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Sample records for piezoelectric pzt thick

  1. Electromechanical Properties of Microcantilever Actuated by Enhanced Piezoelectric PZT Thick Film

    Institute of Scientific and Technical Information of China (English)

    LIU Hong-Mei; ZHAO Quan-Liang; CAO Mao-Sheng; YUAN Jie; DUAN Zhong-Xia; QIU Cheng-Jun

    2008-01-01

    Pb(Zro.53,Tio.47)O3 (PZT) films with thicknesses of 0.8μm, 2μm and 4μm are prepared by a sol-gel method and their longitudinal piezoelectric coefficients are analysed. The results show that the PZT thick films, whose density is closer to bulk PZT, has the better crystallization, with d33 and density much larger than those of PZT thin films. A piezoelectric microcantilever actuated by a 4-μm-thick PZT film is fabricated and its displacement is measured in different frequencies and voltages. The displacement increases linearly with the increasing bias,and the maximum displacement of 0.544 μm is observed at 30kHz for 5V bias. The resonant frequency obtained in the experiment matches quite well with the theoretical result, and it is shown that the resonant frequency of PZT microcantilever could be controlled and predicated.

  2. Evaluation of the effect of porosity and substrate on the piezoelectric behaviour of thick-film PZT elements

    Energy Technology Data Exchange (ETDEWEB)

    Gwirc, S N [Instituto Nacional de TecnologIa Industrial, Electronica e Informatica, CC 157, B1650WAB San Martin, Buenos Aires (Argentina); Negreira, C A [Instituto de Fisica, Laboratorio de Acustica Ultrasonora, Facultad de Ciencias, Igua 4225, 11400 Montevideo (Uruguay)

    2006-10-07

    This work presents a method to establish the elastic and piezoelectric constants of a thick film screen printed PZT composite over an alumina substrate. The calculus procedure uses as input data the parameters from the bulk material because it is basically the same component of which the thick film paste is manufactured. We also need to know frequencies of resonance and anti-resonance as well as the permittivity and density of the film in a poled disc sample. This method takes into account three factors: the additional components such as the glass frit, porosity of the film caused by the low temperature sinter process and the film clamping to the substrate. Each one of these factors reduces the piezoelectric efficiency by a different amount and, consequently, the measured values of the constants. The results obtained in this way are compared with experimental measurements of the effective piezoelectric charge constant d{sub 33} and permittivity with good agreement. Small discrepancies could be explained mainly due to lack of homogeneity in glass as well as in pore distribution.

  3. Screen printed PZT/PZT thick film bimorph MEMS cantilever device for vibration energy harvesting

    DEFF Research Database (Denmark)

    Xu, Ruichao; Lei, Anders; Dahl-Petersen, Christian

    2012-01-01

    We present a microelectromechanical system (MEMS) based PZT/PZT thick film bimorph vibration energy harvester with an integrated silicon proof mass. Most piezoelectric energy harvesting devices use a cantilever beam of a non piezoelectric material as support beneath or in-between the piezoelectri...

  4. Screen printed PZT/PZT thick film bimorph MEMS cantilever device for vibration energy harvesting

    DEFF Research Database (Denmark)

    Xu, Ruichao; Lei, Anders; Christiansen, T.L.

    2011-01-01

    We present a MEMS-based PZT/PZT thick film bimorph vibration energy harvester with an integrated silicon proof mass. The most common piezoelectric energy harvesting devices utilize a cantilever beam of a non piezoelectric material as support beneath or in-between the piezoelectric material....... It provides mechanical support but it also reduces the power output. Our device replaces the support with another layer of the piezoelectric material, and with the absence of an inactive mechanical support all of the stresses induced by the vibrations will be harvested by the active piezoelectric elements....

  5. Advantages of PZT thick film for MEMS sensors

    DEFF Research Database (Denmark)

    Hindrichsen, Christian Carstensen; Lou-Moller, R.; Hansen, K.;

    2010-01-01

    For all MEMS devices a high coupling between the mechanical and electrical domain is desired. Figures of merit describing the coupling are important for comparing different piezoelectric materials. The existing figures of merit are discussed and a new figure of merit is introduced for a fair...... comparison of piezoelectric thin and thick films based MEMS devices, as cantilevers, beams, bridges and membranes. Simple analytical modeling is used to define the new figure of merit. The relevant figure of merits is compared for the piezoelectric material of interest for MEMS applications: ZnO, AIN, PZT...... thin film and PZT thick film. It is shown that MEMS sensors with the PZT thick film TF2100 from InSensor A/S have potential for significant higher voltage sensitivities compared to PZT thin film base MEMS sensors when the total thickness of the MEMS cantilever, beam, bridge or membrane is high...

  6. Oriented Growth of PZT thick film embedded with PZT nanoparticles

    Institute of Scientific and Technical Information of China (English)

    DUAN Zhong-xia; YUAN Jie; ZHAO Quan-liang; LU Ran; CAO Mao-sheng

    2009-01-01

    This paper reports that dense and crack-free (100) oriented lead zirconate titanate (Pb(Zr0.52Ti0.48)O3,PZT) thick film embedded with PZT nanoparticles has been successfully fabricated on Pt/Cr/SiO2/Si substrate by using PT transition layer and PVP additive. The thick film possesses single-phase perovskite structure and perfectly (100) oriented. The (100) orientation degree of the PZT films strongly depended on annealing time and for the 4 μm-thick PZT film which was annealed at 700 ℃ for 5 min is the largest. The (100) orientation degree of the PZT thick film gradually strengthen along with the thickness of film decreasing. The 3 μm-thick PZT thick film which was annealed at 700 ℃ for 5 min has the strongest (100) orientation degree, which is 82. 3%.

  7. Presentation and characterization of novel thick-film PZT microactuators

    Energy Technology Data Exchange (ETDEWEB)

    Chalvet, Vincent; Habineza, Didace, E-mail: didace.habineza@femto-st.fr; Rakotondrabe, Micky; Clévy, Cédric

    2016-04-01

    We propose in this paper the characterization of a new generation of piezoelectric cantilevers called thick-films piezoelectric actuators. Based on the bonding and thinning process of a bulk PZT layer onto a silicon layer, these cantilevers can provide better static and dynamic performances compared to traditional piezocantilevers, additionally to the small dimensions.

  8. Triaxial MEMS accelerometer with screen printed PZT thick film

    DEFF Research Database (Denmark)

    Hindrichsen, Christian Carstensen; Almind, Ninia Sejersen; Brodersen, Simon Hedegaard

    2010-01-01

    . In this work integration of a screen printed piezoelectric PZT thick film with silicon MEMS technology is shown. A high bandwidth triaxial accelerometer has been designed, fabricated and characterized. The voltage sensitivity is 0.31 mV/g in the vertical direction, 0.062 mV/g in the horizontal direction...

  9. Investigation of Top/Bottom electrode and Diffusion Barrier Layer for PZT Thick Film MEMS Sensors

    DEFF Research Database (Denmark)

    Hindrichsen, Christian Carstensen; Pedersen, Thomas; Thomsen, Erik Vilain

    2008-01-01

    Top and bottom electrodes for screen printed piezoelectric lead zirconate titanate, Pb(ZrxTi1 - x)O3 (PZT) thick film are investigated with respect to future MEMS devices. Down to 100 nm thick E-beam evaporated Al and Pt films are patterned as top electrodes on the PZT using a lift-off process...

  10. Investigation of top electrode for PZT thick films based MEMS sensors

    DEFF Research Database (Denmark)

    Hindrichsen, Christian Carstensen; Pedersen, Thomas; Kristiansen, Paw T.;

    2010-01-01

    In this work processing of screen printed piezoelectric PZT thick films on silicon substrates is investigated for use in future MEMS devices. E-beam evaporated Al and Pt are patterned on PZT as a top electrode using a lift-off process with a line width down to 3 mu m. Three test structures are used...

  11. Piezoelectric and mechanical properties of structured PZT-epoxy composites

    NARCIS (Netherlands)

    James, N.K.; Ende, D.A. van den; Lafont, U.; Zwaag, S. van der; Groen, W.A.

    2013-01-01

    Structured lead zirconium titanate (PZT)-epoxy composites are prepared by dielectrophoresis. The piezoelectric and dielectric properties of the composites as a function of PZT volume fraction are investigated and compared with the corresponding unstructured composites. The effect of poling voltage o

  12. Measurement and calculation of PZT thin film longitudinal piezoelectric coefficients.

    Energy Technology Data Exchange (ETDEWEB)

    Christman, J. A.; Kim, S.-H.; Kingon, A. I.; Maiwa, H.; Maria, J.-P.; Streiffer, S. K.

    1999-04-26

    The ferroelectric and piezoelectric properties of 2000 {angstrom} thick chemical solution deposited Pb(Zr{sub x}Ti{sub 1{minus}x})O{sub 3} (PZT) thin films were investigated. Several Zr/Ti ratios were studied: 30/70, 50/50 and 65/35, which correspond to tetragonal, near-morphotropic, and rhombohedral symmetries. In all samples, a {l_brace}111{r_brace}-texture is predominant. Longitudinal piezoelectric coefficients and their dc field dependence were measured using the contact AFM method. The expected trend of a maximum piezoelectric coefficient at or near to the MPB was not observed. The composition dependence was small, with the maximum d{sub 33} occurring in the tetragonal material. To explain the results, crystallographic texture and film thickness effects are suggested. Using a modified phenomenological approach, derived electrostrictive coefficients, and experimental data, d{sub 33} values were calculated. Qualitative agreement was observed between the measured and calculated coefficients. Justifications of modifications to the calculations are discussed.

  13. In situ X-ray diffraction studies on the piezoelectric response of PZT thin films

    Energy Technology Data Exchange (ETDEWEB)

    Davydok, A., E-mail: davydok@mpie.de [Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334, 13397 Marseille (France); Max-Planck-Institut für Eisenforschung, Department Structure and Nano-/Micromechanics of Materials, D-40237 Düsseldorf (Germany); Cornelius, T.W. [Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334, 13397 Marseille (France); Mocuta, C. [SOLEIL Synchrotron, DiffAbs beamline, L' Orme des Merisiers, Saint-Aubin - BP 48, 91192 Gif-sur-Yvette Cedex (France); Lima, E.C. [Universidade Federal do Tocantins, 77500-000 Porto Nacional, TO (Brazil); Araujo, E.B. [Departamento de Fisica e Quimica, Universidade Estadual Paulista, Av. Brasil, 56 Centro, 15385-000 Ilha Solteira, SP (Brazil); Thomas, O. [Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334, 13397 Marseille (France)

    2016-03-31

    Piezoelectric properties of randomly oriented self-polarized PbZr{sub 0.50}Ti{sub 0.50}O{sub 3} (PZT) thin films were investigated using in situ synchrotron X-ray diffraction. Possibilities for investigating the piezoelectric effect using micro-sized hard X-ray beams are demonstrated and perspectives for future dynamical measurements on PZT samples with variety of compositions and thicknesses are given. Studies performed on the crystalline [100, 110] directions evidenced piezoelectric anisotropy. The piezoelectric coefficient d{sub 33} was calculated in terms of the lab reference frame (d{sub perp}) and found to be two times larger along the [100] direction than along the [110] direction. The absolute values for the d{sub perp} amount to 120 and 230 pm/V being in good agreement with experimental and theoretical values found in literature for bulk PZT ceramics. - Highlights: • We performed in situ synchrotron X-ray diffraction studies on (PZT) thin films. • We discuss anisotropy of piezo effect in different crystallographic directions. • Perpendicular component Piezo coefficient of thin PZT layer is defined.

  14. Piezoelectric characteristics of PZT thin films on polymer substrate

    Science.gov (United States)

    Kang, Min-Gyu; Do, Younh-Ho; Oh, Seung-Min; Rahayu, Rheza; Kim, Yiyein; Kang, Chong-Yun; Nahm, Sahn; Yoon, Seok-Jin

    2012-02-01

    The goal of piezoelectric energy harvesting is to improve the power efficiency of devices. One of the approaches for the improvement of power efficiency is to apply the large strain on the piezoelectric materials and then many scientists approached using thin films or nano-structured piezoelectric materials to obtain flexibility. However, the conventional thin film processes available for the fabrication of piezoelectric materials as PbZr0.52Ti0.48O3 (PZT) are not compatible with flexible electronics because they require high processing temperatures (>700^oC) to obtain piezoelectricity. Excimer laser annealing (ELA) is attractive heat process for the low-temperature crystallization, because of its material selectivity and short heating time. In this study, the amorphous PZT thin films were deposited on polymer substrate by rf-sputtering. To crystallize the amorphous films, the ELA was carried out with various conditions as function of the applied laser energy density, the number of pulse, and the repetition rate. To evaluate the piezoelectric characteristics, piezoelectric force microscopy (PFM) and electrometer are used. As a result, we obtained the crystallized PZT thin film on flexible substrate and obtained flexible piezoelectric energy harvester.

  15. MEMS Accelerometer with Screen Printed Piezoelectric Thick Film

    DEFF Research Database (Denmark)

    Hindrichsen, Christian Carstensen; Lau-Moeller, R.; Bove, T.

    2006-01-01

    A bulk-micromachined piezoelectric MEMS accelerometer with screen printed piezoelectric Pb(ZrxTil )O3(PZT) thick film (TF) as the sensing material has been fabricated and characterized. The accelerometer has a four beam structure with a central seismic mass (3600x3600x500 pm3) and a total chip size...

  16. A Piezoelectric PZT Ceramic Mulitlayer Stack for Energy Harvesting Under Dynamic Forces

    Science.gov (United States)

    Xu, Tian-Bing; Siochi, Emilie J.; Kang, Jin Ho; Zuo, Lei; Zhou, Wanlu; Tang, Xiudong; Jiang, Xiaoning

    2011-01-01

    Piezoelectric energy harvesting transducers (PEHTs) are commonly used in motion/vibration energy scavenging devices. To date, most researchers have focused on energy harvesting at narrow bandwidths around the mechanical resonance frequency, and most piezoelectric harvesting devices reported in the literature have very low effective piezoelectric coefficient (d(sub eff)) (piezoelectric coefficients of about 100 pC/N. The level of harvested electrical power for CBPEHTs is on the order of microW even at resonance mode. In order to harvest more electrical energy across broader bandwidth, high effective piezoelectric coefficient structures are needed. In this study, we investigate a "33" longitudinal mode, piezoelectric PZT ceramic multilayer stack (PZT-Stack) with high effective piezoelectric coefficient for high-performance PEHTs. The PZT-Stack is composed of 300 layers of 0.1 mm thick PZT plates, with overall dimensions of 32.4 mm X 7.0 mm X 7.0 mm. Experiments were carried out with dynamic forces in a broad bandwidth ranging from 0.5 Hz to 25 kHz. The measured results show that the effective piezoelectric coefficient of the PZT-stack is about 1 X 10(exp 5) pC/N at off-resonance frequencies and 1.39 X 10(exp 6) pC/N at resonance, which is order of magnitude larger than that of traditional PEHTs. The effective piezoelectric coefficients (d(sub eff)) do not change significantly with applied dynamic forces having root mean square (RMS) values ranging from 1 N to 40 N. In resonance mode, 231 mW of electrical power was harvested at 2479 Hz with a dynamic force of 11.6 N(sub rms), and 7.6 mW of electrical power was generated at a frequency of 2114 Hz with 1 N(sub rms) dynamic force. In off-resonance mode, an electrical power of 18.7 mW was obtained at 680 Hz with a 40 N(sub rms) dynamic force. A theoretical model of energy harvesting for the PZT-Stack is established. The modeled results matched well with experimental measurements. This study demonstrated that high

  17. A Piezoelectric PZT Ceramic Mulitlayer Stack for Energy Harvesting Under Dynamic Forces

    Science.gov (United States)

    Xu, Tian-Bing; Siochi, Emilie J.; Kang, Jin Ho; Zuo, Lei; Zhou, Wanlu; Tang, Xiudong; Jiang, Xiaoning

    2011-01-01

    Piezoelectric energy harvesting transducers (PEHTs) are commonly used in motion/vibration energy scavenging devices. To date, most researchers have focused on energy harvesting at narrow bandwidths around the mechanical resonance frequency, and most piezoelectric harvesting devices reported in the literature have very low effective piezoelectric coefficient (d(sub eff)) (harvested electrical power for CBPEHTs is on the order of microW even at resonance mode. In order to harvest more electrical energy across broader bandwidth, high effective piezoelectric coefficient structures are needed. In this study, we investigate a "33" longitudinal mode, piezoelectric PZT ceramic multilayer stack (PZT-Stack) with high effective piezoelectric coefficient for high-performance PEHTs. The PZT-Stack is composed of 300 layers of 0.1 mm thick PZT plates, with overall dimensions of 32.4 mm X 7.0 mm X 7.0 mm. Experiments were carried out with dynamic forces in a broad bandwidth ranging from 0.5 Hz to 25 kHz. The measured results show that the effective piezoelectric coefficient of the PZT-stack is about 1 X 10(exp 5) pC/N at off-resonance frequencies and 1.39 X 10(exp 6) pC/N at resonance, which is order of magnitude larger than that of traditional PEHTs. The effective piezoelectric coefficients (d(sub eff)) do not change significantly with applied dynamic forces having root mean square (RMS) values ranging from 1 N to 40 N. In resonance mode, 231 mW of electrical power was harvested at 2479 Hz with a dynamic force of 11.6 N(sub rms), and 7.6 mW of electrical power was generated at a frequency of 2114 Hz with 1 N(sub rms) dynamic force. In off-resonance mode, an electrical power of 18.7 mW was obtained at 680 Hz with a 40 N(sub rms) dynamic force. A theoretical model of energy harvesting for the PZT-Stack is established. The modeled results matched well with experimental measurements. This study demonstrated that high effective piezoelectric coefficient structures enable PEHTs to

  18. Investigation of Top/bottom Electrode and Diffusion Barrier Layer for PZT thick film MEMS Sensors

    DEFF Research Database (Denmark)

    Pedersen, Thomas; Hindrichsen, Christian Carstensen; Lou-Møller, R.

    2007-01-01

    In this work screen printed piezoelectric Ferroperm PZ26 lead zirconate titanate (PZT) thick film is used for two MEMS devices. A test structure is used to investigate several aspects regarding bottom and top electrodes. 450 nm ZrO2 thin film is found to be an insufficient diffusion barrier layer...

  19. Local piezoelectric behavior in PZT-based thin films for ultrasound transducers

    Science.gov (United States)

    Griggio, Flavio

    Piezoelectric microelectromechanical systems (MEMS) are currently used in inkjet printers and precision resonators; numerous additional applications are being investigated for sensors, low-voltage actuators, and transducers. This work was aimed at improving piezoelectric MEMS by taking two approaches: 1) identifying factors affecting the piezoelectric response of ferroelectric thin films and 2) demonstrating integration of these films into a high frequency array transducer. It was found that there are several key factors influencing the piezoelectric response of thin films for a given material composition. First, large grain size improves the piezoelectric response. This was demonstrated using chemical solution deposited lead nickel niobate -- lead zirconate titanate (0.3)Pb(Ni 0.33Nb0.67)O3 - (0.7)Pb(Zr0.45Ti 0.55O3), (PNN-PZT) ferroelectric thin films. It was shown that this composition allows greater microstructural control than does PZT. Dielectric permittivities ranging from 1350 to 1520 and a transverse piezoelectric coefficient e31,f as high as -- 9.7 C/m 2 were observed for films of about 0.25 mum in thickness. The permittivity and piezoelectric response as well as extrinsic contributions to the dielectric constant increased by 14 and 12 % respectively for samples with grain sizes ranging from 110 to 270 nm. A second factor influencing the piezoelectric response is film composition with respect to the morphotropic phase boundary (MPB). The composition dependence of the dielectric and piezoelectric nonlinearities was characterized in epitaxially grown (0.3)Pb(Ni0.33Nb0.67)O3-(0.7)Pb(Zr xTi1-xO3) thin films deposited on SrTiO 3 to minimize the influence of large-angle grain boundaries. Tetragonal, MPB and rhombohedral films were prepared by changing the Zr/Ti ratio. The largest dielectric and piezoelectric nonlinearities were observed for the rhombohedral sample; this resulted from a higher domain wall mobility due to a smaller ferroelectric distortion and

  20. A Piezoelectric PZT Ceramic Mulitlayer Stack for Energy Harvesting Under Dynamic Forces

    Science.gov (United States)

    Xu, Tian-Bing; Siochi, Emilie J.; Kang, Jin Ho; Zuo, Lei; Zhou, Wanlu; Tang, Xiudong; Jiang, Xiaoning

    2011-01-01

    Piezoelectric energy harvesting transducers (PEHTs) are commonly used in motion/vibration energy scavenging devices. To date, most researchers have focused on energy harvesting at narrow bandwidths around the mechanical resonance frequency, and most piezoelectric harvesting devices reported in the literature have very low effective piezoelectric coefficient (d(sub eff)) (ceramic multilayer stack (PZT-Stack) with high effective piezoelectric coefficient for high-performance PEHTs. The PZT-Stack is composed of 300 layers of 0.1 mm thick PZT plates, with overall dimensions of 32.4 mm X 7.0 mm X 7.0 mm. Experiments were carried out with dynamic forces in a broad bandwidth ranging from 0.5 Hz to 25 kHz. The measured results show that the effective piezoelectric coefficient of the PZT-stack is about 1 X 10(exp 5) pC/N at off-resonance frequencies and 1.39 X 10(exp 6) pC/N at resonance, which is order of magnitude larger than that of traditional PEHTs. The effective piezoelectric coefficients (d(sub eff)) do not change significantly with applied dynamic forces having root mean square (RMS) values ranging from 1 N to 40 N. In resonance mode, 231 mW of electrical power was harvested at 2479 Hz with a dynamic force of 11.6 N(sub rms), and 7.6 mW of electrical power was generated at a frequency of 2114 Hz with 1 N(sub rms) dynamic force. In off-resonance mode, an electrical power of 18.7 mW was obtained at 680 Hz with a 40 N(sub rms) dynamic force. A theoretical model of energy harvesting for the PZT-Stack is established. The modeled results matched well with experimental measurements. This study demonstrated that high effective piezoelectric coefficient structures enable PEHTs to harvest more electrical energy from mechanical vibrations or motions, suggesting an effective design for high-performance low-footprint PEHTs with potential applications in military, aerospace, and portable electronics. In addition, this study provides a route for using piezoelectric multilayer

  1. Mems-based pzt/pzt bimorph thick film vibration energy harvester

    DEFF Research Database (Denmark)

    Xu, Ruichao; Lei, Anders; Dahl-Petersen, Christian

    2011-01-01

    We describe fabrication and characterization of a significantly improved version of a MEMS-based PZT/PZT thick film bimorph vibration energy harvester with an integrated silicon proof mass. The main advantage of bimorph vibration energy harvesters is that strain energy is not lost in mechanical...... support materials since only PZT is strained, and thus it has a potential for significantly higher output power. An improved process scheme for the energy harvester resulted in a robust fabrication process with a record high fabrication yield of 98.6%. Moreover, the robust fabrication process allowed...... a high pressure treatment of the screen printed PZT thick films prior to sintering, improving the PZT thick film performance and harvester power output reaches 37.1 μW at 1 g....

  2. Sputter deposition of PZT piezoelectric films on thin glass substrates for adjustable x-ray optics.

    Science.gov (United States)

    Wilke, Rudeger H T; Johnson-Wilke, Raegan L; Cotroneo, Vincenzo; Davis, William N; Reid, Paul B; Schwartz, Daniel A; Trolier-McKinstry, Susan

    2013-05-10

    Piezoelectric PbZr(0.52)Ti(0.48)O(3) (PZT) thin films deposited on thin glass substrates have been proposed for adjustable optics in future x-ray telescopes. The light weight of these x-ray optics enables large collecting areas, while the capability to correct mirror figure errors with the PZT thin film will allow much higher imaging resolution than possible with conventional lightweight optics. However, the low strain temperature and flexible nature of the thin glass complicate the use of chemical-solution deposition due to warping of the substrate at typical crystallization temperatures for the PZT. RF magnetron sputtering enabled preparation of PZT films with thicknesses up to 3 μm on Schott D263 glass substrates with much less deformation. X-ray diffraction analysis indicated that the films crystallized with the perovskite phase and showed no indication of secondary phases. Films with 1 cm(2) electrodes exhibited relative permittivity values near 1100 and loss tangents below 0.05. In addition, the remanent polarization was 26 μC/cm(2) with coercive fields of 33 kV/cm. The transverse piezoelectric coefficient was as high as -6.1±0.6 C/m(2). To assess influence functions for the x-ray optics application, the piezoelectrically induced deflection of individual cells was measured and compared with finite-element-analysis calculations. The good agreement between the results suggests that actuation of PZT thin films can control mirror figure errors to a precision of about 5 nm, allowing sub-arcsecond imaging.

  3. Recent Progress on PZT Based Piezoelectric Energy Harvesting Technologies

    Directory of Open Access Journals (Sweden)

    Min-Gyu Kang

    2016-02-01

    Full Text Available Energy harvesting is the most effective way to respond to the energy shortage and to produce sustainable power sources from the surrounding environment. The energy harvesting technology enables scavenging electrical energy from wasted energy sources, which always exist everywhere, such as in heat, fluids, vibrations, etc. In particular, piezoelectric energy harvesting, which uses a direct energy conversion from vibrations and mechanical deformation to the electrical energy, is a promising technique to supply power sources in unattended electronic devices, wireless sensor nodes, micro-electronic devices, etc., since it has higher energy conversion efficiency and a simple structure. Up to now, various technologies, such as advanced materials, micro- and macro-mechanics, and electric circuit design, have been investigated and emerged to improve performance and conversion efficiency of the piezoelectric energy harvesters. In this paper, we focus on recent progress of piezoelectric energy harvesting technologies based on PbZrxTi1-xO3 (PZT materials, which have the most outstanding piezoelectric properties. The advanced piezoelectric energy harvesting technologies included materials, fabrications, unique designs, and properties are introduced to understand current technical levels and suggest the future directions of piezoelectric energy harvesting.

  4. Piezoelectric and mechanical properties of fatigue resistant, self-healing PZT-ionomer composites

    NARCIS (Netherlands)

    James, N.K.; Lafont, U.; Zwaag, S. van der; Groen, W.A.

    2014-01-01

    Piezoelectric ceramic-polymer composites with 0-3 connectivity were fabricated using lead zirconium titanate (PZT) powder dispersed in an ionomer (Zn ionomer) and its reference ethylene methacrylic acid copolymer (EMAA) polymer matrix. The PZT-Zn ionomer and PZT-EMAA composites were prepared by melt

  5. Piezoelectric Energy Harvesting Using PZT Bimorphs and Multilayered Stacks

    Science.gov (United States)

    Panda, Prasanta Kumar; Sahoo, Benudhar; Chandraiah, M.; Raghavan, Sreekumari; Manoj, Bindu; Ramakrishna, J.; Kiran, P.

    2015-11-01

    Piezoelectric materials have a unique ability to interchange electrical and mechanical energy. This property allows the absorption of mechanical energy such as ambient vibration and its transformation into electrical energy. The electrical energy generated can be used to power low-power electronic devices. In the present study, energy harvesting by lead zirconate titanate (PZT) multilayer (ML) stacks and bimorphs is presented. The devices were fabricated by a tape casting technique and were poled at 2 kV/mm for 30 min immersed in a silicone oil bath maintained at 60°C. The energy harvesting characteristics of the fabricated devices were measured in a suitably assembled test setup. The output voltage obtained from the PZT bimorphs and ML stacks was 450 mV and 125 mV, respectively. The higher output voltage from the bimorph is due to its low capacitance.

  6. The Fabrication and Characterization of Piezoelectric PZT/PVDF Electrospun Nanofiber Composites

    Directory of Open Access Journals (Sweden)

    Ji Sun Yun

    2016-03-01

    Full Text Available Piezoelectric nanofiber composites of polyvinylidene fluoride (PVDF polymer and PZT (Pb(Zr0.53Ti0.47O3 ceramics were fabricated by electrospinning. The micro‐ structure of the PZT/PVDF electrospun nanofiber compo‐ sites was characterized using X-ray diffraction (XRD, scanning electron microscopy (SEM and transmission electron microscopy (TEM. The tensile properties (stress- strain curves and electrical properties (P-E hysteresis loops of the PZT/PVDF electrospun nanofiber composites were investigated as a function of PZT content from 0 wt% to 30 wt%. The results demonstrated that a PZT content of 20 wt % had enhanced tensile and piezoelectric characteristics.

  7. Fabrication and characterization of micromachined high-frequency tonpilz transducers derived by PZT thick films.

    Science.gov (United States)

    Zhou, Qifa; Cannata, Jonathan M; Meyer, Richard J; van Tol, David J; Tadigadapa, Srinivas; Hughes, W Jack; Shung, K Kirk; Trolier-McKinstry, Susan

    2005-03-01

    Miniaturized tonpilz transducers are potentially useful for ultrasonic imaging in the 10 to 100 MHz frequency range due to their higher efficiency and output capabilities. In this work, 4 to 10-microm thick piezoelectric thin films were used as the active element in the construction of miniaturized tonpilz structures. The tonpilz stack consisted of silver/lead zirconate titanate (PZT)/lanthanum nickelate (LaNiO3)/silicon on insulator (SOI) substrates. First, conductive LaNiO3 thin films, approximately 300 nm in thickness, were grown on SOI substrates by a metalorganic decomposition (MOD) method. The room temperature resistivity of the LaNiO3 was 6.5 x 10(-6) omega x m. Randomly oriented PZT (52/48) films up to 7-microm thick were then deposited using a sol-gel process on the LaNiO3-coated SOI substrates. The PZT films with LaNiO3 bottom electrodes showed good dielectric and ferroelectric properties. The relative dielectric permittivity (at 1 kHz) was about 1030. The remanent polarization of PZT films was larger than 26 microC/cm2. The effective transverse piezoelectric e31,f coefficient of PZT thick films was about -6.5 C/m2 when poled at -75 kV/cm for 15 minutes at room temperature. Enhanced piezoelectric properties were obtained on poling the PZT films at higher temperatures. A silver layer about 40-microm thick was prepared by silver powder dispersed in epoxy and deposited onto the PZT film to form the tail mass of the tonpilz structure. The top layers of this wafer were subsequently diced with a saw, and the structure was bonded to a second wafer. The original silicon carrier wafer was polished and etched using a Xenon difluoride (XeF2) etching system. The resulting structures showed good piezoelectric activity. This process flow should enable integration of the piezoelectric elements with drive/receive electronics.

  8. PZT thin films for piezoelectric MEMS mechanical energy harvesting

    Science.gov (United States)

    Yeager, Charles

    This thesis describes the optimization of piezoelectric Pb(ZrxTi 1-x)O3 (PZT) thin films for energy generation by mechanical energy harvesting, and self-powered micro-electro-mechanical systems (MEMS). For this purpose, optimization of the material was studied, as was the incorporation of piezoelectric films into low frequency mechanical harvesters. A systematic analysis of the energy harvesting figure of merit was made. As a figure of merit (e31,ƒ)2/epsilon r (transverse piezoelectric coefficient squared over relative permittivity) was utilized. PZT films of several tetragonal compositions were grown on CaF2, MgO, SrTiO3, and Si substrates, thereby separating the dependence of composition on domain orientation. To minimize artifacts associated with composition gradients, and to extend the temperature growth window, PZT films were grown by metal organic chemical vapor deposition (MOCVD). Using this method, epitaxial {001} films achieved c-domain textures above 90% on single crystal MgO and CaF2 substrates. This could be tailored via the thermal stresses established by the differences in thermal expansion coefficients of the film and the substrate. The single-domain e31,ƒ for PZT thin films was determined to exceed -12 C/m2 in the tetragonal phase field for x ≥ 0.19, nearly twice the phenomenologically modeled value. The utilization of c-domain PZT films is motivated by a figure of merit above 0.8 C2/m4 for (001) PZT thin films. Increases to the FoM via doping and hot poling were also quantified; a 1% Mn doping reduced epsilonr by 20% without decreasing the piezoelectric coefficient. Hot poling a device for one hour above 120°C also resulted in a 20% reduction in epsilonr ; furthermore, 1% Mn doping reduced epsilonr by another 12% upon hot poling. Two methods for fabricating thin film mechanical energy harvesting devices were investigated. It was found that phosphoric acid solutions could be used to pattern MgO crystals, but this was typically accompanied by

  9. Towards a digital sound reconstruction MEMS device: Characterization of a single PZT based piezoelectric actuator

    KAUST Repository

    Carreno, Armando Arpys Arevalo

    2015-04-01

    In this paper we report the fabrication and characterization of a single piezoelectric actuator for digital sound reconstruction. This work is the first step towards the implementation of a true digital micro-loudspeaker by means of an array of acoustic actuators. These actuators consist of a flexible membrane fabricated using polyimide, which is actuated using a Lead-Zirconate-Titanate (PZT) piezoelectric ceramic layer working in the d31 actuation mode. The dimensions of the membrane are of 1mm diameter and 4μm in thickness, which is capable of being symmetrically actuated in both upward and downward directions, due to the back etch step releasing the membrane. Our electrical characterization shows an improvement in the polarization of the piezoelectric material after its final etch patterning step, and our mechanical characterization shows the natural modes of resonance of the stacked membrane. © 2015 IEEE.

  10. Enhanced piezoelectric performance of composite sol-gel thick films evaluated using piezoresponse force microscopy.

    Science.gov (United States)

    Liu, Yuanming; Lam, Kwok Ho; Kirk Shung, K; Li, Jiangyu; Zhou, Qifa

    2013-05-14

    Conventional composite sol-gel method has been modified to enhance the piezoelectric performance of ceramic thick films. Lead zirconate titanate (PZT) and lead magnesium niobate-lead titanate (PMN-PT) thick films were fabricated using the modified sol-gel method for ultrasonic transducer applications. In this work, piezoresponse force microscopy was employed to evaluate the piezoelectric characteristics of PZT and PMN-PT composite sol-gel thick films. The images of the piezoelectric response and the strain-electric field hysteresis loop behavior were measured. The effective piezoelectric coefficient (d33,eff) of the films was determined from the measured loop data. It was found that the effective local piezoelectric coefficient of both PZT and PMN-PT composite films is comparable to that of their bulk ceramics. The promising results suggest that the modified composite sol-gel method is a promising way to prepare the high-quality, crack-free ceramic thick films.

  11. Temperature and strain rate effects on the piezoelectric charge production of PZT 95/5

    Science.gov (United States)

    Khan, Amnah S.; Proud, William G.

    2017-01-01

    To develop a better understanding of the piezoelectric ceramic lead zirconate titanate (PZT) 95/5, parameters including varying temperatures, porosities and strain rates have been studied. The effects on the charge output and fracture of poled PZT samples of different porosities have been investigated with compressive strain rates (10-4 - 10+3 s-1) using quasi-static loading equipment, drop-weight towers and Split Hopkinson Pressure Bars (SHPBs). The cylindrical specimens were of 4.4 mm diameter, thickness 0.8 - 4.4 mm, and density 7.3 - 8.3 g cm-3. The temperature range of -20 °C to +80 °C was achieved using purpose-built environmental chambers. The resulting stress-strain relationships are compared; all the samples ultimately displayed a brittle response at failure [1].

  12. Electrical excitation and optical detection of ultrasounds in PZT based piezoelectric transducers

    Energy Technology Data Exchange (ETDEWEB)

    Babilotte, P; Diallo, O; Hue, L-P Tran Hu; Feuillard, G [University Francois Rabelais de Tours, Laboratory Imaging and Brain, Team Ultrasonic Characterisation and Piezoelectricity, ENIVL, Rue de la Chocolaterie, 41034 BLOIS CEDEX (France); Kosec, M; Kuscer, D, E-mail: philippe.babilotte@univ-tours.fr [Josef Stefan Institute, Jamova cesta 39, 1000 LJUBLJANA (Slovenia)

    2011-01-01

    The displacement response of piezoelectric PZT thick films fabricated by means of electrophoretic deposition and laid down an alumina substrate is investigated using coherent optical detection. According to thickness properties determined by electrical impedance measurements, the film presents a resonance around 40 MHz. Other resonance peaks are observed that correspond to eigen modes of the film substrate couple structure. Uniformity of the response of the integrated structure is studied across the surface of the sample when excited by either a continuous or impulse electrical voltage. Results on the amplitude of the detected signal versus the frequency and the input excitation voltage are reported. The optical detection used in these experiments is complementary to conventional techniques of characterization of piezoelectric devices such as electrical impedance measurements and allows getting information on the displacement response of the device.

  13. Mechanical and electrical strain response of a piezoelectric auxetic PZT lattice structure

    Science.gov (United States)

    Fey, Tobias; Eichhorn, Franziska; Han, Guifang; Ebert, Kathrin; Wegener, Moritz; Roosen, Andreas; Kakimoto, Ken-ichi; Greil, Peter

    2016-01-01

    A two-dimensional auxetic lattice structure was fabricated from a PZT piezoceramic. Tape casted and sintered sheets with a thickness of 530 μm were laser cut into inverted honeycomb lattice structure with re-entrant cell geometry (θ = -25°) and poling direction oriented perpendicular to the lattice plane. The in-plane strain response upon applying an uniaxial compression load as well as an electric field perpendicular to the lattice plane were analyzed by a 2D image data detection analysis. The auxetic lattice structure exhibits orthotropic deformation behavior with a negative in-plane Poisson’s ratio of -2.05. Compared to PZT bulk material the piezoelectric auxetic lattice revealed a strain amplification by a factor of 30-70. Effective transversal coupling coefficients {{d}al}31 of the PZT lattice exceeding 4 × 103 pm V-1 were determined which result in an effective hydrostatic coefficient {{d}al}h 66 times larger than that of bulk PZT.

  14. Piezoelectric Resonance Investigation of Zr-rich PZT at Room Temperature

    NARCIS (Netherlands)

    Cereceda, N.; Noheda, B.; Fernandez-del-Castillo, J.R.; Gonzalo, J.A.; Frutos, J. De

    1999-01-01

    We study the piezoelectric resonances in poled PZT ceramics by means of a microscopic model. It connects the microscopic vibrations of the ionic units, cooperatively producing the piezoelectric effect, with the macroscopic piezoelectric parameters. The behaviour at the resonance is well described in

  15. The Fabrication and Characterization of Piezoelectric PZT/PVDF Electrospun Nanofiber Composites

    OpenAIRE

    Ji Sun Yun; Chun Kil Park; Young Hun Jeong; Jeong Ho Cho; Jong-Hoo Paik; Sun Hong Yoon; Kyung-Ran Hwang

    2016-01-01

    Piezoelectric nanofiber composites of polyvinylidene fluoride (PVDF) polymer and PZT (Pb(Zr0.53Ti0.47)O3) ceramics were fabricated by electrospinning. The micro‐ structure of the PZT/PVDF electrospun nanofiber compo‐ sites was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The tensile properties (stress- strain curves) and electrical properties (P-E hysteresis loops) of the PZT/PVDF electrospun nanofiber composites w...

  16. Highly-efficient, flexible piezoelectric PZT thin film nanogenerator on plastic substrates.

    Science.gov (United States)

    Park, Kwi-Il; Son, Jung Hwan; Hwang, Geon-Tae; Jeong, Chang Kyu; Ryu, Jungho; Koo, Min; Choi, Insung; Lee, Seung Hyun; Byun, Myunghwan; Wang, Zhong Lin; Lee, Keon Jae

    2014-04-23

    A highly-efficient, flexible piezoelectric PZT thin film nanogenerator is demonstrated using a laser lift-off (LLO) process. The PZT thin film nanogenerator harvests the highest output performance of ∼200 V and ∼150 μA·cm(-2) from regular bending motions. Furthermore, power sources generated from a PZT thin film nanogenerator, driven by slight human finger bending motions, successfully operate over 100 LEDs. © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  17. Study of dielectric and piezoelectric properties of CNT reinforced PZT-PVA 0-3 composite

    Science.gov (United States)

    Vyas, Prince; Prajapat, Rampratap; Manmeeta, Saxena, Dhiraj

    2016-05-01

    Ferroelectric ceramic/polymer composites have the compliance of polymers which overcome the problems of brittleness in ceramics. By imbedding piezoelectric ceramic powder into a polymer matrix, 0-3 composites with good mechanical properties and high dielectric breakdown strength can be developed. The obtained composites of 0-3 connectivity exhibit the piezoelectric properties of ceramics and flexibility, strength and lightness of polymer. These composites can be used in vibration sensing and transducer applications specially as piezoelectric sensors. A potential way to improve piezoelectric& dielectric properties of theses composites is by inclusion of another conductive phase in these composites as reported in the literature. In present work, we prepared PZT-PVA 0-3 composites with 60% ceramic volume fraction reinforced with CNTs with volume ranging from 0 to 1.5 vol%. These CNT reinforced composites were obtained using hot press method with thickness of 200 µm having 0-3 conductivity. These composites were poled applying DC voltage. Dielectric properties of these samples were obtained in a wide frequency range (100 Hz to 1 Mhz) at room temperature. The piezoelectric properties of these composites were analyzed by measuring piezoelectric charge constants (d33). The dielectric and piezoelectric properties of these composites were studied as a function of CNT volume content. In these reinforced composites, CNTs act as a conductive filler dispersed in the matrix which in turn facilitates poling and results in an increase of the piezoelectric properties of the composite due to formation of percolation path through the composites. With a CNT content of 0.3 vol.% in PZT/PVA/CNTs, an increase of 61.3 % was observed in piezoelectric strain factors (d33). In these CNT reinforced composites, a substantial increase (approx. 67%) was also observed in dielectric constant and approximately 89% increase was observed in dielectric loss factor. Results so obtained are in the good

  18. Measurement of effective piezoelectric coefficients of PZT thin films for energy harvesting application with interdigitated electrodes.

    Science.gov (United States)

    Chidambaram, Nachiappan; Mazzalai, Andrea; Muralt, Paul

    2012-08-01

    Interdigitated electrode (IDE) systems with lead zirconate titanate (PZT) thin films play an increasingly important role for two reasons: first, such a configuration generates higher voltages than parallel plate capacitor-type electrode (PPE) structures, and second, the application of an electric field leads to a compressive stress component in addition to the overall stress state, unlike a PPE structure, which results in tensile stress component. Because ceramics tend to crack at relatively moderate tensile stresses, this means that IDEs have a lower risk of cracking than PPEs. For these reasons, IDE systems are ideal for energy harvesting of vibration energy, and for actuators. Systematic investigations of PZT films with IDE systems have not yet been undertaken. In this work, we present results on the evaluation of the in-plane piezoelectric coefficients with IDE systems. Additionally, we also propose a simple and measurable figure of merit (FOM) to analyze and evaluate the relevant piezoelectric parameter for harvesting efficiency without the need to fabricate the energy harvesting device. Idealized effective coefficients e(IDE) and h(IDE) are derived, showing its composite nature with about one-third contribution of the transverse effect, and about two-thirds contribution of the longitudinal effect in the case of a PZT film deposited on a (100)-oriented silicon wafer with the in-plane electric field along one of the Si directions. Randomly oriented 1-μm-thick PZT 53/47 film deposited by a sol-gel technique, was evaluated and yielded an effective coefficient e(IDE) of 15 C·m(-2). Our FOM is the product between effective e and h coefficient representing twice the electrical energy density stored in the piezoelectric film per unit strain deformation (both for IDE and PPE systems). Assuming homogeneous fields between the fingers, and neglecting the contribution from below the electrode fingers, the FOM for IDE structures with larger electrode gap is derived to be

  19. MEMS-based thick film PZT vibrational energy harvester

    DEFF Research Database (Denmark)

    Lei, Anders; Xu, Ruichao; Thyssen, Anders

    2011-01-01

    We present a MEMS-based unimorph silicon/PZT thick film vibrational energy harvester with an integrated proof mass. We have developed a process that allows fabrication of high performance silicon based energy harvesters with a yield higher than 90%. The process comprises a KOH etch using a mechan......We present a MEMS-based unimorph silicon/PZT thick film vibrational energy harvester with an integrated proof mass. We have developed a process that allows fabrication of high performance silicon based energy harvesters with a yield higher than 90%. The process comprises a KOH etch using...... a mechanical front side protection of an SOI wafer with screen printed PZT thick film. The fabricated harvester device produces 14.0 μW with an optimal resistive load of 100 kΩ from 1g (g=9.81 m s-2) input acceleration at its resonant frequency of 235 Hz....

  20. Fabrication and characterization of MEMS-based PZT/PZT bimorph thick film vibration energy harvesters

    DEFF Research Database (Denmark)

    Xu, Ruichao; Lei, Anders; Dahl-Petersen, Christian

    2012-01-01

    We describe the fabrication and characterization of a significantly improved version of a microelectromechanical system-based PZT/PZT thick film bimorph vibration energy harvester with an integrated silicon proof mass; the harvester is fabricated in a fully monolithic process. The main advantage...... of bimorph vibration energy harvesters is that strain energy is not lost in mechanical support materials since only Pb(ZrxTi1-x)O3 (PZT) is strained; as a result, the effective system coupling coefficient is increased, and thus a potential for significantly higher output power is released. In addition, when...... the two layers are connected in series, the output voltage is increased, and as a result the relative power loss in the necessary rectifying circuit is reduced. We describe an improved process scheme for the energy harvester, which resulted in a robust fabrication process with a record high fabrication...

  1. Design, Modeling and Optimization of a Piezoelectric Pressure Sensor based on a Thin-Film PZT Membrane Containing Nanocrystalline Powders

    Directory of Open Access Journals (Sweden)

    Vahid MOHAMMADI

    2009-11-01

    Full Text Available In this paper fabrication of a 0-3 ceramic/ceramic composite lead zirconate titanate, Pb(Zr0.52Ti0.48O3 thin film has been presented and then a pressure sensor based on multilayer thin-film PZT diaphragm contain of Lead Zirconate Titanate nanocrystalline powders was designed, modeled and optimized. Dynamics characteristics of this multilayer diaphragm have been investigated by ANSYS® FE software. By this simulation the effective parameters of the multilayer PZT diaphragm for improving the performance of a pressure sensor in different ranges of pressure are optimized. The optimized thickness ratio of PZT layer to SiO2 was given in the paper to obtain the maximum deflection of the multilayer thin-film PZT diaphragm. A 0-3 ceramic/ceramic composite lead zirconate titanate, Pb(Zr0.52Ti0.48O3 film has been developed to fabricate the pressure sensor by a hybrid sol gel process. PZT nanopowders fabricated via conventional sol gel method and uniformly dispersed in PZT precursor solution by an attrition mill. XRD analysis shows that perovskite structure would be formed due to the presence of a significant amount of ceramic nanopowders. This texture has a good effect on piezoelectric properties of perovskite structure. The film forms a strongly bonded network and less shrinkage occurs, so the films do not crack during process. Also the aspect ratio through this process would be increased. SEM micrographs indicated that PZT films were uniform, crack free and have a composite microstructure and a piezoelectric coefficient d31 of -40 pC.N-1 and d33 ranged from 50pm.N-1 to 60pm.N-1.

  2. Piezoelectric and mechanical properties of fatigue resistant, self-healing PZT-ionomer composites

    Science.gov (United States)

    James, N. K.; Lafont, U.; van der Zwaag, S.; Groen, W. A.

    2014-05-01

    Piezoelectric ceramic-polymer composites with 0-3 connectivity were fabricated using lead zirconium titanate (PZT) powder dispersed in an ionomer (Zn ionomer) and its reference ethylene methacrylic acid copolymer (EMAA) polymer matrix. The PZT-Zn ionomer and PZT-EMAA composites were prepared by melt extrusion followed by hot pressing. The effects of poling conditions such as temperature, time and electric field on the piezoelectric properties of the composites were investigated. The experimentally observed piezoelectric charge coefficient and dielectric constant of the composites were compared with theoretical models. The results show that PZT-Zn ionomer composites have better piezoelectric properties compared to PZT-EMAA composites. The static and fatigue properties of the composites were investigated. The PZT-Zn ionomer composites were found to have excellent fatigue resistance even at strain levels of 4%. Due to the self-healing capabilities of the ionomer matrix, the loss of piezoelectric properties after high strain tensile cyclic loading could be partially recovered by thermal healing.

  3. Piezoelectric and dielectric properties of Cr-doped PSN-PZN-PZT quaternary piezoelectric ceramics

    Institute of Scientific and Technical Information of China (English)

    SUN Qingchi; WANG Lifeng; LIU Ping; NIE Qiang

    2005-01-01

    PSN-PZN-PZT + x wt.%Cr2O3, x = 0.0-0.9, were prepared by conventional mixed oxide techniques at sintering temperatures of 1220℃-1300℃ for 2 h. The effect of sintering temperature on the microstructure and the piezoelectric properties was investigated by XRD, SEM, and other conventional measurement. The result indicated that with temperature increasing, the valence of Cr ion from Cr5+ or Cr6+ changes into Cr3+, and the piezoelectric properties turn hard. With increasing Cr2O3 content, the amount of rhombohedral phases increases and the morphotropic boundary phase is correspondingly shifts to rhombohedral phase. A uniform microstructure and excellent comprehensive properties were obtained at 1240C as the amount of Cr2O3 is 0.5 wt.%.

  4. PZT/P(VDF-HFP) 0-3 composites as solvent-cast thin films: preparation, structure and piezoelectric properties

    Energy Technology Data Exchange (ETDEWEB)

    Wegener, Michael; Arlt, Kristin [Functional Polymer Systems, Fraunhofer Institute for Applied Polymer Research (IAP), Geiselbergstrasse 69, 14476 Potsdam-Golm (Germany)], E-mail: michael.wegener@iap.fraunhofer.de

    2008-08-21

    Composite films of lead zirconate titanate (PZT) and poly(vinylidene fluoride-hexafluoropropylene) (P(VDF-HFP)) were prepared as 100 {mu}m thin films by solvent casting. Within the 0-3 composites, the ceramic-volume fraction was varied between 0.19 and 0.65, which yielded films with different structural and dielectric properties. These influenced the piezoelectric properties of the composite films found after electric poling, which was performed here at room temperature. The piezoelectric activity, with a maximum piezoelectric coefficient of 11 pC N{sup -1} in the film-thickness direction, originates from the polarization of the embedded ceramic particles as proved by poling experiments in corona discharges as well as in direct contact.

  5. Processing effects for integrated PZT: Residual stress, thickness, and dielectric properties

    Science.gov (United States)

    Ong, Ryan Jason

    This dissertation focuses on the integration of lead zirconate titanate (PZT) films on Pt/Ti/SiO2//Si, and the effect of on properties. Direct deposition of PZT on Si will lead to on-chip power capacitors, non-volatile memory cells, and vibration sensors. However, previous research indicates that the dielectric, ferroelectric and piezoelectric response characteristics for the devices are often inferior to bulk specimens. Property variations have been attributed to changes in several major variables including, chemical composition, phase content, grain size, crystallographic orientation, film thickness, and stress, each of which, in turn, can depend on processing. The first goal of this work was to design a sol-gel processing methodology to control all major variables except film thickness and stress, thus isolating their respective effects on properties. All specimens were verified to be of the Pb(Zr0.53Ti0.47)O3 composition, in the perovskite structure, with a constant grain size of 110nm, and with (111) fiber texture. PZT film thickness was varied from 95nm to 500nm and residual stress was measured to be either 150 or 180MPa, biaxial tensile, depending on thickness. These specimens allowed for new insights into the fundamental differences between bulk materials and thin films. A series-capacitor model accounted for the observed dilution in room-temperature K from >900 to ˜600 as film thickness decreased, but could not account for the absence of the expected dielectric anomaly at high temperatures. Instead, a stress-induced distributed phase transformation related to the polycrystalline nature of the film was proposed to account for the observed behavior. Residual stress reduced the spontaneous polarization values in these specimens to 32muC/cm 2 from the predicted stress-free value of 50muC/cm2. An increase in coercive field was attributed to interfacial capacitance and residual stress, whereas a decrease of 30MPa tensile stress resulted in an increase of d33

  6. Fabrication and Characterization of PZT Thick Films for Sensing and Actuation

    Directory of Open Access Journals (Sweden)

    Kuo-Ching Kuo

    2007-04-01

    Full Text Available Lead Zirconate Titanate oxide (PZT thick films with thicknesses of up to 10 μmwere developed using a modified sol-gel technique. Usually, the film thickness is less than1 μm by conventional sol-gel processing, while the electrical charge accumulation whichreveals the direct effect of piezoelectricity is proportional to the film thickness and thereforerestricted. Two approaches were adopted to conventional sol-gel processing – precursorconcentration modulation and rapid thermal annealing. A 10 μm thick film was successfullyfabricated by coating 16 times via this technique. The thickness of each coating layer wasabout 0.6 μm and the morphology of the film was dense with a crack-free area as large as 16mm2. In addition, the structure, surface morphology and physical properties werecharacterized by X-ray diffraction (XRD, scanning electron microscopy (SEM and atomicforce microscopy (AFM and electrical performance. The dielectric constant and hysteresisloops were measured as electric characteristics. This study investigates the actuation andsensing performance of the vibrating structures with the piezoelectric thick film. Theactuation tests demonstrated that a 4 mm x 4 mm x 6.5 μm PZT film drove a 40 mm x 7 mmx 0.5 mm silicon beam as an actuator. Additionally, it generated an electrical signal of 60mVpp as a sensor, while vibration was input by a shaker. The frequencies of the first twomodes of the beam were compared with the theoretical values obtained by Euler-Bernoullibeam theory. The linearity of the actuation and sensing tests were also examined.

  7. Thickness dependence of electrical properties of PZT films deposited on metal substrates by laser-assisted aerosol deposition.

    Science.gov (United States)

    Baba, S; Tsuda, H; Akedo, J

    2008-05-01

    Dependence of electrical properties-dielectric, ferroelectric, and piezoelectric properties-on film thickness was studied for lead-zirconate titanate (PZT) thick films directly deposited onto stainless-steel (SUS) substrates in actuator devices by using a carbon dioxide (CO(2) ), laser assisted aerosol deposition technique. Optical spectroscopic analysis data and laser irradiation experiments revealed that absorption at a given wavelength by the film increased with increasing film thickness. Dielectric constant epsilon, remanent polarization value P(r), and coercive field strength E(c) of PZT films directly deposited onto a SUS-based piezoelectric actuator substrate annealed by CO(2) laser irradiation at 850 degrees C improved with increasing film thickness, and for films thicker than 25 microm, epsilon 800, P(r) 40 microC/cm(2), and E(c) 45 kV/cm. In contrast, the displacement of the SUS-based actuator with the laser-annealed PZT thick film decreased with increasing film thickness.

  8. Design Optimization of PZT-Based Piezoelectric Cantilever Beam by Using Computational Experiments

    Science.gov (United States)

    Kim, Jihoon; Park, Sanghyun; Lim, Woochul; Jang, Junyong; Lee, Tae Hee; Hong, Seong Kwang; Song, Yewon; Sung, Tae Hyun

    2016-08-01

    Piezoelectric energy harvesting is gaining huge research interest since it provides high power density and has real-life applicability. However, investigative research for the mechanical-electrical coupling phenomenon remains challenging. Many researchers depend on physical experiments to choose devices with the best performance which meet design objectives through case analysis; this involves high design costs. This study aims to develop a practical model using computer simulations and to propose an optimized design for a lead zirconate titanate (PZT)-based piezoelectric cantilever beam which is widely used in energy harvesting. In this study, the commercial finite element (FE) software is used to predict the voltage generated from vibrations of the PZT-based piezoelectric cantilever beam. Because the initial FE model differs from physical experiments, the model is calibrated by multi-objective optimization to increase the accuracy of the predictions. We collect data from physical experiments using the cantilever beam and use these experimental results in the calibration process. Since dynamic analysis in the FE analysis of the piezoelectric cantilever beam with a dense step size is considerably time-consuming, a surrogate model is employed for efficient optimization. Through the design optimization of the PZT-based piezoelectric cantilever beam, a high-performance piezoelectric device was developed. The sensitivity of the variables at the optimum design is analyzed to suggest a further improved device.

  9. Exploring the piezoelectric performance of PZT particulate-epoxy composites loaded in shear

    NARCIS (Netherlands)

    Loock, F.V.; Deutz, D.B.; Zwaag, S.V.D.; Groen, W.A.

    2016-01-01

    The active and passive piezoelectric response of lead zirconium titanate (PZT)-epoxy particulate composites loaded in shear is studied using analytical models, a finite element model and by experiments. The response is compared to that of the same composites when loaded in simple tension. Analogousl

  10. Ferroelectric and piezoelectric properties of epitaxial PZT films and devices on silicon

    NARCIS (Netherlands)

    Nguyen, Minh Duc

    2010-01-01

    In this thesis, the integration of lead zirconate titanate Pb(Zr,Ti)O3 (PZT) thin films into piezoelectric microelectromechanical systems (MEMS) based on silicon is studied. In these structures, all epitaxial oxide layers (thin film/electrode/buffer-layer(s)) were deposited by pulsed laser depositio

  11. Ferroelectric and piezoelectric properties of epitaxial PZT films and devices on silicon

    NARCIS (Netherlands)

    Nguyen, Duc Minh

    2010-01-01

    In this thesis, the integration of lead zirconate titanate Pb(Zr,Ti)O3 (PZT) thin films into piezoelectric microelectromechanical systems (MEMS) based on silicon is studied. In these structures, all epitaxial oxide layers (thin film/electrode/buffer-layer(s)) were deposited by pulsed laser depositio

  12. Enhancing the dielectric property of 0.69PZT-0.31PZNN thick films by optimizing the poling condition

    Science.gov (United States)

    Song, Daniel; Woo, Min Sik; Ahn, Jung Hwan; Sung, Tae Hyun

    2015-05-01

    We investigated how the applied electric-field's magnitude and the poling time affected, respectively, the dielectric property and the microstructure of piezoelectric lead zirconate titanate/lead zirconate nickel niobate (PZT-PZNN) thick films in order to apply the films to piezoelectric energy harvesters. Several 300-µm-thick, 10 × 10-mm2 PZT-PZNN squares were tape cast, laminated, sintered, and poled under 2-, 4-, 6-, 10-, 14-, and 15-kV/mm electric fields for 30 min. The 10-kV/mm electric field produced the highest d 33 × g 33 without mechanically damaging the sample. Further, samples were sintered at 950, 1000, and 1020 °C and subsequently poled at 10 kV/mm (previously determined as the magnitude of the optimal poling electric field) for 15, 30, 60, 120, and 240 min to investigate how the poling time affected the piezoelectric ceramic's microstructure. The optimal poling time for all the sintered samples was 60 min. Further, the piezoelectric ceramics composed of small grains and poled longer than 60 min showed higher dielectric constants. However, those composed of large grains and poled for times shorter than 60 min showed higher dielectric constants because the element mobility of the piezoelectric ceramics increased with increasing poling time.

  13. Enhanced off-resonance magnetoelectric response in laser annealed PZT thick film grown on magnetostrictive amorphous metal substrate

    Energy Technology Data Exchange (ETDEWEB)

    Palneedi, Haribabu [Materials Interface Laboratory, Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology (KAIST), Daejeon 305-701 (Korea, Republic of); Functional Ceramics Group, Korea Institute of Materials Science (KIMS), Changwon 641-831 (Korea, Republic of); Maurya, Deepam; Priya, Shashank [Bio-inspired Materials and Devices Laboratory (BMDL), Center for Energy Harvesting Materials and Systems (CEHMS), Virginia Tech, Blacksburg, Virginia 24061 (United States); Kim, Gi-Yeop; Choi, Si-Young, E-mail: youngchoi@kims.re.kr [Materials Modeling and Characterization Department, Korea Institute of Materials Science (KIMS), Changwon 641-831 (Korea, Republic of); Kang, Suk-Joong L. [Materials Interface Laboratory, Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology (KAIST), Daejeon 305-701 (Korea, Republic of); Kim, Kwang-Ho [School of Materials Science and Engineering, Pusan National University, Busan 609-735 (Korea, Republic of); Ryu, Jungho, E-mail: jhryu@kims.re.kr [Functional Ceramics Group, Korea Institute of Materials Science (KIMS), Changwon 641-831 (Korea, Republic of)

    2015-07-06

    A highly dense, 4 μm-thick Pb(Zr,Ti)O{sub 3} (PZT) film is deposited on amorphous magnetostrictive Metglas foil (FeBSi) by granule spray in vacuum process at room temperature, followed by its localized annealing with a continuous-wave 560 nm ytterbium fiber laser radiation. This longer-wavelength laser radiation is able to anneal the whole of thick PZT film layer without any deteriorative effects, such as chemical reaction and/or atomic diffusion, at the interface and crystallization of amorphous Metglas substrate. Greatly enhanced dielectric and ferroelectric properties of the annealed PZT are attributed to its better crystallinity and grain growth induced by laser irradiation. As a result, a colossal off-resonance magnetoelectric (ME) voltage coefficient that is two orders of magnitude larger than previously reported output from PZT/Metglas film-composites is achieved. The present work addresses the problems involved in the fabrication of PZT/Metglas film-composites and opens up emerging possibilities in employing piezoelectric materials with low thermal budget substrates (suitable for integrated electronics) and designing laminate composites for ME based devices.

  14. Enhanced off-resonance magnetoelectric response in laser annealed PZT thick film grown on magnetostrictive amorphous metal substrate

    Science.gov (United States)

    Palneedi, Haribabu; Maurya, Deepam; Kim, Gi-Yeop; Priya, Shashank; Kang, Suk-Joong L.; Kim, Kwang-Ho; Choi, Si-Young; Ryu, Jungho

    2015-07-01

    A highly dense, 4 μm-thick Pb(Zr,Ti)O3 (PZT) film is deposited on amorphous magnetostrictive Metglas foil (FeBSi) by granule spray in vacuum process at room temperature, followed by its localized annealing with a continuous-wave 560 nm ytterbium fiber laser radiation. This longer-wavelength laser radiation is able to anneal the whole of thick PZT film layer without any deteriorative effects, such as chemical reaction and/or atomic diffusion, at the interface and crystallization of amorphous Metglas substrate. Greatly enhanced dielectric and ferroelectric properties of the annealed PZT are attributed to its better crystallinity and grain growth induced by laser irradiation. As a result, a colossal off-resonance magnetoelectric (ME) voltage coefficient that is two orders of magnitude larger than previously reported output from PZT/Metglas film-composites is achieved. The present work addresses the problems involved in the fabrication of PZT/Metglas film-composites and opens up emerging possibilities in employing piezoelectric materials with low thermal budget substrates (suitable for integrated electronics) and designing laminate composites for ME based devices.

  15. Dielectric and Piezoelectric Properties of 0-3 PZT/PVDF Composite Doped with Polyaniline

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    Lead zirconate titanate (PZT)/polyvinylidenc fluoride (PVDF) 0- 3 piezoelectric composites doped with polyaniline (PANI) were obtained by hot-press method.The polarization properties of the composites were characterized by XRD and P- E hysteresis loops at room temperature.And the dielectric and piezoelectric properties were also measured.The results show that the poling of PZT could be effectively carried out and the dielectric constant εr and dissipation tanδ increase monotonously by increasing the voltme fraction of PANI in the composite.The piezoelectric constant d33, and the planar electromechanical coupling factor kp increase while the mechanical quality factor Qm decreases with the increase in the content of PANI.The d33 , kp and Qm show the extremum valnes at 8 vol%-10 vol% PANI.

  16. Piezoelectric ceramic thick films deposited on silicon substrates by screen printing

    Science.gov (United States)

    Yao, Kui; He, Xujiang; Xu, Yuan; Chen, Meima

    2004-07-01

    Screen-printing processes offer advantages in producing directly patterned and integrated piezoelectric elements, and fill an important technological gap between thin film and bulk ceramics. However, several existing problems in the screen-printed piezoelectric thick films, such as the poor reliability and the required high sintering temperature, are significantly limiting their applications. In this work, lead zirconate titanate (PZT) ceramic films of 30 μm in thickness were deposited on Pt-coated silicon substrates by the screen-printing process, in which the ceramic pastes were prepared through a chemical liquid-phase doping approach. Porous thick films with good adhesion were formed on the substrates at a temperature of 925°C. Stable out-of-plane piezoelectric vibration of the thick films was observed with a laser scanning vibrometer (LSV), and the piezoelectric dilatation magnitude was determined accordingly. Our piezoelectric measurements through the areal displacement detection with LSV exhibited distinct advantages for piezoelectric film characterization, including high reliability, high efficiency, and comprehensive information. The longitudinal piezoelectric coefficients of the thick films were calculated from the measured dilatation data through a numerical simulation. High piezoelectric voltage constants were obtained due to the very low dielectric constant of the porous thick films. The application potentials of our screen-printed thick films as integrated piezoelectric sensors are discussed.

  17. Properties of PZT thick film made on LTCC substrates with dielectric intermediate layers

    Science.gov (United States)

    DÄ browski, Arkadiusz; Golonka, Leszek

    2016-11-01

    Results of experiments on application of various interlayers between LTCC (Low Temperature Cofired Ceramics) substrate and thick-film PZT (Lead Zirconate - Titanate) are described in this work. Thick-film intermediate layers were based on several dielectric materials: TiN, Al2O3, SiC, TiO2, SiC, YSZ, BN. Seven screen printable pastes were prepared on the base of powders of mentioned materials with addition of glass and organic vehicle. The substrates were made of 951 (DuPont), CeramTapeGC (CeramTec) and HL2000 (Heraeus) LTCC tapes. Sandwich type transducers, consisting of barrier layer, gold bottom electrode, PZT layer and silver top electrode were prepared and characterized. Basic piezoelectric parameters - permittivity, effective charge constant (d33(eff)) and remanent polarization were determined. The best properties were obtained for substrates made of 951. In general, interlayers based on TiO2, SiC and Al2O3 improved permittivity and charge constant comparing to bare substrates. For example, for 951 substrate the PZT layer exhibited d33(eff) equal to 160, 215, 250 and 230 pC/N for bare substrate, TiO2 interlayer, SiC interlayer and Al2O3 interlayer, respectively. In case of CeramTape GC substrates determined permittivity was equal to 215, 245, 235 and 275 for bare substrate, TiO2 interlayer, SiC interlayer and Al2O3 interlayer, respectively. In case of TiN and BN materials the parameters were considerably deteriorated.

  18. Micro-particle manipulation by single beam acoustic tweezers based on hydrothermal PZT thick film

    Directory of Open Access Journals (Sweden)

    Benpeng Zhu

    2016-03-01

    Full Text Available Single-beam acoustic tweezers (SBAT, used in laboratory-on-a-chip (LOC device has promising implications for an individual micro-particle contactless manipulation. In this study, a freestanding hydrothermal PZT thick film with excellent piezoelectric property (d33 = 270pC/N and kt = 0.51 was employed for SBAT applications and a press-focusing technology was introduced. The obtained SBAT, acting at an operational frequency of 50MHz, a low f-number (∼0.9, demonstrated the capability to trap and manipulate a micro-particle sized 10μm in the distilled water. These results suggest that such a device has great potential as a manipulator for a wide range of biomedical and chemical science applications.

  19. Micro-particle manipulation by single beam acoustic tweezers based on hydrothermal PZT thick film

    Science.gov (United States)

    Zhu, Benpeng; Xu, Jiong; Li, Ying; Wang, Tian; Xiong, Ke; Lee, Changyang; Yang, Xiaofei; Shiiba, Michihisa; Takeuchi, Shinichi; Zhou, Qifa; Shung, K. Kirk

    2016-01-01

    Single-beam acoustic tweezers (SBAT), used in laboratory-on-a-chip (LOC) device has promising implications for an individual micro-particle contactless manipulation. In this study, a freestanding hydrothermal PZT thick film with excellent piezoelectric property (d33 = 270pC/N and kt = 0.51) was employed for SBAT applications and a press-focusing technology was introduced. The obtained SBAT, acting at an operational frequency of 50MHz, a low f-number (∼0.9), demonstrated the capability to trap and manipulate a micro-particle sized 10μm in the distilled water. These results suggest that such a device has great potential as a manipulator for a wide range of biomedical and chemical science applications. PMID:27014504

  20. Micro-particle manipulation by single beam acoustic tweezers based on hydrothermal PZT thick film

    Energy Technology Data Exchange (ETDEWEB)

    Zhu, Benpeng, E-mail: benpengzhu@hust.edu.cn [School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074 (China); State Key Laboratory of Transducer Technology, Chinese Academy of Sciences, Shanghai 200050 (China); Xu, Jiong; Yang, Xiaofei [School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074 (China); Li, Ying; Lee, Changyang; Zhou, Qifa; Shung, K. Kirk [Department of Biomedical Engineering and NIH Transducer Resource Center, University of Southern California, Los Angeles, California 90089-1111 (United States); Wang, Tian; Xiong, Ke [Department of Physics and Key Laboratory of Acoustic and Photonic Materials and Devices of Ministry of Education, Wuhan University, Wuhan 430072 (China); Shiiba, Michihisa; Takeuchi, Shinichi [Medical Engineering Course, Graduate School of Engineering, Toin University of Yokohama, Yokohama 225-8501 (Japan)

    2016-03-15

    Single-beam acoustic tweezers (SBAT), used in laboratory-on-a-chip (LOC) device has promising implications for an individual micro-particle contactless manipulation. In this study, a freestanding hydrothermal PZT thick film with excellent piezoelectric property (d{sub 33} = 270 pC/N and k{sub t} = 0.51) was employed for SBAT applications and a press-focusing technology was introduced. The obtained SBAT, acting at an operational frequency of 50 MHz, a low f-number (∼0.9), demonstrated the capability to trap and manipulate a micro-particle sized 10μm in the distilled water. These results suggest that such a device has great potential as a manipulator for a wide range of biomedical and chemical science applications.

  1. Research on Composite PZT for Largedisplacement Actuators

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    A new kind of composite piezoelectric ceramics for large-displacement actuators, which were composed of reduced and unreduced layers, was prepared from normal PZT by chemical reduction. The stress distribution inside the composite PZT was researched and the chemical reduction conditions were explored.The actuating properties of reduced PZT were also studied. It is found that the optimal ratio of reduced layer thickness for the composite structure is 0.3; Reduced composite PZT has lower resonance frequency and 3 times larger displacement than that of the traditional PZT; Re-oxide phases are found in reduced layer of composite PZT showing the reduction procedure needs to be improved.

  2. Fabrication and characterization of thick-film piezoelectric lead zirconate titanate ceramic resonators by tape-casting.

    Science.gov (United States)

    Qin, Lifeng; Sun, Yingying; Wang, Qing-Ming; Zhong, Youliang; Ou, Ming; Jiang, Zhishui; Tian, Wei

    2012-12-01

    In this paper, thick-film piezoelectric lead zirconate titanate (PZT) ceramic resonators with thicknesses down to tens of micrometers have been fabricated by tape-casting processing. PZT ceramic resonators with composition near the morphotropic phase boundary and with different dopants added were prepared for piezoelectric transducer applications. Material property characterization for these thick-film PZT resonators is essential for device design and applications. For the property characterization, a recently developed normalized electrical impedance spectrum method was used to determine the electromechanical coefficient and the complex piezoelectric, elastic, and dielectric coefficients from the electrical measurement of resonators using thick films. In this work, nine PZT thick-film resonators have been fabricated and characterized, and two different types of resonators, namely thickness longitudinal and transverse modes, were used for material property characterization. The results were compared with those determined by the IEEE standard method, and they agreed well. It was found that depending on the PZT formulation and dopants, the relative permittivities ε(T)(33)/ε(0) measured at 2 kHz for these thick-films are in the range of 1527 to 4829, piezoelectric stress constants (e(33) in the range of 15 to 26 C/m(2), piezoelectric strain constants (d(31)) in the range of -169 × 10(-12) C/N to -314 × 10(-12) C/N, electromechanical coupling coefficients (k(t)) in the range of 0.48 to 0.53, and k(31) in the range of 0.35 to 0.38. The characterization results shows tape-casting processing can be used to fabricate high-quality PZT thick-film resonators, and the extracted material constants can be used to for device design and application.

  3. The study of dielectric, pyroelectric and piezoelectric properties on hot pressed PZT-PMN systems

    Energy Technology Data Exchange (ETDEWEB)

    Srivastava, Geetika; Umarji, A. M. [Materials Research Centre, Indian Institute of Science, Bangalore-560 012 (India); Maglione, Mario [ICMCB, Universite de Bordeaux,-CNRS, 87, Av Dr Schweitzer 33806 Pessac (France)

    2012-12-15

    Hot uniaxial pressing technique has been adopted for the densification of PZT-PMN system with an aim to yield dense ceramics and to lower the sintering temperature and time for achieving better and reproducible electronic properties. The ceramics having >97% theoretical density and micron size grains are investigated for their dielectric, pyroelectric and piezoelectric properties. The effect of Li and Mn addition has also been studied.

  4. The study of dielectric, pyroelectric and piezoelectric properties on hot pressed PZT-PMN systems

    Directory of Open Access Journals (Sweden)

    Geetika Srivastava

    2012-12-01

    Full Text Available Hot uniaxial pressing technique has been adopted for the densification of PZT-PMN system with an aim to yield dense ceramics and to lower the sintering temperature and time for achieving better and reproducible electronic properties. The ceramics having >97% theoretical density and micron size grains are investigated for their dielectric, pyroelectric and piezoelectric properties. The effect of Li and Mn addition has also been studied.

  5. Lamb wave characteristics of thickness-graded piezoelectric IDT.

    Science.gov (United States)

    Roy Mahapatra, D; Singhal, A; Gopalakrishnan, S

    2005-10-01

    An equivalent single layer model of Lamb wave generation by thickness-graded piezoelectric IDT on host structure is developed. Various additional complexities, such as the coupling between the Lamb wave modes, complicated nature of the electro-mechanical excitation are considered. The model of infinite IDT is extended to deal with the finite IDT with edge discontinuities. The effects of electromechanical coupling and thickness gradation on the wavelength shifts are investigated. The problem of electrically driven instability within the IDT is analyzed. Numerical results are reported by considering Al2O3/PZT IDT as integral part of the host structure, which show that there are significant changes and improvements in the Lamb wave characteristics due to the graded configuration. Most important among these is the reduced dispersiveness of the Lamb wave modes, which is useful in launching a SAW that propagates with narrower pulse width and less attenuation.

  6. Recent Progress on PZT Based Piezoelectric Energy Harvesting Technologies

    OpenAIRE

    Min-Gyu Kang; Woo-Suk Jung; Chong-Yun Kang; Seok-Jin Yoon

    2016-01-01

    Energy harvesting is the most effective way to respond to the energy shortage and to produce sustainable power sources from the surrounding environment. The energy harvesting technology enables scavenging electrical energy from wasted energy sources, which always exist everywhere, such as in heat, fluids, vibrations, etc. In particular, piezoelectric energy harvesting, which uses a direct energy conversion from vibrations and mechanical deformation to the electrical energy, is a promising tec...

  7. Piezoelectric and dielectric characterization of corona and contact poled PZT-epoxy-MWCNT bulk composites

    Science.gov (United States)

    Banerjee, S.; Cook-Chennault, K. A.; Du, W.; Sundar, U.; Halim, H.; Tang, A.

    2016-11-01

    Three-phase lead zirconate titanate (PZT, PbZr0.52Ti0.48O3)-epoxy-multi-walled carbon nanotube (MWCNT) bulk composites were prepared, where the volume fraction of PZT was held constant at 30%, while the volume fraction of the MWCNTs was varied from 1.0%-10%. The samples were poled using either a parallel plate contact or contactless (corona) poling technique. The piezoelectric strain coefficient (d 33), dielectric constant (ɛ), and dielectric loss tangent (tan δ) of the samples were measured at 110 Hz, and compared as a function of poling technique and volume fraction of MWCNTs. The highest values for dielectric constant and piezoelectric strain coefficients were 465.82 and 18.87 pC/N for MWCNT volume fractions of 10% and 6%, respectively. These values were obtained for samples that were poled using the corona contactless method. The impedance and dielectric spectra of the composites were recorded over a frequency range of 100 Hz-20 MHz. The impedance values observed for parallel-plate contact poled samples are higher than that of corona poled composites. The fractured surface morphology and distribution of the PZT particles and MWCNTs were observed with the aid of electron dispersion spectroscopy and a scanning electron microscope. The surface morphology of the MWCNTs was observed with the aid of a field emission transmission electron microscope.

  8. Piezoelectric response of a PZT thin film to magnetic fields from permanent magnet and coil combination

    Science.gov (United States)

    Guiffard, B.; Seveno, R.

    2015-01-01

    In this study, we report the magnetically induced electric field E 3 in Pb(Zr0.57Ti0.43)O3 (PZT) thin films, when they are subjected to both dynamic magnetic induction (magnitude B ac at 45 kHz) and static magnetic induction ( B dc) generated by a coil and a single permanent magnet, respectively. It is found that highest sensitivity to B dc——is achieved for the thin film with largest effective electrode. This magnetoelectric (ME) effect is interpreted in terms of coupling between eddy current-induced Lorentz forces (stress) in the electrodes of PZT and piezoelectricity. Such coupling was evidenced by convenient modelling of experimental variations of electric field magnitude with both B ac and B dc induction magnitudes, providing imperfect open circuit condition was considered. Phase angle of E 3 versus B dc could also be modelled. At last, the results show that similar to multilayered piezoelectric-magnetostrictive composite film, a PZT thin film made with a simple manufacturing process can behave as a static or dynamic magnetic field sensor. In this latter case, a large ME voltage coefficient of under B dc = 0.3 T was found. All these results may provide promising low-cost magnetic energy harvesting applications with microsized systems.

  9. A comparative approach to predicting effective dielectric, piezoelectric and elastic properties of PZT/PVDF composites

    Energy Technology Data Exchange (ETDEWEB)

    Ahmad, Zeeshan [University Department of Physics, T.M. Bhagalpur University, Bhagalpur 812007 (India); Prasad, Ashutosh, E-mail: apd.phy@gmail.co [University Department of Physics, T.M. Bhagalpur University, Bhagalpur 812007 (India); Prasad, K., E-mail: k.prasad65@gmail.co [University Department of Physics, T.M. Bhagalpur University, Bhagalpur 812007 (India)

    2009-11-01

    The present study addresses the problem of quantitative prediction of effective relative permittivity, dielectric loss factor, piezoelectric charge coefficient, and Young's modulus of PZT/PVDF diphasic ceramic-polymer composite as a function of volume fraction of PZT in the different compositions. Theoretical results for effective relative permittivity derived from several dielectric mixture equations like those of Knott, Rother-Lichtenecker, Bruggeman, Maxwell-Wagner-Webmann-Skipetrov or Dias-Dasgupta, Furukawa, Lewin, Wiener, Jayasundere-Smith, Modified Cule-Torquato, Taylor, Poon-Shin and Rao et al. were fitted to the experimental data taken from previous works of Yamada et al. Similarly, the results for effective piezoelectric coefficient and Young's modulus, derived from different appropriate equations were fitted to the corresponding experimental data taken from the literature. The study revealed that only a few equations like modified Rother-Lichtenecker equation, Dias-Dasgupta equation and Rao equation for dielectric and piezoelectric properties while the four new equations developed in the present study of elastic property (Young's modulus) well fitted the corresponding experimental results. Further, the acceptable data put to various regression analyses showed that in most of the cases the third order polynomial regression analysis provided more acceptable fits.

  10. Low Temperature Processing of Nanocrystalline Lead Zirconate Titanate (PZT) Thick Films and Ceramics by a Modified Sol-Gel Route

    Science.gov (United States)

    Zhu, Weiguang; Wang, Zhihong; Zhao, Changlei; Tan, Ooi Kiang; Hng, Huey Hoon

    2002-11-01

    Dispersing fine particles into a sol-gel matrix is a promising process to get a thick 0-3 composite coating layer. In this paper, we have further improved this modified sol-gel process by nanocrystalline composite technique to realize the low temperature annealing. Dense Pb(Zr, Ti)O3 (PZT) thick films of 10 to 50 μm in thickness have been obtained on the platinum-coated silicon substrates by spin-coating at sintering temperature of 600-700°C and fully developed submicron-sized grains have been demonstrated in screen-printing piezoelectric films on alumina substrates at sintering temperature of 700-800°C. The dependence of various properties such as microstructure, crystallization, ferroelectric and dielectric properties of such made thick films on the processing parameters have been investigated. For a 10 μm-thick film spin-coated on silicon wafer, the dielectric loss and relative permittivity are 0.010 and 1024, respectively, at 1 kHz. The remanent polarization (Pr) and the coercive field (Ec) are 13.6 μC/cm2 and 34.5 kV/cm, respectively. Obviously, such made thick film has comparable properties with bulk PZT ceramic. This novel technique can be extensively used in sol-gel, screen-printing, tape-casting, even in traditional ceramic process to reduce the process temperature.

  11. Advances in piezoelectric PZT-based RF MEMS components and systems

    Science.gov (United States)

    Benoit, R. R.; Rudy, R. Q.; Pulskamp, J. S.; Polcawich, R. G.; Bedair, S. S.

    2017-08-01

    There is continuing interest in radio frequency (RF) microelectromechanical system (MEMS) devices due to their ability to offer exceptional RF performance, high linearity and low power consumption. To date, there is an impressive amount of RF MEMS components such as; switches, resonators, varactors, and tunable inductors that have enabled smaller, cheaper and more efficient RF systems. RF MEMS devices contain micromachined components that have the ability to move so that a change in the mechanical state of a device will result in a change to the device’s RF properties. There are many common modes of actuation, including, but not limited to: electrostatic, magnetostatic, piezoelectric, and electrothermal actuation. Although there are attractive aspects and drawbacks to each of these technologies, this paper will focus on advances in the application of piezoelectric actuation, and in particular the use of lead zirconium titanate (PZT), for RF MEMS.

  12. Effects of CeO2 doping on the structure and properties of PSN-PZN-PMS-PZT piezoelectric ceramics

    Institute of Scientific and Technical Information of China (English)

    SUN Qingchi; LU Cuimin; ZHOU Hua

    2005-01-01

    Quinary system piezoelectric ceramics PSN-PZN-PMS-PZT were prepared by using a two-step method. The effects of CeO2 doping on piezoelectric and dielectric properties of the system were investigated at morphotropic phase boundary (MPB). The results reveal that the relative dielectric constant εT33 / ε0, the Curie temperature Tc, the piezoelectric constant d33, the mechanical quality factor Qm, and the electromechanical coupling coefficient Kp are changed with the increase of CeO2 content. On the other hand, the effects of CeO2 doping on the dielectric properties of PSN-PZN-PMS-PZT piezoelectric ceramics at high electric field are consistent with the change at weak electric field. The values of dielectric constant and dielectric loss are enhanced with the increasing of electric field.

  13. Structural and Electrical Properties of PZT/PVDF Piezoelectric Nanocomposites Prepared by Cold-Press and Hot-Press Routes

    Institute of Scientific and Technical Information of China (English)

    ZHANG De-Qing; WANG Da-Wei; YUAN Jie; ZHAO Quan-Liang; WANG Zhi-Ying; CAO Mao-Sheng

    2008-01-01

    @@ The 0-3 PZT/PVDF piezoelectric composites are prepared separately by hot-press and cold-press processes. The effects of the PZT content and the shaping-process on the composites are studied. The experimental results indicate that composites with 70% PZT nanopowders prepared by the hot-press method exhibit excellent piezo-electric and dielectric properties. The maxima of daa and e of the composites prepared by hot-press method are about 30% and 65% higher than those prepared by the cold-press method, respectively. This is mainly attributed to the favourable coupling of the two materials in the process of the hot press and the formation of the β-type PVDF, which possesses better electric properties.

  14. A new traveling wave ultrasonic motor using thick ring stator with nested PZT excitation.

    Science.gov (United States)

    Chen, Weishan; Shi, Shengjun; Liu, Yingxiang; Li, Pei

    2010-05-01

    To avoid the disadvantages of conventional traveling wave ultrasonic motors--lower efficiency PZT working mode of d(31), fragility of the PZT element under strong excitation, fatigue of the adhesive layer under harsh environmental conditions, and low volume of the PZT material in the stator--a new type of traveling wave ultrasonic motor is presented in this paper. Here we implement the stator by nesting 64 PZT stacks in 64 slots specifically cut in a thick metal ring and 64 block springs nested within another 64 slots to produce preloading on the PZT stacks. In this new design, the d33 mode of the PZT is used to excite the flexural vibrations of the stator, and fragility of the PZT ceramics and fatigue of the adhesive layer are no longer an issue. The working principle, FEM simulation, fabrication, and performance measurements of a prototype motor were demonstrated to validate the proposed ideas. Typical output of the prototype motor is no-load speed of 15 rpm and maximum torque of 7.96 N x m. Further improvement will potentially enhance its features by increasing the accuracy in fabrication and adopting appropriate frictional material into the interface between the stator and the rotor.

  15. Shoe-mounted vibration energy harvester of PZT piezoelectric thin films on metal foils

    Science.gov (United States)

    Nishi, T.; Ito, T.; Hida, H.; Kanno, I.

    2016-11-01

    This paper describes shoe-mounted piezoelectric vibration energy harvesters (PVEHs). The PVEHs were fabricated from Pb(ZrTi)O3 (PZT) thin films which were directly deposited onto Pt/Ti-coated stainless steel foil by rf-magnetron sputtering. We experimentally and theoretically evaluated impulse responses of the PVEHs by applying a simple impulse input on the energy harvesters, typical damped free vibration behaviour was clearly observed, and the output signal was in good agreement with the theoretical value. We measured the output power by applying the impulse input with an optimal load resistance of 33.9 kΩ. The maximum output power was approximately 20 μW, which correspond with the calculated value based on theoretical equation. From these results, the theoretical equation we derived might be helpful for design purposes of the shoe-mounted PVEHs.

  16. Design Considerations for Aural Vital Signs Using PZT Piezoelectric Ceramics Sensor Based on the Computerization Method

    Directory of Open Access Journals (Sweden)

    Jerapong Tantrakoon

    2007-11-01

    Full Text Available The purpose was to illustrate how system developed for measurement of the aural vital signs such as patient’s heart and lung sounds in the hospital. For heart sounds measurement must operate the frequency response between 20 – 800 Hz, and lung sounds measurement must operate the frequency response between 160 – 4,000 Hz. The method was designed PZT piezoelectric ceramics for both frequency response in the same PZT sensor. It converts a signal from aural vital sign form to voltage signal. The signal is suitably amplified and re-filtered in band pass frequency band. It is converted to digital signal by an analog to digital conversion circuitry developed for the purpose. The results were that all signals can fed to personal computer through the sound card port. With the supporting software for drawing of graphic on the screen, the signal for a specific duration is accessed and stored in the computer’s memory in term of each patient’s data. In conclusion, the data of each patient call dot pcg (.pcg for drawing graph and dot wave (.wave for sound listening or automatic sending via electronic mail to the physician for later analysis of interpreting the sounds on the basis of their time domain and frequency domain representation to diagnose heart disorders.

  17. Colloidal processing of PMN-PT thick films for piezoelectric sensor applications

    Science.gov (United States)

    Luo, Hongyu

    65%Pb(Mg1/3Nb2/3)O3-35%PbTiO3 (65PMN-35PT, or PMN-PT) is a highly piezoelectric ceramic with superior piezoelectric coefficients over the more popular Pb(Zr0.5Ti0.5)O 3 (PZT). Because of its complex chemistry and high volatility of lead above 1000°C, the perovskite phase of PMN-PT is hard to process and has prevented PMN-PT from various piezoelectric applications, especially in the new area of piezoelectric micro-electro-mechanical systems (PMEMS) involving thick or thin piezoelectric films. In this thesis, a novel precursor suspension method is introduced that substantially lowers the sintering temperature of PMN-PT to 850°C from a PMN precursor powder made by coating Mg(OH) 2 on Nb2O5 particles. The precursor suspension method entails suspending PMN powders in PT precursor and uses the reaction sintering capability of PMN with nano-sized PT in the temperature range of 800°C˜1000°C. Moreover, free-standing PMN-PT thick films were obtained by tape casting the PMN-PT powder. This new geometry of PMN-PT shows giant electric-field enhanced piezoelectric responses comparable with those of single crystals. As an example of application, the PMN-PT thick film is bonded to a thinner layer of copper by electroplating and made into piezoelectric cantilever sensors. In conclusion, the colloidal suspension processing method produces free-standing PMN-PT thick films with ultrahigh piezoelectric properties.

  18. Optimization of electrode geometry and piezoelectric layer thickness of a deformable mirror

    Directory of Open Access Journals (Sweden)

    Nováková Kateřina

    2013-05-01

    Full Text Available Deformable mirrors are the most commonly used wavefront correctors in adaptive optics systems. Nowadays, many applications of adaptive optics to astronomical telescopes, high power laser systems, and similar fast response optical devices require large diameter deformable mirrors with a fast response time and high actuator stroke. In order to satisfy such requirements, deformable mirrors based on piezoelectric layer composite structures have become a subject of intense scientific research during last two decades. In this paper, we present an optimization of several geometric parameters of a deformable mirror that consists of a nickel reflective layer deposited on top of a thin lead zirconate titanate (PZT piezoelectric disk. Honeycomb structure of gold electrodes is deposited on the bottom of the PZT layer. The analysis of the optimal thickness ratio between the PZT and nickel layers is performed to get the maximum actuator stroke using the finite element method. The effect of inter-electrode distance on the actuator stroke and influence function is investigated. Applicability and manufacturing issues are discussed.

  19. Energy harvesting using piezoelectric thick films fabricated by a sol-gel process

    Energy Technology Data Exchange (ETDEWEB)

    Shih, J.L. [McGill Univ., Montreal, PQ (Canada). Dept. of Electrical and Computer Engineering; Kobayashi, M.; Moisan, J.F.; Jen, C.K. [National Research Council of Canada, Boucherville, PQ (Canada). Industrial Materials Inst.

    2008-07-01

    Energy harvesting has been touted as a promising technology to power wireless devices. One of the common energies to be harvested is induced by mechanical vibrations. Piezoelectric materials are often used to get such energy. This study focused on a vibration-based energy harvesting device. Very flexible vibrators using lead-zirconate-titanate (PZT) ceramics were needed. Therefore, a sol-gel spray technology was used to fabricate PZT thick film directly onto metal membranes to serve as mechanical vibrators. The sol-gel process is an economical approach with excellent mass production appeal for both unimorph and bimorph sensors. For this study, the density of the PZT film was less than 85 per cent of the bulk PZT. Using a 20 mm diameter unimorph, the voltage generated from a 5 mm deflection displacement was 13.6 volts peak-to-peak at 10 Hz. With a load resistance of 150 K ohms, the measured average power generated by this sensor was estimated to be 41 {mu}W. A vibration test that lasted for 60 days with a frequency of 10 Hz and at a displacement of approximately 1 mm showed that the sensor is both durable and rugged. 14 refs., 7 figs.

  20. Optimization of a 0.69PZT-0.31PZNN thick film by controlling slurry viscosity and tape-casting blade height

    Science.gov (United States)

    Song, Daniel; Woo, Min Sik; Ahn, Jung Hwan; Sung, Tae Hyun; Kim, Kyoung Bum

    2014-12-01

    We investigated how the viscosities of piezoelectric lead zirconate titanate/lead zirconate nickel niobate (PZT-PZNN) slurry samples affect the laminated-film densities based on various conditions of degassing time for 0, 30, and 60 min. PZT-PZNN slurries with different viscosities were tape casted into green sheets by adjusting the comma blade height to 100, 200, 300, 400, and 500 μm. As a result the slurry viscosity linearly increased with increasing slurry degassing time, and the thickness of the green sheet increased with increasing comma blade height. The density and the dielectric properties of piezoelectric ceramic films with the same thicknesses, but composed of different numbers of layers, were compared. The laminated-film density and the dielectric property d33 × g33 increased with decreasing number of laminated layers. However, when the viscosity of the slurry was too high (degassing time > 60 min) and the comma blade height was too high (comma blade height > 300 μm), the tape-casted green sheet was too thick to have enough time to dry. By controlling the slurry viscosity by adjusting the degassing time and the comma blade height, we were able to optimize the thickness of the green sheet in a tape-casting. The optimal green sheet thickness was < 70 μm, and the number of sheets laminated should be minimized to increase the film's density and dielectric constant.

  1. Optimization of a 0.69PZT-0.31PZNN thick film by controlling slurry viscosity and tape-casting blade height

    Energy Technology Data Exchange (ETDEWEB)

    Song, Daniel; Woo, Minsik; Ahn, Junghwan; Sung, Taehyun [Hanyang University, Seoul (Korea, Republic of); Kim, Kyoungbum [Korea University, Seoul (Korea, Republic of)

    2014-12-15

    We investigated how the viscosities of piezoelectric lead zirconate titanate/lead zirconate nickel niobate (PZT-PZNN) slurry samples affect the laminated-film densities based on various conditions of degassing time for 0, 30, and 60 min. PZT-PZNN slurries with different viscosities were tape casted into green sheets by adjusting the comma blade height to 100, 200, 300, 400, and 500 μm. As a result the slurry viscosity linearly increased with increasing slurry degassing time, and the thickness of the green sheet increased with increasing comma blade height. The density and the dielectric properties of piezoelectric ceramic films with the same thicknesses, but composed of different numbers of layers, were compared. The laminated-film density and the dielectric property d{sub 33} x g{sub 33} increased with decreasing number of laminated layers. However, when the viscosity of the slurry was too high (degassing time > 60 min) and the comma blade height was too high (comma blade height > 300 μm), the tape-casted green sheet was too thick to have enough time to dry. By controlling the slurry viscosity by adjusting the degassing time and the comma blade height, we were able to optimize the thickness of the green sheet in a tape-casting. The optimal green sheet thickness was < 70 μm, and the number of sheets laminated should be minimized to increase the film's density and dielectric constant.

  2. Effect of temperature and loading on output voltage of lead zirconate titanate (PZT-5A) piezoelectric energy harvester

    Science.gov (United States)

    Butt, Z.; Pasha, R. A.

    2016-08-01

    Energy harvesting is the process of acquiring energy from the external sources and then further used to drive any system. Piezoelectric material was operated at various temperature but the characterization of the material mostly performed at room temperature. The depolarization in piezoelectric material occurs when the material is heated to its curie temperature and when mechanical stresses are high to disturb the properties of the material. The aim of this paper is to study the performance of lead zirconate titanate (PZT-5A) piezoelectric material under various temperatures and loading conditions. The output voltage of piezoelectric material decreases with increase of temperature. It was found that output voltage from the harvester increases when loading increases while its temperature decreases.

  3. Performance of PIN-PMN-PT Single Crystal Piezoelectric versus PZT8 Piezoceramic Materials in Ultrasonic Transducers

    Science.gov (United States)

    DeAngelis, D. A.; Schulze, G. W.

    The recent advancements in the manufacturing of single crystal PIN-PMN-PT piezoelectric materials now make them a cost-competitive alternative to PZT4 and PZT8 (Navy Types I and III) piezoceramic materials, which have been the workhorse of power ultrasonic applications (e.g., welding, cutting, sonar, etc.) for over 50 years. Although there are great benefits to the use of single crystal materials with respect to high output, as well as added actuating and sensing abilities, many transducer designers are still reluctant to explore these materials due to inadequate design guidelines for substituting the familiar PZT materials; for example, what are the implications of the higher capacitance, sensitivity to chipping/cracks, aging effects, frequency shifts, or how much preload can be used are all common questions. This research is a case study on the performance of identical ultrasonic transducer bodies, used for semiconductor wire bonding, assembled with either PZT8 or PIN-PMN-PT piezo material. The main purpose of the study is to establish rule-of-thumb design guidelines for direct substitution of single crystal materials in existing PZT8 transducer designs, along with a side-by-side performance comparison to highlight benefits. Several metrics are investigated such as impedance, frequency, displacement gain, quality factor and electromechanical coupling factor.

  4. Synthesis of piezoelectric nanocrystalline PZT powder by stearic acid gel method

    Institute of Scientific and Technical Information of China (English)

    HAO Junjie; WANG Xiaohui; GUI Zhilun; LI Longtu

    2005-01-01

    PZT nanocrystalline powder was prepared by a stearic acid gel method. The crystallization process from the precursor was monitored by infrared spectroscopy, differential thermal analysis, and thermogravimetric analysis. The nano-sized PZT powder was characterized by X-ray diffraction and transmission electron microscopy. It shows that pure single-phase PZT powder could be obtained at 450℃ for 1 h, and the particle size is about 20 nm. With an increase in the calcination temperature, the PZT crystallite size increased.

  5. Study of the microstructure and the hardness of PZT piezoelectric ceramics types I and III used in electro acoustic transducers; Estudo da microestrutura e da microdureza das ceramicas piezoeletricas tipos PZT I e III utilizadas em transdutores eletroacusticos

    Energy Technology Data Exchange (ETDEWEB)

    Cabral, Ricardo de Freitas; Itaboray, Lucas Mendes; Santos, Anna Paula de Oliveira [Centro Universitario de Volta Redonda (UNIFOA), Volta Redonda, RJ (Brazil)

    2015-12-15

    The field of electronic processing of the ceramic piezoelectric type imported powdered led to the production of ceramics with 97% of theoretical density, homogeneous microstructure with great potential for applications in piezoelectric devices such as electro acoustic transducers. However, the production of electronic ceramics National piezoelectric type is not yet able to have as raw material zirconate titanate Lead (PZT) 100% made in Brazil. Thus, this is used for supply of domestic production, the zirconium oxide. In this work, both post PZT types I and III, imported, were uniaxially pressed at 70 MPa and sintered at 1200 and 1250 deg C for 3 hours. Hardness measurements were performed by micro indentation, X-ray diffraction analysis and Scanning Electron Microscopy. The hardness of PZT I was 393 HV. (author)

  6. The effect of calcining temperature on the properties of 0-3 piezoelectric composites of PZT and a liquid crystalline thermosetting polymer

    NARCIS (Netherlands)

    Ende, D.A. van den; Groen, W.A.; Zwaag, S. van der

    2011-01-01

    We report on the optimisation of a recently developed high performance 0-3 piezoelectric composite comprising of the piezoelectric Lead Zirconate Titanate (PZT) powder and a liquid crystalline thermosetting matrix polymer (LCT). The matrix polymer is a liquid crystalline polymer comprising of an HBA

  7. Screen-printed piezoelectric shoe-insole energy harvester using an improved flexible PZT-polymer composites

    Science.gov (United States)

    Almusallam, A.; Torah, R. N.; Zhu, D.; Tudor, M. J.; Beeby, S. P.

    2013-12-01

    This paper reports improved screen-printed piezoelectric composites that can be printed on fabrics or flexible substrates. The materials are flexible and are processed at lower temperature (130°C). One main PZT particle size (2μm) was mixed separately with smaller piezoelectric particles (0.1, 0.3 and 0.8μm) with different weight ratios to investigate the piezoelectric property d33. The blended PZT powder was then mixed with 40% polymer binder and printed on Alumina substrates. The applied poling field, temperature and time were 8MV/m, 160°C and 10min, respectively. The optimum material gives a d33 of 36pC/N with particle sizes of 2μm and 0.8μm and mixed percentages of 82% and 18%, respectively. A screen-printed piezoelectric shoe-insoles (PSI) has been developed as a self-powered force mapping sensor. The PSI was simulated, fabricated and tested. ANSYS results show that one element of PSI sole can produce an open- circuit voltage of 3V when a human of average weight of 70kg makes a gait strike. Experimental results show that one element produced 2V which is less than the simulated results because of the reduction of poling field for the practical device.

  8. Generation of electrical energy using lead zirconate titanate (PZT-5A) piezoelectric material: Analytical, numerical and experimental verifications

    Energy Technology Data Exchange (ETDEWEB)

    Butt, Zubair; Ahmad, Nasir [Dept. of Mechanical, Mechatronics and Manufacturing Engineering, UET Lahore, Faisalabad Campus, Lahore (Pakistan); Pasha, Riffat Asim; Qayyum, Faisal; Anjum, Zeeshan [Dept. of Mechanical Engineering, University of Engineering and Technology, Taxila (Pakistan); Elahi, Hassan [Northwestern Polytechnical University, Xian (China)

    2016-08-15

    Energy harvesting is the process of attaining energy from the external sources and transforming it into usable electrical energy. An analytical model of piezoelectric energy harvester has been developed to determine the output voltage across an electrical circuit when it is forced to undergo a base excitation. This model gives an easy approach to design and investigate the behavior of piezoelectric material. Numerical simulations have been carried out to determine the effect of frequency and loading on a Lead zirconate titanate (PZT-5A) piezoelectric material. It has been observed that the output voltage from the harvester increases when loading increases whereas its resonance frequency decreases. The analytical results were found to be in good agreement with the experimental and numerical simulation results.

  9. Effects of Sr2+substitution on the structural, dielectric, and piezoelectric properties of PZT-PMN ceramics

    Institute of Scientific and Technical Information of China (English)

    Arvind Kumar; S.K. Mishra

    2014-01-01

    This study described the structural, dielectric, and piezoelectric behavior of Pb1-xSrx[(Zr0.52Ti0.48)0.95(Mn1/3Nb2/3)0.05]O3 ceramics (PSZT-PMN, x=0, 0.025, 0.050, and 0.075), prepared by a semi-wet route. X-ray diffraction, dielectric, and piezoelectric investigations were carried out to analyze the crystal structure. The relative dielectric constant and dielectric loss were both calculated as the functions of temperature. The room-temperature dielectric constant reaches a maximum for a Sr2+-modified PZT-PMN ceramic with an x value of 0.050, which corresponds to the morphotropic phase boundary (MPB). Raman spectroscopy studies also confirm the existence of this MPB for x=0.050. The piezoelectric strain coefficients (d33) value shows a maximum response for this composition. In addition, the phase transition temperature decreases significantly when the Sr2+concentration increases in the PZT-PMN ceramics.

  10. Analytical investigation on axisymmetric free vibrations of moderately thick circular functionally graded plate integrated with piezoelectric layers

    Energy Technology Data Exchange (ETDEWEB)

    Rastgoo, A. [University of Tehran, Tehran (Iran, Islamic Republic of); Ebrahimi, F. [lmam Khomeini International University, Qazvin (Iran, Islamic Republic of); Kargarnovin, M. H. [Sharif University of Technology, Tehran (Iran, Islamic Republic of)

    2008-06-15

    In this paper, a free vibration analysis of moderately thick circular functionally graded (FG) plate integrated with two thin piezoelectric (PZT4) layers is presented based on Mindlin plate theory. The material properties of the FG core plate are assumed to be graded in the thickness direction, while the distribution of electric potential field along the thickness of piezoelectric layers is simulated by sinusoidal function. The differential equations of motion are solved analytically for two boundary conditions of the plate: clamped edge and simply supported edge. The analytical solution is validated by comparing the obtained resonant frequencies with those of an isotropic host plate. The emphasis is placed on investigating the effect of varying the gradient index of FG plate on the free vibration characteristics of the structure. Good agreement between the results of this paper and those of the finite element analyses validated the presented approach

  11. Shear piezoelectric coefficients of PZT, LiNbO3 and PMN-PT at cryogenic temperatures

    Science.gov (United States)

    Bukhari, Syed; Islam, Md; Haziot, Ariel; Beamish, John

    2014-12-01

    Piezoelectric transducers are used to detect stress and to generate nanometer scale displacements but their piezoelectric coefficients decrease with temperature, limiting their performance in cryogenic applications. We have developed a capacitive technique and directly measured the temperature dependence of the shear coefficient d15 for ceramic lead zirconium titanate (PZT), 41° X-cut lithium niobate (LiNbO3) and single crystal lead magnesium niobium-lead titanate (PMN-PT). In PZT, d15 decreases nearly linearly with temperature, dropping by factor of about 4 by 1.3 K. LiNbO3 has the smallest room temperature d15, but its value decreased by only 6% at the lowest temperatures. PMN-PT had the largest value of d15 at room temperature (2.9 × 10-9 m/V, about 45 times larger than for LiNbO3) but it decreased rapidly below 75 K; at 1.3 K, d15 was only about 8% of its room temperature value.

  12. Properties of quasi 1-3 piezoelectric PZT-epoxy composites obtained by dielectrophoresis

    NARCIS (Netherlands)

    Ende, D.A. van den; Bory, B.F.; Groen, W.A.; Zwaag, S. van der

    2010-01-01

    The dielectric and piezoelectric properties of piezoelectric particleepoxy polymer composites structured into 1-3 composites via dielectrophoresis during curing are reported. The dielectrophoretic alignment induces a textured microstructure in the composite, with particles forming chains in the dire

  13. Investigations of thickness-shear mode elastic constant and damping of shunted piezoelectric materials with a coupling resonator

    Science.gov (United States)

    Hu, Ji-Ying; Li, Zhao-Hui; Sun, Yang; Li, Qi-Hu

    2016-12-01

    Shear-mode piezoelectric materials have been widely used to shunt the damping of vibrations where utilizing surface or interface shear stresses. The thick-shear mode (TSM) elastic constant and the mechanical loss factor can change correspondingly when piezoelectric materials are shunted to different electrical circuits. This phenomenon makes it possible to control the performance of a shear-mode piezoelectric damping system through designing the shunt circuit. However, due to the difficulties in directly measuring the TSM elastic constant and the mechanical loss factor of piezoelectric materials, the relationships between those parameters and the shunt circuits have rarely been investigated. In this paper, a coupling TSM electro-mechanical resonant system is proposed to indirectly measure the variations of the TSM elastic constant and the mechanical loss factor of piezoelectric materials. The main idea is to transform the variations of the TSM elastic constant and the mechanical loss factor into the changes of the easily observed resonant frequency and electrical quality factor of the coupling electro-mechanical resonator. Based on this model, the formular relationships are set up theoretically with Mason equivalent circuit method and they are validated with finite element (FE) analyses. Finally, a prototype of the coupling electro-mechanical resonator is fabricated with two shear-mode PZT5A plates to investigate the TSM elastic constants and the mechanical loss factors of different circuit-shunted cases of the piezoelectric plate. Both the resonant frequency shifts and the bandwidth changes observed in experiments are in good consistence with the theoretical and FE analyses under the same shunt conditions. The proposed coupling resonator and the obtained relationships are validated with but not limited to PZT5A. Project supported by the National Defense Foundation of China (Grant No. 9149A12050414JW02180).

  14. Enhancement of ferroelectric and piezoelectric properties in PZT thin films with heterolayered structure

    NARCIS (Netherlands)

    Nguyen, D.M.; Nguyen, Chi T.Q.; Trinh, Thong Q.; Nguyen, Tai; Pham, Thao N.; Rijnders, A.J.H.M.; Vu, Hung N.

    2013-01-01

    This paper reports the latest experimental results of multilayered, heterolayered, and alternating heterolayered PZT thin films obtained by spin coating on Pt/Ti/SiO2/Si wafers using Zr-rich (P60) and Ti-rich (P40) solutions which were prepared by sol–gel route process. The ferroelectric and piezoel

  15. Homogeneity Analysis of a MEMS-based PZT Thick Film Vibration Energy Harvester Manufacturing Process

    DEFF Research Database (Denmark)

    Lei, Anders; Xu, Ruichao; Borregaard, Louise M.

    2012-01-01

    This paper presents a homogeneity analysis of a high yield wafer scale fabrication of MEMS-based unimorph silicon/PZT thick film vibration energy harvesters aimed towards vibration sources with peak vibrations in the range of around 300Hz. A wafer with a yield of 91% (41/45 devices) has been...... indicating that the main variation in open circuit voltage performance is caused by varying quality factor. The average resonant frequency was measured to 333Hz with a standard variation of 9.8Hz and a harvesting bandwidth of 5-10Hz. A maximum power output of 39.3μW was achieved at 1g for the best performing...

  16. Dependence of piezoelectric properties on layer thickness for multilayer actuators

    NARCIS (Netherlands)

    Groen, W.A.; Prijs, K.; Saeed, S.

    2010-01-01

    In general, it has been reported that the piezoelectric properties in multilayer actuators decrease for layer thicknesses below 20 microns. This has been investigated for PXE55 which is a material based on PLZT-Pb(Mg 1/2W1/2)O3 and PG01 which is a low sintering version of this material. Results show

  17. AN EXACT ANALYSIS OF FORCED THICKNESS-TWIST VIBRATIONS OF MULTI-LAYERED PIEZOELECTRIC PLATES

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    This paper deals with the thickness-twist vibration of a multi-layered rectangular piezoelectric plate of crystals of 6 mm symmetry or polarized ceramics. An exact solution is obtained from the three-dimensional equations of linear piezoelectricity. The solution is useful to the understanding and design of composite piezoelectric devices. A piezoelectric resonator, a piezoelectric transformer, and a piezoelectric generator are analyzed as examples.

  18. Comparison of the thermal degradation of heavily Nb-doped and normal PZT thin films.

    Science.gov (United States)

    Yang, Jeong-Suong; Kang, Yunsung; Kang, Inyoung; Lim, Seungmo; Shin, Seung-Joo; Lee, Jungwon; Hur, Kangheon

    2017-01-04

    The degradation of Niobium-doped lead zirconate titanate (PZT) and two types of PZT thin films were investigated. Undoped PZT, 2-step PZT and heavily Nb-doped PZT (PNZT) around the morphotropic phase boundary (MPB) were in-situ deposited under optimum condition by RF-magnetron sputtering. All 2 μm thick films had dense perovskite columnar grain structure and self-polarized (100) dominant orientation. PZT thin films were deposited on Pt/TiOx bottom electrode on Si wafer, and Nb doped PZT thin film was on Ir/TiW electrode with help of orientation control. Sputtered PZT films formed on MEMS gyroscope, and the degradation rates were compared at different temperatures. Nb-doped PZT showed the best resistance to the thermal degradation, followed by 2-step PZT. To clarify the effect of oxygen vacancies for the degradation of the film at high temperature, photo-luminescence (PL) measurement was conducted. It confirmed that oxygen vacancy rate was the lowest in heavily Nb-doped PZT. Nb-doping PZT thin films suppressed the oxygen deficit and made high imprint with self-polarization. This defect distribution and high internal field allowed Nb-doped PZT thin film to make the piezoelectric sensors more stable and reliable at high temperature, such as reflow process of micro-electromechanical system (MEMS) packaging.

  19. Homogeneity analysis of high yield manufacturing process of mems-based pzt thick film vibrational energy harvesters

    DEFF Research Database (Denmark)

    Lei, Anders; Xu, Ruichao; Pedersen, C.M.

    2011-01-01

    This work presents a high yield wafer scale fabrication of MEMS-based unimorph silicon/PZT thick film vibrational energy harvesters aimed towards vibration sources with peak frequencies in the range of a few hundred Hz. By combining KOH etching with mechanical front side protection, SOI wafer...... to accurately define the thickness of the silicon part of the harvester and a silicon compatible PZT thick film screen-printing technique, we are able to fabricate energy harvesters on wafer scale with a yield higher than 90%. The characterization of the fabricated harvesters is focused towards the full wafer....../mass-production aspect; hence the analysis of uniformity in harvested power and resonant frequency....

  20. Stress relaxation and estimation of activation volume in a commercial hard PZT piezoelectric ceramic

    Indian Academy of Sciences (India)

    B L Cheng; M J Reece

    2001-04-01

    The stress relaxation of ferroelectric/piezoelectric material was studied using compression testing. The deformation was produced by the switching of ferroelectric domains. The internal stresses were estimated by decremental stress relaxation during unloading. The results were interpreted in terms of reversible and irreversible switching of the domains.

  1. Direct strain energy harvesting in automobile tires using piezoelectric PZT-polymer composites

    NARCIS (Netherlands)

    Ende, D.A. van den; Wiel, H.J. van de; Groen, W.A.; Zwaag, S. van der

    2012-01-01

    Direct piezoelectric strain energy harvesting can be used to power wireless autonomous sensors in environments where low frequency, high strains are present, such as in automobile tires during operation. However, these high strains place stringent demands on the materials with respect to mechanical

  2. Features ofd15 mode PZT-51 ceramic cantilever piezoelectric energy harvester with parallel connection%并联结构d15模式PZT-51悬臂梁的俘能性能

    Institute of Scientific and Technical Information of China (English)

    张智雄; 郑学军; 张勇; 梅靖羚; 费明祥; 祝元坤

    2015-01-01

    Utilizing the high shear piezoelectric coefficient of PZT-51 ceramic, the parallel connection device ofd15 mode PZT-51 cantilever beam was designed and fabricated. The dependences of output peak-to-peak voltage and output power on frequency were studied at various load resistances. The dependence of peak-to-peak voltage on excitation voltage and the resonance transient output voltage were measured at various load resistances. Maximum output peak-to-peak voltage of 1.96 V and maximum output power of 19.21μW for PEH with load resistance of 100kΩare obtained at frequency of 96 Hz. With increasing vibration excitation voltage, the output peak-to-peak voltage of PEH increases. The proposed structure will provide useful guidelines for the design ofd15 mode piezoelectric energy harvesters.%利用高剪切压电系数,设计并制作并联结构d15模式PZT-51悬臂梁装置,测量其在不同负载电阻下输出峰-峰值电压和输出功率随频率变化的关系以及不同负载电阻下共振瞬时输出电压和振动激励电压与输出峰-峰值电压关系.当频率为96 Hz、负载电阻为100 kΩ时,该PZT-51悬臂梁装置的输出峰-峰值电压最大值为1.96 V,输出功率达到最大为19.21 μW.随着振动激励电压的增大,并联结构d15模式PZT-51悬臂梁装置的输出峰-峰值电压随之增大,并联结构d15模式PZT-51悬臂梁俘能特性的研究可为设计d15模式压电俘能器提供指导.

  3. Lamb wave dispersion in a PZT/metal/PZT sandwich plate with imperfect interface

    Science.gov (United States)

    Kurt, Ilkay; Akbarov, Surkay D.; Sezer, Semih

    2016-07-01

    The Lamb wave dispersion in a PZT/Metal/PZT sandwich plate is investigated by employing the exact linear equations of electro-elastic waves in piezoelectric materials within the scope of the plane-strain state. It is assumed that at the interfaces between the piezoelectric face layers and metal core layer, shear-spring and normal-spring type imperfect conditions are satisfied. The degree of this imperfectness is estimated through the corresponding shear-spring and normal-spring type parameters which appear in the contact condition characterizing the transverse and normal displacements' discontinuity. The corresponding dispersion equation is derived, and as a result of the numerical solution to this equation, the dispersion curves are constructed for the first and second lowest modes in the cases where the material of the face layers is PZT and the material of the middle layer is Steel (St). Consequently, for the PZT/St/PZT sandwich plate, the study of the influence of the problem parameters such as the piezoelectric and dielectric constants, layer thickness ratios, non-dimensional shear-spring, and normal-spring type parameters, is carried out. In particular, it is established that the imperfectness of the contact between the layers of the plate causes a decrease in the values of the wave propagation velocity.

  4. Ferroelectricity, Piezoelectricity, and Dielectricity of 0.06PMnN-0.94PZT(45/55 Thin Film on Silicon Substrate

    Directory of Open Access Journals (Sweden)

    Tao Zhang

    2015-01-01

    Full Text Available The high piezoelectricity and high quality factor ferroelectric thin films are important for electromechanical applications especially the micro electromechanical system (MEMS. The ternary compound ferroelectric thin films 0.06Pb(Mn1/3, Nb2/3O3 + 0.94Pb(Zr0.45, Ti0.55O3 (0.06PMnN-0.94PZT(45/55 were deposited on silicon(100 substrates by RF magnetron sputtering method considering that Mn and Nb doping will improve PZT properties in this research. For comparison, nondoped PZT(45/55 films were also deposited. The results show that both of thin films show polycrystal structures with the main (111 and (101 orientations. The transverse piezoelectric coefficients are e31,eff=−4.03 C/m2 and e31,eff=-3.5 C/m2, respectively. These thin films exhibit classical ferroelectricity, in which the coercive electric field intensities are 2Ec=147.31 kV/cm and 2Ec=135.44 kV/cm, and the saturation polarization Ps=30.86 μC/cm2 and Ps=17.74 μC/cm2, and the remnant polarization Pr=20.44 μC/cm2 and Pr=9.87 μC/cm2, respectively. Moreover, the dielectric constants and loss are εr=681 and D=5% and εr=537 and D=4.3%, respectively. In conclusion, 0.06PMnN-0.94PZT(45/55 thin films act better than nondoped films, even though their dielectric constants are higher. Their excellent ferroelectricity, piezoelectricity, and high power and energy storage property, especially the easy fabrication, integration realizable, and potentially high quality factor, make this kind of thin films available for the realistic applications.

  5. A piezoelectric micro generator worked at low frequency and high acceleration based on PZT and phosphor bronze bonding

    Science.gov (United States)

    Tang, Gang; Yang, Bin; Hou, Cheng; Li, Guimiao; Liu, Jingquan; Chen, Xiang; Yang, Chunsheng

    2016-01-01

    Recently, piezoelectric energy harvesters (PEHs) have been paid a lot of attention by many researchers to convert mechanical energy into electrical and low level vibration. Currently, most of PEHs worked under high frequency and low level vibration. In this paper, we propose a micro cantilever generator based on the bonding of bulk PZT wafer and phosphor bronze, which is fabricated by MEMS technology, such as mechanical chemical thinning and etching. The experimental results show that the open-circuit output voltage, output power and power density of this fabricated prototype are 35 V, 321 μW and 8664 μW cm−3 at the resonant frequency of 100.8 Hz, respectively, when it matches an optimal loading resistance of 140 kΩ under the excitation of 3.0 g acceleration. The fabricated micro generator can obtain the open-circuit stable output voltage of 61.2 V when the vibration acceleration arrives at 7.0 g. Meanwhile, when this device is pasted on the vibrating vacuum pump, the output voltage is about 11 V. It demonstrates that this novel proposed device can scavenge high vibration level energy at low frequency for powering the inertial sensors in internet of things application. PMID:27929139

  6. A piezoelectric micro generator worked at low frequency and high acceleration based on PZT and phosphor bronze bonding

    Science.gov (United States)

    Tang, Gang; Yang, Bin; Hou, Cheng; Li, Guimiao; Liu, Jingquan; Chen, Xiang; Yang, Chunsheng

    2016-12-01

    Recently, piezoelectric energy harvesters (PEHs) have been paid a lot of attention by many researchers to convert mechanical energy into electrical and low level vibration. Currently, most of PEHs worked under high frequency and low level vibration. In this paper, we propose a micro cantilever generator based on the bonding of bulk PZT wafer and phosphor bronze, which is fabricated by MEMS technology, such as mechanical chemical thinning and etching. The experimental results show that the open-circuit output voltage, output power and power density of this fabricated prototype are 35 V, 321 μW and 8664 μW cm-3 at the resonant frequency of 100.8 Hz, respectively, when it matches an optimal loading resistance of 140 kΩ under the excitation of 3.0 g acceleration. The fabricated micro generator can obtain the open-circuit stable output voltage of 61.2 V when the vibration acceleration arrives at 7.0 g. Meanwhile, when this device is pasted on the vibrating vacuum pump, the output voltage is about 11 V. It demonstrates that this novel proposed device can scavenge high vibration level energy at low frequency for powering the inertial sensors in internet of things application.

  7. Preparation and Characterization of PZT Wafers

    Science.gov (United States)

    Seal, A.; Rao, B. S. S. Chandra; Kamath, S. V.; Sen, A.; Maiti, H. S.

    2008-07-01

    Piezoelectric materials have recently attracted a lot of attention for ultrasonic structural health monitoring (shm) in aerospace, defence and civilian sectors, where they can act as both actuators and sensors. Incidentally, piezoelectric materials in the form of wafers (pwas-piezoelectric wafer active sensor, approx. 5-10 mm square and 0.2-0.3 mm thickness) are inexpensive, non intrusive and non-resonant wide band devices that can be surface-mounted on existing structures, inserted between the layers of lap joints or embedded inside composite materials. The material of choice for piezoelectric wafers is lead zirconate titanate (PZT) of composition close to morphotropic phase boundary [pb(zr0.52 ti0.48)o3]. However, an excess pbo is normally added to pzt as a densification aid and also to make up for the lead loss during high temperature sintering. Hence, it is of paramount importance to know how the shift of the lead content from the morphotropic composition affects the piezoelectric and mechanical properties of the sintered wafers, keeping in view the importance of mechanical properties of wafers in shm. In the present study, we observed that with the increase in the lead content of the sintered wafers, the dielectric and piezoelectric constants decreased. However, the elastic modulus, hardness and fracture toughness of the wafers increased with increasing lead content in the composition. Hence, the lead content in the sintered wafers should be optimized to get acceptable piezoelectric and mechanical

  8. Effect of Sintering Temperature on Structural and PiezoelectricProperties of PNN-PZT Ceramics

    Directory of Open Access Journals (Sweden)

    Sandeep Mahajan

    2007-01-01

    Full Text Available Sintering temperatures affect the structural and piezoelectric properties of PbNi1/3Nb2/3-PbZrO3-PbTiO3 system considerably; therefore the effect has been studied on mechano-chemicallyprocessed powder. This process involves activating mixed oxides of PbO, NiO, Nb2O5, ZrO2 andTiO2, and in the present study, calcination steps at an intermediate temperatures were skippedwhich are usually required in conventional solid state reaction methods and chemical routes.Single-phase formation was confirmed from XRD patterns which shows rhombohedral structureat higher sintering temperature. Investigations of the microstructure indicate almost linear increasein grain size from 0.98 m to 2.56  m when the sintering temperature was varied from 1050 oC to1150 °C. A high value of planar coupling factor (kp = 67 per cent and piezoelectric charge coefficient(d 33 ~ 750 pm/V; (as determined from strain versus electric field curve at low field were obtainedfor the ceramic specimens sintered at 1100 °C. The maximum strain was observed ~ 0.21 per centat 40 kV/cm applied field for the sample sintered at 1100 °C for 4 h.

  9. Estimation of strain from piezoelectric effect and domain switching in morphotropic PZT by combined analysis of macroscopic strain measurements and synchrotron X-ray data

    Energy Technology Data Exchange (ETDEWEB)

    Kungl, Hans [Institute of Ceramics in Mechanical Engineering, University of Karlsruhe, Haid-und-Neu-Str. 7, 76131 Karlsruhe (Germany)]. E-mail: hans.kungl@ikm.uni-karlsruhe.de; Theissmann, Ralf [Materials Science, Darmstadt University of Technology (Germany); Knapp, Michael [Materials Science, Darmstadt University of Technology (Germany); Baehtz, Carsten [Materials Science, Darmstadt University of Technology (Germany); Fuess, Hartmut [Materials Science, Darmstadt University of Technology (Germany); Wagner, Susanne [Institute of Ceramics in Mechanical Engineering, University of Karlsruhe, Haid-und-Neu-Str. 7, 76131 Karlsruhe (Germany); Fett, Theo [Institute of Ceramics in Mechanical Engineering, University of Karlsruhe, Haid-und-Neu-Str. 7, 76131 Karlsruhe (Germany); Hoffmann, Michael J. [Institute of Ceramics in Mechanical Engineering, University of Karlsruhe, Haid-und-Neu-Str. 7, 76131 Karlsruhe (Germany)

    2007-04-15

    Morphotropic PZT ceramics are State of the art materials for ferroelectric actuators. Essential performance parameters for these materials are strain and hysteresis. On a microscopic scale the strain provided by an electric field is due to two different mechanisms. The piezoelectric effect causes an elongation of the unit cells, whereas domain switching changes their crystallographic orientation by aligning the polarization axis towards the field direction. A method is outlined to estimate the contribution of the two mechanisms to total strain by combining macroscopic strain measurements and X-ray diffraction (XRD) data. Results from macroscopic measurements of remanent and unipolar strain with the corresponding data on texture, derived from in situ synchrotron radiation XRD patterns, are analyzed and evaluated by a semi-empirical approach. The method was applied to six morphotropic, LaSr doped PZT materials of different Zr/Ti ratios. Results are discussed with respect to the differences between the materials.

  10. Enhanced ferroeletric and piezoelectric properties of Nd3+ doped PZT nanoceramics

    Science.gov (United States)

    Kour, Paramjit; Pradhan, Sudipta Kishore; Kumar, Pawan; Sinha, Sanjay Kumar; Kar, Manoranjan

    2016-05-01

    The sol gel technique was used to prepare Pb1-xNdx Zr0.52Ti0.48O3 with x = 0.02, 0.04, 0.06 and 0.10 samples. Room temperature Raman spectra of all the sample were recorded in the range of wave number 30-1000 cm-1. It suggests that the increase in contribution of tetragonal crystallographic phase with the increase in Nd concentration in the sample. FTIR study shows the presence of characteristic bending and streching vibrations of perovskite (ABO3) structure. Ferroelectric and piezoelectric properties were enhanced by the Nd substitution at Pb site of PbZr0.52Ti0.48O3.

  11. Ferroelectric and Piezoelectric Properties of 0.72Pb(Zr0.47Ti0.53)O3-0.28Pb[(Zn0.45Ni0.55)1/3Nb2/3]O3 Thick Films for Energy Harvesting Device Application

    Science.gov (United States)

    Jeong, Young Hun; Kim, Kyoung Bum; Lee, Young-Jin; Cho, Jeong-Ho; Kim, Byoung-Ik; Paik, Jong-Hoo; Nahm, Sahn

    2012-09-01

    The Ferroelectric and piezoelectric properties of 0.72Pb(Zr0.47Ti0.53)O3-0.28Pb[(Zn0.45Ni0.55)1/3Nb2/3]O3 (PZT-PZNN) piezoelectric thick films were investigated for application to energy harvesting devices. The PZT-PZNN thick films were fabricated by a conventional tape casting process. The sintered PZT-PZNN thick film was highly dense and flat when the annealed temperature was 1100 °C. It exhibited substantial ferroelectric and piezoelectric properties of Pr = 20.6 µC/cm2, d33 = 370 pC/N, ɛT33/ɛ0 = 1185, and kp = 0.44. Moreover, its d33·g33, which can characterize high energy density material, is as large as approximately 13050×10-15 m2/N. Therefore, the PZT-PZNN thick film can be a potential piezoelectric material for application to energy harvesting devices.

  12. Temperature Dependent Electrical Properties of PZT Wafer

    Science.gov (United States)

    Basu, T.; Sen, S.; Seal, A.; Sen, A.

    2016-04-01

    The electrical and electromechanical properties of lead zirconate titanate (PZT) wafers were investigated and compared with PZT bulk. PZT wafers were prepared by tape casting technique. The transition temperature of both the PZT forms remained the same. The transition from an asymmetric to a symmetric shape was observed for PZT wafers at higher temperature. The piezoelectric coefficient (d 33) values obtained were 560 pc/N and 234 pc/N, and the electromechanical coupling coefficient (k p) values were 0.68 and 0.49 for bulk and wafer, respectively. The reduction in polarization after fatigue was only ~3% in case of PZT bulk and ~7% for PZT wafer.

  13. Design, Modeling and Optimization of a Piezoelectric Pressure Sensor based on a Thin-Film PZT Membrane Containing Nanocrystalline Powders

    National Research Council Canada - National Science Library

    Vahid Mohammadi; Mohammad Hossein Sheikhi

    2009-01-01

    ...^ thin film has been presented and then a pressure sensor based on multilayer thin-film PZT diaphragm contain of Lead Zirconate Titanate nanocrystalline powders was designed, modeled and optimized...

  14. Impedance Based Characterization of a High-Coupled Screen Printed PZT Thick Film Unimorph Energy Harvester

    DEFF Research Database (Denmark)

    Lei, Anders; Xu, R.; Borregaard, L. M.

    2014-01-01

    . This approach leads to simple closed form expressions for peak power frequency, optimal load, and output power without a tedious mathematical derivative approach. The closed form expressions are validated against the exact numerical solution. The electromechanical model contains a set of only five lumped......The single degree of freedom mass-spring-damper system is the most common approach for deriving a full electromechanical model for the piezoelectric vibration energy harvester. In this paper, we revisit this standard electromechanical model by focusing on the impedance of the piezoelectric device...... parameters which, by means of the piezoelectric impedance expression, all can be determined accurately by electrical measurements. It is shown how four of five lumped parameters can be determined from a single impedance measurement scan, considerably reducing the characterization effort. The remaining...

  15. Microwave Hydrothermal Synthesis PZT of Nanometer Crystal

    Institute of Scientific and Technical Information of China (English)

    Hongxing LIU; Hong DENG; Yan LI; Yanrong LI

    2004-01-01

    It was focused on the applications and developments of microwave hydrothermal synthesis piezoelectric ceramic powder. The microwave hydrothermal vessel was designed and manufactured. The microwave hydrothermal synthesis system was established and the PZT piezoelectric ceramic powder was synthesized. XRD and TEM have been used to characterize the products in detail. The diameter of the PZT powder particle is from 40 to 60 nm.

  16. Temperature effects on the mechanical behaviour of PZT 95/5

    Science.gov (United States)

    Khan, A. S.; Balzer, J. E.; Wilgeroth, J. M.; Proud, W. G.

    2014-05-01

    This research is to develop a better understanding of the piezoelectric ceramic lead zirconate titanate (PZT) 95/5 with varying temperatures, porosities and strain rates. Here, unpoled PZT samples of two different porosities were subjected to a range of compression rates, using quasi-static loading equipment, drop-weight towers and Split Hopkinson Pressure Bars (SHPBs). Varying temperatures were achieved using purpose-made environmental chambers. The resulting stress-strain relationships are compared. The samples were square tiles, 7.5 × 7.5 mm and 3 mm thickness. The density of the standard PZT used here was 7.75 g cm-3 (henceforth described as PZT), whilst the density of the higher porosity PZT was 7.38 g cm-3 (henceforth described as PPZT). This research is part of a wider study.

  17. A variational energy approach for electromechanical analysis of thick piezoelectric beam

    Institute of Scientific and Technical Information of China (English)

    LAU C.W.H.; LIM C.W; LEUNG A.Y.T.

    2005-01-01

    A new two dimensional coupled electromechanical model for athick, laminated beam with piezoelectric and isotropic lamina subjected to static external electric loading is developed. The model combined the first order shear deformation theory for the relatively thick elastic core and linear piezoelectric theory for the piezoelectric lamina. The actuation response is induced through the application of extemal electric voltage. Rayleigh-Ritz method is adopted to model the displacement and potential fields of the beam and governing equations were finally derived from the variational energy principle. The model allows the piezoelectric lamina to be formulated via a two-dimensional model because of the strong electro-mechanical coupling and the presence of a two-dimensional electric field. Numerical examples of piezoelectric laminated beam are presented. It is shown in this paper that a one-dimensional model for the piezoelectric beam-like layer is inadequate.

  18. High-performance piezoelectric thick film based energy harvesting micro-generators for MEMS

    DEFF Research Database (Denmark)

    Zawada, Tomasz; Hansen, Karsten; Lou-Moeller, Rasmus

    2010-01-01

    Energy harvesting, known also as energy scavenging, covers a great body of technologies and devices that transform low grade energy sources such as solar energy, environmental vibrations, thermal energy, human motion into usable electrical energy. In this paper vibrations are used as energy source...... and are transformed by the energy harvesting micro-generator into usable electrical signal. The micro-generator comprises a silicon cantilever with integrated InSensor® TF2100 PZT thick film deposited using screen-printing. The output power versus frequency and electrical load has been investigated. Furthermore......, devices based on modified, pressure treated thick film materials have been tested and compared with the commercial InSensor® TF2100 PZT thick films. It has been found that the structures based on the pressure treated materials exhibit superior properties in terms of energy output....

  19. ELECTRICALLY FORCED VIBRATION OF A THICKNESS-TWIST MODE PIEZOELECTRIC RESONATOR WITH NON-UNIFORM ELECTRODES

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    We study the effect of electrodes with varying thickness on thickness-twist vibration of a piezoelectric plate resonator of crystals of 6 mm symmetry. An exact theoretical analysis is performed. Results show that non-uniform electrodes have a strong effect on mode shapes, and suggest the possibility of using nonuniform electrodes for strong energy trapping.

  20. Design and fabrication of aspherical bimorph PZT optics

    CERN Document Server

    Tseng, T C; Yeh, Z C; Perng, S Y; Wang, D J; Kuan, C K; Chen, J R; Chen, C T

    2001-01-01

    Bimorph piezoelectric optics with a third-order-polynomial surface is designed and a prototype is fabricated as active optics. Two pairs of silicon (Si) and lead zirconate titanate (PZT) piezoelectric ceramic are bonded as Si-PZT-PZT-Si together with a multi-electrode or thin film resistor coating used as the control electrode between Si and PZT and metallic films as grounding between the interface of PZT ceramics. A linear voltage is applied to the bimorph PZT optics by probing the control electrodes from a two-channel controllable power supplier. In doing so, the optics surface can achieve a desired third-order-polynomial surface. Reducing hysteresis and creep in bimorph PZT X-ray optics is the only feasible way by inserting an appropriate capacitor in series with bimorph PZT optics to significantly reduce both effects.

  1. (100)-Textured KNN-based thick film with enhanced piezoelectric property for intravascular ultrasound imaging

    Science.gov (United States)

    Zhu, Benpeng; Zhang, Zhiqiang; Ma, Teng; Yang, Xiaofei; Li, Yongxiang; Shung, K. Kirk; Zhou, Qifa

    2015-04-01

    Using tape-casting technology, 35 μm free-standing (100)-textured Li doped KNN (KNLN) thick film was prepared by employing NaNbO3 (NN) as template. It exhibited similar piezoelectric behavior to lead containing materials: a longitudinal piezoelectric coefficient (d33) of ˜150 pm/V and an electromechanical coupling coefficient (kt) of 0.44. Based on this thick film, a 52 MHz side-looking miniature transducer with a bandwidth of 61.5% at -6 dB was built for Intravascular ultrasound (IVUS) imaging. In comparison with 40 MHz PMN-PT single crystal transducer, the rabbit aorta image had better resolution and higher noise-to-signal ratio, indicating that lead-free (100)-textured KNLN thick film may be suitable for IVUS (>50 MHz) imaging.

  2. An Analytical Method for Calculating P-SV Acoustical Field Excited by a Piezoelectric Strip with Finite Width and Thickness

    Institute of Scientific and Technical Information of China (English)

    ZHANG Bi-Xing; WANG Cheng-Hao; Anders Bostr(o)m

    2005-01-01

    @@ A piezoelectric strip with finite width and thickness is placed on top of an isotropic elastic half-space. Acoustical field can be excited when a voltage is across the piezoelectric strip. An analytical method is presented to calculate the acoustical field by the dynamics characteristics of the piezoelectric strip. Considering the piezoelectric strip as an anisotropic material of the 6 mm-type crystal system, we study the two-dimensional P-SV acoustical fields inside the piezoelectric strip and the isotropic half-space. The displacement and stress distributions are analysed thoroughly. The effects of the width and thickness of the piezoelectric strip and other parameters on the acoustical field are also analysed.

  3. Effect of Lanthanum Substitution on the Structural, dielectric, Ferroelectric and Piezoelectric Properties of Mechanically Activated PZt Electroceramics

    Directory of Open Access Journals (Sweden)

    Ajeet Kumar

    2016-06-01

    Full Text Available Different compositions of (Pb1-xLax (Zr0.60Ti0.40O3 (abbreviated as PLZT x/60/40; x=0, 0.07, 0.08 and 0.10 ceramics were prepared by a combinatorial approach by high energy mechano-chemical ball milling and cold isostatic pressing (CIP. X-ray diffraction patterns and transmission as well as scanning electron microscope were used for the micro-structural and morphological studies. The average particle size of PLZT milled powders was measured from the TEM images and was found to be in the nm range.XRD patterns of the sintered PLZT x/60/40 ceramics confirm the perovskite phase formation after heat treatment. SEM of sintered PLZT x/60/40 ceramics show a close packed dense structure. PLZT 8/60/40 ceramics show the fine grains (~1.3 µm with density ~97 per cent. Dielectric constant and loss were measured as a function of temperature. PLZT 8/60/40 ceramics shows the highest value of room temperature dielectric constant ~2480 at 1 kHz. Ferroelectric studies were done with the help of polarisation (P-E and strain (S-E vs. electric field measurements. PLZT 8/60/40 ceramics shows the maximum value of remnant polarisation (~36 µC/cm2 and strain (~0.27 per cent, respectively. PLZT x/60/40 ceramic samples were poled at optimized poling conditions. The measured values of piezoelectric charge coefficient (d33 and electromechanical coupling factor (kp of PLZT 8/60/40 ceramics were found to be, ~690 pC/N and ~71 per cent, respectively.

  4. Analytical Optimization of Piezoelectric Circular Diaphragm Generator

    Directory of Open Access Journals (Sweden)

    S. Mohammadi

    2013-01-01

    Full Text Available This paper presents an analytical study of the piezoelectric circular diaphragm microgenerator using strain energy method. Piezoelectrics are the intelligent materials that can be used as transducer to convert mechanical energy into electrical energy and vice versa. The aim of this paper is to optimize produced electrical energy from mechanical pressure. Therefore, the circular metal plate equipped with piezoelectric circular patch has been considered with simply and clamped supports. A comprehensive modeling, parametrical study and the effect of the boundary conditions on the performance of the microgenerator have been investigated. The system is under variable pressure from an oscillating pressure source. Results are presented for PZT and PMN-PT piezoelectric materials with steel and aluminum substrates. An optimal value for the radius and thickness of the piezoelectric layer with a special support condition has been obtained.

  5. Influence of La in xPBBiN of ternary nanoceramic composite (1-x0.5PMN-0.5PZT-xPBBiN system by mechanic al activatio n technique for dielectric and piezoelectric properties

    Directory of Open Access Journals (Sweden)

    K. CHANDRAMOULI

    2011-06-01

    Full Text Available (1-x[0.5Pb(Mg0.33Nb0.67O3-0.5Pb(Zr0.53Ti0.47O3]-x[Pb0.557Ba0.38La0.022Bi0.02Nb2O6] with both perovskite and tungsten bronze structured composite have been synthesized through mechanical activation technique. The strong influence of lanthanum addition to the lead-barium-bismuth-niobate (xPBLBiN ceramics in perovskite structured (1-xPMN-PZT on structural and functional properties is confirmed. X-ray diffraction patterns studies showed that these complex composites consisted of perovskite Cubic with tungsten bronze Orthorhombic phases. La modification in PBBiN of a ternary system (1-xPMN-PZTxPBBiN revealed intensified orthorhombicity. As La increased the dielectric and piezoelectric properties tremendously increased in (1-xPMN-PZT-xPBLBiN nanoceramic composite. The optimum dielectric and piezoelectric properties (εRT = 2931, kp = 0.461 and d33 = 428 pC/N were found in x =0.4 composite. We achieved novel nanocomposites synthesized by high energy ball milling method and having binary structures in a single composite with excellent functional properties that can be used for energy harvesting applications.

  6. Dynamic Response of a Thick Piezoelectric Circular Cylindrical Panel: An Exact Solution

    Directory of Open Access Journals (Sweden)

    Atta Oveisi

    2014-01-01

    Full Text Available One of the interesting fields that attracted many researchers in recent years is the smart structures. The piezomaterials, because of their ability in converting both mechanical stress and electricity to each other, are very applicable in this field. However, most of the works available used various inexact two-dimensional theories with certain types of simplification, which are inaccurate in some applications such as thick shells while, in some applications due to request of large displacement/stress, thick piezoelectric panel is needed and two-dimensional theories have not enough accuracy. This study investigates the dynamic steady state response and natural frequency of a piezoelectric circular cylindrical panel using exact three-dimensional solutions based on this decomposition technique. In addition, the formulation is written for both simply supported and clamped boundary conditions. Then the natural frequencies, mode shapes, and dynamic steady state response of the piezoelectric circular cylindrical panel in frequency domain are validated with commercial finite element software (ABAQUS to show the validity of the mathematical formulation and the results will be compared, finally.

  7. Thickness ratio and d 33 effects on flexible piezoelectric unimorph energy conversion

    Science.gov (United States)

    Ha, Taewoo; Zhang, John X. J.; Lu, Nanshu

    2016-03-01

    Piezoelectric unimorphs are bilayer structures where a blanket piezoelectric film (with top and bottom electrodes) is uniformly laminated on an inactive but flexible substrate. Because of their simple construction and flexibility, unimorphs are widely used as a key element in flexible sensors and actuators. The response of a unimorph is governed by the material properties of the film and the substrate as well as their geometric parameters. For low frequency biological energy harvesting, structural optimization is critical due to the dimensional confinement imposed by curvilinear and deformable bio-tissues. Here we report a comprehensive theoretical framework to investigate the effects of the film-to-substrate thickness ratio on voltage, charge, and energy outputs when the unimorph is subjected to eight different boundary/loading conditions. A broad class of power generators can be designed using such a framework under the assumption that the unimorph length is very large compared to its thickness, where the only dimensionless variable is the film-to-substrate thickness ratio. We show that the analytical and finite element modeling results are in excellent agreement. For not so thin unimorphs, there is non-zero normal stress in the thickness direction (σ 3) and d 33 can play a significant role in this case. Non-monotonic dependence of voltage and energy generation on thickness ratio has been found in some cases and optimum thickness ratio for unimorph generator can be predicted. When the unimorph is actuated by voltage applied across the piezo-film thickness, non-monotonic maximum deflection versus thickness ratio is also found. This work provides new physical insights on unimorphs and analytical solutions that can be used for the structural design and optimization of unimorphs under different boundary/loading conditions.

  8. Effect of stiffness and thickness ratio of host plate and piezoelectric patches on reduction of the stress concentration factor

    Science.gov (United States)

    Fesharaki, Javad Jafari; Madani, Seyed Ghasem; Golabi, Sa'id

    2016-09-01

    This paper focuses on the effects of stiffness ratio and thickness ratio on reducing stress concentration factor using piezoelectric patches in a rectangular plate with a hole, as a classical shape. Various locations of actuators and induction of positive/negative strains into the host plate are investigated and the best location of patches is presented. The study investigated the ratio effects and piezoelectric patches bounded on a rectangular host plate having various thicknesses and materials. Results show that the best position of actuators varies based on values of thickness and stiffness ratios of the host plate and piezoelectric patches. Also, the location of maximum stress concentration is transmitted from top and bottom of the hole to another point around the edge by changing the location of the piezoelectric actuators. To verify the results, some experimental tests are applied. The results show good agreement between the finite element analysis and experimental tests.

  9. Fabrication and modeling of piezoelectric transducers for High-Frequency medical imaging

    CERN Document Server

    Abellard, André-Pierre; Holc, Janez; Levassort, Franck; Noshchenko, Oleksandr; Lethiecq, Marc; Kosec, Marija

    2013-01-01

    We have studied the processing of piezoelectric thick films using electrophoretic deposition (EPD) for high-frequency ultrasound applications. Lead-zirconium-titanate (PZT) particles synthetized by solid states synthesis were dispersed in ethanol using ammonium polyacrylate (PAA). The electrophoretic deposition of PZT particles was performed at a constant-current mode. PZT thick-films deposited at 1 mA for 60 seconds were sintered at 900oC for 2 hours in a PbO-controlled atmosphere. The scanning-electron microscopy (SEM) analysis shows that the thickness of PZT layer is uniform and that the pores are homogeneously distributed within the layer. The complex electrical impedance was measured and fitted by KLM scheme in order to deduce the dielectric, mechanical and piezoelectric parameters of the thick-films. The density and thickness of PZT thick films are used as inputs and the thickness coupling factor kt, dielectric constant at constant strain and resonant frequency are deduced. The results show that homogen...

  10. Piezoelectric and magnetoelectric thick films for fabricating power sources in wireless sensor nodes.

    Science.gov (United States)

    Priya, Shashank; Ryu, Jungho; Park, Chee-Sung; Oliver, Josiah; Choi, Jong-Jin; Park, Dong-Soo

    2009-01-01

    In this manuscript, we review the progress made in the synthesis of thick film-based piezoelectric and magnetoelectric structures for harvesting energy from mechanical vibrations and magnetic field. Piezoelectric compositions in the system Pb(Zr,Ti)O(3)-Pb(Zn(1/3)Nb(2/3))O(3) (PZNT) have shown promise for providing enhanced efficiency due to higher energy density and thus form the base of transducers designed for capturing the mechanical energy. Laminate structures of PZNT with magnetostrictive ferrite materials provide large magnitudes of magnetoelectric coupling and are being targeted to capture the stray magnetic field energy. We analyze the models used to predict the performance of the energy harvesters and present a full system description.

  11. Piezoelectric and Magnetoelectric Thick Films for Fabricating Power Sources in Wireless Sensor Nodes

    Directory of Open Access Journals (Sweden)

    Jong-Jin Choi

    2009-08-01

    Full Text Available In this manuscript, we review the progress made in the synthesis of thick film-based piezoelectric and magnetoelectric structures for harvesting energy from mechanical vibrations and magnetic field. Piezoelectric compositions in the system Pb(Zr,TiO3–Pb(Zn1/3Nb2/3O3 (PZNT have shown promise for providing enhanced efficiency due to higher energy density and thus form the base of transducers designed for capturing the mechanical energy. Laminate structures of PZNT with magnetostrictive ferrite materials provide large magnitudes of magnetoelectric coupling and are being targeted to capture the stray magnetic field energy. We analyze the models used to predict the performance of the energy harvesters and present a full system description.

  12. Fabrication and Performances of 1-3-2 Piezoelectric Ceramic/Polymer Composite

    Institute of Scientific and Technical Information of China (English)

    Likun Wang; Guang Li; Hongliang Du; Lei Qin; Shuxiang Li

    2006-01-01

    A novel 1-3-2 piezoelectric composite has been developed, which consists of piezoelectric ceramic plate and 1-3 piezoelectric composite. The composite was fabricated by dicing PZT ceramic along mutual perpendicular two directions and then filling epoxy into grooves. The piezoelectric and electromechanical properties of the novel composite were determined.The results show a coefficient d33 of 405 pC/N, a vibration displacement of 113.5 pm, an acoustic impendence of 13.3 Mraly,a bandwidth of 12 kHz and a thickness electromechanical coupling coefficient of 0.56.

  13. Screen printed thick film based pMUT arrays

    DEFF Research Database (Denmark)

    Hedegaard, Tobias; Pedersen, T; Thomsen, Erik Vilain;

    2008-01-01

    This article reports on the fabrication and characterization of lambda-pitched piezoelectric micromachined ultrasound transducer (pMUT) arrays fabricated using a unique process combining conventional silicon technology and low cost screen printing of thick film PZT. The pMUTs are designed as 8...

  14. Fabrication, characterization and applications of PZT and ITO nanostructures

    Science.gov (United States)

    Xu, Shiyou

    Lead Zirconate Titanate (PbZr1--xTixO 3, PZT) is one of the most important piezoelectric materials, which has been used traditionally as sensors and actuators. One dimensional (1-D) PZT is expected to have great potentials as building blocks for micro and nano sensors and actuators, nano active fiber composites and integrated nanosystems. The objective of this research is to investigate the size effect on mechanical and piezoelectric properties through the fabrication and characterization of 1-D PZT nanostructures such as PZT nanofibers and nanotubes. The electrospinning process and template-assisted method were used to synthesize PZT nanofibers and nanotubes, respectively. Various novel experimental methods, such as atomic force microscopy (AFM) and nanomanipulator, were used to characterize the mechanical and piezoelectric properties of PZT nanostructures. The obtained results have shown that the piezoelectric and mechanical properties of PZT are size dependent. A single PZT nanofiber presented a lower young's modulus (42.99 GPa measured from AFM-base method and 46.6 GPa from vibration-based method, respectively) than that of PZT thin films and bulks. The PZT nanofibers with diameters smaller than 150 nm still demonstrated a strong electromechanical coupling effect. The piezoelectric constant (d 33) of PZT nanofibers increased from 574.1 pm/V to 860.5 pm/V when their diameters decreased from 112 nm to 50 nm. PZT nanotubes were found to have a d33 value of up to 595 pm/V. These values are significantly higher than that of PZT thin films and comparable to that of PZT bulks. The PZT nanofibers and nanotubes developed in this research not only provide new types of sensing and actuation mechanisms for various novel nanodevices, but also provide significantly improved performance compared with their thin film counterpart used in microelectromechanical systems (MEMS). 1-D ITO nanostructures (nanofibers and nanotubes) were synthesized and characterized for potential use

  15. Manufacturing of prestressed piezoelectric unimorphs using a postfired biasing layer.

    Science.gov (United States)

    Juuti, Jari A; Jantunen, Heli; Moilanen, Veli-Pekka; Leppävuori, Seppo

    2006-05-01

    A novel manufacturing method for prestressed piezoelectric unimorphs is introduced and the actuator properties are examined. Prestressed PZT 5A and PZT 5H unimorphs with piezo material thickness of 250 microm and 375 microm were manufactured by using sintering and thermal shrinkage of the prestressing material. The process was carried out by screen printing a layer of AgPd paste on one side of the sintered bulk ceramic. As an alternative method, dielectric low temperature co-fired ceramic (LTCC) tape was used as the prestressing material. Different configurations were tested to obtain high displacements and to make a comparison between materials. After firing, the samples were poled, and the displacement versus load characteristics of the resulting actuators were investigated. A maximum displacement of 118 microm was obtained from a 250 microm thick, prestressed PZT 5H actuator with a diameter of 25 mm, in which LTCC tape was used as the prestressing layer. Similarly, the PZT 5H material provided a maximum displacement of 63 microm with a screen-printed AgPd prestressing layer. The manufacturing method described offers a novel approach for the production of a wide range of integrated active structures on, for instance, an LTCC circuit board. This is especially important because piezoelectric bulk materials with high piezoelectric coefficients can be used to produce high displacements.

  16. Piezoelectricity

    CERN Document Server

    Lubitz, Karl

    2008-01-01

    Piezoelectric materials play a key role in an innovative market. Advances in applications derive from new materials and their development, as well as to new market requirements. This report elucidates these developments by a broad spectrum of examples, comprising ultrasound in medicine and defence industry, and frequency control.

  17. Large electric-field control of perpendicular magnetic anisotropy in strained [Co/Ni] / PZT heterostructures

    Science.gov (United States)

    Gopman, Daniel; Dennis, Cindi; Chen, P. J.; Iunin, Yury; Shull, Robert

    We present a piezoelectric/ferromagnetic heterostructure with PMA - a Co/Ni multilayer sputtered directly onto a Pb(Zr,Ti)O3 (PZT) substrate. Chemical-mechanical polishing was used to reduce the roughness of PZT plates to below 2 nm rms, enabling optimal magnetoelectric coupling via the direct interface between PZT and sputtered Co/Ni films with large PMA (Keff = (95 +/-9 kJ/m3)) . We grew the following layer stack: Ta(3)/Pt(2)/[Co(0.15)/Ni(0.6)]x4/Co(0.15)/Pt(2)/Ta(3); numbers in parentheses indicate thicknesses in nm. Applied electric fields up to +/- 2 MV/m to the PZT generated 0.05% in-plane compression in the Co/Ni multilayer, enabling a large electric-field reduction of the PMA (ΔKeff >= 103 J/m3) and of the coercive field (35%). Our results demonstrate that: (i) heterostructures combining PZT and [Co/Ni] exhibit larger PMA (Keff ~105 J/m3) than previous magnetoelectric heterostructures based on Co/Pt and CoFeB, enabling thermally stable hybrid magnetoelectric/spintronic devices only tens of nm in diameter and (ii) electric-field control of the PMA is promising for more energy efficient switching of spintronic devices.

  18. Doping effects of CuO additives on the properties of low-temperature-sintered PMnN-PZT-based piezoelectric ceramics and their applications on surface acoustic wave devices.

    Science.gov (United States)

    Tsai, Cheng-Che; Chu, Sheng-Yuan; Lu, Chun-Hsien

    2009-03-01

    To develop the anisotropic ceramic substrate with low sintering temperature for surface acoustic wave (SAW) applications, the low cost and feasible material with moderate piezoelectric properties, good dielectric properties, and higher Curie temperature were explored. The piezoelectric ceramics with compositions of Pb[(Mn(1/3)Nb(2/3))(0.06-) (Zr(0.52)Ti(0.48))0.94] O(3) (PMnN-PZT) + 0.5 wt.% PbO + x wt.% CuO (0.05 = x = 0.3) had been prepared by the conventional mixed-oxides method. CuO dopants were used as the sintering aid to improve the bulk density under low sintering temperature (i.e., 980-1040 degrees C). The phase structures, microstructures, frequency behavior of dielectric properties (up to 50 MHz), piezoelectric properties, ferroelectric properties, and temperature stability with the amount of CuO additive were systematically investigated. Experimental results showed that the sintering temperature could be lowered down to 1020 degrees C and still keep reasonably good piezoelectric activity (i.e., high electromechanical coupling factor (k(p)), (k(t)) and dielectric and ferroelectric properties. The preferable composition, obtained at x = 0.1, presented the values of the electromechanical coupling factor (k(p)) (k(t)), mechanical quality factor (Q(m)), piezoelectric charge constant (d(33)), dielectric constant, dielectric loss, temperature coefficient of resonant frequency (TCF(B)), and Curie point (T(c)) of 0.54, 0.48, 850, 238 pc/N, 1450, 0.0023, 1.1 kV/mm, 26 coul/cm(2), -150 ppm/ degrees C, and 348 degrees C. Using this developed low-temperature-sintered material to make the piezoelectric substrate, the SAW filter was fabricated and its properties were measured. Results showed that this device possessed very high value of k(2)(7.13%) with a good TCF (-40.15 ppm/ degrees C), and a surface wave velocity (V(P)) of 2196 m/s.

  19. Performance analysis of piezoelectric bimorph generator

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    In this paper,the theoretical model and simulation of the performance of a piezoelectric (PZT)bimorph generator is introduced.The generator consists of two piezoelectric plates bonded on a substrate metal plate.For an effective electromechanical coupling coefficient (EECC) and the generated energy,the analytical formulae are established with the thickness ratio and the Young's modulus ratio as variables.After giving correlative material parameters,the EECC and generated energy can be computed.The results show that there is a optimal thickness ratio for a piezoelectric bimorph generator to achieve the maximum EECC and electrical energy.The EECC and generated energy decrease with an increase of the Young's modulus ratio.In addition,the influence of mechanical source on electrical energy generation and power output is also considered.

  20. Exact thickness-shear resonance frequency of electroded piezoelectric crystal plates

    Institute of Scientific and Technical Information of China (English)

    WANG Ji; SHEN Li-jun

    2005-01-01

    The determination of the precise thickness-shear frequency of electroded crystal plates has practical importance in quartz crystal resonator design and fabrication, especially when the high fundamental thickness-shear frequency has reduced the crystal plate thickness to such a degree that proper consideration of the effect of electrodes is very important. The electrodes effect as mass loading in the estimation of the resonance frequency has to be modified to consider the stiffness of electrodes, as the relative strength is increasingly noticeable. By following a known procedure in the determination of the thickness-shear frequency of an infinite AT-cut crystal plate, frequency equations of crystal plate without and with piezoelectric effect are obtained in terms of elastic constants and the electrode material density. After solving these equations for the usual design parameters of crystal resonators, the design process can be optimized to pinpoint the precise configuration to avoid time-consuming trial and reduction steps. Since these equations and solutions are presented for widely used materials and parameters, they can be easily integrated into the existing crystal resonator design and manufacturing processes.

  1. Thickness mode EMIS of constrained proof-mass piezoelectric wafer active sensors

    Science.gov (United States)

    Kamas, Tuncay; Giurgiutiu, Victor; Lin, Bin

    2015-11-01

    This paper addresses theoretical and experimental work on thickness-mode electromechanical (E/M) impedance spectroscopy (EMIS) of proof-mass piezoelectric wafer active sensors (PMPWAS). The proof-mass (PM) concept was used to develop a new method for tuning the ultrasonic wave modes and for relatively high frequency local modal sensing by the PM affixed on PWAS. In order to develop the theoretical basis of the PMPWAS tuning concept, analytical analyses were conducted by applying the resonator theory to derive the EMIS of a PWAS constrained on one and both surfaces by isotropic elastic materials. The normalized thickness-mode shapes were obtained for the normal mode expansion (NME) method to eventually predict the thickness-mode EMIS using the correlation between PMPWAS and the structural dynamic properties of the substrate. Proof-masses of different sizes and materials were used to tune the system resonance towards an optimal frequency point. The results were verified by coupled-field finite element analyses (CF-FEA) and experimental results. An application of the tuning effect of PM on the standing wave modes was discussed as the increase in PM thickness shifts the excitation frequency of the wave mode toward the surface acoustic wave (SAW) mode.

  2. Piezoelectric films for high frequency ultrasonic transducers in biomedical applications.

    Science.gov (United States)

    Zhou, Qifa; Lau, Sienting; Wu, Dawei; Shung, K Kirk

    2011-02-01

    Piezoelectric films have recently attracted considerable attention in the development of various sensor and actuator devices such as nonvolatile memories, tunable microwave circuits and ultrasound transducers. In this paper, an overview of the state of art in piezoelectric films for high frequency transducer applications is presented. Firstly, the basic principles of piezoelectric materials and design considerations for ultrasound transducers will be introduced. Following the review, the current status of the piezoelectric films and recent progress in the development of high frequency ultrasonic transducers will be discussed. Then details for preparation and structure of the materials derived from piezoelectric thick film technologies will be described. Both chemical and physical methods are included in the discussion, namely, the sol-gel approach, aerosol technology and hydrothermal method. The electric and piezoelectric properties of the piezoelectric films, which are very important for transducer applications, such as permittivity and electromechanical coupling factor, are also addressed. Finally, the recent developments in the high frequency transducers and arrays with piezoelectric ZnO and PZT thick film using MEMS technology are presented. In addition, current problems and further direction of the piezoelectric films for very high frequency ultrasound application (up to GHz) are also discussed.

  3. Energy harvesting from vertically aligned PZT nanowire arrays

    Science.gov (United States)

    Malakooti, Mohammad H.; Zhou, Zhi; Sodano, Henry A.

    2016-04-01

    In this paper, a nanostructured piezoelectric beam is fabricated using vertically aligned lead zirconate titanate (PZT) nanowire arrays and its capability of continuous power generation is demonstrated through direct vibration tests. The lead zirconate titanate nanowires are grown on a PZT thin film coated titanium foil using a hydrothermal reaction. The PZT thin film serves as a nucleation site while the titanium foil is used as the bottom electrode. Electromechanical frequency response function (FRF) analysis is performed to evaluate the power harvesting efficiency of the fabricated device. Furthermore, the feasibility of the continuous power generation using the nanostructured beam is demonstrated through measuring output voltage from PZT nanowires when beam is subjected to a sinusoidal base excitation. The effect of tip mass on the voltage generation of the PZT nanowire arrays is evaluated experimentally. The final results show the great potential of synthesized piezoelectric nanowire arrays in a wide range of applications, specifically power generation at nanoscale.

  4. Thickness dependence of piezoelectric properties of BiFeO3 films fabricated using rf magnetron sputtering system

    Science.gov (United States)

    Aramaki, Masaaki; Kariya, Kento; Yoshimura, Takeshi; Murakami, Shuichi; Fujimura, Norifumi

    2016-10-01

    The piezoelectric property of BiFeO3 films prepared on a (100) LaNiO3/Si(100) substrate using an rf magnetron sputtering system was investigated for their applications in MEMS vibration energy harvesters. The X-ray diffraction profiles indicate that (100)-oriented BiFeO3 films with thicknesses from 450 to 1750 nm were obtained at a deposition temperature of 510 °C. All the films showed well-defined ferroelectric hysteresis loops at room temperature. The thickness dependence of crystallinity and electrical properties indicated that the films have a bottom layer with a high defect density. The e 31,f piezoelectric coefficient and electromechanical coupling factor (k\\text{31,f}2) increase with increasing film thickness and reach -3.2 C/m2 and 3.3%, respectively, at a thickness of 1750 nm, which is considered to be caused by the decrease in defect density.

  5. Piezoelectric Sensor to Measure Soft and Hard Stiffness with High Sensitivity for Ultrasonic Transducers.

    Science.gov (United States)

    Li, Yan-Rui; Su, Chih-Chung; Lin, Wen-Jin; Chang, Shuo-Hung

    2015-06-11

    During dental sinus lift surgery, it is important to monitor the thickness of the remaining maxilla to avoid perforating the sinus membrane. Therefore, a sensor should be integrated into ultrasonic dental tools to prevent undesirable damage. This paper presents a piezoelectric (PZT) sensor installed in an ultrasonic transducer to measure the stiffness of high and low materials. Four design types using three PZT ring materials and a split PZT for actuator and sensor ring materials were studied. Three sensor locations were also examined. The voltage signals of the sensor and the displacement of the actuator were analyzed to distinguish the low and high stiffness. Using sensor type T1 made of the PZT-1 material and the front location A1 provided a high sensitivity of 2.47 Vm/kN. The experimental results demonstrated that our design can measure soft and hard stiffness.

  6. Piezoelectric Sensor to Measure Soft and Hard Stiffness with High Sensitivity for Ultrasonic Transducers

    Directory of Open Access Journals (Sweden)

    Yan-Rui Li

    2015-06-01

    Full Text Available During dental sinus lift surgery, it is important to monitor the thickness of the remaining maxilla to avoid perforating the sinus membrane. Therefore, a sensor should be integrated into ultrasonic dental tools to prevent undesirable damage. This paper presents a piezoelectric (PZT sensor installed in an ultrasonic transducer to measure the stiffness of high and low materials. Four design types using three PZT ring materials and a split PZT for actuator and sensor ring materials were studied. Three sensor locations were also examined. The voltage signals of the sensor and the displacement of the actuator were analyzed to distinguish the low and high stiffness. Using sensor type T1 made of the PZT-1 material and the front location A1 provided a high sensitivity of 2.47 Vm/kN. The experimental results demonstrated that our design can measure soft and hard stiffness.

  7. Integration of bulk piezoelectric materials into microsystems

    Science.gov (United States)

    Aktakka, Ethem Erkan

    Bulk piezoelectric ceramics, compared to deposited piezoelectric thin-films, provide greater electromechanical coupling and charge capacity, which are highly desirable in many MEMS applications. In this thesis, a technology platform is developed for wafer-level integration of bulk piezoelectric substrates on silicon, with a final film thickness of 5-100microm. The characterized processes include reliable low-temperature (200°C) AuIn diffusion bonding and parylene bonding of bulk-PZT on silicon, wafer-level lapping of bulk-PZT with high-uniformity (+/-0.5microm), and low-damage micro-machining of PZT films via dicing-saw patterning, laser ablation, and wet-etching. Preservation of ferroelectric and piezoelectric properties is confirmed with hysteresis and piezo-response measurements. The introduced technology offers higher material quality and unique advantages in fabrication flexibility over existing piezoelectric film deposition methods. In order to confirm the preserved bulk properties in the final film, diaphragm and cantilever beam actuators operating in the transverse-mode are designed, fabricated and tested. The diaphragm structure and electrode shapes/sizes are optimized for maximum deflection through finite-element simulations. During tests of fabricated devices, greater than 12microm PP displacement is obtained by actuation of a 1mm2 diaphragm at 111kHz with management IC, which incorporates a supply-independent bias circuitry, an active diode for low-dropout rectification, a bias-flip system for higher efficiency, and a trickle battery charger. The overall system does not require a pre-charged battery, and has power consumption of sleep-mode (simulated). Under lg vibration at 155Hz, a 70mF ultra-capacitor is charged from OV to 1.85V in 50 minutes.

  8. Adjustability of resonance frequency by external magnetic field and bias electric field of sandwich magnetoelectric PZT/NFO/PZT composites

    Science.gov (United States)

    Xu, Ling-Fang; Feng, Xing; Sun, Kang; Liang, Ze-Yu; Xu, Qian; Liang, Jia-Yu; Yang, Chang-Ping

    2017-07-01

    Sandwich magnetoelectric composites of PZT/NFO/PZT (PNP) have been prepared by laminating PZT5, NiFe2O4, and PZT5 ceramics in turn with polyvinyl alcohol (PVA) paste. A systematic study of structural, magnetic and ferroelectric properties is undertaken. Structural studies carried out by X-ray diffraction indicate formation of cubic perovskite phase of PZT5 ceramic and cubic spinel phase of NiFe2O4 ceramic. As increasing the content of PZT5 phase, ferroelectric loops and magnetic loops of PNP composites showed increasing remnant electric polarizations and decreasing remnant magnetic moments separately. Both external magnetic fields and bias voltages could regulate the basal radial resonance frequency of the composites, which should be originated with the transformation and coupling of the stress between the piezoelectric phase and magnetostrictive phase. Such magnetoelectric composite provides great opportunities for electrostatically tunable devices.

  9. Smart Energy Materials of PZT Ceramics

    Directory of Open Access Journals (Sweden)

    Mitsuhiro Okayasu

    2017-03-01

    Full Text Available To better understand the material properties of lead zirconate titanate (PZT ceramics, the domain-switching characteristics and electric power generation characteristics have been investigated during loading and unloading by using various experimental techniques. Furthermore, the influence of oscillation condition on the electrical power generation properties of lead zirconate titanate (PZT piezoelectric ceramics has been investigated. It is found that the power generation is directly attributed to the applied load and wave mode. The voltage rises instantly to the maximum level under square-wave mode, although the voltage increases gradually under triangular-wave mode. After this initial increase, there is a rapid fall to zero, followed by generation of increasingly negative voltage as the applied load is removed for all wave modes. Variation of the electric voltage is reflected by the cyclic loading at higher loading frequencies. On the basis of the obtained experimental results for the wave modes, the electrical power generation characteristics of PZT ceramics are proposed, and the voltages generated during loading and unloading are accurately estimated. The electric generation value is decrease with increasing the cyclic number due to the material failure, e.g., domain switching and crack. The influence of domain switching on the mechanical properties PZT piezoelectric ceramics is clarified, and 90 degree domain switching occurs after the load is applied to the PZT ceramic directly. Note that, in this paper, our experimental results obtained in our previous works were introduced

  10. Modeling of PZT-induced Lamb wave propagation in structures by using a novel two-layer spectral finite element

    Science.gov (United States)

    Liu, Xiaotong; Zhou, Li; Ouyang, Qinghua

    2016-04-01

    This paper presents a novel two-layer spectral finite element model, consisting of PZT wafer and host structure, to simulate PZT-induced Lamb wave propagation in beam-like and plate-like structures. Based on the idea of equal displacement on the interface between PZT wafer and host structure, the one-dimensional spectral beam element of PZT-host beam and two-dimensional spectral plate element of PZT-host plate are considered as one hybrid element, respectively. A novel approach is proposed by taking the coupling effect of piezoelectric transducers in the thickness direction into account. The dynamic equation of the two-layer spectral element is derived from Hamilton's principle. Validity of the developed spectral finite element is verified through numerical simulation. The result indicates that, compared with the conventional finite element method (FEM) based on elasticity, the proposed spectral finite element is proved to have a high accuracy in modeling Lamb wave propagation, meanwhile, significantly improve the calculation efficiency.

  11. A state space solution for the bending problem of thick laminated piezoelectric open cylindrical shells

    Institute of Scientific and Technical Information of China (English)

    SHENG Hong-yu; LI He-ping; XU Hai-yan

    2009-01-01

    Based on the theories of three-dimensional elasticity and piezoelectricity, and by assuming appropriate boundary functions, we established a state equation of piezoelectric cylindrical shells. By using the transfer matrix method, we presented an analytical solution that satisfies all the arbitrary boundary conditions at boundary edges, as well as on upper and bottom surfaces. Our solution takes into account all the independent elastic and piezoelectric constants for a piezoelectric orthotropy, and satisfies continuity conditions between plies of the laminates. The principle of the present method and corresponding results can be widely used in many engineering fields and be applied to assess the effectiveness of varions approximate and numerical models.

  12. Excitation of fundamental shear horizontal wave by using face-shear (d36) piezoelectric ceramics

    Science.gov (United States)

    Miao, Hongchen; Dong, Shuxiang; Li, Faxin

    2016-05-01

    The fundamental shear horizontal (SH0) wave in plate-like structures is extremely useful for non-destructive testing (NDT) and structural health monitoring (SHM) as it is non-dispersive. However, currently, the SH0 wave is usually excited by electromagnetic acoustic transducers (EMAT) whose energy conversion efficiency is fairly low. The face-shear ( d 36 ) mode piezoelectrics is more promising for SH0 wave excitation, but this mode cannot appear in conventional piezoelectric ceramics. Recently, by modifying the symmetry of poled PbZr1-xTixO3 (PZT) ceramics via ferroelastic domain engineering, we realized the face-shear d 36 mode in both soft and hard PZT ceramics. In this work, we further improved the face-shear properties of PZT-4 and PZT-5H ceramics via lateral compression under elevated temperature. It was found that when bonded on a 1 mm-thick aluminum plate, the d 36 type PZT-4 exhibited better face-shear performance than PZT-5H. We then successfully excite SH0 wave in the aluminum plate using a face-shear PZT-4 square patch and receive the wave using a face-shear 0.72[Pb(Mg1/3Nb2/3)O3]-0.28[PbTiO3] (PMN-PT) patch. The frequency response and directionality of the excited SH0 wave were also investigated. The SH0 wave can be dominated over the Lamb waves (S0 and A0 waves) from 160 kHz to 280 kHz. The wave amplitude reaches its maxima along the two main directions (0° and 90°). The amplitude can keep over 80% of the maxima when the deviate angle is less than 30°, while it vanishes quickly at the 45° direction. The excited SH0 wave using piezoelectric ceramics could be very promising in the fields of NDT and SHM.

  13. Surface Electroelastic Love Waves in Layered System with a Piezoelectric Substrate and Two Isotropic Layers of Any Thickness

    Directory of Open Access Journals (Sweden)

    Danoyan Z.N.

    2009-09-01

    Full Text Available In the article the existence and behaviour of electroelastic Love waves in three-layered system of a piezoelectric substrate of classes 6, 4, 6mm, 4mm and attached to her two isotropic layers (conductor-dielectric, conductor-conductor of any thickness is investigated, depending on the physicomechanical characteristics of layered system and relative thicknesses of layers. The characteristic equation of a required surface wave is investigated in case of a basic soft layer. The research is based on properties of the electromechanical factor of surface wave given in the work [1-5]. Existence of a Love wave of a gap type caused by extremely piezoelectric effect in particular is shown. The structure and behavior of modes of Love waves are investigated. The qualitative diagrams of “dispersive” curves of modes of Love waves are given . The relation between electroelastic Love waves, pure-elastic Love waves, and Bleustein-Gulyaev waves is discussed.

  14. Modeling of the Through-the-Thickness Electric Potentials of a Piezoelectric Bimorph Using the Spectral Element Method

    Directory of Open Access Journals (Sweden)

    Xingjian Dong

    2014-02-01

    Full Text Available An efficient spectral element (SE with electric potential degrees of freedom (DOF is proposed to investigate the static electromechanical responses of a piezoelectric bimorph for its actuator and sensor functions. A sublayer model based on the piecewise linear approximation for the electric potential is used to describe the nonlinear distribution of electric potential through the thickness of the piezoelectric layers. An equivalent single layer (ESL model based on first-order shear deformation theory (FSDT is used to describe the displacement field. The Legendre orthogonal polynomials of order 5 are used in the element interpolation functions. The validity and the capability of the present SE model for investigation of global and local responses of the piezoelectric bimorph are confirmed by comparing the present solutions with those obtained from coupled 3-D finite element (FE analysis. It is shown that, without introducing any higher-order electric potential assumptions, the current method can accurately describe the distribution of the electric potential across the thickness even for a rather thick bimorph. It is revealed that the effect of electric potential is significant when the bimorph is used as sensor while the effect is insignificant when the bimorph is used as actuator, and therefore, the present study may provide a better understanding of the nonlinear induced electric potential for bimorph sensor and actuator.

  15. An experimental investigation of piezoelectric P(VDF-TrFE) thick film on flexible substrate as energy harvester

    Science.gov (United States)

    Khoon Keat, Chow; Swee Leong, Kok; Kok Tee, Lau

    2017-06-01

    This paper proposes an experimental inves tigation of energy harvester using poly(vinylidene fluoride-trifluoroethylene) or P(VDF-TrFE) thick-film on flexible substrate by using print screen and rod method. Polyester film being used as the substrate where a sandwiched layer of electrode-piezopolymer-electrode thick film is deposited on. The thick-film is then annealed at 100°C and polarized at 100 V for the film with a thickness of about 18µm, being inspected under EDX, FESEM and XRD. The fabricated energy harvester piezoelectric is able to generate a maximum output power of 4.36 µW at an externa l electrical load of 1 kΩ with a maximum peak-to-peak of about 3.0V when an impact free-fall force of 0.2N was applied on the thick-film.

  16. Influence of binding material of PZT coating on microresonator's electrical and mechanical properties

    Science.gov (United States)

    Janusas, Giedrius; Guobiene, Asta; Palevicius, Arvydas; Brunius, Alfredas; Cekas, Elingas; Baltrusaitis, Valentinas; Sakalys, Rokas

    2017-06-01

    Microresonators are fundamental components integrated in hosts of MEMS applications: covering the automotive sector, the telecommunication industry, electronic equipment for surface/material characterization and motion sensing, and etc. The aim of this paper is to investigate the mechanical and electrical properties of PZT film fabricated with three binding materials: polyvinyl butyral (PVB), polymethyl methacrylate (PMMA) and polystyrene (PS) and to evaluate applicability in control of microresonators Q factor. Micro particles of PZT powder were mixed with 20% solution of PVB, PMMA and PS in benzyl alcohol. For investigation of mechanical and electrical properties multilayer cantilevers were made. Obtained PZT and polymer paste was screen printed on copper (thickness 40 μm) using polyester monofilament screen meshes (layer thickness 50 μm) and dried for 30 min at 100°C. Electric dipoles of the PZT particles in composite material were aligned using high voltage generator (5 kV) and a custom-made holder. Electric field was held for 30 min. Surfaces of the applied films were investigated by Atomic Force Microscope NanoWizard(R)3 NanoScience. Dynamic and electrical characteristics of the multilayer were investigated using laser triangular displacement sensor LK-G3000. The measured vibration amplitude and generated electrical potential was collected with USB oscilloscope PicoScope 3424. As the results showed, these cantilevers were able to transform mechanical strain energy into electric potential and, v.v. However, roughness of PZT coatings with PMMA and PS were higher, what could be the reason of the worse quality of the top electrode. However, the main advantage of the created composite piezoelectric material is the possibility to apply it on any uniform or non-uniform vibrating surface and to transform low frequency vibrations into electricity.

  17. Note: Accurate determination of thickness of multiple layers of thin film deposited on a piezoelectric quartz crystal.

    Science.gov (United States)

    Wajid, Abdul

    2013-10-01

    Modern day piezoelectric quartz crystal microbalances for thin film deposition control are based on Z-match equation, which is mathematically valid for deposition of a single material on a given quartz crystal. When multiple layers are deposited, thickness and deposition rate errors accumulate due to mismatch of acoustic impedance of different materials. Here we present a novel method, based on the acoustic transfer matrix formalism, for accurate determination of thickness of an arbitrary number of layers of dissimilar materials deposited on a quartz crystal. Laboratory data show excellent accuracy of the method compared to conventional Z-match equation.

  18. Reliability of vibration energy harvesters of metal-based PZT thin films

    Science.gov (United States)

    Tsujiura, Y.; Suwa, E.; Kurokawa, F.; Hida, H.; Kanno, I.

    2014-11-01

    This paper describes the reliability of piezoelectric vibration energy harvesters (PVEHs) of Pb(Zr,Ti)O3 (PZT) thin films on metal foil cantilevers. The PZT thin films were directly deposited onto the Pt-coated stainless-steel (SS430) cantilevers by rf-magnetron sputtering, and we observed their aging behavior of power generation characteristics under the resonance vibration condition for three days. During the aging measurement, there was neither fatigue failure nor degradation of dielectric properties in our PVEHs (length: 13 mm, width: 5.0 mm, thickness: 104 μm) even under a large excitation acceleration of 25 m/s2. However, we observed clear degradation of the generated electric voltage depending on excitation acceleration. The decay rate of the output voltage was 5% from the start of the measurement at 25 m/s2. The transverse piezoelectric coefficient (e31,f) also degraded with almost the same decay rate as that of the output voltage; this indicates that the degradation of output voltage was mainly caused by that of piezoelectric properties. From the decay curves, the output powers are estimated to degrade 7% at 15 m/s2 and 36% at 25 m/s2 if we continue to excite the PVEHs for 30 years.

  19. Extrusion and properties of lead zirconate titanate piezoelectric ceramics

    DEFF Research Database (Denmark)

    Cai, S.; Millar, C.E.; Pedersen, L.

    1997-01-01

    The purpose of this work was to develop a procedure for fabricating electroceramic actuators with good piezoelectric properties. The preparation of lead zirconate titanate (PZT) piezoelectric ceramic rods and tubes by extrusion processing is described. The microstructure of extrudates was investi......The purpose of this work was to develop a procedure for fabricating electroceramic actuators with good piezoelectric properties. The preparation of lead zirconate titanate (PZT) piezoelectric ceramic rods and tubes by extrusion processing is described. The microstructure of extrudates...

  20. Design of Interleaved Interdigitated Electrode Multilayer Piezoelectric Transformer utilizing Longitudinal and Thickness Mode Vibrations

    DEFF Research Database (Denmark)

    Rødgaard, Martin Schøler; Andersen, Thomas; Andersen, Michael A. E.

    2012-01-01

    In applications of high voltage and low power capacitor charging, conventional magnetic based power converters often suffer from bulky components and poor efficiency. Piezoelectric transformer (PT) based converters however, are compact and efficient, especially at high step-up applications...

  1. Thickness-dependent piezoelectric behaviour and dielectric properties of lanthanum modified BiFeO3 thin films

    Directory of Open Access Journals (Sweden)

    Glenda Biasotto

    2011-03-01

    Full Text Available Bi0.85La0.15FeO3 (BLFO thin films were deposited on Pt(111/Ti/SiO2 /Si substrates by the soft chemical method. Films with thicknesses ranging from 140 to 280 nm were grown on platinum coated silicon substrates at 500°C for 2 hours. The X-ray diffraction analysis of BLFO films evidenced a hexagonal structure over the entire thickness range investigated. The grain size of the film changes as the number of the layers increases, indicating thickness dependence. It is found that the piezoelectric response is strongly influenced by the film thickness. It is shown that the properties of BiFeO3 thin films, such as lattice parameter, dielectric permittivity, piezoeletric coefficient etc., are functions of misfit strains.

  2. Fatigue crack detection in thick steel structures with piezoelectric wafer active sensors

    Science.gov (United States)

    Gresil, M.; Yu, L.; Giurgiutiu, V.

    2011-04-01

    This paper presents a set of numerical and experimental results on the use of guided waves for structural health monitoring (SHM) of crack growth during a fatigue test in a thick steel plate used for civil engineering application. The capability of embedded piezoelectric wafer active sensors (PWAS) to perform in situ nondestructive evaluation (NDE) is explored. Numerical simulation and experimental tests are used to prove that PWAS can perform active SHM using guided wave pitch-catch method and passive SHM using acoustic emission (AE). Multi-physics finite element (MPFEM) codes are used to simulate the transmission and reception of guided waves in a 1-mm plate and their diffraction by a through hole. The MP-FEM approach permitted that the input and output variables be expressed directly in electric terms while the two-ways electromechanical conversion was done internally in the MP-FEM formulation. The analysis was repeated for several hole sizes and a damage index performances was tested. AE simulation was performed with the MP-FEM approach in a 13-mm plate in the shape of the compact tension (CT) fracture mechanics specimen. The AE event was simulated as a pulse of defined duration and amplitude. The electrical signal measured at a receiver PWAS was simulated. Daubechies wavelet transform was used to process the signal and identify its Lamb modes and FFT frequency contents. Experimental tests were performed with PWAS transducers acting as passive receivers of AE signals. The 8-mm thick flange of an I beam was instrumented on one side with PWAS transducers and on the other side with conventional AE transducers (PAC R15I) acting as comparison witnesses. An AE source was simulated using 0.5- mm pencil lead breaks; the PWAS transducers were able to pick up AE signal with good strength. Subsequently, PWAS transducers and R15I sensors were applied to a 13-mm CT specimen subjected to accelerated fatigue testing. The PWAS and R15I transducers signals were collected with

  3. An Unconventional Inchworm Actuator Based on PZT/ERFs Control Technology

    OpenAIRE

    Guojun Liu; Yanyan Zhang; Jianfang Liu; Jianqiao Li; Chunxiu Tang; Tengfei Wang; Xuhao Yang

    2016-01-01

    An unconventional inchworm actuator for precision positioning based on piezoelectric (PZT) actuation and electrorheological fluids (ERFs) control technology is presented. The actuator consists of actuation unit (PZT stack pump), fluid control unit (ERFs valve), and execution unit (hydraulic actuator). In view of smaller deformation of PZT stack, a new structure is designed for actuation unit, which integrates the advantages of two modes (namely, diaphragm type and piston type) of the volume c...

  4. Circular Piezoelectric Accelerometer for High Band Width Application

    DEFF Research Database (Denmark)

    Hindrichsen, Christian Carstensen; Larsen, Jack; Lou-Møller, Rasmus

    2009-01-01

    is used as the sensing material on top of the silicon membrane. Accelerations in the out of plane direction induce a force on the seismic mass bending the membrane and a potential difference is measured in the out of plane direction of the stressed PZT. A resonance frequency of 23.50 kHz, a charge......An uniaxial bulk-micromachined piezoelectric MEMS accelerometer intended for high bandwidth application is fabricated and characterized. A circular seismic mass (radius = 1200 ¿m) is suspended by a 20 ¿m thick annular silicon membrane (radius = 1800 ¿m). A 24 ¿m PZT screen printed thick film...

  5. A uniform-sensitivity omnidirectional shear-horizontal (SH) wave transducer based on a thickness poled, thickness-shear (d15) piezoelectric ring

    Science.gov (United States)

    Huan, Qiang; Miao, Hongchen; Li, Faxin

    2017-08-01

    The fundamental shear horizontal (SH0) wave in plates is of great importance in the field of nondestructive testing (NDT) and structural health monitoring (SHM) since it is the unique non-dispersive guided wave mode. For practical applications, a phased array system based on omnidirectional SH0 wave transducers is most useful as it can cover a wide range of a plate. However, so far very few omnidirectional SH wave transducers have been developed. In this work, we proposed an omnidirectional SH wave piezoelectric transducer (OSH-PT) based on a thickness poled piezoelectric ring. The ring is equally divided into twelve sectors and the electric field is circumferentially applied, resulting in a new thickness-shear (d15) mode. Finite element analysis shows that the proposed OSH-PT can excite single-mode SH0 wave and receive the SH0 wave only. Experiments were then conducted to examine the performance of the proposed OSH-PT. Results indicated that it can generate and receive single-mode SH0 wave in a wide frequency range with nearly uniform sensitivities along all directions. Considering its quite simple configuration, compact size and low cost, the proposed OSH-PT is expected to greatly promote the applications of SH waves in the field of NDT and SHM.

  6. New technique for fabrication of high frequency piezoelectric Micromachined Ultrasound Transducers

    DEFF Research Database (Denmark)

    Pedersen, T; Thomsen, Erik Vilain; Zawada, T

    2008-01-01

    A novel technique for fabrication of linear arrays of high frequency piezoelectric Micromachined Ultrasound Transducers (pMUT) on silicon substrates is presented. Piezoelectric elements are formed by deposition of PZT ((PbZrxTi1-x)O3) into etched features of the silicon substrate...... such that the depth of these features determine the element thickness and hence the resonance frequency. The process leaves a near planar surface which is ideal for further wafer level processing such as top electrode and interconnect formation. A fabricated single element is characterized by pulse echo response....

  7. Voltage generation of piezoelectric cantilevers by laser heating.

    Science.gov (United States)

    Hsieh, Chun-Yi; Liu, Wei-Hung; Chen, Yang-Fang; Shih, Wan Y; Gao, Xiaotong; Shih, Wei-Heng

    2012-11-15

    Converting ambient thermal energy into electricity is of great interest in harvesting energy from the environment. Piezoelectric cantilevers have previously been shown to be an effective biosensor and a tool for elasticity mapping. Here we show that a single piezoelectric (lead-zirconate titanate (PZT)) layer cantilever can be used to convert heat to electricity through pyroelectric effect. Furthermore, piezoelectric-metal (PZT-Ti) bi-layer cantilever showed an enhanced induced voltage over the single PZT layer alone due to the additional piezoelectric effect. This type of device can be a way for converting heat energy into electricity.

  8. Interdigitated-electrode-based MEMS-scale piezoelectric energy harvester modeling and optimization using finite element method.

    Science.gov (United States)

    Toprak, Alperen; Tigli, Onur

    2013-10-01

    This paper presents a novel optimization method for interdigitated electrode (IDE)-based, cantilever-type piezoelectric energy harvesters at microelectromechanical system (MEMS) scale. A new two-stage approach based on the finite element method is proposed to examine the performance of such devices. First, detailed electrostatic poling simulations are presented. The results of these poling orientation simulations are used while calculating electrical energy and conversion efficiency in response to a constant external force. The proposed approach is used to find the optimum piezoelectric material thickness and IDE geometry for a cantilever beam which is constructed on top of a 4-μm Si structural layer and a 1-μm SiO2 isolation layer. Cantilever and IDE lengths are fixed at 320 μm and 240 μm, respectively, whereas the lead zirconate titanate (PZT) thickness, IDE finger widths, and number of finger pairs are varied. Maximum output energy of 0.37 pJ for a 15-μN force is obtained at a PZT thickness of 0.6 μm and an IDE consisting of 12 finger pairs. This energy is reduced to 1.5 fJ for 5 μm PZT thickness with 2 electrode finger pairs, which shows that device geometry has a significant impact on device performance. The proposed method presents an accurate framework for the rapid design and performance prediction of novel piezoelectric energy harvester structures.

  9. High Reliability Cryogenic Piezoelectric Valve Actuator Project

    Data.gov (United States)

    National Aeronautics and Space Administration — Piezoelectric actuators constructed with the "smart material" PZT offer many potential advantages for use in NASA cryo-valve missions relative to conventional...

  10. Directed colloidal assembly and characterization of PZT-polymer composites

    Science.gov (United States)

    Smay, James Earl

    Lead zirconate titanate (PZT)-based layers and 3-D structures were directly assembled using two colloidal routes: (1) tape casting and (2) a layer-by-layer robotic deposition technique, known as robocasting. First, concentrated (φsolids > 0.45) suspensions of PZT-5H and a latex emulsion were tape cast with the aid of viscosifier and surfactant additions. Drying stress evolved to a maximum at φ PZT ˜ 0.49, followed by a reduction and a secondary stress rise attributed to latex coalescence. Dielectric and piezoelectric properties of sintered PZT multilayer laminates exhibited good agreement with those for isostatically pressed and sintered samples. Concentrated, weakly gelled suspensions of PZT 95/5 and poly(ethylene) (PE) latices, a fugitive species, were developed as inks for the robotic deposition of monolithic and tri-layered composite structures. Monoliths, with densities of 93.6% and 96.1%, and composites with a 96.1% dense layer between 93.6% regions were fabricated. The structures displayed equivalent electrical properties to cold isostatically pressed parts. The composites withstood repeated saturation polarization switching as well as a 500 MPa hydrostatic pressure-induced poled ferroelectric (FE) to antiferroelectric (AFE) phase transformation. Concentrated (φPZT = 0.47) PZT-5H gels were developed as inks for the robotic deposition of 3-D, mesoscale periodic structures with self-supporting features such as lattices of rod-like elements and v-shaped test structures. The gels exhibited pH dependent viscoelastic properties and Hershel-Bulkley flow behavior. The deflection of as-deposited spanning elements was measured using laser profilometry. Flow modeling and shape evolution data indicated a core-shell architecture as the ink exited the deposition nozzle, which simultaneously provided strength to form spanning elements and good bonding between layers. The core grew rapidly (˜1s) due to the quick recovery of gel structure in these inks. 3-X type PZT

  11. Effects of adhesive thickness on the Lamb wave pitch-catch signal using bonded piezoelectric wafer transducers

    Science.gov (United States)

    Islam, M. M.; Huang, H.

    2016-08-01

    This paper investigates the effects of adhesive layer on Lamb wave ultrasound pitch-catch signals that are excited and sensed by piezoelectric wafer transducers bonded on a slender structure. Analytical models were established to simulate the longitudinal and flexural vibrations of the structures separately and parametric studies of the bonding layer properties, i.e. the shear transfer parameter, adhesive thickness, and shear modulus, were performed. The parametric studies indicate that there exists an optimal adhesive layer thickness that generates maximum ultrasound pitch-catch signal for both wave modes. This prediction was subsequently validated by measurements. In addition, an improved match between the measured and simulated pitch-catch signals was achieved by adjusting the adhesive layer parameters.

  12. Effect of solid content variations on PZT slip for tape casting

    Directory of Open Access Journals (Sweden)

    Gang Jian

    2012-12-01

    Full Text Available Lead zirconate titanate (PZT particles with pure tetragonal structure were synthesized by solid-state reaction method and used for preparation of slurries with different solid contents (34–80 wt.%. Then, PZT thick films were fabricated by the nonaqueous tape casting method. It was shown that the slurry prepared from ball-milled particles exhibited better rheology properties than slurry from particles which were not ball-milled. Measurement of sedimentation volumes and zeta potentials indicated particle aggregation, resulting in weak stability of the slurries with high solid contents. The microstructure, piezoelectric and ferroelectric properties of PZT sintered films were investigated in terms of solid contents. Ceramic films prepared from the slurry with solid contents of 73 wt.% had the optimal structure and properties. After poling at 200 °C with an applied field of 1.2 kV/cm, a d33 of 294 pC/N was achieved; typical ferroelectric properties were also observed with a Ps of 38 μC/cm2.

  13. Giant magnetoelectric effects in ferrite - PZT multilayer composites

    Science.gov (United States)

    Srinivasan, G.; Rasmussen, E. T.

    2002-03-01

    Materials that respond to both electric and magnetic fields are said to be magnetoelectric (ME) and facilitate field conversion. One way in principle to accomplish strong ME effects is a composite of magnetostrictive and piezoelectric materials in which the coupling is mediated by mechanical deformation. This report is on the synthesis of novel multilayers of magnetostrictive nickel zinc ferrite (NZFO) and piezoelectric lead zirconate titanate (PZT) that show a giant ME effect and maximum field conversion efficiency [1]. Bilayers and multilayers were prepared from thick films obtained by tape casting. The ME voltage coefficient was measured as a function of sample and experimental parameters. The coefficient ranged from 30 to 1500 mV/cm Oe, depending on the sample composition, volume fraction, and field orientation. The transverse coupling is an order of magnitude stronger than the longitudinal coefficient. The ME coefficient is maximum at room temperature and increases with increasing frequency. Data on the dependence of ME coupling on volume fraction of the two phases and bias magnetic field are in excellent agreement with theoretical predictions. - work supported by a grant from the NSF (DMR-0072144) 1. G. Srinivasan, E. T. Rasmussen, J. Gallegos, R. Srinivasan, Yu. I. Bokhan, and V. M. Laletin, Phys. Rev. B 64, 214408 (2001).

  14. Active PZT fibers: a commercial production process

    Science.gov (United States)

    Strock, Harold B.; Pascucci, Marina R.; Parish, Mark V.; Bent, Aaron A.; Shrout, Thomas R.

    1999-07-01

    Lead Zirconate Titanate (PZT) active fibers, from 80 to 250 micrometers in diameter, are produced for the AFOSR/DARPA funded Active Fiber Composites Consortium (AFCC) Program and commercial customers. CeraNova has developed a proprietary ceramics-based technology to produce PZT mono-filaments of the required purity, composition, straightness, and piezoelectric properties for use in active fiber composite structures. CeraNova's process begins with the extrusion of continuous lengths of mono-filament precursor fiber from a plasticized mix of PZT-5A powder. The care that must be taken to avoid mix contamination is described using illustrations form problems experiences with extruder wear and metallic contamination. Corrective actions are described and example microstructures are shown. The consequences of inadequate lead control are also shown. Sintered mono- filament mechanical strength and piezoelectric properties data approach bulk values but the validity of such a benchmark is questioned based on variable correlation with composite performance measures. Comb-like ceramic preform structures are shown that are being developed to minimize process and handling costs while maintaining the required mono-filament straightness necessary for composite fabrication. Lastly, actuation performance data are presented for composite structures fabricated and tested by Continuum Control Corporation. Free strain actuation in excess of 2000 microstrain are observed.

  15. Piezoelectric transducer array microspeaker

    KAUST Repository

    Carreno, Armando Arpys Arevalo

    2016-12-19

    In this paper we present the fabrication and characterization of a piezoelectric micro-speaker. The speaker is an array of micro-machined piezoelectric membranes, fabricated on silicon wafer using advanced micro-machining techniques. Each array contains 2n piezoelectric transducer membranes, where “n” is the bit number. Every element of the array has a circular shape structure. The membrane is made out four layers: 300nm of platinum for the bottom electrode, 250nm or lead zirconate titanate (PZT), a top electrode of 300nm and a structural layer of 50

  16. Study of pyroelectric activity of PZT/PVDF-HFP composite

    Directory of Open Access Journals (Sweden)

    Luiz Francisco Malmonge

    2003-12-01

    Full Text Available Flexible, free-standing piezo and pyroelectric composite with 0 to 3 connectivity was made up from Lead Zirconate Titanate (PZT powder and poly(vinylidene fluoride-hexafluoropropylene (PVDF-HFP copolymer. The pyroelectric and the piezoelectric longitudinal (d33 coefficients were measured. A 50/50 vol.% PZT/PVDF-HFP composite resulted in piezo and pyroelectric coefficients of d33 = 25.0 pC/N and p = 4.5 × 10-4 C/m²K at 70 °C, respectively. Analysis of the complex permittivity in a wide range of frequency was carried out indicating lower permittivity of the composite in comparison with a permittivity of the PZT ceramic. The low value of the permittivity gives a high pyroelectric figure of merit indicating that this material can be used to build a temperature sensor in spite of the lower pyroelectric coefficient compared with PZT.

  17. Synthesis and characterization of 10 nm thick piezoelectric AlN films with high c-axis orientation for miniaturized nanoelectromechanical devices

    Science.gov (United States)

    Zaghloul, Usama; Piazza, Gianluca

    2014-06-01

    The scaling of piezoelectric nanoelectromechanical systems (NEMS) is challenged by the synthesis of ultrathin and high quality piezoelectric films on very thin electrodes. We report the synthesis and characterization of the thinnest piezoelectric aluminum nitride (AlN) films (10 nm) ever deposited on ultrathin platinum layers (2-5 nm) using reactive sputtering. X-ray diffraction, high-resolution transmission electron microscopy, and fast Fourier transform analyses confirmed the proper crystal orientation, fine columnar texture, and the continuous lattice structure within individual grains in the deposited AlN nanometer thick films. The average extracted d31 piezoelectric coefficient for the synthesized films is -1.73 pC/N, which is comparable to the reported values for micron thick and highly c-axis oriented AlN films. The 10 nm AlN films were employed to demonstrate two different types of optimized piezoelectric nanoactuators. The unimorph actuators exhibit vertical displacements as large as 1.1 μm at 0.7 V for 25 μm long and 30 nm thick beams. These results have a great potential to realize miniaturized NEMS relays with extremely low voltage, high frequency resonators, and ultrasensitive sensors.

  18. Comparison of effective transverse piezoelectric coefficients e31,f of Pb(Zr,Ti)O3 thin films between direct and converse piezoelectric effects

    Science.gov (United States)

    Tsujiura, Yuichi; Kawabe, Saneyuki; Kurokawa, Fumiya; Hida, Hirotaka; Kanno, Isaku

    2015-10-01

    We evaluated the effective transverse piezoelectric coefficients (e31,f) of Pb(Zr,Ti)O3 (PZT) thin films from both the direct and converse piezoelectric effects of unimorph cantilevers. (001) preferentially oriented polycrystalline PZT thin films and (001)/(100) epitaxial PZT thin films were deposited on (111)Pt/Ti/Si and (001)Pt/MgO substrates, respectively, by rf-magnetron sputtering, and their piezoelectric responses owing to intrinsic and extrinsic effects were examined. The direct and converse |e31,f| values of the polycrystalline PZT thin films were calculated as 6.4 and 11.5-15.0 C/m2, respectively, whereas those of the epitaxial PZT thin films were calculated as 3.4 and 4.6-4.8 C/m2, respectively. The large |e31,f| of the converse piezoelectric property of the polycrystalline PZT thin films is attributed to extrinsic piezoelectric effects. Furthermore, the polycrystalline PZT thin films show a clear nonlinear piezoelectric contribution, which is the same as the Rayleigh-like behavior reported in bulk PZT. In contrast, the epitaxial PZT thin films on the MgO substrate show a piezoelectric response owing to the intrinsic and linear extrinsic effects, and no nonlinear contribution was observed.

  19. Magnetoelectric effect in metal–PZT laminates

    Indian Academy of Sciences (India)

    S Narendra Babu; T Bhimasankaram; S V Suryanarayana

    2005-08-01

    Magnetoelectric (ME) composites are two-phase composites consisting of piezoelectric and piezomagnetic materials as the participating constituents. These magnetoelectric composites when placed under external magnetic field, show electrical polarization (magnetoelectric output). The ME coupling is mediated by mechanical stress. In the present study, we have synthesized Ni/PZT/Ni and Fe/PZT/Fe layered composites for studying their ME output by dynamic magnetoelectric set up in which both d.c. and a.c. magnetic fields can be varied. The ME output obtained in these composites are higher than those obtained in 40% Ni0.97Co0.03Mn0.01 Fe1.9O4 + 60% BaTi1.02O3.04. The results with varying d.c. and a.c. magnetic fields are presented.

  20. A Resistivity Gradient Piezoelectric FGM Actuator

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    A resistivity gradient actuator based on lead zirconate titanate ceramics was successfully developed and the bending deflections up to 140 μm were obtained. The actuator material was a matrix of PZT ceramic into which smooth gradient of piezoelectric activity was introduced. The application of an electric field then causes the actuator to bend due to differential strains induced by the piezoelectric effect. The resistivity gradient of the actuator was achieved by doping PZT with suitable donor and acceptor dopants. PZT powder was modified and synthesized by using two stage powder fabrication method. The actuator was fabricated by uniaxial pressing followed by isostatic pressing with two layers of different resistivities.

  1. Finite element analysis of the dynamic behavior of radially polarized Functionally Graded Piezoelectric (FGP) structures

    Science.gov (United States)

    Kandasamy, Ramkumar; Cui, Fangsen

    2016-04-01

    In the traditional layered piezoelectric structures, high stress concentrations could cause the structural failure in interlayer surfaces due to repeated strain reversals. To overcome the performance limitations of these structures, the concept of Functionally Graded Materials (FGMs) has been introduced to improve the lifetime, integrity, and reliability of these structures. In this paper, the free and forced vibration of radially polarized Functionally Graded Piezoelectric (FGP) cylinders under different sets of loading are studied. Material properties such as piezoelectric, elastic and permittivity are assumed to change along its thickness, based on a specific gradation function. Four-parameter power law distribution is used to grade the volume fraction of the constituents comprising of PZT-5A and PZT-5H. Material property is assumed to be temperature dependent for a few numerical studies. The present modeling approach is validated by comparing the free and forced vibration of radially polarized Functionally Graded Piezoelectric (FGP) cylinders with those reported in the literature. The effects of material composition, loading and boundary conditions on the dynamic behavior of FGP cylinder are described. Since the modeling of functionally graded piezoelectric systems is challenging, the present study can help in the design and analysis of FGP cylinders.

  2. Magnetoelectric effects in bilayers and multilayers of magnetostrictive and piezoelectric perovskite oxides

    Science.gov (United States)

    Srinivasan, G.; Rasmussen, E. T.; Levin, B. J.; Hayes, R.

    2002-04-01

    The observation of strong magnetoelectric effects is reported in layered composites of ferromagnetic lanthanum manganites and piezoelectric lead zirconate titanate (PZT). Studies were made on thick-film structures of La0.7Sr0.3MnO3 (LSMO)-PZT and La0.7Ca0.3MnO3 (LCMO)-PZT. The low-frequency magnetoelectric (ME) voltage coefficient αE was measured in bilayers and multilayers synthesized by tape casting. The effect is stronger in LSMO-PZT than in LCMO-PZT, and is weaker in multilayers compared to bilayers. A maximum αE of 60 mV/cm Oe is measured for the transverse ME effect and is a factor of 2 to 3 higher than the longitudinal effect. The bias magnetic-field dependence of αE shows hysteresis and remanence. A general increase in αE is observed with increasing frequency or decreasing temperature. There is good qualitative agreement between theory and data for the magnetic-field dependence of αE.

  3. Study on Inter-Diffusion Barrier Layer between PZT Pyroelectric Thick Film and Si Substrate%PZT厚膜与Si衬底互扩散阻挡层研究

    Institute of Scientific and Technical Information of China (English)

    陈冲; 吴传贵; 彭强祥; 罗文博; 张万里; 王书安

    2013-01-01

    在Pt/Ti/SiO2/Si基片上,利用电泳沉积制备PZT热释电厚膜材料.为防止Pb和Si互扩散,在Pt底电极与SiO2/Si衬底间通过直流磁控溅射制备了TiOx薄膜阻挡层.对具有0、300 nm和500 nm TiOx阻挡层的PZT厚膜材料用SEM和能量色散谱仪(EDS)表征了Pb和Si互扩散情况,用动态热释电系数测量仪测试了热释电系数.结果表明,当TiOx阻挡层为500 nm时,可阻挡Pb和Si互扩散,热释电性能最好.热释电系数p=1.5×10-8 C·cm-2·K-1,相对介电常数εr=170,损耗角正切tanδ=0.02,探测度优值因子Fd=1.05×10-5pa-0.5.%PZT thick film as pyroelectric material has been prepared on the Pt/Ti/SiCK/Si substrate by using the electrophoresis deposition (EPD) method. In order to prevent the inter-diffusion between Pb and Si,a TiOx film barrier layer between Pt bottom electrode and SiO2/Si substrate has been prepared by using the DC magnetron sputtering method. The inter-diffusion between Pb and Si in PZT thick film material with TiO, barrier layer thickness of 0, 300 nm and 500 nm respectively have been characterized by SEM and EDS. The pyroelectric coefficient has been measured by the dynamic pyroelectric coefficient instrument. The results show that the inter-diffusion between Pb and Si can be blocked when the thickness of TiOx barrier layer is 500 nm and have the best pyroelectric properties. The pyroelectric coefficient, relative dielectric constant,dielectric loss and detectivity figure of merit are p=1. 5 × 10-8C · cm-2k-1 ,εr = 170,tan 8=0. 02 and Fd = 1. 05 × 10-5 Pa-0.5 respectively.

  4. Piezoelectric properties of the new generation active matrix hybrid (micro-nano) composites

    Science.gov (United States)

    Parali, Levent; Şabikoğlu, İsrafil; Kurbanov, Mirza A.

    2014-11-01

    A hybrid piezoelectric composite structure is obtained by addition of nano-sized BaTiO3, SiO2 to the micro-sized PZT and polymers composition. Although the PZT material itself has excellent piezoelectric properties, PZT-based composite variety is limited. Piezoelectric properties of PZT materials can be varied with an acceptor or a donor added to the material. In addition, varieties of PZT-based sensors can be increased with doping polymers which have physical-mechanical, electrophysical, thermophysical and photoelectrical properties. The active matrix hybrid structure occurs when bringing together the unique piezoelectric properties of micro-sized PZT with electron trapping properties of nano-sized insulators (BaTiO3 or SiO2), and their piezoelectric, mechanic and electromechanic properties significantly change. In this study, the relationship between the piezoelectric constant and the coupling factor values of microstructure (PZT-PVDF) and the hybrid structure (PZT-PVDF-BaTiO3) composite are compared. The d33 value and the coupling factor of the hybrid structure have shown an average of 54 and 62% increase according to microstructure composite, respectively. In addition, the d33 value and the coupling factor of the hybrid structure (PZT-HDPE-SiO2) have exhibited about 68 and 52% increase according to microstructure composite (PZT-HDPE), respectively.

  5. Experiments to Demonstrate Piezoelectric and Pyroelectric Effects

    Science.gov (United States)

    Erhart, Jirí

    2013-01-01

    Piezoelectric and pyroelectric materials are used in many current applications. The purpose of this paper is to explain the basic properties of pyroelectric and piezoelectric effects and demonstrate them in simple experiments. Pyroelectricity is presented on lead zirconium titanate (PZT) ceramics as an electric charge generated by the temperature…

  6. Design of a piezoelectric transducer cylindrical phase modulator for simulating acoustic emission signals

    Institute of Scientific and Technical Information of China (English)

    HE Cunfu; HANG Lijun; WU Bin

    2007-01-01

    To conveniently carry out the pipeline leak experiment in a laboratory,leak acoustic signals are simulated by using the converse piezoelectric effect of a piezoelectric transducer (PZT) cylindrical phase modulator.On the basis of the piezoelectric equations and electromechanical equivalence principle,the transfer function of a PZT cylindrical phase modulator is delivered.A PZT cylindrical phase modulator is designed,and the numerical simulation is conducted.Results prove that the PZT cylindrical phase modulator can effectively simulate leak acoustic emission signals when the frequency is lower than 25 KHz.

  7. Michelson interferometer for the piezoelectric coefficient measurements

    Directory of Open Access Journals (Sweden)

    Muensit, S.

    2002-01-01

    Full Text Available The present work has described the Michelson interferometer which is capable of measuring the vibrational amplitudes in a sub-angstrom range. In the system, a He-Ne laser is used as a monochromatic source of light and a photodiode as a detector to convert an optical signal into an electronic one. Lock-in detections of the electronic signals are applied to relate the vibrational amplitudes to the wavelength of the laser beam. A feedback circuit is introduced in order to stabilize the sensitivity of the interferometric system. With this setup, a mechanical displacement referred to a change in thickness of a vibrating sample can be measured and the corresponding piezoelectric coefficient, i.e. the ratio of the change in sample thickness to the applied voltage, evaluated. In order to check the performance of the system, measurements on lithium niobate (LiNbO3 have been made and its piezoelectric coefficient d33 was confirmed with 2% accuracy. The piezoelectric coefficient d33 for lead zirconate titanate (PZT ceramics was, therefore, determined by this interferometer and found to be 270 pm/V.

  8. Study of pyroelectric activity of PZT/PVDF-HFP composite

    OpenAIRE

    Luiz Francisco Malmonge; José Antonio Malmonge; Walter Katsumi Sakamoto

    2003-01-01

    Flexible, free-standing piezo and pyroelectric composite with 0 to 3 connectivity was made up from Lead Zirconate Titanate (PZT) powder and poly(vinylidene fluoride-hexafluoropropylene) (PVDF-HFP) copolymer. The pyroelectric and the piezoelectric longitudinal (d33) coefficients were measured. A 50/50 vol.% PZT/PVDF-HFP composite resulted in piezo and pyroelectric coefficients of d33 = 25.0 pC/N and p = 4.5 × 10-4 C/m²K at 70 °C, respectively. Analysis of the complex permittivity in a wide ran...

  9. No linealidad en muestras cerámicas de PZT muy delgadas

    Directory of Open Access Journals (Sweden)

    de Frutos, J.

    1999-10-01

    Full Text Available The development of piezoelectric sensors for high frequency requires to work with very thin samples of material. At this thick nesses, the stress concentration produces strong perturbations in the materials, and the origin oF a non linear response, which depends field on working conditions. With the goal to advance in the knowledgement of this phenomenon, and by using Complex Impedance Spectroscopy, we have analysed the response of PZT ceramics with thickness of microns as a function of the applied and the amplitude of the analysis signal. These results allow to establish the base to the development of ultrasonic tunable sensors for high frequency.

    El desarrollo de sensores piezoeléctricos de alta frecuencia, exige trabajar con muestras de material muy delgadas, del orden de micras. En estos espesores, las tensiones de trabajo causan fuertes perturbaciones en los materiales, provocando respuestas no lineales, sumamente dependientes de las condiciones de trabajo. Con el objetivo de avanzar en el conocimiento de este fenómeno, y haciendo uso de la técnica de Espectroscopia de Impedancia Compleja, hemos analizado la respuesta de muestras de PZT cerámico adelgazadas a espesores de micras, en función del campo aplicado y de la amplitud de la señal de análisis. El estudio de estos resultados, puede permitir sentar las bases para el desarrollo de sensores ultrasónicos de alta frecuencia sintonizables.

  10. Study of piezoelectric transducers in smart structure applications

    Science.gov (United States)

    Lam, Kwok Ho

    To develop a novel smart material in civil engineering applications, cement-based 1-3 composites have been fabricated and characterized. The feasibility of the embedded 1-3 composite transducers in structural monitoring applications have been demonstrated in this project. In the present work, piezoelectric ceramic discs and fibres were fabricated and used as the active phases of the 1-3 composites. Lead zirconate titanate (PZT) ceramic discs were fabricated using a conventional dry pressing method. All the parameters of PZT ceramics have been evaluated by a resonance technique. Crack-free PZT ceramic fibres were fabricated using a simple powder mixing method. The microstructural and electrical characterizations show that performance of the ceramic fibres can be comparable to that of the corresponding bulk ceramics. To study the piezoceramic/cement 1-3 composites, the properties of cement have been studied as a function of water content. The elastic properties of cement with different water/cement ratios were characterized using the ultrasonic immersion method. It was found that the cement paste with water/cement ratio of 0.5 is relatively "soft" to be used as the passive phase of a 1-3 composite. When comparing with the ceramics, the acoustic impedance of cement is much closer to that of concrete. Piezoelectric PZT/cement 1-3 composites with a wide range of the ceramic volume fraction (φ= 0.25--0.77) have been fabricated successfully using a dice-and-fill technique. Piezoelectric properties of the 1-3 composites were determined by a resonance technique. The characterization showed that the high piezoelectric characteristics of ceramics were maintained and the effective acoustic impedance of composites was reduced as expected. Even the phase matrix is the cement paste, the thickness electromechanical coupling coefficient kt of the 1-3 composites can be enhanced effectively which approaches to the k33 coefficient of the ceramics. The 1-3 composites were found to

  11. Design of Interleaved Interdigitated Electrode Multilayer Piezoelectric Transformer utilizing Longitudinal and Thickness Mode Vibrations

    DEFF Research Database (Denmark)

    Rødgaard, Martin Schøler; Andersen, Thomas; Andersen, Michael A. E.

    2012-01-01

    . In this paper an interleaved interdigitated electrode (IDE) multilayer PT utilizing longitude and thickness mode vibration for high step-up and high output voltage is developed, for driving capacitive loads of up to 2.5kV. The PT possesses native soft switching capabilities, enabling the utilization of inductor...

  12. Coupled field modeling of E/M impedance of piezoelectric wafer active sensor for cataphoretic coating thickness measurement

    Science.gov (United States)

    Kamas, T.; Tekkalmaz, M.

    2017-04-01

    The cataphoretic electro-coating is one of the most common methods that are used against corrosion as a primary coating layer. The cataphoretic electro-coating is commonly utilized technique especially in protecting of automobile components in automotive industry. This coating method has many advantages such as high corrosion resistance, ability of homogeneous and complete coating of components in any geometry, less pollution, and less risk of ignition. In this study, some specimens in the form of steel sheets coated by the cataphoretic electro-coating method are examined using electro-mechanical impedance spectroscopy (EMIS) method. One of the extensively employed sensor technologies has been permanently installed piezoelectric wafer active sensor (PWAS) for in situ continuous structural health monitoring (SHM). Using the transduction of ultrasonic elastic waves into voltage and vice versa, PWAS has been emerged as one of the major SHM sensing technologies. EMIS method has been utilized as a dynamic descriptor of PWAS and the structure on which it is bonded. EMIS of PWAS-structure couple is a high frequency local modal sensing technique by applying standing waves to indicate the response of the PWAS resonator by determining the resonance and anti-resonance frequencies. To simulate the actual EMIS measurements in the present work, two-dimensional and three-dimensional coupled field finite element models are created for both uncoated and coated steel plates in a commercial FEA software, ANSYS®. The EMIS values of the specimens in certain sizes and coated in different thickness are going to be simulated in broad-band of frequency spectra. The thickness of the coating layer and coating time are of paramount importance for the corrosion resistance. The coating layer thickness and the corresponding coating period will be optimized by analyses of the values obtained from the 2D and 3D EMIS simulations.

  13. Piezoelectric sensors to monitor lubricant film thickness at piston-cylinder contacts in a fired engine

    OpenAIRE

    2013-01-01

    The contact between the piston ring and cylinder liner is the most important sealing interface in an automotive engine. Understanding the contact interactions and lubricant film formation at this interface is crucial for the development of fuel-efficient and low emission engines. This article outlines the development of an ultrasonic approach to enable non-invasive measurement of the lubricant film thickness formed between piston and cylinder wall of a fired engine. The sensor system consiste...

  14. The Microscopic Origin of Residual Stress for Flat Self-Actuating Piezoelectric Cantilevers.

    Science.gov (United States)

    Lee, Jeong Hoon; Hwang, Kyo Seon; Kim, Tae Song

    2011-12-01

    In this study, flat piezoelectric microcantilevers were fabricated under low-stress Pb(Zr0.52Ti0.48)O3 (PZT) film conditions. They were analyzed using the Raman spectrum and wafer curvature methods. Based on the residual stress analysis, we found that a thickness of 1 μm was critical, since stress relaxation starts to occur at greater thicknesses, due to surface roughening. The (111) preferred orientation started to decrease when the film thickness was greater than 1 μm. The d33 value was closely related to the stress relaxation associated with the preferred orientation changes. We examined the harmonic response at different PZT cantilever lengths and obtained a 9.4-μm tip displacement at 3 Vp-p at 1 kHz. These analyses can provide a platform for the reliable operation of piezoelectric microdevices, potentially nanodevice when one needs to have simultaneous control of the residual stress and the piezoelectric properties.

  15. Thickness-dependent Electrical and Piezoelectric Properties of Lead-Free Ferroelectric Ba0.8Sr0.2TiO3 Thin Films

    Directory of Open Access Journals (Sweden)

    D.A. Kiselev

    2016-10-01

    Full Text Available The thickness dependent of electrical and piezoelectric properties of lead-free ferroelectric Ba0.8Sr0.2TiO3 thin films is reported. Ba0.8Sr0.2TiO3 (BST 80/20 thin films for various thickness, ranging from 150 nm to 550 nm, were prepared by high-frequency reactive sputtering of a ceramic target in an oxygen atmosphere on p-type Si substrate. Memory windows and effective dielectric constant of the BST film in Au/BST/Si thin film capacitors is found to increase with the increasing thickness of the film. Domain structure, domain switching and hysteresis loops of the BST 80/20 thin film were investigate via the piezoresponse force microscopy. Complete domain switching and strong piezoresponse are found in the ferroelectric BST film. The piezoelectric coefficient ( and the remnant piezoelectric response (ΔPR of BST 80/20 films is found to increase with the thickness of the film.

  16. Equivalent circuit and optimum design of a multilayer laminated piezoelectric transformer.

    Science.gov (United States)

    Dong, Shuxiang; Carazo, Alfredo Vazquez; Park, Seung Ho

    2011-12-01

    A multilayer laminated piezoelectric Pb(Zr(1-x)Ti(x))O(3) (PZT) ceramic transformer, operating in a half- wavelength longitudinal resonant mode (λ/2 mode), has been analyzed. This piezoelectric transformer is composed of one thickness-polarized section (T-section) for exciting the longitudinal mechanical vibrations, two longitudinally polarized sections (L-section) for generating high-voltage output, and two insulating layers laminated between the T-section and L-section layers to provide insulation between the input and output sections. Based on the piezoelectric constitutive and motion equations, an electro-elasto-electric (EEE) equivalent circuit has been developed, and correspondingly, an effective EEE coupling coefficient was proposed for optimum design of this multilayer transformer. Commercial finite element analysis software is used to determine the validity of the developed equivalent circuit. Finally, a prototype sample was manufactured and experimental data was collected to verify the model's validity.

  17. Electromechanical-Traffic Model of Compression-Based Piezoelectric Energy Harvesting

    Directory of Open Access Journals (Sweden)

    Kok B.C.

    2016-01-01

    Full Text Available Piezoelectric energy harvesting has advantages over other alternative sources due to its large power density, ease of applications, and capability to be fabricated at different scales: macro, micro, and nano. This paper presents an electromechanical-traffic model for roadway compression-based piezoelectric energy harvesting system. A two-degree-of-freedom (2-DOF electromechanical model has been developed for the piezoelectric energy harvesting unit to define its performance in power generation under a number of external excitations on road surface. Lead Zirconate Titanate (PZT-5H is selected as the piezoelectric material to be used in this paper due to its high Piezoelectric Charge Constant (d and Piezoelectric Voltage Constant (g values. The main source of vibration energy that has been considered in this paper is the moving vehicle on the road. The effect of various frequencies on possible generated power caused by different vibration characteristics of moving vehicle has been studied. A single unit of circle-shape Piezoelectric Cymbal Transducer (PCT with diameter of 32 mm and thickness of 0.3 mm be able to generate about 0.12 mW and 13 mW of electric power under 4 Hz and 20 Hz of excitation, respectively. The estimated power to be generated for multiple arrays of PCT is approximately 150 kW/ km. Thus, the developed electromechanical-traffic model has enormous potential to be used in estimating the macro scale of roadway power generation system.

  18. Piezoelectric and mechanical properties of structured PZT–epoxy composites

    NARCIS (Netherlands)

    Kunnamkuzhakkal James, N.; Van den Ende, D.; Lafont, U.; Van der Zwaag, S.; Groen, W.A.

    2013-01-01

    Structured lead zirconium titanate (PZT)–epoxy composites are prepared by dielectrophoresis. The piezoelectric and dielectric properties of the composites as a function of PZT volume fraction are investigated and compared with the corresponding unstructured composites. The effect of poling voltage o

  19. Ceramics like PZT-PMN; Ceramicas do tipo PZT-PMN

    Energy Technology Data Exchange (ETDEWEB)

    Droescher, R.E.; Sousa, V.C. [Universidade Federal do Rio Grande do Sul (LABIOMAT/DEMAT/UFRGS), Porto Alegre, RS (Brazil). Dept. de Materiais. Lab. de Biomateriais; Bergman, C.P. [Universidade Federal do Rio Grande do Sul (LACER/DEMAT/UFRGS), Porto Alegre, RS (Brazil). Dept. de Materiais. Lab. de Ceramicas Avancadas

    2009-07-01

    The goal of this work was to achieve piezoelectric ceramics referring to the system PZT-PMN Pb(Mg{sub 1}/{sub 3}Nb{sub 2}/{sub 3}Zr{sub 0},{sub 52}Ti{sub 0},{sub 48})O{sub 3} . Have been analysed ceramics like 0,65PZT-0,35PMN ((Pb(Mg{sub 0},{sub 1167}Nb{sub 0},{sub 2300}Zr{sub 0},{sub 3380}Ti{sub 0},{sub 3120})O{sub 3}), 0,75PZT-0,25PMN ((Pb(Mg{sub 0},{sub 083}Nb{sub 0}.{sub 1675}Zr{sub 0},{sub 3900}Ti{sub 0},{sub 3600})O3) and the 0,85PZT-0,15PMN ((Pb(Mg{sub 0,0500}Nb{sub 0},{sub 1000}Zr{sub 0},{sub 4420}Ti{sub 0},{sub 4080})O{sub 3}). The influence of the calcination and concentration of PZT on the lattice phases, microstructure and density was evaluated. Then, the method used was the mixed-oxide method, the samples were taken under different temperatures of calcination before the final sinterizing. The DRX and SEM techniques were used to identify the phases formed and analyse the microstructure, respectively. The main result revealed that, the better way is to realize three burns before the final sinterizing at 1200 o C/4 h . Like that, on obtain for sure the average lattice phases, like: perovskite, pyrochlore and PbO and also tend to densify the samples. (author)

  20. Excitation and reception of pure shear horizontal waves by using face-shear d24 mode piezoelectric wafers

    Science.gov (United States)

    Miao, Hongchen; Huan, Qiang; Li, Faxin

    2016-11-01

    The fundamental shear horizontal (SH0) wave in plate-like structures is of great importance in non-destructive testing (NDT) and structural health monitoring (SHM) as it is non-dispersive, while excitation or reception of SH0 waves using piezoelectrics is always a challenge. In this work, we firstly demonstrate via finite element simulations that face-shear piezoelectrics is superior to thickness-shear piezoelectrics in driving SH waves. Next, by using a newly defined face-shear d24 PZT wafer as an actuator and face-shear d36 PMN-PT wafers as sensors, pure SH0 wave was successfully excited in an aluminum plate from 130 to 180 kHz. Then, it was shown that the face-shear d24 PZT wafer could receive the SH0 wave only and filter the Lamb waves over a wide frequency range (120-230 kHz). The directionality of the excited SH0 wave was also investigated using face-shear d24 PZT wafers as both actuators and sensors. Results show that pure SH0 wave can be excited symmetrically along two orthogonal directions (0° and 90°) and the amplitude of the excited SH0 wave can keep over 90% of the maximum amplitude when the deviate angle is within 30°. This work could greatly promote the applications of SH0 wave in NDT and SHM.

  1. Using microwave for processing nanostructured PZT ceramics; Utilizacao de microondas no processamento de ceramicas nanoestruturadas de PZT

    Energy Technology Data Exchange (ETDEWEB)

    Lanza, A.C.; Berti, T.G.; Thomazini, D.; Gelfuso, M.V., E-mail: lanza.work@gmail.com [Universidade Federal de Itajuba (UNIFEI), MG (Brazil). Instituto de Engenharia Mecanica; Eiras, J.A. [Universidade Federal de Sao Carlos (UFSCar), SP (Brazil). Dept. de Fisica

    2012-07-01

    The PZT ceramics have dielectric and piezoelectric properties of technological interest. The method of microwave assisted hydrothermal synthesis becomes interesting since it occurs in a closed environment, the low temperature and time, compared to conventional methods. In this work, PZT powders were dissolved in acid medium, and by adjusting the pH of the solutions obtained were precipitated, subjected to hydrothermal treatment at 120 °C for intervals of 15, 30 and 60 min. The powders were characterized by differential thermal and gravimetric analysis, X-ray diffraction and scanning electron microscopy. The results confirm the formation of PZT phase in one hour with particle size around 55 nm, showing the feasibility of the proposed method. (author)

  2. Thickness-dependent phase boundary in Sm-doped BiFeO3 piezoelectric thin films on Pt/Ti/SiO2/Si substrates.

    Science.gov (United States)

    Sun, Wei; Li, Jing-Feng; Zhu, Fangyuan; Yu, Qi; Cheng, Li-Qian; Zhou, Zhen

    2015-08-14

    Sm-doped BiFeO3 thin films were fabricated on platinized silicon substrates via a sol-gel method. Sm contents and thicknesses were varied in a wide range to investigate their effects on the phase structure and piezoelectricity. X-ray diffraction and Raman spectroscopy experiments revealed a rhombohedral to orthorhombic phase transition and the co-existence of both phases in a certain compositional vicinity. It is found that the proportion of a rhombohedral phase increased with film thickness at the compositions corresponding to the phase transition boundary, indicating the influence of the film thickness on the phase structure. The phase transition phenomenon and film thickness effect on the boundary were also studied by piezoresponse force microscopy. Based on the structure analysis and piezoelectric characterization results, a phase diagram of thickness versus composition was proposed, in which the morphotropic phase boundary was located at 9% to 11% in thinner Sm-doped films and shifted towards the Sm-rich side with increasing thickness.

  3. Bending strength of piezoelectric ceramics and single crystals for multifunctional load-bearing applications.

    Science.gov (United States)

    Anton, Steven R; Erturk, Alper; Inman, Daniel

    2012-06-01

    The topic of multifunctional material systems using active or smart materials has recently gained attention in the research community. Multifunctional piezoelectric systems present the ability to combine multiple functions into a single active piezoelectric element, namely, combining sensing, actuation, or energy conversion ability with load-bearing capacity. Quantification of the bending strength of various piezoelectric materials is, therefore, critical in the development of load-bearing piezoelectric systems. Three-point bend tests are carried out on a variety of piezoelectric ceramics including soft monolithic piezoceramics (PZT-5A and PZT-5H), hard monolithic ceramics (PZT-4 and PZT-8), single-crystal piezoelectrics (PMN-PT and PMN-PZT), and commercially packaged composite devices (which contain active PZT-5A layers). A common 3-point bend test procedure is used throughout the experimental tests. The bending strengths of these materials are found using Euler-Bernoulli beam theory to be 44.9 MPa for PMN-PZT, 60.6 MPa for PMN-PT, 114.8 MPa for PZT- 5H, 123.2 MPa for PZT-4, 127.5 MPa for PZT-8, 140.4 MPa for PZT-5A, and 186.6 MPa for the commercial composite. The high strength of the commercial configuration is a result of the composite structure that allows for shear stresses on the surfaces of the piezoelectric layers, whereas the low strength of the single-crystal materials is due to their unique crystal structure, which allows for rapid propagation of cracks initiating at flaw sites. The experimental bending strength results reported, which are linear estimates without nonlinear ferroelastic considerations, are intended for use in the design of multifunctional piezoelectric systems in which the active device is subjected to bending loads.

  4. Preparation and Properties of Orthogonal Piezoelectric Composite Materials

    Institute of Scientific and Technical Information of China (English)

    Liu Jun; Lu Ying; Zhang Xingguo; Shen Yi; Chen Chun

    2004-01-01

    . PZT piezoelectric ceramic with La2O3, SrCO3, BaO and Sb2O5 was prepared. It has high value of the piezoelectric strain constant d33 ( -681 PC/N) and high value of-d33/d31 (2.65). Orthogonal piezoelectric composite materials was designed and prepared by PZT, DAD- 40 electric conductive adhesive and E51 epoxy resin. The OPCM shows obvious orthogonal anisotropy. The matching property of the interface between piezoelectric ceramic and polymer of OPCM relies on the defects of interface. The proper conductive mid-layer could improve the matching property of the interface.

  5. Powering low-power implants using PZT transducer discs operated in the radial mode

    Science.gov (United States)

    Sanni, Ayodele; Vilches, Antonio

    2013-11-01

    This paper reports experimental results that are used to compare operation characteristics of lead zirconate titanate (PZT) piezoelectric ceramic discs operated in the radial mode. The devices are driven to radially vibrate at their lowest fundamental resonant frequency and thus transmit and receive power when immersed in a liquid phantom. A number of 1 mm × 10 mm (thickness × diameter) PZT discs are characterized experimentally within a propagation tank and results discussed. On the basis of these measured characteristics, a novel application is developed and reported for the first time. This consists of a tuned LC resonator circuit which is used at the receiving disc to maximize sensitivity as well as a Seiko start-up IC S-882Z which is employed to charge a capacitor that drives a PIC microcontroller (μC) once the voltage exceeds 2 V DC. We show that a mean input power of 486 mW RMS results in 976 μW RMS received over a range of 80 mm and that this is sufficient to periodically (every 60 s) power the μC to directly drive a red LED for 5 ms with a current of 4.8 mA/flash. This approach is suitable for low-power, periodically activated analogue bio-implant applications.

  6. Thick Films acoustic sensors devoted to MTR environment measurements. Thick Films acoustic sensors devoted to Material Testing Reactor environment measurements

    Energy Technology Data Exchange (ETDEWEB)

    Very, F.; Rosenkrantz, E.; Combette, P.; Ferrandis, J.Y. [University Montpellier, IES, UMR 5214, F-34000, Montpellier (France); CNRS, IES, UMR 5214, F-34000, Montpellier (France); Fourmentel, D.; Destouches, C.; Villard, J.F. [CEA, DEN, Instrumentation Sensors and Dosimetry Laboratory, Cadarache, F-13108 St Paul lez Durance (France)

    2015-07-01

    The development of advanced instrumentation for in-pile experiments in Material Testing Reactor constitutes a main goal for the improvement of the nuclear fuel behavior knowledge. An acoustic method for fission gas release detection was tested with success during a first experiment called REMORA 3 in 2010 and 2011, and the results were used to differentiate helium and fission gas release kinetics under transient operating conditions. This experiment was lead at OSIRIS reactor (CEA Saclay, France). The maximal temperature on the sensor during the irradiation was about 150 deg. C. In this paper we present a thick film transducer produce by screen printing process. The screen printing of piezoelectric offers a wide range of possible applications for the development of acoustic sensors and piezoelectric structure for measurements in high temperature environment. We firstly produced a Lead Zirconate Titanate (PZT) based paste composed of Pz27 powder from Ferroperm, CF7575 glass, and organic solvent ESL 400. Likewise a Bismuth Titanate based paste synthesized in our laboratory was produced. With these inks we produced thick film up to 130 μm by screen printing process. Material properties characterizations of these thick-film resonators are essential for device design and applications. The piezoelectric coefficients d33 and pyro-electric P(T) coefficient are investigated. The highest P(T) and d33 are respectively 80 μC.m{sup -2}.K{sup -1} and 130 μC.N{sup -1} for the PZT transducer -which validates the fabrication process-. In view of the development of this transducer oriented for high temperature and irradiation environment, we investigated the electrical properties of the transducers for different ranges of frequencies and temperature - from 20 Hz up to 40 MHz between 30 and 400 deg. C. We highlight the evolution of the impedance response and piezoelectric parameters of screen printed piezoelectric structures on alumina. Shortly an irradiation will be realized in

  7. Zr含量对大功率0.125PMN-0.875PZT陶瓷压电性能的影响%Effects of Zr content on piezoelectric properties of 0.125PMN-0.875PZT high power ceramics

    Institute of Scientific and Technical Information of China (English)

    葛宏桂; 刘云飞; 吕忆农; 周怀娟

    2012-01-01

    The 0. 125Pb(Mg1/2 Nb2/3)O_3 -0. 875PbZrxTi1-xO3(0. 125PMN -0. 875PZT) ternary piezoelectric ceramics with different Zr contents ( x = 0. 46 ~ 0. 52 ) were prepared by the two-step solid-state reaction. The sintering,structural and electrical properties of 0. 125PMN-0. 875PZT ceramics with zirconium content were investigated by X-ray diffractmeter ( XRD) and impedance analysis meter. The results indicated that 0. 125PMN-0. 875 PZT ceramics had a single perovskite structure by the two-step synthesis method, and there was a tetragonal-rhombohedral morphotropic phase boundary ( MPB ) with x = 0. 48 ~ 0. 50, and the excellent properties were optimal at x = 0. 49: the bulk density was 7. 84 g/cm3, dielectric loss (tanδ) was 0.76% ,relative dielectric constant (εr) was 2 130, piezoelectric constant (d33) was 320 pC/N, electromechanical coupling coefficient ( Kp ) was 0. 61, and mechanical quality factor ( Qm) was 76.%采用二次合成法制备不同Zr含量(x=0.46~0.52)的0.125Pb(Mg1/3 Nb2/3)O3 -0.875PbZLTi1-xO3(0.125PMN -0.875PZT)三元压电陶瓷.采用X线衍射仪(XRD)、阻抗分析仪等对陶瓷进行表征和性能测试,考察了Zr含量变化对陶瓷烧结相结构、体积密度、介电和压电性能的影响.结果表明:采用二次合成法,制备了纯钙钛矿相结构的陶瓷;当x=0.48~0.50时,0.125PMN -0.875PZT陶瓷处于四方-三方准同型相界(MPB),在x=0.49时制备的0.125PMN -0.875PZT陶瓷性能最佳,体积密度为7.84 g/cm3,介电损耗低至0.76%,相对介电常数为2 130,压电常数为320 pC/N,机电耦合系数达0.61,机械品质因数为76.

  8. Characteristic analysis of diaphragm-type transducer that is thick relative to its size

    Science.gov (United States)

    Ishiguro, Yuya; Zhu, Jing; Tagawa, Norio; Okubo, Tsuyoshi; Okubo, Kan

    2017-07-01

    In recent years, high-performance piezoelectric micromachined ultrasonic transducers (PMUTs) have been fabricated by micro electro mechanical systems (MEMS) technology. For high-resolution imaging, it is important to broaden the frequency bandwidth. By reducing the diaphragm size to increase the resonance frequency, the film thickness becomes relatively larger and hence the transmitting and receiving characteristics may different from those of a usual thin diaphragm. In this study, we examine the performance of a square-diaphragm-type lead zirconate titanate (PZT) transducer through simulations. To realize the desired resonance frequency of 20 MHz, firstly, the diaphragm size and the thickness of the layers of PZT and Si constituting a PMUT are examined, and then, three PZT/Si models with different thicknesses are selected. Subsequently, using the models, we analyze the transmitting efficiency, transmitting bandwidth, receiving sensitivity (piezoelectric voltage/electric charge), and receiving bandwidth using an FEM simulator. It is found that the proposed models can transmit ultrasound independently of the diaphragm vibration and have wide bandwidth of the receiving frequency as compared with that of a typical PMUT.

  9. Theory and operation of 2-D array piezoelectric micromachined ultrasound transducers.

    Science.gov (United States)

    Dausch, David E; Castellucci, John B; Chou, Derrick R; von Ramm, Olaf T

    2008-11-01

    Piezoelectric micromachined ultrasound transducers (pMUTs) are a new approach for the construction of 2-D arrays for forward-looking 3-D intravascular (IVUS) and intracardiac (ICE) imaging. Two-dimensional pMUT test arrays containing 25 elements (5 x 5 arrays) were bulk micromachined in silicon substrates. The devices consisted of lead zirconate titanate (PZT) thin film membranes formed by deep reactive ion etching of the silicon substrate. Element widths ranged from 50 to 200 microm with pitch from 100 to 300 mum. Acoustic transmit properties were measured in de-ionized water with a calibrated hydrophone placed at a range of 20 mm. Measured transmit frequencies for the pMUT elements ranged from 4 to 13 MHz, and mode of vibration differed for the various element sizes. Element capacitance varied from 30 to over 400 pF depending on element size and PZT thickness. Smaller element sizes generally produced higher acoustic transmit output as well as higher frequency than larger elements. Thicker PZT layers also produced higher transmit output per unit electric field applied. Due to flexure mode operation above the PZT coercive voltage, transmit output increased nonlinearly with increased drive voltage. The pMUT arrays were attached directly to the Duke University T5 Phased Array Scanner to produce real-time pulse-echo B-mode images with the 2-D pMUT arrays.

  10. Controllable piezoelectricity of Pb(Zr0.2Ti0.8)O3 film via in situ misfit strain

    Science.gov (United States)

    Lee, Hyeon Jun; Guo, Er-Jia; Kwak, Jeong Hun; Hwang, Seung Hyun; Dörr, Kathrin; Lee, Jun Hee; Young Jo, Ji

    2017-01-01

    The tetragonality (c/a) of a PbZr0.2Ti0.8O3 (PZT) thin film on La0.7Sr0.3MnO3/ 0.72Pb(Mg1/3Nb2/3)O3-0.28PbTiO3 (PMN-PT) substrates was controlled by applying an electric field on the PMN-PT substrate. The piezoelectric response of the PZT thin film under various biaxial strains was observed using time-resolved micro X-ray diffraction. The longitudinal piezoelectric coefficient (d33) was reduced from 29.5 to 14.9 pm/V when the c/a ratio of the PZT film slightly changed from 1.051 to 1.056. Our results demonstrate that the tetragonality of the PZT thin film plays a critical role in determining d33, and in situ strain engineering using electromechanical substrate is useful in excluding the extrinsic effect resulting from the variation in the film thickness or the interface between substrate.

  11. Flexible PET/Al/PZT/Al/PET multi-layered composite for low frequency energy harvesting

    Science.gov (United States)

    Seveno, R.; Carbajo, J.; Dufay, T.; Guiffard, B.; Thomas, J. C.

    2017-04-01

    A flexible piezoelectric device has been realized by depositing lead zirconate titanate (PZT) thin films by chemical solution deposition (CSD) onto very thin aluminium foil (16 µm) and using a polyethylene terephthalate (PET) laminated film (150 µm) as encapsulation. A ruthenium dioxide layer has been used in order to enhance the quality of the PZT/Al interface, improving the dielectric, ferroelectric and piezoelectric properties of the PZT film. The obtained piezoelectric generators have been subjected to large bending motions at low frequencies ranging from 0.1 to 8 Hz and the experimental values of the output voltage, output current and harvested power have been compared to the theoretical values (derived from the electrokinetic model of the piezoelectric material) with very good agreement. Due to the increase of the permittivity of the PZT film by the use of RuO2 interlayer, a moderate decrease of the harvested power at the optimal load resistance is found (from 185 nW to 143 nW at 4.4 Hz), despite the enhancement of the piezoelectric properties. This type of very flexible film, able to withstand a small radius of curvature (1 cm), may yield a promising avenue in the field of low frequency mechanical energy harvesting.

  12. Analysis of Cymbal piezoelectric generator's effective piezoelectric strain constant%Cymbal型压电发电装置等效压电常数分析

    Institute of Scientific and Technical Information of China (English)

    郭帅; 郭吉丰

    2012-01-01

    压电发电工作于低频时所收集的能量与其等效压电常数和等效电压常数的乘积成正比.为了研究Cymbal型压电发电装置的等效压电常数,建立了Cymbal型压电发电装置的三维有限元分析模型,并分析得出了等效压电常数计算公式;详细地分析了Cymbal型发电装置中金属帽的材料和厚度、金属腔底端直径和顶端直径、金属腔高度、压电陶瓷片厚度等因素对等效压电常数的影响,并给出了等效压电常数的优化准则.试验结果表明,经优化后可获得的等效压电常数大约相当于压电陶瓷本身的60倍.%The harvesting energy of piezoelectric generator is proportional to the product of effective piezoelectric strain constant and effective piezoelectric voltage constant at low frequency. In order to study the effective piezoelectric strain constant of the cymbal piezoelectric generator,the 3D finite element analysis (FEA) model of the generator was established, and effective piezoelectric strain constant calculation formula was also given. Besides, the influences of the metal cap material type, the metal cap thickness, the metal cavity bottom diameter, the cavity top diameter, metal cavity height and the PZT thickness on the effective piezoelectric strain constant of cymbal piezoelectric generator were analyzed, and some optimization criterions were given. Results indicate that the obtained effective piezoelectric strain constant is about as 60 times as that of PZT itself.

  13. Fabrication and comparison of PMN-PT single crystal, PZT and PZT-based 1-3 composite ultrasonic transducers for NDE applications.

    Science.gov (United States)

    Kim, Ki-Bok; Hsu, David K; Ahn, Bongyoung; Kim, Young-Gil; Barnard, Daniel J

    2010-08-01

    This paper describes fabrication and comparison of PMN-PT single crystal, PZT, and PZT-based 1-3 composite ultrasonic transducers for NDE applications. As a front matching layer between test material (Austenite stainless steel, SUS316) and piezoelectric materials, alumina ceramics was selected. The appropriate acoustic impedance of the backing materials for each transducer was determined based on the results of KLM model simulation. Prototype ultrasonic transducers with the center frequencies of approximately 2.25 and 5MHz for contact measurement were fabricated and compared to each other. The PMN-PT single crystal ultrasonic transducer shows considerably improved performance in sensitivity over the PZT and PZT-based 1-3 composite ultrasonic transducers.

  14. Sensitivity of PZT Impedance Sensors for Damage Detection of Concrete Structures

    Directory of Open Access Journals (Sweden)

    Yong Lu

    2008-01-01

    Full Text Available Piezoelectric ceramic Lead Zirconate Titanate (PZT based electro-mechanicalimpedance (EMI technique for structural health monitoring (SHM has been successfullyapplied to various engineering systems. However, fundamental research work on thesensitivity of the PZT impedance sensors for damage detection is still in need. In thetraditional EMI method, the PZT electro-mechanical (EM admittance (inverse of theimpedance is used as damage indicator, which is difficult to specify the effect of damage onstructural properties. This paper uses the structural mechanical impedance (SMI extractedfrom the PZT EM admittance signature as the damage indicator. A comparison study on thesensitivity of the EM admittance and the structural mechanical impedance to the damages ina concrete structure is conducted. Results show that the SMI is more sensitive to the damagethan the EM admittance thus a better indicator for damage detection. Furthermore, this paperproposes a dynamic system consisting of a number of single-degree-of-freedom elementswith mass, spring and damper components to model the SMI. A genetic algorithm isemployed to search for the optimal value of the unknown parameters in the dynamic system.An experiment is carried out on a two-storey concrete frame subjected to base vibrations thatsimulate earthquake. A number of PZT sensors are regularly arrayed and bonded to the framestructure to acquire PZT EM admittance signatures. The relationship between the damageindex and the distance of the PZT sensor from the damage is studied. Consequently, thesensitivity of the PZT sensors is discussed and their sensing region in concrete is derived.

  15. Resonant efficiency improvement design of piezoelectric biosensor for bacteria gravimetric sensing.

    Science.gov (United States)

    Tsai, Jang-Zern; Chen, Ching-Jung; Shie, Dung-Ting; Liu, Jen-Tsai

    2014-01-01

    The piezoelectric biosensor have been widely used in ultra-small mass detection of biomolecular, based on PZT piezoelectric material can create a variety of compositions geometrically; it could widely develop a high-frequency resonator and measure the change of the slightest mass while improve the limited detection simultaneously. Therefore, the piezoelectric biosensor of this study was fabricated by a spin-coating method and backside etching process for improving the characteristic of piezoelectric biosensor. The result exhibited that the 250 μm × 250 μm working size has the most favorable piezoelectric characteristic. The tunability was approximately 38.56 % and it showed that reducing the substrate thickness could obtain a clear resonance signal in a range of 60 to 380 MHz. In theory calculated for gravimetric sensing, it could achieve 0.1 ng sensing sensitivity. In gravimetric sensing, the sensing range was between 50,000~100,000 CFU/ml. Sensing range was lower in clinical urinary tract infection (100,000 CFU/ml), thus demonstrating its usefulness for preventive medicine. It can understand the piezoelectric sensor of this study has potential application in the future for biomedical gravimetric sensing.

  16. Effect of various shapes and materials on the generated power for piezoelectric energy harvesting system

    Science.gov (United States)

    Kaur, Sarabjeet; Graak, Pinki; Gupta, Ankita; Chhabra, Priya; Kumar, Dinesh; Shetty, Arjun

    2016-04-01

    Piezoelectric energy harvesting systems are used to convert vicinity vibrations into useful electrical energy. Effect of various shapes and materials open the gateway towards the choice of maximum power generation for the micro and nano world. Comsol Multiphysics was used to simulate the four designed shapes named as Pi, E, Rectangular and T in the size range of less than 1mm but greater than 1 micron. Designed shapes worked under the impact of ambient vibrations using few piezoelectric materials for the maximum power generation so that traditional power sources can be replaced with such piezoelectric energy harvester. A layer of piezoelectric material (PZT-5H, AlN, BaTiO3) of thickness 0.5 µm is added to the cantilever and the base material is silicon of thickness 1.5 µm. Simulations were performed using the piezoelectric device module of Comsol Multiphysics. All three materials were studied for the all four cantilever geometries. The generated power was observed maximum as 382.5 µW in case of the barium titanate material with rectangular shape geometry but the displacement is 0.132 µm which is very less whereas E shape cantilever shows the maximum displacement of 0.6078 µm in case of PZT-5H, Hence rectangular shape with barium titanate material is concluded to be good for maximum power generation but the displacement factor cannot be neglected, hence the cantilever with E shape geometry is considered as the best with a generated power of 49.005 µW and a displacement of 0.6078 µm.

  17. Effects of substrate materials on piezoelectric properties of BaTiO3 thick films deposited by aerosol deposition

    Science.gov (United States)

    Kawakami, Yoshihiro; Watanabe, Masato; Arai, Ken-Ichi; Sugimoto, Satoshi

    2016-10-01

    Piezoelectric properties were evaluated for annealed BaTiO3 (BT) films formed by aerosol deposition on yttria-stabilized zirconia (YSZ) and Fe-Cr-Al-based heat-resistant stainless steel (SS). The piezoelectric constants d 31 of BT films annealed at 1200 °C formed on YSZ and SS were -71 and -41 pm/V, respectively. The effects of different substrates on piezoelectric properties were investigated. The grain sizes of the films formed on YSZ and SS were 1.5 and 1.0 µm, respectively. X-ray diffraction analysis using a two-dimensional stress method revealed that the respective residual stresses of the films formed on YSZ and SS were -55 ± 8 and -32 ± 7 MPa, respectively, as compressive stresses. The c-domain structure was formed preferentially in the films on SS because of its larger compressive stress. These results suggest that differences in piezoelectric properties attributable to substrates result from differences in compressive stress magnitude and the volume fraction between the c- and a-domains.

  18. Research on the equivalent circuit model of a circular flexural-vibration-research on the equivalent circuit model of a circular flexural-vibration-mode piezoelectric transformer with moderate thickness.

    Science.gov (United States)

    Huang, Yihua; Huang, Wenjin; Wang, Qinglei; Su, Xujian

    2013-07-01

    The equivalent circuit model of a piezoelectric transformer is useful in designing and optimizing the related driving circuits. Based on previous work, an equivalent circuit model for a circular flexural-vibration-mode piezoelectric transformer with moderate thickness is proposed and validated by finite element analysis. The input impedance, voltage gain, and efficiency of the transformer are determined through computation. The basic behaviors of the transformer are shown by numerical results.

  19. Influence of the stress on magnetoelectric effect in magnetostrictive-PZT bilayers

    Institute of Scientific and Technical Information of China (English)

    DING Jian-ming; ZHONG Chong-gui; JIANG Qing

    2007-01-01

    In this letter,we investigate the influence of the stress on magnetoelectric(ME)effect in a magnetostrictivePZT bilayer.ME voltage coefficient α*E=δE/δH,where δE is the induced electric field for an applied alternating current (ac)magnetic field δH,is obtained by solving the stressrelated piezoelectric constitutive equation and the conventional magnetostrictive equation with appropriate boundary condition.Based on the free-energy density function of the PZT film in stress state,we get the stress-related piezoelectric charge coefficient Pd*31 and dielectric permittivity Pε*33.After taking the cobalt ferrite(CFO)as magnetostrictive phase,it is found that α*E increases with decreasing 2-d compressive stress for CFO-PZT,which not only is qualitatively consistent with previous experimental measurements,but also provides a possible route to improve the ME effect.

  20. Effect of sintering temperature and composition on microstructure and properties of PMS-PZT ceramics

    Institute of Scientific and Technical Information of China (English)

    DU Hong-liang; PEI Zhi-bin; LI Zhi-min; LUO Fa; ZHU Dong-mei; ZHOU Wan-cheng; QU Shao-bo

    2006-01-01

    The piezoelectric ceramics xPb(Mn1/3Sb2/3)O3-(1-x)Pb(Zr1/2Ti1/2)O3 (abbreviated as PMS-PZT) were synthesized by traditional ceramics process. The effect of sintering temperature and the amount of Pb(Mn1/3Sb2/3)O3 (abbreviated as PMS) on phase structure,microstructure,piezoelectric and dielectric properties of PMS-PZT ceramics was investigated. The results show that the pure perovskite phase is in all ceramics specimens,the phase structure of PMS-PZT ceramics changes from tetragonal phase to single rhombohedral phase with the increasing amount of PMS. The dielectric constant -r,Curie temperature TC,electromechanical coupling factor kp and piezoelectric constant d33 decrease,whereas the mechanical quality factor Qm and dielectric loss tanδ increase with the increasing amount of PMS in system. The optimum sintering temperature is 1 200-1 250 ℃. It is concluded that the PMS-PZT (x=0.07) ceramics sintered at 1 250 ℃ is suitable for high-power piezoelectric transformer. These properties include -r=674.8,tanδ=0.005 25,kp=0.658,Qm1520,d33=230 pC/N,Tc=275 ℃.

  1. High Quality Factor Silicon Cantilever Driven by PZT Actuator for Resonant Based Mass Detection

    CERN Document Server

    Lu, Jian; Zhang, Yi; Mihara, Takashi; Itoh, Toshihiro; Maeda, Ryutaro

    2008-01-01

    A high quality factor (Q-factor) piezoelectric lead zirconat titanate (PZT) actuated single crystal silicon cantilever was proposed in this paper for resonant based ultra-sensitive mass detection. Energy dissipation from intrinsic mechanical loss of the PZT film was successfully compressed by separating the PZT actuator from resonant structure. Excellent Q-factor, which is several times larger than conventional PZT cantilever, was achieved under both atmospheric pressure and reduced pressures. For a 30 micrometer-wide 100 micrometer-long cantilever, Q-factor was measured as high as 1113 and 7279 under the pressure of 101.2 KPa and 35 Pa, respectively. Moreover, it was found that high-mode vibration can be realized by the cantilever for the pursuit of great Q-factor, while support loss became significant because of the increased vibration amplitude at the actuation point. An optimized structure using node-point actuation was suggested then to suppress corresponding energy dissipation.

  2. Characterization of PZT/PVC Composites Added with Carbon Black

    Institute of Scientific and Technical Information of China (English)

    LIU Xiaofang; XIONG Chuanxi; SUN Huajun; DONG Lijie; LI Rui; LIU Yang

    2005-01-01

    A new three-phase PZT/ C/ PVC composite comprising PZT (50vol%), nanocrystalline PVC (50 vol% ) and a small volume fraction f of carbon black (C) was prepared by the hot-pressing technique. The dielectric property of the composite as a function of the frequency and the dielectric and piezoelectric properties as a function of the volume fraction f of C were studied. The measured dielectric property demonstrates that a percolation transition occurs in the three-phase composites as in normal two-phase metal-insulator continuum media. The dielectric constant varies slightly with f at f < 0.1 and increases rapidly when f is close to the percolation threshold at 1 kHz. The optimum properties were obtained for f = 0.5 before the percolation threshold in the PZT/ C/ PVC (50/f/(50 - f) vol% ) composite with its d33 (20 pC/N) being 50% higher than that of the PZT/ PVC (50/50vol% ), and its g33(47.23 × 10-3 Vm/N) and Kp (0.25) much higher than the earlier reported values.XRD patterns and P-E hysteresis loops were used to interpret the experimental results.

  3. Effect of External Vibration on PZT Impedance Signature.

    Science.gov (United States)

    Yang, Yaowen; Miao, Aiwei

    2008-11-01

    Piezoelectric ceramic Lead Zirconate Titanate (PZT) transducers, working on the principle of electromechanical impedance (EMI), are increasingly applied for structural health monitoring (SHM) in aerospace, civil and mechanical engineering. The PZT transducers are usually surface bonded to or embedded in a structure and subjected to actuation so as to interrogate the structure at the desired frequency range. The interrogation results in the electromechanical admittance (inverse of EMI) signatures which can be used to estimate the structural health or integrity according to the changes of the signatures. In the existing EMI method, the monitored structure is only excited by the PZT transducers for the interrogating of EMI signature, while the vibration of the structure caused by the external excitations other than the PZT actuation is not considered. However, many structures work under vibrations in practice. To monitor such structures, issues related to the effects of vibration on the EMI signature need to be addressed because these effects may lead to misinterpretation of the structural health. This paper develops an EMI model for beam structures, which takes into account the effect of beam vibration caused by the external excitations. An experimental study is carried out to verify the theoretical model. A lab size specimen with different external excitations is tested and the effect of vibration on EMI signature is discussed.

  4. Effect of External Vibration on PZT Impedance Signature

    Directory of Open Access Journals (Sweden)

    Yaowen Yang

    2008-11-01

    Full Text Available Piezoelectric ceramic Lead Zirconate Titanate (PZT transducers, working on the principle of electromechanical impedance (EMI, are increasingly applied for structural health monitoring (SHM in aerospace, civil and mechanical engineering. The PZT transducers are usually surface bonded to or embedded in a structure and subjected to actuation so as to interrogate the structure at the desired frequency range. The interrogation results in the electromechanical admittance (inverse of EMI signatures which can be used to estimate the structural health or integrity according to the changes of the signatures. In the existing EMI method, the monitored structure is only excited by the PZT transducers for the interrogating of EMI signature, while the vibration of the structure caused by the external excitations other than the PZT actuation is not considered. However, many structures work under vibrations in practice. To monitor such structures, issues related to the effects of vibration on the EMI signature need to be addressed because these effects may lead to misinterpretation of the structural health. This paper develops an EMI model for beam structures, which takes into account the effect of beam vibration caused by the external excitations. An experimental study is carried out to verify the theoretical model. A lab size specimen with different external excitations is tested and the effect of vibration on EMI signature is discussed.

  5. Micromachined bulk PZT tissue contrast sensor for fine needle aspiration biopsy.

    Science.gov (United States)

    Li, Tao; Gianchandani, Roma Y; Gianchandani, Yogesh B

    2007-02-01

    This paper describes a micromachined piezoelectric sensor, integrated into a cavity at the tip of a biopsy needle, and preliminary experiments to determine if such a device can be used for real-time tissue differentiation, which is needed for needle positioning guidance during fine needle aspiration (FNA) biopsy. The sensor is fabricated from bulk lead zirconate titanate (PZT), using a customized process in which micro electro-discharge machining is used to form a steel tool that is subsequently used for batch-mode ultrasonic micromachining of bulk PZT ceramic. The resulting sensor is 50 microm thick and 200 microm in diameter. It is placed in the biopsy needle cavity, against a steel diaphragm which is 300 microm diameter and has an average thickness of 23 microm. Devices were tested in materials that mimic the ultrasound characteristics of human tissue, used in the training of physicians, and with porcine fat and muscle tissue. In both schemes, the magnitude and frequency of an electrical impedance resonance peak showed tissue-specific characteristics as the needle was inserted. For example, in the porcine tissue, the impedance peak frequency changed approximately 13 MHz from the initial 163 MHz, and the magnitude changed approximately 1600 Omega from the initial 2100 Omega, as the needle moved from fat to muscle. Samples including oils and saline solution were tested for calibration, and an empirical tissue contrast model shows an approximately proportional relationship between measured frequency shift and sample acoustic impedance. These results suggest that the device can complement existing methods for guidance during biopsies.

  6. A study on (K, Na) NbO3 based multilayer piezoelectric ceramics micro speaker

    Science.gov (United States)

    Gao, Renlong; Chu, Xiangcheng; Huan, Yu; Sun, Yiming; Liu, Jiayi; Wang, Xiaohui; Li, Longtu

    2014-10-01

    A flat panel micro speaker was fabricated from (K, Na) NbO3 (KNN)-based multilayer piezoelectric ceramics by a tape casting and cofiring process using Ag-Pd alloys as an inner electrode. The interface between ceramic and electrode was investigated by scanning electron microscope (SEM) and transmission electron microscope (TEM). The acoustic response was characterized by a standard audio test system. We found that the micro speaker with dimensions of 23 × 27 × 0.6 mm3, using three layers of 30 μm thickness KNN-based ceramic, has a high average sound pressure level (SPL) of 87 dB, between 100 Hz-20 kHz under five voltage. This result was even better than that of lead zirconate titanate (PZT)-based ceramics under the same conditions. The experimental results show that the KNN-based multilayer ceramics could be used as lead free piezoelectric micro speakers.

  7. An improved small-deflection electromechanical model for piezoelectric bending beam actuators and energy harvesters

    Science.gov (United States)

    Tabesh, Ahmadreza; Fréchette, Luc G.

    2008-10-01

    The analytical model presented in this paper describes the energy conversion mechanism of a piezoelectric beam (bimorph) under small-deflection static and vibrating conditions. The model provides an improved approach to design and analyze the performance of piezoelectric actuators and energy harvesters (sensors). Conventional models assume a linear voltage distribution over the piezoelectric beam thickness, which is shown here to be invalid. The proposed modeling method improves accuracy by using a quadratic voltage distribution. The equivalent capacitance of a beam shows a 40% discrepancy between a conventional model and the proposed model for PZT5A material. This inaccuracy level is not negligible, especially when the design of micro-power electrical energy harvesting is concerned. The method solves simultaneously the solid mechanics and Maxwell's equations with the constitutive equations for piezoelectric materials. The paper also proposes a phasor-based procedure for measuring the damping of a piezoelectric beam. An experimental setup is developed to verify the validity of the model. The experimental results confirm the accuracy of the improved model and also reveal limitations in using models for small deflections.

  8. Piezoelectric Energy Harvesting for Roadways

    OpenAIRE

    Xiong, Haocheng

    2015-01-01

    Energy harvesting technologies have drawn much attention as an alternative power source of roadway accessories in different scales. Piezoelectric energy harvesting consisting of PZT piezoceramic disks sealed in a protective package is developed in this work to harness the deformation energy of pavement induced by traveling vehicles and generate electrical energy. Six energy harvesters are fabricated and installed at the weigh station on I-81 at Troutville, VA to perform on-site evaluation. T...

  9. Properties of RF-Sputtered PZT Thin Films with Ti/Pt Electrodes

    Directory of Open Access Journals (Sweden)

    Cui Yan

    2014-01-01

    Full Text Available Effect of annealing temperature and thin film thickness on properties of Pb(Zr0.53Ti0.47O3 (PZT thin film deposited via radiofrequency magnetron sputtering technique onto Pt/Ti/SiO2/Si substrate was investigated. Average grain sizes of the PZT thin film were measured by atomic force microscope; their preferred orientation was studied through X-ray diffraction analysis. Average residual stress in the thin film was estimated according to the optimized Stoney formula, and impedance spectroscopy characterization was performed via an intelligent LCR measuring instrument. Average grain sizes of PZT thin films were 60 nm~90 nm and their average roughness was less than 2 nm. According to X-ray diffraction analysis, 600°C is the optimal annealing temperature to obtain the PZT thin film with better crystallization. Average residual stress showed that thermal mismatch was the decisive factor of residual stress in Pt/Ti/SiO2/Si substrate; the residual stress in PZT thin film decreased as their thickness increased and increased with annealing temperature. The dielectric constant and loss angle tangent were extremely increased with the thickness of PZT thin films. The capacitance of the device can be adjusted according to the thickness of PZT thin films.

  10. A biaxial PZT optical scanner for pico-projector applications

    Science.gov (United States)

    Ikegami, K.; Koyama, T.; Saito, T.; Yasuda, Y.; Toshiyoshi, H.

    2015-02-01

    We report a newly developed two-dimensional MEMS optical scanner based on the ADRIP (Arc Discharge Reactive Ion-Plating) deposited piezoelectric PZT film of typical 4 μm. A circular mirror of 1.2 mm in diameter is suspended within a pair of resonant mechanism that oscillates at 25 kHz for ±12° mechanical angle with a typical voltage of 10 V. A gimbal plate including the mirror is supported with another pair of meandering suspensions to tilt the plate in the orthogonal direction at 60 Hz for the off-resonant vertical motion of ±8° mechanical. Overall power consumption of the piezoelectric actuation was 100 mW or less. As a mechanical reinforce, a rib-structure was designed on the backside of the mirror by using a structural optimization tool TOSCA to suppress the dynamic curvature to 100 nm or less. A piezoelectric sensor was also integrated in the identical PZT film after optimizing the electrode shape to pick up the mechanical angle of the scanner and to give a trigger signal to the control system. A plug-in type pico-projector optics and electronics has been assembled in a 7.5 cm × 12 cm × 5 cm volume with RGB lasers to demonstrate a HD (high definition) class image projection of 720 horizontal lines. The fundamental resonance of the entire scanner mechanism was made to be 1 kHz or higher, thereby exhibiting a compatibility with vehicle applications.

  11. Theoretical and experimental investigation of magnetoelectric effect for bending-tension coupled modes in magnetostrictive-piezoelectric layered composites

    Science.gov (United States)

    Hasanyan, D.; Gao, J.; Wang, Y.; Viswan, R.; Li, M.; Shen, Y.; Li, J.; Viehland, D.

    2012-07-01

    In this paper, we discuss a theoretical model with experimental verification for the resonance enhancement of magnetoelectric (ME) interactions at frequencies corresponding to bending-tension oscillations. A dynamic theory of arbitrary laminated magneto-elasto-electric bars was constructed. The model included bending and longitudinal vibration effects for predicting ME coefficients in laminate bar composite structures consisting of magnetostrictive, piezoelectric, and pure elastic layers. The thickness dependence of stress, strain, and magnetic and electric fields within a sample are taken into account, as such the bending deformations should be considered in an applied magnetic or electric field. The frequency dependence of the ME voltage coefficients has obtained by solving electrostatic, magnetostatic, and elastodynamic equations. We consider boundary conditions corresponding to free vibrations at both ends. As a demonstration, our theory for multilayer ME composites was then applied to ferromagnetic-ferroelectric bilayers, specifically Metglas-PZT ones. A theoretical model is presented for static (low-frequency) ME effects in such bilayers. We also performed experiments for these Metglas-PZT bilayers and analyzed the influence of Metglas geometry (length and thickness) and Metglas/PZT volume fraction on the ME coefficient. The frequency dependence of the ME coefficient is also presented for different geometries (length, thickness) of Metglas. The theory shows good agreement with experimental data, even near the resonance frequency.

  12. Performance of PZT based MEMS devices with integrated ZnO electronics

    Science.gov (United States)

    Wallace, Margeaux

    This thesis describes routes to enable increased understanding and performance of lead zirconate titanate-based microelectromechanical systems (MEMS). Emphasis was placed on monolithic integration with interposer electronics, and in understanding the role of mechanical boundary conditions on the ferroelectric/ferroelastic response. Co-processing of ZnO thin film transistors (TFTs) with Pb(Zr0.52 Ti0.48)0.98Nb0.02O3 (PZT)-based piezoelectrics was investigated to assess whether interposer electronics on PZT can serve as a control scheme for large area arrays of sensors or actuators. ZnO TFT processing produced no measured changes in remanent polarization, dielectric constant, loss tangent, or aging rates. The TFT performance also did not degrade when fabricated on top of the PZT, the mobility (> 24 cm/Vs) remaining comparable to TFTs deposited on glass. To show ZnO array integration, a 5x5 array of PZT capacitors on glass was fabricated as a prototype for an adjustable X-ray mirror, where the ZnO TFT were used for row-column addressing of the actuators. 1.5 mum thick sputter deposited PZT on glass patterned with large area (cm2) electrodes had a dielectric constant of >1200, tandelta ˜ 2% and an average remanent polarization >23 muC/cm 2. Photoreactive benzocyclobutene (BCB) electrically isolated the ZnO TFTs from the top electrodes of the piezoelectric. Flex cables were bonded to the wafer using anisotropic conductive film (ACF) to connect the gates (row control) and the drains (column control) in the TFT array to a control box. It was found that when actuating the PZT cells through the TFT array, the glass mirror experienced approximately 1.5 mum of deflection for a 10 V application. Studies on ferroelectric/ferroelastic domain reorientation were also performed on 1.9 mum thick tetragonal {001} oriented PbZr0.3Ti 0.7O3 films doped with 1% Mn. Different mechanical boundary constraints were investigated and domain reorientation was quantified through the intensity

  13. Scaling laws In PZT/Si(001) Thin Films

    Science.gov (United States)

    Ramírez, Juan; Cortes, Alexander; Lopera, Wilson; Gómez, Maria Elena; Prieto, Pedro

    2006-03-01

    Self-affine scaling behavior of ferroelectric Pb(Zr1-xTix)O3 (PZT) thin films grown on Si(001) substrates has been investigated by AFM Atomic Force Microscope. PZT thin films were grown via Rf-sputtering technique at high oxygen pressures and at substrate temperatures 600 ^oC varying the deposition time and keeping all parameters. growth constant. The α-global rough-exponent was founded close to 0.7 indicating a correlated growth. Anomalous scaling behavior was founded in all PZT/Si surfaces. A value of 0.5.for the α-local value was founded. The local value of the roughness exponent is associated to the diffusional process on the first stage growth. Saturation roughness showed oscillation dependence with the PZT-thickness. This dependence can be explained by the mismatch between Si substrate and PZT thin film. These results are corroborated calculating the grain size for all samples. This work was supported by COLCIENCIAS under the Excellence Center for Novel Materials Contract no 0043-2005.

  14. Research into an integrated intelligent structure- A new actuator combining piezoelectric ceramic and electrorheological fluid

    Science.gov (United States)

    Quanlu, Li

    2002-02-01

    The design, preparation, and application of high-performance piezoelectric ceramics, e.g., FD3-PZT and FD4-PZT, then preparation, performance measurement, and applications of composite electrorheological fluids have been studied, respectively. The integrated intelligent structure (i.e., a new actuator) combining the piezoelectric ceramic and the electrorheological fluids, and their applications have been investigated, and emphasis was given to the applications in acoustics and vibration control, etc. as may be noted.

  15. Excitation and reception of single torsional wave T(0,1) mode in pipes using face-shear d24 piezoelectric ring array

    Science.gov (United States)

    Miao, Hongchen; Huan, Qiang; Wang, Qiangzhong; Li, Faxin

    2017-02-01

    Excitation of single fundamental torsional wave T(0, 1) mode is of practical importance in inspecting or monitoring the structural integrity of pipelines, as T(0, 1) wave is the only non-dispersive mode in pipe-like structures. This work presents a piezoelectric ring array to excite and receive single T(0, 1) mode which is made up of a series of equally-spaced face-shear d24 PZT elements around the pipe. Firstly, we proposed that single T(0, 1) mode can be excited by the piezoelectric ring, when the number of d24 PZT elements is slightly greater than n, where F(n, 2) is the highest circumferential order flexural torsional mode within the frequency bandwidth of the drive signal. Then this proposed principle was confirmed by finite element simulations. Later, experimental testing was conducted on a 100 mm outer diameter, 3 mm thick aluminum pipe. Results show that the ring of 24 face-shear d24 PZT elements can suppress all the non-axisymmetric flexural modes at the excitation frequency of 150 kHz so that single T(0, 1) mode is generated. Moreover, such a piezoelectric ring transducer can also filter flexural modes and receive the T(0, 1) mode only at 150 kHz. Note that here the highest circumferential order flexural torsional mode within the frequency bandwidth is F(20, 2), so the experimental results are in good agreement with the proposed principle. The presented ring of face-shear d24 PZT elements is very suitable for severing as the T(0, 1) wave transducer in structural health monitoring system, as it is cost-effective and no external load is required for operation.

  16. Electrical properties and sensing ability of novel piezoelectric ceramic fibers with Pt core

    Science.gov (United States)

    Du, Jianzhou; Qiu, Jinhao; Zhu, Kongjun; Ji, Hongli; Zhao, Huayun

    2012-04-01

    The traditional sintering method was used to sinter the pure and Fe2O3 doped 0.55Pb(Ni0.33Nb0.67)O3-0.45Pb(Zr0.3Ti0.7)O3 (abbreviate as PNN-PZT and PFNN-PZT, respectively) ceramics. The addition of Fe2O3 significantly improved the microstructure and electrical properties. Compared with pure PNN-PZT ceramics, higher dielectric and piezoelectric properties of d31~-390 pC/N, ɛ r ~6298 were obtained for the PFNN-PZT sample sintered at 1175°C for 2 h. Hence, the PFNN-PZT ceramics sample was selected to fabricate piezoelectric ceramic fibers with Pt core (PFC). Both the green fibers and bulk ceramics were sintered at 1150-1225°C for 2 h in a closed crucible, respectively. The effect of sintering temperature on the microstructure and electrical properties of the PFNN-PZT fibers was investigated. The optimal piezoelectric properties are obtained for the sample sintered at 1175°C for 2 h. The relative dielectric constant and piezoelectric constant show peak values of ɛ r~3683, d31~-197.4 pC/N, respectively. The PFC is a new type piezoelectric device, which can be used for sensors or actuators. The results of sensing experiment show that the piezoelectric ceramic fiber with Pt core has high sensitivity for the Lamb waves.

  17. Health monitoring of a continuous rigid frame bridge based on PZT impedance and strain measurements

    Science.gov (United States)

    Zhang, Junbing; Zhu, Hongping; Wang, Dansheng; He, Bo; Zhou, Huaqiang

    2009-07-01

    Critical civil infrastructures such as bridges, dams, and pipelines present a major investment and their safety and security affect the life of citizens and national economic development. So it is very important for engineers and researchers to monitor their integrity while in operation and throughout. In recent years, the piezoelectric-ceramic (PZT) patches, which serve both as impedance sensors and actuators, have been increasingly used for structural health monitoring. This paper presents an impedance-based method, which utilizes the electro-mechanical coupling property of PZT sensors. There are a lot of advantages of this method, such as not based on any physical models, sensitive to tiny damage for its high frequency characteristics. An engineering application of this method for health monitoring of a continuous rigid frame bridge is implemented in this study. Some PZT active sensors are embedded into critical sections of the continuous rigid-frame box beam. The electrical admittances of these distributed PZT sensors are measured when the bridge is constructing or suffering from operational loads. For comparison, strain gauges are arranged in adjacent regions of these PZT sensors to obtain the strains of concrete around them at the same time. Based on the admittance sigatures obtained form PZT sensors and the strain measurements of concrete around them, the health status of the bridge is monitored and evaluated successfully.

  18. Negligible substrate clamping effect on piezoelectric response in (111)-epitaxial tetragonal Pb(Zr, Ti)O{sub 3} films

    Energy Technology Data Exchange (ETDEWEB)

    Yamada, Tomoaki, E-mail: t-yamada@nucl.nagoya-u.ac.jp [Department of Materials, Physics and Energy Engineering, Nagoya University, Furo-cho, Chikusa-ku, Nagoya 464-8603 (Japan); PRESTO, Japan Science and Technology Agency, 4-1-8 Honcho, Kawaguchi, Saitama 332-0012 (Japan); Yasumoto, Jun; Ito, Daisuke; Yoshino, Masahito; Nagasaki, Takanori [Department of Materials, Physics and Energy Engineering, Nagoya University, Furo-cho, Chikusa-ku, Nagoya 464-8603 (Japan); Sakata, Osami [Synchrotron X-ray Station at SPring-8 and Synchrotron X-ray Group, National Institute for Materials Science, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan); Department of Innovative and Engineered Material, Tokyo Institute of Technology, Yokohama 226-8503 (Japan); Imai, Yasuhiko [Japan Synchrotron Radiation Research Institute, SPring-8, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan); Kiguchi, Takanori [Institute for Materials Research, Tohoku University, Sendai, Miyagi 980-8577 (Japan); Shiraishi, Takahisa; Shimizu, Takao; Funakubo, Hiroshi [Department of Innovative and Engineered Material, Tokyo Institute of Technology, Yokohama 226-8503 (Japan)

    2015-08-21

    The converse piezoelectric responses of (111)- and (001)-epitaxial tetragonal Pb(Zr{sub 0.35}Ti{sub 0.65})O{sub 3} [PZT] films were compared to investigate the orientation dependence of the substrate clamping effect. Synchrotron X-ray diffraction (XRD) and piezoelectric force microscopy revealed that the as-grown (111)-PZT film has a polydomain structure with normal twin boundaries that are changed by the poling process to inclined boundaries, as predicted by Romanov et al. [Phys. Status Solidi A 172, 225 (1999)]. Time-resolved synchrotron XRD under bias voltage showed the negligible impact of substrate clamping on the piezoelectric response in the (111)-PZT film, unlike the case for (001)-PZT film. The origin of the negligible clamping effect in the (111)-PZT film is discussed from the viewpoint of the elastic properties and the compensation of lattice distortion between neighboring domains.

  19. Modeling of Magnetoelectric Interaction in Magnetostrictive-Piezoelectric Composites

    Directory of Open Access Journals (Sweden)

    M. I. Bichurin

    2012-01-01

    Full Text Available The paper dwells on the theoretical modeling of magnetoelectric (ME effect in layered and bulk composites based on magnetostrictive and piezoelectric materials. Our analysis rests on the simultaneous solution of elastodynamic or elastostatic and electro/magnetostatic equations. The expressions for ME coefficients as the functions of material parameters and volume fractions of components are obtained. Longitudinal, transverse, and in-plane cases are considered. The use of the offered model has allowed to present the ME effect in ferrite cobalt-barium titanate, ferrite cobalt-PZT, ferrite nickel-PZT, and lanthanum strontium manganite-PZT composites adequately.

  20. Ferroelectric/electrode interfaces: Polarization switching and reliability of PZT capacitors in nonvolatile memories

    Science.gov (United States)

    Chen, Ye (Mike)

    The objective of this work was to investigate how the interface between electrode and PZT influences the PZT capacitor reliability. In order to conduct a well controlled experiment only the top-electrode PZT film interface was modified to study its effect on switching characteristics (i.e. hysteresis loop), voltage switching endurance and polarization retention of state of the art MOCVD grown film (nominally identical). The polycrystalline PZT film (50 -- 90 nm thick) are dominantly tetragonal with small fractions of the rhombohedral phase. XPS analyses of the as-deposited PZT film found the existence of a Pb-rich carbonate surface layer on all PZT film provided by industrial collaborators. Using materials characterizations such as in-situ XPS and ARXPS in tandem with electrical measurements it was determined that the Pb-rich surface layer appears to be an engineered sacrificial layer, which is beneficial in maximizing the switchable polarization and in improving the endurance and opposite-state retention behavior of PZT based FRAM capacitors with Pt electrode. This is because the excess Pb on the PZT surface and the Pb in the surface PZT reacts readily with the Pt during the Pt top electrode deposition creating a Pb-deficient non-ferroelectric interface layer between the top electrode and the PZT film. ARXPS analyses showed that this defective layer was approximately one nanometer thick and this is consistent with the hysteresis loop measurements that indicated a similar interface layer thickness. Inferior switching endurance and polarization retention was found in PZT film with an engineered initial thicker defective interface layer (via a HNO3-clean of the PZT surface prior to the top electrode deposition). This could be due to the fact that this defective interface layer may have thickened during the voltage cycling and/or retention bake. The thickening could be caused by greater carrier trapping and/or interface reaction between the Pb and the Pt. This

  1. Broadband Electromagnetic Emission from PZT Ferroelectric Ceramics after Shock Loading

    Directory of Open Access Journals (Sweden)

    Fiodoras ANISIMOVAS

    2013-12-01

    Full Text Available It was experimentally registered pulsed electromagnetic (EM radiation in frequency range higher than television one using wideband horns with coaxial and waveguide outputs. The EM radiation was received during shock loading of lead zirconate titanate (PZT ceramics cylinders in conventional piezoelectric ignition mechanisms. Digital oscilloscope allows registering whole series of EM pulses and each pulse from the series transmitted from horn antenna of (1 – 18 GHz operating band frequencies. There is (1 – 4 ms delay between the shock and the first pulse of the series. Duration of the series is about (3 – 4 ms. The PZT cylinders were cleaved along their axes and the surfaces formed in the process were investigated by scanning electron microscope. It was concluded that from electrical point of view PZT ceramics contain interacting subsystems. It was found that EM radiation spectrum of pulse detected by waveguide detector heads has harmonics reaching 80 GHz. Presence of harmonics higher than 20 GHz indicates on radiation due to deceleration of electrons emitted during the switching. The EM pulses in the series appear randomly and have different amplitudes which partly confirmed thesis on independent switching dynamics of small volumes governed by a local electric field.DOI: http://dx.doi.org/10.5755/j01.ms.19.4.3137

  2. Broadband Electromagnetic Emission from PZT Ferroelectric Ceramics after Shock Loading

    Directory of Open Access Journals (Sweden)

    Fiodoras ANISIMOVAS

    2013-12-01

    Full Text Available It was experimentally registered pulsed electromagnetic (EM radiation in frequency range higher than television one using wideband horns with coaxial and waveguide outputs. The EM radiation was received during shock loading of lead zirconate titanate (PZT ceramics cylinders in conventional piezoelectric ignition mechanisms. Digital oscilloscope allows registering whole series of EM pulses and each pulse from the series transmitted from horn antenna of (1 – 18 GHz operating band frequencies. There is (1 – 4 ms delay between the shock and the first pulse of the series. Duration of the series is about (3 – 4 ms. The PZT cylinders were cleaved along their axes and the surfaces formed in the process were investigated by scanning electron microscope. It was concluded that from electrical point of view PZT ceramics contain interacting subsystems. It was found that EM radiation spectrum of pulse detected by waveguide detector heads has harmonics reaching 80 GHz. Presence of harmonics higher than 20 GHz indicates on radiation due to deceleration of electrons emitted during the switching. The EM pulses in the series appear randomly and have different amplitudes which partly confirmed thesis on independent switching dynamics of small volumes governed by a local electric field.DOI: http://dx.doi.org/10.5755/j01.ms.19.4.3137

  3. Optical properties of PZT thin films deposited on a ZnO buffer layer

    OpenAIRE

    Schneider, T.; Leduc, D; Cardin, J.; LUPI, C; Barreau, N; Gundel, H.

    2015-01-01

    The optical properties of lead zirconate titanate (PZT) thin films deposited on ZnO were studied by m-lines spectroscopy. In order to retrieve the refractive index and the thickness of both layers from the m-lines spectra, we develop a numerical algorithm for the case of a two-layer system and show its robustness in the presence of noise. The sensitivity of the algorithm of the two-layer model allows us to relate the observed changes in the PZT refractive index to the PZT structural change du...

  4. (001) Oriented piezoelectric films prepared by chemical solution deposition on Ni foils

    Energy Technology Data Exchange (ETDEWEB)

    Yeo, Hong Goo, E-mail: hxy162@psu.edu; Trolier-McKinstry, Susan [Materials Research Institute, The Pennsylvania State University, University Park, Pennsylvania 16802 (United States)

    2014-07-07

    Flexible metal foil substrates are useful in some microelectromechanical systems applications including wearable piezoelectric sensors or energy harvesters based on Pb(Zr,Ti)O₃ (PZT) thin films. Full utilization of the potential of piezoelectrics on metal foils requires control of the film crystallographic texture. In this study, (001) oriented PZT thin films were grown by chemical solution deposition (CSD) on Ni foil and Si substrates. Ni foils were passivated using HfO₂ grown by atomic layer deposition in order to suppress substrate oxidation during subsequent thermal treatment. To obtain the desired orientation of PZT film, strongly (100) oriented LaNiO₃ films were integrated by CSD on the HfO₂ coated substrates. A high level of (001) LaNiO₃ and PZT film orientation were confirmed by X-ray diffraction patterns. Before poling, the low field dielectric permittivity and loss tangents of (001) oriented PZT films on Ni are near 780 and 0.04 at 1 kHz; the permittivity drops significantly on poling due to in-plane to out-of-plane domain switching. (001) oriented PZT film on Ni displayed a well-saturated hysteresis loop with a large remanent polarization ~36 μC/cm², while (100) oriented PZT on Si showed slanted P-E hysteresis loops with much lower remanent polarizations. The |e{sub 31,f}| piezoelectric coefficient was around 10.6 C/m² for hot-poled (001) oriented PZT film on Ni.

  5. Mechanical and dielectric characterization of lead zirconate titanate(PZT)/polyurethane(PU) thin film composite for energy harvesting

    Science.gov (United States)

    Aboubakr, S.; Rguiti, M.; Hajjaji, A.; Eddiai, A.; Courtois, C.; d'Astorg, S.

    2014-04-01

    The Lead Zirconate titanate (PZT) ceramic is known by its piezoelectric feature, but also by its stiffness, the use of a composite based on a polyurethane (PU) matrix charged by a piezoelectric material, enable to generate a large deformation of the material, therefore harvesting more energy. This new material will provide a competitive alternative and low cost manufacturing technology of autonomous systems (smart clothes, car seat, boat sail, flag ...). A thin film of the PZT/PU composite was prepared using up to 80 vol. % of ceramic. Due to the dielectric nature of the PZT, inclusions of this one in a PU matrix raises the permittivity of the composite, on other hand this latter seems to decline at high frequencies.

  6. Highly polarized single-c-domain single-crystal Pb(Mn,Nb)O(3)-PZT thin films.

    Science.gov (United States)

    Wasa, Kiyotaka; Adachi, Hideaki; Nishida, Ken; Yamamoto, Takashi; Matsushima, Tomoaki; Kanno, Isaku; Kotera, Hidetoshi

    2012-01-01

    In-plane unstrained single-c-domain/single-crystal thin films of PZT-based ternary ferroelectric perovskite, ξPb(Mn,Nb)O3-(1 - ξ)PZT, were grown on SrRuO(3)/Pt/MgO substrates using magnetron sputtering followed by quenching. The sputtered unstrained thin films exhibit unique ferroelectric properties: high coercive field, Ec > 180 kV/cm, large remanent polarization, P(r) = 100 μC/cm(2), small relative dielectric constants, ε* = 100 to 150, high Curie temperature, Tc = ~600 °C, and bulk-like large transverse piezoelectric constants, e31,f = -12.0 C/m(2) for PZT(48/52) at ξ = 0.06. The unstrained thin films are an ideal structure to extract the bulk ferroelectric properties. Their micro-structures and ferroelectric properties are discussed in relation to the potential applications for piezoelectric MEMS. © 2012 IEEE

  7. Analysis of axisymmetric and non-axisymmetric wave propagation in a homogeneous piezoelectric solid circular cylinder of transversely isotropic material

    CSIR Research Space (South Africa)

    Shatalov, MY

    2010-01-01

    Full Text Available for PZT-4 and PZT-7A piezoelectric ceramics for circumferential wave numbers m = 1, 2, and 3. It is observed that the dispersion curves are sensitive to the type of the imposed boundary conditions as well as to the measure of the electromechanical coupling...

  8. Analysis of non-axisymmetric wave propagation in a homogeneous piezoelectric solid circular cylinder of transversely isotropic material

    CSIR Research Space (South Africa)

    Shatalov, MY

    2009-01-01

    Full Text Available for PZT-4 and PZT-7A piezoelectric ceramics for circumferential wave numbers m = 1, 2, and 3. It is observed that the dispersion curves are sensitive to the type of the imposed boundary conditions as well as to the measure of the electromechanical coupling...

  9. THE MONOCLINIC PHASE IN PZT: NEW LIGHT ON MORPHOTROPIC PHASE BOUNDARIES

    Energy Technology Data Exchange (ETDEWEB)

    NOHEDA,B.; GONZALO,J.A.; GUO,R.; PARK,S.E.; CROSS,L.E.; COX,D.E.; SHIRANE,G.

    2000-03-09

    A summary of the work recently carried out on the morphotropic phase boundary (MPB) of PZT is presented. By means of x-ray powder diffraction on ceramic samples of excellent quality, the MPB has been successfully characterized by changing temperature in a series of closely spaced compositions. As a result, an unexpected monoclinic phase has been found to exist in between the well-known tetragonal and rhombohedral PZT phases. A detailed structural analysis, together with the investigation of the field effect in this region of compositions, have led to an important advance in understanding the mechanisms responsible for the physical properties of PZT as well as other piezoelectric materials with similar morphotropic phase boundaries.

  10. Liquid Density Sensing Using Resonant Flexural Plate Wave Device with Sol-Gel PZT Thin Films

    CERN Document Server

    Yu, Jyh-Cheng

    2008-01-01

    This paper presents the design, fabrication and preliminary experimental results of a flexure plate wave (FPW) resonator using sol-gel derived lead zirconate titanates (PZT) thin films. The resonator adopts a two-port structure with reflecting grates on the composite membrane of PZT and SiNx. The design of the reflecting grate is derived from a SAW resonator model using COM theory to produce a sharp resonant peak. The comparison between the mass and the viscosity effects from the theoretical expression illustrates the applications and the constraints of the proposed device in liquid sensing. Multiple coatings of sol-gel derived PZT films are adopted because of the cost advantage and the high electromechanical coupling effect over other piezoelectric films. The fabrication issues of the proposed material structure are addressed. Theoretical estimations of the mass and the viscosity effects are compared with the experimental results. The resonant frequency has a good linear correlation with the density of low v...

  11. A Flexible Ultrasound Transducer Array with Micro-Machined Bulk PZT

    Directory of Open Access Journals (Sweden)

    Zhe Wang

    2015-01-01

    Full Text Available This paper proposes a novel flexible piezoelectric micro-machined ultrasound transducer, which is based on PZT and a polyimide substrate. The transducer is made on the polyimide substrate and packaged with medical polydimethylsiloxane. Instead of etching the PZT ceramic, this paper proposes a method of putting diced PZT blocks into holes on the polyimide which are pre-etched. The device works in d31 mode and the electromechanical coupling factor is 22.25%. Its flexibility, good conformal contacting with skin surfaces and proper resonant frequency make the device suitable for heart imaging. The flexible packaging ultrasound transducer also has a good waterproof performance after hundreds of ultrasonic electric tests in water. It is a promising ultrasound transducer and will be an effective supplementary ultrasound imaging method in the practical applications.

  12. Electric properties of textured (K$_{0.44}$Na$_{0.52}$Li$_{0.04}$)(Nb$_{0.86}Ta$_{0.10}$Sb$_{0.04}$)O$_3$ thick film prepared by screen printing method

    Indian Academy of Sciences (India)

    FANG FU; JIWEI ZHAI; ZHENGKUI XU

    2016-08-01

    Textured (K$_{0.44}$Na$_{0.52}$Li$_{0.04}$) (Nb$_{0.86}$Ta$_{0.10}$Sb$_{0.04}$)O$_3$ thick film was fabricated by the screen printing method with plate-like NaNbO3 particles as template. Thick film with 75% grain orientation was prepared. Remnant polarization and coercive field observed from the P–E loops of textured thick film were 3.6 $\\mu$C cm$^{−2}$ and 21 kV cm$^{−1}$, respectively. Textured (K$_{0.44}$Na$_{0.52}$Li$_{0.04}$) (Nb$_{0.86}$Ta$_{0.10}$Sb$_{0.04}$)O$_{3}$ thick film exhibited diffusion behaviour by analysing the temperature dependence of permittivity and loss tangent. The result of leakage current density showed a conduction mechanism of Schottky emission. Piezoelectric (PZT) properties of the thick film were characterized by the relationship of unipolar strain and applied electric field and the PZT constant $d^∗_{33}$ of textured thick film reached to 150 pm V$^{−1}$. Nonlinear PZT property of the thick film was investigated by Rayleigh law.

  13. Characterisation of static actuation behaviour of encapsulated PZT

    Science.gov (United States)

    Doran, Conrad J.; Butler, Raymond J.

    1994-09-01

    Within the field of 'smart' structures considerable interest has been shown in the use of piezoelectric materials both as sensors and actuators. One of the best characterized of these materials is the family of Lead Zirconate Titanate (PZT) based ceramics. The use of PZT in intelligent systems has been fairly widespread, the high modulus of the material give high authority actuation, coupled with a wide operational bandwidth and relative ease of control by the application of an applied voltage. The linearity of the actuation response over a limited range has made PZT a popular choice for high precision, relatively low displacement applications. A number of attempts have been made to utilize such actuators for aerospace, using both surface mounting [1] and embedding techniques [2,3]. The effects of actuators on aeroelastic performance has also been investigated for aerospace applications [4,5]. The current practical solution to this problem appears to be the use of spatially distributed actuators [6]. One of the practical limitations of this problem are the large number of actuators required to produce the required degree of static control. In order to ensure accurate shape control, measurements must be taken to ensure there are no significant difference in the actuator element properties due to factors such as batch processing variation. In the past this has proved difficult due to the extremely brittle nature of the actuator material. More specifically the requirement for thinner elements for use in embedded applications has increased this problem. A method by which the static performance of electroceramic actuators could be quickly established would therefore be desirable. This paper presents the results of recent work to develop a test method to define the static electromechanical properties of encapsulated actuator materials in order to assess their suitability as static actuators for aerospace applications. Preliminary results using a standard PZT material are

  14. Fabrication and properties of SmFe2-PZT magnetoelectric thin films

    KAUST Repository

    Giouroudi, Ioanna

    2013-05-17

    Magnetoelectric (ME) thin film composites are attracting a continually increasing interest due to their unique features and potential applications in multifunctional microdevices and integrated units such as sensors, actuators and energy harvesting modules. By combining piezoelectric and highly magnetostrictive thin films, the potentialities of these materials increase. In this paper we report the fabrication of SmFe2 and PZT thin films and the investigation of their properties. First of all, a ~ 400 nm thin SmFe film was deposited on top of Si/SiO2 substrate by magnetron sputter deposition. Afterwards, a 140 nm Pt bottom electrode was sputtered on top of the SmFe film forming a bottom electrode. Spin coating was employed for the deposition of the 150 nm thin PZT layer. A PZT solution with 10 %Pb excess was utilized for this fabrication step. Finally, circular Pt top electrodes were sputtered as top electrodes. This paper focuses on the microstructure of the individual films characterized by X-Ray diffractometer (XRD) and scanning electron microscopy (SEM). A piezoelectric evaluation system, aixPES, with TF2000E analyzer component was used for the electric hysteresis measurements of PZT thin films and a vibrating sample magnetometer (VSM) was employed for the magnetic characterization of the SmFe. The developed thin films and the fabricated double layer SmFe-PZT exhibit both good ferromagnetic and piezoelectric responses which predict a promising ME composite structure. The quantitative chemical composition of the samples was confirmed by energy dispersive spectroscopy (EDX). © (2013) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.

  15. Thick-film force, slip and temperature sensors for a prosthetic hand

    Science.gov (United States)

    Cranny, A.; Cotton, D. P. J.; Chappell, P. H.; Beeby, S. P.; White, N. M.

    2005-04-01

    Thick-film static and dynamic force sensors have been investigated for their suitability to measure the grip forces exerted upon an object held by a prosthetic hand, and to detect and correspondingly react to the possible slip of a gripped item. The static force sensors exploit the piezoresistive characteristics of commercially available thick-film pastes whilst the dynamic slip sensors utilize the piezoelectric behaviour of proprietary PZT (lead zirconate titanate) pastes. The sensors are located upon stainless steel cantilever type structures that will be placed at the fingertips of each digit of the prosthetic hand. Temperature sensors are also included to provide temperature compensation for the force sensors and to prevent accidental thermal damage to the prosthesis. Results have shown that the static force sensor is capable of measuring fingertip forces in excess of 100 N, with an electrical half-bridge configuration sensitivity approaching 10 µV V-1 N-1 (with scope for improvement) and maximum hysteresis below 4% of full scale, depending on the manner in which the cantilever sensor array is attached to the finger. Failure in the bonding mechanism that secures the PZT layer to the stainless steel cantilever meant that the proposed dynamic force sensor could not be evaluated. However, investigations using the same sensor design fabricated on an alumina substrate have shown the potential of the PZT dynamic force sensor to measure the vibration and hence potentially operate as a slip sensor.

  16. Plasmonic assisted two wave mixing phenomenon for energy transfer in ferroelectric PZT film

    Science.gov (United States)

    Gupta, Reema; Kumari, Satchi; Tomar, Monika; Gupta, Vinay

    2017-04-01

    Ferroelectric - photorefractive PZT thin films have been exploited to study the energy transfer using pump probe technique for the development of optical delay lines. Two-wave mixing has been studied for three different PZT thin film samples deposited using pulsed laser deposition (PLD) technique. Uniform distribution of gold micro-discs of 40 nm thickness and 120 μm diameter over the surface of PZT thin film plays a vital role in enhancing the two-wave mixing. This is due to the ferroelectric domains present in PZT thin film which get polarized as a result of excited surface plasmons at the Au-PZT interface. The dual effect leads to an enhanced energy transfer from pump to 'Probe Beam'. The maximum two-wave mixing gain was found to be about 1.185 and 1.055 respectively for gold micro-discs patterned and bare PZT thin film deposited on STO substrate. In comparison, the PZT thin film covered completely with the gold overlayer does not show any significant two wave mixing gain due to the scattering of light by Au overlayer.

  17. Progress in Dual (Piezoelectric-Magnetostrictive Phase Magnetoelectric Sintered Composites

    Directory of Open Access Journals (Sweden)

    Rashed Adnan Islam

    2012-01-01

    Full Text Available The primary aims of this review article are (a to develop the fundamental understanding of ME behavior in perovskite piezoelectric-spinel magnetostrictive composite systems, (b to identify the role of composition, microstructural variables, phase transformations, composite geometry, and postsintering heat treatment on ME coefficient, and (c to synthesize, characterize, and utilize the high ME coefficient composite. The desired range of ME coefficient in the sintered composite is 0.5–1 V/cm⋅Oe. The studies showed that the soft piezoelectric phase quantified by smaller elastic modulus, large grain size of piezoelectric phase (~1 μm, and layered structures yields higher magnitude of ME coefficient. It is also found that postsintering thermal treatment such as annealing and aging alters the magnitude of magnetization providing an increase in the magnitude of ME coefficient. A trilayer composite was synthesized using pressure-assisted sintering with soft phase [0.9 PZT–0.1 PZN] having grain size larger than 1 μm and soft ferromagnetic phase of composition Ni0.8Cu0.2Zn0.2Fe2O4 [NCZF]. The composite showed a high ME coefficient of 412 and 494 mV/cm⋅Oe after sintering and annealing, respectively. Optimized ferrite to PZT thickness ratio was found to be 5.33, providing ME coefficient of 525 mV/cm⋅Oe. The ME coefficient exhibited orientation dependence with respect to applied magnetic field. Multilayering the PZT layer increased the magnitude of ME coefficient to 782 mV/cm⋅Oe. Piezoelectric grain texturing and nanoparticulate assembly techniques were incorporated with the layered geometry. It was found that with moderate texturing, d33 and ME coefficient reached up to 325 pC/N and 878 mV/cm⋅Oe, respectively. Nanoparticulate core shell assembly shows the promise for achieving large ME coefficient in the sintered composites. A systematic relationship between composition, microstructure, geometry, and properties is

  18. Novel precision piezoelectric step rotary actuator

    Institute of Scientific and Technical Information of China (English)

    LIU Jianfang; YANG Zhigang; ZHAO Hongwei; CHENG Guangming

    2007-01-01

    A novel piezoelectric (PZT) precision step rotary actuator was developed on the basis of PZT technology.It adopts the principle of bionics and works with an inside anchoring/loosening of the stator and a distortion structure of the uniformly distributed thin flexible hinge to solve problems such as ineffective anchoring/loosening,low step rotary frequency,small travel,poor resolution,low speed and unsteady output.The developed actuator is characterized by high frequency (30 Hz),high speed (380 μrad/s),large travel (>270°),high resolution (1 μrad/step),and work stability.It greatly improves the ability to drive the existing PZT step rotary actuator.The new actuator can be applied in the field of micromanipulation and precision engineering,including precision driving and positioning and optics engineering.

  19. TECHNICAL NOTE: The development of a PZT-based microdrive for neural signal recording

    Science.gov (United States)

    Park, Sangkyu; Yoon, Euisung; Lee, Sukchan; Shin, Hee-sup; Park, Hyunjun; Kim, Byungkyu; Kim, Daesoo; Park, Jongoh; Park, Sukho

    2008-04-01

    A hand-controlled microdrive has been used to obtain neural signals from rodents such as rats and mice. However, it places severe physical stress on the rodents during its manipulation, and this stress leads to alertness in the mice and low efficiency in obtaining neural signals from the mice. To overcome this issue, we developed a novel microdrive, which allows one to adjust the electrodes by a piezoelectric device (PZT) with high precision. Its mass is light enough to install on the mouse's head. The proposed microdrive has three H-type PZT actuators and their guiding structure. The operation principle of the microdrive is based on the well known inchworm mechanism. When the three PZT actuators are synchronized, linear motion of the electrode is produced along the guiding structure. The electrodes used for the recording of the neural signals from neuron cells were fixed at one of the PZT actuators. Our proposed microdrive has an accuracy of about 400 nm and a long stroke of about 5 mm. In response to formalin-induced pain, single unit activities are robustly measured at the thalamus with electrodes whose vertical depth is adjusted by the microdrive under urethane anesthesia. In addition, the microdrive was efficient in detecting neural signals from mice that were moving freely. Thus, the present study suggests that the PZT-based microdrive could be an alternative for the efficient detection of neural signals from mice during behavioral states without any stress to the mice.

  20. Study of 1-3 PZT fibre/epoxy composite force sensor

    Science.gov (United States)

    Choy, S. H.; Chan, H. L. W.; Ng, M. W.; Liu, P. C. K.

    2005-09-01

    Lead zirconate titanate (PZT) fibres were prepared by a powder-based extrusion method. Pre-sintered PZT powder mixed with poly(acrylic acid) was spun in a spinnerette to produce fibres. The fibre of ˜400 μm diameter was used to fabricate 1-3 PZT fibre/epoxy composite discs with different volume fractions (ϕ) of PZT. Since the ceramic fibres are rather brittle, their elastic properties cannot be measured directly. In order to determine the properties of the ceramic fibres, effective properties of the fibres/epoxy 1-3 composite were measured. By using a modified series and parallel model, the properties of 1-3 composites can be calculated. Then, the elastic coefficient s33,fibreE, relative permittivity ɛ33,fibreT and piezoelectric strain coefficient d33,fibre of the ceramic fibre could be found. Ring-shaped PZT fibre/epoxy materials composites with different ϕ were fabricated to be used as the sensing material in force sensor applications. The ring-shape composite with ϕ=0.5 was installed into a housing and the sensor was calibrated by different methods and its sensitivity was found to be 144 pC/N within the frequency range of 0.5 6.4 kHz which is much higher than that of a quartz force sensor with a similar structure.

  1. Design and Experiment of PZT Network-based Structural Health Monitoring Scanning System

    Institute of Scientific and Technical Information of China (English)

    Qiu Lei; Yuan Shenfang; Wang Qiang; Sun Yajie; Yang Weiwei

    2009-01-01

    The active Lamb wave and piezoelectric transducer (PZT)-based structural health monitoring (SHM) technology is a kind of efficient approach to estimate the health state of aircraft structure. In practical applications, PZT networks are needed to monitor large scale structures. Scanning many of the different PZT actuator-sensor channels within these PZT networks to achieve on-line SHM task is important. Based on a peripheral component interconnect extensions for instrumentation (PXI) platform, an active Lamb wave and PZT network-based integrated multi-channel scanning system (PXI-ISS) is developed for the purpose of practical applications of SHM, which is compact and portable, and can scan large numbers of actuator-sensor channels and perform damage assessing automatically. A PXI-based 4 channels gain-programmable charge amplifier, an external scanning module with 276 actuator-sensor channels and integrated SHM software are proposed and discussed in detail. The experimental research on a carbon fiber composite wing box of an unmanned aerial vehicle (UAV) for verifying the functions of the PXI-ISS is mainly discussed, including the design of PZTs layer, the method of excitation frequency selection, functional test of damage imaging, stability test of the PXI-ISS, and the loading effect on signals. The experimental results have verified the stability and damage functions of this system.

  2. Development of PZT-excited stroboscopic shearography for full-field nondestructive evaluation

    Science.gov (United States)

    Asemani, Hamidreza; Park, Jinwoo; Lee, Jung-Ryul; Soltani, Nasser

    2017-05-01

    Nondestructive evaluation using shearography requires a way to stress the inspection target. This technique is able to directly measure the displacement gradient distribution on the object surface. Shearography visualizes the internal structural damages as the anomalous pattern in the shearograpic fringe pattern. A piezoelectric (PZT) excitation system is able to generate loadings in the vibrational, acoustic, and ultrasonic regimes. In this paper, we propose a PZT-excited stroboscopic shearography. The PZT excitation could generate vibrational loading, a stationary wavefield, and a nonstationary propagation wave to fulfill the external loading requirement of shearography. The sweeping of the PZT excitation frequency, the formation of a standing wave, and a small shearing to suppress the incident wave were powerful controllable tools to detect the defects. The sweeping of the PZT excitation frequency enabled us to determine one of the defect-sensitive frequencies almost in real time. In addition, because the defect sensitive frequencies always existed in wide and plural ranges, the risk of the defect being overlooked by the inspector could be alleviated. The results of evaluation using stroboscopic shearography showed that an artificial 20 mm-diameter defect could be visualized at the excitation frequencies of 5-8 kHz range and 12.5-15.5 kHz range. This technique provided full field reliable and repeatable inspection results. Additionally, the proposed method overcame the important drawback of the time-averaged shearography, being required to identify the resonance vibration frequency sensitive to the defect.

  3. Impedance adaptation methods of the piezoelectric energy harvesting

    Science.gov (United States)

    Kim, Hyeoungwoo

    In this study, the important issues of energy recovery were addressed and a comprehensive investigation was performed on harvesting electrical power from an ambient mechanical vibration source. Also discussed are the impedance matching methods used to increase the efficiency of energy transfer from the environment to the application. Initially, the mechanical impedance matching method was investigated to increase mechanical energy transferred to the transducer from the environment. This was done by reducing the mechanical impedance such as damping factor and energy reflection ratio. The vibration source and the transducer were modeled by a two-degree-of-freedom dynamic system with mass, spring constant, and damper. The transmissibility employed to show how much mechanical energy that was transferred in this system was affected by the damping ratio and the stiffness of elastic materials. The mechanical impedance of the system was described by electrical system using analogy between the two systems in order to simply the total mechanical impedance. Secondly, the transduction rate of mechanical energy to electrical energy was improved by using a PZT material which has a high figure of merit and a high electromechanical coupling factor for electrical power generation, and a piezoelectric transducer which has a high transduction rate was designed and fabricated. The high g material (g33 = 40 [10-3Vm/N]) was developed to improve the figure of merit of the PZT ceramics. The cymbal composite transducer has been found as a promising structure for piezoelectric energy harvesting under high force at cyclic conditions (10--200 Hz), because it has almost 40 times higher effective strain coefficient than PZT ceramics. The endcap of cymbal also enhances the endurance of the ceramic to sustain ac load along with stress amplification. In addition, a macro fiber composite (MFC) was employed as a strain component because of its flexibility and the high electromechanical coupling

  4. Bending-induced electromechanical coupling and large piezoelectric response in a micromachined diaphragm.

    Science.gov (United States)

    Wang, Zhihong; Yao, Yingbang; Wang, Xianbin; Yue, Weisheng; Chen, Longqing; Zhang, Xi Xiang

    2013-11-04

    We investigated the dependence of electromechanical coupling and the piezoelectric response of a micromachined Pb(Zr₀.₅₂Ti₀.₄₈)O₃ (PZT) diaphragm on its curvature by observing the impedance spectrum and central deflection responses to a small AC voltage. The curvature of the diaphragm was controlled by applying air pressure to its back. We found that a depolarized flat diaphragm does not initially exhibit electromechanical coupling or the piezoelectric response. However, upon the application of static air pressure to the diaphragm, both electromechanical coupling and the piezoelectric response can be induced in the originally depolarized diaphragm. The piezoelectric response increases as the curvature increases and a giant piezoelectric response can be obtained from a bent diaphragm. The obtained results clearly demonstrate that a high strain gradient in a diaphragm can polarize a PZT film through a flexoelectric effect, and that the induced piezoelectric response of the diaphragm can be controlled by adjusting its curvature.

  5. Bending-induced electromechanical coupling and large piezoelectric response in a micromachined diaphragm

    KAUST Repository

    Wang, Zhihong

    2013-11-04

    We investigated the dependence of electromechanical coupling and the piezoelectric response of a micromachined Pb(Zr 0.52 Ti 0.48)O 3 (PZT) diaphragm on its curvature by observing the impedance spectrum and central deflection responses to a small AC voltage. The curvature of the diaphragm was controlled by applying air pressure to its back. We found that a depolarized flat diaphragm does not initially exhibit electromechanical coupling or the piezoelectric response. However, upon the application of static air pressure to the diaphragm, both electromechanical coupling and the piezoelectric response can be induced in the originally depolarized diaphragm. The piezoelectric response increases as the curvature increases and a giant piezoelectric response can be obtained from a bent diaphragm. The obtained results clearly demonstrate that a high strain gradient in a diaphragm can polarize a PZT film through a flexoelectric effect, and that the induced piezoelectric response of the diaphragm can be controlled by adjusting its curvature.

  6. Airflow energy harvesters of metal-based PZT thin films by self-excited vibration

    Science.gov (United States)

    Suwa, E.; Tsujiura, Y.; Kurokawa, F.; Hida, H.; Kanno, I.

    2014-11-01

    We developed self-excited vibration energy harvesters of Pb(Zr,Ti)O3 (PZT) thin films using airflow. To enhance the self-excited vibration, we used 30-μm-thick stainless steel (SS304) foils as base cantilevers on which PZT thin films were deposited by rf-magnetron sputtering. To compensate for the initial bending of PZT/SS304 unimorph cantilever due to the thermal stress, we deposited counter PZT thin films on the back of the SS304 cantilever. We evaluated power-generation performance and vibration mode of the energy harvester in the airflow. When the angle of attack (AOA) was 20° to 30°, large vibration was generated at wind speeds over 8 m/s. By FFT analysis, we confirmed that stable self-excited vibration was generated. At the AOA of 30°, the output power reached 19 μW at wind speeds of 12 m/s.

  7. Soft pneumatic actuator skin with piezoelectric sensors for vibrotactile feedback

    Directory of Open Access Journals (Sweden)

    Harshal Arun Sonar

    2016-01-01

    Full Text Available The latest wearable technologies demand more intuitive and sophisticated interfaces for communication, sensing, and feedback closer to the body. Evidently, such interfaces require flexibility and conformity without losing their functionality even on rigid surfaces. Although there has been various research efforts in creating tactile feedback to improve various haptic interfaces and master-slave manipulators, we are yet to see a comprehensive device that can both supply vibratory actuation and tactile sensing. This paper describes a soft pneumatic actuator (SPA based, SPA-skin prototype that allows bidirectional tactile information transfer to facilitate simpler and responsive wearable interface. We describe the design and fabrication of a 1.4 mm-thick vibratory SPA - skin that is integrated with piezoelectric sensors. We examine in detail the mechanical performance compared to the SPA model and the sensitivity of the sensors for the application in vibrotactile feedback. Experimental findings show that this ultra-thin SPA and the unique integration process of the discrete lead zirconate titanate (PZT based piezoelectric sensors achieve high resolution of soft contact sensing as well as accurate control on vibrotactile feedback by closing the control loop.

  8. Vibration of micromachined circular piezoelectric diaphragms.

    Science.gov (United States)

    Hong, Eunki; Trolier-McKinstry, Susan; Smith, Robert; Krishnaswamy, Silai V; Freidhoff, Carl B

    2006-04-01

    Electrically and mechanically excited resonances in micromachined circular piezoelectric diaphragms have been investigated. The diaphragm structures were piezoelectric unimorphs consisting of Pb(Zr0.52,Ti0.48)O3 (PZT) films and thermally grown silicon oxide (SiO2) layers. For electrical excitation, ring-shaped interdigitated (IDT) electrodes formed on the top of the PZT layer were used to induce strain in the diaphragms. The diaphragm structures behaved much like circular membranes in which the membrane tension was approximately 206 N/m, at the fundamental modes. For higher modes, the resonance frequencies deviated from the theoretical values due to the finite stiffness of the diaphragms. Under mechanical drive, both symmetric and asymmetric modes were excited. However, for electrical excitation, the symmetric modes were dominant due to the symmetry of the driving IDT electrodes. At a pressure of 727 Torr, the quality factor was approximately 250, and this rose to 2000 at pressures below 1 Torr. When a forward bias was applied to the diaphragm, the membrane tension decreased, but under reverse biases the tension increased. However, because of repoling under reverse biases greater than the coercive field of the PZT film, the achievable increase in the membrane tension was limited. In the diaphragm structure, the nonlinear vibration was governed by geometric nonlinearity rather than material nonlinearity. In addition, evidence of non-180 degrees domain wall motion of the PZT layer in released diaphragms was observed.

  9. Characterization of Piezoelectric Ceramic-Polymer Composites for Ultrasonic Sensor Applications

    Science.gov (United States)

    Jung, Kyung Keun; Park, Sang Hyoun; Yoo, Kwang Soo; Ko, Hyun Phill; Yoon, Seok Jin

    The piezoelectric ceramic-polymer composites were prepared by Pb(Zr0.52Ti0.48)O3 (PZT)-based ceramics with high piezoelectricity and electromechanical coupling factor and the polyvinylidene fluoride (PVdF) polymer with high acoustic impedance. The composites with 0-3 connectivity type were fabricated by hot pressing and tape casting methods. Their crystallinity, microstructure, dielectric, and piezoelectric properties were systematically evaluated.

  10. Piezoelectric devices for generating low power

    Science.gov (United States)

    Chilibon, Irinela

    2016-12-01

    This paper reviews concepts and applications in low-power electronics and energy harvesting technologies. Various piezoelectric materials and devices for small power generators useful in renewable electricity are presented. The vibrating piezoelectric device differs from the typical electrical power source in that it has capacitive rather than inductive source impedance, and may be driven by mechanical vibrations of varying amplitude. In general, vibration energy could be converted into electrical energy using one of three techniques: electrostatic charge, magnetic fields and piezoelectric. A low power piezoelectric generator, having a PZT element was realised in order to supply small electronic elements, such as optoelectronic small devices, LEDs, electronic watches, small sensors, interferometry with lasers or Micro-electro-mechanical System (MEMS) array with multi-cantilevers.

  11. Development of Vibrating Disc Piezoelectric Gyroscope

    Directory of Open Access Journals (Sweden)

    A.K. Singh

    2004-07-01

    Full Text Available The paper presents an indigenously developed vibrating disc piezoelectric gyroscope, in which both excitation and detection have been done through piezoelectric, using PZT-5H material. The gyroscope has been driven to resonant state by direct piezoelectric effect, using 20 V ac signal at 93 kHz, and the output has been detected by the reverse piezoelectric effect.The performance of this gyroscope has been tested with 3 microprocessor-controlled turntable, and the output of the gyroscope has been found" to be linearly proportional to the rotationspeed within a range ± 150 °/s. The sensitivity of the gyroscope is about 0.5 mV/°/s, which is comparable to that of other gyroscopes of similar category

  12. BIMORPH PIEZOELECTRIC ACTUATOR FOR SMALL PIPE ROBOT

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    An experimental bimorph piezoelectric element (PZT) actuator for small pipe robot is developed. The robotcan move in φ 20 mm pipe, and can carry a CCD camera for detecting cracks or fine holes on inner surface of pipe. Thevelocity of the robot can reach 17~22 mm/s for vertical pipe up/down, respectively. Moving principle and its perfor-mance characteristics are presented.

  13. Piezoelectric MEMS resonators

    CERN Document Server

    Piazza, Gianluca

    2017-01-01

    This book introduces piezoelectric microelectromechanical (pMEMS) resonators to a broad audience by reviewing design techniques including use of finite element modeling, testing and qualification of resonators, and fabrication and large scale manufacturing techniques to help inspire future research and entrepreneurial activities in pMEMS. The authors discuss the most exciting developments in the area of materials and devices for the making of piezoelectric MEMS resonators, and offer direct examples of the technical challenges that need to be overcome in order to commercialize these types of devices. Some of the topics covered include: Widely-used piezoelectric materials, as well as materials in which there is emerging interest Principle of operation and design approaches for the making of flexural, contour-mode, thickness-mode, and shear-mode piezoelectric resonators, and examples of practical implementation of these devices Large scale manufacturing approaches, with a focus on the practical aspects associate...

  14. High energy-density 0.72Pb(Zr0.47Ti0.53)O3-0.28Pb[(Zn0.45Ni0.55)1/3Nb2/3]O3 thick films fabricated by tape casting for energy-harvesting-device applications

    Science.gov (United States)

    Jeon, Chang Jun; Hwang, Ha Na; Jeong, Young Hun; Yun, Ji Sun; Nam, Joong Hee; Cho, Jeong Ho; Paik, Jong Hoo; Lim, Jong Bong; Nahm, Sahn; Kim, Eung Soo

    2013-11-01

    0.72Pb(Zr0.47Ti0.53)O3-0.28Pb[(Zn0.45Ni0.55)1/3Nb2/3]O3 (0.72PZT-0.28PZNN) thick films were prepared by using a tape casting method to develop new materials with high energy-density applicable to energy-harvesting devices. The piezoelectric strain constant ( d 33), dielectric constant ( ɛ {33/ T }/ ɛ 0), piezoelectric voltage constant ( g 33) and transduction coefficient ( d 33· g 33) of the films were affected by the sintering temperature. These results could be attributed to the crystal structure, microstructures and secondary phases. However, the dielectric loss (tan δ) of the films was not changed remarkably with increasing sintering temperature. Typically, a d 33 of 452 pC/N, ɛ {33/ T }/ ɛ 0 of 1444, d 33· g 33 of 20,340 × 10-15 m2/N and tan δ of 0.15% were obtained for the films sintered at 1050 °C for 1 h. The power generation performance of the piezoelectric unimorph cantilever was assessed to demonstrate the feasibility of the 0.72PZT-0.28PZNN piezoelectric thick film. Also, theoretical models were employed to predict the resonance frequency of the unimorph cantilever generator, and the predicted values were compared with experimental data.

  15. Far infrared and Raman response in tetragonal PZT ceramic films

    Energy Technology Data Exchange (ETDEWEB)

    Buixaderas, E.; Kadlec, C.; Vanek, P.; Drnovsek, S.; Ursic, H.; Malic, B.

    2015-07-01

    PbZr{sub 0}.38Ti{sub 0}.62O{sub 3} and PbZr{sub 0}.36Ti{sub 0}.64{sub O}3 thick films deposited by screen printing on (0 0 0 1) single crystal sapphire substrates and prepared at two different sintering temperatures, were studied by Fourier-transform infrared reflectivity, time-domain TH{sub z} transmission spectroscopy and micro-Raman spectroscopy. The dielectric response is discussed using the Lichtenecker model to account for the porosity of the films and to obtain the dense bulk dielectric functions. Results are compared with bulk tetragonal PZT 42/58 ceramics. The dynamic response in the films is dominated by an overdamped lead-based vibration in the TH{sub z} range, as known in PZT, but its evaluated dielectric contribution is affected by the porosity and roughness of the surface. (Author)

  16. ANALYSIS OF CRACK-TIP SINGULARITIES FOR AN INTERFACIAL PERMEABLE CRACK IN METAL/PIEZOELECTRIC BIMATERIALS

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    By modeling metal as a special piezoelectric material with extremely small piezoelectricity and extremely large permittivity, we have obtained the analytical solutions for an interfacial permeable crack in metal/piezoelectric bimaterials by means of the generalized Stroh formalism.The analysis shows that the stress fields near a permeable interfacial crack tip are usually with three types of singularities: r-1/2±iε and r-1/2. Further numerical calculation on the oscillatory index ε are given for 28 types of metal/piezoelectric bimaterials combined by seven commercial piezoelectric materials: PZT-4, BaTiO3, PZT-5H, PZT-6B, PZT-7A, P-7 and PZT-PIC 151 and four metals: copper, silver, lead and aluminum, respectively. The explicit expressions of the crack tip energy release rate (ERR) and the crack tip generalized stress intensity factors (GSIF) are obtained. It is found that both the ERR and GSIF are independent of the electric displacement loading, although they seriously depends on the mechanical loadings.

  17. Ultrasound backscatter microscope using PZT, fine-grain PZT, and single-crystal perovskite transducers

    Science.gov (United States)

    Olbrish, Kenneth D.; Zipparo, Michael J.; Lopath, Patrick D.; Yu, Clarence; Shrout, Thomas R.; Shung, K. Kirk

    1997-04-01

    Higher frequency ultrasound is rapidly becoming an important tool for dermatologic and ophthalmologic imaging. This brings about a need for improvement in single element transducers operating in the frequency range between 40 MHz and 100 MHz. Several piezoelectric materials may yield improved performance over common lead zirconate titanate (PZT) transducers. This study investigated several different materials incorporated into single element transducers. A static ultrasonic backscatter microscope (UBM) was constructed in the laboratory. This system allowed for a comparative testing of the imaging performance of various transducers. B-mode scans made by individual transducers show differences in image resolution. Clinically, these differences may be important to allow finer detail to be observed in a structure. Not only does this work show differences between transducers constructed from various materials, but it does so in an application-based environment. Previously, only a limited number of materials were used in such a system. This study showed results from several materials that had not been demonstrated before.

  18. PMN-PT-PZT composite films for high frequency ultrasonic transducer applications.

    Science.gov (United States)

    Hsu, Hsiu-Sheng; Benjauthrit, Vatcharee; Zheng, Fan; Chen, Rumin; Huang, Yuhong; Zhou, Qifa; Shung, K Kirk

    2012-06-01

    We have successfully fabricated x(0.65PMN-0.35PT)-(1 - x)PZT (xPMN-PT-(1 - x)PZT), where x is 0.1, 0.3, 0.5, 0.7 and 0.9, thick films with a thickness of approximately 9 µm on platinized silicon substrate by employing a composite sol-gel technique. X-ray diffraction analysis and scanning electron microscopy revealed that these films are dense and creak-free with well-crystallized perovskite phase in the whole composition range. The dielectric constant can be controllably adjusted by using different compositions. Higher PZT content of xPMN-PT-(1 - x)PZT films show better ferroelectric properties. A representative 0.9PMN-PT-0.1PZT thick film transducer is built. It has 200 MHz center frequency with a -6 dB bandwidth of 38% (76 MHz). The measured two-way insertion loss is 65 dB.

  19. Physical properties of inorganic PMW-PNN-PZT ceramics

    Science.gov (United States)

    Sin, Sang-Hoon; Yoo, Ju-hyun; Kim, Yong-Jin; Baek, Sam-ki; Ha, Jun-Soo; No, Chung-Han; Song, Hyun-Seon; Shin, Dong-Chan

    2015-07-01

    In this work, inorganic Pb(Mg1/2W1/2)0.03(Ni1/3Nb2/3)x(Zr0.5Ti0.5)0.97-xO3 (x = 0.02 ∼ 0.12) composition ceramics were fabricated by the conventional solid state reaction method. And then their micro structure and ferroelectric properties were investigated according to the amount of PNN substitution. Small amounts of Li2CO3 and CaCO3 were used in order to decrease the sintering temperature of the ceramics. The 0.10 mol PNN-substituted PMW-PNN- PZT ceramics sintered at 920°C showed the excellent physical properties of piezoelectric constant (d33), electromechanical coupling factor (kp), mechanical quality coefficient (Qm), and dielectric constant of 566 pC/N, 0.61, 73, and 2183, respectively.

  20. Performance of PZT8 Versus PZT4 Piezoceramic Materials in Ultrasonic Transducers

    Science.gov (United States)

    DeAngelis, Dominick A.; Schulze, Gary W.

    PZT8 and PZT4 are the common "hard" piezoceramic materials used in power ultrasonic transducers (e.g., welding, cutting, sonar, etc.). PZT8 is perceived as the better choice for resonant devices, primarily due to its higher mechanical quality factor Qm. PZT8 is also considered a "harder" material compared to PZT4, since it has better stability at higher preloads and drive levels. Many transducer designers never consider PZT4 for their applications, even though it has clear advantages such as higher output (i.e., higher d33). Even the perceived advantage of PZT8 regarding Qm may not be significant for most Langevin, bolted stack type transducers if the mechanical joint losses dominate. This research is a case study on the performance of identical ultrasonic transducers used for semiconductor wire bonding, assembled with either PZT8 or PZT4 materials. The main purpose of the study is to establish rule-of-thumb transducer design guidelines for the selection of PZT8 versus PZT4 materials. Several metrics are investigated such as impedance, frequency, capacitance, dielectric loss, Qm, heating, displacement gain, and electro-mechanical coupling factor. The experimental and theoretical research methods include Bode plots, thermal IR camera imaging, scanning laser vibrometry and coupled-field finite element analysis.

  1. EFFECT OF SOL CONCENTRATION AND SUBSTRATE TYPE ON MICROSTRUCTURE FORMATION OF PZT THIN FILMS

    Directory of Open Access Journals (Sweden)

    ĽUBOMÍR MEDVECKÝ

    2011-03-01

    Full Text Available Pb(Zr0.52Ti0.48O3 (PZT sols were prepared by a modified sol-gel route using both solvents - acetic acid and stabilizer solution (n-propanol : 1,2-propanediol in the rate 10 : 1. The sols were deposited by spin-coating onto platinized Al2O3 or SiO2/Si substrates. Results of SEM and XRD analyses confirmed, that the transformation of the amorphous PZT film to perovskite structure happened after sintering at 650°C. The mechanism of microstructure formation has described for morphologicaly different perovskite particle types in 1, 2 and 3-layered PZT thin films with thickness of 200-500 nm on used substrates. Three different PZT film microstructure types in dependence on the applied sol concentration were found. It was found, that the PZT/Pt/Al2O3 film microstructure at 1.0 M sol concentration was composed of two forms of perovskite particles, big rosette and irregular cuboidal particles. Small spherical particles and rosette structure were found in PZT/Pt/Si/SiO2 films.

  2. Crack detection of railway turnouts using PZT sensors (presentation video)

    Science.gov (United States)

    Ni, Yiqing; Li, Z. G.; Wu, F.

    2014-05-01

    Railway turnouts (railroad switches) are the weakest components of a rail track system. Cracks may occur in the railway turnouts due to cyclic loadings and impact loadings imposed by passing trains. It is of great significance to continuously monitor the health condition of the railway turnouts and promptly detect crack once it initiates. It is well-known that acoustic emission (AE) signals are generated when a crack initiates and propagates. Detecting the high-frequency AE signals by piezoelectric sensors can help identify the crack and its location. This paper reports the design and implementation of a PZT-based system for crack monitoring of railway turnouts. This online monitoring system is activated for signal collection by a trigger system when a train is arriving to pass through the instrumented railway turnout. It mainly detects the AE signals generated when a crack initiates during the train passage or when the initiated crack expands during the passage of a heavy haul wagon. This system has been installed on a railroad line for over one year and has successfully detected the damage occurring at a railroad switch during its service period. This paper also briefs a guided-wave-based system for monitoring of micro-cracks in rail tracks by integrating FBG and PZT sensors.

  3. Poling process optimization of piezo nano composite PZT/polimer

    Science.gov (United States)

    Ridlo, M. Rosyid; Lestari, Titik; Mardiyanto, Oemry, Achiar

    2013-09-01

    The objective of poling process is to make the electric dipole directions to be parallel in the inside perovskite crystal of piezo materials. In simply way, poling was carried out by giving the two sides of a piezo material by highly electrical potential. More parallel of electrical dipoles, it is more strength the piezo characteristics. The optimization involved control of temperature, time depth and the electrical voltage. The samples was prepared by solgel method with precursor tetrabutyl titanat Ti(OC4H9)4, zirconium nitrat Zr(NO3)4ṡ5H2O, Pb(CH3COO)2ṡ3H2O and solution ethylene glycol. Molar ratio Pb:Zr:Ti = 1,1:0,52:0,48 with concidering lossed Pb. Result of solgel process is nano powder PZT. The formed nano powder PZT was then mixed with polimer PVDF and pressed 10 MPa at 150 °C with the size 15 mm in diameter. After poling, piezoelectric constant d33 was measured. The highest d33 = 45 pC/N was found at poling parameters V = 5 kV/ mm, T = 120 °C dan time depth = 1 hours.

  4. Performance of PZT stacks under high-field electric cycling at various temperatures in heavy-duty diesel engine fuel injectors

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Hong [ORNL; Lin, Hua-Tay [ORNL; Stafford, Mr Randy [Cummins Inc., Columbus, Indiana

    2016-01-01

    Testing and characterization of large prototype lead zirconate titanate (PZT) stacks present substantial technical challenges to electronic systems. The work in this study shows that an alternative approach can be pursued by using subunits extracted from prototype stacks. Piezoelectric and dielectric integrity was maintained even though the PZT plate specimens experienced an additional loading process involved with the extraction after factory poling. Extracted 10-layer plate specimens were studied by an electric cycle test under an electric field of 3.0/0.0 kV/mm, 100 Hz to 108 cycles, both at room temperature (22 C) and at 50 C. The elevated temperature had a defined impact on the fatigue of PZT stacks. About 48 and 28% reductions were observed in the piezoelectric and dielectric coefficients, respectively, after 108 cycles at 50 C, compared with reductions of 25 and 15% in the respective coefficients at 22 C. At the same time, the loss tangent varied to a limited extent. The evolution of PZT electrode interfacial layers or nearby dielectric layers should account for the difference in the fatigue rates of piezoelectric and dielectric coefficients. But the basic contribution to observed fatigue may result from the buildup of a bias field that finally suppressed the motion of the domain walls. Finally, monitoring of dielectric coefficients can be an effective tool for on-line lifetime prediction of PZT stacks in service if a failure criterion is defined properly.

  5. Performance of PZT stacks under high-field electric cycling at various temperatures in heavy-duty diesel engine fuel injectors

    Science.gov (United States)

    Wang, Hong; Lee, Sung-Min; Lin, Hua-Tay; Stafford, Randy

    2016-04-01

    Testing and characterization of large prototype lead zirconate titanate (PZT) stacks present substantial technical challenges to electronic systems. The work in this study shows that an alternative approach can be pursued by using subunits extracted from prototype stacks. Piezoelectric and dielectric integrity was maintained even though the PZT plate specimens experienced an additional loading process involved with the extraction after factory poling. Extracted 10-layer plate specimens were studied by an electric cycle test under an electric field of 3.0/0.0 kV/mm, 100 Hz to 108 cycles, both at room temperature (22°C) and at 50°C. The elevated temperature had a defined impact on the fatigue of PZT stacks. About 48 and 28% reductions were observed in the piezoelectric and dielectric coefficients, respectively, after 108 cycles at 50°C, compared with reductions of 25 and 15% in the respective coefficients at 22°C. At the same time, the loss tangent varied to a limited extent. The evolution of PZT-electrode interfacial layers or nearby dielectric layers should account for the difference in the fatigue rates of piezoelectric and dielectric coefficients. But the basic contribution to observed fatigue may result from the buildup of a bias field that finally suppressed the motion of the domain walls. Finally, monitoring of dielectric coefficients can be an effective tool for on-line lifetime prediction of PZT stacks in service if a failure criterion is defined properly.

  6. Ferroelectric and Piezoelectric properties of (111) oriented lanthanum modified lead zirconate titanate film

    Energy Technology Data Exchange (ETDEWEB)

    Dutta, Soma, E-mail: som@nal.res.in; Antony Jeyaseelan, A.; Sruthi, S.

    2014-07-01

    Lanthanum modified lead zirconate titanate (PLZT) thick film with molecular formula of Pb{sub 0.92}La{sub 0.08}(Zr{sub 0.52}Ti{sub 0.48}){sub 0.98}O{sub 3} was grown preferentially along (111) direction on Pt/SiO{sub 2}/Si (platinum/silicon oxide/silicon) substrate by spin coating of chemical solution. The directional growth of the film was facilitated by platinum (Pt) (111) template and rapid thermal annealing. X-ray diffraction pattern and atomic force microscopy revealed the preferential growth of the PLZT film. The film was characterized for ferroelectric and detailed piezoelectric properties in a parallel plate capacitor (metal–PLZT–metal) configuration. Ferroelectric characterization of the film showed saturated hysteresis loop with remanent polarization and coercive electric field values of 10.14 μC/cm{sup 2} and 42 kV/cm, respectively, at an applied field of 300 kV/cm. Longitudinal piezoelectric coefficient (d{sub 33,f}) was measured by employing converse piezoelectric effect where electrical charge response and displacement were measured with electrical voltage excitation on the sample electrodes. The effective transverse piezoelectric coefficient (e{sub 31,f}) was derived from charge measurement with an applied mechanical excitation strain by using the four point bending method. d{sub 33,f} and e{sub 31,f} coefficients of PLZT films were found to be 380 pm/V and − 0.831 C/m{sup 2} respectively. - Highlights: • PLZT (111) film is prepared by spin coating of chemical sol on Pt (111) template. • Piezoelectric d{sub 33} value (380 pm/V) of PLZT film is found 20% higher than PZT. • Transverse piezocoefficient e{sub 31,f} of PLZT film is reported for the first time.

  7. Piezoelectric valve

    Science.gov (United States)

    Petrenko, Serhiy Fedorovich

    2013-01-15

    A motorized valve has a housing having an inlet and an outlet to be connected to a pipeline, a saddle connected with the housing, a turn plug having a rod, the turn plug cooperating with the saddle, and a drive for turning the valve body and formed as a piezoelectric drive, the piezoelectric drive including a piezoelectric generator of radially directed standing acoustic waves, which is connected with the housing and is connectable with a pulse current source, and a rotor operatively connected with the piezoelectric generator and kinematically connected with the rod of the turn plug so as to turn the turn plug when the rotor is actuated by the piezoelectric generator.

  8. Multiscale numerical study on ferroelectric nonlinear response of PZT thin films (Conference Presentation)

    Science.gov (United States)

    Wakabayashi, Hiroki; Uetsuji, Yasutomo; Tsuchiya, Kazuyoshi

    2017-06-01

    PZT thin films have excellent performance in deformation precision and response speed, so it is used widely for actuators and sensors of Micro Electro Mechanical System (MEMS). Although PZT thin films outputs large piezoelectricity at morphotropic phase bounfary (MPB), it shows a complicated hysteresis behavior caused by domain switching and structural phase transition between tetragonal and rhombohedral. In general, PZT thin films have some characteristic crystal morphologies. Additionally mechanical strains occur by lattice mismatch with substrate. Therefore it is important for fabrication and performance improvement of PZT thin films to understand the relation between macroscopic hysteresis response and microstructural changes. In this study, a multiscale nonlinear finite element simulation was proposed for PZT thin films at morphotropic phase boundary (MPB) on the substrate. The homogenization theory was employed for scale-bridging between macrostructure and microstructure. Figure 1 shows the proposed multiscale nonlinear simulation [1-3] based on the homogenization theory. Macrostructure is a homogeneous structure to catch the whole behaviors of actuators and sensors. And microstructure is a periodic inhomogeneous structure consisting of domains and grains. Macrostructure and microstructure are connected perfectly by homogenization theory and are analyzed by finite element method. We utilized an incremental form of fundamental constitutive law in consideration with physical property change caused by domain switching and structural phase transition. The developed multiscale finite element method was applied to PZT thin films with lattice mismatch strain on the substrate, and the relation between the macroscopic hysteresis response and microscopic domain switching and structural phase transition were investigated. Especially, we discuss about the effect of crystal morphologies and lattice mismatch strain on hysteresis response.

  9. Characteristics of magnetic force control device with magnetostrictive and piezoelectric laminate composite

    Science.gov (United States)

    Ueno, Toshiyuki; Qiu, Jinhao; Tani, Junji

    2003-08-01

    A magnetic force control device with laminate composite of giant magnetostrictive material (GMM) and piezo-electric material (PZT) is proposed. This magnetic force control is based on inverse magnetostrictive effect of a magnetic material, whereby the variation of stress applied on the material is converted to that of magnetic force via magnetic circuits. For the purpose of realizing the method in practical applications, disks of GMM and PZT are laminated to control the stress of GMM by electric field on PZT. Due to the capacitive properties of PZT, the device requires little electric energy hence generates no heat to maintain constant force. Furthermore compared with conventional electromagnetics, the device can be fabricated easily and in small size to be suitable for microactuators. This paper presents the principle of the magnetic force control by the lamination of GMM and PZT and investigates the static and dynamic characteristics of several devices to demonstrate their capabilities of the magnetic force control.

  10. An Unconventional Inchworm Actuator Based on PZT/ERFs Control Technology

    Science.gov (United States)

    Liu, Guojun; Zhang, Yanyan; Liu, Jianfang; Li, Jianqiao; Tang, Chunxiu; Wang, Tengfei; Yang, Xuhao

    2016-01-01

    An unconventional inchworm actuator for precision positioning based on piezoelectric (PZT) actuation and electrorheological fluids (ERFs) control technology is presented. The actuator consists of actuation unit (PZT stack pump), fluid control unit (ERFs valve), and execution unit (hydraulic actuator). In view of smaller deformation of PZT stack, a new structure is designed for actuation unit, which integrates the advantages of two modes (namely, diaphragm type and piston type) of the volume changing of pump chamber. In order to improve the static shear yield strength of ERFs, a composite ERFs valve is designed, which adopts the series-parallel plate compound structure. The prototype of the inchworm actuator has been designed and manufactured in the lab. Systematic test results indicate that the displacement resolution of the unconventional inchworm actuator reaches 0.038 μm, and the maximum driving force and velocity are 42 N, 14.8 mm/s, respectively. The optimal working frequency for the maximum driving velocity is 120 Hz. The complete research and development processes further confirm the feasibility of developing a new type of inchworm actuator with high performance based on PZT actuation and ERFs control technology, which provides a reference for the future development of a new type of actuator. PMID:27022234

  11. An Unconventional Inchworm Actuator Based on PZT/ERFs Control Technology.

    Science.gov (United States)

    Liu, Guojun; Zhang, Yanyan; Liu, Jianfang; Li, Jianqiao; Tang, Chunxiu; Wang, Tengfei; Yang, Xuhao

    2016-01-01

    An unconventional inchworm actuator for precision positioning based on piezoelectric (PZT) actuation and electrorheological fluids (ERFs) control technology is presented. The actuator consists of actuation unit (PZT stack pump), fluid control unit (ERFs valve), and execution unit (hydraulic actuator). In view of smaller deformation of PZT stack, a new structure is designed for actuation unit, which integrates the advantages of two modes (namely, diaphragm type and piston type) of the volume changing of pump chamber. In order to improve the static shear yield strength of ERFs, a composite ERFs valve is designed, which adopts the series-parallel plate compound structure. The prototype of the inchworm actuator has been designed and manufactured in the lab. Systematic test results indicate that the displacement resolution of the unconventional inchworm actuator reaches 0.038 μm, and the maximum driving force and velocity are 42 N, 14.8 mm/s, respectively. The optimal working frequency for the maximum driving velocity is 120 Hz. The complete research and development processes further confirm the feasibility of developing a new type of inchworm actuator with high performance based on PZT actuation and ERFs control technology, which provides a reference for the future development of a new type of actuator.

  12. An Unconventional Inchworm Actuator Based on PZT/ERFs Control Technology

    Directory of Open Access Journals (Sweden)

    Guojun Liu

    2016-01-01

    Full Text Available An unconventional inchworm actuator for precision positioning based on piezoelectric (PZT actuation and electrorheological fluids (ERFs control technology is presented. The actuator consists of actuation unit (PZT stack pump, fluid control unit (ERFs valve, and execution unit (hydraulic actuator. In view of smaller deformation of PZT stack, a new structure is designed for actuation unit, which integrates the advantages of two modes (namely, diaphragm type and piston type of the volume changing of pump chamber. In order to improve the static shear yield strength of ERFs, a composite ERFs valve is designed, which adopts the series-parallel plate compound structure. The prototype of the inchworm actuator has been designed and manufactured in the lab. Systematic test results indicate that the displacement resolution of the unconventional inchworm actuator reaches 0.038 μm, and the maximum driving force and velocity are 42 N, 14.8 mm/s, respectively. The optimal working frequency for the maximum driving velocity is 120 Hz. The complete research and development processes further confirm the feasibility of developing a new type of inchworm actuator with high performance based on PZT actuation and ERFs control technology, which provides a reference for the future development of a new type of actuator.

  13. Giant piezoelectric response in piezoelectric/dielectric superlattices due to flexoelectric effect

    Science.gov (United States)

    Liu, Chang; Wu, Huaping; Wang, Jie

    2016-11-01

    Flexoelectricity describes the linear response of electrical polarization to a strain gradient, which can be used to enhance the piezoelectric effect of piezoelectric material or realize the piezoelectric effect in nonpiezoelectric materials. Here, we demonstrate from thermodynamics theory that a giant piezoelectric effect exists in piezoelectric/dielectric superlattices due to flexoelectric effect. The apparent piezoelectric coefficient is calculated from the closed-form of analytical expression of the polarization distribution in the piezoelectric/dielectric superlattice subjected to a normal stress, in which the flexoelectric effect is included. It is found that there exists a strong nonlinear coupling between the flexoelectric and piezoelectric effects, which significantly enhances the apparent piezoelectric coefficient in the piezoelectric/dielectric superlattice. For a specific thickness ratio of the piezoelectric and dielectric layers, the enhanced apparent piezoelectric coefficient in the superlattice is ten times larger than that of its pure piezoelectric counterpart. The present work suggests an effective way to obtain giant apparent piezoelectric effect in piezoelectric/dielectric superlattices through flexoelectric effect.

  14. Rotor damage detection by using piezoelectric impedance

    Science.gov (United States)

    Qin, Y.; Tao, Y.; Mao, Y. F.

    2016-04-01

    Rotor is a core component of rotary machinery. Once the rotor has the damage, it may lead to a major accident. Thus the quantitative rotor damage detection method based on piezoelectric impedance is studied in this paper. With the governing equation of piezoelectric transducer (PZT) in a cylindrical coordinate, the displacement along the radius direction is derived. The charge of PZT is calculated by the electric displacement. Then, by the use of the obtained displacement and charge, an analytic piezoelectric impedance model of the rotor is built. Given the circular boundary condition of a rotor, annular elements are used as the analyzed objects and spectral element method is used to set up the damage detection model. The Electro-Mechanical (E/M) coupled impedance expression of an undamaged rotor is deduced with the application of a low-cost impedance test circuit. A Taylor expansion method is used to obtain the approximate E/M coupled impedance expression for the damaged rotor. After obtaining the difference between the undamaged and damaged rotor impedance, a rotor damage detection method is proposed. This method can directly calculate the change of bending stiffness of the structural elements, it follows that the rotor damage can be effectively detected. Finally, a preset damage configuration is used for the numerical simulation. The result shows that the quantitative damage detection algorithm based on spectral element method and piezoelectric impedance proposed in this paper can identify the location and the severity of the damaged rotor accurately.

  15. The effects of dimensional parameters on sensing and energy harvesting of an embedded PZT in a total knee replacement

    Science.gov (United States)

    Safaei, Mohsen; Anton, Steven R.

    2016-04-01

    Total Knee Replacement (TKR), one of the most common surgeries in the United States, is performed when the patient is experiencing significant amounts of pain or when knee functionality has become substantially degraded. Despite impressive recent developments, only about 85% of patients are satisfied with the pain reduction after one year. Therefore, structural health and performance monitoring are integral for intraoperative and postoperative feedback. In extension of the author's previous work, a new configuration for implementation of piezoelectric transducers in total knee replacement bearings is proposed and FEA modeling is performed to attain appropriate sensing and energy harvesting ability. The predicted force transmission ratio to the PZT (ratio of force applied to the bearing to force transferred to the embedded piezoelectric transducer) is about 6.2% compared to about 5% found for the previous encapsulated design. Dimensional parameters of the polyethylene bearing including the diameter and depth of the PZT pocket as well as the placement geometry of the PZT transducer within the bearing are hypothesized as the most influential parameters on the performance of the designed system. The results show a small change of 1% and 2.3% in the output of the system as a result of variation in the PZT location and pocket diameter, respectively. Whereas, the output of the system is significantly sensitive to the pocket depth; a pocket 0.01 mm deeper than the PZT transducer leads to no force transmission, and a pocket 0.15 mm shallower leads to full load transmission to the PZT. In order to develop a self-powered sensor, the amount of energy harvested from tibial forces for the proposed geometry is investigated.

  16. Displacement and resonance behaviors of a piezoelectric diaphragm driven by a double-sided spiral electrode

    KAUST Repository

    Shen, Zhiyuan

    2012-04-03

    This paper presents the design of a lead zirconate titanate (PZT) diaphragm actuated by double-sided patterned electrodes. Au/Cr electrodes were deposited on bulk PZT wafers by sputtering while patterned by a lift-off process. SU-8 thick film was used to form the structural layer. Double-spiral electrode induced in-plane poling and piezoelectric elongation are converted to an out-of-plane displacement due to the confined boundary condition. The influence of different drive configurations and electrode parameters on deflection has been calculated by finite element methods (FEM) using a uniform field model. Impedance and quasi-static displacement spectra of the diaphragm were measured after poling. Adouble-sided patterned electrode diaphragm can be actuated by more drive configurations than a single-sided one. Compared with a single-sided electrode drive, a double-sided out-of-phase drive configuration increases the coupling coefficient of the fundamental resonance from 7.6% to 11.8%. The displacement response of the diaphragm increases from 2.6 to 8.6nmV 1. Configurations including the electric field component perpendicular to the poling direction can stimulate shear modes of the diaphragm. © 2012 IOP Publishing Ltd.

  17. Nanogenerators consisting of direct-grown piezoelectrics on multi-walled carbon nanotubes using flexoelectric effects

    Science.gov (United States)

    Han, Jin Kyu; Jeon, Do Hyun; Cho, Sam Yeon; Kang, Sin Wook; Yang, Sun A.; Bu, Sang Don; Myung, Sung; Lim, Jongsun; Choi, Moonkang; Lee, Minbaek; Lee, Min Ku

    2016-07-01

    We report the first attempt to prepare a flexoelectric nanogenerator consisting of direct-grown piezoelectrics on multi-walled carbon nanotubes (mwCNT). Direct-grown piezoelectrics on mwCNTs are formed by a stirring and heating method using a Pb(Zr0.52Ti0.48)O3 (PZT)-mwCNT precursor solution. We studied the unit cell mismatch and strain distribution of epitaxial PZT nanoparticles, and found that lattice strain is relaxed along the growth direction. A PZT-mwCNT nanogenerator was found to produce a peak output voltage of 8.6 V and an output current of 47 nA when a force of 20 N is applied. Direct-grown piezoelectric nanogenerators generate a higher voltage and current than simple mixtures of PZT and CNTs resulting from the stronger connection between PZT crystals and mwCNTs and an enhanced flexoelectric effect caused by the strain gradient. These experiments represent a significant step toward the application of nanogenerators using piezoelectric nanocomposite materials.

  18. Instantaneous crack detection using dual PZT transducers

    Science.gov (United States)

    Kim, Seung Bum; Sohn, Hoon

    2008-03-01

    A new guided wave based nondestructive testing (NDT) technique is developed to detect crack damage in metallic plates commonly used in aircraft without using prior baseline data or a predetermined decision boundary. In conventional guided wave based techniques, damage is often identified by comparing the "current" data obtained from a potentially damaged condition of a structure with the "past" baseline data collected at the pristine condition of the structure. However, it has been reported that this type of pattern comparison with the baseline data can lead to increased false alarms due to its susceptibility to varying operational and environmental conditions of the structure. In order to tackle this issue, a reference-free damage detection technique is previously developed using two pairs of collocated lead zirconate titanate transducers (PZTs) placed on both sides of a plate. In this study, this reference-free technique is further advanced so that the PZT transducers can be placed only on one side of the specimen. Crack formation creates Lamb wave mode conversion due to a sudden change in the thickness of the structure. Then, the proposed technique instantly detects the appearance of the crack by extracting this mode conversion from the measured Lamb waves. This study suggests a reference-free statistical approach that enables damage classification using only the current data set. Numerical and experimental results are presented to demonstrate the applicability of the proposed technique to instantaneous crack detection.

  19. NMR quadruopole spectra of PZT from first-principles

    Science.gov (United States)

    Mao, Dandan; Walter, Eric J.; Krakauer, Henry

    2006-03-01

    High performance piezoelectric materials are disordered alloys, so it can be difficult to determine the local atomic geometry. Recently, high field NMR measurements have shown great promise as a microscopic probe of ABO3 perovskite-based alloys by their ability to resolve line-splittings due to nuclear quadrupolar coupling with the electric field gradient (EFG) at the nucleus. We report first-principles LDA calculations of the EFG's in monoclinic and tetragonal Pb(Zr0.5Ti0.5)O3 systems using the linear augmented planewave (LAPW) method, and we compute NMR static powder spectra for ^91Zr, ^47Ti, and ^17O atoms as a function of applied strain. With decreasing c/a ratio PZT converts from tetragonal to monoclinic symmetry. We observe that the calculated NMR spectra show dramatic deviations with decreasing c/a from that in tetragonal P4mm well before the electric polarization begins to rotate away from the [001] direction. This indicates that NMR measurements can be a very accurate probe of local structural changes in perovskite piezoelectrics. G. L. Hoatson, D. H. Zhou, F. Fayon, D. Massiot, and R. L. Vold, Phys. Rev. B, 66, 224103 (2002).

  20. Microstructure and Electromechanical Properties in PMnN-PZT Ceramics Sintered at Different Temperatures

    Institute of Scientific and Technical Information of China (English)

    Baoshan LI; Zhigang ZHU; Guorong LI; Aili DING

    2005-01-01

    The microstructure and piezoelectric properties of Pb[(Zr0.52Ti0.48)0.95(Mn1/3Nb2/3)0.05]O3 (PMnN-PZT) ceramics have been investigated at different sintering temperatures from 1070℃ to 1280℃. The experimental results suggest that grain sizes and electromechanical properties of the ceramics show strong sintering temperature dependences.Double polarization to electric field (P-E) loops of the PMnN-PZT ceramics are assumed to be the result of the pinning effect of the defect dipoles. The results obtained through X-ray photoelectron spectrum suggest that sintering temperature affects valence of the Mn ion and quantity of oxygen vacancies. Hence, a proper explanation is proposed to illustrate the fluctuation of mechanical quality factor (Qm) due to the sintering temperature.

  1. Polarization characterization of PZT disks and of embedded PZT plates by thermal wave methods

    Energy Technology Data Exchange (ETDEWEB)

    Eydam, Agnes, E-mail: Agnes.Eydam@tu-dresden.de; Suchaneck, Gunnar, E-mail: Agnes.Eydam@tu-dresden.de; Gerlach, Gerald [Technische Universität Dresden, Solid State Electronics Laboratory, Helmholtzstraße 18, 01062 Dresden (Germany); Esslinger, Sophia; Schönecker, Andreas; Neumeister, Peter [Fraunhofer Institute for Ceramic Technologies and Systems, Winterbergstraße 28, 01277 Dresden (Germany)

    2014-11-05

    In this work, the thermal wave method was applied to characterize PZT disks and embedded PZT plates with regard to the polarization magnitude and spatial homogeneity. The samples were exposed to periodic heating by means of a laser beam and the pyroelectric response was determined. Thermal relaxation times (single time constants or distributions of time constants) describe the heat losses of the PZT samples to the environment. The resulting pyroelectric current spectrum was fitted to the superposition of thermal relaxation processes. The pyroelectric coefficient gives insight in the polarization distribution. For PZT disks, the polarization distribution in the surface region showed a characteristic decrease towards the electrodes.

  2. A nonlinear model for magnetocapacitance effect in PZT-ring/Terfenol-D-strip magnetoelectric composites

    Science.gov (United States)

    Zhang, Juanjuan; Wen, Jianbiao; Gao, Yuanwen

    2016-06-01

    In previous works, most of them employ a linear constitutive model to describe magnetocapacitance (MC) effect in magnetoelectric (ME) composites, which lead to deficiency in their theoretical results. In view of this, based on a nonlinear magnetostrictive constitutive relation and a linear piezoelectric constitutive relation, we establish a nonlinear model for MC effect in PZT-ring/Terfenol-D-strip ME composites. The numerical results in this paper coincide better with experimental data than that of a linear model, thus, it's essential to utilize a nonlinear constitutive model for predicting MC effect in ME composites. Then the influences of external magnetic fields, pre-stresses, frequencies, and geometric sizes on the MC effect are discussed, respectively. The results show that the external magnetic field is responsible for the resonance frequency shift. And the resonance frequency is sensitive to the ratio of outer and inner radius of the PZT ring. Moreover, some other piezoelectric materials are employed in this model and the corresponding MC effects are calculated, and we find that different type of piezoelectric materials affect the MC effect obviously. The proposed model is more accurate for multifunction devices designing.

  3. Estimate of the changes in the characteristics of a PZT vibrator under a space environment

    Science.gov (United States)

    Kim, Jungsoon; Lee, Sanghoon; Kim, Moojoon

    2015-03-01

    To utilize lead zirconate titanate (PZT) vibrators in the aerospace industry, we formulate the changes in the characteristics of the vibrator for the transverse mode and the thickness mode as functions of the temperature. For practical use, we adopted a few linear functions and a square function as regression functions in order to estimate the characteristics of the commercialized PZT-5 series of ceramics. The input admittance characteristics were calculated using the characteristic functions suggested in this study, and the results showed good agreement with the measured ones.

  4. Optical properties of PZT thin films deposited on a ZnO buffer layer

    OpenAIRE

    Schneider, T.; Leduc, D; Cardin, J.; LUPI, C; Barreau, N; Gundel, H.

    2007-01-01

    International audience; The optical properties of lead zirconate titanate (PZT) thin films deposited on ZnO were studied by m-lines spectroscopy. In order to retrieve the refractive index and the thickness of both layers from the m-lines spectra, we develop a numerical algorithm for the case of a two-layer system and show its robustness in the presence of noise. The sensitivity of the algorithm of the two-layer model allows us to relate the observed changes in the PZT refractive index to the ...

  5. 共晶键合与减薄技术的压电能量采集器%Fabrication of micro piezoelectric energy harvester using eutectic bonding and polishing technology

    Institute of Scientific and Technical Information of China (English)

    李以贵; 颜平; 黄远; 杉山进

    2016-01-01

    This paper presents an energy harvester which operates at less than 1 kHz and consists of a mi-cro silicon-lead zirconate titanate (Si-PZT)cantilever and a nickel mass block on the cantilever.The energy har-vester is a device that can convert the ambient mechanical vibration into electrical energy employing the piezoe-lectric effect.The micro piezo cantilever structure was fabricated by eutectic bonding using gold thin film as a bonding layer.A PZT mechanical polishing process was used to thin the bulk PZT.The thinnest PZT film ob-tained was 8 μm.A nickel mass block (2 mm×2 mm×0.6 mm)was fabricated using micro electroforming process.By optimizing the bonding and polishing processes,the thickness of fabricated Si-PZT cantilever was a-bout 71 μm,and the thicknesses of the silicon beam and the PZT beam were about 47 μm and 24 μm,respec-tively.The results showed that the AC output voltage of the micro energy harvester was around 958 mV at the resonant frequency of 950 Hz and the acceleration of 1.0g .%采用微硅-锆钛酸铅(Si-PZT)悬臂梁结构并在悬臂梁末端附加镍质量块,构成可以工作于低频环境(小于1000 Hz)的微压电能量采集器,一种利用压电效应将环境振动能转换为电能的器件。利用金薄膜作为中间层的共晶键合技术和 PZT研磨减薄技术制备了微压电悬臂梁结构,PZT 减薄实验最好结果为减薄至8μm。镍质量块(2 mm×2 mm×0.6 mm)采用微电铸工艺制备。通过对硅片与块材 PZT 的共晶键合工艺与 PZT 减薄技术的研究,制备出总厚度约为71μm 的 Si-PZT 悬臂梁结构,其中硅梁厚约为47μm,PZT 梁厚约为24μm。制备的微压电振动能量采集器样品的测试结果表明:在谐振频率为950 Hz,1.0g 加速度激励条件下,其交流输出峰值电压可达958 mV。

  6. Magnetoelectric Responses of GMM/PZT/GMM Laminate Composite in Longitudinal Vibration%GMM/PZT/GMM层合材料的纵振磁电响应

    Institute of Scientific and Technical Information of China (English)

    文玉梅; 周丽萍; 李平; 卞雷祥

    2009-01-01

    The adhesive layers and the mechanical losses of materials in giant magnetostrictive material (GMM) and piezoelectric Pb(Zr,Ti)O3 (PZT) laminate composites are vital factors to impact final magneto-electric responses. The effects of the adhesive layer resulting from the shear and longitudinal deformation were considered in the governing motion equations of GMM/PZT/GMM composites, which were established based on Hamilton's principle. The coefficients in the motion equations were specified by the material parameters. To introduce the material losses into the analysis, the mechanical parameters including the compliances of magnetostrictive and piezoelectric materials were represented as complexes. Through the motion equations along with the boundary conditions and the constitutive equations of magnetostrictive/piezoelectric effects, the magnetoelectric responses over frequency and the natural frequencies were provided. The numerical calculations of the magnetoelectric responses in GMM/PZT/GMM laminate composite was presented. By comparing the theoretical magnetoelectric response with the experimental result,shows that the introduction of material losses can provide more acceptable prediction of the magnetoelectric performances.%层状复合结构层间胶层和复合材料的机械损耗是影响层状磁电复合材料磁电响应的重要因素.为了考虑层间胶层的作用,包括其纵向变形和剪切变形产生的效果,应用Hamilton原理建立层状复合结构的运动方程,并用复柔顺系数来反映材料的机械损耗特性.结合层状复合结构的边界条件和磁致伸缩/压电本构方程,就可以得到考虑了胶层作用和材料损耗时,复合结构的固有频率和磁电响应.对GMM(超磁致伸缩材料)/PZT(压电材料)/GMM结构的磁电响应进行了数值计算,将计算结果与实验结果进行了比较,证明考虑胶层作用并引入材料的损耗能够更准确预测复合材料的磁电换能特性.

  7. Electroactive properties of flexible piezoelectric composites

    Directory of Open Access Journals (Sweden)

    Walter Katsumi Sakamoto

    2001-07-01

    Full Text Available A flexible piezoelectric composite with 0-3 connectivity, made from Lead Zirconate Titanate (PZT powder and vegetable-based polyurethane (PU, was doped with small amount of semiconductor powder. As a result a composite with 0-0-3 connectivity was obtained. The nature of absorption and steady state electrical conduction and the dielectric behaviour have been studied for this ceramic/polymer composite. The dielectric loss processes of the composite were observed to be dominated by those the polymer. Adding a semiconductor phase in the composite the electrical conductivity can be controlled and a continuous electric flux path could be created between the PZT grains. This composite may be poled at low voltage and in shorter time compared with composites without a conductive phase.

  8. Monte Carlo Simulation Study of Diffuse Scattering in PZT, Pb(Zr,Ti)O3

    Science.gov (United States)

    Welberry, T. R.; Goossens, D. J.; Withers, R. L.; Baba-Kishi, K. Z.

    2010-05-01

    Transverse polarized diffuse streaks have been observed in diffraction patterns of Pb(Zr1- x Ti x )O3 (PZT) ceramics for compositions ranging from x = 0.3 (rhombohedral phase) to x = 0.7 (tetragonal phase) including the important morphotropic phase boundary (MPB) region ( x = 0.48). The streaks correspond to diffuse planes of scattering in three dimensions, and these are oriented normal to the (cubic) piezo-electric properties of the material, but its presence requires the currently accepted models for the average structure to be reassessed.

  9. Effect of carbon nanotubes on properties of cement-sand-based piezoelectric composites

    Science.gov (United States)

    Kim, Sunjung; Zhao, Ping; Enemuoh, Emmanuel

    2015-04-01

    Carbon Nanotubes (CNTs) were dispersed in a cement-sand-based piezoelectric smart composite as conductive fillers to improve its poling efficiency, leading to a desirable piezoelectric effect. By introducing a small amount of CNTs, continuous electric networks between Lead Zirconate Titanate (PZT) particles were created, thus making the composite poling easier. Specimens were prepared by mixing PZT powders, Portland cement and sand with CNTs, followed by pressing it with a load frame system. The effect of quantity of CNTs ranging from 0 to 1.0 volume percent on properties of the composite, including its piezoelectric coefficient, dielectric constant and loss, and sensing effects, were characterized. It was found that the addition of CNTs facilitated effective poling at room temperature and improved the piezoelectric and dielectric properties of the composite. The composite modified by CNTs achieved optimal properties when the CNTs content was 0.7 vol.%.

  10. Incorporation of piezoelectric Pb(Zr,Ti)O3 fibers into ceramic/polymer composites

    Science.gov (United States)

    Safari, Ahmad; Janas, Victor; Jadidian, Bahram; French, Jonathan D.; Weitz, Gregory E.; Luke, John E.; Cass, Bud

    1996-05-01

    The processing of Pb(Zr,Ti)O3, or PZT, fiber and fiber/polymer composites for transducer applications is discussed. Green PZT fibers, 80 to 100 micrometers in diameter, were formed at Advanced Cerametrics, Inc., using the Viscous Suspension Spinning Process (VSSP). In this process, fine PZT powder is intimately mixed with polymer precursor by high shear mixing. The powder and precursor mixture is spun through a spinneret into a coagulation bath to form fibers. The fibers are washed, dried, and collected on a spool. Yarns containing between 10 and 500 individual fibers were collimated by applying a polymeric sizing to the yarns, and passing the yarns through sizing dies. Yarn bundle tightness and flexibility were controlled by the sizing chemistry. Continuous green yarns were cut to short lengths, or woven in different architectures to create composites with novel microstructures. The short yarns were fired to product PZT straight rods for `pick and place' piezoelectric composites. The woven structures were heat treated and backfilled with polymer to create composites with 1-3, 2-3, and 3-3 connectivity. After heat treatment, the diameter of the individual PZT fibers was 10 to 20 micrometers . Electromechanical characteristics of a number of composites were determined, and will be reported. The PZT VSSP fibers can be used to form fine-scale, large area piezoelectric fiber/polymer composites for use in hydrophones, transducers for medical ultrasonic imaging and non-destructive evaluation, and as sensors and actuators in vibration and noise control.

  11. Analysis of a permeable interface crack in elastic dielectric/piezoelectric bimaterials

    Institute of Scientific and Technical Information of China (English)

    Qun Li; Yiheng Chen

    2007-01-01

    A permeable interface crack between elastic dielectric material and piezoelectric material is studied based on the extended Stroh's formalism. Motivated by strong engi-neering demands to design new composite materials, the authors perform numerical analysis of interface crack tip sin-gularities and the crack tip energy release rates for 35 types of dissimilar bimaterials, respectively, which are constructed by five kinds of elastic dielectric materials: Epoxy, Poly-mer, A1203, SiC, and Si3N4 and seven kinds of practical piezoelectric ceramics: PZT-4, BaTiO3, PZT-5H, PZT-6B,PZT-7A, P-7, and PZT-PIC 151, respectively. The elastic dielectric material with much smaller permittivity than com-mercial piezoelectric ceramics is treated as a special trans-versely isotropic piezoelectric material with extremely small piezoelectricity. The present investigation shows that the structure of the singular field near the permeable interface crack tip consists of three singularities: r-1/2±iε and r-1/2,which is quite different from that in the impermeable inter-face crack. It can be concluded that different far field load-ing cases have significant influence on the near-tip fracture behaviors of the permeable interface crack. Based on the present theoretical treatment and numerical analysis, the elec-tric field induced crack growth is well explained, which pro-vides a better understanding of the failure mechanism induced from interface crack growth in elastic dielectric/piezoelectric bimaterials.

  12. Piezoelectric Film.

    Science.gov (United States)

    Garrison, Steve

    1992-01-01

    Presents activities that utilize piezoelectric film to familiarize students with fundamental principles of electricity. Describes classroom projects involving chemical sensors, microbalances, microphones, switches, infrared sensors, and power generation. (MDH)

  13. A piezoelectric linear ultrasonic motor with the structure of a circular cylindrical stator and slider

    Science.gov (United States)

    Sun, Dongming; Wang, Sheng; Sakurai, Junpei; Choi, Kee-Bong; Shimokohbe, Akira; Hata, Seiichi

    2010-04-01

    A piezoelectric linear ultrasonic motor is proposed, with a cylindrical stator and slider structure. The length and diameter of the motor are about 10 and 1.5 mm, respectively. The stator consists of two piezoelectric ceramic (PZT) tubes connected by a thin film metallic glass (TFMG) pipe. The stator is designed based on theoretical analyses and finite element method (FEM) simulation. The traveling wave propagation is obtained in the FEM simulation under the proper geometrical sizes, suitable boundary conditions and driving voltage signals. The trajectories of particles on the TFMG pipe are elliptical motion. In the experiment, a 25 µm thick TFMG pipe is fabricated using the rotating magnetron sputtering technique and the vibration characteristics of the stator are measured by a laser Doppler vibrometer (LDV) system. Bidirectional motion of the slider is observed around 600 kHz, the maximum velocity is near to 40 mm s - 1 at 50 Vp-p for the loose slider and the maximum output force is 6 mN at 70 Vp-p for the tight slider.

  14. Self-vibration cancellation of a novel bi-directional magnetized NdFeB/magnetostrictive/piezoelectric laminate

    Science.gov (United States)

    Leung, Chung Ming; Wang, Feifei; Wang, Ya

    2016-06-01

    A novel magnetoelectric (ME) laminated composite structure is proposed in this work, aiming to provide a good self-vibration cancellation performance under the magnetic field detection environment. The proposed structure consists of two Terfenol-D magnetostrictive alloy plates which are revised and length-magnetized by two NdFeB magnets bonded on the top surface of a thickness-polarized Pb(Zr, Ti)O3 (PZT) ceramic plate with separate electrodes. Experiments have shown that great vibration suppression up to 44 dB under harmonic disturbance was observed. The ME coefficient of the proposed structure also reaches up to ˜29 mV/Oe at non-resonance frequency and 758 mV/Oe at resonance frequency of 79 kHz which is ˜2 times larger than the traditional L-T Terfenol-D/PZT bilayer configuration of the same scale. Such performance improvement is achieved based on the bi-directional magnetic field bias (HBias) of two NdFeB magnets in magnetostrictive layer, internal in-series electrical wire connection in piezoelectric layer. The proposed design has great potential to be used for industrial applications associated with heavy environmental vibration noise.

  15. PMN-PT nanowires with a very high piezoelectric constant.

    Science.gov (United States)

    Xu, Shiyou; Poirier, Gerald; Yao, Nan

    2012-05-09

    A profound way to increase the output voltage (or power) of the piezoelectric nanogenerators is to utilize a material with higher piezoelectric constants. Here we report the synthesis of novel piezoelectric 0.72Pb(Mg(1/3)Nb(2/3))O(3)-0.28PbTiO(3) (PMN-PT) nanowires using a hydrothermal process. The unpoled single-crystal PMN-PT nanowires show a piezoelectric constant (d(33)) up to 381 pm/V, with an average value of 373 ± 5 pm/V. This is about 15 times higher than the maximum reported value of 1-D ZnO nanostructures and 3 times higher than the largest reported value of 1-D PZT nanostructures. These PMN-PT nanostructures are of good potential being used as the fundamental building block for higher power nanogenerators, high sensitivity nanosensors, and large strain nanoactuators.

  16. Piezoelectric Materials Synthesized by the Hydrothermal Method and Their Applications

    Directory of Open Access Journals (Sweden)

    Takeshi Morita

    2010-12-01

    Full Text Available Synthesis by the hydrothermal method has various advantages, including low reaction temperature, three-dimensional substrate availability, and automatic polarization alignment during the process. In this review, powder synthesis, the fabrication of piezoelectric thin films, and their applications are introduced. A polycrystalline lead zirconate titanate (PZT thin film was applied to a micro ultrasonic motor, and an epitaxial lead titanate (PbTiO3 thin film was estimated as a ferroelectric data storage medium. Ferroelectric and piezoelectric properties were successfully obtained for epitaxial PbTiO3 films. As lead-free piezoelectric powders, KNbO3 and NaNbO3 powders were synthesized by the hydrothermal method and sintered together to form (K,NaNbO3 ceramics, from which reasonable piezoelectric performance was achieved.

  17. Plate-like structure health monitoring based on ultrasonic guided wave technology by using bonded piezoelectric ceramic wafers

    Science.gov (United States)

    Liu, Zenghua; Zhao, Jichen; He, Cunfu; Wu, Bin

    2008-11-01

    Piezoelectric ceramic wafers are applied for the excitation and detection of ultrasonic guided waves to determine the health state of plate-like structures. Two PZT wafers, whose diameter is 11mm and thickness is 0.4mm respectively, are bonded permanently on the surface of a 1mm thick aluminum plate. One of these wafers is actuated by sinusoidal tone burst at various frequencies ranging from 100kHz to 500kHz, the other one is used as a receiver for acquiring ultrasonic guided wave signals. According to the amplitudes and shapes of these received signals, guided wave modes and their proper frequency range by using these wafers are determined. For the improvement of the signal-to-noise ratio, the Daubechies wavelet of order 40 is used for signal denoising as the mother wavelet. Furthermore, the detection of an artificial cylindrical through-hole defect is achieved by using S0 at 300kHz. Experimental results show that it is feasible and effective to detect defects in plate-like structures based on ultrasonic guided wave technology by using bonded piezoelectric ceramic wafers.

  18. A Traveling Wave Type of Piezoelectric Ultrasonic Bidirectional Linear Microactuator

    Science.gov (United States)

    Sun, Dongming; Wang, Sheng; Sakurai, Junpei; Hata, Seiichi; Choi, Kee-Bong; Shimokohbe, Akira

    2009-04-01

    A piezoelectric ultrasonic microactuator is presented, with a cylindrical stator and slider structure. The length and diameter of the microactuator are about 10 and 1.5 mm, respectively. The stator consists of two piezoelectric ceramic (PZT) tubes connected by a thin film metallic glass (TFMG) pipe, which is fabricated using the rotating magnetron sputtering technique. Traveling wave propagation is generated on the TFMG pipe in finite element method (FEM) simulations and also observed in the measurement. Bi-directional motion of the slider was observed around 600 kHz, and the maximum velocity was about 40 mm/s at 25 V.

  19. High Pressure Hydrogen Materials Compatibility of Piezoelectric Films

    Energy Technology Data Exchange (ETDEWEB)

    Alvine, Kyle J.; Shutthanandan, V.; Bennett, Wendy D.; Bonham, Charles C.; Skorski, Daniel C.; Pitman, Stan G.; Dahl, Michael E.; Henager, Charles H.

    2010-12-02

    Abstract: Hydrogen is being considered as a next-generation clean burning fuel. However, hydrogen has well known materials issues, including blistering and embrittlement in metals. Piezoelectric materials are used as actuators in hydrogen fuel technology. We present studies of materials compatibility of piezoelectric films in a high pressure hydrogen environment. Absorption of high pressure hydrogen was studied with Elastic Recoil Detection Analysis (ERDA) and Rutherford Back Scattering (RBS) in lead zirconate titanate (PZT) and barium titanate (BTO) thin films. Hydrogen surface degradation in the form of blistering and Pb mixing was also observed.

  20. Universal phase diagram for high-piezoelectric perovskite systems

    NARCIS (Netherlands)

    Cox, D.E.; Noheda, B.; Shirane, G.; Uesu, Y.; Fujishiro, K.; Yamada, Y.

    2001-01-01

    Strong piezoelectricity in perovskite-type PbZn1-xTixO3 (PZT) and Pb(Zn1/3Nb2/3)O3–PbTiO3 (PZN–PT) systems is generally associated with the existence of a morphotropic phase boundary (MPB) separating regions with rhombohedral and tetragonal symmetry. An x-ray study of PZN–9% PT has revealed the pres

  1. Tonpilz Underwater Acoustic Transducer Integrating Lead-free Piezoelectric Material

    Science.gov (United States)

    Rouffaud, Rémi; Granger, Christian; Hladky-Hennion, Anne-Christine; Thi, Mai Pham; Levassort, Franck

    A Tonpilz transducer based on lead-free piezoelectric material was fabricated, modeled and characterized. The stack is composed of two rings of doped BaTiO3. This composition was initially chosen due to good electromechanical performance (kt at 40%) and high mechanical quality factor (Qm over 500). Comparison of the displacement at the center of the head mass was performed with a PZT-based Tonpilz with the same design for a center frequency at 22 kHz.

  2. Modeling and characterization of dielectrophoretically structured piezoelectric composites using piezoceramic particle inclusions with high aspect ratios

    NARCIS (Netherlands)

    Ende, D.A. van den; Maier, R.A.; Neer, P.L.M.J. van; Zwaag, S. van der; Randall, C.A.; Groen, W.A.

    2013-01-01

    In this work, the piezoelectric properties at high electric fields of dielectrophoretically aligned PZT - polymer composites containing high aspect ratio particles (such as short fibers) are presented. Polarization and strain as a function of electric field are evaluated. The properties of the compo

  3. Vibration piezoelectric energy harvester with multi-beam

    Directory of Open Access Journals (Sweden)

    Yan Cui

    2015-04-01

    Full Text Available This work presents a novel vibration piezoelectric energy harvester, which is a micro piezoelectric cantilever with multi-beam. The characteristics of the PZT (Pb(Zr0.53Ti0.47O3 thin film were measured; XRD (X-ray diffraction pattern and AFM (Atomic Force Microscope image of the PZT thin film were measured, and show that the PZT (Pb(Zr0.53Ti0.47O3 thin film is highly (110 crystal oriented; the leakage current is maintained in nA magnitude, the residual polarisation Pr is 37.037 μC/cm2, the coercive field voltage Ec is 27.083 kV/cm, and the piezoelectric constant d33 is 28 pC/N. In order to test the dynamic performance of the energy harvester, a new measuring system was set up. The maximum output voltage of the single beam of the multi-beam can achieve 80.78 mV under an acceleration of 1 g at 260 Hz of frequency; the maximum output voltage of the single beam of the multi-beam is almost 20 mV at 1400 Hz frequency.

  4. Vibration piezoelectric energy harvester with multi-beam

    Energy Technology Data Exchange (ETDEWEB)

    Cui, Yan, E-mail: yanc@dlut.edu.cn; Zhang, Qunying, E-mail: zhangqunying89@126.com; Yao, Minglei, E-mail: yaomingleiok@126.com [Key Laboratory for Precision and Non-traditional Machining Technology of the Ministry of Education, Dalian University of Technology, 116024, Dalian, Liaoning Province (China); Dong, Weijie, E-mail: dongwj@dlut.edu.cn [School of Electronic and Information Engineering, Dalian University of Technology, 116024, Dalian, Liaoning Province (China); Gao, Shiqiao, E-mail: gaoshq@bit.edu.cn [State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, 100081, Beijing Province (China)

    2015-04-15

    This work presents a novel vibration piezoelectric energy harvester, which is a micro piezoelectric cantilever with multi-beam. The characteristics of the PZT (Pb(Zr{sub 0.53}Ti{sub 0.47})O{sub 3}) thin film were measured; XRD (X-ray diffraction) pattern and AFM (Atomic Force Microscope) image of the PZT thin film were measured, and show that the PZT (Pb(Zr{sub 0.53}Ti{sub 0.47})O{sub 3}) thin film is highly (110) crystal oriented; the leakage current is maintained in nA magnitude, the residual polarisation Pr is 37.037 μC/cm{sup 2}, the coercive field voltage Ec is 27.083 kV/cm, and the piezoelectric constant d{sub 33} is 28 pC/N. In order to test the dynamic performance of the energy harvester, a new measuring system was set up. The maximum output voltage of the single beam of the multi-beam can achieve 80.78 mV under an acceleration of 1 g at 260 Hz of frequency; the maximum output voltage of the single beam of the multi-beam is almost 20 mV at 1400 Hz frequency. .

  5. Extrinsic coefficient charcterisation of PZT ceramics near the morphotropic phase boundary

    Directory of Open Access Journals (Sweden)

    Albareda, A.

    2006-06-01

    Full Text Available PZT ceramics with high piezoelectric coefficients have high extrinsic contributions. This extrinsic behaviour, which is related to the domain wall movement, produces high non-linear effects that are sometimes inconvenient, for example when it increases the losses in power devices. The relation between extrinsic behaviour and non-linearities could be used to provide a good extrinsic characterization of materials in order to optimise the piezoelectric devices. In all cases the physical explanation of the behaviour is sought. The aim of this work is to study the dependence of the linear and non-linear dielectric, piezoelectric and mechanical coefficients on the Ti fraction in PZT ceramic compositions near the morphotropic phase boundary (MPB. The dependence of these coefficients on the defect concentration is also analysed. Hard ceramics belonging to Ferroperm Piezoceramics, with two different acceptor dopant levels, high and low, have been measured.

    Las cerámicas PZT con coeficientes piezoeléctricos elevados poseen contribuciones extrínsecas grandes. Este comportamiento extrínseco, relacionado con el movimiento de las paredes de los dominios, comporta efectos no lineales grandes que no siempre son deseables, por ejemplo, al incrementar las pérdidas de los dispositivos piezoeléctricos. Esta correspondencia entre efectos extrínsecos y no linealidades puede ser utilizada para caracterizar las cerámicas con el fin de optimizar sus propiedades piezoeléctricas. En todos los casos se busca una interpretación física de los resultados obtenidos. El objetivo de este trabajo es el estudio de la dependencia de los coeficientes lineales y no lineales dieléctricos, piezoeléctricos y elásticos con la fracción de Ti en cerámicas PZT con composiciones de Zr-Ti cerca de la transición de fase morfotrópica (MPB. También se analiza la dependencia de estos coeficientes con la concentración de impurezas, utilizando para ello cerámicas de

  6. Flexible energy harvesting from hard piezoelectric beams

    Science.gov (United States)

    Delnavaz, Aidin; Voix, Jérémie

    2016-11-01

    This paper presents design, multiphysics finite element modeling and experimental validation of a new miniaturized PZT generator that integrates a bulk piezoelectric ceramic onto a flexible platform for energy harvesting from the human body pressing force. In spite of its flexibility, the mechanical structure of the proposed device is simple to fabricate and efficient for the energy conversion. The finite element model involves both mechanical and piezoelectric parts of the device coupled with the electrical circuit model. The energy harvester prototype was fabricated and tested under the low frequency periodic pressing force during 10 seconds. The experimental results show that several nano joules of electrical energy is stored in a capacitor that is quite significant given the size of the device. The finite element model is validated by observing a good agreement between experimental and simulation results. the validated model could be used for optimizing the device for energy harvesting from earcanal deformations.

  7. Direct Intracochlear Acoustic Stimulation Using a PZT Microactuator

    Directory of Open Access Journals (Sweden)

    Chuan Luo

    2015-11-01

    Full Text Available Combined electric and acoustic stimulation has proven to be an effective strategy to improve hearing in some cochlear implant users. We describe an acoustic microactuator to directly deliver stimuli to the perilymph in the scala tympani. The 800 µm by 800 µm actuator has a silicon diaphragm driven by a piezoelectric thin film (e.g., lead-zirconium-titanium oxide or PZT. This device could also be used as a component of a bimodal acoustic-electric electrode array. In the current study, we established a guinea pig model to test the actuator for its ability to deliver auditory signals to the cochlea in vivo. The actuator was placed through the round window of the cochlea. Auditory brainstem response (ABR thresholds, peak latencies, and amplitude growth were calculated for an ear canal speaker versus the intracochlear actuator for tone burst stimuli at 4, 8, 16, and 24 kHz. An ABR was obtained after removal of the probe to assess loss of hearing related to the procedure. In some animals, the temporal bone was harvested for histologic analysis of cochlear damage. We show that the device is capable of stimulating ABRs in vivo with latencies and growth functions comparable to stimulation in the ear canal. Further experiments will be necessary to evaluate the efficiency and safety of this modality in long-term auditory stimulation and its ability to be integrated with conventional cochlear implant arrays.

  8. Pyroelectric Charge Release in Rhombohedral PZT

    NARCIS (Netherlands)

    Noheda, Beatriz; Duan, Ning; Cereceda, Noé; Gonzalo, Julio A.

    1998-01-01

    A new experimental set-up controlled by computer has been made to measure the pyroelectric charge of ferroelectric materials with a relatively high conductivity at slow rates of temperature variation. It allowed us to obtain the polarisation vs. temperature behaviour of PZT with various compositions

  9. Flexible graphene-PZT ferroelectric nonvolatile memory

    Science.gov (United States)

    Lee, Wonho; Kahya, Orhan; Tat Toh, Chee; Özyilmaz, Barbaros; Ahn, Jong-Hyun

    2013-11-01

    We report the fabrication of a flexible graphene-based nonvolatile memory device using Pb(Zr0.35,Ti0.65)O3 (PZT) as the ferroelectric material. The graphene and PZT ferroelectric layers were deposited using chemical vapor deposition and sol-gel methods, respectively. Such PZT films show a high remnant polarization (Pr) of 30 μC cm-2 and a coercive voltage (Vc) of 3.5 V under a voltage loop over ±11 V. The graphene-PZT ferroelectric nonvolatile memory on a plastic substrate displayed an on/off current ratio of 6.7, a memory window of 6 V and reliable operation. In addition, the device showed one order of magnitude lower operation voltage range than organic-based ferroelectric nonvolatile memory after removing the anti-ferroelectric behavior incorporating an electrolyte solution. The devices showed robust operation in bent states of bending radii up to 9 mm and in cycling tests of 200 times. The devices exhibited remarkable mechanical properties and were readily integrated with plastic substrates for the production of flexible circuits.

  10. Piezoelectric nanoribbons for monitoring cellular deformations

    Science.gov (United States)

    Nguyen, Thanh D.; Deshmukh, Nikhil; Nagarah, John M.; Kramer, Tal; Purohit, Prashant K.; Berry, Michael J.; McAlpine, Michael C.

    2012-09-01

    Methods for probing mechanical responses of mammalian cells to electrical excitations can improve our understanding of cellular physiology and function. The electrical response of neuronal cells to applied voltages has been studied in detail, but less is known about their mechanical response to electrical excitations. Studies using atomic force microscopes (AFMs) have shown that mammalian cells exhibit voltage-induced mechanical deflections at nanometre scales, but AFM measurements can be invasive and difficult to multiplex. Here we show that mechanical deformations of neuronal cells in response to electrical excitations can be measured using piezoelectric PbZrxTi1-xO3 (PZT) nanoribbons, and we find that cells deflect by 1 nm when 120 mV is applied to the cell membrane. The measured cellular forces agree with a theoretical model in which depolarization caused by an applied voltage induces a change in membrane tension, which results in the cell altering its radius so that the pressure remains constant across the membrane. We also transfer arrays of PZT nanoribbons onto a silicone elastomer and measure mechanical deformations on a cow lung that mimics respiration. The PZT nanoribbons offer a minimally invasive and scalable platform for electromechanical biosensing.

  11. A rotary ultrasonic motor using radial bending mode of ring with nested PZT excitation

    Institute of Scientific and Technical Information of China (English)

    Ying-xiang LIU; Jun-kao LIU; Wei-shan CHEN; Xiao-hui YANG

    2012-01-01

    This study presents and verifies a new idea for constructing a rotary traveling wave ultrasonic motor (USM) that uses the radial bending mode of a ring.In the new design,20 trapezoid cross section slots are cut symmetrically in the outer surface of a thick duralumin alloy ring,where 20 PZT stacks are nested.In each slot,two wedging blocks are set between the PZT stack and the two sides of the slot respectively to apply preloading on the PZT ceramics.Two radial bending modes of the stator that have a phase difference of a quarter wavelength on space are generated by using the d33 operating mode of the PZT elements,and then a flexural traveling wave is formed by the superimposing of two standing waves whose amplitudes are equal and phases are different by 90° temporally.Two conical rotors are pressed to each end of the ring type stator by a coiled spring.The finite element method (FEM) simulation is developed to validate the feasibility of the proposed motor.The maximal speed and torque of the prototype are tested to be 126 r/min and 0.8 N·m,respectively.

  12. Investigation of folded spring structures for vibration-based piezoelectric energy harvesting

    Science.gov (United States)

    Lueke, J.; Rezaei, M.; Moussa, W. A.

    2014-12-01

    This paper presents a fixed-fixed folded spring as an alternative elastic element for beam-based piezoelectric energy harvesting. In order to harvest energy from low frequency vibration in an optimal manner, the natural/operational frequencies of harvesters must be reduced to match low frequency input vibrations. Therefore, natural frequency reduction of vibration-based energy harvesters is critical to maximize output power at low operational frequency. The mechanical optimization of cantilever-based piezoelectric energy harvesters is limited by residual stress-based beam curling that produced through microfabrication adding additional mechanical stiffness to the system. The fixed-fixed folded spring structure presented in this paper allows for increased effective beam length and residual stress relaxation, without out of plane beam curling to further reducing the natural frequency. Multiple designs of folded spring energy harvesters are presented to demonstrate the effect of important design parameters. It is shown that the folded spring harvesters were capable of harvesting electricity at low natural frequencies, ranging from 45 Hz to 3667 Hz. Additionally, the harvesters were shown to be insensitive to microfabrication-based residual stress beam curling. The maximum power output achieved by the folded spring harvesters was 690.5 nW at 226.3 Hz for a single harvesting element of an array, with a PZT layer thickness of 0.24 μm. The work presented in this paper demonstrates that the fixed-fixed folded spring can be used as a viable structural element for low frequency piezoelectric energy harvesting to take advantage of ambient vibrations found in low frequency applications.

  13. A Novel Integrated PZT-Driven Micropump and Microvalve

    Institute of Scientific and Technical Information of China (English)

    Zhaoxin Geng; Dafu Cui; Haining Wang; Changchun Liu; Bo Su

    2006-01-01

    According to the 'elastic buffer mechanism' and the'variable gap mechanism', a new device, which is both micropump and active microvalve actuated by PZT bimorph cantilever, was fabricated with polydimethylsiloxane (PDMS) and silicon chip. The thickness of the micropump membrance is about 180 μm. The diameter and the depth of micropump chamber cavity are 6 mm and 40 μm, respectively. The performances of the micropump, such as pump rate and backpressure, were characterized. As a flow-rectifying element, the diffusers and active valve were used instead of passive check valves. The flow rate and the backpressure of the micropump are about 420 μL/min and 2 kPa when applying a 100 V square wave driving voltage at frequency of 35 Hz.

  14. WAVELET-BASED MODEL OF PIEZOELECTRIC VIBRATION CONTROL FOR CANTILEVERED BEAM-PLATES WITH VARIABLE THICKNESS%变截面梁式压电智能板振动控制的小波模式

    Institute of Scientific and Technical Information of China (English)

    周又和; 王记增; 郑晓静

    2001-01-01

    基于Daubechies小波理论的尺度函数变换,对于变截面悬臂板结构的弯曲建立了由压电片感应器的观测电量识别挠曲变形构形的显式关系式。此基础上,采用具有位移与速度信号负反馈控制律后,建立了抑制振动的压电动力控制程序。由于小波尺度函数逼近具有低带通性质,即具有自动滤除高频分量的能力,该控制程序将不会出现由观测溢出与控制溢出耦合而造成的控制失稳(即在抑制低频(阶)扰动时系统激发出高频(阶)扰动的现象)。数值仿真结果表明:该控制方法所能控制的模态阶数与压电片数相同,而且其控制程序在抑制外界干扰方面是有效的。%Based on the scaling function transform of the Daubechies wavelet theory, an explicit expression of identification of deflection for cantilevered beam-plates with variable thickness is obtained by the measurable electric charges and electricity from the piezoelectric sensors attached on the structures. After that, a control programme to the control system with piezoelectric sensors and actuators is established by means of a control law of feedback of negative signals of the identified deflection and its velocity to suppress vibrations of the structures. Due to the characteristic that the scaling function transform has a function of low-pass filter which can auto-filter out those signals of higher-order dependent upon the resolution level of the wavelet theory, this control program on the basis of the wavelet theory can avoid the phenomenon of control instability that is caused by the coupling of spilling over of sensing and actuating, or in other words, that some higher-order vibrations are excited when a lower-order vibration is suppressed. The numerical simulations show that this control program can effectively suppress those disturbances spread from the lower-order modals of the structure when the number of order of the disturbance is not greater

  15. Frequency spectra of laminated piezoelectric cylinders

    Science.gov (United States)

    Siao, J. C.-T.; Dong, S. B.; Song, J.

    1994-07-01

    A finite-element method is presented for determining the vibrational characteristics of a circular cylinder composed of bonded piezoelectric layers. Finite-element modeling occurs in the radial direction only using quadratic polynomials and the variationally derived partial differential equations are functions of the hoop and axial coordinates (theta, z) and time t. Using solution form Q exp (i(xi(z) + n(theta) + (omega)t)), with Q as the nodal amplitudes, leads to an algebraic eigensystem where any one of the three parameters (n, xi, omega), the circumferential or axial wave number or natural frequency, can act as the eigenvalue. Integer values always are assigned to n, leaving two possible eigenvalue problems. With omega as the eigenvalue and real values assigned to xi, the solutions represent propagating waves or harmonic standing vibrations in an infinite cylinder. When xi is the eigenvalue and real values assigned to omega, this eigensystem admits both real and complex eigendata. Real xi's represent propagating waves or harmonic standing vibrations as noted before. Complex conjugate pairs of xi 's describe end vibrations, which arise when an incident wave impinges upon a free end of a cylindrical bar. They are standing waves whose amplitudes decay sinusoidally or exponentially from the free end into the interior. Two examples are given to illustrate the method of analysis, viz., a solid piezoelectric cylinder of PZT-4 ceramic material and a two-layer cylinder of PZT-4 covering an isotropic material.

  16. Effects of NaNbO3-Co2O3 Co-additive on the Properties of PZN-PZT Ceramics

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    NaNbO3-Co2O3 co-added PZN-PZT (PZCNNT) ceramics were prepared using conventional solid state reaction. The piezoelectric and dielectric properties were measured. The experimental results show that the addition of 0.3mo1% Co2O3 leads to low dielectric loss (tg δ) in PZCNNT ceramics and the proper addition of NaNbO3 not only improves piezoelectric properties but also decreases intensively dielectric loss and mechanical loss. The optimal ceramic having d33=310 pC/N, kp=0.59, εr=985, tg δ=0.0034, Qm=1380 was obtained.

  17. Silver Doped 0.9PMN-PT-0.1PZT Composite Films for very High Frequency Ultrasonic Transducer Applications.

    Science.gov (United States)

    Hsu, Hsiu-Sheng; Benjauthrit, Vatcharee; Wei, Qiang; Huang, Yuhong; Zhou, Qifa; Shung, K Kirk

    2013-05-01

    A series of silver doping concentration into the 0.9PMN-PT-0.1PZT (PMN-PT-PZT) films via the composite sol-gel technique were prepared. The crystallographic properties and microstructures of PMN-PT-PZT films with the silver dopant were investigated. Additionally, the effect of silver doping on dielectric and ferroelectric properties was examined. The results show that in general, the dielectric permittivity and remnant polarization increase as the silver doping concentration is increased. The PMN-PT-PZT+ 2.5 mol% Ag film exhibits a dielectric constant of 3,610 at 1 kHz and a remnant polarization of 57.6 µC/cm(2) at room temperature. From this silver doped film, very high frequency ultrasonic needle transducers were fabricated and evaluated. The representative transducer had the center frequency of 225 MHz with a -6 dB bandwidth of 29% (65 MHz) and 62 dB insertion loss. The performance of this transducer is comparable to other composite sol-gel films transducer. The results suggest that this silver-doped PMN-PT-PZT film is a promising candidate as an alternative piezoelectric film for very high frequency transducer applications.

  18. Silver doped 0.9PMN-PT-0.1PZT composite films for very high frequency ultrasonic transducer applications

    Energy Technology Data Exchange (ETDEWEB)

    Hsu, Hsiu-Sheng [University of Southern California, Department of Biomedical Engineering and NIH Transducer Resource Center, Los Angeles, CA (United States); University of Southern California, Mork Family Department of Chemical Engineering and Materials Science, Los Angeles, CA (United States); Benjauthrit, Vatcharee; Zhou, Qifa; Shung, K.K. [University of Southern California, Department of Biomedical Engineering and NIH Transducer Resource Center, Los Angeles, CA (United States); Wei, Qiang; Huang, Yuhong [Chemat Technology Inc., Northridge, CA (United States)

    2013-05-15

    A series of silver doping concentration into the 0.9PMN-PT-0.1PZT (PMN-PT-PZT) films via the composite sol-gel technique were prepared. The crystallographic properties and microstructures of PMN-PT-PZT films with the silver dopant were investigated. Additionally, the effect of silver doping on dielectric and ferroelectric properties was examined. The results show that in general, the dielectric permittivity and remnant polarization increase as the silver doping concentration is increased. The PMN-PT-PZT+2.5 mol% Ag film exhibits a dielectric constant of 3,610 at 1 kHz and a remnant polarization of 57.6 {mu}C/cm{sup 2} at room temperature. From this silver doped film, very high frequency ultrasonic needle transducers were fabricated and evaluated. The representative transducer had the center frequency of 225 MHz with a -6 dB bandwidth of 29 % (65 MHz) and 62 dB insertion loss. The performance of this transducer is comparable to other composite sol-gel films transducer. The results suggest that this silver-doped PMN-PT-PZT film is a promising candidate as an alternative piezoelectric film for very high frequency transducer applications. (orig.)

  19. Equivalent Circuit Model of Low-Frequency Magnetoelectric Effect in Disk-Type Terfenol-D/PZT Laminate Composites Considering a New Interface Coupling Factor

    Directory of Open Access Journals (Sweden)

    Guofeng Lou

    2017-06-01

    Full Text Available This paper describes the modeling of magnetoelectric (ME effects for disk-type Terfenol-D (Tb0.3Dy0.7Fe1.92/PZT (Pb(Zr,TiO3 laminate composite at low frequency by combining the advantages of the static elastic model and the equivalent circuit model, aiming at providing a guidance for the design and fabrication of the sensors based on magnetoelectric laminate composite. Considering that the strains of the magnetostrictive and piezoelectric layers are not equal in actual operating due to the epoxy resin adhesive bonding condition, the magnetostrictive and piezoelectric layers were first modeled through the equation of motion separately, and then coupled together with a new interface coupling factor kc, which physically reflects the strain transfer between the phases. Furthermore, a theoretical expression containing kc for the transverse ME voltage coefficient αv and the optimum thickness ratio noptim to which the maximum ME voltage coefficient corresponds were derived from the modified equivalent circuit of ME laminate, where the interface coupling factor acted as an ideal transformer. To explore the influence of mechanical load on the interface coupling factor kc, two sets of weights, i.e., 100 g and 500 g, were placed on the top of the ME laminates with the same thickness ratio n in the sample fabrication. A total of 22 T-T mode disk-type ME laminate samples with different configurations were fabricated. The interface coupling factors determined from the measured αv and the DC bias magnetic field Hbias were 0.11 for 500 g pre-mechanical load and 0.08 for 100 g pre-mechanical load. Furthermore, the measured optimum thickness ratios were 0.61 for kc = 0.11 and 0.56 for kc = 0.08. Both the theoretical ME voltage coefficient αv and optimum thickness ratio noptim containing kc agreed well with the measured data, verifying the reasonability and correctness for the introduction of kc in the modified equivalent circuit model.

  20. Equivalent Circuit Model of Low-Frequency Magnetoelectric Effect in Disk-Type Terfenol-D/PZT Laminate Composites Considering a New Interface Coupling Factor.

    Science.gov (United States)

    Lou, Guofeng; Yu, Xinjie; Lu, Shihua

    2017-06-15

    This paper describes the modeling of magnetoelectric (ME) effects for disk-type Terfenol-D (Tb0.3Dy0.7Fe1.92)/PZT (Pb(Zr,Ti)O₃) laminate composite at low frequency by combining the advantages of the static elastic model and the equivalent circuit model, aiming at providing a guidance for the design and fabrication of the sensors based on magnetoelectric laminate composite. Considering that the strains of the magnetostrictive and piezoelectric layers are not equal in actual operating due to the epoxy resin adhesive bonding condition, the magnetostrictive and piezoelectric layers were first modeled through the equation of motion separately, and then coupled together with a new interface coupling factor kc, which physically reflects the strain transfer between the phases. Furthermore, a theoretical expression containing kc for the transverse ME voltage coefficient αv and the optimum thickness ratio noptim to which the maximum ME voltage coefficient corresponds were derived from the modified equivalent circuit of ME laminate, where the interface coupling factor acted as an ideal transformer. To explore the influence of mechanical load on the interface coupling factor kc, two sets of weights, i.e., 100 g and 500 g, were placed on the top of the ME laminates with the same thickness ratio n in the sample fabrication. A total of 22 T-T mode disk-type ME laminate samples with different configurations were fabricated. The interface coupling factors determined from the measured αv and the DC bias magnetic field Hbias were 0.11 for 500 g pre-mechanical load and 0.08 for 100 g pre-mechanical load. Furthermore, the measured optimum thickness ratios were 0.61 for kc = 0.11 and 0.56 for kc = 0.08. Both the theoretical ME voltage coefficient αv and optimum thickness ratio noptim containing kc agreed well with the measured data, verifying the reasonability and correctness for the introduction of kc in the modified equivalent circuit model.

  1. Development and characterization of silicone embedded distributed piezoelectric sensors for contact detection

    Science.gov (United States)

    Acer, Merve; Salerno, Marco; Agbeviade, Kossi; Paik, Jamie

    2015-07-01

    Tactile sensing transfers complex interactive information in a most intuitive sense. Such a populated set of data from the environment and human interactions necessitates various degrees of information from both modular and distributed areas. A sensor design that could provide such types of feedback becomes challenging when the target component has a nonuniform, agile, high resolution, and soft surface. This paper presents an innovative methodology for the manufacture of novel soft sensors that have a high resolution sensing array due to the sensitivity of ceramic piezoelectric (PZT) elements, while uncommonly matched with the high stretchability of the soft substrate and electrode design. Further, they have a low profile and their transfer function is easy to tune by changing the material and thickness of the soft substrate in which the PZTs are embedded. In this manuscript, we present experimental results of the soft sensor prototypes: PZTs arranged in a four by two array form, measuring 1.5-2.3 mm in thickness, with the sensitivity in the range of 0.07-0.12 of the normalized signal change per unit force. We have conducted extensive tests under dynamic loading conditions that include impact, step and cyclic. The presented prototype's mechanical and functional capacities are promising for applications in biomedical systems where soft, wearable and high precision sensors are needed.

  2. Growth and characterization of zinc oxide and PZT films for micromachined acoustic wave devices

    Science.gov (United States)

    Yoon, Sang Hoon

    The ability to detect the presence of low concentrations of harmful substances, such as biomolecular agents, warfare agents, and pathogen cells, in our environment and food chain would greatly advance our safety, provide more sensitive tools for medical diagnostics, and protect against terrorism. Acoustic wave (AW) devices have been widely studied for such applications due to several attractive properties, such as rapid response, reliability, portability, ease of use, and low cost. The principle of these sensors is based on a fundamental feature of the acoustic wave that is generated and detected by a piezoelectric material. The performance of the device, therefore, greatly depends on the properties of piezoelectric thin film. The required properties include a high piezoelectric coefficient and high electromechanical coefficients. The surface roughness and the mechanical properties, such as Young's modulus and hardness, are also factors that can affect the wave propagation of the device. Since the film properties are influenced by the structure of the material, understanding thin film structure is very important for the design of high-performance piezoelectric MEMS devices for biosensor applications. In this research, two piezoelectric thin film materials were fabricated and investigated. ZnO films were fabricated by CSD (Chemical Solution Deposition) and sputtering, and PZT films were fabricated by CSD only. The process parameters for solution derived ZnO and PZT films, such as the substrate type, the effect of the chelating agent, and heat treatment, were studied to find the relationship between process parameters and thin film structure. In the case of the sputtered ZnO films, the process gas types and their ratio, heat treatment in situ, and post deposition were investigated. The key results of systematic experiments show that the combined influence of chemical modifiers and substrates in chemical solution deposition have an effect on the crystallographic

  3. SDIO Workshop on Piezoelectric Ceramic Actuators for Space Applications Held in Alexandria, Virginia on 25 February 1992

    Science.gov (United States)

    1992-06-01

    Advanced Piezoelectric Ceramic Actuator Materials for Space Applications Appendix D-- ACESA, ACTEX and AMASS PZT Material Needs Appendix E-- High Strain...with Embedded Sensors and Actuators ACTEX Advanced Control Technology Experiment Ag silver AMASS Advanced Materials Application to Space Structures...ACESA), Advanced Control Technology Experiment ( ACTEX ), and Advanced Materials Application to Space Structures (AMASS). The ACESA struts, 16 feet long

  4. Analytical Modelling of a Plucked Piezoelectric Bimorph for Energy Harvesting

    CERN Document Server

    Pozzi, Michele

    2012-01-01

    Energy harvesting (EH) is a multidisciplinary research area, involving physics, materials science and engineering, with the objective of providing renewable sources of sufficient power to operate targeted low-power applications. Piezoelectric transducers are often used for vibrational, inertial and direct movement EH. One problem is that, due to the stiffness of the most common material (PZT) and typically useful sizes, intrinsic resonant frequencies are normally high, whereas the available power is often concentrated at low frequencies. The aim of the plucking technique of frequency up-conversion, also known as "pizzicato" excitation, is to bridge this frequency gap. In this paper, the technique is modelled analytically. The analytical model is developed starting from the Euler-Bernoulli beam equations modified for piezoelectric coupling. A system of differential equations and associated initial conditions are derived which describe the free vibration of a piezoelectric bimorph in the last part of the plucki...

  5. A hybrid magnetostrictive-piezoelectric barrel-stave projector

    Institute of Scientific and Technical Information of China (English)

    CHAI Yong; MO Xiping; LIU Yongping; CUI Zheng

    2006-01-01

    A hybrid magnetostrictive-piezoelectric barrel-stave projector is designed and developed. The new type transducer is driven by the union of rare-earth giant magnetostrictive material Terfenol-D and PZT piezoelectric ceramic. Combining the advantages of low frequency performance within a compact size, it proves that the hybrid projector has a much broader band and higher sound power than that with single magnetostrictive or piezoelectric driver by the simulated and measured results. The prototype of the hybrid projector has a size of 88 mm in outside diameter and 316 mm in length, with an underwater resonant frequency of 1.30 kHz,Q factor of 1.43 for -3 dB bandwidth, and transmitting voltage response level of 135.1 dB at the resonant frequency.

  6. Periodical Microstructures Based on Novel Piezoelectric Material for Biomedical Applications.

    Science.gov (United States)

    Janusas, Giedrius; Ponelyte, Sigita; Brunius, Alfredas; Guobiene, Asta; Prosycevas, Igoris; Vilkauskas, Andrius; Palevicius, Arvydas

    2015-12-15

    A novel cantilever type piezoelectric sensing element was developed. Cost-effective and simple fabrication design allows the use of this element for various applications in the areas of biomedicine, pharmacy, environmental analysis and biosensing. This paper proposes a novel piezoelectric composite material whose basic element is PZT and a sensing platform where this material was integrated. Results showed that a designed novel cantilever-type element is able to generate a voltage of up to 80 µV at 50 Hz frequency. To use this element for sensing purposes, a four micron periodical microstructure was imprinted. Silver nanoparticles were precipitated on the grating to increase the sensitivity of the designed element, i.e., Surface Plasmon Resonance (SPR) effect appears in the element. To tackle some issues (a lack of sensitivity, signal delays) the element must have certain electronic and optical properties. One possible solution, proposed in this paper, is a combination of piezoelectricity and SPR in a single element.

  7. Mechanical and Vibration Testing of Carbon Fiber Composite Material with Embedded Piezoelectric Sensors

    Science.gov (United States)

    Duffy, Kirsten P.; Lerch, Bradley A.; Wilmoth, Nathan G.; Kray, Nicholas; Gemeinhardt, Gregory

    2012-01-01

    Piezoelectric materials have been proposed as a means of decreasing turbomachinery blade vibration either through a passive damping scheme, or as part of an active vibration control system. For polymer matrix fiber composite (PMFC) blades, the piezoelectric elements could be embedded within the blade material, protecting the brittle piezoceramic material from the airflow and from debris. Before implementation of a piezoelectric element within a PMFC blade, the effect on PMFC mechanical properties needs to be understood. This study attempts to determine how the inclusion of a packaged piezoelectric patch affects the material properties of the PMFC. Composite specimens with embedded piezoelectric patches were tested in four-point bending, short beam shear, and flatwise tension configurations. Results show that the embedded piezoelectric material does decrease the strength of the composite material, especially in flatwise tension, attributable to failure at the interface or within the piezoelectric element itself. In addition, the sensing properties of the post-cured embedded piezoelectric materials were tested, and performed as expected. The piezoelectric materials include a non-flexible patch incorporating solid piezoceramic material, and two flexible patch types incorporating piezoelectric fibers. The piezoceramic material used in these patches was Navy Type-II PZT.

  8. Modeling and characterization of multilayered d 15 mode piezoelectric energy harvesters in series and parallel connections

    Science.gov (United States)

    Zhu, Y. K.; Yu, Y. G.; Li, L.; Jiang, T.; Wang, X. Y.; Zheng, X. J.

    2016-07-01

    A Timoshenko beam model combined with piezoelectric constitutive equations and an electrical model was proposed to describe the energy harvesting performances of multilayered d 15 mode PZT-51 piezoelectric bimorphs in series and parallel connections. The effect of different clamped conditions was considered for non-piezoelectric and piezoelectric layers in the theoretical model. The frequency dependences of output peak voltage and power at different load resistances and excitation voltages were studied theoretically, and the results were verified by finite element modeling (FEM) simulation and experimental measurements. Results show that the theoretical model considering different clamped conditions for non-piezoelectric and piezoelectric layers could make a reliable prediction for the energy harvesting performances of multilayered d 15 mode piezoelectric bimorphs. The multilayered d 15 mode piezoelectric bimorph in a series connection exhibits a higher output peak voltage and power than that of a parallel connection at a load resistance of 1 MΩ. A criterion for choosing a series or parallel connection for a multilayered d 15 mode piezoelectric bimorph is dependent on the comparison of applied load resistance with the critical resistance of about 55 kΩ. The proposed model may provide some useful guidelines for the design and performance optimization of d 15 mode piezoelectric energy harvesters.

  9. Experimental and Theoretical Investigations of the Impact Localization of a Passive Smart Composite Plate Fabricated Using Piezoelectric Materials

    Directory of Open Access Journals (Sweden)

    M. M. S. Dezfouli

    2013-01-01

    Full Text Available Two passive smart composite plates are fabricated using one and two PZT patches that are cheaper than the PZT wafer. The composite plate is fabricated in low temperature through the hand lay-up method to avoid PZT patch decoupling and wire spoiling. The locus of the impact point is identified using the output voltage to identify the impact location using one sensor. The output voltages of the sensors are analyzed to identify the impact location using two sensors. The locations of the impacts are determined based on the crossing points of two circles and the origin of an intended Cartesian coordinate system that is concentric with one of the sensors. This study proposes the impact location identification of the passive smart composite using the low-cost PZT patch PIC155 instead of common embedded materials (wafer and element piezoelectric.

  10. Ferrite-Piezoelectric Layered Composites: Synthesis and Magnetoelectric Characterization

    Science.gov (United States)

    Hayes, R. W.; Srinivasan, G.

    2004-10-01

    The observation of strong magnetoelectric effects is reported in thick film bilayers and multilayers of ferrite-lead titanate zirconate (PZT). The ferrites used in our studies included pure and zinc substituted cobalt-, nickel- and lithium ferrites. Samples were prepared by sintering 10-40 mm thick films obtained by tape-casting. Measurements of ME voltage coefficients at 10-1000 Hz indicated a giant ME effect in nickel ferrite-PZT, but a relatively weak coupling in other ferrite-PZT systems. Evidence was found for enhancement in ME coefficients when Zn was substituted in ferrites. The Zn-assisted increase was attributed to low anisotropy and high permeability that resulted in favorable magneto-mechanical coupling in the composites. G. Srinivasan, E. T. Rasmussen, and R. Hayes, Phys. Rev. B 67, 014418 (2003) Supported by NSF and ARO grants.

  11. Evaluation of electromechanical coupling parameters of piezoelectric materials by using piezoelectric cantilever with coplanar electrode structure in quasi-stasis.

    Science.gov (United States)

    Zheng, Xuejun; Zhu, Yuankun; Liu, Xun; Liu, Jing; Zhang, Yong; Chen, Jianguo

    2014-02-01

    Based on Timoshenko beam theory, a principle model is proposed to establish the relationship between electric charge and excitation acceleration, and in quasi-stasis we apply the direct piezoelectric effect of multilayer cantilever with coplanar electrode structure to evaluate the piezoelectric strain coefficient d15 and electromechanical coupling coefficient k15. They are measured as 678 pC/N and 0.74 for the commercial piezoelectric ceramic lead zirconate titanate (PZT-51) bulk specimen and 656 pC/N and 0.63 for the lead magnesium niobate (PMN) bulk specimen, and they are in agreement with the calibration and simulation values. The maximum of relative errors is less than 4.2%, so the proposed method is reliable and convenient.

  12. Piezoelectric and ferroelectric properties of lead-free niobium-rich potassium lithium tantalate niobate single crystals

    Energy Technology Data Exchange (ETDEWEB)

    Li, Jun, E-mail: lijuna@hit.edu.cn [Department of Physics, Harbin Institute of Technology, Harbin 150001 (China); Li, Yang [Department of chemistry, Harbin Institute of Technology, Harbin 150001 (China); Zhou, Zhongxiang [Department of Physics, Harbin Institute of Technology, Harbin 150001 (China); Guo, Ruyan; Bhalla, Amar S. [Multifunctional Electronic Materials and Device Research Lab, Department of Electrical and Computer Engineering, The University of Texas at San Antonio, San Antonio 78249 (United States)

    2014-01-01

    Graphical abstract: - Highlights: • Lead-free K{sub 0.95}Li{sub 0.05}Ta{sub 1−x}Nb{sub x}O{sub 3} single crystals were grown using the top-seeded melt growth method. • The piezoelectric and ferroelectric properties of as-grown crystals were systematically investigated. • The piezoelectric properties are very attractive, e.g. for x = 0.60 composition, k{sub t} ≈ 70%, k{sub 31} ≈ 70%, k{sub 33} ≈ 77%, d{sub 31} ≈ 230 pC/N, d{sub 33} ≈ 600 pC/N. • The coercive fields of P–E hysteresis loops are quite small, about or less than 1 kV/mm. - Abstract: Lead-free potassium lithium tantalate niobate single crystals with the composition of K{sub 0.95}Li{sub 0.05}Ta{sub 1−x}Nb{sub x}O{sub 3} (abbreviated as KLTN, x = 0.51, 0.60, 0.69, 0.78) were grown using the top-seeded melt growth method. Their piezoelectric and ferroelectric properties in as-grown crystals have been systematically investigated. The phase transitions and Curie temperatures were determined from dielectric and pyroelectric measurements. Piezoelectric coefficients and electromechanical coupling factors in thickness mode, length-extensional mode and longitudinal mode were obtained. The piezoelectric properties are very attractive, e.g. for x = 0.60 composition, k{sub t} ≈ 70%, k{sub 31} ≈ 70%, k{sub 33} ≈ 77%, d{sub 31} ≈ 230 pC/N, d{sub 33} ≈ 600 pC/N are comparable to the lead-based PZT composition. The polarization versus electric field hysteresis loops show saturated shapes. In short, lead-free niobium-rich KLTN system possesses comparable properties to those in important lead-based piezoelectric material nowadays.

  13. Integrated Structural Health Assessment Using Piezoelectric Active Sensors

    Directory of Open Access Journals (Sweden)

    Jeannette R. Wait

    2005-01-01

    Full Text Available This paper illustrates an integrated approach for identifying structural damage. The method presented utilizes piezoelectric (PZT materials to actuate/sense the dynamic response of the structures. Two damage identification techniques are integrated in this study, including impedance methods and Lamb wave propagations. The impedance method monitors the variations in structural mechanical impedance, which is coupled with the electrical impedance of the PZT patch. In Lamb wave propagations, one PZT patch acting as an actuator launches an elastic wave through the structure, and responses are measured by an array of PZT sensors. The changes in both wave attenuation and reflection are used to detect and locate the damage. Both the Lamb wave and impedance methods operate in high frequency ranges at which there are measurable changes in structural responses even for incipient damage such as small cracks, debonding, or loose connections. The combination of the local impedance method with the wave propagation based approach allows a better characterization of the system’s structural integrity. The paper concludes with experimental results to demonstrate the feasibility of this integrated active sensing technology.

  14. Development of dual PZT transducers for reference-free crack detection in thin plate structures.

    Science.gov (United States)

    Sohn, Hoon; Kim, Seuno Bum

    2010-01-01

    A new Lamb-wave-based nondestructive testing (NDT) technique, which does not rely on previously stored baseline data, is developed for crack monitoring in plate structures. Commonly, the presence of damage is identified by comparing "current data" measured from a potentially damaged stage of a structure with "baseline data" previously obtained at the intact condition of the structure. In practice, structural defects typically take place long after collection of the baseline data, and the baseline data can be also affected by external loading, temperature variations, and changing boundary conditions. To eliminate the dependence on the baseline data comparison, the authors previously developed a reference-free NDT technique using 2 pairs of collocated lead zirconate titanate (PZT) transducers placed on both sides of a plate. This reference-free technique is further advanced in the present study by the necessity of attaching transducers only on a single surface of a structure for certain applications such as aircraft. To achieve this goal, a new design of PZT transducers called dual PZT transducers is proposed. Crack formation creates Lamb wave mode conversion due to a sudden thickness change of the structure. This crack appearance is instantly detected from the measured Lamb wave signals using the dual PZT transducers. This study also suggests a reference-free statistical approach that enables damage classification using only the currently measured data set. Numerical simulations and experiments were conducted using an aluminum plate with uniform thickness and fundamental Lamb waves modes to demonstrate the applicability of the proposed technique to reference-free crack detection.

  15. Using Diffusion Bonding in Making Piezoelectric Actuators

    Science.gov (United States)

    Sager, Frank E.

    2003-01-01

    A technique for the fabrication of piezoelectric actuators that generate acceptably large forces and deflections at relatively low applied voltages involves the stacking and diffusion bonding of multiple thin piezoelectric layers coated with film electrodes. The present technique stands in contrast to an older technique in which the layers are bonded chemically, by use of urethane or epoxy agents. The older chemical-bonding technique entails several disadvantages, including the following: It is difficult to apply the bonding agents to the piezoelectric layers. It is difficult to position the layers accurately and without making mistakes. There is a problem of disposal of hazardous urethane and epoxy wastes. The urethane and epoxy agents are nonpiezoelectric materials. As such, they contribute to the thickness of a piezoelectric laminate without contributing to its performance; conversely, for a given total thickness, the performance of the laminate is below that of a unitary piezoelectric plate of the same thickness. The figure depicts some aspects of the fabrication of a laminated piezoelectric actuator by the present diffusion- bonding technique. First, stock sheets of the piezoelectric material are inspected and tested. Next, the hole pattern shown in the figure is punched into the sheets. Alternatively, if the piezoelectric material is not a polymer, then the holes are punched in thermoplastic films. Then both faces of each punched piezoelectric sheet or thermoplastic film are coated with a silver-ink electrode material by use of a silkscreen printer. The electrode and hole patterns are designed for minimal complexity and minimal waste of material. After a final electrical test, all the coated piezoelectric layers (or piezoelectric layers and coated thermoplastic films) are stacked in an alignment jig, which, in turn, is placed in a curved press for the diffusion-bonding process. In this process, the stack is pressed and heated at a specified curing temperature

  16. Electronically droplet energy harvesting using piezoelectric cantilevers

    KAUST Repository

    Al Ahmad, Mahmoud Al

    2012-01-01

    A report is presented on free falling droplet energy harvesting using piezoelectric cantilevers. The harvester incorporates a multimorph clamped-free cantilever which is composed of five layers of lead zirconate titanate piezoelectric thick films. During the impact, the droplet kinetic energy is transferred into the form of mechanical stress forcing the piezoelectric structure to vibrate. Experimental results show energy of 0.3 μJ per droplet. The scenario of moderate falling drop intensity, i.e. 230 drops per second, yields a total energy of 400 μJ. © 2012 The Institution of Engineering and Technology.

  17. Damping properties of epoxy-based composite embedded with sol–gel-derived Pb(Zr0.53Ti0.47)O3 thin film with different thicknesses

    Indian Academy of Sciences (India)

    Guo Dongyun; Mao Wei; Qin Yan; Huang Zhixiong; Wang Chuanbin; Shen Qiang; Zhang Lianmeng

    2012-06-01

    Pb(Zr0.53Ti0.47)O3 (PZT) thin films were prepared on Pt/Ti/SiO2/Si substrate by sol–gel method. The effect of film thickness on microstructure, ferroelectric and dielectric properties was investigated. The single-phase PZT films were obtained with different thicknesses. PZT films with a thickness of 190–440 nm had better dielectric and ferroelectric properties. The epoxy/PZT film/epoxy sandwiched composites were prepared. The thickness of PZT films influenced their damping properties of the composites, and the epoxy-based composites embedded with 310 nm-thick PZT films had the largest damping loss factor of 0.915.

  18. Gap Waves in Piezoelectric layered Medium

    Directory of Open Access Journals (Sweden)

    Danoyan Z.N.

    2007-03-01

    Full Text Available In the present paper the conditions of existence of shear electroelastic gap waves in piezoelectric-vacuum-dielectric layered system are found. It is shown that in the discontact layered system the gap electroelastic waves can be propagated. It is considered the limiting case when the thickness of vacuuming layer tends to zero. It is proved that the statement of the problem is true when there is no acoustic contact between piezoelectric and dielectric grounded media.

  19. Hydrothermal synthesis and characterization of fluorine & manganese co-doped PZT based cuboidal shaped powder

    Science.gov (United States)

    Nawaz, H.; Shuaib, M.; Saleem, M.; Rauf, A.; Aleem, A.

    2016-08-01

    Cuboidal shaped PZT powder particles based composition Pb0.89(Ba, Sr)0.11(Zr0.52Ti0.48)O3 co- doped with 1 mol% manganese and 2 mol% fluorine was prepared through hydrothermal route. 200-250nm size cuboidal particles were observed under FE-SEM. XRD technique revealed that the perovskite type ceramic structure has a dominant rhombohedral phase. The resultant powder particles were then spray dried, uniaxially pressed and sintered at different temperatures to achieve maximum theoretical density. 98% density was obtained in the pellets at a sintering temperature of 1190°C with an average grain size of 1-3um. The electrical properties of sintered samples were also measured before and after poling to evaluate the effect of dopants on piezoelectric properties.

  20. Piezoelectric particle accelerator

    Energy Technology Data Exchange (ETDEWEB)

    Kemp, Mark A.; Jongewaard, Erik N.; Haase, Andrew A.; Franzi, Matthew

    2017-08-29

    A particle accelerator is provided that includes a piezoelectric accelerator element, where the piezoelectric accelerator element includes a hollow cylindrical shape, and an input transducer, where the input transducer is disposed to provide an input signal to the piezoelectric accelerator element, where the input signal induces a mechanical excitation of the piezoelectric accelerator element, where the mechanical excitation is capable of generating a piezoelectric electric field proximal to an axis of the cylindrical shape, where the piezoelectric accelerator is configured to accelerate a charged particle longitudinally along the axis of the cylindrical shape according to the piezoelectric electric field.

  1. Epitaxial Piezoelectric Pb(Zr0.2Ti0.8O3 Thin Films on Silicon for Energy Harvesting Devices

    Directory of Open Access Journals (Sweden)

    A. Sambri

    2012-01-01

    Full Text Available We report on the properties of ferroelectric Pb(Zr0.2Ti0.8O3 (PZT thin films grown epitaxially on (001 silicon and on the performance of such heterostructures for microfabricated piezoelectric energy harvesters. In the first part of the paper, we investigate the epitaxial stacks through transmission electron microscopy and piezoelectric force microscopy studies to characterize in detail their crystalline structure. In the second part of the paper, we present the electrical characteristics of piezoelectric cantilevers based on these epitaxial PZT films. The performance of such cantilevers as vibration energy transducers is compared with other piezoelectric harvesters and indicates the potential of the epitaxial approach in the field of energy harvesting devices.

  2. Effect of sol temperature on structural, morphological and magnetic properties of PZT thin films on alumina substrate

    Science.gov (United States)

    Sreelalitha, K.; Thyagarajan, K.

    2016-01-01

    In the present study, we investigate the structural, morphological and magnetic properties of sol-gel spin-coated PZT thin films on alumina substrate. The morphotropic phase boundary (MPB) of PZT [Pb (Zr1-xTix)03] between the tetragonal and rhombohedral phases occurs at the Zr/Ti ratio of 52/48. At the MPB the physical properties of PZT are of far-reaching importance due to their possible crystalline phases. In this study Pb(Zr0.52Ti0.48)03 sols are prepared at room temperature and at 125 °C. The gels are coated onto alumina substrate using a spin-coating unit as two and three layers. The structural studies using XRD confirm the perovskite phase formation at an annealing temperature of 660 °C for both films. The structural parameter grain size, dislocation density, lattice parameters and strain were dependent on the sol temperature. The SEM morphology of the samples represents well-developed dense grain structure and thickness in micrometer ranges. The VSM analysis shows diamagnetic and ferromagnetic hysteresis loop. The ferromagnetism at low fields in PZT films is confirmed by studying the magnetic properties of powder made of the same gel. The effect of heat treatment on the gel preparation is observed on structural, morphological and magnetic properties of PZT thin films. The ferromagnetism in PZT can be attributed to oxygen vacancies. The squareness ratio of the films shows the application of the films as a high-density recording medium.

  3. Stripe-PZT Sensor-Based Baseline-Free Crack Diagnosis in a Structure with a Welded Stiffener

    Directory of Open Access Journals (Sweden)

    Yun-Kyu An

    2016-09-01

    Full Text Available This paper proposes a stripe-PZT sensor-based baseline-free crack diagnosis technique in the heat affected zone (HAZ of a structure with a welded stiffener. The proposed technique enables one to identify and localize a crack in the HAZ using only current data measured using a stripe-PZT sensor. The use of the stripe-PZT sensor makes it possible to significantly improve the applicability to real structures and minimize man-made errors associated with the installation process by embedding multiple piezoelectric sensors onto a printed circuit board. Moreover, a new frequency-wavenumber analysis-based baseline-free crack diagnosis algorithm minimizes false alarms caused by environmental variations by avoiding simple comparison with the baseline data accumulated from the pristine condition of a target structure. The proposed technique is numerically as well as experimentally validated using a plate-like structure with a welded stiffener, reveling that it successfully identifies and localizes a crack in HAZ.

  4. Electrical Impedance Measurements of PZT Nanofiber Sensors

    Directory of Open Access Journals (Sweden)

    Richard Galos

    2017-01-01

    Full Text Available Electrical impedance measurements of PZT nanofiber sensors were performed using a variety of methods over a frequency spectrum ranging from DC to 1.8 GHz. The nanofibers formed by electrospinning with diameters ranging from 10 to 150 nm were collected and integrated into sensors using microfabrication techniques. Special matching circuits with ultrahigh input impedance were fabricated to produce low noise, measurable sensor outputs. Material properties including resistivity and dielectric constant are derived from the impedance measurements. The resulting material properties are also compared with those of individual nanofibers being tested using conductive AFM and Scanning Conductive Microscopy.

  5. Piezoelectric Motors, an Overview

    OpenAIRE

    Karl Spanner; Burhanettin Koc

    2016-01-01

    Piezoelectric motors are used in many industrial and commercial applications. Various piezoelectric motors are available in the market. All of the piezoelectric motors use the inverse piezoelectric effect, where microscopically small oscillatory motions are converted into continuous or stepping rotary or linear motions. Methods of obtaining long moving distance have various drive and functional principles that make these motors categorized into three groups: resonance-drive (piezoelectric ult...

  6. PZT压电纤维的制备及性能研究%Study on the Preparation and Properties of PZT Ceramic Fibers

    Institute of Scientific and Technical Information of China (English)

    杨杰; 刘兴钊

    2009-01-01

    以溶胶-凝胶(Sol-Gel)工艺制备的PZT陶瓷粉为原料,采用氧化物粉末装管法制备PZT压电陶瓷纤维.SEM分析显示,该陶瓷纤维呈圆柱型形貌,直径约为250 μm.分析了不同烧结温度下PZT陶瓷纤维的断面微结构及Pb含量变化,得出PZT陶瓷纤维的最佳烧结温度为1 000 ℃.XRD分析表明,此温度下烧结的陶瓷纤维呈单一的钙钛矿结构.实验结果表明,采用氧化物粉末装管法制备的陶瓷纤维大小均匀,结构致密,具有高长径比,克服了传统工艺不能制备结构致密的长纤维的缺陷.%Using the PZT ceramic powder prepared by Sol-Gel method as the raw material, the PZT piezoelectric ceramic fibers have been prepaared by using the Oxide Powder in Tube(OPTT)procedure.The SEM morphology showed that the PZT ceramic fibers had a cylindrical morphology with a diameter of about 250 μm.The sectional micro-structure and the content of Pb of the PZT ceramic fiber were analyzed at different sintering temperature. The result showed that the optimal sintering termperature of the PZT ceramic fiber was 1 000 ℃.The X-ray diffraction patterns showed that the ceramic fibers were pure perovskite structure.Compared with conventional fabrication process,PZT ceramic fibers prepared by the OPIT method have the advantage of dense ,uniform and high height-to-width ratio.

  7. Feasibility of Using PZT Actuators to Study the Dynamic Behavior of a Rotating Disk due to Rotor-Stator Interaction

    Directory of Open Access Journals (Sweden)

    Alexandre Presas

    2014-07-01

    Full Text Available In this paper, PZT actuators are used to study the dynamic behavior of a rotating disk structure due to rotor-stator interaction excitation. The disk is studied with two different surrounding fluids—air and water. The study has been performed analytically and validated experimentally. For the theoretical analysis, the natural frequencies and the associated mode shapes of the rotating disk in air and water are obtained with the Kirchhoff-Love thin plate theory coupled with the interaction with the surrounding fluid. A model for the Rotor Stator Interaction that occurs in many rotating disk-like parts of turbomachinery such as compressors, hydraulic runners or alternators is presented. The dynamic behavior of the rotating disk due to this excitation is deduced. For the experimental analysis a test rig has been developed. It consists of a stainless steel disk (r = 198 mm and h = 8 mm connected to a variable speed motor. Excitation and response are measured from the rotating system. For the rotating excitation four piezoelectric patches have been used. Calibrating the piezoelectric patches in amplitude and phase, different rotating excitation patterns are applied on the rotating disk in air and in water. Results show the feasibility of using PZT to control the response of the disk due to a rotor-stator interaction.

  8. Feasibility of using PZT actuators to study the dynamic behavior of a rotating disk due to rotor-stator interaction.

    Science.gov (United States)

    Presas, Alexandre; Egusquiza, Eduard; Valero, Carme; Valentin, David; Seidel, Ulrich

    2014-07-07

    In this paper, PZT actuators are used to study the dynamic behavior of a rotating disk structure due to rotor-stator interaction excitation. The disk is studied with two different surrounding fluids-air and water. The study has been performed analytically and validated experimentally. For the theoretical analysis, the natural frequencies and the associated mode shapes of the rotating disk in air and water are obtained with the Kirchhoff-Love thin plate theory coupled with the interaction with the surrounding fluid. A model for the Rotor Stator Interaction that occurs in many rotating disk-like parts of turbomachinery such as compressors, hydraulic runners or alternators is presented. The dynamic behavior of the rotating disk due to this excitation is deduced. For the experimental analysis a test rig has been developed. It consists of a stainless steel disk (r = 198 mm and h = 8 mm) connected to a variable speed motor. Excitation and response are measured from the rotating system. For the rotating excitation four piezoelectric patches have been used. Calibrating the piezoelectric patches in amplitude and phase, different rotating excitation patterns are applied on the rotating disk in air and in water. Results show the feasibility of using PZT to control the response of the disk due to a rotor-stator interaction.

  9. Novel composite piezoelectric material for energy harvesting applications

    Science.gov (United States)

    Janusas, Giedrius; Guobiene, Asta; Palevicius, Arvydas; Prosycevas, Igoris; Ponelyte, Sigita; Baltrusaitis, Valentinas; Sakalys, Rokas

    2015-04-01

    Past few decades were concentrated on researches related to effective energy harvesting applied in modern technologies, MEMS or MOEMS systems. There are many methods for harvesting energy as, for example, usage of electromagnetic devices, but most dramatic changes were noticed in the usage of piezoelectric materials in small scale devices. Major limitation faced was too small generated power by piezoelectric materials or high resonant frequencies of such smallscale harvesters. In this research, novel composite piezoelectric material was created by mixing PZT powder with 20% solution of polyvinyl butyral in benzyl alcohol. Obtained paste was screen printed on copper foil using 325 mesh stainless steel screen and dried for 30 min at 100 °C. Polyvinyl butyral ensures good adhesion and flexibility of a new material at the conditions that requires strong binding. Five types of a composite piezoelectric material with different concentrations of PZT (40%, 50%, 60%, 70% and 80 %) were produced. As the results showed, these harvesters were able to transform mechanical strain energy into electric potential and, v.v. In experimental setup, electromagnetic shaker was used to excite energy harvester that is fixed in the custom-built clamp, while generated electric potential were registered with USB oscilloscope PICO 3424. The designed devices generate up to 80 μV at 50 Hz excitation. This property can be applied to power microsystem devices or to use them in portable electronics and wireless sensors. However, the main advantage of the created composite piezoelectric material is possibility to apply it on any uniform or nonuniform vibrating surface and to transform low frequency vibrations into electricity.

  10. Thin PZT-Based Ferroelectric Capacitors on Flexible Silicon for Nonvolatile Memory Applications

    KAUST Repository

    Ghoneim, Mohamed T.

    2015-04-24

    A flexible version of traditional thin lead zirconium titanate ((Pb1.1Zr0.48Ti0.52O3)-(PZT)) based ferroelectric random access memory (FeRAM) on silicon shows record performance in flexible arena. The thin PZT layer requires lower operational voltages to achieve coercive electric fields, reduces the sol-gel coating cycles required (i.e., more cost-effective), and, fabrication wise, is more suitable for further scaling of lateral dimensions to the nano-scale due to the larger feature size-to-depth aspect ratio (critical for ultra-high density non-volatile memory applications). Utilizing the inverse proportionality between substrate\\'s thickness and its flexibility, traditional PZT based FeRAM on silicon is transformed through a transfer-less manufacturable process into a flexible form that matches organic electronics\\' flexibility while preserving the superior performance of silicon CMOS electronics. Each memory cell in a FeRAM array consists of two main elements; a select/access transistor, and a storage ferroelectric capacitor. Flexible transistors on silicon have already been reported. In this work, we focus on the storage ferroelectric capacitors, and report, for the first time, its performance after transformation into a flexible version, and assess its key memory parameters while bent at 0.5 cm minimum bending radius.

  11. The Peano-series solution for modeling shear horizontal waves in piezoelectric plates

    Directory of Open Access Journals (Sweden)

    Ben Ghozlen M.H.

    2012-06-01

    Full Text Available The shear horizontal (SH wave devices have been widely used in electroacoustic. To improve their performance, the phase velocity dispersion and the electromechanical coupling coefficient of the Lamb wave should be calculated exactly in the design. Therefore, this work is to analyze exactly the Lamb waves polarized in the SH direction in homogeneous plate pie.zoelectric material (PZT-5H. An alternative method is proposed to solve the wave equation in such a structure without using the standard method based on the electromechanical partial waves. This method is based on an analytical solution, the matricant explicitly expressed under the Peano series expansion form. Two types of configuration have been addressed, namely the open circuited and the short circuited. Results confirm that the SH wave provides a number of attractive properties for use in sensing and signal processing applications. It has been found that the phase velocity remains nearly constant for all values of h/λ (h is the plate thickness, λ the acoustic wavelength. Secondly the SH0 wave mode can provide very high electromechanical coupling. Graphical representations of electrical and mechanical amounts function of depth are made, they are in agreement with the continuity rules. The developed Peano technique is in agreement with the classical approach, and can be suitable with cylindrical geometry.

  12. Static Analysis of Functionally Graded Piezoelectric Beams under Thermo-Electro-Mechanical Loads

    Directory of Open Access Journals (Sweden)

    Amin Komeili

    2011-01-01

    Full Text Available This paper presents the analysis of static bending of beams made of functionally graded piezoelectric materials (FGPMs under a combined thermo-electro-mechanical load. The Euler Bernoulli theory (EBT, first-order shear deformation theory (FSDT and third-order shear deformation theory (TSDT were employed to compare the accuracy and the reliability of each theory in applications. The material properties vary continuously through the thickness direction. The material compositions were selected from the PZT family. The governing equations were derived from Hamilton's principle and solved using the finite element method and Fourier series method. Cubic Hermit interpolation shape function was used for estimating the transverse deflection, and the linear interpolation function was used for the axial displacement and the shear rotation as well. Fourier series expansion, based on the boundary conditions, were employed to solve the governing equations analytically. The accuracy of the method was validated by comparing the results with the previous studies. Finite element results were compared with the analytical results presented in this paper. A comprehensive parametric study is conducted to show the influence of the voltage, shear deformation, material composition, end supports, and the slenderness ratio on the thermo-electro-mechanical characteristic.

  13. Study on precision piezoelectric rotary step motors with inner anchor/loosen and outer drive

    Institute of Scientific and Technical Information of China (English)

    Jianfang LIU; Zhigang YANG; Ping ZENG; Zunqiang FAN

    2008-01-01

    A new precision rotary piezoelectric(PZT)actuator is proposed to improve its drive performance.Based on piezoelectric technology,the actuator adopts the principle of bionics,with a new method of stator inner anchor/loosen/rotor outer drive and a distortion structure of a thin shelf flexible hinge.This structure improves the stability of the anchor/loosen and step rotary.Its characteristics are evaluated by finite element analysis.The experiment shows that the new rotary PZT actuator works with higher frequency(40 Hz),higher speed (325 μrad/s),wider movement(360°),high resolution (1 μrad/step)and high torque(30 N·cm).The novel actuator can be applied in wide movement and high resolution driving devices such as those for optics engineering,precision positioning and some other micro-manipulation fields.

  14. DEVELOPMENT OF SIGNAL PROCESSING TOOLS AND HARDWARE FOR PIEZOELECTRIC SENSOR DIAGNOSTIC PROCESSES

    Energy Technology Data Exchange (ETDEWEB)

    OVERLY, TIMOTHY G. [Los Alamos National Laboratory; PARK, GYUHAE [Los Alamos National Laboratory; FARRAR, CHARLES R. [Los Alamos National Laboratory

    2007-02-09

    This paper presents a piezoelectric sensor diagnostic and validation procedure that performs in -situ monitoring of the operational status of piezoelectric (PZT) sensor/actuator arrays used in structural health monitoring (SHM) applications. The validation of the proper function of a sensor/actuator array during operation, is a critical component to a complete and robust SHM system, especially with the large number of active sensors typically involved. The method of this technique used to obtain the health of the PZT transducers is to track their capacitive value, this value manifests in the imaginary part of measured electrical admittance. Degradation of the mechanical/electric properties of a PZT sensor/actuator as well as bonding defects between a PZT patch and a host structure can be identified with the proposed procedure. However, it was found that temperature variations and changes in sensor boundary conditions manifest themselves in similar ways in the measured electrical admittances. Therefore, they examined the effects of temperature variation and sensor boundary conditions on the sensor diagnostic process. The objective of this study is to quantify and classify several key characteristics of temperature change and to develop efficient signal processing techniques to account for those variations in the sensor diagnostis process. In addition, they developed hardware capable of making the necessary measurements to perform the sensor diagnostics and to make impedance-based SHM measurements. The paper concludes with experimental results to demonstrate the effectiveness of the proposed technique.

  15. Unique Activity-Meter with Piezoelectric Poly(vinylidene difluoride) Films and Self Weight of the Sensor Nodes

    Science.gov (United States)

    Nogami, Hirofumi; Okada, Hironao; Takamatsu, Seiichi; Kobayashi, Takeshi; Maeda, Ryutaro; Itoh, Toshihiro

    2013-09-01

    We have developed piezoelectric switches for application in ultra low-power wireless sensor nodes to monitor the health condition of chickens. Using Pb(Zr0.52,Ti0.48)O3 (PZT) thin films, we have developed S-shaped PZT cantilevers with proof masses. Since the resonant frequency of PZT devices is approximately 24 Hz, we have utilized their superharmonic resonance to detect chicken movements with frequencies as low as 5-15 Hz. By attaching sensor nodes to chickens, we successfully measured the activity of chickens. However, the PZT devices of other sensor nodes broke down. S-shaped PZT devices are adequate for low vibrations, but are beset by the structural problems of fragmentation upon impact. To address these problems, we examine a method of utilizing poly(vinylidene difluoride) (PVDF) films, which are tough and generate high piezoelectric output voltages under a large stress, as piezoelectric switches. We suggest that the self-weight of sensor nodes be used as the mass of the cantilevers of the PVDF films. One end of a PVDF film is fixed to the case of a sensor node, and the other end is attached to the sensor node. Since PVDF films are subjected to force generated by the self-weight of sensor nodes, high output voltages are expected. A result of measuring output voltages, we confirm the output voltages to be approximately the same as those of PZT devices below 15 Hz at 0.5 m/s2 vibration, which is close to chicken movements. Thus, we consider that we have successfully fabricated a tough wireless sensor node for chickens, utilizing the features of PVDF films.

  16. Multilayer Piezoelectric Stack Actuator Characterization

    Science.gov (United States)

    Sherrit, Stewart; Jones, Christopher M.; Aldrich, Jack B.; Blodget, Chad; Bao, Xioaqi; Badescu, Mircea; Bar-Cohen, Yoseph

    2008-01-01

    Future NASA missions are increasingly seeking to use actuators for precision positioning to accuracies of the order of fractions of a nanometer. For this purpose, multilayer piezoelectric stacks are being considered as actuators for driving these precision mechanisms. In this study, sets of commercial PZT stacks were tested in various AC and DC conditions at both nominal and extreme temperatures and voltages. AC signal testing included impedance, capacitance and dielectric loss factor of each actuator as a function of the small-signal driving sinusoidal frequency, and the ambient temperature. DC signal testing includes leakage current and displacement as a function of the applied DC voltage. The applied DC voltage was increased to over eight times the manufacturers' specifications to investigate the correlation between leakage current and breakdown voltage. Resonance characterization as a function of temperature was done over a temperature range of -180C to +200C which generally exceeded the manufacturers' specifications. In order to study the lifetime performance of these stacks, five actuators from one manufacturer were driven by a 60volt, 2 kHz sine-wave for ten billion cycles. The tests were performed using a Lab-View controlled automated data acquisition system that monitored the waveform of the stack electrical current and voltage. The measurements included the displacement, impedance, capacitance and leakage current and the analysis of the experimental results will be presented.

  17. Characterization of Piezoelectric Stacks for Space Applications

    Science.gov (United States)

    Sherrit, Stewart; Jones, Christopher; Aldrich, Jack; Blodget, Chad; Bao, Xiaoqi; Badescu, Mircea; Bar-Cohen, Yoseph

    2008-01-01

    Future NASA missions are increasingly seeking to actuate mechanisms to precision levels in the nanometer range and below. Co-fired multilayer piezoelectric stacks offer the required actuation precision that is needed for such mechanisms. To obtain performance statistics and determine reliability for extended use, sets of commercial PZT stacks were tested in various AC and DC conditions at both nominal and high temperatures and voltages. In order to study the lifetime performance of these stacks, five actuators were driven sinusoidally for up to ten billion cycles. An automated data acquisition system was developed and implemented to monitor each stack's electrical current and voltage waveforms over the life of the test. As part of the monitoring tests, the displacement, impedance, capacitance and leakage current were measured to assess the operation degradation. This paper presents some of the results of this effort.

  18. Stability and scalability of piezoelectric flags

    CERN Document Server

    Wang, Xiaolin; Li, Chenyang; Young, Yin Lu

    2015-01-01

    We investigate the effect of piezoelectric (PZT) material on the flutter speed, vibration mode and frequency, and energy harvesting power and efficiency of a flexible flag in various fluids. We develop a fully coupled fluid-solid-electric model by combining the inviscid vortex sheet model with a linear electro-mechanical coupling model. A resistance only circuit and a resonant resistance-inductance (RL) circuit are considered. For a purely resistive circuit, an increased electro-mechanical coupling factor results in an increased flutter speed, vibration frequency, averaged electric power and efficiency. A consistent optimal resistance is found that maximizes the flutter speed and the energy harvesting power. For a resonant RL circuit, by tuning the inductance to match the circuit frequency to the flag's vibration frequency, the flutter speed can be greatly decreased, and a larger averaged power and efficiency are obtained. We also consider a model scale set-up with several commonly used commercial materials f...

  19. Vibrations of Thin Piezoelectric Shallow Shells: Two-Dimensional Approximation

    Indian Academy of Sciences (India)

    N Sabu

    2003-08-01

    In this paper we consider the eigenvalue problem for piezoelectric shallow shells and we show that, as the thickness of the shell goes to zero, the eigensolutions of the three-dimensional piezoelectric shells converge to the eigensolutions of a two-dimensional eigenvalue problem.

  20. Development of a Piezoelectric Vacuum Sensing Component for a Wide Pressure Range

    Directory of Open Access Journals (Sweden)

    Bing-Yu Wang

    2014-11-01

    Full Text Available In this study, we develop a clamped–clamped beam-type piezoelectric vacuum pressure sensing element. The clamped–clamped piezoelectric beam is composed of a PZT layer and a copper substrate. A pair of electrodes is set near each end. An input voltage is applied to a pair of electrodes to vibrate the piezoelectric beam, and the output voltage is measured at the other pair. Because the viscous forces on the piezoelectric beam vary at different air pressures, the vibration of the beam depends on the vacuum pressure. The developed pressure sensor can sense a wide range of pressure, from 6.5 × 10−6 to 760 Torr. The experimental results showed that the output voltage is inversely proportional to the gas damping ratio, and thus, the vacuum pressure was estimated from the output voltage.

  1. Piezoelectricity of single- and multi-layer cellular polypropylene film electrets

    Institute of Scientific and Technical Information of China (English)

    QIU Xunlin; XIA Zhongfu; WANG Feipeng

    2007-01-01

    The piezoelectricity of a pressure-treated cellular polypropylene (PP) (commercially available,trade name PQ50) film electret was studied by the measurement of direct- and inverse-piezoelectric d33 coefficient.The sample expanded with optimal parameters has a quasi-static piezo-electric d33 coefficient of more than 600 Pc/N,which is about 40 times as high as that of polyvinylidene fluoride (PVDF). In addition,the hybrid multi-layer system,which properly combines single-layer cellular PP film electrets,shows a quasi-static piezoelectric sensitivity of as high as 2010 Pc/N. This is around three times higher than that of well-known lead zirconate titanate (PZT) ceramics.The results are theoreti-cally and technically helpful to promote the application of cellular PP film electrets.

  2. Solution of two-dimensional scattering problem in piezoelectric/piezomagnetic media using a polarization method

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    Using a polarization method, the scattering problem for a two-dimensional inclusion embedded in infinite piezoelectric/piezomagnetic matrices is investigated. To achieve the purpose, the polarization method for a two-dimensional piezoelectric/piezo-magnetic "comparison body" is formulated. For simple harmonic motion, kernel of the polarization method reduces to a 2-D time-harmonic Green's function, which is ob-tained using the Radon transform. The expression is further simplified under condi-tions of low frequency of the incident wave and small diameter of the inclusion. Some analytical expressions are obtained. The analytical solutions for generalized piezoelec-tric/piezomagnetic anisotropic composites are given followed by simplified results for piezoelectric composites. Based on the latter results, two numerical results are provided for an elliptical cylindrical inclusion in a PZT-5H-matrix, showing the effect of different factors including size, shape, material properties, and piezoelectricity on the scattering cross-section.

  3. Characterization of hard piezoelectric lead-free ceramics.

    Science.gov (United States)

    Zhang, Shujun; Lim, Jong Bong; Lee, Hyeong Jae; Shrout, Thomas R

    2009-08-01

    K4CuNb8O23 doped K(0.45)Na(0.55)NbO3(KNNKCN) ferroelectric ceramics were found to exhibit asymmetrical polarization hysteresis loops, related to the development of an internal bias field. The internal bias field is believed to be the result of defect dipoles of acceptor ions and oxygen vacancies, which lead to piezoelectric "hardening" effect, by stabilizing and pinning of the domain wall motion. The dielectric loss for the hard lead-free piezoelectric ceramic was found to be 0.6%, with mechanical quality factors Q on the order of >1500. Furthermore, the piezoelectric properties were found to decrease and the coercive field increased, when compared with the undoped material, exhibiting a typical characteristic of "hard" behavior. The temperature usage range was limited by the polymorphic phase transition temperature, being 188 degrees C. The full set of material constants was determined for the KNN-KCN materials. Compared with conventional hard PZT ceramics, the lead-free possessed lower dielectric and piezoelectric properties; however, comparable values of mechanical Q, dielectric loss, and coercive fields were obtained, making acceptor modified KNN based lead-free piezoelectric material promising for high-power applications, where leadfree materials are desirable.

  4. Evaluation of polarization of embedded piezoelectrics by the thermal wave method.

    Science.gov (United States)

    Suchaneck, Gunnar; Eydam, Agnes; Hu, Wenguo; Kranz, Burkhart; Drossel, Welf-Guntram; Gerlach, Gerald

    2012-09-01

    This work demonstrates the benefit of the thermal wave method for the evaluation of the polarization state of embedded piezoelectrics. Two types of samples were investigated: A low-temperature co-fired ceramics (LTCC)/lead zirconate titanate (PZT) sensor-actuator and a macro-fiber composite (MFC) actuator. At modulation frequencies below 10 Hz, the pyroelectric response was governed by thermal losses to the embedding layers. Here, the sample behavior was described by a harmonically heated piezoelectric plate exhibiting heat losses to the environment characterized by a single thermal relaxation time.

  5. Domain-orientation-controlled potassium niobate family piezoelectric materials with hydrothermal powders.

    Science.gov (United States)

    Fujiuchi, Yukiko; Morita, Takeshi

    2014-10-01

    Materials of the potassium niobate family, as lead-free piezoelectric materials, are expected to be alternative materials to Pb(Zr,Ti)O3 (PZT) because of their good piezoelectric properties, high Curie temperature, and so on. In particular, single-crystal potassium niobate is a promising ferroelectric material as a surface acoustic substrate and for functional optical effects. It is, however, well known that single crystals are difficult to fabricate because of the instability caused by temperature, external stress, and other factors.

  6. Low Symmetry Phases in Piezoelectric Systems : PZN-xPT Single Crystal and Powder

    NARCIS (Netherlands)

    Noheda, B.; Cox, D.E.; Shirane, G.

    2002-01-01

    In this review we address some of the experimental challenges found in the x-ray diffraction characterization of the low-symmetry phases recently discovered in the Pb(Zr1-xTix)O3 (PZT), Pb(Zn1/3Nb2/3)1-xTixO3 (PZN-PT) and Pb(Mg1/3Nb2/3)1-xTixO3 (PMN-PT) piezoelectric systems around their morphotropi

  7. Ferroelastic contribution to the piezoelectric response in lead zirconate titanate by in situ stroboscopic neutron diffraction

    Science.gov (United States)

    Jones, Jacob L.; Hoffman, Mark; Daniels, John E.; Studer, Andrew J.

    2006-11-01

    Ferroelastic domain switching during dynamic actuation is measured in situ for a piezoelectric lead zirconate titanate (PZT) ceramic utilizing a new capability developed on The Australian Strain Scanner (TASS) at ANSTO. Diffraction patterns are obtained as a function of time during a 1 Hz cycle. The change in the 0 0 2 and 2 0 0 diffraction intensities indicates there is ferroelastic domain switching at sub-coercive (weak) fields.

  8. Integration of Piezoelectric Sensing and Control for Nano-Scale Vibration Suppression in Hard Disk Drives

    OpenAIRE

    Felix, Sarah Helen

    2010-01-01

    This work takes an integrated mechatronic approach to combine a novel sensing scheme with appropriate control methods to improve vibration suppression in hard disk drives (HDDs). Thin-film piezoelectric ZnO strain sensors were integrated into a PZT-actuated HDD suspension by fabricating the sensors directly onto the steel suspension structure that carries the read/write head. This technology allowed for the addition of sensors at arbitrary locations without significantly altering the dynami...

  9. Integration of Piezoelectric Sensing and Control for Nano-Scale Vibration Suppression in Hard Disk Drives

    OpenAIRE

    Felix, Sarah Helen

    2010-01-01

    This work takes an integrated mechatronic approach to combine a novel sensing scheme with appropriate control methods to improve vibration suppression in hard disk drives (HDDs). Thin-film piezoelectric ZnO strain sensors were integrated into a PZT-actuated HDD suspension by fabricating the sensors directly onto the steel suspension structure that carries the read/write head. This technology allowed for the addition of sensors at arbitrary locations without significantly altering the dynami...

  10. Analytical modeling of demagnetizing effect in magnetoelectric ferrite/PZT/ferrite trilayers taking into account a mechanical coupling

    Science.gov (United States)

    Loyau, V.; Aubert, A.; LoBue, M.; Mazaleyrat, F.

    2017-03-01

    In this paper, we investigate the demagnetizing effect in ferrite/PZT/ferrite magnetoelectric (ME) trilayer composites consisting of commercial PZT discs bonded by epoxy layers to Ni-Co-Zn ferrite discs made by a reactive Spark Plasma Sintering (SPS) technique. ME voltage coefficients (transversal mode) were measured on ferrite/PZT/ferrite trilayer ME samples with different thicknesses or phase volume ratio in order to highlight the influence of the magnetic field penetration governed by these geometrical parameters. Experimental ME coefficients and voltages were compared to analytical calculations using a quasi-static model. Theoretical demagnetizing factors of two magnetic discs that interact together in parallel magnetic structures were derived from an analytical calculation based on a superposition method. These factors were introduced in ME voltage calculations which take account of the demagnetizing effect. To fit the experimental results, a mechanical coupling factor was also introduced in the theoretical formula. This reflects the differential strain that exists in the ferrite and PZT layers due to shear effects near the edge of the ME samples and within the bonding epoxy layers. From this study, an optimization in magnitude of the ME voltage is obtained. Lastly, an analytical calculation of demagnetizing effect was conducted for layered ME composites containing higher numbers of alternated layers (n ≥ 5). The advantage of such a structure is then discussed.

  11. Guided wave propagation in multilayered piezoelectric structures

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    A general formulation of the method of the reverberation-ray matrix (MRRM) based on the state space formalism and plane wave expansion technique is presented for the analysis of guided waves in multilayered piezoelectric structures. Each layer of the structure is made of an arbitrarily anisotropic piezoelectric material. Since the state equation of each layer is derived from the three-dimensional theory of linear piezoelectricity, all wave modes are included in the formulation. Within the framework of the MRRM, the phase relation is properly established by excluding exponentially growing functions, while the scattering relation is also appropriately set up by avoiding matrix inversion operation. Consequently, the present MRRM is unconditionally numerically stable and free from computational limitations to the total number of layers, the thickness of individual layers, and the frequency range. Numerical examples are given to illustrate the good performance of the proposed formulation for the analysis of the dispersion characteristic of waves in layered piezoelectric structures.

  12. Drop-by-drop deposition of ceramic slurry for fabrication of PZT microstructures

    Science.gov (United States)

    Klintberg, Lena; Thornell, Greger; Johansson, Stefan A. I.

    1999-10-01

    Most of the techniques available for ceramic microprocessing, e.g. tape casting, sputtering and sol-gel processing suffer from lack of geometrical flexibility although they often allow for good thickness control. With the interest for ceramic material in MST, especially the piezoelectric lead zirconate titanate, often involving more complex geometries, development of complementary technologies seems motivated.

  13. Energy harvesting via thermo-piezoelectric transduction within a heated capillary

    Science.gov (United States)

    Monroe, J. G.; Bhandari, M.; Fairley, J.; Myers, O. J.; Shamsaei, N.; Thompson, S. M.

    2017-07-01

    Thermal-to-kinetic-to-electrical energy conversion is demonstrated through the use of a piezoelectric transducer (PZT) integrated within a section of an oscillating heat pipe (OHP) partially filled with water. The sealed PZT transducer was configured as a bow spring parallel to the dominant flow direction within the OHP. The bottom portion of the OHP was heated in increments of 50 W, while its top portion was actively cooled via water blocks. At ˜50 W, the internal fluid started to oscillate at ˜2-4 Hz due to the non-uniform vapor pressure generated in the OHP evaporator. Low-frequency fluid "pulses" were observed to occur across the flexed, in-line piezoelectric transducer, resulting in its deflection and measureable voltage spikes ranging between 24 and 63 mV. The OHP, while having its internal fluid enthalpy harvested, was found to still have an ultra-high thermal conductivity on-the-order of 10 kW/m K; however, its maximum operating heat load decreased due to the pressure drop introduced by the PZT material. The thermo-piezoelectric harvesting concept made possible via the thermally driven fluid oscillations within an OHP provides a passive method for combined energy harvesting and thermal management that is both scalable and portable.

  14. Characterization of PZT thin films on metal substrates; Charakterisierung von PZT-Duennschichten auf Metallsubstraten

    Energy Technology Data Exchange (ETDEWEB)

    Dutschke, A.

    2008-02-02

    Lead zirconate titanate (PbZr{sub x}Ti{sub 1-x}O{sub 3},PZT) is one of the most applied ceramic materials because of its distinctive piezo- and ferroelectric properties. Prepared as thin films on flexible, metallic substrates it can be used for various applications as strain gauges, key switches, vibration dampers, microactuators and ultrasonic transducers. The aim of this work is to analyze the microstructure and the phase-content of PZT-thin films deposited on temperature- und acid-resistant hastelloy-sheets, to correlate the results with the ferroelectric and dielectric properties. It is demonstrated, that the specific variation of the microstructure can be achieved by different thermal treatments and the selective addition of Neodymium as dopant. Nd-doping leads to a shift of the maximum nucleation rate towards reduced temperatures and a decrease in the rate of growth compared to undoped films. The PZT-films are prepared by a sol-gel-process in fourfold multilayers with a composition near the morphotropic phase boundary, where the tetragonal und rhombohedral perovskite-phases coexist. The crystallisation in Nd-doped and undoped films takes place heterogeneously, preferentially at the interfaces and on the surface of the multilayered films as well as on the inner surface of pores within the films. For the first time, the Zr:Ti fluctuation phenomena emerging in sol-gel derived PZT films is related to the microstructure and the local phase content on a nanometer scale. In this connection it is proved, that long-distance Zr:Ti gradients arise preferentially before and during the crystallisation of the pyrochlore phase. During the following crystallisation of the perovskite phase, the crystallites grow across these gradients without modifying them. It is pointed out that the fluctuation in the Zr:Ti ratio has only minor influence on the amount of the tetragonal or rhombohedral distortion of the crystallites after the transition from the para- to the ferroelectric

  15. Piezoelectric drive circuit

    Science.gov (United States)

    Treu, Jr., Charles A.

    1999-08-31

    A piezoelectric motor drive circuit is provided which utilizes the piezoelectric elements as oscillators and a Meacham half-bridge approach to develop feedback from the motor ground circuit to produce a signal to drive amplifiers to power the motor. The circuit automatically compensates for shifts in harmonic frequency of the piezoelectric elements due to pressure and temperature changes.

  16. Enhanced converse magnetoelectric effect in cylindrical piezoelectric-magnetostrictive composites

    Science.gov (United States)

    Wu, Gaojian; Zhang, Ru; Zhang, Ning

    2016-10-01

    Enhanced converse magnetoelectric (ME) effect has been experimentally observed in cylindrical PZT-Terfenol-D piezoelectric-magnetostrictive bilayered composites, where the piezoelectric and magnetostrictive components are coupled through normal stresses instead of shear stresses that act in most of previous multiferroic composites. A theoretical model based on elastodynamics analysis has been proposed to describe the frequency response of converse ME effect for axial and radial modes in the bilayered cylindrical composites. The theory shows good agreement with the experimental results. The different variation tendency of resonant converse ME coefficient, as well as different variation rate of resonance frequency with bias magnetic field for axial and radial modes is interpreted in terms of demagnetizing effect. This work is of theoretical and technological significance for the application of converse ME effect as magnetic sensor, transducers, coil-free flux switch, etc.

  17. Evaluation of piezoelectric material properties for a higher power output from energy harvesters with insight into material selection using a coupled piezoelectric-circuit-finite element method.

    Science.gov (United States)

    Daniels, Alice; Zhu, Meiling; Tiwari, Ashutosh

    2013-12-01

    Piezoelectric material properties have substantial influence on electrical power output from piezoelectric energy harvesters (PEHs). Understanding their influences is the first step in designing effective PEHs to generate higher power outputs. This paper uses a coupled piezoelectric-circuit-finite element method to study the power outputs of different types of piezoelectric materials, including single crystal, polyvinylidene fluoride (PVDF), and soft and hard lead zirconate titanate (PZT) materials. The purpose of this study is to try to gain an understanding of which piezoelectric material property--the elastic compliance s11, the piezoelectric strain constant d31, the piezoelectric stress constant g31, and the relative dielectric constant ϵ(T)r33, and the associated material properties of the d31 × g31, called the figure of merit (FOM), and the coupling coefficient k31--dominates the power output. A rectangular piezoelectric plate under a low-frequency excitation is used to evaluate piezoelectric material properties for a higher power output. It was found that 1) d31 is a more dominant material property over other material properties for higher power output; 2) FOM was more linearly related to the power output than either the k31 or the d31; and 3) ϵ(T)r33 had some role; when the materials have an identical d31; a lower ϵ(T)r33 was preferred. Because of unexplained outliers, no single material parameter was able to be recommended as selection criteria, but combined FOM with d31 parameters is recommended for selection of piezoelectric material for a higher power output from PEHs.

  18. Amplification of acoustic waves in laminated piezoelectric semiconductor plates

    Energy Technology Data Exchange (ETDEWEB)

    Yang, J.S.; Yang, X.M.; Turner, J.A. [University of Nebraska, Department of Engineering Mechanics, Lincoln, NE (United States)

    2004-12-01

    Two-dimensional equations for coupled extensional, flexural and thickness-shear motions of laminated plates of piezoelectric semiconductors are obtained systematically from the three-dimensional equations by retaining lower order terms in power series expansions in the plate thickness coordinate. The equations are used to analyze extensional waves in a composite plate of piezoelectric ceramics and semiconductors. Dispersion and dissipation due to semiconduction as well as wave amplification by a dc electric field are discussed. (orig.)

  19. Advanced piezoelectric single crystal based transducers for naval sonar applications

    Science.gov (United States)

    Snook, Kevin A.; Rehrig, Paul W.; Hackenberger, Wesley S.; Jiang, Xiaoning; Meyer, Richard J., Jr.; Markley, Douglas

    2006-03-01

    Transducers incorporating single crystal piezoelectric Pb(Mg 1/3Nb 2/3) x-1Ti xO 3 (PMN-PT) exhibit significant advantages over ceramic piezoelectrics such as PZT, including both high electromechanical coupling (k 33 > 90%) and piezoelectric coefficients (d 33 > 2000 pC/N). Conventional orientation gives inherently larger bandwidth and output power than PZT ceramics, however, the anisotropy of the crystal also allows for tailoring of the performance by orienting the crystal along different crystallographic axes. This attribute combined with composition refinements can be used to improve thermal or mechanical stability, which is important in high power, high duty cycle sonar applications. By utilizing the "31" resonance mode, the high power performance of PMN-PT can be improved over traditional "33" mode single crystal transducers, due to an improved aspect ratio. Utilizing novel geometries, effective piezoelectric constants of -600 pC/N to -1200 pC/N have been measured. The phase transition point induced by temperature, pre-stress or field is close to that in the "33" mode, and since the prestress is applied perpendicular to the poling direction in "31" mode elements, they exhibit lower loss and can therefore be driven harder. The high power characteristics of tonpilz transducers can also be affected by the composition of the PMN-PT crystal. TRS modified the composition of PMN-PT to improve the thermal stability of the material, while keeping the loss as low as possible. Three dimensional modeling shows that the useable bandwidth of these novel compositions nearly equals that of conventional PMN-PT. A decrease in the source level of up to 6 dB was calculated, which can be compensated for by the higher drive voltages possible.

  20. High Power Piezoelectric Characterization for Piezoelectric Transformer Development

    Science.gov (United States)

    Ural, Seyit O.

    circuit to leave the resonator in an open circuit condition. The newly introduced open circuits burst have resulted in antiresonance quality factor measurements along with resonance quality factors in a "non-heating" sample. In this technique too, resonance and antiresonance losses showed significant difference. Resonance burst mode characterizations at elevated ambient temperatures have shown that the lower vibration velocity mechanical quality factors appear to be more sensitive to the ambient temperature. Design criteria's to produce the most power dense structure were investigated. Common device shapes were investigated to see which one does enhance the power density of the piezoelectric device. Disk shaped piezoelectric actuators have proven to have lower matching impedances and higher, farther persisting mechanical quality factors with respect to vibration velocities. In order to achieve identical power level, plate shaped samples will have been to strain ~3.5 times more than disk shaped samples. Thus the most power dense structure has been concluded to be a disk shape ~1W/cm3 Once the actuators shape was fixed, further design on structure were conducted with (c)ATILA finite element method. For the transformer application, the design considered following key factors; 1-Controlling the output impedance by optimizing number of layers and layer thicknesses of the multilayer and 2- Evaluation of various electrodes and their affect on high power performance was evaluated. As the thickness of active layers decreased, the number of electrode layers increases. This increase in the metal to piezoelectric ratio and the relative increase in the electrode resistance under high current loads, both will have to be accounted for. Thus; with the piezoelectric composition and the device structure optimized, the research input electrical power. Once the actuators shape was fixed, further design on structure were conducted with (c)ATILA finite element method. For the transformer

  1. Compatibility of RuO2 electrodes with PZT ceramics

    Indian Academy of Sciences (India)

    K T Jacob; G Rajitha; V S Saji

    2009-06-01

    Because of its high electrical conductivity and good diffusion barrier properties ruthenium dioxide (RuO2) is a good electrode material for use with ferroelectric lead zirconate–titanate (PZT) solid solutions. Under certain conditions, RuO2 can react with PZT to form lead ruthenate (Pb2Ru2O6.5) during processing at elevated temperatures resulting in lead depletion from PZT. The standard Gibbs energies of formation of RuO2 and Pb2Ru2O6.5 and activities of components of the PZT solid solution have been determined recently. Using this data along with older thermodynamic information on PbZrO3 and PbTiO3, the stability domain of Pb2Ru2O6.5 is computed as a function of PZT composition, temperature and oxygen partial pressure in the gas phase. The results show PbZrO3-rich compositions are more prone to react with RuO2 at all temperatures. Increasing temperature and decreasing oxygen partial pressure suppress the reaction. Graphically displayed are the reaction zones as a function of oxygen partial pressure and PZT composition at temperatures 973, 1173 and 1373 K.

  2. Standing wave brass-PZT square tubular ultrasonic motor.

    Science.gov (United States)

    Park, Soonho; He, Siyuan

    2012-09-01

    This paper reports a standing wave brass-PZT tubular ultrasonic motor. The motor is composed of a brass square tube with two teeth on each tube end. Four PZT plates are attached to the outside walls of the brass tube. The motor requires only one driving signal to excite vibration in a single bending mode to generate reciprocating diagonal trajectories of teeth on the brass tube ends, which drive the motor to rotate. Bi-directional rotation is achieved by exciting different pairs of PZT plates to switch the bending vibration direction. Through using the brass-PZT tube structure, the motor can take high magnitude vibration to achieve a high output power in comparison to PZT tube based ultrasonic motors. Prototypes are fabricated and tested. The dimension of the brass-PZT tube is 3.975mm×3.975mm×16mm. Measured performance is a no-load speed of >1000RPM, a stall torque of 370μNm and a maximum output power of 16 mW when a sinusoidal driving voltage of 50V is applied. The working frequencies of the motor are 46,050Hz (clockwise) and 46,200Hz (counter-clockwise).

  3. Radial-Electric-Field Piezoelectric Diaphragm Pumps

    Science.gov (United States)

    Bryant, Robert G.; Working, Dennis C.; Mossi, Karla; Castro, Nicholas D.; Mane, Pooma

    2009-01-01

    In a recently invented class of piezoelectric diaphragm pumps, the electrode patterns on the piezoelectric diaphragms are configured so that the electric fields in the diaphragms have symmetrical radial (along-the-surface) components in addition to through-the-thickness components. Previously, it was accepted in the piezoelectric-transducer art that in order to produce the out-of-plane bending displacement of a diaphragm needed for pumping, one must make the electric field asymmetrical through the thickness, typically by means of electrodes placed on only one side of the piezoelectric material. In the present invention, electrodes are placed on both sides and patterned so as to produce substantial radial as well as through-the-thickness components. Moreover, unlike in the prior art, the electric field can be symmetrical through the thickness. Tests have shown in a given diaphragm that an electrode configuration according to this invention produces more displacement than does a conventional one-sided electrode pattern. The invention admits of numerous variations characterized by various degrees of complexity. Figure 1 is a simplified depiction of a basic version. As in other piezoelectric diaphragm pumps of similar basic design, the prime mover is a piezoelectric diaphragm. Application of a suitable voltage to the electrodes on the diaphragm causes it to undergo out-of-plane bending. The bending displacement pushes a fluid out of, or pulls the fluid into, a chamber bounded partly by the diaphragm. Also as in other diaphragm pumps in general, check valves ensure that the fluid flows only in through one port and only out through another port.

  4. Piezoelectric Motors, an Overview

    Directory of Open Access Journals (Sweden)

    Karl Spanner

    2016-02-01

    Full Text Available Piezoelectric motors are used in many industrial and commercial applications. Various piezoelectric motors are available in the market. All of the piezoelectric motors use the inverse piezoelectric effect, where microscopically small oscillatory motions are converted into continuous or stepping rotary or linear motions. Methods of obtaining long moving distance have various drive and functional principles that make these motors categorized into three groups: resonance-drive (piezoelectric ultrasonic motors, inertia-drive, and piezo-walk-drive. In this review, a comprehensive summary of piezoelectric motors, with their classification from initial idea to recent progress, is presented. This review also includes some of the industrial and commercial applications of piezoelectric motors that are presently available in the market as actuators.

  5. Fatigue life characterization for piezoelectric macrofiber composites

    Science.gov (United States)

    Henslee, Isaac A.; Miller, David A.; Tempero, Tyler

    2012-10-01

    In an effort to aid the investigation into lightweight and reliable materials for actuator design, a study was developed to characterize the temperature-dependent lifetime performance of a piezoelectric macrofiber composite (MFC). MFCs are thin rectangular patches of polyimide film, epoxy and a single layer of rectangular lead zirconium titanate (PZT) fibers. In this study, the useful life of the MFC is characterized to determine the effect of temperature on the performance of the composite as it is fatigued by cyclic piezoelectric excitation. The test specimen consists of the MFC laminated to a cantilevered stainless steel beam. Beam strain and tip displacement measurements are used as a basis for determining the performance of the MFC as it is cyclically actuated under various operating temperatures. The temperature of the beam laminate is held constant and then cycled to failure, or 250 million cycles, in order to determine the useful life of the MFC over a temperature range from - 15 to 145 °C. The results of the experiments show a strong temperature dependence of the operational life for the MFC. Damage inside the composite was identified through in situ visual inspection and during post-test microstructural observation; however, no degradation in operational performance was identified as it was cyclically actuated up to the point of failure, regardless of temperature or actuation cycle number.

  6. Experimental Determination of Effect of Variable Resistance on Lead ZirconateTitanate (PZT-5A4Eunder various Thermal and Frequency Conditions

    Directory of Open Access Journals (Sweden)

    Hassan Elahi

    2014-12-01

    Full Text Available A specially designed apparatus and circuit working on the principle of inverse piezoelectricity due to the effect of polarization was used to find the relationship between resistance and peak to peak voltage of Lead Zirconate Titanate (PZT-5A4E by shocking it at variable frequencies and at variable resistances under various thermal conditions within Curie temperature limit using equivalent circuit method. It was found that by increasing temperature, peak to peak voltage increases and similarly by increasing frequency, peak to peak voltage decreases and with the increase in resistance peak to peak voltage decreases.

  7. A T-shape linear piezoelectric motor with single foot.

    Science.gov (United States)

    Liu, Yingxiang; Chen, Weishan; Yang, Xiaohui; Liu, Junkao

    2015-02-01

    A new T-shape piezoelectric motor using the hybrid of two orthogonal longitudinal vibrations is proposed in this work. Six pieces of PZT ceramic plates are bonded on the upside and downside surfaces of a T-shape duralumin alloy base respectively to form the proposed motor. Elliptical movement can be generated on the driving tip by applying sine and cosine voltages to the PZT elements. The horizontal displacement of the driving tip will push the runner while the vertical displacement can overcome the preload. Finite element method is used to accomplish the design and analysis process. The resonance frequencies of the two vibration modes are tuned to be close by modal analysis, while the motion trajectory of the driving tip is observed by transient analysis. After the fabrication of a prototype, the vibration characteristics and mechanical output ability are measured. The no-load speed and the maximum output thrust force of the proposed motor are tested to be 718 mm/s and 3.5 N under an exciting frequency of 53.1 kHz. The proposed T-shape piezoelectric motor exhibits merits of simple structure, easy to realize miniaturization, easy to be fabricated, and high power-to-weight ratio.

  8. Effect of dopants on ferroelectric and piezoelectric properties of lead zirconate titanate thin films on Si substrates

    NARCIS (Netherlands)

    Nguyen, Duc Minh; Trinh, Thong Q.; Dekkers, Jan M.; Houwman, Evert Pieter; Vu, Hung Ngoc; Rijnders, Augustinus J.H.M.

    2014-01-01

    Lead zirconate titanate Pb(Zr0.52Ti0.48)O3 (undoped PZT) and doped PZT thin films with thickness of about 500 nm were grown on Pt/Ti/SiO2/Si substrates by pulsed laser deposition (PLD). In this study, 1.0 mol% Nb-doping (at Zr/Ti site) as donor, 1.0 mol% Fe-doping (at Zr/Ti) as acceptor and 10 mol%

  9. Elastic Properties and Enhanced Piezoelectric Response at Morphotropic Phase Boundaries

    Directory of Open Access Journals (Sweden)

    Francesco Cordero

    2015-12-01

    Full Text Available The search for improved piezoelectric materials is based on the morphotropic phase boundaries (MPB between ferroelectric phases with different crystal symmetry and available directions for the spontaneous polarization. Such regions of the composition x − T phase diagrams provide the conditions for minimal anisotropy with respect to the direction of the polarization, so that the polarization can easily rotate maintaining a substantial magnitude, while the near verticality of the TMPB(x boundary extends the temperature range of the resulting enhanced piezoelectricity. Another consequence of the quasi-isotropy of the free energy is a reduction of the domain walls energies, with consequent formation of domain structures down to nanoscale. Disentangling the extrinsic and intrinsic contributions to the piezoelectricity in such conditions requires a high level of sophistication from the techniques and analyses for studying the structural, ferroelectric and dielectric properties. The elastic characterization is extremely useful in clarifying the phenomenology and mechanisms related to ferroelectric MPBs. The relationship between dielectric, elastic and piezoelectric responses is introduced in terms of relaxation of defects with electric dipole and elastic quadrupole, and extended to the response near phase transitions in the framework of the Landau theory. An account is provided of the anelastic experiments, from torsional pendulum to Brillouin scattering, that provided new important information on ferroelectric MPBs, including PZT, PMN-PT, NBT-BT, BCTZ, and KNN-based systems.

  10. Ferroelectric and piezoelectric responses of (110) and (001)-oriented epitaxial Pb(Zr{sub 0.52}Ti{sub 0.48})O{sub 3} thin films on all-oxide layers buffered silicon

    Energy Technology Data Exchange (ETDEWEB)

    Vu, Hien Thu [International Training Institute for Materials Science (ITIMS), Hanoi University of Science and Technology, No.1 Dai Co Viet Road, Hanoi 10000 (Viet Nam); Nguyen, Minh Duc, E-mail: minh.nguyen@itims.edu.vn [International Training Institute for Materials Science (ITIMS), Hanoi University of Science and Technology, No.1 Dai Co Viet Road, Hanoi 10000 (Viet Nam); Inorganic Materials Science (IMS), MESA + Institute for Nanotechnology, University of Twente, P.O. Box 217, 7500 AE Enschede (Netherlands); SolMateS B.V., Drienerlolaan 5, Building 6, 7522 NB Enschede (Netherlands); Houwman, Evert; Boota, Muhammad [Inorganic Materials Science (IMS), MESA + Institute for Nanotechnology, University of Twente, P.O. Box 217, 7500 AE Enschede (Netherlands); Dekkers, Matthijn [SolMateS B.V., Drienerlolaan 5, Building 6, 7522 NB Enschede (Netherlands); Vu, Hung Ngoc [International Training Institute for Materials Science (ITIMS), Hanoi University of Science and Technology, No.1 Dai Co Viet Road, Hanoi 10000 (Viet Nam); Rijnders, Guus [Inorganic Materials Science (IMS), MESA + Institute for Nanotechnology, University of Twente, P.O. Box 217, 7500 AE Enschede (Netherlands)

    2015-12-15

    Graphical abstract: The cross sections show a very dense structure in the (001)-oriented films (c,d), while an open columnar growth structure is observed in the case of the (110)-oriented films (a,b). The (110)-oriented PZT films show a significantly larger longitudinal piezoelectric coefficient (d33{sub ,f}), but smaller transverse piezoelectric coefficient (d31{sub ,f}) than the (001) oriented films. - Highlights: • We fabricate all-oxide, epitaxial piezoelectric PZT thin films on Si. • The orientation of the films can be controlled by changing the buffer layer stack. • The coherence of the in-plane orientation of the grains and grain boundaries affects the ferroelectric properties. • Good cycling stability of the ferroelectric properties of (001)-oriented PZT thin films. The (110)-oriented PZT thin films show a larger d33{sub ,f} but smaller d31{sub ,f} than the (001)-oriented films. - Abstract: Epitaxial ferroelectric Pb(Zr{sub 0.52}Ti{sub 0.48})O{sub 3} (PZT) thin films were fabricated on silicon substrates using pulsed laser deposition. Depending on the buffer layers and perovskite oxide electrodes, epitaxial films with different orientations were grown. (110)-oriented PZT/SrRuO{sub 3} (and PZT/LaNiO{sub 3}) films were obtained on YSZ-buffered Si substrates, while (001)-oriented PZT/SrRuO{sub 3} (and PZT/LaNiO{sub 3}) were fabricated with an extra CeO{sub 2} buffer layer (CeO{sub 2}/YSZ/Si). There is no effect of the electrode material on the properties of the films. The initial remnant polarizations in the (001)-oriented films are higher than those of (110)-oriented films, but it increases to the value of the (001) films upon cycling. The longitudinal piezoelectric d33{sub ,f} coefficients of the (110) films are larger than those of the (001) films, whereas the transverse piezoelectric d31{sub ,f} coefficients in the (110)-films are less than those in the (001)-oriented films. The difference is ascribed to the lower density (connectivity between

  11. Flexible Pb(Zr0.52Ti0.48)O3 Films for a Hybrid Piezoelectric-Pyroelectric Nanogenerator under Harsh Environments.

    Science.gov (United States)

    Ko, Young Joon; Kim, Dong Yeong; Won, Sung Sik; Ahn, Chang Won; Kim, Ill Won; Kingon, Angus I; Kim, Seung-Hyun; Ko, Jae-Hyeon; Jung, Jong Hoon

    2016-03-01

    In spite of extremely high piezoelectric and pyroelectric coefficients, there are few reports on flexible ferroelectric perovskite film based nanogenerators (NGs). Here, we report the successful growth of a flexible Pb(Zr0.52Ti0.48)O3 (PZT) film and its application to hybrid piezoelectric-pyroelectric NG. A highly flexible Ni-Cr metal foil substrate with a conductive LaNiO3 bottom electrode enables the growth of flexible PZT film having high piezoelectric (140 pC/N) and pyroelectric (50 nC/cm(2)K) coefficients at room temperature. The flexible PZT-based NG effectively scavenges mechanical vibration and thermal fluctuation from sources ranging from the human body to the surroundings such as wind. Furthermore, it stably generates electric current even at elevated temperatures of 100 °C, relative humidity of 70%, and pH of 13 by virtue of its high Curie temperature and strong resistance for water and base. As proof of power generation under harsh environments, we demonstrate the generation of extremely high current at the exhaust pipe of a car, where hot CO and CO2 gases are rapidly expelled to air. This work expands the application of flexible PZT film-based NG for the scavenging mechanical vibration and thermal fluctuation energies even at extreme conditions.

  12. 压电及弹性层厚度对弯曲元件特性影响的研究%Influence of the thickness of piezoelectric and elastic layers on the bender element characteristic

    Institute of Scientific and Technical Information of China (English)

    鄂世举; 杨志刚; 沈传亮

    2009-01-01

    研制一种三叠片型压电双晶片驱动器,上下两层为压电陶瓷材料PZT-5H,中间弹性层为铍青铜.利用激光测试仪LC-2400A及LV-1610对压电弯曲元件的输出位移、位移滞环、蠕变量及基频等特性进行实验测试.通过实验,确定压电弯曲元件的弹性层及压电晶片的厚度对其特性的影响,分析影响压电弯曲元件性能的因素.

  13. A piezoelectric transformer

    Science.gov (United States)

    Won, C. C.

    1993-01-01

    This work describes a modeling and design method whereby a piezoelectric system is formulated by two sets of second-order equations, one for the mechanical system, and the other for the electrical system, coupled through the piezoelectric effect. The solution to this electromechanical coupled system gives a physical interpretation of the piezoelectric effect as a piezoelectric transformer that is a part of the piezoelectric system, which transfers the applied mechanical force into a force-controlled current source, and short circuit mechanical compliance into capacitance. It also transfers the voltage source into a voltage-controlled relative velocity input, and free motional capacitance into mechanical compliance. The formulation and interpretation simplify the modeling of smart structures and lead to physical insight that aids the designer. Due to its physical realization, the smart structural system can be unconditional stable and effectively control responses. This new concept has been demonstrated in three numerical examples for a simple piezoelectric system.

  14. Piezoelectric Wheel System

    Science.gov (United States)

    Juang, Puu-An

    2007-10-01

    A piezoelectric wheel system is proposed for used as a microstepping displacement device including a carrier and two displacement members, which are separately pivoted on the carrier. Each displacement member includes two wheels, and which can not rotate. In addition, each wheel includes a wheel sheet and a piezoelectric element embedded on its surface. When the piezoelectricity element generates and transmits power to the wheel sheet, the wheel induces vibration and deformation. Therefore, owing to the wheel sheets and the touched ground involving their relative motion, the displacement device can be moved or can be oriented its motion direction. The wheel system involves direct movement, and has no rotor requirement. In this research, a three-dimensional (3D) mechanical element with an extra electrical degree of freedom is employed to simulate the dynamic vibration modes of the linear piezoelectric, mechanical, and piezoelectric-mechanical behaviours of the piezoelectric wheel.

  15. Active control of vibrations and noise by electrorheological fluids and piezoelectric materials

    Science.gov (United States)

    Amorosi, Joseph J.

    The combination of electrorheological (ER) fluids and piezoelectric actuators into one actively controlled intelligent sandwich plate structure for either noise or vibration control is investigated in this study. The simply supported sandwich plate consists of a core of four cavities filled with ER fluid, two elastic outer face plates, bottom plate cross stiffeners and symmetrically bonded surface piezoceramic (PZT) actuator patches. Analytical and computational simulations are performed to obtain the resultant structural response to random inputs, noise transmission into a rectangular enclosure, and sound radiation into a semi-infinite acoustic half space. An equivalent, homogeneous plate model is used in the modal decomposition of the derived governing equations of motion. This equivalency is obtained by taking the modal frequencies and mode shapes, calculated by the finite element method, to be that of the sandwich plate. The effect of actively controlling the ER fluid's stiffness material properties is incorporated into the modal frequencies and mode shapes by altering the sandwich plate's core shear and elastic moduli whereas ER fluid controllable damping is directly incorporated into the governing equations of motion as equivalent modal damping. The effect of the PZT actuators is incorporated into the governing equations of motion through direct velocity feedback utilizing collocated control. A two part control strategy is developed. First, the appropriate ER fluid voltage potential and then the PZT actuator gains are selected. Numerical results obtained in this study indicate that using ER and PZT active control up to 50 dB of noise reduction is possible at certain frequency ranges. In addition, about 15 dB reduction of the overall radiated sound pressure level can be obtained. However, for the available ER and PZT materials, the reduction of overall sound pressure to random input is shown to be on the order of 5 to 8 decibels. To improve on noise

  16. Flexible PZT Thin Film Tactile Sensor for Biomedical Monitoring

    Directory of Open Access Journals (Sweden)

    Wen-Jong Wu

    2013-04-01

    Full Text Available This paper presents the development of tactile sensors using the sol-gel process to deposit a PZT thin-film from 250 nm to 1 μm on a flexible stainless steel substrate. The PZT thin-film tactile sensor can be used to measure human pulses from several areas, including carotid, brachial, finger, ankle, radial artery, and the apical region. Flexible PZT tactile sensors can overcome the diverse topology of various human regions and sense the corresponding signals from human bodies. The measured arterial pulse waveform can be used to diagnose hypertension and cardiac failure in patients. The proposed sensors have several advantages, such as flexibility, reliability, high strain, low cost, simple fabrication, and low temperature processing. The PZT thin-film deposition process includes a pyrolysis process at 150 °C/500 °C for 10/5 min, followed by an annealing process at 650 °C for 10 min. Finally, the consistent pulse wave velocity (PWV was demonstrated based on human pulse measurements from apical to radial, brachial to radial, and radial to ankle. It is characterized that the sensitivity of our PZT-based tactile sensor was approximately 0.798 mV/g.

  17. Piezoelectric energy harvesting

    CERN Document Server

    Erturk, Alper

    2011-01-01

    The transformation of vibrations into electric energy through the use of piezoelectric devices is an exciting and rapidly developing area of research with a widening range of applications constantly materialising. With Piezoelectric Energy Harvesting, world-leading researchers provide a timely and comprehensive coverage of the electromechanical modelling and applications of piezoelectric energy harvesters. They present principal modelling approaches, synthesizing fundamental material related to mechanical, aerospace, civil, electrical and materials engineering disciplines for vibration-

  18. Advanced Mechanics of Piezoelectricity

    CERN Document Server

    Qin, Qing-Hua

    2013-01-01

    "Advanced Mechanics of Piezoelectricity" presents a comprehensive treatment of piezoelectric materials using linear electroelastic theory, symplectic models, and Hamiltonian systems. It summarizes the current state of practice and presents the most recent research findings in piezoelectricity. It is intended for researchers and graduate students in the fields of applied mechanics, material science and engineering, computational engineering, and aerospace engineering. Dr. Qinghua Qin is a professor at the School of Engineering, Australian National University, Australia.

  19. Hybrid thermoelectric piezoelectric generator

    Science.gov (United States)

    Montgomery, D. S.; Hewitt, C. A.; Carroll, D. L.

    2016-06-01

    This work presents an integration of flexible thermoelectric and piezoelectric materials into a single device structure. This device architecture overcomes several prohibitive issues facing the combination of traditional thermoelectric and piezoelectric generators, while optimizing performance of the combined power output. The structure design uses a carbon nanotube/polymer thin film as a flexible thermoelectric generator that doubles as an electrode on a piezoelectric generator made of poly(vinylidene fluoride). An example 2 × 2 array of devices is shown to generate 89% of the maximum thermoelectric power, and provide 5.3 times more piezoelectric voltage when compared with a traditional device.

  20. Influence of Parasitic Capacitance on Output Voltage for Series-Connected Thin-Film Piezoelectric Devices

    Directory of Open Access Journals (Sweden)

    Kensuke Kanda

    2012-12-01

    Full Text Available Series-connected thin film piezoelectric elements can generate large output voltages. The output voltage ideally is proportional to the number of connections. However, parasitic capacitances formed by the insulation layers and derived from peripheral circuitry degrade the output voltage. Conventional circuit models are not suitable for predicting the influence of the parasitic capacitance. Therefore we proposed the simplest model of piezoelectric elements to perform simulation program with integrated circuit emphasis (SPICE circuit simulations. The effects of the parasitic capacitances on the thin-film Pb(Zr, TiO3, (PZT elements connected in series on a SiO2 insulator are demonstrated. The results reveal the negative effect on the output voltage caused by the parasitic capacitances of the insulation layers. The design guidelines for the devices using series-connected piezoelectric elements are explained.

  1. Application of PMN-32PT Piezoelectric Crystals for Novel Air-coupled Ultrasonic Transducers

    Science.gov (United States)

    Kazys, Rymantas Jonas; Sliteris, Reimondas; Sestoke, Justina

    Due to very high piezoelectric properties of PMN-PT crystals they may significantly improve performance of air-coupled ultrasonic transducers. For these purpose vibrations of PMN-PT rectangular plates and strips were investigated. An air-coupled ultrasonic transducer and array consisting of 8 single piezoelectric strips were designed. Operation of the transducer was simulated by the finite element method using ANSYS Mechanical APDL Product Launcher software. Spatial distributions of displacements inside piezoelectric elements and matching strip were obtained. Experimental investigations were carried out by the laser Doppler vibrometer Polytec OFV-5000 and the Bruel&Kjaer microphone 4138 with the measurement amplifier NEXUS WH 3219. It was found that performance of the ultrasonic transducer with PMN-32PT crystals was a few times better than of a PZT based ultrasonic transducer.

  2. Ultra-flexible Piezoelectric Devices Integrated with Heart to Harvest the Biomechanical Energy.

    Science.gov (United States)

    Lu, Bingwei; Chen, Ying; Ou, Dapeng; Chen, Hang; Diao, Liwei; Zhang, Wei; Zheng, Jun; Ma, Weiguo; Sun, Lizhong; Feng, Xue

    2015-11-05

    Power supply for medical implantable devices (i.e. pacemaker) always challenges not only the surgery but also the battery technology. Here, we report a strategy for energy harvesting from the heart motion by using ultra-flexible piezoelectric device based on lead zirconate titanate (PZT) ceramics that has most excellent piezoelectricity in commercial materials, without any burden or damage to hearts. Experimental swine are selected for in vivo test with different settings, i.e. opened chest, close chest and awake from anesthesia, to simulate the scenario of application in body due to their hearts similar to human. The results show the peak-to-peak voltage can reach as high as 3 V when the ultra-flexible piezoelectric device is fixed from left ventricular apex to right ventricle. This demonstrates the possibility and feasibility of fully using the biomechanical energy from heart motion in human body for sustainably driving implantable devices.

  3. Research on Effective Electric-Mechanical Coupling Coefficient of Sandwich Type Piezoelectric Ultrasonic Transducer Using Bending Vibration Mode

    Directory of Open Access Journals (Sweden)

    Qiang Zhang

    2015-01-01

    Full Text Available An analytical model on electromechanical coupling coefficient and the length optimization of a bending piezoelectric ultrasonic transducer are proposed. The piezoelectric transducer consists of 8 PZT elements sandwiched between four thin electrodes, and the PZT elements are clamped by a screwed connection between fore beam and back beam. Firstly, bending vibration model of the piezoelectric transducer is built based on the Timoshenko beam theory. Secondly, the analytical model of effective electromechanical coupling coefficient is built based on the bending vibration model. Energy method and electromechanical equivalent circuit method are involved in the modelling process. To validate the analytical model, sandwich type piezoelectric transducer example in second order bending vibration mode is analysed. Effective electromechanical coupling coefficient of the transducer is optimized with simplex reflection technique, and the optimized ratio of length of the transducers is obtained. Finally, experimental prototypes of the sandwich type piezoelectric transducers are fabricated. Bending vibration mode and impedance of the experimental prototypes are tested, and electromechanical coupling coefficient is obtained according to the testing results. Results show that the analytical model is in good agreement with the experimental model.

  4. A novel multi-degree-of-freedom thick-film ultrasonic motor.

    Science.gov (United States)

    Aoyagi, Manaba; Beeby, Steve P; White, Neil M

    2002-02-01

    This paper describes a new multi-degree-of-freedom (MDOF) ultrasonic motor that comprises few parts and is based on low-cost thick-film technology. Conventional ultrasonic motors using bulk lead zirconate titanate (PZT) or thin-film PZT layers are relatively expensive at the present time. Thick-film printed PZT technology provides the opportunity to reduce the costs of ultrasonic motors. To demonstrate the feasibility of this approach, an ultrasonic motor was fabricated from alumina using thick-film printed PZT actuators. The thick-film PZT and electrode layers were printed on a thin alumina plate, and a tiny cylinder was mounted at its center. This cylinder magnifies the lateral displacement of the stator, holds the spherical rotor, and transmits the driving force to the sphere. Three bending vibrations, B22, B30, B03, of the plate were applied to rotate the sphere. Sufficient displacements for rotating the sphere were obtained near the resonance of B22 by applying an excitation voltage of 200 V peak-to-peak via a three-phase drive circuit. Rotations in three orthogonal directions have been observed by controlling the phase of the driving signal to the PZT electrodes, and a MDOF ultrasonic motor was successfully realized.

  5. Study on the electromechanical coupling coefficient of Rayleigh-type surface acoustic waves in semi-infinite piezoelectrics/non-piezoelectrics superlattices.

    Science.gov (United States)

    Chen, Shi; Zhang, Yinhong; Lin, Shuyu; Fu, Zhiqiang

    2014-02-01

    The electromechanical coupling coefficient of Rayleigh-type surface acoustic waves in semi-infinite piezoelectrics/non-piezoelectrics superlattices is investigated by the transfer matrix method. Research results show the high electromechanical coupling coefficient can be obtained in these systems. The optimization design of it is also discussed fully. It is significantly influenced by electrical boundary conditions on interfaces, thickness ratios of piezoelectric and non-piezoelectric layers, and material parameters (such as velocities of pure longitudinal and transversal bulk waves in non-piezoelectric layers). In order to obtain higher electromechanical coupling coefficient, shorted interfaces, non-piezoelectric materials with large velocities of longitudinal and transversal bulk waves, and proper thickness ratios should be chosen.

  6. BIMORPH-TYPE PIEZOELECTRIC THIN FILM BENDING ACTUATORS SYNTHESIZED BY HYDROTHERMAL METHOD

    Institute of Scientific and Technical Information of China (English)

    Du Liqun; Arai Fumihito; Fukuda Toshio; Kwon Guiryong

    2004-01-01

    Lead zirconate titanium solid-solution (PZT) thin films with various thickness are synthesized on titanium substrates by repeated hydrothermal treatments.Young modulus,electric-field- induced displacement and the density of the PZT film are measured respectively.Bimorph- type bending actuators are fabricated using these films.The model,which is used to analyze the driving ability of bimorph-type bending actuators by hydrothermal method,is set up.It can be seen that the driving ability of bimorph-type bending actuators can be greatly improved by optimizing the thickness of PZT thin film and substrate from the theoretical analysis results.The measured values are expected to agree with the theoretical values calculated by the above model.

  7. Design and analysis of a piezoelectric material based touch screen with additional pressure and its acceleration measurement functions

    Science.gov (United States)

    Chu, Xiang-Cheng; Liu, Jia-Yi; Gao, Ren-Long; Chang, Jie; Li, Long-Tu

    2013-12-01

    Touch screens are becoming more and more prevalent in everyday environments due to their convenience and humanized operation. In this paper, a piezoelectric material based touch screen is developed and investigated. Piezoelectric ceramics arrayed under the touch panel at the edges or corners are used as tactile sensors to measure the touch positioning point similarly to conventional touch screens. However, additional touch pressure and its acceleration performance can also be obtained to obtain a higher-level human-machine interface. The piezoelectric ceramics can also be added to a traditional touch screen structure, or they can be used independently to construct a novel touch screen with a high light transmittance approach to a transparent glass. The piezoelectric ceramics were processed from PZT piezoelectric ceramic powder into a round or rectangular shape. According to the varied touch position and physical press strength of a finger, or even a gloved hand or fingernail, the piezoelectric tactile sensors will have different output voltage responses. By calculating the ratio of different piezoelectric tactile sensors’ responses and summing up all piezoelectric tactile sensors’ output voltages, the touch point position, touch pressure and touch force acceleration can be detected. A prototype of such a touch screen is manufactured and its position accuracy, touch pressure and response speed are measured in detail. The experimental results show that the prototype has many advantages such as high light transmittance, low energy cost and high durability.

  8. Piezoelectric Micro- and Nanostructured Fibers Fabricated from Thermoplastic Nanocomposites Using a Fiber Drawing Technique: Comparative Study and Potential Applications.

    Science.gov (United States)

    Lu, Xin; Qu, Hang; Skorobogatiy, Maksim

    2017-02-28

    We report an all-polymer flexible piezoelectric fiber that uses both judiciously chosen geometry and advanced materials in order to enhance fiber piezoelectric response. The microstructured/nanostructured fiber features a soft hollow polycarbonate core surrounded by a spiral multilayer cladding consisting of alternating layers of piezoelectric nanocomposites (polyvinylidene enhanced with BaTiO3, PZT, or CNT) and conductive polymer (carbon-filled polyethylene). The conductive polymer layers serve as two electrodes, and they also form two spatially offset electric connectors on the fiber surface designed for the ease of connectorization. Kilometer-long piezoelectric fibers of sub-millimeter diameters are thermally drawn from a macroscopic preform. The fibers exhibit high output voltage of up to 6 V under moderate bending, and they show excellent mechanical and electrical durability in a cyclic bend-release test. The micron/nanosize multilayer structure enhances in-fiber poling efficiency due to the small distance between the conducting electrodes sandwiching the piezoelectric composite layers. Additionally, the spiral structure greatly increases the active area of the piezoelectric composite, thus promoting higher voltage generation and resulting in 10-100 higher power generation efficiency over the existing piezoelectric cables. Finally, we weave the fabricated piezoelectric fibers into technical textiles and demonstrate their potential applications in power generation when used as a sound detector, smart car seat upholstery, or wearable materials.

  9. Sol-gel PZT and Mn-doped PZT thin films for pyroelectric applications

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Q. [Advanced Materials Group, School of Industrial and Manufactory Science, Cranfield University, Beds (United Kingdom)]. E-mail: q.zhang@cranfield.ac.uk; Whatmore, R.W. [Advanced Materials Group, School of Industrial and Manufactory Science, Cranfield University, Beds (United Kingdom)

    2001-08-07

    Thin films of ferroelectric lead zirconate titanate (PbZr{sub 0.3}Ti{sub 0.7}O{sub 3} PZT30/70) and manganese-doped lead zirconate titanate ((Pb(Zr{sub 0.3}Ti{sub 0.7}){sub 1-x}Mn{sub x})O{sub 3}, where x=0.01, PM01ZT30/70; and x=0.03, PM03ZT30/70) have been prepared using sol-gel processing techniques. These materials can be used as the pyroelectric thin films in uncooled infrared detectors. The thin films were prepared via a sol-gel route based on a hybrid solvent of methanol and ethanol with acetic acid, ethanolamine and ethylene glycol as additives. The final solution is non-moisture sensitive and stable. Films deposited on Pt/Ti/SiO{sub 2}/Si substrates and annealed on a hot plate at 500-530{sup 0}C for a few minutes were seen to fully crystallize into the required perovskite phase and showed excellent ferroelectric behaviour, demonstrated by reproducible hysteresis loops (P{sub r}=33-37 {mu}C cm{sup -2}, Ec(+)=70-100 kV cm{sup -1}, Ec(-)=-170 to -140 kV cm{sup -1}). The pyroelectric coefficient (p) was measured using the Byer-Roundy method. At 20 deg. C, p was 2.11x10{sup -4} C m{sup -2} K{sup -1} for PZT30/70, 3.00x10{sup -4} C m{sup -2} K{sup -1} for PM01ZT30/70 and 2.40x10{sup -4} C m{sup -2} K{sup -1} for PM03ZT30/70 thin films. The detectivity figure-of-merit (F{sub D}) was 1.07x10{sup -5} Pa{sup -0.5} for PZT30/70, 3.07x10{sup -5} Pa{sup -0.5} for PM01ZT30/70 and 1.07x10{sup -5} Pa{sup -0.5} for PM03ZT30/70. These figures compare well with values reported previously. (author)

  10. Modeling of PZT Ferroelectric Ceramic Depolarization Driven by Shock Stress

    Institute of Scientific and Technical Information of China (English)

    LAN Chao-Hui; PENG Yu-Fei; LONG Ji-Dong; WANG Qiang; WANG Wen-Dou

    2011-01-01

    @@ Shock-induced phase transition of ferroelectric ceramic PZT 95/5 causes elastic stiffening and depolarization,releasing stored electrostatic energy into the load circuit.We develop a model to describe the response of the PZT ferroelectric ceramic and implement it into simulation codes.The model is based on the phenomenological theory of phase transition dyynamics and takes into account the effects of the self-generated intensive electrical field and stress.Connected with the discharge model and external circuit, the whole transient process of PZT ceramic depoling can be investigated.The results show the finite transition velocity of the ferroelectric phase and the double wave structure caused by phase transition.Simulated currents are compared with the results from experiments with shock pressures varying from 0.4 to 2.8GPa.

  11. Elastodynamic Impact into Piezoelectric Media

    Science.gov (United States)

    2014-09-01

    boundary condition to the problem of elastodynamic impact into a lead zirconate titanate (PZT-4) target and find that the solutions obtained using... titanate (PZT-4) target are compared with solutions obtained using a finite-difference time-domain (FDTD) code and the commercial finite element (FE

  12. Enhancement of the magnetoelectric coupling in an A-line shape magnetostrictive/piezoelectric structure

    Science.gov (United States)

    Zhang, Juanjuan; Kang, Yan; Yu, Yang; Gao, Yuanwen

    2017-01-01

    In this study, a new kind of magnetoelectric (ME) structure is designed with Terfenol-D, PZT-5A and nonmagnetic and nonelectric trestle. The configuration of this ME structure presents "A-line" type, PZT-5A and Terfenol-D are respectively bonded with the trestles, which adopt the knuckle joint assembly. Differently from the conventional ME layered structure, in the new structure, the deformation of the PZT-5A of larger size is driven by a Terfenol-D layer of smaller size at an external magnetic field. Since the driven force is applied at the ends of piezoelectric layer through the trestles, the whole piezoelectric layer can be completely stretched or compressed, and the larger voltage should be induced. For the new ME structure with mica trestle, the maximum value of αE is twice higher than that for the conventional laminated ME structure. Furthermore, a wider range of response frequency is also observed in this structure. For the new ME structure with ABS trestle, the experimental results indicate that the maximum ME voltage coefficient is measured as high as 31.85 V/cm Oe at 405 Oe.

  13. High-power piezoelectric characteristics of textured bismuth layer structured ferroelectric ceramics.

    Science.gov (United States)

    Ogawa, Hirozumi; Kawada, Shinichiro; Kimura, Masahiko; Shiratsuyu, Kousuke; Sakabe, Yukio

    2007-12-01

    Abstract-The high-power piezoelectric characteristics in h001i oriented ceramics of bismuth layer structured ferroelectrics (BLSF), SrBi(2)Nb(2)O(9) (SBN), (Bi,La)(4)Ti(3)O(12) (BLT), and CaBi(4)Ti(4)O(15) (CBT), were studied by a constant voltage driving method. These textured ceramics were fabricated by a templated grain growth (TGG) method, and their Lotgering factors were 95%, 97%, and 99%, respectively. The vibration velocities of the longitudinal mode (33-mode) increased proportionally to an applied electric field up to 2.5 m/s in these textured BLSF ceramics, although, the vibration velocity of the 33-mode was saturated at more than 1.0 m/s in the Pb(Mn,Nb)O(3)-PZT ceramics. The resonant frequencies were constant up to the vibration velocity of 2.5 m/s in the SBN and CBT textured ceramics; however, the resonant frequency decreased with increasing over the vibration velocity of 1.5 m/s in the BLT textured ceramics. The dissipation power density of the BLT was almost the same as that of the Pb(Mn,Nb)O(3)-PZT ceramics. However, the dissipation power densities of the SBN and CBT were lower than those of the BLT and Pb(Mn,Nb)O(3)-PZT ceramics. The textured SBN and CBT ceramics are good candidates for high-power piezoelectric applications.

  14. Controllability assessment of plate-like structures with uncertainties under piezoelectric actuation

    Science.gov (United States)

    Li, Y. Y.; Cheng, L.

    2005-02-01

    A controllability assessment of plate-like structures with uncertainties under piezoelectric actuation is performed in this paper. Different from the previous studies, a novel index is proposed to quantify the degree of controllability using the sensor/actuator transfer function. Influences of unmodelled high-frequency dynamics and structural parameter variations on controllability are discussed, and the relationship between the indices for the nominal and uncertain cases is derived. In order to validate the controllability assessment numerically, the modelling of a plate with piezoelectric actuation is developed with the consideration of the full coupling between the PZT actuators and the host plate, and verified by experiments. It is demonstrated that a proper design of the polyvinylidene flouride sensor would help eliminate effects of higher order modes on the basis of strain mode shapes. Since the latter is very sensitive to the mass and stiffness added by PZT actuators, the dynamics of PZT actuators must be taken into account during the design, as opposed to the case where a point transducer is used.

  15. Numerical analysis for structural health monitoring of a damaged composite panel using PZT actuators and sensors

    Science.gov (United States)

    Nagabhushana, A.; Spiegel, M.; Adu, S.; Hayes, N.; Paul, D.; Trivedi, K.; Fairbee, B.; Zheng, H.; Gerrity, A.; Kotru, S.; Roy, S.; Barkey, M.; Burkett, S. L.

    2012-04-01

    Reliable damage detection is crucial for assessing the integrity of a structure. In this paper, a numerical study of a composite panel fabricated to simulate a crack is undertaken using finite element methods (FEM). The damage to be considered is a transverse crack which pre-exists in the structure. The finite element models are developed for an undamaged and a damaged composite panel to compute the change in Lamb wave response due to the existence of a crack. The model is validated using shear lag analysis applied at the crack. The results are verified experimentally by comparing the results for an undamaged composite panel and a composite panel fabricated with a simulated crack using the vacuum assisted resin transfer molding (VARTM) process. The responses for each panel are obtained using surface mounted lead zirconate titanate (PZT) actuators and sensors. PZT is used to generate Lamb waves which produce stress throughout the panel thickness. Propagation characteristics of Lamb waves are varied by the presence of damage. The sensor data provide reliable information about the integrity of the structure. Numerical results are compared to the sensor output to ensure accuracy of the damage detection system.

  16. PERFORMANCE, COMBUSTION AND EMISSION CHARACTERISTICS OF PZT LOADED CYANATE MODIFIED EPOXY COATED COMBUSTION CHAMBER IN DIESEL ENGINE

    Directory of Open Access Journals (Sweden)

    Vijaya Kumar K.R

    2010-07-01

    Full Text Available Energy conservation and emissions have become increasing concern over the past few decades. PZT loaded cyanate modified epoxy (60EPCY 20PI coated material were initially investigated for adiabatic diesel engines based on first law of thermodynamics prediction of significant fuel economy improvements, reduction in heat rejection and potential increased power density of the diesel engines. The purpose of 60EPCY 20PI is to focus on developing binder systems with low thermal conductivity and improve the coating durability under high load condition. The coating material is made up of 20% Lead Zirconate Titanate (PZT in 60% Cyanate modified Epoxy system. The triazine ring of cyanate ester offers better thermal resistance characteristics to the epoxy system. Experimental investigation is carried out under different load condition on a single cylinder dieselengine with PZT loaded cyanate modified epoxy resin system of 0.5 mm thickness to the piston, cylinder head with valves and cylinder liner. The result showed 15.89 %of reduced specific fuel consumption. Emissions of unburnt hydrocarbon, carbon monoxide are reduced.

  17. Piezoelectric and pyroelectric properties of Sr-doped PZT (PSZT) with minor manganese additions

    Science.gov (United States)

    Aleem, M. A.; Nawaz, H.; Shuaib, M.; Qaisar, S.; Akbar, M. S.

    2013-06-01

    A systematic study was performed to see the effect of Manganese addition and temperature gradient on the electrical properties of PSZT. Pb0.96 Sr0.04 (Zr0.52Ti0.48) O3 (PSZT) containing 0.3%, 0.5%, and 1% Mn was prepared by the sol gel method in order to ensure good stoichiometry and enhanced purity. The powders were calcined at 550 °C and sintered at 1200 °C to achieve 98% of the theoretical density. High field ac study was performed by (P-E) hysteresis measurements at different temperatures (RT, 60, 90, 120 and 150 °C) using an electric field up to 3 kV/mm. It was observed that for a lower Mn concentration P-E loops are pinched at the center while this constriction is found to decrease for greater concentrations. The optimized results were obtained for the 1 mol% of Mn content with 4 mol% of Sr. The values of Qm, k, d33 and tanδ were measured as 756, 0.38, 257 and 0.002 respectively. Higher temperatures coupled with a gradual increase of the electric field resulted in a shift of the hysteresis loops along electric field axis, indicating the presence of an internal bias field. Dependence of pyroelectric properties on applied electric field was also investigated. The value of pyroelectric coefficient was found maximum 6.25 × 10-4 (C/m2K) at 3 kV/mm.

  18. Analysis of the electrically forced vibrations of piezoelectric mesa resonators

    Institute of Scientific and Technical Information of China (English)

    He Hui-Jing; Nie Guo-Quan; Liu Jin-Xi; Yang Jia-Shi

    2013-01-01

    We study the electrically forced thickness-shear and thickness-twist vibrations of stepped thickness piezoelectric plate mesa resonators made of polarized ceramics or 6-mm class crystals.A theoretical analysis based on the theory of piezoelectricity is performed,and an analytical solution is obtained using the trigonometric series.The electrical admittance,resonant frequencies,and mode shapes are calculated,and strong energy trapping of the modes is observed.Their dependence on the geometric parameters of the resonator is also examined.

  19. Synthesis and characterization of tungsten or calcium doped PZT ceramics; Sintese e caracterizacao do PZT dopado com W ou Ca

    Energy Technology Data Exchange (ETDEWEB)

    Santos, D.M.; Caracas, L.B.; Noronha, R.G.; Santos, M.M.T. dos [Universidade Federal do Maranhao (UFMA), Sao Luis, MA (Brazil). Dept. de Desenho e Tecnologia. Curso de Desenho Industrial; Paiva-Santos, C.O., E-mail: denilson@ufma.b [Universidade Estadual Paulista (IQ/UNESP), Araraquara, SP (Brazil). Inst. de Quimica

    2009-07-01

    Pure and doped (tungsten or calcium) PZT ceramics were prepared by association of the polymeric precursor and partial oxalate method. The phase formation was investigated by thermal analysis (TG/DSC) and X-ray diffraction (XRD). The affect of W or Ca doping PZT and their electrical properties was evaluated. Substitution of W by Ti and Ca by Pb leads to an increase of Curie temperature and broadening of dielectric constant. A typical hysteresis loop was observed at room temperature and the remnant polarization was increased with the content of W and Ca. (author)

  20. On the buckling behavior of piezoelectric nanobeams: An exact solution

    Energy Technology Data Exchange (ETDEWEB)

    Jandaghian, Ali Akbar; Rahmaini, Omid [University of Zanjan, Zanjan (Iran, Islamic Republic of)

    2015-08-15

    In this paper, thermoelectric-mechanical buckling behavior of the piezoelectric nanobeams is investigated based on the nonlocal theory and Euler-Bernoulli beam theory. The electric potential is assumed linear through the thickness of the nanobeam and the governing equations are derived by Hamilton's principle. The governing equations are solved analytically for different boundary conditions. The effects of the nonlocal parameter, temperature change, and external electric voltage on the critical buckling load of the piezoelectric nanobeams are discussed in detail. This study should be useful for the design of piezoelectric nanodevices.

  1. Nonmagnetic driver for piezoelectric actuators

    DEFF Research Database (Denmark)

    Ekhtiari, Marzieh

    2014-01-01

    Piezoelectric actuator drive aims to enable reliable motor performance in strong magnetic fields for magnetic res- onance imaging and computed tomography treatment tables. There are technical limitations in operation of these motors and drive systems related to magnetic interference. Piezoelectric...... actuators. Therefore, piezoelectric transformer-based power converters are used for driving piezoelectric actuator drive motor in the presence of high electromagnetic field....

  2. Synthesis of PZT power by wet-dry method and its structure

    Institute of Scientific and Technical Information of China (English)

    汤卉; 王佳; 高维丽

    2008-01-01

    To prepare PZT powder at lower temperature, lead zirconate titanate (PZT) powder (x(Zr)/x(Ti)=56?44) was prepared by wet-dry method. Glycol was used as the solvent, and zirconium oxychloride was used as zirconium source. The properties and structure of the powder were analyzed by XRD, SEM and Sedimentograph. The effects of sintering parameter such as sintering temperature, keeping time and heating-up velocity on structure of PZT power were investigated. The results show that homogeneous PZT with single-phase perovskite structure can be obtained after sintering at 730 ℃ for 2 h, and the average size of PZT powder is about 113 nm.

  3. Microfabrication and Integration of a Sol-Gel PZT Folded Spring Energy Harvester

    Directory of Open Access Journals (Sweden)

    Jonathan Lueke

    2015-05-01

    Full Text Available This paper presents the methodology and challenges experienced in the microfabrication, packaging, and integration of a fixed-fixed folded spring piezoelectric energy harvester. A variety of challenges were overcome in the fabrication of the energy harvesters, such as the diagnosis and rectification of sol-gel PZT film quality and adhesion issues. A packaging and integration methodology was developed to allow for the characterizing the harvesters under a base vibration. The conditioning circuitry developed allowed for a complete energy harvesting system, consisting a harvester, a voltage doubler, a voltage regulator and a NiMH battery. A feasibility study was undertaken with the designed conditioning circuitry to determine the effect of the input parameters on the overall performance of the circuit. It was found that the maximum efficiency does not correlate to the maximum charging current supplied to the battery. The efficiency and charging current must be balanced to achieve a high output and a reasonable output current. The development of the complete energy harvesting system allows for the direct integration of the energy harvesting technology into existing power management schemes for wireless sensing.

  4. Dynamic modeling and analysis of the PZT-bonded composite Timoshenko beams: Spectral element method

    Science.gov (United States)

    Lee, Usik; Kim, Daehwan; Park, Ilwook

    2013-03-01

    The health of thin laminated composite beams is often monitored using the ultrasonic guided waves excited by wafer-type piezoelectric transducers (PZTs). Thus, for the smart composite beams which consist of a laminated composite base beam and PZT layers, it is very important to develop a very reliable mathematical model and to use a very accurate computational method to predict accurate dynamic characteristics at very high ultrasonic frequency. In this paper, the axial-bending-shear-lateral contraction coupled differential equations of motion are derived first by the Hamilton's principle with Lagrange multipliers. The smart composite beam is represented by a Timoshenko beam model by adopting the first-order shear deformation theory (FSDT) for the laminated composite base beam. The axial deformation of smart composite beam is improved by taking into account the effects of lateral contraction by adopting the concept of Mindlin-Herrmann rod theory. The spectral element model is then formulated by the variation approach from coupled differential equations of motion transformed into the frequency domain via the discrete Fourier transform. The high accuracy of the present spectral element model is verified by comparing with other solution methods: the finite element model developed in this paper and the commercial FEA package ANSYS. Finally the dynamics and wave characteristics of some example smart composite beams are investigated through the numerical studies.

  5. Microfabrication and integration of a sol-gel PZT folded spring energy harvester.

    Science.gov (United States)

    Lueke, Jonathan; Badr, Ahmed; Lou, Edmond; Moussa, Walied A

    2015-05-26

    This paper presents the methodology and challenges experienced in the microfabrication, packaging, and integration of a fixed-fixed folded spring piezoelectric energy harvester. A variety of challenges were overcome in the fabrication of the energy harvesters, such as the diagnosis and rectification of sol-gel PZT film quality and adhesion issues. A packaging and integration methodology was developed to allow for the characterizing the harvesters under a base vibration. The conditioning circuitry developed allowed for a complete energy harvesting system, consisting a harvester, a voltage doubler, a voltage regulator and a NiMH battery. A feasibility study was undertaken with the designed conditioning circuitry to determine the effect of the input parameters on the overall performance of the circuit. It was found that the maximum efficiency does not correlate to the maximum charging current supplied to the battery. The efficiency and charging current must be balanced to achieve a high output and a reasonable output current. The development of the complete energy harvesting system allows for the direct integration of the energy harvesting technology into existing power management schemes for wireless sensing.

  6. INVESTIGATION ON THE BUCKLING OF DELAMINATION BETWEEN ELECTRODE AND PIEZOELECTRIC LAYER WITH FINITE THICKNESS%有限厚压电层表面金属电极脱层的屈曲研究

    Institute of Scientific and Technical Information of China (English)

    杨昌锦; 李尧臣

    2009-01-01

    基于弹性有限变形理论和压电弹性体偏场理论,对上、下表面有金属电极的压电材料板内存在穿透脱层的屈曲问题进行了分析.采用平面应变模型,远处作用有均匀压应变载荷.用Fourier积分变换,界面连续条件和上、下电极表面的边界条件将问题归为第二类Cauchy型奇异积分方程组.利用Gauss-Chebyshev积分公式将该方程组变为一齐次线性代数方程组,以确定脱层屈曲载荷.算例给出了中间层为PZT-4,上、下电极为Pt的结构在不同脱层长厚比时的临界应变及相应屈曲形状.同时分析了压电层的机电耦合效应对临界应变的影响.

  7. Modeling and analysis of a circular PZT energy-generator used in hydraulic liquid absorber%液压流体吸振器用圆形压电发电装置的建模与性能分析

    Institute of Scientific and Technical Information of China (English)

    王淑云; 阚君武; 王鸿云; 李征; 赵子超; 万杰; 曹迪

    2012-01-01

    A piezoelectric energy harvester used in hydraulic liquid absorber was presented. To enhance the energy-generating capability and obtain the optimal structural/material parameters, the analysis model of clamped PZT disk generator under concentrated force was established utilizing the theory of plates and shells. The influences of radius ratio (λ) , thickness ratio (β) as well as material Young's modulus ratio ( ζ) of the PZT disk on energy generation were investigated. The results show that there is an optimal pair of X and β for a PZT disk generator with given ζ to obtain maximal electrical energy. Similarly, in the case of given X and β, there is an optimal ζ, which decreases with the decrease of β and is not influenced by the change of X under given β. At the same time, reducing ζ is helpful for the generator to generate more electrical energy. When aluminum or beryllium bronze plates are used as substrates, the optimal radius ratio and thickness ratio are (0.45, 0.45) or (0.585, 0.6), respectively. The maximal electric energy generated are 1.14643 x 10 -4J and 1.01893 x 10-4J, respectively.%提出一种用于液压流体吸振器的压电发电装置.为提高所用圆形压电振子的发电能力,获得最优的结构及材料性能参数,利用板壳理论建立了固支边界条件下的位移曲线及发电量的理论分析模型,研究了半径比(陶瓷/基板)、厚度比(陶瓷/总厚度)及弹性模量比(基板/陶瓷)等对其发电能力的影响规律.研究表明,在压电振子材料确定时,存在最佳的半径比和厚度比使其发电能力最大;在压电振子结构尺寸确定时,存在最佳的弹性模量比使发电量最大,且厚度比确定时的最佳弹性模量比与半径比无关、半径比确定时的最佳弹性模量比随厚度比的减小而降低;减小弹性模量比有助于提高压电振子的发电能力.铝基板及铍青铜基板压电振子的最佳半径比/厚度比分别为0.45/0.45和0

  8. Fiber-optic raster scanning two-photon endomicroscope using a tubular piezoelectric actuator

    Science.gov (United States)

    Do, Dukho; Yoo, Hongki; Gweon, Dae-Gab

    2014-06-01

    A nonresonant, fiber-optic raster scanning endomicroscope was developed using a quarter-tubular piezoelectric (PZT) actuator. A fiber lever mechanism was utilized to enhance the small actuation range of the tubular PZT actuator and to increase its field-of-view. Finite element method simulation of the endoscopic probe was conducted for various conditions to maximize its scanning range. After fabricating the probe using a double clad fiber, we obtained two-photon fluorescence images using raster beam scanning of the fiber. The outer diameter of the probe was 3.5 mm and its rigid distal length was 30 mm including a high numerical aperture gradient index lens. These features are sufficient for input into the instrumental channel of a commercial colonoscope or gastroscope to obtain high resolution images in vivo.

  9. Bio-inspired piezoelectric artificial hair cell sensor fabricated by powder injection molding

    Science.gov (United States)

    Han, Jun Sae; Oh, Keun Ha; Moon, Won Kyu; Kim, Kyungseop; Joh, Cheeyoung; Seo, Hee Seon; Bollina, Ravi; Park, Seong Jin

    2015-12-01

    A piezoelectric artificial hair cell sensor was fabricated by the powder injection molding process in order to make an acoustic vector hydrophone. The entire process of powder injection molding was developed and optimized for PMN-PZT ceramic powder. The artificial hair cell sensor, which consists of high aspect ratio hair cell and three rectangular mechanoreceptors, was precisely fabricated through the developed powder injection molding process. The density and the dielectric property of the fabricated sensor shows 98% of the theoretical density and 85% of reference dielectric property of PMN-PZT ceramic powder. With regard to homogeneity, three rectangular mechanoreceptors have the same dimensions, with 3 μm of tolerance with 8% of deviation of dielectric property. Packaged vector hydrophones measure the underwater acoustic signals from 500 to 800 Hz with -212 dB of sensitivity. Directivity of vector hydrophone was acquired at 600 Hz as analyzing phase differences of electric signals.

  10. Three-degree-of-freedom ultrasonic motor using a 5-mm-diameter piezoelectric ceramic tube.

    Science.gov (United States)

    Mingsen Guo; Junhui Hu; Hua Zhu; Chunsheng Zhao; Shuxiang Dong

    2013-07-01

    A small three-degree-of-freedom ultrasonic motor has been developed using a simple piezoelectric lead zirconate titanate (PZT)-tube stator (OD 5 mm, ID 3 mm, length 15 mm). The stator drives a ball-rotor into rotational motion around one of three orthogonal (x-, y-, and z-) axes by combing the first longitudinal and second bending vibration modes. A motor prototype was fabricated and characterized; its performance was superior to those of previous motors made with a PZT ceramic/metal composite stator of comparable size. The method for further improving the performance was discussed. The motor can be further miniaturized and it has potential to be applied to medical microrobots, endoscopes or micro laparoscopic devices, and cell manipulation devices.

  11. Preparation and Characterization of PZT films Fabricated on Si Substrate

    Institute of Scientific and Technical Information of China (English)

    YANG Ying

    2006-01-01

    Lead zirconium titanate (PZT) films (Zr/Ti=45:55)with a high dielectric constant are prepared successfully on the low-resistance Si substrate in sol-gel dip-coating process with PT film used as the buffer layer.The dielectric and ferroelectric properties of the films as well as the relationship between crystallization and preparing condition are studied.It is shown that the PZT ferroelectric thin films with a (110) preferred orientation and a well-crystallized perovskite structure could be obtained after annealing at 800℃ for 15 min.The particle size of the sample is about 14-25 nm.The P-E hysteresis loops are measured by means of the Sawyer-Tower test system with a compensation resistor at room temperature.The remanent polarization (Pr) and coercive electric field (Ec) of the measured PZT thin films are 47.7 μC/cm2 and 18 kV/cm,respectively.The relative dielectric constant εr and the dissipation factor tgδ of the PZT thin films were measured with an LCR meter and were found to be 158 and 0.04-0.005,respectively.

  12. Specific Heat, Charge Release and Dielectric Constant of PZT Ceramics

    NARCIS (Netherlands)

    Cereceda, N.; Noheda, B.; Gonzalo, J.A.; Mielcarek, S.; Mroz, B.

    1998-01-01

    Dielectric constant, specific heat and charge release measurements have been performed to study the FRL-FRH and FRH-PC phase transitions in Zr rich PZT (PbZr1-xTixO3). Both transitions have been described together by means of a two order parameters effective field model, in order to include the

  13. Dielectric properties of novel polyurethane-PZT-graphite foam composites

    Science.gov (United States)

    Tolvanen, Jarkko; Hannu, Jari; Nelo, Mikko; Juuti, Jari; Jantunen, Heli

    2016-09-01

    Flexible foam composite materials offer multiple benefits to future electronic applications as the rapid development of the electronics industry requires smaller, more efficient, and lighter materials to further develop foldable and wearable applications. The aims of this work were to examine the electrical properties of three- and four-phase novel foam composites in different conditions, find the optimal mixture for four-phase foam composites, and study the combined effects of lead zirconate titanate (PZT) and graphite fillers. The flexible and highly compressible foams were prepared in a room-temperature mixing process using polyurethane, PZT, and graphite components as well as their combinations, in which air acted as one phase. In three-phase foams the amount of PZT varied between 20 and 80 wt% and the amount of graphite, between 1 and 15 wt%. The four-phase foams were formed by adding 40 wt% of PZT while the amount of graphite ranged between 1 and 15 wt%. The presented results and materials could be utilized to develop new flexible and soft sensor applications by means of material technology.

  14. Piezoelectric cantilever sensors

    Science.gov (United States)

    Shih, Wan Y. (Inventor); Shih, Wei-Heng (Inventor); Shen, Zuyan (Inventor)

    2008-01-01

    A piezoelectric cantilever with a non-piezoelectric, or piezoelectric tip useful as mass and viscosity sensors. The change in the cantilever mass can be accurately quantified by monitoring a resonance frequency shift of the cantilever. For bio-detection, antibodies or other specific receptors of target antigens may be immobilized on the cantilever surface, preferably on the non-piezoelectric tip. For chemical detection, high surface-area selective absorbent materials are coated on the cantilever tip. Binding of the target antigens or analytes to the cantilever surface increases the cantilever mass. Detection of target antigens or analytes is achieved by monitoring the cantilever's resonance frequency and determining the resonance frequency shift that is due to the mass of the adsorbed target antigens on the cantilever surface. The use of a piezoelectric unimorph cantilever allows both electrical actuation and electrical sensing. Incorporating a non-piezoelectric tip (14) enhances the sensitivity of the sensor. In addition, the piezoelectric cantilever can withstand damping in highly viscous liquids and can be used as a viscosity sensor in wide viscosity range.

  15. Periodical Microstructures Based on Novel Piezoelectric Material for Biomedical Applications

    Directory of Open Access Journals (Sweden)

    Giedrius Janusas

    2015-12-01

    Full Text Available A novel cantilever type piezoelectric sensing element was developed. Cost-effective and simple fabrication design allows the use of this element for various applications in the areas of biomedicine, pharmacy, environmental analysis and biosensing. This paper proposes a novel piezoelectric composite material whose basic element is PZT and a sensing platform where this material was integrated. Results showed that a designed novel cantilever-type element is able to generate a voltage of up to 80 µV at 50 Hz frequency. To use this element for sensing purposes, a four micron periodical microstructure was imprinted. Silver nanoparticles were precipitated on the grating to increase the sensitivity of the designed element, i.e., Surface Plasmon Resonance (SPR effect appears in the element. To tackle some issues (a lack of sensitivity, signal delays the element must have certain electronic and optical properties. One possible solution, proposed in this paper, is a combination of piezoelectricity and SPR in a single element.

  16. Concurrent operational modes and enhanced current sensitivity in heterostructure of magnetoelectric ring and piezoelectric transformer

    Science.gov (United States)

    Zhang, Shengyao; Ming Leung, Chung; Kuang, Wei; Wing Or, Siu; Ho, S. L.

    2013-05-01

    A heterostructure possessing two concurrent operational modes: current sensing (CS) mode and current transduction (CT) mode and an enhanced current sensitivity associated with the CT mode is proposed by combining a magnetoelectric ring (MER) with a piezoelectric transformer (PET). The MER is a ring-shaped magnetoelectric laminate having an axially polarized Pb(Zr, Ti)O3 (PZT) piezoelectric ceramic ring sandwiched between two circumferentially magnetized, inter-magnetically biased Tb0.3Dy0.7Fe1.92 (Terfenol-D) short-fiber/NdFeB magnet/epoxy three-phase magnetostrictive composite rings, while the PET is a Rosen-type PZT piezoelectric ceramic transformer. The current sensitivity (SI) and magnetoelectric voltage coefficient (αV) of the heterostructure in the two operational modes are evaluated theoretically and experimentally. The CS mode provides a large SI of ˜10 mV/A over a flat frequency range of 10 Hz-40 kHz with a high resonance SI of 157 mV/A at 62 kHz. The CT mode gives a 6.4-times enhancement in resonance SI, reaching 1000 mV/A at 62 kHz, as a result of the amplified vortex magnetoelectric effect caused by the vortex magnetoelectric effect in the MER, the matching of the resonance frequencies between the MER and the PET, and the resonance voltage step-up effect in the PET.

  17. Performance of tonpilz transducers with segmented piezoelectric stacks using materials with high electromechanical coupling coefficient.

    Science.gov (United States)

    Thompson, Stephen C; Meyer, Richard J; Markley, Douglas C

    2014-01-01

    Tonpilz acoustic transducers for use underwater often include a stack of piezoelectric material pieces polarized along the length of the stack and having alternating polarity. The pieces are interspersed with electrodes, bonded together, and electrically connected in parallel. The stack is normally much shorter than a quarter wavelength at the fundamental resonance frequency so that the mechanical behavior of the transducer is not affected by the segmentation. When the transducer bandwidth is less than a half octave, as has conventionally been the case, for example, with lead zirconate titanate (PZT) material, stack segmentation has no significant effect on the mechanical behavior of the device in its normal operating band near the fundamental resonance. However, when a high coupling coefficient material such as lead magnesium niobate-lead titanate (PMN-PT) is used to achieve a wider bandwidth with the tonpilz, the performance difference between a segmented stack and a similar piezoelectric section with electrodes only at the two ends can be significant. This paper investigates the effects of stack segmentation on the performance of wideband underwater tonpilz acoustic transducers. Included is a discussion of a particular tonpilz transducer design using single crystal piezoelectric material with high coupling coefficient compared with a similar design using more traditional PZT ceramics.

  18. Notes on Piezoelectricity

    Energy Technology Data Exchange (ETDEWEB)

    Redondo, Antonio [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-02-03

    These notes provide a pedagogical discussion of the physics of piezoelectricity. The exposition starts with a brief analysis of the classical (continuum) theory of piezoelectric phenomena in solids. The main subject of the notes is, however, a quantum mechanical analysis. We first derive the Frohlich Hamiltonian as part of the description of the electron-phonon interaction. The results of this analysis are then employed to derive the equations of piezoelectricity. A couple of examples with the zinc blende and and wurtzite structures are presented at the end

  19. Time dependence of piezoelectric d33 coefficient of cellular ferroelectret polypropylene film

    Science.gov (United States)

    Wan, Yongping; Xie, Longtao; Zhang, Xiaoqing; Zhong, Zheng

    2011-03-01

    Due to the inherent viscosity of polymer, piezoelectric response in the thickness direction (d33) of cellular ferroelectret films usually depends on the time of measurement. In this letter, the micromechanical theory of viscoelastic composite was extended to predict the time dependence of the overall piezoelectric d33 coefficient of voided charged polymer foam. Experiments were carried out to find the time spectra of piezoelectric d33 coefficient of voided charged polypropylene film. Theoretical simulation agrees well with experiment data.

  20. Electrical properties of (0 0 1)-textured Pb(Zr,Ti)O 3 thin films with different BaPbO 3 thicknesses

    Science.gov (United States)

    Liang, Chun-Sheng; Wu, Jenn-Ming

    2006-05-01

    The microstructure and electrical properties of highly (0 0 1)-textured lead zirconate titanate (PZT) thin films deposited on BaPbO 3 (BPO) at 475 °C by RF-magnetron sputtering were studied. Twenty-three, 65, and 136 nm-thick BPOs were adopted in this study. The dielectric constant is approximately 433 for Pt/PZT/BPO (23 nm), 443 for Pt/PZT/BPO (65 nm), and 466 for Pt/PZT/BPO (136 nm). The remanant polarization values in these three capacitors are 13.5, 14.9, and 10.9 μC/cm 2, and the coercive field values are 76.6, 71.2, and 54.5 kV/cm, respectively. The fatigue endurance of PZT films decreases with the thickness of BPO. The thickness of BPO layer not only influences the crystallinity of PZT films, but also the a-domain populations in PZT films. The variation of resultant electrical properties is attributed partly to the improvement of crystallinity, and partly to the population of a-domain. The effect of the former is remarkable when the BPO is thin while the latter is dominant when the BPO is thick.

  1. Design considerations for piezoelectric polymer ultrasound transducers.

    Science.gov (United States)

    Brown, L F

    2000-01-01

    Much work has been published on the design of ultrasound transducers using piezoelectric ceramics, but a great deal of this work does not apply when using the piezoelectric polymers because of their unique electrical and mechanical properties. The purpose of this paper is to review and present new insight into seven important considerations for the design of active piezoelectric polymer ultrasound transducers: piezoelectric polymer materials selection, transducer construction and packaging requirements, materials characterization and modeling, film thickness and active area design, electroding selection, backing material design, and front protection/matching layer design. Besides reviewing these design considerations, this paper also presents new insight into the design of active piezoelectric polymer ultrasonic transducers. The design and fabrication of an immersible ultrasonic transducer, which has no adhesive layer between the active element and backing layer, is included. The transducer features direct deposition of poly(vinylidene fluoride-trifluoroethylene) [P(VDF-TrFE)] copolymer onto an insulated aluminum backing substrate. Pulse-echo tests indicated a minimum insertion loss of 37 dB and -6 dB bandwidth of 9.8 to 22 MHz (71%). The use of polymer wear-protection/quarter-wave matching layers is also discussed. Test results on a P(VDF-TrFE) transducer showed that a Mylar/sup TM/ front layer provided a slight increase in pulse-echo amplitude of 15% (or 1.2 dB) and an increase in -6 dB pulse-echo fractional bandwidth from 86 to 95%. Theoretical derivations are reported for optimizing the active area of the piezoelectric polymer element for maximum power transfer at resonance. These derivations are extended to the special case for a low profile (i.e., thin) shielded transducer. A method for modeling the non-linear loading effects of a commercial pulser-receiver is also included.

  2. Energy collection via Piezoelectricity

    Science.gov (United States)

    Naveen Kumar, Ch

    2015-12-01

    In the present days, wireless data transmission techniques are commonly used in electronic devices. For powering them connection needs to be made to the power supply through wires else power may be supplied from batteries. Batteries require charging, replacement and other maintenance efforts. So, some alternative methods need to be developed to keep the batteries full time charged and to avoid the need of any consumable external energy source to charge the batteries. Mechanical energy harvesting utilizes piezoelectric components where deformations produced by different means are directly converted to electrical charge via piezoelectric effect. The proposed work in this research recommends Piezoelectricity as a alternate energy source. The motive is to obtain a pollution-free energy source and to utilize and optimize the energy being wasted. Current work also illustrates the working principle of piezoelectric crystal and various sources of vibration for the crystal.

  3. Modeling the power output of piezoelectric energy harvesters

    KAUST Repository

    Al Ahmad, Mahmoud

    2011-04-30

    Design of experiments and multiphysics analyses were used to develop a parametric model for a d 33-based cantilever. The analysis revealed that the most significant parameters influencing the resonant frequency are the supporting layer thickness, piezoelectric layer thickness, and cantilever length. On the other hand, the most important factors affecting the charge output arethe piezoelectric thickness and the interdigitated electrode dimensions. The accuracy of the developed model was confirmed and showed less than 1% estimation error compared with a commercial simulation package. To estimate the power delivered to a load, the electric current output from the piezoelectric generator was calculated. A circuit model was built and used to estimate the power delivered to a load, which compared favorably to experimentally published power data on actual cantilevers of similar dimensions. © 2011 TMS.

  4. Broadband and High Sensitive Time-of-Flight Diffraction Ultrasonic Transducers Based on PMNT/Epoxy 1–3 Piezoelectric Composite

    Directory of Open Access Journals (Sweden)

    Dongxu Liu

    2015-03-01

    Full Text Available 5–6 MHz PMNT/epoxy 1–3 composites were prepared by a modified dice-and-fill method. They exhibit excellent properties for ultrasonic transducer applications, such as ultrahigh thickness electromechanical coupling coefficient kt (85.7%, large piezoelectric coefficient d33 (1209 pC/N, and relatively low acoustic impedance Z (1.82 × 107 kg/(m2·s. Besides, two types of Time-of-Flight Diffraction (TOFD ultrasonic transducers have been designed, fabricated, and characterized, which have different matching layer schemes with the acoustic impedance of 4.8 and 5.7 × 106 kg/(m2·s, respectively. In the detection on a backwall of 12.7 mm polystyrene, the former exhibits higher detectivity, the relative pulse-echo sensitivity and −6 dB relative bandwidth are −21.93 dB and 102.7%, respectively, while the later exhibits broader bandwidth, the relative pulse-echo sensitivity and −6 dB relative bandwidth are −24.08 dB and 117.3%, respectively. These TOFD ultrasonic transducers based on PMNT/epoxy 1–3 composite exhibit considerably improved performance over the commercial PZT/epoxy 1–3 composite TOFD ultrasonic transducer.

  5. Piezoelectric Energy Harvesting Solutions

    Directory of Open Access Journals (Sweden)

    Renato Caliò

    2014-03-01

    Full Text Available This paper reviews the state of the art in piezoelectric energy harvesting. It presents the basics of piezoelectricity and discusses materials choice. The work places emphasis on material operating modes and device configurations, from resonant to non-resonant devices and also to rotational solutions. The reviewed literature is compared based on power density and bandwidth. Lastly, the question of power conversion is addressed by reviewing various circuit solutions.

  6. Piezoelectrically Enhanced Photocathodes

    Science.gov (United States)

    Beach, Robert A.; Nikzad, Shouleh; Bell, Lloyd Douglas; Strittmatter, Robert

    2011-01-01

    Doping of photocathodes with materials that have large piezoelectric coefficients has been proposed as an alternative means of increasing the desired photoemission of electrons. Treating cathode materials to increase emission of electrons is called "activation" in the art. It has been common practice to activate photocathodes by depositing thin layers of suitable metals (usually, cesium). Because cesium is unstable in air, fabrication of cesiated photocathodes and devices that contain them must be performed in sealed tubes under vacuum. It is difficult and costly to perform fabrication processes in enclosed, evacuated spaces. The proposed piezoelectrically enhanced photocathodes would have electron-emission properties similar to those of cesiated photocathodes but would be stable in air, and therefore could be fabricated more easily and at lower cost. Candidate photocathodes include nitrides of elements in column III of the periodic table . especially compounds of the general formula Al(x)Ga(1.x)N (where 0< or = x < or =.1). These compounds have high piezoelectric coefficients and are suitable for obtaining response to ultraviolet light. Fabrication of a photocathode according to the proposal would include inducement of strain in cathode layers during growth of the layers on a substrate. The strain would be induced by exploiting structural mismatches among the various constituent materials of the cathode. Because of the piezoelectric effect in this material, the strain would give rise to strong electric fields that, in turn, would give rise to a high concentration of charge near the surface. Examples of devices in which piezoelectrically enhanced photocathodes could be used include microchannel plates, electron- bombarded charge-coupled devices, image tubes, and night-vision goggles. Piezoelectrically enhanced photocathode materials could also be used in making highly efficient monolithic photodetectors. Highly efficient and stable piezoelectrically enhanced

  7. Complete set of elastic, dielectric, and piezoelectric constants of [011]C poled rhombohedral Pb(In0.5Nb0.5)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3:Mn single crystals.

    Science.gov (United States)

    Huo, Xiaoqing; Zhang, Shujun; Liu, Gang; Zhang, Rui; Luo, Jun; Sahul, Raffi; Cao, Wenwu; Shrout, Thomas R

    2013-02-21

    Mn modified rhombohedral Pb(In0.5Nb0.5)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3 (PIN-PMN-PT:Mn) single crystals poled along [011]C crystallographic direction exhibit a "2R" engineered domain configuration, with macroscopic mm2 symmetry. The complete sets of material constants were determined using combined resonance and ultrasonic methods, and compared to [001]C poled PIN-PMN-PT:Mn crystals. The thickness shear piezoelectric coefficient d15 and electromechanical coupling factor k15 were found to be on the order of ∼3000 pC/N and 0.92, respectively, with longitudinal piezoelectric coefficient d33 and coupling factor k33 being on the order of ∼1050 pC/N and 0.90. Of particular importance is that PIN-PMN-PT:Mn single crystals exhibited high mechanical quality factor Q33 ∼ 1000, comparable to "hard" PZT8 ceramics, which can also be confirmed by the low extrinsic contribution, being ≤2% from the Rayleigh analysis.

  8. Piezoelectric multilayer actuator life test.

    Science.gov (United States)

    Sherrit, Stewart; Bao, Xiaoqi; Jones, Christopher M; Aldrich, Jack B; Blodget, Chad J; Moore, James D; Carson, John W; Goullioud, Renaud

    2011-04-01

    Potential NASA optical missions such as the Space Interferometer Mission require actuators for precision positioning to accuracies of the order of nanometers. Commercially available multilayer piezoelectric stack actuators are being considered for driving these precision mirror positioning mechanisms. These mechanisms have potential mission operational requirements that exceed 5 years for one mission life. To test the feasibility of using these commercial actuators for these applications and to determine their reliability and the redundancy requirements, a life test study was undertaken. The nominal actuator requirements for the most critical actuators on the Space Interferometry Mission (SIM) in terms of number of cycles was estimated from the Modulation Optics Mechanism (MOM) and Pathlength control Optics Mechanism (POM) and these requirements were used to define the study. At a nominal drive frequency of 250 Hz, one mission life is calculated to be 40 billion cycles. In this study, a set of commercial PZT stacks configured in a potential flight actuator configuration (pre-stressed to 18 MPa and bonded in flexures) were tested for up to 100 billion cycles. Each test flexure allowed for two sets of primary and redundant stacks to be mechanically connected in series. The tests were controlled using an automated software control and data acquisition system that set up the test parameters and monitored the waveform of the stack electrical current and voltage. The samples were driven between 0 and 20 V at 2000 Hz to accelerate the life test and mimic the voltage amplitude that is expected to be applied to the stacks during operation. During the life test, 10 primary stacks were driven and 10 redundant stacks, mechanically in series with the driven stacks, were open-circuited. The stroke determined from a strain gauge, the temperature and humidity in the chamber, and the temperature of each individual stack were recorded. Other properties of the stacks, including the

  9. Effect of thickness on the stress and magnetoelectric coupling in bilayered Pb(Zr{sub 0.52}Ti{sub 0.48})O{sub 3}-CoFe{sub 2}O{sub 4} films

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Jing, E-mail: wang-jing@nuaa.edu.cn, E-mail: cwnan@tsinghua.edu.cn [State Key Laboratory of Mechanics and Control of Mechanical Structures, College of Aerospace Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016 (China); Li, Zheng; Wang, Jianjun; Nan, Cewen, E-mail: wang-jing@nuaa.edu.cn, E-mail: cwnan@tsinghua.edu.cn [School of Materials Science and Engineering, State Key Lab of New Ceramics and Fine Processing, Tsinghua University, Beijing 100084 (China); He, Hongcai [State Key Lab of Electronic Thin Films and Integrated Devices, School of Microelectronics and Solid-State Electronics, University of Electronic Science and Technology of China, Chengdu, Sichuan 610054 (China)

    2015-01-28

    Magnetoelectric bilayered Pb(Zr{sub 0.52}Ti{sub 0.48})O{sub 3}-CoFe{sub 2}O{sub 4}(PZT-CFO) films with different PZT thicknesses were grown on (111)Pt/Ti/SiO{sub 2}/Si substrates using chemical solution spin-coating. Structural characterization by X-ray diffraction and electron microscopy shows pure phases and well-defined interfaces between the PZT and CFO films. The CFO-PZT-substrate structure effectively alleviates the substrate clamping effect for the CFO layer, showing appreciable magnetoelectric responses in the composite films. Both the direct magnetoelectric effect and the magnetic field-induced Raman shifts in the A{sub 1}(TO{sub 1}) soft mode of PZT demonstrate the magnetic-mechanical-electric coupling in the films. The results also indicate that with a constant CFO layer thickness, the thickness of the PZT layer plays an important role in the stress relaxation and strong magnetoelectric coupling. The coupling could be further enhanced by increasing the CFO thickness, optimizing the volume (thickness) fraction of the PZT thickness, and releasing the clamping effect from the substrate.

  10. Stretchable piezoelectric nanocomposite generator

    Science.gov (United States)

    Park, Kwi-Il; Jeong, Chang Kyu; Kim, Na Kyung; Lee, Keon Jae

    2016-06-01

    Piezoelectric energy conversion that generate electric energy from ambient mechanical and vibrational movements is promising energy harvesting technology because it can use more accessible energy resources than other renewable natural energy. In particular, flexible and stretchable piezoelectric energy harvesters which can harvest the tiny biomechanical motions inside human body into electricity properly facilitate not only the self-powered energy system for flexible and wearable electronics but also sensitive piezoelectric sensors for motion detectors and in vivo diagnosis kits. Since the piezoelectric ZnO nanowires (NWs)-based energy harvesters (nanogenerators) were proposed in 2006, many researchers have attempted the nanogenerator by using the various fabrication process such as nanowire growth, electrospinning, and transfer techniques with piezoelectric materials including polyvinylidene fluoride (PVDF) polymer and perovskite ceramics. In 2012, the composite-based nanogenerators were developed using simple, low-cost, and scalable methods to overcome the significant issues with previously-reported energy harvester, such as insufficient output performance and size limitation. This review paper provides a brief overview of flexible and stretchable piezoelectric nanocomposite generator for realizing the self-powered energy system with development history, power performance, and applications.

  11. Energy Harvesting via Piezoelectricity

    Directory of Open Access Journals (Sweden)

    Tanvi Dikshit

    2010-01-01

    Full Text Available In the present era, wireless data transmission techniques are commonly used in electronic devices. For powering them connection needs to be made to the power supply through wires else power may be supplied from batteries. Batteries require charging, replacement and other maintenance efforts. For example, in the applications such as villages, border areas, forests, hilly areas, where generally remote controlled devices are used, continuous charging of the microcells is not possible by conventional charging methods .So, some alternative methods needs to be developed to keep the batteries full time charged and to avoid the need of any consumable external energy source to charge the batteries.. To resolve such problems, Energy harvesting technique is proposed as the best alternative. There exists variety of energy harvesting techniques but mechanical energy harvesting happens to be the most prominent. This technique utilizes piezoelectric components where deformations produced by different means are directly converted to electrical charge via piezoelectric effect. Subsequently the electrical energy can be regulated or stored for further use. The proposed work in this research recommends Piezoelectricity as a alternate energy source. The motive is to obtain a pollution-free energy source and to utilize and optimize the energy being wasted. In this paper two important techniques are stressed upon to harness the energy viz Piezoelectric Windmill and Increased Bandwidth Piezoelectric Crystal. Current work also illustrates the working principle of piezoelectric crystal and various sources of vibration for the crystal.

  12. Longitudinal-bending mode micromotor using multilayer piezoelectric actuator.

    Science.gov (United States)

    Yao, K; Koc, B; Uchino, K

    2001-07-01

    Longitudinal-bending mode ultrasonic motors with a diameter of 3 mm were fabricated using stacked multilayer piezoelectric actuators, which were self-developed from hard lead zirconate titanate (PZT) ceramic. A bending vibration was converted from a longitudinal vibration with a longitudinal-bending coupler. The motors could be bidirectionally operated by changing driving frequency. Their starting and braking torque were analyzed based on the transient velocity response. With a load of moment of inertia 2.5 x 10(-7) kgm2, the motor showed a maximum starting torque of 127.5 microNm. The braking torque proved to be a constant independent on the motor's driving conditions and was roughly equivalent to the maximum starting torque achievable with our micromotors.

  13. Compact piezoelectric stacked actuators for high power applications.

    Science.gov (United States)

    Yao, K; Uchino, K; Xu, Y; Dong, S; Lim, L C

    2000-01-01

    Small, hollow, multilayer actuators with a diameter of 3 mm were fabricated by the stacking method from piezoelectric hard lead zirconate titanate (PZT) ceramics. Langevin vibrators were also constructed with the hollow multilayer actuators. The performance capabilities of the actuator and Langevin vibrator samples were examined under high-power conditions. The high-power vibration level at a given sinusoidal drive voltage was significantly enhanced by using a multilayer structure under either a nonresonance or resonance condition. A maximum vibration velocity of 0.17 m/sec was obtained for the 9-layer actuator sample under nonresonance conditions. The vibration velocity was further improved with the Langevin vibrator driven at the resonance frequency. The temperature rise due to heat generation under high-power conditions was the immediate limitation on the maximum accessible vibration velocity for the stacked actuators.

  14. Piezoelectric-nanowire-enabled power source for driving wireless microelectronics.

    Science.gov (United States)

    Xu, Sheng; Hansen, Benjamin J; Wang, Zhong Lin

    2010-10-19

    Harvesting energy from irregular/random mechanical actions in variable and uncontrollable environments is an effective approach for powering wireless mobile electronics to meet a wide range of applications in our daily life. Piezoelectric nanowires are robust and can be stimulated by tiny physical motions/disturbances over a range of frequencies. Here, we demonstrate the first chemical epitaxial growth of PbZr(x)Ti(1-x)O(3) (PZT) nanowire arrays at 230 °C and their application as high-output energy converters. The nanogenerators fabricated using a single array of PZT nanowires produce a peak output voltage of ~0.7 V, current density of 4 μA cm(-2) and an average power density of 2.8 mW cm(-3). The alternating current output of the nanogenerator is rectified, and the harvested energy is stored and later used to light up a commercial laser diode. This work demonstrates the feasibility of using nanogenerators for powering mobile and even personal microelectronics.

  15. Using piezoelectric sensors for ultrasonic pulse velocity measurements in concrete

    Science.gov (United States)

    Kee, Seong-Hoon; Zhu, Jinying

    2013-11-01

    The ultrasonic pulse velocity (UPV) test has been a widely used non-destructive testing method for concrete structures. However, the conventional UPV test has limitations in consistency of results and applicability in hard-to-access regions of structures. The authors explore the feasibility of embedded piezoelectric (PZT) sensors for ultrasonic measurements in concrete structures. Two PZT sensors were embedded in a reinforced concrete specimen. One sensor worked as an actuator driven by an ultrasonic pulse-receiver, and another sensor worked as a receiver. A series of ultrasonic tests were conducted to investigate the performance of the embedded sensors in crack-free concrete and concrete specimens having a surface-breaking crack under various external loadings. Signals measured by the embedded sensors show a broad bandwidth with a centre frequency around 80 kHz, and very good coherence in the frequency range from 30 to 180 kHz. Furthermore, experimental variability in ultrasonic pulse velocity and attenuation is substantially reduced compared to previously reported values from conventional UPV equipment. Findings from this study demonstrate that the embedded sensors have great potential as a low-cost solution for ultrasonic transducers for health monitoring of concrete in structures.

  16. Parameters Identification for a Composite Piezoelectric Actuator Dynamics

    Directory of Open Access Journals (Sweden)

    Mohammad Saadeh

    2015-03-01

    Full Text Available This work presents an approach for identifying the model of a composite piezoelectric (PZT bimorph actuator dynamics, with the objective of creating a robust model that can be used under various operating conditions. This actuator exhibits nonlinear behavior that can be described using backlash and hysteresis. A linear dynamic model with a damping matrix that incorporates the Bouc–Wen hysteresis model and the backlash operators is developed. This work proposes identifying the actuator’s model parameters using the hybrid master-slave genetic algorithm neural network (HGANN. In this algorithm, the neural network exploits the ability of the genetic algorithm to search globally to optimize its structure, weights, biases and transfer functions to perform time series analysis efficiently. A total of nine datasets (cases representing three different voltage amplitudes excited at three different frequencies are used to train and validate the model. Four cases are considered for training the NN architecture, connection weights, bias weights and learning rules. The remaining five cases are used to validate the model, which produced results that closely match the experimental ones. The analysis shows that damping parameters are inversely proportional to the excitation frequency. This indicates that the suggested hysteresis model is too general for the PZT model in this work. It also suggests that backlash appears only when dynamic forces become dominant.

  17. Distributed Sensing and Shape Control of Piezoelectric Bimorph Mirrors

    Energy Technology Data Exchange (ETDEWEB)

    Redmond, James M.; Barney, Patrick S.; Henson, Tammy D.

    1999-07-28

    As part of a collaborative effort between Sandia National Laboratories and the University of Kentucky to develop a deployable mirror for remote sensing applications, research in shape sensing and control algorithms that leverage the distributed nature of electron gun excitation for piezoelectric bimorph mirrors is summarized. A coarse shape sensing technique is developed that uses reflected light rays from the sample surface to provide discrete slope measurements. Estimates of surface profiles are obtained with a cubic spline curve fitting algorithm. Experiments on a PZT bimorph illustrate appropriate deformation trends as a function of excitation voltage. A parallel effort to effect desired shape changes through electron gun excitation is also summarized. A one dimensional model-based algorithm is developed to correct profile errors in bimorph beams. A more useful two dimensional algorithm is also developed that relies on measured voltage-curvature sensitivities to provide corrective excitation profiles for the top and bottom surfaces of bimorph plates. The two algorithms are illustrated using finite element models of PZT bimorph structures subjected to arbitrary disturbances. Corrective excitation profiles that yield desired parabolic forms are computed, and are shown to provide the necessary corrective action.

  18. Postbuckling investigations of piezoelectric microdevices considering damage effects.

    Science.gov (United States)

    Sun, Zhigang; Wang, Xianqiao

    2014-03-11

    Piezoelectric material has been emerging as a popular building block in MEMS devices owing to its unique mechanical and electrical material properties. However, the reliability of MEMS devices under buckling deformation environments remains elusive and needs to be further explored. Based on the Talreja's tensor valued internal state damage variables as well as the Helmhotlz free energy of piezoelectric material, a constitutive model of piezoelectric materials with damage is presented. The Kachanvo damage evolution law under in-plane compressive loads is employed. The model is applied to the specific case of the postbuckling analysis of the piezoelectric plate with damage. Then, adopting von Karman's plate theory, the nonlinear governing equations of the piezoelectric plates with initial geometric deflection including damage effects under in-plane compressive loads are established. By using the finite difference method and the Newmark scheme, the damage evolution for damage accumulation is developed and the finite difference procedure for postbuckling equilibrium path is simultaneously employed. Numerical results show the postbuckling behaviors of initial flat and deflected piezoelectric plates with damage or no damage under different sets of electrical loading conditions. The effects of applied voltage, aspect ratio of plate, thick-span ratio of plate, damage as well as initial geometric deflections on the postbuckling behaviors of the piezoelectric plate are discussed.

  19. Postbuckling Investigations of Piezoelectric Microdevices Considering Damage Effects

    Directory of Open Access Journals (Sweden)

    Zhigang Sun

    2014-03-01

    Full Text Available Piezoelectric material has been emerging as a popular building block in MEMS devices owing to its unique mechanical and electrical material properties. However, the reliability of MEMS devices under buckling deformation environments remains elusive and needs to be further explored. Based on the Talreja’s tensor valued internal state damage variables as well as the Helmhotlz free energy of piezoelectric material, a constitutive model of piezoelectric materials with damage is presented. The Kachanvo damage evolution law under in-plane compressive loads is employed. The model is applied to the specific case of the postbuckling analysis of the piezoelectric plate with damage. Then, adopting von Karman’s plate theory, the nonlinear governing equations of the piezoelectric plates with initial geometric deflection including damage effects under in-plane compressive loads are established. By using the finite difference method and the Newmark scheme, the damage evolution for damage accumulation is developed and the finite difference procedure for postbuckling equilibrium path is simultaneously employed. Numerical results show the postbuckling behaviors of initial flat and deflected piezoelectric plates with damage or no damage under different sets of electrical loading conditions. The effects of applied voltage, aspect ratio of plate, thick-span ratio of plate, damage as well as initial geometric deflections on the postbuckling behaviors of the piezoelectric plate are discussed.

  20. Layerwise Analysis of Thermal Shape Control in Graded Piezoelectric Beams

    Science.gov (United States)

    Lee, Ho-Jun

    2003-01-01

    A layerwise finite element formulation developed for piezoelectric materials is used to investigate the displacement and stress response of a functionally graded piezoelectric bimorph actuator. The formulation is based on the principles of linear thermopiezoelectricity and accounts for the coupled mechanical, electrical, and thermal response of piezoelectric materials. The layerwise laminate theory is implemented into a linear beam element in order to provide a more accurate representation of the transverse and shear effects that are induced by increased inhomogeneities introduced through-the-thickness by using functionally graded materials. The accuracy of the formulation is verified with previously published experimental results for a piezoelectric bimorph actuator. Additional studies are conducted to analyze the impact of electric and thermal loads on the deflections and stresses in a bimorph actuator. Results of the study help demonstrate the capability of the layerwise theory to provide a more complete representation of shear effects that are no longer negligible even in thin piezoelectric beams. In addition, the effects of varying piezoelectric properties through-the-thickness of the beam are shown to provide additional benefits in minimizing the induced deformations and stresses.

  1. Temperature coefficient of piezoelectric constants in Pb(Mg1/3 Nb2/3O3 - PbTiO3 ceramics

    Directory of Open Access Journals (Sweden)

    Manuel Henrique Lente

    2004-06-01

    Full Text Available In this work, the thermal stability of piezoelectric constants of PMN-PT ceramics in the tetragonal and rhombohedral phases were investigated in a wide range of temperatures. The results showed that the tetragonal PMN-PT presented higher thermal stability and, consequently, the temperature coefficients for the piezoelectric constants were approximately zero. This result revealed to be much better than that commonly found for PZT ceramics. Although the rhombohedral PMN-PT presented a slight lower thermal stability, the values found for the coupling factor were significantly higher than the tetragonal composition.

  2. Measurements of Generated Energy/Electrical Quantities from Locomotion Activities Using Piezoelectric Wearable Sensors for Body Motion Energy Harvesting

    Directory of Open Access Journals (Sweden)

    Antonino Proto

    2016-04-01

    Full Text Available In this paper, two different piezoelectric transducers—a ceramic piezoelectric, lead zirconate titanate (PZT, and a polymeric piezoelectric, polyvinylidene fluoride (PVDF—were compared in terms of energy that could be harvested during locomotion activities. The transducers were placed into a tight suit in proximity of the main body joints. Initial testing was performed by placing the transducers on the neck, shoulder, elbow, wrist, hip, knee and ankle; then, five locomotion activities—walking, walking up and down stairs, jogging and running—were chosen for the tests. The values of the power output measured during the five activities were in the range 6 µW–74 µW using both transducers for each joint.

  3. Measurements of Generated Energy/Electrical Quantities from Locomotion Activities Using Piezoelectric Wearable Sensors for Body Motion Energy Harvesting.

    Science.gov (United States)

    Proto, Antonino; Penhaker, Marek; Bibbo, Daniele; Vala, David; Conforto, Silvia; Schmid, Maurizio

    2016-04-12

    In this paper, two different piezoelectric transducers-a ceramic piezoelectric, lead zirconate titanate (PZT), and a polymeric piezoelectric, polyvinylidene fluoride (PVDF)-were compared in terms of energy that could be harvested during locomotion activities. The transducers were placed into a tight suit in proximity of the main body joints. Initial testing was performed by placing the transducers on the neck, shoulder, elbow, wrist, hip, knee and ankle; then, five locomotion activities-walking, walking up and down stairs, jogging and running-were chosen for the tests. The values of the power output measured during the five activities were in the range 6 µW-74 µW using both transducers for each joint.

  4. Simultaneous liquid viscosity and density determination with piezoelectric unimorph cantilevers

    Science.gov (United States)

    Shih, Wan Y.; Li, Xiaoping; Gu, Huiming; Shih, Wei-Heng; Aksay, Ilhan A.

    2001-01-01

    We have examined both experimentally and theoretically a piezoelectric unimorph cantilever as a liquid viscosity-and-density sensor. The fabricated piezoelectric unimorph consisted of a PbOṡZrO2ṡTiO2 (PZT) layer on a thin stainless-steel plate. In addition to a driving electrode, a sensing electrode was placed on top of the PZT layer, permitting the direct measurement of the resonance frequency. The cantilever was tested using water-glycerol solutions of different compositions. In all three of the tested modes, the resonance frequency decreased while the width of the resonance peak increased with increasing glycerol content. To account for the liquid effect, we consider the cantilever as a sphere of radius R oscillating in a liquid. By including the high and low frequency terms in the induced mass and the damping coefficient of the liquid, we show that for a given liquid density and viscosity the oscillating-sphere model predicts a resonance frequency and peak width that closely agree with experiment. Furthermore, the viscosity and the density of a liquid have been determined simultaneously using the experimentally measured resonance frequency and peak width as inputs to the oscillating-sphere model. The calculated liquid viscosity and density closely agreed with the known values, indicating that our cantilever-based sensor is effective in determining viscosity and density, simultaneously. We also show that scaling analysis predicts an increase in the width of the resonance peak with decreasing cantilever size, an observation in agreement with the large peak widths observed for microcantilevers.

  5. Characterization of PZT Capacitor Structures with Various Electrode Materials Processed In-Situ Using AN Automated, Rotating Elemental Target, Ion Beam Deposition System

    Science.gov (United States)

    Gifford, Kenneth Douglas

    Ferroelectric thin film capacitor structures containing lead zirconate titanate (PZT) as the dielectric, with the chemical formula Pb(rm Zr_{x }Ti_{1-x})O_3, were synthesized in-situ with an automated ion beam sputter deposition system. Platinum (Pt), conductive ruthenium oxide (RuO_2), and two types of Pt-RuO_2 hybrid electrodes were used as the electrode materials. The capacitor structures are characterized in terms of microstructure and electrical characteristics. Reduction or elimination of non-ferroelectric phases, that nucleate during PZT processing on Pt/TiO _2/MgO and RuO_2/MgO substrates, is achieved by reducing the thickness of the individually deposited layers and by interposing a buffer layer (~100-200A) of PbTiO _3 (PT) between the bottom electrode and the PZT film. Capacitor structures containing a Pt electrode exhibit poor fatigue resistance, irregardless of the PZT microstructure or the use of a PT buffer layer. From these results, and results from similar capacitors synthesized with sol-gel and laser ablation, PZT-based capacitor structures containing Pt electrodes are considered to be unsuitable for use in memory devices. Using a PT buffer layer, in capacitor structures containing RuO_2 top and bottom electrodes and polycrystalline, highly (101) oriented PZT, reduces or eliminates the nucleation of zirconium-titanium oxide, non-ferroelectric species at the bottom electrode interface during processing. This results in good fatigue resistance up to ~2times10^ {10} switching cycles. DC leakage current density vs. time measurements follow the Curie-von Schweidler law, J(t) ~ t^ {rm -n}. Identification of the high electric field current conduction mechanism is inconclusive. The good fatigue resistance, low dc leakage current, and excellent retention, qualifies the use of these capacitor structures in non-volatile random access (NVRAM) and dynamic random access (DRAM) memory devices. Excellent fatigue resistance (10% loss in remanent polarization up to

  6. Tape Casting of Honeywell PZT Type III Powder.

    Science.gov (United States)

    1984-02-01

    STANDARDS 193 A . . . • . .I-" ’ .7. ’. .. ’. .-7 . • " U) 1 IV. Tape Casting of Honeywell PZT Type III Poder II~ II * I S Gordon 0. Dayton Beth A. Jones...Street Port Hueneme, CA 93043 Arlington, VA 22217 3 ATTN: Materials Division Attn: Code 431 Naval Research Laboratory Naval Electronics Laboratory...Washington, DC 20375 San Diego, CA 92152 ATTN: Codes 6000 1 ATTN: Electron Materials 6300 1 Sciences Division 2627 1 Naval Air Development Center Naval

  7. Performance of magnetoelectric PZT/Ni multiferroic system for energy harvesting application

    Science.gov (United States)

    Gupta, Reema; Tomar, Monika; Kumar, Ashok; Gupta, Vinay

    2017-03-01

    Magnetoelectric (ME) coefficient of Lead Zirconium Titanate (PZT) thin films has been probed for possible energy harvesting applications. Single phase PZT thin films have been deposited on nickel substrate (PZT/Ni) using pulsed laser deposition (PLD) technique. The effect of PLD process parameters on the ME coupling coefficient in the prepared systems has been investigated. The as grown PZT films on Ni substrate were found to be polycrystalline with improved ferroelectric and ferromagnetic properties. The electrical switching behavior of the PZT thin films were verified using capacitance voltage measurements, where well defined butterfly loops were obtained. The ME coupling coefficient was estimated to be in the range of 94.5 V cm‑1 Oe‑1–130.5 V cm‑1 Oe‑1 for PZT/Ni system, which is large enough for harnessing electromagnetic energy for subsequent applications.

  8. Modeling the thermal behavior of PZT patches during the manufacturing process of smart thermoplastic structures

    Science.gov (United States)

    Elsoufi, L.; Khalil, K.; Lachat, R.; Charon, W.

    2007-08-01

    This paper concerns the manufacturing processes of thermoplastic structures including piezoceramic patches (PZT). The objective of the study reported here was to find a trade-off between the manufacturing conditions and the thermal endurance of the PZT patches. We studied the influence of high temperatures on the PZT efficiency during manufacturing. Two processes were considered: injection molding and thermoforming. The studied object consists of a polypropylene plate containing a PZT patch integrated at different positions. On the one hand, we simulated with ANSYS the thermal transient effects to study the PZT cooling according to the time of its exposure to heat for different fabrication cases and with different manufacturing processes. On the other hand, the loss in PZT generated voltage according to the temperature increment was measured by thermo-mechanical experiences using a dynamical-mechanical analysis machine (DMA) connected to an acquisition chain.

  9. TEMPLATE-ASSISTED FABRICATION AND DIELECTROPHORETIC MANIPULATION OF PZT MICROTUBES

    Directory of Open Access Journals (Sweden)

    VLADIMÍR KOVAĽ

    2012-09-01

    Full Text Available Mesoscopic high aspect ratio ferroelectric tube structures of a diverse range of compositions with tailored physical properties can be used as key components in miniaturized flexible electronics, nano- and micro-electro-mechanical systems, nonvolatile FeRAM memories, and tunable photonic applications. They are usually produced through advanced “bottom-up” or “topdown” fabrication techniques. In this study, a template wetting approach is employed for fabrication of Pb(Zr0.52Ti0.48O3 (PZT microtubes. The method is based on repeated infiltration of precursor solution into macroporous silicon (Si templates at a sub-atmospheric pressure. Prior to crystallization at 750°C, free-standing tubes of a 2-μm outer diameter, extending to over 30 μm in length were released from the Si template using a selective isotropic-pulsed XeF2 reactive ion etching. To facilitate rapid electrical characterization and enable future integration process, directed positioning and aligning of the PZT tubes was performed by dielectrophoresis. The electric field-assisted technique involves an alternating electric voltage that is applied through pre-patterned microelectrodes to a colloidal suspension of PZT tubes dispersed in isopropyl alcohol. The most efficient biasing for the assembly of tubes across the electrode gap of 12 μm was a square wave signal of 5 Vrms and 10 Hz. By varying the applied frequency in between 1 and 10 Hz, an enhancement in tube alignment was obtained.

  10. Strong nonlinear harmonic generation in a PZT/Aluminum resonator

    Energy Technology Data Exchange (ETDEWEB)

    Parenthoine, D; Haumesser, L; Meulen, F Vander; Tran-Huu-Hue, L-P, E-mail: parenthoine@univ-tours.f [University Francois Rabelais of Tours, U 930 Imagerie et Cerveau, CNRS 2448, ENIVL, rue de la Chocolaterie, BP 3410, 41034 Blois (France)

    2009-11-01

    In this work, the extentional vibration mode of a coupled PZT/ Aluminum rod resonator is studied experimentally. Geometrical characteristics of the PZT are its 27 mm length and its 4x4 mm{sup 2} cross section area. The excitation voltage consists in sinusoidal bursts in the frequency range (20-80 kHz). Velocity measurements are performed at both ends of this system, using a laser probe. Strong harmonic distortions in the mechanical response (up to -20 dB with respect to the primary wave amplitude) have been observed. The corresponding input levels are far lower than those which are necessary to observe quadratic second harmonic generation in a free PZT resonator. The strong nonlinear effect can be explained as a super-harmonic resonance of the system due to a specific ratio between the eigen frequencies of the two parts of the resonator. Evolution of fundamental and harmonic responses are observed as a function of input levels, highlighting hysteretic behavior.

  11. Importance of composite parameters in enhanced power conversion efficiency of Terfenol-D/PZT magnetoelectric gyrators

    Science.gov (United States)

    Leung, Chung Ming; Zhuang, Xin; Xu, Junran; Li, Jiefang; Srinivasan, G.; Viehland, D.

    2017-03-01

    A gyrator that is capable of current-to-voltage conversion can be realized with a magnetoelectric (ME) composite of ferromagnetic and ferroelectric phases placed in a coil. Here, we report the dependence of the power conversion efficiency (PE) on the relative thickness of the two ferroic phases in a gyrator of Terfenol-D and PZT. Both experimental and theoretical results on PE as a function of composite parameters, such as thickness ratio of the ferroic layers (n), magnetic field bias (HBias) and several gyrator parameters, such as the resistance load (RL), were discussed. By decreasing the thickness ratio of Terfenol-D to composite (n = 0.28) in coil-ME gyrators, a high power efficiency of 73.9% was found at a fundamental resonance frequency of 72.5 kHz under a HBias of 1000 Oe and RL = 2.6 kΩ in experiments. At the same time, the non-linear mechanical loss was reduced by decreasing the value of n which resulted in a flat response over a wide HBias range. This improved power efficiency promises ME gyrators for power transfer devices.

  12. Q-switched erbium-doped fiber ring laser with piezoelectric transducer-based PS-CFBG

    Science.gov (United States)

    Wu, Liangying; Pei, Li; Wang, Jianshuai; Li, Jing; Ning, Tigang; Liu, Shuo

    2016-09-01

    In this letter, a Q-switched erbium-doped fiber ring laser (EDFRL) with piezoelectric transducer (PZT)-based phase shift chirped fiber Bragg grating (PS-CFBG) has been proposed and demonstrated first. As known, the phase shift can be induced and wiped periodically by applying a modulation signal on the PZT. This makes it possible for the PZT-based PS-CFBG to be used in Q-switched EDFRL. To verify the performance of this Q-switched EDFRL system, some theoretical analyses and experiments have been performed. It is found that, when the PZT is modulated by a signal with frequencies of 1 and 2 kHz, pulse widths of the Q-switched pulse train are 19.8 μs and 15.6 μs, respectively. Besides, the corresponding pulse energies are 1.16 μJ (1 kHz) and 1.91 μJ (2 kHz) with a pump power of 90 mW.

  13. Elastic, piezoelectric, and dielectric properties of Ba(Zr0.2Ti0.8)O3-50(Ba0.7Ca0.3)TiO3 Pb-free ceramic at the morphotropic phase boundary

    Science.gov (United States)

    Xue, Dezhen; Zhou, Yumei; Bao, Huixin; Zhou, Chao; Gao, Jinghui; Ren, Xiaobing

    2011-03-01

    There is an urgent demand for high performance Pb-free piezoelectrics to substitute for the current workhorse, the lead zirconate titanate (PZT) family. Recently, a triple point (also tricritical point) type morphotropic phase boundary (MPB) in Pb-free Ba(Zr0.2Ti0.8)O3-x(Ba0.7Ca0.3)TiO3 system has been reported that shows equally as excellent piezoelectricity as soft PZT at room temperature (Liu and Ren6). In the present study, we measured a full set of elastic, piezoelectric, and dielectric properties for the MPB composition, Ba(Zr0.2Ti0.8)O3-50(Ba0.7Ca0.3)TiO3 (BZT-50BCT), by using a resonance method. The resonant method gives piezoelectric properties d33 = 546 pC/N, g33 = 15.3 × 10-3 Vm/N, electromechanical coupling factor k33 = 65%, and the elastic constant s33E = 19.7 × 10-12 m2/N, c33E = 11.3 × 1010 N/m2, which are close to the properties of soft PZT (PZT-5A). Furthermore, the piezoelectric coefficients (k33, d33), the ferroelectric properties (coercive field, remnant polarization), and the elastic constants (s33D, s33E, c33D, c33E) were also determined as a function of temperature ranging from -50 to 60°C. Our results show that the properties are optimal around MPB temperature (room temperature) and decrease with deviations from the MPB temperature. Nevertheless, the piezoelectric coefficient d33 can maintain an appreciable level of 93 pC/N even at -50°C. The high piezoelectric properties can be ascribed to the low polarization anisotropy as well as the elastic softening at MPB.

  14. High Temperature Piezoelectric Drill

    Science.gov (United States)

    Bao, Xiaoqi; Scott, James; Boudreau, Kate; Bar-Cohen, Yoseph; Sherrit, Stewart; Badescu, Mircea; Shrout, Tom; Zhang, Shujun

    2009-01-01

    The current NASA Decadal mission planning effort has identified Venus as a significant scientific target for a surface in-situ sampling/analyzing mission. The Venus environment represents several extremes including high temperature (460 deg C), high pressure (9 MPa), and potentially corrosive (condensed sulfuric acid droplets that adhere to surfaces during entry) environments. This technology challenge requires new rock sampling tools for these extreme conditions. Piezoelectric materials can potentially operate over a wide temperature range. Single crystals, like LiNbO3, have a Curie temperature that is higher than 1000 deg C and the piezoelectric ceramics Bismuth Titanate higher than 600 deg C. A study of the feasibility of producing piezoelectric drills that can operate in the temperature range up to 500 deg C was conducted. The study includes the high temperature properties investigations of engineering materials and piezoelectric ceramics with different formulas and doping. The drilling performances of a prototype Ultrasonic/Sonic Drill/Corer (USDC) using high temperate piezoelectric ceramics and single crystal were tested at temperature up to 500 deg C. The detailed results of our study and a discussion of the future work on performance improvements are presented in this paper.

  15. The jet impact force of laser-induced bubble under the water-film with different thickness

    Science.gov (United States)

    Li, Beibei; Wang, Bingyang; Liu, Xiumei; He, Jie; Lu, Jian

    2015-05-01

    The effect of water-film on the laser-induced bubble was investigated by a piezoelectric ceramic transducer (PZT) sensor. Both of the collapse time and liquid-jet impact force of the bubble under the water-film were obtained, and the experiments were also completed in different laser energy. The collapse time increase with the thickness of the waterfilm, but the liquid-jet impact force decrease. We consider that the collapse time was affected by both of the rigid boundary and surface, and the increasing of the collapse time is the reason the decreasing of the liquid-jet impact force. The velocity of bubble wall is lower with the longer collapse time for the uniform bubbles energy, so the liquid-jet impact force is lower. For the other reasons, more laser energy would be absorbed by the thicker water-film, but the water was also splashed for the thinner water-film. So, for the thinner water-film, the bubble energy is higher, the liquidjet impact force is higher, but the maximal radius is smaller because of the splash process. In the other hand, both of the collapse time and the liquid-jet impact force are increase with the laser energy. These researches are useful for the laser processing under water.

  16. Stability analysis of piezoelectric beams

    NARCIS (Netherlands)

    Voß, T.; Scherpen, J.M.A.

    2011-01-01

    Piezoelectric materials are used in many engineering application. When modeling piezoelectric materials the standard assumption is that the electromagnetic field which is used to actuate the piezoelectric material is quasi static. In this paper we show that although the assumption of a quasi static

  17. High-fidelity simulation of a standing-wave thermoacoustic-piezoelectric engine

    CERN Document Server

    Lin, Jeffrey; Hesselink, Lambertus

    2015-01-01

    We have carried out wall-resolved fully unstructured Navier--Stokes simulations of a complete standing-wave thermoacoustic piezoelectric (TAP) engine model inspired by the experimental work of Smoker et al. (2012). The computational model is axisymmetric and comprises a 51 cm long cylindrical resonator divided into two sections: one of 19.5 mm in diameter, enclosing a thermoacoustic stack where a linear temperature distribution is imposed via isothermal boundary conditions; the other of 71 mm in diameter, capped by a piezoelectric diaphragm modelled via multi-oscillator broadband time-domain impedance boundary conditions (TDIBCs) matching the measured electromechanical impedance of a PZT-5A diaphragm tuned to the thermoacoustically amplified mode (388 Hz) for maximization of acoustic energy extraction. Simulations were first carried out without energy extraction from quiescent conditions to a limit cycle, for hot-to-cold temperature differences in the range $\\Delta T = 340 - 490\\textrm{ K}$, achieving acousti...

  18. Piezoelectric wave motor

    Science.gov (United States)

    Yerganian, Simon Scott

    2001-07-17

    A piezoelectric motor having a stator in which piezoelectric elements are contained in slots formed in the stator transverse to the desired wave motion. When an electric field is imposed on the elements, deformation of the elements imposes a force perpendicular to the sides of the slot, deforming the stator. Appropriate frequency and phase shifting of the electric field will produce a wave in the stator and motion in a rotor. In a preferred aspect, the piezoelectric elements are configured so that deformation of the elements in direction of an imposed electric field, generally referred to as the d.sub.33 direction, is utilized to produce wave motion in the stator. In a further aspect, the elements are compressed into the slots so as to minimize tensile stresses on the elements in use.

  19. Lead-Free Piezoelectrics

    CERN Document Server

    Nahm, Sahn

    2012-01-01

    Ecological restrictions in many parts of the world are demanding the elimination of Pb from all consumer items. At this moment in the piezoelectric ceramics industry, there is no issue of more importance than the transition to lead-free materials. The goal of Lead-Free Piezoelectrics is to provide a comprehensive overview of the fundamentals and developments in the field of lead-free materials and products to leading researchers in the world. The text presents chapters on demonstrated applications of the lead-free materials, which will allow readers to conceptualize the present possibilities and will be useful for both students and professionals conducting research on ferroelectrics, piezoelectrics, smart materials, lead-free materials, and a variety of applications including sensors, actuators, ultrasonic transducers and energy harvesters.

  20. Effect of Pb content and solution concentration of Pb{sub x}TiO{sub 3} seed layer on (100)-texture and ferroelectric/dielectric behavior of PZT (52/48) thin films

    Energy Technology Data Exchange (ETDEWEB)

    Zhong, Jian; Batra, Vaishali; Han, Hui; Kotru, Sushma, E-mail: skotru@eng.ua.edu [Department of Electrical and Computer Engineering, The University of Alabama, Tuscaloosa, Alabama 35487 (United States); Pandey, Raghvendar K. [Ingram School of Engineering, Texas State University, San Marcos, Texas 78666 (United States)

    2015-09-15

    The effect of Pb content and solution concentration of lead titanate (Pb{sub x}TiO{sub 3}) seed layer on the texture and electric properties of Pb{sub 1.1}(Zr{sub 0.52},Ti{sub 0.48})O{sub 3} (PZT) thin films was investigated. A variety of seed layers (y Pb{sub x}TiO{sub 3}) with varying solution concentration (y = 0.02, 0.05, 0.1, and 0.2 M) and Pb content (x = 1.0, 1.05, 1.1, and 1.2) was deposited on Pt/TiO{sub 2}/SiO{sub 2}/Si substrates using chemical-solution deposition method. PZT films were then deposited on these seed layers using the same process. X-ray diffraction (XRD) and X-ray photoelectron spectroscopy investigations of the seed layers confirm change in crystal structure with variation in the solution properties. XRD studies of PZT films deposited on seed layers demonstrate that the seed layer helps in enhancing (100)-texture and suppressing (111)-texture. It was observed that PZT films prepared on seed layers with lower solution concentrations results in highly (100)-textured films, which further helps to improve the electric properties. The polarization and dielectric constant of the PZT films were seen to increase while the coercive field decreased with increase in (100)-texture. Irrespective of the seed layer solution concentration, higher Pb content in the seed layer deteriorates the PZT film properties. Ninety-five percent to ninety-six percent (100)-texture was obtained from thin PZT films deposited on seed layers of 0.02 M solution concentration with 1.05 and 1.10 Pb contents, which is higher than the values reported for thick PZT films. Optimization of both Pb content and solution concentration of the seed layer is a promising route to achieve highly (100)-textured PZT films with improved electric properties.