typically operate at 30-40 per cent efficiency, such that roughly 15 terawatts of heat is lost to the environment. Thermoelectric modules could potentially convert part of this low-grade waste heat to electricity. Their efficiency depends on the thermoelectric figure of merit ZT of their material components, which is a function of the Seebeck coefficient, electrical resistivity, thermal conductivity and absolute temperature. Over the past five decades it has been challenging to increase ZT > 1, since the parameters of ZT are generally interdependent. While nanostructured thermoelectric materials can increase ZT > 1 (refs 2-4), the materials (Bi, Te, Pb, Sb, and Ag) and processes used are not often easy to scale to practically useful dimensions. Here we report the electrochemical synthesis of large-area, wafer-scale arrays of rough Si nanowires that are 20-300 nm in diameter. These nanowires have Seebeck coefficient and electrical resistivity values that are the same as doped bulk Si, but those with diameters of about 50 nm exhibit 100-fold reduction in thermal conductivity, yielding ZT = 0.6 at room temperature. For such nanowires, the lattice contribution to thermal conductivity approaches the amorphous limit for Si, which cannot be explained by current theories. Although bulk Si is a poor thermoelectric material, by greatly reducing thermal conductivity without much affecting the Seebeck coefficient and electrical resistivity, Si nanowire arrays show promise as high-performance, scalable thermoelectric materials.

  16. Characterization of rough interfaces obtained by boriding

    Campos-Silva, I. [Instituto Politecnico Nacional, SEPI-ESIME, U.P. Adolfo Lopez Mateos, Zacatenco, Mexico D.F. 07738 (Mexico)], E-mail:; Balankin, A.S. [Instituto Politecnico Nacional, SEPI-ESIME, U.P. Adolfo Lopez Mateos, Zacatenco, Mexico D.F. 07738 (Mexico); Sierra, A.H. [Instituto Politecnico Nacional, UPIICSA, Av. Te 950, Col Granjas, Mexico D.F. 08400 (Mexico); Lopez-Perrusquia, N. [Instituto Politecnico Nacional, SEPI-ESIME, U.P. Adolfo Lopez Mateos, Zacatenco, Mexico D.F. 07738 (Mexico); Escobar-Galindo, R. [Instituto de Ciencia de Materiales de Madrid (CSIC), Cantoblanco, Madrid E-28049 (Spain); Morales-Matamoros, D. [Instituto Mexicano del Petroleo, Eje Lazaro Cardenas Norte, Mexico D.F. 07738 (Mexico)


    This study evaluates the morphology of borided interfaces by means of the fractal theory. The boride layers were formed in the AISI M2 steel by applying the paste boriding treatment at temperatures of 1253 and 1273 K and treatment times of 2 and 6 h, while a boron carbide paste thickness of 4 or 5 mm covered the samples surface in order to produce the boron diffusion. The morphology of interfaces formed between FeB and Fe{sub 2}B layers and between Fe{sub 2}B layer and steel substrate was analyzed by the rescaled-range (R/S), root-mean-square (RMS), and Fourier power spectrum (FPS) methods. Moreover, the multi-affine spectra of roughness exponent were obtained by calculating the q-order height-height correlation functions. We found that both interfaces are multi-affine, rather than self-affine. The multi-affine spectra of roughness exponents are found to be different for FeB/Fe{sub 2}B and Fe{sub 2}B/substrate interfaces, but independent on the treatment parameters (boron carbide paste thickness, temperature, and boriding time). Furthermore, we found that the multi-affine spectra of both interfaces behave as it is expected for 'universal multi-fractals' with the Levy index {gamma} = 1, associated with the multiplicative cascades with a log-Cauchy distribution. Furthermore, our data suggest a great homogeneity of the boron diffusion field, characterized by universal fractal dimension D{sub diff} = 2.90 {+-} 0.01. These findings provide a novel insight into the nature of phase formation during the boriding treatment.

  17. Roughness coefficient and its uncertainty in gravel-bed river

    Ji-Sung KIM; Chan-Joo LEE; Won KIM; Yong-Jeon KIM


    Manning's roughness coefficient was estimated for a gravel-bed river reach using field measurements of water level and discharge,and the applicability of various methods used for estimation of the roughness coefficient was evaluated.Results show that the roughness coefficient tends to decrease with increasing discharge and water depth,and over a certain range it appears to remain constant.Comparison of roughness coefficients calculated by field measurement data with those estimated by other methods shows that,although the field-measured values provide approximate roughness coefficients for relatively large discharge,there seems to be rather high uncertainty due to the difference in resultant values.For this reason,uncertainty related to the roughness coefficient was analyzed in terms of change in computed variables.On average,a 20%increase of the roughness coefficient causes a 7% increase in the water depth and an 8% decrease in velocity,but there may be about a 15% increase in the water depth and an equivalent decrease in velocity for certain cross-sections in the study reach.Finally,the validity of estimated roughness coefficient based on field measurements was examined.A 10% error in discharge measurement may lead to more than 10% uncertainty in roughness coefficient estimation,but corresponding uncertainty in computed water depth and velocity is reduced to approximately 5%.Conversely,the necessity for roughness coefficient estimation by field measurement is confirmed.

  18. Covering Based Optimistic Multigranular Approximate Rough Equalities and their Properties



    Full Text Available Since its inception rough set theory has proved itself to be one of the most important models to capture impreciseness in data. However, it was based upon the notion of equivalence relations, which are relatively rare as far as applicability is concerned. So, the basic rough set model has been extended in many directions. One of these extensions is the covering based rough set notion, where a cover is an extension of the concept of partition; a notion which is equivalent to equivalence relation. From the granular computing point of view, all these rough sets are unigranular in character; i.e. they consider only a singular granular structure on the universe. So, there arose the necessity to define multigranular rough sets and as a consequence two types of multigranular rough sets, called the optimistic multigranular rough sets and pessimistic rough sets have been introduced. Four types of covering based optimistic multigranular rough sets have been introduced and their properties are studied. The notion of equality of sets, which is too stringent for real life applications, was extended by Novotny and Pawlak to define rough equalities. This notion was further extended by Tripathy to define three more types of approximate equalities. The covering based optimistic versions of two of these four approximate equalities have been studied by Nagaraju et al recently. In this article, we study the other two cases and provide a comparative analysis.

  19. Trends and sources of ozone and sub-micron aerosols at the Mt. Bachelor Observatory (MBO) during 2004-2015

    Zhang, Lei; Jaffe, Daniel A.


    In this paper, we report the climatology of tropospheric ozone (O3) and sub-micron aerosol scattering at the Mt. Bachelor Observatory (MBO, 2.8 km asl) in central Oregon, USA, during 2004-2015. The seasonal cycle for O3 showed a bimodal pattern with peaks in April and July, while aerosol scattering (σsp) was lognormally distributed with a very high peak in August and a smaller peak in May. The mean O3 concentrations showed positive and significant trends in all seasons except winter, with a slope of 0.6-0.8 ppbv yr-1. Monthly criteria for isolating free tropospheric (FT) and boundary layer influenced (BLI) air masses at MBO were obtained based on comparison of MBO water vapor (WV) distributions to those of Salem (SLE) and Medford (MFR), Oregon, at equivalent pressure level. In all seasons, FT O3 was, on average, higher than BLI O3, but the seasonal patterns were rather similar. For σsp the FT mean in spring was higher, but the BLI mean in summer was significantly higher, indicating the importance of regional wildfire smoke. To better understand the causes for the seasonal and interannual trends at MBO, we identified four major categories of air masses that impact O3, carbon monoxide (CO) and aerosols: upper troposphere and lower stratosphere (UTLS) O3 intrusion, Asian long-range transport (ALRT), Arctic air pollution (AAP) and plumes from the Pacific Northwest region (PNW). ALRT and PNW plumes can be further divided into wildfires (WF), industrial pollution (IP) and mineral dust (MD). Over the 12 years of observations, 177 individual plume events have been identified. Enhancement ratios (ERs) and Ångström exponents (AEs) of aerosols were calculated for all events. The lowest slope of Δσsp/ΔO3 is a unique feature of UTLS events. PNW-WF events have the highest averages for Δσsp/ΔCO, Δσsp/ΔO3 and Δσsp/ΔNOy compared to other events. These ERs decrease during long-range transport due to the shorter residence time of aerosols compared to the other

  20. Surface roughness effects on aluminium-based ultraviolet plasmonic nanolasers

    Chung, Yi-Cheng; Cheng, Pi-Ju; Chou, Yu-Hsun; Chou, Bo-Tsun; Hong, Kuo-Bin; Shih, Jheng-Hong; Lin, Sheng-Di; Lu, Tien-Chang; Lin, Tzy-Rong


    We systematically investigate the effects of surface roughness on the characteristics of ultraviolet zinc oxide plasmonic nanolasers fabricated on aluminium films with two different degrees of surface roughness. We demonstrate that the effective dielectric functions of aluminium interfaces with distinct roughness can be analysed from reflectivity measurements. By considering the scattering losses, including Rayleigh scattering, electron scattering, and grain boundary scattering, we adopt the modified Drude-Lorentz model to describe the scattering effect caused by surface roughness and obtain the effective dielectric functions of different Al samples. The sample with higher surface roughness induces more electron scattering and light scattering for SPP modes, leading to a higher threshold gain for the plasmonic nanolaser. By considering the pumping efficiency, our theoretical analysis shows that diminishing the detrimental optical losses caused by the roughness of the metallic interface could effectively lower (~33.1%) the pumping threshold of the plasmonic nanolasers, which is consistent with the experimental results.

  1. Digital Dermatoscopy Method for Human Skin Roughness Analysis



    Full Text Available In this study we propose a digital dermatoscopy method to measure the human skin roughness. By using this method we eliminate the use of silicon replica. Digital dermatoscopy consists of handheld digital microscope, image processing and information extraction of skin roughness level. To reduce the noise due to the variation of reflection factor on the skin we use median filter. Hence, by Fourier transform the skin texture is imaged in terms of 2D frequency-spatial distribution. Skin roughness is determined from its entropy, where the roughness level is proportional to the entropy. Three types of experiment have been performed by evaluating: (i the skin replicas; (ii young and elderly skin; and (iii seven volunteers treated by anti wrinkle cosmetic in three weeks period. We find that for the first and second experiment that our system did manage to quantify the roughness, while on the third experiment, six of seven volunteers, the roughness are succeeded to identify.

  2. Credit Assessment of Contractors: A Rough Set Method

    LIU Gaojun; ZHU Yan


    A rough set method is presented in this paper to assess the credit of contractors. Unlike traditional methods, the rough set method deduces credit-classifying rules from actual data to predict new cases. The method uses a contractors' database with a genetic algorithm and an exhaustive reduction implemented using ROSETTA software that integrates rough set method. The classification accuracy of the rough set model is not as good as that of a decision tree, logistic regression, and neural network models, but the rough set model more accurately predicts contractors with bad credit. The results show that the rough set model is especially useful for detecting corporations with bad credit in the currently disordered Chinese construction market.

  3. Numerical simulations of seepage flow in rough single rock fractures

    Qingang Zhang


    Full Text Available To investigate the relationship between the structural characteristics and seepage flow behavior of rough single rock fractures, a set of single fracture physical models were produced using the Weierstrass–Mandelbrot functions to test the seepage flow performance. Six single fractures, with various surface roughnesses characterized by fractal dimensions, were built using COMSOL multiphysics software. The fluid flow behavior through the rough fractures and the influences of the rough surfaces on the fluid flow behavior was then monitored. The numerical simulation indicates that there is a linear relationship between the average flow velocity over the entire flow path and the fractal dimension of the rough surface. It is shown that there is good a agreement between the numerical results and the experimental data in terms of the properties of the fluid flowing through the rough single rock fractures.

  4. Rough set理论及其应用%Rough set theory and its applications

    刘开第; 郭奇; 王义闹


    Rough set theory may find some concealed relationships and regulations among data. It is applied to the domains of artificial intelligence, pattern recognition, intelligence information processing and so on. It becomes a theory and a method that international academic attach importance to deal with uncertain data.%Rough set理论能从数据间发现隐含的关联和规律,广泛应用于人工智能、模式识别、智能信息处理等领域,成为最受国际学术界重视的处理不确定数据的理论与方法.

  5. Estimating deep seafloor interface and volume roughness parameters using the multibeam-hydrosweep system

    Chakraborty, B.; Schenke, H.W.; Kodagali, V.N.; Hagen, R.

    composite roughness model, including water-sediment interface roughness and sediment volume roughness parameters the data was modeled. The model effectively uses the near normal incidence angle backscatter to determine the seafloor interface roughness...

  6. Applied Approaches of Rough Set Theory to Web Mining

    SUN Tie-li; JIAO Wei-wei


    Rough set theory is a new soft computing tool, and has received much attention of researchers around the world. It can deal with incomplete and uncertain information. Now,it has been applied in many areas successfully. This paper introduces the basic concepts of rough set and discusses its applications in Web mining. In particular, some applications of rough set theory to intelligent information processing are emphasized.

  7. Deduction of static surface roughness from complex excess attenuation.

    Nichols, Andrew; Attenborough, Keith; Taherzadeh, Shahram


    Data for complex excess attenuation have been used to determine the effective surface admittance and hence characteristic roughness size of a surface comprising a random distribution of semi-cylindrical rods on an acoustically hard plane. The inversion for roughness size is based on a simplified boss model. The technique is shown to be effective to within 4%, up to a threshold roughness packing density of 32%, above which the interaction between scattering elements appears to exceed that allowed by the model.

  8. Investigation of surface roughness influence on hyperbolic metamaterial performance

    S. Kozik


    Full Text Available The main goal of this work was to introduce simple model of surface roughness which does not involve objects with complicated shapes and could help to reduce computational costs. We described and proved numerically that the influence of surface roughness at the interfaces in metal-dielectric composite materials could be described by proper selection of refractive index of dielectric layers. Our calculations show that this model works for roughness with RMS value about 1 nm and below.

  9. Data mining a kidney failure data set using Rough Sets

    Prof. K Govinda Rajulu


    Full Text Available Kidney failure remains one of the dreaded diseases worldwide. The factors of kidney problem/failure remain to be determined. The paper gives the basic idea of rough set theory. The procedure to carry out the operation of rough set theory with lower and upper approximation sets briefly explained. Some applications of rough set theory in the field of medicine w.r.t kidney failures are initiated and some future problems pointed.

  10. Intelligent Intrusion Detection System Model Using Rough Neural Network

    YAN Huai-zhi; HU Chang-zhen; TAN Hui-min


    A model of intelligent intrusion detection based on rough neural network (RNN), which combines the neural network and rough set, is presented. It works by capturing network packets to identify network intrusions or malicious attacks using RNN with sub-nets. The sub-net is constructed by detection-oriented signatures extracted using rough set theory to detect different intrusions. It is proved that RNN detection method has the merits of adaptive, high universality,high convergence speed, easy upgrading and management.

  11. L-Fuzzy Rough Set Based on Complete Residuated Lattice


    Residuated lattice is an important non-classical logic algebra, and L-fuzzy rough set based on residuated lattice can describe the information with incompleteness, fuzziness and uncomparativity in information systems. In this paper, the representation theorems of L-fuzzy rough sets based on residuated lattice are given. The properties and axiomatic definition of the lower and upper approximation operators in L-fuzzy rough sets are discussed.

  12. Performance review of the ROMI-RIP rough mill simulator

    Edward Thomas; Urs Buehlmann


    The USDA Forest Service's ROMI-RIP version 2.0 (RR2) rough mill rip-first simulation program was validated in a recent study. The validation study found that when RR2 was set to search for optimum yield without considering actual rough mill strip solutions, it produced yields that were as much as 7 percent higher (71.1% versus 64.0%) than the actual rough mill....

  13. Incorporating Skew into RMS Surface Roughness Probability Distribution

    Stahl, Mark T.; Stahl, H. Philip.


    The standard treatment of RMS surface roughness data is the application of a Gaussian probability distribution. This handling of surface roughness ignores the skew present in the surface and overestimates the most probable RMS of the surface, the mode. Using experimental data we confirm the Gaussian distribution overestimates the mode and application of an asymmetric distribution provides a better fit. Implementing the proposed asymmetric distribution into the optical manufacturing process would reduce the polishing time required to meet surface roughness specifications.

  14. Surface roughness measurement using dichromatic speckle pattern: an experimental study.

    Fujii, H; Lit, J W


    Surface roughness is studied experimentally by making use of the statistical properties of dichromatic speckle patterns. The rms intensity difference between two speckle patterns produced by two argon laser lines are analyzed in the far field as functions of the object surface roughness and the difference in the two wavenumbers of the illuminating light. By applying previously derived formulas, the rms surface roughness is obtained from rms intensity differences. Glass and metal rough surfaces are used. Other than the scattering arrangement, the experimental setup has a simple spectrometric system and an electronic analyzing circuit.

  15. Influence of metal roughness on SPR sensor performance

    Agarwal, Sajal; Prajapati, Y. K.; Singh, V.


    Roughness of the nano-layer greatly affects the sensor performance. This study is done to quantify the effect of roughness on the sensor performance experimentally. It is seen that the increased thickness of the top metal layer degrades the sensor performance i.e. sensitivity and detection accuracy. The roughness effect on the surface is seen by varying the thickness of intermediate and top metal layers separately. It is seen that 2-5 nm thick intermediate layer and 50 nm thick top layer provides better performance of sensor. Also, mathematical equations are included for the sake of theoretical analysis which indicates the effect of surface roughness on the sensor performance.

  16. Scattering from rough thin films: discrete-dipole-approximation simulations.

    Parviainen, Hannu; Lumme, Kari


    We investigate the wave-optical light scattering properties of deformed thin circular films of constant thickness using the discrete-dipole approximation. Effects on the intensity distribution of the scattered light due to different statistical roughness models, model dependent roughness parameters, and uncorrelated, random, small-scale porosity of the inhomogeneous medium are studied. The suitability of the discrete-dipole approximation for rough-surface scattering problems is evaluated by considering thin films as computationally feasible rough-surface analogs. The effects due to small-scale inhomogeneity of the scattering medium are compared with the analytic approximation by Maxwell Garnett, and the results are found to agree with the approximation.

  17. Photonic wires sidewall roughness measures using AFM capabilities

    Malureanu, Radu; Frandsen, Lars Hagedorn


    Within the last years, interest in photonic wires and photonic crystals grew due to their demonstrated ability of controlling light propagation and characteristics. One of the limitations of such devices is due to the induced roughness during the fabrication process. Generally, an increase...... in roughness leads to loss increase thus limiting the propagation length and postponing the commercialization of such structures. In this paper we present a new algorithm for measuring the sidewall roughness of our devices based on atomic force microscope (AFM) approach. Using this algorithm, the roughness can...... be quantified and thus actions in decreasing it can be taken improving the device's performance....

  18. Estimation of fracture roughness from the acoustic borehole televiewer image

    Bae, Dae Soek; Kim, Chun Soo; Kim, Kyung Soo; Park, Byung Yoon; Koh, Yong Kweon


    Estimation of fracture roughness - as one of the basic hydraulic fracture parameters - is very important in assessing ground water flow described by using discrete fracture network modeling. Former manual estimation of the roughness for each fracture surface of drill cores is above all a tedious, time-consuming work and will often cause some ambiguities of roughness interpretation partly due to the subjective judgements of observers, and partly due to the measuring procedure itself. However, recently, indebt to the highly reliable Televiewer data for the fracture discrimination, it has led to a guess to develop a relationship between the traditional roughness method based on a linear profiles and the method from the Televiewer image based on a ellipsoidal profile. Hence, the aim of this work is to develop an automatic evaluation algorithm for measuring the roughness from the Televiewer images. A highly reliable software named 'FRAFA' has been developed and realized to the extent that its utility merits. In the developing procedure, various problems - such as the examination of a new base line(ellipsoidal) for measuring the unevenness of fracture, the elimination of overlapping fracture signatures or noise, the wavelet estimation according to the type of fractures and the digitalization of roughness etc. - were considered. With these consideration in mind, the newly devised algorithm for the estimation of roughness curves showed a great potential not only for avoiding ambiguities of roughness interpretation but also for the judgement of roughness classification.

  19. 模糊T-粗集的粗糙性测量%Measures of Roughness of Fuzzy T-Rough Sets

    刘华文; 史开泉


    In this paper, we discuss roughness measure of the fuzzy T-rough sets, and introduce an axiom description of the degree of roughness and a characteristic theorem. Furthermore, we give several special expressions of the degree of roughness. The results of this paper will be helpful to the farther study and application of the theory of rough sets and fuzzy sets.

  20. High Reynolds number rough wall turbulent boundary layer experiments using Braille surfaces

    Harris, Michael; Monty, Jason; Nova, Todd; Allen, James; Chong, Min


    This paper details smooth, transitional and fully rough turbulent boundary layer experiments in the New Mexico State high Reynolds number rough wall wind tunnel. The initial surface tested was generated with a Braille printer and consisted of an uniform array of Braille points. The average point height being 0.5mm, the spacing between the points in the span was 0.5mm and the surface consisted of span wise rows separated by 4mm. The wavelength to peak ratio was 8:1. The boundary layer thickness at the measurement location was 190mm giving a large separation of roughness height to layer thickness. The maximum friction velocity was uτ=1.5m/s at Rex=3.8 x10^7. Results for the skin friction co-efficient show that this surface follows a Nikuradse type inflectional curve and that Townsends outer layer similarity hypothesis is valid for rough wall flows with a large separation of scales. Mean flow and turbulence statistics will be presented.

  1. Nanoscale roughness and morphology affect the IsoElectric Point of titania surfaces.

    Francesca Borghi

    Full Text Available We report on the systematic investigation of the role of surface nanoscale roughness and morphology on the charging behaviour of nanostructured titania (TiO2 surfaces in aqueous solutions. IsoElectric Points (IEPs of surfaces have been characterized by direct measurement of the electrostatic double layer interactions between titania surfaces and the micrometer-sized spherical silica probe of an atomic force microscope in NaCl aqueous electrolyte. The use of a colloidal probe provides well-defined interaction geometry and allows effectively probing the overall effect of nanoscale morphology. By using supersonic cluster beam deposition to fabricate nanostructured titania films, we achieved a quantitative control over the surface morphological parameters. We performed a systematical exploration of the electrical double layer properties in different interaction regimes characterized by different ratios of characteristic nanometric lengths of the system: the surface rms roughness Rq, the correlation length ξ and the Debye length λD. We observed a remarkable reduction by several pH units of IEP on rough nanostructured surfaces, with respect to flat crystalline rutile TiO2. In order to explain the observed behavior of IEP, we consider the roughness-induced self-overlap of the electrical double layers as a potential source of deviation from the trend expected for flat surfaces.

  2. Nanoscale roughness and morphology affect the IsoElectric Point of titania surfaces.

    Borghi, Francesca; Vyas, Varun; Podestà, Alessandro; Milani, Paolo


    We report on the systematic investigation of the role of surface nanoscale roughness and morphology on the charging behaviour of nanostructured titania (TiO2) surfaces in aqueous solutions. IsoElectric Points (IEPs) of surfaces have been characterized by direct measurement of the electrostatic double layer interactions between titania surfaces and the micrometer-sized spherical silica probe of an atomic force microscope in NaCl aqueous electrolyte. The use of a colloidal probe provides well-defined interaction geometry and allows effectively probing the overall effect of nanoscale morphology. By using supersonic cluster beam deposition to fabricate nanostructured titania films, we achieved a quantitative control over the surface morphological parameters. We performed a systematical exploration of the electrical double layer properties in different interaction regimes characterized by different ratios of characteristic nanometric lengths of the system: the surface rms roughness Rq, the correlation length ξ and the Debye length λD. We observed a remarkable reduction by several pH units of IEP on rough nanostructured surfaces, with respect to flat crystalline rutile TiO2. In order to explain the observed behavior of IEP, we consider the roughness-induced self-overlap of the electrical double layers as a potential source of deviation from the trend expected for flat surfaces.

  3. Hot wire CVD deposition of nanocrystalline silicon solar cells on rough substrates

    Li, Hongbo B.T., E-mail: [Utrecht University, Faculty of Science, Debye Institute for Nanomaterials Science, P.O. Box 80000, 3508 TA Utrecht (Netherlands); Werf, Karine H.M. van der; Rath, Jatin K.; Schropp, Ruud E.I. [Utrecht University, Faculty of Science, Debye Institute for Nanomaterials Science, P.O. Box 80000, 3508 TA Utrecht (Netherlands)


    In silicon thin film solar cell technology, frequently rough or textured substrates are used to scatter the light and enhance its absorption. The important issue of the influence of substrate roughness on silicon nanocrystal growth has been investigated through a series of nc-Si:H single junction p-i-n solar cells containing i-layers deposited with Hot-wire CVD. It is shown that silicon grown on the surface of an unoptimized rough substrate contains structural defects, which deteriorate solar cell performance. By introducing parameter v, voids/substrate area ratio, we could define a criterion for the morphology of light trapping substrates for thin film silicon solar cells: a preferred substrate should have a v value of less than around 1 x 10{sup -6}, correlated to a substrate surface rms value of lower than around 50 nm. Our Ag/ZnO substrates with rms roughness less than this value typically do not contain microvalleys with opening angles smaller than {approx} 110{sup o}, resulting in solar cells with improved output performance. We suggest a void-formation model based on selective etching of strained Si-Si atoms due to the collision of growing silicon film surface near the valleys of the substrate.

  4. How to select the most relevant 3D roughness parameters of a surface.

    Deltombe, R; Kubiak, K J; Bigerelle, M


    In order to conduct a comprehensive roughness analysis, around sixty 3D roughness parameters are created to describe most of the surface morphology with regard to specific functions, properties or applications. In this paper, a multiscale surface topography decomposition method is proposed with application to stainless steel (AISI 304), which is processed by rolling at different fabrication stages and by electrical discharge tool machining. Fifty-six 3D-roughness parameters defined in ISO, EUR, and ASME standards are calculated for the measured surfaces. Then, expert software "MesRug" is employed to perform statistical analysis on acquired data in order to find the most relevant parameters characterizing the effect of both processes (rolling and machining), and to determine the most appropriate scale of analysis. For the rolling process: The parameter Vmc (the Core Material Volume--defined as volume of material comprising the texture between heights corresponding to the material ratio values of p = 10% and q = 80%) computed at the scale of 3 µm is the most relevant parameter to characterize the cold rolling process. For the EDM Process, the best roughness parameter is SPD that represents the number of peaks per unit area after segmentation of a surface into motifs computed at the scale of 8 µm.

  5. Influence of titanium-substrate roughness on Ca–P–O thin films grown by atomic layer deposition

    Ananda Sagari, A.R., E-mail: [Department of Physics, P.O. Box 35 (YFL), FIN-40014 University of Jyväskylä (Finland); Malm, Jari [Department of Chemistry, P.O. Box 16100, FI-00076 Aalto University, Espoo (Finland); Laitinen, Mikko [Department of Physics, P.O. Box 35 (YFL), FIN-40014 University of Jyväskylä (Finland); Rahkila, Paavo [Department of Biology of Physical Activity, P.O. Box 35, FIN-40014 University of Jyväskylä (Finland); Hongqiang, Ma [Department of Health Sciences, P.O. Box 35 (L), FIN-40014 University of Jyväskylä (Finland); Putkonen, Matti [Department of Chemistry, P.O. Box 16100, FI-00076 Aalto University, Espoo (Finland); Beneq Oy, P.O. Box 262, FI-01511 Vantaa (Finland); Karppinen, Maarit [Department of Chemistry, P.O. Box 16100, FI-00076 Aalto University, Espoo (Finland); Whitlow, Harry J.; Sajavaara, Timo [Department of Physics, P.O. Box 35 (YFL), FIN-40014 University of Jyväskylä (Finland)


    Amorphous Ca–P–O films were deposited on titanium substrates using atomic layer deposition, while maintaining a uniform Ca/P pulsing ratio of 6/1 with varying number of atomic layer deposition cycles starting from 10 up to 208. Prior to film deposition the titanium substrates were mechanically abraded using SiC abrasive paper of 600, 1200, 2000 grit size and polished with 3 μm diamond paste to obtain surface roughness R{sub rms} values of 0.31 μm, 0.26 μm, 0.16 μm, and 0.10 μm, respectively. The composition and film thickness of as-deposited amorphous films were studied using Time-Of-Flight Elastic Recoil Detection Analysis. The results showed that uniform films could be deposited on rough metal surfaces with a clear dependence of substrate roughness on the Ca/P atomic ratio of thin films. The in vitro cell-culture studies using MC3T3 mouse osteoblast showed a greater coverage of cells on the surface polished with diamond paste in comparison to rougher surfaces after 24 h culture. No statistically significant difference was observed between Ca–P–O coated and un-coated Ti surfaces for the measured roughness value. The deposited 50 nm thick films did not dissolve during the cell culture experiment. - Highlights: ► Atomic layer deposition of Ca–P–O films on abraded Ti substrate ► Surface analysis using Time-Of-Flight Elastic Recoil Detection Analysis ► Dependence of substrate roughness on the Ca/P atomic ratio of thin films ► An increase in Ca/P atomic ratio with decreasing roughness ► Mouse osteoblast showed greater coverage of cells in polished surface.

  6. Constraining the roughness degree of slip heterogeneity

    Causse, Mathieu


    This article investigates different approaches for assessing the degree of roughness of the slip distribution of future earthquakes. First, we analyze a database of slip images extracted from a suite of 152 finite-source rupture models from 80 events (Mw = 4.1–8.9). This results in an empirical model defining the distribution of the slip spectrum corner wave numbers (kc) as a function of moment magnitude. To reduce the “epistemic” uncertainty, we select a single slip model per event and screen out poorly resolved models. The number of remaining models (30) is thus rather small. In addition, the robustness of the empirical model rests on a reliable estimation of kc by kinematic inversion methods. We address this issue by performing tests on synthetic data with a frequency domain inversion method. These tests reveal that due to smoothing constraints used to stabilize the inversion process, kc tends to be underestimated. We then develop an alternative approach: (1) we establish a proportionality relationship between kc and the peak ground acceleration (PGA), using a k−2 kinematic source model, and (2) we analyze the PGA distribution, which is believed to be better constrained than slip images. These two methods reveal that kc follows a lognormal distribution, with similar standard deviations for both methods.

  7. Intrusion detection using rough set classification

    张连华; 张冠华; 郁郎; 张洁; 白英彩


    Recently machine learning-based intrusion detection approaches have been subjected to extensive researches because they can detect both misuse and anomaly. In this paper, rough set classification (RSC), a modern learning algorithm, is used to rank the features extracted for detecting intrusions and generate intrusion detection models. Feature ranking is a very critical step when building the model. RSC performs feature ranking before generating rules, and converts the feature ranking to minimal hitting set problem addressed by using genetic algorithm (GA). This is done in classical approaches using Support Vector Machine (SVM) by executing many iterations, each of which removes one useless feature. Compared with those methods, our method can avoid many iterations. In addition, a hybrid genetic algorithm is proposed to increase the convergence speed and decrease the training time of RSC. The models generated by RSC take the form of"IF-THEN" rules, which have the advantage of explication. Tests and comparison of RSC with SVM on DARPA benchmark data showed that for Probe and DoS attacks both RSC and SVM yielded highly accurate results (greater than 99% accuracy on testing set).

  8. Intrusion detection using rough set classification

    张连华; 张冠华; 郁郎; 张洁; 白英彩


    Recently machine learning-based intrusion detection approaches have been subjected to extensive researches because they can detect both misuse and anomaly. In this paper, rough set classification (RSC), a modem learning algorithm,is used to rank the features extracted for detecting intrusions and generate intrusion detection models. Feature ranking is a very critical step when building the model. RSC performs feature ranking before generating rules, and converts the feature ranking to minimal hitting set problem addressed by using genetic algorithm (GA). This is done in classical approaches using Support Vector Machine (SVM) by executing many iterations, each of which removes one useless feature. Compared with those methods, our method can avoid many iterations. In addition, a hybrid genetic algorithm is proposed to increase the convergence speed and decrease the training time of RSC. The models generated by RSC take the form of"IF-THEN" rules,which have the advantage of explication. Tests and comparison of RSC with SVM on DARPA benchmark data showed that for Probe and DoS attacks both RSC and SVM yielded highly accurate results (greater than 99% accuracy on testing set).

  9. Roughness tolerances for Cherenkov telescope mirrors

    Tayabaly, K; Canestrari, R; Bonnoli, G; Lavagna, M; Pareschi, G


    The Cherenkov Telescope Array (CTA) is a forthcoming international ground-based observatory for very high-energy gamma rays. Its goal is to reach sensitivity five to ten times better than existing Cherenkov telescopes such as VERITAS, H.E.S.S. or MAGIC and extend the range of observation to energies down to few tens of GeV and beyond 100 TeV. To achieve this goal, an array of about 100 telescopes is required, meaning a total reflective surface of several thousands of square meters. Thence, the optimal technology used for CTA mirrors manufacture should be both low-cost (~1000 euros/m2) and allow high optical performances over the 300-550 nm wavelength range. More exactly, a reflectivity higher than 85% and a PSF (Point Spread Function) diameter smaller than 1 mrad. Surface roughness can significantly contribute to PSF broadening and limit telescope performances. Fortunately, manufacturing techniques for mirrors are now available to keep the optical scattering well below the geometrically-predictable effect of ...

  10. Thermodynamics of capillary adhesion between rough surfaces.

    de Boer, M P; de Boer, P C T


    According to the Dupré equation, the work of adhesion is equal to the surface energy difference in the separated versus the joined materials minus an interfacial energy term. However, if a liquid is at the interface between two solid materials, evaporation or condensation takes place under equilibrium conditions. The resulting matter exchange is accompanied by heat flow, and can reduce or increase the work of adhesion. Accounting for the energies requires an open-system control volume analysis based on the first law of thermodynamics. Depending on whether evaporation or condensation occurs during separation, a work term that is negative or positive must be added to the surface energy term to calculate the work of adhesion. We develop and apply this energy balance to several different interface geometries and compare the work of adhesion to the surface energy created. The model geometries include a sphere on a flat with limiting approximations and also with an exact solution, a circular disc, and a combination of these representing a rough interface. For the sphere on a flat, the work of adhesion is one half the surface energy created if equilibrium is maintained during the pull-off process.

  11. Spectrophotometric Examination of Rough Print Surfaces

    Erzsébet Novotny


    Full Text Available The objective was to assess the impact of the surface texture of individual creative paper types (coated or patternedon the quality of printing and to identify to what extent the various creative paper types require specific types ofspectrophotometers. We used stereomicroscopic images to illustrate unprinted and printed surfaces of creative papertypes. Surface roughness was measured to obtain data on the unevenness of surfaces. Spectrophotometric tests wereused to select the most suitable spectrophotometer from meters with different illumination setup for testing anygiven print. For the purpose of testing, we used spectrophotometers which are commonly available generally used totest print products for colour accuracy. With the improvement of measuring geometries, illumination setup, colourmeasurement becomes more and more capable of producing reliable results unaffected by surface textures. Our testshave proved this fact by showing that the GretagMacbeth Spectrolino with annular illumination is less sensitive tosurface texture than the X-Rite Spetrodensitometer and the Techkon SpetroDens with directional illumination. Furthertests have brought us to the conclusion that there is a difference even between the two devices with directionalillumination. While the X-Rite 530 Spectrodensitometer is more suitable for testing coated surfaces, the TechkonSpectroDens can come close to ΔE*ab values produced by the annular illuminated device for textured surfaces.

  12. The sub-micron resolution X-ray spectroscopy beamline at NSLS-II

    De Andrade, V.; Thieme, J.; Northrup, P.; Yao, Y.; Lanzirotti, A.; Eng, P.; Shen, Q.


    For many research areas such as life, environmental, earth or material sciences, novel analytical resources have to be developed for an advance understanding of complex natural and engineered systems that are heterogeneous on the micron to the tenths of microns scale. NSLS-II at BNL will be a synchrotron radiation source with an ultra-high brilliance delivering a high current (500 mA). One of the 1st six NSLS-II beamlines will be the Sub-micron Resolution X-ray spectroscopy beamline (SRX), dedicated as an analytical tool to study complex systems on a sub-micron length scale. SRX will comprise two branches thanks to a canted setup with two undulators: the first branch using Kirkpatrick-Baez mirrors as focusing optics will cover the energy range of 4.65-23 keV, allowing for XANES experiments from the Ti to the Rh K-edge. Thanks to a horizontally deflecting double crystal monochromator with maximum stability, a set of slits located on the secondary source, and two sets of complementary and quickly interchangeable KB mirrors, spectroscopy with very high spectral and spatial resolution will be achieved. The spot size will almost fully cover a range from 60×60 to 1300×500 nm 2, providing an attractive adaptability of the observation scale. A 1.5 m long IVU21 will serve as a light source. The expected high flux in a sub-micron-spot (5×10 12 and 7×10 13 ph s -1 at maximum and lowest resolutions) will open new possibilities for spectromicroscopy of trace elements. The 2nd canted undulator will serve as an independent light source for the second branch designed for experiments with X-ray energies in the range of 2-15 keV. Using Fresnel zone plates, the spatial resolution aimed for is around 30 nm with up to 7×10 9 ph s -1 in the spot. This branch would be attractive for many biological applications from life and environmental science due to low-Z elements of interest within that energy range. In both experimental stations, X-ray fluorescence will be used for imaging

  13. Reliability evaluation on a submicron Ni(P) thin film for lead-free soldering

    Ho, C.E., E-mail:; Fan, C.W.; Wu, W.H.; Kuo, T.T.


    The solderability between a Sn–Ag–Cu alloy and a submicron Ni(P) film (0.2 μm) was examined using a focused ion beam and field-emission transmission electron microscope. The Ni(P) was electrolessly deposited between the Au and Cu layers, which possessed a low P content (less than 5 wt.%) and a nanocrystalline structure. After one typical reflow, the Ni(P) film was mostly eliminated from the interface, where Cu{sub 6}Sn{sub 5} with a significant Ni content [(Cu{sub 0.6}Ni{sub 0.4}){sub 6}Sn{sub 5}] nucleated. The subsequent diffusion of Sn to the underlying Cu through molten solder channels among the (Cu{sub 0.6}Ni{sub 0.4}){sub 6}Sn{sub 5} grains yielded a second Cu{sub 6}Sn{sub 5} layer at the (Cu{sub 0.6}Ni{sub 0.4}){sub 6}Sn{sub 5}/Cu interface. The removal of Ni from the Ni(P) during soldering reaction allowed P to nucleate as nanocrystalline Ni{sub 3}(Sn,P) between the two Cu{sub 6}Sn{sub 5} layers, which subsequently translated into a chain of amorphous P–Sn–O pores. The propagation of the porous P–Sn–O destroyed the stability of (Cu{sub 0.6}Ni{sub 0.4}){sub 6}Sn{sub 5} and drove the compound layer to separate from the second Cu{sub 6}Sn{sub 5} after the third reflow. These observations suggest that the exhaustion of the Ni(P) induced spallation of the compound layer, thereby degrading the reliability of the joining interface. - Highlights: ► Solderability of a submicron Ni(P) film was evaluated. ► The exhaustion of the Ni(P) induced intermetallic spalling phenomenon. ► Ni{sub 3}Sn phase might nucleate at the temperature of ∼ 260 °C. ► The Ni(P) thickness is a key factor for the reliability of solder joints.

  14. Design and Implementation of Submicron Level 10T Full Adder in ALU Using Cell Based and SOC Technology



    Full Text Available As technology scales into the nanometer regime leakage current, active power, delay and area are becoming important metric for the analysis and design of complex circuits. The main concern in mobile and battery based systems are leakage current and power dissipation. A transistor resizing approach for 10 transistor single bit full adder cells is used to determine optimal sleep transistor size which reduces power dissipation and leakage current. A submicron level 10-transistor single bit full adder cell is considered to achieve low leakage current, reduced power dissipation and high speed. In this paper initially 10T full adder cell is designed with submicron technique and later this is employed to design an ALU adder unit. The modified ALU is simulated and synthesized successfully on cadence 180nm technology.

  15. Sub-micron silica diaphragm-based fiber-tip Fabry-Perot interferometer for pressure measurement.

    Liao, Changrui; Liu, Shen; Xu, Lei; Wang, Chao; Wang, Yiping; Li, Zhengyong; Wang, Qiao; Wang, D N


    We demonstrate a sub-micron silica diaphragm-based fiber-tip Fabry-Perot interferometer for pressure sensing applications. The thinnest silica diaphragm, with a thickness of ∼320  nm, has been achieved by use of an improved electrical arc discharge technique. Such a sub-micron silica diaphragm breaks the sensitivity limitation imposed by traditional all-silica Fabry-Perot interferometric pressure sensors and, as a result, a high pressure sensitivity of ∼1036  pm/MPa at 1550 nm and a low temperature cross-sensitivity of ∼960  Pa/°C are achieved when a silica diaphragm of ∼500  nm in thickness is used. Moreover, the all-silica spherical structure enhanced the mechanical strength of the micro-cavity sensor, making it suitable for high sensitivity pressure sensing in harsh environments.

  16. A continuous flow micro filtration device for plasma/blood separation using submicron vertical pillar gap structures

    Kang, Tae Goo; Yoon, Yong-Jin; Ji, Hongmiao; Lim, Pei Yi; Chen, Yu


    This work demonstrates a continuous flow plasma/blood separator using a vertical submicron pillar gap structure. The working principle of the proposed separator is based on size exclusion of cells through cross-flow filtration, in which only plasma is allowed to pass through submicron vertical pillars located tangential to the main flow path of the blood sample. The maximum filtration efficiency of 99.9% was recorded with a plasma collection rate of 0.67 µl min-1 for an input blood flow rate of 12.5 µl min-1. The hemolysis phenomenon was observed for an input blood flow rate above 30 µl min-1. Based on the experimental results, we can conclude that the proposed device shows potential for the application of on-chip plasma/blood separation as a part of integrated point-of-care (POC) diagnostics systems.

  17. Exploring the Role of Sub-micron Sized Dust Grains in the Atmospheres of Red L0 - L6 Dwarfs

    Hiranaka, Kay; Douglas, Stephanie T; Marley, Mark S; Baldassare, Vivienne F


    We examine the hypothesis that the red near-infrared colors of some L dwarfs could be explained by a "dust haze" of small particles in their upper atmospheres. This dust haze would exist in conjunction with the clouds found in dwarfs with more typical colors. We developed a model which uses Mie theory and the Hansen particle size distributions to reproduce the extinction due to the proposed dust haze. We apply our method to 23 young L dwarfs and 23 red field L dwarfs. We constrain the properties of the dust haze including particle size distribution and column density using Markov-Chain Monte Carlo methods. We find that sub-micron range silicate grains reproduce the observed reddening. Current brown dwarf atmosphere models include large grain (1--100~$\\mu m$) dust clouds but not submicron dust grains. Our results provide a strong proof of concept and motivate a combination of large and small dust grains in brown dwarf atmosphere models.

  18. Lunar polar craters -- icy, rough or just sloping?

    Eke, Vincent R; Lane, David A; Smith, David; Teodoro, Luis F A


    Circular Polarisation Ratio (CPR) mosaics from Mini-SAR on Chandrayaan-1 and Mini-RF on LRO are used to study craters near to the lunar north pole. The look direction of the detectors strongly affects the appearance of the crater CPR maps. Rectifying the mosaics to account for parallax also significantly changes the CPR maps of the crater interiors. It is shown that the CPRs of crater interiors in unrectified maps are biased to larger values than crater exteriors, because of a combination of the effects of parallax and incidence angle. Using the LOLA Digital Elevation Map (DEM), the variation of CPR with angle of incidence has been studied. For fresh craters, CPR~0.7 with only a weak dependence on angle of incidence or position interior or just exterior to the crater, consistent with dihedral scattering from blocky surface roughness. For anomalous craters, the CPR interior to the crater increases with both incidence angle and distance from the crater centre. Central crater CPRs are similar to those in the cra...

  19. Submicron-bubble-enhanced focused ultrasound for blood-brain barrier disruption and improved CNS drug delivery.

    Ching-Hsiang Fan

    Full Text Available The use of focused ultrasound (FUS with microbubbles has been proven to induce transient blood-brain barrier opening (BBB-opening. However, FUS-induced inertial cavitation of microbubbles can also result in erythrocyte extravasations. Here we investigated whether induction of submicron bubbles to oscillate at their resonant frequency would reduce inertial cavitation during BBB-opening and thereby eliminate erythrocyte extravasations in a rat brain model. FUS was delivered with acoustic pressures of 0.1-4.5 MPa using either in-house manufactured submicron bubbles or standard SonoVue microbubbles. Wideband and subharmonic emissions from bubbles were used to quantify inertial and stable cavitation, respectively. Erythrocyte extravasations were evaluated by in vivo post-treatment magnetic resonance susceptibility-weighted imaging, and finally by histological confirmation. We found that excitation of submicron bubbles with resonant frequency-matched FUS (10 MHz can greatly limit inertial cavitation while enhancing stable cavitation. The BBB-opening was mainly caused by stable cavitation, whereas the erythrocyte extravasation was closely correlated with inertial cavitation. Our technique allows extensive reduction of inertial cavitation to induce safe BBB-opening. Furthermore, the safety issue of BBB-opening was not compromised by prolonging FUS exposure time, and the local drug concentrations in the brain tissues were significantly improved to 60 times (BCNU; 18.6 µg versus 0.3 µg by using chemotherapeutic agent-loaded submicron bubbles with FUS. This study provides important information towards the goal of successfully translating FUS brain drug delivery into clinical use.

  20. Influence of Nanoscale Surface Roughness on Colloidal Force Measurements.

    Zou, Yi; Jayasuriya, Sunil; Manke, Charles W; Mao, Guangzhao


    Forces between colloidal particles determine the performances of many industrial processes and products. Colloidal force measurements conducted between a colloidal particle AFM probe and particles immobilized on a flat substrate are valuable in selecting appropriate surfactants for colloidal stabilization. One of the features of inorganic fillers and extenders is the prevalence of rough surfaces-even the polymer latex particles, often used as model colloidal systems including the current study, have rough surfaces albeit at a much smaller scale. Surface roughness is frequently cited as the reason for disparity between experimental observations and theoretical treatment but seldom verified by direct evidence. This work reports the effect of nanoscale surface roughness on colloidal force measurements carried out in the presence of surfactants. We applied a heating method to reduce the mean surface roughness of commercial latex particles from 30 to 1 nm. We conducted force measurements using the two types of particles at various salt and surfactant concentrations. The surfactants used were pentaethylene glycol monododecyl ether, Pluronic F108, and a styrene/acrylic copolymer, Joncryl 60. In the absence of the surfactant, nanometer surface roughness affects colloidal forces only in high salt conditions when the Debye length becomes smaller than the surface roughness. The adhesion is stronger between colloids with higher surface roughness and requires a higher surfactant concentration to be eliminated. The effect of surface roughness on colloidal forces was also investigated as a function of the adsorbed surfactant layer structure characterized by AFM indentation and dynamic light scattering. We found that when the layer thickness exceeds the surface roughness, the colloidal adhesion is less influenced by surfactant concentration variation. This study demonstrates that surface roughness at the nanoscale can influence colloidal forces significantly and should be taken