Radiation effects on time-dependent deformation: Creep and growth

International Nuclear Information System (INIS)

Simonen, E.P.

1989-03-01

Observations of irradiation creep strain as well as irradiation growth strain and related microstructures are reviewed and compared to mechanisms for radiation effects on time-dependent deformation. Composition, microstructure, stress and temperature affect irradiation creep less than thermal creep. Irradiation creep rates can often dominate thermal creep rates, particularly at low temperatures and low stresses. Irradiation creep mechanisms are classified in two general categories: (1) stress-induced preferential absorption and (2) climb-glide. In the former, creep results from dislocation climb, whereas in the latter, creep results from dislocation glide. The effects of irradiation creep on failure modes in nuclear environments are discussed. 53 refs., 18 figs., 1 tab

Creep model of unsaturated sliding zone soils and long-term deformation analysis of landslides

Science.gov (United States)

Zou, Liangchao; Wang, Shimei; Zhang, Yeming

2015-04-01

Sliding zone soil is a special soil layer formed in the development of a landslide. Its creep behavior plays a significant role in long-term deformation of landslides. Due to rainfall infiltration and reservoir water level fluctuation, the soils in the slide zone are often in unsaturated state. Therefore, the investigation of creep behaviors of the unsaturated sliding zone soils is of great importance for understanding the mechanism of the long-term deformation of a landslide in reservoir areas. In this study, the full-process creep curves of the unsaturated soils in the sliding zone in different net confining pressure, matric suctions and stress levels were obtained from a large number of laboratory triaxial creep tests. A nonlinear creep model for unsaturated soils and its three-dimensional form was then deduced based on the component model theory and unsaturated soil mechanics. This creep model was validated with laboratory creep data. The results show that this creep model can effectively and accurately describe the nonlinear creep behaviors of the unsaturated sliding zone soils. In order to apply this creep model to predict the long-term deformation process of landslides, a numerical model for simulating the coupled seepage and creep deformation of unsaturated sliding zone soils was developed based on this creep model through the finite element method (FEM). By using this numerical model, we simulated the deformation process of the Shuping landslide located in the Three Gorges reservoir area, under the cycling reservoir water level fluctuation during one year. The simulation results of creep displacement were then compared with the field deformation monitoring data, showing a good agreement in trend. The results show that the creeping deformations of landslides have strong connections with the changes of reservoir water level. The creep model of unsaturated sliding zone soils and the findings obtained by numerical simulations in this study are conducive to

Deformation by grain boundary sliding and slip creep versus diffusional creep

International Nuclear Information System (INIS)

Ruano, O A; Sherby, O D; Wadsworth, J.

1998-01-01

A review is presented of the debates between the present authors and other investigators regarding the possible role of diffusional creep in the plastic flow of polycrystalline metals at low stresses. These debates are recorded in eleven papers over the past seventeen years. ln these papers it has been shown that the creep rates of materials in the so-called diffusional creep region are almost always higher than those predicted by the diffusional creep theory. Additionally, the predictions of grain size effects and stress exponents from diffusional creep theory are often not found in the experimental data. Finally, denuded zones have been universally considered to be direct evidence for diffusional creep; but, those reported in the literature are shown to be found only under conditions where a high stress exponent is observed. Also, the locations of the denuded zones do not match those predicted. Alternative mechanisms are described in which diffusion-controlled dislocation creep and/or grain boundary sliding are the dominant deformation processes in low-stress creep. It is proposed that denuded zones are formed by stress-directed grain boundary migration with the precipitates dissolving in the moving grain boundaries. The above observations have led us to the conclusion that grain boundary sliding and slip creep are in fact the principal mechanisms for observations of plastic flow in the so-called diffusional creep regions

Creep of crystals: High-temperature deformation processes in metals, ceramics and minerals

Science.gov (United States)

Poirier, J. P.

An introductory text describing high-temperature deformation processes in metals, ceramics, and minerals is presented. Among the specific topics discussed are: the mechanical aspects of crystal deformation; lattice defects; and phenomenological and thermodynamical analysis of quasi-steady-state creep. Consideration is also given to: dislocation creep models; the effect of hydrostatic pressure on deformation; creep polygonization; and dynamic recrystallization. The status of experimental techniques for the study of transformation plasticity in crystals is also discussed.

Creep deformation behavior in eutectic Sn-Ag solder joints using a novel mapping technique

Energy Technology Data Exchange (ETDEWEB)

Lucas, J.P.; Guo, F.; McDougall, J.; Bieler, T.R.; Subramanian, K.N.; Park, J.K.

1999-11-01

Creep deformation behavior was measured for 60--100 {micro}m thick solder joints. The solder joints investigated consisted of: (1) non-composite solder joints made with eutectic Sn-Ag solder, and (2) composite solder joints with eutectic Sn-Ag solder containing 20 vol.%, 5 {micro}m diameter in-situ Cu{sub 6}Sn{sub 5} intermetallic reinforcements. All creep testing in this study was carried out at room temperature. Qualitative and quantitative assessment of creep deformation was characterized on the solder joints. Creep deformation was analyzed using a novel mapping technique where a geometrical-regular line pattern was etched over the entire solder joint using excimer laser ablation. During creep, the laser-ablation (LA) pattern becomes distorted due to deformation in the solder joint. By imaging the distortion of laser-ablation patterns using the SEM, actual deformation mapping for the entire solder joint is revealed. The technique involves sequential optical/digital imaging of the deformation versus time history during creep. By tracing and recording the deformation of the LA patterns on the solder over intervals of time, local creep data are obtained in many locations in the joint. This analysis enables global and localized creep shear strains and strain rate to be determined.

TEM microstructural analysis of creep deformed CM186LC single crystal Ni-base superalloy

Energy Technology Data Exchange (ETDEWEB)

Dubiel, B.; Czyrska-Filemonowicz, A. [AGH Univ. of Science and Technology, Krakow (Poland); Blackler, M. [Howmet Ltd., Exeter (United Kingdom); Barnard, P.M. [ALSTOM Power Turbo-Systems Technology Centre, Rugby (United Kingdom)

2006-07-01

The nickel based single crystal superalloy CM186LC was extensively investigated as a potential low cost material for industrial gas turbine vanes within the COST522 programme. The alloy exhibits inhomogeneous structure consisting of dendritic regions and eutectic colonies. In the present work attention is focused on microstructural changes observed in single crystal CM186LC following creep deformation at 750 C. Creep tests were conducted at 750 C with an applied stress of 560 or 675 MPa for up to 11440 hours. The microstructure o ruptured and terminated specimens was investigated by scanning (SEM) and transmission (TEM) electron microscopy. TEM analysis revealed the microstructural changes in the CM186LC at primary and secondary creep as well as after creep rupture. (orig.)

Creep deformation in near-γ TiAl. Part 1: The influence of microstructure on creep deformation in Ti-49Al-1V

International Nuclear Information System (INIS)

Worth, B.D.; Jones, J.W.; Allison, J.E.

1995-01-01

The influence of microstructure on creep deformation was examine in the e near-γ TiAl alloy Ti-49Al-1V. Specifically, microstructures with varying volume fractions of lamellar constituent were produced through thermomechanical processing. Creep studies were conducted on these various microstructures under constant load in air at temperatures between 760 C and 870 C and at stresses ranging from 50 to 200 MPa. Microstructure significantly influences the creep behavior of this alloy, with a fully lamellar microstructure yielding the highest creep resistance of the microstructures examined. Creep resistance is dependent on the volume fraction of lamellar constituent, with the lowest creep resistance observed at intermediate lamellar volume fractions. Examination of the creep deformation structure revealed planar slip of dislocations in the equiaxed γ microstructure, while sub-boundary formation was observed in the duplex microstructure. The decrease in creep resistance of the duplex microstructure, compared with the equiaxed γ microstructure, is attributed to an increase in dislocation mobility within the equiaxed γ constituent, that results from partitioning of oxygen from the γ phase to the α 2 phase. Dislocation motion in the fully lamellar microstructure was confined to the individual lamellae, with no evidence of shearing of γ/γ or γ/α 2 interfaces. This suggests that the high creep resistance of the fully lamellar microstructure is a result of the fine spacing of the lamellar structure, which results in a decreased effective slip length for dislocation motion over that found in duplex and equiaxed γ microstructures

Primary and secondary creep in aluminum alloys as a solid state transformation

Science.gov (United States)

Fernández, R.; Bruno, G.; González-Doncel, G.

2016-08-01

Despite the massive literature and the efforts devoted to understand the creep behavior of aluminum alloys, a full description of this phenomenon on the basis of microstructural parameters and experimental conditions is, at present, still missing. The analysis of creep is typically carried out in terms of the so-called steady or secondary creep regime. The present work offers an alternative view of the creep behavior based on the Orowan dislocation dynamics. Our approach considers primary and secondary creep together as solid state isothermal transformations, similar to recrystallization or precipitation phenomena. In this frame, it is shown that the Johnson-Mehl-Avrami-Kolmogorov equation, typically used to analyze these transformations, can also be employed to explain creep deformation. The description is fully compatible with present (empirical) models of steady state creep. We used creep curves of commercially pure Al and ingot AA6061 alloy at different temperatures and stresses to validate the proposed model.

Analysis of stress and deformation in non-stationary creep

International Nuclear Information System (INIS)

Feijoo, R.A.; Taroco, E.; Guerreiro, J.N.C.

1980-12-01

A variational method and its algorithm are presented; they permit the analysis of stress and deformation in non-stationary creep. This algorithm is applied to an infinite cylinder submitted to an internal pressure. The solution obtained is compared with the solution of non-stationary creep problems [pt

Creep deformation and rupture behaviour of 9Cr–1W–0.2V–0.06Ta Reduced Activation Ferritic–Martensitic steel

International Nuclear Information System (INIS)

Vanaja, J.; Laha, K.; Mythili, R.; Chandravathi, K.S.; Saroja, S.; Mathew, M.D.

2012-01-01

Highlights: ► Creep tests on broad temperature and stress ranges were carried out. ► Microstructural instability on creep and thermal exposures were studied using TEM. ► Creep damage tolerance factor of the material was estimated. - Abstract: This paper presents the creep deformation and rupture behaviour of indigenously produced 9Cr–1W–0.2V–0.06Ta Reduced Activation Ferritic–Martensitic (RAFM) steel for fusion reactor application. Creep studies were carried out at 773, 823 and 873 K over a stress range of 100–300 MPa. The creep deformation of the steel was found to proceed with relatively shorter primary regime followed by an extended tertiary regime with virtually no secondary regime. The variation of minimum creep rate of the material with applied stress followed a power law relation, ε m = Aσ n , with stress exponent value ‘n’ decreasing with increase in temperature. The product of minimum creep rate and creep rupture life was found to obey the modified Monkman–Grant relation. The time to onset of tertiary stage of deformation was directly proportional to rupture life. TEM studies revealed relatively large changes in martensitic sub-structure and coarsening of precipitates in the steel on creep exposure as compared to thermal exposure. Microstructural degradation was considered as the prime cause of extended tertiary stage of creep deformation, which was also reflected in the damage tolerance factor λ with a value more than 2.5. In view of the microstructural instability of the material on creep exposure, the variation of minimum creep rate with stress and temperature did not obey Dorn's equation modified by invoking Lagneborg and Bergman's concepts of back stress.

Creep deformation of restorative resin-composites intended for bulk-fill placement.

Science.gov (United States)

El-Safty, S; Silikas, N; Watts, D C

2012-08-01

To determine the creep deformation of several "bulk-fill" resin-composite formulations in comparison with some other types. Six resin-composites; four bulk-fill and two conventional were investigated. Stainless steel split molds (4 mm × 6 mm) were used to prepare cylindrical specimens for creep testing. Specimens were thoroughly irradiated with 650 mW cm(-2). A total of 10 specimens for each material were divided into two groups (n = 5) according to the storage condition; Group A stored dry at 37 °C for 24h and Group B stored in distilled water at 37 °C in an incubator for 24h. Each specimen was loaded (20 MPa) for 2h and unloaded for 2h. The strain deformation was recorded continuously for 4h. Statistical analysis was performed using a two-way ANOVA followed by one-way ANOVA and the Bonferroni post hoc test at a significance level of a = 0.05. The maximum creep strain % ranged from 0.72% up to 1.55% for Group A and the range for Group B increased from 0.79% up to 1.80% due to water sorption. Also, the permanent set ranged from 0.14% up to 0.47% for Group A and from 0.20% up to 0.59% for Group B. Dependent on the material and storage condition, the percentage of creep strain recovery ranged between 64% and 81%. Increased filler loading in the bulk-fill materials decreased the creep strain magnitude. Creep deformation of all studied resin-composites increased with wet storage. The "bulk-fill" composites exhibited an acceptable creep deformation and within the range exhibited by other resin-composites. Copyright © 2012 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Shear Creep Simulation of Structural Plane of Rock Mass Based on Discontinuous Deformation Analysis

Directory of Open Access Journals (Sweden)

Guoxin Zhang

2017-01-01

Full Text Available Numerical simulations of the creep characteristics of the structural plane of rock mass are very useful. However, most existing simulation methods are based on continuum mechanics and hence are unsuitable in the case of large displacements and deformations. The discontinuous deformation analysis method proposed by Genhua is a discrete one and has a significant advantage when simulating the contacting problem of blocks. In this study, we combined the viscoelastic rheological model of Burgers with the discontinuous deformation analysis (DDA method. We also derived the recurrence formula for the creep deformation increment with the time step during numerical simulations. Based on the minimum potential energy principle, the general equilibrium equation was derived, and the shear creep deformation in the structural plane was considered. A numerical program was also developed and its effectiveness was confirmed based on the curves obtained by the creep test of the structural plane of a rock mass under different stress levels. Finally, the program was used to analyze the mechanism responsible for the creep features of the structural plane in the case of the toppling deformation of the rock slope. The results showed that the extended DDA method is an effective one.

Investigation of creep deformation mechanisms at intermediate temperatures in Rene 88 DT

International Nuclear Information System (INIS)

Viswanathan, G.B.; Sarosi, P.M.; Henry, M.F.; Whitis, D.D.; Milligan, W.W.; Mills, M.J.

2005-01-01

Creep deformation substructures in the superalloy Rene 88 DT have been investigated after small-strain (0.2-0.5%) creep at 650 deg C using conventional and high resolution transmission electron microscopy. Clear differences in creep strength and deformation mechanisms have been observed as a function of applied stress and precipitate microstructure. Both coarse and fine bimodal precipitate microstructures have been tested, produced by relatively slow and fast cooling from the supersolvus solutionizing temperature. The finer γ' microstructure exhibited significantly lower creep rates. It has been established that microtwinning caused by the passage of Shockley partial dislocations on successive {1 1 1} planes is the dominant deformation process at low applied stress, and changes to shearing by 1/2[1 1 0] dislocations and Orowan looping around the larger secondary precipitates at higher applied stress. In the coarser microstructure, the dominant deformation mode is isolated faulting where 1/2[1 1 0] dislocations shear the matrix while superlattice extrinsic stacking faults are created in the secondary γ' particles. The detailed mechanisms by which these deformation modes proceed are discussed, leading to the proposition that the thermally activated process for both microtwinning and isolated faulting is similar, involving diffusion-mediated re-ordering within the γ' particles in the wake of shearing 1/6 Shockley partials. Based on the present evidence, it is proposed that the tertiary γ' volume fraction is crucial in dictating the transition in mechanism and the creep strength of these alloys

Post- and interseismic deformation due to both localized and distributed creep at depth (Invited)

Science.gov (United States)

Hetland, E. A.; Zhang, G.; Hines, T.

2013-12-01

There are two end-member representations of the ductile lithosphere (i.e., the lower crust and uppermost mantle) commonly used in models of post- and interseismic deformation around strike-slip faults: either (1) laterally homogeneous ductile layers, with sharp contrasts in rheological properties between the layers, in which creep is distributed; or (2) discrete extensions of the fault at depth in which creep is fully localized. The most realistic representation of the ductile lithosphere on earthquake cycle time scales likely falls between these two end-members. Researchers have considered both distributed and localized creep when interpreting post- and interseismic deformation, although the two mechanisms are most commonly treated separately, with the localized creep often approximated by kinematic slip on planar faults. There are a few noteworthy models that considered the feedback between both distributed and localized creep, although those models were largely constrained to 2D geometries of infinite length faults. The thickness of shear zones in the ductile lithosphere may be comparable to the locking depth of the fault, and the existence of a deep shear zone does not preclude the possibility that some distributed creep occurs in the surrounding lithosphere. Furthermore, variations in rheology, including both rheological models and their parameters, may be more subtle than the discrete contrasts typically assumed. In this presentation, we consider models of postseismic deformation following a finite length, strike-slip fault, as well as models of interseismic deformation around an infinite length strike-slip fault. Both sets of models are capable of localized and distributed creep at depth, and use Maxwell viscoelasticity. We show that the horizontal surface velocities during the early postseismic period are most sensitive to the viscosity of the shear zone; however during much of the interseismic period the shear zone is not apparent from the surface

Evaluation of Permanent Deformation of Unmodified and Rubber-Reinforced SMA Asphalt Mixtures Using Dynamic Creep Test

Directory of Open Access Journals (Sweden)

Herda Yati Katman

2015-01-01

Full Text Available This paper presents the evaluation of permanent deformation of rubber-reinforced SMA asphalt mixtures by using dynamic creep test. The effect of trans-polyoctenamer as a cross-linking agent in permanent deformation of rubberized mixtures was also evaluated. Dynamic creep test was conducted at different stress levels (200 kPa, 400 kPa and temperatures (40°C, 50°C. Permanent deformation parameters such as dynamic creep curve, ultimate strain, and creep strain slope (CSS were used to analyse the results. Finally, the creep behaviour of the specimens was estimated by the Zhou three-stage creep model. The results show that crumb rubber and trans-polyoctenamer significantly affected the parameters especially at high stress and temperatures. Consistent findings were observed for all permanent deformation parameters. Moreover, based on Zhou model, it was concluded that resistance to permanent deformation was improved by application of crumb rubber and trans-polyoctenamer.

Constitutive relations describing creep deformation for multi-axial time-dependent stress states

Science.gov (United States)

McCartney, L. N.

1981-02-01

A THEORY of primary and secondary creep deformation in metals is presented, which is based upon the concept of tensor internal state variables and the principles of continuum mechanics and thermodynamics. The theory is able to account for both multi-axial and time-dependent stress and strain states. The wellknown concepts of elastic, anelastic and plastic strains follow naturally from the theory. Homogeneous stress states are considered in detail and a simplified theory is derived by linearizing with respect to the internal state variables. It is demonstrated that the model can be developed in such a way that multi-axial constant-stress creep data can be presented as a single relationship between an equivalent stress and an equivalent strain. It is shown how the theory may be used to describe the multi-axial deformation of metals which are subjected to constant stress states. The multi-axial strain response to a general cyclic stress state is calculated. For uni-axial stress states, square-wave loading and a thermal fatigue stress cycle are analysed.

Variation of martensite lath width and precipitate size during creep deformation in a 10Cr-Mo steel

International Nuclear Information System (INIS)

Kim, S. H.; Song, B. Z.; Lu, W. S.

2001-01-01

The relationship between creep deformation and microstructural changes in martensitic 10Cr-MoW steel has been studied. Transmission electron microscopy and image analyser were used to determine the variation of precipitates and martensite lath width size during creep deformation and aging. As precipitates are coarsened during creep deformation, dislocations become easy to move and the recovery proceeds rapidly. This leads to the growth of lath width. The average size of precipitates was linearly increased with creep time. On the other hand the growth rate of lath width is constant until tertiary creep, but the growth of lath width is accelerated during tertiary creep. It has been concluded that the growth behavior of lath width are consistent with creep deformation. Because the growth of lath width is controlled by the coarsening of precipitates it is important to form more stable precipitates in creep condition for improvement of creep properties of martensitie steel. Microstructure of martensitic steel is thermally very stable, so the size of precipitates and martensite lath width are hardly changed during aging

Creep deformation mechanisms in a γ titanium aluminide

Energy Technology Data Exchange (ETDEWEB)

Abdallah, Zakaria [Institute of Structural Materials, College of Engineering, Bay Campus, Swansea University, Swansea SA18EN (United Kingdom); Ding, Rengen [School of Metallurgy and Materials, University of Birmingham, Edgbaston, Birmingham B152TT (United Kingdom); Martin, Nigel; Dixon, Mark [Rolls-Royce plc, P.O. Box 31, Derby DE248BJ (United Kingdom); Bache, Martin [Institute of Structural Materials, College of Engineering, Bay Campus, Swansea University, Swansea SA18EN (United Kingdom)

2016-09-15

Titanium aluminides (TiAl) are considered as potential alternatives to replace nickel-based alloys of greater density for selected components within future gas turbine aero-engines. This is attributed to the high specific strength as well as the good oxidation resistance at elevated temperatures. The gamma (γ) titanium aluminide system Ti-45Al-2Mn-2Nb has previously demonstrated promising performance in terms of its physical and mechanical properties. The main aim of the current study, which is a continuation of a previously published paper, aims at evaluating the performance of this titanium aluminide system under high temperature creep conditions. Of particular interest, the paper is strongly demonstrating the precise capability of the Wilshire Equations technique in predicting the long-term creep behaviour of this alloy. Moreover, it presents a physically meaningful understanding of the various creep mechanisms expected under various testing conditions. To achieve this, two creep specimens, tested under distinctly different stress levels at 700 °C have been extensively examined. Detailed microstructural investigations and supporting transmission electron microscopy (TEM) have explored the differences in creep mechanisms active under the two stress regimes, with the deformation mechanisms correlated to Wilshire creep life prediction curves.

Microstructural evolution during creep deformation of an 11CrMoVNb ferritic heat resistant steel

Energy Technology Data Exchange (ETDEWEB)

Lee, Kyu-Ho; Park, Dae-Bum [Korea Institute of Science and Technology, Seoul (Korea, Republic of). Materials and Devices Div.; Korea Univ., Seoul (Korea, Republic of). Dept. of Materials Science; Kwun, S.I. [Korea Univ., Seoul (Korea, Republic of). Dept. of Materials Science; Suh, Jin-Yoo; Jung, Woo-Sang [Korea Institute of Science and Technology, Seoul (Korea, Republic of). Materials and Devices Div.

2010-07-01

The effect of creep deformation on the microstructural development of an 11CrMoVNb ferritic heat resistant steel during high temperature creep test is investigated. Coarsening behavior of the precipitates, M{sub 23}C{sub 6} and MX, and growth behavior of martensite laths of crept specimens are carefully observed from both gage and grip parts of the specimens in order to discuss the effect of deformation. Particle coarsening and martensite lath widening are pronounced in the gage part due to the creep deformation. (orig.)

Creep Deformation and Fracture Processes in OF and OFP Copper

International Nuclear Information System (INIS)

Bowyer, William H.

2004-10-01

The literature on creep processes in many materials, including copper, has been thoroughly reviewed and complemented by Ashby and co-workers. They have provided physical models which describe the deformation and fracture processes with good qualitative and quantitative agreement with experimental data for many cases. A description of the deformation and fracture models is provided and the relevant equations are included in the appendices. Published data from the canister development programme has been compared with the predictions from the models. The purpose was to improve our understanding of (1) a reported benefit to creep performance which arises from additions of 50 ppm phosphorus to oxygen free (OF) copper, and (2) an observed transition from brittle to ductile failure in OF copper. The models adequately describe the general variations in the observed creep behaviour of the experimental materials. Steady state creep rates for OF copper are observed to be up to one order of magnitude higher than the model predicts for pure copper across a wide range of temperatures and stresses in the power law and power law breakdown regimes. For OF copper with 50ppm of phosphorus added (OFP copper), observed steady state creep rates in the power law breakdown regime are up to one order of magnitude lower than the model predicts for pure copper. Creep lives in the experimental OFP material are also higher than creep lives for OF material under similar conditions. The lower creep deformation rates and the longer creep lives of OFP material are attributed the known effects of phosphorus on recovery in copper. The model predicts that the same mechanism will improve creep lives under repository conditions. It is suggested that the factor of improvement under repository conditions will be less than the factor which is observed in the power law breakdown regime. Predicted creep lives, based on measured steady state creep rates and stress exponents ('n' values) are in good agreement

Creep deformation behaviour and microstructural changes in Zr-2.5% Nb alloy

International Nuclear Information System (INIS)

Chaudhuri, S.; Singh, R.; Ghosh, R.N.; Sinha, T.K.; Banerjee, S.

2002-01-01

Cold worked and stress relieved Zr-2.5% Nb alloy is a well-known material used as pressure tubes in Pressurised Heavy Water Reactors. The pressure tubes, made of a typical Zr-alloy, consisting of 2.54% Nb, 0.1175% oxygen and less than 100 ppm impurities, are expected to withstand 9.5 MPa to 12.5 MPa pressure at 250 degC to 310 degC under fast neutron fluxes of 3.5 x 10 17 nm -2 s -1 . These tubes are made by hot extrusion at 780 degC with an extrusion ratio 8.3:1 and 40% cold pilgering followed by annealing at 550 degC for 3 hours and subsequently by 20-30% cold pilgering and stress relieving at 400 degC for 24 hours. The microstructure of such cold worked and stress relieved alloy consists of Β-Zr precipitates in the matrix of elongated Α-Zr grains. Although various factors such as irradiation creep, thermal creep, irradiation growth etc are responsible for limiting the life of pressure tubes; the thermal creep contributes significantly in overall creep deformation. Keeping this in view as well as due to non-availability of adequate published information including creep database on this alloy, an extensive investigation on the thermal creep behaviour of indigenously produced Zr-2.5% Nb alloy was undertaken. The creep tests in air using Mayes' creep testing machines were carried out in the temperature range of 300 degC to 450 degC under stresses in the range of 50 to 550 MPa. Analysis of data revealed that the mechanism of creep deformation remains the same in this range

NORA-2, a model for creep deformation and rupture of zircaloy at high temperatures

International Nuclear Information System (INIS)

Raff, S.; Meyder, R.

1983-01-01

A model has been developed to describe Zircaloy cladding behaviour under LOCA and small leak conditions within specified temperature range and strain rates. The deformation model consists of a strain rate equation with two components representing strain rate controlled contributions from different deformation mechanisms. Transition from one mechanism to the other produces the strain rate dependence of the stress exponent of steady state creep. During transient creep the change of creep mechanisms produces a flow softening behaviour which induces unstable creep. Together with a strain hardening model, the strain history can be described for low and high strain values. The influence of oxidation is taken into account by modelling hardening due to solid solution of oxygen, cracking of the brittle oxide and oxygen stabilised α-phase layers, and by an oxidation-induced creep component in steam atmosphere. The rupture criterion is based on a strain fraction rule whose variables are temperature, strain rate or applied stress, and oxygen content. (author)

Creep equations for gas turbine materials

International Nuclear Information System (INIS)

Kloos, K.H.; Granacher, J.; Preussler, T.

1988-01-01

The long-term high-temperature deformation behaviour of typical gas turbine materials can be described on the basis of a differentiated evaluation which takes the results from thermal tension tests, short-term creep tests with continuous extension measurement, long-term creep tests with discontinuous extension measurement as well as annealing tests with contraction measurement into account. By this, especially the 'negative creeping' can be controlled. Equations were developed for individual materials of the type IN-738 LC, IN-939, IN-100 and FSX-414, which describe the high-temperature deformation behaviour with consideration to the primary and secondary creeping and partly the tertiary creeping. The equations are valid in the entire application-relevant range, i.e. up to 100 000 h in the case of industrial turbine materials. (orig.) [de

Online interferometric study of viscoelastic rupture and necking deformation of as-spun (iPP) fibres due to creep process.

Science.gov (United States)

Sokkar, Taha; El-Farahaty, Kermal; Azzam, Amira

2015-01-01

Creep deformation under constant load leads to rupture when the polymer chains can no longer separate and accommodate the load. This fracture phenomenon is investigated interferometrically. The creep behaviour of as-spun isotactic Polypropylene (iPP) fibres is studied at different stresses, different initial lengths and different radii. The creep rate, which defines the velocity of the creep deformation and the dimensional stability of the material, is studied. The failure time and stress of iPP due to creep process is determined. The necking deformation was in situ detected during creep process. The mean refractive indices (n(P) andn⊥) profiles of iPP fibres were determined at different positions along the fibre axis before and after necking. The relation between the creep behaviour and different optical and structural parameters is investigated. Microinterferograms are given for illustration. © 2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.

Creep fracture mechanics analysis for through-wall cracked pipes under widespread creep condition

International Nuclear Information System (INIS)

Huh, Nam Su; Kim, Yun Jae; Kim, Young Jin

2003-01-01

This paper compares engineering estimation schemes of C * and creep COD for circumferential and axial through-wall cracked pipes at elevated temperatures with detailed 3-D elastic-creep finite element results. Engineering estimation schemes included the GE/EPRI method, the reference stress method where reference stress is defined based on the plastic limit load and the enhanced reference stress method where the reference stress is defined based on the optimized reference load. Systematic investigations are made not only on the effect of creep-deformation behaviour on C * and creep COD, but also on effects of the crack location, the pipe geometry, the crack length and the loading mode. Comparison of the FE results with engineering estimations provides that for idealized power law creep, estimated C * and COD rate results from the GE/EPRI method agree best with FE results. For general creep-deformation laws where either primary or tertiary creep is important and thus the GE/EPRI method is hard to apply, on the other hand, the enhanced reference stress method provides more accurate and robust estimations for C * and COD rate than the reference stress method

Cavitation in the neck of a deformed Ti-47Al-2Nb-2Cr creep specimen

International Nuclear Information System (INIS)

Sneary, P.R.; Beals, R.S.; Bieler, T.R.

1996-01-01

In creep deformation, intergranular cavitation is the predominant damage process that leads to fracture. In addition to the strain rate, nucleation and growth of cavities are the most important issues to examine when considering material lifetimes. Cavities tend to grow on boundaries normal to the tensile stress axis. Constrained cavity growth models describe how the growth rate is retarded due to the need for the surrounding matrix to accommodate the volume increase. Near-γ TiAl has a microstructure that is very sensitive to heat treatment and deformation history. In this study, the authors investigate a necked creep specimen upon which creep rates were evaluated in a history that started with a large stress and steadily decreased by stress changes through the end of the experiment. Since creep rates at similar stresses are as much as an order of magnitude higher than in a specimen deformed in a generally increasing stress change history, the cavitation evident in the neck is expected to be strongly affected by the particular deformation history in the material

Microstructures of beta-silicon carbide after irradiation creep deformation at elevated temperatures

International Nuclear Information System (INIS)

Katoh, Yutai; Kondo, Sosuke; Snead, Lance L.

2008-01-01

Microstructures of silicon carbide were examined by transmission electron microscopy (TEM) after creep deformation under neutron irradiation. Thin strip specimens of polycrystalline and monocrystalline, chemically vapor-deposited, beta-phase silicon carbide were irradiated in the high flux isotope reactor to 0.7-4.2 dpa at nominal temperatures of 640-1080 deg. C in an elastically pre-strained bend stress relaxation configuration with the initial stress of ∼100 MPa. Irradiation creep caused permanent strains of 0.6 to 2.3 x 10 -4 . Tensile-loaded near-surface portions of the crept specimens were examined by TEM. The main microstructural features observed were dislocation loops in all samples, and appeared similar to those observed in samples irradiated in non-stressed conditions. Slight but statistically significant anisotropy in dislocation loop microstructure was observed in one irradiation condition, and accounted for at least a fraction of the creep strain derived from the stress relaxation. The estimated total volume of loops accounted for 10-45% of the estimated total swelling. The results imply that the early irradiation creep deformation of SiC observed in this work was driven by anisotropic evolutions of extrinsic dislocation loops and matrix defects with undetectable sizes

Effect of grain boundary complexions on the deformation behavior of Ni bicrystal during bending creep.

Science.gov (United States)

Reddy, K Vijay; Pal, Snehanshu

2018-03-07

The dependence of creep deformation behavior of nickel bicrystal specimens on grain boundary (GB) complexion was investigated by performing a simulated bending creep test using molecular dynamics methods. Strain burst phenomena were observed during the low temperature [500 K, i.e., creep process. Atomic strain and dislocation analyses showed that the time of occurrence of strain burst depends on how easily GB migration happens in bicrystal specimens. Specimens with kite monolayer segregation GB complexion were found to be stable at low temperature (500 K), whereas specimens with split-kite GB complexion were stable at a comparatively higher temperature (900 K). In case of further elevated creep temperatures, e.g., 1100 K and 1300 K, split-kite GB complexion becomes unstable and leads to early failure of the specimen at those temperatures. Additionally, it was observed that split-kite bilayer segregation and normal kite GB complexions exhibit localized increases in elastic modulus during bending creep process, occurring at temperatures of 1100 K and 1300 K, respectively, due to the formation of interpenetrating icosahedral clusters. Graphical abstract Representative creep curves during bending creep deformation of various grain boundary complexions at 900 K.

Creep curve formularization at 950degC for Hastelloy XR

International Nuclear Information System (INIS)

Kaji, Yoshiyuki; Muto, Yasushi

1991-03-01

Creep tests under constant stress were conducted on a nickel-base heat-resistant alloy, Hastelloy XR, in air at 950degC. Minimum creep strain rate, time to the onset of tertiary creep and time to rupture were obtained as a function of applied stress. Then, a creep constitutive equation was made based on the Garofalo formula for primary and secondary creep and based on the Kachanov-Rabotnov formula for tertiary creep, which could represent fairly well the experimental creep deformation curves under the constant stress conditions. The creep deformation under the constant load condition corresponding to the stress increment was analysed using the creep constitutive equation and strain hardening law. Then the calculated creep strain showed slightly higher value than the experimental creep strain, and the calculated life was shorter than the experimental one. (author)

Deformation mechanisms at intermediate creep temperatures in the Ni-base superalloy Rene 88 DT

International Nuclear Information System (INIS)

Viswanathan, G.B.; Sarosi, Peter M.; Whitis, Deborah H.; Mills, Michael J.

2005-01-01

Creep deformation substructures in superalloy Rene 88 DT have been investigated at two applied stress levels after small-strain (0.5%) creep at 650 deg. C using conventional and high resolution transmission electron microscopy. Clear differences in creep strength and substructures have been observed as a function of applied stress. It has been established that at intermediate temperatures microtwinning caused by the passage of Shockley partial dislocations on successive {1 1 1} planes is the dominant deformation process at low applied stress. At higher applied stress the mechanism changes to planar shearing of the matrix by 1/2 unit dislocations and Orowan looping of the precipitates. Detailed experimental evidences for these operating processes are shown and possible explanation is provided

Significance of primary irradiation creep in graphite

CSIR Research Space (South Africa)

Erasmus, C

2013-05-01

Full Text Available Traditionally primary irradiation creep is introduced into graphite analysis by applying the appropriate amount of creep strain to the model at the initial time-step. This is valid for graphite components that are subjected to high fast neutron flux...

Influence of microstructural parameters on the deformation and failure behaviour of the ODS alloy PM 2000 under creep and creep-fatigue loading

International Nuclear Information System (INIS)

Bothe, K.; Kussmaul, K.; Maile, K.

1999-01-01

The influence of grain size, manufacturing type and specimen direction (anisotropy) with respect to deformation and failure behaviour under creep, fatigue and creep-fatigue load was investigated. Thus, a basis for the correlation between microstructure and mechanical behaviour has been established. The specific damage and failure behaviour could be explained by means of the different microstructures observed. (orig.)

Biaxial creep deformation of Zircaloy-4 in the high alpha phase temperature range

International Nuclear Information System (INIS)

Donaldson, A.T.; Horwood, R.A.; Healey, T.

1983-01-01

The ballooning response of Zircaloy-4 fuel tubes during a postulated loss-of-coolant accident may be calculated from a knowledge of the thermal environment of the rods and the creep deformation characteristics of the cladding. In support of such calculations biaxial creep studies have been performed on fuel tubes supplied by Westinghouse, Wolverine and Sandvik of temperatures in the alpha phase range. This paper presents the results of an investigation of their respective creep behaviour which has resulted in the formulation of equations for use in LOCA fuel ballooning codes. (author)

Internal stress model for pre-primary stage of low-stress creep

International Nuclear Information System (INIS)

Kloc, L

2010-01-01

Initial transient stage in low-stress creep experiments was observed in all such experiments. Recently, evidences were presented that this stage cannot be considered as a normal creep primary stage, though the shape of the creep curve is similar. The strain reached during this so called pre-primary stage is fully recoverable upon unloading; the internal stresses must play important role in the effect. Model of standard linear anelastic solid was modified by introduction of creeping body instead of viscous dashpot. Both power law and hyperbolic sine creep law were used to fit observed creep curves of model and structural materials. Mainly the model using hyeprbolic sine creep law provides good fit to individual creep curves and sets of creep curves at different stresses.

Life prediction of simple structures subject to cyclic primary and secondary loading resulting in creep and platicity

International Nuclear Information System (INIS)

Otter, N.R.; Jones, R.T.

1979-01-01

High temperature reactors are subject to cyclic mechanical and thermal loadings resulting from start up and shut down operations. The design must therefore guard against structural failure resulting from excessive deformation and creep-fatigue damage. Before any simplified inelastic analysis techniques can be applied, their validity needs to be examined under situations representative of the reactor. For this to be carried out it is necessary to determine the behaviour of components, initially geometrically simple, subject to loadings, cyclic primary and secondary in nature, which result in creep and plasticity. Beam-like structures have been investigated on a finite element basis with the aim of determining how cyclic plasticity, creep enhancement and plastic ratchetting vary in relationship with modified shakedown criteria, magnitude of loading and hold time. (orig.)

CANSWEL-2: a computer model of the creep deformation of Zircaloy cladding under loss-of-coolant accident conditions

International Nuclear Information System (INIS)

Haste, T.J.

1982-07-01

The CANSWEL-2 code models cladding creep deformation under conditions relevant to a loss-of-coolant accident (LOCA) in a pressurised water reactor (PWR). It considers in detail the centre rod of a 3 x 3 nominally square array, taking into account azimuthal non-uniformities in cladding thickness and temperature, and the mechanical restraint imposed on contact with neighbouring rods. Any of the rods in the array may assume a non-circular shape. Models are included for primary and secondary creep, dynamic phase change and superplasticity when both alpha- and beta-phase Zircaloy are present. A simple treatment of oxidation strengthening is incorporated. Account is taken of the anisotropic creep behaviour of alpha-phase Zircaloy which leads to cladding bowing. The CANSWEL-2 model is used both as a stand-alone code and also as part of the LOCA analysis code MABEL-2. (author)

Creep Deformation and Rupture Behavior of Single- and Dual-Pass 316LN Stainless-Steel-Activated TIG Weld Joints

Science.gov (United States)

Vijayanand, V. D.; Vasudevan, M.; Ganesan, V.; Parameswaran, P.; Laha, K.; Bhaduri, A. K.

2016-06-01

Creep deformation and rupture behavior of single-pass and dual-pass 316LN stainless steel (SS) weld joints fabricated by an autogenous activated tungsten inert gas welding process have been assessed by performing metallography, hardness, and conventional and impression creep tests. The fusion zone of the single-pass joint consisted of columnar zones adjacent to base metals with a central equiaxed zone, which have been modified extensively by the thermal cycle of the second pass in the dual-pass joint. The equiaxed zone in the single-pass joint, as well as in the second pass of the dual-pass joint, displayed the lowest hardness in the joints. In the dual-pass joint, the equiaxed zone of the first pass had hardness comparable to the columnar zone. The hardness variations in the joints influenced the creep deformation. The equiaxed and columnar zone in the first pass of the dual-pass joint was more creep resistant than that of the second pass. Both joints possessed lower creep rupture life than the base metal. However, the creep rupture life of the dual-pass joint was about twofolds more than that of the single-pass joint. Creep failure in the single-pass joint occurred in the central equiaxed fusion zone, whereas creep cavitation that originated in the second pass was blocked at the weld pass interface. The additional interface and strength variation between two passes in the dual-pass joint provides more restraint to creep deformation and crack propagation in the fusion zone, resulting in an increase in the creep rupture life of the dual-pass joint over the single-pass joint. Furthermore, the differences in content, morphology, and distribution of delta ferrite in the fusion zone of the joints favors more creep cavitation resistance in the dual-pass joint over the single-pass joint with the enhancement of creep rupture life.

Influence of flowing sodium on creep deformation and rupture behaviour of 316L(N) austenitic stainless steel

Energy Technology Data Exchange (ETDEWEB)

Ravi, S., E-mail: sravi@igcar.gov.in [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Laha, K.; Mathew, M.D. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Vijayaraghavan, S.; Shanmugavel, M.; Rajan, K.K. [Fast Reactor Technology Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India); Jayakumar, T. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam 603 102 (India)

2012-08-15

The influence of flowing sodium on creep deformation and rupture behaviour of AISI 316L(N) austenitic stainless steel has been investigated at 873 K over a stress range of 235-305 MPa. The results were compared with those obtained from testing in air environment. The steady state creep rates of the material were not influenced appreciably by the testing environments. The time to onset of tertiary stage of creep deformation was delayed in sodium environment. The creep-rupture lives of the material increased in sodium environment, which became more pronounced at lower applied stresses. The increase in rupture life of the material in flowing sodium was accompanied by an increase in rupture ductility. The creep damage on specimen surface as well as inside the specimen was less in specimen tested in sodium. SEM fractographic investigation revealed predominantly transgranular dimple failure for the specimen tested in sodium, whereas predominantly intergranular creep failure was observed in the air tested specimens. Almost no oxidation was observed in the specimens creep tested in the sodium environment. Absence of oxidation and less creep damage cavitation extended the secondary state in liquid sodium tests and lead to increase in creep rupture life and ductility of the material as compared to in air.

High-Temperature Creep Behaviour and Positive Effect on Straightening Deformation of Q345c Continuous Casting Slab

Science.gov (United States)

Guo, Long; Zhang, Xingzhong

2018-03-01

Mechanical and creep properties of Q345c continuous casting slab subjected to uniaxial tensile tests at high temperature were considered in this paper. The minimum creep strain rate and creep rupture life equations whose parameters are calculated by inverse-estimation using the regression analysis were derived based on experimental data. The minimum creep strain rate under constant stress increases with the increase of the temperature from 1000 °C to 1200 °C. A new casting machine curve with the aim of fully using high-temperature creep behaviour is proposed in this paper. The basic arc segment is cancelled in the new curve so that length of the straightening area can be extended and time of creep behaviour can be increased significantly. For the new casting machine curve, the maximum straightening strain rate at the slab surface is less than the minimum creep strain rate. So slab straightening deformation based on the steel creep behaviour at high temperature can be carried out in the process of Q345c steel continuous casting. The effect of creep property at high temperature on slab straightening deformation is positive. It is helpful for the design of new casting machine and improvement of old casting machine.

Creep of Posidonia Shale at Elevated Pressure and Temperature

Science.gov (United States)

Rybacki, E.; Herrmann, J.; Wirth, R.; Dresen, G.

2017-12-01

The economic production of gas and oil from shales requires repeated hydraulic fracturing operations to stimulate these tight reservoir rocks. Besides simple depletion, the often observed decay of production rate with time may arise from creep-induced fracture closure. We examined experimentally the creep behavior of an immature carbonate-rich Posidonia shale, subjected to constant stress conditions at temperatures between 50 and 200 °C and confining pressures of 50-200 MPa, simulating elevated in situ depth conditions. Samples showed transient creep in the semibrittle regime with high deformation rates at high differential stress, high temperature and low confinement. Strain was mainly accommodated by deformation of the weak organic matter and phyllosilicates and by pore space reduction. The primary decelerating creep phase observed at relatively low stress can be described by an empirical power law relation between strain and time, where the fitted parameters vary with temperature, pressure and stress. Our results suggest that healing of hydraulic fractures at low stresses by creep-induced proppant embedment is unlikely within a creep period of several years. At higher differential stress, as may be expected in situ at contact areas due to stress concentrations, the shale showed secondary creep, followed by tertiary creep until failure. In this regime, microcrack propagation and coalescence may be assisted by stress corrosion. Secondary creep rates were also described by a power law, predicting faster fracture closure rates than for primary creep, likely contributing to production rate decline. Comparison of our data with published primary creep data on other shales suggests that the long-term creep behavior of shales can be correlated with their brittleness estimated from composition. Low creep strain is supported by a high fraction of strong minerals that can build up a load-bearing framework.

Low Temperature Creep of Hot-Extruded Near-Stoichiometric NiTi Shape Memory Alloy. Part I; Isothermal Creep

Science.gov (United States)

Raj, S. V.; Noebe, R. D.

2013-01-01

This two-part paper is the first published report on the long term, low temperature creep of hot-extruded near-stoichiometric NiTi. Constant load tensile creep tests were conducted on hot-extruded near-stoichiometric NiTi at 300, 373 and 473 K under initial applied stresses varying between 200 and 350 MPa as long as 15 months. These temperatures corresponded to the martensitic, two-phase and austenitic phase regions, respectively. Normal primary creep lasting several months was observed under all conditions indicating dislocation activity. Although steady-state creep was not observed under these conditions, the estimated creep rates varied between 10(exp -10) and 10(exp -9)/s. The creep behavior of the two phases showed significant differences. The martensitic phase exhibited a large strain on loading followed by a primary creep region accumulating a small amount of strain over a period of several months. The loading strain was attributed to the detwinning of the martensitic phase whereas the subsequent strain accumulation was attributed to dislocation glide-controlled creep. An "incubation period" was observed before the occurrence of detwinning. In contrast, the austenitic phase exhibited a relatively smaller loading strain followed by a primary creep region, where the creep strain continued to increase over several months. It is concluded that the creep of the austenitic phase occurs by a dislocation glide-controlled creep mechanism as well as by the nucleation and growth of deformation twins.

Does nanocrystalline Cu deform by Coble creep near room temperature?

International Nuclear Information System (INIS)

Li, Y.J.; Blum, W.; Breutinger, F.

2004-01-01

The proposal that nanocrystalline Cu produced by electro deposition (ED) creeps at temperatures slightly above room temperature by diffusive flow via grain boundaries (Coble creep) has been checked by compression tests. It was found that the minimum creep rates obtained in tension are significantly larger than those in compression, probably due to interference of tensile fracture. Scanning electron microscopic investigation showed that the spacing between large-angle grain boundaries is about 10 μm rather than the reported value of 30 nm. Comparison with coarse grained and ultrafine grained Cu produced by equal channel angular pressing showed that the ED-Cu work hardens similarly to coarse grained Cu in contrast to ultrafine grained Cu which reaches its maximum deformation resistance within a small strain interval of 0.04 and has distinctly higher strain rate sensitivity of flow stress. The present results are consistent with the established knowledge that there is no softening by grain boundaries, e.g. due to Coble creep, near room temperature in Cu with grain sizes above 1 μm. The grain boundary effect observed in ultrafine grained Cu is interpreted in terms of modification of dislocation generation and dislocation annihilation by grain boundaries

Reducing the moisture effect on the creep deformation of wood by an irradiation-induced polymer impregnation method

International Nuclear Information System (INIS)

Chia, L.H.L.; Boey, F.Y.C.; Teoh, S.H.

1988-01-01

This paper reports an attempt to reduce the sensitivity of creep deformation to moisture adsorption by impregnating a tropical wood with methyl-methacrylate and subsequent polymerization by γ-irradiation. Beam specimens both of untreated wood and polymer impregnated wood were subjected to a three-point bend creep test under a constant load of 300 N at 23 ± 1 0 C, at three different humidity levels of 50 ± 5, 65 ± 5 and 85 ± 5%. A Norton-Bailey (power law) mathematical model successfully described the creep behaviour, with the creep components determined by a non-linear regression analysis. A significant reduction in the sensitivity of creep deformation to the humidity level was attained for the polymer impregnated wood. This could be explained by the ability of the impregnated polymer to form a strongly adhesive interface with the wood cell material, thereby acting as a physical barrier to reduce the movement of water to and from the wood cell material. (author)

Numerical description of creep of highly creep resistant alloys

International Nuclear Information System (INIS)

Preussler, T.

1991-01-01

Fatigue tests have been performed with a series of highly creep resistant materials for gas turbines and related applications for gaining better creep data up to long-term behaviour. The investigations were performed with selected individual materials in the area of the main applications down to strains and stresses relevant to design, and have attained trial durations of 25000 to 60000 h. In continuing former research, creep equations for a selection of characterizing individual materials have been improved and partly newly developed on the basis of a differentiated evaluation. Concerning the single materials, there are: one melt each of the materials IN-738 LC, IN-939, IN-100, FSX-414 and Inconel 617. The applied differentiated evaluation is based on the elastoplastical behaviour from the hot-drawing test, the creep behaviour from the non interrupted or the interrupted fatigue test, and the contraction behaviour from the annealing test. The creep equations developed describe the high temperature deformation behaviour taking into account primary, secondary and partly the tertiary creep dependent of temperature, stress and time. These equations are valid for the whole application area of the respective material. (orig./MM) [de

Fatigue and creep-fatigue deformation of an ultra-fine precipitate strengthened advanced austenitic alloy

Energy Technology Data Exchange (ETDEWEB)

Carroll, M.C., E-mail: Mark.Carroll@INL.gov [Idaho National Laboratory, 1955 Fremont, PO Box 1625, Idaho Falls, ID 83415-2218 (United States); Carroll, L.J. [Idaho National Laboratory, 1955 Fremont, PO Box 1625, Idaho Falls, ID 83415-2218 (United States)

2012-10-30

An advanced austenitic alloy, HT-UPS (high-temperature ultrafine-precipitation-strengthened), has been identified as an ideal candidate material for the structural components of fast reactors and energy-conversion systems. HT-UPS alloys demonstrate improved creep resistance relative to 316 stainless steel (SS) through additions of Ti and Nb, which precipitate to form a widespread dispersion of stable nanoscale metallic carbide (MC) particles in the austenitic matrix. To investigate the behavior in more representative conditions than are offered by uniaxial creep tests, the low-cycle continuous fatigue and combined creep-fatigue response of an HT-UPS alloy have been investigated at 650 Degree-Sign C and 1.0% total strain, with an R-ratio of -1 and hold times at peak tensile strain of up to 150 min. The cyclic deformation response of HT-UPS is directly compared to that of standard 316 SS. The measured values for total cycles to failure between the two alloys are similar, despite differences in peak stress profiles and in qualitative observations of the deformed microstructures. Crack propagation is primarily transgranular in both fatigue and creep-fatigue of each alloy at the investigated conditions. Internal grain boundary damage in the form of fine cracks resulting from the tensile hold is present following the application of hold times of 60 min and longer, and considerably more internal cracks are quantifiable in 316 SS than in HT-UPS. The dislocation substructures observed in the deformed material differ substantially; an equiaxed cellular structure is observed in the microstructure of 316 SS, whereas HT-UPS exhibits widespread and relatively homogenous tangles of dislocations pinned by the nanoscale MC precipitates. The significant effect of the fine distribution of precipitates on observed fatigue and creep-fatigue response is described in three distinct behavioral regions as the microstructure evolves with continued cycling.

Extension of an anisotropic creep model to general high temperature deformation of a single crystal superalloy

International Nuclear Information System (INIS)

Pan, L.M.; Ghosh, R.N.; McLean, M.

1993-01-01

A physics based model has been developed that accounts for the principal features of anisotropic creep deformation of single crystal superalloys. The present paper extends this model to simulate other types of high temperature deformation under strain controlled test conditions, such as stress relaxation and tension tests at constant strain rate in single crystals subject to axial loading along an arbitrary crystal direction. The approach is applied to the SRR99 single crystal superalloy where a model parameter database is available, determined via analysis of a database of constant stress creep curves. A software package has been generated to simulate the deformation behaviour under complex stress-strain conditions taking into account anisotropic elasticity. (orig.)

Creep Deformation by Dislocation Movement in Waspaloy.

Science.gov (United States)

Whittaker, Mark; Harrison, Will; Deen, Christopher; Rae, Cathie; Williams, Steve

2017-01-12

Creep tests of the polycrystalline nickel alloy Waspaloy have been conducted at Swansea University, for varying stress conditions at 700 °C. Investigation through use of Transmission Electron Microscopy at Cambridge University has examined the dislocation networks formed under these conditions, with particular attention paid to comparing tests performed above and below the yield stress. This paper highlights how the dislocation structures vary throughout creep and proposes a dislocation mechanism theory for creep in Waspaloy. Activation energies are calculated through approaches developed in the use of the recently formulated Wilshire Equations, and are found to differ above and below the yield stress. Low activation energies are found to be related to dislocation interaction with γ' precipitates below the yield stress. However, significantly increased dislocation densities at stresses above yield cause an increase in the activation energy values as forest hardening becomes the primary mechanism controlling dislocation movement. It is proposed that the activation energy change is related to the stress increment provided by work hardening, as can be observed from Ti, Ni and steel results.

Accounting for the residual stress effects on the creep deformation of channel tubes

International Nuclear Information System (INIS)

Knizhnikov, Yu.N.; Platonov, P.A.; Ul'yanov, A.I.

1985-01-01

The effect of the first kind residual stresses arising in the walls of the zirconium base alloy fules in the process of fabrication on the RBMK type reactor channel tube creep is investigated. Models for calculation of the reactor component creep with account for the relaxation of residual stresses distributed by the wall thickness as well as the radiation and temperature fields are developed. On the basis of the analysis of the data obtained it is concluded that the effect of the residual stresses on the RBMK channel tube deformation for a long-term operation is negligible. But for the short-term fests the results can be noticeably distorted by this factor. The role of internal stresses can also manifest when determining the deformation of radiation elongation of the zirconium base alloy samples

Conception of elevated temperature structures. Creep and notion of primary stress

International Nuclear Information System (INIS)

Roche, Roland; Jakubowicz, Henri.

1978-04-01

As an introduction, it is shown that primary and secondary stresses are introduced for taking into account the stress redistribution in ductile materials. But in the creep range, materials are not always ductile and fast fracture can occurs. Besides, stress redistribution due to creep effect is different of plastic redistribution. Therefore the primary stress must be different in the creep range and correction is needed to the conventional values of primary stress. The study of a simple example (parallele bars) gives a practical expression of the correcting factor to be applied to the primary stress [fr

Evaluation of results from an in-pile creep test in the Studsvik R2 reactor

Energy Technology Data Exchange (ETDEWEB)

Pettersson, Kjell [Entropy Materials, Stockholm (Sweden)

2002-01-01

An in-pile creep test with bowing of cladding tubes has been performed in a hot water loop in the Studsvik R2 reactor . One test was performed in the core and one outside the core. The out-of-pile sample showed some minor primary creep strain while the in-pile specimen deformed at a steady rate of 5x10{sup -7}/h . However, when the results were compared to a broader data base of Zircaloy in-pile creep it became clear that the creep deformation observed is a primary creep which occurs before the irradiation creep in Zircaloy reaches a constant steady state creep rate. This primary stage is interpreted as a consequence of the development of an irradiation induced microstructure in Zircaloy which does not reach a steady state until a dose of about 10{sup 21} n/cm{sup 2} . At this stage the steady state irradiation creep starts. From this interpretation it is concluded that it is quite feasible to use the test method on pre-irradiated material in which it can be expected that the steady state will be reached already after short irradiation times.

Creep of crystals

International Nuclear Information System (INIS)

Poirier, J.-P.

1988-01-01

Creep mechanisms for metals, ceramics and rocks, effect of pressure and temperature on deformation processes are considered. The role of crystal defects is analysed, different models of creep are described. Deformation mechanisms maps for different materials are presented

Development of out-of-pile version of instrumented irradiation capsule for determination of online creep deformation

International Nuclear Information System (INIS)

Venkatesu, Sadu; Saxena, Rajesh; Chaurasia, P.K.; Muthuganesh, M.; Murugan, S.; Venugopal, S.

2016-01-01

Materials used for fuel cladding and structural components in fast reactors can undergo significant dimensional and physical changes due to exposure to high energy neutrons. At high temperatures in nuclear environment, material undergoes considerable deformation due to thermal and irradiation creep. Diametral increase of fuel pin due to thermal and irradiation creep, apart from irradiation swelling, reduces the coolant flow area around the fuel pins affecting the effective removal of heat generated in the fuel pins. The changes due to creep can be determined by two types of material irradiation tests in reactor. The first type includes non-instrumented irradiation tests with specimen dimensional evaluations carried out in post-irradiation examinations. The second type includes instrumented irradiation tests with online monitoring and/or controlling of test conditions and real time measurement of changes in dimensions of the specimen. During instrumented irradiation tests, parameters such as specimen temperature, the load exerted on the specimen, specimen elongation, etc. can be monitored and/or controlled using suitable components such as linear variable differential transformers (LVDTs), bellows, thermocouples, etc. Instrumented irradiation experiments in reactors are relatively complex in design but can provide full information on the experimental parameters. Such benefits provide motivation for development of instrumented irradiation capsule to measure creep behavior online during in-pile instrumented irradiation tests. Out-of-pile version of the instrumented irradiation capsule for determination of online creep deformation has been developed and tested in the furnace by raising the temperature gradually up to 330 °C. This paper discusses the details of the design, assembly of experimental set up and experimental results of the out-of-pile version of instrumented capsule developed in our laboratory for determination of online creep deformation. (author)

Dislocation analysis of die-cast Mg-Al-Ca alloy after creep deformation

International Nuclear Information System (INIS)

Terada, Yoshihiro; Itoh, Daigo; Sato, Tatsuo

2009-01-01

Tensile creep tests were combined with detailed transmission electron microscopy in order to characterize the dislocation movements during creep and to explain the creep properties of the Mg-Al-Ca AX52 die-cast alloy at 473 K and stresses from 15 to 70 MPa. TEM observations indicate that dislocations are generated within the primary α-Mg grain in the die-casting process, which consist of both the basal and non-basal segments. The basal segments of dislocations are able to bow out and glide on the basal planes under the influence of a stress, and the jogs follow the basal segments with the help of climb during creep. The creep mechanism for the alloy is deduced as dislocation climb due to the formation of sub-boundaries during creep, while the easy glide of the basal segments of dislocations is controlling the creep rates immediately after the stress application of creep tests.

Dislocation Structures in Creep-deformed Polycrystalline MgO

DEFF Research Database (Denmark)

Bilde-Sørensen, Jørgen

1972-01-01

dislocation segments lie in their slip or climb planes. On the basis of this structure, a model is proposed in which glide is the principal cause of deformation but the rate-limiting process, i.e. annealing of the network, is diffusion-controlled. Theoretical estimates and experimental results agree within 1...... energy of 76 ± 12 kcal/mol. The creep rate is independent of grain size. The dislocation structure was investigated by transmission electron microscopy. The total dislocation density follows the relation, σ=bG√ρ, commonly found for metals. The dislocations form a 3-dimensional network in which many...

Low temperature dissolution creep induced B-type olivine fabric during serpentinization and deformation in mantle wedge

Science.gov (United States)

Liu, W.; Zhang, J.

2017-12-01

The B-type olivine fabric (i.e., the [010]ol axes subnormal to foliation and the [001]ol axes subparallel to the lineation) has been regarded as an important olivine fabric for interpreting global trench-parallel S-wave polarization in fore-arc regions. However, strong serpentinization and cold temperature environment in the mantle wedge should inhibit development of the B-type olivine fabric that requires high temperature to activate solid-state plastic deformation. Here we report fabrics of olivine and antigorite generated at low temperatures (300-370 oC) during serpentinization in a fossil mantle wedge of the Val Malenco area, Central Alps. Olivine in the serpentine matrix develops a pronounced B-type fabric, while antigorite in the same matrix displays a strong crystallographic orientation (CPO) with the (001) and the [010] subparallel to foliation and lineation, respectively. The following evidence leads to the conclusion that the B-type olivine fabric is resulted from dissolution creep assisted by grain boundaries sliding (GBS) and grain rotation, rather than solid-state plastic deformation: (1) serpentinization took place at low temperatures and a fluid-enriched environment, ideal for dissolution-precipitation creep; (2) the voids and zigzag boundaries along the interface between antigorite and olivine suggest a fluid dissolution reaction; (3) the primary coarse olivine develops a nearly random fabric, indicating the B-type fabrics in the fine-grained olivine can't be inherited fabrics. These results document for the first time the B-type olivine CPO formed by dissolution creep at low temperatures during serpentinization and provide a mechanism to reconcile petrofabric observations with geophysical observations of trench parallel fast S-wave seismic anisotropy in fore-arc mantle wedge regions.

Creep deformation and crack growth in a low alloy steel welded pressure vessel containing defects

International Nuclear Information System (INIS)

Coleman, M.C.

1982-01-01

A full-size pressure vessel was tested for effects of welding residual stresses on creep deformation and crack growth. The vessel, based on 1/2 Cr 1/2 Mo 1/4 V main steam pipe, contained four 2CrMo manual metal arc welds, two in the as-welded condition and two stress-relieved. All the welds contained pre-existing defects machined in the heat affected zones. Testing was carried out at two internal steam pressures, 250 and 350 bar, and 565 0 C. Cracked and uncracked areas of the vessel were monitored continuously. Results are presented for the continuous creep deformation observed in both the hoop and axial directions of the welds throughout the 11,400 h of testing, as well as the intermittent strain data obtained during inspections. Crack growth observations are described based on nondestructive examination. The residual stresses measured are also given for both the as-welded and stress relieved weldments. Results obtained are discussed in terms of the effects of welding residual stress on the hoop and axial deformations observed in the welds. Similarly, the effects of residual stress on creep crack growth are considered together with compositional and microstructural implications. 9 figures, 5 tables

Finite element modelling of the creep deformation of T91 steel weldments at 600 C

Energy Technology Data Exchange (ETDEWEB)

Bhadrui, A.K. [Indira Gandhi Centre for Atomic Research, Kalpakkam (India); Gaudig, W. [Stuttgart Univ. (Germany). Staatliche Materialpruefungsanstalt; Theofel, H. [Stuttgart Univ. (Germany). Staatliche Materialpruefungsanstalt; Maile, K. [Stuttgart Univ. (Germany). Staatliche Materialpruefungsanstalt

1996-05-01

Finite element modelling of the creep deformation of T91 steel weldments, welded using the manual metal arc (MMA) and submerged arc (SA) welding processes, was carried out to predict creep curves for both of the weldments under different stresses and compared with the experimental data. The stress and strain redistribution across the length of the transverse-weld specimens has also been predicted. Data of creep tests at 600 C at stresses between 90-130 MPa for the base metal, the MMA and SA weld metals, and the simulated heat-affected zone were used to determine Garofalo`s equation for creep strain. Finite element meshes for both of the weldments were constructed after calculating the HAZ locations using Rosenthal`s heat flow equation. (orig.)

Creep deformation and rupture behavior of type 304/308 stainless steel structural weldments

International Nuclear Information System (INIS)

McAfee, W.J.; Richardson, M.; Sartory, W.K.

1977-01-01

The creep deformation and rupture of type 304/308 stainless steel structural weldments at 593 0 C (1100 0 F) was experimentally investigated to study the comparative behavior of the base metal and weld metal constituents. The tests were conducted in support of ORNL's program to develop high-temperature structural design methods applicable to liquid-metal fast breeder reactor (LMFBR) system components that operate in the creep range. The specimens used were thin-walled, right circular cylinders capped with either flat or hemispherical heads and tested under internal gas pressure. Circumferential welds were located in different regions of the cylinder or head and, with one exception, were geometrically duplicated by all base metal regions in companion specimens. Results are presented on the comparative deformation and rupture behavior of selected points in the base metal and weldment regions of the different specimens and on the overall surface strains for selected specimens

Creep deformation and rupture behavior of CLAM steel at 823 K and 873 K

Science.gov (United States)

Zhong, Boyu; Huang, Bo; Li, Chunjing; Liu, Shaojun; Xu, Gang; Zhao, Yanyun; Huang, Qunying

2014-12-01

China Low Activation Martensitic (CLAM) steel is selected as the candidate structural material in Fusion Design Study (FDS) series fusion reactor conceptual designs. The creep property of CLAM steel has been studied in this paper. Creep tests have been carried out at 823 K and 873 K over a stress range of 150-230 MPa. The creep curves showed three creep regimes, primary creep, steady-state creep and tertiary creep. The relationship between minimum creep rate (ε˙min) and the applied stress (σ) could be described by Norton power law, and the stress exponent n was decreased with the increase of the creep temperature. The creep mechanism was analyzed with the fractographes of the rupture specimens which were examined by scanning electron microscopy (SEM). The coarsening of precipitates observed with transmission electron microscope (TEM) indicated the microstructural degradation after creep test.

Creep deformation and rupture behavior of CLAM steel at 823 K and 873 K

International Nuclear Information System (INIS)

Zhong, Boyu; Huang, Bo; Li, Chunjing; Liu, Shaojun; Xu, Gang; Zhao, Yanyun; Huang, Qunying

2014-01-01

China Low Activation Martensitic (CLAM) steel is selected as the candidate structural material in Fusion Design Study (FDS) series fusion reactor conceptual designs. The creep property of CLAM steel has been studied in this paper. Creep tests have been carried out at 823 K and 873 K over a stress range of 150–230 MPa. The creep curves showed three creep regimes, primary creep, steady-state creep and tertiary creep. The relationship between minimum creep rate (ε-dot min ) and the applied stress (σ) could be described by Norton power law, and the stress exponent n was decreased with the increase of the creep temperature. The creep mechanism was analyzed with the fractographes of the rupture specimens which were examined by scanning electron microscopy (SEM). The coarsening of precipitates observed with transmission electron microscope (TEM) indicated the microstructural degradation after creep test

Nano-scale simulation based study of creep behavior of bimodal nanocrystalline face centered cubic metal.

Science.gov (United States)

Meraj, Md; Pal, Snehanshu

2017-10-11

In this paper, the creep behavior of nanocrystalline Ni having bimodal grain structure is investigated using molecular dynamics simulation. Analysis of structural evolution during the creep process has also been performed. It is observed that an increase in size of coarse grain causes improvement in creep properties of bimodal nanocrystalline Ni. Influence of bimodality (i.e., size difference between coarse and fine grains) on creep properties are found to be reduced with increasing creep temperature. The dislocation density is observed to decrease exponentially with progress of creep deformation. Grain boundary diffusion controlled creep mechanism is found to be dominant at the primary creep region and the initial part of the secondary creep region. After that shear diffusion transformation mechanism is found to be significantly responsible for deformation as bimodal nanocrystalline Ni transforms to amorphous structure with further progress of the creep process. The presence of , , and  distorted icosahedra has a significant influence on creep rate in the tertiary creep regime according to Voronoi cluster analysis.

Creep recovery behaviour of bituminous binders - relevance to permanent deformation of asphalt pavements

CSIR Research Space (South Africa)

Mturi, GAJ

2012-05-01

Full Text Available different modifiers has expanded the range of PMBs to select from when designing pavements in order to avoid pavement deformation. The new binder selection criterion using the Multiple Stress Creep and Recovery (MSCR) protocol as per ASTM D7405 is meant...

Material Parameters for Creep Rupture of Austenitic Stainless Steel Foils

Science.gov (United States)

Osman, H.; Borhana, A.; Tamin, M. N.

2014-08-01

Creep rupture properties of austenitic stainless steel foil, 347SS, used in compact recuperators have been evaluated at 700 °C in the stress range of 54-221 MPa to establish the baseline behavior for its extended use. Creep curves of the foil show that the primary creep stage is brief and creep life is dominated by tertiary creep deformation with rupture lives in the range of 10-2000 h. Results are compared with properties of bulk specimens tested at 98 and 162 MPa. Thin foil 347SS specimens were found to have higher creep rates and higher rupture ductility than their bulk specimen counterparts. Power law relationship was obtained between the minimum creep rate and the applied stress with stress exponent value, n = 5.7. The value of the stress exponent is indicative of the rate-controlling deformation mechanism associated with dislocation creep. Nucleation of voids mainly occurred at second-phase particles (chromium-rich M23C6 carbides) that are present in the metal matrix by decohesion of the particle-matrix interface. The improvement in strength is attributed to the precipitation of fine niobium carbides in the matrix that act as obstacles to the movement of dislocations.

Creep deformation, creep damage accumulation and residual life prediction for three low alloyed CrMo-steels

International Nuclear Information System (INIS)

Kondyr, A.; Sandstroem, R.; Samuelsson, A.

1979-02-01

A detailed analysis of creep strain results for three low alloyed steels of type 0.5 Mo, 1 Cr-0.5 Mo and 2.25 Cr-1 Mo has been undertaken. The results show that, excluding the primary stage, the true strain rate can be described by a simple analytical expression dE/dt = Aexp(B.E) where A and B are constants at constant stress and temperature. A is approximately equal to the minimum strain rate and B inversly proportional to the fracture strain. Furthermore, 1/AB equals the time t sub(r) to rupture. The residual life fraction in creep can be expressed as exp(-B.E) = 1-t/t sub(r) and a creep damage function μ is introduced as μ = 1-ABt. The expressions for strain rate and damage are shown to be a special case of the Rabotnov-Kachanov equations. The analysis has been generalized to account for multiaxial stress states, and as an example creep in a tube with internal pressure is considered. (author)

Biaxial creep deformation of Zircaloy-4 PWR fuel cladding in the alpha,(alpha + beta) and beta phase temperature ranges

International Nuclear Information System (INIS)

Donaldson, A.T.; Healey, T.; Horwood, R.A.L.

1985-01-01

The biaxial creep behaviour of Zircaloy-4 fuel cladding has been determined at temperatures between 973 - 1073 K in the alpha phase range, in the duplex (alpha + beta) region between 1098 - 1223 K and in the beta phase range between 1323 - 1473 K. This paper presents the creep data together with empirical equations which describe the creep deformation response within each phase region. (author)

B-type olivine fabric induced by low temperature dissolution creep during serpentinization and deformation in mantle wedge

Science.gov (United States)

Liu, Wenlong; Zhang, Junfeng; Barou, Fabrice

2018-01-01

The B-type olivine fabric (i.e., the [010] axes subnormal to foliation and the [001] axes subparallel to the lineation) has been regarded as an important olivine fabric for interpreting global trench-parallel S-wave polarization in fore-arc regions. However, strong serpentinization and cold temperature environment in the mantle wedge should inhibit development of the B-type olivine fabric that requires high temperature to activate solid-state plastic deformation. Here we report fabrics of olivine and antigorite generated at low temperatures (300-370 °C) during serpentinization in a fossil mantle wedge of the Val Malenco area, Central Alps. Olivine in the serpentine matrix develops a pronounced B-type fabric, while antigorite in the same matrix displays a strong crystallographic preferred orientation (CPO) with the (001) planes and the [010] axes subparallel to foliation and lineation, respectively. The following evidence leads to the conclusion that the B-type olivine fabric results from dissolution creep assisted by grain boundary sliding (GBS) and grain rotation, rather than solid-state plastic deformation: (1) serpentinization took place at low temperatures and a fluid-enriched environment, ideal for dissolution-precipitation creep; (2) the voids and zigzag boundaries along the interface between antigorite and olivine suggest a fluid dissolution reaction; (3) the primary coarse olivine develops a nearly random fabric, indicating the B-type fabrics in the fine-grained olivine may not be inherited fabrics. These results document for the first time the B-type olivine CPO formed by dissolution creep at low temperatures during serpentinization and provide a mechanism to reconcile petrofabric observations with geophysical observations of trench parallel fast S-wave seismic anisotropy in fore-arc mantle wedge regions.

Phenomenological study of the microdeformations produced at the beginning of primary creep under low stresses in an austenitic stainless steel of Z3CND 18-13 type

International Nuclear Information System (INIS)

Calvet, J.-N.; Le Bret, P.; Roulliay, R.

1975-01-01

A creep machine was modified enabling tests to be carried out at 550 deg C under 8hbar. The modulus of elasticity, yield strength, plastic deformation on loading, creep deformation and total plastic deformation were determined in an austenitic stainless steel of Z3CND 18-13 type. A relationship was established between the plastic deformation on loading and the creep deformation [fr

Thermal ratcheting and creep damage

International Nuclear Information System (INIS)

Clement, G.; Cousseran, P.; Roche, R.L.

1983-08-01

Creep is a cause of deformation; it may also result in rupture in time. Although LMFBR structures are not heavily loaded, they are subjected to large thermal transients. Can structure lifetime be shortened by such transients. Several proposals have been made to assist adesigners with thermal ratcheting in the creep range. Unfortunately these methods are not validated by experiments, and they take only inelastic distorsion into consideration as creep effects. The aim of the work presented here is to correct these deficiencies in providing an experimental basis to ratcheting analysis rules in the creep range, and in considering the effect of cyclic straining (like cyclic thermal stresses) on the time to rupture by creep. Experimental tests have been performed on austenitic stainless steel at 650 0 C for the first item. Results of these tests and results available in the open literature have been used to built a practical rule of ratcheting analysis. This rule giving a conservative value of the creep distortion, is based on the concept of effective primary stress which is an amplification of the primary stress really applied. Concerning the second point (time to rupture), it was necessary to obtain real creep rupture and not instability. According to the proposal of Pr LECKIE, tests were performed on specimen made out of copper, and of aluminium alloys at temperatures between 150 0 C and 300 0 C. With such materials creep rupture is obtained without necking. Experimental tests show that cyclic straining reduces the time to creep rupture under load controlled stress. Caution must be given to the designer: cyclic thermal stress can lead to premature creep rupture

Implications of Microstructural Studies of the SAFOD Gouge for the Strength and Deformation Mechanisms in the Creeping Segment of the San Andreas Fault

Science.gov (United States)

Hadizadeh, J.; Gratier, J. L.; Mittempergher, S.; Renard, F.; Richard, J.; di Toro, G.; Babaie, H. A.

2010-12-01

The San Andreas Fault zone (SAF) in the vicinity of the San Andreas Fault Observatory at Depth (SAFOD)in central California is characterized by an average 21 mm/year aseismic creep and strain release through repeating Mmicroscopy, cathodoluminescence imaging, X-ray fluorescence mapping, and energy dispersive X-ray spectroscopy. The microstructural and analytical data suggest that deformation is by a coupling of cataclastic flow and pressure solution accompanied by widespread alteration of feldspar to clay minerals and other neomineralizations. The clay contents of the gouge and streaks of serpentinite are not uniformly distributed, but weakness of the creeping segment is likely to be due to intrinsically low frictional strength of the fault material. This conclusion, which is based on the overall ratio of clay/non-clay constituents and the presence of talc in the actively deforming zones, is consistent with the 0.3-0.45 coefficient of friction for the drill cuttings tested by others. We also considered weakening by diffusion-accommodated grain boundary sliding. There are two main trends in the microstructural data that provide a basis for explaining the creep rate and seismic activity: 1. Clay content of the gouge including serpentinite and talc increases toward the 1-3m wide borehole casing deformation zones, which are expected to be deforming at above the average creep rate 2. Evidence of pressure solution creep and fracture sealing is more abundant in the siltstone cataclasites than in the shale. Such rocks could act as rigid inclusions that are repeatedly loaded to seismic failure by creep of the surrounding clay gouge. Regular cycles of fracture and restrengthening by fracture sealing in and around the inclusions are thus expected. The inclusions may be viewed as asperity patches (or cluster of patches) that predominantly deform by pressure solution at below the average creep rate.

Effects of segregation of primary alloying elements on the creep response in magnesium alloys

DEFF Research Database (Denmark)

Huang, Y.D.; Dieringa, H.; Hort, N.

2008-01-01

The segregation of primary alloying elements deteriorates the high temperature creep resistance of magnesium alloys. Annealing at high temperatures alleviating their segregations can improve the creep resistance. Present investigation on the effect of segregation of primary alloying elements...... on the creep response may provide some useful information about how to improve the creep resistance of magnesium alloys in the future. (c) 2008 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved....

Creep buckling of shell structures

International Nuclear Information System (INIS)

Miyazaki, Noriyuki; Hagihara, Seiya

2015-01-01

The present article contains a review of the literatures on the creep buckling of shell structures published from late 1950's to recent years. In this article, the creep buckling studies on circular cylindrical shells, spherical shells, partial cylindrical shells and other shells are reviewed in addition to creep buckling criteria. Creep buckling is categorized into two types. One is the creep buckling due to quasi-static instability, in which the critical time for creep buckling is determined by tracing a creep deformation versus time curve. The other is the creep buckling due to kinetic instability, in which the critical time can be determined by examining the shape of total potential energy in the vicinity of a quasi-static equilibrium state. Bifurcation buckling and snap-through buckling during creep deformation belong to this type of creep buckling. A few detailed descriptions are given to the bifurcation and snap-through type of creep buckling based on the present authors' works. (author)

In-situ Creep Testing Capability Development for Advanced Test Reactor

Energy Technology Data Exchange (ETDEWEB)

B. G. Kim; J. L. Rempe; D. L. Knudson; K. G. Condie; B. H. Sencer

2010-08-01

Creep is the slow, time-dependent strain that occurs in a material under a constant strees (or load) at high temperature. High temperature is a relative term, dependent on the materials being evaluated. A typical creep curve is shown in Figure 1-1. In a creep test, a constant load is applied to a tensile specimen maintained at a constant temperature. Strain is then measured over a period of time. The slope of the curve, identified in the figure below, is the strain rate of the test during Stage II or the creep rate of the material. Primary creep, Stage I, is a period of decreasing creep rate due to work hardening of the material. Primary creep is a period of primarily transient creep. During this period, deformation takes place and the resistance to creep increases until Stage II, Secondary creep. Stage II creep is a period with a roughly constant creep rate. Stage II is referred to as steady-state creep because a balance is achieved between the work hardening and annealing (thermal softening) processes. Tertiary creep, Stage III, occurs when there is a reduction in cross sectional area due to necking or effective reduction in area due to internal void formation; that is, the creep rate increases due to necking of the specimen and the associated increase in local stress.

CHOICE THEORY OF CREEP DEFORMATION FOR EVALUATION OF LONG FINE-GRAINED AUTOCLAVED AERATED CONCRETE IN VIEW OF FACTORS CARBONIZATION

Directory of Open Access Journals (Sweden)

D. K-S. Bataev

2015-01-01

Full Text Available Experimental data on the effect of the age of autoclaved aerated concrete with and without carbonation factor to change its physical and mechanical characteristics, as well as by the amount of creep deformation and degree of reversibility. It was found that the solution of applied problems creep theory for structures of autoclaved aerated concrete, in accordance with their carbonation from the effects of atmospheric carbon dioxide, it is necessary to use the theory of elastic-creeping body on the basis of function creep measures in the form proposed by prof. S.V. Alexandrovsky. 

Analyses of Small Punch Creep Deformation Behavior of 316LN Stainless Steel Having Different Nitrogen Contents

Science.gov (United States)

Ganesh Kumar, J.; Laha, K.; Ganesan, V.; Prasad Reddy, G. V.

2018-04-01

The small punch creep (SPC) behavior of 316LN stainless steel (SS) containing 0.07, 0.11 and 0.14 wt.% nitrogen has been investigated at 923 K. The transient and tertiary SPC deformation of 316LN SS with various nitrogen contents have been analyzed according to the equation proposed for SPC deflection, δ = δ0 + δT (1 - e^{ - κ t} ) + \\dot{δ }s t + δ3 e^[ φ( t - tr ) ]. The relationships among the rate of exhaustion of transient creep (κ), steady-state deflection rate (\\dot{δ }s ) and the rate of acceleration of tertiary creep (φ) revealed the interrelationships among the three stages of SPC curve. The first-order reaction rate theory was found to be applicable to SPC deformation throughout the transient as well as tertiary region, in all the investigated steels. The initial and final creep deflection rates were decreased, whereas time to attain steady-state deflection rate increased with the increase in nitrogen content. By increasing the nitrogen content in 316LN SS from 0.07 to 0.14 wt.%, each stage of SPC was prolonged, and consequently, the values of κ, \\dot{δ }s and φ were lowered. Using the above parameters, the master curves for both transient and tertiary SPC deflections were constructed for 316LN SS containing different nitrogen contents.

An axisymmetric method of creep analysis for primary and secondary creep

International Nuclear Information System (INIS)

Jahed, Hamid; Bidabadi, Jalal

2003-01-01

A general axisymmetric method for elastic-plastic analysis was previously proposed by Jahed and Dubey [ASME J Pressure Vessels Technol 119 (1997) 264]. In the present work the method is extended to the time domain. General rate type governing equations are derived and solved in terms of rate of change of displacement as a function of rate of change in loading. Different types of loading, such as internal and external pressure, centrifugal loading and temperature gradient, are considered. To derive specific equations and employ the proposed formulation, the problem of an inhomogeneous non-uniform rotating disc is worked out. Primary and secondary creep behaviour is predicted using the proposed method and results are compared to FEM results. The problem of creep in pressurized vessels is also solved. Several numerical examples show the effectiveness and robustness of the proposed method

Effects of stacking fault energy on the creep behaviors of Ni-base superalloy

International Nuclear Information System (INIS)

Tian, Chenggang; Han, Guoming; Cui, Chuanyong; Sun, Xiaofeng

2014-01-01

Highlights: • The decrease of SFE could promote the dislocation dissociation. • The creep mechanisms were significantly affected by the SFE of the alloys. • The creep properties of the alloys improved with the decrease of SFE by facilitating the microtwinning process. - Abstract: Cobalt in a 23 wt.% Co containing Ni-base superalloys was systematically substituted by Ni in order to study the effects of stacking fault energy (SFE) on the creep mechanisms. The deformation microstructures of the alloys during different creep stages at 725 °C and 630 MPa were investigated by transmission electron microscopy (TEM). The results showed that the creep life increased as the SFE decreased corresponding to the increase of Co content in the alloys. At primary creep stage, the dislocation was difficult to dissociate independent of SFE. In contrast, at secondary and tertiary creep stages the dislocations dissociated at γ/γ′ interface and the partial dislocation started to shear γ′ precipitates, leaving isolated faults (IFs) in high SFE alloy, while the dislocations dissociated in the matrix and the partials swept out the matrix and γ′ precipitates creating extended stacking faults (ESFs) or deformation microtwins which were involved in diffusion-mediated reordering in low SFE alloy. It is suggested that the deformation microtwinning process should be favorable with the decrease of SFE, which could enhance the creep resistance and improve the creep properties of the alloys

Room temperature creep behavior of Ti–Nb–Ta–Zr–O alloy

Energy Technology Data Exchange (ETDEWEB)

Zhang, Wei-dong [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan 410083 (China); Liu, Yong, E-mail: yonliu@csu.edu.cn [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan 410083 (China); Wu, Hong; Lan, Xiao-dong [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan 410083 (China); Qiu, Jingwen [College of Electrical and Mechanical Engineering, Hunan University of Science and Technology, Xiangtan, Hunan 411201 (China); Hu, Te [State Key Laboratory of Powder Metallurgy, Central South University, Changsha, Hunan 410083 (China); Tang, Hui-ping [State Key Laboratory of Porous Metal Materials, Northwestern Institute of Nonferrous Metal Research, Xi' an, Shaanxi 710012 (China)

2016-08-15

The room temperature creep behavior and deformation mechanisms of a Ti–Nb–Ta–Zr–O alloy, which is also called “gum metal”, were investigated with the nanoindentation creep and conventional creep tests. The microstructure was observed with electron backscattered diffraction analysis (EBSD) and transmission electron microscopy (TEM). The results show that the creep stress exponent of the alloy is sensitive to cold deformation history of the alloy. The alloy which was cold swaged by 85% shows high creep resistance and the stress exponent is approximately equal to 1. Microstructural observation shows that creep process of the alloy without cold deformation is controlled by dislocation mechanism. The stress-induced α' martensitic phase transformation also occurs. The EBSD results show that the grain orientation changes after the creep tests, and thus, the creep of the cold-worked alloy is dominated by the shear deformation of giant faults without direct assistance from dislocations. - Highlights: •Nanoindentation was used to investigate room temperature creep behavior of gum metal. •The creep stress exponent of gum metal is sensitive to the cold deformation history. •The creep stress exponent of cold worked gum metal is approximately equal to 1. •The creep of the cold-worked gum metal is governed by the shear deformation of giant faults.

Unified creep-plasticity model for halite

International Nuclear Information System (INIS)

Krieg, R.D.

1980-11-01

There are two national energy programs which are considering caverns in geological salt (NaCl) as a storage repository. One is the disposal of nuclear wastes and the other is the storage of oil. Both short-time and long-time structural deformations and stresses must be predictable for these applications. At 300K, the nominal initial temperature for both applications, the salt is at 0.28 of the melting temperature and exhibits a significant time dependent behavior. A constitutive model has been developed which describes the behavior observed in an extensive set of triaxial creep tests. Analysis of these tests showed that a single deformation mechanism seems to be operative over the stress and temperature range of interest so that the secondary creep data can be represented by a power of the stress over the entire test range. This simple behavior allowed a new unified creep-plasticity model to be applied with some confidence. The resulting model recognizes no inherent difference between plastic and creep strains yet models the total inelastic strain reasonably well including primary and secondary creep and reverse loadings. A multiaxial formulation is applied with a back stress. A Bauschinger effect is exhibited as a consequence and is present regardless of the time scale over which the loading is applied. The model would be interpreted as kinematic hardening in the sense of classical plasticity. Comparisons are made between test data and model behavior

The influence of grain boundary structure on diffusional creep

DEFF Research Database (Denmark)

Thorsen, Peter Anker; Bilde-Sørensen, Jørgen

1999-01-01

the deformation caused by deposition of material at (or removal of material from) grain boundaries. The misorientation across the grain boundaries, and hence the character of the boundaries, was measured with the use of electron back-scattering patterns. The deformation behavior of the individual boundaries......A Cu-2wt%Ni-alloy was deformed in tension in the diffusional creep regime (Nabarro-Herring creep). A periodic grid consisting of alumina was deposited on the surface of the creep specimen prior to creep. This makes it possible to separate the deformation caused by grain boundary sliding from...

Effect of step-wise change of stress and temperature on primary creep of concrete

International Nuclear Information System (INIS)

Furumura, Fukujiro; Abe, Takeo; Shinohara, Yasuji; Kim, Wha-Jung.

1991-01-01

The success of analyzing the behavior of concrete structures at elevated temperature greatly depends on how accurately certain mechanical properties, especially stress-strain curves, creep and thermal expansion, can be determined within wide temperature range. The importance of creep in the design of reinforced and prestressed concrete structures has been more recognized with the advent of the use of concrete at elevated temperature. The creep strain of concrete is affected by stress, time and temperature. The creep law which can predict the creep behavior under varying stress and temperature by using the experimental results of creep strain under constant stress and temperature is indispensable for analyzing the behavior of reinforced concrete structures under varying temperature. Accordingly the main purpose of this study is to clarify the primary creep behavior of concrete under varying stress and temperature. The cylindrical specimens, the testing procedure, the test results and the modified strain hardening law are reported. By using the modified strain hardening law, the primary creep behavior of concrete can be estimated better. (K.I.)

Creep of high temperature composites

International Nuclear Information System (INIS)

Sadananda, K.; Feng, C.R.

1993-01-01

High temperature creep deformation of composites is examined. Creep of composites depends on the interplay of many factors. One of the basic issues in the design of the creep resistant composites is the ability to predict their creep behavior from the knowledge of the creep behavior of the individual components. In this report, the existing theoretical models based on continuum mechanics principles are reviewed. These models are evaluated using extensive experimental data on molydisilicide-silicon carbide composites obtained by the authors. The analysis shows that the rule of mixture based on isostrain and isostress provides two limiting bounds wherein all other theoretical predictions fall. For molydisilicide composites, the creep is predominantly governed by the creep of the majority phase, i.e. the matrix with fibers deforming elastically. The role of back stresses both on creep rates and activation energies are shown to be minimum. Kinetics of creep in MoSi 2 is shown to be controlled by the process of dislocation glide with climb involving the diffusion of Mo atoms

Understanding creep in sandstone reservoirs - theoretical deformation mechanism maps for pressure solution in granular materials

Science.gov (United States)

Hangx, Suzanne; Spiers, Christopher

2014-05-01

Subsurface exploitation of the Earth's natural resources removes the natural system from its chemical and physical equilibrium. As such, groundwater extraction and hydrocarbon production from subsurface reservoirs frequently causes surface subsidence and induces (micro)seismicity. These effects are not only a problem in onshore (e.g. Groningen, the Netherlands) and offshore hydrocarbon fields (e.g. Ekofisk, Norway), but also in urban areas with extensive groundwater pumping (e.g. Venice, Italy). It is known that fluid extraction inevitably leads to (poro)elastic compaction of reservoirs, hence subsidence and occasional fault reactivation, and causes significant technical, economic and ecological impact. However, such effects often exceed what is expected from purely elastic reservoir behaviour and may continue long after exploitation has ceased. This is most likely due to time-dependent compaction, or 'creep deformation', of such reservoirs, driven by the reduction in pore fluid pressure compared with the rock overburden. Given the societal and ecological impact of surface subsidence, as well as the current interest in developing geothermal energy and unconventional gas resources in densely populated areas, there is much need for obtaining better quantitative understanding of creep in sediments to improve the predictability of the impact of geo-energy and groundwater production. The key problem in developing a reliable, quantitative description of the creep behaviour of sediments, such as sands and sandstones, is that the operative deformation mechanisms are poorly known and poorly quantified. While grain-scale brittle fracturing plus intergranular sliding play an important role in the early stages of compaction, these time-independent, brittle-frictional processes give way to compaction creep on longer time-scales. Thermally-activated mass transfer processes, like pressure solution, can cause creep via dissolution of material at stressed grain contacts, grain

Effect of titanium on the creep deformation behaviour of 14Cr-15Ni-Ti stainless steel

Science.gov (United States)

Latha, S.; Mathew, M. D.; Parameswaran, P.; Nandagopal, M.; Mannan, S. L.

2011-02-01

14Cr-15Ni-Ti modified stainless steel alloyed with additions of phosphorus and silicon is a potential candidate material for the future cores of Prototype Fast Breeder Reactor. In order to optimise the titanium content in this steel, creep tests have been conducted on the heats with different titanium contents of 0.18, 0.23, 0.25 and 0.36 wt.% at 973 K at various stress levels. The stress exponents indicated that the rate controlling deformation mechanism was dislocation creep. A peak in the variation of rupture life with titanium content was observed around 0.23 wt.% titanium and the peak was more pronounced at lower stresses. The variation in creep strength with titanium content was correlated with transmission electron microscopic investigations. The peak in creep strength exhibited by the material with 0.23 wt.% titanium is attributed to the higher volume fraction of fine secondary titanium carbide (TiC) precipitates.

Effect of titanium on the creep deformation behaviour of 14Cr-15Ni-Ti stainless steel

Energy Technology Data Exchange (ETDEWEB)

Latha, S. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, Tamil Nadu 603 102 (India); Mathew, M.D., E-mail: mathew@igcar.gov.in [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, Tamil Nadu 603 102 (India); Parameswaran, P.; Nandagopal, M. [Metallurgy and Materials Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, Tamil Nadu 603 102 (India); Mannan, S.L. [National Engineering College, Kovilpatti, Tamil Nadu 628 503 (India)

2011-02-28

14Cr-15Ni-Ti modified stainless steel alloyed with additions of phosphorus and silicon is a potential candidate material for the future cores of Prototype Fast Breeder Reactor. In order to optimise the titanium content in this steel, creep tests have been conducted on the heats with different titanium contents of 0.18, 0.23, 0.25 and 0.36 wt.% at 973 K at various stress levels. The stress exponents indicated that the rate controlling deformation mechanism was dislocation creep. A peak in the variation of rupture life with titanium content was observed around 0.23 wt.% titanium and the peak was more pronounced at lower stresses. The variation in creep strength with titanium content was correlated with transmission electron microscopic investigations. The peak in creep strength exhibited by the material with 0.23 wt.% titanium is attributed to the higher volume fraction of fine secondary titanium carbide (TiC) precipitates.

Effect of titanium on the creep deformation behaviour of 14Cr-15Ni-Ti stainless steel

International Nuclear Information System (INIS)

Latha, S.; Mathew, M.D.; Parameswaran, P.; Nandagopal, M.; Mannan, S.L.

2011-01-01

14Cr-15Ni-Ti modified stainless steel alloyed with additions of phosphorus and silicon is a potential candidate material for the future cores of Prototype Fast Breeder Reactor. In order to optimise the titanium content in this steel, creep tests have been conducted on the heats with different titanium contents of 0.18, 0.23, 0.25 and 0.36 wt.% at 973 K at various stress levels. The stress exponents indicated that the rate controlling deformation mechanism was dislocation creep. A peak in the variation of rupture life with titanium content was observed around 0.23 wt.% titanium and the peak was more pronounced at lower stresses. The variation in creep strength with titanium content was correlated with transmission electron microscopic investigations. The peak in creep strength exhibited by the material with 0.23 wt.% titanium is attributed to the higher volume fraction of fine secondary titanium carbide (TiC) precipitates.

Development of a constitutive model for the plastic deformation and creep of copper and its use in the estimate of the creep life of the copper canister

International Nuclear Information System (INIS)

Pettersson, Kjell

2006-12-01

A previously developed model for the plastic deformation and creep of copper (included as an Appendix to the present report) has been used as the basis for a discussion on the possibility of brittle creep fracture of the copper canister during long term storage of nuclear waste. Reported creep tests on oxygen free (OF) copper have demonstrated that copper can have an extremely low creep ductility. However with the addition of about 50 ppm phosphorus to the copper it appears as if the creep brittleness problem is avoided and that type of copper (OFP) has consequently been chosen as the canister material. It is shown in the report that the experiments performed on OFP copper does not exclude the possibility of creep brittleness of OFP copper in the very long term. The plasticity and creep model has been used to estimate creep life under conditions of intergranular creep cracking according to a model formulated by Cocks and Ashby. The estimated life times widely exceed the design life of the canister. However the observations of creep brittleness in OF copper indicate that the Cocks-Ashby model probably does not apply to the OF copper. Thus additional calculations have been done with the plasticity and creep model in order to estimate stress as a function of time for the probably most severe loading case of the canister with regard to creep failure, an earth quake shear. Despite the fact that the stress in the canister will remain at the 100 MPa level for thousands of years after an earth quake the low temperature, about 50 deg C or less, will make the solid state diffusion process assumed to control the brittle cracking process, too slow to lead to any significant brittle creep cracking in the canister

Metallurgical principles of creep processes

International Nuclear Information System (INIS)

Bolton, C.J.

1977-12-01

A brief review is presented of current theories of a number of the physical processes which can be involved in deformation and fracture under creep conditions. The processes considered are power law creep, diffusion creep, grain boundary sliding, cavitation and other modes of failure, and creep crack growth. The note concludes with some suggestions for future work. (author)

Analysis of local microstructure after shear creep deformation of a fine-grained duplex {gamma}-TiAl alloy

Energy Technology Data Exchange (ETDEWEB)

Peter, D., E-mail: dennis.peter@rub.de [Institute for Materials, Ruhr University Bochum, Universitaetsstrasse 150, 44801 Bochum (Germany); Viswanathan, G.B. [Institute for Materials, Ruhr University Bochum, Universitaetsstrasse 150, 44801 Bochum (Germany)] [Air Force Research Laboratory, Wright-Patterson AFB, OH 45433 (United States); Dlouhy, A. [Institute of Physics of Materials, Academy of Sciences of the Czech Republic, 61662 Brno, Zizkova 22 (Czech Republic); Eggeler, G. [Institute for Materials, Ruhr University Bochum, Universitaetsstrasse 150, 44801 Bochum (Germany)

2010-11-15

The present work characterizes the microstructure of a hot-extruded Ti-45Al-5Nb-0.2B-0.2C (at.%) alloy with a fine-grained duplex microstructure after shear creep deformation (temperature 1023 K; shear stress 175 MPa; shear deformation 20%). Diffraction contrast transmission electron microscopy (TEM) was performed to identify ordinary dislocations, superdislocations and twins. The microstructure observed in TEM is interpreted taking into account the contribution of the applied stress and coherency stresses to the overall local stress state. Two specific locations in the lamellar part of the microstructure were analyzed, where either twins or superdislocations provided c-component deformation in the L1{sub 0} lattice of the {gamma} phase. Lamellar {gamma} grains can be in soft and hard orientations with respect to the resolved shear stress provided by the external load. The presence of twins can be rationalized by the superposition of the applied stress and local coherency stresses. The presence of superdislocations in hard {gamma} grains represents indirect evidence for additional contributions to the local stress state associated with stress redistribution during creep.

A novel deformation mechanism for superplastic deformation

Energy Technology Data Exchange (ETDEWEB)

Muto, H.; Sakai, M. (Toyohashi Univ. of Technology (Japan). Dept. of Materials Science)

1999-01-01

Uniaxial compressive creep tests with strain value up to -0.1 for a [beta]-spodumene glass ceramic are conducted at 1060 C. From the observation of microstructural changes between before and after the creep deformations, it is shown that the grain-boundary sliding takes place via cooperative movement of groups of grains rather than individual grains under the large-scale-deformation. The deformation process and the surface technique used in this work are not only applicable to explain the deformation and flow of two-phase ceramics but also the superplastic deformation. (orig.) 12 refs.

Creep of trabecular bone from the human proximal tibia

Energy Technology Data Exchange (ETDEWEB)

Novitskaya, Ekaterina, E-mail: eevdokim@ucsd.edu [Mechanical and Aerospace Engineering, UC, San Diego, La Jolla, CA 92093 (United States); Materials Science and Engineering Program, UC, San Diego, La Jolla, CA 92093 (United States); Zin, Carolyn [Materials Science and Engineering, Johns Hopkins University, Baltimore, MD 21218 (United States); Chang, Neil; Cory, Esther; Chen, Peter [Departments of Bioengineering and Orthopaedic Surgery, UC, San Diego, La Jolla, CA 92093 (United States); D’Lima, Darryl [Shiley Center for Orthopaedic Research and Education, Scripps Health, La Jolla, CA 92037 (United States); Sah, Robert L. [Materials Science and Engineering Program, UC, San Diego, La Jolla, CA 92093 (United States); Departments of Bioengineering and Orthopaedic Surgery, UC, San Diego, La Jolla, CA 92093 (United States); McKittrick, Joanna [Mechanical and Aerospace Engineering, UC, San Diego, La Jolla, CA 92093 (United States); Materials Science and Engineering Program, UC, San Diego, La Jolla, CA 92093 (United States)

2014-07-01

Creep is the deformation that occurs under a prolonged, sustained load and can lead to permanent damage in bone. Creep in bone is a complex phenomenon and varies with type of loading and local mechanical properties. Human trabecular bone samples from proximal tibia were harvested from a 71-year old female cadaver with osteoporosis. The samples were initially subjected to one cycle load up to 1% strain to determine the creep load. Samples were then loaded in compression under a constant stress for 2 h and immediately unloaded. All tests were conducted with the specimens soaked in phosphate buffered saline with proteinase inhibitors at 37 °C. Steady state creep rate and final creep strain were estimated from mechanical testing and compared with published data. The steady state creep rate correlated well with values obtained from bovine tibial and human vertebral trabecular bone, and was higher for lower density samples. Tissue architecture was analyzed by micro-computed tomography (μCT) both before and after creep testing to assess creep deformation and damage accumulated. Quantitative morphometric analysis indicated that creep induced changes in trabecular separation and the structural model index. A main mode of deformation was bending of trabeculae. - Highlights: • Compressive creep tests of human trabecular bone across the tibia were performed. • The creep rate was found to be inversely proportional to the density of the samples. • μ-computed tomography before and after testing identified regions of deformation. • Bending of the trabeculae was found to be the main deformation mode.

Creep buckling of shells

International Nuclear Information System (INIS)

Stone, C.M.; Nickell, R.E.

1977-01-01

Because of the characteristics of LMFBR primary piping components (thin-walled, low pressure, high temperature), the designer must guard against creep buckling as a potential failure mode for certain critical regions, such as elbows, where structural flexibility and inelastic response may combine to concentrate deformation and cause instability. The ASME Boiler and Pressure Vessel Code, through its elevated temperature Code Case 1592 (Section III, Division 1) provides design rules for Class 1 components aimed at preventing creep buckling during the design life. A similar set of rules is being developed for Class 2 and 3 components at this time. One of the original concepts behind the creep buckling rules was that the variability in creep properties (especially due to the effects of prior heat treatment), the uncertainty about initial imperfections, and the lack of confirmed accuracy of design analysis meant that conservatism would be difficult to assure. As a result, a factor of ten on service life was required (i.e. analysis must show that, under service conditions that extrapolate the life of the component by ten times, creep buckling does not occur). Two obvious problems with this approach are that: first, the creep behavior must also be extrapolated (since most creep experiments are terminated at a small fraction of the design life, extrapolation of creep data is already an issue, irrespective of the creep buckling question); second the nonlinear creep analysis, which is very nearly prohibitively expensive for design life histograms, becomes even more costly. Analytical results for an aluminum cylindrical shell subjected to axial loads at elevated temperatures are used to examine the supposed equivalence of two types of time-dependent buckling safety factors - a factor of ten on service life and a factor of 1.5 on loading

Fatigue and creep deformed microstructures of aged alloys based on Al-4% Cu-0.3% Mg

International Nuclear Information System (INIS)

Reddy, A. Somi

2008-01-01

The addition of 0.4 wt.% of silver or cadmium to the alloy Al-4% Cu-0.3% Mg which has a high Cu:Mg ratio, changes the nature, morphology and dispersion of the precipitates that forms on age hardening at medium temperatures such as 150-200 o C. Fatigue and creep tests were carried out on alloys aged to peak strength at 170 o C. The tensile properties of the alloys aged at 170 o C increased in the order Al-4% Cu, Al-4% Cu-0.3% Mg, Al-4% Cu-0.3% Mg-0.4% Cd, and Al-4% Cu-0.3% Mg-0.4% Ag. Despite differences in their microstructures and tensile properties, the fatigue performance of the alloys was relatively unaffected. Fatigue behaviour was similar in each case and the alloys showed identical fatigue limits. Major differences were observed in the creep performance of the alloys creep tested at 150 o C in the peak strength condition age hardened at 170 o C. Creep performance of the alloys increased in the order of their tensile properties. The purpose of the present work was to discuss the fatigue and creep deformed microstructure of these alloys

Transformation-Induced Creep and Creep Recovery of Shape Memory Alloy.

Science.gov (United States)

Takeda, Kohei; Tobushi, Hisaaki; Pieczyska, Elzbieta A

2012-05-22

If the shape memory alloy is subjected to the subloop loading under the stress-controlled condition, creep and creep recovery can appear based on the martensitic transformation. In the design of shape memory alloy elements, these deformation properties are important since the deflection of shape memory alloy elements can change under constant stress. The conditions for the progress of the martensitic transformation are discussed based on the kinetics of the martensitic transformation for the shape memory alloy. During loading under constant stress rate, temperature increases due to the stress-induced martensitic transformation. If stress is held constant during the martensitic transformation stage in the loading process, temperature decreases and the condition for the progress of the martensitic transformation is satisfied, resulting in the transformation-induced creep deformation. If stress is held constant during the reverse transformation stage in the unloading process, creep recovery appears due to the reverse transformation. The details for these thermomechanical properties are investigated experimentally for TiNi shape memory alloy, which is most widely used in practical applications. The volume fraction of the martensitic phase increases in proportion to an increase in creep strain.

Creep and creep-rupture behavior of Alloy 718

International Nuclear Information System (INIS)

Brinkman, C.R.; Booker, M.K.; Ding, J.L.

1991-01-01

Data obtained from creep and creep-rupture tests conducted on 18 heats of Alloy 718 were used to formulate models for predicting high temperature time dependent behavior of this alloy. Creep tests were conducted on specimens taken from a number of commercial product forms including plate, bar, and forgoing material that had been procured and heat treated in accordance with ASTM specifications B-670 or B-637. Data were obtained over the temperature range of 427 to 760 degree C ad at test times to about 87,000 h. Comparisons are given between experimental data and the analytical models. The analytical models for creep-rupture included one based on lot-centering regression analysis and two based on the Minimum Commitment Method. A ''master'' curve approach was used to develop and equation for estimating creep deformation up to the onset of tertiary creep. 11 refs., 13 figs

Acceleration of Fe2W precipitation and its effect on creep deformation behavior of 8.5Cr-2W-VNb steels with Si

International Nuclear Information System (INIS)

Fujitsuna, N.; Igarashi, M.; Abe, F.

2000-01-01

The effect of Si on the precipitation behavior of M 23 C 6 and Fe 2 W Laves phase during creep and on the creep deformation behavior was studied on 8.5Cr-2W-VNb steels at 650 C for up to 10000 h. During creep and aging, Fe 2 W Laves phase precipitated and then the amount and the mean particle size of Fe 2 W precipitates became larger with increasing Si concentration, while the amount and the mean size of M 23 C 6 was scarcely changed by the addition of Si. It was cleared that Si-addition influence more strongly on the precipitation of Fe 2 W than M 23 C 6 . The creep rupture strength of the steels increased with increasing Si concentration at high stresses and short rupture times less than 2000 h, while it had a maximum at 0.3% Si and then decreased with increasing Si concentration at low stresses and long rupture times longer than 2000 h. The decrease of creep rate in the acceleration creep region was more significant by Si-addition, and the minimum creep rate was decreased by Si-addition at all stress conditions. The change in creep deformation behavior by Si-addition resulted mainly from the change in precipitation behavior of Fe 2 W, such that the decrease of creep rate in transient creep region is more significant by acceleration of Fe 2 W precipitating on the lath boundary to suppress the recovery of the lath structure and that the extreme increase of creep rate after reaching a minimum creep rate and the decrease of duration of acceleration creep region occurred with coarsening of Fe 2 W. (orig.)

Strengthening mechanisms, creep, and fatigue processes in dispersion-hardened niobium alloy. Final scientific report, 1 Feb 89-31 Jan 92

Energy Technology Data Exchange (ETDEWEB)

Mukherjee, A.K.; Gibeling, J.C.

1992-04-20

The creep and fatigue properties of pure Nb and Nb-l%Zr alloy were investigated. A model was developed based on the migration of subgrain boundary that can explain the anomalous primary creep transients found in Nb-l%Zr alloy, due to coarsening of subgrain structure. TEM investigations confirmed that such subgrain coarsening occurs during primary creep of Nb-l%Zr. Baseline low cycle fatigue studies of Nb and Nb-l%Zr were completed. Cyclic hardening is observed and there is a microplastic plateau in Nb. The Nb-1%Zr is stronger in cyclic deformation than Nb, with little influence of strain rate. The deformation in the alloy at both high and low strain rates is controlled by the interaction between gliding edge dislocation and solute atoms.

Creep-fatigue evaluation method for type 304 and 316FR SS

International Nuclear Information System (INIS)

Wada, Y.; Aoto, K.; Ueno, F.

1997-01-01

For long-term creep-fatigue of Type 304SS, intergranular failure is dominant in the case of significant life reduction. It is considered that this phenomenon has its origin in the grain boundary sliding as observed in cavity-type creep-rupture. Accordingly a simplified procedure to estimate intergranular damages caused by the grain boundary sliding is presented in connection with the secondary creep. In the conventional ductility exhaustion method, failure ductility includes plastic strain, and damage estimation is based on the primary creep strain, which is recoverable during strain cycling. Therefore the accumulated creep strain becomes a very large value, and quite different from grain boundary sliding strain. As a new concept on ductility exhaustion, the product of secondary creep rate and time to rupture (Monkman-Grant product) is applied to fracture ductility, and grain boundary sliding strain is approximately estimated using the accumulated secondary creep strain. From the new concept it was shown that the time fraction rule and the conventional ductility exhaustion method can be derived analytically. Furthermore an advanced method on cyclic stress relaxation was examined. If cyclic plastic strain hardening is softened thermally during strain hold, cyclic creep strain behaviour is also softened. An unrecoverable accumulated primary creep strain causes hardening of the primary creep, and the reduction of deformation resistance to the secondary creep caused by thermal softening accelerates grain boundary sliding rate. As the results creep damages depend not on applied stress but on effective stress. The new concept ductility exhaustion method based on the above consideration leads up to simplified time fraction estimation method only by continuous cycling fatigue and monotonic creep which was already developed in PNC for Monju design guide. This method gave good life prediction for the intergranular failure mode and is convenient for design use on the elastic

Creep failure of a spray drier

CSIR Research Space (South Africa)

Carter, P

1998-06-01

Full Text Available , and creep. The calculations pointed to creep, and no positive metallurgic or physical evidence was discovered to support any of the hypotheses. However, the compression stresses implied that creep deformation could have occurred without inducing discernible...

Stone column settlement performance in structured anisotropic clays: the influence of creep

Directory of Open Access Journals (Sweden)

Brian G. Sexton

2016-10-01

Full Text Available The recently developed elasto-viscoplastic Creep-SCLAY1S model has been used in conjunction with PLAXIS 2D to investigate the effectiveness of vibro-replacement in a creep-prone clay. The Creep-SCLAY1S model accounts for anisotropy, bonding, and destructuration, and uses the concept of a constant rate of viscoplastic multiplier to calculate creep strain rate. A comparison of settlement improvement factors with and without creep indicates that ‘total’ settlement improvement factors (primary plus creep are lower than their ‘primary’ counterparts (primary settlement only. The lowest settlement improvement factors arise for analyses incorporating the effect of bonding and destructuration. Examination of the variations of vertical stress with time and depth has indicated that vertical stress is transferred from the soil to the column as the soil creeps. This results in additional column yielding. In addition, the radial and hoop stresses in the soil are lower for the ‘creep’ case. The reduced radial stresses lead to additional column bulging and hence more settlement, whereas the hoop stress reductions appear to be a secondary effect, caused by additional plastic deformation for the ‘creep’ case.

Microstructure in Zircaloy Creep Tested in the R2 Reactor

International Nuclear Information System (INIS)

Pettersson, Kjell

2004-12-01

obstacles to glide. The deformation rate thus decreases with irradiation dose, leading to a primary creep stage. However, finally the loop density saturates after which a steady state creep rate is established

Simultaneous consolidation and creep

DEFF Research Database (Denmark)

Krogsbøll, Anette

1997-01-01

Materials that exhibit creep under constant effective stress typically also show rate dependent behavior. The creep deformations and the rate sensitive behavior is very important when engineering and geological problems with large time scales are considered. When stress induced compaction...

Creep characteristics of precipitation hardened carbon free martensitic alloys

International Nuclear Information System (INIS)

Muneki, S.; Igarashi, M.; Abe, F.

2000-01-01

A new attempt has been demonstrated using carbon free Fe-Ni-Co martensitic alloys strengthened by Laves phase such as Fe 2 W or Fe 2 Mo to achieve homogeneous creep deformation at high temperatures under low stress levels. Creep behavior of the alloys is found to be completely different from that of the conventional high-Cr ferritic steels. The alloys exhibit gradual change in the creep rate with strain both in the transient and acceleration creep regions, and give a larger strain for the minimum creep rate. In these alloys the creep deformation takes place very homogeneously and no heterogeneous creep deformation is enhanced even at low stress levels. The minimum creep rates of the Fe-Ni-Co alloys at 700 C are found to be much lower than that of the conventional steel, which is due to fine dispersion strengthening useful even at 700 C in these alloys. It is thus concluded that the Fe-Ni-Co martensite strengthened by Laves phase is very useful to increase the creep resistance at elevated temperatures over 650 C. (orig.)

An Abnormal Increase of Fatigue Life with Dwell Time during Creep-Fatigue Deformation for Directionally Solidified Ni-Based Superalloy DZ445

Science.gov (United States)

Ding, Biao; Ren, Weili; Deng, Kang; Li, Haitao; Liang, Yongchun

2018-03-01

The paper investigated the creep-fatigue behavior for directionally solidified nickel-based superalloy DZ445 at 900 °C. It is found that the fatigue life shows an abnormal increase when the dwell time exceeds a critical value during creep-fatigue deformation. The area of hysteresis loop and fractograph explain the phenomenon quite well. The shortest life corresponds to the maximal area of hysteresis loop, i. e. the maximum energy to be consumed during the creep-fatigue cycle. The fractographic observation of failed samples further supports the abnormal behavior of fatigue life.

Role of coupled cataclasis-pressure solution deformation in microearthquake activity along the creeping segment of the SAF: Inferences from studies of the SAFOD core samples

Science.gov (United States)

Hadizadeh, J.; Gratier, J.; Renard, F.; Mittempregher, S.; di Toro, G.

2009-12-01

Rocks encountered in the SAFOD drill hole represent deformation in the southern-most extent of the creeping segment of the SAF north of the Parkfield. At the site and toward the northwest the SAF is characterized by aseismic creep as well as strain release through repeating microearthquakes Mmicroscopy, cathodoluminescence imaging, X-ray fluorescence mapping, and energy dispersive X-ray spectroscopy. The observed microstructural deformation that is apparently relevant to the seismological data includes clear evidence of cyclic deformation events, cataclastic flow, and pressure solution creep with attendant vein sealing and fracture healing fabrics. Friction testing of drill cuttings and modeling by others suggest that the overall creep behavior in shale-siltstone gouge may be due to low bulk friction coefficient of 0.2-0.4 for the fault rock. Furthermore, the low resistivity zone extending to about 5km beneath the SAFOD-Middle Mountain area is believed to consist of a pod of fluid-filled fractured and porous rocks. Our microstructural data indicate that the foliated shale-siltstone cataclasites are, in a highly heterogeneous way, more porous and permeable than the host rock and therefore provide for structurally controlled enhanced fluid-rock interactions. This is consistent with the observed pressure solution deformation and the microstructural indications of transiently high fluid pressures. We hypothesize that while the friction laws defining stable sliding are prevalent in bulk deformation of the creeping segment, there exist the possibility of steady conditions for repetitive healing, dilation, and rupture of populations of stress-oriented patches due to operation of pressure solution creep along the fault zone. The limitation on the total area of the locked patches at any given time would be controlled primarily by the imposed tectonic and near field rates of slip and fluid flux within the local permeability structure. The available geophysical data for the

Understanding the mechanisms of amorphous creep through molecular simulation.

Science.gov (United States)

Cao, Penghui; Short, Michael P; Yip, Sidney

2017-12-26

Molecular processes of creep in metallic glass thin films are simulated at experimental timescales using a metadynamics-based atomistic method. Space-time evolutions of the atomic strains and nonaffine atom displacements are analyzed to reveal details of the atomic-level deformation and flow processes of amorphous creep in response to stress and thermal activations. From the simulation results, resolved spatially on the nanoscale and temporally over time increments of fractions of a second, we derive a mechanistic explanation of the well-known variation of creep rate with stress. We also construct a deformation map delineating the predominant regimes of diffusional creep at low stress and high temperature and deformational creep at high stress. Our findings validate the relevance of two original models of the mechanisms of amorphous plasticity: one focusing on atomic diffusion via free volume and the other focusing on stress-induced shear deformation. These processes are found to be nonlinearly coupled through dynamically heterogeneous fluctuations that characterize the slow dynamics of systems out of equilibrium.

In situ monitored in-pile creep testing of zirconium alloys

Science.gov (United States)

Kozar, R. W.; Jaworski, A. W.; Webb, T. W.; Smith, R. W.

2014-01-01

The experiments described herein were designed to investigate the detailed irradiation creep behavior of zirconium based alloys in the HALDEN Reactor spectrum. The HALDEN Test Reactor has the unique capability to control both applied stress and temperature independently and externally for each specimen while the specimen is in-reactor and under fast neutron flux. The ability to monitor in situ the creep rates following a stress and temperature change made possible the characterization of creep behavior over a wide stress-strain-rate-temperature design space for two model experimental heats, Zircaloy-2 and Zircaloy-2 + 1 wt%Nb, with only 12 test specimens in a 100-day in-pile creep test program. Zircaloy-2 specimens with and without 1 wt% Nb additions were tested at irradiation temperatures of 561 K and 616 K and stresses ranging from 69 MPa to 455 MPa. Various steady state creep models were evaluated against the experimental results. The irradiation creep model proposed by Nichols that separates creep behavior into low, intermediate, and high stress regimes was the best model for predicting steady-state creep rates. Dislocation-based primary creep, rather than diffusion-based transient irradiation creep, was identified as the mechanism controlling deformation during the transitional period of evolving creep rate following a step change to different test conditions.

Deformation modeling and the strain transient dip test

International Nuclear Information System (INIS)

Jones, W.B.; Rohde, R.W.; Swearengen, J.C.

1980-01-01

Recent efforts in material deformation modeling reveal a trend toward unifying creep and plasticity with a single rate-dependent formulation. While such models can describe actual material deformation, most require a number of different experiments to generate model parameter information. Recently, however, a new model has been proposed in which most of the requisite constants may be found by examining creep transients brought about through abrupt changes in creep stress (strain transient dip test). The critical measurement in this test is the absence of a resolvable creep rate after a stress drop. As a consequence, the result is extraordinarily sensitive to strain resolution as well as machine mechanical response. This paper presents the design of a machine in which these spurious effects have been minimized and discusses the nature of the strain transient dip test using the example of aluminum. It is concluded that the strain transient dip test is not useful as the primary test for verifying any micromechanical model of deformation. Nevertheless, if a model can be developed which is verifiable by other experimentts, data from a dip test machine may be used to generate model parameters

Influence of Norton's law parameters in the determination of stresses and deformation in materials undergo creep phenomenon

International Nuclear Information System (INIS)

Bevilacqua, L.; Freire, J.L.; Monteiro, E.; Miranda, P.E.V. de

1980-01-01

Experimental results obtained from creep essays for AISI 316 stainless-steel in different temperatures are presented. These results are rounded off by Norton's law for which parameters A e n are determined. It is studied how variations of Norton's law parameters affect the state of stresses and deformation in thin and thick pipes subjected, to internal pressure and constant temperature. It is concluded that for the cases studied the stresses are little affected by the variations of the parameter n and it is difficult too anticipate degrees of the accumulated deformation since the uncertainties or variations in A and n introduce serious errors in the calculation of the deformation velocity [pt

Study of creep behaviour in P-doped copper with slow strain rate tensile tests

International Nuclear Information System (INIS)

Xuexing Yao; Sandstroem, Rolf

2000-08-01

Pure copper with addition of phosphorous is planned to be used to construct the canisters for spent nuclear fuel. The copper canisters can be exposed to a creep deformation up to 2-4% at temperatures in services. The ordinary creep strain tests with dead weight loading are generally employed to study the creep behaviour; however, it is reported that an initial plastic deformation of 5-15% takes place when loading the creep specimens at lower temperatures. The slow strain rate tensile test is an alternative to study creep deformation behaviour of materials. Ordinary creep test and slow strain rate tensile test can give the same information in the secondary creep stage. The advantage of the tensile test is that the starting phase is much more controlled than in a creep test. In a tensile test the initial deformation behaviour can be determined and the initial strain of less than 5% can be modelled. In this study slow strain rate tensile tests at strain rate of 10 -4 , 10 -5 , 10 -6 , and 10 -7 /s at 75, 125 and 175 degrees C have been performed on P-doped pure Cu to supplement creep data from conventional creep tests. The deformation behaviour has successfully been modelled. It is shown that the slow strain rate tensile tests can be implemented to study the creep deformation behaviours of pure Cu

Creep and creep-recovery of a thermoplastic resin and composite

Science.gov (United States)

Hiel, Clem

1988-01-01

The database on advanced thermoplastic composites, which is currently available to industry, contains little data on the creep and viscoelastic behavior. This behavior is nevertheless considered important, particularly for extended-service reliability in structural applications. The creep deformation of a specific thermoplastic resin and composite is reviewed. The problem to relate the data obtained on the resin to the data obtained on the composite is discussed.

Life assessment of Mod.9Cr-1Mo steel. Quantitative evaluation of microstructural damage in creep interrupted specimens and in creep-fatigue specimens

International Nuclear Information System (INIS)

Maruyama, Kouichi; Kato, Syoichi; Nagae, Yuji

1999-02-01

Boiler and steam turbine components in power generating plants are used under creep and creep-fatigue conditions. It is important to measure both creep and creep-fatigue damage of the components in order to assess the residual life of the components. Modified 9Cr-1Mo steel, a candidate material for steam generator in FBR, has a tempered martensitic lath structure. It was proposed in the second report that lath width in the lath structure is closely related to creep strain, and using this relation one can assess residual creep life of a structural component made of the steel. The objectives of this study are to investigate the change of the lath structure during creep.fatigue deformation, and to estimate creep strain by measuring area of cell composing the lath structure. The area of cell can be a better measure of creep deformation than the lath width. The lath structure is covered during creep-fatigue deformation. The lath structure becomes equiaxed cell structure under creep-fatigue more quickly compared with the lath structure recovered during creep. The lath structure recovered under creep-fatigue has a stationary value of the lath width determined by maximum stress at Nf/2. (Nf: number of cycles) If the recovery process of the lath structure can be investigated under creep-fatigue, the lath width can be a measure of the life assessment under creep-fatigue. Area of cell composing the lath structure increases with creep deformation and reaches a stationary value S s determined by creep stress. The rate of increase in the area is faster at a higher stress and temperature. A normalized change in the area of cell, ΔS/ΔS s , was introduced as a measure of the recovery process of martensitic lath structure. ΔS is the change in area of cell from the initial value S 0 , ΔS s is the difference between S s and S 0 . ΔS/ΔS s is uniquely related to creep strain independent of creep conditions. However, the scatter of data in ΔS/ΔS s -strain relation is wider than

Creep of trabecular bone from the human proximal tibia.

Science.gov (United States)

Novitskaya, Ekaterina; Zin, Carolyn; Chang, Neil; Cory, Esther; Chen, Peter; D'Lima, Darryl; Sah, Robert L; McKittrick, Joanna

2014-07-01

Creep is the deformation that occurs under a prolonged, sustained load and can lead to permanent damage in bone. Creep in bone is a complex phenomenon and varies with type of loading and local mechanical properties. Human trabecular bone samples from proximal tibia were harvested from a 71-year old female cadaver with osteoporosis. The samples were initially subjected to one cycle load up to 1% strain to determine the creep load. Samples were then loaded in compression under a constant stress for 2h and immediately unloaded. All tests were conducted with the specimens soaked in phosphate buffered saline with proteinase inhibitors at 37 °C. Steady state creep rate and final creep strain were estimated from mechanical testing and compared with published data. The steady state creep rate correlated well with values obtained from bovine tibial and human vertebral trabecular bone, and was higher for lower density samples. Tissue architecture was analyzed by micro-computed tomography (μCT) both before and after creep testing to assess creep deformation and damage accumulated. Quantitative morphometric analysis indicated that creep induced changes in trabecular separation and the structural model index. A main mode of deformation was bending of trabeculae. Copyright © 2014 Elsevier B.V. All rights reserved.

EFAM ETM-CREEP 03 - the engineering flaw assessment method for creep

International Nuclear Information System (INIS)

Landes, J.D.; Schwalbe, K.H.

2002-01-01

EFAM ETM-CREEP is a document that describes the GKSS procedure for estimating residual lives for structural components that contain crack-like defects and operating in a high temperature regime where they undergo creep deformation. It uses the traditional parameters C t and C * and the ETM parameters δ 5 and δ 5 to characterize the crack extension rates. It relies on input from EFAM ETM 97 for calculating these parameters and from EFAM GTP-CREEP 02 to provide the material property data for crack extension rates and fracture toughness data. (orig.) [de

Creep deformation behavior of weld metal and heat affected zone on 316FR steel thick plate welded joint

International Nuclear Information System (INIS)

Hongo, Hiromichi; Yamazaki, Masayoshi; Watanabe, Takashi; Kinugawa, Junichi; Tanabe, Tatsuhiko; Monma, Yoshio; Nakazawa, Takanori

1999-01-01

Using hot-rolled 316FR stainless plate (50 mm thick) and 16Cr-8Ni-2Mo filler wire, a narrow-gap welded joint was prepared by GTAW (gas tungsten arc welding) process. In addition to conventional round bar specimens of base metals and weld metal, full-thickness joint specimens were prepared for creep test. Creep tests were conducted at 550degC in order to examine creep deformation and rupture behavior in the weld metal of the welded joint. Creep strain distribution on the surface of the joint specimen was measured by moire interferometry. In the welded joint, creep strength of the weld metal zone apart from the surface was larger than that in the vicinity of the surface due to repeating heat cycles during welding. Creep strain and creep rate within the HAZ adjacent to the weld metal zone were smaller than those within the base metal zone. Creep rate of the weld metal zone in the welded joint was smaller than that of the weld metal specimen due to the restraint of the hardened HAZ adjacent to the zone. The full-thickness welded joint specimens showed longer lives than weld metal specimens, though the lives of the latter was shorter than those of the base metal (undermatching). In the full-thickness welded joint specimen, crack started from the last pass layer of the weld metal zone and fracture occurred at the zone. From the results mentioned above, in order to evaluate the creep properties of the welded joint correctly, it is necessary to conduct the creep test using the full-thickness welded joint specimen which includes the weakest zones of the weld metal, the front and back sides of the plate. (author)

Factors influencing creep model equation selection

International Nuclear Information System (INIS)

Holdsworth, S.R.; Askins, M.; Baker, A.; Gariboldi, E.; Holmstroem, S.; Klenk, A.; Ringel, M.; Merckling, G.; Sandstrom, R.; Schwienheer, M.; Spigarelli, S.

2008-01-01

During the course of the EU-funded Advanced-Creep Thematic Network, ECCC-WG1 reviewed the applicability and effectiveness of a range of model equations to represent the accumulation of creep strain in various engineering alloys. In addition to considering the experience of network members, the ability of several models to describe the deformation characteristics of large single and multi-cast collations of ε(t,T,σ) creep curves have been evaluated in an intensive assessment inter-comparison activity involving three steels, 21/4 CrMo (P22), 9CrMoVNb (Steel-91) and 18Cr13NiMo (Type-316). The choice of the most appropriate creep model equation for a given application depends not only on the high-temperature deformation characteristics of the material under consideration, but also on the characteristics of the dataset, the number of casts for which creep curves are available and on the strain regime for which an analytical representation is required. The paper focuses on the factors which can influence creep model selection and model-fitting approach for multi-source, multi-cast datasets

Shearing creep properties of cements with different irregularities on two surfaces

International Nuclear Information System (INIS)

Zhang, Qingzhao; Shen, Mingrong; Ding, Wenqi; Clark, Carl

2012-01-01

The study of creep properties of the rock mass structural plane is of great importance in solving practical problems in rock mass mechanics. The time-dependent deformation and long-term strength of the rock mass are controlled significantly by the creep mechanical behaviour of the structural plane, and the study of creep properties of the rock mass structural plane is an important area in rock mass deformation. This paper presents fundamental research on the mechanical properties of regular jugged discontinuities under various normal stresses, and focuses on the creep property of the structural plane with various slope angles under different normal stress through shear creep tests of the structural plane under shear stress. According to test results, the shear creep property of the structural plane is described and the creep velocity and long-term strength of the structural plane during shear creep is also investigated. Finally, an empirical formula is established to evaluate the shear strength of the discontinuity and a modified Burger model proposed to represent the shear deformation property during creep. (paper)

Use of state variables in the description of irradiation creep and deformation of metals

International Nuclear Information System (INIS)

Hart, E.W.; Li, C.Y.

1976-01-01

The understanding of the effects of irradiation on metal creep and deformation are not yet satisfactory, owing in part to the limitations on experimentation in radiation environment. Because of such limitations, theoretical considerations must play a strong role. Virtually all of the theoretical considerations currently employed are based on micro-mechanical models for the deformation behavior. The recent theoretical and experimental development of a plastic equation of state for metal deformation has led to the identification of some of the principal micro-mechanisms in phenomenological terms. The role of the individual mechanisms can be related to the state variables of the description, and those variables are directly accessible measurable quantities. This paper explores how irradiation might affect this description. It is shown that the radiation flux and the radiation fluence are expected to affect different components of the equation of state. The resultant description makes considerable use of the information developed in radiation-free environment. 5 fig

Effect of loading rate on creep of phosphorous doped copper

Energy Technology Data Exchange (ETDEWEB)

Andersson-Oestling, Henrik C.M.; Sandstroem, Rolf (Swerea KIMAB (Sweden))

2011-12-15

Creep testing of copper intended for nuclear waste disposal has been performed on continuous creep tests machines at a temperature of 75 deg C. The loading time has been varied from 1 hour to 6 months. The rupture strain including both loading and creep strains does not differ from traditional dead weight lever creep test rigs. The loading strain increases with increasing loading time, at the expense of the creep strain. The time dependence of the creep strain has been modelled taking athermal plastic deformation and creep into account. During loading the contribution to the strain from the athermal plastic deformation dominates until the stress is close to the constant load level. When the constant load has been reached there is no more athermal strain and all of the strain comes from creep

Effects of bone damage on creep behaviours of human vertebral trabeculae.

Science.gov (United States)

O'Callaghan, Paul; Szarko, Matthew; Wang, Yue; Luo, Jin

2018-01-01

A subgroup of patients suffering with vertebral fractures can develop progressive spinal deformities over time. The mechanism underlying such clinical observation, however, remains unknown. Previous studies suggested that creep deformation of the vertebral trabeculae may play a role. Using the acoustic emission (AE) technique, this study investigated effects of bone damage (modulus reduction) on creep behaviours of vertebral trabecular bone. Thirty-seven human vertebral trabeculae samples were randomly assigned into five groups (A to E). Bones underwent mechanical tests using similar experimental protocols but varied degree of bone damage was induced. Samples first underwent creep test (static compressive stress of 0.4MPa) for 30min, and then were loaded in compression to a specified strain level (0.4%, 1.0%, 1.5%, 2.5%, and 4% for group A to E, respectively) to induce different degrees of bone damage (0.4%, no damage control; 1.0%, yield strain; 1.5%, beyond yield strain, 2.5% and 4%, post-ultimate strains). Samples were creep loaded (0.4MPa) again for 30min. AE techniques were used to monitor bone damage. Bone damage increased significantly from group A to E (P30% of modulus reduction in group D and E. Before compressive loading, creep deformation was not different among the five groups and AE hits in creep test were rare. After compressive loading, creep deformation was significantly greater in group D and E than those in other groups (Pcreep test were significantly greater in group D and E than in group A, B, and C (Pcreep deformation may occur even when the vertebra was under physiological loads. The boosted creep deformation observed may be attributed to newly created trabecular microfractures. Findings provide a possible explanation as to why some vertebral fracture patients develop progressive spinal deformity over time. Copyright © 2017. Published by Elsevier Inc.

A method of creep damage summation based on accumulated strain for the assessment of creep-fatigue endurance

International Nuclear Information System (INIS)

Hales, R.

1983-01-01

A method of combining long term creep data with relatively short term mechanical behaviour to provide an estimate of creep-fatigue endurance is presented. It is proposed that the creep-fatigue effect in high temperature cyclic deformation is governed by a difference in strain rate around the cycle and the associated variation in ductility with strain rate. (author)

Characterization of the elastic and viscoelastic properties of dentin by a nanoindentation creep test.

Science.gov (United States)

Chuang, Shu-Fen; Lin, Shih-Yun; Wei, Pal-Jen; Han, Chang-Fu; Lin, Jen-Fin; Chang, Hsien-Chang

2015-07-16

Dentin is the main supporting structure of teeth, but its mechanical properties may be adversely affected by pathological demineralization. The purposes of this study were to develop a quantitative approach to characterize the viscoelastic properties of dentin after de- and re-mineralization, and to examine the elastic properties using a nanoindentation creep test. Dentin specimens were prepared to receive both micro- and nano-indentation tests at wet and dry states. These tests were repeatedly performed after demineralization (1% citric acid for 3 days) and remineralization (artificial saliva immersion for 28 days). The nanoindentation test was executed in a creep mode, and the resulting displacement-time responses were disintegrated into primary (transient) and secondary (viscous) creep. The structural changes and mineral densities of dentin were also examined under SEM and microCT, respectively. The results showed that demineralization removed superficial minerals of dentin to the depth of 400 μm, and affected its micro- and nano-hardness, especially in the hydrate state. Remineralization only repaired the minerals at the surface layer, and partially recovered the nanohardness. Both the primary the secondary creep increased in the demineralized dentin, while the hydration further enhanced creep deformation of untreated and remineralized dentin. Remineralization reduced the primary creep of dentin, but did not effectively increase the viscosity. In conclusion, water plasticization increases the transient and viscous creep strains of demineralized dentin and reduces load sustainability. The nanoindentation creep test is capable of analyzing the elastic and viscoelastic properties of dentin, and reveals crucial information about creep responses. Copyright © 2015 Elsevier Ltd. All rights reserved.

The creep and intergranular cracking behavior of Ni-Cr-Fe-C alloys in 360 degree C water

International Nuclear Information System (INIS)

Angeliu, T.M.; Paraventi, D.J.; Was, G.S.

1995-01-01

Mechanical testing of controlled-purity Ni-xCr-9Fe-yC alloys at 360 C revealed an environmental enhancement in IG cracking and time-dependent deformation in high purity and primary water over that exhibited in argon. Dimples on the IG facets indicate a creep void nucleation and growth failure mode. IG cracking was primarily located at the interior of the specimen and not necessarily linked to direct contact with the environment. Controlled potential CERT experiments showed increases in IG cracking as the applied potential decreased, suggesting that hydrogen is detrimental to the mechanical properties. It is proposed that the environment, through the presence of hydrogen, enhances IG cracking by enhancing the matrix dislocation mobility. This is based on observations that dislocation-controlled creep controls the IG cracking of controlled-purity Ni-xCr-9Fe-yC in argon at 360 C and grain boundary cavitation and sliding results that show the environmental enhancement of the creep rate is primarily due to an increase in matrix plastic deformation. However, controlled potential CLT experiments did not exhibit a change in the creep rate as the applied potential decreased. While this does not clearly support hydrogen assisted creep, the material may already be saturated with hydrogen at these applied potentials and thus no effect was realized. Chromium and carbon decrease the IG cracking in high purity and primary water by increasing the creep resistance. The surface film does not play a significant role in the creep or IG cracking behavior under the conditions investigated

Predicting sample lifetimes in creep fracture of heterogeneous materials

Science.gov (United States)

Koivisto, Juha; Ovaska, Markus; Miksic, Amandine; Laurson, Lasse; Alava, Mikko J.

2016-08-01

Materials flow—under creep or constant loads—and, finally, fail. The prediction of sample lifetimes is an important and highly challenging problem because of the inherently heterogeneous nature of most materials that results in large sample-to-sample lifetime fluctuations, even under the same conditions. We study creep deformation of paper sheets as one heterogeneous material and thus show how to predict lifetimes of individual samples by exploiting the "universal" features in the sample-inherent creep curves, particularly the passage to an accelerating creep rate. Using simulations of a viscoelastic fiber bundle model, we illustrate how deformation localization controls the shape of the creep curve and thus the degree of lifetime predictability.

Standard test method for creep-fatigue crack growth testing

CERN Document Server

American Society for Testing and Materials. Philadelphia

2010-01-01

1.1 This test method covers the determination of creep-fatigue crack growth properties of nominally homogeneous materials by use of pre-cracked compact type, C(T), test specimens subjected to uniaxial cyclic forces. It concerns fatigue cycling with sufficiently long loading/unloading rates or hold-times, or both, to cause creep deformation at the crack tip and the creep deformation be responsible for enhanced crack growth per loading cycle. It is intended as a guide for creep-fatigue testing performed in support of such activities as materials research and development, mechanical design, process and quality control, product performance, and failure analysis. Therefore, this method requires testing of at least two specimens that yield overlapping crack growth rate data. The cyclic conditions responsible for creep-fatigue deformation and enhanced crack growth vary with material and with temperature for a given material. The effects of environment such as time-dependent oxidation in enhancing the crack growth ra...

Radiation-induced creep and swelling

International Nuclear Information System (INIS)

Heald, P.T.

1977-01-01

The physical basis for radiation induced creep and swelling is reviewed. The interactions between the point defects and dislocations are recalled since these interactions are ultimately responsible for the observable deformation phenomena. Both the size misfit interaction and the induced inhomogeneity interaction are considered since the former gives rise to irradiation swelling while the latter, which depends on both internal and external stresses, results in irradiation creep. The defect kinetics leading to the deformation processes are discussed in terms of chemical rate theory. The rate equations for the spatially averaged interstitial and vacancy concentrations are expressed in terms of the microstructural sink strengths and the solution of these equations leads to general expressions for the deformation rates

A study on creep properties of laminated rubber bearings. Pt. 1. Creep properties and numerical simulations of thick rubber bearings

International Nuclear Information System (INIS)

Matsuda, Akihiro; Yabana, Shuichi

2000-01-01

In this report, to evaluate creep properties and effects of creep deformation on mechanical properties of thick rubber bearings for three-dimensional isolation system, we show results of compression creep test for rubber bearings of various rubber materials and shapes and development of numerical simulation method. Creep properties of thick rubber bearings were obtained from compression creep tests. The creep strain shows steady creep that have logarithmic relationships between strain and time and accelerated creep that have linear relationships. We make numerical model of a rubber material with nonlinear viscoelastic constitutional equations. Mechanical properties after creep loading test are simulated with enough accuracy. (author)

Development of evaluation technique of high temperature creep characteristics by small punch-creep test method (I)

International Nuclear Information System (INIS)

Baek, Seung Se; Na, Sung Hun; Yu, Hyo Sun; Na, Eui Gyun

2001-01-01

In this study, a Small Punch Creep(SP-Creep) test using miniaturized specimen(10 x 10 x 0.5mm) is described to develop the new creep test method for high temperature structural materials. The SP-Creep test is applied to 2.25Cr-1Mo(STBA24) steel which is widely used as boiler tube material. The test temperatures applied for the creep deformation of miniaturized specimens are between 550∼600 .deg. C. The SP-Creep curves depend definitely on applied load and creep temperature, and show the three stages of creep behavior like in conventional uniaxial tensile creep curves. The load exponent of miniaturized specimen decrease with increasing test temperature, and its behavior is similar to stress exponent behavior of uniaxial creep test. The creep activation energy obtained from the relationship between SP-Creep rate and test temperature decreases as the applied load increases. A predicting equation of SP-Creep rate for 2.25Cr-1Mo steel is suggested, and a good agreement between experimental and calculated data has been found

Recent Methodologies for Creep Deformation Analysis and Its Life Prediction

International Nuclear Information System (INIS)

Kim, Woo-Gon; Park, Jae-Young; Iung

2016-01-01

To design the high-temperature creeping materials, various creep data are needed for codification, as follows: i) stress vs. creep rupture time for base metals and weldments (average and minimum), ii) stress vs. time to 1% total strain (average), iii) stress vs. time to onset of tertiary creep (minimum), and iv) constitutive eqns. for conducting time- and temperature- dependent stress-strain (average), and v) isochronous stress-strain curves (average). Also, elevated temperature components such as those used in modern power generation plant are designed using allowable stress under creep conditions. The allowable stress is usually estimated on the basis of up to 10"5 h creep rupture strength at the operating temperature. The master curve of the “sinh” function was found to have a wider acceptance with good flexibility in the low stress ranges beyond the experimental data. The proposed multi-C method in the LM parameter revealed better life prediction than a single-C method. These improved methodologies can be utilized to accurately predict the long-term creep life or strength of Gen-IV nuclear materials which are designed for life span of 60 years

Irradiation creep and growth of zircaloy-4 tubes

International Nuclear Information System (INIS)

Lansiart, S.; Darchis, L.; Pelchat, J.

1990-01-01

The influence of temperature and fast neutron flux on irradiation creep and growth of stress relieved zircaloy-4 pressurized tubes has been derived from experimental irradiations in NaK, performed up to 2.5 10 25 n.m -2 in the temperature range [280, 350] 0 C. A significant influence of temperature on axial growth has been observed: at 280 0 C the elongation can no longer be expressed as a linear function of fluence as for the 350 0 C irradiation temperature; diametral growth, on the other hand, always appears negligible. Irradiation creep obviously depends on temperature too; the diametral strain (including thermal part) has been modelled as a sum of primary and secondary terms, the former being independent of fluence. For the tubing considered it is observed that the ranking of the different batches, with respect to diametral creep resistance, is the same before and under irradiation. Concerning axial creep strain the stress relieved material behaves as does an isotropic tube. This is not the case of recrystallized zircaloy-4 F, which shows a non negligible axial deformation, related to the diametral creep one, even though this diametral irradiation creep strain is strongly reduced comparatively to that of the stress relieved material. The comparison of the two materials growth rates is more complex since their dependence on temperature and flux differs

Assessment of Creep Deformation, Damage, and Rupture Life of 304HCu Austenitic Stainless Steel Under Multiaxial State of Stress

Science.gov (United States)

Sahoo, K. C.; Goyal, Sunil; Parameswaran, P.; Ravi, S.; Laha, K.

2018-03-01

The role of the multiaxial state of stress on creep deformation and rupture behavior of 304HCu austenitic stainless steel was assessed by performing creep rupture tests on both smooth and notched specimens of the steel. The multiaxial state of stress was introduced by incorporating circumferential U-notches of different root radii ranging from 0.25 to 5.00 mm on the smooth specimens of the steel. Creep tests were carried out at 973 K over the stress range of 140 to 220 MPa. In the presence of notch, the creep rupture strength of the steel was found to increase with the associated decrease in rupture ductility. Over the investigated stress range and notch sharpness, the strengthening was found to increase drastically with notch sharpness and tended toward saturation. The fractographic studies revealed the mixed mode of failure consisting of transgranular dimples and intergranular creep cavitation for shallow notches, whereas the failure was predominantly intergranular for relatively sharper notches. Detailed finite element analysis of stress distribution across the notch throat plane on creep exposure was carried out to assess the creep failure of the material in the presence of notch. The reduction in von-Mises stress across the notch throat plane, which was greater for sharper notches, increased the creep rupture strength of the material. The variation in fracture behavior of the material in the presence of notch was elucidated based on the von-Mises, maximum principal, and hydrostatic stresses. Electron backscatter diffraction analysis of creep strain distribution across the notch revealed localized creep straining at the notch root for sharper notches. A master curve for predicting creep rupture life under the multiaxial state of stress was generated considering the representative stress having contributions from both the von-Mises and principal stress components of the stress field in the notch throat plane. Rupture ductility was also predicted based on the

Grain boundary precipitation strengthening mechanism in W containing advanced creep resistant ferritic steels

Energy Technology Data Exchange (ETDEWEB)

Shibata, T.; Hasegawa, Y. [Tohoku Univ., Sendai (Japan)

2010-07-01

Grain boundary precipitation strengthening is expected to be a decisive factor in developing ferritic creep resistant steels. This study examined the grain boundary precipitation strengthening mechanism extracting the effect of the tempered martensitic microstructure and precipitates on the high angle grain boundary in M{sub 23}C4{sub 6} type carbide and the Fe{sub 2}W type Laves phase effect of the creep deformation fixing the grain boundary according to transmission electron microscope (TEM) observation. A creep test was carried out at high temperature in order to evaluate the high angle boundary strengthening effect simulating the long-term creep deformation microstructure by the lath structure disappearance. The correlation of the creep rupture time and the grain boundary shielding ratio were found to be independent of precipitate type. The creep deformation model represents block boundary shielding by precipitates as the decisive factor for W containing ferritic creep resistant steels. (orig.)

Evaluation of permanent deformation characteristics of unmodified and Polyethylene Terephthalate modified asphalt mixtures using dynamic creep test

International Nuclear Information System (INIS)

Baghaee Moghaddam, Taher; Soltani, Mehrtash; Karim, Mohamed Rehan

2014-01-01

Highlights: • Waste PET was utilized as modifier in asphalt mixture. • Deformation characteristics of asphalt mixtures were assessed. • Dynamic creep test was conducted at different temperatures and stress levels. • Permanent deformation models were introduced. - Abstract: One of the major types of plastics that can be found in Municipal Solid Waste (MSW) is Polyethylene Terephthalate (PET) which is a non-biodegradable semi-crystalline thermoplastic polymer, and is considered as polyester material. Generating large amount of waste PET, mainly as bottles, would cause environmental hazards by disposing in landfills. This paper aims to evaluate effects of utilizing waste PET flakes as modifier in asphalt mixture as an alternative solution to overcome the potential risks arise from producing large amount of waste PET as well as evaluating the deformation characteristics of unmodified and PET modified asphalt mixtures. To achieve this aim, different percentages of PET were designated for this investigation, namely: 0%, 0.2%, 0.4%, 0.6%, 0.8% and 1% by weight of aggregate particles, and dynamic creep test was performed at different stress levels (300 kPa and 400 kPa) and temperatures (10 °C, 25 °C and 40 °C). Consequently, Zhou three-stage model was developed. The results showed that permanent deformation characteristics of asphalt mixture were considerably improved by utilization of PET modification, when the permanent strain was remarkably decreased in PET modified mixture compared to the conventional mixture at all stress levels and temperatures. Besides, based on Zhou model, it was concluded that elastic and visco-elastic properties of asphalt mixture were improved by application of PET modification

Oxidation and creep failure of alloy 617 foils at high temperature

Energy Technology Data Exchange (ETDEWEB)

Sharma, S.K.; Ko, G.D.; Li, F.X. [Department of Mechanical Engineering, Chonnam National University, Gwangju 500 757 (Korea, Republic of); Kang, K.J. [Department of Mechanical Engineering, Chonnam National University, Gwangju 500 757 (Korea, Republic of)], E-mail: kjkang@chonnam.ac.kr

2008-08-31

The microstructure of thermally grown oxides (TGO) and the creep properties of alloy 617 were investigated. Oxidation and creep tests were performed on 100 {mu}m thick foils at 800-1000 deg. C in air environment, while the thickness of TGO was monitored in situ. According to energy dispersive X-ray (EDX) mapping micrographs observation, superficial dense oxides, chromia (Cr{sub 2}O{sub 3}), which was thermodynamically unstable at 1000 deg. C, and discrete internal oxides, alumina ({alpha}-Al{sub 2}O{sub 3}), were found. Consequently, the weight of the foil specimen decreased due to the spalling and volatilization of the Cr{sub 2}O{sub 3} oxide layer after an initial weight-gaining. Secondary and tertiary creeps were observed at 800 deg. C, while the primary, secondary and tertiary creeps were observed at 1000 deg. C. Dynamic recrystallization occurred at 800 deg. C and 900 deg. C, while partial dynamic recrystallization at 1000 deg. C. The apparent activation energy, Q{sub app}, for the creep deformation was 271 kJ/mol, which was independent of the applied stress.

Cavitation contributes substantially to tensile creep in silicon nitride

International Nuclear Information System (INIS)

Luecke, W.E.; Wiederhorn, S.M.; Hockey, B.J.; Krause, R.F. Jr.; Long, G.G.

1995-01-01

During tensile creep of a hot isostatically pressed (HIPed) silicon nitride, the volume fraction of cavities increases linearly with strain; these cavities produce nearly all of the measured strain. In contrast, compressive creep in the same stress and temperature range produces very little cavitation. A stress exponent that increases with stress (var-epsilon ∝ σ n , 2 < n < 7) characterizes the tensile creep response, while the compressive creep response exhibits a stress dependence of unity. Furthermore, under the same stress and temperature, the material creeps nearly 100 times faster in tension than in compression. Transmission electron microscopy (TEM) indicates that the cavities formed during tensile creep occur in pockets of residual crystalline silicate phase located at silicon nitride multigrain junctions. Small-angle X-ray scattering (SAXS) from crept material quantifies the size distribution of cavities observed in TEM and demonstrates that cavity addition, rather than cavity growth, dominates the cavitation process. These observations are in accord with a model for creep based on the deformation of granular materials in which the microstructure must dilate for individual grains t slide past one another. During tensile creep the silicon nitride grains remain rigid; cavitation in the multigrain junctions allows the silicate to flow from cavities to surrounding silicate pockets, allowing the dilation of the microstructure and deformation of the material. Silicon nitride grain boundary sliding accommodates this expansion and leads to extension of the specimen. In compression, where cavitation is suppressed, deformation occurs by solution-reprecipitation of silicon nitride

Study of the temperature dependence of the uniaxial creep property of similar material of new soft rock

Science.gov (United States)

Wang, Y. Y.; Wu, Y.; Fan, X. Y.; Zhang, J. L.; Guo, P.; Li, J. G.

2017-11-01

Using the experimental method, the experimental research of creep properties were conducted under different temperature ranging from 10°C to 60°C. The similar material of new soft rock consists of paraffin, which can obtain that the deformation contains the instantaneous elastic deformation and creep deformation through the uniaxial creep experimental results. And thus the increase of temperature has great influence on the creep characteristics of similar soft rock according to the creep curve of similar soft rock at 10°C to 60°C. With the increase of temperature, the slope of the stress-strain curve of similar soft rock is increasing, while the average of the creep modulus is decreasing, which means that the capacity of resist deformation is reduced. Therefore, the creeps law of high-temperature and short-time can be shown the creep phenomenon of low-temperature and long-time, and further shorten the creep experimental cycle.

Creep cavitation effects in polycrystalline alumina

International Nuclear Information System (INIS)

Porter, J.R.; Blumenthal, W.; Evans, A.G.

1981-01-01

Fine grained polycrystalline alumina has been deformed in creep at high temperatures, to examine the evolution of cavities at grain boundaries. Cavities with equilibrium and crack-like morphologies have been observed, distributed nonuniformly throughout the material. The role of these cavities during creep has been described. A transition from equilibrium to crack-like morphology has been observed and correlated with a model based on the influence of the surface to boundary diffusivity ratio and the local tensile stress. The contribution of cavitation to the creep rate and total creep strain has been analyzed and excluded as the principal cause of the observed non-linear creep rate

Quantitative analysis of microstructure deformation in creep fenomena of ferritic SA-213 T22 and austenitic SA-213 TP304H material

Science.gov (United States)

Mulyana, Cukup; Taufik, Ahmad; Gunawan, Agus Yodi; Siregar, Rustam Efendi

2013-09-01

The failure of critical component of fossil fired power plant that operated in creep range (high stress, high temperature and in the long term) depends on its microstructure characteristics. Ferritic low carbon steel (2.25Cr-1Mo) and Austenitic stainless alloy (18Cr-8Ni) are used as a boiler tube in the secondary superheater outlet header to deliver steam before entering the turbin. The tube failure is occurred in a form of rupture, resulting trip that disrupts the continuity of the electrical generation. The research in quantification of the microstructure deformation has been done in predicting the remaining life of the tube through interrupted accelerated creep test. For Austenitic Stainless Alloy (18Cr-8Ni), creep test was done in 550°C with the stress 424.5 MPa and for Ferritic Low Carbon Steel (2.25Cr-1Mo) in 570°C with the stress 189 MPa. The interrupted accelerated creep test was done by stopping the observation in condition 60%, 70%, 80% and 90% of remaining life, the creep test fracture was done before. Then the micro hardness test, photo micro, SEM and EDS were obtained from those samples. Refer to ASTM E122, microstructure parameters were calculated. The results indicated that there are a consistency of decreasing their grain diameters, increasing their grain size numbers, micro hardness, and the length of crack or void number per unit area with the decreasing of remaining life. While morphology of grain (stated in parameter α=LV/LH) relatively constant for austenitic. However, for ferritic the change of morphology revealed significantly. Fracture mode propagation of ferritic material is growth with voids transgranular and intergranular crack, and for austenitic material the fracture growth with intergranular creep fracture void and wedge crack. In this research, it was proposed a formulation of mathematical model for creep behavior corresponding their curve fitting resulted for the primary, secondary and tertiary in accelerated creep test. In

Final Report on in-reactor creep-fatigue deformation behaviour of a CuCrZr alloy: COFAT 1

Energy Technology Data Exchange (ETDEWEB)

Singh, B.N. [Risoe National Lab. - DTU, Materials Research Dept., Roskilde (Denmark); Taehtinen, S.; Moilanen, P. [VTT Industrial Systems (Finland); Jacquet, P.; Dekeyser, J. [SCK-CEN, Reactor Technology Design Dept., Mol (Belgium); Edwards, D.J. [Pacific Northwest National Lab., Reactor Technology Design Dept., Richland (United States); Li, M. [Oak Ridge National Lab., Materials Science and Technology Div., Oak Ridge, Tennessee (United States); Stubbins, J.F. [Univ. of Illinois, Dept. of Nuclear, Plasma and Radiological Engineering, Urbane, Illinois (United States)

2007-08-15

At present, practically nothing is known about the deformation behaviour of materials subjected simultaneously to external cyclic force and neutron irradiation. The main objective of the present work is to determine experimentally the mechanical response and resulting microstructural changes in CuCrZr(HT1) alloy exposed concurrently to flux of neutrons and creep-fatigue cyclic loading directly in a fission reactor. Special experimental facilities were designed and fabricated for this purpose. A number of in-reactor creep-fatigue experiments were successfully carried out in the BR-2 reactor at Mol (Belgium). In the present report we first describe the experimental facilities and the details of the in-reactor creep-fatigue experiments carried out at 363 and 343K at a strain amplitude of 0.5% with hold-times of 10 and 100s, respectively. For comparison purposes, similar creep-fatigue tests were performed outside of the reactor. (i.e. in the absence of neutron irradiation). During in-reactor tests, the mechanical response was continuously registered throughout the whole test. The results are first presented in the form of hysteresis loops confirming that the nature of deformation during these tests was truly cyclic. The temporal evolution of the stress response in the specimens is presented in the form of the average maximum stress amplitude as a function of the number of cycles as well as a function of displacement dose accumulated during the tests. The results illustrate the nature and magnitude of cyclic hardening as well as softening as a function of the number of cycles and displacement dose. Details of the microstructure were investigated using TEM and STEM techniques. The fracture surface morphology was investigated using SEM technique. Both mechanical and microstructural results are briefly discussed. The main conclusion emerging from the limited amount of present results is that neither the irradiation nor the duration of the hold-time have any significant

Tests on creep and influence of creep on strength of concrete under multiaxial stresses

International Nuclear Information System (INIS)

Lanig, N.; Stoeckl, S.; Kupfer, H.

1988-12-01

Long-time tests of three-axially loaded, sealed cylindrical specimens d = 15 cm, h = 40 cm, were carried out. The 20-cm-cube strength of the concrete was app. 45 N/mm 2 . The creep stresses were chosen in the following ranges: 0,3 ≤ σ c /β c ≤ 2,1; 0 ≤ σ r /σ l ≤ 1,0. The creep coefficients obtained were clearly depending on the multi-axial stress conditions. The creep coefficients for a t = 2 years loading were reaching app. 1 for σ l /β c = 0,3 and app. 3 for σ l /β c = 2,1, when the test evaluation was based on the initial deformations meausred after 1 minute. For σ l /β c = 2,1 the creep coefficients obtained were about 4 times as large, proceeding form calculated elastic deformations. Further evaluations concerned the Young's modulus E, Poisson's ratio μ, the bulk modulus K and the shear modulus G. The preceding permanent load leads to an increase in the Young's modulus of the concrete in longitudinal direction of the specimen up to about 4 times the value of not preloaded comparative specimens. (orig.) [de

Creep of parylene-C film

KAUST Repository

Lin, Jeffrey Chun-Hui

2011-06-01

The glass transition temperature of as-deposited parylene-C is first measured to be 50°C with a ramping-temperature-dependent modulus experiment. The creep behavior of parylene-C film in the primary and secondary creep region is then investigated below and above this glass transition temperature using a dynamic mechanical analysis (DMA) machine Q800 from TA instruments at 8 different temperatures: 10, 25, 40, 60, 80, 100, 120 and 150°C. The Burger\\'s model, which is the combined Maxwell model and Kelvin-Voigt model, fits well with our primary and secondary creep data. Accordingly, the results show that there\\'s little or no creep below the glass transition temperature. Above the glass transition temperature, the primary creep and creep rate increases with the temperature, with a retardation time constant around 6 minutes. © 2011 IEEE.

The contrasting roles of creep and stress relaxation in the time-dependent deformation during in-situ cooling of a nickel-base single crystal superalloy.

Science.gov (United States)

Panwisawas, Chinnapat; D'Souza, Neil; Collins, David M; Bhowmik, Ayan

2017-09-11

Time dependent plastic deformation in a single crystal nickel-base superalloy during cooling from casting relevant temperatures has been studied using a combination of in-situ neutron diffraction, transmission electron microscopy and modelling. Visco-plastic deformation during cooling was found to be dependent on the stress and constraints imposed to component contraction during cooling, which mechanistically comprises creep and stress relaxation. Creep results in progressive work hardening with dislocations shearing the γ' precipitates, a high dislocation density in the γ channels and near the γ/γ' interface and precipitate shearing. When macroscopic contraction is restricted, relaxation dominates. This leads to work softening from a decreased dislocation density and the presence of long segment stacking faults in γ phase. Changes in lattice strains occur to a similar magnitude in both the γ and γ' phases during stress relaxation, while in creep there is no clear monotonic trend in lattice strain in the γ phase, but only a marginal increase in the γ' precipitates. Using a visco-plastic law derived from in-situ experiments, the experimentally measured and calculated stresses during cooling show a good agreement when creep predominates. However, when stress relaxation dominates accounting for the decrease in dislocation density during cooling is essential.

Design of creep machine and creep specimen chamber for carrying out creep tests in flowing liquid sodium

Energy Technology Data Exchange (ETDEWEB)

Ravi, S., E-mail: sravi@igcar.gov.in; Laha, K.; Sakthy, S.; Mathew, M.D.; Jayakumar, T.

2014-02-15

Highlights: • Design of a lever type creep machine for carrying out creep test in flowing sodium. • Leveling of lever during creep was achieved by automated movement of fulcrum. • Design of creep chamber for providing constant sodium flow rate across creep specimen. • Minimum use of bellow in chamber for sodium containment and mechanical isolation. • Mini-lever mechanism to counter balance load reduction on specimen due to bellow stiffness. - Abstract: A creep testing system has been designed, fabricated, installed and validated for carrying out creep tests in flowing liquid sodium. The testing system consists of two sections namely creep testing machine and an environmental chamber. The testing system has the ability of (i) applying tensile load to the test specimen through a lever, (ii) monitoring continuously the creep elongation and (iii) allowing sodium to flow around the creep specimen at constant velocity. The annular space between the creep specimen and the environmental chamber has been suitably designed to maintain constant sodium flow velocity. Primary and secondary bellows are employed in the environmental chamber to (i) mechanically isolate the creep specimen, (ii) prevent the flowing sodium in contact with air and (iii) maintain an argon gas cover to the leaking sodium if any from primary bellow, with a provision to an alarm get activated by a spark plug. The lever-horizontality during creep test has been maintained by automatically lifting up the fulcrum instead of lowering down the pull rod as conventionally used. A mini lever mechanism has been incorporated in the load train to counter balance the load reduction on specimen from the changing stiffness of the bellows. The validation of the testing system has been established by carrying out creep tests on 316L(N) stainless steel at 873 K over a wide stress range and comparing the results with those obtained in air by employing the developed and conventional creep testing machines.

Standard test method for creep-fatigue testing

CERN Document Server

American Society for Testing and Materials. Philadelphia

2009-01-01

1.1 This test method covers the determination of mechanical properties pertaining to creep-fatigue deformation or crack formation in nominally homogeneous materials, or both by the use of test specimens subjected to uniaxial forces under isothermal conditions. It concerns fatigue testing at strain rates or with cycles involving sufficiently long hold times to be responsible for the cyclic deformation response and cycles to crack formation to be affected by creep (and oxidation). It is intended as a test method for fatigue testing performed in support of such activities as materials research and development, mechanical design, process and quality control, product performance, and failure analysis. The cyclic conditions responsible for creep-fatigue deformation and cracking vary with material and with temperature for a given material. 1.2 The use of this test method is limited to specimens and does not cover testing of full-scale components, structures, or consumer products. 1.3 This test method is primarily ...

Study of elementary mechanisms of creep in uranium as a function of temperature (150 deg. to 760 deg. C) by activation energy measurements

International Nuclear Information System (INIS)

Grenier, P.

1966-06-01

Creep tests were carried out on single crystals and polycrystalline specimens of uranium in both the α and β phases over the temperature range 150 - 760 deg. C. The determination of the activation energy for creep and the study of its variation with temperature made it possible to distinguish various temperature ranges in which one or more elementary mechanisms govern deformation. Micrographic observations after creep and the study of the variation of creep-rate with load support the conclusions. The creep behavior of single crystals is identical with that of polycrystalline material below 325 deg. C. From 325 deg. C to one upper limiting temperature whose value depends on the purity and previous history of the metal, the creep deformation of uranium is controlled by cross-slip. From this limiting temperature up to 520 deg. C, the creep of uranium involves two independent mechanisms operating simultaneously, the movement of screw dislocation by cross-slip and the climbing of edge dislocations out of their slip plane. Between 520 deg. C and the α - β transformation temperature creep in polycrystals is governed by the climb of edge dislocations out of their slip planes, by a pile up mechanism in the case of primary creep and by dipole annihilation in the case of secondary creep. In single crystals creep is dependent on the climb of edge dislocations into pre-existent sub-boundaries and their subsequent rearrangement within these boundaries. In the β phase the creep of polycrystals is governed by the diffusional climb of edge dislocations. Between 450 and 630 deg. C small alloy additions of molybdenum modify the creep characteristics of uranium although the deformation mechanisms involved are analogous to those in the pure metal. (author) [fr

Brittle Creep Failure, Critical Behavior, and Time-to-Failure Prediction of Concrete under Uniaxial Compression

Directory of Open Access Journals (Sweden)

Yingchong Wang

2015-01-01

Full Text Available Understanding the time-dependent brittle deformation behavior of concrete as a main building material is fundamental for the lifetime prediction and engineering design. Herein, we present the experimental measures of brittle creep failure, critical behavior, and the dependence of time-to-failure, on the secondary creep rate of concrete under sustained uniaxial compression. A complete evolution process of creep failure is achieved. Three typical creep stages are observed, including the primary (decelerating, secondary (steady state creep regime, and tertiary creep (accelerating creep stages. The time-to-failure shows sample-specificity although all samples exhibit a similar creep process. All specimens exhibit a critical power-law behavior with an exponent of −0.51 ± 0.06, approximately equal to the theoretical value of −1/2. All samples have a long-term secondary stage characterized by a constant strain rate that dominates the lifetime of a sample. The average creep rate expressed by the total creep strain over the lifetime (tf-t0 for each specimen shows a power-law dependence on the secondary creep rate with an exponent of −1. This could provide a clue to the prediction of the time-to-failure of concrete, based on the monitoring of the creep behavior at the steady stage.

Some aspects of anelastic and microplastic creep of pure Al and two Al-alloys

Energy Technology Data Exchange (ETDEWEB)

Sgobba, S. (Lab. de Metallurgie Mecanique, Dept. des Materiaux, Ecole Polytechnique Federale de Lausanne (Switzerland)); Kuenzi, H.U. (Lab. de Metallurgie Mecanique, Dept. des Materiaux, Ecole Polytechnique Federale de Lausanne (Switzerland)); Ilschner, B. (Lab. de Metallurgie Mecanique, Dept. des Materiaux, Ecole Polytechnique Federale de Lausanne (Switzerland))

1993-11-01

Anelastic creep of pure Al, commercial Al-Cu and a binary Al-Cu alloy has been measured at room temperature by means of a high resolution laser interferometer. The irreversible component of the deformation was also quantified from measurements of the anelastic creep recovery. The dependence of the deformation-time curves on thermal treatment and cold work is analyzed. The mechanisms responsible for the room temperature anelastic creep are discussed. Materials loaded below their elastic limit can present either a pure anelastic behavior (commercial Al-Cu) or additional viscoelastic creep (pure Al, high purity Al-Cu). For commercial Al-Cu, the presence of an irreversible deformation appears to be mainly related to the state of the surface. A viscoelastic after effect has been measured for this alloy after a Cu-electroplating treatment. As a typical result for room temperature creep, the irreversible deformation depends logarithmically on load time. (orig.).

Some aspects of anelastic and microplastic creep of pure Al and two Al-alloys

International Nuclear Information System (INIS)

Sgobba, S.; Kuenzi, H.U.; Ilschner, B.

1993-01-01

Anelastic creep of pure Al, commercial Al-Cu and a binary Al-Cu alloy has been measured at room temperature by means of a high resolution laser interferometer. The irreversible component of the deformation was also quantified from measurements of the anelastic creep recovery. The dependence of the deformation-time curves on thermal treatment and cold work is analyzed. The mechanisms responsible for the room temperature anelastic creep are discussed. Materials loaded below their elastic limit can present either a pure anelastic behavior (commercial Al-Cu) or additional viscoelastic creep (pure Al, high purity Al-Cu). For commercial Al-Cu, the presence of an irreversible deformation appears to be mainly related to the state of the surface. A viscoelastic after effect has been measured for this alloy after a Cu-electroplating treatment. As a typical result for room temperature creep, the irreversible deformation depends logarithmically on load time. (orig.)

Creep properties of phosphorus alloyed oxygen free copper under multiaxial stress state

International Nuclear Information System (INIS)

Rui Wu; Sandstroem, Rolf; Seitisleam, Facredin

2009-10-01

Phosphorus alloyed oxygen free copper (Cu-OFP) canisters are planned to be used for spent nuclear fuel in Sweden. The copper canisters will be subjected to creep under multiaxial stress states in the repository. Creep tests have therefore been carried out at 75 deg C using double notch specimens with notch acuities of 0.5, 2, 5, and 18.8, respectively. The creep lifetime for notched specimens is considerably longer than that for the smooth one at a given net section stress, indicating that the investigated Cu-OFP is notch insensitive (notch strengthening). The notch strengthening factor in time is, for instance, greater than 70 at 180 MPa for the bluntest notch (notch acuity = 0.5). The creep lifetime is notch acuity dependent. The sharper the notch, the longer the creep lifetime is. The creep deformation is to a significant extent concentrated to the region around the notches. Different deformation on the two notches is observed. Both axial and radial strains on the failed notch are several times larger than those on the unbroken one. Linear relation between the axial and the radial strains on the notches is found. Transgranular failure is predominant, independent of stress, rupture time, and notch acuity. Adjacent to fracture, elongated grains along the stress direction, separate pores and cavities are often visible. On the unbroken notch, fewer separate cavities and cracks are only seen intergranularly for the sharper notches (notch acuity > 2). To interpret the tests for the notched creep specimens, finite element computations have been performed. A fundamental model for primary and secondary creep without fitting parameters has been used as constitutive equation. The FEM-modelling could represent the creep strain versus time curves for the notched specimens in a satisfactory way. In these curves the strain on loading is included. From the FEM-computations a stationary creep stress could be assessed, which is close to the reference stress. For a given

Creep of quartz by dislocation and grain boundary processes

Science.gov (United States)

Fukuda, J. I.; Holyoke, C. W., III; Kronenberg, A. K.

2015-12-01

Wet polycrystalline quartz aggregates deformed at temperatures T of 600°-900°C and strain rates of 10-4-10-6 s-1 at a confining pressure Pc of 1.5 GPa exhibit plasticity at low T, governed by dislocation glide and limited recovery, and grain size-sensitive creep at high T, governed by diffusion and sliding at grain boundaries. Quartz aggregates were HIP-synthesized, subjecting natural milky quartz powder to T=900°C and Pc=1.5 GPa, and grain sizes (2 to 25 mm) were varied by annealing at these conditions for up to 10 days. Infrared absorption spectra exhibit a broad OH band at 3400 cm-1 due to molecular water inclusions with a calculated OH content (~4000 ppm, H/106Si) that is unchanged by deformation. Rate-stepping experiments reveal different stress-strain rate functions at different temperatures and grain sizes, which correspond to differing stress-temperature sensitivities. At 600-700°C and grain sizes of 5-10 mm, flow law parameters compare favorably with those for basal plasticity and dislocation creep of wet quartzites (effective stress exponents n of 3 to 6 and activation enthalpy H* ~150 kJ/mol). Deformed samples show undulatory extinction, limited recrystallization, and c-axis maxima parallel to the shortening direction. Similarly fine-grained samples deformed at 800°-900°C exhibit flow parameters n=1.3-2.0 and H*=135-200 kJ/mol corresponding to grain size-sensitive Newtonian creep. Deformed samples show some undulatory extinction and grain sizes change by recrystallization; however, grain boundary deformation processes are indicated by the low value of n. Our experimental results for grain size-sensitive creep can be compared with models of grain boundary diffusion and grain boundary sliding using measured rates of silicon grain boundary diffusion. While many quartz mylonites show microstructural and textural evidence for dislocation creep, results for grain size-sensitive creep may apply to very fine-grained (<10 mm) quartz mylonites.

Determination of safety margins for creep loaded primary circuit components in case of loss of pressure accidents of a HTR plant (SR 383)

International Nuclear Information System (INIS)

Breitbach, G.; Ahmed, K.; Over, H.; Schubert, F.; Nickel, H.

1991-10-01

The wall thickness of tubes in high temperature plants must be limited in such a way that pressure differences can not produce unadmissible deformations. For HTR (PNP-Plant) the postulated loss of secondary pressure is one of the considered accidents. In that case the tubes of the heat exchangers are loaded by the outher pressure of the primary coolant. So the risk of a creep collapse is given. The report is related to experimental and theoretical work for the creep collapse phenomena. HTR relevant tube geometries of the high temperature alloys NiCr22Co12Mo (INCONEL 617) and X10NiCrAlTi 32 20 (INCOLOY 800) were tested at temperatures of 900 and 950deg C and outer pressure loads in the range 40 bars. The experimental results are compared with theoretically computed values and discussed. The problem of safety margin is treated. Further, simplified procedures are developed for the estimation of the collapse time. (orig.) [de

Deformation and collapse of zircaloy fuel rod cladding into plenum axial gaps

International Nuclear Information System (INIS)

Pfennigwerth, P.L.; Gorscak, D.A.; Selsley, I.A.

1983-01-01

To minimize support structure, blanket and reflector fuel rods of the thoria urania-fueled Light Water Breeder Reactor (LWBR) were designed with non-freestanding Zircaloy-4 cladding. An analytical model was developed to predict deformation of unirradiated cladding into axial gaps of fuel rod plenum regions where it is unsupported. This model uses the ACCEPT finite element computer program to calculate elastic-plastic deformation of cladding due to external pressure. The finite element is 20-node, triquadratic, isoparametric, and 3-dimensional. Its curved surface permits accurate modeling of the tube geometry, including geometric nonuniformities such as circumferential wall thickness variation and initial tube out-of-roundness. Progressive increases in axial gap length due to cladding elongation and fuel stack shrinkage are modeled, as are deformations of fuel pellets and stainless steel support sleeves which bound plenum axial gaps in LWBR type blanket fuel rods. Zircaloy-4 primary and secondary thermal creep representations were developed from uniaxial creep testing of fuel rod tubing. Creep response to multi-axial loading is modeled with a variation of Hill's formulation for anisotropic materials. Coefficients accounting for anisotropic thermal creep in Zircaloy-4 tubes were developed from creep testing of externally pressurized tubes having fixed axial gaps in the range 2.5 cm to 5.7 cm and radial clearances over simulated fuel pellets ranging from zero to 0.089 mm. (orig./RW)

Comparative study of the creep behaviour of single crystals and polycrystals of alpha uranium

International Nuclear Information System (INIS)

Andre, J.P.

1964-03-01

In the first chapter, one describes the creep machine developed to study the deformation of uranium at high temperature in vacuum with a continuous recording. The second chapter presents the results concerning the polycrystals of uranium. The application of the DORN method gives an activation energy for creep of 42 ± 2 Kc, above 550 Celsius degrees, equal to the activation energy for self-diffusion. The study of the variation of the creep rate with the applied stress and the metallographic observations of the deformation induced polygonization allow to conclude that the deformation is controlled by climb of dislocations. In the third chapter, the deformation above 550 Celsius degrees of single crystals of uranium (obtained by β → α change) is studied. The major deformation mode is slip. The preexisting polygonization of these single crystals is very stable and the disorientation between adjacent sub-grains increases with the deformation. The activation energy for creep is higher than that for polycrystals. These results show the influence of the polygonization due to the β → α change on the creep behaviour of α uranium. (authors) [fr

Room temperature creep in metals and alloys

Energy Technology Data Exchange (ETDEWEB)

Deibler, Lisa Anne [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States). Materials Characterization and Performance

2014-09-01

Time dependent deformation in the form of creep and stress relaxation is not often considered a factor when designing structural alloy parts for use at room temperature. However, creep and stress relaxation do occur at room temperature (0.09-0.21 T_m for alloys in this report) in structural alloys. This report will summarize the available literature on room temperature creep, present creep data collected on various structural alloys, and finally compare the acquired data to equations used in the literature to model creep behavior. Based on evidence from the literature and fitting of various equations, the mechanism which causes room temperature creep is found to include dislocation generation as well as exhaustion.

Multiaxial creep of tubes of Alloy 800 and Alloy 617 at high temperature

International Nuclear Information System (INIS)

Penkalla, H.J.; Schubert, F.; Nickel, H.

1989-01-01

The deformation behaviour under multiaxial loading at temperature higher than 800 deg. C is strongly controlled by creep. For dimensioning and inelastic analysis the use of v. Mises theory and Norton's creep law for stationary creep are demonstrated for different combination of internal pressure and axial or torsional stress or strains. The experimental results are in satisfactory agreement with the theoretical predicted deformation behaviour if values for the coefficient k and n in Norton's creep law are used, which are close to the real creep resistance in the component. (author). 11 refs, 12 figs, 2 tabs

Cyclic Creep Behavior of Modified 9Cr-1Mo Steel at 600 .deg. C

International Nuclear Information System (INIS)

Kim, Woo Gon; Kim, Dae Whan; Jang, Jin Sung; Park, Jae Young

2012-01-01

Cyclic deformation behavior is important in practice because high-temperature structural components are exposed under the cyclic conditions of repeated loading. In static creep (SC), the response of the material is simple as a static state of monotonic loading. However, in cyclic creep (CC), it is complex as dynamic loading. Cyclic creep data have been rarely reported until now. In particular, it is not understood well whether cyclic creep will accelerate or retard the creep rate compared with static creep, because it is not only the plastic deformation under cyclic loading is drastically different from monotonic loading, but also the cyclic response is dependent on the cycling frequency, stress range, stress ratio, and hold periods of cycling. Therefore, it is necessary to clarify the cyclic creep behavior influencing the creep deformation and fracture process. In this study, a series of cyclic creep tests was carried out using magnitudes of stress range of constant stress ratio (R=0.1) under continuous tension-tension loading cycles at a hold time of 10 minutes. Cyclic curves were monitored and obtained with time variations, and the properties of the cyclic creep tests were compared with those of static creep tests. The fracture microstructures were observed and analyzed

Creep damage behaviour of modified 9Cr-1Mo steel weld joints

International Nuclear Information System (INIS)

Sakthivel, T.; Laha, K.; Vasudevan, M.; Panneer Selvi, S.

2016-01-01

Creep deformation and rupture behaviour of modified 9Cr-1Mo steel weld joints fabricated by single-pass activated TIG (A-TIG) and shielded metal arc welding (SMAW) processes have been investigated at 923 K over a stress range of 50 to 110 MPa after post weld heat treatment (PWHT). The weld joints exhibited significantly lower creep rupture lives than the base metal at lower applied stresses. Creep rupture location of the weld joints were found to occur in the ICHAZ. An extensive localized creep deformation, coarsening of M 23 C 6 precipitates in the ICHAZ with creep exposure led to the premature type IV failure of the joints. The coarsening of M 23 C 6 precipitates was extensive in the mid-section of the ICHAZ than the sub-surface of the joints, and was more predominant in the SMAW joint. While A-TIG weld joint exhibited reduced creep cavitation and coarsening of M 23 C 6 precipitates due to lower deformation constraints by adjacent regions in the ICHAZ. Hence, A-TIG weld joint exhibited higher creep rupture life than the SMAW joint. (author)

Creep analysis of silicone for podiatry applications.

Science.gov (United States)

Janeiro-Arocas, Julia; Tarrío-Saavedra, Javier; López-Beceiro, Jorge; Naya, Salvador; López-Canosa, Adrián; Heredia-García, Nicolás; Artiaga, Ramón

2016-10-01

This work shows an effective methodology to characterize the creep-recovery behavior of silicones before their application in podiatry. The aim is to characterize, model and compare the creep-recovery properties of different types of silicone used in podiatry orthotics. Creep-recovery phenomena of silicones used in podiatry orthotics is characterized by dynamic mechanical analysis (DMA). Silicones provided by Herbitas are compared by observing their viscoelastic properties by Functional Data Analysis (FDA) and nonlinear regression. The relationship between strain and time is modeled by fixed and mixed effects nonlinear regression to compare easily and intuitively podiatry silicones. Functional ANOVA and Kohlrausch-Willians-Watts (KWW) model with fixed and mixed effects allows us to compare different silicones observing the values of fitting parameters and their physical meaning. The differences between silicones are related to the variations of breadth of creep-recovery time distribution and instantaneous deformation-permanent strain. Nevertheless, the mean creep-relaxation time is the same for all the studied silicones. Silicones used in palliative orthoses have higher instantaneous deformation-permanent strain and narrower creep-recovery distribution. The proposed methodology based on DMA, FDA and nonlinear regression is an useful tool to characterize and choose the proper silicone for each podiatry application according to their viscoelastic properties. Copyright © 2016 Elsevier Ltd. All rights reserved.

A Critical Analysis of the Conventionally Employed Creep Lifing Methods.

Science.gov (United States)

Abdallah, Zakaria; Gray, Veronica; Whittaker, Mark; Perkins, Karen

2014-04-29

The deformation of structural alloys presents problems for power plants and aerospace applications due to the demand for elevated temperatures for higher efficiencies and reductions in greenhouse gas emissions. The materials used in such applications experience harsh environments which may lead to deformation and failure of critical components. To avoid such catastrophic failures and also increase efficiency, future designs must utilise novel/improved alloy systems with enhanced temperature capability. In recognising this issue, a detailed understanding of creep is essential for the success of these designs by ensuring components do not experience excessive deformation which may ultimately lead to failure. To achieve this, a variety of parametric methods have been developed to quantify creep and creep fracture in high temperature applications. This study reviews a number of well-known traditionally employed creep lifing methods with some more recent approaches also included. The first section of this paper focuses on predicting the long-term creep rupture properties which is an area of interest for the power generation sector. The second section looks at pre-defined strains and the re-production of full creep curves based on available data which is pertinent to the aerospace industry where components are replaced before failure.

Low-temperature creep of austenitic stainless steels

Science.gov (United States)

Reed, R. P.; Walsh, R. P.

2017-09-01

Plastic deformation under constant load (creep) in austenitic stainless steels has been measured at temperatures ranging from 4 K to room temperature. Low-temperature creep data taken from past and unreported austenitic stainless steel studies are analyzed and reviewed. Creep at cryogenic temperatures of common austenitic steels, such as AISI 304, 310 316, and nitrogen-strengthened steels, such as 304HN and 3116LN, are included. Analyses suggests that logarithmic creep (creep strain dependent on the log of test time) best describe austenitic stainless steel behavior in the secondary creep stage and that the slope of creep strain versus log time is dependent on the applied stress/yield strength ratio. The role of cold work, strain-induced martensitic transformations, and stacking fault energy on low-temperature creep behavior is discussed. The engineering significance of creep on cryogenic structures is discussed in terms of the total creep strain under constant load over their operational lifetime at allowable stress levels.

A study on stress analysis of small punch-creep test and its experimental correlations with uniaxial-creep test

International Nuclear Information System (INIS)

Lee, Song In; Baek, Seoung Se; Kwon, Il Hyun; Yu, Hyo Sun

2002-01-01

A basic research was performed to ensure the usefulness of Small Punch-creep(SP-creep) test for residual life evaluation of heat resistant components effectively. This paper presents analytical results of initial stress and strain distributions in SP specimen caused by constant loading for SP-creep test and its experimental correlations with uniaxial creep(Ten-creep) test on 9CrlMoVNb steel. It was shown that the initial maximum equivalent stress, σ eq · max from FE analysis was correlated with steady-state equivalent creep strain rate, ε qf-ss , rupture time, t r , activation energy, Q and Larson-Miller parameter, LMP during SP-creep deformation. The simple correlation laws, σ SP - σ TEN , P SP -σ TEN and Q SP -Q TEN adopted to established a quantitative correlation between SP-creep and Ten-creep test data. Especially, the activation energy obtained from SP-creep test is linearly related to that from Ten-creep test at 650 deg. C as follows : Q SP-P =1.37 Q TEN , Q SP-σ =1.53 Q TEN

Muscle Activity Adaptations to Spinal Tissue Creep in the Presence of Muscle Fatigue

Science.gov (United States)

Nougarou, François

2016-01-01

Aim The aim of this study was to identify adaptations in muscle activity distribution to spinal tissue creep in presence of muscle fatigue. Methods Twenty-three healthy participants performed a fatigue task before and after 30 minutes of passive spinal tissue deformation in flexion. Right and left erector spinae activity was recorded using large-arrays surface electromyography (EMG). To characterize muscle activity distribution, dispersion was used. During the fatigue task, EMG amplitude root mean square (RMS), median frequency and dispersion in x- and y-axis were compared before and after spinal creep. Results Important fatigue-related changes in EMG median frequency were observed during muscle fatigue. Median frequency values showed a significant main creep effect, with lower median frequency values on the left side under the creep condition (p≤0.0001). A significant main creep effect on RMS values was also observed as RMS values were higher after creep deformation on the right side (p = 0.014); a similar tendency, although not significant, was observed on the left side (p = 0.06). A significant creep effects for x-axis dispersion values was observed, with higher dispersion values following the deformation protocol on the left side (p≤0.001). Regarding y-axis dispersion values, a significant creep x fatigue interaction effect was observed on the left side (p = 0.016); a similar tendency, although not significant, was observed on the right side (p = 0.08). Conclusion Combined muscle fatigue and creep deformation of spinal tissues led to changes in muscle activity amplitude, frequency domain and distribution. PMID:26866911

Creep buckling analysis of shells

International Nuclear Information System (INIS)

Stone, C.M.; Nickell, R.E.

1977-01-01

The current study was conducted in an effort to determine the degree of conservatism or lack of conservatism in current ASME design rules concerning time-dependent (creep) buckling. In the course of this investigation, certain observations were made concerning the numerical solution of creep buckling problems. It was demonstrated that a nonlinear finite element code could be used to solve the time-dependent buckling problem. A direct method of solution was presented which proved to be computationally efficient and provided answers which agreed very well with available analytical solutions. It was observed that the calculated buckling times could vary widely for small errors in computed displacements. The presence of high creep strain rates contributed to the prediction of early buckling times when calculated during the primary creep stage. The predicted time estimates were found to increase with time until the secondary stage was reached and the estimates approached the critical times predicted without primary creep. It can be concluded, therefore, that for most nuclear piping components, whose primary creep stage is small compared to the secondary stage, the effect of primary creep is negligible and can be omitted from the calculations. In an evaluation of the past and current ASME design rules for time-dependent, load controlled buckling, it was concluded that current use of design load safety factors is not equivalent to a safety factor of ten on service life for low creep exponents

A phenomenological theory of transient creep

International Nuclear Information System (INIS)

Ajaja, O.; Ardell, A.J.

1979-01-01

A new creep theory is proposed which takes into account the strain generated during the annihilation of dislocations. This contribution is found to be very significant when recovery is appreciable, and is mainly responsible for the decreasing creep rate associated with the normal primary creep of class II materials. The theory provides excellent semiquantitative rationalization for the types of creep curves presented in the preceding paper. In particular, the theory predicts a change in the shape of the primary creep curve from normal to inverted as recovery becomes less important, i.e. as the applied stress and/or temperature decrease(s). It also predicts a minimum creep rate under certain circumstances, hence pseudo-tertiary behaviour. These different types of creep curves are predicted even though the net dislocation density decreases monotonically with time in all cases. Qualitative rationalization is presented for the inverted transient which always follows a stress drop in class II materials, as well as for the inverted primary and sigmoidal creep behaviour of class I solid solutions. (author)

Creep rupture behavior of welded Grade 91 steel

Energy Technology Data Exchange (ETDEWEB)

Shrestha, Triratna [Department of Chemical and Materials Engineering, University of Idaho, Moscow, ID 83844 (United States); Basirat, Mehdi [Department of Mechanical Engineering, University of Idaho, Moscow, ID 83844 (United States); Alsagabi, Sultan; Sittiho, Anumat [Department of Chemical and Materials Engineering, University of Idaho, Moscow, ID 83844 (United States); Charit, Indrajit, E-mail: icharit@uidaho.edu [Department of Chemical and Materials Engineering, University of Idaho, Moscow, ID 83844 (United States); Potirniche, Gabriel P. [Department of Mechanical Engineering, University of Idaho, Moscow, ID 83844 (United States)

2016-07-04

Creep rupture behavior of fusion welded Grade 91 steel was studied in the temperature range of 600 – 700 °C and at stresses of 50–200 MPa. The creep data were analyzed in terms of the Monkman-Grant relation and Larson-Miller parameter. The creep damage tolerance factor was used to identify the origin of creep damage. The creep damage was identified as the void growth in combination with microstructural degradation. The fracture surface morphology of the ruptured specimens was studied by scanning electron microscopy and deformed microstructure examined by transmission electron microscopy, to further elucidate the rupture mechanisms.

Nanogranular origin of concrete creep.

Science.gov (United States)

Vandamme, Matthieu; Ulm, Franz-Josef

2009-06-30

Concrete, the solid that forms at room temperature from mixing Portland cement with water, sand, and aggregates, suffers from time-dependent deformation under load. This creep occurs at a rate that deteriorates the durability and truncates the lifespan of concrete structures. However, despite decades of research, the origin of concrete creep remains unknown. Here, we measure the in situ creep behavior of calcium-silicate-hydrates (C-S-H), the nano-meter sized particles that form the fundamental building block of Portland cement concrete. We show that C-S-H exhibits a logarithmic creep that depends only on the packing of 3 structurally distinct but compositionally similar C-S-H forms: low density, high density, ultra-high density. We demonstrate that the creep rate ( approximately 1/t) is likely due to the rearrangement of nanoscale particles around limit packing densities following the free-volume dynamics theory of granular physics. These findings could lead to a new basis for nanoengineering concrete materials and structures with minimal creep rates monitored by packing density distributions of nanoscale particles, and predicted by nanoscale creep measurements in some minute time, which are as exact as macroscopic creep tests carried out over years.

Seismic Creep, USA Images

Data.gov (United States)

National Oceanic and Atmospheric Administration, Department of Commerce — Seismic creep is the constant or periodic movement on a fault as contrasted with the sudden rupture associated with an earthquake. It is a usually slow deformation...

Correlation between microstructure and the creep behaviour at high temperature of Alloy 800 H

International Nuclear Information System (INIS)

Spiradek, K.; Degischer, H.P.; Lahodny, H.

1989-01-01

A systematic metallographic study was performed to identify the nature of the microstructural changes occurring during high temperature creep deformation of Alloy 800 H. Creep tests were carried out at 800 deg. C under constant load conditions corresponding to the initial stresses between 25 and 80 MPa. Some tests were interrupted after certain elongations to provide the samples for electron microscopy. Emphasis was put on the creep periods relevant to design where only a few per cent of deformation are tolerable. The influence of the initial material conditions on the creep behaviour was examined. Variations of the initial microstructures were achieved by different solution treatments (980/1250) deg. C, preageing at 800 deg. C (0/6400) h and cold deformation up to 10% followed by ageing at 800 deg. C. The results of the microstructural examinations were correlated with the creep curves that provide a basis for identification of the creep mechanisms operating at the test conditions. (author). 14 refs, 17 figs

Creep and relaxation behavior of Inconel-617

International Nuclear Information System (INIS)

Osthoff, W.; Ennis, P.J.; Nickel, H.; Schuster, H.

1984-01-01

The static and dynamic creep behavior of Inconel alloy 617 has been determined in constant load creep tests, relaxation tests, and stress reduction tests in the temperature range 1023 to 1273 K. The results have been interpreted using the internal stress concept: The dependence of the internal stress on the applied stress and test temperature was determined. In a few experiments, the influence of cold deformation prior to the creep test on the magnitude of the internal stress was also investigated. It was found that the experimentally observed relaxation behavior could be more satisfactorily described using the Norton creep equation modified by incorporation of the internal stress than by the conventional Norton creep equation

Relaxation of Shot-Peened Residual Stresses Under Creep Loading (Preprint)

National Research Council Canada - National Science Library

Buchanan, Dennis J; John, Reji; Brockman, Robert A

2008-01-01

... loading, near and above the monotonic yield strength of IN100. The model incorporates the dominant creep deformation mechanism, coupling between the creep and plasticity models, and effects of prior plastic strain...

On the spherical nanoindentation creep of metallic glassy thin films at room temperature

Energy Technology Data Exchange (ETDEWEB)

Zhang, T.H.; Ye, J.H. [Institution of Micro/Nano-Mechanical Testing Technology & Application, College of Mechanical Engineering, Zhejiang University of Technology, Hangzhou 310014 (China); Feng, Y.H. [State Key Laboratory of Nonlinear Mechanics (LNM), Institute of Mechanics, Chinese Academy of Sciences, Beijing 100190 (China); Ma, Y., E-mail: may@zjut.edu.cn [Institution of Micro/Nano-Mechanical Testing Technology & Application, College of Mechanical Engineering, Zhejiang University of Technology, Hangzhou 310014 (China)

2017-02-08

Metallic glassy thin films with eight kind of compositions were successfully prepared on Si substrate by magnetron sputtering. The room-temperature creep tests were performed at plastic regions for each sample relying on spherical nanoindetation. The creep deformations were studied by recording the total creep displacement and strain after 2000 s holding. More pronounced creep deformation was observed in the sample with lower glass transition temperature (T{sub g}). Strain rate sensitivity (SRS) was then calculated from the steady-state creep and exhibited a negative correlation with increasing T{sub g}. It is suggested that creep mechanism of the nano-sized metallic glass was T{sub g}-dependent, according to the demarcation of SRS values. Based on the obtained SRS, shear transformation zone (STZ) size in each sample could be estimated. The results indicated that an STZ involves about 25–60 atoms for the employed eight samples and is strongly tied to T{sub g}. The characteristic of STZ size in metallic glassy thin films was discussed in terms of applied method and deformation modes.

The influence of the grain boundary structure on diffusional creep

International Nuclear Information System (INIS)

Thorsen, P.A.

1998-05-01

An experiment was carried out to quantify the deformation in the diffusional creep domain. It was found that material had indisputably been deposited at grain boundaries in tension. A characterisation of 131 boundaries in terms of their misorientation was carried out and this was correlated to the observed deformation. Twin boundaries below a certain limit of deviation from an exact twin misorientation were totally inactive in the deformation. A large qualitative difference was found in the way general boundaries take part in the deformation. The experiments have taken place at Materials Research Department, Risoe National Laboratory at Roskilde. The present thesis has been submitted in partial fulfillment of the requirements for the Ph.D. degree in physics at the Niels Bohr Institute, University of Copenhagen. Besides the results of the creep experiment the thesis contains a description of the theoretical background to diffusional creep models. Also, the results from an investigation of helium bubble formation in an irradiated copper sample is included. (au)

Creep Behavior of Porous Supports in Metal-support Solid Oxide Fuel Cells

DEFF Research Database (Denmark)

Boccaccini, Dino; Frandsen, Henrik Lund; Blennow Tullmar, Peter

2013-01-01

Creep is the inelastic deformation of a material at high temperatures over long periods of time. It can be defined as timedependent deformation at absolute temperatures greater than one half the absolute melting. Creep resistance is a key parameter for high temperature steel components, e.g. SOFC...... metal supports, where high corrosion resistance is a major design requirement. The four variables affecting creep rate are strain, time, temperature, and stress level and make creep difficult to quantify. In this work, the creep parameters of a SOFC metal support have been determined for the first time...... by means of a thermo mechanical analyzer (TMA) for stresses in the range of 1-17 MPa and temperatures between 650-750 °C. The creep parameters of Crofer® 22 APU were also acquired and compared with values obtained from literature to validate the technique....

Complex finite element sensitivity method for creep analysis

International Nuclear Information System (INIS)

Gomez-Farias, Armando; Montoya, Arturo; Millwater, Harry

2015-01-01

The complex finite element method (ZFEM) has been extended to perform sensitivity analysis for mechanical and structural systems undergoing creep deformation. ZFEM uses a complex finite element formulation to provide shape, material, and loading derivatives of the system response, providing an insight into the essential factors which control the behavior of the system as a function of time. A complex variable-based quadrilateral user element (UEL) subroutine implementing the power law creep constitutive formulation was incorporated within the Abaqus commercial finite element software. The results of the complex finite element computations were verified by comparing them to the reference solution for the steady-state creep problem of a thick-walled cylinder in the power law creep range. A practical application of the ZFEM implementation to creep deformation analysis is the calculation of the skeletal point of a notched bar test from a single ZFEM run. In contrast, the standard finite element procedure requires multiple runs. The value of the skeletal point is that it identifies the location where the stress state is accurate, regardless of the certainty of the creep material properties. - Highlights: • A novel finite element sensitivity method (ZFEM) for creep was introduced. • ZFEM has the capability to calculate accurate partial derivatives. • ZFEM can be used for identification of the skeletal point of creep structures. • ZFEM can be easily implemented in a commercial software, e.g. Abaqus. • ZFEM results were shown to be in excellent agreement with analytical solutions

Low-temperature creep of nanocrystalline titanium(IV) oxide

Energy Technology Data Exchange (ETDEWEB)

Hahn, H.; Averback, R.S. (Dept. of Materials Sceince and Engineering, Univ. of Illinois, Urbana, IL (United States))

1991-11-01

This paper reports that nanocrystalline TiO[sub 2] with densities higher than 99% of rutile has been deformed in compression without fracture at temperatures between 600[degrees] and 800[degrees] C. The total strains exceed 0.6 at strain rates as high as 10[sup [minus]3] s[sup [minus]1]. The original average grain size of 40 nm increases during the creep deformation to final values in the range of 120 to 1000 nm depending on the temperature and total deformation. The stress exponent of the strain rate, n, is approximately 3 and the grain size dependence is d[sup [minus]q] with q in the range of 1 to 1.5. It is concluded that the creep deformation occurs by an interface reaction controlled mechanism.

Orthotropic creep in polyethylene glycol impregnated archaeological oak from the Vasa ship - Results of creep experiments in a museum-like climate

Science.gov (United States)

Vorobyev, Alexey; van Dijk, Nico P.; Kristofer Gamstedt, E.

2018-02-01

Creep in archaeological oak samples and planks from the Vasa ship impregnated with polyethylene glycol (PEG) has been studied in museum-like climate. Creep studies of duration up to three years have been performed in nearly constant relative humidity and temperature of the controlled museum climate. Cubic samples were subjected to compressive creep tests in all orthotropic directions. Additionally, the creep behaviour of planks with and without PEG and of recent oak was tested in four-point bending. The experimental results have been summarised and also compared with reference results from recent oak wood. The effect of variable ambient conditions on creep and mass changes is discussed. The experimental results of creep in the longitudinal direction showed deformations even for the low stresses. There is relatively much more scatter in creep behaviour, and not all samples showed linear viscoelastic response. The creep in radial and tangential directions of the cubes and the plank samples showed a strong dependency on the ambient conditions. Some samples showed expansion for decreasing moisture content, possibly caused by the thermal expansion of the PEG component. For the planks, increasing creep deformation was observed induced by changing ambient conditions. Such behaviour may be related to e.g. oscillations in ambient conditions and presence of PEG in the wood cell wall and cell lumen. The behaviour of PEG archaeological wood depends on the level of deterioration that occurred over centuries. However, although the findings presented here apply to this specific case, they provide a unique view on such wood.

On the Volterra integral equation relating creep and relaxation

International Nuclear Information System (INIS)

Anderssen, R S; De Hoog, F R; Davies, A R

2008-01-01

The evolving stress–strain response of a material to an applied deformation is causal. If the current response depends on the earlier history of the stress–strain dynamics of the material (i.e. the material has memory), then Volterra integral equations become the natural framework within which to model the response. For viscoelastic materials, when the response is linear, the dual linear Boltzmann causal integral equations are the appropriate model. The choice of one rather than the other depends on whether the applied deformation is a stress or a strain, and the associated response is, respectively, a creep or a relaxation. The duality between creep and relaxation is known explicitly and is referred to as the 'interconversion equation'. Rheologically, its importance relates to the fact that it allows the creep to be determined from knowledge of the relaxation and vice versa. Computationally, it has been known for some time that the recovery of the relaxation from the creep is more problematic than the creep from the relaxation. Recent research, using discrete models for the creep and relaxation, has confirmed that this is an essential feature of interconversion. In this paper, the corresponding result is generalized for continuous models of the creep and relaxation

Deformation rates in northern Cascadia consistent with slow updip propagation of deep interseismic creep

Science.gov (United States)

Bruhat, Lucile; Segall, Paul

2017-10-01

Interpretations of interseismic slip deficit on the northern Cascadia megathrust are complicated by an enigmatic `gap' between the downdip limit of the locked region, inferred from kinematic inversions of deformation rates, and the top of the episodic tremor and slip (ETS) zone. Recent inversions of global positioning system (GPS) and tide gauge/leveling data for shear stress rates acting on the megathrust found a ˜21 km locking depth with a steep slip-rate gradient at its base is required to fit the data. Previous studies have assumed the depth distribution of interseismic slip rate to be time invariant; however, steep slip-rate gradients could also result from the updip propagation of slip into the locked region. This study explores models where interseismic slip penetrates up into the locked zone. We consider the creeping region, corresponding to the gap and the ETS zone, as a quasi-static crack driven by the plate velocity at its downdip end. We derive a simple model that allows for crack propagation over time, and provides analytical expressions for stress drop within the crack, slip and slip rate on the fault. It is convenient to expand the non-singular slip-rate distribution in a sum of Chebyshev polynomials. Estimation of the polynomial coefficients is underdetermined, yet provides a useful way of testing particular solutions and provides bounds on the updip propagation rate. When applied to the deformation rates in northern Cascadia, best-fitting models reveal that a very slow updip propagation, between 30 and 120 m yr-1 along the fault, could explain the steep slip-rate profile, needed to fit the data. This work provides a new tool for estimating interseismic slip rates, between purely kinematic inversions and full physics-based modeling, allowing for the possibility for updip expansion of the creeping zone.

Finite Element Modeling of Thermo Creep Processes Using Runge-Kutta Method

Directory of Open Access Journals (Sweden)

Yu. I. Dimitrienko

2015-01-01

Full Text Available Thermo creep deformations for most heat-resistant alloys, as a rule, nonlinearly depend on stresses and are practically non- reversible. Therefore, to calculate the properties of these materials the theory of plastic flow is most widely used. Finite-element computations of a stress-strain state of structures with account of thermo creep deformations up to now are performed using main commercial software, including ANSYS package. However, in most cases to solve nonlinear creep equations, one should apply explicit or implicit methods based on the Euler method of approximation of time-derivatives. The Euler method is sufficiently efficient in terms of random access memory in computations, however this method is cumbersome in computation time and does not always provide a required accuracy for creep deformation computations.The paper offers a finite-element algorithm to solve a three-dimensional problem of thermo creep based on the Runge-Kutta finite-difference schemes of different orders with respect to time. It shows a numerical test example to solve the problem on the thermo creep of a beam under tensile loading. The computed results demonstrate that using the Runge-Kutta method with increasing accuracy order allows us to obtain a more accurate solution (with increasing accuracy order by 1 a relative error decreases, approximately, by an order too. The developed algorithm proves to be efficient enough and can be recommended for solving the more complicated problems of thermo creep of structures.

Creep in commercially pure metals

International Nuclear Information System (INIS)

Nabarro, F.R.N.

2006-01-01

The creep of commercially pure polycrystalline metals under constant stress has four stages: a virtually instantaneous extension, decelerating Andrade β creep, almost steady-state Andrade κ creep, and an acceleration towards failure. Little is known about the first stage, and the fourth stage has been extensively reviewed elsewhere. The limited experimental evidence on the physical mechanism of the second stage is reviewed and a critical discussion is given of various theories of this stage. The dependence of strain rate on stress in the third, steady-state, period seems to fall into two regimes, a power law with an exponent of about 4-5, and a rather closely exponential law. The limits of the parameters within which a simple theory of the exponential dependence can be expected to be valid are discussed, and found to be compatible with experiments. Theories of the power-law dependence are discussed, and, appear to be unconvincing. The theoretical models do not relate closely to the metallographic and other physical observations. In view of the weakness of theory, experiments which may indicate the physical processes dominant in steady-state creep are reviewed. It is usually not clear whether they pertain to the power-law or the exponential regime. While the theories all assume that most of the deformation occurs homogeneously within the grains, most experimental observations point strongly to a large deformation at or close to the grain boundaries. However, a detailed study of dislocation processes in a single grain of polycrystalline foil strained in the electron microscope shows that most of the observed strain can be accounted for by the motion of single dislocations through the subgrain structure. There is no clear reconciliation of these two sets of observations. Grain-boundary sliding cannot occur without intragranular deformation. One or other process may dominate the overall deformation; the geometrically dominant process may not be the rate

Characterization of creep properties and creep textures in pure aluminum processed by equal-channel angular pressing

International Nuclear Information System (INIS)

Kawasaki, Megumi; Beyerlein, Irene J.; Vogel, Sven C.; Langdon, Terence G.

2008-01-01

High-purity aluminum was processed by equal-channel angular pressing (ECAP) and then tested under creep conditions at 473 K. The results show conventional power-law creep with a stress exponent of n = 5 which is consistent with an intragranular dislocation process involving the glide and climb of dislocations. It is demonstrated that diffusion creep is not important in these tests because the ultrafine grains produced by ECAP are not stable at this temperature. Texture measurements were undertaken using the high-pressure preferred orientation neutron time-of-flight diffractometer and they reveal significant differences in the evolution of texture during creep in pressed and unpressed specimens. These experimental measurements of texture are in excellent agreement with theoretical textures predicted using a visco-plastic self-consistent model that limits deformation to plastic slip. The calculations provide additional confirmation that creep occurs through an intragranular dislocation process

Creep deformation behavior at long-term in P23/T23 steels

Energy Technology Data Exchange (ETDEWEB)

Sawada, K.; Tabuchi, M.; Kimura, K. [National Institute for Materials Science (Japan)

2008-07-01

Creep behavior of ASME P23/T23 steels was investigated and analyzed, focusing on creep strength degradation at long-term. Creep rupture strength at 625 C and 650 C dropped at long-term in both P23 and T23 steels. The stress exponent of minimum creep rate at 625 C and 650 C was 7.8-13 for higher stresses and 3.9-5.3 for lower stresses in the P23/T23 steels. The change of stress exponent with stress levels was consistent with the drop in creep rupture strength at long-term. The Monkman-Grant rule was confirmed in the range examined in P23 steel, while the data points deviated from the rule at long-term in the case of T23 steel. The creep ductility of P23 steel was high over a wide stress and temperature range. On the other hand, in T23 steel, creep ductility at 625 C and 650 C decreased as time to rupture increased. The change in ductility may cause the deviation from the Monkman-Grant rule. Fracture mode changed from transgranular to intergranular fracture in the long-term at 625 C and 650 C. (orig.)

Slow creep in soft granular packings.

Science.gov (United States)

Srivastava, Ishan; Fisher, Timothy S

2017-05-14

Transient creep mechanisms in soft granular packings are studied numerically using a constant pressure and constant stress simulation method. Rapid compression followed by slow dilation is predicted on the basis of a logarithmic creep phenomenon. Characteristic scales of creep strain and time exhibit a power-law dependence on jamming pressure, and they diverge at the jamming point. Microscopic analysis indicates the existence of a correlation between rheology and nonaffine fluctuations. Localized regions of large strain appear during creep and grow in magnitude and size at short times. At long times, the spatial structure of highly correlated local deformation becomes time-invariant. Finally, a microscale connection between local rheology and local fluctuations is demonstrated in the form of a linear scaling between granular fluidity and nonaffine velocity.

Study on sand particles creep model and open pit mine landslide mechanism caused by sand fatigue liquefaction

Science.gov (United States)

Du, Dong-Ning; Wang, Lai-Gui; Zhang, Xiang-Dong; Zhang, Shu-Kun

2017-06-01

The sand particles in the sand - rock composite slope of the open pit mine occurs creep deformation and fatigue liquefaction under the action of vehicle load vibration and hydraulic gradient, which causes landslide geological disasters and it destroys the surface environment. To reveal the mechanism, a mechanics model based on the model considering the soil structural change with a new “plastic hinge” element is developed, to improve its constitutive and creep curve equations. Data from sand creep experiments are used to identify the parameters in the model and to validate the model. The results show that the mechanical model can describe the rotation progress between the sand particles, disclose the negative acceleration creep deformation stage during the third phase, and require fewer parameters while maintaining accuracy. It provides a new creep model considering rotation to analyze sand creep mechanism, which provides a theoretical basis for revealing the open pit mine landslide mechanism induced by creep deformation and fatigue liquefaction of sandy soil.

Critical view on the creep modelling procedures

Czech Academy of Sciences Publication Activity Database

Kloc, Luboš

2015-01-01

Roč. 128, č. 4 (2015), s. 540-542 ISSN 0587-4246. [ISPMA 2014 - International Symposium on Physics of Materials /13./. Praha, 31.08.2014-04.09.2014] R&D Projects: GA MPO FR-TI4/406 Institutional support: RVO:68081723 Keywords : Creep * Creep deformation * Grain boundaries * Phase structure * Strain rate Subject RIV: JJ - Other Materials Impact factor: 0.525, year: 2015

Atomistic simulations of diffusional creep in a nanocrystalline body-centered cubic material

International Nuclear Information System (INIS)

Millett, Paul C.; Desai, Tapan; Yamakov, Vesselin; Wolf, Dieter

2008-01-01

Molecular dynamics (MD) simulations are used to study diffusion-accommodated creep deformation in nanocrystalline molybdenum, a body-centered cubic metal. In our simulations, the microstructures are subjected to constant-stress loading at levels below the dislocation nucleation threshold and at high temperatures (i.e., T > 0.75T melt ), thereby ensuring that the overall deformation is indeed attributable to atomic self-diffusion. The initial microstructures were designed to consist of hexagonally shaped columnar grains bounded by high-energy asymmetric tilt grain boundaries (GBs). Remarkably the creep rates, which exhibit a double-exponential dependence on temperature and a double power-law dependence on grain size, indicate that both GB diffusion in the form of Coble creep and lattice diffusion in the form of Nabarro-Herring creep contribute to the overall deformation. For the first time in an MD simulation, we observe the formation and emission of vacancies from high-angle GBs into the grain interiors, thus enabling bulk diffusion

Prediction of macroscopic and local stress-strain behaviors of perforated plates under primary and secondary creep conditions

International Nuclear Information System (INIS)

Igari, Toshihide; Tokiyoshi, Takumi; Mizokami, Yorikata

2000-01-01

Prediction methods of macroscopic and local creep behaviors of perforated plates are examined in order to apply these methods to the structural design of perforated structures such as heat exchangers used in elevated temperatures. Both primary and secondary creeps are considered for predicting macroscopic and local creep behaviors of perorated plates which are made of actual structural materials. Both uniaxial and multiaxial loading of perforated plates are taken into consideration. The concept of effective stress is applied to the prediction of macroscopic creep behaviors of perforated plates, and the predicted results are compared with the numerical results by FEM for the unit section of perorated plated under creep, in order to confirm the propriety of the proposed method. Based on the idea that stress exponents in creep equations govern the stress distribution of perforated plates, a modified Neuber's rule is used for predicting local stress and strain concentrations. The propriety of this prediction method is shown through a comparison of the prediction with the numerical results by FEM for the unit section of perforated plates under creep, and experimental results by the Moire method. (author)

The influence of the grain boundary structure on diffusional creep

Energy Technology Data Exchange (ETDEWEB)

Thorsen, P.A

1998-05-01

An experiment was carried out to quantify the deformation in the diffusional creep domain. It was found that material had indisputably been deposited at grain boundaries in tension. A characterisation of 131 boundaries in terms of their misorientation was carried out and this was correlated to the observed deformation. Twin boundaries below a certain limit of deviation from an exact twin misorientation were totally inactive in the deformation. A large qualitative difference was found in the way general boundaries take part in the deformation. The experiments have taken place at Materials Research Department, Risoe National Laboratory at Roskilde. The present thesis has been submitted in partial fulfillment of the requirements for the Ph.D. degree in physics at the Niels Bohr Institute, University of Copenhagen. Besides the results of the creep experiment the thesis contains a description of the theoretical background to diffusional creep models. Also, the results from an investigation of helium bubble formation in an irradiated copper sample is included. (au) 7 tabs., 56 ills., 75 refs.

NIRVANA, a high-temperature creep model for Zircaloy fuel sheathing

International Nuclear Information System (INIS)

Sills, H.E.; Holt, R.A.

1979-05-01

We have developed a multi-component model to describe the transient plastic deformation of Zircaloy fuel sheathing during high-temperature transients. From deformation maps we identify three deformation mechanisms which, in principle, occur in all three phase fields of Zircaloy (α, α+β, β): diffusional creep, dislocation creep, and athermal strian. A strain component occurring during the α → β transformation is also identified. Microstructural changes which alter deformation rates -grain structure, recrystallization, phase transformation -are accounted for. The individual components of the model represent known metallurgical phenomena. The combined model gives excellent agreement with transient test data from 700-1800 K, a range of heating rates from 0-100 K.s -1 , and a range of strain rates from 10 -5 to 10 -1 .s -1 . To enable comparison with available data the transient creep model was combined with an axially uniform, thin-walled tube representation having anisotropic material properties. The resulting computer code, NIRVANA provides facilities for simulating uniaxial and biaxial tube tests over specified stress/temperature histories. (author)

A comprising steady-state creep model for the austenitic AISI 316 L(N) steel

International Nuclear Information System (INIS)

Rieth, Michael

2007-01-01

Low-stress creep data of a recently finished special long-term program now allows for much better long-term predictions of the ITER related material 316 L(N) and also enables deformation modeling for a broader stress range. The present work focuses mainly on the set-up of a steady-state creep model with help of well-known rate-equations for different deformation mechanisms. In addition, the impact of microstructure changes and precipitation formation on steady-state creep is studied. The resulting creep model consists of a summation of contributions for diffusion creep, power-law creep, and power-law breakdown. The final creep model agrees well with experimental data for temperatures between 550 and 750 deg C and for shear stresses above 30 MPa. The most important finding of this work is that for very low stresses the model predicts far higher creep rates than can be extrapolated from tests performed at the usual stress range of experimental programs

The microstructure and creep behavior of cold rolled udimet 188 sheet.

Science.gov (United States)

Boehlert, C J; Longanbach, S C

2011-06-01

Udimet 188 was subjected to thermomechanical processing (TMP) in an attempt to understand the effects of cold-rolling deformation on the microstructure and tensile-creep behavior. Commercially available sheet was cold rolled to varying amounts of deformation (between 5-35% reduction in sheet thickness) followed by a solution treatment at 1,464 K (1,191 °C) for 1 h and subsequent air cooling. This sequence was repeated four times to induce a high-volume fraction of low-energy grain boundaries. The resultant microstructure was characterized using electron backscattered diffraction. The effect of the TMP treatment on the high-temperature [1,033-1,088 K (760-815 °C)] creep behavior was evaluated. The measured creep stress exponents (6.0-6.8) suggested that dislocation creep was dominant at 1,033 K (760 °C) for stresses ranging between 100-220 MPa. For stresses ranging between 25-100 MPa at 1,033 K (760 °C), the stress exponents (2.3-2.8) suggested grain boundary sliding was dominant. A significant amount of grain boundary cracking was observed both on the surface and subsurface of deformed samples. To assess the mechanisms of crack nucleation, in situ scanning electron microscopy was performed during the elevated-temperature tensile-creep deformation. Cracking occurred preferentially along general high-angle grain boundaries (GHAB) and less than 25% of the cracks were found on low-angle grain boundaries (LAB) and coincident site lattice boundaries (CSLB). Creep rupture experiments were performed at T = 1,088 K (815 °C) and σ = 165 MPa and the greatest average time-to-rupture was exhibited by the TMP sheet with the greatest fraction of LAB+CSLB. However, a clear correlation was not exhibited between the grain boundary character distribution and the minimum creep rates. The findings of this work suggest that although grain boundary engineering may be possible for this alloy, simply relating the fraction of grain boundary types to the creep resistance is not

A Model for Creep and Creep Damage in the γ-Titanium Aluminide Ti-45Al-2Mn-2Nb.

Science.gov (United States)

Harrison, William; Abdallah, Zakaria; Whittaker, Mark

2014-03-14

Gamma titanium aluminides (γ-TiAl) display significantly improved high temperature mechanical properties over conventional titanium alloys. Due to their low densities, these alloys are increasingly becoming strong candidates to replace nickel-base superalloys in future gas turbine aeroengine components. To determine the safe operating life of such components, a good understanding of their creep properties is essential. Of particular importance to gas turbine component design is the ability to accurately predict the rate of accumulation of creep strain to ensure that excessive deformation does not occur during the component's service life and to quantify the effects of creep on fatigue life. The theta (θ) projection technique is an illustrative example of a creep curve method which has, in this paper, been utilised to accurately represent the creep behaviour of the γ-TiAl alloy Ti -45Al-2Mn-2Nb. Furthermore, a continuum damage approach based on the θ-projection method has also been used to represent tertiary creep damage and accurately predict creep rupture.

Transitions in creep mechanisms and creep anisotropy in Zr-1Nb-1Sn-0.2Fe sheet

International Nuclear Information System (INIS)

Murty, K.L.; Ravi, J.; Wiratmo

1995-01-01

The creep characteristics of a Zr-1Nb-1Sn-0.2Fe alloy sheet were investigated at temperatures from 773 to 923K and at stresses ranging from 9 to 150MPa along both the rolling and transverse directions. Transitions in creep mechansims are noted, with diffusional viscous creep at low stresses, viscous-glide-controlled microcreep in the intermediate stress regime and the climb of edge dislocations at high stresses. The creep anisotropy decreases with a decrease in the stress exponent and the creep rates differ by only 30% in the viscous creep regime, while an order-of-magnitude difference is noted at high stresses. The solute-strengthening effect of Nb addition is evident in the stress regime where appropriate data are available. These transitions in creep mechansims clearly reveal the dangers in blind extrapolation of short-term high stress data to low stresses and long times relevant to in-reactor conditions. The creep behavior of these materials is similar to that noted in Class I alloys, while the transitions in deformation mechanisms in Zircaloy-4 resemble those found in pure metals or Class II alloys with no viscous glide mechanism. ((orig.))

Non-Contact Measurements of Creep Properties of Refractory Materials

Science.gov (United States)

Lee, Jonghyun; Bradshaw, Richard C.; Hyers, Robert W.; Rogers, Jan R.; Rathz, Thomas J.; Wall, James J.; Choo, Hahn; Liaw, Peter

2006-01-01

State-of-the-art technologies for hypersonic aircraft, nuclear electric/thermal propulsion for spacecraft, and more efficient jet engines are driving ever more demanding needs for high-temperature (>2000 C) materials. At such high temperatures, creep rises as one of the most important design factors to be considered. Since conventional measurement techniques for creep resistance are limited to about 17OO0C, a new technique is in demand for higher temperatures. This paper presents a non-contact method using electrostatic levitation (ESL) which is applicable to both metallic and non-metallic materials. The samples were rotated quickly enough to cause creep deformation by centrifugal acceleration. The deformation of the samples was captured with a high speed camera and then the images were analyzed to estimate creep resistance. Finite element analyses were performed and compared to the experiments to verify the new method. Results are presented for niobium and tungsten, representative refractory materials at 2300 C and 2700 C respectively.

Research on high-temperature compression and creep behavior of porous Cu–Ni–Cr alloy for molten carbonate fuel cell anodes

Directory of Open Access Journals (Sweden)

Li W.

2015-06-01

Full Text Available The effect of porosity on high temperature compression and creep behavior of porous Cu alloy for the new molten carbonate fuel cell anodes was examined. Optical microscopy and scanning electron microscopy were used to investigate and analyze the details of the microstructure and surface deformation. Compression creep tests were utilized to evaluate the mechanical properties of the alloy at 650 °C. The compression strength, elastic modulus, and yield stress all increased with the decrease in porosity. Under the same creep stress, the materials with higher porosity exhibited inferior creep resistance and higher steadystate creep rate. The creep behavior has been classified in terms of two stages. The first stage relates to grain rearrangement which results from the destruction of large pores by the applied load. In the second stage, small pores are collapsed by a subsequent sintering process under the load. The main deformation mechanism consists in that several deformation bands generate sequentially under the perpendicular loading, and in these deformation bands the pores are deformed by flattering and collapsing sequentially. On the other hand, the shape of a pore has a severe influence on the creep resistance of the material, i.e. every increase of pore size corresponds to a decrease in creep resistance.

Creep in Topopah Spring Member welded tuff. Yucca Mountain Site Characterization Project

Energy Technology Data Exchange (ETDEWEB)

Martin, R.J. III; Boyd, P.J.; Noel, J.S. [New England Research, Inc., White River Junction, VT (United States); Price, R.H. [Sandia National Labs., Albuquerque, NM (United States)

1995-06-01

A laboratory investigation has been carried out to determine the effects of elevated temperature and stress on the creep deformation of welded tuffs recovered from Busted Butte in the vicinity of Yucca Mountain, Nevada. Water saturated specimens of tuff from thermal/mechanical unit TSw2 were tested in creep at a confining pressure of 5.0 MPa, a pore pressure of 4.5 MPa, and temperatures of 25 and 250 C. At each stress level the load was held constant for a minimum of 2.5 {times} 10{sup 5} seconds and for as long as 1.8 {times} 10{sup 6} seconds. One specimen was tested at a single stress of 80 MPa and a temperature of 250 C. The sample failed after a short time. Subsequent experiments were initiated with an initial differential stress of 50 or 60 MPa; the stress was then increased in 10 MPa increments until failure. The data showed that creep deformation occurred in the form of time-dependent axial and radial strains, particularly beyond 90% of the unconfined, quasi-static fracture strength. There was little dilatancy associated with the deformation of the welded tuff at stresses below 90% of the fracture strength. Insufficient data have been collected in this preliminary study to determine the relationship between temperature, stress, creep deformation to failure, and total failure time at a fixed creep stress.

Creep in Topopah Spring Member welded tuff. Yucca Mountain Site Characterization Project

International Nuclear Information System (INIS)

Martin, R.J. III; Boyd, P.J.; Noel, J.S.; Price, R.H.

1995-06-01

A laboratory investigation has been carried out to determine the effects of elevated temperature and stress on the creep deformation of welded tuffs recovered from Busted Butte in the vicinity of Yucca Mountain, Nevada. Water saturated specimens of tuff from thermal/mechanical unit TSw2 were tested in creep at a confining pressure of 5.0 MPa, a pore pressure of 4.5 MPa, and temperatures of 25 and 250 C. At each stress level the load was held constant for a minimum of 2.5 x 10 5 seconds and for as long as 1.8 x 10 6 seconds. One specimen was tested at a single stress of 80 MPa and a temperature of 250 C. The sample failed after a short time. Subsequent experiments were initiated with an initial differential stress of 50 or 60 MPa; the stress was then increased in 10 MPa increments until failure. The data showed that creep deformation occurred in the form of time-dependent axial and radial strains, particularly beyond 90% of the unconfined, quasi-static fracture strength. There was little dilatancy associated with the deformation of the welded tuff at stresses below 90% of the fracture strength. Insufficient data have been collected in this preliminary study to determine the relationship between temperature, stress, creep deformation to failure, and total failure time at a fixed creep stress

Study on deformation behavior and life evaluation method for SUS304 notched plate under bending creep fatigue loading

International Nuclear Information System (INIS)

Fukuda, Yoshio; Satoh, Yoshimi; Nakamura, Kazuhiro; Takahashi, Yukio; Kuwabara, Kazuo.

1990-01-01

Creep-fatigue tests were carried out on notched plates under cyclic bending loads out of plane at 550degC, and the local strain at the notch-root and micro crack propagation behavior were measured. Then, inelastic analysis was performed for the experiment by using three kinds of constitutive models, such as kinematic hardening, ORNL and Ohno models. From the comparison of the experiment with the results of analysis, the following conclusions were obtained. (1) Creep strain caused at the notch-root during load holding was negligibly small compared with plastic strain, so that the neighborhood of the notch-root is subjected to constrained strain type damage. (2) The strain range at the notch-root can be calculated from the results of elastic-plastic analysis for monotonic loading independent of the constitutive models used, where the cyclic stress-strain relationship was used as the material monotonic deformation property. (3) The mean strain calculated was consistent with the experimental value in case of kinematic hardening or ORNL model, while not in case of Ohno model. (4) A method for predicting the crack initiation life of a notched plate has been proposed on the basis of micro-crack propagation behavior obtained by a fundamental creep-fatigue test. (author)

Predominantly elastic crack growth under combined creep-fatigue cycling

International Nuclear Information System (INIS)

Lloyd, G.J.

1979-01-01

A rationalization of the various observed effects of combined creep-fatigue cycling upon predominantly elastic fatigue-crack propagation in austenitic steel is presented. Existing and new evidence is used to show two main groups of behaviour: (i) material and cycling conditions which lead to modest increases (6-8 times) in the rate of crack growth are associated with relaxation-induced changes in the material deformation characteristics, and (ii) material and cycling conditions severe enough to generate internal fracture damage lead to significant (up to a factor of 30) increases in crack growth rate when compared with fast-cycling crack propagation rates at the same temperature. A working hypothesis is presented to show that the boundary between the two groups occurs when the scale of the nucleated creep damage is of the same magnitude as the crack tip opening displacement. This leads to the possibility of unstable crack advance. Creep crack growth rates are shown to provide an upper bound to creep-fatigue crack growth rates when crack advance is unstable. If the deformation properties only are affected by the creep-fatigue cycling then creep crack growth rates provide a lower bound. The role of intergranular oxygen corrosion in very low frequency crack growth tests is also briefly discussed. (author)

Low stress creep of stainless steel

International Nuclear Information System (INIS)

Crossland, I.G.; Clay, B.D.; Baker, C.

1976-06-01

The creep of 20%Cr, 25%Ni, Nb stainless steel has been examined at temperatures from 675 to 775 0 C at sheer stressed below 13 MPa and grain sizes from 6 to 20μm. The results have indicated that the initial creep rates were linearly dependent upon stress but with a threshold stress below which no creep occurred, i.e. Bingham behaviour; in addition, the creep activation energy at small strains was substantially lower than the lattice self-diffusion value and the initial creep rates were approximately related to the grain size through an inverse cube relation. It has been concluded that at low strains (approaching the initial elastic deflection) the creep mechanism was probably that of grain boundary diffusion creep (Coble, 1963) and this is further supported by the close agreement between the observed and theoretically predicted creep rate values. Steady-state creep rates were not observed; initially the creep rates fell rapidly with strain after which a more gradual decrease occurred. Whilst the creep rate - stress relationship continued to be of a Bingham form, the progressive reduction in creep rate with strain was found to be mainly attributable to an increase in the effective viscosity, threshold stress effects being generally of secondary importance. A model has been proposed which explains the initial creep rates as being due to Cable creep with elastic accommodation at grain boundary particles. At higher strains grain boundary collapse caused by vacancy sinking is accommodated at precipitate particles by plastic deformation of the adjacent matrix material. (author)

Stainless Steel Foil with Improved Creep-Resistance for Use in Primary Surface Recuperators for Gas Turbine Engines

International Nuclear Information System (INIS)

Browning, P.F.; Fitzpatrick, M.; Grubb, J.F.; Klug, R.C.; Maziasz, P.J.; Montague, J.P.; Painter, R.A.; Swindeman, R.W.

1998-01-01

Primary surface recuperators (PSRs) are compact heat-exchangers made from thin-foil type 347 austenitic stainless steel, which boost the efficiency of land-based gas turbine engines. Solar Turbines uses foil folded into a unique corrugated pattern to maximize the primary surface area for efficient heat transfer between hot exhaust gas on one side, and the compressor discharge air on the other side of the foil. Allegheny-Ludlum produces 0.003 - 0.0035 in. thick foil for a range of current turbine engines using PSRs that operate at up to 660 degrees C. Laboratory-scale processing modification experiments recently have demonstrated that dramatic improvements can be achieved in the creep resistance of such typical 347 stainless steel foils. The modified processing enables fine NbC carbide precipitates to develop during creep at 650-700 degrees C, which provides strength even with a fine grain size. Such improved creep-resistance is necessary for advanced turbine systems that will demand greater materials performance and reliability at higher operating conditions. The next challenges are to better understand the nature of the improved creep resistance in these 347 stainless steel foil, and to achieve similar improvements with scale-up to commercial foil production

Creep mitigation in composites using carbon nanotube additives

Energy Technology Data Exchange (ETDEWEB)

Zhang, W [Department of Mechanical Aerospace and Nuclear Engineering, Rensselaer Polytechnic Institute, 110 8th Street, Troy, NY 12180 (United States); Joshi, A [Department of Chemical and Biological Engineering, Rensselaer Polytechnic Institute, 110 8th Street, Troy, NY 12180 (United States); Wang, Z [Department of Mechanical Aerospace and Nuclear Engineering, Rensselaer Polytechnic Institute, 110 8th Street, Troy, NY 12180 (United States); Kane, R S [Department of Chemical and Biological Engineering, Rensselaer Polytechnic Institute, 110 8th Street, Troy, NY 12180 (United States); Koratkar, N [Department of Mechanical Aerospace and Nuclear Engineering, Rensselaer Polytechnic Institute, 110 8th Street, Troy, NY 12180 (United States)

2007-05-09

A major limitation of thermosetting epoxy based polymeric materials in long-term structural applications is mechanical creep. Here it is demonstrated that single-walled carbon nanotube additives in low weight fractions (0.1-0.25%) are effective in limiting the load-induced re-orientation of epoxy chains, resulting in a significant slowing of the creep response. Nanotube additives could therefore be the key enabler for the long-term higher-temperature application of polymeric structures which would otherwise fail by excessive creep deformation.

Creep mitigation in composites using carbon nanotube additives

International Nuclear Information System (INIS)

Zhang, W; Joshi, A; Wang, Z; Kane, R S; Koratkar, N

2007-01-01

A major limitation of thermosetting epoxy based polymeric materials in long-term structural applications is mechanical creep. Here it is demonstrated that single-walled carbon nanotube additives in low weight fractions (0.1-0.25%) are effective in limiting the load-induced re-orientation of epoxy chains, resulting in a significant slowing of the creep response. Nanotube additives could therefore be the key enabler for the long-term higher-temperature application of polymeric structures which would otherwise fail by excessive creep deformation

Diffusion creep and its inhibition in a stainless steel

International Nuclear Information System (INIS)

Crossland, I.G.; Clay, B.D.

1977-01-01

The creep of 20% Cr, 25% Ni, Nb stainless steel was examined at low stresses and temperatures around 0.55 T/sub m/. The initial creep behaviour was consistent with the Coble theory of grain boundary diffusion creep; however, steady state creep was not observed and the creep rates quickly fell below the Coble theoretical values although they still remained greater than the Herring--Nabarro predictions. This reduction in creep rate was attributable to an increase in the effective viscosity of the steel rather than to any change in threshold stress. A model is proposed which explains the initial creep rates as being due to Coble creep with elastic accommodation at grain boundary particles. At higher strains grain boundary collapse caused by vacancy sinking is accommodated at precipitate particles by plastic deformation of the adjacent matrix material. 11 figures

Experimental studies of fiber concrete creep

Directory of Open Access Journals (Sweden)

Korneeva Irina

2017-01-01

Full Text Available The results of two-stage experimental studies of the strength and deformation characteristics of fibrous concrete reinforced with steel fiber. In the experiments we used steel fiber with bent ends, which practically does not form "hedgehogs", which allows to achieve an even distribution of the fiber by volume. At the first stage, the cube and prismatic strength, deformability at central compression, a number of special characteristics are determined: water absorption, frost resistance, abrasion; the optimal percentage of fiber reinforcement and the maximum size of the coarse aggregate fraction were selected. Fiber reinforcement led to an increase in the strength of concrete at compression by 1,35 times and an increase in the tensile strength at bending by 3,4 times. At the second stage, the creep of fibrous concrete and plain concrete of similar composition at different stress levels was researched. Creep curves are plotted. It is shown that the use of fiber reinforcement leads to a decrease in creep strain by 21 to 30 percent, depending on the stress level.

Variability of tissue mineral density can determine physiological creep of human vertebral cancellous bone.

Science.gov (United States)

Kim, Do-Gyoon; Shertok, Daniel; Ching Tee, Boon; Yeni, Yener N

2011-06-03

Creep is a time-dependent viscoelastic deformation observed under a constant prolonged load. It has been indicated that progressive vertebral deformation due to creep may increase the risk of vertebral fracture in the long-term. The objective of this study was to examine the relationships of creep with trabecular architecture and tissue mineral density (TMD) parameters in human vertebral cancellous bone at a physiological static strain level. Architecture and TMD parameters of cancellous bone were analyzed using microcomputerized tomography (micro-CT) in specimens cored out of human vertebrae. Then, creep and residual strains of the specimens were measured after a two-hour physiological compressive constant static loading and unloading cycle. Creep developed (3877 ± 2158 με) resulting in substantial levels of non-recoverable post-creep residual strain (1797 ± 1391 με). A strong positive linear correlation was found between creep and residual strain (r = 0.94, p creep rate. The TMD variability (GL(COV)) was the strongest correlate of creep rate (r = 0.79, p < 0.001). This result suggests that TMD variability may be a useful parameter for estimating the long-term deformation of a whole vertebral body. The results further suggest that the changes in TMD variability resulting from bone remodeling are of importance and may provide an insight into the understanding of the mechanisms underlying progressive failure of vertebral bodies and development of a clinical fracture. Copyright © 2011 Elsevier Ltd. All rights reserved.

Modelling of creep curves of Ni3Ge single crystals

Science.gov (United States)

Starenchenko, V. A.; Starenchenko, S. V.; Pantyukhova, O. D.; Solov'eva, Yu V.

2015-01-01

In this paper the creep model of alloys with L12 superstructure is presented. The creep model is based on the idea of the mechanisms superposition connected with the different elementary deformation processes. Some of them are incident to the ordered structure L12 (anomalous mechanisms), others are typical to pure metals with the fcc structure (normal mechanisms): the accumulation of thermal APBs by means of the intersection of moving dislocations; the formation of APB tubes; the multiplication of superdislocations; the movement of single dislocations; the accumulation of point defects, such as vacancies and interstitial atoms; the accumulation APBs at the climb of edge dislocations. This model takes into account the experimental facts of the wetting antiphase boundaries and emergence of the disordered phase within the ordered phase. The calculations of the creep curves are performed under different conditions. This model describes different kinds of the creep curves and demonstrates the important meaning of the deformation superlocalisation leading to the inverse creep. The experimental and theoretical results coincide rather well.

Numerical Modeling of Subglacial Sediment Deformation

DEFF Research Database (Denmark)

Damsgaard, Anders

2015-01-01

may cause mass loss in the near future to exceed current best estimates. Ice flow in larger ice sheets focuses in fast-moving streams due to mechanical non-linearity of ice. These ice streams often move at velocities several magnitudes larger than surrounding ice and consequentially constitute...... glaciers move by deforming their sedimentary beds. Several modern ice streams, in particular, move as plug flows due to basal sediment deformation. An intense and long-winded discussion about the appropriate description for subglacial sediment mechanics followed this discovery, with good reason...... incompatible with commonly accepted till rheology models. Variation in pore-water pressure proves to cause reorganization in the internal stress network and leads to slow creeping deformation. The rate of creep is non-linearly dependent on the applied stresses. Granular creep can explain slow glacial...

Review of recent irradiation-creep results

International Nuclear Information System (INIS)

Coghlan, W.A.

1982-05-01

Materials deform faster under stress in the presence of irradiation by a process known as irradiation creep. This phenomenon is important to reactor design and has been the subject of a large number of experimental and theoretical investigations. The purpose of this work is to review the recent experimental results to obtain a summary of these results and to determine those research areas that require additional information. The investigations have been classified into four subgroups based on the different experimental methods used. These four are: (1) irradiation creep using stress relaxation methods, (2) creep measurements using pressurized tubes, (3) irradiation creep from constant applied load, and (4) irradiation creep experiments using accelerated particles. The similarity and the differences of the results from these methods are discussed and a summary of important results and suggested areas for research is presented. In brief, the important results relate to the dependence of creep on swelling, temperature, stress state and alloying additions. In each of these areas new results have been presented and new questions have arisen which require further research to answer. 65 references

Modeling Long-term Creep Performance for Welded Nickel-base Superalloy Structures for Power Generation Systems

Energy Technology Data Exchange (ETDEWEB)

Shen, Chen

2015-01-01

We report here a constitutive model for predicting long-term creep strain evolution in’ strengthened Ni-base superalloys. Dislocation climb-bypassing’, typical in intermediate’ volume fraction (~20%) alloys, is considered as the primary deformation mechanism. Dislocation shearing’ to anti-phase boundary (APB) faults and diffusional creep are also considered for high-stress and high-temperature low-stress conditions, respectively. Additional damage mechanism is taken into account for rapid increase in tertiary creep strain. The model has been applied to Alloy 282, and calibrated in a temperature range of 1375-1450°F, and stress range of 15-45ksi. The model parameters and a MATLAB code are provided. This report is prepared by Monica Soare and Chen Shen at GE Global Research. Technical discussions with Dr. Vito Cedro are greatly appreciated. This work was supported by DOE program DE-FE0005859

A simple model for indentation creep

Science.gov (United States)

Ginder, Ryan S.; Nix, William D.; Pharr, George M.

2018-03-01

A simple model for indentation creep is developed that allows one to directly convert creep parameters measured in indentation tests to those observed in uniaxial tests through simple closed-form relationships. The model is based on the expansion of a spherical cavity in a power law creeping material modified to account for indentation loading in a manner similar to that developed by Johnson for elastic-plastic indentation (Johnson, 1970). Although only approximate in nature, the simple mathematical form of the new model makes it useful for general estimation purposes or in the development of other deformation models in which a simple closed-form expression for the indentation creep rate is desirable. Comparison to a more rigorous analysis which uses finite element simulation for numerical evaluation shows that the new model predicts uniaxial creep rates within a factor of 2.5, and usually much better than this, for materials creeping with stress exponents in the range 1 ≤ n ≤ 7. The predictive capabilities of the model are evaluated by comparing it to the more rigorous analysis and several sets of experimental data in which both the indentation and uniaxial creep behavior have been measured independently.

Neutron irradiation creep in stainless steel alloys

Energy Technology Data Exchange (ETDEWEB)

Schuele, Wolfgang (Commission of the European Union, Institute for Advanced Materials, I-21020 Ispra (Vatican City State, Holy See) (Italy)); Hausen, Hermann (Commission of the European Union, Institute for Advanced Materials, I-21020 Ispra (Vatican City State, Holy See) (Italy))

1994-09-01

Irradiation creep elongations were measured in the HFR at Petten on AMCR steels, on 316 CE-reference steels, and on US-316 and US-PCA steels varying the irradiation temperature between 300 C and 500 C and the stress between 25 and 300 MPa. At the beginning of an irradiation a type of primary'' creep stage is observed for doses up to 3-5 dpa after which dose the secondary'' creep stage begins. The primary'' creep strain decreases in cold-worked steel materials with decreasing stress and decreasing irradiation temperature achieving also negative creep strains depending also on the pre-treatment of the materials. These primary'' creep strains are mainly attributed to volume changes due to the formation of radiation-induced phases, e.g. to the formation of [alpha]-ferrite below about 400 C and of carbides below about 700 C, and not to irradiation creep. The secondary'' creep stage is found for doses larger than 3 to 5 dpa and is attributed mainly to irradiation creep. The irradiation creep rate is almost independent of the irradiation temperature (Q[sub irr]=0.132 eV) and linearly dependent on the stress. The total creep elongations normalized to about 8 dpa are equal for almost every type of steel irradiated in the HFR at Petten or in ORR or in EBR II. The negative creep elongations are more pronounced in PCA- and in AMCR-steels and for this reason the total creep elongation is slightly smaller at 8 dpa for these two steels than for the other steels. ((orig.))

Effects of microstructure on light ion irradiation creep in nickel

International Nuclear Information System (INIS)

Henager, C.H. Jr.; Simonen, E.P.; Bradley, E.R.; Stang, R.G.

1982-10-01

The concept of inhomogeneous slip or localized deformation is introduced to account for a weak dependence of irradiation creep on initial microstructure. Specimens of pure Ni with three different microstructures were irradiated at 473 0 K with 15 to 17 MeV deuterons in the PNL light ion irradiation creep apparatus. A dispersed barrier model for climb-glide creep was unable to account for the observed creep rates and creep strains. The weak dependence on microstructure was consistent with the SIPA creep mechanism but a high stress enhanced bias had to be assumed to account for the creep rates. Also, SIPA was unable to account for the observed creep strains. The modeling utilized rate theory calculations of point defect fluxes and transmission electron microscopy for sink sizes and densities

Viscoelastic characterization of carbon fiber-epoxy composites by creep and creep rupture tests

International Nuclear Information System (INIS)

Farina, Luis Claudio

2009-01-01

One of the main requirements for the use of fiber-reinforced polymer matrix composites in structural applications is the evaluation of their behavior during service life. The warranties of the integrity of these structural components demand a study of the time dependent behavior of these materials due to viscoelastic response of the polymeric matrix and of the countless possibilities of design configurations. In the present study, creep and creep rupture test in stress were performed in specimens of unidirectional carbon fiber-reinforced epoxy composites with fibers orientations of 60 degree and 90 degree, at temperatures of 25 and 70 degree C. The aim is the viscoelastic characterization of the material through the creep curves to some levels of constant tension during periods of 1000 h, the attainment of the creep rupture envelope by the creep rupture curves and the determination of the transition of the linear for non-linear behavior through isochronous curves. In addition, comparisons of creep compliance curves with a viscoelastic behavior prediction model based on Schapery equation were also performed. For the test, a modification was verified in the behavior of the material, regarding the resistance, stiffness and deformation, demonstrating that these properties were affected for the time and tension level, especially in work temperature above the ambient. The prediction model was capable to represent the creep behavior, however the determination of the equations terms should be considered, besides the variation of these with the applied tension and the elapsed time of test. (author)

Degradation of mechanical properties of CrMo creep resistant steel operating under conditions of creep

Directory of Open Access Journals (Sweden)

J. Michel

2012-01-01

Full Text Available Mechanical properties of a steam tube made of CrMo creep resistant steel are analysed in this contribution after up to 2,6•105 hours service life in creep conditions at temperature 530 °C and calculated stress level in the tube wall 46,5 MPa. During service life there were in the steel gradual micro structure changes, fi rst pearlite spheroidization, precipitation, coaugulation and precipitate coarsening. Nevertheless the strength and deformation properties of the steel (Re, Rm, A5, Z, and the resistance to brittle fracture and the creep strength limit, were near to unchanged after 2,1•105 hours in service. The steam tube is now in service more than 2,6•105 h.

Deformation behavior of UO2 at temperatures above 24000C

International Nuclear Information System (INIS)

Slagle, O.D.

1978-08-01

An experimental system was developed for measuring the high-temperature creep rates of ceramic nuclear fuels to temperatures near their melting points. The results of a series of experiments carried out on UO 2 at temperatures above 2400 0 C are reported. The strain rate was found to be proportional to the 5.7 power of the stress while activation energies ranged from 250 to 340 Kcal/mole. An expression for describing the primary creep was derived from the initial time dependence of the deformation after stress application. A technique for studying the hot pressing behavior at 2580 0 C was devised but no definitive results were obtained from the first series of experiments. An empirical relationship is proposed for calculating the creep rates at very high temperatures

Creep-fatigue deformation behaviour of OFHC-copper and CuCrZr alloy with different heat treatments and with and without neutron irradiation

International Nuclear Information System (INIS)

Singh, B.N.; Johansen, B.S.; Li, M.; Stubbins, J.F.

2005-08-01

The creep-fatigue interaction behaviour of a precipitation hardened CuCrZr alloy was investigated at 295 and 573 K. To determine the effect of irradiation a number of fatigue specimens were irradiated at 333 and 573 K to a dose level in the range of 0.2 - 0.3 dpa and were tested at room temperature and 573 K, respectively. The creep-fatigue deformation behaviour of OFHC-copper was also investigated but only in the unirradiated condition and at room temperature. The creep-fatigue interaction was simulated by applying a certain holdtime on both tension and compression sides of the cyclic loading with a frequency of 0.5 Hz. Holdtimes of up to 1000 seconds were used. Creep-fatigue experiments were carried out using strain, load and extension controlled modes of cyclic loading. In addition, a number of 'interrupted' creep-fatigue tests were performed on the prime aged CuCuZr specimens in the strain controlled mode with a strain amplitude of 0.5% and a holdtime of 10 seconds. The lifetimes in terms of the number of cycles to failure were determined at different strain and load amplitudes at each holdtime. Post-deformation microstructures was investigated using a transmission electron microscopy. The main results of these investigations are presented and their implications are briefly discussed in the present report. The central conclusion emerging from the present work is that the application of holdtime generally reduces the number of cycles to failure. The largest reduction was found to be in the case of OFHC-copper. Surprisingly, the magnitude of this reduction is found to be larger at lower levels of strain or stress amplitudes, particularly when the level of the stress amplitude is below the monotonic yield strength of the material. The reduction in the yield strength due to overaging heat treatments causes a substantial decrease in the number of cycles to failure at all holdtimes investigated. The increase in the yield strength due to neutron irradiation at 333 K

Prediction of Axial and Radial Creep in CANDU 6 Pressure Tubes

International Nuclear Information System (INIS)

Radu, Vasile S.

2013-01-01

Status and proposals: 1. A review of literature concerning on the in-reactor deformation of PTs has been carried ouţ. 2. A model based on MFNN has been proposed to assess the radial and axial creep of CANDU 6 PTs. 3. Preliminary discussion with Cernavoda NPP (Romania) has been lunched, and now the preparation of official documents (collaboration in providing the inspection data from fuel channel in Unit 1 and 2) are in progress. 4. Further activities: • Improvement MFNN to accommodate complex data base (eventually with many variables) for radial and axial in-reactor deformation PT, and to satisfy the requirements from NPP Cernavoda and hopefully from present CRP database; • To build-up a database by running the creep equations (if the creep constants are provided by AECL); training of MFNN on them and to qualify it as a tool for PT in-reactor deformation prediction

Development of a Zircaloy creep and failure model for LOCA conditions

International Nuclear Information System (INIS)

Raff, S.; Meyder, R.

1981-01-01

The present status of NORA model for zircaloy-4 creep and failure in the high temperature region (from 600 deg C up to 1200 deg C) is described. Temperature dependence, strain hardening and oxygen content are found to be the most important features of the strain rate creep equation. The failure criterion is based on a modified strain fraction rule. Variables of this criterion are temperature, strain rate or applied stress respectively and oxygen content. Concerning the application of the deformation model, deduced from uniaxial tests, to tube deformation calculation the axial ballooning shape has to be taken into account. Its influence on the tube stress components and therefore on strain rate is discussed. A further improvement of the deformation model concerning yield drop and irregular creep behaviour aims at the enlargement of the range of applicability and reduction of the error band of the model

Low temperature irradiation creep of tungsten and molybdenum

International Nuclear Information System (INIS)

Pouchou, J.-L.

1975-12-01

It is demonstrated that the mechanism of stress biased nucleation of dislocation loops may contribute significantly to the low temperature irradiation creep. This is achieved by measuring length and electrical resistivity changes at liquid hydrogen temperature, under fission fragments bombardement. From these measurements (correlated with some electron microscopy observations of irradiated samples), the following three stages of deformation appear: at low doses (smaller than 10 -2 displacement per atom) the deformation is mainly an increase in volume due to point defects. The study of this stage gives the formation volume of a Frenkel pair, and the number of point defects created by an initial fission fragment; for doses higher than 10 -2 d.p.a., the point defects saturation is reached. At this stage, vacancies and interstitials collapse into loops, the nucleation of which is polarized by the applied stress. At zero stress, the corresponding creep rate is zero. At high stresses (>50 kg/mm 2 ), creep rate saturates at value of the order of 10 -21 (FF/cm 3 ) -1 ; because of the recombinations of loops, the creep rate decreases continuously during irradiation. The recombinations lead to a dense dislocation network (formed at doses of 1 d.p.a.), the climb of which oriented by the applied stress gives rise to a steady state creep. The creep rate is smaller, by at least one order of magnitude, than that which is observed in the stage of loop formation [fr

Concrete for PCRVs: strength of concrete under triaxial loading and creep at elevated temperatures

International Nuclear Information System (INIS)

Linse, D.; Aschl, H.; Stoeckl, S.

1975-01-01

To provide detailed information for the calculation of prestressed concrete reactor vessels, investigations of the behaviour of concrete under multiaxial loading and on creep at elevated temperatures were made at the Institut fuer Massivbau of the Technical University of Munich. The strength of concrete under triaxial compression is dependent on the stress ratio. The less the stresses differ from hydrostatic compression the more strength increases. Triaxial compression increases very much the deformability of concrete. Plastic deformations of +-10% and more (all stresses compression, but not equal, strains compression or tension) are possible without large cracks. The creep deformations are considerably dependent on the temperature. Creep at 80 0 C is about three to four times higher than at 20 0 C. The Poisson's ratio of creep at elevated temperature seems to be bigger than at normal temperatures at a rate of loading of 35% and 50% of the ultimate strength. (Auth.)

Understanding effects of microstructural inhomogeneity on creep response – New approaches to improve the creep resistance in magnesium alloys

Directory of Open Access Journals (Sweden)

Yuanding Huang

2014-06-01

Full Text Available Previous investigations indicate that the creep resistance of magnesium alloys is proportional to the stability of precipitated intermetallic phases at grain boundaries. These stable intermetallic phases were considered to be effective to suppress the deformation by grain boundary sliding, leading to the improvement of creep properties. Based on this point, adding the alloying elements to form the stable intermetallics with high melting point became a popular way to develop the new creep resistant magnesium alloys. The present investigation, however, shows that the creep properties of binary Mg–Sn alloy are still poor even though the addition of Sn possibly results in the precipitation of thermal stable Mg2Sn at grain boundaries. That means other possible mechanisms function to affect the creep response. It is finally found that the poor creep resistance is attributed to the segregation of Sn at dendritic and grain boundaries. Based on this observation, new approaches to improve the creep resistance are suggested for magnesium alloys because most currently magnesium alloys have the commonality with the Mg–Sn alloys.

Creep and precipitation behaviors of AL6XN austenitic steel at elevated temperatures

Science.gov (United States)

Meng, L. J.; Sun, J.; Xing, H.

2012-08-01

Creep behaviors of the solution-treated AL6XN austenitic stainless steel have been investigated at 873-1023 K and 120-260 MPa. The results showed that the creep stress exponent and activation energy of the AL6XN steel are 5 and 395.4 kJ/mol, respectively in the power-law breakdown regime. TEM observations revealed that dislocations distributed homogenously in grains. The creep deformation mechanism is mainly attributed to viscous dislocation glide. Precipitates in the steel after creep deformation were additionally analyzed by TEM, and the results showed that there are four different types of precipitates, such as M23C6, M6C, σ phase and Laves phase. The M23C6 carbides were observed at grain boundaries in the steel after creep at 873 K. The M6C, σ phase and Laves phase precipitates were found when the creep temperature increases to 923-1023 K. Although the AL6XN steel exhibited low steady state creep rates, a high volume fraction of brittle precipitates of σ and Laves phases reduced the creep lifetime of the steel at elevated temperatures.

Creep and precipitation behaviors of AL6XN austenitic steel at elevated temperatures

Energy Technology Data Exchange (ETDEWEB)

Meng, L.J. [School of Materials Science and Engineering, Shanghai Jiaotong University, Dongchuan Road 800, Shanghai 200240 (China); Sun, J., E-mail: jsun@sjtu.edu.cn [School of Materials Science and Engineering, Shanghai Jiaotong University, Dongchuan Road 800, Shanghai 200240 (China); Xing, H. [School of Materials Science and Engineering, Shanghai Jiaotong University, Dongchuan Road 800, Shanghai 200240 (China)

2012-08-15

Creep behaviors of the solution-treated AL6XN austenitic stainless steel have been investigated at 873-1023 K and 120-260 MPa. The results showed that the creep stress exponent and activation energy of the AL6XN steel are 5 and 395.4 kJ/mol, respectively in the power-law breakdown regime. TEM observations revealed that dislocations distributed homogenously in grains. The creep deformation mechanism is mainly attributed to viscous dislocation glide. Precipitates in the steel after creep deformation were additionally analyzed by TEM, and the results showed that there are four different types of precipitates, such as M{sub 23}C{sub 6}, M{sub 6}C, {sigma} phase and Laves phase. The M{sub 23}C{sub 6} carbides were observed at grain boundaries in the steel after creep at 873 K. The M{sub 6}C, {sigma} phase and Laves phase precipitates were found when the creep temperature increases to 923-1023 K. Although the AL6XN steel exhibited low steady state creep rates, a high volume fraction of brittle precipitates of {sigma} and Laves phases reduced the creep lifetime of the steel at elevated temperatures.

A phenomenological creep model for nickel-base single crystal superalloys at intermediate temperatures

Science.gov (United States)

Gao, Siwen; Wollgramm, Philip; Eggeler, Gunther; Ma, Anxin; Schreuer, Jürgen; Hartmaier, Alexander

2018-07-01

For the purpose of good reproduction and prediction of creep deformation of nickel-base single crystal superalloys at intermediate temperatures, a phenomenological creep model is developed, which accounts for the typical γ/γ‧ microstructure and the individual thermally activated elementary deformation processes in different phases. The internal stresses from γ/γ‧ lattice mismatch and deformation heterogeneity are introduced through an efficient method. The strain hardening, the Orowan stress, the softening effect due to dislocation climb along γ/γ‧ interfaces and the formation of dislocation ribbons, and the Kear–Wilsdorf-lock effect as key factors in the main flow rules are formulated properly. By taking the cube slip in \\{100\\} slip systems and \\{111\\} twinning mechanisms into account, the creep behavior for [110] and [111] loading directions are well captured. Without specific interaction and evolution of dislocations, the simulations of this model achieve a good agreement with experimental creep results and reproduce temperature, stress and crystallographic orientation dependences. It can also be used as the constitutive relation at material points in finite element calculations with complex boundary conditions in various components of superalloys to predict creep behavior and local stress distributions.

Prediction of Creep Behaviour of the Hybrid Composite Material Using the Accelerated Characterisation Method

International Nuclear Information System (INIS)

Larbi, S.; Berradj, M.; Djebbar, A.; Bilek, A.

2011-01-01

We present in this study a creep behavior in flexure of a hybrid composite consisting of a polyester matrix containing methyl methacrylate reinforced by two bidirectional fabrics. The first one is made with E-glass fibers and the second one is made of a knitted polyamide 66. The mass fractions are 13% for the glass fabric and 9% for the polyamide fabric. The specimens, of dimensions (L = 60, l = 15 and h = 2.3 mm) containing 06 alternating layers (2P/2V/2P) were fabricated by using the vacuum bag molding method. Bending tests performed at different temperatures allowed us first to determine the load levels for the creep tests. Creep tests at different loads (5 to 43 MPa) and different temperatures (23'deg' to 80'deg' C) show a noticeable increase of creep deformation for both tests under the same load and different temperatures just as those carried out at different loads under the same temperature. The initial deformation varies significantly with the load but very little with temperature. The application of the Findley model shows good correlation with experimental results. Model parameters were identified. Creep deformation satisfies the principle of superposition time-temperature-stress (TTSSP). Findley's model has subsequently been coupled with the principle of superposition of time-temperature-stress to plot master curves at different stresses and temperatures; this enables prediction of creep deformation in the long term. (author)

Thermal ratcheting and creep damage

International Nuclear Information System (INIS)

Clement, G.; Cousseran, P.; Roche, R.L.

1983-01-01

Several proposals have been made to assist adesigners with thermal ratcheting in the creep range, the more known has been made by O'DONNELL and POROWSKY. Unfortunately these methods are not validated by experiments, and they take only inelastic distortion into consideration as creep effects. The aim of the work presented here is to correct these deficiencies - in providing an experimental basis to ratcheting analysis rules in the creep range, - in considering the effect of cyclic straining (like cyclic thermal stresses) on the time to rupture by creep. Experimental tests have been performed on austenitic stainless steel at 650 0 C for the first item. Results of these tests and results available in the open literature have been used to built a practical rule of ratcheting analysis. This rule giving a conservative value of the creep distortion, is based on the concept of effective primary stress which is an amplification of the primary stress really applied. Concerning the second point (time to rupture), it was necessary to obtain real creep rupture and not instability. According to the proposal of Pr LECKIE, tests were performed on specimens made out of copper, and of aluminium alloys at temperatures between 150 0 C and 300 0 C. With such materials creep rupture is obtained without necking. Experimental tests show that cyclic straining reduces the time to creep rupture under load controlled stress. Caution must be given to the designer: cyclic thermal stress can lead to premature creep rupture. (orig./GL)

Correlation of Creep Behavior of Domal Salts

International Nuclear Information System (INIS)

Munson, D.E.

1999-01-01

The experimentally determined creep responses of a number of domal salts have been reported in, the literature. Some of these creep results were obtained using standard (conventional) creep tests. However, more typically, the creep data have come from multistage creep tests, where the number of specimens available for testing was small. An incremental test uses abrupt changes in stress and temperature to produce several time increments (stages) of different creep conditions. Clearly, the ability to analyze these limited data and to correlate them with each other could be of considerable potential value in establishing the mechanical characteristics of salt domes, both generally and specifically. In any analysis, it is necessary to have a framework of rules to provide consistency. The basis for the framework is the Multimechanism-Deformation (M-D) constitutive model. This model utilizes considerable general knowledge of material creep deformation to supplement specific knowledge of the material response of salt. Because the creep of salt is controlled by just a few micromechanical mechanisms, regardless of the origin of the salt, certain of the material parameters are values that can be considered universal to salt. Actual data analysis utilizes the methodology developed for the Waste Isolation Pilot Plant (WIPP) program, and the response of a bedded pure WIPP salt as the baseline for comparison of the domal salts. Creep data from Weeks Island, Bryan Mound, West Hackberry, Bayou Choctaw, and Big Hill salt domes, which are all sites of Strategic Petroleum Reserve (SPR) storage caverns, were analyzed, as were data from the Avery Island, Moss Bluff, and Jennings salt domes. The analysis permits the parameter value sets for the domal salts to be determined in terms of the M-D model with various degrees of completeness. In turn this permits detailed numerical calculations simulating cavern response. Where the set is incomplete because of the sparse database, reasonable

Effects of composition on the in-reactor creep of AISI 316

International Nuclear Information System (INIS)

Bates, J.F.; Gilbert, E.R.

1980-01-01

Pre- and postirradiation measurements of pressurized tube specimens irradiated at 450/degree/C to 4.6*10/sup 22/ n/cm/sup 2/(E>0.1 MeV) have indicated that increases in the solute concentrations of silicon, phosphorus, and molybdenum retard irradiation creep. The data suggest that carbon and nitrogen act synergistically with the major influence on creep being the nitrogen concentration. Irradiation-induced creep is insensitive to cobalt variations. There is a trend for specimens with higher swelling to exhibit higher creep. As the shear modulus increases, irradiation creep also increases. This shear modulus correlation is opposite to one observed for thermal creep deformation. 8 refs

Microstructure-sensitive modelling of dislocation creep in polycrystalline FCC alloys: Orowan theory revisited

Energy Technology Data Exchange (ETDEWEB)

Galindo-Nava, E.I., E-mail: eg375@cam.ac.uk; Rae, C.M.F.

2016-01-10

A new approach for modelling dislocation creep during primary and secondary creep in FCC metals is proposed. The Orowan equation and dislocation behaviour at the grain scale are revisited to include the effects of different microstructures such as the grain size and solute atoms. Dislocation activity is proposed to follow a jog-diffusion law. It is shown that the activation energy for cross-slip E{sub cs} controls dislocation mobility and the strain increments during secondary creep. This is confirmed by successfully comparing E{sub cs} with the experimentally determined activation energy during secondary creep in 5 FCC metals. It is shown that the inverse relationship between the grain size and dislocation creep is attributed to the higher number of strain increments at the grain level dominating their magnitude as the grain size decreases. An alternative approach describing solid solution strengthening effects in nickel alloys is presented, where the dislocation mobility is reduced by dislocation pinning around solute atoms. An analysis on the solid solution strengthening effects of typical elements employed in Ni-base superalloys is also discussed. The model results are validated against measurements of Cu, Ni, Ti and 4 Ni-base alloys for wide deformation conditions and different grain sizes.

High temperature creep-fatigue design

International Nuclear Information System (INIS)

Tavassoli, A. A. F.; Fournier, B.; Sauzay, M.

2010-01-01

Generation IV fission and future fusion reactors envisage development of more efficient high temperature concepts where materials performances are key to their success. This paper examines different types of high temperature creep-fatigue interactions and their implications on design rules for the structural materials retained in both programmes. More precisely, the paper examines current status of design rules for the stainless steel type 316L(N), the conventional Modified 9Cr-1Mo martensitic steel and the low activation Eurofer steel. Results obtained from extensive high temperature creep, fatigue and creep-fatigue tests performed on these materials and their welded joints are presented. These include sequential creep-fatigue and relaxation creep-fatigue tests with hold times in tension, in compression or in both. Effects of larger plastic deformations on fatigue properties are studied through cyclic creep tests or fatigue tests with extended hold time in creep. In most cases, mechanical test results are accompanied with microstructural and fractographic observations. In the case of martensitic steels, the effect of oxidation is examined by performing creep-fatigue tests on identical specimens in vacuum. Results obtained are analyzed and their implications on design allowable and creep-fatigue interaction diagrams are presented. While reasonable confidence is found in predicting creep-fatigue damage through existing code procedures for austenitic stainless steels, effects of cyclic softening and coarsening of microstructure of martensitic steels throughout the fatigue life on materials properties need to be taken into account for more precise damage calculations. In the long-term, development of ferritic/martensitic steels with stable microstructure, such as ODS steels, is proposed. (authors)

High temperature creep-fatigue design

Energy Technology Data Exchange (ETDEWEB)

Tavassoli, A. A. F.; Fournier, B.; Sauzay, M. [CEA Saclay, DEN DMN, F-91191 Gif Sur Yvette (France)

2010-07-01

Generation IV fission and future fusion reactors envisage development of more efficient high temperature concepts where materials performances are key to their success. This paper examines different types of high temperature creep-fatigue interactions and their implications on design rules for the structural materials retained in both programmes. More precisely, the paper examines current status of design rules for the stainless steel type 316L(N), the conventional Modified 9Cr-1Mo martensitic steel and the low activation Eurofer steel. Results obtained from extensive high temperature creep, fatigue and creep-fatigue tests performed on these materials and their welded joints are presented. These include sequential creep-fatigue and relaxation creep-fatigue tests with hold times in tension, in compression or in both. Effects of larger plastic deformations on fatigue properties are studied through cyclic creep tests or fatigue tests with extended hold time in creep. In most cases, mechanical test results are accompanied with microstructural and fractographic observations. In the case of martensitic steels, the effect of oxidation is examined by performing creep-fatigue tests on identical specimens in vacuum. Results obtained are analyzed and their implications on design allowable and creep-fatigue interaction diagrams are presented. While reasonable confidence is found in predicting creep-fatigue damage through existing code procedures for austenitic stainless steels, effects of cyclic softening and coarsening of microstructure of martensitic steels throughout the fatigue life on materials properties need to be taken into account for more precise damage calculations. In the long-term, development of ferritic/martensitic steels with stable microstructure, such as ODS steels, is proposed. (authors)

Effect of microstructure on light ion irradiation creep in nickel

International Nuclear Information System (INIS)

Henager, C.H. Jr.; Simonen, E.P.; Bradley, E.R.; Stang, R.G.

1983-01-01

The concept of inhomogeneous slip or localized deformation is introduced to account for a weak dependence of irradiation creep on initial microstructure. Specimens of pure nickel (Ni) with three different microstructures were irradiated at 473 K with 15-17 MeV deuterons in the Pacific Northwest Laboratory (PNL) light ion irradiation creep apparatus. A dispersed barrier model for Climb-Glide (CG) creep was unable to account for the observed creep rates and creep strains. The weak dependence on microstructure was consistent with the Stress Induced Preferential Absorption (SIPA) creep mechanism but a high stress enhanced bias had to be assumed to account for the creep rates. Also, SIPA was unable to account for the observed creep strains. The CG and SIPA modeling utilized rate theory calculations of point defect fluxes and transmission electron microscopy for sink sizes and densities. (orig.)

Studies of Grain Boundaries in Materials Subjected to Diffusional Creep

DEFF Research Database (Denmark)

Nørbygaard, Thomas

Grain boundaries in crystalline Cu(2%Ni) creep specimens have been studied by use of scanning and transmission electron microscopy in order to establish the mechanism of deformation. Creep rate measurements and dependencies were found to fit reasonably well with the model for diffusional creep......) with the activity displayed during diffusional creep testing. It was found that boundaries with low deviation from perfect Σ did not contribute macroscopically to the creep strain. A resist deposition procedure was examined to improve the reference surface grid so as to allow determination of the grain boundary...... plane by use of simple stereomicroscopy directly on the surface. The etched pattern deteriorated heav-ily during creep testing, supposedly because of dislocation creep, due to exces-sive creep stress. Grain boundaries have been studied and characterised by TEM providing an insight into the diversity...

Creep properties of welded joints in OFHC copper for nuclear waste containment

International Nuclear Information System (INIS)

Ivarsson, B.; Oesterberg, J.O.

1988-08-01

In Sweden it has been suggested that copper canisters are used for containment of spent nuclear fuel. These canisters will be subjected to temperatures up to 100 degrees C and external pressures up to 15 MPa. Since the material is pure (OFHC) copper, creep properties must be considered when the canisters are dimensioned. The canisters are sealed by electron beam welding which will affect the creep properties. Literature data for copper - especially welded joints - at the temperatures of interest is very scare. Therefore uniaxial creep tests of parent metal, weld metal, and simulated HAZ structures have been performed at 110 degrees C. These tests revealed considerable differences in creep deformation and rupture strength. The weld metal showed creep rates and rupture times ten times higher and ten times shorter, respectively, than those of the parent metal. The simulated HAZ was equally strongen than the parent metal. These differences were to some extent verified by results from creep tests of cross-welded specimens which, however, showed even shorter rupture times. Constitutive equations were derived from the uniaxial test results. To check the applicability of these equations to multiaxial conditions, a few internal pressure creep tests of butt-welded tubes were performed. Attemps were made to simulate their creep behaviour by constitutive equations were used. These calculations failed due to too great differences in creep deformation behaviour across the welded joint. (authors)

Creep Rupture Properties for Base and Weld Metals of Alloy 617

International Nuclear Information System (INIS)

Kim, Woo-Gon; Kim, Min-Hwan; Park, Jae-Young; Ekaputra, I. M. W.

2015-01-01

The allowable deformation in the welds is also restricted to half the deformation permitted for the base metal, since the ductility of the welds at elevated temperatures is generally low. For a design use, the data of the tensile and creep properties for Alloy 617 WM should be sufficiently provided, and in particular, to develop a design code of Alloy 617 WM. However, the data for the WM are very rare and limited until now, although the data for the BM are available in the ASME draft code case, which was suspended at the end of the 1980s owing to a lack of support and interes. In this report, the creep data for Alloy 617 WM, which was fabricated by a gas tungsten arc welding (GTAW) procedure, were obtained by a series of creep tests at 800 .deg. C, and the creep properties of the WM were compared with those of the BM. The high-temperature creep properties for Alloy 617 WM, fabricated by a gas tungsten arc welding (GTAW) procedure, were investigated by a series of creep tests with different stress levels at 800 .deg. C, and the creep test data for the WM were compared with those of the BM. From the results, it was found that the WM had a slightly longer creep rupture life and lower creep rate than the BM, and a particularly lower rupture elongation. The lower creep rate in the WM was due to the lower rupture elongation than the BM

Rationalization of activation energies for creep of dispersion strengthened aluminium materials

International Nuclear Information System (INIS)

Carreno, F.; Ruano, O. A.

2001-01-01

The high apparent activation energies for creep of various aluminum dispersion strengthened materials have been analyzed. A direct relationship between the activation energies and stress exponents for every material has been observed. The values of the Q a p/n a p ratios group around some constant values, Q m , which depend solely on the deformation mechanism. Therefore, Q m establishes an easy, fast and reliable criterion to determine the underlying creep deformation mechanism of any reinforced materials. (Author) 18 refs

Tensile cracks in creeping solids

International Nuclear Information System (INIS)

Riedel, H.; Rice, J.R.

1979-02-01

The loading parameter determining the stress and strain fields near a crack tip, and thereby the growth of the crack, under creep conditions is discussed. Relevant loading parameters considered are the stress intensity factor K/sub I/, the path-independent integral C*, and the net section stress sigma/sub net/. The material behavior is modelled as elastic-nonlinear viscous where the nonlinear term describes power law creep. At the time t = 0 load is applied to the cracked specimen, and in the first instant the stress distribution is elastic. Subsequently, creep deformation relaxes the initial stress concentration at the crack tip, and creep strains develop rapidly near the crack tip. These processes may be analytically described by self-similar solutions for short times t. Small scale yielding may be defined. In creep problems, this means that elastic strains dominate almost everywhere except in a small creep zone which grows around the crack tip. If crack growth ensues while the creep zone is still small compared with the crack length and the specimen size, the stress intensity factor governs crack growth behavior. If the calculated creep zone becomes larger than the specimen size, the stresses become finally time-independent and the elastic strain rates can be neglected. In this case, the stress field is the same as in the fully-plastic limit of power law hardening plasticity. The loading parameter which determines the near tip fields uniquely is then the path-independent integral C*.K/sub I/ and C* characterize opposite limiting cases. The case applied in a given situation is decided by comparing the creep zone size with the specimen size and the crack length. Besides several methods of estimating the creep zone size, a convenient expression for a characteristic time is derived, which characterizes the transition from small scale yielding to extensive creep of the whole specimen

Creep in crystalline rock with application to high level nuclear waste repository

International Nuclear Information System (INIS)

Eloranta, P.; Simonen, A.

1992-06-01

The time-dependent strength and deformation properties of hard crystalline rock are studied. Theoretical models defining the phenomena which can effect these properties are reviewed. The time- dependent deformation of the openings in the proposed nuclear waste repository is analysed. The most important factors affecting the subcritical crack growth in crystalline rock are the stress state, the chemical environment, temperature and microstructure of the rock. There are several theoretical models for the analysis of creep and cyclic fatigue: deformation diagrams, rheological models thermodynamic models, reaction rate models, stochastic models, damage models and time-dependent safety factor model. They are defective in describing the three-axial stress condition and strength criteria. In addition, the required parameters are often too difficult to determine with adequate accuracy. Therefore these models are seldom applied in practice. The effect of microcrack- driven creep on the stability of the work shaft, the emplacement tunnel and the capsulation hole of a proposed nuclear waste repository was studied using a numerical model developed by Atomic Energy of Canada Ltd. According to the model, the microcrack driven creep progresses very slowly in good quality rock. Poor rock quality may accelerate the creep rate. The model is very sensitive to the properties of the rock and secondary stress state. The results show that creep causes no stability problems on excavations in good rock. The results overestimate the effect of the creep, because the analysis omitted the effect of support structures and backfilling

Spectral analysis of creep recovery process in finemet type amorphous alloy

NARCIS (Netherlands)

Jurikova, A; Csach, K; Miskuf, J; Bengus, VZ; Ocelik, Vaclav

2002-01-01

The creep recovery process in Finemet type amorphous alloy leas been analyzed using the method for calculating the relaxation tithe spectra. The influence of structural relaxation and temperature on the spectra shape lags been studied. The creep recovery spectrum of the anelastic deformation of the

Mechanical and microstructural behavior of oxide dispersion strengthened 8Cr-2W and 8Cr-1W steels during creep deformation

Energy Technology Data Exchange (ETDEWEB)

Shinozuka, K.; Tamura, M.; Esaka, H. [National Defense Academy, Dept. MS and E, Kanagawa (Japan); Shiba, K.; Nakamura, K. [Japan Atomic Energy Agency, Tokai-mura, Naga-gun, Ibaraki-ken (Japan)

2007-07-01

Full text of publication follows: Oxide dispersion strengthened (ODS) steel is a promising candidate for fusion reactor material because of excellent mechanical properties. However, the ODS steel exhibits some defects, such as mechanical anisotropy and little elongation . To reveal details of these defects, we investigated correlations between mechanical and microstructural behavior of ODS ferritic steels during creep deformation at high temperature. The materials used in this study are two kinds of hot rolled ODS steels: Fe-8Cr-2W-0.2V-0.1Ta-0.2Ti-0.4Y{sub 2}O{sub 3} (J1) and Fe-8Cr-1W-0.2Ti-0.4Y{sub 2}O{sub 3} (J2). Creep tests was carried out on specimens sampling along both the rolling direction and the cross direction at 670, 700 and 730 deg. C. Microstructural analyses were made on the normalized and tempered condition by using OM, SEM, TEM and XRD. Creep ruptured and interrupted specimens were also investigated. Both J1 and J2 existed two phases, namely martensite and {delta}-ferrite which was elongated in the rolling direction. Y-Ti complex oxide particles were finely dispersed in martensite and {delta}- ferrite phases. Results of creep tests indicated that the time-to-rupture of specimens of J1 were much longer than J2, and the time-to-rupture of specimens sampling along the rolling direction were longer than cross direction. Accordingly, J1 sampling along hot rolling direction was the strongest, for instance, the time-to-rupture was 11400 h at 700 deg. C and 162 MPa. All specimens indicated that elongation was less than 1.3 % and the rupture occurred at steady state creep region from creep curves. Internal cracks were propagated in martensite phase along elongated {delta}-ferrite phase in the direction of hot rolling. On the other hand, {delta}-ferrite phases seemed to prevent combining cracks. These results suggest that elongated {delta}-ferrite and internal clacks in martensite strongly affect on the anisotropy and little elongation of creep. (authors)

Irradiation creep induced anisotropy in a/2 dislocation populations

International Nuclear Information System (INIS)

Gelles, D.S.

1984-05-01

The contribution of anisotropy in Burgers vector distribution to irradiation creep behavior has been largely ignored in irradiation creep models. However, findings on Frank loops suggest that it may be very important. Procedures are defined to identify the orientations of a/2 Burgers vectors for dislocations in face-centered cubic crystals. By means of these procedures the anisotropy in Burgers vector populations was determined for three Nimonic PE16 pressurized tube specimens irradiated under stress. Considerable anisotropy in Burgers vector population develops during irradiation creep. It is inferred that dislocation motion during irradiation creep is restricted primarily to a climb of a/2 dislocations on 100 planes. Effect of these results on irradiation creep modeling and deformation induced irradiation growth is considered

Relationship between strain and central deflection in small punch creep specimens

International Nuclear Information System (INIS)

Yang Zhen; Wang Zhiwen

2003-01-01

Acquiring information about creep strain directly from small punch creep tests is difficult because the deformation behaviour of the small punch specimen is complicated. A routine is suggested in the present paper to treat this problem indirectly. Based on a finite element analysis, it is proposed that the relationship of central deflection δ to central creep strain ε c of a specimen subjected to creep can be represented approximately by the relationship of central deflection δ to central (elastic-plastic) strain ε of a specimen not subjected to creep. With this hypothesis, the δ∼ε c relation of the small punch creep specimen is obtained by resorting to a rigid-plastic membrane stretch forming model. Finally, small punch creep test results are used to evaluate creep strain and creep strain rate by taking advantage of this δ∼ε c relation

Ratcheting deformation of advanced 316 steel under creep-plasticity condition

Energy Technology Data Exchange (ETDEWEB)

Kawashima, Fumiko; Ishikawa, Akiyoshi; Asada, Yasuhide [Tokai Univ., Tokyo (Japan). Dept. of Mechanical Engineering

1998-11-01

Tension-torsion biaxial ratcheting tests have been conducted with Advanced 316 Steel (316FR Steel) at 650 C under a cyclic strain rate of 10{sup -3} to 10{sup -5} s{sup -1}. Accumulation of ratcheting strain has been measured. Accumulated ratchet strain has shown to be much larger than predicted based on a usual method of the linear superposition of strains due to creep and plasticity. The result shows there observed the creep-plasticity interaction in the observation. (orig.)

Effect of initial temper on the creep behavior of precipitation–hardened WE43 alloy

Energy Technology Data Exchange (ETDEWEB)

Kang, Y.H. [The Group of Magnesium Alloys and Their Applications, Institute of Metal Research Chinese Academy of Sciences, 62 Wencui Road, Shenyang 110016 (China); University of the Chinese Academy of Sciences, Beijing 100049 (China); Wang, X.X.; Zhang, N. [Shenyang Liming Aero–Engine Group Corporation, Aero–Engine Corporation of China, Shenyang 110043 (China); Yan, H., E-mail: hyan@imr.ac.cn [The Group of Magnesium Alloys and Their Applications, Institute of Metal Research Chinese Academy of Sciences, 62 Wencui Road, Shenyang 110016 (China); Chen, R.S., E-mail: rschen@imr.ac.cn [The Group of Magnesium Alloys and Their Applications, Institute of Metal Research Chinese Academy of Sciences, 62 Wencui Road, Shenyang 110016 (China)

2017-03-24

The effect of initial tempers with different characteristics of precipitates and contents of supersaturated solute atoms, including the homogenized, peak–aged and over–aged conditions, on the tensile creep behavior of WE43 alloy has been investigated at 523 K. Results show that the peak–aged alloy at 523 K obtained superior creep resistance than the homogenized, peak–aged at 498 K and over–aged at 523 K alloy. A uniform dispersion of β precipitates was dynamically formed within steady–stage creep microstructure of the homogenized WE43 alloy after creep deformation of 200 h. It is found that the precipitate size and distribution is similar with the alloy aged equal time without the applied stress. In addition, the WE43 alloy in all tempers obtains similar precipitate size and distribution in their steady–stage creep microstructures. Therefore, it is inferred that the various initial tempers mainly affect the primary creep stage. Furthermore, numerous dislocations were detected between precipitates and the stress exponent n is 4.5, which is close to 5. Thereby, dislocation climb is suggested to be the creep mechanism. The reason for the peak–aged alloy at 523 K obtained superior creep resistance is that the initial uniform dispersion of β″ and β′ precipitates have smaller precipitate size and higher precipitate density than that of the homogenized and over–aged alloy, which are more effectively to hider dislocation climb. However, a deterioration of creep resistance was occurred in the peak−aged alloy at 498 K due to precipitate recovery when crept at 523 K. As a consequence, WE43 alloy in peak–aged temper at 523 K achieves the highest creep resistance.

Effects of NaCl, pH, and Potential on the Static Creep Behavior of AA1100

Science.gov (United States)

Wan, Quanhe; Quesnel, David J.

2013-03-01

The creep rates of AA1100 are measured during exposure to a variety of aggressive environments. NaCl solutions of various concentrations have no influence on the steady-state creep behavior, producing creep rates comparable to those measured in lab air at room temperature. However, after an initial incubation period of steady strain rate, a dramatic increase of strain rate is observed on exposure to HCl solutions and NaOH solutions, as well as during cathodic polarization of specimens in NaCl solutions. Creep strain produces a continuous deformation and elongation of the sample surface that is comparable to slow strain rates at crack tips thought to control the kinetics of crack growth during stress corrosion cracking (SCC). In this experiment, we separate the strain and surface deformation from the complex geometry of the crack tip to better understand the processes at work. Based on this concept, two possible explanations for the environmental influences on creep strain rates are discussed relating to the anodic dissolution of the free surface and hydrogen influences on deformation mechanisms. Consistencies of pH dependence between corrosion creep and SCC at low pH prove a creep-involved SCC mechanism, while the discrepancies between corrosion creep behavior and previous SCC results at high pH indicate a rate-limit step change in the crack propagation of the SCC process.

Design project of the experimental device for studying the uranium Creep in the reactor; Predprojekat eksperimentalnog uredjaja za ispitivanje CREEP-a urana u reaktoru

Energy Technology Data Exchange (ETDEWEB)

Pavicevic, M [Institute of Nuclear Sciences Boris Kidric, Odeljenje za reaktorsku eksperimentalnu tehniku, Vinca, Beograd (Serbia and Montenegro)

1963-12-15

The objective of this task was constructing a device for creep testing of uranium, i.e permanent deformation of the irradiated fuel. Deformation results from the influence of thermal neutron flux, temperature, time of irradiation, mechanical stress. This describes two possible technical solutions experimental device for creep testing in the vertical experimental channel and in the horizontal experimental channel of the RA reactor. In addition to the design details, the report covers calculations of heat generation, antireactivity, activation of the materials of the constructed experimental loop, mechanical calculations as well as description of measurements and regulation of the uranium sample temperature.

Power series like relation of power law and coupled creep ...

African Journals Online (AJOL)

When a solid deforms at high temperature its microstructure may in some sense be altered- holes and cracks may nucleate and grow inside the solid by various mechanism controlled by diffusion and by power law creep or by a combination of these mechanisms. Considering a coupled diffusion power law creep mechanism ...

Contribution on creep polygonization study in crystals. Creep of single crystalline silver chloride and sodium chloride

International Nuclear Information System (INIS)

Pontikis, Vassilis

1977-01-01

Subgrain formation and their influence on plastic behavior of materials has been studied in the case of single crystals of silver chloride and sodium chloride crept at high temperature (T > 0.5 T melting ). It is shown that the creep rate ε is a function of the mean subgrain diameter d. For secondary creep ε ∝ d k with k = 2 for NaCl and AgCl. During secondary creep, the substructure changes continuously: sub-boundaries migrate and sub-grains rotate. We find that sub-boundaries migration accounts for 35 pc of the total strain and that subgrain misorientation θ increases linearly with strain ε: θ ∝ 0.14 ε. The stability of permanent creep seems related to the power that the substructure is able to dissipate. The possible subgrain formation mechanisms are examined. It is shown that subgrain formation is closely related to the geometrical conditions of deformation and to the heterogeneities of this later. (author) [fr

Creep crack growth in phosphorus alloyed oxygen free copper

Energy Technology Data Exchange (ETDEWEB)

Wu, Rui; Seitisleam, Facredin (Swerea KIMAB (Sweden)); Sandstroem, Rolf; Jin, Lai-Zhe (Materials Science and Engineering, Royal Inst. of Technology (Sweden))

2011-01-15

Using standard compact tension (CT) specimens taken from a pierce and draw cylinder, creep crack growth (CCG) has been studied in phosphorus-alloyed oxygen-free copper (Cu-OFP) parent metal at 22, 75, 175, and 215 deg C. Pre- and post-test metallography are performed. At higher temperatures the rupture time of CCG is shorter by a factor up of 65 than that of uniaxial at same stress/reference stress. At 175 and 215 deg C, crack does grow by creep about 10 mm before final instantaneous failure. In contrast, there is hardly any visible crack growth at 22 and 75 deg C. The tests were interrupted after 5000 to 13000 hours. For ruptured tests at 175 and 215 deg C, strongly elongated and deformed grains are observed adjacent to crack. Extensive and intergranular creep cavities and microcracks are found several mm around crack. For interrupted tests at 22 and 75 deg C, strongly elongated and deformed grains, creep cavities, as well as microcracks are observed close to crack tip. Surface cracks from both sides have initiated and grown about 45 deg to the load direction towards inside. For the interrupted tests, hardness adjacent to crack tip has more than doubled because of work hardening, or heavy deformation. This is consistent with large crack tip opening. The true strain at the crack tip is estimated to 10 and 4 for the tests at 22 and 75 deg C, respectively. The stress state behind the crack tip has been modelled with FEM. Stress relaxation after loading has also been taken into account. A model for the creep damage based on the creep strain rate has been formulated that can describe the uniaxial creep rupture data without fitting parameters. Based on the formulation for the creep damage, a model for the crack propagation has been set up. When the creep damage has reached the value unity in front of the crack tip, the crack is assumed to propagate. Taking multiaxial effects into account the observed life times of the CT specimens can be well described. The multiaxial

Creep crack growth in phosphorus alloyed oxygen free copper

International Nuclear Information System (INIS)

Wu, Rui; Seitisleam, Facredin; Sandstroem, Rolf; Jin, Lai-Zhe

2011-01-01

Using standard compact tension (CT) specimens taken from a pierce and draw cylinder, creep crack growth (CCG) has been studied in phosphorus-alloyed oxygen-free copper (Cu-OFP) parent metal at 22, 75, 175, and 215 deg C. Pre- and post-test metallography are performed. At higher temperatures the rupture time of CCG is shorter by a factor up of 65 than that of uniaxial at same stress/reference stress. At 175 and 215 deg C, crack does grow by creep about 10 mm before final instantaneous failure. In contrast, there is hardly any visible crack growth at 22 and 75 deg C. The tests were interrupted after 5000 to 13000 hours. For ruptured tests at 175 and 215 deg C, strongly elongated and deformed grains are observed adjacent to crack. Extensive and intergranular creep cavities and microcracks are found several mm around crack. For interrupted tests at 22 and 75 deg C, strongly elongated and deformed grains, creep cavities, as well as microcracks are observed close to crack tip. Surface cracks from both sides have initiated and grown about 45 deg to the load direction towards inside. For the interrupted tests, hardness adjacent to crack tip has more than doubled because of work hardening, or heavy deformation. This is consistent with large crack tip opening. The true strain at the crack tip is estimated to 10 and 4 for the tests at 22 and 75 deg C, respectively. The stress state behind the crack tip has been modelled with FEM. Stress relaxation after loading has also been taken into account. A model for the creep damage based on the creep strain rate has been formulated that can describe the uniaxial creep rupture data without fitting parameters. Based on the formulation for the creep damage, a model for the crack propagation has been set up. When the creep damage has reached the value unity in front of the crack tip, the crack is assumed to propagate. Taking multiaxial effects into account the observed life times of the CT specimens can be well described. The multiaxial

Metallurgical considerations in the design of creep exposed, high temperature components for advanced power plants

International Nuclear Information System (INIS)

Schubert, F.

1990-08-01

Metallic components in advanced power generating plants are subjected to temperatures at which the material properties are significantly time-dependent, so that the creep properties become dominant for the design. In this investigation, methods by which such components are to be designed are given, taking into account metallurgical principles. Experimental structure mechanics testing of component related specimens carried out for representative loading conditions has confirmed the proposed methods. The determination of time-dependent design values is based on a scatterband evaluation of long-term testing data obtained for a number of different heats of a given alloy. The application of computer-based databank systems is recommendable. The description of the technically important secondary creep rate based on physical metallurgy principles can be obtained using the exponential relationship originally formulated by Norton, ε min = k.σ n . The deformation of tubes observed under internal pressure with a superimposed static or cyclic tensile stress and a torsion loading can be adequately described with the derived, three-dimensional creep equation (Norton). This is also true for the description of creep ratcheting and creep buckling phenomena. By superimposing a cyclic stress, the average creep rate is increased in one of the principal deformation axes. This is also true for the creep crack growth rate. The Norton equation can be used to derive this type of deformation behaviour. (orig.) [de

Damage in Creep Aging Process of an Al-Zn-Mg-Cu Alloy: Experiments and Modeling

Directory of Open Access Journals (Sweden)

Chao Lei

2018-04-01

Full Text Available In creep age forming (CAF, large integral panel components of high-strength aluminum alloy can be shaped and strengthened under external elastic loading at an elevated temperature through creep deformation and age hardening, simultaneously. However, the high ribbed structure on panel may induce stress concentration, inhomogeneous plastic deformation and even damage evolution on the bending rib, leading to the difficulty in controlling forming precision and material properties. Therefore, the generation and evolution of damage are necessary to be considered in the design of CAF. Taking 7050 aluminum alloy as the case material, the continuous and interrupted creep aging tests at 165 °C and three stress levels (300, 325, and 350 MPa were conducted, and the corresponding material properties, precipitate, and damage microstructures were studied by mechanical properties tests, transmission electron microscope (TEM and scanning electron microscope (SEM characterizations. With the increase of stress level, the creep deformation occurs easier, the precipitates grow up faster, the creep damage occurs earlier, the growth rate and the size of microvoids increase, the mechanical properties decrease more rapidly, and the dominant mechanism of creep fracture changes from shear to microvoid coalescence. To simulate creep aging behavior with damage, a continuum damage mechanics (CDM based model is calibrated and numerically implemented into ABAQUS solver via CREEP subroutine. The CAF of 7050 aluminum alloy panels with different height ribs were conducted by experiment and FE simulation. The forming process presents a typical stress relaxation phenomenon. The creep damage mainly occurs on the bending rib due to the severe stress concentration. With the increase of rib height, the creep strain and damage degree increase, but the springback decreases.

High-resolution TEM microscopy study of the creep behaviour of carbon-based cathode materials

Energy Technology Data Exchange (ETDEWEB)

Wang, Wei, E-mail: wwlyzwkj@126.com [College of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471023 (China); Collaborative Innovation Center of Nonferrous Metals Henan Province, Luoyang 471023 (China); Chen, Weijie [College of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471023 (China); Collaborative Innovation Center of Nonferrous Metals Henan Province, Luoyang 471023 (China); Gu, Wanduo [Collaborative Innovation Center of Nonferrous Metals Henan Province, Luoyang 471023 (China)

2017-02-27

Creep is in close relationship with the materials deterioration and deformation of the cathodes in aluminum reduction cells. The purpose of this work is to obtain the creep mechanism of the carbon cathode for aluminum electrolysis. A modified Rapoport equipment was used for measuring the creep strain of the semi-graphitic cathodes during aluminum electrolysis with CR=2.5 and at temperature of 945 ℃. The arrangement of carbon atom has been studied after hexagonal graphite converting into rhombohedral graphite during aluminum electrolysis by XRD and high-resolution transmission electron microscopy (HRTEM). The creep deformation of the carbon cathode has a close relationship with the mobile dislocation walls. These results will be helpful in controlling the cathode quality and its performance in aluminum reduction cells.

Fragmentation of α2 plates in a fully lamellar TiAl during creep

International Nuclear Information System (INIS)

Wang, J.G.; Hsiung, L.M.; Nieh, T.G.

1999-01-01

The fragmentation and spheroidization of α 2 laths in a fully-lamellar TiAl alloy during creep were examined. Three possible mechanisms, Rayleigh's perturbation model, subgrain boundary groove mechanism and intersection of deformation twins with α 2 lamellae were presented and discussed. During creep deformation, the pile-up of interfacial dislocations leads to a change of planar interface, which, in turn, causes a difference in local chemical potential, and further results in the spheroidization of α 2 lamellae. On the other hand, the deformation of the α 2 phase is expected to be induced by the high local stress concentration introduced by the pile up of interfacial dislocations. The dynamic recovery process may lead to the formation of subgrain boundaries in the α 2 lamellae, which results in the spheroidization and termination of α 2 lamellae with the aid of diffusion during creep

Creep of parylene-C film

KAUST Repository

Lin, Jeffrey Chun-Hui; Deng, Peigang; Lam, Gilbert; Lu, Bo; Lee, Yi-Kuen; Tai, Yu-Chong

2011-01-01

The glass transition temperature of as-deposited parylene-C is first measured to be 50°C with a ramping-temperature-dependent modulus experiment. The creep behavior of parylene-C film in the primary and secondary creep region is then investigated

Survey of creep properties of copper intended for nuclear waste disposal

Energy Technology Data Exchange (ETDEWEB)

Andersson-Oestling, Henrik C.M. (Swerea KIMAB AB, Stockholm (Sweden)); Sandstroem, Rolf (Materials Science and Engineering, School of Industrial Engineering and Management, Royal Inst. of Technology (KTH), Stockholm (Sweden))

2009-12-15

Creep in copper for application in canisters for nuclear waste disposal is surveyed. The importance of phosphorus doping to obtain adequate properties is demonstrated experimentally as well as explained theoretically. Creep tests results for electron beam and friction stir welds are compared. The latter type of welds has properties that are close to those of parent metal. The relation between slow strain rate tensile and creep is described. Fundamental constitutive equations are presented that are suitable for finite element modelling. These equations are used to simulate creep deformation in canisters

Influence of phosphorus on the creep ductility of copper

International Nuclear Information System (INIS)

Sandström, Rolf; Wu, Rui

2013-01-01

Around 1990 it was discovered that pure copper could have extra low creep ductility in the temperature interval 180–250 °C. The material was intended for use in canisters for nuclear waste disposal. Although extra low creep ductility was not observed much below 180 °C and the temperature in the canister will never exceed 100 °C, it was feared that the creep ductility could reach low values at lower temperatures after long term exposure. If 50 ppm phosphorus was added to the copper the low creep ductility disappeared. A creep cavitation model is presented that can quantitatively describe the cavitation behaviour in uniaxial and multiaxial creep tests as well as the observed creep ductility for copper with and without phosphorus. A so-called double ledge model has been introduced that demonstrates why the nucleation rate of creep cavities is often proportional to the creep rate. The phosphorus agglomerates at the grain boundaries and limits their local deformation and thereby reduces the formation and growth of cavities. This explains why extra low creep ductility does not occur in phosphorus alloyed copper

Sigmoidal creep transients and the second law of Newton

International Nuclear Information System (INIS)

Montemayor-Aldrete, J.A.; Orozco, E.

1990-01-01

The main features of sigmoidal transients, not only for viscous glide but also for Power-Law Creep are explained in a physical way. Also the experimental data for the average internal stress, (σ i ), and the mobile dislocation density, ρ m , at the inflection point of sigmoidal creep curves for Germanium and Cu-16at%Al are fully described. Finally, the stress and temperature dependence of the total plastic deformation at the inflection point for sigmoidal creep curves in Cu-11.5at%Al are also catered for (Author)

Study of creep microstructure in aluminium at medium temperatures

International Nuclear Information System (INIS)

Caillard, Daniel

1980-01-01

This research thesis focused on the use of electronic microscopy for the study of the properties of a sub-structure which appears during the second stage of creep in aluminium under intermediate temperatures. The author used conventional observations at 100 kV performed on thin blades manufactured after the macroscopic creep test, and in situ deformation observations in the high voltage microscope for the examination of thicker blades. After a review of knowledge on creep and on creep models, the author describes the used experimental conditions, notably for in situ experiments, their benefits and limitations. Geometric properties of various dislocation networks present in sub-grains and sub-boundaries are then described. A creep model is then proposed, based on the previous observations, and is compared with other published experimental results

Modifications on the behaviour of AISI 304 stainless steel submitted to creep caused by intermediate treatment of annealing

International Nuclear Information System (INIS)

Barreto, L.F.P.; Monteiro, S.N.

1982-01-01

Type AISI 304 austenitic stainless steel samples which have been previously creep deformed at 750 0 C, were annealed at 1100 0 C. The effects of this heat treatment in the mechanical behavior of this material when retested in creep were investigated. The results were analysed by taking into account the structural modifications observed and the controlling mechanisms which operate during the deformation and fracture occurring in the creep process. (Author) [pt

Assessment of long-term creep strength of grade 91 steel

Energy Technology Data Exchange (ETDEWEB)

Kimura, Kazuhiro; Sawada, Kota; Kushima, Hideaki [National Inst. for Materials Science, Tsukuba, Ibaraki (Japan)

2010-07-01

In 2004 and 2005 long-term creep rupture strength of ASME Grade 91 type steels of plate, pipe, forging and tube materials was evaluated in Japan by means of region splitting analysis method in consideration of 50% of 0.2% offset yield stress. According to the evaluated 100,000h creep rupture strength of 94MPa for plate, pipe and forging steels and 92MPa for tube steel at 600 C, allowable tensile stress of the steels regulated in the Interpretation for the Technical Standard for Thermal Power Plant was slightly reduced. New creep rupture data of the steels obtained in the long-term indicate further reduction of long-term creep rupture strength. Not only creep rupture strength, but also creep deformation property of the ASME Grade 91 steel was investigated and need of reevaluation of long-term creep strength of Grade 91 steel was indicated. A refinement of region splitting analysis method for creep rupture like prediction was discussed. (orig.)

A microstructural study of fault rocks from the SAFOD: Implications for the deformation mechanisms and strength of the creeping segment of the San Andreas Fault

Science.gov (United States)

Hadizadeh, Jafar; Mittempergher, Silvia; Gratier, Jean-Pierre; Renard, Francois; Di Toro, Giulio; Richard, Julie; Babaie, Hassan A.

2012-09-01

The San Andreas Fault zone in central California accommodates tectonic strain by stable slip and microseismic activity. We study microstructural controls of strength and deformation in the fault using core samples provided by the San Andreas Fault Observatory at Depth (SAFOD) including gouge corresponding to presently active shearing intervals in the main borehole. The methods of study include high-resolution optical and electron microscopy, X-ray fluorescence mapping, X-ray powder diffraction, energy dispersive X-ray spectroscopy, white light interferometry, and image processing. The fault zone at the SAFOD site consists of a strongly deformed and foliated core zone that includes 2-3 m thick active shear zones, surrounded by less deformed rocks. Results suggest deformation and foliation of the core zone outside the active shear zones by alternating cataclasis and pressure solution mechanisms. The active shear zones, considered zones of large-scale shear localization, appear to be associated with an abundance of weak phases including smectite clays, serpentinite alteration products, and amorphous material. We suggest that deformation along the active shear zones is by a granular-type flow mechanism that involves frictional sliding of microlithons along phyllosilicate-rich Riedel shear surfaces as well as stress-driven diffusive mass transfer. The microstructural data may be interpreted to suggest that deformation in the active shear zones is strongly displacement-weakening. The fault creeps because the velocity strengthening weak gouge in the active shear zones is being sheared without strong restrengthening mechanisms such as cementation or fracture sealing. Possible mechanisms for the observed microseismicity in the creeping segment of the SAF include local high fluid pressure build-ups, hard asperity development by fracture-and-seal cycles, and stress build-up due to slip zone undulations.

Deformation of high-temperature superconductors

International Nuclear Information System (INIS)

Goretta, K.C.; Routbort, J.L.; Miller, D.J.; Chen, N.; Dominguez-Rodriguez, A.; Jimenez-Melendo, M.; De Arellano-Lopez, A.R.

1994-08-01

Of the many families of high-temperature superconductors, only the properties of those discovered prior to 1989 - Y-Ba-Cu-O, Tl-Ba(Sr)-Ca-Cu-O, and Bi(Pb)-Sr-Ca-Cu-O - have been studied extensively. Deformation tests have been performed on YBa 2 Cu 3 O x (Y-123), YBa 2 Cu 4 O x (Y-124), TlBa 2 Ca 2 Cu 3 O x (Bi-2223). The tests have revealed that plasticity is generally limited in these compounds and that the rate-controlling diffusional kinetics for creep are very slow. Nevertheless, hot forming has proved to be quite successful for fabrication of bulk high-temperature superconductors, so long as deformation rates are low or large hydrostatic stresses are applied. Steady-state creep data have proved to be useful in designing optimal heat treatments for superconductors and in support of more-fundamental diffusion experiments. The high-temperature superconductors are highly complex oxides, and it is a challenge to understand their deformation responses. In this paper, results of interest and operant creep mechanisms will be reviewed

Simulation of finite-strain inelastic phenomena governed by creep and plasticity

Science.gov (United States)

Li, Zhen; Bloomfield, Max O.; Oberai, Assad A.

2017-11-01

Inelastic mechanical behavior plays an important role in many applications in science and engineering. Phenomenologically, this behavior is often modeled as plasticity or creep. Plasticity is used to represent the rate-independent component of inelastic deformation and creep is used to represent the rate-dependent component. In several applications, especially those at elevated temperatures and stresses, these processes occur simultaneously. In order to model these process, we develop a rate-objective, finite-deformation constitutive model for plasticity and creep. The plastic component of this model is based on rate-independent J_2 plasticity, and the creep component is based on a thermally activated Norton model. We describe the implementation of this model within a finite element formulation, and present a radial return mapping algorithm for it. This approach reduces the additional complexity of modeling plasticity and creep, over thermoelasticity, to just solving one nonlinear scalar equation at each quadrature point. We implement this algorithm within a multiphysics finite element code and evaluate the consistent tangent through automatic differentiation. We verify and validate the implementation, apply it to modeling the evolution of stresses in the flip chip manufacturing process, and test its parallel strong-scaling performance.

Stress-affected microstructural development and creep-swelling interrelationship

International Nuclear Information System (INIS)

Brager, H.R.; Garner, F.A.; Gilbert, E.R.; Flinn, J.E.; Wolfer, W.G.

1977-05-01

Macroscopic measurement of the deformations arising from swelling and creep during neutron irradiation indicate that both processes are dependent on the magnitude and possibly the sign of the applied stress state. Current modeling efforts also indicate that a strong interaction exists between swelling and creep through the stress state. Because the macroscopic distortions arise from the integrated microscopic strains associated with specific microstructural elements, the effect of applied stress on microstructural development has been studied

The relationship of whole human vertebral body creep to geometric, microstructural, and material properties.

Science.gov (United States)

Oravec, Daniel; Kim, Woong; Flynn, Michael J; Yeni, Yener N

2018-05-17

Creep, the time dependent deformation of a structure under load, is an important viscoelastic property of bone and may play a role in the development of permanent deformity of the vertebrae in vivo leading to clinically observable spinal fractures. To date, creep properties and their relationship to geometric, microstructural, and material properties have not been described in isolated human vertebral bodies. In this study, a range of image-based measures of vertebral bone geometry, bone mass, microarchitecture and mineralization were examined in multiple regression models in an effort to understand their contribution to creep behavior. Several variables, such as measures of mineralization heterogeneity, average bone density, and connectivity density persistently appeared as significant effects in multiple regression models (adjusted r 2 : 0.17-0.56). Although further work is needed to identify additional tissue properties to fully describe the portion of variability not explained by these models, these data are expected to help understand mechanisms underlying creep and improve prediction of vertebral deformities that eventually progress to a clinically observable fracture. Copyright © 2018 Elsevier Ltd. All rights reserved.

Creep Measurement Video Extensometer

Science.gov (United States)

Jaster, Mark; Vickerman, Mary; Padula, Santo, II; Juhas, John

2011-01-01

Understanding material behavior under load is critical to the efficient and accurate design of advanced aircraft and spacecraft. Technologies such as the one disclosed here allow accurate creep measurements to be taken automatically, reducing error. The goal was to develop a non-contact, automated system capable of capturing images that could subsequently be processed to obtain the strain characteristics of these materials during deformation, while maintaining adequate resolution to capture the true deformation response of the material. The measurement system comprises a high-resolution digital camera, computer, and software that work collectively to interpret the image.

Study of elementary mechanisms of creep in uranium as a function of temperature (150 deg. to 760 deg. C) by activation energy measurements; Etude des mecanismes elementaires de deformation par fluage de l'uranium en fonction de la temperature (de 150 deg. a 760 deg. C) par la mesure des energies d'activation

Energy Technology Data Exchange (ETDEWEB)

Grenier, P [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

1967-07-01

Creep tests were carried out on single crystals and polycrystalline specimens of uranium in both the {alpha} and {beta} phases over the temperature range 150 - 760 deg. C. The determination of the activation energy for creep and the study of its variation with temperature made it possible to distinguish various temperature ranges in which one or more elementary mechanisms govern deformation. Micrographic observations after creep and the study of the variation of creep-rate with load support the conclusions. The creep behavior of single crystals is identical with that of polycrystalline material below 325 deg. C. From 325 deg. C to one upper limiting temperature whose value depends on the purity and previous history of the metal, the creep deformation of uranium is controlled by cross-slip. From this limiting temperature up to 520 deg. C, the creep of uranium involves two independent mechanisms operating simultaneously, the movement of screw dislocation by cross-slip and the climbing of edge dislocations out of their slip plane. Between 520 deg. C and the {alpha} - {beta} transformation temperature creep in polycrystals is governed by the climb of edge dislocations out of their slip planes, by a pile up mechanism in the case of primary creep and by dipole annihilation in the case of secondary creep. In single crystals creep is dependent on the climb of edge dislocations into pre-existent sub-boundaries and their subsequent rearrangement within these boundaries. In the {beta} phase the creep of polycrystals is governed by the diffusional climb of edge dislocations. Between 450 and 630 deg. C small alloy additions of molybdenum modify the creep characteristics of uranium although the deformation mechanisms involved are analogous to those in the pure metal. (author) [French] Des essais de fluage a diverses temperatures comprises entre 150 et 760 deg. C ont ete effectues sur des polycristaux et des monocristaux d'uranium, en phase {alpha} et en phase {beta}. La

Thermal creep behavior of N36 zirconium alloy cladding tube

International Nuclear Information System (INIS)

Wang, P.; Zhao, W.; Dai, X.

2015-01-01

N36 is an alloy containing Zr, Sn, Nb and Fe that is developed by China as a superior cladding material to meet the performance of PWR fuel assembly at the maximum fuel rod burn-up. The creep characteristics of N36 zirconium alloy cladding tube were investigated at temperature from 593 K to 723 K with stress ranging from 20 MPa to 160 MPa. Transitions in creep mechanisms were noted, showing the distinct three rate-controlled creep mechanisms for the alloy at test conditions. In the region of low stresses with stress exponent n ∼ 1 and activation energy Q ∼ (104±4) kJ.mol -1 , Coble creep, based on diffusion of materials through grain boundaries, is the dominant rate-controlling mechanism, which contributes to the creep deformation. The formation of slip bands acts as an accommodation mechanism. In the region of middle stress with stress exponent n ∼ 3 and activation energy Q ∼ (195±7) kJ.mol -1 , micro-creep, caused by viscous gliding of dislocations due to the interaction of O atoms with dislocations, controls the deformation. In the high stress region with stress exponent n ∼ 5-6 and activation energy Q ∼ (210±10) kJ.mol -1 , two mechanisms of the climb of edge dislocations (EDC) and the motion of jogged screw dislocation (MJS) contribute to rate controlling process. In test conditions N36 alloy cladding tube behaves a type of creep similar to that noted in class-I (A) alloys

A methodology to analyze the creep behaviour of nuclear fuel waste containers

Energy Technology Data Exchange (ETDEWEB)

Dutton, R [Atomic Energy of Canada Ltd., Pinawa, MB (Canada). Whiteshell Labs.

1995-12-01

The concept for the disposal of used-fuel waste from CANDU reeactors operating in Canada comprises a system of natural and engineered barriers surrounding the waste in a mined vault situated at a depth of 500 - 1000 m in plutonic rock of the Canadian Shield. The fuel would be packaged in a highly durable metal container, within a matrix of compacted particulate. The design of the container takes into account that it would be subjected to an external hydrostatic pressure. Consideration of the rate of radioactive decay of the radionuclides contained in the fuel, suggests that the lifetime of the container should be at least 500 years. Consequently, the role of creep deformation, and the possibility of creep rupture of the container shell, must be included in the assessment of time-dependent mechanical integrity. This report describes an analytical approach that can be used to quantify the long-term creep properties of the container material and facilitate the engineering design. The overall objective is to formulate a constitutive creep equation that provides the required input for a finite element computer model being developed to analyze the elastic-plastic behaviour of the container. Alternative forms of such equations are reviewed. It is shown that the capability of many of these equations to extrapolate over long time scales is limited by their empirical nature. Thus, the recommended equation is based on current mechanistic understanding of creep deformation and creep rupture. A criterion for determining the onset of material failure by creep rupture, that could be used in the design of containers with extended structural integrity, is proposed. Interpretation and extrapolation will be supported by the complementary Deformation and Fracture Mechanism Maps. (author) 103 refs., 2 tabs., 54 figs.

A methodology to analyze the creep behaviour of nuclear fuel waste containers

International Nuclear Information System (INIS)

Dutton, R.

1995-12-01

The concept for the disposal of used-fuel waste from CANDU reeactors operating in Canada comprises a system of natural and engineered barriers surrounding the waste in a mined vault situated at a depth of 500 - 1000 m in plutonic rock of the Canadian Shield. The fuel would be packaged in a highly durable metal container, within a matrix of compacted particulate. The design of the container takes into account that it would be subjected to an external hydrostatic pressure. Consideration of the rate of radioactive decay of the radionuclides contained in the fuel, suggests that the lifetime of the container should be at least 500 years. Consequently, the role of creep deformation, and the possibility of creep rupture of the container shell, must be included in the assessment of time-dependent mechanical integrity. This report describes an analytical approach that can be used to quantify the long-term creep properties of the container material and facilitate the engineering design. The overall objective is to formulate a constitutive creep equation that provides the required input for a finite element computer model being developed to analyze the elastic-plastic behaviour of the container. Alternative forms of such equations are reviewed. It is shown that the capability of many of these equations to extrapolate over long time scales is limited by their empirical nature. Thus, the recommended equation is based on current mechanistic understanding of creep deformation and creep rupture. A criterion for determining the onset of material failure by creep rupture, that could be used in the design of containers with extended structural integrity, is proposed. Interpretation and extrapolation will be supported by the complementary Deformation and Fracture Mechanism Maps. (author) 103 refs., 2 tabs., 54 figs

Influence of sequential room-temperature compressive creep on flow stress of TA2

Science.gov (United States)

Mengyuan, Zhang; Boqin, Gu; Jiahui, Tao

2018-03-01

This paper studied the sequential room temperature compressive creep and its effects on compressive properties of TA2 with stress-control loading pattern by using cylindrical compressive test specimen. The significant time-dependent deformation under constant load was observed in the TA2 at room temperature, and the deformation was dependent on the loading process under the same loading stress rate. It was also found that the occurrence of room temperature compressive creep obviously enhanced the subsequent yielding strength and flow stress of TA2 due to the increase of network dislocation density. And the effects of room temperature creep on the strain rate-stress behavior could be explained by the local mobile dislocation density model.

Effect of texture on creep deformation behavior of Zr-2.5Nb alloy

International Nuclear Information System (INIS)

Guguloth, Krishna; Swaminathan, J.; Mitra, Rahul; Ghosh, R.N.; Singh, R.N.; Chakravartty, J.K.

2016-01-01

Zr-2.5%Nb alloys are extensively used as high temperature pressure tubes in nuclear reactor. Therefore creep behavior of this alloy is of considerable importance. The paper presents creep strain-time plots on two sets of specimens made from two as received pressure tubes having different diameters. These tubes were reported to have undergone different processing routes; both tubes were autoclaved at the same temperature in the steam atmosphere. A comparison of the creep strain-time plots of the two sets of specimen under identical test conditions showed a marked difference. The chemical composition and the microstructure of the two sets of samples were also found to be similar. Therefore X-ray diffraction patterns were taken from the two tubes. The ratio of intensity of two prominent reflections from 0002 and 1120 planes of alpha Zr in the case of 90mm tube was found to be 1.79; whereas that from the 110mm tube was 0.25. This suggests that in the case of 110mm tube most of the basal planes were less favorably oriented with respect to the loading axis. This is the reason why creep strength of 110mm tube was found to be higher. The paper also describes how the effect of texture can be incorporated in evaluating the creep behavior of Zr-Nb alloy. This suggests that a relatively larger volume of creep test data on Zr-2.5Nb pressure tube is necessary to account for the effect texture so that a reliable estimate of its creep life could be obtained. (author)

Creep behaviour of modified 9Cr-1Mo ferritic steel

International Nuclear Information System (INIS)

Choudhary, B.K.; Isaac Samuel, E.

2011-01-01

Creep deformation and fracture behaviour of indigenously developed modified 9Cr-1Mo steel for steam generator (SG) tube application has been examined at 823, 848 and 873 K. Creep tests were performed on flat creep specimens machined from normalised and tempered SG tubes at stresses ranging from 125 to 275 MPa. The stress dependence of minimum creep rate obeyed Norton's power law. Similarly, the rupture life dependence on stress obeyed a power law. The fracture mode remained transgranular at all test conditions examined. The analysis of creep data indicated that the steel obey Monkman-Grant and modified Monkman-Grant relationships and display high creep damage tolerance factor. The tertiary creep was examined in terms of the variations of time to onset of tertiary creep with rupture life, and a recently proposed concept of time to reach Monkman-Grant ductility, and its relationship with rupture life that depends only on damage tolerance factor. SG tube steel exhibited creep-rupture strength comparable to those reported in literature and specified in the nuclear design code RCC-MR.

Multi-axial Creep and the LICON Methodology for Accelerated Creep Testing

International Nuclear Information System (INIS)

Bowyer, William H.

2006-05-01

The copper-Iron canister for disposal of nuclear waste in the Swedish Programme has a design life exceeding 100,000 years. Whilst the operating temperature (100 deg C max.) and operating stress (50 MPa max.) are modest, the very long design life does require that the likely creep performance of the canister should be investigated. Many studies have been carried out by SKB but these have all involved very short duration tests at relatively high stresses. The process of predicting canister creep life by extrapolation of data from such tests has been challenged for two main reasons. The first is that the deformation and failure mechanisms in the tests employed are different from the mechanism expected under service conditions and the second is that the extrapolation is extreme. It has been recognised that there is usually scope for some increase in test temperatures and stresses which will accelerate the development of creep damage without compromising the use of extrapolation for life prediction. Cane demonstrated that in steels designed for high temperature and pressure applications, conditions of multi-axial stressing could lead to increases or decreases in the rate of damage accumulation without changing the damage mechanism. This provided a third method for accelerating creep testing which has been implemented as the LICON method. This report aims to explain the background to the LICON method and its application to the case of the copper canister. It seems likely that the method could be used to improve our knowledge of the creep resistance of the copper canister. Multiplication factors that may be achieved by the technique could be increased by attention to specimen design but an extensive and targeted programme of data collection on creep of copper would still be needed to implement the method to best advantage

Multi-axial Creep and the LICON Methodology for Accelerated Creep Testing

Energy Technology Data Exchange (ETDEWEB)

Bowyer, William H. [Meadow End Farm, Farnham (United Kingdom)

2006-05-15

The copper-Iron canister for disposal of nuclear waste in the Swedish Programme has a design life exceeding 100,000 years. Whilst the operating temperature (100 deg C max.) and operating stress (50 MPa max.) are modest, the very long design life does require that the likely creep performance of the canister should be investigated. Many studies have been carried out by SKB but these have all involved very short duration tests at relatively high stresses. The process of predicting canister creep life by extrapolation of data from such tests has been challenged for two main reasons. The first is that the deformation and failure mechanisms in the tests employed are different from the mechanism expected under service conditions and the second is that the extrapolation is extreme. It has been recognised that there is usually scope for some increase in test temperatures and stresses which will accelerate the development of creep damage without compromising the use of extrapolation for life prediction. Cane demonstrated that in steels designed for high temperature and pressure applications, conditions of multi-axial stressing could lead to increases or decreases in the rate of damage accumulation without changing the damage mechanism. This provided a third method for accelerating creep testing which has been implemented as the LICON method. This report aims to explain the background to the LICON method and its application to the case of the copper canister. It seems likely that the method could be used to improve our knowledge of the creep resistance of the copper canister. Multiplication factors that may be achieved by the technique could be increased by attention to specimen design but an extensive and targeted programme of data collection on creep of copper would still be needed to implement the method to best advantage.

Probability based high temperature engineering creep and structural fire resistance

CERN Document Server

Razdolsky, Leo

2017-01-01

This volume on structural fire resistance is for aerospace, structural, and fire prevention engineers; architects, and educators. It bridges the gap between prescriptive- and performance-based methods and simplifies very complex and comprehensive computer analyses to the point that the structural fire resistance and high temperature creep deformations will have a simple, approximate analytical expression that can be used in structural analysis and design. The book emphasizes methods of the theory of engineering creep (stress-strain diagrams) and mathematical operations quite distinct from those of solid mechanics absent high-temperature creep deformations, in particular the classical theory of elasticity and structural engineering. Dr. Razdolsky’s previous books focused on methods of computing the ultimate structural design load to the different fire scenarios. The current work is devoted to the computing of the estimated ultimate resistance of the structure taking into account the effect of high temperatur...

Study of precipitation phenomena during the creep of austenitic stainless steels

International Nuclear Information System (INIS)

Le May, I.; Bassett, B.J.; White, W.E.

1975-01-01

Creep-rupture data for two austenitic stainless steels, AISI Types 310 and 316, are presented, together with observations of precipitation taking place during creep. While the effects of creep deformation on precipitation in the Type 310 were negligible, ferrite precipitation was considerably greater in the Type 316 undergoing creep than in unstressed material. Ferrite precipitation appears to promote grain boundary cavitation and internal cracking, thus reducing creep resistance and a correlation has been noted between increased ferrite precipitation and apparent further weakening of the Type 316 over the temperature range 730 to 800 0 C approximately, as evidenced by breaks in the isostress lines on a plot of log (time to rupture) versus temperature

Thermally activated creep and fluidization in flowing disordered materials

Science.gov (United States)

Merabia, Samy; Detcheverry, François

2016-11-01

When submitted to a constant mechanical load, many materials display power law creep followed by fluidization. A fundamental understanding of these processes is still far from being achieved. Here, we characterize creep and fluidization on the basis of a mesoscopic viscoplastic model that includes thermally activated yielding events and a broad distribution of energy barriers, which may be lowered under the effect of a local deformation. We relate the creep exponent observed before fluidization to the width of barrier distribution and to the specific form of stress redistribution following yielding events. We show that Andrade creep is accompanied by local strain hardening driven by stress redistribution and find that the fluidization time depends exponentially on the applied stress. The simulation results are interpreted in the light of a mean-field analysis, and should help in rationalizing the creep phenomenology in disordered materials.

Creep and fatigue of alloy 800 in helium

International Nuclear Information System (INIS)

Cook, R.H.

1975-01-01

Proposals for use of Alloy 800 as a H.T.R. boiler material have prompted studies of its creep and high temperature fatigue properties in impure helium with comparative tests in air. In impure helium, as expected in a H.T.R., reactions of potential importance are selective oxidation (of chromium, aluminium and titanium) and possibly carburisation from carbon monoxide or methane. In air, general oxidation will occur, possibly accompanied by nitridation. The effects of these reactions will depend on specimen geometry and the nature of the deformation. Two important possibilities are: (i) that environment affects the structure and properties of a surface zone of material undegoing uniform deformation (this may modify creep rate and crack nucleation); and (ii) that environment affects behaviour of a small region (e.g. at the root of a notch or ahead of a crack) in a specimen undergoing non-uniform deformation (this will modify crack growth and hence rupture life or fatigue endurance). This paper summarises experimental work demonstrating an influence of the above reactions on mechanical properties of austenitic steels and nickel-based alloys, drawing examples where possible from the limited data available on Alloy 800. Whilst nitridation and carburisation may simply increase creep resistance at the expense of ductility (and possibly of fatigue resistance), the effects of oxidation are complex. A high oxygen pressures (as in air) oxygen may reduce creep and fatigue resistance by promoting cavitation but formation of oxide in cracks can reduce their propagation rate. At low oxygen pressures, as expected in H.T.R. helium, oxygen enhanced cavitation is less likely, but selective oxidation along grain boundaries can sometimes assist crack nucleation. (author)

Creep analysis of fuel plates for the Advanced Neutron Source

International Nuclear Information System (INIS)

Swinson, W.F.; Yahr, G.T.

1994-11-01

The reactor for the planned Advanced Neutron Source will use closely spaced arrays of fuel plates. The plates are thin and will have a core containing enriched uranium silicide fuel clad in aluminum. The heat load caused by the nuclear reactions within the fuel plates will be removed by flowing high-velocity heavy water through narrow channels between the plates. However, the plates will still be at elevated temperatures while in service, and the potential for excessive plate deformation because of creep must be considered. An analysis to include creep for deformation and stresses because of temperature over a given time span has been performed and is reported herein

Investigations on fuel can plastic deformations

International Nuclear Information System (INIS)

Boutard, J.L.; Dupouy, J.M.

1979-01-01

To the extent where the elongation of claddings differs from the mean swelling, the diametral plastic deformation can include, apart from that due to fission gases or the mechanical oxide-cladding interaction, contributions due to swelling prevented along the axis or to growth phenomena. The high thermal activation of the creep of hyper quenched steel unlike cold rolled steel, gives rise to the problem of a contribution to creep in the reactor other than the term SIPA. The impact of mechanisms of diffusion deformation on the boundary decohesion criteria is discussed in conclusion [fr

Low ductility creep failure in austenitic weld metals

International Nuclear Information System (INIS)

Thomas, R.G.

Creep tests have been carried out for times of up to approx. 22,000 hrs on three austenitic weld metals of nominal composition 17Cr-8Ni-2Mo, 19Cr-12Ni-3Mo+Nb and 17Cr-10Ni-2Mo. The two former deposits were designed to produce delta-ferrite contents in the range 3-9% while the latter was designed to be fully austenitic. The common feature of all three weld metals was that they all gave very low strains at failure, typically approx. 1%. The microstructures of the failed creep specimens have been studied using optical and electron microscopy and the precipitate structures related to the occurrence of low creep strains. Creep deformation and fracture mechanisms in austenitic materials in general have been reviewed and this has been used as a basis for discussion of the observations of the present work. Finally, some of the factors that can be controlled to improve long-term creep ductility have been appraised

The creep of multi-layered moderately thick shells of revolution under asymmetrical loading

International Nuclear Information System (INIS)

Takezono, S.; Migita, K.

1987-01-01

In the present paper the authors study the creep deformation of the multi-layered thick shells of revolution under asymmetrical loads. The equations of equilibrium and the strain-displacement relations are derived from the Reissner-Naghdi theory (1941, 1957) for elastic shells where a consideration on the effect of shear deformation is given. In the theory of creep it is assumed that in a given increment of time the total strain increments are composed of an elastic part and a part due to creep. The elastic strains are proportional to the stresses by Hooke's law. For the constitutive equations in the creep range, McVetty's equation modified by Arrhenius' equation for thermal effect is employed. The basic differential equations on the creep problems derived for the incremental values with respect to time are numerically solved by a finite difference method and the solutions at any time are obtained by summation of the incremental values. Resultant forces and resultant moments are given from numerical integration of the stresses by Simpson's 1/3 rules. (orig./GL)

Creep life assessment of Mod.9Cr-1Mo steel. Pt. 2. Quantitative evaluation of microstructural damage in creep-interrupted specimens

International Nuclear Information System (INIS)

Sawada, Kota; Maruyama, Kouichi; Komine, Ryuji; Nagae, Yuji

1998-02-01

Mod.9Cr-1Mo steel has a martensitic lath structure. Recovery of the lath structure takes place in the course of creep. Microstructural degradation due to the recovery results in the acceleration of creep rate and the subsequent failure of a specimen. Change of lath width during creep of the steel was quantitatively investigated to propose a residual life assessment methodology based on the recovery process. Since the steel was tempered at 1053K, the lath structure is thermally stable at the testing temperatures (848K-923K). However, recovery of lath structure readily takes place during creep, indicating that the recovery is induced by creep deformation. Lath width d increases with creep strain and saturates to a value d s determined by creep stress. The increase of d is faster at a higher stress and temperature. A normalized change in lath width, Δd/Δd s , was introduced to explain the variation of lath growth rate with creep stress and temperature. Δd is the change in lath width from the initial value d 0 , and Δd s is the difference between d s and d 0 . Δd/Δd s is uniquely related to creep strain ε and the relationship is independent of creep stress as well as creep temperature. This Δd/Δd s -ε relationship obtained by an accelerated creep test at a higher temperature or stress is applicable to any creep condition including service conditions of engineering plants. Creep strain can be evaluated from the measurement of Δd/Δd s based on the Δd/Δd s -ε relationship. A creep curve under any creep condition can readily be calculated by creep data of the steel. Combining these information one can assess residual life of a structural component made of the steel. (author)

Effect of simulated sampling disturbance on creep behaviour of rock salt

Science.gov (United States)

Guessous, Z.; Gill, D. E.; Ladanyi, B.

1987-10-01

This article presents the results of an experimental study of creep behaviour of a rock salt under uniaxial compression as a function of prestrain, simulating sampling disturbance. The prestrain was produced by radial compressive loading of the specimens prior to creep testing. The tests were conducted on an artifical salt to avoid excessive scattering of the results. The results obtained from several series of single-stage creep tests show that, at short-term, the creep response of salt is strongly affected by the preloading history of samples. The nature of this effect depends upon the intensity of radial compressive preloading, and its magnitude is a function of the creep stress level. The effect, however, decreases with increasing plastic deformation, indicating that large creep strains may eventually lead to a complete loss of preloading memory.

Flexural creep of coated SiC-fiber-reinforced glass-ceramic composites

International Nuclear Information System (INIS)

Sun, E.Y.

1995-01-01

This study reports the flexural creep behavior of a fiber-reinforced glass-ceramic and associated changes in microstructure. SiC fibers were coated with a dual layer of SiC/BN to provide a weak interface that was stable at high temperatures. Flexural creep, creep-rupture, and creep-strain recovery experiments were conducted on composite material and barium-magnesium aluminosilicate matrix from 1,000 to 1,200 C. Below 1,130 C, creep rates were extremely low (∼10 -9 s -1 ), preventing accurate measurement of the stress dependence. Above 1,130 C, creep rates were in the 10 -8 s -1 range. The creep-rupture strength of the composite at 1,100 C was about 75--80% of the fast fracture strength. Creep-strain recovery experiments showed recovery of up to 90% under prolonged unloading. Experimental creep results from the composite and the matrix were compared, and microstructural observations by TEM were employed to assess the effectiveness of the fiber coatings and to determine the mechanism(s) of creep deformation and damage

A planar model study of creep in metal matrix composites with misaligned short fibres

DEFF Research Database (Denmark)

Sørensen, N.J.

1993-01-01

The effect of fibre misalignment on the creep behaviour of metal matrix composites is modelled, including hardening behaviour (stage 1), dynamic recovery and steady state creep (stage 2) of the matrix material, using an internal variable constitutive model for the creep behaviour of the metal...... matrix. Numerical plane strain results in terms of average properties and detailed local deformation behaviour up to large strains are needed to show effects of fibre misalignment on the development of inelastic strains and the resulting over-all creep resistance of the material. The creep resistance...

On the microstructural basis of creep strength and creep-fatigue interaction in 9-12 % Cr steels for application in power plants

Energy Technology Data Exchange (ETDEWEB)

Chilukuru, H

2007-03-06

As part of the efforts of preserving the environment it is necessary to reduce of the CO2 emissions from power plants. This can be done by increasing the plant efficiency. Research groups around the world are engaged in developing new steels capable of sustaining higher stresses and temperatures envisaged for high-efficiency power plants. Research carried out in Europe is organized within the COST Programme (Co-Operation in Science and Technology) aiming at replacing the conventional steels of type X20CrMoV121 by the new class of 9-12% Cr-steels with modified composition. The resistance of materials against deformation at elevated temperatures depends on their microstructure. Frequently in 9-12% Cr-steels improved short-term creep properties do not persist in the long-term service [1, 2, 3, 4, 5, 6]. This is related with insufficient microstructural stability. Hardening contributions in 9-12% Cr-steels come from solute atoms of the ferritic matrix, from dislocations, and from precipitates of foreign phases within the matrix. The term ''carbide stabilized substructure hardening'' of 9-12% Cr steels [7, 8] indicates that the hardening contributions are interdependent. The dislocations are the carriers of plastic deformation. They interact with each other, with solute atoms and with precipitates. The dislocation-dislocation interaction leads to formation of planar dislocation networks constituting low-angle boundaries. They form a subgrain structure within the grains. At present, a full and detailed understanding of the effects exerted by the different components of microstructure on creep strength is still lacking. The present work makes a contribution to the efforts of understanding the microstructural basis of creep strength and of creep-fatigue interaction by transmission electron microscopic structure investigations coupled with creep tests. Investigations by transmission electron microscopy (TEM) were carried out with regard to hardening by subgrain boundaries

On the microstructural basis of creep strength and creep-fatigue interaction in 9-12 % Cr steels for application in power plants

Energy Technology Data Exchange (ETDEWEB)

Chilukuru, H.

2007-03-06

As part of the efforts of preserving the environment it is necessary to reduce of the CO2 emissions from power plants. This can be done by increasing the plant efficiency. Research groups around the world are engaged in developing new steels capable of sustaining higher stresses and temperatures envisaged for high-efficiency power plants. Research carried out in Europe is organized within the COST Programme (Co-Operation in Science and Technology) aiming at replacing the conventional steels of type X20CrMoV121 by the new class of 9-12% Cr-steels with modified composition. The resistance of materials against deformation at elevated temperatures depends on their microstructure. Frequently in 9-12% Cr-steels improved short-term creep properties do not persist in the long-term service [1, 2, 3, 4, 5, 6]. This is related with insufficient microstructural stability. Hardening contributions in 9-12% Cr-steels come from solute atoms of the ferritic matrix, from dislocations, and from precipitates of foreign phases within the matrix. The term ''carbide stabilized substructure hardening'' of 9-12% Cr steels [7, 8] indicates that the hardening contributions are interdependent. The dislocations are the carriers of plastic deformation. They interact with each other, with solute atoms and with precipitates. The dislocation-dislocation interaction leads to formation of planar dislocation networks constituting low-angle boundaries. They form a subgrain structure within the grains. At present, a full and detailed understanding of the effects exerted by the different components of microstructure on creep strength is still lacking. The present work makes a contribution to the efforts of understanding the microstructural basis of creep strength and of creep-fatigue interaction by transmission electron microscopic structure investigations coupled with creep tests. Investigations by transmission electron microscopy (TEM) were carried out with regard to hardening by

High-temperature transient creep properties of CANDU pressure tubes

International Nuclear Information System (INIS)

Fong, R.W.L.; Chow, C.K.

2002-06-01

During a hypothetical large break loss-of-coolant accident (LOCA), the coolant flow would be reduced in some fuel channels and would stagnate and cause the fuel temperature to rise and overheat the pressure tube. The overheated pressure tube could balloon (creep radially) into contact with its moderator-cooled calandria tube. Upon contact, the stored thermal energy in the pressure tube is transferred to the calandria tube and into the moderator, which acts as a heat sink. For safety analyses, the modelling of fuel channel deformation behaviour during a large LOCA requires a sound knowledge of the high-temperature creep properties of Zr-2.5Nb pressure tubes. To this extent, a ballooning model to predict pressure-tube deformation was developed by Shewfelt et al., based on creep equations derived using uniaxial tensile specimens. It has been recognized, however, that there is an inherent variability in the high-temperature creep properties of CANDU pressure tubes. The variability, can be due to different tube-manufacturing practices, variations in chemical compositions, and changes in microstructure induced by irradiation during service in the reactor. It is important to quantify the variability of high-temperature creep properties so that accurate predictions on pressure-tube creep behaviour can be made. This paper summarizes recent data obtained from high-temperature uniaxial creep tests performed on specimens taken from both unirradiated (offcut) and irradiated pressure tubes, suggesting that the variability is attributed mainly to the initial differences in microstructure (grain size, shape and preferred orientation) and also from tube-to-tube variations in chemical composition, rather than due to irradiation exposure. These data will provide safety analysts with the means to quantify the uncertainties in the prediction of pressure-tube contact temperatures during a postulated large break LOCA. (author)

Anomalous creep behaviour of 316 stainless steel at 550 deg C

International Nuclear Information System (INIS)

Hyde, T.H.

1986-01-01

The results of fifteen constant-load creep tests at 550 0 C, with nominal stresses in the range 200 to 360 MPa and with test durations of up to 14000h, are presented. The usual primary, secondary and tertiary creep behaviour was exhibited for nominal stresses greater than about 330 MPa. At lower stresses, 'renewed' primary and secondary creep regions were observed. The renewed secondary creep strain rates were found to be about an order of magnitude greater than the initial secondary creep strain rates. The results indicate that the occurence of the renewed primary and secondary creep regions is associated with time-dependent exposure to a temperature of 550 0 C. The presence or magnitude of the prior stress level does not appear to have any significant effect. The results are relevant to design procedures because extrapolation of short duration or high stress data to long-term design lifetimes is often required. Unless the possibility of the occurence of renewed primary and secondary creep is taken into account, gross errors in strain predictions could occur. (author)

Creep behavior evaluation of welded joint

International Nuclear Information System (INIS)

Susei, Shuzo; Matsui, Shigetomo; Mori, Eisuke; Shimizu, Shigeki; Satoh, Keisuke.

1980-01-01

In the creep design of high temperature structural elements, it is necessary to grasp the creep performance of joints as a whole, paying attention to the essential lack of uniformity between the material qualities of parent metals and welds. In this study, the factors controlling the creep performance of butt welded joints were investigated theoretically, when they were subjected to lateral tension and longitudinal tension. It was clarified that the rupture time in the case of laterally pulled joints was determined by the ratio of the creep rupture times of weld metals and parent metals, and the rupture time in the case of longitudinally pulled joints was determined by the ratio of the creep rupture times and the ratio of the creep strain rates of weld metals and parent metals. Moreover, when the joints of the former ratio less than 1 and the latter ratio larger than 1 were investigated experimentally, the rupture time in the case of laterally pulled joints was affected by the relative thickness, and when the relative thickness was large, the theoretical and the experimental values coincided, but the relative thickness was small, the theoretical values gave the evaluation on safe side as compared with the experimental values due to the effect of restricting deformation. In the case of longitudinally pulled joints, the theoretical and the experimental values coincided relatively well. The diagram of classifying the creep performance of welded joints was proposed. (Kako, I.)

Evaluation of long-term creep behaviour on K-cladding tubes

International Nuclear Information System (INIS)

Bang, J. G.; Jeong, Y. H.; Jeong, Y. H.

2003-01-01

KAERI has developed new zirconium alloys for high burnup fuel cladding. To evaluate the performance of these alloys, various out-pile tests are conducting. At high burnup, the creep resistance as well as corrosion resistance is one of the major factors determining nuclear fuel performance. Long-term creep test was performed at 350 .deg. C and 400 .deg. C and 100, 120, 135, and 150 MPa of applied hoop stress to evaluate the creep properties. The creep resistance was strongly affected by the final heat treatment conditions, while there was no effect of intermediate heat treatment. The creep strain of the recrystallized alloys is higher than that of the stress-relieved alloys by a factor of 3. The alloying elements also influenced the creep behaviour. Increase of Sn content enhanced the creep resistance, while Nb decreased the creep resistance. As a result of texture analysis, basal pole was directed to normal direction, while prism pole was to rolling direction. The development of the deformation texture and the ammealing texture showed almost similar process to Zircaloy cladding

Superplastic Creep of Metal Nanowires From Rate-Dependent Plasticity Transition.

Science.gov (United States)

Tao, Weiwei; Cao, Penghui; Park, Harold S

2018-04-30

Understanding the time-dependent mechanical behavior of nanomaterials such as nanowires is essential to predict their reliability in nanomechanical devices. This understanding is typically obtained using creep tests, which are the most fundamental loading mechanism by which the time-dependent deformation of materials is characterized. However, due to existing challenges facing both experimentalists and theorists, the time-dependent mechanical response of nanowires is not well-understood. Here, we use atomistic simulations that can access experimental time scales to examine the creep of single crystal FCC metal (Cu, Ag, Pt) nanowires. We report that both Cu and Ag nanowires show significantly increased ductility and superplasticity under low creep stresses, where the superplasticity is driven by a rate-dependent transition in defect nucleation from twinning to trailing partial dislocations at the micro or millisecond timescale. The transition in deformation mechanism also governs a corresponding transition in the stress-dependent creep time at the microsecond (Ag) and millisecond (Cu) timescales. Overall, this work demonstrates the necessity of accessing timescales that far exceed those seen in conventional atomistic modeling for accurate insights into the time-dependent mechanical behavior and properties of nanomaterials.

Measurement of Creep Properties of Ultra-High-Temperature Materials by a Novel Non-Contact Technique

Science.gov (United States)

Hyers, Robert W.; Lee, Jonghyun; Rogers, Jan R.; Liaw, Peter K.

2007-01-01

A non-contact technique for measuring the creep properties of materials has been developed and validated as part of a collaboration among the University of Massachusetts, NASA Marshall Space Flight Center Electrostatic Levitation Facility (ESL), and the University of Tennessee. This novel method has several advantages over conventional creep testing. The sample is deformed by the centripetal acceleration from the rapid rotation, and the deformed shapes are analyzed to determine the strain. Since there is no contact with grips, there is no theoretical maximum temperature and no concern about chemical compatibility. Materials may be tested at the service temperature even for extreme environments such as rocket nozzles, or above the service temperature for accelerated testing of materials for applications such as jet engines or turbopumps for liquid-fueled engines. The creep measurements have been demonstrated to 2400 C with niobium, while the test facility, the NASA MSFC ESL, has processed materials up to 3400 C. Furthermore, the ESL creep method employs a distribution of stress to determine the stress exponent from a single test, versus the many tests required by conventional methods. Determination of the stress exponent from the ESL creep tests requires very precise measurement of the surface shape of the deformed sample for comparison to deformations predicted by finite element models for different stress exponents. An error analysis shows that the stress exponent can be determined to about 1% accuracy with the current methods and apparatus. The creep properties of single-crystal niobium at 1985 C showed excellent agreement with conventional tests performed according to ASTM Standard E-139. Tests on other metals, ceramics, and composites relevant to rocket propulsion and turbine engines are underway.

Influence of loading path and precipitates on indentation creep behavior of wrought Mg–6 wt% Al–1 wt% Zn magnesium alloy

Energy Technology Data Exchange (ETDEWEB)

Nautiyal, Pranjal [Discipline of Mechanical Engineering, Indian Institute of Information Technology, Design & Manufacturing, Jabalpur, Madhya Pradesh 482005 (India); Department of Applied Mechanics, Indian Institute of Technology, Delhi 110016 (India); Jain, Jayant [Department of Applied Mechanics, Indian Institute of Technology, Delhi 110016 (India); Agarwal, Arvind, E-mail: agarwala@fiu.edu [Department of Mechanical and Materials Engineering, Florida International University, Miami, FL 33174 (United States)

2016-01-05

This study reports the effect of loading path and precipitates on indentation induced creep behavior of AZ61 magnesium alloy. Indentation creep tests were performed on solution-treated and peak-aged extruded AZ61 magnesium alloy, and Atomic Force Microscopy (AFM) investigations were carried out to study deformation mechanisms. Twinning is the dominant creep mechanism for indentation along the extrusion direction (ED) in solution-treated alloy. A combination of slip and twinning appears to be the prominent mechanisms for indentation creep perpendicular to ED. Creep flow is arrested for indentation perpendicular to ED, due to slip–twin interactions. Influence of precipitates on creep deformation was also studied. Aged specimen exhibited higher creep resistance than solution-treated specimen. Unlike solution-treated specimens, twinning was not observed in aged alloy. Creep in aged specimen was attributed to slip.

Mechanism of creep in stainless steel

International Nuclear Information System (INIS)

Monteiro, S.N.; Silveira, T.L.

In the present work the creep criterions to identify the deformation mechanisms through the exponent of the strain rate versus stress relationship are presented. When applied to several stainless steels these criterions show an apparent contradiction for the proper mechanism acting at Σ/D above 10 9 /cm 2 . Microstructural aspects interfering in different manners with the fracture of these steels could be a reason for rationalizing the contradictory behavior. This is discussed in suggested deformation maps for the steels investigated [pt

Evaluation of permanent deformation of CRM-reinforced SMA and its correlation with dynamic stiffness and dynamic creep.

Science.gov (United States)

Mashaan, Nuha Salim; Karim, Mohamed Rehan

2013-01-01

Today, rapid economic and industrial growth generates increasing amounts of waste materials such as waste tyre rubber. Attempts to inspire a green technology which is more environmentally friendly that can produce economic value are a major consideration in the utilization of waste materials. The aim of this study is to evaluate the effect of waste tyre rubber (crumb rubber modifier (CRM)), in stone mastic asphalt (SMA 20) performance. The virgin bitumen (80/100) penetration grade was used, modified with crumb rubber at four different modification levels, namely, 6%, 12%, 16%, and 20% by weight of the bitumen. The testing undertaken on the asphalt mix comprises the indirect tensile (dynamic stiffness), dynamic creep, and wheel tracking tests. By the experimentation, the appropriate amount of CRM was found to be 16% by weight of bitumen. The results show that the addition of CRM into the mixture has an obvious significant effect on the performance properties of SMA which could improve the mixture's resistance against permanent deformation. Further, higher correlation coefficient was obtained between the rut depth and permanent strain as compared to resilient modulus; thus dynamic creep test might be a more reliable test in evaluating the rut resistance of asphalt mixture.

Evaluation of Permanent Deformation of CRM-Reinforced SMA and Its Correlation with Dynamic Stiffness and Dynamic Creep

Directory of Open Access Journals (Sweden)

Nuha Salim Mashaan

2013-01-01

Full Text Available Today, rapid economic and industrial growth generates increasing amounts of waste materials such as waste tyre rubber. Attempts to inspire a green technology which is more environmentally friendly that can produce economic value are a major consideration in the utilization of waste materials. The aim of this study is to evaluate the effect of waste tyre rubber (crumb rubber modifier (CRM, in stone mastic asphalt (SMA 20 performance. The virgin bitumen (80/100 penetration grade was used, modified with crumb rubber at four different modification levels, namely, 6%, 12%, 16%, and 20% by weight of the bitumen. The testing undertaken on the asphalt mix comprises the indirect tensile (dynamic stiffness, dynamic creep, and wheel tracking tests. By the experimentation, the appropriate amount of CRM was found to be 16% by weight of bitumen. The results show that the addition of CRM into the mixture has an obvious significant effect on the performance properties of SMA which could improve the mixture's resistance against permanent deformation. Further, higher correlation coefficient was obtained between the rut depth and permanent strain as compared to resilient modulus; thus dynamic creep test might be a more reliable test in evaluating the rut resistance of asphalt mixture.

Creep properties of Hastelloy X and their application to structural design

International Nuclear Information System (INIS)

Kiyoshige, Masanori; Murase, Koichi; Fujioka, Junzo; Shimizu, Shigeki; Satoh, Keisuke

1977-01-01

Creep and stress rupture tests on three heats of Hastelloy X differing in the manufacturing process were carried out at 800 0 C, 900 0 C and 1000 0 C. Interpretation of the observed creep properties was made, and a method for predicting necessary design data from the experimentally obtained results was discussed. The results are as follows. (1) It was difficult to separate the primary, secondary and tertiary creep stages in the creep curve of Hastelloy X of the present tests. However, those were made distinguishable by plotting the results in a double-logarithmic coordinates. From these creep rate curves, the primary and secondary creep rates and the times to the initiation of secondary and tertiary creeps were derived. (2) It is considered that the same stress and temperature dependences between the primary and secondary creep rates exist in the creep behaviour of Hastelloy X of the present tests. (3) All the creep data, except the isochronous stress-strain curve, required for the design such as stress vs. rupture time, stress vs. secondary creep rate and stress vs. time to initiation of tertiary creep could be arranged through the Larson-Miller parameter. On the other hand, the isochronous stress-strain curve was figured out by estimating creep curves. The constitutive equations of creep for a heat of Hastelloy X proposed in this paper and the isochronous stress-strain curves derived from these constitutive equations were consistent with the experimental data obtained for the corresponding material. (auth.)

Effects of mechanical-thermal treatments on the creep behaviour of a niobium stabilized stainless steel

International Nuclear Information System (INIS)

Rossi, J.L.

1987-01-01

The influence of microstructural variables controlled by mechanical-thermal treatments on the creep behavior of DIN-Werkstoff Nr. 1,4981 stainless steel a material candidate for use as cladding of fast breeder reactor fuel elements, was studied. The effect of the solution treatment, predeformation, predeformation plus aging and cycles of predeformation-aging, on the creep results obtained at 990 K, for applied stresses in the range 70 MPa - 310 MPa, are analysed. The results show: this material presents a creep strength superior to that show by AISI 316 stainless steel; a transition on the creep behavior is observed at a certain stress; the mechanical-thermal treatments were seen to be ineffective on the improvement of the creep strength; the pre-deformation and pre-deformation plus aging treatments were seen to induce material embrittlement whereas the cyclic treatments induced increased ductility. Transmission electron microscopy, X ray diffraction of extracted precipitates, and microanalysis were use to characterize the microstructure of this material. (author)

Creep and inverse stress relaxation behaviors of carbon nanotube yarns.

Science.gov (United States)

Misak, H E; Sabelkin, V; Miller, L; Asmatulu, R; Mall, S

2013-12-01

Creep, creep recovery and inverse stress relaxation behaviors of carbon nanotube yarns that consisted of 1-, 30-, and 100-yarn(s) were characterized. Primary and secondary creep stages were observed over the duration of 336 h. The primary creep stage lasted for about 4 h at an applied load equal to 75% of the ultimate tensile strength. The total strain in the primary stage was significantly larger in the carbon nanotube multi-yarn than in the carbon nanotube 1-yarn. In the secondary stage, 1-yarn also had a smaller steady state strain rate than the multi-yarn, and it was independent of number of yarns in multi-yarn. Strain response under cyclic creep loading condition was comparable to its counterpart in non-cyclic (i.e., standard) creep test except that strain response during the first cycle was slightly different from the subsequent cycles. Inverse creep (i.e., strain recovery) was observed in the 100-yarn during the cyclic creep tests after the first unloading cycle. Furthermore, inverse stress relaxation of the multi-yarns was characterized. Inverse stress relaxation was larger and for longer duration with the larger number of yarns.

Effect of Long-Term Thermal Exposures on Microstructure and Impression Creep in 304HCu Grade Austenitic Stainless Steel

Science.gov (United States)

Dash, Manmath Kumar; Karthikeyan, T.; Mythili, R.; Vijayanand, V. D.; Saroja, S.

2017-10-01

This paper presents the results of microstructural evolution and mechanical properties in 304H Cu grade austenite stainless (SS 304HCu) during long-term exposure at high temperatures. The predicted phase composition as a function of temperature obtained using JMatPro® software was confirmed in conjunction with the microstructural evolution characterized by scanning and transmission electron microscopy. Microstructures revealed primary Nb(C,N), M23C6 precipitates at γ-grain boundaries, fine secondary Nb(C,N) intragranular carbides, and a uniform precipitation of <40-nm-sized spherical Cu-rich phase after thermal aging for 10,000 hours at 903 K (630 °C). The impression creep rate at 300 MPa increased by a factor of 20 between 873 K and 923 K (600 °C and 650 °C). The creep rate at 903 K (630 °C) was found to moderately reduce with aging time, signifying the role of Cu-rich phase in improving the creep resistance. The deformation zones and the recrystallization behavior of the plastic zone in creep tested specimen was assessed using Electron backscatter diffraction technique.

Nanoindentation creep behavior of human enamel.

Science.gov (United States)

He, Li-Hong; Swain, Michael V

2009-11-01

In this study, the indentation creep behavior of human enamel was investigated with a nanoindentation system and a Berkovich indenter at a force of 250 mN with one-step loading and unloading method. A constant hold period of 900 s was incorporated into each test at the maximum load as well at 5 mN minimum load during unloading. The indentation creep at the maximum load and creep recovery at the minimum load was described with a double exponential function and compared with other classic viscoelastic models (Debye/Maxwell and Kohlrausch-Williams-Watts). Indentation creep rate sensitivity, m, of human enamel was measured for the first time with a value of approximately 0.012. Enamel displayed both viscoelastic and viscoplastic behavior similar to that of bone. These results indicate that, associated with entrapment of particulates between teeth under functional loading and sliding wear conditions, the enamel may inelastically deform but recover upon its release. This behavior may be important in explaining the excellent wear resistance, antifatigue, and crack resistant abilities of natural tooth structure. (c) 2008 Wiley Periodicals, Inc.

Creep simulation of adhesively bonded joints using modified generalized time hardening model

Energy Technology Data Exchange (ETDEWEB)

Sadigh, Mohammad Ali Saeimi [Azarbaijan Shahid Madani University, Tabriz (Iran, Islamic Republic of)

2016-04-15

Creep behavior of double lap adhesively bonded joints was investigated using experimental tests and numerical analysis. Firstly, uniaxial creep tests were carried out to obtain the creep characteristics and constitutive parameters of the adhesive at different stress and temperature levels. Generalized time hardening model was used to predict the creep behavior of the adhesive. This model was modified to simulate the creep behavior at different stress and temperature levels. Secondly, the developed model was used to simulate the creep behavior of bonded joints using finite element based numerical analysis. Creep deformations of the joints were measured experimentally and good agreement was observed in comparison with the results obtained using numerical simulation. Afterward, stress redistribution due to the creep along the adhesively bonded joint was obtained numerically. It was observed that temperature level had a significant effect on the stress redistribution along the adhesive thickness.

The transient creep of vapor deposited Ti-6Al-4V

International Nuclear Information System (INIS)

Warren, J.; Wadley, H.N.G.

1996-01-01

Titanium matrix composites can be synthesized by the consolidation of ceramic fibers (for example, alumina and silicon carbide monofilaments) coated with titanium alloy deposited on the fiber by physical vapor deposition (PVD). Consolidation involves deformation of the matrix coating by both transient and steady-state creep. In a recent paper the mechanisms responsible for steady-state creep in PVD Ti-6Al-4V, between 600 and 900 C, were determined. The analysis of the data first presented has been extended here to consider the transient creep behavior of the material and identify an analogous constitutive law for use in simulating the transient creep contribution to consolidation

Grain-boundary sliding in a TiAl alloy with fine-grained duplex microstructure during 750 deg. C creep

Energy Technology Data Exchange (ETDEWEB)

Peter, D. [Ruhr University Bochum, Institute for Materials, D-44780 Bochum (Germany); Viswanathan, G.B., E-mail: Viswanathan.11@osu.edu [Ruhr University Bochum, Institute for Materials, D-44780 Bochum (Germany) and Department of Materials Science and Engineering, Ohio State University, Columbus, OH 43210 (United States); Wagner, M.F.-X.; Eggeler, G. [Ruhr University Bochum, Institute for Materials, D-44780 Bochum (Germany)

2009-06-15

Constant-load creep experiments at a temperature of 750 deg. C and a nominal stress of 300 MPa were conducted on a fine-grained Ti-45Al-5Nb-0.2B-0.2C (in at.%) alloy with a duplex microstructure. Microstructures before and after creep (accumulated strain: 9.6%) were analyzed using scanning and transmission electron microscopy (SEM and TEM). TEM analysis after creep indicates that the individual microstructural constituents of the fine duplex microstructure, namely, the equiaxed {gamma} and the lamellar {alpha}{sub 2}/{gamma} colonies, undergo varying degrees of deformation and develop various substructures. Lamellar grains deform by dislocation creep. They show clear evidence for dislocation and twin activity. In contrast, only few dislocations are found in the equiaxed grains. We show that the regions with small equiaxed {gamma} grains, representing 65-75 vol.% of the microstructure, deform by grain-boundary sliding.

Grain-boundary sliding in a TiAl alloy with fine-grained duplex microstructure during 750 deg. C creep

International Nuclear Information System (INIS)

Peter, D.; Viswanathan, G.B.; Wagner, M.F.-X.; Eggeler, G.

2009-01-01

Constant-load creep experiments at a temperature of 750 deg. C and a nominal stress of 300 MPa were conducted on a fine-grained Ti-45Al-5Nb-0.2B-0.2C (in at.%) alloy with a duplex microstructure. Microstructures before and after creep (accumulated strain: 9.6%) were analyzed using scanning and transmission electron microscopy (SEM and TEM). TEM analysis after creep indicates that the individual microstructural constituents of the fine duplex microstructure, namely, the equiaxed γ and the lamellar α 2 /γ colonies, undergo varying degrees of deformation and develop various substructures. Lamellar grains deform by dislocation creep. They show clear evidence for dislocation and twin activity. In contrast, only few dislocations are found in the equiaxed grains. We show that the regions with small equiaxed γ grains, representing 65-75 vol.% of the microstructure, deform by grain-boundary sliding.

Predicting Hot Deformation of AA5182 Sheet

Science.gov (United States)

Lee, John T.; Carpenter, Alexander J.; Jodlowski, Jakub P.; Taleff, Eric M.

Aluminum 5000-series alloy sheet materials exhibit substantial ductilities at hot and warm temperatures, even when grain size is not particularly fine. The relatively high strain-rate sensitivity exhibited by these non-superplastic materials, when deforming under solute-drag creep, is a primary contributor to large tensile ductilities. This active deformation mechanism influences both plastic flow and microstructure evolution across conditions of interest for hot- and warm-forming. Data are presented from uniaxial tensile and biaxial bulge tests of AA5182 sheet material at elevated temperatures. These data are used to construct a material constitutive model for plastic flow, which is applied in finite-element-method (FEM) simulations of plastic deformation under multiaxial stress states. Simulation results are directly compared against experimental data to explore the usefulness of this constitutive model. The effects of temperature and stress state on plastic response and microstructure evolution are discussed.

FY17 Status Report on the Micromechanical Finite Element Modeling of Creep Fracture of Grade 91 Steel

Energy Technology Data Exchange (ETDEWEB)

Messner, M. C. [Argonne National Lab. (ANL), Argonne, IL (United States); Truster, T. J. [Univ. of Tennessee, Knoxville, TN (United States); Cochran, K. B. [DR& C Inc.; Parks, D. M. [DR& C Inc.; Sham, T. -L. [Argonne National Lab. (ANL), Argonne, IL (United States)

2017-09-01

Advanced reactors designed to operate at higher temperatures than current light water reactors require structural materials with high creep strength and creep-fatigue resistance to achieve long design lives. Grade 91 is a ferritic/martensitic steel designed for long creep life at elevated temperatures. It has been selected as a candidate material for sodium fast reactor intermediate heat exchangers and other advanced reactor structural components. This report focuses on the creep deformation and rupture life of Grade 91 steel. The time required to complete an experiment limits the availability of long-life creep data for Grade 91 and other structural materials. Design methods often extrapolate the available shorter-term experimental data to longer design lives. However, extrapolation methods tacitly assume the underlying material mechanisms causing creep for long-life/low-stress conditions are the same as the mechanisms controlling creep in the short-life/high-stress experiments. A change in mechanism for long-term creep could cause design methods based on extrapolation to be non-conservative. The goal for physically-based microstructural models is to accurately predict material response in experimentally-inaccessible regions of design space. An accurate physically-based model for creep represents all the material mechanisms that contribute to creep deformation and damage and predicts the relative influence of each mechanism, which changes with loading conditions. Ideally, the individual mechanism models adhere to the material physics and not an empirical calibration to experimental data and so the model remains predictive for a wider range of loading conditions. This report describes such a physically-based microstructural model for Grade 91 at 600° C. The model explicitly represents competing dislocation and diffusional mechanisms in both the grain bulk and grain boundaries. The model accurately recovers the available experimental creep curves at higher stresses

Advances in the assessment of creep data

Energy Technology Data Exchange (ETDEWEB)

Holdsworth, S.R.

2010-07-01

Many of the classical models representing the creep and rupture behaviour of metals were developed prior to and during the 1950s and 1960s, and their subsequent exploitation, in particular for the assessment of large creep property datasets, was initially limited by the capability of the analytical tools available at the time. The formation of ECCC (the European Creep Collaborative Committee) in 1991, with a main objective of providing reliable peer reviewed long-time creep property values for European Design and Product Standards, led to the development of rigorous assessment procedures such as PD6605 and DESA incorporating post assessment tests to verify: physical realism, effectiveness of model-fit within the range of the source experimental data, and extrapolation credibility. The first ECCC assessment recommendations published in 1996 undoubtedly provided a catalyst for others to exploit the availability of low cost, powerful desktop computers to develop rigorous methodologies for the physically realistic analysis of uniaxial and multi-axial data for the reliable and accurate characterisation of creep strain, and rupture strength and ductility properties. More recent improvements in data assessment methodologies have been driven by the need to effectively model the creep deformation and rupture characteristics of the complex new generation alloys and fabrications being designed to cater for the continually evolving requirements of modern advanced power plant. These advances in the assessment of creep data are reviewed. (orig.)

A study of precipitation phenomena during the creep of austenitic stainless steels

International Nuclear Information System (INIS)

Le May, I.; White, W.E.; Bassett, B.J.

1975-01-01

Creep-rupture data for two austenitic stainless steels, AISI Types 310 and 316, are presented, together with observations of precipitation taking place during creep. While the effects of creep deformation on precipitation in the Type 310 were negligible, ferrite precipitation was considerably greater in the Type 316 undergoing creep than in unstressed material. Ferrite precipitation appears to promote grain boundary cavitation and internal cracking, thus reducing creep resistance, and a correlation has been noted between increased ferrite precipitation and apparent further weakening of the Type 316 over the temperature range 730 0 C to 800 0 C approximately, as evidenced by breaks in the isostress lines on a plot of log (time to rupture) versus temperature. (author)

Microstructural degradation mechanisms during creep in strength enhanced high Cr ferritic steels and their evaluation by hardness measurement

International Nuclear Information System (INIS)

Ghassemi Armaki, Hassan; Chen, Ruiping; Kano, Satoshi; Maruyama, Kouichi; Hasegawa, Yasushi; Igarashi, Masaaki

2011-01-01

Graphical abstract: Effect of static recovery on the acceleration of subgrain coarsening during creep plastic deformation. Display Omitted Highlights: → Short-term 'H' and long-term 'L' creep regions have different creep characteristics. → Strain-induced recovery of subgrains proceeds in the both creep regions 'H' and 'L'. → In region ''L', two additional degradation mechanisms accelerate creep failure. → Thermal coarsening of precipitates and subgrains appear during long-term creep ''L'. → In region 'L', strain-induced coarsening of precipitates accelerates creep failure. - Abstract: There are two creep regions with different creep characteristics: short-term creep region 'H', where precipitates and subgrains are thermally stable, and long-term creep region 'L', where thermal coarsening of precipitates and subgrains appear. In region 'H', the normalized subgrain size (λ-λ 0 )/(λ * -λ 0 ) has a linear relation with creep strain and its slope is 10ε -1 . But, region L is the time range in which the static recovery and the strain-induced recovery progress simultaneously. In this region, the static recovery accelerates the strain-induced recovery, and subgrain size is larger than that line which neglects the contribution of the static recovery. In region 'L', the Δλ/Δλ * -strain present a linear relation with a slope 35ε -1 . There is a linear relation between hardness and subgrain size. Hardness drop, H 0 - H, as a function of Larson-Miller parameter can be a good measure method for assessment of hardness drop and consequently degradation of microstructure. Hardness drop shows an identical slope in creep region 'H', whereas hardness drop due to thermal aging and creep in region 'L' show together a similar slope. In region 'H', degradation of microstructure is mainly due to recovery of subgrains controlled by creep plastic deformation, and precipitates do not have a major role. However, in creep region 'L', there are three degradation mechanisms

Constant structure creep experiments on aluminium

Czech Academy of Sciences Publication Activity Database

Milička, Karel

2011-01-01

Roč. 49, č. 5 (2011), s. 307-318 ISSN 0023-432X R&D Projects: GA AV ČR IAA2041203 Institutional research plan: CEZ:AV0Z20410507 Keywords : mechanical properties * high temperature deformation * creep * aluminium Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 0.451, year: 2011

Triaxial quasi-static compression and creep behavior of bedded salt from southeastern New Mexico

International Nuclear Information System (INIS)

Hansen, F.D.

1979-11-01

This report summarizes the results obtained from a series of triaxial quasi-static compression and creep tests on specimens of bedded salt recovered at depth intervals of 1953 to 1954 and 2711 to 2722 feet in AEC Hole No. 7 in southeastern New Mexico. The primary objective was the determination of the deformational characteristics of the salt for prescribed stress and temperature states under quasi-static and time-dependent conditions. The test conditions encompassed confining pressures of 500 and 2000 psi, differential axial stresses of 1500, 3000 and 4500 psi, temperatures of 23 and 100 0 C, and time durations of several hours to ten days. The data analysis was confined primarily to power law fits to the creep strain-time measurements and to an evaluation of the principal strain ratio behavior for the various test conditions and axial strain magnitudes

Effects of 14 MeV neutron irradiation on creep of nickel and niobium

International Nuclear Information System (INIS)

Barmore, W.; Ruotola, A.; Raymond, E.; Mukherjee, A.

1983-01-01

Flux, stress and temperature effects on the creep strength of nickel and niobium were observed in situ at the RTNS-II 14 MeV neutron source at Lawrence Livermore National Laboratory. Creep test were done on Ni and Nb near 0.3 Tsub(m) with stresses to 280 MPa in a high vacuum test unit using a digital computer for control and data acquisition. Cyclic flux tests produced dramatic changes in creep rate. This creep behavior is attributed to the point defect fluctuations in the crystal structure. Analysis of creep and stress relaxation under steady state flux indicates that an intermediate temperature, thermally activated deformation mechanism is rate controlling. (orig.)

Creep properties of a thermally grown alumina

Energy Technology Data Exchange (ETDEWEB)

Kang, K.J. [Department of Mechanical Engineering, Chonnam National University, Kwangju 500-757 (Korea, Republic of)], E-mail: kjkang@chonnam.ac.kr; Mercer, C. [Materials Department, University of California, Santa Barbara, CA 93106-5050 (United States)

2008-04-15

A unique test system has been developed to measure creep properties of actual thermally grown oxides (TGO) formed on a metal foil. The thickness of TGO, load and displacement can be monitored in situ at high temperature. Two batches of FeCrAlY alloys which differ from each other in contents of yttrium and titanium were selected as the {alpha}-Al{sub 2}O{sub 3} TGO forming materials. The creep tests were performed on {alpha}-Al{sub 2}O{sub 3} of thickness 1-4 {mu}m, thermally grown at 1200 deg. C in air. The strength of the substrate was found to be negligible, provided that the TGO and substrate thickness satisfy: h{sub TGO} > 1 {mu}m and H{sub sub} {<=} 400 {mu}m. The steady-state creep results for all four TGO thicknesses obtained on batch I reside within a narrow range, characterized by a parabolic creep relation. It is nevertheless clear that the steady-state creep rates vary with TGO thickness: decreasing as the thickness increases. For batch II, the steady-state creep rates are higher and now influenced more significantly by TGO thickness. In comparison with previous results of the creep properties for bulk polycrystalline {alpha}-Al{sub 2}O{sub 3} at a grain size of {approx}2 {mu}m, the creep rates for the TGO were apparently higher, but both were significantly affected by yttrium content. The higher creep rate and dependency on the TGO thickness led to a hypothesis that the deformation of the TGO under tensile stress at high temperature was not a result of typical creep mechanisms such as diffusion of vacancies or intra-granular motion of dislocations, but a result of inter-grain growth of TGO. Results also indicate that the amount of yttrium may influence the growth strain as well as the creep rate.

Creep collapse of thick-walled heat transfer tube subjected to external pressure at high temperature

International Nuclear Information System (INIS)

Ioka, Ikuo; Kaji, Yoshiyuki; Terunuma, Isao; Nekoya, Shin-ichi; Miyamoto, Yoshiaki

1994-09-01

A series of creep collapse tests of thick-walled heat transfer tube were examined experimentally and analytically to confirm an analytical method for creep deformation behavior of a heat transfer tube of an intermediate heat exchanger (IHX) at a depressurization accident of secondary cooling system of HTTR (High Temperature Engineering Test Reactor). The tests were carried out using thick-walled heat transfer tubes made of Hastelloy XR at 950degC in helium gas environment. The predictions of creep collapse time obtained by a general purpose FEM-code ABAQUS were in good agreement with the experimental results. A lot of cracks were observed on the outer surface of the test tubes after the creep collapse. However, the cracks did not pass through the tube wall and, therefore, the leak tightness was maintained regardless of a collapse deformation for all tubes tested. (author)

Improved Creep Measurements for Ultra-High Temperature Materials

Science.gov (United States)

Hyers, Robert W.; Ye, X.; Rogers, Jan R.

2010-01-01

Our team has developed a novel approach to measuring creep at extremely high temperatures using electrostatic levitation (ESL). This method has been demonstrated on niobium up to 2300 C, while ESL has melted tungsten (3400 C). This method has been extended to lower temperatures and higher stresses and applied to new materials, including a niobium-based superalloy, MASC. High-precision machined spheres of the sample are levitated in the NASA MSFC ESL, a national user facility and heated with a laser. The samples are rotated with an induction motor at up to 30,000 revolutions per second. The rapid rotation loads the sample through centripetal acceleration, producing a shear stress of about 60 MPa at the center, causing the sample to deform. The deformation of the sample is captured on high-speed video, which is analyzed by machine-vision software from the University of Massachusetts. The deformations are compared to finite element models to determine the constitutive constants in the creep relation. Furthermore, the non-contact method exploits stress gradients within the sample to determine the stress exponent in a single test.

Fault zone structure and kinematics from lidar, radar, and imagery: revealing new details along the creeping San Andreas Fault

Science.gov (United States)

DeLong, S.; Donnellan, A.; Pickering, A.

2017-12-01

Aseismic fault creep, coseismic fault displacement, distributed deformation, and the relative contribution of each have important bearing on infrastructure resilience, risk reduction, and the study of earthquake physics. Furthermore, the impact of interseismic fault creep in rupture propagation scenarios, and its impact and consequently on fault segmentation and maximum earthquake magnitudes, is poorly resolved in current rupture forecast models. The creeping section of the San Andreas Fault (SAF) in Central California is an outstanding area for establishing methodology for future scientific response to damaging earthquakes and for characterizing the fine details of crustal deformation. Here, we describe how data from airborne and terrestrial laser scanning, airborne interferometric radar (UAVSAR), and optical data from satellites and UAVs can be used to characterize rates and map patterns of deformation within fault zones of varying complexity and geomorphic expression. We are evaluating laser point cloud processing, photogrammetric structure from motion, radar interferometry, sub-pixel correlation, and other techniques to characterize the relative ability of each to measure crustal deformation in two and three dimensions through time. We are collecting new and synthesizing existing data from the zone of highest interseismic creep rates along the SAF where a transition from a single main fault trace to a 1-km wide extensional stepover occurs. In the stepover region, creep measurements from alignment arrays 100 meters long across the main fault trace reveal lower rates than those in adjacent, geomorphically simpler parts of the fault. This indicates that deformation is distributed across the en echelon subsidiary faults, by creep and/or stick-slip behavior. Our objectives are to better understand how deformation is partitioned across a fault damage zone, how it is accommodated in the shallow subsurface, and to better characterize the relative amounts of fault creep

The effect of oxidation on the creep behavior of austenitic stainless steels

International Nuclear Information System (INIS)

Assis, A.M.C.A.; Monteiro, S.N.

1979-01-01

The manifestation of superficial oxidation in creep rupture tests performed with three austenitic, stainless steels under constant load in furnaces open to the atmosphere, between the temperature of 550 0 C and 800 0 C is discussed. There is experimental evidence that the superficial oxidation effects are associated, in each material, to the testing temperature, to the duration of the test and to the degree of deformation reached. The influence of the oxidatio is related to the acting deformation mechanisms. The possible corrosion action on the characteristics of the mechanical behavior of the materials under creep is analysed. (Author) [pt

Sub-Surface and Bulk Creep Behaviour of Polyurethane/Clay Nanocomposites.

Science.gov (United States)

Jin, J; Yusoh, K; Zhang, H X; Song, M

2016-03-01

A series of exfoliated and intercalated polyurethane organoclay nanocomposites were prepared by in situ polymerization of polyol/organoclay mixture, chain extender and diisocyanate. The creep behaviour of subsurface and bulk of the polyurethane coatings was investigated by nanoindentation technique and uniaxial conventional creep testing method, respectively. The results showed that the creep resistance of the nanocomposites was significantly improved by incorporation of organoclay. The enhancement of creep resistance was dependent on clay content as well as organoclay structure (exfoliation or intercalation) in the polymer matrix. With 1 wt% organoclay, the creep resistance increased by about 50% for the intercalated organoclay and 6% for the exfoliated organoclay systems, respectively, compared to the pristine polyurethane. Viscoelastic model was employed to investigate the effect of organoclay loadings on the creep performance of the polyurethane. Results showed the model was in good agreement with the experimental data. Incorporation of clay leads to an increase in elastic deformation especially in exfoliated polyurethane nanocomposites and induces a higher initial displacement at the early stage of creep.

Hot deformation of polycrystalline uranium dioxide: from microscopic mechanisms to macroscopic behaviour

International Nuclear Information System (INIS)

Dherbey, Francine

2000-01-01

The improvement of nuclear fuels performances in PWR requires in particular an enhancement of creep ability of uranium dioxide in order to minimise rupture risks of the cladding material during interactions between pellets and cladding. The aim of this study is to investigate the link between the ceramic macroscopic thermo-mechanical behaviour and the changes in the fuel microstructure during deformation. Stoichiometric UO 2 pellets with various grains sizes from 9 pm to 36 μm have been deformed by compression at intermediate temperatures, i.e. near T M /2, and quenched under stress. The damage is characterised by the presence of cavities at low stresses and cracks at high stresses, both along grain boundaries parallel to the compression axis. Inside grains, dislocations organise themselves into cellular substructures in which sub-boundaries are made of dislocation hexagonal networks. In these conditions, uranium dioxide deformation is described by grain boundary sliding, which is the main origin of material damage, partially accommodated by dislocational creep inside grains. A steady-state creep model is proposed on a physical basis. It accounts for the almost similar contributions of two mechanisms which are grain boundaries sliding and intragranular creep, and takes into account the grain boundary roughness. In contrast with phenomenological descriptions used up to now, this picture leads to a unique creep law on the whole range of stresses explored here, from 10 MPa to 80 MPa. The creep rate controlling mechanism seems to be the migration of sub-boundaries. The deformation at constant strain rate is controlled by the same mechanisms as creep. (author) [fr

Influence of specimen size on the creep of rock salt

International Nuclear Information System (INIS)

Senseny, P.E.

1982-01-01

Triaxial compression creep data for Avery Island dome salt are analyzed to determine the influence of specimen size on creep deformation. Laboratory experiments were performed on 50- and 100-mm-diameter specimens in the temperature range from 25 to 200 0 C and the axial stress difference range from 2.5 to 31.0 MPa. The strain-vs-time data from each test are divided into transient and steady-state components. Results of statistical analysis of these data show that transient creep of the small specimens is a stronger function of stress, temperature, and time than is transient creep of the larger specimens. Analysis of the steady-state data show no size effect, however. 14 references, 7 figures, 3 tables

Analytical, Numerical, and Experimental Investigation on a Non-Contact Method for the Measurements of Creep Properties of Ultra-High-Temperature Materials

Science.gov (United States)

Lee, Jonghyun; Hyers, Robert W.; Rogers, Jan R.; Rathz, Thomas J.; Choo, Hahn; Liaw, Peter

2006-01-01

Responsive access to space requires re-use of components such as rocket nozzles that operate at extremely high temperatures. For such applications, new ultra-hightemperature materials that can operate over 2,000 C are required. At the temperatures higher than the fifty percent of the melting temperature, the characterization of creep properties is indispensable. Since conventional methods for the measurement of creep is limited below 1,700 C, a new technique that can be applied at higher temperatures is strongly demanded. This research develops a non-contact method for the measurement of creep at the temperatures over 2,300 C. Using the electrostatic levitator in NASA MSFC, a spherical sample was rotated to cause creep deformation by centrifugal acceleration. The deforming sample was captured with a digital camera and analyzed to measure creep deformation. Numerical and analytical analyses have also been conducted to compare the experimental results. Analytical, numerical, and experimental results showed a good agreement with one another.

Indentation creep behavior of cold sprayed aluminum amorphous/nano-crystalline coatings

Energy Technology Data Exchange (ETDEWEB)

Babu, P. Suresh [International Advanced Research Centre for Powder Metallurgy and New Materials (ARCI), Balapur, Hyderabad 500005, Andhra Pradesh (India); Nanomechanics and Nanotribology Laboratory, Department of Mechanical and Materials Engineering, Florida International University, Miami, FL 33174 (United States); Jha, R.; Guzman, M. [Nanomechanics and Nanotribology Laboratory, Department of Mechanical and Materials Engineering, Florida International University, Miami, FL 33174 (United States); Sundararajan, G. [International Advanced Research Centre for Powder Metallurgy and New Materials (ARCI), Balapur, Hyderabad 500005, Andhra Pradesh (India); Agarwal, Arvind, E-mail: agarwala@fiu.edu [Nanomechanics and Nanotribology Laboratory, Department of Mechanical and Materials Engineering, Florida International University, Miami, FL 33174 (United States)

2016-03-21

In this study, we report room temperature creep properties of cold sprayed aluminum amorphous/nanocrystalline coating using nanoindentation technique. Creep experiments were also performed on heat treated coatings to study the structural stability and its influence on the creep behavior. The peak load and holding time were varied from 1000 to 4000 µN and 0 to 240 s respectively. Stress exponent value (n) vary from 5.6 to 2.3 in as-sprayed (AS) coatings and 7.2–4.8 in heat treated (HT) coatings at peak load of 1000–4000 µN at 240 s hold time. Higher stress exponent value indicates heat treated coatings have more resistance to creep deformation than as-sprayed coatings. Relaxed, partially crystallized structure with less porosity, and stronger inter-splat boundaries restrict the deformation in heat treated coatings as compared to greater free volume generation in amorphous as-sprayed coatings. The computed activation volume of heat treated coatings is twice of as-sprayed coatings indicating greater number of atom participation in shear band formation in heat treated coatings. The proposed mechanism was found to be consistent with the stress exponent values.

Finite element-implementation of creep of concrete for thin-shell analysis using nonlinear constitutive relations and creep compliance functions

International Nuclear Information System (INIS)

Walter, H.; Mang, H.A.

1991-01-01

A procedure for combining nonlinear short-time behavior of concrete with nonlinear creep compliance functions is presented. It is an important ingredient of a computer code for nonlinear finite element (FE) analysis of prestressed concrete shells, considering creep, shrinkage and ageing of concrete, and relaxation of the prestressing steel. The program was developed at the Institute for Strength of Materials of Technical University of Vienna, Austria. The procedure has resulted from efforts to extend the range of application of a Finite Element program, abbreviated as FESIA, which originally was capable of modeling reinforeced concrete in the context of thin-shell analysis, using nonlinear constitutive relations for both, conrete and steel. The extension encompasses the time-dependent behavior of concrete: Creep, shrinkage and ageing. Creep is modeled with the help of creep compliance functions which may be nonlinear to conform with the short-time constitutive relations. Ageing causes an interdependence between long-time and short-time deformations. The paper contains a description of the physical background of the procedure and hints on the implementation of the algorithm. The focus is on general aspects. Details of the aforementioned computer program are considered only where this is inevitable. (orig.)

Creep crack growth by grain boundary cavitation under monotonic and cyclic loading

Science.gov (United States)

Wen, Jian-Feng; Srivastava, Ankit; Benzerga, Amine; Tu, Shan-Tung; Needleman, Alan

2017-11-01

Plane strain finite deformation finite element calculations of mode I crack growth under small scale creep conditions are carried out. Attention is confined to isothermal conditions and two time histories of the applied stress intensity factor: (i) a monononic increase to a plateau value subsequently held fixed; and (ii) a cyclic time variation. The crack growth calculations are based on a micromechanics constitutive relation that couples creep deformation and damage due to grain boundary cavitation. Grain boundary cavitation, with cavity growth due to both creep and diffusion, is taken as the sole failure mechanism contributing to crack growth. The influence on the crack growth rate of loading history parameters, such as the magnitude of the applied stress intensity factor, the ratio of the applied minimum to maximum stress intensity factors, the loading rate, the hold time and the cyclic loading frequency, are explored. The crack growth rate under cyclic loading conditions is found to be greater than under monotonic creep loading with the plateau applied stress intensity factor equal to its maximum value under cyclic loading conditions. Several features of the crack growth behavior observed in creep-fatigue tests naturally emerge, for example, a Paris law type relation is obtained for cyclic loading.

Creep behaviour of polyurethanes applied in the offshore industry under dynamic service conditions

Energy Technology Data Exchange (ETDEWEB)

Aquino, Fabio G.; Sheldrake, Terry; Clevelario, Judimar; Pires, Fabio S. [Wellstream International S/A - Rio de Janeiro, RJ (Brazil)], e-mail: fabio.aquino@wellstream.com; Souza, Miguel L. [Newtech Ltda, Sao Carlos, SP (Brazil)

2011-07-01

The oil industry commonly uses flexible pipes to convey oil and gas from wells to platforms that move constantly due to weather and tidal conditions. In this scenario, polymeric components are required to transitioning between the flexible material of the pipelines to the rigid material of the platform; polyurethanes are versatile polymers suitable for performing such services. As this material is subjected to constant loading during working conditions, and it its durability is to be maintained for several decades, it is important to determine the material's creep properties that relate to deformation caused by constant loading, which can represent an indirect measurement of the material's lifetime. In this study, creep behaviour data on the polyurethane samples was collected and an asymmetrical and nonlinear behaviour was observed. Additionally the material presented a creep fracture line with points only above 150% of deformation, considerably exceeding maximum values for its service conditions, which is limited to 10% of deformation considering the worst loading case for design premises of the final artifact. (author)

Using UAVSAR to Estimate Creep Along the Superstition Hills Fault, Southern California

Science.gov (United States)

Donnellan, A.; Parker, J. W.; Pierce, M.; Wang, J.

2012-12-01

UAVSAR data were first acquired over the Salton Trough region, just north of the Mexican border in October 2009. Second passes of data were acquired on 12 and 13 April 2010, about one week following the 5 April 2010 M 7.2 El Mayor - Cucapah earthquake. The earthquake resulted in creep on several faults north of the main rupture, including the Yuha, Imperial, and Superstition Hills faults. The UAVSAR platform acquires data about every six meters in swaths about 15 km wide. Tropospheric effects and residual aircraft motion contribute to error in the estimation of surface deformation in the Repeat Pass Interferometry products. The Superstition Hills fault shows clearly in the associated radar interferogram; however, error in the data product makes it difficult to infer deformation from long profiles that cross the fault. Using the QuakeSim InSAR Profile tool we extracted line of site profiles on either side of the fault delineated in the interferogram. We were able to remove much of the correlated error by differencing profiles 250 m on either side of the fault. The result shows right-lateral creep of 1.5±.4 mm along the northern 7 km of the fault in the interferogram. The amount of creep abruptly changes to 8.4±.4 mm of right lateral creep along at least 9 km of the fault covered in the image to the south. The transition occurs within less than 100 m along the fault. We also extracted 2 km long line of site profiles perpendicular to this section of the fault. Averaging these profiles shows a step across the fault of 14.9±.3 mm with greater creep on the order of 20 mm on the northern two profiles and lower creep of about 10 mm on the southern two profiles. Nearby GPS stations P503 and P493 are consistent with this result. They also confirm that the creep event occurred at the time of the El Mayor - Cucapah earthquake. By removing regional deformation resulting from the main rupture we were able to invert for the depth of creep from the surface. Results indicate

First Research Coordination Meeting on Prediction of Axial and Radial Creep in HWR Pressure Tubes. Presentations

International Nuclear Information System (INIS)

2013-01-01

Pressure tube deformation is a critical aging issue in operating Heavy Water Reactors (HWRs). According to the service year, horizontal pressure tubes have three kinds of deformation: diametral creep leading to the flow bypass and the penalty to critical heat flux for fuel rods, longitudinal creep leading to the interference of feeder pipes and/or with fuelling machine, and sagging leading to the interference with in-core components and potential contact between the pressure tube and calandria tube. The CRP scope includes the establishment of a database for pressure tube deformation, microstructure characterization of pressure tube materials collected from HWRs currently operating in Member States and development of a prediction model for pressure tube deformation

Indentation Creep Behavior of Nugget Zone of Friction Stir Welded 2014 Aluminum Alloy

Science.gov (United States)

Das, Jayashree; Robi, P. S.; Sankar, M. Ravi

2018-04-01

The present study is aimed at evaluating the creep behavior of the nugget zone of friction welded 2014 Aluminum alloy by indentation creep tests. Impression creep testing was carried out at different temperatures of 300°C, 350°C and 400 °C with stress 124.77MPa, 187.16MPa, 249.55 MPa using a 1.0 mm diameter WC indenter. Experiments were conducted till the curve enters the steady state creep region. Constitutive modeling of creep behavior was carried out considering the temperature, stress and steady state creep rate. Microstructural investigation of the crept specimen at 400°C temperature and 187.16 MPa load was carried out and found that the small precipitates accumulate along the grain boundaries at the favorable conditions of the creep temperature and stress, new precipitates evolve due to the ageing. The grains are broken and deformed due to the creep phenomena.

The role of cell structure during creep of cold worked copper

Energy Technology Data Exchange (ETDEWEB)

Sandström, Rolf, E-mail: rsand@kth.se

2016-09-30

In previous work it was demonstrated that cold work could reduce the creep rate of phosphorus doped copper (Cu-OFP) by up to six orders of magnitude at 75 °C at a given applied stress. Cu-OFP will be used in canisters for final disposal of spent nuclear fuel. A dislocation model for the cell structure in the cold deformed material has been formulated. A distinction is made between the balanced dislocation content in the cell walls where the number of dislocations of opposite sign match and the unbalanced content where they do not. The recovery rate of the unbalanced content is much lower than that of the balanced content. Taking this into account, it has been possible to model the creep curves of both 12% and 24% cold worked Cu-OFP. The general appearance of the two sets of creep curves are distinctly different, which can be explained by the higher recovery rate in the 24% deformed state.

Increased variability of bone tissue mineral density resulting from estrogen deficiency influences creep behavior in a rat vertebral body.

Science.gov (United States)

Kim, Do-Gyoon; Navalgund, Anand R; Tee, Boon Ching; Noble, Garrett J; Hart, Richard T; Lee, Hye Ri

2012-11-01

Progressive vertebral deformation increases the fracture risk of a vertebral body in the postmenopausal patient. Many studies have observed that bone can demonstrate creep behavior, defined as continued time-dependent deformation even when mechanical loading is held constant. Creep is a characteristic of viscoelastic behavior, which is common in biological materials. We hypothesized that estrogen deficiency-dependent alteration of the mineral distribution of bone at the tissue level could influence the progressive postmenopausal vertebral deformity that is observed as the creep response at the organ level. The objective of this study was thus to examine whether the creep behavior of vertebral bone is changed by estrogen deficiency, and to determine which bone property parameters are responsible for the creep response of vertebral bone at physiological loading levels using an ovariectomized (OVX) rat model. Correlations of creep parameters with bone mineral density (BMD), tissue mineral density (TMD) and architectural parameters of both OVX and sham surgery vertebral bone were tested. As the vertebral creep was not fully recovered during the post-creep unloading period, there was substantial residual displacement for both the sham and OVX groups. A strong positive correlation between loading creep and residual displacement was found (r=0.868, pcreep behavior of the OVX group (pcreep caused progressive, permanent reduction in vertebral height for both the sham and OVX groups. In addition, estrogen deficiency-induced active bone remodeling increased variability of trabecular TMD in the OVX group. Taken together, these results suggest that increased variability of trabecular TMD resulting from high bone turnover influences creep behavior of the OVX vertebrae. Copyright © 2012 Elsevier Inc. All rights reserved.

Aseismic creep along the North Anatolian Fault quantified by coupling microstructural strain and chemical analyses

Science.gov (United States)

Kaduri, Maor; Gratier, Jean-Pierre; Renard, François; Çakir, Ziyadin; Lasserre, Cécile

2017-04-01

In the last decade aseismic creep has been noted as one of the key processes along tectonic plate boundaries. It contributes to the energy budget during the seismic cycle, delaying or triggering the occurrence of large earthquakes. Several major continental active faults show spatial alternation of creeping and locked segments. A great challenge is to understand which parameters control the transition from seismic to aseismic deformation in fault zones, such as the lithology, the degree of deformation from damage rocks to gouge, and the stress driven fault architecture transformations at all scales. The present study focuses on the North Anatolian Fault (Turkey) and characterizes the mechanisms responsible for the partition between seismic and aseismic deformation. Strain values were calculated using various methods, e.g. Fry, R-φs from microstructural measurements in gouge and damage samples collected on more than 30 outcrops along the fault. Maps of mineral composition were reconstructed from microprobe measurements of gouge and damage rock microstructure, in order to calculate the relative mass changes due to stress driven processes during deformation. Strain values were extracted, in addition to the geometrical properties of grain orientation and size distribution. Our data cover subsamples in the damage zones that were protected from deformation and are reminiscent of the host rock microstructure and composition, and subsamples that were highly deformed and recorded both seismic and aseismic deformations. Increase of strain value is linked to the evolution of the orientation of the grains from random to sheared sub-parallel and may be related to various parameters: (1) relative mass transfer increase with increasing strain indicating how stress driven mass transfer processes control aseismic creep evolution with time; (2) measured strain is strongly related with the initial lithology and with the evolution of mineral composition: monomineralic rocks are

A constitutive model for representing coupled creep, fracture, and healing in rock salt

International Nuclear Information System (INIS)

Chan, K.S.; Bodner, S.R.; Munson, D.E.; Fossum, A.F.

1996-01-01

The development of a constitutive model for representing inelastic flow due to coupled creep, damage, and healing in rock salt is present in this paper. This model, referred to as Multimechanism Deformation Coupled Fracture model, has been formulated by considering individual mechanisms that include dislocation creep, shear damage, tensile damage, and damage healing. Applications of the model to representing the inelastic flow and fracture behavior of WIPP salt subjected to creep, quasi-static loading, and damage healing conditions are illustrated with comparisons of model calculations against experimental creep curves, stress-strain curves, strain recovery curves, time-to-rupture data, and fracture mechanism maps

Creep resistance and material degradation of a candidate Ni–Mo–Cr corrosion resistant alloy

Energy Technology Data Exchange (ETDEWEB)

Shrestha, Sachin L., E-mail: sachin@ansto.gov.au [Institute of Materials Engineering, Australian Nuclear Science and Technology Organisation (ANSTO), Locked Bag 2001, Kirrawee DC, NSW 2232 (Australia); Bhattacharyya, Dhriti [Institute of Materials Engineering, Australian Nuclear Science and Technology Organisation (ANSTO), Locked Bag 2001, Kirrawee DC, NSW 2232 (Australia); Yuan, Guangzhou; Li, Zhijun J. [Center of Thorium Molten Salts Reactor System, Shanghai Institute of Applied Physics, Chinese Academy of Sciences (China); Budzakoska-Testone, Elizabeth; De Los Reyes, Massey; Drew, Michael; Edwards, Lyndon [Institute of Materials Engineering, Australian Nuclear Science and Technology Organisation (ANSTO), Locked Bag 2001, Kirrawee DC, NSW 2232 (Australia)

2016-09-30

This study investigated the creep deformation properties of GH3535, a Ni–Mo–Cr corrosion resistant structural alloy being considered for use in future Gen IV molten salt nuclear reactors (MSR) operating at around 700 °C. Creep testing of the alloy was conducted at 650–750 °C under applied stresses between 85–380 MPa. From the creep rupture results the long term creep strain and rupture life of the alloy were estimated by applying the Dorn Shepard and Larson Miller time-temperature parameters and the alloy's allowable ASME design stresses at the MSR's operating temperature were evaluated. The material's microstructural degradation at creep rupture was characterised using scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). The microstructural study revealed that the material failure was due to wedge cracking at triple grain boundary points and cavitation at coarse secondary grain boundary precipitates, nucleated and grown during high temperature exposure, leading to intergranular crack propagation. EBSD local misorientation maps clearly show that the root cause of cavitation and crack propagation was due to large strain localisation at the grain boundaries and triple points instigated by grain boundary sliding during creep deformation. This caused the grain boundary decohesion and subsequent material failure.

Creep and rupture behavior of weld-deposited Type 16-8-2 stainless steel at 5930C

International Nuclear Information System (INIS)

Ward, A.L.; Blackburn, L.D.

1976-03-01

The creep and rupture behavior of weld-deposited Type 16-8-2 stainless steel at 593 0 C was investigated over the time range from 3.6 x 10 4 s to 2.5 x 10 7 s. Equations relating stress to the time to rupture, the time to the onset of tertiary creep, and the time to produce a given creep strain were obtained. The experimental results indicate that the control of welding parameters (e.g. current, voltage and travel speed) within reasonable ranges can yield weld deposits with consistent time-dependent properties. Limited data suggest that high temperature (1065 0 C) post-weld annealing significantly alters only the flow curve for plastic deformation, while long-term thermal exposure at an intermediate temperature (565 0 C) produces only minor changes in either the plastic deformation or creep behavior of the weld materials

Cyclic compressive creep-elastoplastic behaviors of in situ TiB_2/Al-reinforced composite

International Nuclear Information System (INIS)

Zhang, Qing; Zhang, Weizheng; Liu, Youyi; Guo, BingBin

2016-01-01

This paper presents a study on the cyclic compressive creep-elastoplastic behaviors of a TiB_2-reinforced aluminum matrix composite (ZL109) at 350 °C and 200 °C. According to the experimental results, under cyclic elastoplasticity and cyclic coupled compressive creep-elastoplasticity, the coupled creep will cause changes in isotropic stress and kinematic stress. Isotropic stress decreases with coupled creep, leading to cyclic softening. Positive kinematic stress, however, increases with coupled creep, leading to cyclic hardening. Transmission electron microscopy (TEM) observations of samples under cyclic compressive creep-elastoplasticity with different temperatures and strain amplitudes indicate that more coupled creep contributes to more subgrain boundaries but fewer intracrystalline dislocations. Based on the macro tests and micro observations, the micro mechanism of compressive creep's influence on cyclic elastoplasticity is elucidated. Dislocations recovering with coupled creep leads to isotropic softening, whereas subgrain structures created by coupled creep lead to kinematic hardening during cyclic deformation.

Thermal creep of Zircaloy-4 cladding

International Nuclear Information System (INIS)

Murty, K.L.; Clevinger, G.S.; Papazoglou, T.P.

1977-01-01

Data on the hoop creep characteristics of Zircaloy tubing were collected at temperatures between 600 F and 800 F, and at stress levels ranging from 10 ksi to 25 ksi using internal pressurization tests. At low driving forces, exposures as long as 2000 hours were found insufficient to establish steady state creep. The experimental data at temperatures of 650 F to 800 F correlate well with an exponential stress dependence, and the activation energy for creep was found to be in excellent agreement with that for self-diffusion. The range of stresses and temperatures is too small to study the overall effect of these variables on the activation energy for creep. The experimental steady state creep-rates and those predicted from the creep equation used agree within a factor of 1.3. These correlations imply that the mechanism for hoop creep of Zircaloy-4 cladding is characterized by an activation energy of approximately 60 kcal/mole and an activation area of about 20b 3 . In addition, the exponential stress dependence implies that the activation area for creep is stress-independent. These results suggest that the climb of edge dislocations is the rate controlling mechanism for creep of Zircaloy-4. The transient creep regime was also analysed on the premise that primary creep is directly related to the rate of dispersal of dislocation entanglements by climb. (Auth.)

Microstructural evolution of uranium dioxide following compression creep tests: An EBSD and image analysis study

Energy Technology Data Exchange (ETDEWEB)

Iltis, X., E-mail: xaviere.iltis@cea.fr [CEA, DEN, DEC, Cadarache, 13108 Saint-Paul-Lez-Durance (France); Gey, N. [Laboratoire d’Etude des Microstructures et de Mécanique des Matériaux (LEM3), CNRS UMR 7239, Université de Lorraine, Ile du Saulcy, 57045 Metz Cedex 1 (France); Cagna, C. [CEA, DEN, DEC, Cadarache, 13108 Saint-Paul-Lez-Durance (France); Hazotte, A. [Laboratoire d’Etude des Microstructures et de Mécanique des Matériaux (LEM3), CNRS UMR 7239, Université de Lorraine, Ile du Saulcy, 57045 Metz Cedex 1 (France); Sornay, Ph. [CEA, DEN, DEC, Cadarache, 13108 Saint-Paul-Lez-Durance (France)

2015-01-15

Highlights: • Image analysis and EBSD are performed on creep tested UO{sub 2} pellets. • Development of intergranular voids, with increasing strain, is quantified. • EBSD evidences a sub-structuration process within the grains and quantifies it. • Creep mechanisms are discussed on the basis of these results. - Abstract: Sintered UO{sub 2} pellets with relatively large grains (∼25 μm) are tested at 1500 °C under a compressive stress of 50 MPa, at different deformation levels up to 12%. Electron Back Scattered Diffraction (EBSD) is used to follow the evolution, with deformation, of grains (size, shape, orientation) and sub-grains. Image analyses of SEM images are performed to characterize emergence of a population of micron size voids. For the considered microstructure and test conditions, the results show that the deformation process of UO{sub 2} globally corresponds to grain boundary sliding, partly accommodated by a dislocational creep within the grains, leading to a highly sub-structured state.

Investigation of Rock Failure Pattern in Creep by Digital Speckle Correlation Method

Directory of Open Access Journals (Sweden)

Yunliang Tan

2013-01-01

Full Text Available In order to study the mechanical characteristics from creep deformation to failure of rock, the tests of uniaxial compression and pushing steel-plate anchored in rock were performed, by using RLJW-2000 servo test synchronizing with Digital Speckle Correlation Method (DSCM. The investigations showed that for a uniaxial compressive specimen, when load arrived at 0.5σc, displacement clusters orderly formed, which was ahead of the macrocreep strain occurring in a slight jump mode when load arrived at 0.7σc. When the load level arrived at 0.8σc, displacement clusters gathered to be a narrow band. After that, the specimen abruptly fractured in a shear mode. In the creep pushing steel-plate test, when pushing force arrived at 25 kN, crack began to occur, the horizontal displacement field as well as shear strain field concentrated continuously along the interface between steel-plate and rock, and a new narrow concentrating band gathered in the upper layer. When pushing force arrived at 27.5 kN, another new narrow shear deformation band formed in the lower layer. Then, the steel-plate was pushed out quickly accompanying strong creep deformation.

Material pre-conditioning effects on the creep behaviour of 316H stainless steel

International Nuclear Information System (INIS)

Mehmanparast, A.; Davies, C.M.; Dean, D.W.; Nikbin, K.

2013-01-01

Material pre-conditioning by, for example, pre-strain through component bending and welding is known to alter the creep deformation and creep crack growth (CCG) behaviour of 316H stainless steel. Experimental test data on the creep deformation and crack growth behaviour of 316H weldment compact tension specimens at 550 °C, where the starter defect was introduced into the heat affected zone (HAZ), have been compared to those of obtained from similar specimens manufactured from parent material, which had been subjected to 8% compressive plastic pre-strain at room temperature. Similar degrees of accelerated cracking behaviour compared to parent material, for given values of C*, were exhibited in both 316H HAZ and pre-compressed parent materials. This acceleration has been attributed to the influence of material hardening effects and the reduction of creep ductility in the pre-conditioned materials. These results are discussed in terms of the potential for using material pre-conditioning to assist in predicting the long term cracking behaviour of high temperature 316H stainless steel plant components from shorter term laboratory CCG tests

In-reactor deformation and fracture of austenitic stainless steels

International Nuclear Information System (INIS)

Bloom, E.E.; Wolfer, W.G.

1978-01-01

An experimental technique for determining in-reactor fracture strain was developed and demonstrated. Differential swelling between a sample holder and a test specimen with a lower swelling rate produced uniaxial deformation. In-reactor deformations of 0.7 to 2.1% were achieved in type 304 stainless steel previously irradiated to fluences up to 8.8 x 10 26 n/m 2 without fracture. These strains are significantly higher than found in postirradiation creep-rupture tests on similar samples. From the measured strain values and published irradiation creep data and correlations, the stress levels during the irradiation were calculated. On the basis of previous postirradiation creep-rupture results, many of the samples that did not fail would be predicted to fail. Thus we conclude that the in-reactor rupture life is longer than predicted by postirradiation tests. Strain in a fractured sample was estimated to be less than 3.8%, and the in-reactor fractures were intergranular--the same fracture mode as found in postirradiation tests. Irradiation creep may relax stresses at crack tips and sliding boundaries, thus retarding the initiation and/or growth of cracks and leading to longer rupture lives in-reactor. However, the very high ductility or superplastic behavior predicted by the strain rate sensitivity of irradiation creep is not achieved because of the eventual interruption of the deformation process by grain boundary fracture

A coupled creep plasticity model for residual stress relaxation of a shot-peened nickel-based superalloy

Science.gov (United States)

Buchanan, Dennis J.; John, Reji; Brockman, Robert A.; Rosenberger, Andrew H.

2010-01-01

Shot peening is a commonly used surface treatment process that imparts compressive residual stresses into the surface of metal components. Compressive residual stresses retard initiation and growth of fatigue cracks. During component loading history, shot-peened residual stresses may change due to thermal exposure, creep, and cyclic loading. In these instances, taking full credit for compressive residual stresses would result in a nonconservative life prediction. This article describes a methodical approach for characterizing and modeling residual stress relaxation under elevated temperature loading, near and above the monotonic yield strength of INI 00. The model incorporates the dominant creep deformation mechanism, coupling between the creep and plasticity models, and effects of prior plastic strain to simulate surface treatment deformation.

The anisotropic creep behaviour of zircaloy-4 fuel cladding at 1073 K

International Nuclear Information System (INIS)

Rosinger, H.E.; Bowden, J.; Shewfelt, R.S.W.

1982-04-01

The anisotropy coefficients (F, G and H) of Hill's equation, suitably modified for creep deformation, have been determined for Zircaloy-4 fuel cladding from steady-state creep tests at an elevated temperature. Creep specimens were subjected to both uniaxial and biaxial loads (via internal pressure) at 1073 K and the strain measured concurrently in the axial and tangential directions. It has been found that Zircaloy-4 fuel cladding is almost, but not completely, isotropic at 1073 K; the values of F, G and H are 0.57, 0.48 and 0.45 respectively

Investigation on creep behavior of geo-materials with suction control technique

Directory of Open Access Journals (Sweden)

Nishimura Tomoyoshi

2016-01-01

Full Text Available The compacted bentonite which has typical couple problem associated to thermal - hydration - mechanical – chemical (THMC consist of one component of engineered barrier. Recently, the couple THMC formulation modelling suggested by some researchers can be predicted basically phenomena for engineered barrier that approach to correct evaluate satisfied facilities. The compacted bentonite is essentially unsaturated condition, some behaviors for bentonite has similar or close with generally expansive unsaturated soils. Therefore, hydrations have given significant influence on deformation of compacted bentonite such as swelling. There are many researches for swelling behavior of compacted bentonite within soaking. Extended theoretical or experimental investigations for unsaturated soil mechanics are possible to describe the strength-deformation behavior of compacted bentonite with suction controlling principle. A new method of determining the failure phase such as great axis deformation and destructions like strip of surface in the laboratory is described and the creep behavior of compacted bentonite is considered under maintain of high relative humidity environment. The creep deformation measured using improved cyclic relative humidity control apparatus in terms of specific suction control technique.

Creep deformation of high Cr-Mo ferritic/martensitic steels by material softening

International Nuclear Information System (INIS)

Kim, Sung Ho; Song, B. J.; Ryu, Woo Seog

2005-01-01

High Cr (9-12%Cr) ferritic/martensitic steels represent a valuable alternative to austenitic stainless steel for high temperature applications up to 600 .deg. C both in power and petrochemical plant, as well as good resistance to oxidation and corrosion. Material softening is the main physical phenomenon observed in the crept material. Thermally-induced change (such as particle coarsening or matrix solute depletion) and strain-induced change (such as dynamic subgrain growth) of microstructure degraded the alloy strength. These microstructural changes during a creep test cause the material softening, so the strength of the materials decreased. Many researches have been performed for the microstructural changes during a creep test, but the strength of crept materials has not been measured. In the present work, we measured the yield and tensile strength of crept materials using Indentationtyped Tensile Test System (AIS 2000). Material softening was quantitatively evaluated with a creep test condition, such as temperature and applied stress

Heat-to-heat variability of irradiation creep and swelling of HT9 irradiated to high neutron fluence at 400-600{degrees}C

Energy Technology Data Exchange (ETDEWEB)

Toloczko, M.B.; Garner, F.A. [Pacific Northwest National Lab., Richland, WA (United States)

1996-10-01

Irradiation creep data on ferritic/martensitic steels are difficult and expensive to obtain, and are not available for fusion-relevant neutron spectra and displacement rates. Therefore, an extensive creep data rescue and analysis effort is in progress to characterize irradiation creep of ferritic/martensitic alloys in other reactors and to develop a methodology for applying it to fusion applications. In the current study, four tube sets constructed from three nominally similar heats of HT9 subjected to one of two heat treatments were constructed as helium-pressurized creep tubes and irradiated in FFTF-MOTA at four temperatures between 400 and 600{degrees}C. Each of the four heats exhibited a different stress-free swelling behavior at 400{degrees}C, with the creep rate following the swelling according to the familiar B{sub o} + DS creep law. No stress-free swelling was observed at the other three irradiation temperatures. Using a stress exponent of n = 1.0 as the defining criterion, {open_quotes}classic{close_quotes} irradiation creep was found at all temperatures, but, only over limited stress ranges that decreased with increasing temperature. The creep coefficient B{sub o} is a little lower ({approx}50%) than that observed for austenitic steel, but the swelling-creep coupling coefficient D is comparable to that of austenitic steels. Primary transient creep behavior was also observed at all temperatures except 400{degrees}C, and thermal creep behavior was found to dominate the deformation at high stress levels at 550 and 600{degrees}C.

High-temperature creep of equiaxed Cd-26.5 at % Zn eutectic in the superplastic regime

International Nuclear Information System (INIS)

Tonejc, Anton; Poirier, J.-P.

1976-01-01

The temperature and stress dependence on the secondary creep rate of the Cd+26.5Zn eutectoid in the superplastic domain was studied in constant-stress compression creep. Experiments were performed in the following ranges of temperature, stress and grain size: 170C 2 , 1<10μm. In all cases secondary creep was established after a strain approximately equal to 4%. For temperatures higher than 200C all the techniques yielded the same value for m (m=0.49+-0.03) in the whole investigated range of stresses. For T=170C a lower value of m was found (m=0.33). The activation energy was determined and found equal to 25Kcal/mol. Micrographic examinations were performed on sectioned samples at several stages of deformation. The grain size was found to be identical for various conditions of temperature and stress and very stable with respect to deformation. The experimental results of the creep tests are discussed in relation with the microstructural aspects

In-pile creep test technique for zirconium alloys examination in BR-10 reactor channels

International Nuclear Information System (INIS)

Pevchikh, Yu.M.; Kruglov, A.S.; Troyanov, V.M.

2002-01-01

The irradiation enhanced creep phenomenon was discovered in stainless steels as a specific physical process accompanying high-intensity neutron flux irradiation in fast reactors. IPPE is also experienced in irradiation creep test activities, studying different types of materials under irradiation in BR-10 fast reactor. Series of in-channel type test facilities were constructed and tested in BR-10 reactor's 'dry' channels in order to carry out full-scale instrumented examination regarded to in-pile creep behaviour of different reactor materials. As a result, a specific test technique, named 'Tensometric method', has been developed and experimentally proved to be power enough in order to investigate irradiation creep of materials right in situ under neutron irradiation. The main peculiarity of test facility, which is constructed to apply the tensometric method, consists in absence of any special deformation-measurement cell at all. The in-pile creep strain measurement technique developed at IPPE is based on the non-direct measurement of specimen's deformation (either linear tensile strain or angular twisting one), which directly affects the loaded draws' tension parameters. Starting from 1993, in-pile creep experiments to investigate in-reactor creep behaviour of E110 and E635 zirconium alloys were carried out in BR-10. Experimental results and data collected during more than 20-year of BR-10 in-reactor creep test experience can be assumed as a strong evidence that the tensometric technique is a powerful instrument, which can give a chance to study different irradiation effects on reactor materials directly under irradiation. (author)

Analysis of Simple Creep Stress Calculation Methods for Creep Life Assessment

Energy Technology Data Exchange (ETDEWEB)

Seo, Jun Min; Lee, Han Sang; Kim, Yun Jae [Korea Univ., Daejeon (Korea, Republic of)

2017-08-15

Creep analysis takes much more time than elastic or elastic-plastic analysis. In this study, we conducted elastic and elastic-plastic analysis and compared the results with creep analysis results. In the elastic analysis, we used primary stress, which can be classified by the Mα-tangent method and stress intensities recommended in the ASME code. In the elastic-plastic analysis, we calculated the parameters recommended in the R5 code. For the FE models, a bending load, uniaxial load, and biaxial load were applied to the cross shaped welded plate, and a bending load and internal pressure were applied to the elbow pipe. To investigate the element size sensitivity, we conducted FE analysis for various element sizes for the cases where bending load was applied to the cross shaped welded plate. There was no significant difference between the creep.

Biaxial Creep Specimen Fabrication

Energy Technology Data Exchange (ETDEWEB)

JL Bump; RF Luther

2006-02-09

This report documents the results of the weld development and abbreviated weld qualification efforts performed by Pacific Northwest National Laboratory (PNNL) for refractory metal and superalloy biaxial creep specimens. Biaxial creep specimens were to be assembled, electron beam welded, laser-seal welded, and pressurized at PNNL for both in-pile (JOYO reactor, O-arai, Japan) and out-of-pile creep testing. The objective of this test campaign was to evaluate the creep behavior of primary cladding and structural alloys under consideration for the Prometheus space reactor. PNNL successfully developed electron beam weld parameters for six of these materials prior to the termination of the Naval Reactors program effort to deliver a space reactor for Project Prometheus. These materials were FS-85, ASTAR-811C, T-111, Alloy 617, Haynes 230, and Nirnonic PE16. Early termination of the NR space program precluded the development of laser welding parameters for post-pressurization seal weldments.

Biaxial Creep Specimen Fabrication

International Nuclear Information System (INIS)

JL Bump; RF Luther

2006-01-01

This report documents the results of the weld development and abbreviated weld qualification efforts performed by Pacific Northwest National Laboratory (PNNL) for refractory metal and superalloy biaxial creep specimens. Biaxial creep specimens were to be assembled, electron beam welded, laser-seal welded, and pressurized at PNNL for both in-pile (JOYO reactor, O-arai, Japan) and out-of-pile creep testing. The objective of this test campaign was to evaluate the creep behavior of primary cladding and structural alloys under consideration for the Prometheus space reactor. PNNL successfully developed electron beam weld parameters for six of these materials prior to the termination of the Naval Reactors program effort to deliver a space reactor for Project Prometheus. These materials were FS-85, ASTAR-811C, T-111, Alloy 617, Haynes 230, and Nirnonic PE16. Early termination of the NR space program precluded the development of laser welding parameters for post-pressurization seal weldments

Creep behaviour of heat resistant steels. Pt. 2

International Nuclear Information System (INIS)

Kloos, K.H.; Granacher, J.; Oehl, M.

1993-01-01

Creep data scatter bands of steels 2.25 Cr-1 Mo and 12 Cr-1 Mo-0.3 V were evaluated with the aid of model functions based on time temperature parameters. From the times to reach given strain values, mean isostrain curves in the stress time diagramme were calculated and therefrom, mean creep curves were derived. On this basis, creep equations were established, which include primary-, secondary- and tertiary-creep and are valid in the main range of application of each steel. Further, mean stress strain curves from hot tensile tests were used to describe the initial plastic strain in the creep equations. The values calculated with the established creep equations agreed relatively well with the correspondent original scatter band values from the creep tests. (orig.) [de

Lattice continuum and diffusional creep.

Science.gov (United States)

Mesarovic, Sinisa Dj

2016-04-01

Diffusional creep is characterized by growth/disappearance of lattice planes at the crystal boundaries that serve as sources/sinks of vacancies, and by diffusion of vacancies. The lattice continuum theory developed here represents a natural and intuitive framework for the analysis of diffusion in crystals and lattice growth/loss at the boundaries. The formulation includes the definition of the Lagrangian reference configuration for the newly created lattice, the transport theorem and the definition of the creep rate tensor for a polycrystal as a piecewise uniform, discontinuous field. The values associated with each crystalline grain are related to the normal diffusional flux at grain boundaries. The governing equations for Nabarro-Herring creep are derived with coupled diffusion and elasticity with compositional eigenstrain. Both, bulk diffusional dissipation and boundary dissipation accompanying vacancy nucleation and absorption, are considered, but the latter is found to be negligible. For periodic arrangements of grains, diffusion formally decouples from elasticity but at the cost of a complicated boundary condition. The equilibrium of deviatorically stressed polycrystals is impossible without inclusion of interface energies. The secondary creep rate estimates correspond to the standard Nabarro-Herring model, and the volumetric creep is small. The initial (primary) creep rate is estimated to be much larger than the secondary creep rate.

Effect of equal-channel angular pressing on the creep resistance of precipitation-strengthened alloys

Czech Academy of Sciences Publication Activity Database

Sklenička, Václav; Král, Petr; Dvořák, Jiří; Kvapilová, Marie; Kawasaki, M.; Langdon, T. G.

667-669, - (2011), s. 897-902 ISSN 0255-5476. [NanoSPD5 - International Conference on Nanomaterials by Severe Plastic Deformation /5./. Nanjing, 21.03.2011-25.03.2011] Institutional research plan: CEZ:AV0Z20410507 Keywords : creep * equal-channel angular pressing * precipitation- strength ened alloys * creep damage Subject RIV: JG - Metallurgy

Modeling creep deformation of a two-phase TiAI/Ti3Al alloy with a lamellar microstructure

Science.gov (United States)

Bartholomeusz, Michael F.; Wert, John A.

1994-10-01

A two-phase TiAl/Ti3Al alloy with a lamellar microstructure has been previously shown to exhibit a lower minimum creep rate than the minimum creep rates of the constituent TiAl and Ti3Al single-phase alloys. Fiducial-line experiments described in the present article demonstrate that the creep rates of the constituent phases within the two-phase TiAl/Ti3Al lamellar alloy tested in compression are more than an order of magnitude lower than the creep rates of single-phase TiAl and Ti3Al alloys tested in compression at the same stress and temperature. Additionally, the fiducial-line experiments show that no interfacial sliding of the phases in the TiAl/Ti3Al lamellar alloy occurs during creep. The lower creep rate of the lamellar alloy is attributed to enhanced hardening of the constituent phases within the lamellar microstructure. A composite-strength model has been formulated to predict the creep rate of the lamellar alloy, taking into account the lower creep rates of the constituent phases within the lamellar micro-structure. Application of the model yields a very good correlation between predicted and experimentally observed minimum creep rates over moderate stress and temperature ranges.

ACCEPT: a three-dimensional finite element program for large deformation elastic-plastic-creep analysis of pressurized tubes (LWBR/AWBA Development Program)

International Nuclear Information System (INIS)

Hutula, D.N.; Wiancko, B.E.

1980-03-01

ACCEPT is a three-dimensional finite element computer program for analysis of large-deformation elastic-plastic-creep response of Zircaloy tubes subjected to temperature, surface pressures, and axial force. A twenty-mode, tri-quadratic, isoparametric element is used along with a Zircaloy materials model. A linear time-incremental procedure with residual force correction is used to solve for the time-dependent response. The program features an algorithm which automatically chooses the time step sizes to control the accuracy and numerical stability of the solution. A contact-separation capability allows modeling of interaction of reactor fuel rod cladding with fuel pellets or external supports

Effects of impurity trapping on irradiation-induced swelling and creep

Energy Technology Data Exchange (ETDEWEB)

Mansur, L. K.; Yoo, M. H.

1977-12-01

A general theory of the effects of point defect trapping on radiation-induced swelling and creep deformation rates is developed. The effects on the fraction of defects recombining, and on void nucleation, void growth and creep due to the separate processes of dislocation climb-glide and dislocation climb (the so-called SIPA mechanism) are studied. Trapping of vacancies or interstitials increases total recombination and decreases the rates of deformation processes. For fixed trapping parameters, the reduction is largest for void nucleation, less for void growth and creep due to dislocation climb-glide, and least for creep due to dislocation climb. With this formation, the effects of trapping at multiple vacancy and interstitial traps and of spatial and temporal variation in trap concentrations may be determined. Alternative pictures for viewing point defect trapping in terms of effective recombination and diffusion coefficients are derived. It is shown that previous derivations of these coefficients are incorrect. A rigorous explanation is given of the well-known numerical result that interstitial trapping is significant only if the binding energy exceeds the difference between the vacancy and interstitial migration energies, while vacancy trapping is significant even at small binding energies. Corrections which become necessary at solute concentrations above about 0.1% are described. Numerical results for a wide range of material and irradiation parameters are presented.

Deformation mechanisms in the San Andreas Fault zone - a comparison between natural and experimentally deformed microstructures

Science.gov (United States)

van Diggelen, Esther; Holdsworth, Robert; de Bresser, Hans; Spiers, Chris

2010-05-01

The San Andreas Fault (SAF) in California marks the boundary between the Pacific plate and the North American plate. The San Andreas Fault Observatory at Depth (SAFOD) is located 9 km northwest of the town of Parkfield, CA and provide an extensive set of samples through the SAF. The SAFOD drill hole encountered different lithologies, including arkosic sediments from the Salinian block (Pacific plate) and claystones and siltstones from the Great Valley block (North American plate). Fault deformation in the area is mainly by a combination of micro-earthquakes and fault creep. Deformation of the borehole casing indicated that the SAFOD drill hole cross cuts two actively deforming strands of the SAF. In order to determine the deformation mechanisms in the actively creeping fault segments, we have studied thin sections obtained from SAFOD phase 3 core material using optical and electron microscopy, and we have compared these natural SAFOD microstructures with microstructures developed in simulated fault gouges deformed in laboratory shear experiments. The phase 3 core material is divided in three different core intervals consisting of different lithologies. Core interval 1 consists of mildly deformed Salinian rocks that show evidence of cataclasis, pressure solution and reaction of feldspar to form phyllosilicates, all common processes in upper crustal rocks. Most of Core interval 3 (Great Valley) is also only mildly deformed and very similar to Core interval 1. Bedding and some sedimentary features are still visible, together with limited evidence for cataclasis and pressure solution, and reaction of feldspar to form phyllosilicates. However, in between the relatively undeformed rocks, Core interval 3 encountered a zone of foliated fault gouge, consisting mostly of phyllosilicates. This zone is correlated with one of the zones of localized deformation of the borehole casing, i.e. with an actively deforming strand of the SAF. The fault gouge zone shows a strong, chaotic

Mechanical Behavior of Low Porosity Carbonate Rock: From Brittle Creep to Ductile Creep.

Science.gov (United States)

Nicolas, A.; Fortin, J.; Gueguen, Y.

2014-12-01

Mechanical compaction and associated porosity reduction play an important role in the diagenesis of porous rocks. They may also affect reservoir rocks during hydrocarbon production, as the pore pressure field is modified. This inelastic compaction can lead to subsidence, cause casing failure, trigger earthquake, or change the fluid transport properties. In addition, inelastic deformation can be time - dependent. In particular, brittle creep phenomena have been deeply investigated since the 90s, especially in sandstones. However knowledge of carbonates behavior is still insufficient. In this study, we focus on the mechanical behavior of a 14.7% porosity white Tavel (France) carbonate rock (>98% calcite). The samples were deformed in a triaxial cell at effective confining pressures ranging from 0 MPa to 85 MPa at room temperature and 70°C. Experiments were carried under dry and water saturated conditions in order to explore the role played by the pore fluids. Two types of experiments have been carried out: (1) a first series in order to investigate the rupture envelopes, and (2) a second series with creep experiments. During the experiments, elastic wave velocities (P and S) were measured to infer crack density evolution. Permeability was also measured during creep experiments. Our results show two different mechanical behaviors: (1) brittle behavior is observed at low confining pressures, whereas (2) ductile behavior is observed at higher confining pressures. During creep experiments, these two behaviors have a different signature in term of elastic wave velocities and permeability changes, due to two different mechanisms: development of micro-cracks at low confining pressures and competition between cracks and microplasticity at high confining pressure. The attached figure is a summary of 20 triaxial experiments performed on Tavel limestone under different conditions. Stress states C',C* and C*' and brittle strength are shown in the P-Q space: (a) 20°C and dry

Changes in creep of polymethylmetacrylate after irradiation

International Nuclear Information System (INIS)

Peschanskaya, N.N.; Smolyanskij, A.S.; Suvorova, V.Yu.

1992-01-01

A study was made on PMMA, irradiated by different doses of 60 Co γ-radiation in vacuum under creep during compression. It is shown that occurence of tendency to failure at +20 degC is observed at doses of D > 100 kGy (> 10 Mrad), whereas sufficient decrease of deformation before failure takes place at D > 350 kGy. Peculiarities of behaviour of irradiated and nonirradiated PMMA under compression and tension were correlated. It is noted that critical irradiation doses may differ sufficiently for different loading conditions, deformation and longevity characteristics

Monitoring the Deformation of High-Rise Buildings in Shanghai Luijiazui Zone by Tomo-Psinsar

Science.gov (United States)

Zhou, L. F.; Ma, P. F.; Xia, Y.; Xie, C. H.

2018-05-01

In this study, we utilize a Tomography-based Persistent Scatterers Interferometry (Tomo-PSInSAR) approach for monitoring the deformation performances of high-rise buildings, i.e. SWFC and Jin Mao Tower, in Shanghai Lujiazui Zone. For the purpose of this study, we use 31 Stripmap acquisitions from TerraSAR-X missions, spanning from December 2009 to February 2013. Considering thermal expansion, creep and shrinkage are two long-term movements that occur in high-rise buildings with concrete structures, we use an extended 4-D SAR phase model, and three parameters (height, deformation velocity, and thermal amplitude) are estimated simultaneously. Moreover, we apply a two-tier network strategy to detect single and double PSs with no need for preliminary removal of the atmospheric phase screen (APS) in the study area, avoiding possible error caused by the uncertainty in spatiotemporal filtering. Thermal expansion is illustrated in the thermal amplitude map, and deformation due to creep and shrinkage is revealed in the linear deformation velocity map. The thermal amplitude map demonstrates that the derived thermal amplitude of the two high-rise buildings both dilate and contract periodically, which is highly related to the building height due to the upward accumulative effect of thermal expansion. The linear deformation velocity map reveals that SWFC is subject to deformation during the new built period due to creep and shrinkage, which is height-dependent movements in the linear velocity map. It is worth mention that creep and shrinkage induces movements that increase with the increasing height in the downward direction. In addition, the deformation rates caused by creep and shrinkage are largest at the beginning and gradually decrease, and at last achieve a steady state as time goes infinity. On the contrary, the linear deformation velocity map shows that Jin Mao Tower is almost stable, and the reason is that it is an old built building, which is not influenced by creep