Composition quantification of electron-transparent samples by backscattered electron imaging in scanning electron microscopy

Energy Technology Data Exchange (ETDEWEB)

Müller, E., E-mail: erich.mueller@kit.edu; Gerthsen, D.

2017-02-15

The contrast of backscattered electron (BSE) images in scanning electron microscopy (SEM) depends on material parameters which can be exploited for composition quantification if some information on the material system is available. As an example, the In-concentration in thin In{sub x}Ga{sub 1−x}As layers embedded in a GaAs matrix is analyzed in this work. The spatial resolution of the technique is improved by using thin electron-transparent specimens instead of bulk samples. Although the BSEs are detected in a comparably small angular range by an annular semiconductor detector, the image intensity can be evaluated to determine the composition and local thickness of the specimen. The measured intensities are calibrated within one single image to eliminate the influence of the detection and amplification system. Quantification is performed by comparison of experimental and calculated data. Instead of using time-consuming Monte-Carlo simulations, an analytical model is applied for BSE-intensity calculations which considers single electron scattering and electron diffusion. - Highlights: • Sample thickness and composition are quantified by backscattered electron imaging. • A thin sample is used to achieve spatial resolution of few nanometers. • Calculations are carried out with a time-saving electron diffusion model. • Small differences in atomic number and density detected at low electron energies.

Analytical expressions for the electron backscattering coefficient

International Nuclear Information System (INIS)

August, H.J.; Wernisch, J.

1989-01-01

Several analytical expressions for the electron backscattering coefficient for massive homogeneous samples are compared with experimental data, directing special attention to the dependence of this quantity on the electron acceleration energy. It is shown that this dependence generally cannot be neglected. The expression proposed by Hunger and Kuechler turns out to be better than that of Love and Scott, although even the better formula can be slightly improved by a small modification. (author)

Monte Carlo simulation of MOSFET dosimeter for electron backscatter using the GEANT4 code.

Science.gov (United States)

Chow, James C L; Leung, Michael K K

2008-06-01

The aim of this study is to investigate the influence of the body of the metal-oxide-semiconductor field effect transistor (MOSFET) dosimeter in measuring the electron backscatter from lead. The electron backscatter factor (EBF), which is defined as the ratio of dose at the tissue-lead interface to the dose at the same point without the presence of backscatter, was calculated by the Monte Carlo simulation using the GEANT4 code. Electron beams with energies of 4, 6, 9, and 12 MeV were used in the simulation. It was found that in the presence of the MOSFET body, the EBFs were underestimated by about 2%-0.9% for electron beam energies of 4-12 MeV, respectively. The trend of the decrease of EBF with an increase of electron energy can be explained by the small MOSFET dosimeter, mainly made of epoxy and silicon, not only attenuated the electron fluence of the electron beam from upstream, but also the electron backscatter generated by the lead underneath the dosimeter. However, this variation of the EBF underestimation is within the same order of the statistical uncertainties as the Monte Carlo simulations, which ranged from 1.3% to 0.8% for the electron energies of 4-12 MeV, due to the small dosimetric volume. Such small EBF deviation is therefore insignificant when the uncertainty of the Monte Carlo simulation is taken into account. Corresponding measurements were carried out and uncertainties compared to Monte Carlo results were within +/- 2%. Spectra of energy deposited by the backscattered electrons in dosimetric volumes with and without the lead and MOSFET were determined by Monte Carlo simulations. It was found that in both cases, when the MOSFET body is either present or absent in the simulation, deviations of electron energy spectra with and without the lead decrease with an increase of the electron beam energy. Moreover, the softer spectrum of the backscattered electron when lead is present can result in a reduction of the MOSFET response due to stronger

The ELSA laser beamline for electron polarization measurements via Compton backscattering

Energy Technology Data Exchange (ETDEWEB)

Switka, Michael; Hinterkeuser, Florian; Koop, Rebecca; Hillert, Wolfgang [Electron Stretcher Facility ELSA, Physics Institute of Bonn University (Germany)

2016-07-01

The Electron Stretcher Facility ELSA provides a spin polarized electron beam with energies of 0.5 - 3.2 GeV for double polarization hadron physics experiments. As of 2015, the laser beamline of the polarimeter based on Compton backscattering restarted operation. It consists of a cw disk laser with design total beam power of 40 W and features two polarized 515 nm photon beams colliding head-on with the stored electron beam in ELSA. The polarization measurement is based on the vertical profile asymmetry of the back-scattered photons, which is dependent on the polarization degree of the stored electron beam. After recent laser repairs, beamline and detector modifications, the properties of the beamline have been determined and first measurements of the electron polarization degree were conducted. The beamline performance and first measurements are presented.

A multislice theory of electron scattering in crystals including backscattering and inelastic effects.

Science.gov (United States)

Spiegelberg, Jakob; Rusz, Ján

2015-12-01

In the framework of the slice transition operator technique, a general multislice theory for electron scattering in crystals is developed. To achieve this generalization, we combine the approaches for inelastic scattering derived by Yoshioka [J. Phys. Soc. Jpn. 12, 6 (1957)] and backscattering based on the formalism of Chen and Van Dyck [Ultramicroscopy 70, 29-44 (1997)]. A computational realization of the obtained equations is suggested. The proposed computational scheme is tested on elastic backscattering of electrons, where we consider single backscattering in analogy to the computational scheme proposed by Chen and Van Dyck. Copyright © 2015 Elsevier B.V. All rights reserved.

Notes on representing grain size distributions obtained by electron backscatter diffraction

International Nuclear Information System (INIS)

Toth, Laszlo S.; Biswas, Somjeet; Gu, Chengfan; Beausir, Benoit

2013-01-01

Grain size distributions measured by electron backscatter diffraction are commonly represented by histograms using either number or area fraction definitions. It is shown here that they should be presented in forms of density distribution functions for direct quantitative comparisons between different measurements. Here we make an interpretation of the frequently seen parabolic tales of the area distributions of bimodal grain structures and a transformation formula between the two distributions are given in this paper. - Highlights: • Grain size distributions are represented by density functions. • The parabolic tales corresponds to equal number of grains in a bin of the histogram. • A simple transformation formula is given to number and area weighed distributions. • The particularities of uniform and lognormal distributions are examined

Monte Carlo simulation of Tabata's electron backscattering experiments

International Nuclear Information System (INIS)

Kirihara, Y.; Namito, Y.; Iwase, H.; Hirayama, H.

2010-01-01

Electron backscattering coefficients, η, obtained from several targets in the MeV range were calculated by using electron-photon Monte Carlo transport calculation codes, i.e., EGS5 and ITS 3.0. These calculated values were compared with those obtained from the electron backscattering experiment performed by Tabata using an ionization chamber . We found that Tabata's estimation of the multiplication factor of the ionization chamber, f, had a non-negligible error. Then, we calculated the ionization chamber output, I, which is a product of η and f. The ratios of I between the experimental and the calculated values were within 1.5 and 1.3 for the EGS5 code and the ITS 3.0 code, respectively. The ratios of η between the experimental and the calculated values were within 2.4 and 1.5 for the EGS5 code and the ITS 3.0 code, respectively. The differences between the experimental and the calculated values of I and η are large for low-Z targets (Be and C). Here, the ratios obtained by using the ITS 3.0 code are closer to unity than those obtained by using the EGS5 code. The reason of this is the fact that the calculated value obtained by using the ITS 3.0 code is underestimated for low-Z targets; this underestimation can, in turn, be attributed to the use of the default value of the number of steps in the electron transport algorithm in the ITS 3.0 code.

Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations

Energy Technology Data Exchange (ETDEWEB)

Burch, Matthew J.; Fancher, Chris M.; Patala, Srikanth [Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC (United States); De Graef, Marc [Department of Materials Science and Engineering, Carnegie Mellon University, Pittsburg, PA (United States); Dickey, Elizabeth C. [Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC (United States)

2017-02-15

A novel technique, which directly and nondestructively maps polar domains using electron backscatter diffraction (EBSD) is described and demonstrated. Through dynamical diffraction simulations and quantitative comparison to experimental EBSD patterns, the absolute orientation of a non-centrosymmetric crystal can be determined. With this information, the polar domains of a material can be mapped. The technique is demonstrated by mapping the non-ferroelastic, or 180°, ferroelectric domains in periodically poled LiNbO{sub 3} single crystals. Further, the authors demonstrate the possibility of mapping polarity using this technique in other polar materials system. - Highlights: • A novel technique to directly polar domains utilizing EBSD is demonstrated. • The technique relies on dynamical diffraction simulations of EBSD patterns. • The technique is demonstrated by mapping 180° domains in LiNbO{sub 3} single crystals. • Further application of this technique to other materials classes is discussed.

Quantitative characterization of abyssal seafloor with transit multibeam backscatter data

Science.gov (United States)

Pockalny, R. A.; Ferrini, V. L.

2014-12-01

The expanding volume of deep-water multibeam echosounder data provides emerging opportunities for the improved characterization of the abyssal seafloor. Nearly 500 cruises criss-cross the oceans with modern wide-swath multibeam systems, and these cruise tracks have imaged a variety of morphologic, tectonic and magmatic environments. The qualitative analysis of the seafloor backscatter data strongly suggests a local and regional variability that correlates with sediment thickness, sediment type and/or depositional environment. We present our initial attempts to develop a method that quantifies this observed seafloor backscatter variability and to explore the causes and potential implications of this variability. Our approach is rooted in the Angular Range Analysis methodology, which utilizes changes in backscatter amplitude observed as a function of grazing angle, to characterize the seafloor. The primary difference in our approach is that we do not invert for geo-acoustical parameters, but rather explores empirical relationships between geological observations and stacked slope and y-intercept values. In addition, we also include the mean and the variance of detrended backscatter measurements. Our initial results indicate intriguing relationships between backscatter parameters and the CaCO3 content of surface sediments. Seafloor regions reported to have high manganese nodule concentrations also tend to have characteristic trends in backscatter parameters. We will present these regional correlations as well as some preliminary statistical analyses of the backscatter parameters and key environmental factors.

Distribution of uranium in kolm. Evidence from backscattered electron imagery

Energy Technology Data Exchange (ETDEWEB)

Parnell, J [Dep. of Geology, Belfast (Northern Ireland)

1985-02-06

The distribution of uranium in kolm from Upper Cambriam alum shales has been studied using backscattered electron imagery, and found to be concentrated in discrete mineral phases. Authigenic minerals in kolm include pyrite, galena, and a cerium-bearing mineral referable to monazite. Uranium occurs within the monazite and generally shows a close relationship with phosphorus. Uranium bearing monazite has also been identified within the host alum shale.

Electron backscatter diffraction characterization of laser-induced periodic surface structures on nickel surface

Energy Technology Data Exchange (ETDEWEB)

Sedao, Xxx, E-mail: sedao.xxx@gmail.com [Laboratoire Hubert Curien, Université Jean Monnet, 42000 St-Etienne (France); Maurice, Claire [Laboratoire Georges Friedel, Ecole Nationale Supérieure des Mines, 42023 St-Etienne (France); Garrelie, Florence; Colombier, Jean-Philippe; Reynaud, Stéphanie [Laboratoire Hubert Curien, Université Jean Monnet, 42000 St-Etienne (France); Quey, Romain; Blanc, Gilles [Laboratoire Georges Friedel, Ecole Nationale Supérieure des Mines, 42023 St-Etienne (France); Pigeon, Florent [Laboratoire Hubert Curien, Université Jean Monnet, 42000 St-Etienne (France)

2014-05-01

Graphical abstract: -- Highlight: •Lattice rotation and its distribution in laser-induced periodic surface structures (LIPSS) and the subsurface region on a nickel substrate are revealed using electron backscatter diffraction (EBSD). -- Abstract: We report on the structural investigation of laser-induced periodic surface structures (LIPSS) generated in polycrystalline nickel target after multi-shot irradiation by femtosecond laser pulses. Electron backscatter diffraction (EBSD) is used to reveal lattice rotation caused by dislocation storage during LIPSS formation. Localized crystallographic damages in the LIPSS are detected from both surface and cross-sectional EBSD studies. A surface region (up to 200 nm) with 1–3° grain disorientation is observed in localized areas from the cross-section of the LIPSS. The distribution of the local disorientation is inhomogeneous across the LIPSS and the subsurface region.

3D invariant embedding model for backscattering electrons applied to materials characterization

International Nuclear Information System (INIS)

Figueroa, C.; Nieva, N.; Heluani, S.P.

2007-01-01

In this work, the results of a 3D model used to describe the fraction of backscattered electrons, together with its energy and angular distributions, are reported. This 3D model is the result of improvements in the Invariant Embedding Approach to Microanalysis (IEAM). Comparisons with experiment show that the theoretical results follow the general trend of experimental data, when parameters (such as atomic number, energy of the impinging electrons and tilted angle) are changed

Angle selective backscattered electron contrast in the low-voltage scanning electron microscope: Simulation and experiment for polymers

Energy Technology Data Exchange (ETDEWEB)

Wan, Q., E-mail: qwan2@sheffield.ac.uk [Department of Material Science and Engineering, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom); Masters, R.C. [Department of Material Science and Engineering, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom); Lidzey, D. [Department of Physics and Astronomy, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom); Abrams, K.J. [Department of Material Science and Engineering, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom); Dapor, M. [European Centre for Theoretical Studies in Nuclear Physics and Related Areas (ECT-FBK) and Trento Institute for Fundamental Physics and Applications (TIFPA-INFN), via Sommarive 18, I-38123 Trento (Italy); Plenderleith, R.A. [Department of Material Science and Engineering, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom); Rimmer, S. [Department of Chemistry, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom); Claeyssens, F.; Rodenburg, C. [Department of Material Science and Engineering, University of Sheffield, Western Bank, Sheffield S10 2TN (United Kingdom)

2016-12-15

Recently developed detectors can deliver high resolution and high contrast images of nanostructured carbon based materials in low voltage scanning electron microscopes (LVSEM) with beam deceleration. Monte Carlo Simulations are also used to predict under which exact imaging conditions purely compositional contrast can be obtained and optimised. This allows the prediction of the electron signal intensity in angle selective conditions for back-scattered electron (BSE) imaging in LVSEM and compares it to experimental signals. Angle selective detection with a concentric back scattered (CBS) detector is considered in the model in the absence and presence of a deceleration field, respectively. The validity of the model prediction for both cases was tested experimentally for amorphous C and Cu and applied to complex nanostructured carbon based materials, namely a Poly(N-isopropylacrylamide)/Poly(ethylene glycol) Diacrylate (PNIPAM/PEGDA) semi-interpenetration network (IPN) and a Poly(3-hexylthiophene-2,5-diyl) (P3HT) film, to map nano-scale composition and crystallinity distribution by avoiding experimental imaging conditions that lead to a mixed topographical and compositional contrast - Highlights: • An optimised model for nano-scale analysis of beam sensitive materials by LVSEM. • Simulation and separation of composition and topography in a CBS detector. • Selective angle backscattered electron collection for mapping of polymers.

Angle selective backscattered electron contrast in the low-voltage scanning electron microscope: Simulation and experiment for polymers

International Nuclear Information System (INIS)

Wan, Q.; Masters, R.C.; Lidzey, D.; Abrams, K.J.; Dapor, M.; Plenderleith, R.A.; Rimmer, S.; Claeyssens, F.; Rodenburg, C.

2016-01-01

Recently developed detectors can deliver high resolution and high contrast images of nanostructured carbon based materials in low voltage scanning electron microscopes (LVSEM) with beam deceleration. Monte Carlo Simulations are also used to predict under which exact imaging conditions purely compositional contrast can be obtained and optimised. This allows the prediction of the electron signal intensity in angle selective conditions for back-scattered electron (BSE) imaging in LVSEM and compares it to experimental signals. Angle selective detection with a concentric back scattered (CBS) detector is considered in the model in the absence and presence of a deceleration field, respectively. The validity of the model prediction for both cases was tested experimentally for amorphous C and Cu and applied to complex nanostructured carbon based materials, namely a Poly(N-isopropylacrylamide)/Poly(ethylene glycol) Diacrylate (PNIPAM/PEGDA) semi-interpenetration network (IPN) and a Poly(3-hexylthiophene-2,5-diyl) (P3HT) film, to map nano-scale composition and crystallinity distribution by avoiding experimental imaging conditions that lead to a mixed topographical and compositional contrast - Highlights: • An optimised model for nano-scale analysis of beam sensitive materials by LVSEM. • Simulation and separation of composition and topography in a CBS detector. • Selective angle backscattered electron collection for mapping of polymers.

Absorption and backscatter of internal conversion electrons in the measurements of surface contamination of 137Cs

International Nuclear Information System (INIS)

Yunoki, A.; Kawada, Y.; Yamada, T.; Unno, Y.; Sato, Y.; Hino, Y.

2013-01-01

We measured 4π and 2π counting efficiencies for internal conversion electrons (ICEs), gross β-particles and also β-rays alone with various source conditions regarding absorber and backing foil thickness using e-X coincidence technique. Dominant differences regarding the penetration, attenuation and backscattering properties among ICEs and β-rays were revealed. Although the abundance of internal conversion electrons of 137 Cs- 137 Ba is only 9.35%, 60% of gross counts may be attributed to ICEs in worse source conditions. This information will be useful for radionuclide metrology and for surface contamination monitoring. - Highlights: • Counting efficiencies for internal conversion electrons from 137 Cs were measured, and compared with those for β-rays. • Electron-X coincidence technique was employed. • A thin NaI(Tl) scintillation detector was used for X-ray detection. • Backscattering fractions of electrons and beta particles were studied by similar experiments

Application of electron back-scatter diffraction to texture research

International Nuclear Information System (INIS)

Randle, V.

1996-01-01

The application of electron back-scatter diffraction (EBSD) to materials research is reviewed. A brief history of the technique is given, followed by a description of present-day operation. The methodology of 'microtexture', i.e. spatially specific orientations, is described and recent examples of its application using EBSD are given, in particular to interstitial-free steel processing, growth of phases in a white iron and grain boundary phenomena in a superplastic alloy. The advantages and disadvantages of EBSD compared to use of X-rays for texture determination are discussed in detail

A simple way to obtain backscattered electron images in a scanning transmission electron microscope.

Science.gov (United States)

Tsuruta, Hiroki; Tanaka, Shigeyasu; Tanji, Takayoshi; Morita, Chiaki

2014-08-01

We have fabricated a simple detector for backscattered electrons (BSEs) and incorporated the detector into a scanning transmission electron microscope (STEM) sample holder. Our detector was made from a 4-mm(2) Si chip. The fabrication procedure was easy, and similar to a standard transmission electron microscopy (TEM) sample thinning process based on ion milling. A TEM grid containing particle objects was fixed to the detector with a silver paste. Observations were carried out using samples of Au and latex particles at 75 and 200 kV. Such a detector provides an easy way to obtain BSE images in an STEM. © The Author 2014. Published by Oxford University Press on behalf of The Japanese Society of Microscopy. All rights reserved. For permissions, please e-mail: journals.permissions@oup.com.

In situ electron backscattered diffraction of individual GaAs nanowires

Energy Technology Data Exchange (ETDEWEB)

Prikhodko, S.V. [Department of Materials Science and Engineering, University of California Los Angeles, Los Angeles, CA 90095 (United States)], E-mail: sergey@seas.ucla.edu; Sitzman, S. [Oxford Instruments America, Concord, MA 01742 (United States); Gambin, V. [Northrop Grumman Space Technology, Redondo Beach, CA 90278 (United States); Kodambaka, S. [Department of Materials Science and Engineering, University of California Los Angeles, Los Angeles, CA 90095 (United States)

2008-12-15

We suggest and demonstrate that electron backscattered diffraction, a scanning electron microscope-based technique, can be used for non-destructive structural and morphological characterization of statistically significant number of nanowires in situ on their growth substrate. We obtain morphological, crystal phase, and crystal orientation information of individual GaAs nanowires in situ on the growth substrate GaAs(1 1 1) B. Our results, verified using transmission electron microscopy and selected area electron diffraction analyses of the same set of wires, indicate that most wires possess a wurtzite structure with a high density of thin structural defects aligned normal to the wire growth axis, while others grow defect-free with a zincblende structure. The demonstrated approach is general, applicable to other material systems, and is expected to provide important insights into the role of substrate structure on nanowire structure on nanowire crystallinity and growth orientation.

High-efficiency detector of secondary and backscattered electrons for low-dose imaging in the ESEM.

Science.gov (United States)

Neděla, Vilém; Tihlaříková, Eva; Runštuk, Jiří; Hudec, Jiří

2018-01-01

A new Combined System for high-efficiency detection of Secondary and Backscattered Electrons (CSSBE) in the ESEM consists of three detectors: an ionisation SE detector, an improved scintillation BSE detector, and a new Ionisation Secondary Electron Detector with an electrostatic Separator (ISEDS). The ISEDS optimizes conditions for electron-gas ionisation phenomena in the ESEM to achieve a strongly amplified signal from the secondary electrons with a minimal contribution from backscattered and beam electrons. For this purpose, it is originally equipped with an electrostatic separator, which focuses signal electrons towards a detection electrode and controls the concentration of positive ions above the sample. The working principle of the ISEDS is explained by simulations of signal electron trajectories in gas using the EOD program with our Monte Carlo module. The ability to detect the signal electrons in a selected range of energies is described with Geant4 Monte Carlo simulations of electron-solid interactions and proven by experimental results. High-efficiency detection of the ISEDS is demonstrated by imaging a low atomic number sample under a reduced beam energy of 5 keV, very low beam currents of up to 0.2 pA, and gas pressure of hundreds of Pa. Copyright © 2017 Elsevier B.V. All rights reserved.

Direct observation of the hydrogen peak in the energy distribution of electrons backscattered elastically from polyethylene

International Nuclear Information System (INIS)

Varga, D.; Toekesi, K.; Berenyi, Z.; Toth, J.; Koever, L.

2004-01-01

Complete text of publication follows. Observation of the hydrogen peak is either challenging or impossible task for the conventional electron spectroscopy. Hydrogen was observed earlier in electron scattering experiments using transmission geometry and formvar film. In this work we show an alternative way for the detection of hydrogen peak analyzing the spectra of elastically backscattered electrons from polyethylene ((CH 2 ) n ). We take advantage of the fact that the elastic peak from polyethylene split into carbon and hydrogen components. The energy of the elastically scattered electrons is shifted from the nominal values due to the energy transfer between the primary electron and the target atoms (recoil effect). Due to the motion of the scattering atoms, a broadering of the energy width of the spectra takes place. We performed Monte Carlo simulation for 2 keV electrons penetrated and elastically backscattered from polyethylene sample. In our calculations both the elastic and inelastic scattering events were taken into account. We further assume that the thermal motion of the target atoms follows the Maxwell-Boltzmann energy distribution. After each elastic scattering the recoil energy was calculated according to ref Fig. 1 shows the geometric configuration used in the calculation. The initial angle of incident beam (θ) was 50 deg. Fig. 2 shows the gray scale plot of the intensity of electrons backscattered elastically from polyethylene. The separation between the carbon and hydrogen peaks is clearly seen. Our results show that the multiple electron scattering causes only minor changes in the energy shifts and broadenings of elastic peaks. Moreover, our simulations are in good agreement with our experimental observations. (author)

Contribution of back-scattered electromagnetic rays to the Moessbauer conversion electron spectrum

International Nuclear Information System (INIS)

Ruskov, T.; Ruskov, R.; Paneva, D.; Lefterov, D.

1999-01-01

The contribution of back-scattered electromagnetic rays in a 57 Fe conversion electron Moessbauer spectrum is considered using proportional counter as a detector. A simplified method for measuring this contribution is described. The experimental results show that this contribution strongly depends on the construction of the counter and the selected fraction in the pulse-height spectrum

Backscattering/transmission of 2 MeV He{sup ++} ions quantitative correlation study

Energy Technology Data Exchange (ETDEWEB)

Berec, V., E-mail: bervesn@gmail.com [Institute of Nuclear Sciences Vinca, University of Belgrade, P.O. Box 522, 11001 Belgrade (Serbia); Germogli, G.; Mazzolari, A.; Guidi, V. [INFN Sezione di Ferrara and Dipartimento di Fisica e Scienze della Terra, Via Saragat 1, 44100 Ferrara (Italy); De Salvador, D. [Dipartimento di Fisica, Università di Padova, Via Marzolo n.8, 35131 Padova (Italy); INFN Laboratori Nazionali di Legnaro, Viale Università 2, 35020 Legnaro, PD (Italy); Bacci, L. [INFN Laboratori Nazionali di Legnaro, Viale Università 2, 35020 Legnaro, PD (Italy)

2015-07-15

In this work we report on detailed findings of planar channeling oscillations of 2 MeV He{sup ++} particles in (1 1 0) silicon crystal. The exact correlation and coherence mechanism between confined particles oscillating trajectories are analyzed theoretically and experimentally in backscattering/transmission geometry. Regular patterns of channeled He{sup ++} ion planar oscillations are shown to be dominated by the crystal harmonic-oscillator potential and multiple scattering effect. For the first time it was shown that under the planar channeling conditions trajectories of positively charged particles exhibit observable correlation dynamics, including the interference effect. Quantitative estimation of channeling efficiency is performed using path integral method.

Carbon/Hydrogen ratio determination in hydrocarbons and its mixtures by electron backscattering technique

International Nuclear Information System (INIS)

Padron, I.; Desdin, L.F.; Navarro, A.; Fuentes, M.

1996-01-01

A method carbon/hydrogen ratio (C/H) determination in hydrocarbons and its mixtures was improved using the electron backscattering technique. Besides the hetero atoms (S,O and N) influence in petroleum is studied for being able to determinate the C/H ratio in cuban petroleum with high sulphur contents

Comparative study of macrotexture analysis using X-ray diffraction and electron backscattered diffraction techniques

International Nuclear Information System (INIS)

Serna, Marilene Morelli

2002-01-01

The macrotexture is one of the main characteristics in metallic materials, which the physical properties depend on the crystallographic direction. The analysis of the macrotexture to middles of the decade of 80 was just accomplished by the techniques of Xray diffraction and neutrons diffraction. The possibility of the analysis of the macrotexture using, the technique of electron backscattering diffraction in the scanning electronic microscope, that allowed to correlate the measure of the orientation with its location in the micro structure, was a very welcome tool in the area of engineering of materials. In this work it was studied the theoretical aspects of the two techniques and it was used of both techniques for the analysis of the macrotexture of aluminum sheets 1050 and 3003 with intensity, measured through the texture index 'J', from 2.00 to 5.00. The results obtained by the two techniques were shown reasonably similar, being considered that the statistics of the data obtained by the technique of electron backscatter diffraction is much inferior to the obtained by the X-ray diffraction. (author)

Energy analyzer for Auger electron spectroscopy and low-energy backscattering ion spectroscopy

International Nuclear Information System (INIS)

Volkov, S.S.; Gorelik, V.A.; Gutenko, V.T.; Protopopov, O.D.; Trubitsin, A.A.; Shuvalova, Z.A.; Yakushev, G.A.

1988-01-01

Energy analyzer for electron Auger spectroscopy and low-energy backscattering ion spectroscopy is described. Analyzer presents one-cascade variant of cylindrical mirror with second-order focusing. Energy relative resolution is continuously adjusted within 0.2-1.2% limits. Signal/noise relation by Cu Auger-line at 1 muA current of exciting beam changes upper limit of range 150-450

Tackling pseudosymmetry problems in electron backscatter diffraction (EBSD) analyses of perovskite structures

Science.gov (United States)

Mariani, Elisabetta; Kaercher, Pamela; Mecklenburgh, Julian; Wheeler, John

2016-04-01

Perovskite minerals form an important mineral group that has applications in Earth science and emerging alternative energy technologies, however crystallographic quantification of these minerals with electron backscatter diffraction (EBSD) is not accurate due to pseudosymmetry problems. The silicate perovskite Bridgmanite, (Mg,Fe)SiO3, is understood to be the dominant phase in the Earth's lower mantle. Gaining insight into its physical and rheological properties is therefore vital to understand the dynamics of the Earth's deep interior. Rock deformation experiments on analogue perovskite phases, for example (Ca,Sr)TiO3, combined with quantitative microstructural analyses of the recovered samples by EBSD, yield datasets that can reveal what deformation mechanisms may dominate the flow of perovskite in the lower mantle. Additionally, perovskite structures have important technological applications as new, suitable cathodes for the operation of more efficient and environmentally-friendly solid oxide fuel cells (SOFC). In recent years they have also been recognised as a potential substitute for silicon in the next generation of photovoltaic cells for the construction of economic and energy efficient solar panels. EBSD has the potential to be a valuable tool for the study of crystal orientations achieved in perovskite substrates as crystal alignment has a direct control on the properties of these materials. However, perovskite structures currently present us with challenges during the automated indexing of Kikuchi bands in electron backscatter diffraction patterns (EBSPs). Such challenges are represented by the pseudosymmetric character of perovskites, where atoms are subtly displaced (0.005 nm to 0.05 nm) from their higher symmetry positions. In orthorhombic Pbnm perovskites, for example, pseudosymmetry may be evaluated from the c/a unit cell parameter ratio, which is very close to 1. Two main types of distortions from the higher symmetry structure are recognised: a

Electron backscatter diffraction as a useful method for alloys microstructure characterization

Energy Technology Data Exchange (ETDEWEB)

Klimek, Leszek; Pietrzyk, Bozena

2004-11-17

Microstructure examination of cast Co-Cr-Mo alloy is presented in this paper. The surface morphology and chemical composition of the alloy were investigated by means of scanning electron microscopy (SEM) and energy dispersive X-ray microanalysis (EDX). An identification of alloy phases was carried out using electron backscatter diffraction (EBSD). Two different kinds of precipitates in metallic matrix were found. They were identified as MC and M{sub 23}C{sub 6} type of carbides in Co-lattice solid solution. The advantages and limits of the EBSD method are described. It is presented that EBSD, as excellent tool for phase identification, is a valuable supplementary method for materials research.

Automated Quantitative Rare Earth Elements Mineralogy by Scanning Electron Microscopy

Science.gov (United States)

Sindern, Sven; Meyer, F. Michael

2016-09-01

Increasing industrial demand of rare earth elements (REEs) stems from the central role they play for advanced technologies and the accelerating move away from carbon-based fuels. However, REE production is often hampered by the chemical, mineralogical as well as textural complexity of the ores with a need for better understanding of their salient properties. This is not only essential for in-depth genetic interpretations but also for a robust assessment of ore quality and economic viability. The design of energy and cost-efficient processing of REE ores depends heavily on information about REE element deportment that can be made available employing automated quantitative process mineralogy. Quantitative mineralogy assigns numeric values to compositional and textural properties of mineral matter. Scanning electron microscopy (SEM) combined with a suitable software package for acquisition of backscatter electron and X-ray signals, phase assignment and image analysis is one of the most efficient tools for quantitative mineralogy. The four different SEM-based automated quantitative mineralogy systems, i.e. FEI QEMSCAN and MLA, Tescan TIMA and Zeiss Mineralogic Mining, which are commercially available, are briefly characterized. Using examples of quantitative REE mineralogy, this chapter illustrates capabilities and limitations of automated SEM-based systems. Chemical variability of REE minerals and analytical uncertainty can reduce performance of phase assignment. This is shown for the REE phases parisite and synchysite. In another example from a monazite REE deposit, the quantitative mineralogical parameters surface roughness and mineral association derived from image analysis are applied for automated discrimination of apatite formed in a breakdown reaction of monazite and apatite formed by metamorphism prior to monazite breakdown. SEM-based automated mineralogy fulfils all requirements for characterization of complex unconventional REE ores that will become

In situ quantitative characterisation of the ocean water column using acoustic multibeam backscatter data

Science.gov (United States)

Lamarche, G.; Le Gonidec, Y.; Lucieer, V.; Lurton, X.; Greinert, J.; Dupré, S.; Nau, A.; Heffron, E.; Roche, M.; Ladroit, Y.; Urban, P.

2017-12-01

Detecting liquid, solid or gaseous features in the ocean is generating considerable interest in the geoscience community, because of their potentially high economic values (oil & gas, mining), their significance for environmental management (oil/gas leakage, biodiversity mapping, greenhouse gas monitoring) as well as their potential cultural and traditional values (food, freshwater). Enhancing people's capability to quantify and manage the natural capital present in the ocean water goes hand in hand with the development of marine acoustic technology, as marine echosounders provide the most reliable and technologically advanced means to develop quantitative studies of water column backscatter data. This is not developed to its full capability because (i) of the complexity of the physics involved in relation to the constantly changing marine environment, and (ii) the rapid technological evolution of high resolution multibeam echosounder (MBES) water-column imaging systems. The Water Column Imaging Working Group is working on a series of multibeam echosounder (MBES) water column datasets acquired in a variety of environments, using a range of frequencies, and imaging a number of water-column features such as gas seeps, oil leaks, suspended particulate matter, vegetation and freshwater springs. Access to data from different acoustic frequencies and ocean dynamics enables us to discuss and test multifrequency approaches which is the most promising means to develop a quantitative analysis of the physical properties of acoustic scatterers, providing rigorous cross calibration of the acoustic devices. In addition, high redundancy of multibeam data, such as is available for some datasets, will allow us to develop data processing techniques, leading to quantitative estimates of water column gas seeps. Each of the datasets has supporting ground-truthing data (underwater videos and photos, physical oceanography measurements) which provide information on the origin and

Microstructural evolution in adiabatic shear bands of copper at high strain rates: Electron backscatter diffraction characterization

International Nuclear Information System (INIS)

Tang Lin; Chen Zhiyong; Zhan Congkun; Yang Xuyue; Liu Chuming; Cai Hongnian

2012-01-01

The microstructural evolution of adiabatic shear bands in annealed copper with different large strains at high strain rates has been investigated by electron backscatter diffraction. The results show that mechanical twinning can occur with minimal contribution to shear localization under dynamic loading. Elongated ultrafine grains with widths of 100–300 nm are observed during the evolution of the adiabatic shear bands. A rotational dynamic recrystallization mechanism is proposed to explain the formation of the elongated ultrafine grains. - Highlights: ► The microstructural evolution of ASB is studied by electron backscatter diffraction. ► Twinning can occur in ASB while the contribution to shear localization is slight. ► Elongated ultrafine grains are observed during the evolution process of ASB. ► A possible mechanism is proposed to explain the microstructure evolution of ASB.

Dark-field imaging based on post-processed electron backscatter diffraction patterns of bulk crystalline materials in a scanning electron microscope.

Science.gov (United States)

Brodusch, Nicolas; Demers, Hendrix; Gauvin, Raynald

2015-01-01

Dark-field (DF) images were acquired in the scanning electron microscope with an offline procedure based on electron backscatter diffraction (EBSD) patterns (EBSPs). These EBSD-DF images were generated by selecting a particular reflection on the electron backscatter diffraction pattern and by reporting the intensity of one or several pixels around this point at each pixel of the EBSD-DF image. Unlike previous studies, the diffraction information of the sample is the basis of the final image contrast with a pixel scale resolution at the EBSP providing DF imaging in the scanning electron microscope. The offline facility of this technique permits the selection of any diffraction condition available in the diffraction pattern and displaying the corresponding image. The high number of diffraction-based images available allows a better monitoring of deformation structures compared to electron channeling contrast imaging (ECCI) which is generally limited to a few images of the same area. This technique was applied to steel and iron specimens and showed its high capability in describing more rigorously the deformation structures around micro-hardness indents. Due to the offline relation between the reference EBSP and the EBSD-DF images, this new technique will undoubtedly greatly improve our knowledge of deformation mechanism and help to improve our understanding of the ECCI contrast mechanisms. Copyright © 2014 Elsevier B.V. All rights reserved.

Low-temperature system for simultaneous counting of conversion electrons and backscattered [gamma]-rays in Moessbauer effect experiment

Energy Technology Data Exchange (ETDEWEB)

Ruskov, Todor (Institute for Nuclear Research and Nuclear Energy, Tsarigradsko shosse 72, Sofia 1784 (Bulgaria)); Passage, Guener (Institute for Nuclear Research and Nuclear Energy, Tsarigradsko shosse 72, Sofia 1784 (Bulgaria)); Rastanawi, Abdallah (Institute for Nuclear Research and Nuclear Energy, Tsarigradsko shosse 72, Sofia 1784 (Bulgaria)); Radev, Rumen (Institute for Nuclear Research and Nuclear Energy, Tsarigradsko shosse 72, Sofia 1784 (Bulgaria))

1994-12-01

A system for simultaneous detection of conversion electrons, emitted after resonant exciting of [sup 57]Fe, and resonant backscattered [gamma]-rays and X-rays, accompanying the conversion electrons, is described. The system includes a helium proportional counter, for detection of conversion electrons, and a toroidal ''Keisch-type'' proportional counter, connected to the vacuum part of a helium cryostat. ((orig.))

Backscattered electron imaging at low emerging angles: A physical approach to contrast in LVSEM

Energy Technology Data Exchange (ETDEWEB)

Cazaux, J., E-mail: jacques.cazaux@univ-reims.fr [LISM, EA 4695 Faculty of Sciences, BP 1039, 51687 Reims Cedex 2 (France); Kuwano, N. [Malaysia–Japan International Institute of Technology, Universiti Teknologi Malaysia, Jalan Semarak, 54100 Kuala Lumpur (Malaysia); Sato, K. [Steel Research Laboratory, JFE Steel Corporation, 1 Kawasaki-cho, Chuo-ku, Chiba 260-0835 (Japan)

2013-12-15

Due to the influence of refraction effects on the escape probability of the Back-Scattered Electrons (BSE), an expression of the fraction of these BSE is given as a function of the beam energy, E°, and emission angle (with respect to the normal) α. It has been shown that these effects are very sensitive to a local change of the work function in particular for low emerging angles. This sensitivity suggests a new type of contrast in Low Voltage Scanning Electron Microscopy (LVSEM for E°<2 keV): the work function contrast. Involving the change of ϕ with crystalline orientation, this possibility is supported by a new interpretation of a few published images. Some other correlated contrasts are also suggested. These are topographical contrasts or contrasts due to subsurface particles and cracks. Practical considerations of the detection system and its optimization are indicated. - Highlights: • Refraction effects experienced by Back-Scattered Electrons at sample/vacuum interfaces are evaluated as a function of energy and angles. • Sensitive to local work function changes with crystalline orientation these effects concern mainly keV-electrons at low emerging angles. • A new type of contrast in SEM is thus deduced and illustrated. • Some other correlated contrasts, topographical contrasts or contrasts due to subsurface particles and cracks are also suggested.

Quantitative secondary electron detection

Science.gov (United States)

Agrawal, Jyoti; Joy, David C.; Nayak, Subuhadarshi

2018-05-08

Quantitative Secondary Electron Detection (QSED) using the array of solid state devices (SSD) based electron-counters enable critical dimension metrology measurements in materials such as semiconductors, nanomaterials, and biological samples (FIG. 3). Methods and devices effect a quantitative detection of secondary electrons with the array of solid state detectors comprising a number of solid state detectors. An array senses the number of secondary electrons with a plurality of solid state detectors, counting the number of secondary electrons with a time to digital converter circuit in counter mode.

Time-lapse misorientation maps for the analysis of electron backscatter diffraction data from evolving microstructures

NARCIS (Netherlands)

Wheeler, J.; Cross, A.; Drury, M.; Hough, R.M.; Mariani, E.; Piazolo, S.; Prior, D.J.

2011-01-01

A “time-lapse misorientation map” is defined here as a map which shows the orientation change at each point in an evolving crystalline microstructure between two different times. Electron backscatter diffraction data from in situ heating experiments can be used to produce such maps, which then

Evaluation of the photon monitor backscatter in medical electron accelerators

International Nuclear Information System (INIS)

Zrenner, M.; Krieger, H.

1999-01-01

Background: Modern linear accelerators permit the use of irregular fields due to their flexible collimator systems with separately movable jaws or multileaf collimators. When using such irregular fields in the clinical practice output factors have to be corrected for enhanced backscatter to the dose monitor as compared with the conventional block shieldings. Methods: A method is presented to detect the monitor backscatter contributions to the output factor for irregular field settings. Results: The monitor backscatter factors have been measured using a telescopic device for 2 different treatment head geometries (Varian Clinac 2100C/D, General Electric Saturne 15) and for 3 photon radiation qualities (nominal energies X6, X18, X12). A method is introduced to calculate the monitor backscatter for arbitrary irregular treatment fields from the experimental data for square or rectangular fields. Conclusions: Besides the corrections for changes in phantom scatter and changes in the aperture, corrections for monitor backscatter have to be taken into account in many clinical cases. They can contribute up to more than 10% compared with the monitor values for free regular fields. (orig.) [de

Experimental observations of electron-backscatter effects from high-atomic-number anodes in large-aspect-ratio, electron-beam diodes

Energy Technology Data Exchange (ETDEWEB)

Cooperstein, G; Mosher, D; Stephanakis, S J; Weber, B V; Young, F C [Naval Research Laboratory, Washington, DC (United States); Swanekamp, S B [JAYCOR, Vienna, VA (United States)

1997-12-31

Backscattered electrons from anodes with high-atomic-number substrates cause early-time anode-plasma formation from the surface layer leading to faster, more intense electron beam pinching, and lower diode impedance. A simple derivation of Child-Langmuir current from a thin hollow cathode shows the same dependence on the diode aspect ratio as critical current. Using this fact, it is shown that the diode voltage and current follow relativistic Child-Langmuir theory until the anode plasma is formed, and then follows critical current after the beam pinches. With thin hollow cathodes, electron beam pinching can be suppressed at low voltages (< 800 kV) even for high currents and high-atomic-number anodes. Electron beam pinching can also be suppressed at high voltages for low-atomic-number anodes as long as the electron current densities remain below the plasma turn-on threshold. (author). 8 figs., 2 refs.

Correlation of electron backscatter diffraction and piezoresponse force microscopy for the nanoscale characterization of ferroelectric domains in polycrystalline lead zirconate titanate

Science.gov (United States)

Burnett, T. L.; Weaver, P. M.; Blackburn, J. F.; Stewart, M.; Cain, M. G.

2010-08-01

The functional properties of ferroelectric ceramic bulk or thin film materials are strongly influenced by their nanostructure, crystallographic orientation, and structural geometry. In this paper, we show how, by combining textural analysis, through electron backscattered diffraction, with piezoresponse force microscopy, quantitative measurements of the piezoelectric properties can be made at a scale of 25 nm, smaller than the domain size. The combined technique is used to obtain data on the domain-resolved effective single crystal piezoelectric response of individual crystallites in Pb(Zr0.4Ti0.6)O3 ceramics. The results offer insight into the science of domain engineering and provide a tool for the future development of new nanostructured ferroelectric materials for memory, nanoactuators, and sensors based on magnetoelectric multiferroics.

A scanning electron microscope method for automated, quantitative analysis of mineral matter in coal

Energy Technology Data Exchange (ETDEWEB)

Creelman, R.A.; Ward, C.R. [R.A. Creelman and Associates, Epping, NSW (Australia)

1996-07-01

Quantitative mineralogical analysis has been carried out in a series of nine coal samples from Australia, South Africa and China using a newly-developed automated image analysis system coupled to a scanning electron microscopy. The image analysis system (QEM{asterisk}SEM) gathers X-ray spectra and backscattered electron data from a number of points on a conventional grain-mount polished section under the SEM, and interprets the data from each point in mineralogical terms. The cumulative data in each case was integrated to provide a volumetric modal analysis of the species present in the coal samples, expressed as percentages of the respective coals` mineral matter. Comparison was made of the QEM{asterisk}SEM results to data obtained from the same samples using other methods of quantitative mineralogical analysis, namely X-ray diffraction of the low-temperature oxygen-plasma ash and normative calculation from the (high-temperature) ash analysis and carbonate CO{sub 2} data. Good agreement was obtained from all three methods for quartz in the coals, and also for most of the iron-bearing minerals. The correlation between results from the different methods was less strong, however, for individual clay minerals, or for minerals such as calcite, dolomite and phosphate species that made up only relatively small proportions of the mineral matter. The image analysis approach, using the electron microscope for mineralogical studies, has significant potential as a supplement to optical microscopy in quantitative coal characterisation. 36 refs., 3 figs., 4 tabs.

Effects of focused ion beam milling on electron backscatter diffraction patterns in strontium titanate and stabilized zirconia

DEFF Research Database (Denmark)

Saowadee, Nath; Agersted, Karsten; Bowen, Jacob R.

2012-01-01

This study investigates the effect of focused ion beam (FIB) current and accelerating voltage on electron backscatter diffraction pattern quality of yttria‐stabilized zirconia (YSZ) and Nb‐doped strontium titanate (STN) to optimize data quality and acquisition time for 3D‐EBSD experiments by FIB...

Compton backscattered collmated X-ray source

Science.gov (United States)

Ruth, Ronald D.; Huang, Zhirong

2000-01-01

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Compton backscattered collimated x-ray source

Science.gov (United States)

Ruth, R.D.; Huang, Z.

1998-10-20

A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

Relationship between the v2PO4/amide III ratio assessed by Raman spectroscopy and the calcium content measured by quantitative backscattered electron microscopy in healthy human osteonal bone

Science.gov (United States)

Roschger, Andreas; Gamsjaeger, Sonja; Hofstetter, Birgit; Masic, Admir; Blouin, Stéphane; Messmer, Phaedra; Berzlanovich, Andrea; Paschalis, Eleftherios P.; Roschger, Paul; Klaushofer, Klaus; Fratzl, Peter

2014-06-01

Raman microspectroscopy and quantitative backscattered electron imaging (qBEI) of bone are powerful tools to investigate bone material properties. Both methods provide information on the degree of bone matrix mineralization. However, a head-to-head comparison of these outcomes from identical bone areas has not been performed to date. In femoral midshaft cross sections of three women, 99 regions (20×20 μ) were selected inside osteons and interstitial bone covering a wide range of matrix mineralization. As the focus of this study was only on regions undergoing secondary mineralization, zones exhibiting a distinct gradient in mineral content close to the mineralization front were excluded. The same regions were measured by both methods. We found a linear correlation (R2=0.75) between mineral/matrix as measured by Raman spectroscopy and the wt. %Mineral/(100-wt. %Mineral) as obtained by qBEI, in good agreement with theoretical estimations. The observed deviations of single values from the linear regression line were determined to reflect biological heterogeneities. The data of this study demonstrate the good correspondence between Raman and qBEI outcomes in describing tissue mineralization. The obtained correlation is likely sensitive to changes in bone tissue composition, providing an approach to detect potential deviations from normal bone.

Time evolution analysis of the electron distribution in Thomson/Compton back-scattering

International Nuclear Information System (INIS)

Petrillo, V.; Bacci, A.; Curatolo, C.; Maroli, C.; Serafini, L.; Rossi, A. R.

2013-01-01

We present the time evolution of the energy distribution of a relativistic electron beam after the Compton back-scattering with a counter-propagating laser field, performed in the framework of the Quantum Electrodynamics, by means of the code CAIN. As the correct angular distribution of the spontaneous emission is accounted, the main effect is the formation of few stripes, followed by the diffusion of the more energetic particles toward lower values in the longitudinal phase space. The Chapman-Kolmogorov master equation gives results in striking agreement with the numerical ones. An experiment on the Thomson source at SPARC-LAB is proposed

Analysis of soft magnetic materials by electron backscatter diffraction as a powerful tool

Directory of Open Access Journals (Sweden)

David Schuller

2018-04-01

Full Text Available The current work demonstrates that electron backscatter diffraction (EBSD is a powerful and versatile characterization technique for investigating soft magnetic materials. The properties of soft magnets, e.g., magnetic losses strongly depend on the materials chemical composition and microstructure, including grain size and shape, texture, degree of plastic deformation and elastic strain. In electrical sheet stacks for e-motor applications, the quality of the machined edges/surfaces of each individual sheet is of special interest. Using EBSD, the influence of the punching process on the microstructure at the cutting edge is quantitatively assessed by evaluating the crystallographic misorientation distribution of the deformed grains. Using an industrial punching process, the maximum affected deformation depth is determined to be 200 - 300 μm. In the case of laser cutting, the affected deformation depth is determined to be approximately zero. Reliability and detection limits of the developed EBSD approach are evaluated on non-affected sample regions and model samples containing different indentation test bodies. A second application case is the investigation of the recrystallization process during the annealing step of soft magnetic composites (SMC toroids produced by powder metallurgy as a function of compaction pressure, annealing parameters and powder particle size. With increasing pressure and temperature, the recrystallized area fraction (e.g., grains with crystallographic misorientations 3°.

Identification of phases in zinc alloy powders using electron backscatter diffraction

Energy Technology Data Exchange (ETDEWEB)

Perez, Martin G. [Graduate Center for Materials Research, University of Missouri-Rolla, Rolla, MO 65409 (United States); Kenik, Edward A. [Oak Ridge National Laboratory, 100 Bethel Valley Rd., Bldg. 4515, MS-6064, P.O. Box 2008, Oak Ridge, TN 37831 (United States); O' Keefe, Matthew J. [Graduate Center for Materials Research, University of Missouri-Rolla, Rolla, MO 65409 (United States)]. E-mail: mjokeefe@umr.edu; Miller, F. Scott [Graduate Center for Materials Research, University of Missouri-Rolla, Rolla, MO 65409 (United States); Johnson, Benedict [Graduate Center for Materials Research, University of Missouri-Rolla, Rolla, MO 65409 (United States)

2006-05-25

Scanning electron microscopy and electron backscatter diffraction (EBSD) were used for the structural characterization of phases in Zn alloy powders. Commercial Zn alloy powders contained additions of <1000 ppm of Bi, In, Al or Mg. Bismuth and In have extremely low solubility in Zn and form intermetallic Bi-In compounds which segregate to the Zn grain boundaries. The Bi-In phases were <0.3 {mu}m in size, had low melting points, and were not abundant enough for EBSD analysis. Increasing the alloying additions 20-40-fold resulted in Bi-In phases >1 {mu}m that could be used for EBSD analysis for phase characterization. Deformation-free microstructures were obtained by mechanical polishing and ion milling. The Zn matrix was characterized as Zn via EBSD. A BiIn{sub 2} phase was identified in the powder microstructures via EBSD. An In phase with 8-9 wt.% Bi was identified using low voltage energy dispersive spectroscopy and closely matched the composition predicted by the Bi-In phase diagram.

Electron backscatter diffraction: Strategies for reliable data acquisition and processing

International Nuclear Information System (INIS)

Randle, Valerie

2009-01-01

In electron backscatter diffraction (EBSD) software packages there are many user choices both in data acquisition and in data processing and display. In order to extract maximum scientific value from an inquiry, it is helpful to have some guidelines for best practice in conducting an EBSD investigation. The purpose of this article therefore is to address selected topics of EBSD practice, in a tutorial manner. The topics covered are a brief summary on the principles of EBSD, specimen preparation, calibration of an EBSD system, experiment design, speed of data acquisition, data clean-up, microstructure characterisation (including grain size) and grain boundary characterisation. This list is not meant to cover exhaustively all areas where EBSD is used, but rather to provide a resource consisting of some useful strategies for novice EBSD users.

Electron and ion currents relevant to accurate current integration in MeV ion backscattering spectrometry

International Nuclear Information System (INIS)

Matteson, S.; Nicolet, M.A.

1979-01-01

The magnitude and characteristics of the currents which flow in the target and the chamber of an MeV ion backscattering spectrometer are examined. Measured energy distributions and the magnitude of high-energy secondary electron currents are reported. An empirical universal curve is shown to fit the energy distribution of secondary electrons for several combinations of ion energy, targets and ion species. The magnitude of tertiary electron currents which arise at the vacuum vessel walls is determined for various experimental situations and is shown to be non-negligible in many cases. An experimental arrangement is described which permits charge integrations to 1% arruracy without restricting access to the target as a Faraday cage does. (Auth.)

Secondary electron emission from metals and semi-conductor compounds

International Nuclear Information System (INIS)

Ono, Susumu; Kanaya, Koichi

1979-01-01

Attempt was made to present the sufficient solution of the secondary electron yield of metals and semiconductor compounds except insulators, applying the free electron scattering theory to the absorption of secondary electrons generated within a solid target. The paper is divided into the sections describing absorption coefficient and escape depth, quantitative characteristics of secondary yield, angular distribution of secondary electron emission, effect of incident angle to secondary yield, secondary electron yield transmitted, and lateral distribution of secondary electron emission, besides introduction and conclusion. The conclusions are as follows. Based on the exponential power law for screened atomic potential, secondary electron emission due to both primary and backscattered electrons penetrating into metallic elements and semi-conductive compounds is expressed in terms of the ionization loss in the first collision for escaping secondary electrons. The maximum yield and the corresponding primary energy can both consistently be derived as the functions of three parameters: atomic number, first ionization energy and backscattering coefficient. The yield-energy curve as a function of the incident energy and the backscattering coefficient is in good agreement with the experimental results. The energy dependence of the yield in thin films and the lateral distribution of secondary yield are derived as the functions of the backscattering coefficient and the primary energy. (Wakatsuki, Y.)

Effect of different electron elastic-scattering cross sections on inelastic mean free paths obtained from elastic-backscattering experiments

International Nuclear Information System (INIS)

Jablonskiz, A.; Salvatz, F.; Powellz, C.J.

2004-01-01

Inelastic mean free paths (IMFPs) of electrons with energies between 100 eV and 5,000 eV have been frequently obtained from measurements of elastic-backscattering probabilities for different specimen materials. A calculation of these probabilities is also required to determine IMFPs. We report calculations of elastic-backscattering probabilities for gold at energies of 100 eV and 500 eV with differential elastic-scattering cross sections obtained from the Thomas-Fermi-Dirac potential and the more reliable Dirac-Hartree-Fock potential. For two representative experimental configurations, the average deviation between IMFPs obtained with cross sections from the two potentials was 11.4 %. (author)

Time-lapse misorientation maps for the analysis of electron backscatter diffraction data from evolving microstructures

International Nuclear Information System (INIS)

Wheeler, J.; Cross, A.; Drury, M.; Hough, R.M.; Mariani, E.; Piazolo, S.; Prior, D.J.

2011-01-01

A 'time-lapse misorientation map' is defined here as a map which shows the orientation change at each point in an evolving crystalline microstructure between two different times. Electron backscatter diffraction data from in situ heating experiments can be used to produce such maps, which then highlight areas of microstructural change and also yield statistics indicative of how far different types of boundary (with different misorientations) have moved.

Lattice constant measurement from electron backscatter diffraction patterns

DEFF Research Database (Denmark)

Saowadee, Nath; Agersted, Karsten; Bowen, Jacob R.

2017-01-01

Kikuchi bands in election backscattered diffraction patterns (EBSP) contain information about lattice constants of crystallographic samples that can be extracted via the Bragg equation. An advantage of lattice constant measurement from EBSPs over diffraction (XRD) is the ability to perform local ...

Backscattered electron emission after proton impact on carbon and gold films: Experiments and simulations

Energy Technology Data Exchange (ETDEWEB)

Hespeels, F.; Heuskin, A.C. [University of Namur, PMR, 61 rue de Bruxelles, B-5000 Namur (Belgium); Scifoni, E. [TIFPA-INFN, Trento Institute for Fundamental Physics and Applications, Via Sommarive 14, I-38123 Trento (Italy); GSI-Helmholtzzentrum für Schwerionenforschung, Biophysik, Max Planck-Strasse 1, D-64291 Darmstadt (Germany); Kraemer, M. [GSI-Helmholtzzentrum für Schwerionenforschung, Biophysik, Max Planck-Strasse 1, D-64291 Darmstadt (Germany); Lucas, S., E-mail: stephane.lucas@unamur.be [University of Namur, PMR, 61 rue de Bruxelles, B-5000 Namur (Belgium)

2017-06-15

This work aims at measuring the proton induced secondary electron energy spectra from nanometer thin films. Backscattered electron energy spectra were measured within an energy range from 0 to 600 eV using a Retarding Field Analyser (RFA). This paper presents energy spectra obtained for proton (0.5 MeV; 1 MeV; 1.5 MeV; 2 MeV) irradiation of thin carbon films (50 and 100 nm thick) and thin gold film (200 nm). These experimental spectra were compared with Monte Carlo simulations based on TRAX code and Geant4 simulation toolkit. Good agreement between experimental, TRAX and Geant4 results were observed for the carbon target. For the gold target, we report major differences between both Monte Carlo environments. Limitation of Geant4 models for low energy electron emission was highlighted. On the contrary, TRAX simulations present encouraging results for the modeling of low-energy electron emission from gold target.

Monte Carlo simulation of electron depth distribution and backscattering for carbon films deposited on aluminium as a function of incidence angle and primary energy

Science.gov (United States)

Dapor, Maurizio

2005-01-01

Carbon films are deposited on various substrates (polymers, polyester fabrics, polyester yarns, metal alloys) both for experimental and technological motivations (medical devices, biocompatible coatings, food package and so on). Computational studies of the penetration of electron beams in supported thin film of carbon are very useful in order to compare the simulated results with analytical techniques data (obtained by scanning electron microscopy and/or Auger electron spectroscopy) and investigate the film characteristics. In the present paper, the few keV electron depth distribution and backscattering coefficient for the special case of film of carbon deposited on aluminium are investigated, by a Monte Carlo simulation, as a function of the incidence angle and primary electron energy. The simulated results can be used as a way to evaluate the carbon film thickness by a set of measurements of the backscattering coefficient.

A Dictionary Approach to Electron Backscatter Diffraction Indexing.

Science.gov (United States)

Chen, Yu H; Park, Se Un; Wei, Dennis; Newstadt, Greg; Jackson, Michael A; Simmons, Jeff P; De Graef, Marc; Hero, Alfred O

2015-06-01

We propose a framework for indexing of grain and subgrain structures in electron backscatter diffraction patterns of polycrystalline materials. We discretize the domain of a dynamical forward model onto a dense grid of orientations, producing a dictionary of patterns. For each measured pattern, we identify the most similar patterns in the dictionary, and identify boundaries, detect anomalies, and index crystal orientations. The statistical distribution of these closest matches is used in an unsupervised binary decision tree (DT) classifier to identify grain boundaries and anomalous regions. The DT classifies a pattern as an anomaly if it has an abnormally low similarity to any pattern in the dictionary. It classifies a pixel as being near a grain boundary if the highly ranked patterns in the dictionary differ significantly over the pixel's neighborhood. Indexing is accomplished by computing the mean orientation of the closest matches to each pattern. The mean orientation is estimated using a maximum likelihood approach that models the orientation distribution as a mixture of Von Mises-Fisher distributions over the quaternionic three sphere. The proposed dictionary matching approach permits segmentation, anomaly detection, and indexing to be performed in a unified manner with the additional benefit of uncertainty quantification.

Evaluation of computational models and cross sections used by MCNP6 for simulation of electron backscattering

Energy Technology Data Exchange (ETDEWEB)

Poškus, Andrius, E-mail: andrius.poskus@ff.vu.lt

2016-02-01

This work evaluates the accuracy of the single-event (SE) and condensed-history (CH) models of electron transport in Monte Carlo simulations of electron backscattering from thick layers of Be, C, Al, Cu, Ag, Au and U at incident electron energies from 200 eV to 15 MeV. The CH method is used in simulations performed with MCNP6.1, and the SE method is used in simulations performed with an open-source single-event code MCNelectron written by the author of this paper. Both MCNP6.1 and MCNelectron use mainly ENDF/B-VI.8 library data, but MCNelectron allows replacing cross sections of certain types of interactions by alternative datasets from other sources. The SE method is evaluated both using only ENDF/B-VI.8 cross sections (the “SE-ENDF/B method”, which is equivalent to using MCNP6.1 in SE mode) and with an alternative set of elastic scattering cross sections obtained from relativistic (Dirac) partial-wave (DPW) calculations (the “SE-DPW method”). It is shown that at energies from 200 eV to 300 keV the estimates of the backscattering coefficients obtained using the SE-DPW method are typically within 10% of the experimental data, which is approximately the same accuracy that is achieved using MCNP6.1 in CH mode. At energies below 1 keV and above 300 keV, the SE-DPW method is much more accurate than the SE-ENDF/B method due to lack of angular distribution data in the ENDF/B library in those energy ranges. At energies from 500 keV to 15 MeV, the CH approximation is roughly twice more accurate than the SE-DPW method, with the average relative errors equal 7% and 14%, respectively. The energy probability density functions (PDFs) of backscattered electrons for Al and Cu, calculated using the SE method with DPW cross sections when energy of incident electrons is 20 keV, have an average absolute error as low as 4% of the average PDF. This error is approximately twice less than the error of the corresponding PDF calculated using the CH approximation. It is concluded

Application of particle-induced X-ray emission, backscattering spectrometry and scanning electron microscopy in the evaluation of orthodontic materials

International Nuclear Information System (INIS)

Gihwala, D.; Mars, J.A.; Pineda-Vargas, C.

2013-01-01

The focus of this investigation was on orthodontic materials used in the manufacture of dental brackets. The properties of these dental materials are subjected to various physical parameters such as elongation, yield strength and elasticity that justify their application. In turn, these parameters depend on the quantitative elemental concentration distribution (QECD) in the materials used in the manufacture. For compositional analysis, proton-induced X-ray emission (PIXE), backscatter spectrometry (BS) and scanning electron microscopy (SEM) were applied. QECD analysis was performed to correlate the physical parameters with the composition and to quantify imperfections in the materials. PIXE and BS analyses were performed simultaneously with a 3 MeV proton beam while electrons accelerated at 25 keV were used for the SEM analysis. From the QECDs it was observed that: (1) the major elements Cr, Fe and Ni were homogeneously distributed in the orthodontic plate; (2) the distribution of Mo and O correlated with one another; (3) there was a spread of Cr around regions of high C concentration; and, (4) areas of high concentrations of Mo and O corresponded to a decrease in C concentrations. Elemental concentration correlations are shown to indicate the similarities and differences in the ease of formation of phases, based on the tangent of linearity. (author)

Interlinking backscatter, grain size and benthic community structure

Science.gov (United States)

McGonigle, Chris; Collier, Jenny S.

2014-06-01

The relationship between acoustic backscatter, sediment grain size and benthic community structure is examined using three different quantitative methods, covering image- and angular response-based approaches. Multibeam time-series backscatter (300 kHz) data acquired in 2008 off the coast of East Anglia (UK) are compared with grain size properties, macrofaunal abundance and biomass from 130 Hamon and 16 Clamshell grab samples. Three predictive methods are used: 1) image-based (mean backscatter intensity); 2) angular response-based (predicted mean grain size), and 3) image-based (1st principal component and classification) from Quester Tangent Corporation Multiview software. Relationships between grain size and backscatter are explored using linear regression. Differences in grain size and benthic community structure between acoustically defined groups are examined using ANOVA and PERMANOVA+. Results for the Hamon grab stations indicate significant correlations between measured mean grain size and mean backscatter intensity, angular response predicted mean grain size, and 1st principal component of QTC analysis (all p PERMANOVA for the Hamon abundance shows benthic community structure was significantly different between acoustic groups for all methods (p ≤ 0.001). Overall these results show considerable promise in that more than 60% of the variance in the mean grain size of the Clamshell grab samples can be explained by mean backscatter or acoustically-predicted grain size. These results show that there is significant predictive capacity for sediment characteristics from multibeam backscatter and that these acoustic classifications can have ecological validity.

A compact Compton backscatter X-ray source for mammography and coronary angiography

International Nuclear Information System (INIS)

Nguyen, D.C.; Kinross-Wright, J.M.; Weber, M.E.; Volz, S.K.; Gierman, S.M.; Hayes, K.; Vernon, W.; Goldstein, D.J.

1998-01-01

This is the final report of a three-year, Laboratory Directed Research and Development (LDRD) project at Los Alamos National Laboratory (LANL). The project objective is to generate a large flux of tunable, monochromatic x-rays for use in mammography and coronary angiography. The approach is based on Compton backscattering of an ultraviolet solid-state laser beam against the high-brightness 20-MeV electron beams from a compact linear accelerator. The direct Compton backscatter approach failed to produce a large flux of x-rays due to the low photon flux of the scattering solid-state laser. The authors have modified the design of a compact x-ray source to the new Compton backscattering geometry with use of a regenerative amplifier free-electron laser. They have successfully demonstrated the production of a large flux of infrared photons and a high-brightness electron beam focused in both dimensions for performing Compton backscattering in a regenerative amplifier geometry

Determination of the analyzing power of the A4 Compton-backscattering polarimeter for the measurement of the longitudinal spin polarization of the MAMI electron beam

International Nuclear Information System (INIS)

Diefenbacher, Juergen

2010-01-01

The A4 experiment determines the strange quark contribution to the electromagnetic from factors of the nucleon by measuring the parity violation in elastic electron nucleon scattering. These measurements are carried out using the spin polarized electron beam of the Mainzer Mikrotron (MAMI) with beam energies in the range from 315 to 1508 MeV. For the data analysis it is essential to determine the degree of polarization of the electron beam in order to extract the physics asymmetry from the measured parity violating asymmetry. For this reason the A4 collaboration has developed a novel type of Compton laser backscattering polarimeter that allows for a non-destructive measurement of the beam polarization in parallel to the running parity experiment. In the scope of this work the polarimeter was refined in order to enable reliable continuous operation of the polarimeter. The data acquisition system for the photon and electron detector was re-designed and optimized to cope with high count rates. A novel detector (LYSO) for the backscattered photons was commissioned. Furthermore, GEANT4 simulations of the detectors have been performed and an analysis environment for the extraction of Compton asymmetries from the backscattered photon data has been developed. The analysis makes use of the possibility to detect backscattered photons in coincidence with the scattered electrons, thus tagging the photons. The tagging introduces a differential energy scale which enables the precise determination of the analyzing power. In this work the analyzing power of the polarimeter has been determined. Therefore, at a beam current of 20 μA the product of electron and laser polarization can be determined, while the parity experiment is running, with a statistical accuracy of 1 % in 24 hours at 855 MeV or 2 =0.6 (GeV/c) 2 the analysis yields a raw asymmetry of A Roh PV =(-20.0±0.9 stat ) x 10 -6 at the moment. For a beam polarization of 80 % the total error would be 1,68 x 10 -6 with ΔP e

Comparison of STIM and particle backscattering spectrometry mass determination for quantitative microanalysis of cultured cells

International Nuclear Information System (INIS)

Deves, G.; Ortega, R.

2001-01-01

In biological sample microanalysis, a mass-normalisation method is commonly used as a quantitative index of elemental concentrations determined by particle-induced X-ray emission (PIXE). The organic mass can either be determined using particle backscattering spectrometry (BS) or scanning transmission ion microscopy (STIM). However, the accuracy of quantitative microanalysis in samples such as cultured cells is affected by beam-induced loss of organic mass during analysis. The aim of this paper is to compare mass measurements determined by particle BS or by STIM. In order to calibrate STIM and BS analyses, we measured by both techniques the thickness of standard foils of polycarbonate (3 and 6 μm), Mylar[reg] (4 μm), Kapton[reg] (7.5 μm) and Nylon[reg] (15 μm), as well as biological samples of mono-layered cultured cells. Non-damaging STIM analysis of samples before PIXE irradiation is certainly one of the most accurate ways to determine the sample mass, however, this requires strong experimental handling. On the other hand, BS performed simultaneously to PIXE is the simplest method to determine the local mass in polymer foils, but appears less accurate in the case of cultured cells

Backscatter dose from metallic materials due to obliquely incident high-energy photon beams

International Nuclear Information System (INIS)

Nadrowitz, Roger; Feyerabend, Thomas

2001-01-01

If metallic material is exposed to ionizing radiation of sufficient high energy, an increase in dose due to backscatter radiation occurs in front of this material. Our purpose in this study was to quantify these doses at variable distances between scattering materials and the detector at axial beam angles between 0 deg. (zero angle in beams eye view) and 90 deg. . Copper, silver and lead sheets embedded in a phantom of perspex were exposed to 10 MV-bremsstrahlung. The detector we developed is based on the fluorescence property of pyromellitic acid (1,2,4,5 benzenetetracarboxylic acid) after exposure to ionizing radiation. Our results show that the additional doses and the corresponding dose distribution in front of the scattering materials depend quantitatively and qualitatively on the beam angle. The backscatter dose increases with varying beam angle from 0 deg. to 90 deg. up to a maximum at 55 deg. for copper and silver. At angles of 0 deg. and 55 deg. the integral backscatter doses over a tissue-equivalent depth of 2 mm are 11.2% and 21.6% for copper and 24% and 28% for silver, respectively. In contrast, in front of lead there are no obvious differences of the measured backscatter doses at angles between 0 deg. and 55 deg. With a further increase of the beam angle from 55 deg. to 90 deg. the backscatter dose decreases steeply for all three materials. In front of copper a markedly lower penetrating depth of the backscattered electrons was found for an angle of 0 deg. compared to 55 deg. This dependence from the beam angle was less pronounced in front of silver and not detectable in front of lead. In conclusion, the dependence of the backscatter dose from the angle between axial beam and scattering material must be considered, as higher scattering doses have to be considered than previously expected. This may have a clinical impact since the surface of metallic implants is usually curved

Backscatter dose from metallic materials due to obliquely incident high-energy photon beams

Energy Technology Data Exchange (ETDEWEB)

Nadrowitz, Roger; Feyerabend, Thomas [Medical University of Luebeck, Germany, Department of Radiotherapy and Nuclear Medicine, Ratzeburger Allee 160, Luebeck, D-23538 (Germany)

2001-06-01

If metallic material is exposed to ionizing radiation of sufficient high energy, an increase in dose due to backscatter radiation occurs in front of this material. Our purpose in this study was to quantify these doses at variable distances between scattering materials and the detector at axial beam angles between 0 deg. (zero angle in beams eye view) and 90 deg. . Copper, silver and lead sheets embedded in a phantom of perspex were exposed to 10 MV-bremsstrahlung. The detector we developed is based on the fluorescence property of pyromellitic acid (1,2,4,5 benzenetetracarboxylic acid) after exposure to ionizing radiation. Our results show that the additional doses and the corresponding dose distribution in front of the scattering materials depend quantitatively and qualitatively on the beam angle. The backscatter dose increases with varying beam angle from 0 deg. to 90 deg. up to a maximum at 55 deg. for copper and silver. At angles of 0 deg. and 55 deg. the integral backscatter doses over a tissue-equivalent depth of 2 mm are 11.2% and 21.6% for copper and 24% and 28% for silver, respectively. In contrast, in front of lead there are no obvious differences of the measured backscatter doses at angles between 0 deg. and 55 deg. With a further increase of the beam angle from 55 deg. to 90 deg. the backscatter dose decreases steeply for all three materials. In front of copper a markedly lower penetrating depth of the backscattered electrons was found for an angle of 0 deg. compared to 55 deg. This dependence from the beam angle was less pronounced in front of silver and not detectable in front of lead. In conclusion, the dependence of the backscatter dose from the angle between axial beam and scattering material must be considered, as higher scattering doses have to be considered than previously expected. This may have a clinical impact since the surface of metallic implants is usually curved.

Application of backscatter electrons for large area imaging of cavities produced by neutron irradiation

Energy Technology Data Exchange (ETDEWEB)

Pastukhov, V.I. [Joint Stock Company “Institute of Nuclear Materials” (JSC “INM”), Zarechny, Sverdlovsk Region (Russian Federation); Ural Federal University Named After the First President of Russia, B. N. Yeltsyn, Ekaterinburg (Russian Federation); National Research Nuclear University MEPhI (Moscow Engineering Physics Institute), Moscow (Russian Federation); Averin, S.A.; Panchenko, V.L. [Joint Stock Company “Institute of Nuclear Materials” (JSC “INM”), Zarechny, Sverdlovsk Region (Russian Federation); National Research Nuclear University MEPhI (Moscow Engineering Physics Institute), Moscow (Russian Federation); Portnykh, I.A. [Joint Stock Company “Institute of Nuclear Materials” (JSC “INM”), Zarechny, Sverdlovsk Region (Russian Federation); Freyer, P.D. [Westinghouse Electric Company, Pittsburgh, PA (United States); Giannuzzi, L.A. [L.A. Giannuzzi & Associates LLC, Fort Myers, FL (United States); Garner, F.A., E-mail: frank.garner@dslextreme.com [National Research Nuclear University MEPhI (Moscow Engineering Physics Institute), Moscow (Russian Federation); Radiation Effects Consulting LLC, Richland, WA (United States); Texas A& M University, College Station, TX (United States)

2016-11-15

It is shown that with proper optimization, backscattered electrons in a scanning electron microscope can produce images of cavity distribution in austenitic steels over a large specimen surface for a depth of ∼500–700 nm, eliminating the need for electropolishing or multiple specimen production. This technique is especially useful for quantifying cavity structures when the specimen is known or suspected to contain very heterogeneous distributions of cavities. Examples are shown for cold-worked EK-164, a very heterogeneously-swelling Russian fast reactor fuel cladding steel and also for AISI 304, a homogeneously-swelling Western steel used for major structural components of light water cooled reactors. This non-destructive overview method of quantifying cavity distribution can be used to direct the location and number of required focused ion beam prepared transmission electron microscopy specimens for examination of either neutron or ion-irradiated specimens. This technique can also be applied in stereo mode to quantify the depth dependence of cavity distributions.

Backscattered electron SEM imaging of resin sections from plant specimens: observation of histological to subcellular structure and CLEM.

Science.gov (United States)

Rizzo, N W; Duncan, K E; Bourett, T M; Howard, R J

2016-08-01

We have refined methods for biological specimen preparation and low-voltage backscattered electron imaging in the scanning electron microscope that allow for observation at continuous magnifications of ca. 130-70 000 X, and documentation of tissue and subcellular ultrastructure detail. The technique, based upon early work by Ogura & Hasegawa (1980), affords use of significantly larger sections from fixed and resin-embedded specimens than is possible with transmission electron microscopy while providing similar data. After microtomy, the sections, typically ca. 750 nm thick, were dried onto the surface of glass or silicon wafer and stained with heavy metals-the use of grids avoided. The glass/wafer support was then mounted onto standard scanning electron microscopy sample stubs, carbon-coated and imaged directly at an accelerating voltage of 5 kV, using either a yttrium aluminum garnet or ExB backscattered electron detector. Alternatively, the sections could be viewed first by light microscopy, for example to document signal from a fluorescent protein, and then by scanning electron microscopy to provide correlative light/electron microscope (CLEM) data. These methods provide unobstructed access to ultrastructure in the spatial context of a section ca. 7 × 10 mm in size, significantly larger than the typical 0.2 × 0.3 mm section used for conventional transmission electron microscopy imaging. Application of this approach was especially useful when the biology of interest was rare or difficult to find, e.g. a particular cell type, developmental stage, large organ, the interface between cells of interacting organisms, when contextual information within a large tissue was obligatory, or combinations of these factors. In addition, the methods were easily adapted for immunolocalizations. © 2015 The Author. Journal of Microscopy published by John Wiley & Sons, Ltd on behalf of the Royal Microscopical Society.

Assessing strain mapping by electron backscatter diffraction and confocal Raman microscopy using wedge-indented Si

Energy Technology Data Exchange (ETDEWEB)

Friedman, Lawrence H.; Vaudin, Mark D.; Stranick, Stephan J.; Stan, Gheorghe; Gerbig, Yvonne B.; Osborn, William; Cook, Robert F., E-mail: robert.cook@nist.gov

2016-04-15

The accuracy of electron backscatter diffraction (EBSD) and confocal Raman microscopy (CRM) for small-scale strain mapping are assessed using the multi-axial strain field surrounding a wedge indentation in Si as a test vehicle. The strain field is modeled using finite element analysis (FEA) that is adapted to the near-indentation surface profile measured by atomic force microscopy (AFM). The assessment consists of (1) direct experimental comparisons of strain and deformation and (2) comparisons in which the modeled strain field is used as an intermediate step. Direct experimental methods (1) consist of comparisons of surface elevation and gradient measured by AFM and EBSD and of Raman shifts measured and predicted by CRM and EBSD, respectively. Comparisons that utilize the combined FEA–AFM model (2) consist of predictions of distortion, strain, and rotation for comparison with EBSD measurements and predictions of Raman shift for comparison with CRM measurements. For both EBSD and CRM, convolution of measurements in depth-varying strain fields is considered. The interconnected comparisons suggest that EBSD was able to provide an accurate assessment of the wedge indentation deformation field to within the precision of the measurements, approximately 2×10{sup −4} in strain. CRM was similarly precise, but was limited in accuracy to several times this value. - Highlights: • We map strain by electron backscatter diffraction and confocal Raman microscopy. • The test vehicle is the multi-axial strain field of wedge-indented silicon. • Strain accuracy is assessed by direct experimental intercomparison. • Accuracy is also assessed by atomic force microscopy and finite element analyses. • Electron diffraction measurements are accurate; Raman measurements need refinement.

Assessing strain mapping by electron backscatter diffraction and confocal Raman microscopy using wedge-indented Si

International Nuclear Information System (INIS)

Friedman, Lawrence H.; Vaudin, Mark D.; Stranick, Stephan J.; Stan, Gheorghe; Gerbig, Yvonne B.; Osborn, William; Cook, Robert F.

2016-01-01

The accuracy of electron backscatter diffraction (EBSD) and confocal Raman microscopy (CRM) for small-scale strain mapping are assessed using the multi-axial strain field surrounding a wedge indentation in Si as a test vehicle. The strain field is modeled using finite element analysis (FEA) that is adapted to the near-indentation surface profile measured by atomic force microscopy (AFM). The assessment consists of (1) direct experimental comparisons of strain and deformation and (2) comparisons in which the modeled strain field is used as an intermediate step. Direct experimental methods (1) consist of comparisons of surface elevation and gradient measured by AFM and EBSD and of Raman shifts measured and predicted by CRM and EBSD, respectively. Comparisons that utilize the combined FEA–AFM model (2) consist of predictions of distortion, strain, and rotation for comparison with EBSD measurements and predictions of Raman shift for comparison with CRM measurements. For both EBSD and CRM, convolution of measurements in depth-varying strain fields is considered. The interconnected comparisons suggest that EBSD was able to provide an accurate assessment of the wedge indentation deformation field to within the precision of the measurements, approximately 2×10"−"4 in strain. CRM was similarly precise, but was limited in accuracy to several times this value. - Highlights: • We map strain by electron backscatter diffraction and confocal Raman microscopy. • The test vehicle is the multi-axial strain field of wedge-indented silicon. • Strain accuracy is assessed by direct experimental intercomparison. • Accuracy is also assessed by atomic force microscopy and finite element analyses. • Electron diffraction measurements are accurate; Raman measurements need refinement.

Ion backscattering techniques applied in materials science research

International Nuclear Information System (INIS)

Sood, D.K.

1978-01-01

The applications of Ion Backscattering Technique (IBT) to material analysis have expanded rapidly during the last decade. It is now regarded as an analysis tool indispensable for a versatile materials research program. The technique consists of simply shooting a beam of monoenergetic ions (usually 4 He + ions at about 2 MeV) onto a target, and measuring their energy distribution after backscattering at a fixed angle. Simple Rutherford scattering analysis of the backscattered ion spectrum yields information on the mass, the absolute amount and the depth profile of elements present upto a few microns of the target surface. The technique is nondestructive, quick, quantitative and the only known method of analysis which gives quantitative results without recourse to calibration standards. Its major limitations are the inability to separate elements of similar mass and a complete absence of chemical-binding information. A typical experimental set up and spectrum analysis have been described. Examples, some of them based on the work at the Bhabha Atomic Research Centre, Bombay, have been given to illustrate the applications of this technique to semiconductor technology, thin film materials science and nuclear energy materials. Limitations of IBT have been illustrated and a few remedies to partly overcome these limitations are presented. (auth.)

Damage measurement of structural material by electron backscatter diffraction. Quantification of measurement quality toward standardization of measurement procedure

International Nuclear Information System (INIS)

Kamaya, Masayuki

2011-01-01

Several attempts have been made to assess the damage induced in materials by crystal orientation distributions identified using electron backscatter diffraction (EBSD). In particular, the local misorientation, which is the misorientation between neighboring measurement points, was shown to correlate well with the degree of material damage such as plastic strain, fatigue and creep. However, the damage assessments conducted using the local misorientations were qualitative rather than quantitative. The local misorientation can be correlated theoretically with physical parameters such as dislocation density. However, the error in crystal orientation measurements makes quantitative evaluation of the local misorientation difficult. Furthermore, the local misorientation depends on distance between the measurement points (step size). For a quantitative assessment of the local misorientation, the error in the crystal orientation measurements must be reduced or the degree of error must be shown quantitatively. In this study, first, the influence of the quality of measurements (accuracy of measurements) and step size on the local misorientation was investigated using stainless steel specimens damaged by tensile deformation or fatigue. By performing the crystal orientation measurements with different conditions, it was shown that the quality of measurement could be represented by the error index, which was previously proposed by the author. Secondly, a filtering process was applied in order to improve the accuracy of crystal orientation measurements and its effect was investigated using the error index. It was revealed that the local misorientations obtained under different measurement conditions could be compared quantitatively only when the error index and the step size were almost or exactly the same. It was also shown that the filtering process could successfully reduce the measurement error and step size dependency of the local misorientations. By applying the filtering

Electron backscatter diffraction applied to lithium sheets prepared by broad ion beam milling.

Science.gov (United States)

Brodusch, Nicolas; Zaghib, Karim; Gauvin, Raynald

2015-01-01

Due to its very low hardness and atomic number, pure lithium cannot be prepared by conventional methods prior to scanning electron microscopy analysis. Here, we report on the characterization of pure lithium metallic sheets used as base electrodes in the lithium-ion battery technology using electron backscatter diffraction (EBSD) and X-ray microanalysis using energy dispersive spectroscopy (EDS) after the sheet surface was polished by broad argon ion milling (IM). No grinding and polishing were necessary to achieve the sufficiently damage free necessary for surface analysis. Based on EDS results the impurities could be characterized and EBSD revealed the microsctructure and microtexture of this material with accuracy. The beam damage and oxidation/hydration resulting from the intensive use of IM and the transfer of the sample into the microscope chamber was estimated to be effect on the surface temperature. However, a cryo-stage should be used if available during milling to guaranty a heating artefact free surface after the milling process. © 2014 Wiley Periodicals, Inc.

Bragg's Law diffraction simulations for electron backscatter diffraction analysis

International Nuclear Information System (INIS)

Kacher, Josh; Landon, Colin; Adams, Brent L.; Fullwood, David

2009-01-01

In 2006, Angus Wilkinson introduced a cross-correlation-based electron backscatter diffraction (EBSD) texture analysis system capable of measuring lattice rotations and elastic strains to high resolution. A variation of the cross-correlation method is introduced using Bragg's Law-based simulated EBSD patterns as strain free reference patterns that facilitates the use of the cross-correlation method with polycrystalline materials. The lattice state is found by comparing simulated patterns to collected patterns at a number of regions on the pattern using the cross-correlation function and calculating the deformation from the measured shifts of each region. A new pattern can be simulated at the deformed state, and the process can be iterated a number of times to converge on the absolute lattice state. By analyzing an iteratively rotated single crystal silicon sample and recovering the rotation, this method is shown to have an angular resolution of ∼0.04 o and an elastic strain resolution of ∼7e-4. As an example of applications, elastic strain and curvature measurements are used to estimate the dislocation density in a single grain of a compressed polycrystalline Mg-based AZ91 alloy.

Strong Localization in Disordered Media: Analysis of the Backscattering Cone

KAUST Repository

Delgado, Edgar

2012-06-01

A very interesting effect in light propagation through a disordered system is Anderson localization of light, this phenomenon emerges as the result of multiple scattering of waves by electric inhomogeneities like spatial variations of index of refraction; as the amount of scattering is increased, light propagation is converted from quasi-diffusive to exponentially localized, with photons confined in a limited spatial region characterized by a fundamental quantity known as localization length. Light localization is strongly related to another interference phenomenon emerged from the multiple scattering effect: the coherent backscattering effect. In multiple scattering of waves, in fact, coherence is preserved in the backscattering direction and produces a reinforcement of the field flux originating an observable peak in the backscattered intensity, known as backscattering cone. The study of this peak provide quantitative information about the transport properties of light in the material. In this thesis we report a complete FDTD ab-initio study of light localization and coherent backscattering. In particular, we consider a supercontinuum pulse impinging on a sample composed of randomly positioned scatterers. We study coherent backscattering by averaging over several realizations of the sample properties. We study then the coherent backscattering cone properties as the relative permittivity of the sample is changed, relating the latter with the light localization inside the sample. We demonstrate important relationships between the width of the backscattering cone and the localization length, which shows a linear proportionality in the strong localization regime.

Accurate measurement of the orientation relationship of lath martensite and bainite by electron backscatter diffraction analysis

International Nuclear Information System (INIS)

Miyamoto, G.; Takayama, N.; Furuhara, T.

2009-01-01

A new method to determine the orientation relationship between martensite and bainite with the parent austenite is developed based on electron backscatter diffraction analysis. This method can determine the orientation relationship accurately without the presence of retained austenite, and is applicable to lath martensite and bainite in low-alloyed carbon steels. The angles between close-packed directions are about 3 o for lath martensite regardless of the carbon content, while the angles between close-packed planes become smaller with increasing carbon content.

On the optimum resolution of transmission-electron backscattered diffraction (t-EBSD)

Energy Technology Data Exchange (ETDEWEB)

Bremen, R. van; Ribas Gomes, D.; Jeer, L.T.H. de; Ocelík, V., E-mail: v.ocelik@rug.nl; De Hosson, J.Th.M.

2016-01-15

The work presented aims at determining the optimum physical resolution of the transmission-electron backscattered diffraction (t-EBSD) technique. The resolution depends critically on intrinsic factors such as the density, atomic number and thickness of the specimen but also on the extrinsic experimental set-up of the electron beam voltage, specimen tilt and detector position. In the present study, the so-called physical resolution of a typical t-EBSD set-up was determined with the use of Monte Carlo simulations and confronted to experimental findings. In the case of a thin Au film of 20 nm, the best resolution obtained was 9 nm whereas for a 100 nm Au film the best resolution was 66 nm. The precise dependence of resolution on thickness was found to vary differently depending on the specific elements involved. This means that the resolution of each specimen should be determined individually. Experimentally the median probe size of the t-EBSD for a 140 nm thick AuAg specimen was measured to be 87 nm. The first and third quartiles of the probe size measurements were found to be 60 nm and 118 nm. Simulation of this specimen resulted in a resolution of 94 nm which fits between these quartiles. - Highlights: • Intrinsic and extrinsic factors affecting resolution of t-EBSD are determined and characterized. • Distinction between resolutions of transmitted and detected electrons is determined. • The simulated results are confirmed experimentally on 140 nm thick AuAg foil.

Analysis of soft magnetic materials by electron backscatter diffraction as a powerful tool

Science.gov (United States)

Schuller, David; Hohs, Dominic; Loeffler, Ralf; Bernthaler, Timo; Goll, Dagmar; Schneider, Gerhard

2018-04-01

The current work demonstrates that electron backscatter diffraction (EBSD) is a powerful and versatile characterization technique for investigating soft magnetic materials. The properties of soft magnets, e.g., magnetic losses strongly depend on the materials chemical composition and microstructure, including grain size and shape, texture, degree of plastic deformation and elastic strain. In electrical sheet stacks for e-motor applications, the quality of the machined edges/surfaces of each individual sheet is of special interest. Using EBSD, the influence of the punching process on the microstructure at the cutting edge is quantitatively assessed by evaluating the crystallographic misorientation distribution of the deformed grains. Using an industrial punching process, the maximum affected deformation depth is determined to be 200 - 300 μm. In the case of laser cutting, the affected deformation depth is determined to be approximately zero. Reliability and detection limits of the developed EBSD approach are evaluated on non-affected sample regions and model samples containing different indentation test bodies. A second application case is the investigation of the recrystallization process during the annealing step of soft magnetic composites (SMC) toroids produced by powder metallurgy as a function of compaction pressure, annealing parameters and powder particle size. With increasing pressure and temperature, the recrystallized area fraction (e.g., grains with crystallographic misorientations particle boundaries or areas with existing plastic deformation. The progress of recrystallization is visualized as a function of time and of different particle to grain size distributions. Here, large particles with coarse internal grain structures show a favorable recrystallization behavior which results in large bulk permeability of up to 600 - 700 and lower amount of residual misorientations (>3°).

Understanding deformation with high angular resolution electron backscatter diffraction (HR-EBSD)

Science.gov (United States)

Britton, T. B.; Hickey, J. L. R.

2018-01-01

High angular resolution electron backscatter diffraction (HR-EBSD) affords an increase in angular resolution, as compared to ‘conventional’ Hough transform based EBSD, of two orders of magnitude, enabling measurements of relative misorientations of 1 x 10-4 rads (~ 0.006°) and changes in (deviatoric) lattice strain with a precision of 1 x 10-4. This is achieved through direct comparison of two or more diffraction patterns using sophisticated cross-correlation based image analysis routines. Image shifts between zone axes in the two-correlated diffraction pattern are measured with sub-pixel precision and this realises the ability to measure changes in interplanar angles and lattice orientation with a high degree of sensitivity. These shifts are linked to strains and lattice rotations through simple geometry. In this manuscript, we outline the basis of the technique and two case studies that highlight its potential to tackle real materials science challenges, such as deformation patterning in polycrystalline alloys.

Card controlled beta backscatter thickness measuring instrument

International Nuclear Information System (INIS)

Schlesinger, J.

1978-01-01

An improved beta backscatter instrument for the nondestructive measurement of the thickness of thin coatings on a substrate is described. Included therein is the utilization of a bank of memory stored data representative of isotope, substrate, coating material and thickness range characteristics in association with a control card having predetermined indicia thereon selectively representative of a particular isotope, substrate material, coating material and thickness range for conditioning electronic circuit means by memory stored data selected in accord with the predetermined indicia on a control card for converting backscattered beta particle counts into indicia of coating thickness

Computation of Nonlinear Backscattering Using a High-Order Numerical Method

Science.gov (United States)

Fibich, G.; Ilan, B.; Tsynkov, S.

2001-01-01

The nonlinear Schrodinger equation (NLS) is the standard model for propagation of intense laser beams in Kerr media. The NLS is derived from the nonlinear Helmholtz equation (NLH) by employing the paraxial approximation and neglecting the backscattered waves. In this study we use a fourth-order finite-difference method supplemented by special two-way artificial boundary conditions (ABCs) to solve the NLH as a boundary value problem. Our numerical methodology allows for a direct comparison of the NLH and NLS models and for an accurate quantitative assessment of the backscattered signal.

Three-dimensional imaging of hidden objects using positron emission backscatter

International Nuclear Information System (INIS)

Lee, Dongwon; Cowee, Misa; Fenimore, Ed; Galassi, Mark; Looker, Quinn; Mcneil, Wendy V.; Stonehill, Laura; Wallace, Mark

2009-01-01

Positron emission backscatter imaging is a technique for interrogation and three-dimensional (3-D) reconstruction of hidden objects when we only have access to the objects from one side. Using time-of-flight differences in detected direct and backscattered positron-emitted photons, we construct 3-D images of target objects. Recently at Los Alamos National Laboratory, a fully three-dimensional imaging system has been built and the experimental results are discussed in this paper. Quantitative analysis of images reconstructed in both two- and three-dimensions are also presented.

Orientation effects on indexing of electron backscatter diffraction patterns

International Nuclear Information System (INIS)

Nowell, Matthew M.; Wright, Stuart I.

2005-01-01

Automated Electron Backscatter Diffraction (EBSD) has become a well-accepted technique for characterizing the crystallographic orientation aspects of polycrystalline microstructures. At the advent of this technique, it was observed that patterns obtained from grains in certain crystallographic orientations were more difficult for the automated indexing algorithms to accurately identify than patterns from other orientations. The origin of this problem is often similarities between the EBSD pattern of the correct orientation and patterns from other orientations or phases. While practical solutions have been found and implemented, the identification of these problem orientations generally occurs only after running an automated scan, as problem orientations are often readily apparent in the resulting orientation maps. However, such an approach only finds those problem orientations that are present in the scan area. It would be advantageous to identify all regions of orientation space that may present problems for automated indexing prior to initiating an automated scan, and to minimize this space through the optimization of acquisition and indexing parameters. This work presents new methods for identifying regions in orientation space where the reliability of the automated indexing is suspect prior to performing a scan. This methodology is used to characterize the impact of various parameters on the indexing algorithm

A preliminary electron backscattered diffraction study of sintered NdFeB-type magnets.

Science.gov (United States)

Lillywhite, S J; Williams, A J; Davies, B E; Harris, I R

2002-03-01

This paper reports, for the first time, the use of electron backscattered diffraction (EBSD) to study orientation in sintered NdFeB type magnets. The magnetic properties of NdFeB magnets are greatly improved if a strong crystallographic texture is firstly achieved, namely, the direction of the c-axis is along the direction of magnetization. A systematic survey of sample preparation techniques showed that samples that were mechanically polished and then etched gave the most reliable EBSD data. Analyses were made using both fully automated EBSD scans and by EBSD measurements taken after manual movement of the beam. The EBSD results are presented as secondary electron SEM micrographs, orientation images and 001 pole figures. For the selection of grains investigated, the deviation of the c-axis was shown to be between 10 degrees and 30 degrees from the ideal [001]//magnetization direction. It is demonstrated that EBSD is a valuable tool for characterizing the microstructure and texture relationships and for assessing the performance of the processing routes of NdFeB magnets.

Simulation of multistatic and backscattering cross sections for airborne radar

Science.gov (United States)

Biggs, Albert W.

1986-07-01

In order to determine susceptibilities of airborne radar to electronic countermeasures and electronic counter-countermeasures simulations of multistatic and backscattering cross sections were developed as digital modules in the form of algorithms. Cross section algorithms are described for prolate (cigar shape) and oblate (disk shape) spheroids. Backscattering cross section algorithms are also described for different categories of terrain. Backscattering cross section computer programs were written for terrain categorized as vegetation, sea ice, glacial ice, geological (rocks, sand, hills, etc.), oceans, man-made structures, and water bodies. PROGRAM SIGTERRA is a file for backscattering cross section modules of terrain (TERRA) such as vegetation (AGCROP), oceans (OCEAN), Arctic sea ice (SEAICE), glacial snow (GLASNO), geological structures (GEOL), man-made structures (MAMMAD), or water bodies (WATER). AGCROP describes agricultural crops, trees or forests, prairies or grassland, and shrubs or bush cover. OCEAN has the SLAR or SAR looking downwind, upwind, and crosswind at the ocean surface. SEAICE looks at winter ice and old or polar ice. GLASNO is divided into a glacial ice and snow or snowfields. MANMAD includes buildings, houses, roads, railroad tracks, airfields and hangars, telephone and power lines, barges, trucks, trains, and automobiles. WATER has lakes, rivers, canals, and swamps. PROGRAM SIGAIR is a similar file for airborne targets such as prolate and oblate spheroids.

Backscatter, anisotropy, and polarization of solar hard X-rays

International Nuclear Information System (INIS)

Bai, T.; Ramaty, R.

1978-01-01

Hard X-rays incident upon the photosphere with energies > or approx. =15 keV have high probabilities of backscatter due to Compton collisions with electrons. This effect has a strong influence on the spectrum, intensity, and polarization of solar hard X-rays - especially for anisotropic models in which the primary X-rays are emitted predominantly toward the photosphere. We have carried out a detailed study of X-ray backscatter, and we have investigated the interrelated problems of anisotropy, polarization, center-to-limb variation of the X-ray spectrum, and Compton backscatter in a coherent fashion. The results of this study are compared with observational data. Because of the large contribution from backscatter, for an anisotropic primary X-ray source which is due to bremsstrahlung of accelerated electrons moving predominantly down toward the photosphere, the observed X-ray flux around 30 keV does not depend significantly on the position of flare on the Sun. For such an anisotropic source, the X-ray spectrum observed in the 15-50 keV range becomes steeper with the increasing heliocentric angle of the flare. These results are compatible with the data. The degree of polarization of the sum of the primary and reflected X-rays with energies between about 15 and 30 keV can be very large for anisotropic primary X-ray sources, but it is less than about 4% for isotropic sources. We also discuss the characteristics of the brightness distribution of the X-ray albedo patch created by the Compton backscatter. The height and anisotropy of the primary hard X-ray source might be inferred from the study of the albedo patch

Reconstruction of Laser-Induced Surface Topography from Electron Backscatter Diffraction Patterns.

Science.gov (United States)

Callahan, Patrick G; Echlin, McLean P; Pollock, Tresa M; De Graef, Marc

2017-08-01

We demonstrate that the surface topography of a sample can be reconstructed from electron backscatter diffraction (EBSD) patterns collected with a commercial EBSD system. This technique combines the location of the maximum background intensity with a correction from Monte Carlo simulations to determine the local surface normals at each point in an EBSD scan. A surface height map is then reconstructed from the local surface normals. In this study, a Ni sample was machined with a femtosecond laser, which causes the formation of a laser-induced periodic surface structure (LIPSS). The topography of the LIPSS was analyzed using atomic force microscopy (AFM) and reconstructions from EBSD patterns collected at 5 and 20 kV. The LIPSS consisted of a combination of low frequency waviness due to curtaining and high frequency ridges. The morphology of the reconstructed low frequency waviness and high frequency ridges matched the AFM data. The reconstruction technique does not require any modification to existing EBSD systems and so can be particularly useful for measuring topography and its evolution during in situ experiments.

High resolution electron backscatter diffraction (EBSD) data from calcite biominerals in recent gastropod shells.

Science.gov (United States)

Pérez-Huerta, Alberto; Dauphin, Yannicke; Cuif, Jean Pierre; Cusack, Maggie

2011-04-01

Electron backscatter diffraction (EBSD) is a microscopy technique that reveals in situ crystallographic information. Currently, it is widely used for the characterization of geological materials and in studies of biomineralization. Here, we analyze high resolution EBSD data from biogenic calcite in two mollusk taxa, Concholepas and Haliotis, previously used in the understanding of complex biomineralization and paleoenvironmental studies. Results indicate that Concholepas has less ordered prisms than in Haliotis, and that in Concholepas the level of order is not homogenous in different areas of the shell. Overall, the usefulness of data integration obtained from diffraction intensity and crystallographic orientation maps, and corresponding pole figures, is discussed as well as its application to similar studies. © 2010 Elsevier Ltd. All rights reserved.

A study of intergranular corrosion of austenitic stainless steel by electrochemical potentiodynamic reactivation, electron back-scattering diffraction and cellular automaton

Energy Technology Data Exchange (ETDEWEB)

Yu Xiaofei [Department of Chemistry, Shandong University, Jinan 250100 (China); Chen Shenhao [Department of Chemistry, Shandong University, Jinan 250100 (China); State Key Laboratory for Corrosion and Protection, Shenyang 110016 (China)], E-mail: shchen@sdu.edu.cn; Liu Ying; Ren Fengfeng [Department of Chemistry, Shandong University, Jinan 250100 (China)

2010-06-15

The impact of solution and sensitization treatments on the intergranular corrosion (IGC) of austenitic stainless steel (316) was studied by electrochemical potentiodynamic reactivation (EPR) test, and the results showed the degree of sensitization (DOS) decreased as solution treatment temperature and time went up, but it increased as sensitization temperature prolonged. Factors that affected IGC were investigated by field emission scanning electron microscope (FE-SEM) and electron back-scattering diffraction (EBSD). Furthermore, the precipitation evolution of Cr-rich carbides and the distribution of chromium concentration were simulated by cellular automaton (CA), clearly showing the effects of solution and sensitization treatments on IGC.

The potential of materials analysis by electron rutherford backscattering as illustrated by a case study of mouse bones and related compounds.

Science.gov (United States)

Vos, Maarten; Tökési, Károly; Benkö, Ilona

2013-06-01

Electron Rutherford backscattering (ERBS) is a new technique that could be developed into a tool for materials analysis. Here we try to establish a methodology for the use of ERBS for materials analysis of more complex samples using bone minerals as a test case. For this purpose, we also studied several reference samples containing Ca: calcium carbonate (CaCO(3)) and hydroxyapatite and mouse bone powder. A very good understanding of the spectra of CaCO(3) and hydroxyapatite was obtained. Quantitative interpretation of the bone spectrum is more challenging. A good fit of these spectra is only obtained with the same peak widths as used for the hydroxyapatite sample, if one allows for the presence of impurity atoms with a mass close to that of Na and Mg. Our conclusion is that a meaningful interpretation of spectra of more complex samples in terms of composition is indeed possible, but only if widths of the peaks contributing to the spectra are known. Knowledge of the peak widths can either be developed by the study of reference samples (as was done here) or potentially be derived from theory.

Giant Andreev Backscattering through a Quantum Point Contact Coupled via a Disordered Two-Dimensional Electron Gas to Superconductors

International Nuclear Information System (INIS)

den Hartog, S.G.; van Wees, B.J.; Klapwijk, T.M.; Nazarov, Y.V.; Borghs, G.

1997-01-01

We have investigated the superconducting-phase-modulated reduction in the resistance of a ballistic quantum point contact (QPC) connected via a disordered two-dimensional electron gas (2DEG) to superconductors. We show that this reduction is caused by coherent Andreev backscattering of holes through the QPC, which increases monotonically by reducing the bias voltage to zero. In contrast, the magnitude of the phase-dependent resistance of the disordered 2DEG displays a nonmonotonic reentrant behavior versus bias voltage. copyright 1997 The American Physical Society

Assessment of surface hardening effects from shot peening on a Ni-based alloy using electron backscatter diffraction techniques

International Nuclear Information System (INIS)

Child, D.J.; West, G.D.; Thomson, R.C.

2011-01-01

An electron backscatter diffraction (EBSD)-based tool is described to assess the depth of strain-hardening effects of shot-peening treatments applied to the Ni-based superalloy, Udimet (copy right) alloy 720Li. The method consists of a statistical analysis of a number of data points from each grain scanned based on the grain orientation spread and their relative position from the shot-peened edge. The output is a quantitative measure of the depth of strain-hardening effects. The tool is used at various shot-peening intensities to demonstrate the ability to distinguish between these changes, using a range of intensities from 4 to 10 Almen. An increase in shot-peening intensity is observed to increase the depth of strain-hardening effects in the alloy. A comparison with residual stress measurements using X-ray diffraction for the same material shows that the strain-hardened depth determined by EBSD extends to approximately half the distance of the residual stress present due to shot peening. A comparison is also made with predicted profiles from the Peenstress SM model and subsequent microhardness testing. A positive correlation is observed between strained hardened depth and surface roughness of the peened samples. In each case, the increases in surface roughness and strain-hardened depth diminish toward the upper end of the shot-peening intensity range studied for this alloy.

Determination of dislocation density by electron backscatter diffraction and X-ray line profile analysis in ferrous lath martensite

International Nuclear Information System (INIS)

Berecz, Tibor; Jenei, Péter; Csóré, András; Lábár, János; Gubicza, Jenő

2016-01-01

The microstructure and the dislocation density in as-quenched ferrous lath martensite were studied by different methods. The blocks, packets and variants formed due to martensitic transformation were identified and their sizes were determined by electron backscatter diffraction (EBSD). Concomitant transmission electron microscopy (TEM) investigation revealed that the laths contain subgrains with the size between 50 and 100 nm. A novel evaluation procedure of EBSD images was elaborated for the determination of the density and the space distribution of geometrically necessary dislocations from the misorientation distribution. The total dislocation density obtained by X-ray diffraction line profile analysis was in good agreement with the value determined by EBSD, indicating that the majority of dislocations formed due to martensitic transformation during quenching are geometrically necessary dislocations.

In situ electron backscatter diffraction (EBSD) during the compression of micropillars

International Nuclear Information System (INIS)

Niederberger, C.; Mook, W.M.; Maeder, X.; Michler, J.

2010-01-01

For the first time, in situ electron backscatter diffraction (EBSD) measurements during compression experiments by a modified nanoindenter on micron-sized single crystal pillars are demonstrated here. The experimental setup and the requirements concerning the compression sample are described in detail. EBSD mappings have been acquired before loading, under load and after unloading for consecutive compression cycles on a focused ion beam (FIB) milled GaAs micropillar. In situ EBSD allows for the determination of crystallographic orientation with sub-100 nm spatial resolution. Thereby, it provides highly localized information pertaining to the deformation phenomena such as elastic bending of the micropillar or the formation of deformation twins and plastic orientation gradients due to geometrically necessary dislocations. The most striking features revealed by in situ EBSD are the non-negligible amount of reversible (elastic) bending of the micropillar and the fact that deformation twinning and dislocation glide initiate where the bending is strongest. Due to this high spatial and orientation resolution, in situ EBSD measurements during micromechanical testing are demonstrated to be a promising technique for the investigation of deformation phenomena at the nano- to micro-scale.

Bragg's Law diffraction simulations for electron backscatter diffraction analysis

Energy Technology Data Exchange (ETDEWEB)

Kacher, Josh, E-mail: jkacherbyu@gmail.com [Department of Mechanical Engineering, Brigham Young University, 455B Crabtree Technology Building, Provo, UT 84602 (United States); Landon, Colin; Adams, Brent L.; Fullwood, David [Department of Mechanical Engineering, Brigham Young University, 455B Crabtree Technology Building, Provo, UT 84602 (United States)

2009-08-15

In 2006, Angus Wilkinson introduced a cross-correlation-based electron backscatter diffraction (EBSD) texture analysis system capable of measuring lattice rotations and elastic strains to high resolution. A variation of the cross-correlation method is introduced using Bragg's Law-based simulated EBSD patterns as strain free reference patterns that facilitates the use of the cross-correlation method with polycrystalline materials. The lattice state is found by comparing simulated patterns to collected patterns at a number of regions on the pattern using the cross-correlation function and calculating the deformation from the measured shifts of each region. A new pattern can be simulated at the deformed state, and the process can be iterated a number of times to converge on the absolute lattice state. By analyzing an iteratively rotated single crystal silicon sample and recovering the rotation, this method is shown to have an angular resolution of {approx}0.04{sup o} and an elastic strain resolution of {approx}7e-4. As an example of applications, elastic strain and curvature measurements are used to estimate the dislocation density in a single grain of a compressed polycrystalline Mg-based AZ91 alloy.

Monte-Carlo study of the influence of backscattered electrons on the transmission of a mini-orange β spectrometer

Science.gov (United States)

Detistov, Pavel; Balabanski, Dimiter L.

2015-04-01

This work work is a part of the performance investigation of the recently constructed Mini-Orange beta spectrometer. The spectrometer has eight different configurations using three different magnet shapes and combination of three, four, and six magnet pieces allowing detection of electrons in wide kinetic energy range. The performance of the device is studied using the GEANT4 simulation tool. Evaluation of the device's basic parameters has been made, paying special attention to the backscattering, for which a study of the dependence of this process on the energy and the angle is made.

ILC beam energy measurement by means of laser Compton backscattering

Energy Technology Data Exchange (ETDEWEB)

Muchnoi, N. [Budker Inst. for Nuclear Physics, Novosibirsk (Russian Federation); Schreiber, H.J.; Viti, M. [Deutsches Elektronen-Synchrotron (DESY), Zeuthen (Germany)

2008-10-15

A novel, non-invasive method of measuring the beam energy at the International Linear Collider is proposed. Laser light collides head-on with beam particles and either the energy of the Compton scattered electrons near the kinematic end-point is measured or the positions of the Compton backscattered {gamma}-rays, the edge electrons and the unscattered beam particles are recorded. A compact layout for the Compton spectrometer is suggested. It consists of a bending magnet and position sensitive detectors operating in a large radiation environment. Several options for high spatial resolution detectors are discussed. Simulation studies support the use of an infrared or green laser and quartz fiber detectors to monitor the backscattered photons and edge electrons. Employing a cavity monitor, the beam particle position downstream of the magnet can be recorded with submicrometer precision. Such a scheme provides a feasible and promising method to access the incident beam energy with precisions of 10{sup -4} or better on a bunch-to-bunch basis while the electron and positron beams are in collision. (orig.)

ILC beam energy measurement by means of laser Compton backscattering

International Nuclear Information System (INIS)

Muchnoi, N.; Schreiber, H.J.; Viti, M.

2008-10-01

A novel, non-invasive method of measuring the beam energy at the International Linear Collider is proposed. Laser light collides head-on with beam particles and either the energy of the Compton scattered electrons near the kinematic end-point is measured or the positions of the Compton backscattered γ-rays, the edge electrons and the unscattered beam particles are recorded. A compact layout for the Compton spectrometer is suggested. It consists of a bending magnet and position sensitive detectors operating in a large radiation environment. Several options for high spatial resolution detectors are discussed. Simulation studies support the use of an infrared or green laser and quartz fiber detectors to monitor the backscattered photons and edge electrons. Employing a cavity monitor, the beam particle position downstream of the magnet can be recorded with submicrometer precision. Such a scheme provides a feasible and promising method to access the incident beam energy with precisions of 10 -4 or better on a bunch-to-bunch basis while the electron and positron beams are in collision. (orig.)

Development of a model using narrow slit beam profiles to account for the backscatter response of an amorphous silicon electronic portal imaging device

International Nuclear Information System (INIS)

Maria Das, K.J.; Ostapiak, Orest

2008-01-01

An electronic portal imaging device (EPID), currently used for determining proper patient placement during irradiation in a radiotherapy treatment, can also be used for the purpose of pre- treatment IMRT QA. However, the Varian aS500 portal imager exhibits dosimetric artifacts caused by non-uniform backscatter from mechanical support structures located behind the imager

Electromagnetic backscattering from one-dimensional drifting fractal sea surface II: Electromagnetic backscattering model

International Nuclear Information System (INIS)

Xie Tao; Zhao Shang-Zhuo; Fang He; Yu Wen-Jin; He Yi-Jun; Perrie, William

2016-01-01

Sea surface current has a significant influence on electromagnetic (EM) backscattering signals and may constitute a dominant synthetic aperture radar (SAR) imaging mechanism. An effective EM backscattering model for a one-dimensional drifting fractal sea surface is presented in this paper. This model is used to simulate EM backscattering signals from the drifting sea surface. Numerical results show that ocean currents have a significant influence on EM backscattering signals from the sea surface. The normalized radar cross section (NRCS) discrepancies between the model for a coupled wave-current fractal sea surface and the model for an uncoupled fractal sea surface increase with the increase of incidence angle, as well as with increasing ocean currents. Ocean currents that are parallel to the direction of the wave can weaken the EM backscattering signal intensity, while the EM backscattering signal is intensified by ocean currents propagating oppositely to the wave direction. The model presented in this paper can be used to study the SAR imaging mechanism for a drifting sea surface. (paper)

A versatile atomic number correction for electron-probe microanalysis

International Nuclear Information System (INIS)

Love, G.; Cox, M.G.; Scott, V.D.

1978-01-01

A new atomic number correction is proposed for quantitative electron-probe microanalysis. Analytical expressions for the stopping power S and back-scatter R factors are derived which take into account atomic number of the target, incident electron energy and overvoltage; the latter expression is established using Monte Carlo calculations. The correct procedures for evaluating S and R for multi-element specimens are described. The new method, which overcomes some limitations inherent in earlier atomic number corrections, may readily be used where specimens are inclined to the electron beam. (author)

Backscatter and attenuation characterization of ventricular myocardium

Science.gov (United States)

Gibson, Allyson Ann

2009-12-01

This Dissertation presents quantitative ultrasonic measurements of the myocardium in fetal hearts and adult human hearts with the goal of studying the physics of sound waves incident upon anisotropic and inhomogeneous materials. Ultrasound has been used as a clinical tool to assess heart structure and function for several decades. The clinical usefulness of this noninvasive approach has grown with our understanding of the physical mechanisms underlying the interaction of ultrasonic waves with the myocardium. In this Dissertation, integrated backscatter and attenuation analyses were performed on midgestational fetal hearts to assess potential differences in the left and right ventricular myocardium. The hearts were interrogated using a 50 MHz transducer that enabled finer spatial resolution than could be achieved at more typical clinical frequencies. Ultrasonic data analyses demonstrated different patterns and relative levels of backscatter and attenuation from the myocardium of the left ventricle and the right ventricle. Ultrasonic data of adult human hearts were acquired with a clinical imaging system and quantified by their magnitude and time delay of cyclic variation of myocardial backscatter. The results were analyzing using Bayes Classification and ROC analysis to quantify potential advantages of using a combination of two features of cyclic variation of myocardial backscatter over using only one or the other feature to distinguish between groups of subjects. When the subjects were classified based on hemoglobin A1c, the homeostasis model assessment of insulin resistance, and the ratio of triglyceride to high-density lipoprotein-cholesterol, differences in the magnitude and normalized time delay of cyclic variation of myocardial backscatter were observed. The cyclic variation results also suggested a trend toward a larger area under the ROC curve when information from magnitude and time delay of cyclic variation is combined using Bayes classification than when

Application of Electron Backscattered Diffraction (EBSD) and Atomic Force Microscopy (AFM) to Determine Texture, Mesotexture, and Grain Boundary Energies in Ceramics

International Nuclear Information System (INIS)

Glass, S.J.; Rohrer, G.S.; Saylor, D.M.; Vedula, V.R.

1999-01-01

Crystallographic orientations in alumina (Al 2 0 3 ) and magnesium aluminate spinel (MgAl 2 0 4 ) were obtained using electron backscattered diffraction (EBSD) patterns. The texture and mesotexture (grain boundary mis-orientations) were random and no special boundaries were observed. The relative grain boundary energies were determined by thermal groove geometries using atomic force microscopy (AFM) to identify relationships between the grain boundary energies and mis-orientations

The Correlation Characteristics of Polarization Backscattering Matrix of Dense Chaff Clouds

Directory of Open Access Journals (Sweden)

B. Tang

2018-04-01

Full Text Available This paper studied the correlation characteristics of the polarization backscattering matrix of the dense chaff cloud with uniform orientation and location distributions in circular symmetry region. Based on the theoretical analysis and numerical experiments, the correlation coefficients of the four elements in the polarization backscattering matrix are obtained, and the results indicate that the cross to co-polar correlation coefficient is still zero; and that the sum of the co-polar cross-correlation coefficient and the two times of linear depolarization ratio equals one. The results are beneficial for better understanding of the backscattering characteristics of dense chaff clouds, and are useful in the application of jamming recognition in radar electronic warfare. Numerical experiments are performed by using the method of moments.

Analysis of a nuclear backscattering and reaction data by the method of convolution integrals

International Nuclear Information System (INIS)

Lewis, M.B.

1979-02-01

A quantitative description of nuclear backscattering and reaction processes is made. Various formulas pertinent to nuclear microanalysis are assembled in a manner useful for experimental application. Convolution integrals relating profiles of atoms in a metal substrate to the nuclear reaction spectra obtained in the laboratory are described and computed. Energy straggling and multiple scattering are explicitly included and shown to be important. Examples of the application of the method to simple backscattering, oxide films, and implanted gas are discussed. 7 figures, 1 table

A critical evaluation of quantitative and qualitative analysis by means of energy-dispersive X-ray measurement in a scanning electron microscope

International Nuclear Information System (INIS)

Blum, F.

1978-12-01

The bombardment of solids in the scanning electron microscope (SEM) by means of energetic electrons results in the generation and emission of various signals that carry information about the characteristics of the target. Those signals which are related to the present context, e.g. the secondary and backscattered electrons as well as the characteristic and continuous X-radiation, are discussed. The brief description of the SEM and the energy dispersive X-ray (EDX) spectrometer is followed by a discussion of various obstacles affecting the reliability of X-ray intensity measurements and data reduction procedures. The observed relative X-ray intensities from pure elements were determined as a function of the atomic number. These functional dependence curves, which were established under standard conditions, served as reliable reference data for the purpose of quantitative corrections. The performance limits of a typical SEM-EDX analytical system were assessed by analysing quantitatively various types of standard reference materials and inhomogeneous samples. A brief discussion of the X-ray source is given in order to estimate whether the recorded X-ray intensities are representative of the electron bombarded areas. This is of importance when microanalyses are performed on inclusions or near phase boundaries. The use of oxide glasses which are suitable to evaluate and interrelative SEM-EDX systems is discussed. The analysis of metal alloys, which developed exaggerated surface topography when sputtered in an ion microprobe mass analyser or glow discharge lamp, is presented as a typical example for the investigation of rough-surface samples [af

Dynamic coherent backscattering mirror

Energy Technology Data Exchange (ETDEWEB)

Zeylikovich, I.; Xu, M., E-mail: mxu@fairfield.edu [Physics Department, Fairfield University, Fairfield, CT 06824 (United States)

2016-02-15

The phase of multiply scattered light has recently attracted considerable interest. Coherent backscattering is a striking phenomenon of multiple scattered light in which the coherence of light survives multiple scattering in a random medium and is observable in the direction space as an enhancement of the intensity of backscattered light within a cone around the retroreflection direction. Reciprocity also leads to enhancement of backscattering light in the spatial space. The random medium behaves as a reciprocity mirror which robustly converts a diverging incident beam into a converging backscattering one focusing at a conjugate spot in space. Here we first analyze theoretically this coherent backscattering mirror (CBM) phenomenon and then demonstrate the capability of CBM compensating and correcting both static and dynamic phase distortions occurring along the optical path. CBM may offer novel approaches for high speed dynamic phase corrections in optical systems and find applications in sensing and navigation.

Analysis of seafloor backscatter strength dependence on the survey azimuth using multibeam echosounder data

Science.gov (United States)

Lurton, Xavier; Eleftherakis, Dimitrios; Augustin, Jean-Marie

2018-06-01

The sediment backscatter strength measured by multibeam echosounders is a key feature for seafloor mapping either qualitative (image mosaics) or quantitative (extraction of classifying features). An important phenomenon, often underestimated, is the dependence of the backscatter level on the azimuth angle imposed by the survey line directions: strong level differences at varying azimuth can be observed in case of organized roughness of the seabed, usually caused by tide currents over sandy sediments. This paper presents a number of experimental results obtained from shallow-water cruises using a 300-kHz multibeam echosounder and specially dedicated to the study of this azimuthal effect, with a specific configuration of the survey strategy involving a systematic coverage of reference areas following "compass rose" patterns. The results show for some areas a very strong dependence of the backscatter level, up to about 10-dB differences at intermediate oblique angles, although the presence of these ripples cannot be observed directly—neither from the bathymetry data nor from the sonar image, due to the insufficient resolution capability of the sonar. An elementary modeling of backscattering from rippled interfaces explains and comforts these observations. The consequences of this backscatter dependence upon survey azimuth on the current strategies of backscatter data acquisition and exploitation are discussed.

Developments in quantitative electron probe microanalysis

International Nuclear Information System (INIS)

Tixier, R.

1977-01-01

A study of the range of validity of the formulae for corrections used with massive specimen analysis is made. The method used is original; we have shown that it was possible to use a property of invariability of corrected intensity ratios for standards. This invariance property provides a test for the self consistency of the theory. The theoretical and experimental conditions required for quantitative electron probe microanalysis of thin transmission electron microscope specimens are examined. The correction formulae for atomic number, absorption and fluorescence effects are calculated. Several examples of experimental results are given, relative to the quantitative analysis of intermetallic precipitates and carbides in steels. Advances in applications of electron probe instruments related to the use of computer and the present development of fully automated instruments are reviewed. The necessary statistics for measurements of X ray count data are studied. Estimation procedure and tests are developed. These methods are used to perform a statistical check of electron probe microanalysis measurements and to reject rogue values. An estimator of the confidence interval of the apparent concentration is derived. Formulae were also obtained to optimize the counting time in order to obtain the best precision in a minimum amount of time [fr

Practical considerations in the calculation of orientation distribution functions from electron back-scattered diffraction patterns

International Nuclear Information System (INIS)

Bowen, A.W.

1994-01-01

Using model data sets for the Brass orientation, the importance of scatter width, angular accuracy and grain size and volume fraction on the sensitivity of the calculated Orientation Distribution Functions have been determined in order to highlight some of the practical considerations needed in the processing of experimental data from individual grain orientation measurements determined by the Electron Back-Scattered Diffraction technique. It is suggested that the most appropriate scatter width can be calculated from the maximum function height versus scatter width curve in order to accommodate variations in texture sharpness. The sensitivity of the ODF to careful sample preparation, mounting and pattern analysis, in order to keep errors in angular accuracy to 1 or less is demonstrated, as is the imperative need to correct for the size of grains, and their volume fractions. (orig.)

Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy

Directory of Open Access Journals (Sweden)

Pia C. Lansåker

2014-10-01

Full Text Available Gold nanoparticle films are of interest in several branches of science and technology, and accurate sample characterization is needed but technically demanding. We prepared such films by DC magnetron sputtering and recorded their mass thickness by Rutherford backscattering spectroscopy. The geometric thickness dg—from the substrate to the tops of the nanoparticles—was obtained by scanning electron microscopy (SEM combined with image analysis as well as by atomic force microscopy (AFM. The various techniques yielded an internally consistent characterization of the films. In particular, very similar results for dg were obtained by SEM with image analysis and by AFM.

Monte-Carlo study of the influence of backscattered electrons on the transmission of a mini-orange β spectrometer

International Nuclear Information System (INIS)

Detistov, Pavel; Balabanski, Dimiter L

2015-01-01

This work work is a part of the performance investigation of the recently constructed Mini-Orange beta spectrometer. The spectrometer has eight different configurations using three different magnet shapes and combination of three, four, and six magnet pieces allowing detection of electrons in wide kinetic energy range. The performance of the device is studied using the GEANT4 simulation tool. Evaluation of the device's basic parameters has been made, paying special attention to the backscattering, for which a study of the dependence of this process on the energy and the angle is made. (paper)

A framework to quantify uncertainties of seafloor backscatter from swath mapping echosounders

Science.gov (United States)

Malik, Mashkoor; Lurton, Xavier; Mayer, Larry

2018-06-01

Multibeam echosounders (MBES) have become a widely used acoustic remote sensing tool to map and study the seafloor, providing co-located bathymetry and seafloor backscatter. Although the uncertainty associated with MBES-derived bathymetric data has been studied extensively, the question of backscatter uncertainty has been addressed only minimally and hinders the quantitative use of MBES seafloor backscatter. This paper explores approaches to identifying uncertainty sources associated with MBES-derived backscatter measurements. The major sources of uncertainty are catalogued and the magnitudes of their relative contributions to the backscatter uncertainty budget are evaluated. These major uncertainty sources include seafloor insonified area (1-3 dB), absorption coefficient (up to > 6 dB), random fluctuations in echo level (5.5 dB for a Rayleigh distribution), and sonar calibration (device dependent). The magnitudes of these uncertainty sources vary based on how these effects are compensated for during data acquisition and processing. Various cases (no compensation, partial compensation and full compensation) for seafloor insonified area, transmission losses and random fluctuations were modeled to estimate their uncertainties in different scenarios. Uncertainty related to the seafloor insonified area can be reduced significantly by accounting for seafloor slope during backscatter processing while transmission losses can be constrained by collecting full water column absorption coefficient profiles (temperature and salinity profiles). To reduce random fluctuations to below 1 dB, at least 20 samples are recommended to be used while computing mean values. The estimation of uncertainty in backscatter measurements is constrained by the fact that not all instrumental components are characterized and documented sufficiently for commercially available MBES. Further involvement from manufacturers in providing this essential information is critically required.

Electron backscatter diffraction study of dislocation content of a macrozone in hot-rolled Ti-6Al-4V alloy

International Nuclear Information System (INIS)

Britton, T. Ben; Birosca, Soran; Preuss, Michael; Wilkinson, Angus J.

2010-01-01

We compare the dislocation substructure within macrozone and non-macrozone regions of hot-rolled Ti-6Al-4 V. Hough-based and cross-correlation-based analysis of electron backscatter diffraction (EBSD) patterns are used to establish the grain orientations and intra-granular misorientations, respectively. The set of geometrically necessary dislocations (GNDs) that support measured lattice curvatures and minimize the total GND line energy are calculated. The GND content in the macrozone is approximately twice that in the non-macrozone region, and GNDs are present at densities ∼10 times higher than GNDs.

Calculated effects of backscattering on skin dosimetry for nuclear fuel fragments

International Nuclear Information System (INIS)

Aydarous, A. Sh

2008-01-01

The size of hot particles contained in nuclear fallout ranges from 10 nm to 20 μm for the worldwide weapons fallout. Hot particles from nuclear power reactors can be significantly bigger (100 μm to several millimetres). Electron backscattering from such particles is a prominent secondary effect in beta dosimetry for radiological protection purposes, such as skin dosimetry. In this study, the effect of electron backscattering due to hot particles contamination on skin dose is investigated. These include parameters such as detector area, source radius, source energy, scattering material and source density. The Monte-Carlo Neutron Particle code (MCNP4C) was used to calculate the depth dose distribution for 10 different beta sources and various materials. The backscattering dose factors (BSDF) were then calculated. A significant dependence is shown for the BSDF magnitude upon detector area, source radius and scatterers. It is clearly shown that the BSDF increases with increasing detector area. For high Z scatterers, the BSDF can reach as high as 40 and 100% for sources with radii 0.1 and 0.0001 cm, respectively. The variation of BSDF with source radius, source energy and source density is discussed. (authors)

Validation of automated supervised segmentation of multibeam backscatter data from the Chatham Rise, New Zealand

Science.gov (United States)

Hillman, Jess I. T.; Lamarche, Geoffroy; Pallentin, Arne; Pecher, Ingo A.; Gorman, Andrew R.; Schneider von Deimling, Jens

2018-06-01

Using automated supervised segmentation of multibeam backscatter data to delineate seafloor substrates is a relatively novel technique. Low-frequency multibeam echosounders (MBES), such as the 12-kHz EM120, present particular difficulties since the signal can penetrate several metres into the seafloor, depending on substrate type. We present a case study illustrating how a non-targeted dataset may be used to derive information from multibeam backscatter data regarding distribution of substrate types. The results allow us to assess limitations associated with low frequency MBES where sub-bottom layering is present, and test the accuracy of automated supervised segmentation performed using SonarScope® software. This is done through comparison of predicted and observed substrate from backscatter facies-derived classes and substrate data, reinforced using quantitative statistical analysis based on a confusion matrix. We use sediment samples, video transects and sub-bottom profiles acquired on the Chatham Rise, east of New Zealand. Inferences on the substrate types are made using the Generic Seafloor Acoustic Backscatter (GSAB) model, and the extents of the backscatter classes are delineated by automated supervised segmentation. Correlating substrate data to backscatter classes revealed that backscatter amplitude may correspond to lithologies up to 4 m below the seafloor. Our results emphasise several issues related to substrate characterisation using backscatter classification, primarily because the GSAB model does not only relate to grain size and roughness properties of substrate, but also accounts for other parameters that influence backscatter. Better understanding these limitations allows us to derive first-order interpretations of sediment properties from automated supervised segmentation.

The potential of materials analysis by electron Rutherford backscattering as illustrated by a case study of mouse bones and related compounds

International Nuclear Information System (INIS)

Vos, M.; Toekesi, K.; Benkoe, I.

2012-01-01

Complete text of publication follows. Electron Rutherford backscattering (ERBS) has a number of distinct advantages for semi-quantitative analysis of samples. These are for example: a) Its high energy makes it rather insensitive to surface effects. b) The peaks appear well approximated by Gaussian with no obvious problems due to background subtraction. c) All the electrons involved have very similar kinetic energy, and hence one does not need to consider changes of the mean-free path or the analyzer transmission function. d) There are no intrinsic satellites to complicate the quantitative interpretation. On the other hand ERBS has a weak point, peaks tend to overlap. Peak separation is proportional to the incoming energy E0, but the intrinsic peak width increases proportional to the square root of E 0 . In practice one has to live with overlapping peaks. In the present work we mainly focus on the measurement and analysis procedure, and compare our best estimate of the concentration of the various elements in mouse bone with that obtained in a recent paper. The promise of ERBS as an analytical technique is clear from the successful analysis of the simple case of calcium carbonate and the somewhat more complicated case of hydroxyapatite. Here agreement between the measured and actual composition are on a very respectable 10% level. The actual bone sample showed more variation in outcome and a somewhat less satisfactory agreement between experiment and theory (see Fig. 1). The variation in outcome between the different measurements can be due to the fact that we average over very few grains, and that the grain composition will vary somewhat with its original position in the bone. In summary, ERBS can become a useful tool to study bone mineralization. As our knowledge of bone mineralization is incomplete this is currently an active topic of multidisciplinary research involving people working in physics, chemistry and biological/medical sciences. One of the important

Quantitative seafloor characterization using angular backscatter data of the multi-beam echo-sounding system - Use of models and model free techniques

Digital Repository Service at National Institute of Oceanography (India)

Chakraborty, B.

processing gain, bottom slope corrections, and bottom insonification area normalisation were proposed to generate angular backscattering strength for modelling to infer bottom roughness parameters. A software package (NORGCOR) for similar purpose... bottom backscatter data from multibeam system. For each seafloor area, processed backscatter strength values [presented in Fig.: I(c)], are binned at intervals of 1° from --45° to +45°, and averaged over the entire dataset (approximately around 100...

Oscillations in the spectrum of nonlinear Thomson-backscattered radiation

Directory of Open Access Journals (Sweden)

C. A. Brau

2004-02-01

Full Text Available When an electron beam collides with a high-intensity laser beam, the spectrum of the nonlinear Thomson scattering in the backward direction shows strong oscillations like those in the spectrum of an optical klystron. Laser gain on the backward Thomson scattering is estimated using the Madey theorem, and the results suggest that Thomson-backscatter free-electron lasers are possible at wavelengths extending to the far uv using a terawatt laser beam from a chirped-pulse amplifier and a high-brightness electron beam from a needle cathode.

In situ electron backscatter diffraction investigation of recrystallization in a copper wire.

Science.gov (United States)

Brisset, François; Helbert, Anne-Laure; Baudin, Thierry

2013-08-01

The microstructural evolution of a cold drawn copper wire (reduction area of 38%) during primary recrystallization and grain growth was observed in situ by electron backscatter diffraction. Two thermal treatments were performed, and successive scans were acquired on samples undergoing heating from ambient temperature to a steady state of 200°C or 215°C. During a third in situ annealing, the temperature was continuously increased up to 600°C. Nuclei were observed to grow at the expense of the deformed microstructure. This growth was enhanced by the high stored energy difference between the nuclei and their neighbors (driving energy in recrystallization) and by the presence of high-angle grain boundaries of high mobility. In the early stages of growth, the nuclei twin and the newly created orientations continue to grow to the detriment of the strained copper. At high temperatures, the disappearance of some twins was evidenced by the migration of the incoherent twin boundaries. Thermal grooving of grain boundaries is observed at these high temperatures and affects the high mobile boundaries but tends to preserve the twin boundaries of lower energy. Thus, grooving may contribute to the twin vanishing.

Can X-ray spectrum imaging replace backscattered electrons for compositional contrast in the scanning electron microscope?

Science.gov (United States)

Newbury, Dale E; Ritchie, Nicholas W M

2011-01-01

The high throughput of the silicon drift detector energy dispersive X-ray spectrometer (SDD-EDS) enables X-ray spectrum imaging (XSI) in the scanning electron microscope to be performed in frame times of 10-100 s, the typical time needed to record a high-quality backscattered electron (BSE) image. These short-duration XSIs can reveal all elements, except H, He, and Li, present as major constituents, defined as 0.1 mass fraction (10 wt%) or higher, as well as minor constituents in the range 0.01-0.1 mass fraction, depending on the particular composition and possible interferences. Although BSEs have a greater abundance by a factor of 100 compared with characteristic X-rays, the strong compositional contrast in element-specific X-ray maps enables XSI mapping to compete with BSE imaging to reveal compositional features. Differences in the fraction of the interaction volume sampled by the BSE and X-ray signals lead to more delocalization of the X-ray signal at abrupt compositional boundaries, resulting in poorer spatial resolution. Improved resolution in X-ray elemental maps occurs for the case of a small feature composed of intermediate to high atomic number elements embedded in a matrix of lower atomic number elements. XSI imaging strongly complements BSE imaging, and the SDD-EDS technology enables an efficient combined BSE-XSI measurement strategy that maximizes the compositional information. If 10 s or more are available for the measurement of an area of interest, the analyst should always record the combined BSE-XSI information to gain the advantages of both measures of compositional contrast. Copyright © 2011 Wiley Periodicals, Inc.

Analysis of recrystallization behavior of hot-deformed austenite reconstructed from electron backscattering diffraction orientation maps of lath martensite

International Nuclear Information System (INIS)

Kubota, Manabu; Ushioda, Kohsaku; Miyamoto, Goro; Furuhara, Tadashi

2016-01-01

The recrystallization behavior of hot-deformed austenite of a 0.55% C steel at 800 °C was investigated by a method of reconstructing the parent austenite orientation map from an electron backscattering diffraction orientation map of lath martensite. Recrystallized austenite grains were clearly distinguished from un-recrystallized austenite grains. Very good correlation was confirmed between the static recrystallization behavior investigated mechanically by double-hit compression tests and the change in austenite microstructure evaluated by the reconstruction method. The recrystallization behavior of hot-deformed 0.55% C steel at 800 °C is directly revealed and it was observed that by addition of 0.1% V the recrystallization was significantly retarded.

Modified Sternglass theory for the emission of secondary electrons by fast-electron impact

International Nuclear Information System (INIS)

Suszcynsky, D.M.; Borovsky, J.E.

1992-01-01

The Sternglass theory [Sternglass, Phys. Rev. 108, 1 (1957)] for fast-ion-induced secondary-electron emission from metals has been modified to predict the secondary-electron yield from metals impacted by energetic (several keV to about 200 keV) electrons. The primary modification of the theory accounts for the contribution of the backscattered electrons to the production of secondary electrons based on a knowledge of the backscattered-electron energy distribution. The modified theory is in reasonable agreement with recent experimental data from gold targets in the 6--30-keV electron energy range

Users guide to the HELIOS backscattering spectrometer (BSS)

International Nuclear Information System (INIS)

Bunce, L.J.

1986-10-01

The BSS is a backscattering spectrometer installed on the Harwell 136 Mev electron linear accelerator, HELIOS. A general description of the instrument is given, along with the time of flight scales, and the run and sample changer control units. The sample environment, vacuum system and detectors of the BSS are described, as well as the preparation, starting and running of an experiment using the BSS. (UK)

Initial microstructural study of a Ce-La alloy using electron backscattered diffraction

International Nuclear Information System (INIS)

Scott, Thomas B.; Younes, Charles M.; Ling, Michael; Jones, Christopher P.; Nicholson, John A.; Heard, Peter J.; Jenkins, Roderick

2011-01-01

Research highlights: → First ever successful EBSD microstructural analysis of Ce-La alloy. → Successful preparation using electro-polishing in the open laboratory. → Equiaxed grains 20-40 μm in size dominate the microstructure, with random orientations, relatively straight grain boundary contacts and no evidence for crystal twinning. → All grains matched to a fcc γ-phase. → Problematic presence of entrapped oxide particles. - Abstract: To better understand and exploit the unique electronic and structural properties of f-block metals and their alloys it is perceived that an improved knowledge of the microstructural characteristics and phase changes as a function of temperature and pressure, is necessary. For other different types of metallic systems, the use of electron back-scattered diffraction (EBSD) is becoming a common practice in order to obtain detailed microstructural information, but this has, as yet, been very limited in case of f-block metals. Because of their extreme affinity to oxygen and rapid surface reaction, EBSD studies of this metal-category are very sparse with only one work published on cerium metal providing an example of technical hurdles for a prerequisite oxide-free metal surface. Specifically the need to remove the oxide by ion etching was considered essential to enable a successful EBSD analysis. The current work presents the results of a first attempt to characterise the microstructure of a Ce-La alloy using EBSD. It demonstrates that high quality diffraction patterns and crystal orientation maps can be successfully obtained following a carefully controlled preparation of the alloy surface in the open laboratory by applying a simple and reproducible electro-polishing procedure without a further need for ion etching in vaccuo.

Electron Backscatter Diffraction Studies on the Formation of Superlattice Metal Hydride Alloys

Directory of Open Access Journals (Sweden)

Shuli Yan

2017-12-01

Full Text Available Microstructures of a series of La-Mg-Ni-based superlattice metal hydride alloys produced by a novel method of interaction of a LaNi5 alloy and Mg vapor were studied using a combination of X-ray energy dispersive spectroscopy and electron backscatter diffraction. The conversion rate of LaNi5 increased from 86.8% into 98.2%, and the A2B7 phase abundance increased from 42.5 to 45.8 wt % and reduced to 39.2 wt % with the increase in process time from four to 32 h. During the first stage of reaction, Mg formed discrete grains with the same orientation, which was closely related to the orientation of the host LaNi5 alloy. Mg then diffused through the ab-phase of LaNi5 and formed the AB2, AB3, and A2B7 phases. Diffusion of Mg stalled at the grain boundary of the host LaNi5 alloy. Good alignments in the c-axis between the newly formed superlattice phases and LaNi5 were observed. The density of high-angle grain boundary decreased with the increase in process time and was an indication of lattice cracking.

The relationship between VHF radar auroral backscatter amplitude and Doppler velocity: a statistical study

Directory of Open Access Journals (Sweden)

B. A. Shand

Full Text Available A statistical investigation of the relationship between VHF radar auroral backscatter intensity and Doppler velocity has been undertaken with data collected from 8 years operation of the Wick site of the Sweden And Britain Radar-auroral Experiment (SABRE. The results indicate three different regimes within the statistical data set; firstly, for Doppler velocities <200 m s^–1, the backscatter intensity (measured in decibels remains relatively constant. Secondly, a linear relationship is observed between the backscatter intensity (in decibels and Doppler velocity for velocities between 200 m s^–1 and 700 m s^–1. At velocities greater than 700 m s^–1 the backscatter intensity saturates at a maximum value as the Doppler velocity increases. There are three possible geophysical mechanisms for the saturation in the backscatter intensity at high phase speeds: a saturation in the irregularity turbulence level, a maximisation of the scattering volume, and a modification of the local ambient electron density. There is also a difference in the dependence of the backscatter intensity on Doppler velocity for the flow towards and away from the radar. The results for flow towards the radar exhibit a consistent relationship between backscatter intensity and measured velocities throughout the solar cycle. For flow away from the radar, however, the relationship between backscatter intensity and Doppler velocity varies during the solar cycle. The geometry of the SABRE system ensures that flow towards the radar is predominantly associated with the eastward electrojet, and flow away is associated with the westward electrojet. The difference in the backscatter intensity variation as a function of Doppler velocity is attributed to asymmetries between the eastward and westward electrojets and the geophysical parameters controlling the backscatter amplitude.

The relationship between VHF radar auroral backscatter amplitude and Doppler velocity: a statistical study

Directory of Open Access Journals (Sweden)

B. A. Shand

1996-08-01

Full Text Available A statistical investigation of the relationship between VHF radar auroral backscatter intensity and Doppler velocity has been undertaken with data collected from 8 years operation of the Wick site of the Sweden And Britain Radar-auroral Experiment (SABRE. The results indicate three different regimes within the statistical data set; firstly, for Doppler velocities <200 m s–1, the backscatter intensity (measured in decibels remains relatively constant. Secondly, a linear relationship is observed between the backscatter intensity (in decibels and Doppler velocity for velocities between 200 m s–1 and 700 m s–1. At velocities greater than 700 m s–1 the backscatter intensity saturates at a maximum value as the Doppler velocity increases. There are three possible geophysical mechanisms for the saturation in the backscatter intensity at high phase speeds: a saturation in the irregularity turbulence level, a maximisation of the scattering volume, and a modification of the local ambient electron density. There is also a difference in the dependence of the backscatter intensity on Doppler velocity for the flow towards and away from the radar. The results for flow towards the radar exhibit a consistent relationship between backscatter intensity and measured velocities throughout the solar cycle. For flow away from the radar, however, the relationship between backscatter intensity and Doppler velocity varies during the solar cycle. The geometry of the SABRE system ensures that flow towards the radar is predominantly associated with the eastward electrojet, and flow away is associated with the westward electrojet. The difference in the backscatter intensity variation as a function of Doppler velocity is attributed to asymmetries between the eastward and westward electrojets and the geophysical parameters controlling the backscatter amplitude.

Accurate virus quantitation using a Scanning Transmission Electron Microscopy (STEM) detector in a scanning electron microscope.

Science.gov (United States)

Blancett, Candace D; Fetterer, David P; Koistinen, Keith A; Morazzani, Elaine M; Monninger, Mitchell K; Piper, Ashley E; Kuehl, Kathleen A; Kearney, Brian J; Norris, Sarah L; Rossi, Cynthia A; Glass, Pamela J; Sun, Mei G

2017-10-01

A method for accurate quantitation of virus particles has long been sought, but a perfect method still eludes the scientific community. Electron Microscopy (EM) quantitation is a valuable technique because it provides direct morphology information and counts of all viral particles, whether or not they are infectious. In the past, EM negative stain quantitation methods have been cited as inaccurate, non-reproducible, and with detection limits that were too high to be useful. To improve accuracy and reproducibility, we have developed a method termed Scanning Transmission Electron Microscopy - Virus Quantitation (STEM-VQ), which simplifies sample preparation and uses a high throughput STEM detector in a Scanning Electron Microscope (SEM) coupled with commercially available software. In this paper, we demonstrate STEM-VQ with an alphavirus stock preparation to present the method's accuracy and reproducibility, including a comparison of STEM-VQ to viral plaque assay and the ViroCyt Virus Counter. Copyright © 2017 The Authors. Published by Elsevier B.V. All rights reserved.

Implementation of a near backscattering imaging system on the National Ignition Facility

International Nuclear Information System (INIS)

Mackinnon, A.J.; McCarville, T.; Piston, K.; Niemann, C.; Jones, G.; Reinbachs, I.; Costa, R.; Celeste, J.; Holtmeier, G.; Griffith, R.; Kirkwood, R.; MacGowan, B.; Glenzer, S.H.; Latta, M.R.

2004-01-01

A near backscattering imaging diagnostic system is being implemented on the first quad of beams on the National Ignition Facility. This diagnostic images diffusing scatter plates, placed around the final focus lenses on the National Ignition Facility target chamber, to quantitatively measure the fraction of light backscattered outside of the focusing cone angle of incident laser beam. A wide-angle imaging system relays an image of light scattered outside the lens onto a gated charge coupled device camera, providing 3 mm resolution over a 2 m field of view. To account for changes of the system throughput due to exposure to target debris the system will be routinely calibrated in situ at 532 and 355 nm using a dedicated pulsed laser source

Spatially resolved determination of lattice distortions in silicon nanostructures by means of electron-backscattering diffraction

International Nuclear Information System (INIS)

Krause, Michael

2013-01-01

In the submitted thesis, a novel combined approach of both focused ion beam (FIB) based target preparation and strain determination using electron backscatter diffraction (EBSD) in semiconductor nanostructures is presented. In the first part, a powerful cross-correlation algorithm for detecting small feature shifts within EBSD patterns and, consequently, determining the strain, is presented. The corresponding strain sensitivity is demonstrated using dynamically simulated diffraction patterns. Furthermore, novel procedures for automated pattern analysis are introduced. Results of systematic studies concerning the influence of ion species, ion energy and dose density on the surface quality of silicon surfaces are presented in the second part. For that matter, the assessment of surface amorphization and rippling is based on high resolution microstructural diagnostics (TEM, AFM, Raman) and molecular dynamics simulation. The high application potential of combined FIB preparation and strain analysis using EBSD is exemplarily demonstrated for a 60 nm thick sSOI-sample. The good agreement with established techniques like Raman spectroscopy and X-ray diffraction is also shown.

Damage Assessment of Heat Resistant Steels through Electron BackScatter Diffraction Strain Analysis under Creep and Creep-Fatigue Conditions

Science.gov (United States)

Fujiyama, Kazunari; Kimachi, Hirohisa; Tsuboi, Toshiki; Hagiwara, Hiroyuki; Ogino, Shotaro; Mizutani, Yoshiki

EBSD(Electron BackScatter Diffraction) analyses were conducted for studying the quantitative microstructural metrics of creep and creep-fatigue damage for austenitic SUS304HTB boiler tube steel and ferritic Mod.9Cr piping steel. KAM(Kernel Average Misorientation) maps and GOS(Grain Orientation Spread) maps were obtained for these samples and the area averaged values KAMave and GOSave were obtained. While the increasing trends of these misorientation metrics were observed for SUS304HTB steel, the decreasing trends were observed for damaged Mod.9Cr steel with extensive recovery of subgrain structure. To establish more universal parameter representing the accumulation of damage to compensate these opposite trends, the EBSD strain parameters were introduced for converting the misorientation changes into the quantities representing accumulated permanent strains during creep and creep-fatigue damage process. As KAM values were dependent on the pixel size (inversely proportional to the observation magnification) and the permanent strain could be expressed as the shear strain which was the product of dislocation density, Burgers vector and dislocation movement distance, two KAM strain parameters MεKAMnet and MεδKAMave were introduced as the sum of product of the noise subtracted KAMnet and the absolute change from initial value δKAMave with dislocation movement distance divided by pixel size. MεδKAMave parameter showed better relationship both with creep strain in creep tests and accumulated creep strain range in creep-fatigue tests. This parameter can be used as the strain-based damage evaluation and detector of final failure.

Backscattering analysis of high frequency ultrasonic imaging for ultrasound-guided breast biopsy

Science.gov (United States)

Cummins, Thomas; Akiyama, Takahiro; Lee, Changyang; Martin, Sue E.; Shung, K. Kirk

2017-03-01

A new ultrasound-guided breast biopsy technique is proposed. The technique utilizes conventional ultrasound guidance coupled with a high frequency embedded ultrasound array located within the biopsy needle to improve the accuracy in breast cancer diagnosis.1 The array within the needle is intended to be used to detect micro- calcifications indicative of early breast cancers such as ductal carcinoma in situ (DCIS). Backscattering analysis has the potential to characterize tissues to improve localization of lesions. This paper describes initial results of the application of backscattering analysis of breast biopsy tissue specimens and shows the usefulness of high frequency ultrasound for the new biopsy related technique. Ultrasound echoes of ex-vivo breast biopsy tissue specimens were acquired by using a single-element transducer with a bandwidth from 41 MHz to 88 MHz utilizing a UBM methodology, and the backscattering coefficients were calculated. These values as well as B-mode image data were mapped in 2D and matched with each pathology image for the identification of tissue type for the comparison to the pathology images corresponding to each plane. Microcalcifications were significantly distinguished from normal tissue. Adenocarcinoma was also successfully differentiated from adipose tissue. These results indicate that backscattering analysis is able to quantitatively distinguish tissues into normal and abnormal, which should help radiologists locate abnormal areas during the proposed ultrasound-guided breast biopsy with high frequency ultrasound.

Backscatter measurements for NIF ignition targets (invited).

Science.gov (United States)

Moody, J D; Datte, P; Krauter, K; Bond, E; Michel, P A; Glenzer, S H; Divol, L; Niemann, C; Suter, L; Meezan, N; MacGowan, B J; Hibbard, R; London, R; Kilkenny, J; Wallace, R; Kline, J L; Knittel, K; Frieders, G; Golick, B; Ross, G; Widmann, K; Jackson, J; Vernon, S; Clancy, T

2010-10-01

Backscattered light via laser-plasma instabilities has been measured in early NIF hohlraum experiments on two beam quads using a suite of detectors. A full aperture backscatter system and near backscatter imager (NBI) instrument separately measure the stimulated Brillouin and stimulated Raman scattered light. Both instruments work in conjunction to determine the total backscattered power to an accuracy of ∼15%. In order to achieve the power accuracy we have added time-resolution to the NBI for the first time. This capability provides a temporally resolved spatial image of the backscatter which can be viewed as a movie.

Backscatter measurements for NIF ignition targets (invited)

Energy Technology Data Exchange (ETDEWEB)

Moody, J. D.; Datte, P.; Krauter, K.; Bond, E.; Michel, P. A.; Glenzer, S. H.; Divol, L.; Suter, L.; Meezan, N.; MacGowan, B. J.; Hibbard, R.; London, R.; Kilkenny, J.; Wallace, R.; Knittel, K.; Frieders, G.; Golick, B.; Ross, G.; Widmann, K.; Jackson, J. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94550 (United States); and others

2010-10-15

Backscattered light via laser-plasma instabilities has been measured in early NIF hohlraum experiments on two beam quads using a suite of detectors. A full aperture backscatter system and near backscatter imager (NBI) instrument separately measure the stimulated Brillouin and stimulated Raman scattered light. Both instruments work in conjunction to determine the total backscattered power to an accuracy of {approx}15%. In order to achieve the power accuracy we have added time-resolution to the NBI for the first time. This capability provides a temporally resolved spatial image of the backscatter which can be viewed as a movie.

Backscatter measurements for NIF ignition targets (invited)

International Nuclear Information System (INIS)

Moody, J. D.; Datte, P.; Krauter, K.; Bond, E.; Michel, P. A.; Glenzer, S. H.; Divol, L.; Suter, L.; Meezan, N.; MacGowan, B. J.; Hibbard, R.; London, R.; Kilkenny, J.; Wallace, R.; Knittel, K.; Frieders, G.; Golick, B.; Ross, G.; Widmann, K.; Jackson, J.

2010-01-01

Backscattered light via laser-plasma instabilities has been measured in early NIF hohlraum experiments on two beam quads using a suite of detectors. A full aperture backscatter system and near backscatter imager (NBI) instrument separately measure the stimulated Brillouin and stimulated Raman scattered light. Both instruments work in conjunction to determine the total backscattered power to an accuracy of ∼15%. In order to achieve the power accuracy we have added time-resolution to the NBI for the first time. This capability provides a temporally resolved spatial image of the backscatter which can be viewed as a movie.

Multibeam sonar backscatter data processing

Science.gov (United States)

Schimel, Alexandre C. G.; Beaudoin, Jonathan; Parnum, Iain M.; Le Bas, Tim; Schmidt, Val; Keith, Gordon; Ierodiaconou, Daniel

2018-06-01

Multibeam sonar systems now routinely record seafloor backscatter data, which are processed into backscatter mosaics and angular responses, both of which can assist in identifying seafloor types and morphology. Those data products are obtained from the multibeam sonar raw data files through a sequence of data processing stages that follows a basic plan, but the implementation of which varies greatly between sonar systems and software. In this article, we provide a comprehensive review of this backscatter data processing chain, with a focus on the variability in the possible implementation of each processing stage. Our objective for undertaking this task is twofold: (1) to provide an overview of backscatter data processing for the consideration of the general user and (2) to provide suggestions to multibeam sonar manufacturers, software providers and the operators of these systems and software for eventually reducing the lack of control, uncertainty and variability associated with current data processing implementations and the resulting backscatter data products. One such suggestion is the adoption of a nomenclature for increasingly refined levels of processing, akin to the nomenclature adopted for satellite remote-sensing data deliverables.

A correlative approach to segmenting phases and ferrite morphologies in transformation-induced plasticity steel using electron back-scattering diffraction and energy dispersive X-ray spectroscopy.

Science.gov (United States)

Gazder, Azdiar A; Al-Harbi, Fayez; Spanke, Hendrik Th; Mitchell, David R G; Pereloma, Elena V

2014-12-01

Using a combination of electron back-scattering diffraction and energy dispersive X-ray spectroscopy data, a segmentation procedure was developed to comprehensively distinguish austenite, martensite, polygonal ferrite, ferrite in granular bainite and bainitic ferrite laths in a thermo-mechanically processed low-Si, high-Al transformation-induced plasticity steel. The efficacy of the ferrite morphologies segmentation procedure was verified by transmission electron microscopy. The variation in carbon content between the ferrite in granular bainite and bainitic ferrite laths was explained on the basis of carbon partitioning during their growth. Copyright © 2014 Elsevier B.V. All rights reserved.

Phase analysis in duplex stainless steel: comparison of EBSD and quantitative metallography methods

International Nuclear Information System (INIS)

Michalska, J; Chmiela, B

2014-01-01

The purpose of the research was to work out the qualitative and quantitative analysis of phases in DSS in as-received state and after thermal aging. For quantitative purposes, SEM observations, EDS analyses and electron backscattered diffraction (EBSD) methods were employed. Qualitative analysis of phases was performed by two methods: EBSD and classical quantitative metallography. A juxtaposition of different etchants for the revealing of microstructure and brief review of sample preparation methods for EBSD studies were presented. Different ways of sample preparation were tested and based on these results a detailed methodology of DSS phase analysis was developed including: surface finishing, selective etching methods and image acquisition. The advantages and disadvantages of applied methods were pointed out and compared the accuracy of the analysis phase performed by both methods

Quantitative transmission electron microscopy at atomic resolution

International Nuclear Information System (INIS)

Allen, L J; D'Alfonso, A J; Forbes, B D; Findlay, S D; LeBeau, J M; Stemmer, S

2012-01-01

In scanning transmission electron microscopy (STEM) it is possible to operate the microscope in bright-field mode under conditions which, by the quantum mechanical principle of reciprocity, are equivalent to those in conventional transmission electron microscopy (CTEM). The results of such an experiment will be presented which are in excellent quantitative agreement with theory for specimens up to 25 nm thick. This is at variance with the large contrast mismatch (typically between two and five) noted in equivalent CTEM experiments. The implications of this will be discussed.

Experimental evidence concerning the significant information depth of electron backscatter diffraction (EBSD)

Energy Technology Data Exchange (ETDEWEB)

Wisniewski, Wolfgang, E-mail: wolfgang.w@uni-jena.de [Otto-Schott-Institut, Jena University, Fraunhoferstr. 6, 07743 Jena (Germany); Saager, Stefan [Fraunhofer Institute for Organic Electronics, Electron Beam and Plasma Technology FEP, Winterbergstraße 28, 01277 Dresden (Germany); Böbenroth, Andrea [Fraunhofer Institute for the Microstructure of Materials and Systems IMWS, Walter-Huelse-Straße 1, 06120 Halle (Saale) (Germany); Rüssel, Christian [Otto-Schott-Institut, Jena University, Fraunhoferstr. 6, 07743 Jena (Germany)

2017-02-15

Experiments concerning the information depth of electron backscatter diffraction (EBSD) are performed on samples featuring an amorphous wedge on a crystalline substrate and a crystalline wedge on an amorphous substrate. The effects of the acceleration voltage and exemplary software settings on the ability to measure through an amorphous layer are presented. Changes in the EBSD-signal could be detected through a ≈142 nm thick layer of amorphous Si while orientation measurements could be performed through a ≈116 nm thick layer when using a voltage of 30 kV. The complexity of the information depth significant to a given EBSD-pattern and the multiple parameters influencing it are discussed. It is suggested that a “core information depth” is significant to high quality patterns while a larger “maximum information depth” becomes relevant when the pattern quality decreases or the sample is inhomogeneous within the information volume, i.e. in the form of partially crystalline materials or crystal layers in the nm scale. - Highlights: • Experimental evidence of the significant information depth of EBSD is presented. • Effects of the voltage and exemplary software settings are discussed. • Dependence of the significant information depth on the pattern quality is proposed. • The information depth may reach up to 142 nm in Si when using a voltage of 30 kV. • The information depth depends on the available technology.

Auger electron spectroscopy and Rutherford backscattering studies of copper in 2024-T3 aluminum following electrochemical anodization in phosphoric acid

Science.gov (United States)

Solomon, J. S.

1981-05-01

The effects of the electrochemical anodization of dioxidized 2024-T3 aluminum on copper were characterized by Auger electron spectroscopy and Rutherford backscattering. Anodization was performed in phosphoric acid at constant potential. Data is presented which shows that constant potential anodization of 2024-T3 is more efficient than aluminum in terms of oxide growth rates for short anodization times. However the maximum anodic oxide thickness achievable on the alloy is less than the pure metal. Copper is shown to be enriched at the oxide metal interface because of its diffusion from the bulk during anodization. The presence of copper at the oxide-metal interface is shown to affect oxide morphology.

Analytic representation of the backscatter correction factor at the exit of high energy photon beams

International Nuclear Information System (INIS)

Kappas, K.; Rosenwald, J.C.

1991-01-01

In high-energy X-ray beams, the dose calculated near the exit surface under electronic equilibrium conditions is generally over-estimated since it is derived from measurements performed in water with large thickness of backscattering material. The resulting error depends on a number of parameters such as beam energy, field dimension, thickness of overlying and underlying material. The authors have systematically measured for 4 different energies and for different para- meters and for different combinations of the above parameters, the reduction of dose due to backscatter. This correction is expressed as a multiplicative factor, called 'Backscatter Correction Factor' (BCF). This BCF is larger for lower energies, larger field sizes and larger depths. The BCF has been represented by an analytical expression which involves an exponential function of the backscattering thickness and linear relationships with depth field size and beam quality index. Using this expression, the BCF can be calculated within 0.5% for any conditions in the energy range investigated. (author). 14 refs.; 4 figs.; 3 tabs

Electron backscatter diffraction studies of focused ion beam induced phase transformation in cobalt

Energy Technology Data Exchange (ETDEWEB)

Jones, H.G., E-mail: helen.jones@npl.co.uk [National Physical Laboratory, Hampton Road, Teddington, Middlesex TW11 0LW (United Kingdom); Day, A.P. [Aunt Daisy Scientific Ltd, Claremont House, High St, Lydney GL15 5DX (United Kingdom); Cox, D.C. [National Physical Laboratory, Hampton Road, Teddington, Middlesex TW11 0LW (United Kingdom); Advanced Technology Institute, University of Surrey, Guildford GU2 7XH (United Kingdom)

2016-10-15

A focused ion beam microscope was used to induce cubic to hexagonal phase transformation in a cobalt alloy, of similar composition to that of the binder phase in a hardmetal, in a controlled manner at 0°, 45° and 80° ion incident angles. The cobalt had an average grain size of ~ 20 μm, allowing multiple orientations to be studied, exposed to a range of doses between 6 × 10{sup 7} and 2 × 10{sup 10} ions/μm{sup 2}. Electron backscatter diffraction (EBSD) was used to determine the original and induced phase orientations, and area fractions, before and after the ion beam exposure. On average, less phase transformation was observed at higher incident angles and after lower ion doses. However there was an orientation effect where grains with an orientation close to (111) planes were most susceptible to phase transformation, and (101) the least, where grains partially and fully transformed at varying ion doses. - Highlights: •Ion-induced phase change in FCC cobalt was observed at multiple incidence angles. •EBSD was used to study the relationship between grain orientation and transformation. •Custom software analysed ion dose and phase change with respect to grain orientation. •A predictive capability of ion-induced phase change in cobalt was enabled.

Lines of Evidence–Incremental Markings in Molar Enamel of Soay Sheep as Revealed by a Fluorochrome Labeling and Backscattered Electron Imaging Study

Science.gov (United States)

Kierdorf, Horst; Kierdorf, Uwe; Frölich, Kai; Witzel, Carsten

2013-01-01

We studied the structural characteristics and periodicities of regular incremental markings in sheep enamel using fluorochrome injections for vital labeling of forming enamel and backscattered electron imaging in the scanning electron microscope. Microscopic analysis of mandibular first molars revealed the presence of incremental markings with a daily periodicity (laminations) that indicated successive positions of the forming front of interprismatic enamel. In addition to the laminations, incremental markings with a sub-daily periodicity were discernible both in interprismatic enamel and in enamel prisms. Five sub-daily increments were present between two consecutive laminations. Backscattered electron imaging revealed that each sub-daily growth increment consisted of a broader and more highly mineralized band and a narrower and less mineralized band (line). The sub-daily markings in the prisms of sheep enamel morphologically resembled the (daily) prisms cross striations seen in primate enamel. Incremental markings with a supra-daily periodicity were not observed in sheep enamel. Based on the periodicity of the incremental markings, maximum mean daily apposition rates of 17.0 µm in buccal enamel and of 13.4 µm in lingual enamel were recorded. Enamel extension rates were also high, with maximum means of 180 µm/day and 217 µm/day in upper crown areas of buccal and lingual enamel, respectively. Values in more cervical crown portions were markedly lower. Our results are in accordance with previous findings in other ungulate species. Using the incremental markings present in primate enamel as a reference could result in a misinterpretation of the incremental markings in ungulate enamel. Thus, the sub-daily growth increments in the prisms of ungulate enamel might be mistaken as prism cross striations with a daily periodicity, and the laminations misidentified as striae of Retzius with a supra-daily periodicity. This would lead to a considerable overestimation of

Deformation micro-mechanism for compression of magnesium alloys at room temperature analyzed by electron backscatter diffraction

International Nuclear Information System (INIS)

Song, G.S.; Chen, Q.Q.; Zhang, S.H.; Xu, Y.

2015-01-01

Highlights: • In-situ tracking on the evolution of grains orientation of magnesium alloy was carried out by EBSD. • Distributions of twin bands were closely related to the activation of extension twin variants. • Activation of extension twin significantly changes the order of Schmid factor of slips. • Pyramidal slips become the dominant deformation mode at the late stage of compression. - Abstract: In-situ tracking on the evolution of grains orientation of rolled magnesium alloy sheets compressed uniaxially at room temperature was carried out by the method of electron backscatter diffraction (EBSD), and meanwhile, distributions of twin bands, activations of twin and slips were also analyzed. The results show that the distributions of twin bands were closely related to the activation of extension twin variants. The activation of extension twin significantly changes the order of Schmid factor of different slips, and accordingly affects the activation of slips during the subsequent deformation

An analytical model for light backscattering by coccoliths and coccospheres of Emiliania huxleyi.

Science.gov (United States)

Fournier, Georges; Neukermans, Griet

2017-06-26

We present an analytical model for light backscattering by coccoliths and coccolithophores of the marine calcifying phytoplankter Emiliania huxleyi. The model is based on the separation of the effects of diffraction, refraction, and reflection on scattering, a valid assumption for particle sizes typical of coccoliths and coccolithophores. Our model results match closely with results from an exact scattering code that uses complex particle geometry and our model also mimics well abrupt transitions in scattering magnitude. Finally, we apply our model to predict changes in the spectral backscattering coefficient during an Emiliania huxleyi bloom with results that closely match in situ measurements. Because our model captures the key features that control the light backscattering process, it can be generalized to coccoliths and coccolithophores of different morphologies which can be obtained from size-calibrated electron microphotographs. Matlab codes of this model are provided as supplementary material.

Spatially coded backscatter radiography

International Nuclear Information System (INIS)

Thangavelu, S.; Hussein, E.M.A.

2007-01-01

Conventional radiography requires access to two opposite sides of an object, which makes it unsuitable for the inspection of extended and/or thick structures (airframes, bridges, floors etc.). Backscatter imaging can overcome this problem, but the indications obtained are difficult to interpret. This paper applies the coded aperture technique to gamma-ray backscatter-radiography in order to enhance the detectability of flaws. This spatial coding method involves the positioning of a mask with closed and open holes to selectively permit or block the passage of radiation. The obtained coded-aperture indications are then mathematically decoded to detect the presence of anomalies. Indications obtained from Monte Carlo calculations were utilized in this work to simulate radiation scattering measurements. These simulated measurements were used to investigate the applicability of this technique to the detection of flaws by backscatter radiography

X-ray backscatter imaging for radiography by selective detection and snapshot: Evolution, development, and optimization

Science.gov (United States)

Shedlock, Daniel

Compton backscatter imaging (CBI) is a single-sided imaging technique that uses the penetrating power of radiation and unique interaction properties of radiation with matter to image subsurface features. CBI has a variety of applications that include non-destructive interrogation, medical imaging, security and military applications. Radiography by selective detection (RSD), lateral migration radiography (LMR) and shadow aperture backscatter radiography (SABR) are different CBI techniques that are being optimized and developed. Radiography by selective detection (RSD) is a pencil beam Compton backscatter imaging technique that falls between highly collimated and uncollimated techniques. Radiography by selective detection uses a combination of single- and multiple-scatter photons from a projected area below a collimation plane to generate an image. As a result, the image has a combination of first- and multiple-scatter components. RSD techniques offer greater subsurface resolution than uncollimated techniques, at speeds at least an order of magnitude faster than highly collimated techniques. RSD scanning systems have evolved from a prototype into near market-ready scanning devices for use in a variety of single-sided imaging applications. The design has changed to incorporate state-of-the-art detectors and electronics optimized for backscatter imaging with an emphasis on versatility, efficiency and speed. The RSD system has become more stable, about 4 times faster, and 60% lighter while maintaining or improving image quality and contrast over the past 3 years. A new snapshot backscatter radiography (SBR) CBI technique, shadow aperture backscatter radiography (SABR), has been developed from concept and proof-of-principle to a functional laboratory prototype. SABR radiography uses digital detection media and shaded aperture configurations to generate near-surface Compton backscatter images without scanning, similar to how transmission radiographs are taken. Finally, a

Plastic strain characterization in austenitic stainless steels and nickel alloys by electron backscatter diffraction

Energy Technology Data Exchange (ETDEWEB)

Saez-Maderuelo, A., E-mail: alberto.saez@ciemat.es [CIEMAT, Av. Complutense, 22-28040 Madrid (Spain); Castro, L.; Diego, G. de [CIEMAT, Av. Complutense, 22-28040 Madrid (Spain)

2011-09-01

Stress corrosion cracking (SCC) is enhanced by cold work and causes many problems in components of the nuclear power plants. Besides, during manufacturing, installation, welding and service of the material, residual strains can be produced increasing the susceptibility to SCC. For this reason, it is important to characterize the degree of plastic strain due to dislocation accumulation in each crystal. Electron backscatter diffraction (EBSD), in conjunction with scanning electron microscope (SEM), has been a great advance in this field because it enables to estimate the plastic strain in a quick and easy way. Nevertheless, over the last few years, a lot of different mathematical expressions to estimate the plastic strain have appeared in the literature. This situation hinders the election of one of them by a novel scientist in this field. Therefore, in this paper some of the more common expressions used in the calculation of the angular misorientation have been presented and discussed in order to clarify their more important aspects. Then, using one of these expressions (average local misorientation), curves relating misorientation density with known levels of strain will be obtained for an austenitic stainless steel 304L and nickel base alloy 690, which have shown a linear behaviour that is in good agreement with results found in the literature. Finally, using curves obtained in previous steps, levels of plastic strain in a plate of nickel base alloy 600 welded with weld metal 182 were estimated between 8 and 10% for a high temperature mill annealing sample.

Plastic strain characterization in austenitic stainless steels and nickel alloys by electron backscatter diffraction

International Nuclear Information System (INIS)

Saez-Maderuelo, A.; Castro, L.; Diego, G. de

2011-01-01

Stress corrosion cracking (SCC) is enhanced by cold work and causes many problems in components of the nuclear power plants. Besides, during manufacturing, installation, welding and service of the material, residual strains can be produced increasing the susceptibility to SCC. For this reason, it is important to characterize the degree of plastic strain due to dislocation accumulation in each crystal. Electron backscatter diffraction (EBSD), in conjunction with scanning electron microscope (SEM), has been a great advance in this field because it enables to estimate the plastic strain in a quick and easy way. Nevertheless, over the last few years, a lot of different mathematical expressions to estimate the plastic strain have appeared in the literature. This situation hinders the election of one of them by a novel scientist in this field. Therefore, in this paper some of the more common expressions used in the calculation of the angular misorientation have been presented and discussed in order to clarify their more important aspects. Then, using one of these expressions (average local misorientation), curves relating misorientation density with known levels of strain will be obtained for an austenitic stainless steel 304L and nickel base alloy 690, which have shown a linear behaviour that is in good agreement with results found in the literature. Finally, using curves obtained in previous steps, levels of plastic strain in a plate of nickel base alloy 600 welded with weld metal 182 were estimated between 8 and 10% for a high temperature mill annealing sample.

Recommendations for processing atmospheric attenuated backscatter profiles from Vaisala CL31 ceilometers

Science.gov (United States)

Kotthaus, Simone; O'Connor, Ewan; Münkel, Christoph; Charlton-Perez, Cristina; Haeffelin, Martial; Gabey, Andrew M.; Grimmond, C. Sue B.

2016-08-01

Ceilometer lidars are used for cloud base height detection, to probe aerosol layers in the atmosphere (e.g. detection of elevated layers of Saharan dust or volcanic ash), and to examine boundary layer dynamics. Sensor optics and acquisition algorithms can strongly influence the observed attenuated backscatter profiles; therefore, physical interpretation of the profiles requires careful application of corrections. This study addresses the widely deployed Vaisala CL31 ceilometer. Attenuated backscatter profiles are studied to evaluate the impact of both the hardware generation and firmware version. In response to this work and discussion within the CL31/TOPROF user community (TOPROF, European COST Action aiming to harmonise ground-based remote sensing networks across Europe), Vaisala released new firmware (versions 1.72 and 2.03) for the CL31 sensors. These firmware versions are tested against previous versions, showing that several artificial features introduced by the data processing have been removed. Hence, it is recommended to use this recent firmware for analysing attenuated backscatter profiles. To allow for consistent processing of historic data, correction procedures have been developed that account for artefacts detected in data collected with older firmware. Furthermore, a procedure is proposed to determine and account for the instrument-related background signal from electronic and optical components. This is necessary for using attenuated backscatter observations from any CL31 ceilometer. Recommendations are made for the processing of attenuated backscatter observed with Vaisala CL31 sensors, including the estimation of noise which is not provided in the standard CL31 output. After taking these aspects into account, attenuated backscatter profiles from Vaisala CL31 ceilometers are considered capable of providing valuable information for a range of applications including atmospheric boundary layer studies, detection of elevated aerosol layers, and model

A digital instrument for nondestructive measurements of coating thicknesses by beta backscattering

Science.gov (United States)

Farcasiu, D. M.; Apostolescu, T.; Bozdog, H.; Badescu, E.; Bohm, V.; Stanescu, S. P.; Jianu, A.; Bordeanu, C.; Cracium, M. V.

1992-02-01

The elements of nondestructive gauging of coatings applied on various metal bases are presented. The intensity of the backscattered beta radiations is related to the thickness of the coating. With a fixed measuring geometry and radioactive sources (147Pm, 204Tl, 90Sr+90Y) the intensity of the backscattered beta particles is dependent on the following parameters: coating thickness, atomic number of the coating material and of the base, the beta particle energy and the surface finish. It can be used for the measurement of a wide range of coating thicknesses provided that the difference between the coating and the support atomic numbers is at least 20%. Fields of application include electronics, electrotechnique and so on.

A digital instrument for nondestructive measurements of coating thicknesses by beta backscattering

International Nuclear Information System (INIS)

Farcasiu, D.M.; Apostolescu, T.; Bozdog, H.; Badescu, E.; Bohm, V.; Stanescu, S.P.; Jianu, A.; Bordeanu, C.; Craciun, M.V.

1992-01-01

The elements of nondestructive gauging of coatings applied on various metal bases are presented. The intensity of the backscattered beta radiations is related to the thickness of the coating. With a fixed measuring geometry and radioactive sources ( 147 Pm, 204 Tl, 90 Sr+ 90 Y) the intensity of the backscattered beta particles is dependent on the following parameters: Coating thickness, atomic number of the coating material and of the base, the beta particle energy and the surface finish. It can be used for the measurement of a wide range of coating thicknesses provided that the difference between the coating and the support atomic numbers is at least 20%. Fields of application include electronics, electrotechnique and so on. (orig.)

Quantitative determination of elastic and inelastic attenuation coefficients by off-axis electron holography

International Nuclear Information System (INIS)

Kern, F.; Wolf, D.; Pschera, P.; Lubk, A.

2016-01-01

Off-axis electron holography is a well-established transmission electron microscopy technique, typically employed to investigate electric and magnetic fields in and around nanoscale materials, which modify the phase of the reconstructed electron wave function. Here, we elaborate on a detailed analysis of the two characteristic intensity terms that are completing the electron hologram, the conventional image intensity and the interference fringe intensity. We show how both are related to elastic and inelastic scattering absorption at the sample and how they may be separated to analyze the chemical composition of the sample. Since scattering absorption is aperture dependent, a quantitative determination of the corresponding attenuation coefficients (reciprocal mean free path lengths) requires the use of holographic image modi with well-defined objective aperture stops in the back-focal plane of the objective lens. The proposed method extends quantitative electron holography to a correlated three-in-one characterization of electric and magnetic fields, Z-contrast and dielectric losses in materials. - Highlights: • Quantitative determination of attenuation coefficients by electron holography. • Separation of elastic and inelastic attenuation coefficients (mean free path length). • Quantitative determination of the objective aperture semi-angle influence. • Compilation of elastic and inelastic attenuation from different materials.

Quantitative determination of elastic and inelastic attenuation coefficients by off-axis electron holography

Energy Technology Data Exchange (ETDEWEB)

Kern, F.; Wolf, D.; Pschera, P.; Lubk, A.

2016-12-15

Off-axis electron holography is a well-established transmission electron microscopy technique, typically employed to investigate electric and magnetic fields in and around nanoscale materials, which modify the phase of the reconstructed electron wave function. Here, we elaborate on a detailed analysis of the two characteristic intensity terms that are completing the electron hologram, the conventional image intensity and the interference fringe intensity. We show how both are related to elastic and inelastic scattering absorption at the sample and how they may be separated to analyze the chemical composition of the sample. Since scattering absorption is aperture dependent, a quantitative determination of the corresponding attenuation coefficients (reciprocal mean free path lengths) requires the use of holographic image modi with well-defined objective aperture stops in the back-focal plane of the objective lens. The proposed method extends quantitative electron holography to a correlated three-in-one characterization of electric and magnetic fields, Z-contrast and dielectric losses in materials. - Highlights: • Quantitative determination of attenuation coefficients by electron holography. • Separation of elastic and inelastic attenuation coefficients (mean free path length). • Quantitative determination of the objective aperture semi-angle influence. • Compilation of elastic and inelastic attenuation from different materials.

The Harwell back-scattering spectrometer

International Nuclear Information System (INIS)

Windsor, C.G.; Bunce, L.J.; Borcherds, P.H.; Cole, I.; Fitzmaurice, M.; Johnson, D.A.G.; Sinclair, R.N.

1976-01-01

Neutron diffraction spectra in which both high resolution (Δ Q/Q approximately equal to 0.003) and high intensity are maintained up to scattering vectors as high as 30A -1 (sin theta/lambda = 2.5) have been obtained with the back-scattering spectrometer (BSS) recently installed on the Harwell electron linac. The theory behind the spectrometer design is described, and it is shown how the above resolution requirement leads to its basic features of a 12m incident flight path, a 2m scattering flight path and a scattering angle (2theta) acceptance from 165 0 to 175 0 . Examples of the resolution, intensity and background are given. It is shown that the problem of frame overlap may be overcome by using an absorbing filter. (author)

User expectations for multibeam echo sounders backscatter strength data-looking back into the future

Science.gov (United States)

Lucieer, Vanessa; Roche, Marc; Degrendele, Koen; Malik, Mashkoor; Dolan, Margaret; Lamarche, Geoffroy

2018-06-01

With the ability of multibeam echo sounders (MBES) to measure backscatter strength (BS) as a function of true angle of insonification across the seafloor, came a new recognition of the potential of backscatter measurements to remotely characterize the properties of the seafloor. Advances in transducer design, digital electronics, signal processing capabilities, navigation, and graphic display devices, have improved the resolution and particularly the dynamic range available to sonar and processing software manufacturers. Alongside these improvements the expectations of what the data can deliver has also grown. In this paper, we identify these user-expectations and explore how MBES backscatter is utilized by different communities involved in marine seabed research at present, and the aspirations that these communities have for the data in the future. The results presented here are based on a user survey conducted by the GeoHab (Marine Geological and Biological Habitat Mapping) association. This paper summarises the different processing procedures employed to extract useful information from MBES backscatter data and the various intentions for which the user community collect the data. We show how a range of backscatter output products are generated from the different processing procedures, and how these results are taken up by different scientific disciplines, and also identify common constraints in handling MBES BS data. Finally, we outline our expectations for the future of this unique and important data source for seafloor mapping and characterisation.

The Use of Backscattered Electron Imaging and Transmission Electron Microscopy to Assess Bone Architecture and Mineral Loci: Effect of Intermittent Slow-Release Sodium Fluoride Therapy

Science.gov (United States)

Zerwekh, Joseph E.; Bellotto, Dennis; Prostak, Kenneth S.; Hagler, Herbert K.; Pak, Charles Y. C.

1996-04-01

Backscattered electron imaging (BEI) and transmission electron microscopy (TEM) were used to examine the effects of treatment with intermittent slow-release sodium fluoride (SRNaF) and continuous calcium citrate on bone architecture and crystallinity. Examination was performed in nondecalcified biopsies obtained from patients following up to four years of therapy (placebo or SRNaF) and compared to pretreatment biopsies from each patient, as well as to bone from young, normal subjects. BEI images disclosed increased areas of recent bone formation following fluoride administration. There was no evidence of a mineralization defect in any biopsy and both cortical and trabecular architecture remained normal. TEM analysis demonstrated intrafibrillar platelike crystals and extrafibrillar needlelike crystals for both the pre- and post-treatment biopsies as well as for the bone from young normal subjects. There was no evidence of increased crystal size or of an increase in extrafibrillar mineral deposition. These observations suggest that intermittent SRNaF and continuous calcium therapy exerts an anabolic action on the skeleton not accompanied by a mineralization defect or an alteration of bone mineral deposition. The use of BEI and TEM holds promise for the study of the pathophysiology and treatment of metabolic bone diseases.

Quantitative autoradiography - a method of radioactivity measurement

International Nuclear Information System (INIS)

Treutler, H.C.; Freyer, K.

1988-01-01

In the last years the autoradiography has been developed to a quantitative method of radioactivity measurement. Operating techniques of quantitative autoradiography are demonstrated using special standard objects. Influences of irradiation quality, of backscattering in sample and detector materials, and of sensitivity and fading of the detectors are considered. Furthermore, questions of quantitative evaluation of autoradiograms are dealt with, and measuring errors are discussed. Finally, some practical uses of quantitative autoradiography are demonstrated by means of the estimation of activity distribution in radioactive foil samples. (author)

Quantitative study of magnetic field distribution by electron holography and micromagnetic simulations

International Nuclear Information System (INIS)

Beleggia, M.; Schofield, M.A.; Zhu, Y.; Malac, M.; Liu, Z.; Freeman, M.

2003-01-01

The magnetic configuration of a submicrometer Ni 88 Fe 12 permalloy island has been quantitatively mapped by off-axis electron holography. The two main contributions to the electron-optical phase shift, namely the phase shifts induced by the electrostatic and magnetic potentials, including fringing fields, were separated by inverting the specimen of 180 deg. with respect to the electron beam and directly measuring the mean inner potential. A quantitative map of the projected magnetic induction in the sample was thereby retrieved and compared to results of micromagnetic and electromagnetic calculations, providing the minimum-energy configuration and the phase shift, respectively

Transition to turbulence via spatiotemporal intermittency in stimulated Raman backscattering

International Nuclear Information System (INIS)

Skoric, M.M.; Jovanovic, M.S.; Rajkovic, M.R.

1996-01-01

The spatiotemporal evolution of stimulated Raman backscattering in a bounded, uniform, weakly dissipative plasma is studied. The nonlinear model of a three-wave interaction involves a quadratic coupling of slowly varying complex amplitudes of the laser pump, the backscattered and the electron plasma wave. The corresponding set of coupled partial differential equations with nonlinear phase detuning that is taken into account is solved numerically in space time with fixed nonzero source boundary conditions. The study of the above open, convective, weakly confined system reveals a quasiperiodic transition to spatiotemporal chaos via spatiotemporal intermittency. In the analysis of transitions a dual scheme borrowed from fields of nonlinear dynamics and statistical physics is applied. An introduction of a nonlinear three-wave interaction to a growing family of paradigmatic equations which exhibit a route to turbulence via spatiotemporal intermittency is outlined in this work. copyright 1996 The American Physical Society

Measurement of back-scattered radiation from micro multileaf collimator into the beam monitor chamber from a dual energy linear accelerator

Directory of Open Access Journals (Sweden)

Muralidhar K

2007-01-01

Full Text Available Measurements designed to find the collimator backscatter into the beam monitor chamber from Micro Multileaf collimator of 6 MV photon beams of the Siemens Primus linear accelerator were made with the help of dose rate feedback control. The photons and electrons backscattered from the upper and lower secondary collimator jaws give rise to a significant increase in the ion charge measured by monitor chamber. This increase varies between the different accelerators. The output measurements were carried out in air at the isocenter. The effect of collimator backscatter was investigated by measuring the pulse width, number of beam pulses per monitor unit, monitor unit rate and dose for different mMLC openings. These measurements were made with and without dose rate feedback control, i.e., with constant electron beam current in the accelerator. Monitor unit rate (MU/min was almost constant for all field sizes. The maximum variation between the open and the closed feedback control circuits was 2.5%. There was no difference in pulse width and negligible difference in pulse frequency. Maximum value of backscattered radiation from the micro Multileaf collimator into the beam monitor chamber was found to be 0.5%.

Quantitative energy-dispersive electron probe X-ray microanalysis ...

Indian Academy of Sciences (India)

Abstract. An energy-dispersive electron probe X-ray microanalysis (ED-EPMA) technique us- ing an energy-dispersive X-ray detector with an ultra-thin window, designated as low-Z particle. EPMA, has been developed. The low-Z particle EPMA allows the quantitative determination of concentrations of low-Z elements such ...

Quasimonochromatic x-rays generated from nonlinear Thomson backscattering

International Nuclear Information System (INIS)

Lan Pengfei; Lu Peixiang; Cao Wei; Wang Xinlin

2007-01-01

The nonlinear Thomson backscattering in a circularly polarized Gaussian laser pulse is investigated and spectral characteristics of the emission are discussed. It is indicated that the frequency of the emitted light is up-shifted by the nonlinear doppler effect. By using a properly focused laser beam or putting the electron before the focus, the variety of the nonlinear Doppler shift during the interaction can be minimized and quasimonochromatic x-rays are generated. Taking into account the emission power, the optimum situations for generating quasimonochromatic x-rays are explored

On one peculiarity of the model describing the interaction of the electron beam with the semiconductor surface

Science.gov (United States)

Stepovich, M. A.; Amrastanov, A. N.; Seregina, E. V.; Filippov, M. N.

2018-01-01

The problem of heat distribution in semiconductor materials irradiated with sharply focused electron beams in the absence of heat exchange between the target and the external medium is considered by mathematical modeling methods. For a quantitative description of energy losses by probe electrons a model based on a separate description of the contributions of absorbed in the target and backscattered electrons and applicable to a wide class of solids and a range of primary electron energies is used. Using the features of this approach, the nonmonotonic dependence of the temperature of the maximum heating in the target on the energy of the primary electrons is explained. Some modeling results are illustrated for semiconductor materials of electronic engineering.

Relating P-band AIRSAR backscatter to forest stand parameters

Science.gov (United States)

Wang, Yong; Melack, John M.; Davis, Frank W.; Kasischke, Eric S.; Christensen, Norman L., Jr.

1993-01-01

As part of research on forest ecosystems, the Jet Propulsion Laboratory (JPL) and collaborating research teams have conducted multi-season airborne synthetic aperture radar (AIRSAR) experiments in three forest ecosystems including temperate pine forest (Duke, Forest, North Carolina), boreal forest (Bonanza Creek Experimental Forest, Alaska), and northern mixed hardwood-conifer forest (Michigan Biological Station, Michigan). The major research goals were to improve understanding of the relationships between radar backscatter and phenological variables (e.g. stand density, tree size, etc.), to improve radar backscatter models of tree canopy properties, and to develop a radar-based scheme for monitoring forest phenological changes. In September 1989, AIRSAR backscatter data were acquired over the Duke Forest. As the aboveground biomass of the loblolly pine forest stands at Duke Forest increased, the SAR backscatter at C-, L-, and P-bands increased and saturated at different biomass levels for the C-band, L-band, and P-band data. We only use the P-band backscatter data and ground measurements here to study the relationships between the backscatter and stand density, the backscatter and mean trunk dbh (diameter at breast height) of trees in the stands, and the backscatter and stand basal area.

Very high latitude F-region irregularities observed by HF-radar backscatter

International Nuclear Information System (INIS)

Baker, K.B.; Greenwald, R.A.; Tsunoda, R.T.

1983-01-01

In February and March, 1982, a coherent scatter HF radar was operated from Cleary, Alaska to observe 7- to 15-m wavelength F-region plasma irregularities near the poleward edge of the auroral zone and in the polar cap. The radar operated for five days from February 25 to March 1 and produced approximately 700,000 Doppler spectra during that time. Of those nearly 700,000 spectra, approximately 10% showed backscattered power 3 dB or more above the noise level. A ray tracing technique using electron densities determined by the Chatanika incoherent scatter radar was used to predict locations where the HF waves were approximately normal to the magnetic field. If those locations were also to contain small scale electron density structure, then one would expect them to backscatter the HF waves. Several comparisons were made between predicted and observed locations of radiowave backscatter and excellent agreement was obtained. In addition, comparisons of the Doppler velocities observed by the coherent scatter HF radar and those observed by the Chatanika radar showed good agreement, suggesting that the plasma irregularities observed by the HF radar drift with the ambient plasma. In addition, average vector velocities calculated for the entire 5-day period show a flow pattern consistent with polar cap convection models. This again indicates that the irregularities drift with the plasma, as is predicted by a number of theories of F-region plasma irregularities. In the summer of 1983, the research program begun with those measurements will be continued with a steerable phased-array HF radar located at Goose Bay, Labrador, that will view the same ionospheric region as does the Sondre Stromfjord incoherent scatter radar

Seafloor multibeam backscatter calibration experiment: comparing 45°-tilted 38-kHz split-beam echosounder and 30-kHz multibeam data

Science.gov (United States)

Ladroit, Yoann; Lamarche, Geoffroy; Pallentin, Arne

2018-06-01

Obtaining absolute seafloor backscatter measurements from hydrographic multibeam echosounders is yet to be achieved. We propose a low-cost experiment to calibrate the various acquisition modes of a 30-kHz Kongsberg EM 302 multibeam echosounder in a range of water depths. We use a 38-kHz Simrad EK60 calibrated fisheries split-beam echosounder mounted at 45° angle on the vessel's hull as a reference for the calibration. The processing to extract seafloor backscatter from the EK60 requires bottom detection, ray tracing and motion compensation to obtain acceptable geo-referenced backscatter measurements from this non-hydrographic system. Our experiment was run in Cook Strait, New Zealand, on well-known seafloor patches in shallow, mid, and deep-water depths. Despite acquisition issues due to weather, our results demonstrate the strong potential of such an approach to obtain system's absolute calibration which is required for quantitative use of backscatter strength data.

A laser driven pulsed X-ray backscatter technique for enhanced penetrative imaging.

Science.gov (United States)

Deas, R M; Wilson, L A; Rusby, D; Alejo, A; Allott, R; Black, P P; Black, S E; Borghesi, M; Brenner, C M; Bryant, J; Clarke, R J; Collier, J C; Edwards, B; Foster, P; Greenhalgh, J; Hernandez-Gomez, C; Kar, S; Lockley, D; Moss, R M; Najmudin, Z; Pattathil, R; Symes, D; Whittle, M D; Wood, J C; McKenna, P; Neely, D

2015-01-01

X-ray backscatter imaging can be used for a wide range of imaging applications, in particular for industrial inspection and portal security. Currently, the application of this imaging technique to the detection of landmines is limited due to the surrounding sand or soil strongly attenuating the 10s to 100s of keV X-rays required for backscatter imaging. Here, we introduce a new approach involving a 140 MeV short-pulse (< 100 fs) electron beam generated by laser wakefield acceleration to probe the sample, which produces Bremsstrahlung X-rays within the sample enabling greater depths to be imaged. A variety of detector and scintillator configurations are examined, with the best time response seen from an absorptive coated BaF2 scintillator with a bandpass filter to remove the slow scintillation emission components. An X-ray backscatter image of an array of different density and atomic number items is demonstrated. The use of a compact laser wakefield accelerator to generate the electron source, combined with the rapid development of more compact, efficient and higher repetition rate high power laser systems will make this system feasible for applications in the field. Content includes material subject to Dstl (c) Crown copyright (2014). Licensed under the terms of the Open Government Licence except where otherwise stated. To view this licence, visit http://www.nationalarchives.gov.uk/doc/open-government-licence/version/3 or write to the Information Policy Team, The National Archives, Kew, London TW9 4DU, or email: psi@ nationalarchives.gsi.gov.uk.

Concept and realization of the A4 Compton backscattering polarimeter at MAMI

Energy Technology Data Exchange (ETDEWEB)

Lee, Jeong Han

2008-12-15

The main concern of the A4 parity violation experiment at the Mainzer Microtron accelerator facility is to study the electric and magnetic contributions of strange quarks to the charge and magnetism of the nucleons at the low momentum transfer region. More precisely, the A4 collaboration investigates the strange quarks' contribution to the electric and magnetic vector form factors of the nucleons. Thus, it is important that the A4 experiment uses an adequate and precise non-destructive online monitoring tool for the electron beam polarization when measuring single spin asymmetries in elastic scattering of polarized electrons from unpolarized nucleons. As a consequence, the A4 Compton backscattering polarimeter was designed and installed such that we can take the absolute measurement of the electron beam polarization without interruption to the parity violation experiment. The present study shows the development of an electron beam line that is called the chicane for the A4 Compton backscattering polarimeter. The chicane is an electron beam transport line and provides an interaction region where the electron beam and the laser beam overlap. After studying the properties of beam line components carefully, we developed an electron beam control system that makes a beam overlap between the electron beam and the laser beam. Using the system, we can easily achieve the beam overlap in a short time. The electron control system, of which the performance is outstanding, is being used in production beam times. And the study presents the development of a scintillating fiber electron detector that reduces the statistical error in the electron polarization measurement. We totally redesigned the scintillating fiber detector. The data that were taken during a 2008 beam time shows a huge background suppression, approximately 80 percent, while leaving the Compton spectra almost unchanged when a coincidence between the fiber detector and the photon detector is used. Thus, the

Determination of the analyzing power of the A4 Compton-backscattering polarimeter for the measurement of the longitudinal spin polarization of the MAMI electron beam; Bestimmung der Analysierstaerke des A4-Compton-Rueckstreupolarimeters zur Messung der longitudinalen Spinpolarisation des MAMI-Elektronenstrahls

Energy Technology Data Exchange (ETDEWEB)

Diefenbacher, Juergen

2010-08-22

The A4 experiment determines the strange quark contribution to the electromagnetic from factors of the nucleon by measuring the parity violation in elastic electron nucleon scattering. These measurements are carried out using the spin polarized electron beam of the Mainzer Mikrotron (MAMI) with beam energies in the range from 315 to 1508 MeV. For the data analysis it is essential to determine the degree of polarization of the electron beam in order to extract the physics asymmetry from the measured parity violating asymmetry. For this reason the A4 collaboration has developed a novel type of Compton laser backscattering polarimeter that allows for a non-destructive measurement of the beam polarization in parallel to the running parity experiment. In the scope of this work the polarimeter was refined in order to enable reliable continuous operation of the polarimeter. The data acquisition system for the photon and electron detector was re-designed and optimized to cope with high count rates. A novel detector (LYSO) for the backscattered photons was commissioned. Furthermore, GEANT4 simulations of the detectors have been performed and an analysis environment for the extraction of Compton asymmetries from the backscattered photon data has been developed. The analysis makes use of the possibility to detect backscattered photons in coincidence with the scattered electrons, thus tagging the photons. The tagging introduces a differential energy scale which enables the precise determination of the analyzing power. In this work the analyzing power of the polarimeter has been determined. Therefore, at a beam current of 20 {mu}A the product of electron and laser polarization can be determined, while the parity experiment is running, with a statistical accuracy of 1 % in 24 hours at 855 MeV or <1 % in 12 hours at 1508 MeV. Combining this with the determination of the laser polarization carried out in parallel work (Y. Imai), the uncertainty of the electron beam polarization in

Quantitative methods for the analysis of electron microscope images

DEFF Research Database (Denmark)

Skands, Peter Ulrik Vallø

1996-01-01

The topic of this thesis is an general introduction to quantitative methods for the analysis of digital microscope images. The images presented are primarily been acquired from Scanning Electron Microscopes (SEM) and interfermeter microscopes (IFM). The topic is approached though several examples...... foundation of the thesis fall in the areas of: 1) Mathematical Morphology; 2) Distance transforms and applications; and 3) Fractal geometry. Image analysis opens in general the possibility of a quantitative and statistical well founded measurement of digital microscope images. Herein lies also the conditions...

Stimulated Raman backscattering at high laser intensities

Energy Technology Data Exchange (ETDEWEB)

Skoric, M M [Vinca Inst. of Nuclear Sciences, Belgrade (Yugoslavia); Tajima, Toshiki; Sasaki, Akira; Maluckov, A; Jovanovic, M

1998-03-01

Signatures of Stimulated Raman backscattering of a short-pulse high-intensity laser interacting with an underdense plasma are discussed. We introduce a nonlinear three-wave interaction model that accounts for laser pump depletion and relativistic detuning. A mechanism is revealed based on a generic route to chaos, that predicts a progressive increase of the backscatter complexity with a growing laser intensity. Importance of kinetic effects is outlined and demonstrated in fluid-hybrid and particle simulations. As an application, we show that spectral anomalies of the backscatter, predicted by the above model, are consistent with recent sub-picosecond, high-intensity laser gas-target measurements at Livermore and elsewhere. Finally, a recently proposed scheme for generation of ultra-short, low-prepulse laser pulses by Raman backscattering in a thin foil target, is shown. (author)

Understanding the radar backscattering from flooded and nonflooded Amazonian forests: results from canopy backscatter modeling

International Nuclear Information System (INIS)

Wang, Y.; Hess, L.L.; Filoso, S.; Melack, J.M.

1995-01-01

To understand the potential of using multiwavelength imaging radars to detect flooding in Amazonian floodplain forests, we simulated the radar backscatter from a floodplain forest with a flooded or nonflooded ground condition at C-, L-, and P-bands. Field measurements of forest structure in the Anavilhanas archipelago of the Negro River, Brazil, were used as inputs to the model. Given the same wavelength or incidence angle, the ratio of backscatter from the flooded forest to that from the nonflooded forest was higher at HH polarization than at VV polarization. Given the same wavelength or polarization, the ratio was larger at small incidence angles than at large incidence angles. Given the same polarization or incidence angle, the ratio was larger at a long wavelength than at a short wavelength. As the surface soil moisture underneath the nonflooded forest increased from 10% to 50% of volumetric moisture, the flooded/nonflooded backscatter ratio decreased; the decreases were small at C- and L-band but large at P-band. When the leaf size was comparable to or larger than the wavelength of C-band, the leaf area index (LAI) had a large effect on the simulated C-band (not L-band or P-band) backscatter from the flooded and nonflooded forests. (author)

Nodule bottom backscattering study using multibeam echosounder

Digital Repository Service at National Institute of Oceanography (India)

Chakraborty, B.; Raju, Y.S.N.; Nair, R.R.

A study is carried out to observe the angular dependence of backscattering strength at nodule area where grab sample and photographic data is available. Theoretical study along with the experimentally observed data shows that the backscattering...

An Ultrasonic Backscatter Instrument for Cancellous Bone Evaluation in Neonates

Directory of Open Access Journals (Sweden)

Chengcheng Liu

2015-09-01

Full Text Available Ultrasonic backscatter technique has shown promise as a noninvasive cancellous bone assessment tool. A novel ultrasonic backscatter bone diagnostic (UBBD instrument and an in vivo application for neonatal bone evaluation are introduced in this study. The UBBD provides several advantages, including noninvasiveness, non-ionizing radiation, portability, and simplicity. In this study, the backscatter signal could be measured within 5 s using the UBBD. Ultrasonic backscatter measurements were performed on 467 neonates (268 males and 199 females at the left calcaneus. The backscatter signal was measured at a central frequency of 3.5 MHz. The delay (T1 and duration (T2 of the backscatter signal of interest (SOI were varied, and the apparent integrated backscatter (AIB, frequency slope of apparent backscatter (FSAB, zero frequency intercept of apparent backscatter (FIAB, and spectral centroid shift (SCS were calculated. The results showed that the SOI selection had a direct influence on cancellous bone evaluation. The AIB and FIAB were positively correlated with the gestational age (|R| up to 0.45, P10 µs. Moderate positive correlations (|R| up to 0.45, P10 µs. The T2 mainly introduced fluctuations in the observed correlation coefficients. The moderate correlations observed with UBBD demonstrate the feasibility of using the backscatter signal to evaluate neonatal bone status. This study also proposes an explicit standard for in vivo SOI selection and neonatal cancellous bone assessment.

A study on the secondary electrons in a clinical electron beam

International Nuclear Information System (INIS)

Krithivas, G.; Rao, S.N.

1989-01-01

The central axis dose of a 12 MeV clinical electron beam is investigated in terms of an axial component due to primary electrons in the central ray and a lateral component due to secondary electrons originating from multiple scattering of electrons in the off-axis rays. To this effect secondary electron fluence measurements in a polystyrene medium irradiated with a collimated beam are made with a sensitive diode detector. This leads to a construction of secondary electron depth-dose profiles for beam sizes of diameters ranging from 1.7 to 17.4 cm. The results indicate that the lateral electrons account for 25% of the dose in the therapeutic region. For these electrons, the depth of dose maximum is correlated with diffusion depth and maximum lateral excursion in the medium. Dose component due to backscatter electrons at depths is also investigated using a thin-window parallel-plate ion chamber. The role of lateral and backscatter electrons in characterising central axis per cent depth-dose is discussed. (author)

3D Backscatter Imaging System

Science.gov (United States)

Whitaker, Ross (Inventor); Turner, D. Clark (Inventor)

2016-01-01

Systems and methods for imaging an object using backscattered radiation are described. The imaging system comprises both a radiation source for irradiating an object that is rotationally movable about the object, and a detector for detecting backscattered radiation from the object that can be disposed on substantially the same side of the object as the source and which can be rotationally movable about the object. The detector can be separated into multiple detector segments with each segment having a single line of sight projection through the object and so detects radiation along that line of sight. Thus, each detector segment can isolate the desired component of the backscattered radiation. By moving independently of each other about the object, the source and detector can collect multiple images of the object at different angles of rotation and generate a three dimensional reconstruction of the object. Other embodiments are described.

Comparison of Ultrasound Attenuation and Backscatter Estimates in Layered Tissue-Mimicking Phantoms among Three Clinical Scanners

Science.gov (United States)

Nam, Kibo; Rosado-Mendez, Ivan M.; Wirtzfeld, Lauren A.; Ghoshal, Goutam; Pawlicki, Alexander D.; Madsen, Ernest L.; Lavarello, Roberto J.; Oelze, Michael L.; Zagzebski, James A.; O’Brien, William D.; Hall, Timothy J.

2013-01-01

Backscatter and attenuation coefficient estimates are needed in many quantitative ultrasound strategies. In clinical applications, these parameters may not be easily obtained because of variations in scattering by tissues overlying a region of interest (ROI). The goal of this study is to assess the accuracy of backscatter and attenuation estimates for regions distal to nonuniform layers of tissue-mimicking materials. In addition, this work compares results of these estimates for “layered” phantoms scanned using different clinical ultrasound machines. Two tissue-mimicking phantoms were constructed, each exhibiting depth-dependent variations in attenuation or backscatter. The phantoms were scanned with three ultrasound imaging systems, acquiring radio frequency echo data for offline analysis. The attenuation coefficient and the backscatter coefficient (BSC) for sections of the phantoms were estimated using the reference phantom method. Properties of each layer were also measured with laboratory techniques on test samples manufactured during the construction of the phantom. Estimates of the attenuation coefficient versus frequency slope, α0, using backscatter data from the different systems agreed to within 0.24 dB/cm-MHz. Bias in the α0 estimates varied with the location of the ROI. BSC estimates for phantom sections whose locations ranged from 0 to 7 cm from the transducer agreed among the different systems and with theoretical predictions, with a mean bias error of 1.01 dB over the used bandwidths. This study demonstrates that attenuation and BSCs can be accurately estimated in layered inhomogeneous media using pulse-echo data from clinical imaging systems. PMID:23160474

Vibrational and electronic excitation of hexatriacontane thin films by low energy electron impact

International Nuclear Information System (INIS)

Vilar, M.R.; Schott, M.; Pfluger, P.

1990-01-01

Thin polycrystalline films of hexatriacontane (HTC) were irradiated with low energy (E=0.5--15 eV) electrons, and off-specular backscattered electron spectra were measured. Below E∼7 eV, single and multiple vibrational excitations only are observed, which relax the electrons down to the bottom of the HTC conduction band. Due to the negative electron affinity of HTC, thermal electrons are emitted into vacuum. Structure in the backscattered electron current at kinetic energies about 1.5 and 4 eV are associated to conduction band density of states. Above E∼7 eV, the dominant losses correspond to electronic excitations, excitons, or above a threshold (energy of the electron inside the HTC film) at 9.2±0.1 eV, electron--hole pair generation. The latter process is very efficient and reaches a yield of the order of one ∼11 eV. Evidence for chemical reaction above E∼4 eV is observed

X-ray backscatter imaging with a spiral scanner

International Nuclear Information System (INIS)

Bossi, R.H.; Cline, J.L.; Friddell, K.D.

1989-01-01

X-ray backscatter imaging allows radiographic inspections to be performed with access to only one side of the object. A collimated beam of radiation striking an object will scatter x-rays by Compton scatter and x-ray fluorescence. A detector located on the source side of the part will measure the backscatter signal. By plotting signal strength as gray scale intensity vs. beam position on the object, an image of the object can be constructed. A novel approach to the motion of the collimated incident beam is a spiral scanner. The spiral scanner approach, described in this paper, can image an area of an object without the synchronized motion of the object or detector, required by other backscatter imaging techniques. X-ray backscatter is particularly useful for flaw detection in light element materials such as composites. The ease of operation and the ability to operate non-contact from one side of an object make x-ray backscatter imaging of increasing interest to industrial inspection problems

On line ultrasonic integrated backscatter

International Nuclear Information System (INIS)

Landini, L.; Picano, E.; Mazzarisi, A.; Santarelli, F.; Benassi, A.; De Pieri, G.

1988-01-01

A new equipment for on-line evaluation of index based on two-dimensional integrated backscatter from ultrasonic images is described. The new equipment is fully integrated into a B-mode ultrasonic apparatus which provides a simultaneous display of conventional information together with parameters of tissue characterization. The system has been tested with a backscattering model of microbubbles in polysaccharide solution, characterized by a physiological exponential time decay. An exponential fitting to the experimental data was performed which yielded r=0.95

Backscattering at a pulsed neutron source, the MUSICAL instrument

International Nuclear Information System (INIS)

Alefeld, B.

1995-01-01

In the first part the principles of the neutron backscattering method are described and some simple considerations about the energy resolution and the intensity are presented. A prototype of a backscattering instrument, the first Juelich instrument, is explained in some detail and a representative measurement is shown which was performed on the backscattering instrument IN10 at the ILL in Grenoble. In the second part a backscattering instrument designed for a pulsed neutron source is proposed. It is shown that a rather simple modification, which consists in the replacement of the Doppler drive of the conventional backscattering instrument by a multi silicon monochromator crystal (MUSICAL) leads to a very effective instrument, benefitting from the peak flux of the pulsed source. ((orig.))

Super-virtual Interferometric Separation and Enhancement of Back-scattered Surface Waves

KAUST Repository

Guo, Bowen

2015-08-19

Back-scattered surface waves can be migrated to detect near-surface reflectors with steep dips. A robust surface-wave migration requires the prior separation of the back-scattered surface-wave events from the data. This separation is often difficult to implement because the back-scattered surface waves are masked by the incident surface waves. We mitigate this problem by using a super-virtual interferometric method to enhance and separate the back-scattered surface waves. The key idea is to calculate the virtual back-scattered surface waves by stacking the resulting virtual correlated and convolved traces associated with the incident and back-scattered waves. Stacking the virtual back-scattered surface waves improves their signal-to-noise ratio and separates the back-scattered surface-waves from the incident field. Both synthetic and field data results validate the robustness of this method.

Backscattering of projectile-bound electrons from solid surfaces

International Nuclear Information System (INIS)

Tobisch, M.; Schosnig, M.; Kroneberger, K.; Kuzel, M.; Maier, R.; Jung, M.; Fiedler, C.; Rothard, H.; Clouvas, A.; Suarez, S.; Groeneveld, K.O.

1994-01-01

The contribution of projectile ionization (PI) to secondary electron emission is studied by collision of H 2 + and H 3 + ions (400 keV/u and 700 keV/u) with carbon, copper and gold targets (600 A). The measured doubly differential intensity distribution shows a peak of lost projectile electrons near - v p . We describe the subtraction of the contribution of target ionization (TI), and compare the remaining electron intensities with a BEA calculation. For solids we observe a strong energy shift of the electron loss peak, which is compared with the influence of electron transport and binding energy. Furthermore, the low energy tail of the electron loss peak indicates the simultaneous occurrence of PI and TI. Finally we discuss the influence of surface conditions and the dependence of the observation angles on the measured electron intensities. (orig.)

Effect of Welding Heat Input on Microstructure and Texture of Inconel 625 Weld Overlay Studied Using the Electron Backscatter Diffraction Method

Science.gov (United States)

Kim, Joon-Suk; Lee, Hae-Woo

2016-12-01

The grain size and the texture of three specimens prepared at different heat inputs were determined using optical microscopy and the electron backscatter diffraction method of scanning electron microscopy. Each specimen was equally divided into fusion line zone (FLZ), columnar dendrite zone (CDZ), and surface zone (SZ), according to the location of the weld. Fine dendrites were observed in the FLZ, coarse dendrites in the CDZ, and dendrites grew perpendicular to the FLZ and CDZ. As the heat input increased, the melted zone in the vicinity of the FLZ widened due to the higher Fe content. A lower image quality value was observed for the FLZ compared to the other zones. The results of grain size measurement in each zone showed that the grain size of the SZ became larger as the heat input increased. From the inverse pole figure (IPF) map in the normal direction (ND) and the rolling direction (RD), as the heat input increased, a specific orientation was formed. However, a dominant [001] direction was observed in the RD IPF map.

Quantitative in situ magnetization reversal studies in Lorentz microscopy and electron holography

International Nuclear Information System (INIS)

Rodríguez, L.A.; Magén, C.; Snoeck, E.; Gatel, C.; Marín, L.; Serrano-Ramón, L.

2013-01-01

A generalized procedure for the in situ application of magnetic fields by means of the excitation of the objective lens for magnetic imaging experiments in Lorentz microscopy and electron holography is quantitatively described. A protocol for applying magnetic fields with arbitrary in-plane magnitude and orientation is presented, and a freeware script for Digital Micrograph ™ is provided to assist the operation of the microscope. Moreover, a method to accurately reconstruct hysteresis loops is detailed. We show that the out-of-plane component of the magnetic field cannot be always neglected when performing quantitative measurements of the local magnetization. Several examples are shown to demonstrate the accuracy and functionality of the methods. - Highlights: • Generalized procedure for application of magnetic fields with the TEM objective lens. • Arbitrary in-plane magnetic field magnitude and orientation can be applied. • Method to accurately reconstruct hysteresis loops by electron holography. • Out-of-plane field component should be considered in quantitative measurements. • Examples to illustrate the method in Lorentz microscopy and electron holography

Characteristics of Si-PIN diode X-ray detector with DSP electronics

International Nuclear Information System (INIS)

Dutta, Juhi; Tapader, Srijita; Bisoi, Abhijit; Ray, Sudatta; Saha Sarkar, M.; Pramanik, Dibyadyuti; Saha, Archisman

2012-01-01

In the present work, the studies to investigate the features of PIN diodes detector coupled with a digital processor have been extended. At low energies, backscattered Compton peaks are close in energy to photo peak of the gamma of interest. Thus the backscattered peaks pose a serious problem in the analysis of spectra of low energy gamma rays. It has been initiated some measurements to quantitatively estimate the same as function of energy and Z of the scatterer. Recently there has been application of backscattering in high-resolution gamma backscatter imaging for technical applications

Staining plastic blocks with triiodide to image cells and soft tissues in backscattered electron SEM of skeletal and dental tissues

Directory of Open Access Journals (Sweden)

A Boyde

2012-07-01

Full Text Available Backscattered electron scanning electron microscopy (BSE SEM is an invaluable method for studying the histology of the hard, mineralised components of poly-methyl methacrylate (PMMA or other resin embedded skeletal and dental tissues. Intact tissues are studied in micro-milled or polished block faces with an electron-optical section thickness of the order of a half to one micron and with the area of the section as big as a whole – large or small – bone organ. However, BSE SEM does not give information concerning the distribution of uncalcified, ‘soft’, cellular and extracellular matrix components. This can be obtained by confocal microscopy of the same block and the two sorts of images merged but the blocks have to be studied in two microscope systems. The present work shows a new, simple and economic approach to visualising both components by using the triiodide ion in Lugol's iodine solution to stain the block surface prior to the application of any conductive coating – and the latter can be omitted if charging is suppressed by use of poor vacuum conditions in the SEM sample chamber. The method permits the use of archival tissue, and it will be valuable in studies of both normal growth and development and pathological changes in bones and joints, including osteoporosis and osteoarthritis, and tissue adaptation to implants.

High-energy gamma-ray beams from Compton-backscattered laser light

International Nuclear Information System (INIS)

Sandorfi, A.M.; LeVine, M.J.; Thorn, C.E.; Giordano, G.; Matone, G.

1983-01-01

Collisions of light photons with relativistic electrons have previously been used to produce polarized #betta#-ray beams with modest (-10%) resolution but relatively low intensity. In contrast, the LEGS project (Laser + Electron Gamma Source) at Brookhaven will produce a very high flux (>2 x 10 7 s - 1 ) of background-free polarized #betta# rays whose energy will be determined to a high accuracy (δE = 2.3 MeV). Initially, 300(420)-MeV #betta# rays will be produced by backscattering uv light from the new 2.5(3.0)-GeV X-ray storage ring of the National Synchrotron Light Source (NSLS). The LEGS facility will operate as one of many passive users of the NSLS. In a later stage of the project, a Free Electron Laser is expectred to extend the #betta#-ray energy up to 700 MeV

High-energy gamma-ray beams from Compton-backscattered laser light

Energy Technology Data Exchange (ETDEWEB)

Sandorfi, A.M.; LeVine, M.J.; Thorn, C.E.; Giordano, G.; Matone, G.

1983-01-01

Collisions of light photons with relativistic electrons have previously been used to produce polarized ..gamma..-ray beams with modest (-10%) resolution but relatively low intensity. In contrast, the LEGS project (Laser + Electron Gamma Source) at Brookhaven will produce a very high flux (>2 x 10/sup 7/ s/sup -1/) of background-free polarized ..gamma.. rays whose energy will be determined to a high accuracy (..delta..E = 2.3 MeV). Initially, 300(420)-MeV ..gamma.. rays will be produced by backscattering uv light from the new 2.5(3.0)-GeV X-ray storage ring of the National Synchrotron Light Source (NSLS). The LEGS facility will operate as one of many passive users of the NSLS. In a later stage of the project, a Free Electron Laser is expectred to extend the ..gamma..-ray energy up to 700 MeV.

Estimating sub-surface dispersed oil concentration using acoustic backscatter response.

Science.gov (United States)

Fuller, Christopher B; Bonner, James S; Islam, Mohammad S; Page, Cheryl; Ojo, Temitope; Kirkey, William

2013-05-15

The recent Deepwater Horizon disaster resulted in a dispersed oil plume at an approximate depth of 1000 m. Several methods were used to characterize this plume with respect to concentration and spatial extent including surface supported sampling and autonomous underwater vehicles with in situ instrument payloads. Additionally, echo sounders were used to track the plume location, demonstrating the potential for remote detection using acoustic backscatter (ABS). This study evaluated use of an Acoustic Doppler Current Profiler (ADCP) to quantitatively detect oil-droplet suspensions from the ABS response in a controlled laboratory setting. Results from this study showed log-linear ABS responses to oil-droplet volume concentration. However, the inability to reproduce ABS response factors suggests the difficultly in developing meaningful calibration factors for quantitative field analysis. Evaluation of theoretical ABS intensity derived from the particle size distribution provided insight regarding method sensitivity in the presence of interfering ambient particles. Copyright © 2013 Elsevier Ltd. All rights reserved.

Evidence of a tropospheric aerosol backscatter background mode

Science.gov (United States)

Rothermel, Jeffry; Bowdle, David A.; Vaughan, J. Michael; Post, Madison J.

1989-01-01

Vertical profiles of atmospheric aerosol backscatter coefficients at 10.6 microns obtained with airborne and ground-based lidar are compared. Both sets of profiles show a high frequency of occurrence of low backscatter over a limited range of values in the middle and upper troposphere. It is suggested that this narrow range indicates a ubiquitous background mode for atmospheric backscatter around the globe. Implications of such a mode for global scale aerosol models and for the design of satellite-borne lidar-based sensors are discussed.

Preliminary backscatter results from the hydrosweep multibeam system

Digital Repository Service at National Institute of Oceanography (India)

Hagen, R.A.; Chakraborty, B.; Schenke, H.W.

of Oceanography to convert the measured electrical energy into acoustic backscatter energy. This conversion includes corrections for the position, slope, and area of the scattering surface. In this paper we present backscatter data from several areas surveyed...

A new standardless quantitative electron probe microanalysis technique applied to III-V compound semiconductors

International Nuclear Information System (INIS)

Zangalis, K.P.; Christou, A.

1982-01-01

The present paper introduces a new standardless quantitative scheme for off-line electron microprobe analysis applications. The analysis is based on standard equations of the type Isub(i)=Csub(i)fsub(ZAF)βsub(i) and is specifically suitable for compound semiconductors. The roots to the resultant nth-degree polynomial are the unknown concentrations. Methods for computing Csub(i) when coefficients βsub(i) are unknown are also outlined. Applications of standardless analysis to GaAs and InP specimens are compared with results obtained by Auger electron spectroscopy and quantitative electron probe analysis with standards. (Auth.)

Taking apart the enhanced backscattering cone: Interference fringes from reciprocal paths in multiple light scattering

International Nuclear Information System (INIS)

Bret, Boris P. J.; Ferreira, Flavio P.; Nunes-Pereira, Eduardo J.; Belsley, Michael

2010-01-01

We report the decomposition of the enhanced backscattering cone into its constitutive interference fringes. These fringes are due to the constructive interference between reciprocal paths of any multiply scattered wave after ensemble averaging. An optical setup combining a two-point continuous-wave illumination and matching detection allows the observation of the fringes and, therefore, the quantitative characterization of the Green's function for light propagation between the two points in a multiple-scattering media.

The effect of pattern overlap on the accuracy of high resolution electron backscatter diffraction measurements

Energy Technology Data Exchange (ETDEWEB)

Tong, Vivian, E-mail: v.tong13@imperial.ac.uk [Department of Materials, Imperial College London, Prince Consort Road, London SW7 2AZ (United Kingdom); Jiang, Jun [Department of Materials, Imperial College London, Prince Consort Road, London SW7 2AZ (United Kingdom); Wilkinson, Angus J. [Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH (United Kingdom); Britton, T. Ben [Department of Materials, Imperial College London, Prince Consort Road, London SW7 2AZ (United Kingdom)

2015-08-15

High resolution, cross-correlation-based, electron backscatter diffraction (EBSD) measures the variation of elastic strains and lattice rotations from a reference state. Regions near grain boundaries are often of interest but overlap of patterns from the two grains could reduce accuracy of the cross-correlation analysis. To explore this concern, patterns from the interior of two grains have been mixed to simulate the interaction volume crossing a grain boundary so that the effect on the accuracy of the cross correlation results can be tested. It was found that the accuracy of HR-EBSD strain measurements performed in a FEG-SEM on zirconium remains good until the incident beam is less than 18 nm from a grain boundary. A simulated microstructure was used to measure how often pattern overlap occurs at any given EBSD step size, and a simple relation was found linking the probability of overlap with step size. - Highlights: • Pattern overlap occurs at grain boundaries and reduces HR-EBSD accuracy. • A test is devised to measure the accuracy of HR-EBSD in the presence of overlap. • High pass filters can sometimes, but not generally, improve HR-EBSD measurements. • Accuracy of HR-EBSD remains high until the reference pattern intensity is <72%. • 9% of points near a grain boundary will have significant error for 200nm step size in Zircaloy-4.

An electron back-scattered diffraction study on the microstructure evolution of AZ31 Mg alloy during equal channel angular extrusion

International Nuclear Information System (INIS)

Jin Li; Lin Dongliang; Mao Dali; Zeng Xiaoqin; Ding Wenjiang

2006-01-01

Microstructure evolution of AZ31 Mg alloy during equal channel angular extrusion (ECAE) was investigated by electron back-scattered diffraction (EBSD). The grains of AZ31 Mg alloy were refined significantly after ECAE 1-8 passes at 498 K and the distributions of grain size tended to be more uniform with pass number increasing. Frequency of sub-boundaries and low angle grain boundaries (LAGBs) increased at initial stage of deformation, and sub-boundaries and LAGBs evolved into high angle grain boundaries (HAGBs) with further deformation, which resulted in the high frequency of HAGBs in the alloy after ECAE 8 passes. Preferred misorientation angle with frequency peak near 30 deg. and 90 deg. were observed. The frequency peaks were weak after ECAE 1 pass but became stronger with the increase of pass numbers. Micro-textures were formed in AZ31 microstructure during ECAE and were stronger with the pass number increasing

Compton Backscattering Concept for the Production of Molybdenum-99

International Nuclear Information System (INIS)

Merminga, L.; Krafft, G.A.

2009-01-01

The medical isotope Molybdenum-99 is presently used for 80-85% of all nuclear medicine procedures and is produced by irradiating highly enriched uranium U-235 targets in NRU reactors. It was recently proposed that an electron linac be used for the production of 99Mo via photo-fission of a natural uranium target coming from the excitation of the giant dipole resonance around 15 MeV. The photons can be produced using the braking radiation ('bremsstrahlung') spectrum of an electron beam impinged on a high Z material. In this paper we present an alternate concept for the production of 99Mo which is also based on photo-fission of U-238, but where the ∼15 MeV gamma-rays are produced by Compton backscattering of laser photons from relativistic electrons. We assume a laser wavelength of 330 nm, resulting in 485 MeV electron beam energy, and 10 mA of average current. Because the induced energy spread on the electron beam is a few percent, one may recover most of the electron beam energy, which substantially increases the efficiency of the system. The accelerator concept, based on a three-pass recirculation system with energy recovery, is described and efficiency estimates are presented.

Secondary signal imaging (SSI) electron tomography (SSI-ET): A new three-dimensional metrology for mesoscale specimens in transmission electron microscope.

Science.gov (United States)

Han, Chang Wan; Ortalan, Volkan

2015-09-01

We have demonstrated a new electron tomography technique utilizing the secondary signals (secondary electrons and backscattered electrons) for ultra thick (a few μm) specimens. The Monte Carlo electron scattering simulations reveal that the amount of backscattered electrons generated by 200 and 300keV incident electrons is a monotonic function of the sample thickness and this causes the thickness contrast satisfying the projection requirement for the tomographic reconstruction. Additional contribution of the secondary electrons emitted from the edges of the specimens enhances the visibility of the surface features. The acquired SSI tilt series of the specimen having mesoscopic dimensions are successfully reconstructed verifying that this new technique, so called the secondary signal imaging electron tomography (SSI-ET), can directly be utilized for 3D structural analysis of mesoscale structures. Published by Elsevier Ltd.

Comparisons between MCNP, EGS4 and experiment for clinical electron beams.

Science.gov (United States)

Jeraj, R; Keall, P J; Ostwald, P M

1999-03-01

Understanding the limitations of Monte Carlo codes is essential in order to avoid systematic errors in simulations, and to suggest further improvement of the codes. MCNP and EGS4, Monte Carlo codes commonly used in medical physics, were compared and evaluated against electron depth dose data and experimental backscatter results obtained using clinical radiotherapy beams. Different physical models and algorithms used in the codes give significantly different depth dose curves and electron backscattering factors. The default version of MCNP calculates electron depth dose curves which are too penetrating. The MCNP results agree better with experiment if the ITS-style energy-indexing algorithm is used. EGS4 underpredicts electron backscattering for high-Z materials. The results slightly improve if optimal PRESTA-I parameters are used. MCNP simulates backscattering well even for high-Z materials. To conclude the comparison, a timing study was performed. EGS4 is generally faster than MCNP and use of a large number of scoring voxels dramatically slows down the MCNP calculation. However, use of a large number of geometry voxels in MCNP only slightly affects the speed of the calculation.

Proton non-Rutherford backscattering study of oxidation kinetics in Cu and Fe sulphides

International Nuclear Information System (INIS)

Chiari, M.; Giuntini, L.; Pratesi, G.; Santo, A.P.

1998-01-01

Non-Rutherford backscattering spectrometry (NBS) with 2.4 MeV protons was performed for depth profiling of oxygen in three species of copper and iron sulphides - pyrite, chalcopyrite and bornite - on both altered and fresh surfaces. The tarnished surfaces were obtained by bathing samples in H 2 O 2 (35% vol.) for 100 and 1000 s. The spectra collected were compared to simulations to extract quantitative data on oxygen depth distributions for the different bathing times. The measurements have shown that the kinetics of oxidation has completely different patterns in the three investigated minerals. (orig.)

Effect of the cortex on ultrasonic backscatter measurements of cancellous bone

International Nuclear Information System (INIS)

Hoffmeister, Brent K; Holt, Andrew P; Kaste, Sue C

2011-01-01

Ultrasonic backscatter techniques offer a promising new approach for detecting changes in bone caused by osteoporosis. However, several challenges impede clinical implementation of backscatter techniques. This study examines how the dense outer surface of bone (the cortex) affects backscatter measurements of interior regions of porous (cancellous) bone tissue. Fifty-two specimens of bone were prepared from 13 human femoral heads so that the same region of cancellous bone could be ultrasonically interrogated through the cortex or along directions that avoided the cortex. Backscatter signals were analyzed over a frequency range of 0.8-3.0 MHz to determine two ultrasonic parameters: apparent integrated backscatter (AIB) and frequency slope of apparent backscatter (FSAB). The term 'apparent' means that the parameters are sensitive to the frequency-dependent effects of diffraction and attenuation. Significant (p < 0.001) changes in AIB and FSAB indicated that measurements through the cortex decreased the apparent backscattered power and increased the frequency dependence of the power. However, the cortex did not affect the correlation of AIB and FSAB with the x-ray bone mineral density of the specimens. This suggests that results from many previous in vitro backscatter studies of specimens of purely cancellous bone may be extrapolated with greater confidence to in vivo conditions.

Effect of the cortex on ultrasonic backscatter measurements of cancellous bone

Energy Technology Data Exchange (ETDEWEB)

Hoffmeister, Brent K; Holt, Andrew P [Department of Physics, Rhodes College, Memphis, TN (United States); Kaste, Sue C, E-mail: hoffmeister@rhodes.edu [Department of Diagnostic Imaging, St Jude Children' s Research Hospital, Memphis, TN (United States)

2011-10-07

Ultrasonic backscatter techniques offer a promising new approach for detecting changes in bone caused by osteoporosis. However, several challenges impede clinical implementation of backscatter techniques. This study examines how the dense outer surface of bone (the cortex) affects backscatter measurements of interior regions of porous (cancellous) bone tissue. Fifty-two specimens of bone were prepared from 13 human femoral heads so that the same region of cancellous bone could be ultrasonically interrogated through the cortex or along directions that avoided the cortex. Backscatter signals were analyzed over a frequency range of 0.8-3.0 MHz to determine two ultrasonic parameters: apparent integrated backscatter (AIB) and frequency slope of apparent backscatter (FSAB). The term 'apparent' means that the parameters are sensitive to the frequency-dependent effects of diffraction and attenuation. Significant (p < 0.001) changes in AIB and FSAB indicated that measurements through the cortex decreased the apparent backscattered power and increased the frequency dependence of the power. However, the cortex did not affect the correlation of AIB and FSAB with the x-ray bone mineral density of the specimens. This suggests that results from many previous in vitro backscatter studies of specimens of purely cancellous bone may be extrapolated with greater confidence to in vivo conditions.

Quantitative damage depth profiles in arsenic implanted HgCdTe

Energy Technology Data Exchange (ETDEWEB)

Lobre, C., E-mail: clement.lobre@cea.fr [CEA-Leti, MINATEC, 17 rue des Martyrs, 38054 Grenoble cedex 9 (France); Jalabert, D. [CEA-INAC/UJF-Grenoble 1 UMR-E, MINATEC, 17 rue des Martyrs, 38054 Grenoble cedex 9 (France); Vickridge, I.; Briand, E.; Benzeggouta, D. [Institut des NanoSciences de Paris, UMR 7588 du CNRS, Universite de Pierre et Marie Curie, Paris (France); Mollard, L. [CEA-Leti, MINATEC, 17 rue des Martyrs, 38054 Grenoble cedex 9 (France); Jouneau, P.H. [CEA-INAC/UJF-Grenoble 1 UMR-E, MINATEC, 17 rue des Martyrs, 38054 Grenoble cedex 9 (France); Ballet, P. [CEA-Leti, MINATEC, 17 rue des Martyrs, 38054 Grenoble cedex 9 (France)

2013-10-15

Rutherford backscattering experiments under channeling conditions (RBS-c) have been carried out on Hg{sub 0.77}Cd{sub 0.23}Te (MCT) layers implanted with arsenic. Accurate damage profiles have been extracted through a simple formalism for implanted and annealed layers. Quantitative damage profiles are correlated with structural defects observed by bright-field scanning transmission electron microscopy (BF-STEM) and chemical composition measured by secondary ion mass spectrometry (SIMS). Evolution of damage for increasing ion implantation fluence has been investigated by these three complementary techniques. Evidence is found of irradiation induced annealing during implantation. A fast damage recovery has been observed for post-implantation thermal anneals. In the case of an implanted layer annealed during 1 h, the damage profile, associated with arsenic concentration measurements, indicates the presence of complexes involving arsenic.

Quantitative damage depth profiles in arsenic implanted HgCdTe

International Nuclear Information System (INIS)

Lobre, C.; Jalabert, D.; Vickridge, I.; Briand, E.; Benzeggouta, D.; Mollard, L.; Jouneau, P.H.; Ballet, P.

2013-01-01

Rutherford backscattering experiments under channeling conditions (RBS-c) have been carried out on Hg 0.77 Cd 0.23 Te (MCT) layers implanted with arsenic. Accurate damage profiles have been extracted through a simple formalism for implanted and annealed layers. Quantitative damage profiles are correlated with structural defects observed by bright-field scanning transmission electron microscopy (BF-STEM) and chemical composition measured by secondary ion mass spectrometry (SIMS). Evolution of damage for increasing ion implantation fluence has been investigated by these three complementary techniques. Evidence is found of irradiation induced annealing during implantation. A fast damage recovery has been observed for post-implantation thermal anneals. In the case of an implanted layer annealed during 1 h, the damage profile, associated with arsenic concentration measurements, indicates the presence of complexes involving arsenic

Secondary electron emission from insulators

International Nuclear Information System (INIS)

Kanaya, K.; Ono, S.; Ishigaki, F.

1978-01-01

The high yield of secondary electron emission from insulators due to electron bombardment may be the result of an increase of the depth of escape. The free-electron scattering theory is applied to the high energy of primary beams, but cannot be applied to the low energy of secondary escaping beams because of the large energy gap of the insulators. The plasmon loss with the valence electron is considered when the secondary electrons escape. Based on the energy retardation power formula of the penetration and energy loss of an electron probe into solid targets, secondary electron emissions from insulators are calculated from the assumptions that the distribution of the secondary electrons due to both incident and back-scattered electrons within the target is isotropic and that it follows the absorption law of the Lenard type. The universal yield-energy curve of the secondary electron emission, which is deduced as a function of three parameters such as ionisation potential, valence electron and the back-scattered coefficient in addition to the free-electron density effect, is found to be in good agreement with the experimental results. (author)

Advanced technique for ultra-thin residue inspection with sub-10nm thickness using high-energy back-scattered electrons

Science.gov (United States)

Han, Jin-Hee

2018-03-01

Recently the aspect ratio of capacitor and via hole of memory semiconductor device has been dramatically increasing in order to store more information in a limited area. A small amount of remained residues after etch process on the bottom of the high aspect ratio structure can make a critical failure in device operation. Back-scattered electrons (BSE) are mainly used for inspecting the defect located at the bottom of the high aspect ratio structure or analyzing the overlay of the multi-layer structure because these electrons have a high linearity with the direction of emission and a high kinetic energy above 50eV. However, there is a limitation on that it cannot detect ultra-thin residue material having a thickness of several nanometers because the surface sensitivity is extremely low. We studied the characteristics of BSE spectra using Monte Carlo simulations for several cases which the high aspect ratio structures have extreme microscopic residues. Based on the assumption that most of the electrons emitted without energy loss are localized on the surface, we selected the detection energy window which has a range of 20eV below the maximum energy of the BSE. This window section is named as the high-energy BSE region. As a result of comparing the detection sensitivity of the conventional and the high-energy BSE detection mode, we found that the detection sensitivity for the residuals which have 2nm thickness is improved by more than 10 times in the high-energy BSE mode. This BSE technology is a new inspection method that can greatly be improved the inspection sensitivity for the ultra-thin residual material presented in the high aspect ratio structure, and its application will be expanded.

Ocean subsurface particulate backscatter estimation from CALIPSO spaceborne lidar measurements

Science.gov (United States)

Chen, Peng; Pan, Delu; Wang, Tianyu; Mao, Zhihua

2017-10-01

A method for ocean subsurface particulate backscatter estimation from the Cloud-Aerosol Lidar with Orthogonal Polarization (CALIOP) on the Cloud-Aerosol Lidar and Infrared Pathfinder Satellite Observation (CALIPSO) satellite was demonstrated. The effects of the CALIOP receiver's transient response on the attenuated backscatter profile were first removed. The two-way transmittance of the overlying atmosphere was then estimated as the ratio of the measured ocean surface attenuated backscatter to the theoretical value computed from wind driven wave slope variance. Finally, particulate backscatter was estimated from the depolarization ratio as the ratio of the column-integrated cross-polarized and co-polarized channels. Statistical results show that the derived particulate backscatter by the method based on CALIOP data agree reasonably well with chlorophyll-a concentration using MODIS data. It indicates a potential use of space-borne lidar to estimate global primary productivity and particulate carbon stock.

Improvements in backscatter measurement devices

International Nuclear Information System (INIS)

Saunders, J.; Hay, W.D.

1978-01-01

Improvements in measuring the thickness of a coating on a substrate by the technique of backscattered particles are described. These improvements enable the measurements to be carried out continuously as an integral part of the coating production line and also permit measurements where the coated elements are separated from one another by a predetermined distance. The former is achieved by situating the backscatter probe and detector on the rim of the measurement wheel and rotating this wheel at a speed such that the coated element and probe are stationary relative to one another. The latter improvement is achieved by an indexing apparatus which automatically positions the probe beside a coated element. (U.K.)

Prospects for quantitative and time-resolved double and continuous exposure off-axis electron holography

Energy Technology Data Exchange (ETDEWEB)

Migunov, Vadim, E-mail: v.migunov@fz-juelich.de [Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons, Peter Grünberg Institute, Forschungszentrum Jülich, D-52425 Jülich (Germany); Dwyer, Christian [Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons, Peter Grünberg Institute, Forschungszentrum Jülich, D-52425 Jülich (Germany); Department of Physics, Arizona State University, Tempe, AZ 85287 (United States); Boothroyd, Chris B. [Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons, Peter Grünberg Institute, Forschungszentrum Jülich, D-52425 Jülich (Germany); Pozzi, Giulio [Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons, Peter Grünberg Institute, Forschungszentrum Jülich, D-52425 Jülich (Germany); Department of Physics and Astronomy, University of Bologna, viale B. Pichat 6/2, Bologna 40127 (Italy); Dunin-Borkowski, Rafal E. [Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons, Peter Grünberg Institute, Forschungszentrum Jülich, D-52425 Jülich (Germany)

2017-07-15

The technique of double exposure electron holography, which is based on the superposition of two off-axis electron holograms, was originally introduced before the availability of digital image processing to allow differences between electron-optical phases encoded in two electron holograms to be visualised directly without the need for holographic reconstruction. Here, we review the original method and show how it can now be extended to permit quantitative studies of phase shifts that oscillate in time. We begin with a description of the theory of off-axis electron hologram formation for a time-dependent electron wave that results from the excitation of a specimen using an external stimulus with a square, sinusoidal, triangular or other temporal dependence. We refer to the more general method as continuous exposure electron holography, present preliminary experimental measurements and discuss how the technique can be used to image electrostatic potentials and magnetic fields during high frequency switching experiments. - Highlights: • Double and continuous exposure electron holography are described in detail. • The ability to perform quantitative studies of phase shifts that are oscillating in time is illustrated. • Theoretical considerations related to noise are presented. • Future high frequency electromagnetic switching experiments are proposed.

Identification of major backscattering sources in trees and shrubs at 10 GHz

Science.gov (United States)

Zoughi, R.; Wu, L. K.; Moore, R. K.

1986-01-01

A short-range very-fine-resolution FM-CW radar scatterometer has been used to identify the primary contributors to 10-GHz radar backscatter from pine, pin oak, American sycamore and sugar maple trees, and from creeping juniper shrubs. This system provided a range resolution of 11 cm and gave a 16-cm diameter illumination area at the target range of about 4 m. For a pine tree, the needles caused the strongest backscatter as well as the strongest attenuation in the radar signal. Cones, although insignificant contributors to the total backscatter, were more important for backscattering than for attenuation. For the rest of the trees, leaves were the strongest cause of backscattering and attenuation. However, in the absence of leaves, the petioles, small twigs, and branches gave relatively strong backscatter. For American sycamore and sugar maple trees, the fruits did not affect the total backscatter unless they were packed in clusters. For creeping juniper the backscattered energy and attenuation in the radar signal were mainly due to the top two layers of the evergreen scales. The contribution of the tree trunks was not determined.

Critical voltage effects in electron channeling patterns

International Nuclear Information System (INIS)

Farrow, R.C.

1984-01-01

Electron channeling patterns were used to study critical voltage effects in the metals molybdenum and tungsten. The purpose was to characterize both theoretically and experimentally how a critical voltage will affect the channeling pattern line shapes. The study focused on the second order critical voltage that results from the degeneracy between the Bloch wave states of the (110) and (220) reflections. Theoretical (110) series electron channeling pattern line profiles were calculated using the dynamical theory of Hirsch and Humphreys (1970). A 10 beam dynamical electron diffraction calculation was performed (using complex Fourier lattice potentials) to generate Bloch wave coefficients, excitation amplitudes, and absorption coefficients needed for determining backscattering coefficients and subsequent backscattered electron intensities. The theoretical model is applicable to electron diffraction at all energies since no high energy approximation or perturbation method was used

BATS - Backscattering And Time-of-flight Spectrometer

International Nuclear Information System (INIS)

Van Eijck, L.; Seydel, T.; Frick, B.; Schober, H.

2011-01-01

The new backscattering spectrometer IN16b will go into commissioning end 2011, providing in its final state about ten times higher count rate than its predecessor, IN16. Here we propose to increase its dynamic range by a factor of 7 with the TOF mode extension, BATS. This will make IN16b the leading high resolution backscattering spectrometer for incoherent quasi-elastic and inelastic neutron scattering; it will be competitive to the coarser resolution inverted geometry backscattering spectrometers that are being brought online at spallation sources. The increased dynamic range will extend the scope of science addressed on IN16b, generating considerable potential in fields such as the hydrogen economy (proton conduction, fuel cells, hydrogen storage), soft matter, biology and nano-science (nano-scale confinement, functionalized polymers). Such a large impact can be achieved using only a moderate investment. (authors)

Volume cross section of auroral radar backscatter and RMS plasma fluctuations inferred from coherent and incoherent scatter data: a response on backscatter volume parameters

Directory of Open Access Journals (Sweden)

M. V. Uspensky

2011-06-01

Full Text Available Norway and Finland STARE radar measurements in the eastward auroral electrojet are combined with EISCAT CP-1 measurements of the electron density and electric field vector in the common scattering volume to investigate the variation of the auroral radar volume cross section (VCS with the flow angle of observations (radar look direction with respect to the E×B electron drift. The data set available consists of ~6000 points for flow angles of 40–85° and electron drifts between 500 and 2000 m s−1. The EISCAT electron density N(h-profile data are used to estimate the effective electron density, aspect angle and thickness of the backscattering layer. It is shown that the flow angle variation of the VCS is rather weak, only ~5 dB within the range of the considered flow angles. The VCS values themselves respond almost linearly to the square of both the electron drift velocity magnitude and the effective electron density. By adopting the inferred shape of the VCS variation with the flow angle and the VCS dependence upon wavelength, the relative amplitude of electrostatic electron density fluctuations over all scales is estimated. Inferred values of 2–4 percent react nearly linearly to the electron drift velocity in the range of 500–1000 m s−1 but the rate of increase slows down at electron drifts >1000 m s−1 and density fluctuations of ~5.5 percent due to, perhaps, progressively growing nonlinear wave losses.

A correlative approach to segmenting phases and ferrite morphologies in transformation-induced plasticity steel using electron back-scattering diffraction and energy dispersive X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Gazder, Azdiar A., E-mail: azdiar@uow.edu.au [Electron Microscopy Centre, University of Wollongong, New South Wales 2500 (Australia); Al-Harbi, Fayez; Spanke, Hendrik Th. [School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, New South Wales 2522 (Australia); Mitchell, David R.G. [Electron Microscopy Centre, University of Wollongong, New South Wales 2500 (Australia); Pereloma, Elena V. [Electron Microscopy Centre, University of Wollongong, New South Wales 2500 (Australia); School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, New South Wales 2522 (Australia)

2014-12-15

Using a combination of electron back-scattering diffraction and energy dispersive X-ray spectroscopy data, a segmentation procedure was developed to comprehensively distinguish austenite, martensite, polygonal ferrite, ferrite in granular bainite and bainitic ferrite laths in a thermo-mechanically processed low-Si, high-Al transformation-induced plasticity steel. The efficacy of the ferrite morphologies segmentation procedure was verified by transmission electron microscopy. The variation in carbon content between the ferrite in granular bainite and bainitic ferrite laths was explained on the basis of carbon partitioning during their growth. - Highlights: • Multi-condition segmentation of austenite, martensite, polygonal ferrite and ferrite in bainite. • Ferrites in granular bainite and bainitic ferrite segmented by variation in relative carbon counts. • Carbon partitioning during growth explains variation in carbon content of ferrites in bainites. • Developed EBSD image processing tools can be applied to the microstructures of a variety of alloys. • EBSD-based segmentation procedure verified by correlative TEM results.

On the annealing behaviour of dysprosium ion implanted nickel: a combined study using Rutherford backscattering, transmission electron microscopy, and total current spectroscopy

International Nuclear Information System (INIS)

Chadderton, L.T.; Johnson, E.

1977-01-01

Despite continuing improvements in applications of the analytical method of Rutherford backscattering (RBS) to solid state physics it is recognized that more complete information can be obtained if other techniques - for example transmission electron microscopy (TEM) - are employed simultaneously. Experiments are described in which a combined RBS and TEM study of the annealing of nickel, rendered amorphous by implantation of 20 keV dysprosium ions is supplemented with a completely new technique - total current spectroscopy (TCS). In TCS low energy electrons (0-15 eV) are used to probe the damaged nickel. Observations have been made during annealing of both the reappearance of the bulk band structure of the metal and of a 'surface peak' which is highly sensitive to the recovery process. Changes in the height of the surface peak reveal three sharp annealing stages, the first two being preceded by reverse annealing which correlates well with RBS and TEM results. The first annealing stage - following the amorphous to crystalline transition - may be associated with electronic effects in the vicinity of the Curie point. Changes in the position of the surface peak allow one to trace the diffusion of dysprosium to the surface. Quantum mechanical resonances at the damage/crystal interface have also been followed throughout annealing. The initially amorphous layer (approximately 2.2nm) increases in thickness slightly during recovery. (Auth.)

Quantitative analysis of complexes in electron irradiated CZ silicon

International Nuclear Information System (INIS)

Inoue, N.; Ohyama, H.; Goto, Y.; Sugiyama, T.

2007-01-01

Complexes in helium or electron irradiated silicon are quantitatively analyzed by highly sensitive and accurate infrared (IR) absorption spectroscopy. Carbon concentration (1x10 15 -1x10 17 cm -3 ) and helium dose (5x10 12 -5x10 13 cm -2 ) or electron dose (1x10 15 -1x10 17 cm -2 ) are changed by two orders of magnitude in relatively low regime compared to the previous works. It is demonstrated that the carbon-related complex in low carbon concentration silicon of commercial grade with low electron dose can be detected clearly. Concentration of these complexes is estimated. It is clarified that the complex configuration and thermal behavior in low carbon and low dose samples is simple and almost confined within the individual complex family compared to those in high concentration and high dose samples. Well-established complex behavior in electron-irradiated sample is compared to that in He-irradiated samples, obtained by deep level transient spectroscopy (DLTS) or cathodoluminescence (CL), which had close relation to the Si power device performance

Comparisons between MCNP, EGS4 and experiment for clinical electron beams

International Nuclear Information System (INIS)

Jeraj, R.; Keall, P.J.; Ostwald, P.M.

1999-01-01

Understanding the limitations of Monte Carlo codes is essential in order to avoid systematic errors in simulations, and to suggest further improvement of the codes. MCNP and EGS4, Monte Carlo codes commonly used in medical physics, were compared and evaluated against electron depth dose data and experimental backscatter results obtained using clinical radiotherapy beams. Different physical models and algorithms used in the codes give significantly different depth dose curves and electron backscattering factors. The default version of MCNP calculates electron depth dose curves which are too penetrating. The MCNP results agree better with experiment if the ITS-style energy-indexing algorithm is used. EGS4 underpredicts electron backscattering for high- Z materials. The results slightly improve if optimal PRESTA-I parameters are used. MCNP simulates backscattering well even for high- Z materials. To conclude the comparison, a timing study was performed. EGS4 is generally faster than MCNP and use of a large number of scoring voxels dramatically slows down the MCNP calculation. However, use of a large number of geometry voxels in MCNP only slightly affects the speed of the calculation. (author)

Texture development study during the primary recrystallization of ferritic steels by using X ray and electron backscattering diffraction

International Nuclear Information System (INIS)

Loew, Marjorie

2006-01-01

X ray and electron backscattering diffraction, in distinct levels, were applied to evaluate microstructural changes in two low carbon ferritic steels (2 per cent Si and ABNT 1006), observing the texture development in cold lamination step (skin-pass) and in the subsequent annealing at 760 deg C. In these two steels, results showed that after the skin-pass and annealing in the conditions of the present work, the observed phenomenon is the primary recrystallization. By applying skin-pass dislocations were introduced mostly in low Taylor factor grains as they are prone to be more deformed. Nucleation and grain growth were observed in high density dislocation cell regions. Silicon presence delayed the recovery favoring the sub-boundaries increase. It was not observed the abnormal grain growth, even in the presence of Gross grains. CSL boundaries did not guarantee the grains growth. Growing nuclei gave rise to grains with distinct orientations, showing that the grain growth was not dependent on the previous presence of grains with the developed orientation. This fact demonstrates that the abnormal grain growth is not necessarily related to the Gross grains. (author)

Comparison between magnetic force microscopy and electron back-scatter diffraction for ferrite quantification in type 321 stainless steel

Energy Technology Data Exchange (ETDEWEB)

Warren, A.D., E-mail: Xander.Warren@bristol.ac.uk [Interface Analysis Centre, HH Wills Laboratory, University of Bristol, Bristol BS8 1FD (United Kingdom); Harniman, R.L. [School of Chemistry, University of Bristol, Bristol BS8 1 TS (United Kingdom); Collins, A.M. [School of Chemistry, University of Bristol, Bristol BS8 1 TS (United Kingdom); Bristol Centre for Functional Nanomaterials, Nanoscience and Quantum Information Centre, University of Bristol, Bristol BS8 1FD (United Kingdom); Davis, S.A. [School of Chemistry, University of Bristol, Bristol BS8 1 TS (United Kingdom); Younes, C.M. [Interface Analysis Centre, HH Wills Laboratory, University of Bristol, Bristol BS8 1FD (United Kingdom); Flewitt, P.E.J. [Interface Analysis Centre, HH Wills Laboratory, University of Bristol, Bristol BS8 1FD (United Kingdom); School of Physics, HH Wills Laboratory, University of Bristol, Bristol BS8 1FD (United Kingdom); Scott, T.B. [Interface Analysis Centre, HH Wills Laboratory, University of Bristol, Bristol BS8 1FD (United Kingdom)

2015-01-15

Several analytical techniques that are currently available can be used to determine the spatial distribution and amount of austenite, ferrite and precipitate phases in steels. The application of magnetic force microscopy, in particular, to study the local microstructure of stainless steels is beneficial due to the selectivity of this technique for detection of ferromagnetic phases. In the comparison of Magnetic Force Microscopy and Electron Back-Scatter Diffraction for the morphological mapping and quantification of ferrite, the degree of sub-surface measurement has been found to be critical. Through the use of surface shielding, it has been possible to show that Magnetic Force Microscopy has a measurement depth of 105–140 nm. A comparison of the two techniques together with the depth of measurement capabilities are discussed. - Highlights: • MFM used to map distribution and quantify ferrite in type 321 stainless steels. • MFM results compared with EBSD for same region, showing good spatial correlation. • MFM gives higher area fraction of ferrite than EBSD due to sub-surface measurement. • From controlled experiments MFM depth sensitivity measured from 105 to 140 nm. • A correction factor to calculate area fraction from MFM data is estimated.

A model for backscattering characteristics of tall prairie grass canopies at microwave frequencies

International Nuclear Information System (INIS)

Bakhtiari, S.; Zoughi, R.

1991-01-01

We have developed a discrete microwave scattering model, describing the radar backscattering coefficient from two treatments (burned and unburned) of tall prairie grass canopies at VV (electric field vector of the transmitted and received signals are vertically oriented) and HH (electric field vector of the transmitted and received signals and horizontally oriented) polarizations, based on the physical, biophysical, and geometrical characteristics of such canopies. Grass blades are modeled as thin and finite dielectric ellipsoids with arbitrary orientations. Scattering by an individual grass blade is formulated using a generalization of the Rayleigh—Gans approximation with a quasistatic solution for the expansion of the interior field. By associating, with each grass blade, various appropriate distribution functions, the relative orientation, location, height, cross section, and permittivity of each grass blade is taken into account. This makes for a more realistic overall description of the canopy. Kirchhoff's surface scattering is used to model the backscatter from the soil surface. An incoherent summation of the effect of grass blades and soil surface is adopted to obtain the total canopy backscattering coefficient, taking into account the attenuation experienced by the signal as it travels through the canopy. The results of this model are given for 1.5, 5, and 10 GHz (L-, C-, and X-band). Although for the shorter wavelengths (X-band) the Rayleigh—Gans criteria is not totally satisfied, nevertheless, the limited available measured X-band data compare relatively well with the results of this model both quantitatively and qualitatively. (author)

Multi-beam backscatter image data processing techniques employed to EM 1002 system

Digital Repository Service at National Institute of Oceanography (India)

Fernandes, W.A.; Chakraborty, B.

to compensate outer-beam backscatter strength data in such a way that the effect of angular backscatter strength is removed. In this work we have developed backscatter data processing techniques for EM1002 multi-beam system...

Quantitative biological measurement in Transmission Electron Tomography

International Nuclear Information System (INIS)

Mantell, Judith M; Verkade, Paul; Arkill, Kenton P

2012-01-01

It has been known for some time that biological sections shrink in the transmission electron microscope from exposure to the electron beam. This phenomenon is especially important in Electron Tomography (ET). The effect on shrinkage of parameters such as embedding medium or sample type is less well understood. In addition anisotropic area shrinkage has largely been ignored. The intention of this study is to explore the shrinkage on a number of samples ranging in thickness from 200 nm to 500 nm. A protocol was developed to determine the shrinkage in area and thickness using the gold fiducials used in electron tomography. In brief: Using low dose philosophy on the section, a focus area was used prior to a separate virgin study area for a series of known exposures on a tilted sample. The shrinkage was determined by measurements on the gold beads from both sides of the section as determined by a confirmatory tomogram. It was found that the shrinkage in area (approximately to 90-95% of the original) and the thickness (approximately 65% of the original at most) agreed with pervious authors, but that a lmost all the shrinkage was in the first minute and that although the direction of the in-plane shrinkage (in x and y) was sometimes uneven the end result was consistent. It was observed, in general, that thinner samples showed more percentage shrinkage than thicker ones. In conclusion, if direct quantitative measurements are required then the protocol described should be used for all areas studied.

Quantitative biological measurement in Transmission Electron Tomography

Science.gov (United States)

Mantell, Judith M.; Verkade, Paul; Arkill, Kenton P.

2012-07-01

It has been known for some time that biological sections shrink in the transmission electron microscope from exposure to the electron beam. This phenomenon is especially important in Electron Tomography (ET). The effect on shrinkage of parameters such as embedding medium or sample type is less well understood. In addition anisotropic area shrinkage has largely been ignored. The intention of this study is to explore the shrinkage on a number of samples ranging in thickness from 200 nm to 500 nm. A protocol was developed to determine the shrinkage in area and thickness using the gold fiducials used in electron tomography. In brief: Using low dose philosophy on the section, a focus area was used prior to a separate virgin study area for a series of known exposures on a tilted sample. The shrinkage was determined by measurements on the gold beads from both sides of the section as determined by a confirmatory tomogram. It was found that the shrinkage in area (approximately to 90-95% of the original) and the thickness (approximately 65% of the original at most) agreed with pervious authors, but that a lmost all the shrinkage was in the first minute and that although the direction of the in-plane shrinkage (in x and y) was sometimes uneven the end result was consistent. It was observed, in general, that thinner samples showed more percentage shrinkage than thicker ones. In conclusion, if direct quantitative measurements are required then the protocol described should be used for all areas studied.

Three-dimensional characterization of bainitic microstructures in low-carbon high-strength low-alloy steel studied by electron backscatter diffraction

International Nuclear Information System (INIS)

Kang, J.S.; Seol, Jae-Bok; Park, C.G.

2013-01-01

We investigated the microstructural evolution of high strength low alloy steel, Fe–2.0Mn–0.15Si–0.05C (wt.%), by varying the continuous cooling rates from 1 K/s to 50 K/s using three-dimensional electron backscatter diffraction and transmission electron microscopy. Granular bainitic microstructure was prevalent under a slow cooling rate of 1–10 K/s, while lath-type bainite was dominant at a high cooling rate of 50 K/s. The acicular ferrite that was the major microstructure under the intermediate ranges of cooling rates between 10 K/s and 30 K/s was tangled with each other, leading to a three-dimensional interwoven structure with highly misoriented grains. Because of the formation of three-dimensional structures, we propose that the terms “acicular ferrite” and “bainitic ferrite,” which are currently used in steel, be replaced by the terms “interwoven acicular bainite” and “lath bainite,” respectively. Moreover, we also confirmed that the cooling rate is an important factor in determining whether bainitic microstructures occur in the form of granular bainite, interwoven bainite, or lath bainite. - Highlights: • The morphology of bainitic grains was characterized by 3D-EBSD. • The ‘interwoven bainite’ and ‘lath bainite’ were suggested. • Interwoven bainite consisted of lenticular plates that were interlinked in 3D regime. • The packets of lath bainite were aligned in a specific direction

Three-dimensional characterization of bainitic microstructures in low-carbon high-strength low-alloy steel studied by electron backscatter diffraction

Energy Technology Data Exchange (ETDEWEB)

Kang, J.S. [Department of Materials Science and Engineering, POSTECH, Pohang 790-784 (Korea, Republic of); Technical Research Laboratories, POSCO, Pohang 790-300 (Korea, Republic of); Seol, Jae-Bok, E-mail: j.seol@mpie.de [Max-Planck-Institut für Eisenforschung, Max-Planck-Str. 1, D-40237 Düsseldorf (Germany); Park, C.G. [Department of Materials Science and Engineering, POSTECH, Pohang 790-784 (Korea, Republic of)

2013-05-15

We investigated the microstructural evolution of high strength low alloy steel, Fe–2.0Mn–0.15Si–0.05C (wt.%), by varying the continuous cooling rates from 1 K/s to 50 K/s using three-dimensional electron backscatter diffraction and transmission electron microscopy. Granular bainitic microstructure was prevalent under a slow cooling rate of 1–10 K/s, while lath-type bainite was dominant at a high cooling rate of 50 K/s. The acicular ferrite that was the major microstructure under the intermediate ranges of cooling rates between 10 K/s and 30 K/s was tangled with each other, leading to a three-dimensional interwoven structure with highly misoriented grains. Because of the formation of three-dimensional structures, we propose that the terms “acicular ferrite” and “bainitic ferrite,” which are currently used in steel, be replaced by the terms “interwoven acicular bainite” and “lath bainite,” respectively. Moreover, we also confirmed that the cooling rate is an important factor in determining whether bainitic microstructures occur in the form of granular bainite, interwoven bainite, or lath bainite. - Highlights: • The morphology of bainitic grains was characterized by 3D-EBSD. • The ‘interwoven bainite’ and ‘lath bainite’ were suggested. • Interwoven bainite consisted of lenticular plates that were interlinked in 3D regime. • The packets of lath bainite were aligned in a specific direction.

A didactic proposal about Rutherford backscattering spectrometry with theoretic, experimental, simulation and application activities

Science.gov (United States)

Corni, Federico; Michelini, Marisa

2018-01-01

Rutherford backscattering spectrometry is a nuclear analysis technique widely used for materials science investigation. Despite the strict technical requirements to perform the data acquisition, the interpretation of a spectrum is within the reach of general physics students. The main phenomena occurring during a collision between helium ions—with energy of a few MeV—and matter are: elastic nuclear collision, elastic scattering, and, in the case of non-surface collision, ion stopping. To interpret these phenomena, we use classical physics models: material point elastic collision, unscreened Coulomb scattering, and inelastic energy loss of ions with electrons, respectively. We present the educational proposal for Rutherford backscattering spectrometry, within the framework of the model of educational reconstruction, following a rationale that links basic physics concepts with quantities for spectra analysis. This contribution offers the opportunity to design didactic specific interventions suitable for undergraduate and secondary school students.

Morphology, surface roughness, electron inelastic and quasi-elastic scattering in elastic peak electron spectroscopy of polymers

International Nuclear Information System (INIS)

Lesiak, B.; Kosinski, A.; Nowakowski, R.; Koever, L.; Toth, J.; Varga, D.; Cserny, I.; Sulyok, A.; Gergely, G.

2006-01-01

Complete text of publication follows. Elastic peak electron spectroscopy (EPES) deals with the interaction of electrons with atoms of a solid surface, studying the distribution of electrons backscattered elastically. The nearest vicinity of the elastic peak, (low kinetic energy region) reflects both, electron inelastic and quasi-elastic processes. The incident electrons produce surface excitations, inducing surface plasmons with the corresponding loss peaks separated by 1 - 20 eV energy from the elastic peak. Quasi-elastic losses result from the recoil of scattering atoms of different atomic number, Z. The respective energy shift and Doppler broadening of the elastic peak depend on Z, the primary electron energy, E, and the measurement geometry. Quantitative surface analytical application of EPES, such as determination of parameters describing electron transport, requires a comparison of experimental data with corresponding data derived from Monte Carlo (MC) simulation. Several problems occur in EPES studies of polymers. The intensity of elastic peak, considered in quantitative surface analysis, is influenced by both, the inelastic and quasi-elastic scattering processes (especially for hydrogen scattering atoms and primary electron energy above 1000 eV). An additional factor affecting the elastic peak intensity is the surface morphology and roughness. The present work compares the effect of these factors on the elastic peak intensity for selected polymers (polyethylene, polyaniline and polythiophenes). X-ray photoelectron spectroscopy (XPS) and helium pycnometry are applied for deriving the surface atomic composition and the bulk density, while scanning electron microscopy (SEM) and atomic force microscopy (AFM) for determining surface morphology and roughness. According to presented results, the influence of surface morphology and roughness is larger than those of surface excitations or recoil of hydrogen atoms. The component due to recoil of hydrogen atoms can be

Uniqueness for the inverse backscattering problem for angularly controlled potentials

International Nuclear Information System (INIS)

Rakesh; Uhlmann, Gunther

2014-01-01

We consider the problem of recovering a smooth, compactly supported potential on R 3 from its backscattering data. We show that if two such potentials have the same backscattering data and the difference of the two potentials has controlled angular derivatives, then the two potentials are identical. In particular, if two potentials differ by a finite linear combination of spherical harmonics with radial coefficients and have the same backscattering data then the two potentials are identical. (paper)

Backscatter measurements of 11-cm equatorial spread-F irregularities

International Nuclear Information System (INIS)

Tsunoda, R.T.

1980-01-01

In the equatorial F-region ionosphere, a turbulent cascade process has been found to exist that extends from irregularity spatial wavelengths longer than tens of kilometers down to wavelengths as short as 36 cm. To investigate the small-scale regime of wavelengths less than 36 cm, an equatorial radar experiment was conducted using a frequency of 1320 MHz that corresponds to an irregularity wavelength of 11 cm. The first observations of radar backscatter from 11-cm field-aligned irregularities (FAI) are described. These measurements extend the spatial wavelength regime of F-region FAI to lengths that approach both electron gyroradius and the Debye length. Agreement of these results with the theory of high-frequency drift waves suggests that these observations may be unique to the equatorial ionosphere. That is, the requirement of low electron densities for which the theroy calls may preclude the existence of 11-cm FAI elsewhere in the F-region ionosphere, except in equatorial plasma bubbles

New method for characterizing paper coating structures using argon ion beam milling and field emission scanning electron microscopy.

Science.gov (United States)

Dahlström, C; Allem, R; Uesaka, T

2011-02-01

We have developed a new method for characterizing microstructures of paper coating using argon ion beam milling technique and field emission scanning electron microscopy. The combination of these two techniques produces extremely high-quality images with very few artefacts, which are particularly suited for quantitative analyses of coating structures. A new evaluation method has been developed by using marker-controlled watershed segmentation technique of the secondary electron images. The high-quality secondary electron images with well-defined pores makes it possible to use this semi-automatic segmentation method. One advantage of using secondary electron images instead of backscattered electron images is being able to avoid possible overestimation of the porosity because of the signal depth. A comparison was made between the new method and the conventional method using greyscale histogram thresholding of backscattered electron images. The results showed that the conventional method overestimated the pore area by 20% and detected around 5% more pores than the new method. As examples of the application of the new method, we have investigated the distributions of coating binders, and the relationship between local coating porosity and base sheet structures. The technique revealed, for the first time with direct evidence, the long-suspected coating non-uniformity, i.e. binder migration, and the correlation between coating porosity versus base sheet mass density, in a straightforward way. © 2010 The Authors Journal compilation © 2010 The Royal Microscopical Society.

Development of a sub-MeV X-ray source via Compton backscattering

International Nuclear Information System (INIS)

Kawase, K.; Kando, M.; Hayakawa, T.; Daito, I.; Kondo, S.; Homma, T.; Kameshima, T.; Kotaki, H.; Chen, L.-M.; Fukuda, Y.; Faenov, A.; Shizuma, T.; Shimomura, T.; Yoshida, H.; Hajima, R.; Fujiwara, M.; Bulanov, S.V.; Kimura, T.; Tajima, T.

2011-01-01

At the Kansai Photon Science Institute of the Japan Atomic Energy Agency, we have developed a Compton backscattered X-ray source in the energy region of a few hundred keV. The X-ray source consists of a 150-MeV electron beam, with a pulse duration of 10 ps (rms), accelerated by a Microtron accelerator and an Nd:YAG laser, with a pulse duration of 10 ns (FWHM). In the first trial experiment, the X-ray flux is estimated to be (2.2±1.0)x10 2 photons/pulse. For the actual application of an X-ray source, it is important to increase the generated X-ray flux as much as possible. Thus, for the purpose of increasing the X-ray flux, we have developed the pulse compression system for the Nd:YAG laser via stimulated Brillouin scattering (SBS). The SBS pulse compression has the great advantages of a high conversion efficiency and a simple structure. In this article, we review the present status of the Compton backscattered X-ray source and describe the SBS pulse compression system.

Optical Backscattering Measured by Airborne Lidar and Underwater Glider

Directory of Open Access Journals (Sweden)

James H. Churnside

2017-04-01

Full Text Available The optical backscattering from particles in the ocean is an important quantity that has been measured by remote sensing techniques and in situ instruments. In this paper, we compare estimates of this quantity from airborne lidar with those from an in situ instrument on an underwater glider. Both of these technologies allow much denser sampling of backscatter profiles than traditional ship surveys. We found a moderate correlation (R = 0.28, p < 10−5, with differences that are partially explained by spatial and temporal sampling mismatches, variability in particle composition, and lidar retrieval errors. The data suggest that there are two different regimes with different scattering properties. For backscattering coefficients below about 0.001 m−1, the lidar values were generally greater than the glider values. For larger values, the lidar was generally lower than the glider. Overall, the results are promising and suggest that airborne lidar and gliders provide comparable and complementary information on optical particulate backscattering.

Quantitative image analysis of WE43-T6 cracking behavior

International Nuclear Information System (INIS)

Ahmad, A; Yahya, Z

2013-01-01

Environment-assisted cracking of WE43 cast magnesium (4.2 wt.% Yt, 2.3 wt.% Nd, 0.7% Zr, 0.8% HRE) in the T6 peak-aged condition was induced in ambient air in notched specimens. The mechanism of fracture was studied using electron backscatter diffraction, serial sectioning and in situ observations of crack propagation. The intermetallic (rare earthed-enriched divorced intermetallic retained at grain boundaries and predominantly at triple points) material was found to play a significant role in initiating cracks which leads to failure of this material. Quantitative measurements were required for this project. The populations of the intermetallic and clusters of intermetallic particles were analyzed using image analysis of metallographic images. This is part of the work to generate a theoretical model of the effect of notch geometry on the static fatigue strength of this material.

Problems of standardized handling and quantitative evaluation of autoradiograms

International Nuclear Information System (INIS)

Treutler, H.C.; Freyer, K.

1985-01-01

In the last years autoradiography has gained increasing importance as a quantitative method of measuring radioactivity or element concentration. Mostly relative measurements are carried out. The optical density of the photographic emulsion produced by a calibrated radiation source is compared with that produced by a sample. The influences of different parameters, such as beta particle energy, backscattering, fading of the latent image, developing conditions, matrix effects and others on the results are described and the errors of the quantitative evaluation of autoradiograms are assessed. The performance of the method is demonstrated taking the quantitative determination of gold in silicon as an example

Study of multibeam techniques for bathymetry and seabottom backscatter applications

Digital Repository Service at National Institute of Oceanography (India)

Nair, R.R.; Chakraborty, B.

Indian ocean is presented using Hydrosweep-multibeam installed onboard ORV Sagarkanya. A seabottom classification model is proposed which can be applied for multibeam backscatter data. Certain aspects of the multibeam backscatter signal data processing...

Experimental observation of the improvement in MTF from backthinning a CMOS direct electron detector

International Nuclear Information System (INIS)

McMullan, G.; Faruqi, A.R.; Henderson, R.; Guerrini, N.; Turchetta, R.; Jacobs, A.; Hoften, G. van

2009-01-01

The advantages of backthinning monolithic active pixel sensors (MAPS) based on complementary metal oxide semiconductor (CMOS) direct electron detectors for electron microscopy have been discussed previously; they include better spatial resolution (modulation transfer function or MTF) and efficiency at all spatial frequencies (detective quantum efficiency or DQE). It was suggested that a 'thin' CMOS detector would have the most outstanding properties because of a reduction in the proportion of backscattered electrons. In this paper we show, theoretically (using Monte Carlo simulations of electron trajectories) and experimentally that this is indeed the case. The modulation transfer functions of prototype backthinned CMOS direct electron detectors have been measured at 300 keV. At zero spatial frequency, in non-backthinned 700-μm-thick detectors, the backscattered component makes up over 40% of the total signal but, by backthinning to 100, 50 or 35 μm, this can be reduced to 25%, 15% and 10%, respectively. For the 35 μm backthinned detector, this reduction in backscatter increases the MTF by 40% for spatial frequencies between 0.1 and 1.0 Nyquist. As discussed in the main text, reducing backscattering in backthinned detectors should also improve DQE.

Multifunctional skin-like electronics for quantitative, clinical monitoring of cutaneous wound healing.

Science.gov (United States)

Hattori, Yoshiaki; Falgout, Leo; Lee, Woosik; Jung, Sung-Young; Poon, Emily; Lee, Jung Woo; Na, Ilyoun; Geisler, Amelia; Sadhwani, Divya; Zhang, Yihui; Su, Yewang; Wang, Xiaoqi; Liu, Zhuangjian; Xia, Jing; Cheng, Huanyu; Webb, R Chad; Bonifas, Andrew P; Won, Philip; Jeong, Jae-Woong; Jang, Kyung-In; Song, Young Min; Nardone, Beatrice; Nodzenski, Michael; Fan, Jonathan A; Huang, Yonggang; West, Dennis P; Paller, Amy S; Alam, Murad; Yeo, Woon-Hong; Rogers, John A

2014-10-01

Non-invasive, biomedical devices have the potential to provide important, quantitative data for the assessment of skin diseases and wound healing. Traditional methods either rely on qualitative visual and tactile judgments of a professional and/or data obtained using instrumentation with forms that do not readily allow intimate integration with sensitive skin near a wound site. Here, an electronic sensor platform that can softly and reversibly laminate perilesionally at wounds to provide highly accurate, quantitative data of relevance to the management of surgical wound healing is reported. Clinical studies on patients using thermal sensors and actuators in fractal layouts provide precise time-dependent mapping of temperature and thermal conductivity of the skin near the wounds. Analytical and simulation results establish the fundamentals of the sensing modalities, the mechanics of the system, and strategies for optimized design. The use of this type of "epidermal" electronics system in a realistic clinical setting with human subjects establishes a set of practical procedures in disinfection, reuse, and protocols for quantitative measurement. The results have the potential to address important unmet needs in chronic wound management. © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

HF coherent backscatter in the ionosphere: In situ measurements of SuperDARN backscatter with e-POP RRI

Science.gov (United States)

Perry, G. W.; James, H. G.; Hussey, G. C.; Howarth, A. D.; Yau, A. W.

2017-12-01

We report in situ polarimetry measurements of HF scattering obtained by the Enhanced Polar Outflow Probe (e-POP) Radio Receiver Instrument (RRI) during a coherent backscatter scattering event detected by the Saskatoon Super Dual Auroral Radar Network (SuperDARN). On April 1, 2015, e-POP conducted a 4 minute coordinated experiment with SuperDARN Saskatoon, starting at 3:38:44 UT (21:38:44 LT). Throughout the experiment, SuperDARN was transmitting at 17.5 MHz and e-POP's ground track moved in a northeastward direction, along SuperDARN's field-of-view, increasing in altitude from 331 to 352 km. RRI was tuned to 17.505 MHz, and recorded nearly 12,000 SuperDARN radar pulses during the experiment. In the first half of the experiment, radar pulses recorded by RRI were "well behaved": they retained their transmitted amplitude envelope, and their pulse-to-pulse polarization characteristics were coherent - Faraday rotation was easily measured. During the second half of the experiment the pulses showed clear signs of scattering: their amplitude envelopes became degraded and dispersed, and their pulse-to-pulse polarization characteristics became incoherent - Faraday rotation was difficult to quantify. While these pulses were being received by RRI, SuperDARN Saskatoon detected a latitudinal band of coherent backscatter at e-POP's location, indicating that the scattered pulses measured by RRI may be a signature of HF backscatter. In this presentation, we will outline the polarimetric details of the scattered pulses, and provide an analytic interpretation of RRI's measurements to give new insight into the nature of HF coherent backscatter mechanism taking place in the terrestrial ionosphere.

Light backscattering efficiency and related properties of some phytoplankters

Science.gov (United States)

Ahn, Yu-Hwan; Bricaud, Annick; Morel, André

1992-11-01

By using a set-up that combines an integrating sphere with a spectroradiometer LI-1800 UW, the backscattering properties of nine different phytoplankters grown in culture have been determined experimentally for the wavelengths domain ν = 400 up to 850 nm. Simultaneously, the absorption and attenuation properties, as well as the size distribution function, have been measured. This set of measurements allowed the spectral values of refractive index, and subsequently the volume scattering functions (VSF) of the cells, to be derived, by operating a scattering model previously developed for spherical and homogeneous cells. The backscattering properties, measured within a restricted angular domain (approximately between 132 and 174°), have been compared to theoretical predictions. Although there appear some discrepancies between experimental and predicted values (probably due to experimental errors as well as deviations of actual cells from computational hypotheses), the overall agreement is good; in particular the observed interspecific variations of backscattering values, as well as the backscattering spectral variation typical of each species, are well accounted for by theory. Using the computed VSF, the measured backscattering properties can be converted (assuming spherical and homogeneous cells) into efficiency factors for backscattering ( overlineQbb) . Thhe spectral behavior of overlineQbb appears to be radically different from that for total scattering overlineQb. For small cells, overlineQ (λ) is practically constant over the spectrum, whereas overlineQb(λ) varies approximately according to a power law (λ -2). As the cell size increases, overlineQbb conversely, becomes increasingly featured, whilst overlineQb becomes spectrally flat. The chlorophyll-specific backscattering coefficients ( b b∗ appear highly variable and span nearly two orders of magnitude. The chlorophyll-specific absorption and scattering coefficients, a ∗ and b ∗, are mainly ruled by

Doubly versus singly positively charged oxygen ions back-scattered from a silicon surface under dynamic O2+ bombardment

International Nuclear Information System (INIS)

Franzreb, Klaus; Williams, Peter; Loerincik, Jan; Sroubek, Zdenek

2003-01-01

Mass-resolved (and emission-charge-state-resolved) low-energy ion back-scattering during dynamic O 2 + bombardment of a silicon surface was applied in a Cameca IMS-3f secondary ion mass spectrometry (SIMS) instrument to determine the bombarding energy dependence of the ratio of back-scattered O 2+ versus O + . While the ratio of O 2+ versus O + drops significantly at reduced bombarding energies, O 2+ back-scattered from silicon was still detectable at an impact energy (in the lab frame) as low as about 1.6 keV per oxygen atom. Assuming neutralization prior to impact, O 2+ ion formation in an asymmetric 16 O→ 28 Si collision is expected to take place via 'collisional double ionization' (i.e. by promotion of two outer O 2p electrons) rather than by the production of an inner-shell (O 2s or O 1s) core hole followed by Auger-type de-excitation during or after ejection. A molecular orbital (MO) correlation diagram calculated for a binary 'head-on' O-Si collision supports this interpretation

Relating multifrequency radar backscattering to forest biomass: Modeling and AIRSAR measurement

Science.gov (United States)

Sun, Guo-Qing; Ranson, K. Jon

1992-01-01

During the last several years, significant efforts in microwave remote sensing were devoted to relating forest parameters to radar backscattering coefficients. These and other studies showed that in most cases, the longer wavelength (i.e. P band) and cross-polarization (HV) backscattering had higher sensitivity and better correlation to forest biomass. This research examines this relationship in a northern forest area through both backscatter modeling and synthetic aperture radar (SAR) data analysis. The field measurements were used to estimate stand biomass from forest weight tables. The backscatter model described by Sun et al. was modified to simulate the backscattering coefficients with respect to stand biomass. The average number of trees per square meter or radar resolution cell, and the average tree height or diameter breast height (dbh) in the forest stand are the driving parameters of the model. The rest of the soil surface, orientation, and size distributions of leaves and branches, remain unchanged in the simulations.

Acoustic backscatter at a Red Sea whale shark aggregation site

KAUST Repository

Hozumi, Aya; Kaartvedt, Stein; Rø stad, Anders; Berumen, Michael L.; Cochran, Jesse E.M.; Jones, Burton

2018-01-01

An aggregation of sexually immature whale sharks occurs at a coastal submerged reef near the Saudi Arabian Red Sea coast each spring. We tested the hypothesis that these megaplanktivores become attracted to a prey biomass peak coinciding with their aggregation. Acoustic backscatter of the water column at 120 kHz and 333 kHz –a proxy for potential prey biomass –was continuously measured spanning the period prior to, during, and subsequent to the seasonal whale shark aggregations. No peak in acoustic backscatter was observed at the time of the aggregation. However, we observed a decrease in acoustic backscatter in the last days of deployment, which coincided the trailing end of whale shark season. Organisms forming the main scattering layer performed inverse diel vertical migration, with backscatter peaking at mid-depths during the day and in the deeper half of the water column at night. Target strength analyses suggested the backscatter was likely composed of fish larvae. Subsurface foraging behavior of the whale sharks within this aggregation has not been described, yet this study does not support the hypothesis that seasonal peaks in local whale shark abundance correspond to similar peaks in prey availability.

Acoustic backscatter at a Red Sea whale shark aggregation site

KAUST Repository

Hozumi, Aya

2018-03-28

An aggregation of sexually immature whale sharks occurs at a coastal submerged reef near the Saudi Arabian Red Sea coast each spring. We tested the hypothesis that these megaplanktivores become attracted to a prey biomass peak coinciding with their aggregation. Acoustic backscatter of the water column at 120 kHz and 333 kHz –a proxy for potential prey biomass –was continuously measured spanning the period prior to, during, and subsequent to the seasonal whale shark aggregations. No peak in acoustic backscatter was observed at the time of the aggregation. However, we observed a decrease in acoustic backscatter in the last days of deployment, which coincided the trailing end of whale shark season. Organisms forming the main scattering layer performed inverse diel vertical migration, with backscatter peaking at mid-depths during the day and in the deeper half of the water column at night. Target strength analyses suggested the backscatter was likely composed of fish larvae. Subsurface foraging behavior of the whale sharks within this aggregation has not been described, yet this study does not support the hypothesis that seasonal peaks in local whale shark abundance correspond to similar peaks in prey availability.

Optimal Time Allocation in Backscatter Assisted Wireless Powered Communication Networks

Science.gov (United States)

Lyu, Bin; Yang, Zhen; Gui, Guan; Sari, Hikmet

2017-01-01

This paper proposes a wireless powered communication network (WPCN) assisted by backscatter communication (BackCom). This model consists of a power station, an information receiver and multiple users that can work in either BackCom mode or harvest-then-transmit (HTT) mode. The time block is mainly divided into two parts corresponding to the data backscattering and transmission periods, respectively. The users first backscatter data to the information receiver in time division multiple access (TDMA) during the data backscattering period. When one user works in the BackCom mode, the other users harvest energy from the power station. During the data transmission period, two schemes, i.e., non-orthogonal multiple access (NOMA) and TDMA, are considered. To maximize the system throughput, the optimal time allocation policies are obtained. Simulation results demonstrate the superiority of the proposed model. PMID:28587171

Interference phenomena at backscattering by ice crystals of cirrus clouds.

Science.gov (United States)

Borovoi, Anatoli; Kustova, Natalia; Konoshonkin, Alexander

2015-09-21

It is shown that light backscattering by hexagonal ice crystals of cirrus clouds is formed within the physical-optics approximation by both diffraction and interference phenomena. Diffraction determines the angular width of the backscattering peak and interference produces the interference rings inside the peak. By use of a simple model for distortion of the pristine hexagonal shape, we show that the shape distortion leads to both oscillations of the scattering (Mueller) matrix within the backscattering peak and to a strong increase of the depolarization, color, and lidar ratios needed for interpretation of lidar signals.

Microstructural characterization by electron backscatter diffraction of a hot worked Al-Cu-Mg alloy

Energy Technology Data Exchange (ETDEWEB)

Cepeda-Jimenez, C.M., E-mail: cm.cepeda@cenim.csic.es [Department of Physical Metallurgy, CENIM, CSIC, Av. Gregorio del Amo 8, 28040 Madrid (Spain); Hidalgo, P.; Carsi, M.; Ruano, O.A.; Carreno, F. [Department of Physical Metallurgy, CENIM, CSIC, Av. Gregorio del Amo 8, 28040 Madrid (Spain)

2011-03-25

Research highlights: {yields} The most favourable conditions for hot workability have been determined. {yields} EBSD was employed to characterize the obtained microtexture and microstructure. {yields} The Al 2024 alloy torsion tested at 408 deg. C and 2.1 s{sup -1} showed maximum ductility. {yields} Solid solution and fine precipitates favour a fine microstructure at 408 deg. C. {yields} The increase in test temperature to 467 deg. C produces a sharp decrease in ductility. - Abstract: Hot torsion tests to fracture to simulate thermomechanical processing were carried out on a solution-treated Al-Cu-Mg alloy (Al 2024-T351) at constant temperature. Torsion tests were conducted in the range 278-467 deg. C, and at two strain rates, 2.1 and 4.5 s{sup -1}. Electron backscatter diffraction (EBSD) was employed to characterize the microtexture and microstructure before and after testing. The microstructural evolution during torsion deformation at different temperatures and strain rate conditions determines the mechanical properties at room temperature of the Al 2024 alloy since grain refining, dynamic precipitation and precipitate coalescence occur during the torsion test. These mechanical properties were measured by Vickers microhardness tests. At 408 deg. C and 2.1 s{sup -1} the optimum combination of solid solution and incipient precipitation gives rise to maximum ductility and large fraction of fine and misoriented grains (f{sub HAB} = 54%). In contrast, the increase in test temperature to 467 deg. C produces a sharp decrease in ductility, attributed to the high proportion of alloying elements in solid solution. Both the stress-strain flow curves obtained by torsion tests and the final microstructures are a consequence of recovery phenomena and the dynamic nature of the precipitation process taking place during deformation.

Microstructural characterization by electron backscatter diffraction of a hot worked Al-Cu-Mg alloy

International Nuclear Information System (INIS)

Cepeda-Jimenez, C.M.; Hidalgo, P.; Carsi, M.; Ruano, O.A.; Carreno, F.

2011-01-01

Research highlights: → The most favourable conditions for hot workability have been determined. → EBSD was employed to characterize the obtained microtexture and microstructure. → The Al 2024 alloy torsion tested at 408 deg. C and 2.1 s -1 showed maximum ductility. → Solid solution and fine precipitates favour a fine microstructure at 408 deg. C. → The increase in test temperature to 467 deg. C produces a sharp decrease in ductility. - Abstract: Hot torsion tests to fracture to simulate thermomechanical processing were carried out on a solution-treated Al-Cu-Mg alloy (Al 2024-T351) at constant temperature. Torsion tests were conducted in the range 278-467 deg. C, and at two strain rates, 2.1 and 4.5 s -1 . Electron backscatter diffraction (EBSD) was employed to characterize the microtexture and microstructure before and after testing. The microstructural evolution during torsion deformation at different temperatures and strain rate conditions determines the mechanical properties at room temperature of the Al 2024 alloy since grain refining, dynamic precipitation and precipitate coalescence occur during the torsion test. These mechanical properties were measured by Vickers microhardness tests. At 408 deg. C and 2.1 s -1 the optimum combination of solid solution and incipient precipitation gives rise to maximum ductility and large fraction of fine and misoriented grains (f HAB = 54%). In contrast, the increase in test temperature to 467 deg. C produces a sharp decrease in ductility, attributed to the high proportion of alloying elements in solid solution. Both the stress-strain flow curves obtained by torsion tests and the final microstructures are a consequence of recovery phenomena and the dynamic nature of the precipitation process taking place during deformation.

Standards for backscattering analysis

International Nuclear Information System (INIS)

Mitchell, I.V.; Eschbach, H.L.

1978-01-01

The need for backscattering standards appears to be twofold and depends on the uses and requirements of the users. The first is as a calibrated reference by which samples of a similar nature to the standard may be absolutely compared. The second is as a means of intercomparing the relative results obtained by different laboratories using, as near as possible, identical samples. This type of comparison is of a relative nature and the absolute values are not necessarily required. In the present work the authors try to satisfy both needs by providing identical samples which have been absolutely calibrated to a high accuracy. Very thin copper and vanadium layers were evaporated onto bismuth implanted silicon crystals and on glass plates under carefully controlled conditions. The mass of the deposits was determined in situ using a sensitive UHV microbalance. In addition, two quartz oscillator monitors were used. The samples have been analysed by Rutherford backscattering and the absolute quantity of bismuth determined by a comparison with the known amounts of deposited material. (Auth.)

A Micropulse eye-safe all-fiber molecular backscatter coherent temperature lidar

Directory of Open Access Journals (Sweden)

Abari Cyrus F.

2016-01-01

Full Text Available In this paper, we analyze the performance of an all-fiber, micropulse, 1.5 μm coherent lidar for remote sensing of atmospheric temperature. The proposed system benefits from the recent advances in optics/electronics technology, especially an all-fiber image-reject homodyne receiver, where a high resolution spectrum in the baseband can be acquired. Due to the presence of a structured spectra resulting from the spontaneous Rayleigh-Brillouine scattering, associated with the relevant operating regimes, an accurate estimation of the temperature can be carried out. One of the main advantages of this system is the removal of the contaminating Mie backscatter signal by electronic filters at the baseband (before signal conditioning and amplification. The paper presents the basic concepts as well as a Monte-Carlo system simulation as the proof of concept.

Quantitative study of substorm-associated VLF phase anomalies and precipitating energetic electrons on November 13, 1979

International Nuclear Information System (INIS)

Kikuchi, T.; Evans, D.S.

1983-01-01

The phase anomalies associated with substorms are observed on VLF signals propagating on transauroral paths (transmitters at OMEGA-ALDRA (13.6 kHz), GBR (16.0 kHz), and OMEGA--NORTH DAKOTA (13.6 kHz)) which were continually received at Inubo, Japan, during the events on November 13, 1979. Detailed comparisons are made between these phase anomalies and geomagnetic bays, and quantitative relations are obtained with precipitating energetic electrons (E>30, E>100, and E>300 keV) detected on board the TIROS-N and NOAA 6 satellites. It is concluded that two types of VLF phase anomalies exist which, in turn, are associated with two phases in the history of energetic electron precipitation into the atmosphere. The first type of phase anomaly is associated with direct injection of energetic electrons into the outer magnetosphere and atmosphere which, in turn, is completely correlated in time with development of the auroral electrojet current system. The second type arises from energetic electrons which subsequently precipitate from a trapped electron population and has a delayed onset and prolonged duration. An excellent quantitative correlation is obtained between the logarithm of the electron flux and the magnitude of the phase anomaly on the OMEGA-ALDRA signal. From the local time characteristics of this quantitative relation it is deduced that the electrons with E>300 keV are the main source of D region ionization responsible for the VLF phase anomaly

Aerosol backscatter measurements at 10.6 microns with airborne and ground-based CO2 Doppler lidars over the Colorado High Plains. II - Backscatter structure

Science.gov (United States)

Bowdle, David A.; Rothermel, Jeffry; Vaughan, J. Michael; Post, Madison J.

1991-01-01

Measurements of tropospheric aerosol volume backscatter coefficients at 10.6-microns wavelength were obtained with airborne continuous wave and ground-based pulsed CO2 Doppler lidars over the Colorado High Plains during a 20-day period in summer 1982. A persistent 'background' layer was found between 6- and 10-km altitude, with a generally uniform backscatter mixing ratio of about 10 to the -10th sq m/kg per sr. The upper boundary of this background layer varied with the tropopause height; the lower boundary varied with the strength and diurnal cycle of convective mixing in the planetary boundary layer (PBL). For quiescent meteorological conditions, the transition from the PBL to the background layer was usually very sharp, with backscatter decreases sometimes as large as 3 decades in about 70 m. Sharp gradients were also found at the boundaries of shallow (tens of meters) subvisible cirrus clouds. For less stable conditions, associated with vertical aerosol transport by deep cumuliform clouds, backscatter tended to decrease exponentially with altitude.

Backscatter Correction Algorithm for TBI Treatment Conditions

Energy Technology Data Exchange (ETDEWEB)

Sanchez-Nieto, B.; Sanchez-Doblado, F.; Arrans, R.; Terron, J.A. [Dpto. Fisiología Médica y Biofísica, Universidad de Sevilla, Avda. Sánchez Pizjuán, 4. E-41009, Sevilla (Spain); Errazquin, L. [Servicio Oncología Radioterápica, Hospital Univ.V. Macarena. Dr. Fedriani, s/n. E-41009, Sevilla (Spain)

2015-01-15

The accuracy requirements in target dose delivery is, according to ICRU, ±5%. This is so not only in standard radiotherapy but also in total body irradiation (TBI). Physical dosimetry plays an important role in achieving this recommended level. The semi-infinite phantoms, customarily used for dosimetry purposes, give scatter conditions different to those of the finite thickness of the patient. So dose calculated in patient’s points close to beam exit surface may be overestimated. It is then necessary to quantify the backscatter factor in order to decrease the uncertainty in this dose calculation. The backward scatter has been well studied at standard distances. The present work intends to evaluate the backscatter phenomenon under our particular TBI treatment conditions. As a consequence of this study, a semi-empirical expression has been derived to calculate (within 0.3% uncertainty) the backscatter factor. This factor depends lineally on the depth and exponentially on the underlying tissue. Differences found in the qualitative behavior with respect to standard distances are due to scatter in the bunker wall close to the measurement point.

High-field electron-photon interactions

International Nuclear Information System (INIS)

Hartemann, F V.

1999-01-01

Recent advances in novel technologies (including chirped-pulse amplification, femtosecond laser systems operating in the TW-PW range, high-gradient rf photoinjectors, and synchronized relativistic electron bunches with subpicosecond durations and THz bandwidths) allow experimentalists to study the interaction of relativistic electrons with ultrahigh-intensity photon fields. Ponderomotive scattering can accelerate these electrons with extremely high gradients in a three-dimensional vacuum laser focus. The nonlinear Doppler shift induced by relativistic radiation pressure in Compton backscattering is shown to yield complex nonlinear spectra which can be modified by using temporal laser pulse shaping techniques. Colliding laser pulses, where ponderomotive acceleration and Compton backscattering are combined, could also yield extremely short wavelength photons. Finally, one expects strong radiative corrections when the Doppler-upshifted laser wavelength approaches the Compton scale. These are discussed within the context of high-field classical electrodynamics, a new discipline borne out of the aforementioned innovations

Toward 3D structural information from quantitative electron exit wave analysis

International Nuclear Information System (INIS)

Borisenko, Konstantin B; Moldovan, Grigore; Kirkland, Angus I; Wang, Amy; Van Dyck, Dirk; Chen, Fu-Rong

2012-01-01

Simulations show that using a new direct imaging detector and accurate exit wave restoration algorithms allows nearly quantitative restoration of electron exit wave phase, which can be regarded as only qualitative for conventional indirect imaging cameras. This opens up a possibility of extracting accurate information on 3D atomic structure of the sample even from a single projection.

Monte Carlo Simulation of Quantitative Electron Probe Microanalysis of the PWR Spent Fuel with a Pt Coating

International Nuclear Information System (INIS)

Kwon, Hyoung Mun; Lee, Hyung Kwon; Son, Young Zoon; Chun, Yong Bum

2012-01-01

The PWR spent fuel sample should be coated with conducting material in order to provide a path for electrons and to prevent charging. Generally, the ZAF method has been used for quantitative electron probe microanalysis of conducting samples. However, the coated samples are not applicable for the ZAF method. Probe current, primary electron energy and x-ray produced by the primary beam are attenuated within the coating films. The electron and X-ray depth distributions for a quantitative electron probe micro analysis were simulated by the CASINO Monte Carlo program [2] to evaluate the x-ray attenuation within the Pt coating films. The target samples are the PWR spent fuels with 50 GWd/tU of burnup , 6 years of cooling time and a Pt coating film (3, 5, 7, 10 and 15 nm thickness)

Monte Carlo Simulation of Quantitative Electron Probe Microanalysis of the PWR Spent Fuel with a Pt Coating

Energy Technology Data Exchange (ETDEWEB)

Kwon, Hyoung Mun; Lee, Hyung Kwon; Son, Young Zoon; Chun, Yong Bum [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

2012-05-15

The PWR spent fuel sample should be coated with conducting material in order to provide a path for electrons and to prevent charging. Generally, the ZAF method has been used for quantitative electron probe microanalysis of conducting samples. However, the coated samples are not applicable for the ZAF method. Probe current, primary electron energy and x-ray produced by the primary beam are attenuated within the coating films. The electron and X-ray depth distributions for a quantitative electron probe micro analysis were simulated by the CASINO Monte Carlo program [2] to evaluate the x-ray attenuation within the Pt coating films. The target samples are the PWR spent fuels with 50 GWd/tU of burnup , 6 years of cooling time and a Pt coating film (3, 5, 7, 10 and 15 nm thickness)

Multiple scattering wavelength dependent backscattering of kaolin dust in the IR: Measurements and theory

Science.gov (United States)

Ben-David, Avishai

1992-01-01

Knowing the optical properties of aerosol dust is important for designing electro-optical systems and for modeling the effect on propagation of light in the atmosphere. As CO2 lidar technology becomes more advanced and is used for multiwavelength measurements, information on the wavelength dependent backscattering of aerosol dust particles is required. The volume backscattering coefficient of aerosols in the IR is relatively small. Thus, only a few field measurements of backscattering, usually at only a few wavelengths, are reported in the literature. We present spectral field measurements of backscattering of kaolin dust in the 9-11 micron wavelength range. As the quantity of dust increases, multiple scattering contributes more to the measured backscattered signal. The measurements show the effect of the dust quantity of the spectral backscatter measurements. A simple analytical two stream radiative transfer model is applied to confirm the measurements and to give insight to the multiple scattering spectra of backscattering.

A dedicated beam line for Rutherford backscattering analysis at IFIN-HH cyclotron

International Nuclear Information System (INIS)

Ivanov, E. A.; Dudu, D.; Plostinaru, D.; Catana, D.; Vata, I.

2003-01-01

Rutherford back-scattering technique (RBS) is an analytical tool that uses elastic scattering of 1-5 MeV charged particles for analysis of the surface and the outer few micrometers of solids. IFIN-HH RBS system consists of the U-120 Cyclotron, a dedicated beam line and a scattering chamber with sample manipulators and particle detectors. In our RBS system the samples are bombarded with 2-5 alpha particles accelerated by U-120 Cyclotron (in 3-rd subharmonic regime) while the scattered particles are detected by a surface barrier detector. The signal from the detector is processed by common nuclear electronics and the particle energy spectra are stored in a computer based multichannel analyser. The data evaluation is accomplished using standard procedures and computer codes. The necessary vacuum inside chamber is obtained with an oil-free turbo pump. The beam spot dimension on the target is 1x1 mm. The standard measurement are done at Θ = 165 angle. The samples are electrically insulated and can be rotated around a vertical axis. The advantage of the RBS technique lies in the quantitative analysis of major and minor constituents lying in the first 0.5 to 2.0 micrometers of a material. Depending on the sample structure and composition, the detection limits vary from 10 11 to 10 15 at. cm -2 for heavy and light elements, respectively. The depth distribution of constituents can be reconstructed with a depth resolution of 10-20 nm. The RBS technique is non-destructive since the erosion and the radiation degradation of the sample material by the particle impact is negligible. The most extensive use of the RBS technique is in the field of electronic and optical materials, special coatings and in the study of various physico-chemical processes on the solid surfaces. (authors)

MEASURING THE PARTICULATE BACKSCATTERING OF INLAND WATERS: A COMPARISON OF TECHNIQUES

Directory of Open Access Journals (Sweden)

G. Campbell

2012-07-01

Full Text Available The objective of this work was to examine whether the standard particulate backscattering IOP (Inherent Optical Properties measurement method could be simplified. IOP measurements are essential for parameterising several forms of algorithms used to estimate water quality parameters from airborne and satellite images. Field measurements of the backscattering IOPs are more difficult to make than absorption measurements as correction of the raw Hydroscat-6 backscattering sensor observations is required to allow for the systematic errors associated with the water and water quality parameter absorption. The standard approach involves making simultaneous measurement of the absorption and attenuation of the water with an absorption and attenuation meter (ac-9 or making assumptions about the particulate backscattering probability. Recently, a number of papers have been published that use an alternative method to retrieve the particulate backscattering spectrum by using laboratory measured absorption values and in situ spectroradiometric observations. The alternative method inverts a model of reflectance iteratively using non-linear least squares fitting to solve for the particulate backscattering at 532 nm (bbp0(532 and the particulate backscattering spectral slope (γ. In this paper, eleven observations made at Burdekin Falls Dam, Australia are used to compare the alternative reflectance method to the conventional corrected Hydroscat-6 observations. Assessment of the alternative reflectance method showed that the result of the inversions were highly dependent on the starting conditions. To overcome this limitation, Particle Swarm Optimisation, a stochastic search technique which includes a random element in the search approach, was used. It was found that when compared to the conventionally corrected Hydroscat-6 observations, the alternative reflectance method underestimated bbp0(532 by approximately 50% and overestimated γ by approximately 40

Quantitative vs. qualitative approaches to the electronic structure of solids

International Nuclear Information System (INIS)

Oliva, J.M.; Llunell, Miquel; Alemany, Pere; Canadell, Enric

2003-01-01

The usefulness of qualitative and quantitative theoretical approaches in solid state chemistry is discussed by considering three different types of problems: (a) the distribution of boron and carbon atoms in MB 2 C 2 (M=Ca, La, etc.) phases, (b) the band structure and Fermi surface of low-dimensional transition metal oxides and bronzes, and (c) the correlation between the crystal and electronic structure of the ternary nitride Ca 2 AuN

Monokinetic electron backsttering from amorphous or polycrystalline specimens

International Nuclear Information System (INIS)

Ahmed, H.E.D.H.

1983-06-01

We have considered the interaction of electrons with thin amorphous specimens: one part of these electrons is transmitted through the substance, the other being backscattered. This last phenomena, which is not perfectly understood, has been studied in the energy range from 0.3 to 3 MeV. First this work deals with the realization of a fully automatic apparatus which has been adapted to the column of the 3 MeV electron microscope of the HVFM laboratory in Toulouse. The variation of the transmission and backscattering coefficients, for amorphous and polycrystalline specimens, is determined. From this coefficient the electron range in this substance can be deduced. In addition the experimental results can be used to understand the image contrast in scanning electron microscopy. A short presentation of the cross-section, introduces the theoretical study of Monte-Carlo calculation. The Monte-Carlo calculation is used to take into account all elementary processus, which take place during electron scattering [fr

Response function and optimum configuration of semiconductor backscattered-electron detectors for scanning electron microscopes

International Nuclear Information System (INIS)

Rau, E. I.; Orlikovskiy, N. A.; Ivanova, E. S.

2012-01-01

A new highly efficient design for semiconductor detectors of intermediate-energy electrons (1–50 keV) for application in scanning electron microscopes is proposed. Calculations of the response function of advanced detectors and control experiments show that the efficiency of the developed devices increases on average twofold, which is a significant positive factor in the operation of modern electron microscopes in the mode of low currents and at low primary electron energies.

Power Control for Passive QAM Multisensor Backscatter Communication Systems

Directory of Open Access Journals (Sweden)

Shengbo Hu

2017-01-01

Full Text Available To achieve good quality of service level such as throughput, power control is of great importance to passive quadrature amplitude modulation (QAM multisensor backscatter communication systems. First, we established the RF energy harvesting model and gave the energy condition. In order to minimize the interference of subcarriers and increase the spectral efficiency, then, the colocated passive QAM backscatter communication signal model is presented and the nonlinear optimization problems of power control are solved for passive QAM backscatter communication systems. Solutions include maximum and minimum access interval, the maximum and minimum duty cycle, and the minimal RF-harvested energy under the energy condition for node operating. Using the solutions above, the maximum throughput of passive QAM backscatter communication systems is analyzed and numerical calculation is made finally. Numerical calculation shows that the maximal throughput decreases with the consumed power and the number of sensors, and the maximum throughput is decreased quickly with the increase of the number of sensors. Especially, for a given consumed power of sensor, it can be seen that the throughput decreases with the duty cycle and the number of sensors has little effect on the throughput.

WE-EF-210-05: Diagnosis and Quantification of Liver Steatosis with Quantitative Ultrasound Backscatter Technique

Energy Technology Data Exchange (ETDEWEB)

Andre, M [VA Medical Center, Encinitas, CA (United States); University of California, San Diego, San Diego, CA (United States); Heba, E; Lin, S; Wolfson, T; Ang, B; Gamst, A; Sirlin, C; Loomba, R [University of California, San Diego, San Diego, CA (United States); Han, A; Erdman, J; O’Brien, W [University of Illinois, Urbana, IL (United States)

2015-06-15

Purpose: Nonalcoholic fatty liver disease (NAFLD) is the most common cause of chronic liver disease in the United States, affects 30% of adult Americans and may progress to more serious diseases. Liver biopsy is the standard method for diagnosing NAFLD. MRI can accurately diagnose and quantify hepatic steatosis but is expensive. Sonography with qualitative interpretation by radiologists is lower cost, more accessible but less sensitive for detection. The objective of this study, using MRI proton density fat fraction (PDFF) as reference, is to assess the accuracy for diagnosing and quantifying steatosis with two quantitative US parameters-- backscatter coefficient (BSC) and attenuation coefficient (AC)--derived from RF signals using the calibration phantom technique. Methods: We performed a prospective, cross-sectional analysis of a cohort of adults (n=204) with NAFLD (MRI-PDFF≥5%) and without NAFLD (controls). Subjects underwent MRI-PDFF and BSC and AC US analyses of the liver on the same day. Patients were randomly assigned to training (n=102, mean age 51±17 years, mean body mass index 31±7 kg/m{sup 2}) and validation (n=102, mean age 49±17 years, body mass index 30±6 kg/m{sup 2}) groups; 69% of patients in each group had NAFLD. Results: BSC provided AUC 0.98 (95% CI 0.95–1.00, p<0.0001) for diagnosis of NAFLD; the optimal BSC cut-off provided sensitivity, specificity, positive and negative predictive values (PPV, NPV) of 87%, 91%, 95%, and 76%, respectively. AC provided AUC 0.89 (95% CI 0.81–0.96, p<0.0001) for diagnosis of steatosis; the optimal AC cut-off provided sensitivity, specificity, PPV, NPV of 80%, 84%, 92%, and 66%, respectively. BSC and AC both correlated significantly with MRI-PDFF (P<0.0001). Conclusion: QUS BSC and AC can accurately diagnose and quantify hepatic steatosis, using MRI-PDFF as reference. With further validation, QUS may emerge as an inexpensive, widely available tool for NAFLD assessment. General support: NIH R01 CA111289, K

Influence of surface topography on elastically backscattered electrons

International Nuclear Information System (INIS)

Ding, X; Da, B; Gong, J B; Ding, Z J; Mao, S F

2014-01-01

A Monte Carlo simulation, taking into account of the detailed surface roughness of a realistic solid sample, has been performed to study the surface topography influence on elastic peak intensity. To describe quantitatively the surface topography effect, here we introduce surface roughness parameter (SRP) according to the ratio of elastic peak intensities between a rough surface and an ideal planar surface. Simulation results for Al sample have shown that SRP varies with surface roughness particularly at large incidence/emission angles

Fast and Precise Beam Energy Measurement using Compton Backscattering at e+e- Colliders

CERN Document Server

Kaminskiy, V V; Muchnoi, N Yu; Zhilich, V N

2017-01-01

The report describes a method for a fast and precise beam energy measurement in the beam energy range 0.5-2 GeV and its application at various e+e- colliders. Low-energy laser photons interact head-on with the electron or positron beam and produce Compton backscattered photons whose energy is precisely measured by HPGe detector. The method allows measuring the beam energy with relative accuracy of ∼2-5.10-5. The method was successfully applied at VEPP-4M, VEPP-3, VEPP-2000 (BINP, Russia) and BEPC-II (IHEP, China).

Backscattering analysis of AuGe-Ni ohmic contacts of n-GaAs

International Nuclear Information System (INIS)

Nassibian, A.G.; Kalkur, T.S.; Sutherland, G.J.; Cohen, D.

1985-01-01

AuGe-Ni is widely used for the fabrication of ohmic contacts to n-GaAs. The alloying behaviour of evaporated AuGe-Ni alloyed by furnace and Scanning Electron Beam, is characterised by Rutherford backscattering with 2MeV 4 He ions. Since the formation of alloyed AuGe-Ni contacts involves redistribution and diffusion of Ga, As, Ni, Ge and Au, it is difficult to separate the corresponding yields due to gold, Ga As, Ni and Ge in the spectrum. The technique used in the investigation involves assumption of depth distribution of elements and computing the resultant spectrum

A classification of spectral populations observed in HF radar backscatter from the E region auroral electrojets

Directory of Open Access Journals (Sweden)

S. E. Milan

2001-02-01

Full Text Available Observations of HF radar backscatter from the auroral electrojet E region indicate the presence of five major spectral populations, as opposed to the two predominant spectral populations, types I and II, observed in the VHF regime. The Doppler shift, spectral width, backscatter power, and flow angle dependencies of these five populations are investigated and described. Two of these populations are identified with type I and type II spectral classes, and hence, are thought to be generated by the two-stream and gradient drift instabilities, respectively. The remaining three populations occur over a range of velocities which can greatly exceed the ion acoustic speed, the usual limiting velocity in VHF radar observations of the E region. The generation of these spectral populations is discussed in terms of electron density gradients in the electrojet region and recent non-linear theories of E region irregularity generation.Key words. Ionosphere (ionospheric irregularities

Quantitative Near-field Microscopy of Heterogeneous and Correlated Electron Oxides

Science.gov (United States)

McLeod, Alexander Swinton

Scanning near-field optical microscopy (SNOM) is a novel scanning probe microscopy technique capable of circumventing the conventional diffraction limit of light, affording unparalleled optical resolution (down to 10 nanometers) even for radiation in the infrared and terahertz energy regimes, with light wavelengths exceeding 10 micrometers. However, although this technique has been developed and employed for more than a decade to a qualitatively impressive effect, researchers have lacked a practically quantitative grasp of its capabilities, and its application scope has so far remained restricted by implementations limited to ambient atmospheric conditions. The two-fold objective of this dissertation work has been to address both these shortcomings. The first half of the dissertation presents a realistic, semi-analytic, and benchmarked theoretical description of probe-sample near-field interactions that form the basis of SNOM. Owing its name to the efficient nano-focusing of light at a sharp metallic apex, the "lightning rod model" of probe-sample near-field interactions is mathematically developed from a flexible and realistic scattering formalism. Powerful and practical applications are demonstrated through the accurate prediction of spectroscopic near-field optical contrasts, as well as the "inversion" of these spectroscopic contrasts into a quantitative description of material optical properties. Thus enabled, this thesis work proceeds to present quantitative applications of infrared near-field spectroscopy to investigate nano-resolved chemical compositions in a diverse host of samples, including technologically relevant lithium ion battery materials, astrophysical planetary materials, and invaluable returned extraterrestrial samples. The second half of the dissertation presents the design, construction, and demonstration of a sophisticated low-temperature scanning near-field infrared microscope. This instrument operates in an ultra-high vacuum environment

Mitigating the effect of optical back-scatter in multispectral underwater imaging

International Nuclear Information System (INIS)

Mortazavi, Halleh; Oakley, John P; Barkat, Braham

2013-01-01

Multispectral imaging is a very useful technique for extracting information from the underwater world. However, optical back-scatter changes the intensity value in each spectral band and this distorts the estimated spectrum. In this work, a filter is used to detect the level of optical back-scatter in each spectral band from a set of multispectral images. Extraction of underwater object spectra can be done by subtracting the estimated level of optical back-scatter and scaling the remainder in each spectral band from the captured image in the corresponding band. An experiment has been designed to show the performance of the proposed filter for correcting the set of multispectral underwater images and recovering the pixel spectra. The multispectral images are captured by a B/W CCD digital camera with a fast tunable liquid-crystal filter in 33 narrow spectral bands in clear and different levels of turbid water. Reference estimates for the optical back-scatter spectra are found by comparing a clear and a degraded set of multispectral images. The accuracy and consistency of the proposed method, the extended Oakley–Bu cost function, is examined by comparing the estimated values with the reference level of an optical back-scatter spectrum. The same comparison is made for the simple estimation approach. The results show that the simple method is not reliable and fail to estimate the level of optical back-scatter spectrum accurately. The results from processing experimental images in turbid water show that the effect of optical back-scatter can be mitigated in the image of each spectral band and, as a result, the spectra of the object can be recovered. However, for a very high level of turbid water the recovery is limited because of the effect of extinction. (paper)

Electron transport in heterogeneous media

International Nuclear Information System (INIS)

Falcao, Rossana Cavalieri

1992-05-01

In this work it is presented a model to calculate dose enhancement in the vicinity of plane interfaces irradiated by therapeutic electron beams. The proposed model is based on an approximation of the Boltzmann Equation. The solutions presented to the equation are exact on its angular dependency, making it possible to observe that at low Z/high Z interfaces the dose enhancement is due to an increase of the backscattering. For the inverse situation a decrease of the backscattering can be observed. Calculations have been made for some tissue-metal interfaces irradiated by 13 MeV electron beam. The dose perturbations in tissue were obtained and the results were compared with experimental data as well as Monte Carlo simulations. In both cases the agreement found was very good. (author)

Remarks on some reference materials for applications in elastic peak electron spectroscopy

International Nuclear Information System (INIS)

Jablonski, A.; Zemek, J.

2010-01-01

The quantification of results of electron spectroscopies, AES and XPS, requires knowledge of the inelastic mean free path (IMFP) of signal electrons in solids. This parameter determines the surface sensitivity of both techniques. There are two methods of determining the IMFPs that provide these parameters in agreement with the definition: (1) calculations based on the experimental optical data, and (2) calculations based on measurements of the electron elastic backscattering intensity. The latter method requires the use of some reference material for which the IMFP is known. In 1999, an extensive analysis of the published IMFPs has been performed; the results indicated that there is a very good agreement between the calculated and measured IMFPs for four elemental solids: Ni, Cu, Ag and Au. The averaged IMFPs for these elements are known under the name of the recommended IMFPs. However, no preference among these four elements has been established. In the present work, an attempt is made to select an element for which the recommended IMFPs result in the best agreement between the calculated and measured intensities of elastic electron backscattering. For this purpose, the elastic backscattering intensity has been measured at eight electron energies varying from 200 to 1500 eV. At each energy, the intensity was measured over a wide range of emission angles from 35deg to 74deg. The experiments were accompanied with Monte Carlo calculations of the elastic backscattering probability for the same energies and experimental configurations. It has been found, from comparison, that the best agreement is observed for Au, and this element is thus recommended as the reference material. It has been shown that the shape of the emission angle dependence of the elastic backscattering intensity is noticeably influenced by the surface energy losses. (author)

Super-virtual Interferometric Separation and Enhancement of Back-scattered Surface Waves

KAUST Repository

Guo, Bowen; Hanafy, Sherif; Schuster, Gerard T.

2015-01-01

Back-scattered surface waves can be migrated to detect near-surface reflectors with steep dips. A robust surface-wave migration requires the prior separation of the back-scattered surface-wave events from the data. This separation is often difficult

Retrieving forest stand parameters from SAR backscatter data using a neural network trained by a canopy backscatter model

International Nuclear Information System (INIS)

Wang, Y.; Dong, D.

1997-01-01

It was possible to retrieve the stand mean dbh (tree trunk diameter at breast height) and stand density from the Jet Propulsion Laboratory (JPL) Airborne Synthetic Aperture Radar (AIRSAR) backscatter data by using threelayered perceptron neural networks (NNs). Two sets of NNs were trained by the Santa Barbara microwave canopy backscatter model. One set of the trained NNs was used to retrieve the stand mean dbh, and the other to retrieve the stand density. Each set of the NNs consisted of seven individual NNs for all possible combinations of one, two, and three radar wavelengths. Ground and multiple wavelength AIRSAR backscatter data from two ponderosa pine forest stands near Mt. Shasta, California (U.S.A.) were used to evaluate the accuracy of the retrievals. The r.m.s. and relative errors of the retrieval for stand mean dbh were 6.1 cm and 15.6 per cent for one stand (St2), and 3.1 cm and 6.7 per cent for the other stand (St11). The r.m.s. and relative errors of the retrieval for stand density were 71.2 treesha-1 and 23.0 per cent for St2, and 49.7 treesha-1 and 21.3 per cent for St11. (author)

Quantitative Ultrasound Characterization of Cancer Radiotherapy Effects In Vitro

International Nuclear Information System (INIS)

Vlad, Roxana M.; Alajez, Nehad M.; Giles, Anoja B.Sc.; Kolios, Michael C.; Czarnota, Gregory J.

2008-01-01

Purpose: Currently, no routinely used imaging modality is available to assess tumor responses to cancer treatment within hours to days after radiotherapy. In this study, we demonstrate the preclinical application of quantitative ultrasound methods to characterize the cellular responses to cancer radiotherapy in vitro. Methods and Materials: Three different cell lines were exposed to radiation doses of 2-8 Gy. Data were collected with an ultrasound scanner using frequencies of 10-30 MHz. As indicators of response, ultrasound integrated backscatter and spectral slope were determined from the cell samples. These parameters were corrected for ultrasonic attenuation by measuring the attenuation coefficient. Results: A significant increase in the ultrasound integrated backscatter of 4-7 dB (p < 0.001) was found for radiation-treated cells compared with viable cells at all radiation doses. The spectral slopes decreased in the cell samples that predominantly underwent mitotic arrest/catastrophe after radiotherapy, consistent with an increase in cell size. In contrast, the spectral slopes did not change significantly in the cell samples that underwent a mix of cell death (apoptosis and mitotic arrest), with no significant change in average cell size. Conclusion: The changes in ultrasound integrated backscatter and spectral slope were direct consequences of cell and nuclear morphologic changes associated with cell death. The results indicate that this combination of quantitative ultrasonic parameters has the potential to assess the cell responses to radiation, differentiate between different types of cell death, and provide a preclinical framework to monitor tumor responses in vivo

Compositional Signatures in Acoustic Backscatter Over Vegetated and Unvegetated Mixed Sand-Gravel Riverbeds

Science.gov (United States)

Buscombe, D.; Grams, P. E.; Kaplinski, M. A.

2017-10-01

Multibeam acoustic backscatter has considerable utility for remote characterization of spatially heterogeneous bed sediment composition over vegetated and unvegetated riverbeds of mixed sand and gravel. However, the use of high-frequency, decimeter-resolution acoustic backscatter for sediment classification in shallow water is hampered by significant topographic contamination of the signal. In mixed sand-gravel riverbeds, changes in the abiotic composition of sediment (such as homogeneous sand to homogeneous gravel) tend to occur over larger spatial scales than is characteristic of small-scale bedform topography (ripples, dunes, and bars) or biota (such as vascular plants and periphyton). A two-stage method is proposed to filter out the morphological contributions to acoustic backscatter. First, the residual supragrain-scale topographic effects in acoustic backscatter with small instantaneous insonified areas, caused by ambiguity in the local (beam-to-beam) bed-sonar geometry, are removed. Then, coherent scales between high-resolution topography and backscatter are identified using cospectra, which are used to design a frequency domain filter that decomposes backscatter into the (unwanted) high-pass component associated with bedform topography (ripples, dunes, and sand waves) and vegetation, and the (desired) low-frequency component associated with the composition of sediment patches superimposed on the topography. This process strengthens relationships between backscatter and sediment composition. A probabilistic framework is presented for classifying vegetated and unvegetated substrates based on acoustic backscatter at decimeter resolution. This capability is demonstrated using data collected from diverse settings within a 386 km reach of a canyon river whose bed varies among sand, gravel, cobbles, boulders, and submerged vegetation.

Compositional signatures in acoustic backscatter over vegetated and unvegetated mixed sand-gravel riverbeds

Science.gov (United States)

Buscombe, Daniel; Grams, Paul E.; Kaplinski, Matt A.

2017-01-01

Multibeam acoustic backscatter has considerable utility for remote characterization of spatially heterogeneous bed sediment composition over vegetated and unvegetated riverbeds of mixed sand and gravel. However, the use of high-frequency, decimeter-resolution acoustic backscatter for sediment classification in shallow water is hampered by significant topographic contamination of the signal. In mixed sand-gravel riverbeds, changes in the abiotic composition of sediment (such as homogeneous sand to homogeneous gravel) tend to occur over larger spatial scales than is characteristic of small-scale bedform topography (ripples, dunes, and bars) or biota (such as vascular plants and periphyton). A two-stage method is proposed to filter out the morphological contributions to acoustic backscatter. First, the residual supragrain-scale topographic effects in acoustic backscatter with small instantaneous insonified areas, caused by ambiguity in the local (beam-to-beam) bed-sonar geometry, are removed. Then, coherent scales between high-resolution topography and backscatter are identified using cospectra, which are used to design a frequency domain filter that decomposes backscatter into the (unwanted) high-pass component associated with bedform topography (ripples, dunes, and sand waves) and vegetation, and the (desired) low-frequency component associated with the composition of sediment patches superimposed on the topography. This process strengthens relationships between backscatter and sediment composition. A probabilistic framework is presented for classifying vegetated and unvegetated substrates based on acoustic backscatter at decimeter resolution. This capability is demonstrated using data collected from diverse settings within a 386 km reach of a canyon river whose bed varies among sand, gravel, cobbles, boulders, and submerged vegetation.

Analysis of Backscatter and Seafloor Acoustical Properties across deepwater sandwaves in Cook Strait, New Zealand

Science.gov (United States)

Lurton, X.; Lamarche, G.

2011-12-01

Central Cook Strait, New Zealand presents a variety of geological landforms subjected to intense hydrodynamic conditions. A comprehensive EM300 multibeam coverage of the strait was used to develop a method to objectively characterise the seafloor substrate. Specific post-processing was applied to the backscatter data to correct the signal from sensor bias, and was completed by correlating a quantitative description of backscatter with the field data. The final calibrated Backscattering Strength (BS) provides information on the physical characteristics of the seafloor. The BS imagery was used for both qualitative and quantitative interpretation, and give access to a level of detail higher than with conventional multibeam bathymetry. We developed a functional descriptive model of the physical BS angular response, describing satisfactorily the various typical BS responses met over Cook Strait and providing a first-order interpretation of the substrate composition. The full model needs 6 input parameters, but a practical classification can be obtained with only two (the BS value at 45° and the specular-to-oblique contrast). We analyse the BS angular response of sandwaves and erosional bedforms typically met in the central Cook Strait. The sandwave fields occur in 200-350 m of water depth and exhibit large-scale topographical features (wavelengths 100 - 250 m; vertical amplitudes 2 - 10 m). They are conspicuous in the backscatter imagery, and analysing their BS variations according to topography is specially informative. The BS level has a sharp minimum at the wave crests and is maximal inside the troughs, with a typical dynamics of 6 dB. Such a variation cannot be explained by the dependence on incident angle retrieved from local high-resolution bathymetry. Hence we infer that the reflectivity variations observed on the sandwaves are due to sediment facies changes, from fine to coarse sand in this case. This is corroborated by the fact that some sandwave fields with

Ultrasonic characterization of cancellous bone using apparent integrated backscatter

Energy Technology Data Exchange (ETDEWEB)

Hoffmeister, B K [Department of Physics, Rhodes College, 2000 North Parkway, Memphis, TN 38112 (United States); III, C I Jones [Department of Physics, Rhodes College, 2000 North Parkway, Memphis, TN 38112 (United States); Caldwell, G J [Department of Physics, Rhodes College, 2000 North Parkway, Memphis, TN 38112 (United States); Kaste, S C [Department of Diagnostic Imaging, St Jude Children' s Research Hospital, Memphis, TN 38105 (United States)

2006-06-07

Apparent integrated backscatter (AIB) is a measure of the frequency-averaged (integrated) backscattered power contained in some portion of a backscattered ultrasonic signal. AIB has been used extensively to study soft tissues, but its usefulness as a tissue characterization technique for cancellous bone has not been demonstrated. To address this, we performed measurements on 17 specimens of cancellous bone over two different frequency ranges using a 1 MHz and 5 MHz broadband ultrasonic transducer. Specimens were obtained from bovine tibiae and prepared in the shape of cubes (15 mm side length) with faces oriented along transverse (anterior, posterior, medial and lateral) and longitudinal (superior and inferior) principal anatomic directions. A mechanical scanning system was used to acquire multiple backscatter signals from each direction for each cube. AIB demonstrated highly significant linear correlations with bone mineral density (BMD) for both the transverse (R{sup 2} = 0.817) and longitudinal (R{sup 2} = 0.488) directions using the 5 MHz transducer. In contrast, the correlations with density were much weaker for the 1 MHz transducer (R{sup 2} = 0.007 transverse, R{sup 2} = 0.228 longitudinal). In all cases where a significant correlation was observed, AIB was found to decrease with increasing BMD.

Monte Carlo simulation of the electron and X-ray depth distribution for quantitative electron probe microanalysis of PWR spent fuels

Energy Technology Data Exchange (ETDEWEB)

Kwon, Hyoung Mun; Lee, Hyung Kwon; Son, Young Zoon; Chun, Yong Bum [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

2011-10-15

Electron probe microanalysis requires several corrections to quantify an element of a specimen. The X-rays produced by the primary beam are created at some depth in the specimen. This distribution is usually represented as the function {Phi}(pz), and it is possible to calculate the correction factors for atomic number and absorption effects. The electron and X-ray depth distributions for a quantitative electron probe micro analysis were simulated by the CASINO Monte Carlo program to quantify some elements of the PWR spent fuel with 50 GWd/tU of burnup and 2 years of cooling time

Monte Carlo simulation of the electron and X-ray depth distribution for quantitative electron probe microanalysis of PWR spent fuels

International Nuclear Information System (INIS)

Kwon, Hyoung Mun; Lee, Hyung Kwon; Son, Young Zoon; Chun, Yong Bum

2011-01-01

Electron probe microanalysis requires several corrections to quantify an element of a specimen. The X-rays produced by the primary beam are created at some depth in the specimen. This distribution is usually represented as the function Φ(pz), and it is possible to calculate the correction factors for atomic number and absorption effects. The electron and X-ray depth distributions for a quantitative electron probe micro analysis were simulated by the CASINO Monte Carlo program to quantify some elements of the PWR spent fuel with 50 GWd/tU of burnup and 2 years of cooling time

Effects of Biota on Backscatter: Experiments with the Portable Acoustic Laboratory (PAL)

National Research Council Canada - National Science Library

Jones, Christopher

2003-01-01

.... Monitoring showed a sudden drop in backscatter, but this was short lived. Abundant mysid shrimp appeared to have caused microtopographic changes that quickly raised backscatter intensity to near-background levels...

Study of the influence of ultraviolet radiation on aggregative properties of blood red cell by light backscattering

International Nuclear Information System (INIS)

Azhnaj, L.; Chueltehm, D.

1988-01-01

The method based on the fact of measurable intensity of backscattered laser beam resulting from the angular distribution of scattered light is investigated. The method permits study of the mechanisms of aggregation and disaggregation processes by ultraviolet radiation and action of some inductors. The ultraviolet light acting directly on erythrocyte rouleaus of 10 x 100 μ causes the scattering of laser beam of wavelength 632,8 nm. According the above mentioned fact at an agle of approximately 180 0 the light intensity is measured. Stabilized blood sample is exposed to laser beam by means of fiber optics. Backscattering light transmitted through the photomultiplier and direct current supply is recorded. Quantitative concept of erythrocyte aggregation process is calculated from the plot. Blood sample is mixed by magnetic mixer and the measuring temperature is kept constantly at 37 0 C. Accordingly, the present model can adequately reproduce complex blood red cells kinetics. The influence of ultraviolet radiation and different kinds of inductors on erythrocytes' aggregation is experimentally studied depending on time. 2 figs. (B.Sh.)

Quantitative analysis of reflection electron energy loss spectra to determine electronic and optical properties of Fe–Ni alloy thin films

International Nuclear Information System (INIS)

Tahir, Dahlang; Oh, Sukh Kun; Kang, Hee Jae; Tougaard, Sven

2016-01-01

Highlights: • Electronic and optical properties of Fe-Ni alloy thin films grown on Si (1 0 0) were studied via quantitative analyses of reflection electron energy loss spectra (REELS). • The energy loss functions (ELF) are dominated by a plasmon peak at 23.6 eV for Fe and moves gradually to lower energies in Fe-Ni alloys towards the bulk plasmon energy of Ni at 20.5 eV. • Fe has a strong effect on the dielectric and optical properties of Fe-Ni alloy thin films even for an alloy with 72% Ni. Electronic and optical properties of Fe-Ni alloy thin films grown on Si (1 0 0) were studied via quantitative analyses of reflection electron energy loss spectra (REELS). - Abstract: Electronic and optical properties of Fe–Ni alloy thin films grown on Si (1 0 0) by ion beam sputter deposition were studied via quantitative analyses of reflection electron energy loss spectra (REELS). The analysis was carried out by using the QUASES-XS-REELS and QUEELS-ε(k,ω)-REELS softwares to determine the energy loss function (ELF) and the dielectric functions and optical properties by analyzing the experimental spectra. For Ni, the ELF shows peaks around 3.6, 7.5, 11.7, 20.5, 27.5, 67 and 78 eV. The peak positions of the ELF for Fe_2_8Ni_7_2 are similar to those of Fe_5_1Ni_4_9, even though there is a small peak shift from 18.5 eV for Fe_5_1Ni_4_9 to 18.7 eV for Fe_2_8Ni_7_2. A plot of n, k, ε_1, and ε_2 shows that the QUEELS-ε(k,ω)-REELS software for analysis of REELS spectra is useful for the study of optical properties of transition metal alloys. For Fe–Ni alloy with high Ni concentration (Fe_2_8Ni_7_2), ε_1, and ε_2 have strong similarities with those of Fe. This indicates that the presence of Fe in the Fe–Ni alloy thin films has a strong effect.

Electron beam energy monitoring using thermoluminescent dosimeters and electron back scattering

International Nuclear Information System (INIS)

Nelson, Vinod; Gray, Alison

2013-01-01

Periodic checks of megavoltage electron beam quality are a fundamental requirement in ensuring accurate radiotherapy treatment delivery. In the present work, thermoluminescent dosimeters (TLDs) positioned on either side of a lead sheet at the surface of a water equivalent phantom were used to monitor electron beam quality using the electron backscattering method. TLD100 and TLD100H were evaluated as upstream detectors and TLD200, TLD400 and TLD500 were evaluated as downstream detectors. The evaluation assessed the test sensitivity and correlation, long and short term reproducibility, dose dependence and glow curve features. A prototype of an in-air jig suitable for use in postal TLD dose audits was also developed and an initial evaluation performed. The results indicate that the TLD100-TLD200 combination provides a sensitive and reproducible method to monitor electron beam quality. The light weight and easily fabricated in-air jig was found to produce acceptable results and has the potential to be used by radiation monitoring agencies to carry out TLD postal quality assurance audits, similar to audits presently being conducted for photon beams. -- Highlights: ► Monitoring electron beam quality via electron backscattering was investigated. ► Different thermoluminescent materials were evaluated as detectors. ► A TLD100-TLD200 combination produced the most sensitive and reproducible results. ► An in-air jig was evaluated to allow measurements via postal dose audits

Correlation and uncertainties evaluation in backscattering of entrance surface air kerma measurements

Energy Technology Data Exchange (ETDEWEB)

Teixeira, G.J.; Sousa, C.H.S.; Peixoto, J.G.P., E-mail: gt@ird.gov.br [Instituto de Radioproteção e Dosimetria (IRD/CNEN-RJ), Rio de Janeiro, RJ (Brazil)

2017-07-01

The air kerma measurement is important to verify the applied doses in radiodiagnostic. The literature determines some methods to measure the entrance surface air kerma or entrance surface dose but some of this methods may increase the measurement with the backscattering. Were done setups of measurements to do correlations between them. The expanded uncertainty exceeded 5% for measurements with backscattering, reaching 8.36%, while in situations where the backscattering was avoided, the uncertainty was 3.43%. (author)

Quantitative measurement of lightning-induced electron precipitation using VLF remote sensing

Science.gov (United States)

Peter, William Bolton

This dissertation examines the detection of lightning-induced energetic electron precipitation via subionospheric Very Low Frequency (VLF) remote sensing. The primary measurement tool used is a distributed set of VLF observing sites, the Holographic Array for Ionospheric/Lightning Research (HAIL), located along the eastern side of the Rocky Mountains in the Central United States. Measurements of the VLF signal perturbations indicate that 90% of the precipitation occurs over a region ˜8 degrees in latitudinal extent, with the peak of the precipitation poleward displaced ˜7 degrees from the causative discharge. A comparison of the VLF signal perturbations recorded on the HAIL array with a comprehensive model of LEP events allows for the quantitative measurement of electron precipitation and ionospheric density enhancement with unprecedented quantitative detail. The model consists of three major components: a test-particle model of gyroresonant whistler-induced electron precipitation; a Monte Carlo simulation of energy deposition into the ionosphere; and a model of VLF subionospheric signal propagation. For the two representative LEP events studied, the model calculates peak VLF amplitude and phase perturbations within a factor of three of those observed, well within the expected variability of radiation belt flux levels. The modeled precipitated energy flux (E>45 keV) peaks at ˜1 x 10-2 [ergs s-1 cm -2], resulting in a peak loss of ˜0.001% from a single flux tube at L˜2.2, consistent with previous satellite measurements of LEP events. Metrics quantifying the ionospheric density enhancement (N ILDE) and the electron precipitation (Gamma) are strongly correlated with the VLF signal perturbations calculated by the model. A conversion ratio Psi relates VLF signal amplitude perturbations (DeltaA) to the time-integrated precipitation (100-300 keV) along the VLF path (Psi=Gamma / DeltaA). The total precipitation (100-300 keV) induced by one of the representative LEP

Determination of grain boundary mobility during recrystallization by statistical evaluation of electron backscatter diffraction measurements

International Nuclear Information System (INIS)

Basu, I.; Chen, M.; Loeck, M.; Al-Samman, T.; Molodov, D.A.

2016-01-01

One of the key aspects influencing microstructural design pathways in metallic systems is grain boundary motion. The present work introduces a method by means of which direct measurement of grain boundary mobility vs. misorientation dependence is made possible. The technique utilizes datasets acquired by means of serial electron backscatter diffraction (EBSD) measurements. The experimental EBSD measurements are collectively analyzed, whereby datasets were used to obtain grain boundary mobility and grain aspect ratio with respect to grain boundary misorientation. The proposed method is further validated using cellular automata (CA) simulations. Single crystal aluminium was cold rolled and scratched in order to nucleate random orientations. Subsequent annealing at 300 °C resulted in grains growing, in the direction normal to the scratch, into a single deformed orientation. Growth selection was observed, wherein the boundaries with misorientations close to Σ7 CSL orientation relationship (38° 〈111〉) migrated considerably faster. The obtained boundary mobility distribution exhibited a non-monotonic behavior with a maximum corresponding to misorientation of 38° ± 2° about 〈111〉 axes ± 4°, which was 10–100 times higher than the mobility values of random high angle boundaries. Correlation with the grain aspect ratio values indicated a strong growth anisotropy displayed by the fast growing grains. The observations have been discussed in terms of the influence of grain boundary character on grain boundary motion during recrystallization. - Highlights: • Statistical microstructure method to measure grain boundary mobility during recrystallization • Method implementation independent of material or crystal structure • Mobility of the Σ7 boundaries in 5N Al was calculated as 4.7 × 10"–"8 m"4/J ⋅ s. • Pronounced growth selection in the recrystallizing nuclei in Al • Boundary mobility values during recrystallization 2–3 orders of magnitude

A classification of spectral populations observed in HF radar backscatter from the E region auroral electrojets

Directory of Open Access Journals (Sweden)

S. E. Milan

Full Text Available Observations of HF radar backscatter from the auroral electrojet E region indicate the presence of five major spectral populations, as opposed to the two predominant spectral populations, types I and II, observed in the VHF regime. The Doppler shift, spectral width, backscatter power, and flow angle dependencies of these five populations are investigated and described. Two of these populations are identified with type I and type II spectral classes, and hence, are thought to be generated by the two-stream and gradient drift instabilities, respectively. The remaining three populations occur over a range of velocities which can greatly exceed the ion acoustic speed, the usual limiting velocity in VHF radar observations of the E region. The generation of these spectral populations is discussed in terms of electron density gradients in the electrojet region and recent non-linear theories of E region irregularity generation.

Key words. Ionosphere (ionospheric irregularities

Non-relativistic electron transport in metals: a Monte Carlo approach

International Nuclear Information System (INIS)

Rahimi, F.; Ghal eh, N.

2001-01-01

A simple Monte Carlo procedure is described for simulating the multiple scattering and absorption of electrons with the incident energy in the range 1-50 keV moving through a slab of uniformly distributed material of given atomic number, density and thickness. The simulation is based on a screened Rutherford cross-section and Bethe continuous energy-loss equation. A FORTRAN program is written to determine backscattering, transmission and absorption coefficients, providing the user with a graphical output of the electron trajectories. The results of several simulations are presented by using various numbers of electrons, showing a good agreement with the experiment. The program is used to analyze the relation between the energy and the range of electron in the slab, the backscattering, absorption, transmission coefficients and the angular distribution

Distinguishing Biologically Controlled Calcareous Biomineralization in Fossil Organisms Using Electron Backscatter Diffraction (EBSD)

Science.gov (United States)

Päßler, Jan-Filip; Jarochowska, Emilia; Bestmann, Michel; Munnecke, Axel

2018-02-01

Although carbonate-precipitating cyanobacteria are ubiquitous in aquatic ecosystems today, the criteria used to identify them in the geological record are subjective and rarely testable. Differences in the mode of biomineralization between cyanobacteria and eukaryotes, i.e. biologically induced calcification (BIM) vs. biologically controlled calcification (BCM), result in different crystallographic structures which might be used as a criterion to test cyanobacterial affinities. Cyanobacteria are often used as a ‘wastebasket taxon’, to which various microfossils are assigned. The lack of a testable criterion for the identification of cyanobacteria may bias their fossil record severely. We employed electron backscatter diffraction (EBSD) to investigate the structure of calcareous skeletons in two microproblematica widespread in Palaeozoic marine ecosystems: Rothpletzella, hypothesized to be a cyanobacterium, and an incertae sedis microorganism Allonema. We used a calcareous trilobite shell as a BCM reference. The mineralized structure of Allonema has a simple single-layered structure of acicular crystals perpendicular to the surface of the organism. The c-axes of these crystals are parallel to the elongation and thereby normal to the surface of the organism. EBSD pole figures and misorientation axes distribution reveal a fibre texture around the c-axis with a small degree of variation (up to 30°), indicating a highly ordered structure. A comparable pattern was found in the trilobite shell. This structure allows excluding biologically induced mineralization as the mechanism of shell formation in Allonema. In Rothpletzella, the c-axes of the microcrystalline sheath show a broader clustering compared to Allonema, but still reveal crystals tending to be perpendicular to the surface of the organism. The misorientation axes of adjacent crystals show an approximately random distribution. Rothpletzella also shares morphological similarities with extant cyanobacteria. We

Geometrically necessary dislocation densities in olivine obtained using high-angular resolution electron backscatter diffraction

Energy Technology Data Exchange (ETDEWEB)

Wallis, David, E-mail: davidwa@earth.ox.ac.uk [Department of Earth Sciences, University of Oxford, South Parks Road, Oxford, Oxfordshire, OX1 3AN (United Kingdom); Hansen, Lars N. [Department of Earth Sciences, University of Oxford, South Parks Road, Oxford, Oxfordshire, OX1 3AN (United Kingdom); Ben Britton, T. [Department of Materials, Imperial College London, Royal School of Mines, Exhibition Road, London SW7 2AZ (United Kingdom); Wilkinson, Angus J. [Department of Materials, University of Oxford, Parks Road, Oxford, Oxfordshire, OX1 3PH (United Kingdom)

2016-09-15

Dislocations in geological minerals are fundamental to the creep processes that control large-scale geodynamic phenomena. However, techniques to quantify their densities, distributions, and types over critical subgrain to polycrystal length scales are limited. The recent advent of high-angular resolution electron backscatter diffraction (HR-EBSD), based on diffraction pattern cross-correlation, offers a powerful new approach that has been utilised to analyse dislocation densities in the materials sciences. In particular, HR-EBSD yields significantly better angular resolution (<0.01°) than conventional EBSD (~0.5°), allowing very low dislocation densities to be analysed. We develop the application of HR-EBSD to olivine, the dominant mineral in Earth's upper mantle by testing (1) different inversion methods for estimating geometrically necessary dislocation (GND) densities, (2) the sensitivity of the method under a range of data acquisition settings, and (3) the ability of the technique to resolve a variety of olivine dislocation structures. The relatively low crystal symmetry (orthorhombic) and few slip systems in olivine result in well constrained GND density estimates. The GND density noise floor is inversely proportional to map step size, such that datasets can be optimised for analysing either short wavelength, high density structures (e.g. subgrain boundaries) or long wavelength, low amplitude orientation gradients. Comparison to conventional images of decorated dislocations demonstrates that HR-EBSD can characterise the dislocation distribution and reveal additional structure not captured by the decoration technique. HR-EBSD therefore provides a highly effective method for analysing dislocations in olivine and determining their role in accommodating macroscopic deformation. - Highlights: • Lattice orientation gradients in olivine were measured using HR-EBSD. • The limited number of olivine slip systems enable simple least squares inversion for GND

Optical diagnostics of CO2 laser-fusion targets using backscattered light

International Nuclear Information System (INIS)

Casperson, D.E.

1981-01-01

With the f/2.4 focusing optics on one of the eight Helios CO 2 laser beam lines, direct backscattered light from a variety of glass microballoon targets has been observed. The quantities that have been measured include: (1) the total backscattered energy; (2) relative amplitudes of the backscattered fundamental and low harmonics (n = 1, 2, 3) of the 10.6 μm incident light; (3) the 3/2 harmonic emission from a double pulse backscatter experiment; (4) the temporally resolved 10.6 μm light using a fast pyroelectric detector and a Los Alamos 5-GHz oscilloscope; and (5) the time-integrated spectrally resolved fundamental using a 3/4 meter spectrometer and a high resolution pyroelectric detector array (resolution approx. 40 A at 10.6 μm). The suitability of these diagnostics for evaluating the CO 2 laser plasma in terms of stimulated scattering processes, plasma density gradients, velocity of the critical surface, etc., is discussed

A QUANTITATIVE STUDY OF THE EVOLUTION OF GASES FROM ELECTRON TUBES AND MATERIALS.

Science.gov (United States)

A continuous quantitative and qualitative gas analysis system has been designed, built and calibrated. The system incorporates an omegatron mass...processing and materials parameters as they affect the kinds and quantities of gases evolved by electron tubes. CO2, CO, and H2 in roughly equal

Electron Backscatter Diffraction (EBSD) Analysis and U-Pb Geochronology of the Oldest Lunar Zircon: Constraining Early Lunar Differentiation and Dating Impact-Related Deformation

Science.gov (United States)

Timms, Nick; Nemchin, Alexander; Grange, Marion; Reddy, Steve; Pidgeon, Bob; Geisler, Thorsten; Meyer, Chuck

2009-01-01

The evolution of the early moon was dominated by two processes (i) crystallization of the Lunar Magma Ocean (LMO) and differentiation of potassium-rare earth element-phosphorous-rich residual magma reservoir referred to as KREEP, and (ii) an intense meteorite bombardment referred to as lunar cataclysm . The exact timing of these processes is disputed, and resolution relies on collection and interpretation of precise age data. This study examines the microstructure and geochronology of zircon from lunar impact breccias collected during the Apollo 17 mission. A large zircon clast within lunar breccia 72215,195 shows sector zoning in optical microscopy, cathodoluminescence (CL) imaging and Raman mapping, and indicates that it was a relict fragment of a much larger magmatic grain. Sensitive high resolution ion microprobe (SHRIMP) U-Pb analysis of the zircon shows that U and Th concentration correlate with sector zoning, with darkest CL domains corresponding with high-U and Th (approx.150 and approx.100 ppm respectively), and the brightest-CL sectors containing approx.30-50 ppm U and approx.10-20 ppm Th. This indicates that variations in optical CL and Raman properties correspond to differential accumulation of alpha-radiation damage in each sector. Electron backscatter diffraction (EBSD) mapping shows that the quality of electron backscatter patterns (band contrast) varies with sector zoning, with the poorest quality patterns obtained from high-U and Th, dark-CL zones. EBSD mapping also reveals a deformation microstructure that is cryptic in optical, CL and Raman imaging. Two orthogonal sets of straight discrete and gradational low-angle boundaries accommodate approx.12 misorientation across the grain. The deformation bands are parallel to the crystallographic {a}-planes of the zircon, have misorientation axes parallel to the c-axis, and are geometrically consistent with formation by dislocation creep associated with {010} slip. The deformation bands are unlike curved

Quantitative characterization of microstructure of pure copper processed by ECAP

Czech Academy of Sciences Publication Activity Database

Šedivý, O.; Beneš, V.; Ponížil, P.; Král, Petr; Sklenička, Václav

2013-01-01

Roč. 32, č. 2 (2013), s. 65-75 ISSN 1580-3139 Institutional support: RVO:68081723 Keywords : electron backscatter diffraction * ultrafine-grained metals * microstructure * microstructure characterization * grain boundaries Subject RIV: BB - Applied Statistics, Operational Research Impact factor: 0.697, year: 2013

Characterizing Indian Ocean manganese nodule-bearing seafloor using multi-beam angular backscatter

Digital Repository Service at National Institute of Oceanography (India)

Chakraborty, B.; Kodagali, V.N.

backscattering in delineating seafloor parameters characteristic of nodule-rich sediments. In this paper, processed Hydrosweep multi-beam backscatter data from 45 spot locations in the CIOB (where nodule samples are available) were analysed to estimate seafloor...

The experimental method of measurement for spatial distribution of full aperture backscatter light by circular PIN-array

International Nuclear Information System (INIS)

Zhao Xuefeng; Wang Chuanke; Hu Feng; Kuang Longyu; Wang Zhebin; Li Sanwei; Liu Shengye; Jiang Gang

2011-01-01

The spatial distribution of backscatter light is very important for understanding the production of backscatter light. The experimental method of spatial distribution of full aperture backscatter light is based on the circular PIN array composed of concentric orbicular multi-PIN detectors. The image of backscatter light spatial distribution of full aperture SBS is obtained by measuring spatial distribution of full aperture backscatter light using the method in the experiment of laser hohlraum targets interaction at 'Shenguang II'. A preliminary method to measure spatial distribution of full aperture backscatter light is established. (authors)

RHIC electron lenses upgrades

Energy Technology Data Exchange (ETDEWEB)

Gu, X. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Altinbas, Z. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Bruno, D. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Binello, S. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Costanzo, M. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Drees, A. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Fischer, W. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Gassner, D. M. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Hock, J. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Hock, K. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Harvey, M. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Luo, Y. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Marusic, A. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Mi, C. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Mernick, K. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Minty, M. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Michnoff, R. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Miller, T. A. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Pikin, A. I. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Robert-Demolaize, G. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Samms, T. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Shrey, T. C. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Schoefer, V. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Tan, Y. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Than, R. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; Thieberger, P. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.; White, S. M. [Brookhaven National Lab. (BNL), Upton, NY (United States). Collider-Accelerator Dept.

2015-05-03

In the Relativistic Heavy Ion Collider (RHIC) 100 GeV polarized proton run in 2015, two electron lenses were used to partially compensate for the head-on beam-beam effect for the first time. Here, we describe the design of the current electron lens, detailing the hardware modifications made after the 2014 commissioning run with heavy ions. A new electron gun with 15-mm diameter cathode is characterized. The electron beam transverse profile was measured using a YAG screen and fitted with a Gaussian distribution. During operation, the overlap of the electron and proton beams was achieved using the electron backscattering detector in conjunction with an automated orbit control program.

Towards quantitative electrostatic potential mapping of working semiconductor devices using off-axis electron holography

DEFF Research Database (Denmark)

Yazdi, Sadegh; Kasama, Takeshi; Beleggia, Marco

2015-01-01

Pronounced improvements in the understanding of semiconductor device performance are expected if electrostatic potential distributions can be measured quantitatively and reliably under working conditions with sufficient sensitivity and spatial resolution. Here, we employ off-axis electron...... holography to characterize an electrically-biased Si p-. n junction by measuring its electrostatic potential, electric field and charge density distributions under working conditions. A comparison between experimental electron holographic phase images and images obtained using three-dimensional electrostatic...

Multi-temporal RADARSAT-1 and ERS backscattering signatures of coastal wetlands in southeastern Louisiana

Science.gov (United States)

Kwoun, Oh-Ig; Lu, Z.

2009-01-01

Using multi-temporal European Remote-sensing Satellites (ERS-1/-2) and Canadian Radar Satellite (RADARSAT-1) synthetic aperture radar (SAR) data over the Louisiana coastal zone, we characterize seasonal variations of radar backscat-tering according to vegetation type. Our main findings are as follows. First, ERS-1/-2 and RADARSAT-1 require careful radiometric calibration to perform multi-temporal backscattering analysis for wetland mapping. We use SAR backscattering signals from cities for the relative calibration. Second, using seasonally averaged backscattering coefficients from ERS-1/-2 and RADARSAT-1, we can differentiate most forests (bottomland and swamp forests) and marshes (freshwater, intermediate, brackish, and saline marshes) in coastal wetlands. The student t-test results support the usefulness of season-averaged backscatter data for classification. Third, combining SAR backscattering coefficients and an optical-sensor-based normalized difference vegetation index can provide further insight into vegetation type and enhance the separation between forests and marshes. Our study demonstrates that SAR can provide necessary information to characterize coastal wetlands and monitor their changes.

Effect of species structure and dielectric constant on C-band forest backscatter

Science.gov (United States)

Lang, R. H.; Landry, R.; Kilic, O.; Chauhan, N.; Khadr, N.; Leckie, D.

1993-01-01

A joint experiment between Canadian and USA research teams was conducted early in Oct. 1992 to determine the effect of species structure and dielectric variations on forest backscatter. Two stands, one red pine and one jack pine, in the Petawawa National Forestry Institute (PNFI) were utilized for the experiment. Extensive tree architecture measurements had been taken by the Canada Centre for Remote Sensing (CCRS) several months earlier by employing a Total Station surveying instrument which provides detailed information on branch structure. A second part of the experiment consisted of cutting down several trees and using dielectric probes to measure branch and needle permittivity values at both sites. The dielectric and the tree geometry data were used in the George Washington University (GWU) Vegetation Model to determine the C band backscattering coefficients of the individual stands for VV polarization. The model results show that backscatter at C band comes mainly from the needles and small branches and the upper portion of the trunks acts only as an attenuator. A discussion of variation of backscatter with specie structure and how dielectric variations in needles for both species may affect the total backscatter returns is provided.

An optimized Faraday cage design for electron beam current measurements

International Nuclear Information System (INIS)

Turner, J.N.; Hausner, G.G.; Parsons, D.F.

1975-01-01

A Faraday cage detector is described for measuring electron beam intensity for use with energies up to 1.2 Mev, with the present data taken at 100 keV. The design features a readily changeable limiting aperture and detector cup geometry, and a secondary electron suppression grid. The detection efficiency of the cage is shown to be limited only by primary backscatter through the detector solid angle of escape, which is optimized with respect to primary backscattered electrons and secondary electron escape. The geometry and stopping material of the detection cup are varied, and the results show that for maximum detection efficiency with carbon as the stopping mateiral, the solid angle of escape must be equal to or less than 0.05πsr. The experimental results are consistent within the +-2% accuracy of the detection electronics, and are not limited by the Faraday cage detection efficiency. (author)

A high intensity beam line of γ-rays up to 22MeV energy based on Compton backscattering

International Nuclear Information System (INIS)

Guo, W.; Xu, W.; Chen, J.G.; Ma, Y.G.; Cai, X.Z.; Wang, H.W.; Xu, Y.; Wang, C.B.; Lu, G.C.; Tian, W.D.; Yuan, R.Y.; Xu, J.Q.; Wei, Z.Y.; Yan, Z.; Shen, W.Q.

2007-01-01

Shanghai Laser Electron Gamma Source, a high intensity beam line of γ-ray, has been proposed recently. The beam line is expected to generate γ-rays up to the maximum energy of 22MeV by Compton backscattering between a CO 2 laser and electrons in the 3.5 GeV storage ring of the Shanghai Synchrotron Radiation Facility. The flux of non-collimated γ-rays is estimated to be 10 9 -10 10 s -1 when a CO 2 laser of several hundred Watt power is employed. We will discuss physics issues in the design and optimization of the beam line

Development of a secondary electron energy analyzer for a transmission electron microscope.

Science.gov (United States)

Magara, Hideyuki; Tomita, Takeshi; Kondo, Yukihito; Sato, Takafumi; Akase, Zentaro; Shindo, Daisuke

2018-04-01

A secondary electron (SE) energy analyzer was developed for a transmission electron microscope. The analyzer comprises a microchannel plate (MCP) for detecting electrons, a coil for collecting SEs emitted from the specimen, a tube for reducing the number of backscattered electrons incident on the MCP, and a retarding mesh for selecting the energy of SEs incident on the MCP. The detection of the SEs associated with charging phenomena around a charged specimen was attempted by performing electron holography and SE spectroscopy using the energy analyzer. The results suggest that it is possible to obtain the energy spectra of SEs using the analyzer and the charging states of a specimen by electron holography simultaneously.

Polarization phenomena on coherent particle backscattering by random media

International Nuclear Information System (INIS)

Gorodnichev, E.E.; Dudarev, S.L.; Rogozkin, D.B.

1990-01-01

An exact solution is found for the problem of coherent enhanced backscattering of spin 1/2 particles by random media with small-radius scatterers. The polarization features in the angular spectrum are analyzed for particles reflected by three- and two-dimensional disordered systems and by medium with Anderson disorder (periodic system of random scatterers). The analysis is carried out in the case of magnetic and spin-orbit interaction with the scattering centers. The effects predicted have not any analogues on coherent backscattering of light and scalar waves

SU-C-BRC-05: Monte Carlo Calculations to Establish a Simple Relation of Backscatter Dose Enhancement Around High-Z Dental Alloy to Its Atomic Number

Energy Technology Data Exchange (ETDEWEB)

Utsunomiya, S; Kushima, N; Katsura, K; Tanabe, S; Hayakawa, T; Sakai, H; Yamada, T; Takahashi, H; Abe, E; Wada, S; Aoyama, H [Niigata University, Niigata (Japan)

2016-06-15

Purpose: To establish a simple relation of backscatter dose enhancement around a high-Z dental alloy in head and neck radiation therapy to its average atomic number based on Monte Carlo calculations. Methods: The PHITS Monte Carlo code was used to calculate dose enhancement, which is quantified by the backscatter dose factor (BSDF). The accuracy of the beam modeling with PHITS was verified by comparing with basic measured data namely PDDs and dose profiles. In the simulation, a high-Z alloy of 1 cm cube was embedded into a tough water phantom irradiated by a 6-MV (nominal) X-ray beam of 10 cm × 10 cm field size of Novalis TX (Brainlab). The ten different materials of high-Z alloys (Al, Ti, Cu, Ag, Au-Pd-Ag, I, Ba, W, Au, Pb) were considered. The accuracy of calculated BSDF was verified by comparing with measured data by Gafchromic EBT3 films placed at from 0 to 10 mm away from a high-Z alloy (Au-Pd-Ag). We derived an approximate equation to determine the relation of BSDF and range of backscatter to average atomic number of high-Z alloy. Results: The calculated BSDF showed excellent agreement with measured one by Gafchromic EBT3 films at from 0 to 10 mm away from the high-Z alloy. We found the simple linear relation of BSDF and range of backscatter to average atomic number of dental alloys. The latter relation was proven by the fact that energy spectrum of backscatter electrons strongly depend on average atomic number. Conclusion: We found a simple relation of backscatter dose enhancement around high-Z alloys to its average atomic number based on Monte Carlo calculations. This work provides a simple and useful method to estimate backscatter dose enhancement from dental alloys and corresponding optimal thickness of dental spacer to prevent mucositis effectively.

Refinement of Monte Carlo simulations of electron-specimen interaction in low-voltage SEM

International Nuclear Information System (INIS)

Kieft, Erik; Bosch, Eric

2008-01-01

A Monte Carlo tool is presented for the simulation of secondary electron (SE) emission in a scanning electron microscope (SEM). The tool is based on the Geant4 platform of CERN. The modularity of this platform makes it comparatively easy to add and test individual physical models. Our aim has been to develop a flexible and generally applicable tool, while at the same time including a good description of low-energy (<50 eV) interactions of electrons with matter. To this end we have combined Mott cross-sections with phonon-scattering based cross-sections for the elastic scattering of electrons, and we have adopted a dielectric function theory approach for inelastic scattering and generation of SEs. A detailed model of the electromagnetic fields from an actual SEM column has been included in the tool for ray tracing of secondary and backscattered electrons. Our models have been validated against experimental results through comparison of the simulation results with experimental yields, SE spectra and SEM images. It is demonstrated that the resulting simulation package is capable of quantitatively predicting experimental SEM images and is an important tool in building a deeper understanding of SEM imaging.

Mapping ionospheric backscatter measured by the SuperDARN HF radars – Part 2: Assessing SuperDARN virtual height models

Directory of Open Access Journals (Sweden)

T. K. Yeoman

2008-05-01

Full Text Available The Super Dual Auroral Radar Network (SuperDARN network of HF coherent backscatter radars form a unique global diagnostic of large-scale ionospheric and magnetospheric dynamics in the Northern and Southern Hemispheres. Currently the ground projections of the HF radar returns are routinely determined by a simple rangefinding algorithm, which takes no account of the prevailing, or indeed the average, HF propagation conditions. This is in spite of the fact that both direct E- and F-region backscatter and 1½-hop E- and F-region backscatter are commonly used in geophysical interpretation of the data. In a companion paper, Chisham et al. (2008 have suggested a new virtual height model for SuperDARN, based on average measured propagation paths. Over shorter propagation paths the existing rangefinding algorithm is adequate, but mapping errors become significant for longer paths where the roundness of the Earth becomes important, and a correct assumption of virtual height becomes more difficult. The SuperDARN radar at Hankasalmi has a propagation path to high power HF ionospheric modification facilities at both Tromsø on a ½-hop path and SPEAR on a 1½-hop path. The SuperDARN radar at Þykkvibǽr has propagation paths to both facilities over 1½-hop paths. These paths provide an opportunity to quantitatively test the available SuperDARN virtual height models. It is also possible to use HF radar backscatter which has been artificially induced by the ionospheric heaters as an accurate calibration point for the Hankasalmi elevation angle of arrival data, providing a range correction algorithm for the SuperDARN radars which directly uses elevation angle. These developments enable the accurate mappings of the SuperDARN electric field measurements which are required for the growing number of multi-instrument studies of the Earth's ionosphere and magnetosphere.

Quantitative electron microscopical autoradiography of calcium during amelogenesis

International Nuclear Information System (INIS)

Nagai, Yoshinori; Frank, R.M.

1975-01-01

The migration of 45 Ca through the stratum intermedium and through the secreting ameloblasts towards enamel has been studied by electron microscopical autoradiography in the toothgerms of newborn cats. A quantitative procedure was applied to the study of the 45 Ca migration in amelogenesis and two pathways were demonstrated. The relatively more important direct route passed through the stratum intermedium and the ameloblast intercellular spaces and reached the enamel directly. The second pathway consisted of an intracellular migration through the ameloblast. 45 Ca penetrated the cell through its basal pole. The mitochondrias were the most highly labeled organelles at the different experimental time intervals studied. A total absence of silver grains was noted over the secretory ameloblastic bodies. At 6 hours, the highest labeling was observed over enamel. (auth.)

Selection Algorithm for the CALIPSO Lidar Aerosol Extinction-to-Backscatter Ratio

Science.gov (United States)

Omar, Ali H.; Winker, David M.; Vaughan, Mark A.

2006-01-01

The extinction-to-backscatter ratio (S(sub a)) is an important parameter used in the determination of the aerosol extinction and subsequently the optical depth from lidar backscatter measurements. We outline the algorithm used to determine Sa for the Cloud and Aerosol Lidar and Infrared Pathfinder Spaceborne Observations (CALIPSO) lidar. S(sub a) for the CALIPSO lidar will either be selected from a look-up table or calculated using the lidar measurements depending on the characteristics of aerosol layer. Whenever suitable lofted layers are encountered, S(sub a) is computed directly from the integrated backscatter and transmittance. In all other cases, the CALIPSO observables: the depolarization ratio, delta, the layer integrated attenuated backscatter, beta, and the mean layer total attenuated color ratio, gamma, together with the surface type, are used to aid in aerosol typing. Once the type is identified, a look-up-table developed primarily from worldwide observations, is used to determine the S(sub a) value. The CALIPSO aerosol models include desert dust, biomass burning, background, polluted continental, polluted dust, and marine aerosols.

Cavitation inception by the backscattering of pressure waves from a bubble interface

Energy Technology Data Exchange (ETDEWEB)

Takahira, Hiroyuki, E-mail: takahira@me.osakafu-u.ac.jp; Ogasawara, Toshiyuki, E-mail: oga@me.osakafu-u.ac.jp; Mori, Naoto, E-mail: su101064@edu.osakafu-u.ac.jp; Tanaka, Moe [Osaka Prefecture University, 1-1 Gakuen-cho, Naka-ku, Sakai-shi, Osaka 599-8531 (Japan)

2015-10-28

The secondary cavitation that occurs by the backscattering of focused ultrasound from a primary cavitation bubble caused by the negative pressure part of the ultrasound (Maxwell, et al., 2011) might be useful for the energy exchange due to bubble oscillations in High Intensity Focused Ultrasound (HIFU). The present study is concerned with the cavitation inception by the backscattering of ultrasound from a bubble. In the present experiment, a laser-induced bubble which is generated by a pulsed focused laser beam with high intensity is utilized as a primary cavitation bubble. After generating the bubble, focused ultrasound is emitted to the bubble. The acoustic field and the bubble motion are observed with a high-speed video camera. It is confirmed that the secondary cavitation bubble clouds are generated by the backscattering from the laser-induced bubble. The growth of cavitation bubble clouds is analyzed with the image processing method. The experimental results show that the height and width of the bubble clouds grow in stepwise during their evolution. The direct numerical simulations are also conducted for the backscattering of incident pressure waves from a bubble in order to evaluate a pressure field near the bubble. It is shown that the ratio of a bubble collapse time t{sub 0} to a characteristic time of wave propagation t{sub S}, η = t{sub 0}/t{sub s}, is an important determinant for generating negative pressure region by backscattering. The minimum pressure location by the backscattering in simulations is in good agreement with the experiment.

Backscattering and negative polarization of agglomerate particles.

Science.gov (United States)

Zubko, Evgenij; Shkuratov, Yuriy; Hart, Matthew; Eversole, Jay; Videen, Gorden

2003-09-01

We used the discrete dipole approximation to study the backscattering of agglomerate particles consisting of oblong monomers. We varied the aspect ratio of the monomers from approximately 1 (sphere) to 4, while we kept the total particle volume equivalent to that of an x = 10 sphere for m = 1.59 + i0 and 1.50 + i0 and considered two values of agglomerate packing density: rho = 0.25 and rho = 0.1. We found that these particles do not display a prominent brightness opposition effect but do produce significant negative polarization over a range of near-backscattering angles. Increasing the monomers' aspect ratio can make the negative polarization much more prominent. We have noted also that decreasing m and p can reduce the amplitude of the negative polarization for these particles.

Tropospheric aerosol backscatter background mode at CO2 wavelengths

Science.gov (United States)

Rothermel, Jeffry; Bowdle, David A.; Menzies, Robert T.; Post, Madison J.; Vaughan, J. Michael

1989-01-01

A comparison is made between three climatologies of backscatter measurements in the troposphere and lower stratosphere at CO2 wavelengths. These were obtained from several locations using ground-based and airborne lidar systems. All three measurement sets show similar features, specifically, a high frequency of occurrence of low backscatter over a limited range of values in the middle and upper atmosphere (the 'background mode'). This background mode is important for the design and performance simulation of the prospective satellite sensors that rely on atmospheric aerosols as scattering targets.

Stimulated Brillouin backscattering losses in weakly inhomogeneous laser-produced plasmas

International Nuclear Information System (INIS)

Eidmann, K.; Brederlow, G.; Brodmann, R.; Petsch, R.; Sigel, R.; Tsarkiris, G.; Volk, R.; Witkowski, S.

1979-02-01

Studies of the reflection from a plane solid target plasma produced with a 1TW iodine laser (lambda = 1.3μm) at pulse durations of 300 ps are presented. The specularly reflected and the backscattered light was observed separately at different angles of incidence, intensities and spot sizes (up to 400 μm). Stimulated Brillouin scattering was identified as the main mechanism for backscattering with saturation at 20 - 30% reflection. (orig.) [de

Quantitative in situ magnetization reversal studies in Lorentz microscopy and electron holography.

Science.gov (United States)

Rodríguez, L A; Magén, C; Snoeck, E; Gatel, C; Marín, L; Serrano-Ramón, L; Prieto, J L; Muñoz, M; Algarabel, P A; Morellon, L; De Teresa, J M; Ibarra, M R

2013-11-01

A generalized procedure for the in situ application of magnetic fields by means of the excitation of the objective lens for magnetic imaging experiments in Lorentz microscopy and electron holography is quantitatively described. A protocol for applying magnetic fields with arbitrary in-plane magnitude and orientation is presented, and a freeware script for Digital Micrograph(™) is provided to assist the operation of the microscope. Moreover, a method to accurately reconstruct hysteresis loops is detailed. We show that the out-of-plane component of the magnetic field cannot be always neglected when performing quantitative measurements of the local magnetization. Several examples are shown to demonstrate the accuracy and functionality of the methods. © 2013 Elsevier B.V. All rights reserved.

Investigation of small-scale tokamak plasma turbulence by correlative UHR backscattering diagnostics

International Nuclear Information System (INIS)

Gusakov, E Z; Gurchenko, A D; Altukhov, A B; Bulanin, V V; Esipov, L A; Kantor, M Yu; Kouprienko, D V; Lashkul, S I; Petrov, A V; Stepanov, A Yu

2006-01-01

Fine scale turbulence is considered nowadays as a possible candidate for the explanation of anomalous ion and electron energy transport in magnetized fusion plasmas. The unique correlative upper hybrid resonance backscattering (UHR BS) technique is applied at the FT-2 tokamak for investigation of density fluctuations excited in this turbulence. The measurements are carried out in Ohmic discharge at several values of plasma current and density and during current ramp up experiment. The moveable focusing antennas set have been used in experiments allowing probing out of equatorial plane. The radial wave number spectra of the small-scale component of tokamak turbulence are determined from the correlation data with high spatial resolution. Two small-scale modes possessing substantially different phase velocities are observed in plasma under conditions when the threshold for the electron temperature gradient mode excitation is overcome. The possibility of plasma poloidal velocity profile determination using the UHR BS signal is demonstrated

Quantitative analysis of Josephson-quasiparticle current in superconducting single-electron transistors

International Nuclear Information System (INIS)

Nakamura, Y.; Chen, C.D.; Tsai, J.S.

1996-01-01

We have investigated Josephson-quasiparticle (JQP) current in superconducting single-electron transistors in which charging energy E C was larger than superconducting gap energy Δ and junction resistances were much larger than R Q ≡h/4e 2 . We found that not only the shapes of the JQP peaks but also their absolute height were reproduced quantitatively with a theory by Averin and Aleshkin using a Josephson energy of Ambegaokar-Baratoff close-quote s value. copyright 1996 The American Physical Society

High Resolution Bathymetry and Backscatter of a High-Frequency Test Area

National Research Council Canada - National Science Library

Flood, Roger

2001-01-01

.... This is due to the presence of east-west trending wave-generated ripples with amplitudes of about 15 cm and wavelengths of about 75 cm on the ridge, with backscatter being higher when the sound beams are perpendicular to the ripples. The backscatter patterns on multi beam records may thus be used for determining the presence and orientation of small-scale topographic relief.

Radio-analysis of hydrogenous material using neutron back-scattering technique

International Nuclear Information System (INIS)

Holly, Wiam Ahmed Alteghany

2014-10-01

In this work, we have explored the possibility of using neutron back-scattering technique in performing radio analysis for samples of hydrogenous materials such as explosives, drugs, crude oil and water, looking for different signals that may be used to discriminate these samples. Monte Carlo simulations were carried out to model the detection system and select the optimal geometry as well. The results were determined in terms of the energy spectra of the back-scattered neutrons.(Author)

Quantitative electron microscopical autoradiography of calcium during dentinogenesis

Energy Technology Data Exchange (ETDEWEB)

Nagai, Y [Tokyo Dental Coll. (Japan); Frank, R M

1975-03-01

/sup 45/Ca migration from the dental papilla and the odontablasts towards predentin and dentin has been studied through electron microscopical autoradiography in toothgerms of newborn cats. A quantitative procedure was applied to the study of the /sup 45/Ca migration in dentinogenesis. Two pathways of almost identical importance have been demonstrated. The direct pathway followed the intercellular spaces of the dental papilla and of the odontoblasts and reached the dentin via predentin. The second road, after passage through the intercellular spaces of the dental papilla, consisted of an intracellular migration through the odontoblast. The mitochondria and the golgi apparatus were progressively the most labelet at 5 min., 30 min. and 1 h. after intravenous injection. The calcium diffused into the odontablastic process without being associated with the dense granule. At 6 hours, maximum radioactivity was observed in the intertubular dentin.

RFID tag modification for full depth backscatter modulation

Science.gov (United States)

Scott, Jeffrey Wayne [Pasco, WA; Pratt, Richard M [Richland, WA

2010-07-20

A modulated backscatter radio frequency identification device includes a diode detector configured to selectively modulate a reply signal onto an incoming continuous wave; communications circuitry configured to provide a modulation control signal to the diode detector, the diode detector being configured to modulate the reply signal in response to be modulation control signal; and circuitry configured to increase impedance change at the diode detector which would otherwise not occur because the diode detector rectifies the incoming continuous wave while modulating the reply signal, whereby reducing the rectified signal increases modulation depth by removing the reverse bias effects on impedance changes. Methods of improving depth of modulation in a modulated backscatter radio frequency identification device are also provided.

Standard-target calibration of an acoustic backscatter system

Science.gov (United States)

Foote, Kenneth G.; Martini, Marinna A.

2010-01-01

The standard-target method used to calibrate scientific echo sounders and other scientific sonars by a single, solid elastic sphere is being adapted to acoustic backscatter (ABS) systems. Its first application, to the AQUAscat 1000, is described. The on-axis sensitivity and directional properties of transducer beams at three operating frequencies, nominally 1, 2.5, and 4 MHz, have been determined using a 10-mm-diameter sphere of tungsten carbide with 6% cobalt binder. Preliminary results are reported for the 1-MHz transducer. Their application to measurements of suspended sediment made in situ with the same device is described. This will enable the data to be expressed directly in physical units of volume backscattering.

ISIS 1 measurements of high-frequency backscatter inside the ionosphere

International Nuclear Information System (INIS)

James, H.G.

1989-01-01

A study has been made of high-frequency backscatter observed by the ISIS 1 topside sounder at orbital heights from approximately 600 to 800 km. Signals are detected during high-latitude passes at radar ranges x of up to about 400 km and at frequencies from about the X mode cutoff at the spacecraft (usually around 5 MHz) up to 10 MHz typically and 18 MHz occasionally. The signals are interpreted as coherent aspect-sensitive scatter. The absolute power of return signals at high latitudes usually varies as x -2 for x ≤ 150 km. This implies that the scattering cross-section density σ is constant for all azimuths about the magnetic field and for ranges out to 150 km or, in other words, that irregularity patches have a constant σ over cross-field dimensions of 300 km. At larger ranges the signal often falls off more sharply with x, indicating azimuthal variations in σ. The cross section scaled from the data using the radar equation is found to have values centered near 10 -8 to 10 -7 m -1 for the most intense signals, referred to an assumed polar-aspect angle sensitivity. However, the magnitude of σ drops by about 2 orders of magnitude in the frequency range 5-15 MHz. Previous statistical studies have established that strong backscatter is restricted to auroral latitudes. Here the polar distribution of backscatter has been plotted for two sets of passes over the south pole, one collected during austral winter and the other during summer. The strongest backscatter is located at invariant latitudes around 80 degree. Backscatter is significantly stronger and distributed more extensively over the polar cap in winter than in summer

Forty-five degree backscattering-mode nonlinear absorption imaging in turbid media.

Science.gov (United States)

Cui, Liping; Knox, Wayne H

2010-01-01

Two-color nonlinear absorption imaging has been previously demonstrated with endogenous contrast of hemoglobin and melanin in turbid media using transmission-mode detection and a dual-laser technology approach. For clinical applications, it would be generally preferable to use backscattering mode detection and a simpler single-laser technology. We demonstrate that imaging in backscattering mode in turbid media using nonlinear absorption can be obtained with as little as 1-mW average power per beam with a single laser source. Images have been achieved with a detector receiving backscattered light at a 45-deg angle relative to the incoming beams' direction. We obtain images of capillary tube phantoms with resolution as high as 20 microm and penetration depth up to 0.9 mm for a 300-microm tube at SNR approximately 1 in calibrated scattering solutions. Simulation results of the backscattering and detection process using nonimaging optics are demonstrated. A Monte Carlo-based method shows that the nonlinear signal drops exponentially as the depth increases, which agrees well with our experimental results. Simulation also shows that with our current detection method, only 2% of the signal is typically collected with a 5-mm-radius detector.

Laser-based air data system for aircraft control using Raman and elastic backscatter for the measurement of temperature, density, pressure, moisture, and particle backscatter coefficient.

Science.gov (United States)

Fraczek, Michael; Behrendt, Andreas; Schmitt, Nikolaus

2012-01-10

Flight safety in all weather conditions demands exact and reliable determination of flight-critical air parameters. Air speed, temperature, density, and pressure are essential for aircraft control. Conventional air data systems can be impacted by probe failure caused by mechanical damage from hail, volcanic ash, and icing. While optical air speed measurement methods have been discussed elsewhere, in this paper, a new concept for optically measuring the air temperature, density, pressure, moisture, and particle backscatter is presented, being independent on assumptions on the atmospheric state and eliminating the drawbacks of conventional aircraft probes by providing a different measurement principle. The concept is based on a laser emitting laser pulses into the atmosphere through a window and detecting the signals backscattered from a fixed region just outside the disturbed area of the fuselage flows. With four receiver channels, different spectral portions of the backscattered light are extracted. The measurement principle of air temperature and density is based on extracting two signals out of the rotational Raman (RR) backscatter signal of air molecules. For measuring the water vapor mixing ratio-and thus the density of the moist air-a water vapor Raman channel is included. The fourth channel serves to detect the elastic backscatter signal, which is essential for extending the measurements into clouds. This channel contributes to the detection of aerosols, which is interesting for developing a future volcanic ash warning system for aircraft. Detailed and realistic optimization and performance calculations have been performed based on the parameters of a first prototype of such a measurement system. The impact and correction of systematic error sources, such as solar background at daytime and elastic signal cross talk appearing in optically dense clouds, have been investigated. The results of the simulations show the high potential of the proposed system for

Optical Modeling of Spectral Backscattering and Remote Sensing Reflectance From Emiliania huxleyi Blooms

Directory of Open Access Journals (Sweden)

Griet Neukermans

2018-05-01

Full Text Available In this study we develop an analytical model for spectral backscattering and ocean color remote sensing of blooms of the calcifying phytoplankton species Emiliania huxleyi. Blooms of this coccolithophore species are ubiquitous and particularly intense in temperate and subpolar ocean waters. We first present significant improvements to our previous analytical light backscattering model for E. huxleyi coccoliths and coccospheres by accounting for the elliptical shape of coccoliths and the multi-layered coccosphere architecture observed on detailed imagery of E. huxleyi liths and coccospheres. Our new model also includes a size distribution function that closely matches measured E. huxleyi size distributions. The model for spectral backscattering is then implemented in an analytical radiative transfer model to evaluate the variability of spectral remote sensing reflectance with respect to changes in the size distribution of the coccoliths and during a hypothetical E. huxleyi bloom decay event in which coccospheres shed their liths. Our modeled remote sensing reflectance spectra reproduced well the bright milky turquoise coloring of the open ocean typically associated with the final stages of E. huxleyi blooms, with peak reflectance at a wavelength of 0.49 μm. Our results also show that the magnitude of backscattering from coccoliths when attached to or freed from the coccosphere does not differ much, contrary to what is commonly assumed, and that the spectral shape of backscattering is mainly controlled by the size and morphology of the coccoliths, suggesting that they may be estimated from spectral backscattering.

Is scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) quantitative?

Science.gov (United States)

Newbury, Dale E; Ritchie, Nicholas W M

2013-01-01

Scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) is a widely applied elemental microanalysis method capable of identifying and quantifying all elements in the periodic table except H, He, and Li. By following the "k-ratio" (unknown/standard) measurement protocol development for electron-excited wavelength dispersive spectrometry (WDS), SEM/EDS can achieve accuracy and precision equivalent to WDS and at substantially lower electron dose, even when severe X-ray peak overlaps occur, provided sufficient counts are recorded. Achieving this level of performance is now much more practical with the advent of the high-throughput silicon drift detector energy dispersive X-ray spectrometer (SDD-EDS). However, three measurement issues continue to diminish the impact of SEM/EDS: (1) In the qualitative analysis (i.e., element identification) that must precede quantitative analysis, at least some current and many legacy software systems are vulnerable to occasional misidentification of major constituent peaks, with the frequency of misidentifications rising significantly for minor and trace constituents. (2) The use of standardless analysis, which is subject to much broader systematic errors, leads to quantitative results that, while useful, do not have sufficient accuracy to solve critical problems, e.g. determining the formula of a compound. (3) EDS spectrometers have such a large volume of acceptance that apparently credible spectra can be obtained from specimens with complex topography that introduce uncontrolled geometric factors that modify X-ray generation and propagation, resulting in very large systematic errors, often a factor of ten or more. © Wiley Periodicals, Inc.

Comparison of SeaWinds Backscatter Imaging Algorithms

Science.gov (United States)

Long, David G.

2017-01-01

This paper compares the performance and tradeoffs of various backscatter imaging algorithms for the SeaWinds scatterometer when multiple passes over a target are available. Reconstruction methods are compared with conventional gridding algorithms. In particular, the performance and tradeoffs in conventional ‘drop in the bucket’ (DIB) gridding at the intrinsic sensor resolution are compared to high-spatial-resolution imaging algorithms such as fine-resolution DIB and the scatterometer image reconstruction (SIR) that generate enhanced-resolution backscatter images. Various options for each algorithm are explored, including considering both linear and dB computation. The effects of sampling density and reconstruction quality versus time are explored. Both simulated and actual data results are considered. The results demonstrate the effectiveness of high-resolution reconstruction using SIR as well as its limitations and the limitations of DIB and fDIB. PMID:28828143

Active pixel sensor array as a detector for electron microscopy.

Science.gov (United States)

Milazzo, Anna-Clare; Leblanc, Philippe; Duttweiler, Fred; Jin, Liang; Bouwer, James C; Peltier, Steve; Ellisman, Mark; Bieser, Fred; Matis, Howard S; Wieman, Howard; Denes, Peter; Kleinfelder, Stuart; Xuong, Nguyen-Huu

2005-09-01

A new high-resolution recording device for transmission electron microscopy (TEM) is urgently needed. Neither film nor CCD cameras are systems that allow for efficient 3-D high-resolution particle reconstruction. We tested an active pixel sensor (APS) array as a replacement device at 200, 300, and 400 keV using a JEOL JEM-2000 FX II and a JEM-4000 EX electron microscope. For this experiment, we used an APS prototype with an area of 64 x 64 pixels of 20 microm x 20 microm pixel pitch. Single-electron events were measured by using very low beam intensity. The histogram of the incident electron energy deposited in the sensor shows a Landau distribution at low energies, as well as unexpected events at higher absorbed energies. After careful study, we concluded that backscattering in the silicon substrate and re-entering the sensitive epitaxial layer a second time with much lower speed caused the unexpected events. Exhaustive simulation experiments confirmed the existence of these back-scattered electrons. For the APS to be usable, the back-scattered electron events must be eliminated, perhaps by thinning the substrate to less than 30 microm. By using experimental data taken with an APS chip with a standard silicon substrate (300 microm) and adjusting the results to take into account the effect of a thinned silicon substrate (30 microm), we found an estimate of the signal-to-noise ratio for a back-thinned detector in the energy range of 200-400 keV was about 10:1 and an estimate for the spatial resolution was about 10 microm.

Backscattering of gyrotron radiation and short-wavelength turbulence during electron cyclotron resonance plasma heating in the L-2M stellarator

Energy Technology Data Exchange (ETDEWEB)

Batanov, G. M.; Borzosekov, V. D., E-mail: tinborz@gmail.com; Kovrizhnykh, L. M.; Kolik, L. V.; Konchekov, E. M.; Malakhov, D. V.; Petrov, A. E.; Sarksyan, K. A.; Skvortsova, N. N.; Stepakhin, V. D.; Kharchev, N. K. [Russian Academy of Sciences, Prokhorov General Physics Institute (Russian Federation)

2013-06-15

Backscattering of gyrotron radiation ({theta} = {pi}) by short-wavelength density fluctuations (k{sub Up-Tack} = 30 cm{sup -1}) in the plasma of the L-2M stellarator was studied under conditions of electron cyclotron resonance (ECR) plasma heating at the second harmonic of the electron gyrofrequency (75 GHz). The scattering of the O-wave emerging due to the splitting of the linearly polarized gyrotron radiation into the X- and O-waves was analyzed. The signal obtained after homodyne detection of scattered radiation is a result of interference of the reference signal, the quasi-steady component, and the fast oscillating component. The coefficients of reflection of the quasi-steady component, R{sub =}{sup 2}(Y), and fast oscillating component, R{sub {approx}}{sup 2}(Y), of scattered radiation are estimated. The growth of the R{sub {approx}}{sup 2}(Y) coefficient from 3.7 Multiplication-Sign 10{sup -4} to 5.2 Multiplication-Sign 10{sup -4} with increasing ECR heating power from 190 to 430 kW is found to correlate with the decrease in the energy lifetime from 1.9 to 1.46 ms. The relative density of short-wavelength fluctuations is estimated to be Left-Pointing-Angle-Bracket n{sub {approx}}{sup 2} Right-Pointing-Angle-Bracket / Left-Pointing-Angle-Bracket n{sub e}{sup 2} Right-Pointing-Angle-Bracket = 3 Multiplication-Sign 10{sup -7}. It is shown that the frequencies of short-wavelength fluctuations are in the range 10-150 kHz. The recorded short-wavelength fluctuations can be interpreted as structural turbulence, the energy of which comprises {approx}10% of the total fluctuations energy. Simulations of transport processes show that neoclassical heat fluxes are much smaller than anomalous ones. It is suggested that short-wavelength turbulence plays a decisive role in the anomalous heat transport.

Backscatter in a cloudy atmosphere as a lightning-threat indicator

International Nuclear Information System (INIS)

Kocifaj, Miroslav; Videen, Gorden; Klačka, Jozef

2015-01-01

We present a remote-sensing method for identifying electrically charged droplets in clouds. Our methodology utilizes the electromagnetic (EM) radiation backscattered by the cloud at multiple wavelengths. In general, the backscatter from collections of charged and neutral particles differs in Rayleigh regime. While a uniformly charged sphere can resonate with an incident EM radiation depending on electrostatic potential at the particle surface, the scatter by a neutral particle is governed by the Lorenz–Mie theory, thus resulting in different surface excitations. The effects of electric charges and other microphysical parameters on the electromagnetic interactions with particles are not easily separable. Because the spectral profile of the dielectric function for liquid water (or alternatively icy grains) is known, retrieval of net charges are possible based on the optical behavior of the backscattered EM signals. Such information can be used to determine charge build-up in the atmosphere, which is a condition for lightning. A basic configuration of a measuring system for lightning threats is discussed and described schematically. - Highlights: • Electrically charged and neutral particles scatter in a different way. • Net surface charge on spherical particles is a modulator of backscatter signal. • Radar echoes are source of information on electrically charged droplets. • Remote-sensing method can be used to identify increased chance of lightning

Use of backscattered electron imaging, X-ray microanalysis and X-ray microscopy in demonstrating physiological cell death

International Nuclear Information System (INIS)

Bowen, I.D.; Worrill, N.A.; Winters, C.A.; Mullarkey, K.

1988-01-01

The cytochemical localization of enzymatic activity by means of backscattered electron imaging (BEI) is reviewed and the application of BEI to changes in acid phosphatase and ATPase distribution during physiological (programmed) cell death in Heliothis midgut is explored. Programmed cell death entails the release of nascent free acid phosphatase as extracisternal hydrolase. This shift can readily be detected by means of the atomic number contrast imparted by BEI of the lead phosphatase reaction product, thus enabling the distribution of dying cells to be mapped. BEI is particularly useful in this context as it allows the examination of bulk specimens at low magnification. Death of cells is also accompanied by a collapse in ATPase activity which shows up as cytochemically negative areas in the X-ray microscope and by means of BEI. Acid phosphatase in normal cells is localized in the apical microvilli and lysosomes. Senescent or dying cells, however, clearly show a basally situated free hydrolase which migrates throughout the cell. Parallel TEM results confirm that this enzyme is ribosomal and extracisternal rather than lysosomal in origin. ATPase activity is largely limited to the apical microvilli, although there is some activity associated with the basal plasma membranes. The apical ATPase, however is partially resistant to ouabain. Young and mature cells are positive although in the latter case some microvilli may be lost as the cells acquire a negative cap or dome. Inhibition by bromotetramizole indicates that apical activity is not to any significant extent contributed to by alkaline phosphatase. Degenerate or dead cells are negative and can be seen as a mozaic of black patches among normal cells when imaged by means of BEI or X-ray microscopy

Diffuse optical microscopy for quantification of depth-dependent epithelial backscattering in the cervix

Science.gov (United States)

Bodenschatz, Nico; Lam, Sylvia; Carraro, Anita; Korbelik, Jagoda; Miller, Dianne M.; McAlpine, Jessica N.; Lee, Marette; Kienle, Alwin; MacAulay, Calum

2016-06-01

A fiber optic imaging approach is presented using structured illumination for quantification of almost pure epithelial backscattering. We employ multiple spatially modulated projection patterns and camera-based reflectance capture to image depth-dependent epithelial scattering. The potential diagnostic value of our approach is investigated on cervical ex vivo tissue specimens. Our study indicates a strong backscattering increase in the upper part of the cervical epithelium caused by dysplastic microstructural changes. Quantization of relative depth-dependent backscattering is confirmed as a potentially useful diagnostic feature for detection of precancerous lesions in cervical squamous epithelium.

Quantitative muscle ultrasound in Duchenne muscular dystrophy: a comparison of techniques.

Science.gov (United States)

Shklyar, Irina; Geisbush, Tom R; Mijialovic, Aleksandar S; Pasternak, Amy; Darras, Basil T; Wu, Jim S; Rutkove, Seward B; Zaidman, Craig M

2015-02-01

Muscle pathology in Duchenne muscular dystrophy (DMD) can be quantified using ultrasound by measuring either the amplitudes of sound-waves scattered back from the tissue [quantitative backscatter analysis (QBA)] or by measuring these backscattered amplitudes after compression into grayscale levels (GSL) obtained from the images. We measured and compared QBA and GSL from 6 muscles of 25 boys with DMD and 25 healthy subjects, aged 2-14 years, with age and, in DMD, with function (North Star Ambulatory Assessment). Both QBA and GSL were measured reliably (intraclass correlation ≥ 0.87) and were higher in DMD than controls (P muscle increased (rho ≥ 0.47, P muscle did not. QBA and GSL measured from superficial regions of muscle can similarly quantify muscle pathology in DMD. © 2014 Wiley Periodicals, Inc.

Rough surface mitigates electron and gas emission

International Nuclear Information System (INIS)

Molvik, A.

2004-01-01

Heavy-ion beams impinging on surfaces near grazing incidence (to simulate the loss of halo ions) generate copious amounts of electrons and gas that can degrade the beam. We measured emission coefficients of η e (le) 130 and η 0 ∼ 10 4 respectively, with 1 MeV K + incident on stainless steel. Electron emission scales as η e ∝ 1/cos(θ), where θ is the ion angle of incidence relative to normal. If we were to roughen a surface by blasting it with glass beads, then ions that were near grazing incidence (90 o ) on smooth surface would strike the rims of the micro-craters at angles closer to normal incidence. This should reduce the electron emission: the factor of 10 reduction, Fig. 1(a), implies an average angle of incidence of 62 o . Gas desorption varies more slowly with θ (Fig. 1(b)) decreasing a factor of ∼2, and along with the electron emission is independent of the angle of incidence on a rough surface. In a quadrupole magnet, electrons emitted by lost primary ions are trapped near the wall by the magnetic field, but grazing incidence ions can backscatter and strike the wall a second time at an azimuth where magnetic field lines intercept the beam. Then, electrons can exist throughout the beam (see the simulations of Cohen, HIF News 1-2/04). The SRIM (TRIM) Monte Carlo code predicts that 60-70% of 1 MeV K + ions backscatter when incident at 88-89 o from normal on a smooth surface. The scattered ions are mostly within ∼10 o of the initial direction but a few scatter by up to 90 o . Ion scattering decreases rapidly away from grazing incidence, Fig. 1(c ). At 62 deg. the predicted ion backscattering (from a rough surface) is 3%, down a factor of 20 from the peak, which should significantly reduce electrons in the beam from lost halo ions. These results are published in Phys. Rev. ST - Accelerators and Beams

Spacecraft charging: incoming and outgoing electrons

CERN Document Server

Lai, Shu T.

2013-04-22

This paper presents an overview of the roles played by incoming and outgoing electrons in spacecraft surface and stresses the importance of surface conditions for spacecraft charging. The balance between the incoming electron current from the ambient plasma and the outgoing currents of secondary electrons, backscattered electrons, and photoelectrons from the surfaces determines the surface potential. Since surface conditions significantly affect the outgoing currents, the critical temperature and the surface potential are also significantly affected. As a corollary, high level differential charging of adjacent surfaces with very different surface conditions is a space hazard.

Dosimetric evaluation of lead and tungsten eye shields in electron beam treatment

International Nuclear Information System (INIS)

Shiu, Almon S.; Tung, Samuel S.; Gastorf, Robert J.; Hogstrom, Kenneth R.; Morrison, William H.; Peters, Lester J.

1996-01-01

Purpose: The purpose of this study is to report that commercially available eye shields (designed for orthovoltage x-rays) are inadequate to protect the ocular structures from penetrating electrons for electron beam energies equal to or greater than 6 MeV. Therefore, a prototype medium size tungsten eye shield was designed and fabricated. The advantages of the tungsten eye shield over lead are discussed. Methods and Materials: Electron beams (6-9 MeV) are often used to irradiate eyelid tumors to curative doses. Eye shields can be placed under the eyelids to protect the globe. Film and thermoluminescent dosimeters (TLDs) were used within a specially constructed polystyrene eye phantom to determine the effectiveness of various commercially available internal eye shields (designed for orthovoltage x-rays). The same procedures were used to evaluate a prototype medium size tungsten eye shield (2.8 mm thick), which was designed and fabricated for protection of the globe from penetrating electrons for electron beam energy equal to 9 MeV. A mini-TLD was used to measure the dose enhancement due to electrons backscattered off the tungsten eye shield, both with or without a dental acrylic coating that is required to reduce discomfort, permit sterilization of the shield, and reduce the dose contribution from backscattered electrons. Results: Transmission of a 6 MeV electron beam through a 1.7 mm thick lead eye shield was found to be 50% on the surface (cornea) of the phantom and 27% at a depth of 6 mm (lens). The thickness of lead required to stop 6-9 MeV electron beams is impractical. In place of lead, a prototype medium size tungsten eye shield was made. For 6 to 9 MeV electrons, the doses measured on the surface (cornea) and at 6 mm (lens) and 21 mm (retina) depths were all less than 5% of the maximum dose of the open field (4 x 4 cm). Electrons backscattered off a tungsten eye shield without acrylic coating increased the lid dose from 85 to 123% at 6 MeV and 87 to 119% at

Modification of Spalart-Allmaras model with consideration of turbulence energy backscatter using velocity helicity

International Nuclear Information System (INIS)

Liu, Yangwei; Lu, Lipeng; Fang, Le; Gao, Feng

2011-01-01

The correlation between the velocity helicity and the energy backscatter is proved in a DNS case of 256 3 -grid homogeneous isotropic decaying turbulence. The helicity is then proposed to be employed to improve turbulence models and SGS models. Then Spalart-Allmaras turbulence model (SA) is modified with the helicity to take account of the energy backscatter, which is significant in the region of corner separation in compressors. By comparing the numerical results with experiments, it can be concluded that the modification for SA model with helicity can appropriately represent the energy backscatter, and greatly improves the predictive accuracy for simulating the corner separation flow in compressors. -- Highlights: → We study the relativity between the velocity helicity and the energy backscatter. → Spalart-Allmaras turbulence model is modified with the velocity helicity. → The modified model is employed to simulate corner separation in compressor cascade. → The modification can greatly improve the accuracy for predicting corner separation. → The helicity can represent the energy backscatter in turbulence and SGS models.

High resolution electron back-scatter diffraction analysis of thermally and mechanically induced strains near carbide inclusions in a superalloy

Energy Technology Data Exchange (ETDEWEB)

Karamched, Phani S., E-mail: phani.karamched@materials.ox.ac.uk [Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH (United Kingdom); Wilkinson, Angus J. [Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH (United Kingdom)

2011-01-15

Cross-correlation-based analysis of electron back-scatter diffraction (EBSD) patterns has been used to obtain high angular resolution maps of lattice rotations and elastic strains near carbides in a directionally solidified superalloy MAR-M-002. Lattice curvatures were determined from the EBSD measurements and used to estimate the distribution of geometrically necessary dislocations (GNDs) induced by the deformation. Significant strains were induced by thermal treatment due to the lower thermal expansion coefficient of the carbide inclusions compared to that of the matrix. In addition to elastic strains the mismatch was sufficient to have induced localized plastic deformation in the matrix leading to a GND density of 3 x 10{sup 13} m{sup -2} in regions around the carbide. Three-point bending was then used to impose strain levels within the range {+-}12% across the height of the bend bar. EBSD lattice curvature measurements were then made at both carbide-containing and carbide-free regions at different heights across the bar. The average GND density increases with the magnitude of the imposed strain (both in tension and compression), and is markedly higher near the carbides particles. The higher GND densities near the carbides (order of 10{sup 14} m{sup -2}) are generated by the large strain gradients produced around the plastically rigid inclusion during mechanical deformation with some minor contribution from the pre-existing residual deformation caused by the thermal mismatch between carbide and nickel matrix.

The Full Aperture Backscatter Station Measurement System on the National Ignition Facility

International Nuclear Information System (INIS)

Bower, D; McCarville, T; Alvarez, S; Ault, L; Brown, M; Chrisp, M; Damian, C; DeHope, W; Froula, D; Glenzer, S; Grace, S; Gu, K; Holdener, F; Huffer, C; Kamperschroer, J; Kelleher, T; Kimbrough, J

2004-01-01

A Full Aperture Backscatter Station (FABS) target diagnostic has been activated on the first four beams of the National Ignition Facility (NIF). Backscattered light from the target propagates back down the beam path into the FABS diagnostic system. FABS measures both stimulated Brillouin scattering (SBS) and stimulated Raman scattering (SRS) with a suite of measurement instruments. Digital cameras and spectrometers record spectrally resolved energy for both P and S polarized light. Streaked spectrometers measure the spectral and temporal behavior of the backscattered light. Calorimeters and fast photodetectors measure the integrated energy and temporal behavior of the light, respectively. This paper provides an overview of the FABS measurements system and detailed descriptions of the diagnostic instruments and the optical path

Waterfall notch-filtering for restoration of acoustic backscatter records from Admiralty Bay, Antarctica

Science.gov (United States)

Fonseca, Luciano; Hung, Edson Mintsu; Neto, Arthur Ayres; Magrani, Fábio José Guedes

2018-06-01

A series of multibeam sonar surveys were conducted from 2009 to 2013 around Admiralty Bay, Shetland Islands, Antarctica. These surveys provided a detailed bathymetric model that helped understand and characterize the bottom geology of this remote area. Unfortunately, the acoustic backscatter records registered during these bathymetric surveys were heavily contaminated with noise and motion artifacts. These artifacts persisted in the backscatter records despite the fact that the proper acquisition geometry and the necessary offsets and delays were applied during the survey and in post-processing. These noisy backscatter records were very difficult to interpret and to correlate with gravity-core samples acquired in the same area. In order to address this issue, a directional notch-filter was applied to the backscatter waterfall in the along-track direction. The proposed filter provided better estimates for the backscatter strength of each sample by considerably reducing residual motion artifacts. The restoration of individual samples was possible since the waterfall frame of reference preserves the acquisition geometry. Then, a remote seafloor characterization procedure based on an acoustic model inversion was applied to the restored backscatter samples, generating remote estimates of acoustic impedance. These remote estimates were compared to Multi Sensor Core Logger measurements of acoustic impedance obtained from gravity core samples. The remote estimates and the Core Logger measurements of acoustic impedance were comparable when the shallow seafloor was homogeneous. The proposed waterfall notch-filtering approach can be applied to any sonar record, provided that we know the system ping-rate and sampling frequency.

Multi-angle backscatter classification and sub-bottom profiling for improved seafloor characterization

Science.gov (United States)

Alevizos, Evangelos; Snellen, Mirjam; Simons, Dick; Siemes, Kerstin; Greinert, Jens

2018-06-01

This study applies three classification methods exploiting the angular dependence of acoustic seafloor backscatter along with high resolution sub-bottom profiling for seafloor sediment characterization in the Eckernförde Bay, Baltic Sea Germany. This area is well suited for acoustic backscatter studies due to its shallowness, its smooth bathymetry and the presence of a wide range of sediment types. Backscatter data were acquired using a Seabeam1180 (180 kHz) multibeam echosounder and sub-bottom profiler data were recorded using a SES-2000 parametric sonar transmitting 6 and 12 kHz. The high density of seafloor soundings allowed extracting backscatter layers for five beam angles over a large part of the surveyed area. A Bayesian probability method was employed for sediment classification based on the backscatter variability at a single incidence angle, whereas Maximum Likelihood Classification (MLC) and Principal Components Analysis (PCA) were applied to the multi-angle layers. The Bayesian approach was used for identifying the optimum number of acoustic classes because cluster validation is carried out prior to class assignment and class outputs are ordinal categorical values. The method is based on the principle that backscatter values from a single incidence angle express a normal distribution for a particular sediment type. The resulting Bayesian classes were well correlated to median grain sizes and the percentage of coarse material. The MLC method uses angular response information from five layers of training areas extracted from the Bayesian classification map. The subsequent PCA analysis is based on the transformation of these five layers into two principal components that comprise most of the data variability. These principal components were clustered in five classes after running an external cluster validation test. In general both methods MLC and PCA, separated the various sediment types effectively, showing good agreement (kappa >0.7) with the Bayesian

Retrieval method of aerosol extinction coefficient profile based on backscattering, side-scattering and Raman-scattering lidar

Science.gov (United States)

Shan, Huihui; Zhang, Hui; Liu, Junjian; Tao, Zongming; Wang, Shenhao; Ma, Xiaomin; Zhou, Pucheng; Yao, Ling; Liu, Dong; Xie, Chenbo; Wang, Yingjian

2018-03-01

Aerosol extinction coefficient profile is an essential parameter for atmospheric radiation model. It is difficult to get higher signal to noise ratio (SNR) of backscattering lidar from the ground to the tropopause especially in near range. Higher SNR problem can be solved by combining side-scattering and backscattering lidar. Using Raman-scattering lidar, aerosol extinction to backscatter ratio (lidar ratio) can be got. Based on side-scattering, backscattering and Raman-scattering lidar system, aerosol extinction coefficient is retrieved precisely from the earth's surface to the tropopause. Case studies show this method is reasonable and feasible.

Numerical simulation of range and backscattering for keV protons incident on random targets

International Nuclear Information System (INIS)

Robinson, J.E.; Agamy, S.

1975-01-01

Using a Monte-Carlo technique, projected range distributions and backscattering coefficients have been calculated for keV protons normally incident on heavy targets. For an incident reduced energy range of 1 less than epsilon 0 less than 20, both the projected range distributions and backscattering coefficients have been found to be in good agreement with a third order Edgeworth range approximation. Backscattered energy and angular distributions have also been calculated and are compared to available theoretical and experimental data. (4 figs.) (U.S.)

Electronic structure of some adenosine receptor antagonists. III. Quantitative investigation of the electronic absorption spectra of alkyl xanthines

Science.gov (United States)

Moustafa, H.; Shalaby, Samia H.; El-sawy, K. M.; Hilal, Rifaat

2002-07-01

Quantitative and comparative investigation of the electronic absorption spectra of theophylline, caffeine and their derivatives is reported. The spectra of theophylline, caffeine and theobromine were compared to establish the predominant tautomeric species in solution. This comparison, analysis of solvent effects and assignments of the observed transitions via MO computations indicate the exits of only one tautomeric species in solution that is the N7 form. A low-lying triplet state was identified which corresponds to a HOMO-LUMO transition. This relatively long-lived T 1 state is always less polar than the ground state and may very well underlie the photochemical reactivity of alkyl xanthines. Substituents of different electron donating or withdrawing strengths and solvent effects are investigated and analyzed. The present analysis is facilitated via computer deconvolution of the observed spectra and MO computation.

Moessbauer backscatter spectrometer with full data processing capability

International Nuclear Information System (INIS)

1976-01-01

The design and operation of a Moessbauer backscatter spectrometer with full data processing capability is described, and the investigation of the applicability of this technique to a variety of practical metallurgical problems is discussed

An electronic portfolio for quantitative assessment of surgical skills in undergraduate medical education.

Science.gov (United States)

Sánchez Gómez, Serafín; Ostos, Elisa María Cabot; Solano, Juan Manuel Maza; Salado, Tomás Francisco Herrero

2013-05-06

We evaluated a newly designed electronic portfolio (e-Portfolio) that provided quantitative evaluation of surgical skills. Medical students at the University of Seville used the e-Portfolio on a voluntary basis for evaluation of their performance in undergraduate surgical subjects. Our new web-based e-Portfolio was designed to evaluate surgical practical knowledge and skills targets. Students recorded each activity on a form, attached evidence, and added their reflections. Students self-assessed their practical knowledge using qualitative criteria (yes/no), and graded their skills according to complexity (basic/advanced) and participation (observer/assistant/independent). A numerical value was assigned to each activity, and the values of all activities were summated to obtain the total score. The application automatically displayed quantitative feedback. We performed qualitative evaluation of the perceived usefulness of the e-Portfolio and quantitative evaluation of the targets achieved. Thirty-seven of 112 students (33%) used the e-Portfolio, of which 87% reported that they understood the methodology of the portfolio. All students reported an improved understanding of their learning objectives resulting from the numerical visualization of progress, all students reported that the quantitative feedback encouraged their learning, and 79% of students felt that their teachers were more available because they were using the e-Portfolio. Only 51.3% of students reported that the reflective aspects of learning were useful. Individual students achieved a maximum of 65% of the total targets and 87% of the skills targets. The mean total score was 345 ± 38 points. For basic skills, 92% of students achieved the maximum score for participation as an independent operator, and all achieved the maximum scores for participation as an observer and assistant. For complex skills, 62% of students achieved the maximum score for participation as an independent operator, and 98% achieved

Numerical study of bandwidth effect on stimulated Raman backscattering in nonlinear regime

Science.gov (United States)

Zhou, H. Y.; Xiao, C. Z.; Zou, D. B.; Li, X. Z.; Yin, Y.; Shao, F. Q.; Zhuo, H. B.

2018-06-01

Nonlinear behaviors of stimulated Raman scattering driven by finite bandwidth pumps are studied by one dimensional particle-in-cell simulations. The broad spectral feature of plasma waves and backscattered light reveals the different coupling and growth mechanisms, which lead to the suppression effect before the deep nonlinear stage. It causes nonperiodic plasma wave packets and reduces packet and etching velocities. Based on the negative frequency shift and electron energy distribution, the long-time evolution of instability can be divided into two stages by the relaxation time. It is a critical time after which the alleviation effects of nonlinear frequency shift and hot electrons are replaced by enhancement. Thus, the broadband pump suppresses instability at early time. However, it aggravates in the deep nonlinear stage by lifting the saturation level due to the coupling of the incident pump with each frequency shifted plasma wave. Our simulation results show that the nonlinear effects are valid in a bandwidth range from 2.25% to 3.0%, and the physics are similar within a nearby parameter space.

Simultaneous integral measurement of electron energy and charge albedoes

International Nuclear Information System (INIS)

Lockwood, G.J.; Miller, G.H.; Halbleib, J.A. Sr.

Results of a series of experiments in which backscattered energy has been determined from precise energy deposition measurements using an improved technique are presented. The fraction of the energy backscattered for electrons incident on Be, Ti, Mo, and Ta is determined as a function of energy and angle of incidence. The improved technique for the absolute measurement of energy deposition using calorimeters involves square-wave (on-off) modulation of the beam. Uncertainties in the measured backscattered energy are 1 to 6 percent, except for Be at normal incidence where they must agree by definition. Experiment and theory agree quite well for Mo and Be at 60 0 . The measured data for Ta and Ti are clearly higher than the calculated results, which is not completely understood. (U.S.)

Forest anisotropy assessment by means of spatial variations analysis of PolSAR backscattering

Directory of Open Access Journals (Sweden)

A. V. Dmitriev

2017-06-01

Full Text Available The possibility to synthesize polarization response from earth covers at any desired combination of transmit and receive antenna polarizations is the significant advantage of polarimetric radar. It permits better identification of dominant scattering mechanisms especially when analyzing polarization signatures. These signatures depict more details of physical information from target backscattering in various polarization bases. However, polarization signatures cannot reveal spatial variations of the radar backscattering caused by volume heterogeneity of a target. This paper proposes a new approach for estimating volume target heterogeneity from polarimetric synthetic aperture radar (PolSAR images. The approach is based on the analysis of a novel type of polarization signature, which we call fractal polarization signature (FPS. This signature is a result of polarization synthesis of initial fully polarimetric data and subsequent fractal analysis of synthesized images. It is displayed as a 3D plot and can be produced for each point in an image. It is shown that FPS describes backscattering variations or image roughness at different states of polarization. Fully polarimetric data of SIR-C and ALOS PALSAR at ascending/descending orbits were used for testing the proposed approach. The azimuthal dependence of the radar backscattering variations is discovered when analyzing backscattering from a pine forest. It correlates with the results of a field survey of trees branch distribution.

Low-frequency acousto-optic backscattering of Bessel light beams

Science.gov (United States)

Khilo, Nikolai A.; Belyi, Vladimir N.; Khilo, Petr A.; Kazak, Nikolai S.

2018-05-01

The use of Bessel light beams, as well as Bessel acoustic beams, substantially enhances the capabilities of acousto-optic methods for control of optical field. We present a theoretical study of the process of optical Bessel beams conversion by means of backward acousto-optic scattering on a Bessel acoustic field in a transversely isotropic crystal. It is shown that, with an appropriate choice of Bessel beams parameters, the backscattering in visible spectral range can be realized at relatively low acoustic frequencies less than one gigahertz. Under conditions of phase matching and transverse spatial synchronism, the efficiency of backscattering is sufficiently high, which is interesting, for example, for construction of acousto-optic spectral analyzers.

Evaluation of eye shields made of tungsten and aluminum in high-energy electron beams

International Nuclear Information System (INIS)

Weaver, Randi D.; Gerbi, Bruce J.; Dusenbery, Kathryn E.

1998-01-01

Purpose: To protect the lens and cornea of the eye when treating the eyelid with electrons, we designed a tungsten and aluminum eye shield that protected both the lens and cornea, and also limited the amount of backscatter to the overlying eyelid when using electron beam therapy. Methods and Materials: Custom curved tungsten eye shields, 2 mm and 3 mm thick, were placed on Kodak XV film on 8 cm polystyrene and irradiated to evaluate the transmission through the shields. To simulate the thickness of the eyelid and to hold the micro-TLDs, an aquaplast mold was made to match the curvature of the eye shields. Backscatter was measured by placing the micro-TLDs on the beam entrance side to check the dose to the underside of the eyelid. Measurements were done with no aluminum, 0.5, and 1.0 mm of aluminum on top of the tungsten eye shields. The measurements were repeated with 2- and 3-mm flat pieces of lead to determine both the transmission and the backscatter dose for this material. Results: Tungsten proved to be superior to lead for shielding the underlying structures and for reducing backscatter. At 6 MeV, a 3-mm flat slab of tungsten plus 0.5 mm of aluminum, resulted in .042 Gy under the shield when 1.00 Gy is delivered to d max . At 6 MeV for a 3-mm lead plus 0.5-mm aluminum, .046 Gy was measured beneath the shield, a 9.5% decrease with the tungsten. Backscatter was also decreased from 1.17 to 1.13 Gy, a 4% decrease, when using tungsten plus 0.5 mm of aluminum vs. the same thickness of lead. Measurements using 9 MeV were performed in the same manner. With 3 mm tungsten and 0.5 mm of aluminum, at 3 mm depth the dose was .048 Gy compared to .079 Gy with lead and aluminum (39% decrease). Additionally, the backscatter dose was 3% less using tungsten. Simulating the lens dose 3 mm beyond the shield for the 2-mm and 3-mm custom curved tungsten eye shields plus 0.5 mm of aluminum was .030 and .024 Gy, respectively, using 6 MeV (20% decrease). Using 9-MeV electrons, the dose

Bathymetry and acoustic backscatter-outer mainland shelf, eastern Santa Barbara Channel, California

Science.gov (United States)

Dartnell, Peter; Finlayson, David P.; Ritchie, Andrew C.; Cochrane, Guy R.; Erdey, Mercedes D.

2012-01-01

In 2010 and 2011, scientists from the U.S. Geological Survey (USGS), Pacific Coastal and Marine Science Center (PCMSC), acquired bathymetry and acoustic-backscatter data from the outer shelf region of the eastern Santa Barbara Channel, California. These surveys were conducted in cooperation with the Bureau of Ocean Energy Management (BOEM). BOEM is interested in maps of hard-bottom substrates, particularly natural outcrops that support reef communities in areas near oil and gas extraction activity. The surveys were conducted using the USGS R/V Parke Snavely, outfitted with an interferometric sidescan sonar for swath mapping and real-time kinematic navigation equipment. This report provides the bathymetry and backscatter data acquired during these surveys in several formats, a summary of the mapping mission, maps of bathymetry and backscatter, and Federal Geographic Data Committee (FGDC) metadata.

Response function of NaI(Tl) detectors and multiple backscattering of gamma rays in aluminium

International Nuclear Information System (INIS)

Sabharwal, Arvind D.; Singh, Manpreet; Singh, Bhajan; Sandhu, B.S.

2008-01-01

The response function, converting the observed pulse-height distribution of a NaI(Tl) detector to a true photon spectrum, is obtained experimentally with the help of an inverse matrix approach. The energy of gamma-ray photons continuously decreases as the number of scatterings increases in a sample having finite dimensions when one deals with the depth of the sample. The present experiments are undertaken to study the effect of target thickness on intensity distribution of gamma photons multiply backscattered from an aluminium target. A NaI(Tl) gamma-ray detector detects the photons backscattered from the aluminium target. The subtraction of analytically estimated singly scattered distribution from the observed intensity distribution (originating from interactions of primary gamma-ray photons with the target) results in multiply backscattered events. We observe that for each incident gamma photon energy, the number of multiply backscattered photons increases with increase in target thickness and then saturates at a particular target thickness called the saturation thickness (depth). Saturation thickness for multiply backscattering of gamma photons is found to decrease with increase in energy of incident gamma-ray photons

Jet-Tagged Back-Scattering Photons for Quark Gluon Plasma Tomography

Energy Technology Data Exchange (ETDEWEB)

Fries, Rainer J. [Cyclotron Institute and Department of Physics and Astronomy, Texas A and M University, College Station, TX 77845 (United States); De, Somnath; Srivastava, Dinesh K. [Variable Energy Cyclotron Centre, 1/AF, Bidhan Nagar, Kolkata – 700064 (India)

2013-05-02

Direct photons are important probes for quark gluon plasma created in high energy nuclear collisions. Various sources of direct photons in nuclear collisions are known, each of them endowed with characteristic information about the production process. However, it has been challenging to separate direct photon sources through measurements of single inclusive photon spectra and photon azimuthal asymmetry. Here we explore a method to identify photons created from the back-scattering of high momentum quarks off quark gluon plasma. We show that the correlation of back-scattering photons with a trigger jet leads to a signal that should be measurable at RHIC and LHC.

Scanning electron microscopy and micro-analyses

International Nuclear Information System (INIS)

Brisset, F.; Repoux, L.; Ruste, J.; Grillon, F.; Robaut, F.

2008-01-01

Scanning electron microscopy (SEM) and the related micro-analyses are involved in extremely various domains, from the academic environments to the industrial ones. The overall theoretical bases, the main technical characteristics, and some complements of information about practical usage and maintenance are developed in this book. high-vacuum and controlled-vacuum electron microscopes are thoroughly presented, as well as the last generation of EDS (energy dispersive spectrometer) and WDS (wavelength dispersive spectrometer) micro-analysers. Beside these main topics, other analysis or observation techniques are approached, such as EBSD (electron backscattering diffraction), 3-D imaging, FIB (focussed ion beams), Monte-Carlo simulations, in-situ tests etc.. This book, in French language, is the only one which treats of this subject in such an exhaustive way. It represents the actualized and totally updated version of a previous edition of 1979. It gathers the lectures given in 2006 at the summer school of Saint Martin d'Heres (France). Content: 1 - electron-matter interactions; 2 - characteristic X-radiation, Bremsstrahlung; 3 - electron guns in SEM; 4 - elements of electronic optics; 5 - vacuum techniques; 6 - detectors used in SEM; 7 - image formation and optimization in SEM; 7a - SEM practical instructions for use; 8 - controlled pressure microscopy; 8a - applications; 9 - energy selection X-spectrometers (energy dispersive spectrometers - EDS); 9a - EDS analysis; 9b - X-EDS mapping; 10 - technological aspects of WDS; 11 - processing of EDS and WDS spectra; 12 - X-microanalysis quantifying methods; 12a - quantitative WDS microanalysis of very light elements; 13 - statistics: precision and detection limits in microanalysis; 14 - analysis of stratified samples; 15 - crystallography applied to EBSD; 16 - EBSD: history, principle and applications; 16a - EBSD analysis; 17 - Monte Carlo simulation; 18 - insulating samples in SEM and X-ray microanalysis; 18a - insulating

Anisotropy of the apparent frequency dependence of backscatter in formalin fixed human myocardium.

Science.gov (United States)

Hall, C S; Verdonk, E D; Wickline, S A; Perez, J E; Miller, J G

1997-01-01

Measurements of the frequency dependence of ultrasonic backscatter are presented for specific angles of insonification for regions of infarcted and noninfarcted human myocardium. A 5-MHz transducer was used to insonify cylindrical cores taken from 7 noninfarcted regions and 12 infarcted regions of the left ventricular free wall of 6 formalin-fixed human hearts explanted because of ischemic cardiomyopathy. The dependence of apparent (uncompensated for diffraction effects and attenuation) backscatter on frequency was approximated by a power-law dependence, magnitude of B(f)2 = afn. Under ideal conditions in a lossless medium, the effect of not compensating for the effects of diffraction and attenuation leads to the value of n to be 2.0 for Rayleigh scatterers while the frequency dependence of the fully compensated backscatter coefficient would be f4. The value of n was determined over the frequency range, 3-7 MHz. Both nonifarcted and infarcted myocardium exhibited anisotropy of the frequency dependence of backscatter, with maxima occurring at angles that were perpendicular to the predominant myofiber direction and minima when parallel to the fibers. Perpendicular insonification yielded results for n of 1.8 +/- 0.1 for noninfarcted myocardium and 1.2 +/- 0.1 for infarcted myocardium while parallel insonification yielded results of 0.4 +/- 0.1 for noninfarcted and 0.0 +/- 0.1 for infarcted myocardium. The functional form of the angle-dependent backscatter is similar for both noninfarcted and infarcted myocardium, although the frequency dependence is clearly different for both tissue states for all angles of insonification. The results of this study indicate that the anisotropy of the frequency dependence of backscatter may play a significant role in ultrasonic imaging and is an important consideration for ultrasonic tissue characterization in myocardium.

Recommendations for improved and coherent acquisition and processing of backscatter data from seafloor-mapping sonars

Science.gov (United States)

Lamarche, Geoffroy; Lurton, Xavier

2018-06-01

Multibeam echosounders are becoming widespread for the purposes of seafloor bathymetry mapping, but the acquisition and the use of seafloor backscatter measurements, acquired simultaneously with the bathymetric data, are still insufficiently understood, controlled and standardized. This presents an obstacle to well-accepted, standardized analysis and application by end users. The Marine Geological and Biological Habitat Mapping group (Geohab.org) has long recognized the need for better coherence and common agreement on acquisition, processing and interpretation of seafloor backscatter data, and established the Backscatter Working Group (BSWG) in May 2013. This paper presents an overview of this initiative, the mandate, structure and program of the working group, and a synopsis of the BSWG Guidelines and Recommendations to date. The paper includes (1) an overview of the current status in sensors and techniques available in seafloor backscatter data from multibeam sonars; (2) the presentation of the BSWG structure and results; (3) recommendations to operators, end-users, sonar manufacturers, and software developers using sonar backscatter for seafloor-mapping applications, for best practice methods and approaches for data acquisition and processing; and (4) a discussion on the development needs for future systems and data processing. We propose for the first time a nomenclature of backscatter processing levels that affords a means to accurately and efficiently describe the data processing status, and to facilitate comparisons of final products from various origins.

Evaluating multiple causes of persistent low microwave backscatter from Amazon forests after the 2005 drought

Science.gov (United States)

Hagen, Stephen; Braswell, Bobby; Milliman, Tom; Herrick, Christina; Peterson, Seth; Roberts, Dar; Keller, Michael; Palace, Michael

2017-01-01

Amazonia has experienced large-scale regional droughts that affect forest productivity and biomass stocks. Space-borne remote sensing provides basin-wide data on impacts of meteorological anomalies, an important complement to relatively limited ground observations across the Amazon’s vast and remote humid tropical forests. Morning overpass QuikScat Ku-band microwave backscatter from the forest canopy was anomalously low during the 2005 drought, relative to the full instrument record of 1999–2009, and low morning backscatter persisted for 2006–2009, after which the instrument failed. The persistent low backscatter has been suggested to be indicative of increased forest vulnerability to future drought. To better ascribe the cause of the low post-drought backscatter, we analyzed multiyear, gridded remote sensing data sets of precipitation, land surface temperature, forest cover and forest cover loss, and microwave backscatter over the 2005 drought region in the southwestern Amazon Basin (4°-12°S, 66°-76°W) and in adjacent 8°x10° regions to the north and east. We found moderate to weak correlations with the spatial distribution of persistent low backscatter for variables related to three groups of forest impacts: the 2005 drought itself, loss of forest cover, and warmer and drier dry seasons in the post-drought vs. the pre-drought years. However, these variables explained only about one quarter of the variability in depressed backscatter across the southwestern drought region. Our findings indicate that drought impact is a complex phenomenon and that better understanding can only come from more extensive ground data and/or analysis of frequent, spatially-comprehensive, high-resolution data or imagery before and after droughts. PMID:28873422

The beam energy measurement system for the Beijing electron-positron collider

International Nuclear Information System (INIS)

Zhang, J.Y.; Abakumova, E.V.; Achasov, M.N.; Blinov, V.E.; Cai, X.; Dong, H.Y.; Fu, C.D.; Harris, F.A.; Kaminsky, V.V.; Krasnov, A.A.; Liu, Q.; Mo, X.H.; Muchnoi, N.Yu.; Nikolaev, I.B.; Qin, Q.; Qu, H.M.; Olsen, S.L.; Pyata, E.E.; Shamov, A.G.; Shen, C.P.

2012-01-01

The beam energy measurement system (BEMS) for the upgraded Beijing electron-positron collider BEPC-II is described. The system is based on measuring the energies of Compton back-scattered photons. The relative systematic uncertainty of the electron and positron beam energy determination is estimated as 2⋅10 -5 .

Stimulated brillouin backscatter of a short-pulse laser

International Nuclear Information System (INIS)

Hinkel, D.E.; Williams, E.A.; Berger, R.L.

1994-01-01

Stimulated Brillouin backscattering (SBBS) from a short-pulse laser, where the pulse length is short compared to the plasma length, is found to be qualitatively different than in the long pulse regime, where the pulse length is long compared to the plasma length. We find that after an initial transient of order the laser pulse length transit time, the instability reaches a steady state in the variables x' = x - V g t, t' = t, where V g is the pulse group velocity. In contrast, SBBS in a long pulse can be absolutely unstable and grows indefinitely, or until nonlinearities intervene. We find that the motion of the laser pulse induces Doppler related effects that substantially modify the backscattered spectrum at higher intensities, where the instability is strongly coupled (i.e. , has a growth rate large compared to the ion acoustic frequency)

Experimental evaluation of multiple Compton backscattering of gamma rays in copper

International Nuclear Information System (INIS)

Sabharwal, Arvind D.; Singh, Manpreet; Singh, Bhajan; Sandhu, B.S.

2009-01-01

The gamma ray photons continue to soften in energy as the number of scatterings increases in thick target, and results in the generation of singly and multiply scattered events. The number of these multiply scattered events increases with an increase in target thickness and saturates beyond a particular target thickness known as saturation depth. The present experiment is undertaken to study the saturation depth for 279 and 320 keV incident gamma ray photons multiply backscattered from copper targets of varying thickness. The backscattered photons are detected by a Nal(Tl) gamma detector whose pulse-height distribution is converted into a photon spectrum with the help of an inverse matrix approach. To extract the contribution of multiply backscattered photons only, the spectrum of singly scattered photon is reconstructed analytically. We observe that the numbers of multiply scattered events increases with an increase in target thickness and then saturate. The saturation depth is found to be decreasing with increase in incident gamma energy. (author)

Surface sterilization by low energy electron beams

International Nuclear Information System (INIS)

Sekiguchi, Masayuki; Tabei, Masae

1989-01-01

The germicidal effectiveness of low energy electron beams (175 KV) against bacterial cells was investigated. The dry spores of Bacillus pumilus ATCC 27142 and Bacillus globigii ATCC 9372 inoculated on carrier materials and irradiated by gamma rays showed the exponential type of survival curves whereas they showed sigmoidal ones when exposed to low energy electron beams. When similarly irradiated, the wet spores inoculated on membrane filter showed the same survival curves as the dry spores inoculated on carrier materials. The wet vegetative cells of Escherichia coli ATCC 25922 showed exponential curves when exposed to gamma and electron beam irradiation. Low energy electron beams in air showed little differences from nitrogen stream in their germicidal effectiveness against dry spores of B. pumilus. The D values of B. pumilus spores inoculated on metal plates decreased as the amounts of backscattering electrons from the plates increased. There was adequate correlation between the D value (linear region of survival curve), average D value (6D/6) and 1% survival dose and backscattering factor. Depth dose profile and backscatterig dose of low energy electron beams were measured by radiochromic dye film dosimeter (RCD). These figures were not always in accord with the observed germicidal effectiveness against B. pumilus spores because of varying thickness of RCD and spores inoculated on carrier material. The dry spores were very thin and this thinness was useful in evaluating the behavior of low energy electrons. (author)

A new Langmuir probe concept for rapid sampling of space plasma electron density

International Nuclear Information System (INIS)

Jacobsen, K S; Pedersen, A; Moen, J I; Bekkeng, T A

2010-01-01

In this paper we describe a new Langmuir probe concept that was invented for the in situ investigation of HF radar backscatter irregularities, with the capability to measure absolute electron density at a resolution sufficient to resolve the finest conceivable structure in an ionospheric plasma. The instrument consists of two or more fixed-bias cylindrical Langmuir probes whose radius is small compared to the Debye length. With this configuration, it is possible to acquire absolute electron density measurements independent of electron temperature and rocket/satellite potential. The system was flown on the ICI-2 sounding rocket to investigate the plasma irregularities which cause HF backscatter. It had a sampling rate of more than 5 kHz and successfully measured structures down to the scale of one electron gyro radius. The system can easily be adapted for any ionospheric rocket or satellite, and provides high-quality measurements of electron density at any desired resolution

A new numerical technique to design satellite energetic electron detectors

CERN Document Server

Tuszewski, M G; Ingraham, J C

2002-01-01

Energetic charged particles trapped in the magnetosphere are routinely detected by satellite instruments. However, it is generally difficult to extract quantitative energy and angular information from such measurements because the interaction of energetic electrons with matter is rather complex. Beam calibrations and Monte-Carlo (MC) simulations are often used to evaluate a flight instrument once it is built. However, rules of thumb and past experience are common tools to design the instrument in the first place. Hence, we have developed a simple numerical procedure, based on analytical probabilities, suitable for instrumental design and evaluation. In addition to the geometrical response, the contributions of surface backscattering, edge penetration, and bremsstrahlung radiation are estimated. The new results are benchmarked against MC calculations for a simple test case. Complicated effects, such as the contribution of the satellite to the instrumental response, can be estimated with the new formalism.

Incidence angle normalization of radar backscatter data

Science.gov (United States)

NASA’s Soil Moisture Passive Active (SMAP) satellite (~2014) will include a radar system that will provide L-band multi-polarization backscatter at a constant incidence angle of 40º. During the pre-launch phase of the project there is a need for observations that will support the radar-based soil mo...

Ultrasonic Characterization of Tissues via Backscatter Frequency Dependence

DEFF Research Database (Denmark)

Stetson, Paul F.; Sommer, F.G.

1997-01-01

, significantly lower mean frequency of ultrasound backscattered from cirrhotic, compared to normal, liver tissue was noted, Studies of benign and malignant liver tumors (hemangiomas and metastases, respectively) indicated differences in frequency content of these tumors, compared to the adjacent normal liver...

Optimization of phantom backscatter thickness and lateral scatter volume for radiographic film dosimetry

International Nuclear Information System (INIS)

Srivastava, R.P.; De Wagter, C.

2012-01-01

The aim of this study is to determine the optimal backscatter thickness and lateral phantom dimension beyond the irradiated volume for the dosimetric verification with radiographic film when applying large field sizes. Polystyrene and Virtual Water™ phantoms were used to study the influence of the phantom backscatter thickness. EDR2 and XV films were used in 6 and 18 MV photon beams. The results show 11.4% and 6.4% over-response of the XV2 film when compared to the ion chamber for 6 MV 30×30 and 10×10 cm 2 field sizes, respectively, when the phantom backscatter thickness is 5 cm. For the same setup, measurements with EDR2 films indicate 8.5% and 1.7% over-response. The XV2 film response in the polystyrene phantom is about 2.0% higher than in the Virtual Water™ phantom for the 6 MV beam and 20 cm backscatter thickness. Similar results were obtained for EDR2 film. In the lateral scatter study, film response was nearly constant within 5 cm of lateral thickness and it increases when lateral thickness increases due to more multiple scatter of low energy photons. The backscatter thickness of the phantom should be kept below 7 cm for the accuracy of the film dosimetry. The lateral extension of the phantom should not be more than 5 cm from the field boundary in case of large irradiated volumes.

Studies of currents and electric fields in the auroral zone ionosphere using radar auroral backscatter

International Nuclear Information System (INIS)

Greenwald, R.A.

1980-01-01

During the 1970s several advances have been made in the understanding of radar aurora. Recent VHF studies have shown that Doppler data obtained from radar auroral backscatter can be used to measure the E-region electron drift velocity, the F-region plasma velocity, and the ionospheric electric field. This type of measurement is particularly valuable when it is made with dual auroral radar systems similar to STARE (Scandinavian Twin Auroral Radar Experiment). Over the past two years STARE has been used to study electric field patterns associated with electrojet and field-aligned currents, magnetospheric convection, the Harang discontinuity, Pc5 micropulsations, and the substorm expansion phase. (Auth.)

X-ray backscatter radiography. Intrusive instead of penetrating, X-ray shadow phenomenon

International Nuclear Information System (INIS)

Wrobel, Norma; Kolkoori, Sanjeevareddy; Osterloh, Kurt; European Federation for Non-Destructive Testing

2013-01-01

Generally, the primary practical advantage of X-ray backscattering radiography is that there is no need to place a detector on the side of the specimen opposite to the source. Such a situation usually is encountered whenever the specimen is not only standing right in front of a wall or even inside a wall but also if the specimen is such big that radiography is not possible because of the layer thickness to be penetrated. The method used here differs fundamentally from the conventional method to interrogate the object with a scanning beam ('pencil beam') and to collect the whole backscattered radiation from the area. The object is fully illuminated by a (uncollimated) cone beam. Here, the image is recorded with a camera of absorbent material (tungsten, lead), which contains a matrix detector as the image receiver. The optical effect is generated by a special twisted slit collimator which operates according to an extended pinhole camera. The independent positioning of source and camera allows a variable irradiation geometry which causes different images as a result. As a consequence, a complex object in front of a backscattering wall appears completely different than standing alone. So X-ray backscatter images have to be interpreted according to their illumination with X-rays and their surroundings. (orig.)

Characterization of highly scattering media by measurement of diffusely backscattered polarized light

Science.gov (United States)

Hielscher, Andreas H.; Mourant, Judith R.; Bigio, Irving J.

2000-01-01

An apparatus and method for recording spatially dependent intensity patterns of polarized light that is diffusely backscattered from highly scattering media are described. These intensity patterns can be used to differentiate different turbid media, such as polystyrene-sphere and biological-cell suspensions. Polarized light from a He-Ne laser (.lambda.=543 nm) is focused onto the surface of the scattering medium, and a surface area of approximately 4.times.4 cm centered on the light input point is imaged through polarization analysis optics onto a CCD camera. A variety of intensity patterns may be observed by varying the polarization state of the incident laser light and changing the analyzer configuration to detect different polarization components of the backscattered light. Experimental results for polystyrene-sphere and Intralipid suspensions demonstrate that the radial and azimuthal variations of the observed pattern depend on the concentration, size, and anisotropy factor, g, of the particles constituting the scattering medium. Measurements performed on biological cell suspensions show that intensity patterns can be used to differentiate between suspensions of cancerous and non-cancerous cells. Introduction of the Mueller-matrix for diffusely backscattered light, permits the selection of a subset of measurements which comprehensively describes the optical properties of backscattering media.

Model for H- and D- production by hydrogen backscattering

International Nuclear Information System (INIS)

Hiskes, J.R.; Schneider, P.J.

1980-01-01

The Marlowe Monte-Carlo backscattering code has been used to calculate particle reflection coefficients and energy distributions for H, D incident upon Li, K, Ni, Cu, Mo, Ag, Cs, Hf, W, Pt, and U surfaces. The backscattered energy and angular distributions are combined with a model for formation and survival probabilities for H - , D - leaving the surface. A least-squares fit of experimental measurements of H - yields from the composite surface, Cs/Cu, has been used to obtain two semi-empirical constants, α, β which enter into the formation and survival probabilities. These probabilities are used to calculate the production probability which in turn provides an upper limit to the negative ion yield. The choice of electrode material is discussed as a function of atomic number

Quantitative characterization of cleavage and hydrogen-assisted quasi-cleavage fracture surfaces with the use of confocal laser scanning microscopy

International Nuclear Information System (INIS)

Merson, E.; Kudrya, A.V.; Trachenko, V.A.; Merson, D.; Danilov, V.; Vinogradov, A.

2016-01-01

“True” cleavage (TC) and quasi-cleavage (QC) fracture surfaces of low-carbon steel specimens tested in liquid nitrogen and after hydrogen charging respectively were investigated by quantitative confocal laser scanning microscopy (CLSM) and conventional scanning electron microscopy (SEM) with electron-backscattered diffraction (EBSD). Topological and crystallographic features of the TC fracture surface are found in good agreement with the generally accepted cleavage mechanism: TC facets diameters correspond to those of grains; the crack path strictly follows the crystallographic orientation of grains and the most of the cleavage cracks are parallel to {100} planes. On the 2D SEM images, the QC facets appeared resembling the TC ones in terms of river line patterns, shapes and sizes. However, the substantial differences between the topography of these two kinds of fracture surfaces were revealed by 3D CLSM: the average misorientation angle between QC facets and the roughness of the QC fracture surface were much lower than those measured for TC. It is demonstrated that all these features are attributed to the specific fracture mechanism operating during hydrogen-assisted cracking.

Quantitative characterization of cleavage and hydrogen-assisted quasi-cleavage fracture surfaces with the use of confocal laser scanning microscopy

Energy Technology Data Exchange (ETDEWEB)

Merson, E. [Institute of Advanced Technologies, Togliatti State University, 445667 (Russian Federation); Kudrya, A.V.; Trachenko, V.A. [Department of Physical Metallurgy and the Physics of Strength, NUST MISiS, Moscow 119490 (Russian Federation); Merson, D. [Institute of Advanced Technologies, Togliatti State University, 445667 (Russian Federation); Laboratory for Advanced Materials, Kazan Federal University, Naberezhnye Chelny 423812, Republic of Tatarstan (Russian Federation); Danilov, V. [Institute of Advanced Technologies, Togliatti State University, 445667 (Russian Federation); Vinogradov, A. [Institute of Advanced Technologies, Togliatti State University, 445667 (Russian Federation); Department of Engineering Design and Materials, Norwegian University of Science and Technology – NTNU, N-7491 Trondheim (Norway)

2016-05-17

“True” cleavage (TC) and quasi-cleavage (QC) fracture surfaces of low-carbon steel specimens tested in liquid nitrogen and after hydrogen charging respectively were investigated by quantitative confocal laser scanning microscopy (CLSM) and conventional scanning electron microscopy (SEM) with electron-backscattered diffraction (EBSD). Topological and crystallographic features of the TC fracture surface are found in good agreement with the generally accepted cleavage mechanism: TC facets diameters correspond to those of grains; the crack path strictly follows the crystallographic orientation of grains and the most of the cleavage cracks are parallel to {100} planes. On the 2D SEM images, the QC facets appeared resembling the TC ones in terms of river line patterns, shapes and sizes. However, the substantial differences between the topography of these two kinds of fracture surfaces were revealed by 3D CLSM: the average misorientation angle between QC facets and the roughness of the QC fracture surface were much lower than those measured for TC. It is demonstrated that all these features are attributed to the specific fracture mechanism operating during hydrogen-assisted cracking.

Quantitative Determination of Spring Water Quality Parameters via Electronic Tongue

Directory of Open Access Journals (Sweden)

Noèlia Carbó

2017-12-01

Full Text Available The use of a voltammetric electronic tongue for the quantitative analysis of quality parameters in spring water is proposed here. The electronic voltammetric tongue consisted of a set of four noble electrodes (iridium, rhodium, platinum, and gold housed inside a stainless steel cylinder. These noble metals have a high durability and are not demanding for maintenance, features required for the development of future automated equipment. A pulse voltammetry study was conducted in 83 spring water samples to determine concentrations of nitrate (range: 6.9–115 mg/L, sulfate (32–472 mg/L, fluoride (0.08–0.26 mg/L, chloride (17–190 mg/L, and sodium (11–94 mg/L as well as pH (7.3–7.8. These parameters were also determined by routine analytical methods in spring water samples. A partial least squares (PLS analysis was run to obtain a model to predict these parameter. Orthogonal signal correction (OSC was applied in the preprocessing step. Calibration (67% and validation (33% sets were selected randomly. The electronic tongue showed good predictive power to determine the concentrations of nitrate, sulfate, chloride, and sodium as well as pH and displayed a lower R2 and slope in the validation set for fluoride. Nitrate and fluoride concentrations were estimated with errors lower than 15%, whereas chloride, sulfate, and sodium concentrations as well as pH were estimated with errors below 10%.

Improved detection and mapping of deepwater hydrocarbon seeps: optimizing multibeam echosounder seafloor backscatter acquisition and processing techniques

Science.gov (United States)

Mitchell, Garrett A.; Orange, Daniel L.; Gharib, Jamshid J.; Kennedy, Paul

2018-02-01

Marine seep hunting surveys are a current focus of hydrocarbon exploration surveys due to recent advances in offshore geophysical surveying, geochemical sampling, and analytical technologies. Hydrocarbon seeps are ephemeral, small, discrete, and therefore difficult to sample on the deep seafloor. Multibeam echosounders are an efficient seafloor exploration tool to remotely locate and map seep features. Geophysical signatures from hydrocarbon seeps are acoustically-evident in bathymetric, seafloor backscatter, midwater backscatter datasets. Interpretation of these signatures in backscatter datasets is a fundamental component of commercial seep hunting campaigns. Degradation of backscatter datasets resulting from environmental, geometric, and system noise can interfere with the detection and delineation of seeps. We present a relative backscatter intensity normalization method and an oversampling acquisition technique that can improve the geological resolvability of hydrocarbon seeps. We use Green Canyon (GC) Block 600 in the Northern Gulf of Mexico as a seep calibration site for a Kongsberg EM302 30 kHz MBES prior to the start of the Gigante seep hunting program to analyze these techniques. At GC600, we evaluate the results of a backscatter intensity normalization, assess the effectiveness of 2X seafloor coverage in resolving seep-related features in backscatter data, and determine the off-nadir detection limits of bubble plumes using the EM302. Incorporating these techniques into seep hunting surveys can improve the detectability and sampling of seafloor seeps.

Improved detection and mapping of deepwater hydrocarbon seeps: optimizing multibeam echosounder seafloor backscatter acquisition and processing techniques

Science.gov (United States)

Mitchell, Garrett A.; Orange, Daniel L.; Gharib, Jamshid J.; Kennedy, Paul

2018-06-01

Marine seep hunting surveys are a current focus of hydrocarbon exploration surveys due to recent advances in offshore geophysical surveying, geochemical sampling, and analytical technologies. Hydrocarbon seeps are ephemeral, small, discrete, and therefore difficult to sample on the deep seafloor. Multibeam echosounders are an efficient seafloor exploration tool to remotely locate and map seep features. Geophysical signatures from hydrocarbon seeps are acoustically-evident in bathymetric, seafloor backscatter, midwater backscatter datasets. Interpretation of these signatures in backscatter datasets is a fundamental component of commercial seep hunting campaigns. Degradation of backscatter datasets resulting from environmental, geometric, and system noise can interfere with the detection and delineation of seeps. We present a relative backscatter intensity normalization method and an oversampling acquisition technique that can improve the geological resolvability of hydrocarbon seeps. We use Green Canyon (GC) Block 600 in the Northern Gulf of Mexico as a seep calibration site for a Kongsberg EM302 30 kHz MBES prior to the start of the Gigante seep hunting program to analyze these techniques. At GC600, we evaluate the results of a backscatter intensity normalization, assess the effectiveness of 2X seafloor coverage in resolving seep-related features in backscatter data, and determine the off-nadir detection limits of bubble plumes using the EM302. Incorporating these techniques into seep hunting surveys can improve the detectability and sampling of seafloor seeps.

Interferometric evidence for the observation of ground backscatter originating behind the CUTLASS coherent HF radars

Science.gov (United States)

Milan, S. E.; Jones, T. B.; Robinson, T. R.; Thomas, E. C.; Yeoman, T. K.

1997-01-01

Interferometric techniques allow the SuperDARN coherent HF radars to determine the elevation angles of returned backscatter, giving information on the altitude of the scatter volume, in the case of ionospheric backscatter, or the reflection altitude, in the case of ground backscatter. Assumptions have to be made in the determination of elevation angles, including the direction of arrival, or azimuth, of the returned signals, usually taken to be the forward look-direction (north) of the radars, specified by the phasing of the antenna arrays. It is shown that this assumption is not always valid in the case of ground backscatter, and that significant returns can be detected from the backward look-direction of the radars. The response of the interferometer to backscatter from behind the radar is modelled and compared with observations. It is found that ground backscatter from a field-of-view that is the mirror image of the forward-looking field-of-view is a common feature of the observations, and this interpretation successfully explains several anomalies in the received backscatter. Acknowledgements. The authors are grateful to Prof. D. J. Southwood (Imperial College, London), J. C. Samson (University of Alberta, Edmonton), L. J. Lanzerotti (AT&T Bell Laboratories), A. Wolfe (New York City Technical College) and to Dr. M. Vellante (University of LÁquila) for helpful discussions. They also thank Dr. A. Meloni (Istituto Nazionale di Geofisica, Roma) who made available geomagnetic field observations from LÁquila Geomagnetic Observatory. This research activity at LÁquila is supported by MURST (40% and 60% contracts) and by GIFCO/CNR. Topical Editor K.-H. Glaßmeier thanks C. Waters and S. Fujita for their help in evaluating this paper.-> Correspondence to :P. Francia->

Method and Apparatus for Computed Imaging Backscatter Radiography

Science.gov (United States)

Shedlock, Daniel (Inventor); Meng, Christopher (Inventor); Sabri, Nissia (Inventor); Dugan, Edward T. (Inventor); Jacobs, Alan M. (Inventor)

2013-01-01

Systems and methods of x-ray backscatter radiography are provided. A single-sided, non-destructive imaging technique utilizing x-ray radiation to image subsurface features is disclosed, capable of scanning a region using a fan beam aperture and gathering data using rotational motion.

Improvement of sensitivity in high-resolution Rutherford backscattering spectroscopy

International Nuclear Information System (INIS)

Hashimoto, H.; Nakajima, K.; Suzuki, M.; Kimura, K.; Sasakawa, K.

2011-01-01

The sensitivity (limit of detection) of high-resolution Rutherford backscattering spectroscopy (HRBS) is mainly determined by the background noise of the spectrometer. There are two major origins of the background noise in HRBS, one is the stray ions scattered from the inner wall of the vacuum chamber of the spectrometer and the other is the dark noise of the microchannel plate (MCP) detector which is commonly used as a focal plane detector of the spectrometer in HRBS. In order to reject the stray ions, several barriers are installed inside the spectrometer and a thin Mylar foil is mounted in front of the detector. The dark noise of the MCP detector is rejected by the coincidence measurement with the secondary electrons emitted from the Mylar foil upon the ion passage. After these improvements, the background noise is reduced by a factor of 200 at a maximum. The detection limit can be improved down to 10 ppm for As in Si at a measurement time of 1 h under ideal conditions.

Local thermal conductivity of polycrystalline AlN ceramics measured by scanning thermal microscopy and complementary scanning electron microscopy techniques

International Nuclear Information System (INIS)

Zhang Yue-Fei; Wang Li; Wei Bin; Ji Yuan; Han Xiao-Dong; Zhang Ze; Heiderhoff, R.; Geinzer, A. K.; Balk, L. J.

2012-01-01

The local thermal conductivity of polycrystalline aluminum nitride (AlN) ceramics is measured and imaged by using a scanning thermal microscope (SThM) and complementary scanning electron microscope (SEM) based techniques at room temperature. The quantitative thermal conductivity for the AlN sample is gained by using a SThM with a spatial resolution of sub-micrometer scale through using the 3ω method. A thermal conductivity of 308 W/m·K within grains corresponding to that of high-purity single crystal AlN is obtained. The slight differences in thermal conduction between the adjacent grains are found to result from crystallographic misorientations, as demonstrated in the electron backscattered diffraction. A much lower thermal conductivity at the grain boundary is due to impurities and defects enriched in these sites, as indicated by energy dispersive X-ray spectroscopy. (condensed matter: structural, mechanical, and thermal properties)

High-frequency attenuation and backscatter measurements of rat blood between 30 and 60 MHz

International Nuclear Information System (INIS)

Huang, Chih-Chung

2010-01-01

There has recently been a great deal of interest in noninvasive high-frequency ultrasound imaging of small animals such as rats due to their being the preferred animal model for gene therapy and cancer research. Improving the interpretation of the obtained images and furthering the development of the imaging devices require a detailed knowledge of the ultrasound attenuation and backscattering of biological tissue (e.g. blood) at high frequencies. In the present study, the attenuation and backscattering coefficients of the rat red blood cell (RBC) suspensions and whole blood with hematocrits ranging from 6% to 40% were measured between 30 and 60 MHz using a modified substitution approach. The acoustic parameters of porcine blood under the same conditions were also measured in order to compare differences in the blood properties between these two animals. For porcine blood, both whole blood and RBC suspension were stirred at a rotation speed of 200 rpm. Three different rotation speeds of 100, 200 and 300 rpm were carried out for rat blood experiments. The attenuation coefficients of both rat and porcine blood were found to increase linearly with frequency and hematocrit (the values of coefficients of determination (r 2 ) are around 0.82-0.97 for all cases). The average attenuation coefficient of rat whole blood with a hematocrit of 40% increased from 0.26 Nepers mm -1 at 30 MHz to 0.47 Nepers mm -1 at 60 MHz. The maximum backscattering coefficients of both rat and porcine RBC suspensions were between 10% and 15% hematocrits at all frequencies. The fourth-power dependence of backscatter on frequency was approximately valid for rat RBC suspensions with hematocrits between 6% and 40%. However, the frequency dependence of the backscatter estimate deviates from a fourth-power law for porcine RBC suspension with hematocrit higher than 20%. The backscattering coefficient plateaued for hematocrits higher than 15% in porcine blood, but for rat blood it was maximal around a

Uranium-contaminated soils: Ultramicrotomy and electron beam analysis

International Nuclear Information System (INIS)

Buck, E.C.; Dietz, N.L.; Bates, J.K.; Cunnane, J.C.

1994-01-01

Uranium contaminated soils from the Fernald Operation Site, Ohio, have been examined by a combination of optical microscopy, scanning electron microscopy with backscattered electron detection (SEM/BSE), and analytical electron microscopy (AEM). A method is described for preparing of transmission electron microscopy (TEM) thin sections by ultramicrotomy. By using these thin sections, SEM and TEM images can be compared directly. Uranium was found in iron oxides, silicates (soddyite), phosphates (autunites), and fluorite. Little uranium was associated with clays. The distribution of uranium phases was found to be inhomogeneous at the microscopic level

A method to correct coordinate distortion in EBSD maps

International Nuclear Information System (INIS)

Zhang, Y.B.; Elbrønd, A.; Lin, F.X.

2014-01-01

Drift during electron backscatter diffraction mapping leads to coordinate distortions in resulting orientation maps, which affects, in some cases significantly, the accuracy of analysis. A method, thin plate spline, is introduced and tested to correct such coordinate distortions in the maps after the electron backscatter diffraction measurements. The accuracy of the correction as well as theoretical and practical aspects of using the thin plate spline method is discussed in detail. By comparing with other correction methods, it is shown that the thin plate spline method is most efficient to correct different local distortions in the electron backscatter diffraction maps. - Highlights: • A new method is suggested to correct nonlinear spatial distortion in EBSD maps. • The method corrects EBSD maps more precisely than presently available methods. • Errors less than 1–2 pixels are typically obtained. • Direct quantitative analysis of dynamic data are available after this correction

Results of Monte-Carlo studies on backscattering and sputtering from 'pocket' and 'finned' structures

International Nuclear Information System (INIS)

Brown, K.P.

1978-01-01

A Monte-Carlo computer program which has been developed for studying backscattering and sputtering processes involving high energy particles in complex vacuum structures has been used to show that useful reductions in backscattering and sputtering can be achieved by pocketing or finning the wall surfaces of plasma containment vessels. (author)

Quantitation of tetrabromobisphenol-A from dust sampled on consumer electronics by dispersed liquid-liquid microextraction

International Nuclear Information System (INIS)

Di Napoli-Davis, Gina; Owens, Janel E.

2013-01-01

Tetrabromobisphenol-A (TBBPA) is a brominated flame retardant used worldwide. Despite its widespread use, there are few data concerning environmental concentrations of TBBPA. Thus, the objective of this work was to optimize an ultrasound-assisted dispersed liquid-liquid microextraction (DLLME) method to analyze swabbed surfaces of consumer electronics to determine TBBPA concentrations. Upon sample preparation with DLLME, TBBPA was derivatized with acetic anhydride and then analyzed by gas chromatography–mass spectrometry (GC/MS). Using a 13 C 12 -TBBPA internal standard to improve precision and quantitation, a recovery study was performed. At concentrations of 250–1000 ng/mL, recoveries were 104–106%. Sample preparation with solid phase extraction had comparable recoveries, although overall, improved analyte recovery and precision were achieved with DLLME. In a small survey study, TBBPA concentrations in dust collected from 100 cm 2 areas on electronic surfaces (monitor, microwave, refrigerator, and TV) were determined to range from less than the LOQ to 523 ng/mL. -- Highlights: •Tetrabromobisphenol-A (TBBPA) concentrations in dust samples were determined. •Dust samples were collected from surfaces of consumer electronics. •Dispersed liquid-liquid microextraction was used to prepare samples for GC/MS. •A 13 C 12 -labeled internal standard was used to improve precision and quantitation. •TBBPA was found in dust samples at levels below LOQ to 523 ng/mL. -- This work describes the analysis of the brominated flame retardant, tetrabromobisphenol-A (TBBPA), from dust sampled on surfaces of consumer electronics

Quantitative annular dark field scanning transmission electron microscopy for nanoparticle atom-counting: What are the limits?

International Nuclear Information System (INIS)

De Backer, A; De Wael, A; Gonnissen, J; Martinez, G T; Béché, A; Van Aert, S; MacArthur, K E; Jones, L; Nellist, P D

2015-01-01

Quantitative atomic resolution annular dark field scanning transmission electron microscopy (ADF STEM) has become a powerful technique for nanoparticle atom-counting. However, a lot of nanoparticles provide a severe characterisation challenge because of their limited size and beam sensitivity. Therefore, quantitative ADF STEM may greatly benefit from statistical detection theory in order to optimise the instrumental microscope settings such that the incoming electron dose can be kept as low as possible whilst still retaining single-atom precision. The principles of detection theory are used to quantify the probability of error for atom-counting. This enables us to decide between different image performance measures and to optimise the experimental detector settings for atom-counting in ADF STEM in an objective manner. To demonstrate this, ADF STEM imaging of an industrial catalyst has been conducted using the near-optimal detector settings. For this experiment, we discussed the limits for atomcounting diagnosed by combining a thorough statistical method and detailed image simulations. (paper)

Quantitative analysis of biological fluids by electron probe and X ray spectrometry

International Nuclear Information System (INIS)

Girod, Chantal

1986-01-01

In order to know the kidney normal operation and to have an insight on cellular transport mechanisms and hormonal regulations at the nephron level, a technique based on the use of an electron probe has been developed for the elemental analysis of micro-volumes of biological fluids. This academic document reports applications of this technique on animals on which such fluids have been sampled at different levels of the nephron. As these samples are available in too small volumes to be dosed by conventional methods, they have been quantitatively analysed by using an electronic probe based analyser in order to determine concentrations of all elements with an atomic number greater than that of carbon. After a presentation of the implemented method and hardware, the author thus describes how an analysis is performed, and reports and discusses an example (analysis conditions, data acquisition, data processing, minimum detectable concentration, reasons for measurement scattering)

Multi-Polarization ASAR Backscattering from Herbaceous Wetlands in Poyang Lake Region, China

Directory of Open Access Journals (Sweden)

Huiyong Sang

2014-05-01

Full Text Available Wetlands are one of the most important ecosystems on Earth. There is an urgent need to quantify the biophysical parameters (e.g., plant height, aboveground biomass and map total remaining areas of wetlands in order to evaluate the ecological status of wetlands. In this study, Environmental Satellite/Advanced Synthetic Aperture Radar (ENVISAT/ASAR dual-polarization C-band data acquired in 2005 is tested to investigate radar backscattering mechanisms with the variation of hydrological conditions during the growing cycle of two types of herbaceous wetland species, which colonize lake borders with different elevation in Poyang Lake region, China. Phragmites communis (L. Trin. is semi-aquatic emergent vegetation with vertical stem and blade-like leaves, and the emergent Carex spp. has rhizome and long leaves. In this study, the potential of ASAR data in HH-, HV-, and VV-polarization in mapping different wetland types is examined, by observing their dynamic variations throughout the whole flooding cycle. The sensitivity of ASAR backscattering coefficients to vegetation parameters of plant height, fresh and dry biomass, and vegetation water content is also analyzed for Phragmites communis (L. Trin. and Carex spp. The research for Phragmites communis (L. Trin. shows that HH polarization is more sensitive to plant height and dry biomass than HV polarization. ASAR backscattering coefficients are relatively less sensitive to fresh biomass, especially in HV polarization. However, both are highly dependent on canopy water content. In contrast, the dependence of HH- and HV- backscattering from Carex community on vegetation parameters is poor, and the radar backscattering mechanism is controlled by ground water level.

Application of neutron backscatter techniques to level measurement problems

International Nuclear Information System (INIS)

Leonardi-Cattolica, A.M.; McMillan, D.H.; Telfer, A.; Griffin, L.H.; Hunt, R.H.

1982-01-01

We have designed and built portable level detectors and fixed level monitors based on neutron scattering and detection principles. The main components of these devices, which we call neutron backscatter gauges, are a neutron emitting radioisotope, a neutron detector, and a ratemeter. The gauge is a good detector for hydrogen but is much less sensitive to most other materials. This allows level measurements of hydrogen bearing materials, such as hydrocarbons, to be made through the walls of metal vessels. Measurements can be made conveniently through steel walls which are a few inches thick. We have used neutron backscatter gauges in a wide variety of level measurement applications encountered in the petrochemical industry. In a number of cases, the neutron techniques have proven to be superior to conventional level measurement methods, including gamma ray methods

Quantitative electron microscopy and spectroscopy of MgB2 wires and tapes

International Nuclear Information System (INIS)

Birajdar, B; Peranio, N; Eibl, O

2008-01-01

In MgB 2 the correlation of microstructure with superconducting properties, in particular the critical current density, requires powerful analytical tools. Critical current densities and electrical resistivities of different MgB 2 superconductors differ by orders of magnitudes and the current limiting mechanisms have not been fully understood. Granularity of MgB 2 is one significant reason for reduced critical current densities and is introduced intrinsically by the anisotropy of B c2 but also extrinsically by the microstructure of the material. B c2 enhancement by doping is another important challenge for chemical analysis and, at present, doping levels are not well controlled on the sub-μm scale. In this paper the quantitative electron microscopy and spectroscopy methods essential for the microstructural analysis of MgB 2 are described. By quantitative electron microscopy and spectroscopy we mean a combined SEM and TEM analysis that covers various length scales from μm to nm. Contamination-free sample preparation, chemical mapping including B, and advanced chemical quantification using x-ray microanalysis were essential elements of the applied methodology. The methodology was applied to in situ and ex situ MgB 2 wires and tapes with and without SiC additives. Quantitative B analysis by EDX spectroscopy was applied quantitatively in the SEM and TEM, which is a major achievement. Although MgB 2 is a binary system, the thermodynamics of phase formation is complex, and the complexity is dramatically increased if additives like SiC are used. The small, sub-μm grain sizes of the matrix and secondary phases require TEM methods. However, granularity on the μm scale was also identified and underlines the importance of the combined SEM and TEM studies. Significant differences in the microstructure were observed for in situ and ex situ samples. This holds particularly if SiC was added and yielded Mg 2 Si for in situ samples annealed at 600-650 deg. C and Mg-Si-O phases

Quantitative characterization of the orientation spread within individual grains in copper after tensile deformation

DEFF Research Database (Denmark)

Krog-Pedersen, Stine; Bowen, Jacob R.; Pantleon, Wolfgang

2009-01-01

By means of electron backscatter diffraction, orientations are determined on a regular grid on a polished section of a copper specimen after tensile deformation to 25%. Individual grains separated by boundaries with disorientation angles above 7° are identified and the microtexture in the form...

Probing insect backscatter cross section and melanization using kHz optical remote detection system

Science.gov (United States)

Gebru, Alem; Brydegaard, Mikkel; Rohwer, Erich; Neethling, Pieter

2017-01-01

A kHz optical remote sensing system is implemented to determine insect melanization features. This is done by measuring the backscatter signal in the visible and near-infrared (VIS-NIR) and short-wave infrared (SWIR) in situ. It is shown that backscatter cross section in the SWIR is insensitive to melanization and absolute melanization can be derived from the ratio of backscatter cross section of different bands (SWIR/VIS-NIR). We have shown that reflectance from insect is stronger in the SWIR as compared to NIR and VIS. This reveals that melanization plays a big role to determine backscatter cross section. One can use this feature as a tool to improve insect species and age classification. To support the findings, we illustrated melanization feature using three different insects [dead, dried specimens of snow white moth (Spilosoma genus), fox moth (Macrothylacia), and leather beetle (Odontotaenius genus)]. It is shown that reflectance from the leather beetle in the VIS and NIR is more affected by melanization as compared with snow white moth.

Analysis of electron beam damage of exfoliated MoS2 sheets and quantitative HAADF-STEM imaging

International Nuclear Information System (INIS)

Garcia, Alejandra; Raya, Andres M.; Mariscal, Marcelo M.; Esparza, Rodrigo; Herrera, Miriam; Molina, Sergio I.; Scavello, Giovanni; Galindo, Pedro L.; Jose-Yacaman, Miguel; Ponce, Arturo

2014-01-01

In this work we examined MoS 2 sheets by aberration-corrected scanning transmission electron microscopy (STEM) at three different energies: 80, 120 and 200 kV. Structural damage of the MoS 2 sheets has been controlled at 80 kV according a theoretical calculation based on the inelastic scattering of the electrons involved in the interaction electron–matter. The threshold energy for the MoS 2 material has been found and experimentally verified in the microscope. At energies higher than the energy threshold we show surface and edge defects produced by the electron beam irradiation. Quantitative analysis at atomic level in the images obtained at 80 kV has been performed using the experimental images and via STEM simulations using SICSTEM software to determine the exact number of MoS 2 layers. - Highlights: • MoS 2 sheets were exfoliated by using hydrogen gas flow to separate the MoS 2 layers. • The optimum energy to avoid structural damage was calculated. • Cs-corrected STEM imaging was used to obtain atomic resolution images. • Three energies were used in STEM imaging: 80, 120 and 200 kV. • A quantitative method for determining the number of layers has been applied

Electron-cloud simulation results for the PSR and SNS

International Nuclear Information System (INIS)

Pivi, M.; Furman, M.A.

2002-01-01

We present recent simulation results for the main features of the electron cloud in the storage ring of the Spallation Neutron Source (SNS) at Oak Ridge, and updated results for the Proton Storage Ring (PSR) at Los Alamos. In particular, a complete refined model for the secondary emission process including the so called true secondary, rediffused and backscattered electrons has been included in the simulation code

Depth distribution of damage obtained by Rutherford backscattering combined with channeling

International Nuclear Information System (INIS)

Behrisch, R.; Roth, J.

1976-01-01

The different approaches to determine depth distributions of damage in solids by Rutherford backscattering combined with channeling are reviewed. These methods are best applicable for damage introduced by ion bombardment. Most investigations up to now have been done at semiconductors where the ion damage seems to be more suited for analysis by this method than the ion damage in metals. The quantity used for getting depth profiles is mostly the increase in minimum yields in single alignment Rutherford backscattering, while only few measurements have been done at double alignment and at slight misalignment, i.e., the sides of the channeling dips

Shallow water acoustic backscatter and reverberation measurements using a 68-kHz cylindrical array

Science.gov (United States)

Gallaudet, Timothy Cole

2001-10-01

The characterization of high frequency, shallow water acoustic backscatter and reverberation is important because acoustic systems are used in many scientific, commercial, and military applications. The approach taken is to use data collected by the Toroidal Volume Search Sonar (TVSS), a 68 kHz multibeam sonar capable of 360° imaging in a vertical plane perpendicular to its direction of travel. With this unique capability, acoustic backscatter imagery of the seafloor, sea surface, and horizontal and vertical planes in the volume are constructed from data obtained in 200m deep waters in the Northeastern Gulf of Mexico when the TVSS was towed 78m below the surface, 735m astern of a towship. The processed imagery provide a quasi-synoptic characterization of the spatial and temporal structure of boundary and volume acoustic backscatter and reverberation. Diffraction, element patterns, and high sidelobe levels are shown to be the most serious problems affecting cylindrical arrays such as the TVSS, and an amplitude shading method is presented for reducing the peak sidelobe levels of irregular-line and non-coplanar arrays. Errors in the towfish's attitude and motion sensor, and irregularities in the TVSS's transmitted beampattern produce artifacts in the TVSS-derived bathymetry and seafloor acoustic backscatter imagery. Correction strategies for these problems are described, which are unique in that they use environmental information extracted from both ocean boundaries. Sea surface and volume acoustic backscatter imagery are used to explore and characterize the structure of near-surface bubble clouds, schooling fish, and zooplankton. The simultaneous horizontal and vertical coverage provided by the TVSS is shown to be a primary advantage, motivating further use of multibeam sonars in these applications. Whereas boundary backscatter fluctuations are well described by Weibull, K, and Rayleigh mixture probability distributions, those corresponding to volume backscatter are

Electron transport in heterogeneous media; Transporte de eletrons em meios heterogeneos

Energy Technology Data Exchange (ETDEWEB)

Falcao, Rossana Cavalieri

1992-05-15

In this work it is presented a model to calculate dose enhancement in the vicinity of plane interfaces irradiated by therapeutic electron beams. The proposed model is based on an approximation of the Boltzmann Equation. The solutions presented to the equation are exact on its angular dependency, making it possible to observe that at low Z/high Z interfaces the dose enhancement is due to an increase of the backscattering. For the inverse situation a decrease of the backscattering can be observed. Calculations have been made for some tissue-metal interfaces irradiated by 13 MeV electron beam. The dose perturbations in tissue were obtained and the results were compared with experimental data as well as Monte Carlo simulations. In both cases the agreement found was very good. (author)

Physical aspects of quantitative particles analysis by X-ray fluorescence and electron microprobe techniques

International Nuclear Information System (INIS)

Markowicz, A.

1986-01-01

The aim of this work is to present both physical fundamentals and recent advances in quantitative particles analysis by X-ray fluorescence (XRF) and electron microprobe (EPXMA) techniques. A method of correction for the particle-size effect in XRF analysis is described and theoretically evaluated. New atomic number- and absorption correction procedures in EPXMA of individual particles are proposed. The applicability of these two correction methods is evaluated for a wide range of elemental composition, X-ray energy and sample thickness. Also, a theoretical model for composition and thickness dependence of Bremsstrahlung background generated in multielement bulk specimens as well as thin films and particles are presented and experimantally evaluated. Finally, the limitations and further possible improvements in quantitative particles analysis by XFR and EPXMA are discussed. 109 refs. (author)

Anelasticity of olivine single crystals investigated by stress-reduction tests and high-angular resolution electron backscatter diffraction

Science.gov (United States)

Wallis, D.; Hansen, L. N.; Kempton, I.; Wilkinson, A. J.

2017-12-01

Geodynamic phenomena, including glacial isostatic adjustment and postseismic deformation, can involve transient deformation in response to changes in differential stress acting on mantle rocks. As such, rheological models of transient deformation are incorporated in predictions of associated processes, including sea-level rise and stress redistribution after earthquakes. However, experimental constraints on rheological models for transient deformation of mantle materials are sparse. In particular, experiments involving stress reductions have been lacking. Moreover, a material's response to a reduction in stress can provide clues to the microphysical processes controlling deformation. To constrain models of transient deformation of mantle rocks we performed stress-reduction tests on single crystals of olivine at 1250-1300°C. Mechanical and piezoelectric actuators controlled constant initial stress during creep. At various strain intervals stress was reduced near-instantaneously using the piezoelectric actuator, inducing both elastic and anelastic (time-dependent) lengthening of the samples. A range of magnitudes of stress reduction were applied, typically unloading 10-90% of the initial stress. High-angular resolution electron backscatter diffraction (HR-EBSD), based on cross-correlation of diffraction patterns, was used to map dislocation density and elastic strain distributions in the recovered samples. Magnitudes of anelastic back-strain increase with increasing magnitudes of stress reduction and show a marked increase when stress reductions exceed 50% of the initial stress, consistent with previous observations in metals and alloys. This observation is inconsistent with the Burgers rheological model commonly used to describe transient behaviour and suggests that the style of rheological behaviour depends on the magnitude of stress change. HR-EBSD maps reveal that the crystal lattices are smoothly curved and generally lack subgrain boundaries and elastic strain

Automated determination of crystal orientations from electron backscattering patterns

DEFF Research Database (Denmark)

Lassen, Niels Christian Krieger

1994-01-01

of the position of the bands or the zone axes of EBSPs have existed for several years now. Until recently, however, the localization of either the bands or the zone axes of EBSPs has required the valuable time and attention of a human operator, thus obviously limiting the amounts of orientation data that can...... quantitatively is therefore described. Presently, little is known about the uncertainty of the lattice orientations which can be measuted from EBSPs. This subject will be discussed in detail in this thesis. With the application of newly developed statistical methods for analyzing orientation data...... it will be shown how the relative precision of lattice orientations measured from EBSPs can be described. By applying this methodology to a large number of EBSPs of varying quality it is demonstrated that the precision of automatically measured crystal orientations is comparable to the precision obtained, when...

Using multi-beam echo sounder backscatter data for sediment classification in very shallow water environments

NARCIS (Netherlands)

Amiri-Simkooei, A.R.; Snellen, M.; Simons, D.G.

2009-01-01

In a recent work described in Ref. [1], an angle-independent methodology was developed to use the multi-beam echo sounder backscatter (MBES) data for the seabed sediment classification. The method employs the backscatter data at a certain angle to obtain the number of sediment classes and to

Electron beam influence on the carbon contamination of electron irradiated hydroxyapatite thin films

International Nuclear Information System (INIS)

Hristu, Radu; Stanciu, Stefan G.; Tranca, Denis E.; Stanciu, George A.

2015-01-01

Highlights: • Carbon contamination mechanisms of electron-beam-irradiated hydroxyapatite. • Atomic force microscopy phase imaging used to detect carbon contamination. • Carbon contamination dependence on electron energy, irradiation time, beam current. • Simulation of backscattered electrons confirms the experimental results. - Abstract: Electron beam irradiation which is considered a reliable method for tailoring the surface charge of hydroxyapatite is hindered by carbon contamination. Separating the effects of the carbon contamination from those of irradiation-induced trapped charge is important for a wide range of biological applications. In this work we focus on the understanding of the electron-beam-induced carbon contamination with special emphasis on the influence of the electron irradiation parameters on this phenomenon. Phase imaging in atomic force microscopy is used to evaluate the influence of electron energy, beam current and irradiation time on the shape and size of the resulted contamination patterns. Different processes involved in the carbon contamination of hydroxyapatite are discussed

High-resolution backscatter power observations of 440-MHz E region coherent echoes at Millstone Hill

International Nuclear Information System (INIS)

Foster, J.C.; Tetenbaum, D.

1991-01-01

A 40-μs pulse length has been used to provide 10-s temporal and 6-km range resolution observations of E region coherent backscatter from the premidnight eastward electrojet region to the north of Millstone Hill. The observations can be divided into two categories: strong events in which the backscattered amplitude nears saturation and weak events in which spatial structure and large-amplitude variations are common. Calibrated observations find a typical volume scattering coefficient of ∼10 -11 m -1 at 440 MHz during strong events with a maximum level of 9 x 10 -10 m -1 observed for brief intervals. During less intense events the radar backscatter is modulated by ∼30dB in amplitude at Pc 5 frequencies (150-500 s) by waves with spatial wavelength 50-100 km. The observations support the premise that the weak irregularities grow linearly with electric field strength and reach a saturation amplitude beyond which the oscillating electric field of the Pc pulsation has little effect. The observed variation of backscattered power with range is interpreted using a geometrical model which accounts for the detailed antenna beam pattern, a magnetic aspect angle sensitivity of -10 dB per degree, and a thin layer of irregularities centered at 110 km altitude. For strongly driven conditions a comparison of the range variation of backscattered power with the thin layer model suggests that the signal power becomes increasingly dominated by strong scatters confined to a narrower altitude range. The apparent altitude extent of the strongest irregularities decreases by a factor of 2 as the amplitude of the backscattered signal increases by a factor of 10

Corneal backscatter in insulin-dependent and non-insulin-dependent diabetes mellitus patients: a pilot study

Directory of Open Access Journals (Sweden)

Ana M Calvo-Maroto

Full Text Available ABSTRACT Purpose: To compare central corneal backscatter obtained from Scheimpflug images between patients with insulin-dependent and non-insulin-dependent diabetes mellitus (IDDM and NIDDM, respectively and healthy controls. Methods: Seven patients with IDDM (7 eyes, eleven patients with NIDDM (11 eyes, and sixteen healthy subjects (16 eyes were included in this pilot study. Scheimpflug imaging system (Pentacam, Oculus Inc., Germany was used to obtain optical sections of the cornea. Seven meridians were analyzed for each eye, oriented from 70° to 110°. Optical density values for the central 3-mm and 5-mm zones of the cornea were obtained by image analysis using external software. Results: Corneal backscatter was significantly higher in the diabetic patients than in the controls for the central 3-mm (p=0.016 and 5-mm (p=0.014 zones. No significant differences in corneal backscatter were found between the IDDM and NIDDM groups for either zone (both p>0.05. In the NIDDM group, significant correlations were observed for both central zones between corneal backscatter and age (3 mm: r=0.604, p=0.025; 5 mm: r=0.614, p=0.022 and central corneal thickness (3 mm: r=0.641, p=0.017; 5 mm: r=0.671, p=0.012; this was not found in the IDDM group (p>0.05. The presence of diabetes showed a significant effect on central corneal backscatter (Kruskal-Wallis test, p<0.001. Conclusions: Diabetic patients showed higher values of corneal light backscatter than healthy subjects. Corneal optical density analysis may be a useful tool for monitoring and assessing the ocular changes caused by diabetes.

A three-dimensional, two-way, parabolic equation model for acoustic backscattering in a cylindrical coordinate system

DEFF Research Database (Denmark)

Zhu, Dong; Jensen, Leif Bjørnø

2000-01-01

. The major drawback of using the cylindrical coordinate system, when the backscattering solution is valid within a limited area, is analyzed using a geometrical-optical interpretation. The model may be useful for studying three-dimensional backscattering phenomena comprising azimuthal diffraction effects...

Electromagnetic backscattering from freak waves in (1 + 1)-dimensional deep-water

International Nuclear Information System (INIS)

Tao, Xie; Tao, Shen; Wei, Chen; Hai-Lan, Kuang; Perrie, William

2010-01-01

To study the electromagnetic (EM) backscatter characteristics of freak waves at moderate incidence angles, we establish an EM backscattering model for freak waves in (1 + 1)-dimensional deep water. The nonlinear interaction between freak waves and Bragg short waves is considered to be the basic hydrodynamic spectra modulation mechanism in the model. Numerical results suggest that the EM backscattering intensities of freak waves are less than those from the background sea surface at moderate incidence angles. The normalised radar cross sections (NRCSs) from freak waves are highly polarisation dependent, even at low incidence angles, which is different from the situation for normal sea waves; moreover, the NRCS of freak waves is more polarisation dependent than the background sea surface. NRCS discrepancies between freak waves and the background sea surface with using horizontal transmitting horizomtal (HH) polarisation are larger than those using vertical transmitting vertical (VV) polarisation, at moderate incident angles. NRCS discrepancies between freak waves and background sea surface decreases with the increase of incidence angle, in both HH and VV polarisation radars. As an application, in the synthetic-aperture radar (SAR) imaging of freak waves, we suggest that freak waves should have extremely low backscatter NRCSs for the freak wave facet with the strongest slope. Compared with the background sea surface, the freak waves should be darker in HH polarisation echo images than in VV echo images, in SAR images. Freak waves can be more easily detected from the background sea surface in HH polarisation images than in VV polarisation images. The possibility of detection of freak waves at low incidence angles is much higher than at high incidence angles. (classical areas of phenomenology)

Near-surface fault detection by migrating back-scattered surface waves with and without velocity profiles

KAUST Repository

Yu, Han

2016-04-26

We demonstrate that diffraction stack migration can be used to discover the distribution of near-surface faults. The methodology is based on the assumption that near-surface faults generate detectable back-scattered surface waves from impinging surface waves. We first isolate the back-scattered surface waves by muting or FK filtering, and then migrate them by diffraction migration using the surface wave velocity as the migration velocity. Instead of summing events along trial quasi-hyperbolas, surface wave migration sums events along trial quasi-linear trajectories that correspond to the moveout of back-scattered surface waves. We have also proposed a natural migration method that utilizes the intrinsic traveltime property of the direct and the back-scattered waves at faults. For the synthetic data sets and the land data collected in Aqaba, where surface wave velocity has unexpected perturbations, we migrate the back-scattered surface waves with both predicted velocity profiles and natural Green\\'s function without velocity information. Because the latter approach avoids the need for an accurate velocity model in event summation, both the prestack and stacked migration images show competitive quality. Results with both synthetic data and field records validate the feasibility of this method. We believe applying this method to global or passive seismic data can open new opportunities in unveiling tectonic features.

Quantitative low-energy electron diffraction analysis of the GaN(000-1) (1×1) reconstruction

Czech Academy of Sciences Publication Activity Database

Romanyuk, Olexandr; Jiříček, Petr; Paskova, T.

2012-01-01

Roč. 606, 7-8 (2012), s. 740-743 ISSN 0039-6028 R&D Projects: GA ČR GPP204/10/P028 Institutional research plan: CEZ:AV0Z10100521 Keywords : gallium nitride * semiconductor surfaces * quantitative low-energy electron diffraction * LEED Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.838, year: 2012

Mapping local anisotropy axis for scattering media using backscattering Mueller matrix imaging

Science.gov (United States)

He, Honghui; Sun, Minghao; Zeng, Nan; Du, E.; Guo, Yihong; He, Yonghong; Ma, Hui

2014-03-01

Mueller matrix imaging techniques can be used to detect the micro-structure variations of superficial biological tissues, including the sizes and shapes of cells, the structures in cells, and the densities of the organelles. Many tissues contain anisotropic fibrous micro-structures, such as collagen fibers, elastin fibers, and muscle fibers. Changes of these fibrous structures are potentially good indicators for some pathological variations. In this paper, we propose a quantitative analysis technique based on Mueller matrix for mapping local anisotropy axis of scattering media. By conducting both experiments on silk sample and Monte Carlo simulation based on the sphere-cylinder scattering model (SCSM), we extract anisotropy axis parameters from different backscattering Mueller matrix elements. Moreover, we testify the possible applications of these parameters for biological tissues. The preliminary experimental results of human cancerous samples show that, these parameters are capable to map the local axis of fibers. Since many pathological changes including early stage cancers affect the well aligned structures for tissues, the experimental results indicate that these parameters can be used as potential tools in clinical applications for biomedical diagnosis purposes.

Model-independent quantitative measurement of nanomechanical oscillator vibrations using electron-microscope linescans

Energy Technology Data Exchange (ETDEWEB)

Wang, Huan; Fenton, J. C.; Chiatti, O. [London Centre for Nanotechnology, University College London, 17–19 Gordon Street, London WC1H 0AH (United Kingdom); Warburton, P. A. [London Centre for Nanotechnology, University College London, 17–19 Gordon Street, London WC1H 0AH (United Kingdom); Department of Electronic and Electrical Engineering, University College London, Torrington Place, London WC1E 7JE (United Kingdom)

2013-07-15

Nanoscale mechanical resonators are highly sensitive devices and, therefore, for application as highly sensitive mass balances, they are potentially superior to micromachined cantilevers. The absolute measurement of nanoscale displacements of such resonators remains a challenge, however, since the optical signal reflected from a cantilever whose dimensions are sub-wavelength is at best very weak. We describe a technique for quantitative analysis and fitting of scanning-electron microscope (SEM) linescans across a cantilever resonator, involving deconvolution from the vibrating resonator profile using the stationary resonator profile. This enables determination of the absolute amplitude of nanomechanical cantilever oscillations even when the oscillation amplitude is much smaller than the cantilever width. This technique is independent of any model of secondary-electron emission from the resonator and is, therefore, applicable to resonators with arbitrary geometry and material inhomogeneity. We demonstrate the technique using focussed-ion-beam–deposited tungsten cantilevers of radius ∼60–170 nm inside a field-emission SEM, with excitation of the cantilever by a piezoelectric actuator allowing measurement of the full frequency response. Oscillation amplitudes approaching the size of the primary electron-beam can be resolved. We further show that the optimum electron-beam scan speed is determined by a compromise between deflection of the cantilever at low scan speeds and limited spatial resolution at high scan speeds. Our technique will be an important tool for use in precise characterization of nanomechanical resonator devices.

A methodology for the extraction of quantitative information from electron microscopy images at the atomic level

International Nuclear Information System (INIS)

Galindo, P L; Pizarro, J; Guerrero, E; Guerrero-Lebrero, M P; Scavello, G; Yáñez, A; Sales, D L; Herrera, M; Molina, S I; Núñez-Moraleda, B M; Maestre, J M

2014-01-01

In this paper we describe a methodology developed at the University of Cadiz (Spain) in the past few years for the extraction of quantitative information from electron microscopy images at the atomic level. This work is based on a coordinated and synergic activity of several research groups that have been working together over the last decade in two different and complementary fields: Materials Science and Computer Science. The aim of our joint research has been to develop innovative high-performance computing techniques and simulation methods in order to address computationally challenging problems in the analysis, modelling and simulation of materials at the atomic scale, providing significant advances with respect to existing techniques. The methodology involves several fundamental areas of research including the analysis of high resolution electron microscopy images, materials modelling, image simulation and 3D reconstruction using quantitative information from experimental images. These techniques for the analysis, modelling and simulation allow optimizing the control and functionality of devices developed using materials under study, and have been tested using data obtained from experimental samples

Comparative study on the dependence of quantitative results in the electron microscopic autoradiography on the type of developer (Microdol X, Phenidon)

International Nuclear Information System (INIS)

David, H.; Marx, I.; Nanoff, S.

1978-01-01

It was the aim of the investigation to compare quantitative results of electron microscopic autoradiographs after the use of different developers (Microdol X, Phenidon) adapting morphometrical methods. Erythroblasts of rabbit were tested after incorporation of 3 H-uridine in vitro. Both developers showed the same tendency at higher rates of incorporation (basophilic erythroblasts and polychromatic erythroblasts). Using Phenidon, however, we could obtain only half the values for the individual cell components. At high rates of incorporation Microdol X results in an overlapping of the silver filaments. Thus, more distinct grains can be reached by Phenidon. At smaller rates of incorporation (orthochromatic erythroblasts) after using. Phenidon a quantitative evaluation is however influenced by too many factors of uncertainty so that according to our investigations Microdol X is better suited for a quantitative evaluation of electron microscopic autoradiographs. (author)

IMPROVED PARAMETERIZATION OF WATER CLOUD MODEL FOR HYBRID-POLARIZED BACKSCATTER SIMULATION USING INTERACTION FACTOR

Directory of Open Access Journals (Sweden)

S. Chauhan

2017-07-01

Full Text Available The prime aim of this study was to assess the potential of semi-empirical water cloud model (WCM in simulating hybrid-polarized SAR backscatter signatures (RH and RV retrieved from RISAT-1 data and integrate the results into a graphical user interface (GUI to facilitate easy comprehension and interpretation. A predominant agricultural wheat growing area was selected in Mathura and Bharatpur districts located in the Indian states of Uttar Pradesh and Rajasthan respectively to carry out the study. The three-date datasets were acquired covering the crucial growth stages of the wheat crop. In synchrony, the fieldwork was organized to measure crop/soil parameters. The RH and RV backscattering coefficient images were extracted from the SAR data for all the three dates. The effect of four combinations of vegetation descriptors (V1 and V2 viz., LAI-LAI, LAI-Plant water content (PWC, Leaf water area index (LWAI-LWAI, and LAI-Interaction factor (IF on the total RH and RV backscatter was analyzed. The results revealed that WCM calibrated with LAI and IF as the two vegetation descriptors simulated the total RH and RV backscatter values with highest R2 of 0.90 and 0.85 while the RMSE was lowest among the other tested models (1.18 and 1.25 dB, respectively. The theoretical considerations and interpretations have been discussed and examined in the paper. The novelty of this work emanates from the fact that it is a first step towards the modeling of hybrid-polarized backscatter data using an accurately parameterized semi-empirical approach.

Direct detection of near-surface faults by migration of back-scattered surface waves

KAUST Repository

Yu, Han

2014-08-05

We show that diffraction stack migration can be used to estimate the distribution of near-surface faults. The assumption is that near-surface faults generate detectable back-scattered surface waves from impinging surface waves. The processing steps are to isolate the back-scattered surface waves, and then migrate them by diffraction migration using the surface wave velocity as the migration velocity. Instead of summing events along trial quasi-hyperbolas, surface wave migration sums events along trial quasi-linear trajectories that correspond to the moveout of back-scattered surface waves. A deconvolution filter derived from the data can be used to collapse a dispersive arrival into a non-dispersive event. Results with synthetic data and field records validate the feasibility of this method. Applying this method to USArray data or passively recorded exploration data might open new opportunities in mapping tectonic features over the extent of the array.

Reson 8101 Backscatter imagery of Penguin Bank, Molokai, Hawaii, USA

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — Backscatter imagery extracted from gridded bathymetry of Penguin Bank, Molokai, Hawaii, USA. These data provide almost complete coverage between 0 and 100 meters....

Investigations of multiple backscattering and albedos of 1.12 MeV gamma photons in elements and alloys

International Nuclear Information System (INIS)

Sabharwal, Arvind D.; Singh, Bhajan; Sandhu, B.S.

2009-01-01

The energy and intensity distributions of multiple backscattering of 1.12 MeV gamma photons emerging from targets of elements and alloys are observed as a function of thickness and atomic number (Z) of the target. The numbers of these multiply backscattered events show an increase with increase in target thickness, and then saturate for a particular thickness of the target called saturation thickness (depth). The saturation thickness decreases with increasing atomic number and varies as e -Z . The multiple backscattering, an interfering background noise in Compton profile, has been successfully used to assign the 'effective atomic number' to alloys. Monte Carlo calculations also support the present experimental results. The number, energy and dose albedos are also found to be saturating for the same thickness where the numbers of multiply backscattered events saturate.

The beam energy measurement system for the Beijing electron-positron collider

International Nuclear Information System (INIS)

Abakumova, E.V.; Achasov, M.N.; Blinov, V.E.; Cai, X.; Dong, H.Y.; Fu, C.D.; Harris, F.A.; Kaminsky, V.V.; Krasnov, A.A.; Liu, Q.; Mo, X.H.; Muchnoi, N.Yu.; Nikolaev, I.B.; Qin, Q.; Qu, H.M.; Olsen, S.L.; Pyata, E.E.; Shamov, A.G.; Shen, C.P.; Todyshev, K.Yu.

2011-01-01

The beam energy measurement system (BEMS) for the upgraded Beijing electron-positron collider BEPC-II is described. The system is based on measuring the energies of Compton back-scattered photons. The relative systematic uncertainty of the electron and positron beam energy determination is estimated as 2×10 -5 . The relative uncertainty of the beam's energy spread is about 6%.

The Backscattering Phase Function for a Sphere with a Two-Scale Relief of Rough Surface

Science.gov (United States)

Klass, E. V.

2017-12-01

The backscattering of light from spherical surfaces characterized by one and two-scale roughness reliefs has been investigated. The analysis is performed using the three-dimensional Monte-Carlo program POKS-RG (geometrical-optics approximation), which makes it possible to take into account the roughness of objects under study by introducing local geometries of different levels. The geometric module of the program is aimed at describing objects by equations of second-order surfaces. One-scale roughness is set as an ensemble of geometric figures (convex or concave halves of ellipsoids or cones). The two-scale roughness is modeled by convex halves of ellipsoids, with surface containing ellipsoidal pores. It is shown that a spherical surface with one-scale convex inhomogeneities has a flatter backscattering phase function than a surface with concave inhomogeneities (pores). For a sphere with two-scale roughness, the dependence of the backscattering intensity is found to be determined mostly by the lower-level inhomogeneities. The influence of roughness on the dependence of the backscattering from different spatial regions of spherical surface is analyzed.

A study of the breakdown of Friedel's law in electron backscatter Kikuchi diffraction patterns: Application to zincblende-type structures

International Nuclear Information System (INIS)

Baba-Kishi, K.Z.

1991-01-01

The breakdown of Friedel's law has been observed in backscatter Kikuchi diffraction patterns (BKDP) obtained in the scanning electron microscope (SEM) from a series of zincblende structures including GaAs, InP, GaSb, CdHgTe and the minerals sphalerite (ZnS), chalcopyrite (CuFeS 2 ) and tetrahedrite (Cu 12 Sb 4 S 13 ). Differences in intensities were observed between the reflections 11anti 1 and 5anti 1anti 1 in InP, GaSb, CdHgTe and sphalerite, thus allowing the non-centrosymmetric point group anti 43 m to be determined. In GaAs, differences in intensities were noted between anti 511 and anti 5anti 11. In chalcopyrite and tetrahedrite, non-equivalent intensities were observed between anti 215 and 2anti 1anti 5 and between 3anti 1anti 2 and 31anti 2, respectively. In addition, BKDPs obtained from chalcopyrite revealed a small displacement at the point where the pair of equivalent reflections anti 406 and 460 intersect within the Kikuchi band 02anti 2. The presence of this displacement together with observation of the breakdown of Friedel's law confirmed the tetragonal point group anti 42m for chalcopyrite. Although the point groups of GaAs, chalcopyrite and tetrahedrite were derived successfully using BKDPs, determination of their space groups proved unsuccessful. The superstructure reflections were invisible because the structure factors are very small. The behaviour of the invisible 200 reflection in GaAs is investigated using many-beam dynamical intensity profiles calculated across the h00 systematic row of reflections. Dynamical intensity profiles calculated across the h00 systematic rows of reflections for Ge, InP and sphalerite are also discussed. (orig.)

New applications of old processes in nondestructive testing - irradiation and backscatter methods

International Nuclear Information System (INIS)

Segebade, C.

1995-01-01

The application of two non-destructive test processes based on photon irradiation measurement is described. The photon backscatter process and the irradiation measurement were used in the technical field and in examining artificial articles. With the aid of the two beam absorption method, wall thicknesses on large liquid containers made of polyethylene and of steel were measured. The same process with a somewhat modified test rig was used in measuring pipe wall thickness on an antique musical instrument. The components made of turbine blade material were excited to X-ray fluorescence with a source of radio nuclides and analysed with a semiconductor detector. This is particularly advantageous for elements which cannot be determined or can only be determined with difficulty by 'conventional' methods (e.g.: yttrium, rhenium). Also the wall thickness measurement for large (diameter approx. 6 m) plastic pipes with the aid of gamma backscatter is described, as is humidity measurement in brick material. Finally, there is a report on wood profile measurement in a stringed instrument with the aid of gamma backscatter. (orig./HP) [de

Airborne detection of oceanic turbidity cell structure using depth-resolved laser-induced water Raman backscatter

Science.gov (United States)

Hoge, F. E.; Swift, R. N.

1983-01-01

Airborne laser-induced, depth-resolved water Raman backscatter is useful in the detection and mapping of water optical transmission variations. This test, together with other field experiments, has identified the need for additional field experiments to resolve the degree of the contribution to the depth-resolved, Raman-backscattered signal waveform that is due to (1) sea surface height or elevation probability density; (2) off-nadir laser beam angle relative to the mean sea surface; and (3) the Gelbstoff fluorescence background, and the analytical techniques required to remove it. When converted to along-track profiles, the waveforms obtained reveal cells of a decreased Raman backscatter superimposed on an overall trend of monotonically decreasing water column optical transmission.

Backscattering Moessbauer spectroscopy of Martian dust

International Nuclear Information System (INIS)

Bertelsen, P.; Madsen, M. B.; Binau, C. S.; Goetz, W.; Gunnlaugsson, H. P.; Hviid, S. F.; Kinch, K. M.; Klingelhoefer, G.; Leer, K.; Madsen, D. E.; Merrison, J.; Olsen, M.; Squyres, S. W.

2005-01-01

We report on the determination of the mineralogy of the atmospherically suspended Martian dust particles using backscattering 57 Fe Moessbauer spectroscopy on dust accumulated onto the magnets onboard the Mars Exploration Rovers. The spectra can be interpreted in terms of minerals of igneous origin, and shows only limited, if any, amounts of secondary minerals that may have formed in the presence of liquid water. These findings suggest that the dust has formed in a dry environment over long time in the history of the planet.

Aspects of electron acoustic wave physics in laser backscatter from plasmas

International Nuclear Information System (INIS)

Sircombe, N J; Arber, T D; Dendy, R O

2006-01-01

Recent experimental results from the Trident laser confirm the importance of kinetic effects in determining laser reflectivities at high intensities. Examples observed include scattering from low frequency electron acoustic waves (EAWs) and the first few stages of a cascade towards turbulence through the Langmuir decay instability. Interpretive and predictive computational capability in this area is assisted by the development of Vlasov codes, which offer high velocity space resolution in high energy regions of particle phase space and do not require analytical pre-processing of the fundamental equations. A direct Vlasov solver, capable of resolving these kinetic processes, is used here to address fundamental aspects of the existence and stability of the electron acoustic wave, together with its collective scattering properties. These simulations are extended to realistic laser and plasma parameters characteristic of single hot-spot experiments. Results are in qualitative agreement with experiments displaying both stimulated Raman and stimulated electron acoustic scattering. The amplitude of simulated EAWs is greater than that observed experimentally and is accompanied by a higher phase velocity. These minor differences can be attributed to the limitations of a one-dimensional collisionless model

Effect of the stimulated Brillouin backscattering on selffocusing threshold

International Nuclear Information System (INIS)

Rubenchik, A.M.; Shapiro, E.G.; Turitsyn, S.K.

1994-03-01

In many physical problems stimulated Brillouin scattering (SBS) and selffocusing are manifested simultaneously. We consider effect of the stimulated Brillouin backscattering (SBS) on self-focusing of laser radiation in plasmas. It was found that the self-focusing may be supressed substantionally by the SBS effect

An algorithm to determine backscattering ratio and single scattering albedo

Digital Repository Service at National Institute of Oceanography (India)

Suresh, T.; Desa, E.; Matondkar, S.G.P.; Mascarenhas, A.A.M.Q.; Nayak, S.R.; Naik, P.

Algorithms to determine the inherent optical properties of water, backscattering probability and single scattering albedo at 490 and 676 nm from the apparent optical property, remote sensing reflectance are presented here. The measured scattering...

Assessment of the CALIPSO Lidar 532 nm attenuated backscatter calibration using the NASA LaRC airborne High Spectral Resolution Lidar

Directory of Open Access Journals (Sweden)

R. R. Rogers

2011-02-01

Full Text Available The Cloud-Aerosol Lidar with Orthogonal Polarization (CALIOP instrument on the Cloud-Aerosol Lidar and Infrared Pathfinder Satellite Observations (CALIPSO spacecraft has provided global, high-resolution vertical profiles of aerosols and clouds since it became operational on 13 June 2006. On 14 June 2006, the NASA Langley Research Center (LaRC High Spectral Resolution Lidar (HSRL was deployed aboard the NASA Langley B-200 aircraft for the first of a series of 86 underflights of the CALIPSO satellite to provide validation measurements for the CALIOP data products. To better assess the range of conditions under which CALIOP data products are produced, these validation flights were conducted under both daytime and nighttime lighting conditions, in multiple seasons, and over a large range of latitudes and aerosol and cloud conditions. This paper presents a quantitative assessment of the CALIOP 532 nm calibration (through the 532 nm total attenuated backscatter using internally calibrated airborne HSRL underflight data and is the most extensive study of CALIOP 532 nm calibration. Results show that HSRL and CALIOP 532 nm total attenuated backscatter agree on average within 2.7% ± 2.1% (CALIOP lower at night and within 2.9% ± 3.9% (CALIOP lower during the day, demonstrating the accuracy of the CALIOP 532 nm calibration algorithms. Additionally, comparisons with HSRL show consistency of the CALIOP calibration before and after the laser switch in 2009 as well as improvements in the daytime version 3.01 calibration scheme compared with the version 2 calibration scheme. Potential biases and uncertainties in the methodology relevant to validating satellite lidar measurements with an airborne lidar system are discussed and found to be less than 4.5% ± 3.2% for this validation effort with HSRL. Results from this study are also compared with prior assessments of the CALIOP 532 nm attenuated backscatter calibration.

Influence of backscattering on the spatial resolution of semiconductor X-ray detectors

International Nuclear Information System (INIS)

Hoheisel, M.; Korn, A.; Giersch, J.

2005-01-01

Pixelated X-ray detectors using semiconductor layers or scintillators as absorbers are widely used in high-energy physics, medical diagnosis, or non-destructive testing. Their good spatial resolution performance makes them particularly suitable for applications where fine details have to be resolved. Intrinsic limitations of the spatial resolution have been studied in previous simulations. These simulations focused on interactions inside the conversion layer. Transmitted photons were treated as a loss. In this work, we also implemented the structure behind the conversion layer to investigate the impact of backscattering inside the detector setup. We performed Monte Carlo simulations with the program ROSI (Roentgen Simulation) which is based on the well-established EGS4 algorithm. Line-spread functions of different fully implemented detectors were simulated. In order to characterize the detectors' spatial resolution, the modulation transfer functions (MTF) were calculated. The additional broadening of the line-spread function by carrier transport has been ignored in this work. We investigated two different detector types: a directly absorbing pixel detector where a semiconductor slab is bump-bonded to a readout ASIC such as the Medipix-2 setup with Si or GaAs as an absorbing semiconductor layer, and flat-panel detectors with a Se or a CsI converter. We found a significant degradation of the MTF compared to the case without backscattering. At energies above the K-edge of the backscattering material the spatial resolution drops and can account for the observed low-frequency drop of the MTF. Ignoring this backscatter effect might lead to misinterpretations of the charge sharing effect in counting pixel detectors

Transport properties and superconductivity in presence of backscattering

International Nuclear Information System (INIS)

Chen, H.; Mattis, D.

1992-01-01

In this paper, the authors achieve an exact evaluation of the Kubo formula for electrical resistivity, with a model in which random impurity scattering is parametrized by random back-scattering matrix elements. If the alloy is a superconductor, our theory allows us to correlate T c with the normal-phase resistivity. The results are in nice agreement with experiment

Micro-PIXE for the quantitative imaging of chemical elements in single cells

International Nuclear Information System (INIS)

Ortega, R.

2013-01-01

Full text: The knowledge of the intracellular distribution of biological relevant metals is important to understand their mechanisms of action in cells, either for physiological, toxicological or pathological processes. However, the direct detection of trace metals in single cells is a challenging task that requires sophisticated analytical developments. The aim of this seminar will be to present the recent achievements in this field using micro-PIXE analysis. The combination of micro-PIXE with RBS (Rutherford Backscattering Spectrometry) and STIM (Scanning Transmission lon Microscopy) allows the quantitative determination of trace metal content within sub-cellular compartments. The application of STlM analysis will be more specifically highlighted as it provides high spatial resolution imaging (<200 nm) and excellent mass sensitivity (<0.1 ng). Application of the STIM-PIXE-RBS methodology is absolutely needed when organic mass loss appears during PIXE-RBS irradiation. This combination of STIM-PIXE-RBS provides fully quantitative determination of trace element content, expressed in μg/g, which is a quite unique capability for micro-PIXE compared to other micro-analytical methods such as the electron and synchrotron X-ray fluorescence or the techniques based on mass spectrometry. Examples of micro-PIXE studies for subcellular imaging of trace elements in the various fields of interest will be presented such as metal-based toxicology, pharmacology, and neuro degeneration [1] R. Ortega, G. Devés, A. Carmona. J. R. Soc. Interface, 6, (2009) S649-S658. (author)

Statistical properties of intensity of partially polarised semiconductor laser light backscattered by a single-mode optical fibre

International Nuclear Information System (INIS)

Alekseev, A E; Potapov, V T; Gorshkov, B G

2015-01-01

We report the results of studying statistical properties of the intensity of partially polarised coherent light backscattered by a single mode optical fibre. An expression is derived for the deviation of the backscattered light intensity depending on the scattering region length, the degree of the light source coherence and the degree of scattered light polarisation. It is shown that the backscattered light in a fibre scattered-light interferometer is partially polarised with the polarisation degree P = 1/3 in the case of external perturbations of the interferometer fibre. (scattering of light)

Quantitative electron probe microanalysis of boron in binary borides

International Nuclear Information System (INIS)

Bastin, G.F.; Heijligers, H.J.M.

1986-01-01

Quantitative electron probe microanalysis has been performed in 27 binary borides in the range of 4-30 keV, both for the metals as well as for Boron. The procedures along which accurate intensity measurements for B-K α must be carried out are discussed in detail. A total of 196 k-ratios with respect to elemental standards for the metal X-ray lines and 180 k-ratios for B-K α relative to elemental Boron have been obtained. These data have been used to arrive at an improved parameterization for the φ(ρz) approach in matrix correction. The resulting new program (BAS861) was compared to 5 other current correction programs. At the same occasion the available set of mass absorption coefficients for Boron was tested on its consistency and better values suggested where necessary. Finally it is shown that the modified version of the Gaussian φ(ρz) approach (BAS861 program) is highly successful in the matrix correction for B-K α : a relative root-mean-square value of 6.30% was obtained. (Auth.)

Sensitivity improvement of a laser interferometer limited by inelastic back-scattering, employing dual readout

International Nuclear Information System (INIS)

Meinders, Melanie; Schnabel, Roman

2015-01-01

Inelastic back-scattering of stray light is a long-standing and fundamental problem in high-sensitivity interferometric measurements and a potential limitation for advanced gravitational-wave (GW) detectors. The emerging parasitic interferences cannot be distinguished from a scientific signal via conventional single readout. In this work, we propose the subtraction of inelastic back-scatter signals by employing dual homodyne detection on the output light, and demonstrate it for a table-top Michelson interferometer. The additional readout contains solely parasitic signals and is used to model the scatter source. Subtraction of the scatter signal reduces the noise spectral density and thus improves the measurement sensitivity. Our scheme is qualitatively different from the previously demonstrated vetoing of scatter signals and opens a new path for improving the sensitivity of future GW detectors and other back-scatter limited devices. (paper)

A Pilot Comparative Study of Quantitative Ultrasound, Conventional Ultrasound, and MRI for Predicting Histology-Determined Steatosis Grade in Adult Nonalcoholic Fatty Liver Disease.

Science.gov (United States)

Paige, Jeremy S; Bernstein, Gregory S; Heba, Elhamy; Costa, Eduardo A C; Fereirra, Marilia; Wolfson, Tanya; Gamst, Anthony C; Valasek, Mark A; Lin, Grace Y; Han, Aiguo; Erdman, John W; O'Brien, William D; Andre, Michael P; Loomba, Rohit; Sirlin, Claude B

2017-05-01

The purpose of this study is to explore the diagnostic performance of two investigational quantitative ultrasound (QUS) parameters, attenuation coefficient and backscatter coefficient, in comparison with conventional ultrasound (CUS) and MRI-estimated proton density fat fraction (PDFF) for predicting histology-confirmed steatosis grade in adults with nonalcoholic fatty liver disease (NAFLD). In this prospectively designed pilot study, 61 adults with histology-confirmed NAFLD were enrolled from September 2012 to February 2014. Subjects underwent QUS, CUS, and MRI examinations within 100 days of clinical-care liver biopsy. QUS parameters (attenuation coefficient and backscatter coefficient) were estimated using a reference phantom technique by two analysts independently. Three-point ordinal CUS scores intended to predict steatosis grade (1, 2, or 3) were generated independently by two radiologists on the basis of QUS features. PDFF was estimated using an advanced chemical shift-based MRI technique. Using histologic examination as the reference standard, ROC analysis was performed. Optimal attenuation coefficient, backscatter coefficient, and PDFF cutoff thresholds were identified, and the accuracy of attenuation coefficient, backscatter coefficient, PDFF, and CUS to predict steatosis grade was determined. Interobserver agreement for attenuation coefficient, backscatter coefficient, and CUS was analyzed. CUS had 51.7% grading accuracy. The raw and cross-validated steatosis grading accuracies were 61.7% and 55.0%, respectively, for attenuation coefficient, 68.3% and 68.3% for backscatter coefficient, and 76.7% and 71.3% for MRI-estimated PDFF. Interobserver agreements were 53.3% for CUS (κ = 0.61), 90.0% for attenuation coefficient (κ = 0.87), and 71.7% for backscatter coefficient (κ = 0.82) (p hepatic steatosis grade in patients with NAFLD.

Investigation of sheared liquids by neutron backscattering and reflectivity

CERN Document Server

Wolff, M; Hock, R; Frick, B; Zabel, H

2002-01-01

We have investigated by neutron scattering structural and dynamical properties of water solutions of the triblock copolymer P85 under shear. To this end a shear cell that suits the requirements for neutron backscattering and another for reflectivity experiments have been built. In reflectivity measurements we find the polymer concentration (nominal concentration of 33% by weight) to vary right at the surface between 12% and 52% for hydrophilic or hydrophobic coated silicon wavers, for temperatures between 18 C and 73 C and for shear rates up to 2500 s sup - sup 1. Additional structural changes deeper in the bulk are also observed. On the backscattering instrument (IN10 at ILL) we find that the liquid appears to stick to the plates of the shear cell, implying an unusual macroscopic velocity distribution that differs from that found earlier for lubrication oils. We report further on changes of the quasielastic line width in the direction of the shear gradient for different temperatures and shear rates. (orig.)

Uranium-contaminated soils: Ultramicrotomy and electron beam analysis

International Nuclear Information System (INIS)

Buck, E.C.; Dietz, N.L.; Bates, J.K.; Cunnane, J.C.

1994-02-01

Uranium-contaminated soils from the U.S. Department of Energy (DOE) Fernald Site, Ohio, have been examined by a combination of scanning electron microscopy with backscattered electron imaging (SEM/BSE) and analytical electron microscopy (AEM). The inhomogeneous distribution of particulate uranium phases in the soil required the development of a method for using ultramicrotomy to prepare transmission electron microscopy (TEM) thin sections of the SEM mounts. A water-miscible resin was selected that allowed comparison between SEM and TEM images, permitting representative sampling of the soil. Uranium was found in iron oxides, silicates (soddyite), phosphates (autunites), and fluorite (UO 2 ). No uranium was detected in association with phyllosilicates in the soil

Remote measurement of water color in coastal waters. [spectral radiance data used to obtain quantitative values for chlorophyll and turbidity

Science.gov (United States)

Weldon, J. W.

1973-01-01

An investigation was conducted to develop procedure to obtain quantitative values for chlorophyll and turbidity in coastal waters by observing the changes in spectral radiance of the backscattered spectrum. The technique under consideration consists of Examining Exotech model 20-D spectral radiometer data and determining which radiance ratios best correlated with chlorophyll and turbidity measurements as obtained from analyses of water samples and sechi visibility readings. Preliminary results indicate that there is a correlation between backscattered light and chlorophyll concentration and secchi visibility. The tests were conducted with the spectrometer mounted in a light aircraft over the Mississippi Sound at altitudes of 2.5K, 2.8K and 10K feet.

High-precision thickness measurements using beta backscatter

International Nuclear Information System (INIS)

Heckman, R.V.

1978-11-01

A two-axis, automated fixture for use with a high-intensity Pm-147 source and a photomultiplier-scintillation beta-backscatter probe for making thickness measurements has been designed and built. A custom interface was built to connect the system to a minicomputer, and software was written to position the tables, control the probe, and make the measurements. Measurements can be made in less time with much greater precision than by the method previously used

Fiscal 1998 development report on the high-accuracy quantitative analysis technique of catalyst surfaces by electron spectroscopy; 1998 nendo denshi bunkoho ni yoru shokubai hyomen koseido teiryo bunseki gijutsu no kaihatsu

Energy Technology Data Exchange (ETDEWEB)

NONE

1999-03-01

This project aims at development of the high-accuracy quantitative analysis technique by electron spectroscopy for surface analysis of catalysts and semiconductors. Since conventional analysis technique using an energy-fixed X-ray excitation source is inadequate to obtain satisfactory surface sensitivity and quantitative accuracy for catalysts, for development of the titled technique, this project makes experiment using energy-variable synchrotron radiation to modify the parameter on motion of low-speed electrons in solids which is obtained by Monte Carlo calculation. For establishment of the high-accuracy quantitative analysis technique of surface compositions of materials such as catalyst of which performance is dominated by utmost surface, the project studies the attenuation length of electrons in solids by electron spectroscopy using soft X-rays from synchrotron radiation. In this fiscal year, the project established the equipment and technique for high-accuracy quantitative analysis of the thickness and electron attenuation length of silicon oxide films on silicon wafers by electron spectroscopy. (NEDO)

Particle-in-cell studies of laser-driven hot spots and a statistical model for mesoscopic properties of Raman backscatter

International Nuclear Information System (INIS)

Albright, B.J.; Yin, L.; Bowers, K.J.; Kline, J.L.; Montgomery, D.S.; Fernandez, J.C.; Daughton, W.

2006-01-01

The authors use explicit particle-in-cell simulations to model stimulated scattering processes in media with both solitary and multiple laser hot spots. These simulations indicate coupling among hot spots, whereby scattered light, plasma waves, and hot electrons generated in one laser hot spot may propagate to neighboring hot spots, which can be destabilized to enhanced backscatter. A nonlinear statistical model of a stochastic beam exhibiting this coupled behavior is described here. Calibration of the model using particle-in-cell simulations is performed, and a threshold is derived for 'detonation' of the beam to high reflectivity. (authors)

Electron backscatter diffraction study of deformation and recrystallization textures of individual phases in a cross-rolled duplex steel

Energy Technology Data Exchange (ETDEWEB)

Zaid, Md; Bhattacharjee, P.P., E-mail: pinakib@iith.ac.in

2014-10-15

The evolution of microstructure and texture during cross-rolling and annealing was investigated by electron backscatter diffraction in a ferritic–austenitic duplex stainless steel. For this purpose an alloy with nearly equal volume fraction of the two phases was deformed by multi-pass cross-rolling process up to 90% reduction in thickness. The rolling and transverse directions were mutually interchanged in each pass by rotating the sample by 90° around the normal direction. In order to avoid deformation induced phase transformation and dynamic strain aging, the rolling was carried out at an optimized temperature of 898 K (625 °C) at the warm-deformation range. The microstructure after cross warm-rolling revealed a lamellar structure with alternate arrangement of the bands of two phases. Strong brass and rotated brass components were observed in austenite in the steel after processing by cross warm-rolling. The ferrite in the cross warm-rolling processed steel showed remarkably strong RD-fiber (RD//< 011 >) component (001)< 011 >. The development of texture in the two phases after processing by cross warm-rolling could be explained by the stability of the texture components. During isothermal annealing of the 90% cross warm-rolling processed material the lamellar morphology was retained before collapse of the lamellar structure to the mutual interpenetration of the phase bands. Ferrite showed recovery resulting in annealing texture similar to the deformation texture. In contrast, the austenite showed primary recrystallization without preferential orientation selection leading to the retention of deformation texture. The evolution of deformation and annealing texture in the two phases of the steel was independent of one another. - Highlights: • Effect of cross warm-rolling on texture formation is studied in duplex steel. • Brass texture in austenite and (001)<110 > in ferrite are developed. • Ferrite shows recovery during annealing retaining the (001

Evaluation of Four Supervised Learning Methods for Benthic Habitat Mapping Using Backscatter from Multi-Beam Sonar

Directory of Open Access Journals (Sweden)

Jacquomo Monk

2012-11-01

Full Text Available An understanding of the distribution and extent of marine habitats is essential for the implementation of ecosystem-based management strategies. Historically this had been difficult in marine environments until the advancement of acoustic sensors. This study demonstrates the applicability of supervised learning techniques for benthic habitat characterization using angular backscatter response data. With the advancement of multibeam echo-sounder (MBES technology, full coverage datasets of physical structure over vast regions of the seafloor are now achievable. Supervised learning methods typically applied to terrestrial remote sensing provide a cost-effective approach for habitat characterization in marine systems. However the comparison of the relative performance of different classifiers using acoustic data is limited. Characterization of acoustic backscatter data from MBES using four different supervised learning methods to generate benthic habitat maps is presented. Maximum Likelihood Classifier (MLC, Quick, Unbiased, Efficient Statistical Tree (QUEST, Random Forest (RF and Support Vector Machine (SVM were evaluated to classify angular backscatter response into habitat classes using training data acquired from underwater video observations. Results for biota classifications indicated that SVM and RF produced the highest accuracies, followed by QUEST and MLC, respectively. The most important backscatter data were from the moderate incidence angles between 30° and 50°. This study presents initial results for understanding how acoustic backscatter from MBES can be optimized for the characterization of marine benthic biological habitats.

Wavelength-dependent backscattering measurements for quantitative monitoring of apoptosis, Part 1: early and late spectral changes are indicative of the presence of apoptosis in cell cultures

Science.gov (United States)

Mulvey, Christine S.; Zhang, Kexiong; Liu, Wei-Han Bobby; Waxman, David J.; Bigio, Irving J.

2011-11-01

Apoptosis, a form of programmed cell death with unique morphological and biochemical features, is dysregulated in cancer and is activated by many cancer chemotherapeutic drugs. Noninvasive assays for apoptosis in cell cultures can aid in screening of new anticancer agents. We have previously demonstrated that elastic scattering spectroscopy can monitor apoptosis in cell cultures. In this report we present data on monitoring the detailed time-course of scattering changes in a Chinese hamster ovary (CHO) and PC-3 prostate cancer cells treated with staurosporine to induce apoptosis. Changes in the backscattering spectrum are detectable within 10 min, and continue to progress up to 48 h after staurosporine treatment, with the magnitude and kinetics of scattering changes dependent on inducer concentration. Similar responses were observed in CHO cells treated with several other apoptosis-inducing protocols. Early and late scattering changes were observed under conditions shown to induce apoptosis via caspase activity assay and were absent under conditions where apoptosis was not induced. Finally, blocking caspase activity and downstream apoptotic morphology changes prevented late scattering changes. These observations demonstrate that early and late changes in wavelength-dependent backscattering correlate with the presence of apoptosis in cell cultures and that the late changes are specific to apoptosis.

Full aperture backscatter diagnostic for the NIF laser facility (abstract)

International Nuclear Information System (INIS)

Sewall, Noel; Lewis, Izzy; Kirkwood, Robert; Moody, John; Celeste, John

2001-01-01

The current schemes for achieving ignition on the National Ignition Facility require efficient coupling of energy from 192 laser beams to the deuterium--tritium fuel capsule. Each laser beam must propagate through a long scalelength plasma region before being converted to x rays (indirect drive) or being absorbed on the capsule (direct drive). Laser-plasma instabilities such as stimulated Brillouin and stimulated Raman scattering (SBS and SRS) will scatter a fraction of the incident laser energy out of the target leading to an overall reduction in the coupling efficiency. It is important to measure the character of this scattered light in order to understand it and to develop methods for reducing it to acceptable levels. We are designing a system called the full aperature backscatter diagnostic with the capability to measure the time-dependent amplitude and spectral content of the light which is backscattered through the incident beam focusing optic. The backscattered light will be collected over about 85% of the full beam aperture and separated into the SBS wavelength band (348--354 nm) and the SRS wavelength band (400--700 nm). Spectrometers coupled to streak cameras will provide time-resolved spectra for both scattered light components. The scattered light amplitude will be measured with fast and slow diodes. The entire system will be routinely calibrated. Analysis of the data will provide important information for reducing scattered power, achieving power balance, and finally achieving ignition

Field emitted electron trajectories for the CEBAF cavity

International Nuclear Information System (INIS)

Yunn, B.C.; Sundelin, R.M.

1993-06-01

Electromagnetic fields of the superconducting 5-cell CEBAF cavity with its fundamental power coupler are solved numerically with URMEL and MAFIA codes. Trajectories of field emitted electrons following the Fowler-Nordheim relation are studied with a numerical program which accepts the URMEL/MAFIA fields. Emission sites and gradients are determined for those electrons which can reach the cold ceramic window either directly or by an energetic backscattering. The peak and average impact energy and current are found. The generation of dark current by field emitted electrons has also been studied, and its relevance to CEBAF operation is briefly discussed

Measurement of the thickness of thin films by backscattered protons

International Nuclear Information System (INIS)

Samaniego, L.E.Q.

1976-07-01

The method of backscattered protons has been used to measure the thickness of thin films. A monoenergetic beam of protons is directed on the film to be measured and the backscattered protons are detected with a particle detector. The film thickness is calculated from the energy spectrum of the protons. In the case of films consisting of several layers of elements with well separated atomic masses, it is possible to separate the spectra of protons scattered from the different elements, permitting a measurement of the thicknesses of the different layers. The method consists of calculating the energy loss of the protons throughout their trajectory, from the point of incidence on the film to the final detection. Thicknesses were measured for the following film combinations: gold on mylar, chromium on mylar, gold on chromium on mylar, and pure mylar. (Author) [pt

Simultaneous observations at different altitudes of ionospheric backscatter in the eastward electrojet

Directory of Open Access Journals (Sweden)

S. E. Milan

1998-01-01

Full Text Available A common feature of evening near-range ionospheric backscatter in the CUTLASS Iceland radar field of view is two parallel, approximately L-shell-aligned regions of westward flow which are attributed to irregularities in the auroral eastward electrojet region of the ionosphere. These backscatter channels are separated by approximately 100–200 km in range. The orientation of the CUTLASS Iceland radar beams and the zonally aligned nature of the flow allows an approximate determination of flow angle to be made without the necessity of bistatic measurements. The two flow channels have different azimuthal variations in flow velocity and spectral width. The nearer of the two regions has two distinct spectral signatures. The eastern beams detect spectra with velocities which saturate at or near the ion-acoustic speed, and have low spectral widths (less than 100 m s–1, while the western beams detect lower velocities and higher spectral widths (above 200 m s–1. The more distant of the two channels has only one spectral signature with velocities above the ion-acoustic speed and high spectral widths. The spectral characteristics of the backscatter are consistent with E-region scatter in the nearer channel and upper-E-region or F-region scatter in the further channel. Temporal variations in the characteristics of both channels support current theories of E-region turbulent heating and previous observations of velocity-dependent backscatter cross-section. In future, observations of this nature will provide a powerful tool for the investigation of simultaneous E- and F-region irregularity generation under similar (nearly co-located or magnetically conjugate electric field conditions.Key words. Auroral ionosphere · Ionospheric irregularities · Plasma convection

The use of multibeam backscatter intensity data as a tool for mapping glacial deposits in the Central North Sea, UK

Science.gov (United States)