WorldWideScience

Sample records for pc-controlled radiochemistry systems

  1. Radiochemistry

    International Nuclear Information System (INIS)

    Urch, D.S.

    1990-01-01

    This chapter is concerned with recent advanced in radiochemistry. The new book, 'Radiochemistry', is reviewed. The impact of nuclear fission and fusion on chemistry is discussed. The production of isotopes and the importance of labelled compounds to nuclear medicine is emphasised. A section on the chemical effects of nuclear transformations is included. The final section discusses the impact of radioactive substances on the environment and the need to train more radiochemists in view of their declining numbers is stressed. (UK)

  2. Radiochemistry

    International Nuclear Information System (INIS)

    Keller, C.

    1988-01-01

    The author presents a survey of radiochemistry, addressing theoretical aspects, such as properties of man-made elements and decay laws, and practical aspects, including nuclear reactor chemistry, and measurement of radiation. This book provides background in the theory of nuclear and radiochemistry, and describes production of radio-elements, nuclear reactor design, and use of radio-nuclides in industry and research. It incorporates recent advances in nuclear physics, such as identification of quarks and their properties, and the discovery of proton emission

  3. Radiochemistry

    International Nuclear Information System (INIS)

    Urch, D.S.

    1988-01-01

    Annual Reports will review the following topics: techniques for the preparation of specific isotopes; the reactions initiated by atoms and ions produced by nuclear reactions, including nuclear decay but omitting radiation chemistry; methods for the preparation of labelled molecules; environmental aspects of radiochemistry; and finally some miscellaneous items. The general chemistry of those elements that happen to be radioactive or those reactions that happen to involve radioactive isotopes will not be considered here. (author)

  4. Radiochemistry

    International Nuclear Information System (INIS)

    Urch, D.S.

    1983-01-01

    Radiochemical techniques and procedures are used in most branches of chemistry; a review of recent progress in radiochemistry must therefore be selective if it is not to cover too wide an area and to repeat consideration of topics covered on other sections of Annual Reports. The topics that will form the main sections of this review are those where radioactivity would seem to be of prime importance, (i) the production of specific radioactive isotopes, (ii) the synthesis of labelled molecules and (iii) chemical reactions initiated by nuclear transformations (but excluding radiation chemistry). The safety aspects of radiochemistry will also be considered. But the inorganic chemistry, as opposed to the radiochemistry, of the heavy radioactive elements is more conveniently considered elsewhere in this Report. Perhaps, however, some recent reviews should be noted, on the chemistry of polonium and of radon, and the appearance of four Gmelin supplements for uranium (solvent extraction, compounds with Group V elements and germanium, ion exchange and chromatography, and the analytical chemistry of uranium), and two general articles on the transuranium elements. Other reviews of transuranium chemistry have considered lower and higher oxidation states, the solution chemistry of the actinides, and the production and chemistry of the trans-plutonium elements. (author)

  5. Study on the subject system of environmental radiochemistry

    International Nuclear Information System (INIS)

    Qiang Yi zhong

    1992-11-01

    The environmental radiochemistry is a new frontier discipline. So, it is very important to study the system of this subject. A brief introduction of its development background and history are presented. The definition of the environmental radiochemistry has been studied. Main contents containing in the subject have been classified and reviewed in accordance with different modalities. Five major features of the environmental radiochemistry are suggested. Issues to be considered recently in the environmental radiochemistry are also discussed

  6. Radiochemistry

    International Nuclear Information System (INIS)

    Urch, D.S.

    1991-01-01

    This section of Annual Reports will review recent developments in those branches of chemistry where nuclear transformations are of importance, but will exclude a consideration of the general chemical properties of elements that happen to be radioactive or of radiation chemistry. Much of the review will, be devoted to progress in the preparation of molecules of increasing complexity, labelled with short-lived positron emitting isotopes. A book, New Trends in Radiopharmaceutical Synthesis, Quality Assurance and Regulatory Control has appeared. Trends in the teaching of radiochemistry were considered at a recent meeting of the American Chemical Society. Concern was voiced about the current status of radio- and nuclear-chemistry education. There will be an increasing need for trained radiochemists and it is necessary to ensure that the topic is introduced into the school science curriculum. Failure in the hunt for the elusive 'super-heavy' elements is discussed in 'Elements beyond Uranium'. (author)

  7. An automatic injection system for rapid radiochemistry

    International Nuclear Information System (INIS)

    Nurmia, M.J.; Kreek, S.A.; Kadkhodayan, B.; Gregorich, K.E.; Lee, D.M.; Hoffman, D.C.

    1992-01-01

    A description is given of the Automated Injection System (AIS), a pneumatically actuated device for automated collection of nuclear reaction products from a He/KCl gas jet transport system. The AIS is used with the Automated Chemical Chromatographic Element Separation System; together these two devices facilitate completely automated separation procedures with improved speed and reproducibility

  8. Radiochemistry Project

    International Nuclear Information System (INIS)

    Anon.

    Researches carried out in the 'Radiochemistry Project' of the Agricultural Nuclear Energy Center, Piracicaba, Sao Paulo State, Brazil, are described. Such researches comprise: dosimetry and radiological protection; development of techniques and methods of chemical analysis and radiochemistry. (M.A.) [pt

  9. Radiochemistry days

    International Nuclear Information System (INIS)

    1998-09-01

    This document provides the 44 papers (transparencies used during the presentations and posters) presented at the Radiochemistry Days, held September 3-4, 1998 in Nantes, France. The main studied topics were problematic questions concerning the nuclear fuel cycle and in particular the management, storage of radioactive wastes and the environmental impact. (O.M.)

  10. A Decade of Experience in Implementing Quality Management System at Radiochemistry and Environmental Laboratory (RAS)

    International Nuclear Information System (INIS)

    Norfaizal Mohamed; Nita Salina Abu Bakar; Zal U'yun Wan Mahmood; Wo, Y.M.; Abdul Kadir Ishak; Nurrul Assyikeen Md Jaffary; Noor Fadzilah Yusof

    2016-01-01

    Quality management system has been introduced to a few laboratories in the Malaysian Nuclear Agency (Nuclear Malaysia) for the purpose to enhance the delivery of quality services to customers. Radiochemistry and Environmental Laboratory (RAS) is a service center in Nuclear Malaysia has implemented a quality management system in procedures carried out and has obtained accreditation for MS ISO/ IEC 17025 since 8 December 2005. This paper is intended to share experiences RAS in implementing a quality management system in accordance with standard MS ISO/ IEC 17025 accreditation and managed to keep it to this day. In addition, the RAS achievements including issues and challenges in implementing the quality management system in the past 10 years will also be discussed. (author)

  11. Advances in intense beams, beam delivery, targetry, and radiochemistry at advanced cyclotron systems

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, R.R. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada)]. E-mail: djohnson@advancedcyclotron.com; Watt, R. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); Kovac, B. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); Zyuzin, A. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); Van Lier, E. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); Erdman, K.L. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); Gyles, Wm. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); Sabaiduc, V. [Advanced Cyclotron Systems Inc., 7851 Alderbridge Way, Richmond, BC, V6X 2A4 (Canada); McQuarrie, S.A. [Faculty of Medicine and Dentistry, University of Alberta, Edmonton, AB, T6G 1Z2 (Canada); Wilson, J. [Faculty of Medicine and Dentistry, University of Alberta, Edmonton, AB, T6G 1Z2 (Canada); Backhouse, C. [Department of Electrical Engineering, University of Alberta, Edmonton, AB (Canada); Gelbart, Wm. [Advanced System Design, C22, S6, RR1, Garden Bay, BC, V0N 1S0 (Canada); Kuo, T. [4654 N. Larwin Ave., Concorde, CA 94521 United States (United States)

    2007-08-15

    The increasing demand for radionuclides for PET and SPECT has resulted in ACSI system improvements starting from the cyclotron and proceeding to the Radiochemistry Modules. With more TR30 cyclotrons installed and operating at full capacity, emphasis has been placed on improving the operational components to reduce both the incidence of failure and subsequent maintenance time. A cyclotron system has been developed that meets the needs of a regional radiopharmacy that supplies both positron and single photon emitters that would not otherwise be available. This new system has been named the TR24. In order to deal with some of the challenges of high currents, a method has been developed for passivating the entrance window foil during high current irradiation of a water target used to produce F-18. A method has been developed for passivating the entrance window foil to reduce unwanted chemical species that interfere with radiopharmaceutical production. Preliminary results for novel radioiodine production technique using the TR19/9 are also discussed.

  12. Advances in intense beams, beam delivery, targetry, and radiochemistry at advanced cyclotron systems

    Science.gov (United States)

    Johnson, R. R.; Watt, R.; Kovac, B.; Zyuzin, A.; Van Lier, E.; Erdman, K. L.; Gyles, Wm.; Sabaiduc, V.; McQuarrie, S. A.; Wilson, J.; Backhouse, C.; Gelbart, Wm.; Kuo, T.

    2007-08-01

    The increasing demand for radionuclides for PET and SPECT has resulted in ACSI system improvements starting from the cyclotron and proceeding to the Radiochemistry Modules. With more TR30 cyclotrons installed and operating at full capacity, emphasis has been placed on improving the operational components to reduce both the incidence of failure and subsequent maintenance time. A cyclotron system has been developed that meets the needs of a regional radiopharmacy that supplies both positron and single photon emitters that would not otherwise be available. This new system has been named the TR24. In order to deal with some of the challenges of high currents, a method has been developed for passivating the entrance window foil during high current irradiation of a water target used to produce F-18. A method has been developed for passivating the entrance window foil to reduce unwanted chemical species that interfere with radiopharmaceutical production. Preliminary results for novel radioiodine production technique using the TR19/9 are also discussed.

  13. Advances in intense beams, beam delivery, targetry, and radiochemistry at advanced cyclotron systems

    International Nuclear Information System (INIS)

    Johnson, R.R.; Watt, R.; Kovac, B.; Zyuzin, A.; Van Lier, E.; Erdman, K.L.; Gyles, Wm.; Sabaiduc, V.; McQuarrie, S.A.; Wilson, J.; Backhouse, C.; Gelbart, Wm.; Kuo, T.

    2007-01-01

    The increasing demand for radionuclides for PET and SPECT has resulted in ACSI system improvements starting from the cyclotron and proceeding to the Radiochemistry Modules. With more TR30 cyclotrons installed and operating at full capacity, emphasis has been placed on improving the operational components to reduce both the incidence of failure and subsequent maintenance time. A cyclotron system has been developed that meets the needs of a regional radiopharmacy that supplies both positron and single photon emitters that would not otherwise be available. This new system has been named the TR24. In order to deal with some of the challenges of high currents, a method has been developed for passivating the entrance window foil during high current irradiation of a water target used to produce F-18. A method has been developed for passivating the entrance window foil to reduce unwanted chemical species that interfere with radiopharmaceutical production. Preliminary results for novel radioiodine production technique using the TR19/9 are also discussed

  14. Chemistry and radiochemistry strategies supported by FA3-EPRTM and UK-EPRTM auxiliary systems: performances and control

    International Nuclear Information System (INIS)

    Tigeras, Arancha; Fourment, Pierre; Elgallaf; Anas; Chupin, Antoine; Fauvel, Nicola

    2012-09-01

    The design and the operation of auxiliary systems play an essential role in: - the preservation of the primary circuit integrity, - the prevention of hydrogen risk, - the control of the boron concentration and radioactivity, - the application of pH and zinc programmes. While the source term generation mainly depends on the primary circuit material and primary coolant chemistry conditioning, the source term spreading is directly linked to the auxiliary systems treatment and performances. Indeed, the auxiliary systems regulate the boron, hydrogen, lithium and zinc injection as well as the countermeasures to ensure the reactivity control and the hazardous H 2 /O 2 mixture prevention. The main principles governing the chemistry and radiochemistry in the auxiliary systems are based on the application of: - Design features for hydrogen and boron management. - Criteria for selecting the appropriate material of each system considering the functional requirements and the source term build up reduction. - Measures for minimizing the activity deposition on the surfaces of components and pipings. - Adequate and reliable systems of purification for reducing the accumulation of liquid/gas radioactivity and impurities in the circuits and for optimizing the waste production. - Chemistry program for limiting the material corrosion of auxiliary systems and preventing the source term transfer to the core. - Appropriate sampling locations and equipment to monitor the chemistry and radiochemistry parameters. This paper describes the operation of the main auxiliary systems of FLAMANVILLE3-EPR TM and UK-EPR- TM participating in the chemistry/radiochemistry management such as Chemical and Volume Control System (CVCS), Reactor Borated Water Make-up System (RBWMS), Coolant Treatment System (CTS), Gaseous Waste Processing System (GWPS), Fuel Pool Purification System (PTR [FPPS/FPCS]) also. The performances requested to these systems and the chemistry programs applied to them are discussed

  15. Study on the Effects of Sample Density on Gamma Spectrometry System Measurement Efficiency at Radiochemistry and Environment Laboratory

    International Nuclear Information System (INIS)

    Wo, Y.M.; Dainee Nor Fardzila Ahmad Tugi; Khairul Nizam Razali

    2015-01-01

    The effects of sample density on the measurement efficiency of the gamma spectrometry system were studied by using four sets multi nuclide standard sources of various densities between 0.3 - 1.4 g/ ml. The study was conducted on seven unit 25 % coaxial HPGe detector gamma spectrometry systems in Radiochemistry and Environment Laboratory (RAS). Difference on efficiency against gamma emitting radionuclides energy and measurement systems were compared and discussed. Correction factor for self absorption caused by difference in sample matrix density of the gamma systems were estimated. The correction factors are to be used in quantification of radionuclides concentration in various densities of service and research samples in RAS. (author)

  16. Radiochemistry division. Chapter 2

    International Nuclear Information System (INIS)

    Anon.

    In radiochemistry, the experiments made in 1976 were in the following fields: in nuclear chemistry, the study of heavy-ion reaction mechanisms of fusion and fission, quasi-elastic transfer reactions; in radiochemistry the study of the physico-chemical properties of the actinides and transuranium elements and the search for natural superheavy elements [fr

  17. Nuclear and radiochemistry

    CERN Document Server

    Konya, Jozsef

    2012-01-01

    The field of nuclear and radiochemistry is wide-reaching, with results having functions and use across a variety of disciplines. Drawing on 40 years of experience in teaching and research, this concise book explains the basic principles and applications of the primary areas of nuclear and radiochemistry. Separate chapters cover each main area of recent radiochemistry. This includes nuclear medicine and chemical aspects of nuclear power plants, namely the problems of nuclear wastes and nuclear analysis (both bulk and surface analysis), with the analytical methods based on the interactions of

  18. Radiochemistry of uranium

    Energy Technology Data Exchange (ETDEWEB)

    Gindler, J.E.

    1962-03-01

    This volume which deals with the radiochemistry of uranium is one of a series of monographs on radiochemistry of the elements. There is included a review of the nuclear and chemical features of particular interest to the radiochemist, a discussion of problems of dissolution of a sample and counting technique, and finally, a collection of radiochemical procedures for the element as found in the literature.

  19. Radiochemistry and actinide chemistry

    International Nuclear Information System (INIS)

    Guillaumont, R.; Peneloux, A.

    1989-01-01

    The analysis of trace amounts of actinide elements by means of radiochemistry, is discussed. The similarities between radiochemistry and actinide chemistry, in the case of species amount by cubic cm below 10 12 , are explained. The parameters which allow to define what are the observable chemical reactions, are given. The classification of radionuclides in micro or macrocomponents is considered. The validity of the mass action law and the partition function in the definition of the average number of species for trace amounts, is investigated. Examples illustrating the results are given

  20. Prospects in radiochemistry

    International Nuclear Information System (INIS)

    Guillaumont, R.

    1988-01-01

    This paper draws the basic research direction concerning activities with or on radionuclides related only to chemistry that is to say taking into account degrees of oxidation or valence. Chemical behaviour of very diluted element or even of one atom only, present trends and importance of radiochemistry in the fuel cycle are reviewed [fr

  1. Radiochemistry days; Journees radiochimie

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1998-09-01

    This document provides the 44 papers (transparencies used during the presentations and posters) presented at the Radiochemistry Days, held September 3-4, 1998 in Nantes, France. The main studied topics were problematic questions concerning the nuclear fuel cycle and in particular the management, storage of radioactive wastes and the environmental impact. (O.M.)

  2. Comprehensive nuclear counting and detector characterisation system for the radiochemistry laboratory

    International Nuclear Information System (INIS)

    Parthasarathy, R.; Saisubalakshmi, D.; Mishra, G.K.; Srinivas, K.C.; Venkatasubramani, C.R.

    2004-01-01

    The paper describes a comprehensive nuclear pulse counting system that can cater to up to seven nuclear detector set-ups located in different places in the laboratory. Each detector set up has an interfacing module that conditions the amplifier pulses and transmits them to a common counting system. The microcontroller-based system receives these pulses through a multiplexer and counts the pulses for a user specified preset time. The system has a routine to determine detector plateau characteristics and fix the detector operating voltage. In this mode, the system collects the EHT-versus- counts data in a EHT programmed sequence and plots the profile. The system conducts the counting routine for a stipulated number of times and does all necessary statistical tests to ensure the proper functioning of the detector under test. The system also includes a test routine that checks the performance of the counting system by connecting it to a local pulse generator. The microcontroller based system interacts with a PC through RS232 communication for user interaction and reporting. (author)

  3. Radiochemistry as a (rho)R Diagnostic with the RAGS Gas Collection System

    International Nuclear Information System (INIS)

    Nelson, S.L.; Shaughnessy, D.A.; Schneider, D.H.; Stoeffl, W.; Moody, K.J.; Cerjan, C.; Stoyer, M.A.; Bernstein, L.A.; Bleuel, D.L.; Hoffman, R.

    2010-01-01

    Radiochemical diagnostic techniques such as gas-phase capsule debris analysis may prove to be successful methods for establishing the success or failure of ignition experiments at the National Ignition Facility (NIF). Samples in the gas phase offer the most direct method of collection by simply pumping out the large target chamber following a NIF shot. The target capsules will be prepared with dopants which will produce radioactive noble gas isotopes upon activation with neutrons. We have designed and constructed the Radchem Apparatus for Gas Sampling (RAGS) in order to collect post-shot gaseous samples for NIF capsule diagnostics. The design of RAGS incorporates multiple stages intended to purify, transfer, and count the radioactive decays from gaseous products synthesized in NIF experiments. At the moment the dopant of choice is 124 Xe, which will undergo (n,γ) and (n, 2n) reactions to produce 125 Xe and 123 Xe. The half-lives of each are on the order of multiple hours and are suitable for long-term gamma-counting. These isotopes and the rest of the gases evolved in a NIF shot will be drawn through the NIF turbo pumps, past the temporarily shuttered cryo pumps (to aid our collection efficiency), and towards the first main portion of the RAGS system: the pre-cleaner. The pre-cleaner will consist of a water removal system, a series of heated getter cartridges to remove most other impurities such as N 2 , O 2 , CO 2 , etc., and a residual gas analyzer (RGA) to monitor vacuum quality. The noble gases will flow through the precleaner and into the second stage of the system: the cryo collector. This cryo collector consists of a main cryo head for noble gas collection which will operate for approximately five minutes post-shot. Afterwards a valve will close and isolate the pre-cleaner, while the cryo head warms to release the Xe gas to one of two locations - either a second cryo station for in-situ gamma counting, or to a small cooled gas bottle for removal and

  4. XVIII Mendeleev congress on general and applied chemistry. Summaries of reports in five volumes. Volume 5. IV Russian-French symposium Supramolecular systems in chemistry and biology. II Russian-Indian symposium on organic chemistry. International symposium on present-day radiochemistry Radiochemistry: progress and prospects. International symposium Green chemistry, stable evolution and social responsibility of chemists. Symposium Nucleophilic hydrogen substitution in aromatic systems and related reactions

    International Nuclear Information System (INIS)

    2007-01-01

    The 5 volume of the XVIII Mendeleev congress on general and applied chemistry includes summaries of reports on the subjects of sypramolecular systems in chemistry and biology, organic chemistry, modern radiochemistry, green chemistry - development and social responsibility of chemists, nucleophilic hydrogen substitution in aromatic systems and related chemical reactions [ru

  5. Experiments in radiochemistry

    International Nuclear Information System (INIS)

    Schwankner, R.

    1980-11-01

    Twelve experiments in radiochemistry, nuclear chemistry, radiation detection and radiation measurement are presented which have been tested in teaching practice. Criteria of selection were minimum apparative expenditure, preparation time, radiation exposure, and danger of incorporation or contamination. The experiments will teach students how to handle unsealed radioactive materials within a fraction of a permissible values and thus train them in radiochemical techniques of working. Theoretical, historical and topical aspects are mentioned in order to give the students some background. A detailed bibliography of relevant publications is given. (orig./HP) [de

  6. Radiochemistry and nuclear chemistry

    CERN Document Server

    Choppin, Gregory; RYDBERG, JAN; Ekberg, Christian

    2013-01-01

    Radiochemistry or nuclear chemistry is the study of radiation from an atomic and molecular perspective, including elemental transformation and reaction effects, as well as physical, health and medical properties. This revised edition of one of the earliest and best-known books on the subject has been updated to bring into teaching the latest developments in research and the current hot topics in the field. To further enhance the functionality of this text, the authors have added numerous teaching aids, examples in MathCAD with variable quantities and options, hotlinks to relevant text secti

  7. Microfluidic technology for PET radiochemistry

    International Nuclear Information System (INIS)

    Gillies, J.M.; Prenant, C.; Chimon, G.N.; Smethurst, G.J.; Dekker, B.A.; Zweit, J.

    2006-01-01

    This paper describes the first application of a microfabricated reaction system to positron emission tomography (PET) radiochemistry. We have applied microfluidic technology to synthesise PET radiopharmaceuticals using 18 F and 124 I as labels for fluorodeoxyglucose (FDG) and Annexin-V, respectively. These reactions involved established methods of nucleophilic substitution on a mannose triflate precursor and direct iodination of the protein using iodogen as an oxidant. This has demonstrated a proof of principle of using microfluidic technology to radiochemical reactions involving low and high molecular weight compounds. Using microfluidic reactions, [ 18 F]FDG was synthesised with a 50% incorporation of the available F-18 radioactivity in a very short time of 4 s. The radiolabelling efficiency of 124 I Annexin-V was 40% after 1 min reaction time. Chromatographic analysis showed that such reaction yields are comparable to conventional methods, but in a much shorter time. The yields can be further improved with more optimisation of the microfluidic device itself and its fluid mixing profiles. This demonstrates the potential for this technology to have an impact on rapid and simpler radiopharmaceutical synthesis using short and medium half-life radionuclides

  8. The operational benefits of integrated PC control of gamma irradiation plants

    International Nuclear Information System (INIS)

    Comben, M.; Stephens, P.

    1998-01-01

    Compared with the traditional PLC control systems used on many gamma irradiation plants, the semi-intelligent decision making capabilities of a fully integrated PC control system can bring many benefits to the plant operator. The authors will describe how plant operation is fully automatic with the PC control providing all the input-output data required to run the plant efficiently and safely. Detailed product tracking, with live on-screen data, can be incorporated to give both plant operator and product manufacturer complete confidence in the irradiation process. Advanced features such as on-line diagnostics and mechanical part failure prediction are also described. Also available is automated dosimetry, reducing the opportunity for human error, whilst at the same time saving on staff costs and providing highly professional dose validation reports and comprehensive routine dosimetry documentation. The benefits of PURIDEC's PC control system are not only available with its new plants. The system can be supplied as an upgrade to plants of all ages and design giving the current operator all the benefits described in the paper

  9. Radiochemistry in the world: a biblio-metric study (1989-1998)

    International Nuclear Information System (INIS)

    Guillaumont, R.; Madic, Ch.; Pichot, Ch.; Rousseau-Hans, F.

    2002-01-01

    The study analyzes the world literature in the field of radiochemistry. It tries to represent the radiochemistry, through the development of its sub-fields in the different parts of the world and through the international collaboration patterns. Most data come from the INIS (International Nuclear Information System) database operated by the International Atomic Energy Agency (IAEA) and cover the 1989-1998 era. Less rich countries publish proportionally more in fundamental radiochemistry whereas high developed countries invest more in nuclear medicine. Another aspect of the radiochemistry is approached with the study of scientific national and international journals which publish articles in this field. English remains the most important language used in the fundamental fields of radiochemistry while national languages, such as russian, japanese and chinese, keep a certain importance in applied sciences like earth sciences, waste management and nuclear medicine. (author)

  10. Annual report 2011. Institute of Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Bernhard, G [ed.

    2011-07-01

    The Institute of Radiochemistry (IRC) IS one of the seven institutes of the Helmholtz- Zentrum Dresden-Rossendorf (HZDR). The research activities are fully integrated into the ''Nuclear Safety Research Program'' of the Helmholtz Association and focused on the topic ''Safety of Nuclear Waste Disposal''. The research objectives are to generate better process understanding and data for the long-term safety analysis of a nuclear waste disposal in the deep geological underground. A better knowledge about the dominating processes essential for radionuclide (actinide) mobilization and immobilization on the molecular level is needed for the assessment of the macroscopic processes which determine the transport and distribution of radioactivity in the environment. Special emphasis is put on the biological mediated transport of long-lived radionuclides in the geosphere and their interaction with different biosystems like biota and human organism for a better calculation of environmental and health risks. Advanced knowledge is needed for description of the processes dominating at the interfaces between geo- and bio-systems related to the distribution of long-lived radionuclides in various bio-systems along the food chain. More than 120 scientists, technicians, and students, working on their Ph.D., diploma, master, or bachelor thesis, were employed at the Institute of Radiochemistry in 2011. About 20 Ph.D. students are working at the institute. Promotion of young scientists is an important requirement to ensure the competence and further excellent scientific results in the discipline of radiochemistry in future times. We accomplished many new scientific results in the past year, which are presented in this Annual Report, and about 50 original papers were published in peer-reviewed international scientific journals. In 2011, the future research profile of the HZDR was under discussion with the aim to focus the research fields and programs. One result of this process was the

  11. Annual report 2011. Institute of Radiochemistry

    International Nuclear Information System (INIS)

    Bernhard, G.

    2011-01-01

    The Institute of Radiochemistry (IRC) IS one of the seven institutes of the Helmholtz- Zentrum Dresden-Rossendorf (HZDR). The research activities are fully integrated into the ''Nuclear Safety Research Program'' of the Helmholtz Association and focused on the topic ''Safety of Nuclear Waste Disposal''. The research objectives are to generate better process understanding and data for the long-term safety analysis of a nuclear waste disposal in the deep geological underground. A better knowledge about the dominating processes essential for radionuclide (actinide) mobilization and immobilization on the molecular level is needed for the assessment of the macroscopic processes which determine the transport and distribution of radioactivity in the environment. Special emphasis is put on the biological mediated transport of long-lived radionuclides in the geosphere and their interaction with different biosystems like biota and human organism for a better calculation of environmental and health risks. Advanced knowledge is needed for description of the processes dominating at the interfaces between geo- and bio-systems related to the distribution of long-lived radionuclides in various bio-systems along the food chain. More than 120 scientists, technicians, and students, working on their Ph.D., diploma, master, or bachelor thesis, were employed at the Institute of Radiochemistry in 2011. About 20 Ph.D. students are working at the institute. Promotion of young scientists is an important requirement to ensure the competence and further excellent scientific results in the discipline of radiochemistry in future times. We accomplished many new scientific results in the past year, which are presented in this Annual Report, and about 50 original papers were published in peer-reviewed international scientific journals. In 2011, the future research profile of the HZDR was under discussion with the aim to focus the research fields and programs. One result of this process was the

  12. Annual report 2011. Institute of Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Bernhard, G. (ed.)

    2011-07-01

    The Institute of Radiochemistry (IRC) IS one of the seven institutes of the Helmholtz- Zentrum Dresden-Rossendorf (HZDR). The research activities are fully integrated into the ''Nuclear Safety Research Program'' of the Helmholtz Association and focused on the topic ''Safety of Nuclear Waste Disposal''. The research objectives are to generate better process understanding and data for the long-term safety analysis of a nuclear waste disposal in the deep geological underground. A better knowledge about the dominating processes essential for radionuclide (actinide) mobilization and immobilization on the molecular level is needed for the assessment of the macroscopic processes which determine the transport and distribution of radioactivity in the environment. Special emphasis is put on the biological mediated transport of long-lived radionuclides in the geosphere and their interaction with different biosystems like biota and human organism for a better calculation of environmental and health risks. Advanced knowledge is needed for description of the processes dominating at the interfaces between geo- and bio-systems related to the distribution of long-lived radionuclides in various bio-systems along the food chain. More than 120 scientists, technicians, and students, working on their Ph.D., diploma, master, or bachelor thesis, were employed at the Institute of Radiochemistry in 2011. About 20 Ph.D. students are working at the institute. Promotion of young scientists is an important requirement to ensure the competence and further excellent scientific results in the discipline of radiochemistry in future times. We accomplished many new scientific results in the past year, which are presented in this Annual Report, and about 50 original papers were published in peer-reviewed international scientific journals. In 2011, the future research profile of the HZDR was under discussion with the aim to focus the research fields and programs

  13. Specificity of discoveries in radiochemistry

    International Nuclear Information System (INIS)

    Krivomazov, A.N.

    1977-01-01

    The development of radiochemistry as a science is elucidated. On the basis of original papers and archives materials which have become available only recently, specific features of opening the law of radioactive displacements and isotopy of radioactive elements are presented in detail. A contribution of Hevesy, Russel, Fajans, and Soddy into the solution of this problem is considered; an important role of Rutherford in putting down the priority conflict is shown. Two stages of scientific generalization are singled out in the history of opening the law of radioactive displacements: the stage of the rules and the stage of the laws. On this basis the solutions of the priority problems have been reconsidered. It is shown that the history of radiochemistry is rich in discoveries which have undergone a relatively long evolution

  14. Nobel prize awards in radiochemistry

    International Nuclear Information System (INIS)

    Adloff, J.P.

    2012-01-01

    In 1996 the Editors of Radiochimica Acta brought out a special volume of the journal to celebrate the hundredth anniversary of the discovery of radioactivity. On the occasion of the 50 th anniversary of Radiochimica Acta, which follows closely upon the centenary of Marie Curie's second Nobel Prize in 1911, the author has the privilege to informally review 'Radiochemistry and Nobel Prize Awards', including discoveries of radioelements and new fields in chemistry based on radiochemical methods. (orig.)

  15. Analytical results of radiochemistry of the JRR-3M

    International Nuclear Information System (INIS)

    Yoshijima, Tetsuo; Tanaka, Sumitoshi

    1997-07-01

    The JRR-3 was modified for upgrading to enhance the experimental capabilities in 1990 as JRR-3M. JRR-3M is pool type research reactor, moderated and cooled by light water with a maximum thermal power of 20 MWt and a thermal neutron flux of about 2x10 14 n/cm 2 ·sec. The core internal structure and fuel cladding tube is made by aluminum alloy. The cooling systems are composed of primary cooling system, secondary cooling system, heavy water reflector system and helium gas system. The primary piping system, reactor pool and heavy water reflector system is constructed of type 304 stainless steel. The main objectives of radiochemistry are check the general corrosion of structural materials and detection of failed fuel elements for safe operation of reactor plant. In this report analytical results of radiochemistry and evaluation of radionuclides of cooling systems in the JRR-3M are described. (author)

  16. Nuclear Forensics and Radiochemistry: Chemistry

    Energy Technology Data Exchange (ETDEWEB)

    Rundberg, Robert S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-11-17

    The chemical behavior of radioactive elements can differ from conventional wisdom because the number of atoms can be unusually small. Kinetic effects and unusual oxidation states are phenomena that make radiochemistry different from conventional analytic chemistry. The procedures developed at Los Alamos are designed to minimize these effects and provide reproducible results over a wide range of sample types. The analysis of nuclear debris has the additional complication of chemical fractionation and the incorporation of environmental contaminants. These are dealt with through the use of three component isotope ratios and the use of appropriate end members.

  17. Nobel prize awards in radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Adloff, J.P. [Strasbourg Univ. (France)

    2012-07-01

    In 1996 the Editors of Radiochimica Acta brought out a special volume of the journal to celebrate the hundredth anniversary of the discovery of radioactivity. On the occasion of the 50{sup th} anniversary of Radiochimica Acta, which follows closely upon the centenary of Marie Curie's second Nobel Prize in 1911, the author has the privilege to informally review 'Radiochemistry and Nobel Prize Awards', including discoveries of radioelements and new fields in chemistry based on radiochemical methods. (orig.)

  18. Radiochemistry in nuclear power plants

    International Nuclear Information System (INIS)

    Schwarz, W.

    2007-01-01

    Radiochemistry is employed in nuclear power plants not as an end in itself but, among other things, as a main prerequisite of optimum radiation protection. Radiochemical monitoring of various loops provides important information about sources of radioactivity, activity distribution in the plant and its changes. In the light of these analytical findings, plant crews are able to take measures having a positive effect on radiation levels in the plant. The example of a BWR plant is used to show, among other things, how radiochemical analyses helped to reduce radiation levels in a plant and, as a consequence, to decrease clearly radiation exposure of the personnel despite higher workloads. (orig.)

  19. Nuclear Forensics and Radiochemistry: Fission

    Energy Technology Data Exchange (ETDEWEB)

    Rundberg, Robert S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-11-07

    Radiochemistry has been used to study fission since it’ discovery. Radiochemical methods are used to determine cumulative mass yields. These measurements have led to the two-mode fission hypothesis to model the neutron energy dependence of fission product yields. Fission product yields can be used for the nuclear forensics of nuclear explosions. The mass yield curve depends on both the fuel and the neutron spectrum of a device. Recent studies have shown that the nuclear structure of the compound nucleus can affect the mass yield distribution.

  20. Fifty years of Erlangen radiochemistry

    International Nuclear Information System (INIS)

    Morell, W.

    2007-01-01

    On June 29, 2006, the Radiochemical Laboratory of AREVA NP GmbH (formerly Siemens AG) in Erlangen celebrated its fiftieth anniversary. The occasion was marked by an event attended by more than 1,000 guests, among them Werner Gebauhr, the 85-year-old founder and first head of the Laboratory; the Managing Directors of AREVA NP GmbH, Ralf Gueldner and Ruediger Steuerlein; representatives of universities, research institutions, power utilities, and public authorities. The present head of the Radiochemical Laboratory, Wilfred Morell, sketched the highlights of the work performed over the past fifty years, which ranged from solid-state and very-high-purity materials technologies to development and service activities for nuclear technology. Manfred Erve, head of the Technical Center of AREVA NP GmbH, of which the Radiochemical Laboratory is a part, emphasized the changes in priorities over the past fifty years, which had always been met successfully by Radiochemistry. In the scientific part of the event, Wolfgang Schwarz (E.ON Kernkraftwerk GmbH, KKW Isar), Ulf Ilg (EnBW Kraftwerk AG, KKW Philippsburg), and Hans-Josef Allelein (Gesellschaft fuer Anlagen- und Reaktorsicherheit mbH) explained 3 major subject areas in which Erlangen Radio-chemistry over many years has contributed basic findings (see other articles in this atw issue). On the occasion of the anniversary, a comprehensive booklet was published under the title of '50 Jahre Radiochemie Erlangen - 1956-2006'. (orig.)

  1. Research on coolant radiochemistry

    International Nuclear Information System (INIS)

    Yeon, Jei Won; Kim, W. H.; Park, Y. J.; Im, J. K.; Jung, Y. J.; Jee, K. Y.; Choi, K. C.

    2004-04-01

    The final objective of this study is to develop the technology on the reduction of radioactive material formed in reactor coolant circuit. The contents of this study are composed of the simulation of primary cooling system, chemistry measurement technology in the high-temperature high-pressure environments, and coolant chemistry control technology. The main results are as follows; High-temperature and high-pressure loop system was designed and fabricated, which is to inducing CRUD growth condition on the surface of cladding. The high-temperature pH measurement system was established with YSZ sensing electrode and Ag/AgCl reference electrode. The performance of pH electrode was confirmed in the temperature range 200∼280 .deg. C. Coolant chemistry control technologies such as the neutron irradiation technique of boric acid solution, the evaluation on high-temperature electrochemical behavior of coolant, and the measurement of physicochemical properties of micro-particles were developed. The results of this study can be useful for the understanding of chemical phenomena occurred in reactor coolant and for the study on the reduction of radioactive material in primary coolant, which will be carried out in the next research stage

  2. Research on Coolant Radiochemistry

    International Nuclear Information System (INIS)

    Ha, Yeong Keong; Kim, W. H.; Yeon, J. W.; Jung, Y. J.; Choi, K. C.; Choi, K. S.; Park, Y. J.; Cho, Y. H.

    2007-06-01

    The final objective of this study is to develop a method for reducing radioactive materials formed in the reactor coolant circuit. This second stage research was categorized into the following three subgroups: the development of the estimation technique of microscopic chemical variation at high temperatures and pressures, the fundamental study on the thermodynamics at high temperatures and pressures, and the study on the deposition of metal oxides and the determination of the main factors responsible for the growth of CRUD. First, in the development of the estimation technique of microscopic chemical change at high temperatures and pressures, the technique for measuring coolant chemistry such as pH, conductivity and Eh was developed to be appropriate for the high temperature and pressure condition. The coolant chemistry measuring system including the self-devised high temperature pH sensor can be applied to the field of nuclear reactor and contribute on a large scale in the automation of the coolant chemistry control and the establishment of the real-time on-line measuring technique. Secondly, the dissociation constant of water and the solubility of metal oxides were measured in the fundamental study on the thermodynamics at high temperatures and pressures. Finally, in the study on the deposition of metal oxides and the determination of the main factors responsible for the growth of CRUD, the careful investigation of the deposition phenomena of micro particles on the cladding surface showed that subcooled boiling and the dissolved hydrogen are the main factors responsible for the growth of CRUD. In addition, the basis was provided for the construction of a new particle behavior model in the reactor coolant circuit

  3. Radiochemistry

    International Nuclear Information System (INIS)

    Majer, Vladimir

    1942-01-01

    The value of this monograph lies in the fact that it was one of the first monographs on this topic published not only within the national boundaries but also worldwide. The book was written during World War II, when the country was occupied by the Nazis and no Czech scientific research was possible; so the author devoted his free time to writing this monograph, which had influence on many young scientists and indirectly played a role in the founding of the Nuclear Physic Institute after the war. The author founded and was the first head of the Department of Nuclear Chemistry at the then Faculty of Technical and Nuclear Physics. (P.A.)

  4. Radiochemistry

    International Nuclear Information System (INIS)

    Vandevelde, L.

    1998-01-01

    The objectives, the programme, and the achievements of research activities at the Belgian Nuclear Research Centre SCK-CEN in the field of nuclear analytical techniques are summarized. Major efforts in 1997 went to the ARIANE project on the measurement of isotopic composition data of high-burnup LWR fuels. Another project consisted in the testing of a novel anion exchanger composed of a resin embedded in porous silica beads. This exchanger was examined to recover plutonium from spent fuel. Further efforts went to quality assurance and the provision of radiochemical and chemical analytical services to internal and external clients

  5. Radiochemistry

    International Nuclear Information System (INIS)

    Vandevelde, L.

    1998-01-01

    The objectives, the program, and the achievements of research activities at the Belgian Nuclear Research Centre SCK-CEN in the field of nuclear analytical techniques for 1997 are summarized. The main objectives are to provide reliable and accurate methods for the identification and quantification of alpha- and gamma-emitting radionuclides in a wide variety of matrices, to develop and to optimize the separation schemes to meet the requirements for preparing sources for these measurement techniques, to maintain and to improve the existing quality-assurance procedures in the framework of the Beltest accreditation

  6. Radiochemistry and radiochemical separations. A current bibliography

    International Nuclear Information System (INIS)

    Bujdoso, E.

    1999-01-01

    A current bibliography for years 1993-1996 with 159 references was compiled on radiochemistry and radiochemical separations based on the INIS Atomindex. The references are arranged in alphabetical order of first authors. (N.T.)

  7. Environmental radiochemistry and radioactivity. A current bibliography

    International Nuclear Information System (INIS)

    Bujdoso, E.

    1999-01-01

    A current bibliography with 146 references has been compiled on environmental radiochemistry and radioactivity for years 1993-1997 based on INIS Atomindex. The references are arranged alphabetically by first authors' names. (N.T.)

  8. Radiochemistry Programme biennial progress report 1984 and 1985

    International Nuclear Information System (INIS)

    1986-01-01

    This biennial progress report of the Radiochemistry Programme covers the calendar years 1984 and 1985. This report is organised into sections in a manner similar to the organisation of the Radiochemistry Programme. Thus the section on Fuel Behaviour Studies include post-irradiation studies (where the emphasis has been on setting up of facilities), mass spectrometry an nuclear chemistry. Process Chemistry Section covers the activities relating to fuel reprocessing as well as preparation and characterisation of fuel materials. Solid State Chemistry Section deals with thermophysical properties, thermogravimetry, oxygen potentials etc. In the Sodium Chemistry Section the developments relating to on-line meters and their applications are stressed in addition to studies on ternary systems involving sodium and oxygen. Developments in analytical chemistry and analytical services are covered in the next two Sections. Technical Services Section deals with developments in instrumentation and mechanical fabrication. (author)

  9. Synthesis of tracers using automated radiochemistry and robotics

    International Nuclear Information System (INIS)

    Dannals, R.F.

    1992-07-01

    Synthesis of high specific activity radiotracers labeled with short-lived positron-emitting radionuclides for positron emission tomography (PET) often requires handling large initial quantities of radioactivity. High specific activities are required when preparing tracers for use in PET studies of neuroreceptors. A fully automated approach for tracer synthesis is highly desirable. This proposal involves the development of a system for the Synthesis of Tracers using Automated Radiochemistry and Robotics (STARR) for this purpose. While the long range objective of the proposed research is the development of a totally automated radiochemistry system for the production of major high specific activity 11 C-radiotracers for use in PET, the specific short range objectives are the automation of 11 C-methyl iodide ( 11 CH 3 I) production via an integrated approach using both radiochemistry modular labstations and robotics, and the extension of this automated capability to the production of several radiotracers for PET (initially, 11 C-methionine, 3-N-[ 11 C-methyl]spiperone, and [ 11 C]-carfentanil)

  10. Radiochemistry Education at Washington State University: Sustaining Academic Radiochemistry for the Nation

    International Nuclear Information System (INIS)

    Clark, Sue B.; Nash, Ken; Benny, Paul; Clark, Aurora; Wall, Nathalie; Wall, Don; Yoo, Choong-Shik

    2009-01-01

    Since 2002, Washington State University has been building radiochemistry as a component of its overall chemistry program. Using an aggressive hiring strategy and leveraged funds from the state of Washington and federal agencies, six radiochemistry faculty members have been added to give a total of seven radiochemists out of a department of twenty-five faculty members. These faculty members contribute to a diverse curriculum in radiochemistry, and the Chemistry Department now enjoys a significant increase in the number of trainees, the quantity of research expenditures, and the volume and quality of peer-reviewed scientific literature generated by the radiochemistry faculty and the trainees. These three factors are essential for sustaining the radiochemistry education and research program at any academic institution.

  11. Status: nuclear and radiochemistry discipline

    International Nuclear Information System (INIS)

    Ramakumar, K.L.

    2013-01-01

    There is no universally accepted definition for the term 'nuclear chemistry'. We may regard nuclear chemistry as an interdisciplinary subject with roots in physics, biology, and chemistry. The basic aspects include among others (i) nuclear reactions and energy levels, (ii) the types and energetics of radioactive decay, (iii) the formation and properties of radioactive elements, (iv) the effect of individual isotopes on chemical and physical properties, and (v) the effects of nuclear radiation on matter. Research in (i) and (ii) is often indistinguishable in purpose and practice from that in nuclear physics, although for nuclear chemists, chemical techniques may play a significant role. (iii) and (iv) can be classified as radiochemistry and isotope chemistry, while (v) falls in the classification of radiation chemistry. There is an urgent need in India also to have similar mechanism. Different universities, research organizations and the education administrators should join hands to address this issue in a focused manner. This is all the more needed urgently as the nuclear power programme and other applications are expected to increase many fold in coming years

  12. Institute of Radiochemistry. Annual report 1992

    International Nuclear Information System (INIS)

    Bernhard, G.

    1993-05-01

    The Institute for Radiochemistry of the Research Center Rossendorf Inc. (FZR) started its work on 1 January 1992. As part of the FZR the Institute of Radiochemistry (IRC) is supported by the Free State of Saxony and the Federal Republic of Germany on the basis of equal shares. Furthermore the IRC has experienced helpful support in form of additional grants. This Annual Report summerizes the research activities achieved in the first year. Some papers result from research activities done in the different divisions of radiochemistry of the former Nuclear Research Centre Rossendorf. Problems of radioecology influence the present research programme and profile of this institute. The major goal of the IRC is fundamental and applied research on the field of the transport behaviour of radiochemical pollutants in the biosphere. Owing to the fact that Saxony and Thuringia are partly contaminated from previous uranium mining activities these investigations are of actual importance. (orig./BBR)

  13. Nuclear and Radiochemistry Fundamentals and Applications

    CERN Document Server

    Lieser, Karl Heinrich

    2001-01-01

    This handbook gives a complete and concise description of the up-to-date knowledge of nuclear and radiochemsitry and applications in the various fields of science. I is based on teaching courses and on research for over 40 years. The book is addressed to any researcher whishing sound knowledge about the properties of matter, be it a chemist, a physicist, a medical doctor, a mineralogist or a biologist. They will all find it a valuable source of information about the principles and applications of nuclear and radiochemistry. Research in radiochemistry includes: Study of radioactice matter in na

  14. Teaching nuclear and radiochemistry at undergraduate colleges

    International Nuclear Information System (INIS)

    Kinard, W.F.

    1993-01-01

    A large fraction of the potential graduate students in chemistry come from undergraduate colleges. The exposure of these students to the field of nuclear and radiochemistry is limited by the fact that few professionals actively involved in the field teach at these schools. There is also increasing competition for the limited number of chemistry students by other chemical specializations. Innovative approaches such as a short course to introduce students to nuclear and radiochemistry and some of the needs for undergraduate teaching are discussed. (author) 6 refs.; 2 figs

  15. Radiochemistry Education and Research Program at the Pennsylvania State University

    International Nuclear Information System (INIS)

    Uenlue, Kenan

    2009-01-01

    A new Radiochemistry Education and Research Program was started at the Pennsylvania University, Radiation Science and Engineering Center. The program was initially supported by the Department of Energy, Radiochemistry Education Award Program (REAP). Using REAP funding as leverage we obtained support from the Los Alamos National Laboratory, Department of Homeland Security, Domestic Nuclear Detection Office, various internal funding from PSU and other entities. The PSU radiochemistry program primarily addresses radiochemistry education and secondarily nuclear and radiochemistry research. The education program consists of bolstering our existing radiochemistry and related courses; Nuclear and Radiochemistry, Radiation Detection and Measurement, Radiological Safety and developing new courses, e.g., Laboratory Experiments in Applied Nuclear and Radiochemistry, and Nuclear Methods in Science. A new laboratory has been created with state of the art equipment for the Laboratory Experiments in Applied Nuclear and Radiochemistry course. We also plan to revitalize the nuclear and radiochemistry research programs. We established a state-of-the-art Neutron Activation Analysis Laboratory and a gamma ray spectroscopy laboratory that has 10 stations including state-of-the-art nuclear spectroscopy hardware and software. In addition, we embarked on an expansion plan that included building a new neutron beam hall and neutron beam ports with a cold neutron source. One of the reasons to have a cold neutron source is for the development of a prompt gamma activation analysis facility. A detailed description of PSU radiochemistry education and research program will be given and the future plans will be discussed.

  16. Radiochemistry in the world: a biblio-metric study (1989-1998); La radiochimie dans le monde: etude bibliometrique (1989-1998)

    Energy Technology Data Exchange (ETDEWEB)

    Guillaumont, R. [Academie des Sciences, 75 - Paris (France); Madic, Ch. [CEA Saclay, Dir. de l' Energie Nucleaire DEN, 91 - Gif sur Yvette (France); Pichot, Ch. [CEA Saclay, Dept. Patrimoine et Infrastructures, DEN/DPI/STI/SID, 91 - Gif sur Yvette (France); Rousseau-Hans, F. [CEA Saclay, Direction des Technologies de l' Information, DTI/SITI/LII, 91 - Gif sur Yvette (France)

    2002-07-01

    The study analyzes the world literature in the field of radiochemistry. It tries to represent the radiochemistry, through the development of its sub-fields in the different parts of the world and through the international collaboration patterns. Most data come from the INIS (International Nuclear Information System) database operated by the International Atomic Energy Agency (IAEA) and cover the 1989-1998 era. Less rich countries publish proportionally more in fundamental radiochemistry whereas high developed countries invest more in nuclear medicine. Another aspect of the radiochemistry is approached with the study of scientific national and international journals which publish articles in this field. English remains the most important language used in the fundamental fields of radiochemistry while national languages, such as russian, japanese and chinese, keep a certain importance in applied sciences like earth sciences, waste management and nuclear medicine. (author)

  17. Radiochemistry teaching and research activities in Brazil

    International Nuclear Information System (INIS)

    Vasconcellos, M.B.A.; Saiki, M.

    2006-01-01

    Much concern has been expressed lately about the decline of teaching and research activities in radiochemistry in many countries, as was discussed in an IAEA Technical Meeting in Antalya, Turkey, in 2002, and also at MTAA-11 in Guildford, UK. In the IAEA meeting, a survey was presented about the current situation in different regions of the world (Eastern Europe, East and West Asia, Africa, North America and Latin America) by experts of each region. In the case of Brazil, which has nuclear research reactors and also cyclotrons in operation, the teaching and research activities in radiochemistry are concentrated in the three main institutes of the Brazilian Nuclear Energy Commission, in the University of Sao Paulo and in other universities, in different regions of the country. In the present paper, a closer look is given to the radiochemistry teaching and research activities that are being conducted nowadays in Brazil, comprising: number of radiochemistry courses and students being formed, main research areas being conducted, as well as research and production of radioisotopes for nuclear medicine, using nuclear reactors and cyclotrons. (author)

  18. Forty-five years of radiochemistry education

    International Nuclear Information System (INIS)

    Preiss, I.L.; Rensselaer Polytechnic Inst., Troy, NY

    1993-01-01

    H.M. Clark introduced radiochemistry as an undergraduate program at Rensselear in 1947. The development of the course and the companion courses under Clark and Preiss that now form the radiochemical educational experience at RPI is outlined. Prospects for the future directions of the field and the educational requirements are discussed. (author)

  19. Workshop on selected aspects of radiochemistry

    International Nuclear Information System (INIS)

    1991-11-01

    The aspects chosen for the workshop are: isotope preparation, separation methods; radiochemical methods and analyses; environmental protection and radiochemistry; the chemistry of the fifth halogen, astatine. From the 28 contributions presented at the workshop, 24 are of relevance in the INIS and EDB scope and are separately retrievable from the database. (BBR) [de

  20. Radiochemistry and nuclear methods of analysis

    International Nuclear Information System (INIS)

    Ehmann, W.D.; Vance, D.

    1991-01-01

    This book provides both the fundamentals of radiochemistry as well as specific applications of nuclear techniques to analytical chemistry. It includes such areas of application as radioimmunoassay and activation techniques using very short-lined indicator radionuclides. It emphasizes the current nuclear methods of analysis such as neutron activation PIXE, nuclear reaction analysis, Rutherford backscattering, isotope dilution analysis and others

  1. Radiochemistry Division annual progress report for 1977

    International Nuclear Information System (INIS)

    Iyer, R.H.; Natarajan, P.R.

    1979-01-01

    The research and development work carried by the Radiochemistry Division of the Bhabha Atomic Research Centre, Bombay, during the calendar year 1977 in the areas of reactor chemistry, actinide chemistry, process chemistry of neptunium and plutonium-239, radioanalytical chemistry and nuclear chemistry has been reported. (M.G.B.)

  2. Radiochemistry Division annual progress report : 1992

    International Nuclear Information System (INIS)

    Natarajan, V.; Godbole, S.V.; Iyer, R.H.

    1994-01-01

    The research and development activities of the Radiochemistry Division during 1992 are briefly described in the form of individual summaries grouped under the headings: 1) Nuclear Chemistry, 2) Actinide Chemistry, 3) Spectroscopy, and 4) Instrumentation. A list of publications numbering 95 by the scientific staff of the Division is also included in the report. (author). 35 figs., 56 tabs

  3. Radiochemistry Division annual progress report: 1986

    International Nuclear Information System (INIS)

    Datta, T.

    1988-01-01

    Research and Development (R and D) activities of the Radiochemistry Division of Bhabha Atomic Research Centre, Bombay during 1986 are reported. Some of the highlights of these activities are solvent extraction studies on U(VI) and trivalent Am, Cm and Cf, low energy and medium energy fission of actinides, nuclear reactions on 197 Au, perturbed angular correlation studies on polymerisation of Hf(IV) and EPR studies on Am doped BaCO 3 , SrSO 4 and LiKSO 4 . Investigations on the complexation, hydrolysis and speciation of Am(III) in phosphate and carbonate media have been carried out with a view to understanding the behaviour of Am ions in natural and waste water systems. The angular momentum studies have shown that fission fragment angular momentum increases with increasing excitation energy and angular momentum of the fissioning due to coupling of various collective rotational degrees of freedom. Angular distribution studies have shown that asymmetric mode fragments have higher anisotropy compared to the symmetric mode fragments due to extended saddle point shape and hence larger effective moment of inertia. Studies on alpha induced nuclear reaction on 197 Au have provided evidence for non-equilibrium particle emission process as against the expected compound nucleus mechanism. EPR and TSL studies on actinide doped solids have shown stabilisation of radicals produced on irradiations as well as provided evidence for chemically induced dynamic nuclear polarization. At the end of the report, a list of publications of the staff members of the Division during the report is given. These publications include journal articles, conference paper and technical reports. (Orig.)

  4. Radiochemistry Division annual progress report : 1991

    International Nuclear Information System (INIS)

    Natarajan, V.; Godbole, S.V.; Iyer, R.H.

    1993-01-01

    The research and development activities of the Radiochemistry Division during 1991 are briefly described under the headings: (i) Nuclear chemistry, (ii) Actinide chemistry, and (iii) Spectroscopy. In the field of nuclear chemistry, the main emphasis has been on the studies of fission process induced by reactor neutrons and light and heavy ions on actinides and low Z (Z c superconductors. A list of publications by the scientific staff of the Division is given at the end. (author). 31 figs., 49 tabs

  5. Experiments for training in nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Moebius, S.

    1988-01-01

    An experimental training program for education in Nuclear and Radiochemistry is outlined. Didactical aspects are discussed, the installation of a suitable radiochemical laboratory is described and the precautions for radiation protection summarized. Experiments including theoretical introduction, survey of apparatus and materials involved and experimental procedures are given for the topics of radiation and their measurement, radiochemical methods and application of radioisotopes. Technical terms most often used during the course are explained and a comprehensive literature survey is finally compiled. (orig.) [de

  6. Nuclear and radiochemistry fundamentals and applications

    CERN Document Server

    Lieser, Karl Heinrich

    2001-01-01

    his new edition of the best-selling handbook gives a complete and concise description of the latest knowledge on nuclear and radiochemistry as well as their applications in the various fields of science. It is based on over 40 years experience in teaching courses and research.The book is aimed at all researchers seeking sound knowledge about the properties of matter, whether chemists, physicists, medical doctors, mineralogists or biologists. All of them will find this a valuable source of information

  7. Experiments for training in nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Moebius, S.

    1985-03-01

    An experimental training program for education in Nuclear and Radiochemistry is outlined. Didactical aspects are discussed, the installation of a suitable radiochemical laboratory is described and the precautions for radiation protection summarized. Experiments including theoretical introduction, survey of apparatus and materials involved and experimental procedures are given for the topics of Radiation and Their Measurement, Radiochemical Methods and Application of Radioisotopes. Technical Terms most often used during the course are explained and a comprehensive literature survey is finally compiled. (orig.) [de

  8. Radiochemistry and nuclear methods of analysis

    International Nuclear Information System (INIS)

    Ehmann, W.D.; Vance, D.E.

    1993-01-01

    In comparison with other aspects of physical science, nuclear and radiochemistry are small contributors to the overall scheme of things. Nuclear science is, however, an important player in various aspects of medicine, life sciences, industrial technology, physical sciences, archeometry and art, and theoretical/computational sciences. This new book fills the need for a contemporary text with a good mix of simple introductory theory, experimental methodology, and instrumentation for beginning students of nuclear science

  9. Annual report 2009. Institute of Radiochemistry

    International Nuclear Information System (INIS)

    Bernhard, G.

    2010-01-01

    The annual report 2009 of the institute of radiochemistry covers the following topics: Part 1: Actinides (metals) in biosystems; Part 2: Actinides in waste repositories. The research projects were aimed to the basic knowledge about coordination of actinide element transport and transfer in the environment, bacteria influence on the immobilization of heavy metals in water and soils, microbial diversity in biofilms and clays, protein applications for biosensors, dominating processes of soil-liquid interfaces, sorption and surface complexation processes.

  10. Future directions for separation science in nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Pruett, D.J.

    1986-01-01

    Solvent extraction and ion exchange have been the most widely used separation techniques in nuclear and radiochemistry since their development in the 1940s. Many successful separations processes based on these techniques have been used for decades in research laboratories, analytical laboratories, and industrial plants. Thus, it is easy to conclude that most of the fundamental and applied research that is needed in these areas has been done, and that further work in these ''mature'' fields is unlikely to be fruitful. A more careful review, however, reveals that significant problems remain to be solved, and that there is a demand for the development of new reagents, methods, and systems to solve the increasingly complex separations problems in the nuclear field. Specifically, new separation techniques based on developments in membrane technology and biotechnology that have occurred over the last 20 years should find extensive applications in radiochemical separations. Considerable research is needed in such areas as interfacial chemistry, the design and control of highly selective separation agents, critically evaluated data bases and mathematical models, and the fundamental chemistry of dilute solutions if these problems are to be solved and new techniques developed in a systematic way. Nonaqueous separation methods, such as pyrochemical and fluoride volatility processes, have traditionally played a more limited role in nuclear and radiochemistry, but recent developments in the chemistry and engineering of these processes promises to open up new areas of research and application in the future

  11. Forschungszentrum Rossendorf, Institute of Radiochemistry. Annual report 2004

    Energy Technology Data Exchange (ETDEWEB)

    Bernhard, G [ed.

    2005-07-01

    The Institute of Radiochemistry (IRC), one of the six Institutes of the Forschungszentrum Rossendorf (FZR) performs basic and applied research in the fields of radiochemistry and radioecology. Motivation and background of our research are environmental processes relevant for the installation of nuclear waste repositories, for remediation of uranium mining and milling sites, and for radioactive contaminations caused by nuclear accidents and fallout. Because of their high radiotoxicity and long half-life the actinides are of special interest. The research is focused on a better understanding of the chemical behavior of actinides in the environment on a molecular level. We will increase our efforts to study both the speciation of actinides on bio-molecular interfaces and their transport in bio-systems. Current topics of our research work are: aquatic chemistry of actinides, actinides in bio-systems, interaction of actinides with solid phases, Reactive transport of actinides. About 60 scientists, technicians and PhD students are employed at the Institute of Radiochemistry. We accomplished many new scientific results in the past year, which are presented in this annual report. Among them only few can be highlighted in this preface. Further progress was achieved in understanding the formation and characterization of uranium containing colloids. The newly installed method of laser-induced breakdown detection was very helpful for the identification of uranium colloids under anoxic conditions. We were very successful in the determination of formation pathways and structure of various actinide complexes. These results contribute to a better understanding of actinide speciation in geo- and bio-systems, especially with respect to the chemical processes on the interfaces. The results achieved in the characterization of the properties, modification, and interaction of the S-layers of Bacillus sphaericus with uranium and some other heavy metals strengthen our hope to use this

  12. Forschungszentrum Rossendorf, Institute of Radiochemistry. Annual report 2004

    International Nuclear Information System (INIS)

    Bernhard, G.

    2005-01-01

    The Institute of Radiochemistry (IRC), one of the six Institutes of the Forschungszentrum Rossendorf (FZR) performs basic and applied research in the fields of radiochemistry and radioecology. Motivation and background of our research are environmental processes relevant for the installation of nuclear waste repositories, for remediation of uranium mining and milling sites, and for radioactive contaminations caused by nuclear accidents and fallout. Because of their high radiotoxicity and long half-life the actinides are of special interest. The research is focused on a better understanding of the chemical behavior of actinides in the environment on a molecular level. We will increase our efforts to study both the speciation of actinides on bio-molecular interfaces and their transport in bio-systems. Current topics of our research work are: aquatic chemistry of actinides, actinides in bio-systems, interaction of actinides with solid phases, Reactive transport of actinides. About 60 scientists, technicians and PhD students are employed at the Institute of Radiochemistry. We accomplished many new scientific results in the past year, which are presented in this annual report. Among them only few can be highlighted in this preface. Further progress was achieved in understanding the formation and characterization of uranium containing colloids. The newly installed method of laser-induced breakdown detection was very helpful for the identification of uranium colloids under anoxic conditions. We were very successful in the determination of formation pathways and structure of various actinide complexes. These results contribute to a better understanding of actinide speciation in geo- and bio-systems, especially with respect to the chemical processes on the interfaces. The results achieved in the characterization of the properties, modification, and interaction of the S-layers of Bacillus sphaericus with uranium and some other heavy metals strengthen our hope to use this

  13. Education of radiochemistry in the University of Helsinki, Finland

    International Nuclear Information System (INIS)

    Lehto, J.

    2005-01-01

    Laboratory of Radiochemistry is one of the seven laboratories in the Department of Chemistry, University of Helsinki. In the department there are altogether 220 employees of which 25 work in the Laboratory of Radiochemistry. Laboratory of Radiochemistry is the only radiochemical institute within Finnish universities. It gives teaching in a wide range of topics including most areas of radiochemistry. Teaching in radiochemistry is given at the master's level. Prior to taking radiochemistry as their major students have studied two to three years of chemistry and other fields of sciences. Compulsory courses in radiochemistry are: (1) Principles of radioactivity and radiochemistry (8 credit units), includes two weeks' laboratory course. (2) Radiation safety (2 cu), includes one day laboratory work. (3) Detection and measurement of radiation (5 cu), includes two weeks' laboratory course. (4) Chemistry and analysis of radionuclides (5 cu), includes two weeks' laboratory course. There are several optional courses of which students have to take at least three: (1) Chemistry of the nuclear fuel cycle (3 cu), students write an essay. (2) Environmental radioactivity (3 cu), students write an essay and give a seminar lecture. (3) Radiopharmaceutical chemistry (3 cu), includes one week laboratory course. (4) Radioactive tracer techniques (3 cu), includes one week laboratory course. (5) Radiation chemistry (3 cu), includes one week laboratory course. (6) Chemistry of uranium series in the environment (3 cu). (7) Atmospheric radioactivity (3 cu), students write an essay. After finalising the required radiochemistry courses, and other studies (40 cu), students make their project work and write a master's thesis (together 40 cu). Project work and master's thesis are done in one of the research projects of the laboratory. The research projects are working in the following fields: 1) migration and retention of radionuclides in the geo sphere, 2) selective separation of radionuclides

  14. Education of radiochemistry in the University of Helsinki, Finland

    International Nuclear Information System (INIS)

    Lehto, J.

    2005-01-01

    Laboratory of Radiochemistry is one of the seven laboratories in the Department of Chemistry, University of Helsinki. In the department there are altogether 220 employees of which 25 work in the Laboratory of Radiochemistry. Laboratory of Radiochemistry is the only radiochemical institute within Finnish universities. It gives teaching in a wide range of topics including most areas of radiochemistry. Teaching in radiochemistry is given at the master's level. Prior to taking radiochemistry as their major students have studied two to three years of chemistry and other fields of sciences. Compulsory courses in radiochemistry are: Principles of radioactivity and radiochemistry (8 credit units), includes two weeks' laboratory course. Radiation safety (2 cu), includes one day laboratory work. Detection and measurement of radiation (5 cu), includes two weeks' laboratory course. Chemistry and analysis of radionuclides (5 cu), includes two weeks' laboratory course There are several optional courses of which students have to take at least three: Chemistry of the nuclear fuel cycle (3 cu), students write an essay. Environmental radioactivity (3 cu), students write an essay and give a seminar lecture. Radiopharmaceutical chemistry (3 cu), includes one week laboratory course. Radioactive tracer techniques (3 cu), includes one week laboratory course. Radiation chemistry (3 cu), includes one week laboratory course. Chemistry of uranium series in the environment (3 cu). Atmospheric radioactivity (3 cu), students write an essay. After finalising the required radiochemistry courses, and other studies (40 cu), students make their project work and write a master's thesis (together 40 cu). Project work and master's thesis are done in one of the research projects of the laboratory. The research projects are working in the following fields: 1) migration and retention of radionuclides in the geo sphere, 2) selective separation of radionuclides from nuclear waste effluents, 3

  15. Forschungszentrum Rossendorf, Institute of Radiochemistry. Annual report 2000

    International Nuclear Information System (INIS)

    2001-05-01

    The Institute of Radiochemistry (IRC), one of the five institutes of the Forschungszentrum Rossendorf (FZR) performs basic and applied research in the fields of radiochemistry and radioecology. Main goal is the quantification of the interaction and mobility of radionuclides in the geo- and biosphere. Because of their high radiotoxicity and long half-life the actinides are of special interest. Among the actinides uranium and its manifold interactions plays a major role in the institute's research activities. In addition the interactions of some important long-lived fission and decay products are studied. More than 60 scientists, technicians and PhD students are employed in the Institute of Radiochemistry. The research is focused on understanding the fundamental processes relevant for the behavior of radionuclides in the environment. Main topics are: Aquatic chemistry, Radionuclide interaction with mineral surfaces, Radionuclide interaction with biological materials (microbes and plants), Modeling the radionuclide transport, Development of spectroscopic speciation methods. Further progress was achieved in understanding the interaction mechanism of actinides with humic acids. The coordination numbers and bond distances of the coordinated oxygens have been determined by X-ray absorption spectroscopy for tetra- and pentavalent actinides (Np(IV) and Np(V)). It was shown that the carboxylic groups of the humic acid form monodentate complexes with the neptonyl ions. We extended our laser spectroscopic capabilities by installing a new laser system with ultra-short pulses (130 fs) for fluorescence measurements of organic substances. We intend to gain information on actinide complexes with organic ligands by studying the fluorescence properties of the organics with very short life times. The laser system and the method were successfully validated by the determination of the well-known uranyl-salicylic acid complexation. Although surface complexation concepts are more and more

  16. The SFU/TRIUMF Radiochemistry Institute

    International Nuclear Information System (INIS)

    Ruth, T.J.; D'Auria, J.M.

    1993-01-01

    An institute for the training of radiochemist was proposed in 1989 by scientists/educators from Simon Fraser University (SFU) and the TRIUMF Nuclear Research Facility in Canada. The intensive program spans 6 weeks and includes seminars and problem sessions as well as practical laboratory experience. Topics include health physics, synthesis of short lived radiopharmaceuticals, automation and quality control. The first offering was in May-June 1990. Based on this experience a textbook on Radiochemistry and Radiopharmaceutical Chemistry has been initiated. Parts of the program may be implemented into a credit course to be offered through the Department of Chemistry at SFU. (author) 6 refs.; 3 tabs

  17. Radiochemistry Division biennial progress report: 1995-1996

    International Nuclear Information System (INIS)

    Tomar, B.S.; Pujari, P.K.; Mathur, J.N.; Mohapatra, P.K.; Murali, M.S.; Natarajan, V.; Jayanthakumar, M.L.

    1997-01-01

    The research and development activities of Radiochemistry Division during 1995-96 are briefly described under the headings : (1) nuclear chemistry; (2) actinide chemistry; (3) spectroscopy and (4) instrumentation. Nuclear chemistry work deals with the areas of nuclear reactions, nuclear spectroscopy, nuclear probes and radioanalytical techniques. The research programme in actinide chemistry centered on development of novel procedures for the separation of actinides, guest-host chemistry of lanthanides, actinides and fission products and extractants for solvent extraction. Spectroscopy section activities are summarised under (1) basic research in the solid state chemistry; (2) development of analytical spectroscopic methods for the trace metal determination in nuclear materials; (3) chemical quality control of plutonium 239, uranium 233 and thorium based nuclear fuels. Instrumentation group deals mainly with servicing and maintenance of electronic instruments and allied systems. A list of publications, by the scientific staff of the Divisions is also included. (author)

  18. Radiochemistry Division biennial progress report: 1995-1996

    Energy Technology Data Exchange (ETDEWEB)

    Tomar, B S; Pujari, P K; Mathur, J N; Mohapatra, P K; Murali, M S; Natarajan, V; Jayanthakumar, M L [eds.; Radiochemistry Division, Bhabha Atomic Research Centre, Mumbai (India)

    1998-12-31

    The research and development activities of Radiochemistry Division during 1995-96 are briefly described under the headings : (1) nuclear chemistry; (2) actinide chemistry; (3) spectroscopy and (4) instrumentation. Nuclear chemistry work deals with the areas of nuclear reactions, nuclear spectroscopy, nuclear probes and radioanalytical techniques. The research programme in actinide chemistry centered on development of novel procedures for the separation of actinides, guest-host chemistry of lanthanides, actinides and fission products and extractants for solvent extraction. Spectroscopy section activities are summarised under (1) basic research in the solid state chemistry; (2) development of analytical spectroscopic methods for the trace metal determination in nuclear materials; (3) chemical quality control of plutonium 239, uranium 233 and thorium based nuclear fuels. Instrumentation group deals mainly with servicing and maintenance of electronic instruments and allied systems. A list of publications, by the scientific staff of the Divisions is also included. (author)

  19. Recent radiochemistry observations at the Riverton and Maybell tailings piles

    International Nuclear Information System (INIS)

    Smith, A.R.; Moed, B.A.

    1982-09-01

    Preliminary results are presented from the radiochemistry effort of the Lawrence Berkeley Laboratory integrated study of the inactive uranium mill tailings sites at Riverton, Wyoming and Maybell, Colorado. These results were obtained primarily by use of #betta#-ray spectrometric techniques, and included both field and laboratory application of NaI(Tl) crystal and Ge-semiconductor detector systems. Current interpretation of this evidence indicated there has been downward migration of uranium within the tailings column since its emplacement, and upward movement of several radionuclides from the tailings into the overlying cover material. The mechanisms responsible for these migrations are believed to involve fluid transport, and are further believed to be active at the present time

  20. Radiochemistry and the Study of Fission

    Energy Technology Data Exchange (ETDEWEB)

    Rundberg, Robert S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-11-14

    These are slides from a lecture given at UC Berkeley. Radiochemistry has been used to study fission since its discovery. Radiochemical methods are used to determine cumulative mass yields. These measurements have led to the two-mode fission hypothesis to model the neutron energy dependence of fission product yields. Fission product yields can be used for the nuclear forensics of nuclear explosions. The mass yield curve depends on both the fuel and the neutron spectrum of a device. Recent studies have shown that the nuclear structure of the compound nucleus can affect the mass yield distribution. The following topics are covered: In the beginning: the discovery of fission; forensics using fission products: what can be learned from fission products, definitions of R-values and Q-values, fission bases, K-factors and fission chambers, limitations; the neutron energy dependence of the mass yield distribution (the two mode fission hypothesis); the influence of nuclear structure on the mass yield distribution. In summary: Radiochemistry has been used to study fission since its discovery. Radiochemical measurement of fission product yields have provided the highest precision data for developing fission models and for nuclear forensics. The two-mode fission hypothesis provides a description of the neutron energy dependence of the mass yield curve. However, data is still rather sparse and more work is needed near second and third chance fission. Radiochemical measurements have provided evidence for the importance of nuclear states in the compound nucleus in predicting the mass yield curve in the resonance region.

  1. Nuclear chemistry and Radiochemistry in the USA

    International Nuclear Information System (INIS)

    Kronenberg, A.

    2004-01-01

    Nuclear chemistry and radiochemistry are very young sciences which developed at an extremely brisk pace within a very short period of time after the discovery of nuclear fission in 1938, and caused profound societal changes. In the United States, nuclear chemistry developed very differently from Germany, where nuclear research initially had been banned after the Second World War. The prime mover in the development in the United States was the Manhattan Project, the construction of the atomic bomb. The counteract the impending shortage of qualified personnel, important institutions have begun to establish training and support programs in the field. The National Laboratories in the United States introduced a National Security Internship Program, while the U.S. Department of Energy (DOE) tries to promote cooperation, and thus the training of personnel, by launching programs of its own. Yet, a greater shortage of qualified personnel is becoming apparent. The situation of nuclear chemistry and radiochemistry in the United States can be summarized in the finding that research at the National Laboratories is very wide ranging. It receives sufficient funds from the DOE. However, the National Laboratories show a very high proportion of elderly personnel, a problem which will have to be corrected in the years to come. This may be helped by the Summer Schools financed by the DOE, though a summer school of six weeks cannot replace a sound training in nuclear chemistry of the kind still to be found in Germany. (orig.) [de

  2. FZR Institute of Radiochemistry. Annual report 1991

    International Nuclear Information System (INIS)

    Bernhard, G.

    1992-04-01

    The Research Center Rossendorf Inc. was founded on 1 January 1992 as an Institute of the Blue List. It is financed in equal shares by the Free State of Saxony and the Federal Republic of Germany. The Research Center Rossendorf (FZR) carries out its scientific work in five institutes: Institute of Ion Beam Physics and Materials Research; Institute of Nuclear and Hadronic Physics; Institute of Safety Research; Institute of Bioanorganic and Radiopharmaceutical Chemistry; Institute of Radiochemistry. The presentation of the Institute of Radiochemistry is to be considered a description of working tasks from today's angle. In the course of the formation process up to the end of the year specifications and partly also substantial changes will have to be considered. Although the Research Center Rossendorf has been recently founded, its plans are based of course on the scientific experiences of its staff. The said experiences form the basis for the status report on the lines of work. The last part compiles abridged versions of individual results achieved in 1991, documenting for specialists the work done by the groups of scientists. (orig./BBR) [de

  3. Summer Schools in Nuclear and Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Silber, Herbert B. [San Jose State University

    2013-06-20

    The ACS Summer Schools in Nuclear and Radiochemistry (herein called “Summer Schools”) were funded by the U.S. Department of Energy and held at San Jose State University (SJSU) and Brookhaven National Laboratory (BNL). The Summer Schools offer undergraduate students with U.S. citizenship an opportunity to complete coursework through ACS accredited chemistry degree programs at SJSU or the State University of New York at Stony Brook (SBU). The courses include lecture and laboratory work on the fundamentals and applications of nuclear and radiochemistry. The number of students participating at each site is limited to 12, and the low student-to-instructor ratio is needed due to the intense nature of the six-week program. To broaden the students’ perspectives on nuclear science, prominent research scientists active in nuclear and/or radiochemical research participate in a Guest Lecture Series. Symposia emphasizing environmental chemistry, nuclear medicine, and career opportunities are conducted as a part of the program. The Department of Energy’s Office of Basic Energy Sciences (BES) renewed the five-year proposal for the Summer Schools starting March 1, 2007, with contributions from Biological and Environmental Remediation (BER) and Nuclear Physics (NP). This Final Technical Report covers the Summer Schools held in the years 2007-2011.

  4. Radiochemistry and the Study of Fission

    International Nuclear Information System (INIS)

    Rundberg, Robert S.

    2016-01-01

    These are slides from a lecture given at UC Berkeley. Radiochemistry has been used to study fission since its discovery. Radiochemical methods are used to determine cumulative mass yields. These measurements have led to the two-mode fission hypothesis to model the neutron energy dependence of fission product yields. Fission product yields can be used for the nuclear forensics of nuclear explosions. The mass yield curve depends on both the fuel and the neutron spectrum of a device. Recent studies have shown that the nuclear structure of the compound nucleus can affect the mass yield distribution. The following topics are covered: In the beginning: the discovery of fission; forensics using fission products: what can be learned from fission products, definitions of R-values and Q-values, fission bases, K-factors and fission chambers, limitations; the neutron energy dependence of the mass yield distribution (the two mode fission hypothesis); the influence of nuclear structure on the mass yield distribution. In summary: Radiochemistry has been used to study fission since its discovery. Radiochemical measurement of fission product yields have provided the highest precision data for developing fission models and for nuclear forensics. The two-mode fission hypothesis provides a description of the neutron energy dependence of the mass yield curve. However, data is still rather sparse and more work is needed near second and third chance fission. Radiochemical measurements have provided evidence for the importance of nuclear states in the compound nucleus in predicting the mass yield curve in the resonance region.

  5. Radiochemistry in chemistry and chemistry related undergraduate programmes in Argentina

    International Nuclear Information System (INIS)

    Fornaciari Iljadica, M.C.; Furnari, J.C.; Cohen, I.M.

    2006-01-01

    The evolution of education in Argentina at the university level is described. The detailed search of the educational offer shows that less than half of the universities (35 out of 92) include chemistry and chemistry related undergraduate programmes in their curriculum. The revision of the position of radiochemistry in these programmes reveals that only seven courses on radiochemistry are currently offered. Radiochemistry is included only in few programmes in chemistry and biochemistry. With respect to the programmes in chemical engineering the situation is worse. This offer is strongly concentrated in Buenos Aires and its surroundings. (author)

  6. Assessment of radiological status of underground tunnel of radiochemistry wing

    International Nuclear Information System (INIS)

    Patre, D.K.; Thanamani, S.; Ojha, Shashikala; Murali, S.

    2012-01-01

    Radiochemistry Wing, RLG has design based safety systems for lab exhaust and glove box ventilation exhaust. The respective exhaust headers are routed from the lab exhaust point to the filter house. The concretized underground tunnel runs between Radiochemistry wing, RLG and Filter house about 100 m away. It houses the main exhaust tunnel made of MS, has reportedly developed leakage in the MS lines of exhaust due to ageing. It was indicated by the inadequate ventilation to the lab exhaust which reduced ∼ 10 % of the total exhaust. It was decided to carry out the replacement of main exhaust duct subject to radiological safety and clearance from the regulatory agencies. Since the duct had been in use since past 40 years, HP assessment on contamination status, clearance from local safety committee and related regulatory agency are mandatory. In view of the same, the study on radiological parameters was taken up and the paper describes the results of our radiological surveillance. Proposed replacement work involves approximately estimated surface area of duct as 520 m 2 , volume of the material as 106 m 3 and the weight of material of exhaust duct as 12.5 tons. Underground tunnel of radiochemistry wing consists of 3 main segments. It was monitored thoroughly by radiation survey. Spot air sample was collected during the radiological survey. Around 200 swipes were taken from various portions of the segments and the effluent pipelines. Last two tunnel segment were not approachable. Smear swipes were taken from top, side, bottom and floor of each segment. Calibrated scintillation counters were used for assessment of μ air activity and μ contamination check. Spot air samples were taken during different operations showed no activity. Dose rate in the tunnel was found to be less than 1 μSv/h (0.1 mR/h). The μ contamination levels were found in increasing order from the first segment to the last segment. (0.05 - 0.1 Bq/cm 2 ). Effluent pipelines were found to have

  7. Radiochemistry and associated nuclear chemistry in the beginning of the twenty-first century

    International Nuclear Information System (INIS)

    Goeij, J.J.M. de

    2002-01-01

    In many countries radiochemistry and associated nuclear chemistry are facing decreasing attention in scientific and technological education and training. In addition, research facilities involving radioactivity are dealing with growing difficulties, e.g. in respect to finances, staff, public support, and legislation. Quite often it is suggested that radiochemistry has matured and does not need any further development. Moreover, it is stated that radiochemical methods are out-run by new, non-nuclear methods, and thus have actually lost their raison d'etre. Altogether this leads to a situation where radioactivity and radiochemistry are partly vanishing both as a science and as a tool. This situation calls for a closer examination for areas where radiochemistry may continue to play a useful, if not a decisive role, and some guidelines were presented how to proceed in the near future. For that purpose a definition of radiochemistry is given to demarcate it from other areas. Nuclear chemistry as an adjacent field is strongly connected with radiochemistry, and in the frame of the presentation a relevant part of it is considered here as integrated in radiochemistry. The various areas of radiochemistry may be classified into three categories, which partly overlap. The first category is the field of the fundamental aspects of radiochemistry itself. This category covers among others nuclear reaction cross-sections, production routes with associated yields and radionuclidic impurities, decay schemes of radionuclides, radiochemical separations, recoil and hot-atom chemistry, isotope effects and fractionation, and interaction of radiation with matter and detection. The second category covers fields where radioactivity is inextricably bound to the subject involved. This holds e.g. for the entire nuclear fuel cycle, study of the very heavy elements (Z > 100), primordial radioactivity on earth, cosmogenic radioactivity in atmosphere and cosmos, and radionuclides for dating. The

  8. Radiochemistry at the University of Missouri-Columbia. A joint venture with chemistry, nuclear engineering, molecular biology, biochemistry, and the Missouri University Research Reactor (MURR)

    International Nuclear Information System (INIS)

    Miller, W.H.; Duval, P.; Jurisson, S.S.; Robertson, J.D.; Wall, J.D.; Quinn, T.P.; Volkert, W.A.; Neumeyer, G.M.

    2005-01-01

    Missouri University, a recipient of a U.S. Department of Energy Radiochemistry Education Award Program (REAP) grant in 1999, has significantly expanded its education and research mission in radiochemistry. While MU had a viable radiochemistry program through existing faculty expertise and the utilization of the Missouri University Research Reactor, the REAP award allowed MU to leverage its resources in significantly expanding capabilities in radiochemistry. Specifically, the grant enabled the: (1) hiring of a new faculty member in actinide radiochemistry (Dr. Paul Duval); (2) support of six graduate students in radiochemistry; (3) purchase of new radiochemistry laboratory equipment; (4) more extensive collaboration with DOE scientists through interactions with faculty and graduate students, and (5) revised radiochemical curriculum (joint courses across disciplines and new courses in actinide chemistry). The most significant impact of this award has been in encouraging interdisciplinary education and research. The proposal was initiated by a joint effort between Nuclear Engineering and Chemistry, but also included faculty in biochemistry, radiology, and molecular biology. Specific outcomes of the REAP grant thus far are: (1) increased educational and research capabilities in actinide chemistry (faculty hire and equipment acquisition); (2) increased integration of biochemistry and radiochemistry (e.g., radiochemical analysis of uranium speciation in biological systems); (3) stronger interdisciplinary integration of molecular biology and radiochemical sciences (alpha-emitters for treating cancer); (4) new and more extensive interactions with national laboratory facilities (e.g., student internships at LANL and LLBL, faculty and lab scientist exchange visits, analytical measurements and collaboration with the Advanced Photon Source), and (7) new research funding opportunities based on REAP partnership. (author)

  9. Polylinear regression analysis in radiochemistry

    International Nuclear Information System (INIS)

    Kopyrin, A.A.; Terent'eva, T.N.; Khramov, N.N.

    1995-01-01

    A number of radiochemical problems have been formulated in the framework of polylinear regression analysis, which permits the use of conventional mathematical methods for their solution. The authors have considered features of the use of polylinear regression analysis for estimating the contributions of various sources to the atmospheric pollution, for studying irradiated nuclear fuel, for estimating concentrations from spectral data, for measuring neutron fields of a nuclear reactor, for estimating crystal lattice parameters from X-ray diffraction patterns, for interpreting data of X-ray fluorescence analysis, for estimating complex formation constants, and for analyzing results of radiometric measurements. The problem of estimating the target parameters can be incorrect at certain properties of the system under study. The authors showed the possibility of regularization by adding a fictitious set of data open-quotes obtainedclose quotes from the orthogonal design. To estimate only a part of the parameters under consideration, the authors used incomplete rank models. In this case, it is necessary to take into account the possibility of confounding estimates. An algorithm for evaluating the degree of confounding is presented which is realized using standard software or regression analysis

  10. KfK Institute for Radiochemistry. Progress report on research and development activities in 1990

    International Nuclear Information System (INIS)

    1991-03-01

    The activities undertaken by the Institue of Radiochemistry (IRCH) in 1990 under the following projects are presented: (1) Pollutant control in the environment (water and soil, systems analysis and environmental engineering; (2) nuclear fusion (blanket development, tritium technology); (3) radioactive waste management (basic works on reprocessing technologies, waste products, and ultimate storage facilities); (4) microtechnology (chemical microsensor development, and (5) other research projects (institute-related non-sponsored research). In the annex the publications by the IRCH staff are listed. (BBR) [de

  11. KfK Institute for Radiochemistry. Progress report on research and development activities in 1991

    International Nuclear Information System (INIS)

    1992-03-01

    The activities undertaken by the Institute of Radiochemistry (IRCH) in 1991 under the following projects are presented: (1) Pollutant control in the environment (water and soil, systems analysis and environmental engineering; (2) nuclear fusion (blanket development, tritium technology); (3) radioactive waste management (basic works on reprocessing technologies, waste products, and ultimate storage facilities); (4) microtechnology (chemical microsensor development, and (5) other research projects (institute-related non-sponsored research). In the annex the publications by the IRCH staff are listed. (orig.) [de

  12. Radiochemistry Division annual progress report for 1976

    International Nuclear Information System (INIS)

    Iyer, R.H.

    1978-01-01

    An account of the work done in the Radiochemistry Division of the Bhabha Atomic Research Centre, Bombay, during the calendar year 1976 is given. Some of the major highlights are: (1) development of a technique LEADTRAP using lead as a tracer for determination of total uranium and plutonium in the accountability tank in the fuel reprocessing plants, (2) fabrication of a compact unit of each gamma absorptiometer, the acidity monitor and the calorimeter for in-line monitoring of fuel reprocessing streams, (3) design and fabrication of an annular neutron counter, and (4) participation in the international intercomparison experiments PAFEX-II for the determination of plutonium in dissolver solutions and the processing of Ge(Li) gamma spectra, both organised by the IAEA. (M.G.B.)

  13. Radiochemistry Division annual progress report: 1988

    International Nuclear Information System (INIS)

    1990-01-01

    The report covers the research and development (R and D) work carried out by Radiochemistry Division, Bhabha Atomic Research Centre, Bombay during the period 1987-1988. The R and D work is reported in the form of individual summari es grouped under the headings: (1)Actinide Chemistry, (2)Nuclear Chemistry, and (3)Spectroscopy. Some of the highlights of the work are studies on : (a)solvent extraction and complexation behaviour of actinides, (b)helium ion induced fission of 238 U and 165 Ho and fission yield of 252 Cf(sf), (c)separation of rare earths from fission products, (d)positron annihilation spectroscopy of high Tc superconductors, and (e)EPR spectroscopy of high Tc superconductors. Radioanalytical services and radiation sources given to the other Divisions and Organisations are listed. A list of publications and symposia papers by scientists of the Division is also given. 45 figs., 49 tabs

  14. Radiochemistry Division annual progress report for 1973

    International Nuclear Information System (INIS)

    Iyer, R.H.; Natarajan, P.R.

    1975-01-01

    The R and D work carried out in the Radiochemistry Division of the Bhabha Atomic Research Centre, Bombay, during 1973 is reported under the following topical headings : process chemistry (of transuranic elements), radioanalytical chemistry and services, chemical quality control of Pu fuels, heavy element chemistry, nuclear chemistry and instrumentation. The major highlights are : preparation of 238 Pu, non-destructive estimation of Pu by X-ray fluorescence and gamma counting, determining impurities in trace amounts in uranium and plutonium fuels, determination of solubility of PuF 3 in molten fluoride mixtures as a part of the chemical development programme for the molten salt reactor concept, studies on correlation between average total kinetic energy, fission asymmetry and shell structure. (M.G.B.)

  15. Radiochemistry programme : biennial progress report (1988 - 1989)

    International Nuclear Information System (INIS)

    1991-01-01

    The Research and Development activities of the Radiochemistry Division of Indira Gandhi Centre for Atomic Research, Kalpakkam during the period 1988-89 are desribed in the form of summaries. The main thrust of R and D activities is on fast breeder reactor technology. The summarises are arranged under the headings : (1) Chemistry of Liquid Alkali Metals, (2) High Temperature Chemistry of Advanced Materials, (3) Chemistry of Nuclear Fuel Reprocessing, (4) Post-Irradiation analysis and Nuclear Chemistry, (5) Analytical Characterisation of Materials, (6) Analytical Services and (7) Instrumentation and Mechanical Services. At the end, a list of publications by scientists of the Division published during the report period is given. The list includes papers published in journals, papers presented at various symposia, conferences etc, and technical reports. (author). tabs., figs

  16. Application of strong phosphoric acid to radiochemistry

    International Nuclear Information System (INIS)

    Terada, Kikuo

    1977-01-01

    Not only inorganic and organic compounds but also natural substrances, such as accumulations in soil, are completely decomposed and distilled by heating with strong phosphoric acid for 30 to 50 minutes. As applications of strong phosphoric acid to radiochemistry, determination of uranium and boron by use of solubilization effect of this substance, titration of uranyl ion by use of sulfuric iron (II) contained in this substance, application to tracer experiment, and determination of radioactive ruthenium in environmental samples are reviewed. Strong phosphoric acid is also applied to activation analysis, for example, determination of N in pyrographite with iodate potassium-strong phosphoric acid method, separation of Os and Ru with sulfuric cerium (IV) - strong phosphoric acid method or potassium dechromate-strong phosphoric acid method, analysis of Se, As and Sb rocks and accumulations with ammonium bromide, sodium chloride and sodium bromide-strong phosphoric acid method. (Kanao, N.)

  17. Radiochemistry Division annual progress report for 1982

    International Nuclear Information System (INIS)

    Bhargava, V.K.; Rao, V.K.

    1984-01-01

    The progress report of the Radiochemistry Division of the Bhabha Atomic Research Centre, Bombay, presents the research and development work carried out during 1982 in the form of individual summaries arranged under the headings: reactor fuel chemistry, heavy element chemistry, radioanalytical chemistry, and nuclear chemistry. Some of the highlights of the R and D activities are: (1) optimisation of the chemical parameters for the preparation of UO 2 microspheres by internal gelation method, (2) synergetic extraction studies of various actinides from aqueous solutions, (3) development of methods of determination of uranium, 241 Am and 239 Pu, (4) fission studies of 232 Th, 236 U, 252 Cf and 229 Th, (5) determination of half-life of 241 Pu by various methods. A list of publications of the members of the Division published during 1982 is also given. (M.G.B.)

  18. Radiochemistry Division annual progress report : 1990

    International Nuclear Information System (INIS)

    Iyer, R.H.

    1992-01-01

    This progress report provides an account of the research and development activities of the Radiochemistry Division during the year 1990 in the areas of nuclear chemistry, actinide chemistry and spectroscopy. The main area of work in nuclear chemistry is centered around the fission process induced by reactor neutrons, and light and heavy ions on actinides and low Z (Z<80) elements. Actinide chemistry research is concerned mostly with extraction, complexation and separation of actinide ions from aqueous media using a variety of organic reagents under different experimental conditions. Spectroscopic studies include development and optimisation of chemical/analytical methods for separation and determination of trace metallic impurities and rare earths in fuel materials and EPR and microwave studies on several compounds to understand their superconducting, structural and magnetic properties. A list of publications by the scientific staff of the Division during 1990 is also given in the report. (author). 45 figs., 44 tabs

  19. Ethanolic carbon-11 chemistry: The introduction of green radiochemistry

    International Nuclear Information System (INIS)

    Shao, Xia; Fawaz, Maria V.; Jang, Keunsam; Scott, Peter J.H.

    2014-01-01

    The principles of green chemistry have been applied to a radiochemistry setting. Eleven carbon-11 labeled radiopharmaceuticals have been prepared using ethanol as the only organic solvent throughout the entire manufacturing process. The removal of all other organic solvents from the process simplifies production and quality control (QC) testing, moving our PET Center towards the first example of a green radiochemistry laboratory. All radiopharmaceutical doses prepared are suitable for clinical use. - Highlights: • We report application of the principles of green chemistry to a radiochemistry setting. • Radiopharmaceuticals are prepared using ethanol as the only organic solvent. • Green radiochemistry simplifies production and QC in busy clinical production laboratories. • Residual solvent analysis can be relegated to a quarterly or annual QC test

  20. Nuclear and radiochemistry in China. Present status and future perspectives

    International Nuclear Information System (INIS)

    Shi, W.Q.; Zhao, Y.L.; Chai, Z.F.

    2012-01-01

    Nuclear and radiochemistry is one of the frontier areas of chemistry with high impact on national security, energy supply, scientific advances, social and economic development. Nuclear and radiochemistry in China is now experiencing a renaissance, which is being strongly motivated by China's huge demand for nuclear energy. With this in review, the progress in nuclear and radiochemistry of China is selectively addressed. Some hot topics have been summarized and the main research results achieved by Chinese scientists in this field are highlighted, with emphasis on the basic nuclear chemistry, actinide and trans-actinide chemistry, chemistry of spent nuclear fuel reprocessing, radioanalytical chemistry, environmental radiochemistry and radiopharmaceutical chemistry, etc. Some measures about how to promote the radiochemical education and research in China are suggested, and future perspectives are briefly outlined as well. (orig.)

  1. 7th Nuclear Chemistry, Radiochemistry and Radiation Chemistry Symposium

    International Nuclear Information System (INIS)

    1988-07-01

    The conference heard a total of 58 papers of which 56 were incorporated in INIS, namely those dealing with radioimmunoassay, radiation shielding materials, and radiochemistry of technetium, iodine, uranium, rare earths and actinides. (MR)

  2. Institutional results of the Argentine Graduate Programme in Radiochemistry

    International Nuclear Information System (INIS)

    Cohen, I.M.

    2006-01-01

    The evolution of radiochemistry at the National Atomic Energy Commission (CNEA) in Argentina is analyzed. The antecedents of the establishment, in 1998, of the Master Programme in Radiochemistry, jointly organized by CNEA and the Buenos Aires Regional Faculty of the National Technological University are revised, and the structure of the Programme is described. On the basis of the thesis works, the initial trends are discussed. Finally, the institutional results of the Programme are described. (author)

  3. Radiochemistry Division annual progress report: 1993

    International Nuclear Information System (INIS)

    Natarajan, V.; Godbole, S.V.; Iyer, R.H.

    1995-01-01

    The research and development activities of the Radiochemistry Division of BARC during the year 1993 are briefly described under the headings: (i) nuclear chemistry; (ii) actinide chemistry; (iii) spectroscopy and (iv) instrumentation. Nuclear chemistry work deals with areas of nuclear reactions, nuclear fission, nuclear spectroscopy, nuclear data measurements and synthesis of transplutonium isotopes. The research programme in actinide chemistry deals mainly with the complexation of actinides, lanthanides and fission products from aqueous media with organic reagents such as amides, diamides, CMPO, crown ethers and macrocyclic ligands. Spectroscopic studies include electron paramagnetic resonance and optical investigations to probe phase transitions in actinide and other compounds, investigation of role of radiation induced radical ions in the thermoluminescence of actinide doped phosphors, photoacoustic spectra of uranium compounds and development of analytical methods for the determination of silver and rare earths from uranium and thorium oxide matrices. The instrumentation group has developed electronic circuitry and software support for installing a pilot plant for the preparation of dry gel microspheres of UO 2 and (U, Pu)O 2 . A list of publications by the scientific staff of the Division is also included. (author). refs., 38 figs., 26 tabs

  4. Radiochemistry Division annual progress report: 1994

    International Nuclear Information System (INIS)

    Babu, Y.; Seshagiri, T.K.; Iyer, R.H.

    1996-01-01

    The research and development activities of Radiochemistry Division during 1994 are briefly described under the headings: (i) nuclear chemistry; (ii) actinide chemistry; (iii) spectroscopy and (iv) instrumentation. Nuclear chemistry work deals with the areas of nuclear reactions, nuclear fission, nuclear spectroscopy, nuclear data measurements, neutron activation analysis and positron annihilation spectroscopy. The research programme in actinide chemistry deals mainly with the complexation of the actinides, lanthanides and fission products from aqueous media with organic reagents such as amides, diamides, HTTA, CMPO, BEHSO and macrocyclic ligands. Spectroscopic studies include electron paramagnetic resonance investigations of actinide and other compounds, investigation of role of radiation induced radical ions in the thermoluminescence of actinide/lanthanide doped phosphors and development of analytical methods for the determination of metallic impurities in plutonium, uranium, thorium oxide and yttrium aluminium garnet matrices. A sinusoidal waveform generator for facilitating electrochemical etching of nuclear tracks and an IBM PC/AT based data station for the IR spectrophotometer were developed by the instrumentation group. A list of publications, numbering 107, by the Scientific staff of the Division is also included in the report. (author). refs., 32 tabs., 31 figs

  5. Annual Report 2010. Institute of Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Bernhard, G. (ed.)

    2011-10-26

    The Institute of Radiochemistry is one of the six research institutes of the Helmholtz center Dresden-Rossendorf. The report covers contributions in two parts. Part 1; long-lived radionuclides in biosystems: Several contributions concern the determination of formation and structures of various uranium, americium, and curium complexes with relevant organic and inorganic ligands. First results about the dependency of uranium(VI) complexation with small organic ligands at elevated temperatures were achieved. New insights in the mechanisms of luminescence quenching of uranyl complexes by density functional theory calculations are reported. Bacteria, algae, and fungi can influence the mobilization or immobilization of heavy metals in water and soils. Part II: long-lived radionuclides at permanent disposal sites. Several contributions report research on the behavior of biofilms in uranium contaminated sites. To describe the aqueous transport of actinides and other long-lived radionuclides the dominating processes on the liquid/solid interfaces must be considered. Interesting results about the sorption and surface complexation of different metals (long-lived radionuclides) during interaction with various mineral surfaces, and colloids were achieved. Substantial progress was made on knowledge about the visualization and quantification of fluid flow in salt rock formations by using positron emission tomography.

  6. Radiochemistry Division: annual progress report for 1980

    International Nuclear Information System (INIS)

    Jayadevan, N.C.; Manohar, S.B.

    1982-01-01

    The research and development (R and D) activities of the Radiochemistry Division of the Bhabha Atomic Research Centre (BARC), Bombay, during 1980 are reported in the form of individual summaries under the headings: reactor chemistry, heavy element chemistry, process chemistry (of actinides), nuclear chemistry and instrumentation. Some of the highlights of the R and D activities are: (1) setting up of the facilities for the prepa.ration of (U,Pu)O 2 microspheres by sot-gel process on laboratory scale, (2) studies on synergistic extraction of Am, Cm, Bk, Cf, Th(IV), Np(IV) and Pu(IV) with mixtures of TTA and oxodonor6s like TBP, (3) kinetics of radiation induced oxidation of Pu(IV) and that of reduction of Pu(VII), (4) determination of fission yields of 138 Xe, 139 Cs, 252 Cf and 229 Th, (5) measuring of gamma ray abundance of 229 Th and isotopic ratios in thorium and plutonium and (6) design and fabrication of an osmistor for the determination of the molecular weight of actinide complexes. A list of papers published in journals and papers presented at conference/symposia during the year is also given. (M.G.B.)

  7. Radiochemistry Division: Annual progress report for 1981

    International Nuclear Information System (INIS)

    Jayadevan, N.C.; Manohar, S.B.

    1983-01-01

    The progress report of the Radiochemistry Division of Bhabha Atomic Research Centre presents the research and development work carried out during 1981 in the form of individual summaries arranged under the headings: reactor fuel chemistry, heavy element chemistry, radioanalytical chemistry, and nuclear chemistry. Some of the highlights of the work are: (1) modification of the gelation set-up for making plutonium containing gel particles to get better yields of (U,Pu)O 2 containing up to 15% of plutonium, (2) studies on solvent extraction of Am(III), Cm(III), Bk(III) and Cf(III) by 1-phenyl-2-methyl-4-benzoyl pyrazolone-5 (HPMBP), (3) study of the radiation chemistry and photochemistry of aqueous solutions of plutonium, (4) study of crystal structure of uranyl oxalate and sulphates, (5) ESR study, thermoluminescence and spectral studies of americium doped SrSO 4 , phosphors, (6) determination of uranium and plutonium by spectrophotometry, mass spectroscopy and alpha spectroscopy, (7) determination of isotopic ratios of plutonium isotopes by gamma spectroscopy, (8) studies on several aspects of fission chemistry of 229 Th and 252 Cf, and (9) fabrication of a neutron well coincidence counter. (M.G.B.)

  8. Century of radiochemistry. History and future

    International Nuclear Information System (INIS)

    Myasoedov, B.F.

    2000-01-01

    Several periods in radiochemistry development history are observed. In the report the sources of radionuclide income into environment are examined including long-lived transuranic elements on the different stages of full nuclear fuel cycle. Radioactive substance contamination analysis is given for different regions of Russia from natural and man-caused sources. Potential danger of long-lived radionuclide and transuranic element presence in the wastes of nuclear fuel cycle plants is shown. Data related with the sequences of nuclear weapon testing on the proving grounds near Semipalatinsk, and Novaya Zemlya are presented. The modern radioecological situation around the reprocessing plant 'Mayak', which was constructed more than 40 years ago for the production of plutonium for military purposes, is overviewed. The following topics are considered: lake Karachay; artificial water reservoirs contaminated by radionuclides; solid radioactive wastes and their vitrification. Some new approaches, methods and tools developed at the Vernadsky Institute of Russian Academy of Sciences for determination of different radionuclides in various environmental samples from the impact zone of the facility are discussed. The data on distribution, occurrence forms and migration processes of 90 Sr, 137 Cs, 237 Np, 239 Pu, and 241 Am in aquatic and terrestrial ecosystems are presented. (author)

  9. Radiochemistry course in the undergraduate nuclear science program at Universiti Kebangsaan Malaysia

    International Nuclear Information System (INIS)

    Sarmani, S.B.; Yahaya, R.B.; Yasir, M.S.; Majid, A.Ab.; Khoo, K.S.; Rahman, I.A.; Mohamed, F.

    2015-01-01

    Universiti Kebangsaan Malaysia offered an undergraduate degree program in Nuclear Science since 1980 and the programme has undergone several modifications due to changes in national policy and priority. The programme covers nuclear sub-disciplines such as nuclear physics, radiobiology, radiochemistry, radiation chemistry and radiation safety. The radiochemistry component consists of radiochemistry, chemistry in nuclear industry, radiochemical analysis laboratory, radiopharmaceutical chemistry subjects and mini research project in radiochemistry. (author)

  10. The Nuclear and Radiochemistry in Chemistry Education Curriculum Project

    International Nuclear Information System (INIS)

    Robertson, J.D.; Missouri University, Columbia, MO; Kleppinger, E.W.

    2005-01-01

    Given the mismatch between supply of and demand for nuclear scientists, education in nuclear and radiochemistry has become a serious concern. The Nuclear and Radiochemistry in Chemistry Education (NRIChEd) Curriculum Project was undertaken to reintroduce the topics normally covered in a one-semester radiochemistry course into the traditional courses of a four-year chemistry major: general chemistry, organic chemistry, quantitative and instrumental analysis, and physical chemistry. NRIChEd uses a three-pronged approach that incorporates radiochemistry topics when related topics in the basic courses are covered, presents special topics of general interest as a vehicle for teaching nuclear and radiochemistry alongside traditional chemistry, and incorporates the use of non-licensed amounts of radioactive substances in demonstrations and student laboratory experiments. This approach seeks not only to reestablish nuclear science in the chemistry curriculum, but to use it as a tool for elucidating fundamental and applied aspects of chemistry as well. Moreover, because of its relevance in many academic areas, nuclear science enriches the chemistry curriculum by encouraging interdisciplinary thinking and problem solving. (author)

  11. Integrated research training program of excellence in radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Lapi, Suzanne [Washington Univ., St. Louis, MO (United States)

    2015-09-18

    The overall goal of this “Integrated Research Training Program of Excellence in Radiochemistry” is to provide a rich and deep research experience in state-of-the-art radiochemistry and in the fundamentals of radioisotopic labeling and tracer methodology to develop researchers who are capable of meeting the challenges of designing and preparing radiotracers of broad applicability for monitoring and imaging diverse biological systems and environmental processes. This program was based in the Departments of Radiology and Radiation Oncology at Washington University Medical School and the Department of Chemistry at the University of Illinois at Urbana Champaign, and it was initially directed by Professor Michael J. Welch as Principal Investigator. After his passing in 2012, the program was led by Professor Suzanne E. Lapi. Programmatic content and participant progress was overseen by an Internal Advisory Committee of senior investigators consisting of the PIs, Professor Mach from the Department of Radiology at Washington University and Professor John A. Katzenellenbogen of the Department of Chemistry at the University of Illinois. A small External Advisory Committee to give overall program guidance was also constituted of experts in radiolabeled compounds and in their applications in environmental and plant science.

  12. Radiochemistry Division : annual progress report for 1978

    International Nuclear Information System (INIS)

    Subramanian, M.S.; Satya Prakash

    1981-01-01

    The research and development (R and D) activities of the Radiochemistry Division of the Bhabha Atomic Research Centre (BARC), Bombay, during 1978 are reported in the form of individual summaries under the headings: reactor chemistry, heavy element chemistry, process chemistry, radioanalytical chemistry and services, nuclear chemistry, and instrumentation. Some of the highlights of the R and D activities are: (1) preparation of microspheres of uranium oxide and uranium-thorium oxides by sol-gel process, (2) study of vaporization thermodynamics of Th and U by transpiration and boiling techniques, (3) preparation and characterisation of uranium(III) sulphates and double sulphates by X-ray, thermal and infra-red analysis, (4) extraction of trivalent actinides and lanthanides by long chain amines from chloride solutions, (5) study of radiation chemical behaviour of U(VI) in hydrochloric acid and sulphuric acid media, (6) purification and concentration of neptunium by the primary and secondary amines, (7) development of gamma spectroscopic method for determination of isotopic composition of plutonium using low energy gamma rays of plutonium isotopes, (8) standardisation of method of determination of isotopic abundances of uranium at nanogram level by thermal ionisation mass spectroscopy, (9) extraction photometric determination of Pu(IV) and Np(IV) present in mixtures, (10) study of various aspects of nuclear fission such as charge distribution, mass distribution and fragment angular momentum in low energy fission of actinides, and (11) fabrication of: (a) spark counting unit for counting fission tracks in their plastic films, (b) autoranging alpha monitor to be used with fractionating column, (c) remote pipetter for use in hot cells and (d) a thermoluminescence unit for glovebox operation. (M.G.B.)

  13. The Crisis in Radiochemistry and Nuclear Chemistry Education

    International Nuclear Information System (INIS)

    Hoffman, D C

    2005-01-01

    A brief summary of the current status of radiochemistry and nuclear chemistry in the U. S. and abroad will be given. Current and future needs for scientists in these fields, especially in the U. S., will be discussed. Challenges that must be met in order to reverse the ''catastrophic'' downward trend in the numbers of students, faculty, and university programs in radiochemistry and nuclear chemistry will be considered, and some potential ways to reinvigorate and expand relevant university research and educational programs will be suggested

  14. The Texas A&M Radioisotope Production and Radiochemistry Program

    Energy Technology Data Exchange (ETDEWEB)

    Akabani, Gamal [Texas A & M Univ., College Station, TX (United States)

    2016-08-31

    The main motivation of the project at Texas A&M University was to carry out the production of critically needed radioisotopes used in medicine for diagnostic and therapy, and to establish an academic program in radionuclide production and separation methods. After a lengthy battle with the Texas A&M University Radiation Safety Office, the Texas Department of State Health Services granted us a license for the production of radionuclides in July 2015, allowing us to work in earnest in our project objectives. Experiments began immediately after licensing, and we started the assembly and testing of our target systems. There were four analytical/theoretical projects and two experimental target systems. These were for At-211 production and for Zn- 62/Cu-62 production. The theoretical projects were related to the production of Mo-99/Tc-99m using (a) a subcritical aqueous target system and (b) production of Tc-99m from accelerator-generated Mo-99 utilizing a photon-neutron interaction with enriched Mo-100 targets. The two experimental projects were the development of targetry systems and production of At-211 and Zn-62/Cu-62 generator. The targetry system for At-211 has been tested and production of At-211 is chronic depending of availability of beam time at the cyclotron. The installation and testing of the targetry system for the production of Zn-62/Cu-62 has not been finalized. A description of the systems is described. The academic program in radionuclide production and separation methods was initiated in the fall of 2011; due to the lack of a radiochemistry laboratory, it was suspended. We expect to re-start the academic program at the Texas A&M Institute for Preclinical Studies under the Molecular Imaging Program.

  15. The Texas A&M Radioisotope Production and Radiochemistry Program

    International Nuclear Information System (INIS)

    Akabani, Gamal

    2016-01-01

    The main motivation of the project at Texas A&M University was to carry out the production of critically needed radioisotopes used in medicine for diagnostics and therapy, and to establish an academic program in radionuclide production and separation methods. After a lengthy battle with the Texas A&M University Radiation Safety Office, the Texas Department of State Health Services granted us a license for the production of radionuclides in July 2015, allowing us to work in earnest in our project objectives. Experiments began immediately after licensing, and we started the assembly and testing of our target systems. There were four analytical/theoretical projects and two experimental target systems. These were for At-211 production and for Zn-62/Cu-62 production. The theoretical projects were related to the production of Mo-99/Tc-99m using a) a subcritical aqueous target system and b) production of Tc-99m from accelerator-generated Mo-99 utilizing a photon-neutron interaction with enriched Mo-100 targets. The two experimental projects were the development of targetry systems and production of At-211 and Zn-62/Cu-62 generator. The targetry system for At-211 has been tested and production of At-211 is chronic depending of availability of beam time at the cyclotron. The installation and testing of the targetry system for the production of Zn-62/Cu-62 has not been finalized. A description of the systems is described. The academic program in radionuclide production and separation methods was initiated in the fall of 2011 and, due to the lack of a radiochemistry laboratory, it was suspended. We expect to re-start the academic program at the Texas A&M Institute for Preclinical Studies under the Molecular Imaging Program.

  16. The Texas A&M Radioisotope Production and Radiochemistry Program

    International Nuclear Information System (INIS)

    Akabani, Gamal

    2016-01-01

    The main motivation of the project at Texas A&M University was to carry out the production of critically needed radioisotopes used in medicine for diagnostic and therapy, and to establish an academic program in radionuclide production and separation methods. After a lengthy battle with the Texas A&M University Radiation Safety Office, the Texas Department of State Health Services granted us a license for the production of radionuclides in July 2015, allowing us to work in earnest in our project objectives. Experiments began immediately after licensing, and we started the assembly and testing of our target systems. There were four analytical/theoretical projects and two experimental target systems. These were for At-211 production and for Zn- 62/Cu-62 production. The theoretical projects were related to the production of Mo-99/Tc-99m using (a) a subcritical aqueous target system and (b) production of Tc-99m from accelerator-generated Mo-99 utilizing a photon-neutron interaction with enriched Mo-100 targets. The two experimental projects were the development of targetry systems and production of At-211 and Zn-62/Cu-62 generator. The targetry system for At-211 has been tested and production of At-211 is chronic depending of availability of beam time at the cyclotron. The installation and testing of the targetry system for the production of Zn-62/Cu-62 has not been finalized. A description of the systems is described. The academic program in radionuclide production and separation methods was initiated in the fall of 2011; due to the lack of a radiochemistry laboratory, it was suspended. We expect to re-start the academic program at the Texas A&M Institute for Preclinical Studies under the Molecular Imaging Program.

  17. The Texas A&M Radioisotope Production and Radiochemistry Program

    Energy Technology Data Exchange (ETDEWEB)

    Akabani, Gamal [Texas A & M Univ., College Station, TX (United States). Dept. of Nuclear Engineering. Dept. of Veterinary Integrative Biosciences

    2016-10-28

    The main motivation of the project at Texas A&M University was to carry out the production of critically needed radioisotopes used in medicine for diagnostics and therapy, and to establish an academic program in radionuclide production and separation methods. After a lengthy battle with the Texas A&M University Radiation Safety Office, the Texas Department of State Health Services granted us a license for the production of radionuclides in July 2015, allowing us to work in earnest in our project objectives. Experiments began immediately after licensing, and we started the assembly and testing of our target systems. There were four analytical/theoretical projects and two experimental target systems. These were for At-211 production and for Zn-62/Cu-62 production. The theoretical projects were related to the production of Mo-99/Tc-99m using a) a subcritical aqueous target system and b) production of Tc-99m from accelerator-generated Mo-99 utilizing a photon-neutron interaction with enriched Mo-100 targets. The two experimental projects were the development of targetry systems and production of At-211 and Zn-62/Cu-62 generator. The targetry system for At-211 has been tested and production of At-211 is chronic depending of availability of beam time at the cyclotron. The installation and testing of the targetry system for the production of Zn-62/Cu-62 has not been finalized. A description of the systems is described. The academic program in radionuclide production and separation methods was initiated in the fall of 2011 and, due to the lack of a radiochemistry laboratory, it was suspended. We expect to re-start the academic program at the Texas A&M Institute for Preclinical Studies under the Molecular Imaging Program.

  18. The modern trends in radiochemistry and their applications

    International Nuclear Information System (INIS)

    Cohen, I.M.; Furnari, J.C.

    2012-01-01

    The utilization of Radiochemistry and Nuclear Chemistry is described, particularly with respect to nuclear analytical techniques and radioisotope applications in several fields. Especially, and in connections with the recent advances of Nuclear Medicine, the present contributions of Radiopharmacy, linked to both diagnostic and therapeutic methods, are outlined. The modern trends and their future are discussed. (authors). [es

  19. 5. National Conference on Radiochemistry and Nuclear Chemistry. Abstracts

    International Nuclear Information System (INIS)

    Fuks, L.

    2009-01-01

    Held in Krakow-Przegorzaly (24-27 May 2009) 5. National Conference on Radiochemistry and Nuclear Chemistry focused on the following research topics: (a) radioanalytical methods; (b) environmental studies; (c) radiopharmacy; (d) isotopic effects; (e) nuclear safety. Participants presented 6 plenary lectures, 24 communications and 38 posters

  20. Some aspects of research relevant to environment radiochemistry

    International Nuclear Information System (INIS)

    Chen Shi; Ma Mingxie

    1997-01-01

    The authors suggest some research aspects relevant to environmental radiochemistry from the view point of environmental protection and radiation protection: the migration behavior of radionuclides, their interaction with environment medium and their speciation in environment. The status and prospect of these aspects and the relationship between them are discussed

  1. A web-based course in nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Landsberger, S.; Plionis, A.

    2009-01-01

    Over the last six years through a Department of Energy Radiochemistry Education Award Program (REAP) we have developed a completely webbased course in nuclear and radiochemistry given at the University of Texas at Austin. This course has had nuclear and radiation engineering and chemistry graduate students. While the course also has an extensive laboratory component only the lectures are web based. The lectures begin with a historical introduction of radiochemistry followed by two movies on Madame Curie. This is followed by the usual lectures on radioactivity, fundamental properties, radioactive decay, decay modes, and nuclear reactions. As section on radioactive waste management and nuclear fuel cycle is also presented. Lectures in neutron activation analysis, geo- and cosmochemistry, and plutonium chemistry have also been developed. All lectures are in power point with many animations and a significant number of solved problems. All students are required to make a short oral presentation on some aspect of nuclear and radiochemistry in their research or a chosen topic. (author)

  2. Quality assurance in radiochemistry - a report from practice

    International Nuclear Information System (INIS)

    Kopka, K.; Burkert, D.; Wagner, S.; Kriens, M.; Schober, O.

    2005-01-01

    The Department of Nuclear Medicine in Muenster has been certified since January 17 th 2003 by external auditing according to DIN EN ISO 9001:2000. The compliance with EN ISO 9001:2000 was approved by the European Association of Nuclear Medicine (EANM) in August 2003. To date, the certificate assignment (No. 2384D) to the nuclear medicinal facilities of the University Hospital in Muenster (UKM) is unique in Germany particularly because the certification not only covers the diagnostic and therapeutical scope of the Department of Nuclear Medicine but also for the first time contains the in-house-production of radionuclides and radiopharmaceuticals including radioactive waste disposal. Consequently, the routine duties and responsibilities of a section radiochemistry which is imbedded in a clinical organisation have been standardised and well documented for the first time according to DIN EN ISO 9001:2000. The operational procedures for radiopharmaceutical chemistry are documented in the work areas 'conventional' radiochemistry laboratory (radionuclide laboratory) as well as modern production facility for PET radiochemistry. The implementation of standard operational procedures (SOPs) cause an increase of efficiency in a radiochemistry task group with two graduate radiopharmaceutical chemists and two well-trained technical/laboratory assistants. (orig.)

  3. Determination Performance Of Gamma Spectrometry Co-Axial HPGE Detector In Radiochemistry And Environment Group, Nuclear Malaysia

    International Nuclear Information System (INIS)

    Mei-Woo, Y.

    2014-01-01

    Gamma Spectrometry System is used to measure qualitatively and quantitatively a gamma emitting radionuclide. The accuracy of the measurement very much depends on the performance specifications of the HPGe detectors. From this study it found that all the seven co-axial HPGe detectors in Radiochemistry and Environment Group, Nuclear Malaysia are in good working conditions base on the verification of performance specifications namely Resolution, Peak Shape, Peak-to-Compton ratio and Relative Efficiency against the warranted value from the manufacturers. (author)

  4. Abstracts Book of 3. All-Polish Conference on Radiochemistry and Nuclear Chemistry

    International Nuclear Information System (INIS)

    2001-01-01

    The development of radiochemistry and nuclear chemistry in Poland have been presented during the 3. All-Polish Conference on Radiochemistry and Nuclear Chemistry held in Kazimierz Dolny in May 2001. The broad range of problems connected with radiochemistry and nuclear chemistry application in environmental protection and quality control, nuclear medicine and radiation protection, radioactive waste processing and many other scientific and everyday problems solution have been extensively presented and discussed

  5. Proceedings of 26. annual academic conference of China Chemical Society--modern nuclear chemistry and radiochemistry

    International Nuclear Information System (INIS)

    2008-08-01

    26. annual academic conference of China Chemical Society was held in Tianjing, 13-16 July, 2008. This proceedings is about modern nuclear chemistry and radiochemistry, the contents include: new elements and new nuclides; advanced nuclear chemistry; radiochemistry and national security; new radiopharmaceutical chemistry; modern radiological analytical chemistry and large scientific facilities; radiological environmental chemistry and nuclear radioactive waste; actinide chemistry and transactinide chemistry; radiochemistry and cross discipline, etc.

  6. Facilitating the design and operation of radiochemistry autosynthesizers

    International Nuclear Information System (INIS)

    Feliu, A.L.

    1990-01-01

    Both research and routine medical applications of positron emission tomography critically depend on rapid and reliable radiopharmaceutical syntheses. This work describes new computer techniques for controlling automated synthesizers, which feature: a graphical interface for easy operation, software reconfiguration without reprogramming to accommodate changes in chemistry, and both remote and unattended control modes. These concepts were implemented in a simple yet powerful program, PREPARE, which controls a commercially-built radiochemistry synthesizer, and in a fully-functional simulation, AUTOMATE, which explores synthesizer multitasking given a single PC. Unlike most black box and robotic approaches to radiochemistry synthesis which are highly chemistry- and hardware-specific, PREPARE and AUTOMATE have been designed as generic programs, supporting a palette of basic devices (valves, stepper motors, etc.)

  7. Practicum of applied radioactivity and radiochemistry by Herforth and Koch

    International Nuclear Information System (INIS)

    Herforth, L.; Huebner, K.

    1989-01-01

    The more-than-thirty-year history of a textbook of the application of radionuclides is described. In many countries the book has been proved useful for teaching specialists in the field of isotope technique. Above this it is accepted as a compendium for uses of radiophysical and radiochemical methods in science and industry. For 1991 a new, completely revised edition is planned entitled HERFORTH/KOCH Praktikum der angewandten Radioaktivitaet und Radiochemie (HERFORTH/KOCH Practicum of Applied Radioactivity and Radiochemistry). (author)

  8. Forschungszentrum Rossendorf, Institute of Radiochemistry. Annual report 2001

    International Nuclear Information System (INIS)

    Fanghaenel, T.; Bernhard, G.; Engelmann, H.J.

    2002-05-01

    The Institute of Radiochemistry (IRC), one of the five institutes of the Forschungszentrum Rossendorf (FZR) performs basic and applied research in the fields of radiochemistry and radioecology. Main goal is the quantification of the interaction and mobility of radionuclides in the geo- and biosphere. Because of their high radiotoxicity and long half-life the actinides are of special interest. Among the actinides uranium and its manifold interactions plays a major role in the institute's research activities. In addition the interactions of some important long-lived fission and decay products are studied. More than 60 scientists, technicians and PhD students are employed in the Institute of Radiochemistry. The research is focused on understanding the fundamental processes relevant for the behavior of radionuclides in the environment. Main topics are: Aquatic chemistry, Radionuclide interaction with mineral surfaces, Radionuclide interaction with biological materials (bacteria and plants), Modeling the radionuclide transport, Development of spectroscopic speciation methods We accomplished many new scientific results in the past year, which are presented in this Annual Report. (orig.)

  9. Radiochemistry programme biennial progress report (1986 and 1987)

    International Nuclear Information System (INIS)

    1988-01-01

    This biennial report covers the calendar years 1986 and 1987. This period has seen significant growth in the research activities of the Radiochemistry Programme and this is reflected in this report. The report is organised subject-wise into sections dealing with Fuel Chemistry and Thermodynamics, Sodium Chemistry, Analytical Chemistry and Instrumentation. The major part of the activities of the Radiochemistry Programme relates to fuel chemistry including thermophysical and thermodynamic properties of fuel materials, chemistry of fuel reprocessing and facilities as well as techniques for post-irradiation studies. Sodium chemistry is a smaller but important R and D activity, which has reached full maturity during the period of this report. Analytical chemistry and instrumentation are essential supporting activities. The rapid progress made over the last two years are reflected in the number of items covered in this report. In order to keep the total length of this report under control, the editors had to restrict the individual activities to one or two pages. Though the details of various studies are not presented here, it is hoped that the report gives an overview of the progress made by the Radiochemistry Programme in the last two years. The list of publications given at the end also reflects the growth in research programmes. (author)

  10. Development of an interdisciplinary curriculum in radiochemistry at the university of Iowa

    Energy Technology Data Exchange (ETDEWEB)

    Schultz, M.K. [Department of Radiology and Radiation Oncology, Carver College of Medicine, The University of Iowa, 500 Newton Road, MLB180, Iowa City, IA 52240 (United States); De Vries, D.J. [Radiation and Isotopes for Health, Radiation, Radionuclides and Reactors, Technische Universitite Delft, Delft (Netherlands); Forbes, T.Z. [Department of Chemistry, College of Liberal Arts and Sciences, The University of Iowa, CB W374, Iowa City, IA 52242 (United States)

    2013-07-01

    An interdisciplinary curriculum in radiochemistry is under development at the University of Iowa. The program represents a collaboration between the Departments of Radiology and Chemistry with strong support from the College of Medicine and the College of Liberal Arts and Sciences. The University has undertaken this venture in response to a national and international need for professionals with skills and knowledge of nuclear chemistry and radiochemistry. Students enrolling in this program will benefit from a diverse spectrum of extramurally-funded projects for which radiochemistry is a cornerstone of research and development. Recently, a symposium was conducted at the University of Iowa to determine the undergraduate educational foundation that will produce desirable personnel for the diverse sectors related to radiochemistry. Professionals and researchers from around the United States were invited to contribute their perspectives on aspects of radiochemistry that would be important to include in the undergraduate program. Here, we present a brief communication of the draft curriculum, which is based on our understanding of the current need for radio-chemists and nuclear chemists across disciplines and is informed by our communications with participants in the radiochemistry symposium. Recurring themes, which were stressed by participants, included the need for the development of specialized hands-on open-source laboratory training, internship opportunities, and the inclusion of inexpensive-simple radiochemistry laboratory modules that could be included in early analytical laboratory instruction to attract students to the study of radiochemistry and nuclear chemistry. (authors)

  11. Development of an interdisciplinary curriculum in radiochemistry at the university of Iowa

    International Nuclear Information System (INIS)

    Schultz, M.K.; De Vries, D.J.; Forbes, T.Z.

    2013-01-01

    An interdisciplinary curriculum in radiochemistry is under development at the University of Iowa. The program represents a collaboration between the Departments of Radiology and Chemistry with strong support from the College of Medicine and the College of Liberal Arts and Sciences. The University has undertaken this venture in response to a national and international need for professionals with skills and knowledge of nuclear chemistry and radiochemistry. Students enrolling in this program will benefit from a diverse spectrum of extramurally-funded projects for which radiochemistry is a cornerstone of research and development. Recently, a symposium was conducted at the University of Iowa to determine the undergraduate educational foundation that will produce desirable personnel for the diverse sectors related to radiochemistry. Professionals and researchers from around the United States were invited to contribute their perspectives on aspects of radiochemistry that would be important to include in the undergraduate program. Here, we present a brief communication of the draft curriculum, which is based on our understanding of the current need for radio-chemists and nuclear chemists across disciplines and is informed by our communications with participants in the radiochemistry symposium. Recurring themes, which were stressed by participants, included the need for the development of specialized hands-on open-source laboratory training, internship opportunities, and the inclusion of inexpensive-simple radiochemistry laboratory modules that could be included in early analytical laboratory instruction to attract students to the study of radiochemistry and nuclear chemistry. (authors)

  12. Radiochemistry in India. A saga of five decades

    International Nuclear Information System (INIS)

    Manchanda, V.K.; Sungkyunkwan Univ., Suwon

    2012-01-01

    Radiochemistry in India essentially blossomed under the auspices of the Department of Atomic Energy (DAE) for the last 55 years or so. Major activities in this area are centred at Bhabha Atomic Research Centre, Mumbai (BARC) and Indira Gandhi Centre for Atomic Research, Kalpakkam (IGCAR). Though there were several centers of excellence which were established by renowned radiochemists during the 1960s at the academic institutions in different parts of the country and nurtured by their close associates during the eighties and nineties, their glamour did not last long and only very few have sustained the challenges presented by social and technological upheaval of last five decades. Board of Research in Nuclear Sciences (BRNS), an organ of DAE has been in the forefront for promotion of education and research in nuclear sciences at academic institutions. It sponsors symposia in Nuclear and Radiochemistry (NUCAR), Nuclear Analytical Chemistry (NAC) and Applications of Radioisotopes in Chemistry, Environment and Biology (ARCEB) which are organized periodically to provide a platform for interaction of the radiochemists within and outside DAE. A professional body, viz. Indian Association of Nuclear Chemists and Allied Scientists (IANCAS), formed in early eighties at BARC, Mumbai has been spearheading the campaign to popularize the subject of radiochemistry in schools and colleges through workshops and publishing monographs and thematic bulletins regularly in the area of interest to the radiochemists. During the last five decades, radiochemistry programme at BARC has centered around attaining excellence in basic research utilizing radiations and radioisotopes to unravel various nuclear and chemical phenomena, related to actinides and fission products. This programme encompassed a number of research and development areas such as nuclear fission, nuclear reactions, nuclear probes for materials study, nuclear and chemical properties of actinides, actinide spectroscopy

  13. Application of the principle of supramolecular chemistry in the fields of radiochemistry and radiation chemistry

    International Nuclear Information System (INIS)

    Shen Xinghai; Chen Qingde; Gao Hongcheng

    2008-01-01

    Supramolecular chemistry, one of the front fields in chemistry, is defined as 'chemistry beyond the molecule', bearing on the organized entities of higher complexity that result from the association of two or more chemical species held together by intermolecular forces. This article focuses on the application of the principle of supramolecular chemistry in the fields of radiochemistry and radiation chemistry. The following aspects are concerned: (1) the recent progress of supramolecular chemistry; (2) the application of the principle of supramolecular chemistry and the functions of supramolecular system, i.e., recognition, assembly and translocation, in the extraction of nuclides; (3) the application of microemulsion, ionic imprinted polymers, ionic liquids and cloud point extraction in the enrichment of nuclides; (4) the radiation effect of supramolecular systems. (authors)

  14. Educational experiments of radiochemistry in the nuclear engineering school

    International Nuclear Information System (INIS)

    Akatsu, Eiko

    1995-06-01

    Educational experiments of radiochemistry are described. They were an improvement of educational experiment of burn-up measurement as well as experiments on a solvent extraction, a cation exchange behavior of 60 Co, liquid scintillation spectrometry and half-life determination of 87 Rb, and determination of 137 Cs in sea water. Two or one of the experiments were ordinarily studied, depending the occasional situations, by the students of the general course or of the nuclear engineering course in the Nuclear Engineering School, Nuclear Education Center, JAERI from 1976 to 1994. (author)

  15. University-level education in nuclear and radiochemistry in Slovenia

    International Nuclear Information System (INIS)

    Smodis, B.

    2006-01-01

    The status of education in nuclear and radiochemistry in Slovenia is reviewed and elucidated at both undergraduate and graduate levels. It is observed that both the quantity and the quality of studies have deteriorated during recent years/decades, thus following similar trends in the developed countries. Presently, no dedicated study of radioactivity is offered within the country. The main reason for this deterioration is a general decline of interest for studying nuclear sciences and the limited need for such specialization in a small country such as Slovenia. (author)

  16. Incorporating nuclear and radiochemistry in the traditional undergraduate chemistry program

    International Nuclear Information System (INIS)

    Robertson, J.D.; Kleppinger, E.W.

    1994-01-01

    Although many areas of major national need depend critically on professionals trained in nuclear and radiochemistry, there has been a steady decline in both the educational opportunities and student interest in this area. One major factor that has contributed greatly to the lack of student interest in nuclear and radiochemistry is that most undergraduate students in chemistry and other sciences are no longer introduced to these topics. This deficiency in the traditional chemistry curriculum, coupled with the negative public perception towards all things open-quotes nuclear,close quotes has resulted in a serious shortage of individuals with a background in this area. The authors are trying to address this problem by open-quotes educating the educators.close quotes The authors are developing a set of summer workshops to provide faculty from four-year colleges with the curriculum materials, training, and motivation to incorporate these topics on a continuing basis in their traditional undergraduate chemistry curricula. The first series of workshops is scheduled for the summer of 1995

  17. Web-based radiochemistry training at the University of Texas at Austin

    International Nuclear Information System (INIS)

    Landsberger, S.; Strassberg, E.; Schnmidt, K.

    2005-01-01

    Outline of a comprehensive website based offering of a basic graduate level or senior undergraduate level course in nuclear and radiochemistry is presented. This password protected course follows classical pedagogical treatment of the subject. However, it has been augmented by the implementation of Flash animations to better teach basic nuclear and radiochemistry concepts. As well, the website is linked to many Internet related resources. All lectures and problems are presented in Microsoft Power Point format with Flash animations incorporated. A series of six experiments in radiochemistry, also offered in the course is available in a downloadable Microsoft Word format. (author)

  18. Application of power ultrasound in radiochemistry

    International Nuclear Information System (INIS)

    Moisy, Ph.; Venault, L.; Blanc, P.; Madic, C.; Nikitenko, S.

    1998-01-01

    The chemical effects of ultrasound are related to cavitation process: nucleation, bubble growth and cavitation collapse. Sono-chemical reactions occur due to the rapid heating of the contents of cavitation bubbles. The shock-waves generated by cavitation collapse cause intense emulsification of the immiscible liquids. The CEA/Marcoule research group investigated the effect of power ultrasound on the homogeneous and heterogeneous (liquid-liquid) actinide reactions, in aqueous nitric acid media. It was found that U(IV), Np(V) and Pu(III) can be rapidly oxidized in HNO 3 solutions by HNO 2 , generated by the effect of power ultrasound on HNO 3 solutions. HNO 2 , formed during HNO 3 sono-lysis, decomposes hydrazinium nitrate within the cavitation bubbles. This makes it possible to the control actinide oxidation states without adding any side chemical reagents (NaNO 2 , for example). The quantitative data on the effect in the ultrasonic field in nitric acid medium are discussed, and sono-chemical mechanisms are proposed for nitrous acid formation and hydrazinium nitrate decomposition. In the presence of anti-nitrous reagents, such as hydrazinium nitrate and sulfamic acid, U(IV) was found to be oxidized and Pu(IV) reduced by H 2 O 2 formed as the result of aqueous nitric acid sono-lysis. The kinetics of H 2 O 2 formation is faster than in water, for the same sono-chemical conditions. Np(V) is rapidly oxidized, by aqueous phase HNO 2 , under the effect of ultrasound on the two-phase system TBP-dodecane/HNO 3 . Intense emulsification of the liquid/liquid system accelerates the mass transfer, of Np(VI) formed, into the organic phase. The quantitative effect of power ultrasound in aqueous nitric acid, with or without anti-nitrous reagents, can be used to predict the behavior of actinides in the ultrasonic field in nitric acid medium. (author)

  19. Radioactive wastes management in a radiochemistry laboratory

    International Nuclear Information System (INIS)

    Silva, Ana C.A.; Pereira, Wagner de S; Py Junior, Delcy de A.; Antunes, Ivan M.; Kelecom, Alphonse

    2009-01-01

    The Laboratorio de Monitoracao Ambiental (AMB) of the Unidade de Tratamento de Minerio (UTM) belonging to the Industrias Nucleares do Brasil is a chemical, radiochemical and radiometric laboratory, that analyses the natural radionuclides present in samples coming from the various installation of Industrias Nucleares do Brasil (INB). To minimize the radiological environmental impact, that laboratory has adopted a washing system of the chapel exhausting, that recirculate the washing water. These water can accumulate the radionuclides coming from the samples, that are liberated together the exhaustion gases from the chapels. Also, the water coming from the analyses and the sample releases (environmental and of the process) represent the liquid effluents of the AMB. The release of this effluent must pass by chemical and radiological criteria. From the radiological viewpoint, that release must be based on the Brazilian Nuclear Energy Commission (CNEN) regulations. This work try to establish the monitoring frequency, the radionuclides to be analysed, the form of liberation of those effluents, and the analytical techniques to be used. The radionuclides to be analysed will be U-nat, Ra-226 and Pb-210, of the uranium series, and the Th-232 and Ra-228, of the thorium series. The effluents must be monitored either before the release or, at least, twice a year. The effluents considered radioactive wastes, will be send to waste dam by the radioprotection service, or to the effluent treatment for controlled liberation for the environment

  20. Actinyl chemistry at the Centre for Radiochemistry Research

    International Nuclear Information System (INIS)

    May, Iain; Copping, Roy; Cornet, Stephanie M.; Talbot-Eeckelears, Catherine E.; Gaunt, Andrew J.; John, Gordon H.; Redmond, Mike P.; Sharrad, Clint A.; Sutton, Andrew D.; Collison, David; Fox, O. Danny; Jones, Chris J.; Sarsfield, Mark J.; Taylor, Robin J.

    2007-01-01

    Increasing our basic chemical knowledge of the actinyl cations ({AnO 2 } 2+/+ , where An = U, Np, Pu or Am) is vital for underpinning the development of novel nuclear waste management and nuclear fuel processing technologies, as well as increasing our understanding of actinide behaviour in the environment. Over recent years there have been significant advances made in uranyl, neptunyl and plutonyl chemistry, with the main focus on uranyl. At the Centre for Radiochemistry Research (CRR), University of Manchester, there are ongoing projects investigating the coordination chemistry of the actinyl cations. These projects are undertaken at the CRR and at higher specific activity alpha facilities accessed through Nexia Solutions and the EU ACTINET programme, as well as concomitant computational chemistry projects at University College London. Recent discoveries have included the complexation of transuranic actinyl cations with tri-lacunary heteropolytungstate ligands and spectroscopic and structural evidence for the direct coordination of the pertechnetate anion to {UO 2 } 2+

  1. Application of thin-layer chromatography in radiochemistry

    International Nuclear Information System (INIS)

    Maki, Yasuyuki; Murakami, Yukio.

    1976-01-01

    In relation to the experimental procedures of thin-layer chromatography (TLC) in radiochemistry, the authors explained the preparation and development of radioactive test solutions, the methods of detection by autoradiography of isolated spots and by the calculation of measuring apparatus, and the identification of isolated spots. Next they outlined the carrier-free isolation and purification of nuclides, the quantification in combination with γ-ray spectrum, confirmation of the purity of RI-labeled medical supplies, their application to RI generator, thin-layer electrophoresis, in which electrophoresis and TLC were combined, and the application of this electrophoresis to isolation in recoil chemistry and to analysis and identification in carrier-free chemistry. (Kanao, K.)

  2. Topics in nuclear and radiochemistry for college curricula and high school science programs

    Energy Technology Data Exchange (ETDEWEB)

    1990-01-01

    The concern with the current status and trends of nuclear chemistry and radiochemistry education in academic institutions was addressed in a recent workshop. The 1988 workshop considered the important contributions that scientist with nuclear and radiochemistry backgrounds have made and are continuing to make to other sciences and to various applied fields. Among the areas discussed were environmental studies, life sciences, materials science, separation technology, hot atom chemistry, cosmochemistry, and the rapidly growing field of nuclear medicine. It is intent of the organizer and participants of this symposium entitled Topics in Nuclear and Radiochemistry for College Curricula and High School Science Program'' to provide lecture material on topics related to nuclear and radiochemistry to educators. It is our hope that teachers, who may or may not be familiar with the field, will find this collections of articles useful and incorporate some of them into their lectures.

  3. A century of radiochemistry. Its growth and development as a unique scientific discipline

    International Nuclear Information System (INIS)

    Jervis, R.E.

    1999-01-01

    In recognition of the 1997 anniversary of the first century of radiochemistry, a review is made of its unique contribution to the emergence of nuclear science, its development from the use of very basic chemical techniques initially to a battery of more sophisticated procedures, and its changing role as it has become widely applied in many fields of science. Synergistically, these fields have been able to develop with the aid of radiochemistry while at the same time, radiochemical methods developed to meet the demands of such applications, Among these, during the second half of the century, has been radiochemistry applied to quantitative chemical analysis: RAA or, nuclear analytical chemistry, and typical examples of its use in the authors' laboratory are described, including some recent INAA results on development of novel 'activable' tracer coding for forensic use with specialized and high security materials. The specific contributions, during the century, of Japanese pioneers in radiochemistry are also cited. (author)

  4. Challenges and Opportunities in Nuclear Science and Radiochemistry Education at the University of Missouri

    International Nuclear Information System (INIS)

    Robertson, J. David; Etter, Randy L.; Neumeyer, Gayla M.; Miller, William H.

    2009-01-01

    Over the last thirty years, numerous reports and workshops have documented the decline in nuclear and radiochemistry education programs in the United States. Practitioners and stakeholders are keenly aware of the impact this decline will have on emerging technologies and critical research and are fully committed to rebuilding programs in nuclear and radiochemistry. The challenge is, however, to persuade our academic peers and administrations to invest in nuclear and radiochemistry education and training programs in view of multiple competing priorities. This paper provides an overview of the expansion of the radiochemistry program and the creation of the Nuclear Energy Technology Workforce (NETWork) Center at the University of Missouri, Columbia and the lessons learned along the way.

  5. Topics in nuclear and radiochemistry for college curricula and high school science programs

    International Nuclear Information System (INIS)

    1990-01-01

    The concern with the current status and trends of nuclear chemistry and radiochemistry education in academic institutions was addressed in a recent workshop. The 1988 workshop considered the important contributions that scientist with nuclear and radiochemistry backgrounds have made and are continuing to make to other sciences and to various applied fields. Among the areas discussed were environmental studies, life sciences, materials science, separation technology, hot atom chemistry, cosmochemistry, and the rapidly growing field of nuclear medicine. It is intent of the organizer and participants of this symposium entitled ''Topics in Nuclear and Radiochemistry for College Curricula and High School Science Program'' to provide lecture material on topics related to nuclear and radiochemistry to educators. It is our hope that teachers, who may or may not be familiar with the field, will find this collections of articles useful and incorporate some of them into their lectures

  6. Flow injection analysis: Emerging tool for laboratory automation in radiochemistry

    International Nuclear Information System (INIS)

    Egorov, O.; Ruzicka, J.; Grate, J.W.; Janata, J.

    1996-01-01

    Automation of routine and serial assays is a common practice of modern analytical laboratory, while it is virtually nonexistent in the field of radiochemistry. Flow injection analysis (FIA) is a general solution handling methodology that has been extensively used for automation of routine assays in many areas of analytical chemistry. Reproducible automated solution handling and on-line separation capabilities are among several distinctive features that make FI a very promising, yet under utilized tool for automation in analytical radiochemistry. The potential of the technique is demonstrated through the development of an automated 90 Sr analyzer and its application in the analysis of tank waste samples from the Hanford site. Sequential injection (SI), the latest generation of FIA, is used to rapidly separate 90 Sr from interfering radionuclides and deliver separated Sr zone to a flow-through liquid scintillation detector. The separation is performed on a mini column containing Sr-specific sorbent extraction material, which selectively retains Sr under acidic conditions. The 90 Sr is eluted with water, mixed with scintillation cocktail, and sent through the flow cell of a flow through counter, where 90 Sr radioactivity is detected as a transient signal. Both peak area and peak height can be used for quantification of sample radioactivity. Alternatively, stopped flow detection can be performed to improve detection precision for low activity samples. The authors current research activities are focused on expansion of radiochemical applications of FIA methodology, with an ultimate goal of creating a set of automated methods that will cover the basic needs of radiochemical analysis at the Hanford site. The results of preliminary experiments indicate that FIA is a highly suitable technique for the automation of chemically more challenging separations, such as separation of actinide elements

  7. ROBL - a CRG beamline for radiochemistry and materials research at the ESRF

    International Nuclear Information System (INIS)

    Matz, W.; Schell, N.; Bernhard, G.; Claussner, J.; Oehme, W.; Prokert, F.; Reich, T.; Schlenk, R.; Proehl, D.; Funke, H.; Eichhorn, F.; Betzl, M.; Dienel, S.; Brendler, V.; Denecke, M.A.; Krug, H.; Neumann, W.; Huettig, G.; Reichel, P.; Strauch, U.

    1999-04-01

    The paper describes the Rossendorf Beamline (ROBL) built by the Forschungszentrum Rossendorf at th ESRF. ROBL comprises two different and independently operating experimental stations: a radiochemistry laboratory for X-ray absorption spectroscopy of non-sealed radioactive samples and a general purpose materials research station for X-ray diffraction and reflectometry mainly of thin films and interfaces modified by ion beam techniques. The radiochemistry set-up is worldwide a unique installation at a modern synchrotron radiation source. (orig.) [de

  8. Radiochemistry methods in DOE methods for evaluating environmental and waste management samples

    International Nuclear Information System (INIS)

    Fadeff, S.K.; Goheen, S.C.

    1994-08-01

    Current standard sources of radiochemistry methods are often inappropriate for use in evaluating US Department of Energy environmental and waste management (DOE/EW) samples. Examples of current sources include EPA, ASTM, Standard Methods for the Examination of Water and Wastewater and HASL-300. Applicability of these methods is limited to specific matrices (usually water), radiation levels (usually environmental levels), and analytes (limited number). Radiochemistry methods in DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) attempt to fill the applicability gap that exists between standard methods and those needed for DOE/EM activities. The Radiochemistry chapter in DOE Methods includes an ''analysis and reporting'' guidance section as well as radiochemistry methods. A basis for identifying the DOE/EM radiochemistry needs is discussed. Within this needs framework, the applicability of standard methods and targeted new methods is identified. Sources of new methods (consolidated methods from DOE laboratories and submissions from individuals) and the methods review process will be discussed. The processes involved in generating consolidated methods add editing individually submitted methods will be compared. DOE Methods is a living document and continues to expand by adding various kinds of methods. Radiochemistry methods are highlighted in this paper. DOE Methods is intended to be a resource for methods applicable to DOE/EM problems. Although it is intended to support DOE, the guidance and methods are not necessarily exclusive to DOE. The document is available at no cost through the Laboratory Management Division of DOE, Office of Technology Development

  9. Program and curriculum development in radiochemistry at Washington State University to educate the next generation of radiochemists in the US

    International Nuclear Information System (INIS)

    Clark, S.B.; Nash, K.; Benny, P.; Elliston, J.; Buckely, P.

    2005-01-01

    Washington State University (WSU) has -been the recipient of grant funds from the U.S. Department of Energy's Office of Nuclear Science and Technology to enhance its curriculum and service activities in radiochemistry. These funds have been used to hire new faculty, redesign undergraduate and graduate courses in radiochemistry, and initiate summer programs in radiochemistry for regional college faculty and high school teachers. The funds received from the federal government were matched by investments from the state of Washington. These investments have resulted in many positive changes in the Chemistry Department and the Nuclear Radiation Center at WSU. The number of students graduating from our radiochemistry programs has increased markedly, and the level of additional extra mural funding for our programs has also increased. These activities will be described, and feedback from employers of our radiochemistry graduates will be provided. Plans for future radiochemistry program development will also be discussed.

  10. Accurate monitoring developed by EDF for FA-3-EPRTM and UK-EPRTM: chemistry-radiochemistry design and procedures

    International Nuclear Information System (INIS)

    Tigeras, Arancha; Bouhrizi, Sofia; Pierre, Marine; L'Orphelin, Jean-Matthieu

    2012-09-01

    The monitoring of chemistry and radiochemistry parameters is a fundamental need in nuclear power plants in order to ensure: - The reactivity control in real time, - The barrier integrity surveillance by means of the fuel cladding failures detection and the primary-pressure boundary components control, - The water quality to limit the radiation build-up and the material corrosion permitting to prepare the maintenance, radioprotection and waste operations. - The efficiency of treatment systems and hence the minimization of chemical and radiochemical substances discharges The relevant chemistry and radiochemistry parameters to be monitored are selected depending on the chemistry conditioning of systems, the source term evaluations, the corrosion mechanisms and the radioactivity consequences. In spite of the difficulties for obtaining representative samples under all circumstances, the EPR M design provides the appropriate provisions and analytical procedures for ensuring the reliable and accurate monitoring of parameters in compliance with the specification requirements. The design solutions, adopted for Flamanville 3-EPR M and UK-EPR M , concerning the sampling conditions and locations, the on-line and analytical equipment, the procedures and the results transmission to control room and chemistry laboratory are supported by ALARP considerations, international experience and researches concerning the nuclides behavior (corrosion product and actinides solubility, fission product degassing, impurities and additives reactions also). This paper details the means developed by EDF for making successful and meaningful sampling and measurements to achieve the essential objectives associated with the monitoring. (authors)

  11. Radiochemistry Division: triennial progress report (for) 1983-1985

    International Nuclear Information System (INIS)

    Datta, T.

    1987-01-01

    The present report includes contributions pertaining to the studies of nuclear and chemical properties of actinides. These studies have been mostly concerned with the basic investigation, besides the research and development work connected with chemical quality control of plutonium-based fuels for trace metallic constituents. The nuclear properties are being studied in the Nuclear Chemistry and Instrumentation Section while the chemical properties are being studied in the Actinide Chemistry Section and the Spectroscopy Section. The work in the Actinide Chemistry Section deals essentially with properties of ions in solutions and preparation of solid compounds, to understand the complexing behaviour of actinides. The work in the Spectroscopy Section is concerned essentially with the study of actinide solids using EPR, TSL and optical spectroscopic techniques. The considerable advances made in the basic study of actinides are reflected in the number of publications in well-known international journals. The research and development work of the Division is fully supported by Instrumentation Group of the Division which looks after the maintenance of instruments of not only the Radiochemistry Division but also the Fuel Chemistry Division and design and fabrication of special electronic instruments needed for the research and development work. (author)

  12. Nuclear and radiochemistry research: from development to deployment

    International Nuclear Information System (INIS)

    Tomar, B.S.

    2015-01-01

    Fundamental research in nuclear and radiochemistry is essential in building the expertise in quality assurance and quality control (QA/QC) of nuclear materials, which in turn is important for harnessing nuclear energy for peaceful purposes. Expansion of nuclear fuel cycle activities throws several new challenges before the nuclear scientists with regard to the chemical quality control, quality assurance, accounting of special nuclear materials, improving the detection limits of the trace elements, etc. Nondestructive assay (NDA) of nuclear materials is important from the point of view of nuclear material accounting and control. The requirement of QA/QC of finished products as well as accounting of special nuclear materials in waste packets can be met through NDA techniques. For this purpose passive gamma and neutron based techniques are employed for Pu based materials. On the other hand, NDA of uranium based fuels need active interrogation methods for quantitative assay in sealed packets, while isotopic composition can be measured using high resolution gamma ray spectrometry in suitable gamma energy region. Some of the other elements, such as, boron in finished products can be assayed using ion beam analysis techniques, such as proton induced gamma emission (PIGE) employing low energy proton beams. In the present talk, a few examples of such challenges and their possible solutions would be discussed. (author)

  13. Biennial report of Radiochemistry Division 1997-1998

    International Nuclear Information System (INIS)

    Sastry, M.D.; Manchanda, V.K.; Ramaswami, A.; Goswami, A.; Manohar, S.B.

    2000-03-01

    This report describes the work carried by Radiochemistry Division of BARC during the period 1997 and 1998. The work is divided in three main branches (1) Nuclear Chemistry (2) Actinides Chemistry (3) Actinide Spectroscopy. During this period research in nuclear chemistry was focussed on nuclear fission, nuclear reactions, neutron activation analysis, use of nuclear techniques for understanding of physico-chemical phenomena and developmental activities in non-destructive assay techniques. The research work on chemistry of actinides was directed on basic as well as applied studies related to complexation and extraction behaviour of actinides and lanthanides with a variety of novel ligands. The choice of complexing ligands was made with a view to examining the suitability in reprocessing streams, treatment of high level active waste and recovery of valuables. The third part spectroscopy of actinides describes the basic studies solid state spectroscopy of actinides and analytical spectroscopy for trace metallic assay. The solid state spectroscopy investigations were carried out using EPR, ENDOR, fluorescence, thermally stimulated luminescence and photo acoustic for spectroscopy techniques. In the analytical spectroscopy work a lot of stress was given on finding suitable chemical separation procedures for pre concentration of trace metals and a determination by ICP-AES/ETA-AAS techniques. (author)

  14. Cooperation in education and training in nuclear- and radiochemistry in Europe

    International Nuclear Information System (INIS)

    John, J.; Čuba, V.; Němec, M.

    2014-01-01

    In this paper, the motivation, history and status of coordination of education and training in nuclear- and radiochemistry in Europe will be reviewed and correlated to similar activities in other nuclear fields such as the nuclear engineering of radiological protection. The achievements of the Euratom FP7 project 'Cooperation In education in Nuclear CHemistry (CINCH)' will be described in detail. This description will cover both the status review and the development activities of this collaboration. In the status review field, the results of a detailed survey of the universities and curricula in nuclear- and radiochemistry in Europe and Russia will be presented. In the development activities field, the main achievements of the CINCH project will be presented. They are particularly the NukWik - an open platform for collaboration and sharing teaching materials in nuclear- and radiochemistry based on a wiki engine

  15. Facilitating the design and operation of computer-controlled radiochemistry synthesizers with an open-quotes Electronic Toolboxclose quotes

    International Nuclear Information System (INIS)

    Feliu, A.L.

    1991-01-01

    Positron emission tomography (PET) is a non-invasive diagnostic imaging technique requiring rapid and reliable radiopharmaceutical production. Automated systems offer a host of potential advantages over manually or remotely operated apparatus, including reduced personnel requirements, lower radiation exposure to personel, reliable yields, and reproducible product purity. However, the burden of routine radiopharmaceutical production most often remains a labor-intensive responsibility of highly trained radiochemists. In order to ease the transition between manual, remote-controlled, and computer-controlled radiochemical synthesis, an electronic toolbox with graphical user interface was developed as a generic process control system compatible with a variety of common radiochemical operations. This work is specifically aimed to make automated techniques more accessible by emphasizing the similarities between manual and automated chemistry and by minimizing the computer programming effort required. This paper discusses the structural elements of the electronic toolbox approach to radiochemistry process control, and its ramifications for the designers and end-users of automated synthesizers

  16. Cooperation in education and training in nuclear- and radiochemistry in Europe

    International Nuclear Information System (INIS)

    Jan John; Jukka Lehto; Teija Koivula; Jon Petter Omtvedt

    2015-01-01

    The motivation, history and status of coordination of education and training in nuclear- and radiochemistry in Europe are reviewed. The achievements of the Euratom FP7 project 'Cooperation In education in Nuclear CHemistry (CINCH)' are described. Attention is paid to the results of the survey of universities teaching nuclear chemistry and their respective curricula evaluation, to the plan to introduce the EuroMaster in nuclear- and radiochemistry quality label recognized and guaranteed by the European Association for Chemical and Molecular Sciences (EuCheMS), and to CINCH NucWik - an interactive database proposed and implemented as an open structure in the form of a 'Wiki'. (author)

  17. Utilizations of intense pulsed neutron source in radiochemistry and radiation chemistry

    International Nuclear Information System (INIS)

    Shiokawa, Takanobu; Yoshihara, Kenji; Kaji, Harumi; Kusaka, Yuzuru; Tabata, Yoneho.

    1975-01-01

    Intense pulsed neutron sources is expected to supply more useful and fundamental informations in radiochemistry and radiation chemistry. Short-lived intermediate species may be detected and the mechanisms of radiation induced reactions will be elucidated more precisely. Analytical application of pulsed neutrons is also very useful. (auth.)

  18. Training Grant in Radiochemistry and Radiotracer Development. Design and Synthesis of Molecular and Nanoparticulate Probes

    Energy Technology Data Exchange (ETDEWEB)

    Hanson, Robert N. [Northeastern Univ., Boston, MA (United States)

    2015-01-15

    Original overall objective was to develop a training program within the Department of Chemistry and Chemical Biology that would provide an experience in radiochemistry. A combination of educational and research experiences would prepare organic chemistry graduate students to enter the field.

  19. Book of Abstracts of IV. All-Polish Conference on Radiochemistry and Nuclear Chemistry

    International Nuclear Information System (INIS)

    2005-01-01

    The different aspects of radiochemistry have been presented and discussed. Especially application of radiochemical methods for preparation of biologically active compounds usable in nuclear medicine and biology as well as for isotope separation and purification have been presented in details. The application of radiochemical methods convenient for environmental monitoring and contamination control have been extensively represented as well

  20. The reestablishment of radiochemistry academic programs in the United States - 59025

    International Nuclear Information System (INIS)

    Williamson, Craig

    2012-01-01

    Document available in abstract form only. Full text of publication follows: Despite its importance in national security, medicine, energy, and in waste management radiochemistry education in the United States has gone through two lost decades. In the 1970's ten to fifteen universities were granting between thirty (30) and forty (40) doctoral degrees a year. By the 1980's those numbers had declined to twenty (20) and thirty (30) a year, by the 1990's the numbers had again decreased to below fifteen (15) Ph.D.s a year. In the year 2000, the data shows that only 5 Ph.D.s in radiochemistry were awarded. The causes for this decline is directly attributed to the lack of federal support for an academic discipline that for the most part depends on federal funding. In 2011, it is expected that over thirty (30) doctoral degrees in radiochemistry will be conferred. The turn around in radiochemistry education in the United States can be directly attributed to the support provided by the U.S. Departments of Energy, Defense and Homeland Security. In addition, support has come from the U.S. Nuclear Regulatory Commission and from the National Nuclear Security Administration. The form of this support has been extensive from proposed undergraduate research programs, scholarships, graduate fellowships, junior faculty awards, curriculum awards, and grants

  1. Radiochemistry methods in DOE Methods for Evaluating Environmental and Waste Management Samples: Addressing new challenges

    International Nuclear Information System (INIS)

    Fadeff, S.K.; Goheen, S.C.; Riley, R.G.

    1994-01-01

    Radiochemistry methods in Department of Energy Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) add to the repertoire of other standard methods in support of U.S. Department of Energy environmental restoration and waste management (DOE/EM) radiochemical characterization activities. Current standard sources of radiochemistry methods are not always applicable for evaluating DOE/EM samples. Examples of current sources include those provided by the US Environmental Protection Agency, the American Society for Testing and Materials, Standard Methods for the Examination of Water and Wastewater, and Environmental Measurements Laboratory Procedures Manual (HASL-300). The applicability of these methods is generally limited to specific matrices (usually water), low-level radioactive samples, and a limited number of analytes. DOE Methods complements these current standard methods by addressing the complexities of EM characterization needs. The process for determining DOE/EM radiochemistry characterization needs is discussed. In this context of DOE/EM needs, the applicability of other sources of standard radiochemistry methods is defined, and gaps in methodology are identified. Current methods in DOE Methods and the EM characterization needs they address are discussed. Sources of new methods and the methods incorporation process are discussed. The means for individuals to participate in (1) identification of DOE/EM needs, (2) the methods incorporation process, and (3) submission of new methods are identified

  2. Avoiding shortage of radio-chemists with the NAMP radiochemistry webinars

    International Nuclear Information System (INIS)

    Paviet-Hartmann, P.; Akbarzadeh, M.; Griggs, J.

    2013-01-01

    The U.S. Department of Energy originally created the National Analytical Management Program (NAMP) to help coordinate its analytical capabilities and to address national needs in technology and resources. In support of this mission, the NAMP established a subcommittee to promote training and education in radiochemistry to avert the predicted loss in expertise. In cooperation with the U.S. Environmental Protection Agency and university partners, the NAMP developed a series of two-hour webinar presentations by experts on different topics relevant to radiochemistry. These webinars are intended to be of interest to those already in the workforce who may need a refresher course or a better understanding of specific radiochemistry topics. The live webinars include slides presentation, and engage the attendees by giving them the opportunity to ask questions during the live event through the web-cast interface. Certificates may be given for attendance during the live webinar. The success of these webinars relies not only on the presenters who are internationally recognized experts but also on how we promote them: we advertised them through a dedicated web site, social networks or flyers. Another important point is that they are free are accessible online in 2 formats: audio-video recording and pdf files. Recorded and archived versions comprise a library vital to future generations of radio-chemists and scientists interested in radiochemistry. The first webinar, An Overview of Actinide Chemistry, was presented on April 20, 2012. The overwhelmingly positive feedback from participants clearly demonstrates that the NAMP webinars are making a difference by providing unique educational opportunities in radiochemistry

  3. Avoiding shortage of radio-chemists with the NAMP radiochemistry webinars

    Energy Technology Data Exchange (ETDEWEB)

    Paviet-Hartmann, P. [Idaho National Laboratory, 995 University Blvd, Idaho Falls, ID 83402 (United States); Akbarzadeh, M. [Nuclear Waste Partnership, LLC, 1400 university Dr, Carlsbad, NM 88220 (United States); Griggs, J. [US Environmental Protection Agency, NAREL, 540 S. Morris Ave, Montgomery, AL 36115-2601 (United States)

    2013-07-01

    The U.S. Department of Energy originally created the National Analytical Management Program (NAMP) to help coordinate its analytical capabilities and to address national needs in technology and resources. In support of this mission, the NAMP established a subcommittee to promote training and education in radiochemistry to avert the predicted loss in expertise. In cooperation with the U.S. Environmental Protection Agency and university partners, the NAMP developed a series of two-hour webinar presentations by experts on different topics relevant to radiochemistry. These webinars are intended to be of interest to those already in the workforce who may need a refresher course or a better understanding of specific radiochemistry topics. The live webinars include slides presentation, and engage the attendees by giving them the opportunity to ask questions during the live event through the web-cast interface. Certificates may be given for attendance during the live webinar. The success of these webinars relies not only on the presenters who are internationally recognized experts but also on how we promote them: we advertised them through a dedicated web site, social networks or flyers. Another important point is that they are free are accessible online in 2 formats: audio-video recording and pdf files. Recorded and archived versions comprise a library vital to future generations of radio-chemists and scientists interested in radiochemistry. The first webinar, An Overview of Actinide Chemistry, was presented on April 20, 2012. The overwhelmingly positive feedback from participants clearly demonstrates that the NAMP webinars are making a difference by providing unique educational opportunities in radiochemistry.

  4. Expedited Synthesis of Fluorine-18 Labeled Phenols. A Missing Link in PET Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Katzenellenbogen, John A. [Univ. of Illinois, Champaign, IL (United States); Zhou, Dong [Washington Univ., St. Louis, MO (United States)

    2015-03-26

    Fluorine-18 (F-18) is arguably the most valuable radionuclide for positron emission tomographic (PET) imaging. However, while there are many methods for labeling small molecules with F-18 at aliphatic positions and on electron-deficient aromatic rings, there are essentially no reliable and practical methods to label electron-rich aromatic rings such as phenols, with F-18 at high specific activity. This is disappointing because fluorine-labeled phenols are found in many drugs; there are also many interesting plant metabolites and hormones that contain either phenols or other electron-rich aromatic systems such as indoles whose metabolism, transport, and distribution would be interesting to study if they could readily be labeled with F-18. Most approaches to label phenols with F-18 involve the labeling of electron-poor precursor arenes by nucleophilic aromatic substitution, followed by subsequent conversion to phenols by oxidation or other multi-step sequences that are often inefficient and time consuming. Thus, the lack of good methods for labeling phenols and other electron-rich aromatics with F-18 at high specific activity represents a significant methodological gap in F-18 radiochemistry that can be considered a “Missing Link in PET Radiochemistry”. The objective of this research project was to develop and optimize a series of unusual synthetic transformations that will enable phenols (and other electron-rich aromatic systems) to be labeled with F-18 at high specific activity, rapidly, reliably, and conveniently, thereby bridging this gap. Through the studies conducted with support of this project, we have substantially advanced synthetic methodology for the preparation of fluorophenols. Our progress is presented in detail in the sections below, and much has been published or presented publication; other components are being prepared for publication. In essence, we have developed a completely new method to prepare o-fluorophenols from non-aromatic precursors

  5. The automated radiosynthesis and purification of the opioid receptor antagonist, [6-O-methyl-11C]diprenorphine on the GE TRACERlab FXFE radiochemistry module.

    Science.gov (United States)

    Fairclough, Michael; Prenant, Christian; Brown, Gavin; McMahon, Adam; Lowe, Jonathan; Jones, Anthony

    2014-05-15

    [6-O-Methyl-(11)C]diprenorphine ([(11)C]diprenorphine) is a positron emission tomography ligand used to probe the endogenous opioid system in vivo. Diprenorphine acts as an antagonist at all of the opioid receptor subtypes, that is, μ (mu), κ (kappa) and δ (delta). The radiosynthesis of [(11)C]diprenorphine using [(11)C]methyl iodide produced via the 'wet' method on a home-built automated radiosynthesis set-up has been described previously. Here, we describe a modified synthetic method to [(11)C]diprenorphine performed using [(11)C]methyl iodide produced via the gas phase method on a GE TRACERlab FXFE radiochemistry module. Also described is the use of [(11)C]methyl triflate as the carbon-11 methylating agent for the [(11)C]diprenorphine syntheses. [(11)C]Diprenorphine was produced to good manufacturing practice standards for use in a clinical setting. In comparison to previously reported [(11)C]diprenorphine radiosyntheisis, the method described herein gives a higher specific activity product which is advantageous for receptor occupancy studies. The radiochemical purity of [(11)C]diprenorphine is similar to what has been reported previously, although the radiochemical yield produced in the method described herein is reduced, an issue that is inherent in the gas phase radiosynthesis of [(11)C]methyl iodide. The yields of [(11)C]diprenorphine are nonetheless sufficient for clinical research applications. Other advantages of the method described herein are an improvement to both reproducibility and reliability of the production as well as simplification of the purification and formulation steps. We suggest that our automated radiochemistry route to [(11)C]diprenorphine should be the method of choice for routine [(11)C]diprenorphine productions for positron emission tomography studies, and the production process could easily be transferred to other radiochemistry modules such as the TRACERlab FX C pro. Copyright © 2014 John Wiley & Sons, Ltd.

  6. The American Chemical Society's Division of Nuclear Chemistry and Technology's summer schools in nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Peterson, J.R.

    1997-01-01

    This successful educational program in nuclear and radiochemistry for advanced undergraduate students is described. Funding from the U.S. Department of Energy supports 24 fellowships for participants in the intensive six-week programs at San Jose State University (CA) and Brookhaven National Laboratory (NY). Students are provided transportation to and from the school site, room and board, books, lab supplies, and six units of college credit. The instructional program consists of lectures and laboratory exercises that cover the fundamentals of nuclear theory, radiochemistry, nuclear instrumentation, radiological safety, and applications in research, medicine, and industry. Guest lectures and field trips broaden the students' exposure to nuclear science. Assistance is provided in the following year to those students who wish to join a research project at a university or national laboratory, and thereafter, in their applications to graduate or professional school. (author)

  7. Support for the American Chemical Society's Summer Schools in Nuclear and Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Mantica, Paul F. [Michigan State University

    2013-06-20

    The ACS Summer Schools in Nuclear and Radiochemistry were held at San Jose State University (SJSU) and Brookhaven National Laboratory (BNL). The Summer Schools offer undergraduate students with U.S. citizenship an opportunity to complete coursework through ACS accredited chemistry degree programs at SJSU or the State University of New York at Stony Brook (SBU). The courses include lecture and laboratory work on the fundamentals and applications of nuclear and radiochemistry. The number of students participating at each site is limited to 12, and the low student-to-instructor ratio is needed due to the intense nature of the six-week program. To broaden the students’ perspectives on nuclear science, prominent research scientists active in nuclear and/or radiochemical research participate in a Guest Lecture Series. Symposia emphasizing environmental chemistry, nuclear medicine, and career opportunities are conducted as a part of the program.

  8. Final report on research and development work 1979 by the Institute for Radiochemistry

    International Nuclear Information System (INIS)

    1980-02-01

    The report gives a brief survey of the state of the research, development, and service activities in the Institute for Radiochemistry in Karlsruhe Nuclear Research Centre. The work is to be classified in the main points analytics, nuclear chemistry, isotope service, and water chemistry, with the analytic and nuclear-chemical tasks being mainly project-related. A bibliography of the publications made by the staff of the institute during 1979 is annected. (RB) [de

  9. Designing flexible, ''chemist-friendly'' software to control a radiochemistry autosynthesizer

    International Nuclear Information System (INIS)

    Feliu, A.L.

    1989-01-01

    To enhance the utility of process control software to control radiochemistry autosynthesizers used with short-lived positron-emitting isotopes, a scheme is proposed by which routine executive-level tasks, hardware control operations, and chemical procedures have been segregated. This strategy can lead to chemist-friendly control programs for any desired hardware configuration, as illustrated in new software designed to exploit the features and flexibility of the CTI/Siemens Chemical Process Control Unit. (author)

  10. Radiochemistry Institute of Karlsruhe Nuclear Research Centre. Progress report on R and D work in 1985

    International Nuclear Information System (INIS)

    1986-02-01

    The Radiochemistry Institute carried out R and D work within the framework of the following projects: Project PWA, Reprocessing and Waste Treatment; project PSB, Fast Breeder Reactor; project PKF, Nuclear Fusion. Basic and applied problems in the field of surface chemistry and surface analysis were studied under the working programme 'Solids and Materials Research', and 'Technology - Man - Environment' was a point of main interest that gathered a number of working programmes in the field of water chemistry. (orig./RB) [de

  11. The 1986-1989 activity report of the Radiochemistry Group of the Orsay IPN

    International Nuclear Information System (INIS)

    Guillaumont, R.

    1989-01-01

    The 1986-1989 activity report of the Radiochemistry Group of the Nuclear Physics Institute (at Orsay), is presented. The research fields purposes and evolution are summarized. The following topics are presented: synthesis and study of pure or doped thorium compounds, high resolution spectroscopy, thermodynamics/kinetics in aqueous solutions, 6d elements, investigations on Ta, Kd, U, UO2 and cold fusion. The presentation of the research team, administrative aspects, publications, conferences and future research programs are also included [fr

  12. The importance of radiochemistry and indicator methods for the chemistry of traces

    International Nuclear Information System (INIS)

    Benes, P.; Majer, V.

    1980-01-01

    Sensitivity is compared for common chemical methods with respect to nonradioactive materials and methods for determining trace amounts of radioactive substances. The concept of trace amounts is explained and some other notions and terms are discussed from the point of view of chemistry and radiochemistry. The problem of radiation effect is briefly assessed on a sample of material containing trace amounts of a radionuclide and the isotopic effect problem in hydrogen is treated. (M.S.)

  13. The radiochemistry, a multi-disciplinary science for the 21. century

    International Nuclear Information System (INIS)

    David, F.

    1999-04-01

    The basic radiochemistry occupies an avant-garde place in inorganic chemistry. It covers a very vast multi-disciplinary field, important for about 40% of the periodic table. It allows understanding better the periodic classification and it is directly connected with various disciplines: metal physical chemistry, solid compounds, solutions, thermodynamics, etc. The applications are also multi-disciplinary, mainly in nuclear industries but also in analysis, geology, biochemistry, medicine, archaeology, astrophysics. This report is a short variant of the document delivered in 1988 for CNRS. It treats neither all the aspects of radiochemistry or the priorities in this field but points out the main directions of this discipline and the fields of research which should be studied in more details. The content is as follows: - Introduction; - I. Definition and radiochemistry's domain of action; - II. The actinides constitute a particularly interesting series of the periodic table; - III. Research on actinides to be developed; III.1 Metals; III.2 Solid compounds; III.3 Gas compounds; III.4 Chemistry in solution (water ions, oxidation degrees, thermodynamic properties, chemical species in solution, non-aqueous media, chemical kinetics, chemistry at the atom scale); IV. Other radioelements; IV.1 The trans-actinide elements; IV.2 The long-lived fission products; V. Radiochemical methods; VI. Study of the 4f and 5f elements is interesting from the point of view of physico-chemical theories; VII. The heavy elements are implied in the nuclear power production; VII.1 Reprocessing the nuclear fuels; VII.2 Waste management; VIII. Conclusions

  14. Abstracts book: asia-pacific symposium on radiochemistry-05 (APSORC-05)

    International Nuclear Information System (INIS)

    2005-01-01

    The third asia-pacific symposium on radiochemistry was held in Beijing, China October 17-21, 2005, the major topics of the symposium are as follows: 1. Nuclear reactions (including fission), nuclear decay/structure, and radioactive isotope beams. 2. Sciences of actinide, heavy and superheavy elements. 3. Nuclear analytical techniques using neutrons, ions, X-rays, synchrotron radiation, etc. 4. Applications of nuclear and radiochemical techniques in life sciences; nanomaterial sciences, environmental sciences, archaeological sciences, geo- and cosmo-sciences, isotopic battery, ect. 5. Nuclear probes in new material sciences: Mossbauer, perturbed angular correlations, positron annihilation, etc. 6. Radiopharmaceutical chemistry (including Tc chemistry) and radioisotope production. 7. Nuclear energy chemistry, including fuel reprocessing, nuclear reactor chemistry, uranium conversion, waste management and disposal, etc. 8. Environmental radiochemistry (including nuclides migration) and radioecology. 9. Radiochemical separation methods and chemical speciation; radiation dosimetry and metrology. 10. Issues on education of nuclear and radiochemistry. Total 312 peer-reviewed abstracts were contained in the abstracts book.

  15. Use of the TRIGA Reactor by the Radiochemistry Group of the Atominstitute of the Austrian Universities

    International Nuclear Information System (INIS)

    Bichler, M.; Buchtela, K.; Grass, F.; Ismail, S.

    1994-01-01

    The Radiochemistry Group of the Atominstitute of the Austrian Universities uses the TRIGA Mark II Reactor mainly for neutron activation analysis. Transport of samples to and from the irradiation positions in the reactor is performed by fast pneumatic transfer systems (transfer time 20 msec and 300 msec) and slow conventional transport facilities. Gamma-spectrometric instrumentation equipped with loss free counting systems is used to handle the high count rates up to 500 000 counts/sec. During the last years neutron activation analysis was applied to investigate environmental samples (soil, dust, incineration ash), geological samples (rocks, sediments, fossils, volcanic gases), biological materials (lichens, mushrooms and other plant materials, human diet, biological reference materials), raw materials (phosphate, coal) and archaeological materials (ancient glass). Lichen analysis was used for environmental monitoring. The content of some of the trace elements can be correlated with industrial activities, like manganese content with steel industry, the occurrence of vanadium and nickel with oil firing plants and stainless steel industry, selenium is found in lichen near coal firing plants. The amount of chlorine and sodium indicates the application of salt for road treatment during winter time, aluminum, scandium and hafnium content depends on the amount of dust in the environment. A further environmental application of neutron activation analysis is the determination of trace elements in volcanic gases. The halogens, arsenic, antimony, selenium, tellurium and mercury were determined and their daily output was calculated. The distribution of trace elements in fossils of known age gives us a geochemical key to condition and development of the paleo-environment. For this purpose we determined rare earth elements in 250 million years old microfossils (conodonts). Neutron activation analysis served also for some non scientific but nevertheless useful purposes: Organic

  16. CINCH-II project. Next step in the coordination of education in nuclear- and radiochemistry in Europe

    International Nuclear Information System (INIS)

    John, Jan; Cuba, Vaclav; Nemec, Mojmir

    2013-01-01

    Any of the potential options for the nuclear power – both the renaissance, if any, or the phase out – will require significant numbers of the respective specialists, amongst others the nuclear and/or radiochemists. In parallel, a significant demand exists for these specialists in non-energy fields, such as environmental protection, radiopharmacy, nuclear medicine, biology, authorities, etc. Since the numbers of staff in teaching and the number of univerzities with facilities licensed for the work with open sources of ionizing radiation has decreased on or sometimes even below the critical level, coordination and collaboration are required to maintain the necessary teaching and training capabilities. The CINCH-II project, aiming at the Coordination of education and training In Nuclear CHemistry in Europe, will be a direct continuation of the CINCH-I project which, among others, identified the EuroMaster in Nuclear Chemistry quality label recognized and guaranteed by the European Chemistry Thematic Network Association as an optimum common mutual recognition system in the field of education in Nuclear Chemistry in Europe, surveyed the status of Nuclear Chemistry in industry / the needs of the end-users, developed an efficient system of education/training compact modular courses, or developed and tested two electronic tools as a basis of a future efficient distance learning system. In the first part of this paper, the achievements of the CINCH-I project will be described. This description will cover both the status review and the development activities of this Collaboration. In the status review field, the results of a detailed survey of the universities and curricula in nuclear- and radiochemistry in Europe and Russia will be presented. Another survey mapped the nuclear- and radiochemistry in industry – specifically the training and education needs of the end users. In the development activities field, the main achievements of the CINCH-project will be presented

  17. Perspectives on teaching nuclear and radiochemistry at the Pennsylvania State University

    International Nuclear Information System (INIS)

    Catchen, G.L.

    1993-01-01

    Some perspectives on teaching the subject of nuclear and radiochemistry are presented in the form of a historical narrative. In addition, a program is briefly reviewed, which was developed approximately in 1985, to enhance learning in a specific course on the subject. This program involved developing illustrations, course notes, and video tutorials evaluating their effectiveness. After having used these aids extensively, their efficacy is commented on. The role of a nuclear science course in a nuclear engineering curriculum is also briefly discussed. (author) 4 refs

  18. Marie Sklodowska-Curie and her contributions to chemistry, radiochemistry and radiotherapy

    International Nuclear Information System (INIS)

    Waclawek, Witold; Waclawek, Maria

    2011-01-01

    In 2009, the prestigious American scientific magazine New Scientist carried out a worldwide poll on the most inspirational woman in science. Mme. Curie received nearly as many as twice the votes cast for the candidate in second place. Given the level of regard for this exceptional woman - the first person to be honored with two Nobel Prizes, initially in physics and later in chemistry, and the first woman to serve as Professor at the University of Paris - this article briefly describes her life and her contributions to chemistry, radiochemistry and radiotherapy. (orig.)

  19. Characterization of past and present waste streams from the 325 Radiochemistry Building

    International Nuclear Information System (INIS)

    Pottmeyer, J.A.; Weyns-Rollosson, M.I.; Dicenso, K.D.; DeLorenzo, D.S.; Duncan, D.R.

    1993-12-01

    The purpose of this report is to characterize, as far as possible, the solid waste generated by the 325 Radiochemistry Building since its construction in 1953. Solid waste as defined in this document is any containerized or self-contained material that has been declared waste. This characterization is of particular interest in the planning of transuranic (TRU) waste retrieval operations including the Waste Receiving and Processing (WRAP) Facility. Westinghouse Hanford Company (Westinghouse Hanford) and Battelle Pacific Northwest Laboratory (PNL) activities at Building 325 have generated approximately 4.4% and 2.4%, respectively, of the total volume of TRU waste currently stored at the Hanford Site

  20. The present status and prospects for the development of radiochemistry and nuclear chemistry in Poland

    International Nuclear Information System (INIS)

    Narbutt, J.; Chmielewski, A.G.

    2001-01-01

    The report deals with a short history, achievements and trends of development of radiochemistry and nuclear chemistry in the world. It also presents the main achievements and short programmes of fundamental and applied research, as well as works on technology, as delivered by more than thirty research institutes and universities in Poland. The related teaching activities of Polish academic centers has been briefly discussed. The documents enclosed [list of publications (1997-2000; list of research groups; list of apparatus] bring a more detailed representation of the Polish research centers' activity in this field. (author)

  1. Preparation of high purity plutonium oxide for radiochemistry instrument calibration standards and working standards

    International Nuclear Information System (INIS)

    Wong, A.S.; Stalnaker, N.D.

    1997-04-01

    Due to the lack of suitable high level National Institute of Standards and Technology (NIST) traceable plutonium solution standards from the NIST or commercial vendors, the CST-8 Radiochemistry team at Los Alamos National Laboratory (LANL) has prepared instrument calibration standards and working standards from a well-characterized plutonium oxide. All the aliquoting steps were performed gravimetrically. When a 241 Am standardized solution obtained from a commercial vendor was compared to these calibration solutions, the results agreed to within 0.04% for the total alpha activity. The aliquots of the plutonium standard solutions and dilutions were sealed in glass ampules for long term storage

  2. The Institute of Radiochemistry, University of Liege, (Sart-Tilman), Belgium

    International Nuclear Information System (INIS)

    Duyckaerts, G.

    1977-01-01

    The Institute of Radiochemistry, erected in the new Sart-Tilman campus of the University of Liege has been especially planned and equipped for research on actinide chemistry. The two-floor building is well adapted for work in glove-boxes and well ventilated hoods with highly radioactive α-emitters. For the last ten years, research has been carried out in the following directions: synthesis and structural analysis of actinide compounds, thermodynamic evaluations on actinide compounds by microcalorimetry, electrochemistry of actinides in fused salts, redox properties of actinides in fused salts by absorption spectrophotometry, solution chemistry of actinides by solvent extraction, ion exchange and electrochemistry. (T.G.)

  3. The Department of Energy/American Chemical Society Summer School in Nuclear and Radiochemistry at San Jose State University

    International Nuclear Information System (INIS)

    Kinard, W.F.; Silber, H.B.

    2005-01-01

    A Summer School in Nuclear Chemistry sponsored by the U. S. Department of Energy and the American Chemical Society has been held at San Jose State University for the past 20 years. The intent of the program is to introduce outstanding college students to the field of nuclear and radiochemistry with the goal that some of these students will consider careers on nuclear science. The program features radiochemistry experiments along with radiation safety training, guest lectures by well known nuclear scientists and field trips to nuclear chemistry facilities in the San Francisco area. (author)

  4. Automating radiochemistry: Considerations for commerical suppliers of devices

    International Nuclear Information System (INIS)

    Schmidt, D.G.

    1993-01-01

    The fundamental decision to automate a particular radiochemical synthesis for in house use depends primarily on the demand for the compound and the total number of studies to be carried out with that compound. For a commercial supplier of automated chemistry systems, much more goes in to the decision to design, develop and produce a particular automated chemistry system. There is a dramatic difference in design effort between an industrial environment and an academic environment. An in house system must be built only once and needs only to incrementally simplify the synthesis process. A commercial product must: have reasonable manufacturing costs; be easy to use; be aesthetically pleasing; be easy to install and service; be functionally integral with other equipment sold by the manufacturer; be marketable within the regulatory environment; address radiation safety issues. This paper discusses issues that guide commercial suppliers in the formation of their product lines

  5. Optimum Condition for Plutonium Electrodeposition Process in Radiochemistry and Environment Laboratory, Nuclear Malaysia

    International Nuclear Information System (INIS)

    Yii, Mei-Wo; Abdullah Siddiqi Ismail

    2014-01-01

    Determination of alpha emitting plutonium radionuclides such as Pu-238, Pu-239 and Pu-240 concentrations inside a sample require lots of radiochemistry purification process to separate them from other interfering alpha emitters. These pure isotopes are then been electrodeposited onto a stainless steel disc and quantified using alpha spectrometry counter. In Radiochemistry and Environment Laboratory (RAS), Nuclear Malaysia, the quantification is done by comparing these isotopes with the recovery of known amount plutonium tracer, Pu-242, that been added into the sample prior analysis. This study been conducted to find the optimum conditions for the electrolysis process used at RAS. Four variable parameters that may interfere the percentage recovery of tracer hence the current, cathode to anode distance, pH and electrolysis duration had been identify and studied. Study was carry out using Pu-242 standard solution and the deposition disc was counted using Zinc Sulphite (silver) counter. Studies outcome suggested that the optimum conditions to reduce plutonium ion happens at 1-1.1 ampere of current, 3-5 mm of electrodes distance, pH 2.2-2.5 and a minimal electrolysis duration of 2 hours. (author)

  6. Research in the fields of radiochemistry and activation analysis using the LENA TRIGA nuclear plant

    International Nuclear Information System (INIS)

    Maxia, V.; Meloni, S.; Stella, R.; Brandone, A.

    1972-01-01

    In the past two years most of the research effort at the Radiochemistry Laboratory and National Research Council Centre for Radiochemistry and Activation Analysis has been devoted to research and development of activation analysis using the TRIGA Mark II LENA reactor of the University of Pavia. Pile neutrons have been used both in steady state and pulse mode, in the determination of oxygen in non ferrous materials. Neutron activation has been applied to the determination of some atmospheric particulate pollutants. Another field, in which activation analysis has been applied, is forensic research. Methods have been developed for the determination of antimony, barium and copper in gunpowder residues. By using inorganic materials such as molybdenum dibromide, zinc ferrocyanide and cadmium metal in granular form it was possible to set up simple chemical procedures in the activation analysis of trace amounts of noble metals in metallic matrices (high purity nickel and copper), geochemical materials (rocks and meteorites) and biological materials (orchard leaves). Neutron activation analysis was also used to investigate on the extraction of the platinum group metals from iodide and thiocyanate solutions at low concentrations

  7. An operating environment with multitasking capabilities for radiochemistry autosynthesizers

    International Nuclear Information System (INIS)

    Feliu, A.L.

    1990-01-01

    AUTOMATE is an operating environment which has been developed for control of commercially available autosynthesizers of radiopharmaceuticals. The software is a user-friendly multitasking system with graphical display, compatible with standard 80x86 personal computers running MS-DOS. Up to four autosynthesizers may be controlled with the software simultaneously. Applications for both routine use and research are discussed

  8. Scientific conference on inorganic chemistry and radiochemistry devoted to centenary from birthday of academician V.I. Spitsyn. Program of conference and summary of reports

    International Nuclear Information System (INIS)

    2002-01-01

    Program and summaries of reports of the Scientific conference on inorganic chemistry and radiochemistry devoted to the centenary from the birthday of academician V.I. Spitsyn are presented. The conference took place at the Chemical department of the Moscow State University named for M.V. Lomonosov 17 - 18 April, 2002. Part of the reports was devoted to the work of academician V.I. Spitsyn, his investigations into radiochemistry and radiation chemistry. Scientific explorations in the fields of solid chemistry, inorganic and coordination chemistry, radiochemistry and chemical technology are discussed [ru

  9. (18)F-labeled positron emission tomographic radiopharmaceuticals in oncology: an overview of radiochemistry and mechanisms of tumor localization.

    Science.gov (United States)

    Vallabhajosula, Shankar

    2007-11-01

    Molecular imaging is the visualization, characterization, and measurement of biological processes at the molecular and cellular levels in a living system. At present, positron emission tomography/computed tomography (PET/CT) is one the most rapidly growing areas of medical imaging, with many applications in the clinical management of patients with cancer. Although [(18)F]fluorodeoxyglucose (FDG)-PET/CT imaging provides high specificity and sensitivity in several kinds of cancer and has many applications, it is important to recognize that FDG is not a "specific" radiotracer for imaging malignant disease. Highly "tumor-specific" and "tumor cell signal-specific" PET radiopharmaceuticals are essential to meet the growing demand of radioisotope-based molecular imaging technology. In the last 15 years, many alternative PET tracers have been proposed and evaluated in preclinical and clinical studies to characterize the tumor biology more appropriately. The potential clinical utility of several (18)F-labeled radiotracers (eg, fluoride, FDOPA, FLT, FMISO, FES, and FCH) is being reviewed by several investigators in this issue. An overview of design and development of (18)F-labeled PET radiopharmaceuticals, radiochemistry, and mechanism(s) of tumor cell uptake and localization of radiotracers are presented here. The approval of clinical indications for FDG-PET in the year 2000 by the Food and Drug Administration, based on a review of literature, was a major breakthrough to the rapid incorporation of PET into nuclear medicine practice, particularly in oncology. Approval of a radiopharmaceutical typically involves submission of a "New Drug Application" by a manufacturer or a company clearly documenting 2 major aspects of the drug: (1) manufacturing of PET drug using current good manufacturing practices and (2) the safety and effectiveness of a drug with specific indications. The potential routine clinical utility of (18)F-labeled PET radiopharmaceuticals depends also on

  10. Radiochemistry; Radiochemie

    Energy Technology Data Exchange (ETDEWEB)

    Majer, Vladimir

    1942-07-01

    The value of this monograph lies in the fact that it was one of the first monographs on this topic published not only within the national boundaries but also worldwide. The book was written during World War II, when the country was occupied by the Nazis and no Czech scientific research was possible; so the author devoted his free time to writing this monograph, which had influence on many young scientists and indirectly played a role in the founding of the Nuclear Physic Institute after the war. The author founded and was the first head of the Department of Nuclear Chemistry at the then Faculty of Technical and Nuclear Physics. (P.A.)

  11. Radiochemistry - today

    International Nuclear Information System (INIS)

    Drawe, H.

    1980-01-01

    After a longer starting period many radiation techniques have prevailed practically. Today radiation processes are usual components of chemistry, biology, medicine, and technologies in the most common sense. This paper deals with the latest state of radiation chemistry, whereas the possible practical applications are in the foreground of discussion as to reach mainly practicians in laboratory and industry. But also physicians, pharmacists and chemical engineers should be informed about the possibilities of application of high energyy radiation. Because radiation chemistry has also enriched works of related subjects, for example physical, organic and inorganic chemistry, this paper will also be of interest for experts of these disciplines. (orig.) [de

  12. Activities to foster training in nuclear and radiochemistry from IACS, IAEA-Vienna

    International Nuclear Information System (INIS)

    Rossbach, M.; Narasimhan, D.V.S.; Chmielewski, A.; Einav, I.; Thereska, J.; Haji-Saeid, M.

    2005-01-01

    Uses of radioisotopes and radiation in medicine, industry, agriculture are amongst the most beneficial applications of atomic energy for peaceful purposes. The International Atomic Energy Agency aims - in accordance with its statute - to accelerate and enlarge the contribution of atomic energy to peace, health and prosperity throughout the world. The various Technical Divisions of the Agency carry out this mandate and enhance, particularly through 'manpower development activities' the nuclear applications of radiation and isotopes. Staff members of the 'Industrial Applications and Chemistry Section' in the Department of Nuclear Sciences and Applications of the IAEA have supported more than 600 trainees per year for education in nuclear and radiochemistry through fellowships, training courses and workshops. Provision of printed material in various disciplines is supporting our educational efforts. (author)

  13. A systematic investigation of PET Radionuclide Specific Activity on Miniaturization of Radiochemistry

    Energy Technology Data Exchange (ETDEWEB)

    Jeanne M Link, PhD

    2012-03-08

    The PET radionuclides, 18F and 11C consist of very high radiation to mass amounts and should be easily adapted to new technologies such as chip chemistry with nanofluidics. However, environmental contamination with nonradioactive fluorine, carbon and other trace contaminants add sufficient mass, micrograms to milligrams, to prevent adapting PET radiochemistry to the nanochip technologies. In addition, the large volumes of material required for beam irradiation make it necessary to also remove the 18F and 11C from their chemical matrices. These steps add contaminants. The work described in this report was a systematic investigation of sources of these contaminants and methods to reduce these contaminants and the reaction volumes for radiochemical synthesis. Several methods were found to lower the contaminants and matrices to within a factor of 2 to 100 of those needed to fully implement chip technology but further improvements are needed.

  14. Activities of the neutron activation analysis laboratory of the radiochemistry division of IPEN - CNEN/SP

    International Nuclear Information System (INIS)

    Vasconcellos, M.B.A.

    1988-10-01

    Neutron activation analysis (NAA) is one of the relevant applications of nuclear research reactors. Due to the high neutron fluxes available in these reactors, an excellent sensitivity of analysis is attained for many elements. NAA is one of the most sensitive, precise and accurate analytical methods for trace element determination. NAA has been one of the main activities of the Radiochemistry Division of IPEN, since the beginning of the operation of the nuclear reactor IEA-R1. Most of the effort was devoted to research work, aimed to improvements in the method as well as to its applications to several kinds of matrixes (geological, biological, metallic, environmental, forensic). Besides, analytical services were also offered, to the CNEN, to industries, universities, mining companies and research institutes. In the present paper, a review is made of the research work being developed presently at the Radiochesmitry Division of IPEN. A discussion is also made of the planned expansion of the analytical services offered [pt

  15. The inverse electron demand Diels-Alder click reaction in radiochemistry.

    Science.gov (United States)

    Reiner, Thomas; Zeglis, Brian M

    2014-04-01

    The inverse electron-demand Diels-Alder (IEDDA) cycloaddition between 1,2,4,5-tetrazines and strained alkene dienophiles is an emergent variety of catalyst-free 'click' chemistry that has the potential to have a transformational impact on the synthesis and development of radiopharmaceuticals. The ligation is selective, rapid, high-yielding, clean, and bioorthogonal and, since its advent in 2008, has been employed in a wide variety of chemical settings. In radiochemistry, the reaction has proven particularly useful with (18)  F and has already been utilized to create a number of (18)  F-labeled agents, including the PARP1-targeting small molecule (18)  F-AZD2281, the αv β3 integrin-targeting peptide (18)  F-RGD, and the GLP-1-targeting peptide (18)  F-exendin. The inherent flexibility of the ligation has also been applied to the construction of radiometal-based probes, specifically the development of a modular strategy for the synthesis of radioimmunoconjugates that effectively eliminates variability in the construction of these agents. Further, the exceptional speed and biorthogonality of the reaction have made it especially promising in the realm of in vivo pretargeted imaging and therapy, and pretargeted imaging strategies based on the isotopes (111) In, (18)  F, and (64) Cu have already proven capable of producing images with high tumor contrast and low levels of uptake in background, nontarget organs. Ultimately, the characteristics of inverse electron-demand Diels-Alder click chemistry make it almost uniquely well-suited for radiochemistry, and although the field is young, this ligation has the potential to make a tremendous impact on the synthesis, development, and study of novel radiopharmaceuticals. Copyright © 2013 John Wiley & Sons, Ltd.

  16. Nuclear chemistry on the Czech Technical University in Prague after introduction of structured study and foundation of the Centre for Radiochemistry and Radiation Chemistry

    International Nuclear Information System (INIS)

    John, J.

    2007-01-01

    In this presentation the author (head of the Centre for Radiochemistry and Radiation Chemistry) give a short review of history of the Department of Nuclear Chemistry and of the Centre for Radiochemistry and Radiation Chemistry of the Czech Technical University in Prague. Education in structured study in specialisation of nuclear chemistry in bachelor level, master level, as well as post-graduate study in nuclear chemistry with academic degree PhD. are realised. Some scientific results are presented

  17. Support for Students, Postdoctoral Fellows and Trainees to Attend Radiochemistry-­Related Symposia at Pacifichem 2015

    Energy Technology Data Exchange (ETDEWEB)

    Wilbur, Daniel Scott [Univ. of Washington, Seattle, WA (United States). Dept. of Radiation Oncology

    2016-02-06

    This project was undertaken to meet the growing need for training personnel who will be involved in professional careers requiring knowledge of radiochemistry, such as those working in radionuclide production, and in biological, industrial, medical and environmental fields that use radionuclides in their work. The goal of the project was to provide financial assistance to students and trainees from academic and government institutions (US preferred) to attend selected radiochemistry-­related symposia at the Pacifichem 2015 meeting held in Honolulu, Hawaii in December 2015. The funding, meant to provide a portion of an awardee’s travel cost, was specifically directed at attendance to the following symposia: #363, Isotope production-­ Providing Important Materials for Research and Applications; #215, Chemistry of Molecular Imaging, and #11, Chemistry for Development of Theranostic Radiopharmaceuticals. Those symposia were held December 16th (am & pm: #11, #363), December 17th (am: #11, #363; pm: #275) and December 18th (am & pm: #275). Pacifichem meetings are held every 5 years in Honolulu, Hawaii. The meetings are joint sponsored by a number of Chemistry Societies from Pacific Rim countries. The meetings are composed of a large number of symposia (>300) on a wide variety of topics, which make them similar to small meetings within the larger overall meeting. Therefore, attendance at the three symposia within Pacifichem 2015 was similar to attending a meeting focused entirely on radiochemistry-­related topics. To obtain the financial assistance, the student/trainee: (a) had to be an undergraduate student, graduate student or Postdoctoral Fellow in a physical science department or National Laboratory; (b) had to submit a letter from their supervisor indicating that he/she will be enrolled as a student/trainee at the time of the meeting, and were committed to attending the meeting; and (c) had to submit a resume or curriculum vitae along with a brief statement of

  18. User's and reference guide to the INEL RML/analytical radiochemistry sample tracking database version 1.00

    International Nuclear Information System (INIS)

    Femec, D.A.

    1995-09-01

    This report discusses the sample tracking database in use at the Idaho National Engineering Laboratory (INEL) by the Radiation Measurements Laboratory (RML) and Analytical Radiochemistry. The database was designed in-house to meet the specific needs of the RML and Analytical Radiochemistry. The report consists of two parts, a user's guide and a reference guide. The user's guide presents some of the fundamentals needed by anyone who will be using the database via its user interface. The reference guide describes the design of both the database and the user interface. Briefly mentioned in the reference guide are the code-generating tools, CREATE-SCHEMA and BUILD-SCREEN, written to automatically generate code for the database and its user interface. The appendices contain the input files used by the these tools to create code for the sample tracking database. The output files generated by these tools are also included in the appendices

  19. Activities of the Laboratory of Neutron Activation Analysis in the Radiochemistry Division - IPEN/CNEN/SP/Brazil

    International Nuclear Information System (INIS)

    Vasconcellos, M.B.A.

    1988-01-01

    Neutron activation analysis (NAA) is one of the relevant applications of nuclear research reactors. Due to the high neutron fluxes available in these reactors, an excellent sensitivity of analysis is attained for many elements. NAA is one of the most sensitive, precise and accurate analytical methods for trace element determination. NAA has been one of the main activities of the Radiochemistry Division of IPEN, since the befinning of the operation of the nuclear reactor IEA-R1. Most of the effort was devoted to research work, aimed to improvements in the method as well as to its applications to several kinds of matrixes (geological, biological, metallic, environmental, forensic). Besides, analytical services were also offered, to the CNEN, to industries, universities, mining companies and research institutes. In the present paper, a review is made of the research work being developed presently at the Radiochemistry Division of IPEN. A discussion is also made of the planned expansion of the analytical services offered. (author) [pt

  20. Performance characterization of the PET-CT tomograph at the PET-cyclotron-radiochemistry site of Messina University

    OpenAIRE

    Amato, Ernesto; Baldari, Sergio; Tomasello, Francesco

    2015-01-01

    A PET-cyclotron-radiochemistry plant was built at Messina University Hospital, whose diagnostics section was equipped with a PET-CT scanner composed by a time of flight PET and a 16-slice CT. The present note reports about the results of tomograph's acceptance tests, which had been planned and carried out in order to verify the correspondence of the specific scanner's performances declared by the firm and the fulfillment of Italian law's minimal criteria of acceptability. Acceptance tests...

  1. Conception and syllabus on radiochemistry and radioecology principles for general student groups of a university chemical department

    International Nuclear Information System (INIS)

    Bogdanov, R.V.

    1994-01-01

    The problem of basic principles of selecting materials for general courses on diverse subjects in chemical science is discussed. Relying on certain general rules and proceeding from specificity of radiochemistry, the author suggests a variant of syllabus including radiochemical and radioecological blocks intented for 48 academic hours. In methodical respect emphasis is made on theoretical material presentation in close combination with various nuclear methods used in chemical studies. 6 refs., 1 fig

  2. Astatine-211 Radiochemistry: The Development Of Methodologies For High Activity Level Radiosynthesis

    International Nuclear Information System (INIS)

    Zalutsky, Michael R.

    2012-01-01

    Targeted radionuclide therapy is emerging as a viable approach for cancer treatment because of its potential for delivering curative doses of radiation to malignant cell populations while sparing normal tissues. Alpha particles such as those emitted by 211At are particularly attractive for this purpose because of their short path length in tissue and high energy, making them highly effective in killing cancer cells. The current impact of targeted radiotherapy in the clinical domain remains limited despite the fact that in many cases, potentially useful molecular targets and labeled compounds have already been identified. Unfortunately, putting these concepts into practice has been impeded by limitations in radiochemistry methodologies. A critical problem is that the synthesis of therapeutic radiopharmaceuticals provides additional challenges in comparison to diagnostic reagents because of the need to perform radio-synthesis at high levels of radioactivity. This is particularly important for α-particle emitters such as 211At because they deposit large amounts of energy in a highly focal manner. The overall objective of this project is to develop convenient and reproducible radiochemical methodologies for the radiohalogenation of molecules with the α-particle emitter 211At at the radioactivity levels needed for clinical studies. Our goal is to address two problems in astatine radiochemistry: First, a well known characteristic of 211At chemistry is that yields for electrophilic astatination reactions decline as the time interval after radionuclide isolation from the cyclotron target increases. This is a critical problem that must be addressed if cyclotrons are to be able to efficiently supply 211At to remote users. And second, when the preparation of high levels of 211At-labeled compounds is attempted, the radiochemical yields can be considerably lower than those encountered at tracer dose. For these reasons, clinical evaluation of promising 211At-labeled targeted

  3. ASTATINE-211 RADIOCHEMISTRY: THE DEVELOPMENT OF METHODOLOGIES FOR HIGH ACTIVITY LEVEL RADIOSYNTHESIS

    Energy Technology Data Exchange (ETDEWEB)

    MICHAEL R. ZALUTSKY

    2012-08-08

    Targeted radionuclide therapy is emerging as a viable approach for cancer treatment because of its potential for delivering curative doses of radiation to malignant cell populations while sparing normal tissues. Alpha particles such as those emitted by 211At are particularly attractive for this purpose because of their short path length in tissue and high energy, making them highly effective in killing cancer cells. The current impact of targeted radiotherapy in the clinical domain remains limited despite the fact that in many cases, potentially useful molecular targets and labeled compounds have already been identified. Unfortunately, putting these concepts into practice has been impeded by limitations in radiochemistry methodologies. A critical problem is that the synthesis of therapeutic radiopharmaceuticals provides additional challenges in comparison to diagnostic reagents because of the need to perform radio-synthesis at high levels of radioactivity. This is particularly important for {alpha}-particle emitters such as 211At because they deposit large amounts of energy in a highly focal manner. The overall objective of this project is to develop convenient and reproducible radiochemical methodologies for the radiohalogenation of molecules with the {alpha}-particle emitter 211At at the radioactivity levels needed for clinical studies. Our goal is to address two problems in astatine radiochemistry: First, a well known characteristic of 211At chemistry is that yields for electrophilic astatination reactions decline as the time interval after radionuclide isolation from the cyclotron target increases. This is a critical problem that must be addressed if cyclotrons are to be able to efficiently supply 211At to remote users. And second, when the preparation of high levels of 211At-labeled compounds is attempted, the radiochemical yields can be considerably lower than those encountered at tracer dose. For these reasons, clinical evaluation of promising 211At

  4. Nuclear chemistry and Radiochemistry in the USA; Kern- und Radiochemie in den USA

    Energy Technology Data Exchange (ETDEWEB)

    Kronenberg, A. [Los Alamos National Lab., NM (United States). Isotope and Nuclear Chemistry Div.; Stoyer, M. [Lawrence Livermore National Lab., CA (United States)

    2004-04-01

    Nuclear chemistry and radiochemistry are very young sciences which developed at an extremely brisk pace within a very short period of time after the discovery of nuclear fission in 1938, and caused profound societal changes. In the United States, nuclear chemistry developed very differently from Germany, where nuclear research initially had been banned after the Second World War. The prime mover in the development in the United States was the Manhattan Project, the construction of the atomic bomb. The counteract the impending shortage of qualified personnel, important institutions have begun to establish training and support programs in the field. The National Laboratories in the United States introduced a National Security Internship Program, while the U.S. Department of Energy (DOE) tries to promote cooperation, and thus the training of personnel, by launching programs of its own. Yet, a greater shortage of qualified personnel is becoming apparent. The situation of nuclear chemistry and radiochemistry in the United States can be summarized in the finding that research at the National Laboratories is very wide ranging. It receives sufficient funds from the DOE. However, the National Laboratories show a very high proportion of elderly personnel, a problem which will have to be corrected in the years to come. This may be helped by the Summer Schools financed by the DOE, though a summer school of six weeks cannot replace a sound training in nuclear chemistry of the kind still to be found in Germany. (orig.) [German] Kern- und Radiochemie sind sehr junge Wissenschaften, die sich nach der Entdeckung der Kernspaltung 1938 innerhalb kuerzester Zeit extrem rasant entwickelt und tiefe gesellschaftliche Veraenderungen bewirkt haben. In den USA hat sich die Kernchemie sehr unterschiedlich im Vergleich zu Deutschland entwickelt, wo die Kernforschung nach dem 2. Weltkrieg vorerst verboten war. Massgeblich in den USA war dabei das Manhatten-Projekt zum Bau von Nuklearwaffen

  5. Centrifugal micro-fluidic platform for radiochemistry: Potentialities for the chemical analysis of nuclear spent fuels

    International Nuclear Information System (INIS)

    Bruchet, Anthony; Mariet, Clarisse; Taniga, Velan; Descroix, Stephanie; Malaquin, Laurent; Goutelard, Florence

    2013-01-01

    The use of a centrifugal micro-fluidic platform is for the first time reported as an alternative to classical chromatographic procedures for radiochemistry. The original design of the micro-fluidic platform has been thought to fasten and simplify the prototyping process with the use of a circular platform integrating four rectangular microchips made of thermoplastic. The microchips, dedicated to anion-exchange chromatographic separations, integrate a localized monolithic stationary phase as well as injection and collection reservoirs. The results presented here were obtained with a simplified simulated nuclear spent fuel sample composed of non-radioactive isotopes of Europium and Uranium, in proportion usually found for uranium oxide nuclear spent fuel. While keeping the analytical results consistent with the conventional procedure (extraction yield for Europium of ∼97%), the use of the centrifugal micro-fluidic platform allowed to reduce the volume of liquid needed by a factor of ∼250. Thanks to their unique 'easy-to-use' features, centrifugal micro-fluidic platforms are potential successful candidates for the down-scaling of chromatographic separation of radioactive samples (automation, multiplexing, easy integration in glove-boxes environment and low cost of maintenance). (authors)

  6. Education of radiochemistry and radiation chemistry at a college of medical technology

    International Nuclear Information System (INIS)

    Asano, Takeyoshi

    2005-01-01

    The present report aims at introducing my creative textbook on the subject. The contents start from the history of the 20th century on discovery and use of radiation and radioisotope''. In the study of the history the students can aware of their position in a future profession as a medical radiation worker. In addition, own originality for the textbook was shown in the descriptions of (1) Auger effect of EC decay nuclide used remarkably in nuclear medicine, (2) the relation between isotope, isotone and isobar and the kind of nuclear reaction, (3) the distinction of the use of isotope dilution method in substoichiometry and radioimmunoassay, (4) nuclear reactor chemistry (nuclear fuel cycle and disposal of high level radioactive waste), (5) fundamental constants used in radioisotope techniques and (6) the exposure dose in taking a side view of the radiation chemistry. A questionnaire survey after the closing the lesson showed that the students took an interest in 60% of the contents in the textbook of radiochemistry and radiation chemistry. (author)

  7. Review Article : Utilization of Environmental Radiochemistry Techniques for Selection and Evaluation of Nuclear Facility Sites

    International Nuclear Information System (INIS)

    Atta, E.R.; Madbouly, A.M.; Zakaria, Kh.M.

    2016-01-01

    This research review puts necessary considerations on the available environmental radiochemistry techniques for selection and evaluation of a nuclear facility sites.The main bjective in site evaluation for nuclear facilities in terms of nuclear safety is to protect the site workers, the public and the environment from the effects of ionizing radiation release from nuclear facilities due to accidents. The extreme sensitivity and speed of radiochemical methods make their applications of considerable importance in several fields and they have found many uses. Information about the existed radioactivity in the different nuclear facilities is an essential requirement for their environmental assessment. It is necessary to estimate the various radioactivity levels in the environment through qualitative and quantitative analytical techniques and to assess the potential effects of the nuclear facility in the region by considering the characteristics of sites.The siting and site evaluation requirements are discussed. Emphasis was given to types of radiochemical techniques used for characterization of the site parameters which determine the potential hazards of the site on the facility and the facility on the site. Emphasis has been also given to the quantitative and qualitative analysis of naturally occurring radionuclides for monitoring and control .There are some techniques employed such as radioactive tracer technique, liquid scintillation technique, gamma spectrometry technique, neutron activation analysis technique, fluorimetric technique and isotope hydrology technique.

  8. Organisation in the Harwell Radiochemistry Laboratories for Dealing with Radiation Accidents

    Energy Technology Data Exchange (ETDEWEB)

    Hudswell, F. [Atomic Energy Research Establishment, Harwell, Didcot, Berks. (United Kingdom)

    1969-10-15

    The radiochemistry laboratories contain extensive facilities for the handling of large quantities of alpha emitters and beta/gamma active materials. Safety in this area is surveyed by a local safety committee, which has been responsible for the development of both the working rules for the avoidance of radiation accidents and the organisation for dealing with them should they occur. The emergency control organisation within the high activity area is linked with and approved by the site organisation. Local control within the building can be undertaken by any one of a number of senior staff, who is advised by a health physicist, engineer and other scientists, and who delegates executive responsibility for emergency stations to a number of scientific and engineering staff. An incident in the area which affects other areas in the establishment is controlled by the establishment emergency organisation but will also involve the local control post as a source of action and information. Reciprocally, local control may be required to receive evacuees from a remote incident area. Safety manuals and emergency plans are revised periodically. Exercises are mounted several times a year and are followed by discussions of the weaknesses found. Attempts are made to remedy the weaknesses in subsequent exercises. (author)

  9. ERA—European Radiochemists Association: Report on the activities of the Working Party for Nuclear and Radiochemistry of the Federation of European Chemical Societies

    Science.gov (United States)

    Kolar, Z. I.; Ware, A. R.

    2003-01-01

    The European Radiochemists Association started almost simultaneously with the appearance of the first issue of the Radiochemistry in Europe newsletter in August 1995. The objective of the European Radiochemists Association (ERA) is to extend and improve communication between radiochemists in Europe through a newsletter. Liaison persons within each country or group exchange details of their activities, set up a diary of relevant international events and exchange details of specialist equipment, facilities and technology. In the year 2000 the Federation of European Chemical Societies decided to form a working party on nuclear and radiochemistry. It is a formalisation of the European Radiochemists Association. Each chemical society is allowed to nominate a member to the Working Party on Nuclear and Radiochemistry. Currently we have 12 nominated members plus two invited and one observer. In addition to the ERA aims and objectives it proposes to put together a syllabus of radiochemistry for undergraduate and post-graduate students—this aspect has been a part of our support of the International Atomic Energy Agency initiative. Also the aim of the working party is to support other working parties and divisions, to press the Federation of the European Chemical Societies for financial structure. To this end an Expression of Interest has been tabled with the Framework 6 Programme for networking within radiochemistry in Europe. The WP will liaise with the International Isotope Society and the International Society on Radiopharmaceutical Chemistry and Biology to seek to communicate and to consider ways of working together.

  10. KfK, Institute for Radiochemistry. Report on the results of research and development performances 1989

    International Nuclear Information System (INIS)

    1990-03-01

    In 1989 the Institute for Radiochemistry became involved with research and development tasks in the context of the following projects: 'Reprocessing and Waste Treatment' (PWA), 'Fast Breeder' (PSB), 'Nuclear Fusion' (PKF) and 'Terminal Storage' (ELA). Environmental analysis and water technology within the Institute were amongst the programmes collected together in the project 'Environment and Safety'. Problems to do with surface chemistry and analysis were dealt with under 'Microtechnology'. Within the 'Reprocessing and Waste Treatment Project', the studies carried out in the Institute concentrated chiefly on investigating ways of simplifying the reprocessing process, especially in the reprocessing of fast-breeder fuels and waste reduction and treatment. In the 'Fast Breeder' project, further investigations were carried out on oxide fuel rods. In the 'Nuclear Fusion' project, the subject of investigation was chemical problems in the field of tritium technology as they arise during the recovery of tritium from tritium compounds in the internal or external fuel cycle of a fusion reactor. To this end, studies were carried out on the physical-chemical analysis of ceramic breeder materials. Research were carried out on the analysis and description of surfaces and on the reactions occurring on these surfaces and on the reactions occurring on these surfaces with regard to the application of knowledge gained from this programme to problems within environmental research, nuclear technology and microtechnology. The Water Chemistry Department working mainly on 'Environment and Safety' carried out chemical research and method development in the following subject areas: New technologies for the removal of problem constituents from water, the production of useable water and sewage recycling and the analysis and description of water pollutants. (orig./HK) [de

  11. Proficiency Test Program Involvement as a Tool for External Quality Control for Radiochemistry and Environmental Laboratory, Malaysian Nuclear Agency

    International Nuclear Information System (INIS)

    Nurrul Assyikeen Mohd Jaffary; Wo, Y.M.; Zal U'yun Wan Mahmood; Norfaizal Mohamed; Abdul Kadir Ishak; Noor Fadzilah Yusof; Jalal Sharib

    2016-01-01

    As the only Laboratory in Malaysia under the IAEA Analytical Laboratories for the Measurement of Environmental Radioactivity (ALMERA) Network, the Radiochemistry and Environmental Laboratory (RAS), Malaysian Nuclear Agency participates in the proficiency test programmes organised by ALMERA to achieve mutual acceptance of analytical data. The ALMERA has been providing quality support of proficiency tests using sets of different samples matrices and radionuclide levels typically encountered in environmental and food monitoring laboratories. The involvement of RAS laboratory in the IAEA proficiency tests gives opportunity to improve the laboratory capability and personnel skills in the field of radioactivity testing. (author)

  12. Chemistry and radiochemistry of As, Re and Rh isotopes relevant to radiopharmaceutical applications: high specific activity radionuclides for imaging and treatment.

    Science.gov (United States)

    Feng, Yutian; Phelps, Tim E; Carroll, Valerie; Gallazzi, Fabio; Sieckman, Gary; Hoffman, Timothy J; Barnes, Charles L; Ketring, Alan R; Hennkens, Heather M; Jurisson, Silvia S

    2017-10-31

    The chemistry and radiochemistry of high specific activity radioisotopes of arsenic, rhenium and rhodium are reviewed with emphasis on University of Missouri activities over the past several decades, and includes recent results. The nuclear facilities at the University of Missouri (10 MW research reactor and 16.5 MeV GE PETtrace cyclotron) allow research and development into novel theranostic radionuclides. The production, separation, enriched target recovery, radiochemistry, and chelation chemistry of 72,77 As, 186,188 Re and 105 Rh are discussed.

  13. Eurac: a project to strengthen scientific academic competence and analytical skills within radiation protection, radiochemistry and radioecology

    Energy Technology Data Exchange (ETDEWEB)

    Tamponnet, C. [Institut de Radioprotection et de Surete Nucleaire, 13 - Saint Paul lez Durance (France); Salbu, B.; Skipperud, L. [Norwegian Univ. of Life Sciences, Aas (Norway); Mitchell, P. [University College Dublin, Dublin (Ireland); Holm, E. [Lund Univ. (Sweden); Garciatenorio, R. [Seville Univ. (Spain); Kovats, N. [Veszprem Univ. (Hungary); Abbott, A. [Westlakes Research Institute, Moor Row (United Kingdom); Davids, C. [Norwegian Radiation Protection Authority, Osteras (Norway); Garelick, H.; Priest, N. [Middlesex Univ., Enfield (United Kingdom)

    2006-07-01

    The E.u.r.a.c. project is consultative or consensual and aims to assess the current and potential levels of postgraduate provision in selected linked disciplines associated with radiological protection and radioecological competence within universities and other higher education institutes of the Eu and new entrant nations in the context of demand. Based on consultations with European stakeholders E.u.r.a.c. will propose those actions that could be taken by European Institutions and relevant organisations in Member States to secure the future of nuclear radiological protection, radiochemistry and radioecology postgraduate education in an expanded Eu. The objective are: assess the needs for co-ordinated postgraduate education in the Eu and new entrant nations in order to strengthen the scientific academic competence and analytical skills within radiological protection, radiochemistry and radioecology, secure the future recruitment of appropriately skilled postgraduates to meet the needs of European stakeholders; recommend, following consultations, actions that could be taken within the Eu to help the postgraduate education needs identified. four work packages are studied: determination of existing competence and infrastructures, estimation of future scientific needs, development of possible postgraduate education solutions, assessments and recommendations. (N.C.)

  14. Eurac: a project to strengthen scientific academic competence and analytical skills within radiation protection, radiochemistry and radioecology

    International Nuclear Information System (INIS)

    Tamponnet, C.; Salbu, B.; Skipperud, L.; Mitchell, P.; Holm, E.; Garciatenorio, R.; Kovats, N.; Abbott, A.; Davids, C.; Garelick, H.; Priest, N.

    2006-01-01

    The E.u.r.a.c. project is consultative or consensual and aims to assess the current and potential levels of postgraduate provision in selected linked disciplines associated with radiological protection and radioecological competence within universities and other higher education institutes of the Eu and new entrant nations in the context of demand. Based on consultations with European stakeholders E.u.r.a.c. will propose those actions that could be taken by European Institutions and relevant organisations in Member States to secure the future of nuclear radiological protection, radiochemistry and radioecology postgraduate education in an expanded Eu. The objective are: assess the needs for co-ordinated postgraduate education in the Eu and new entrant nations in order to strengthen the scientific academic competence and analytical skills within radiological protection, radiochemistry and radioecology, secure the future recruitment of appropriately skilled postgraduates to meet the needs of European stakeholders; recommend, following consultations, actions that could be taken within the Eu to help the postgraduate education needs identified. four work packages are studied: determination of existing competence and infrastructures, estimation of future scientific needs, development of possible postgraduate education solutions, assessments and recommendations. (N.C.)

  15. Research activities in the fields of radiochemistry and neutron activation analysis using the LENA nuclear plant in Pavia

    International Nuclear Information System (INIS)

    Caramella-Crespi, V.; Case, M. Di; Gallorini, M.; Ganzerli-Valentini, M.

    1976-01-01

    The activity of the Radiochemistry Laboratory and National Research Council Center for Radiochemistry and Activation Analysis in the past two years has been mainly devoted to the following subjects: Several elements (V, Mn, Cu, Cd, Zn, Cr, Co, Fe, Cs, Rb, Sc) have been determined in biological, geological and cosmological matrices (as sediments, river waters, vegetables, foods, Italian condritic meteorites). Comparative measurements have been carried out using different techniques, such as atomic absorption and X-ray fluorescence; comparative investigations have been developed with different radioanalytical methods for Cr trace determination. A new rapid separation procedure of Hg, Se and As has been set up, based on selective behaviour toward granular copper. The evaluation of trace elements amount in Sardinian coal samples has been also accomplished. In the field of biomedical applications levels of trace elements were determined in the principal usual foods used by people of the lower Dahomey to the purpose of studying the correlation between the food content of these elements and the population's intake. Inorganic exchangers studies have been carried out on molybdenum dibromide, tantalum carbide and metallic copper retention properties and on the related absorption mechanism. X-ray fluorescence has been used as an analytical tool to integrate neutron activation analysis in the determination of Cr, Zn, Fe in environmental matrices. (author)

  16. Teaching of foundations of radiochemistry on chemical faculty of Moscow State University after M.V. Lomonosov. Methodical ensuring of the subject

    International Nuclear Information System (INIS)

    Luk'yanov, V.B.; Berdonosov, S.S.; Fedoseev, V.M.

    1995-01-01

    The peculiarities of the lecture course on radiochemistry principles in the Moscow State University after M.V. Lomonosov are considered. The methodical provision of the lectures including the curriculum, methodical aids, tasks for self-control and for lecture control, as well as, summary questionary forms, is discussed. 3 refs

  17. Management of liquid radioactive waste from research and training laboratories of radiochemistry and radioecology

    International Nuclear Information System (INIS)

    Krasnopyorova, A.P.; Yuhno, G.D.; Sytnik, O.Y.

    2001-01-01

    Full text: Liquid radioactive waste (LRW), that is formed in research and training cycle of radiochemistry and radioecology laboratories of Kharkov National University, corresponds to medium active one (10 5 -10 7 Bq/l). Since the great number of different radioactive isotopes is involved in research conducted by the laboratories, liquid waste contains various radioactive contaminations. As a rule these are the water solutions of salts with concentration of 0.8-1.0 gm/l, containing mixture of 45 Ca, 65 Zn, 90 Sr, 173 Cs radionuclides. Accumulation of liquid waste from the laboratories is comparatively small, approximately 20-30 I per month. A great while LRW from the laboratories had been accumulated in special protective containers and delivered to the central waste disposal. Numerous studies has shown that LRW storage in special containers may only be temporal, since durable holding of waste necessarily gives rise to corrosion of the facing materials, and therefore diffusion of radioactive substances into environment. In addition long-term LRW storage is disadvantageous from economic point of view. Only conversion of LWR into solid state provides safe protection of environment and decreases volumes of waste. At present LRW from the laboratories is necessarily decontaminated and concentrated before being disposed.To that end the sorption methods are used, in which radionuclides from solution are concentrated in solid phase. Since small volumes of LRW are accumulated in the laboratories, the simple scheme of LRW treatment and conversion into solid residual has been designed. It comprises two steps. At the first stage consists in combining of lime-soda-ash softening with the ion-exchange sorption on the finely divided solid sorbent. Natural zeolite, clinoptilolite from Sokimitsk deposit of Ukraine, is used as the sorbent. Usage of clinoptilolite is justified by its high selectivity and sorption power in regard to 90 Sr, 137 Cs, 65 Zn radionuclides. Both low cost and

  18. Performance characterization of the PET-CT tomograph at the PET-cyclotron-radiochemistry site of Messina University

    Directory of Open Access Journals (Sweden)

    Ernesto Amato

    2015-10-01

    Full Text Available A PET-cyclotron-radiochemistry plant was built at Messina University Hospital, whose diagnostics section was equipped with a PET-CT scanner composed by a time of flight PET and a 16-slice CT. The present note reports about the results of tomograph's acceptance tests, which had been planned and carried out in order to verify the correspondence of the specific scanner's performances declared by the firm and the fulfillment of Italian law's minimal criteria of acceptability. Acceptance tests gave positive results for all the physical parameters measured. The assessment of CT slice thickness, with regard to the thinner slices of 0.75 and 0.6 mm, required the employment of a manual procedure exploiting a phantom equipped with low inclination ramps. These results allowed us to assess a baseline of performance parameters to be taken as a reference for periodic constance tests.

  19. Research activities in the fields of radiochemistry and neutron activation analysis using the LENA nuclear plant in Pavia

    International Nuclear Information System (INIS)

    Maggi, L.; Genova, N.; DiCasa, M.; Carmella-Crespi, V.

    1978-01-01

    In the past two years the activity of the Radiochemistry Laboratory and CNR Centre of Radiochemistry and Activation Analysis was mainly devoted to studies of nuclear activation analysis applied to different fields using the LENA reactor. Three NBS vegetable reference standards, Orchard Leaves, Tomato Leaves and Pine Needles, were analyzed for their halogen content. Halogen determination in foodstuff, vegetables and organic tissues gives valuable information on metabolic, nutritional, pollution and epidemiological fields. A detailed study on macro- and micro-elements content in Sardinian coal and its ashes was performed, in order to assess the possibility of using it as a fuel in electric power generating plants. Instrumental neutron activation analysis was used for the determination of Al, Si, Mn, Mg, Na, V, CI, Ce, Yb, Th, Cr, Hf, Cs, Se, Rb, Fe, Co, Ta, Eu, K, La and Sb. A multielement trace analysis of rock samples was developed in cooperation with scientists from other Universities; the determination of R.E., U, Th, Zr, Cs, Ba, Ni, Sc, Ta, Hf, Sr, and Cr by instrumental neutron activation analysis was carried out in connection with orogenetic studies of African Rocks. In the archaeological field ancient artefacts recently discovered during a digging campaign at Monza's Cathedral (Italy) were analyzed with the aim to trace their origin and compare their composition with similar samples whose dating is certain. As a contribute to the international program of certifying NBS reference standard materials, chromium in the Brewer's Yeast, recently proposed as a new SRM, was determined by both instrumental and destructive neutron activation analysis. In the study of the role and behaviour of trace elements in human physiology, vanadium was investigated in human blood, as a trace element of increasing interest in connection with its origin from pollutants. Nuclear activation analysis was also applied to marine organism samples under a contract for oceanographic research

  20. Contributions of radiochemistry and nuclear analytical techniques to society and technology: some examples of 35 years’ experience in Delft

    International Nuclear Information System (INIS)

    Bode, Peter

    2013-01-01

    Budget cuts and the oscillating public debates on the benefits of nuclear research reactor facilities are a continuous threat to many nuclear institutions. University affiliated institutions often face additional problems if their facilities offer sufficient scientific challenge and if an education in nuclear sciences provide students a sound outlook for a professional career. Such discussions may be an excuse for non-fulfilment of vacancies and reduced priority in the academic curriculum. Universities tend to reallocate their funds to more contemporary sciences such as molecular biology and nanotechnology. Their choices are based on relevance, quality viability and productivity. Relevance is often measured on the basis of external funding of research programs as well as on career opportunities for students. However, the areas with opportunities for external funding are largely determined by socio-economic developments, sometimes even at the (inter)national political level. The thematic areas in the scientific Framework Programs of the European Union illustrate this. The relevance and viability of an expensive facility like a nuclear reactor centre can also be demonstrated by making the facilities available to provide measurements on request by outsiders. Ideally, such services should be sustainable, but even the existence may lead to consider the centre being of regional or national importance. Nuclear reactor centres have various options for such services, like production of radionuclides; neutron transmutation doping; neutron activation analysis; neutron radiography and others. This contribution gives examples of the typical analytical services provided by the Interuniversity Reactor Institute of the Delft University of Technology. This institute houses the only university research reactor in the Netherlands, a 2 MW swimming pool reactor, with associated facilities for neutron research, neutron activation and radiochemistry. Within the services provided by the

  1. First meeting on the CRP 'standardized high current solid targets for cyclotron production of diagnostic and therapeutic radionuclides'

    International Nuclear Information System (INIS)

    Winkel, P. van den

    2000-01-01

    The Cyclotron Department of the VUB has three groups performing research in the field of target development, production of radionuclides and their application in nuclear medicine. 1. The Physics Group is busy on the optimization of beam parameters, on the determination of cross sections and on neutron spectrometry. 2. The Inorganic Radiochemistry Group performs research on solid target electroplating (Tl, Zn, Cd, Rh ... ), on optimisation of target carrier geometry and cooling and on automated PC-controlled radiochemistry (Tl-201, Ga-67, In-111) and recovery systems and the associated software written in Modula-2 and Visual Basic. 3. The Organic Radiochemistry Group develops new techniques for radiolabelling of organic molecules (fatty acids, neuroleptics, synthetic polypeptides...) useful in diagnostic and therapeutic nuclear medicine. All three groups take part in bulk productions of radionuclides

  2. Transmutation studies using SSNTD and radiochemistry and the associated production of secondary neutrons

    CERN Document Server

    Brandt, R; Wan, J S; Schmidt, T; Langrock, E J; Vater, P; Adam, J; Bamblevski, V P; Bradnova, V; Gelovani, L K; Kalinnikov, V K; Krivopustov, M I; Kulakov, B A; Sosnin, A N; Perelygin, V P; Pronskikh, V S; Stegailov, V I; Tsoupko-Sitnikov, V M; Modolo, G; Odoj, R; Philippen, P W; Adloff, J C; Pape, F; Debeauvais, M; Zamani-Valassiadou, M; Hashemi-Nezhad, S R; Dwivedi, K K; Guo Shi Lun; Li, L; Wang, Y L; Wilson, B

    1999-01-01

    Experiments using 1.5 GeV, 3.7 GeV and 7.4 GeV protons from the Synchrophasotron, LHE, JINR, Dubna, Russia, on extended Pb- and U- targets were carried out using SSNTD and radiochemical sensors for the study of secondary neutron $9 fluences. We also carried out first transmutation studies on the long-lived radwaste nuclei /sup 129/I and /sup 237/Np. In addition, we carried out computer code simulation studies on these systems using LAHET and DCM/CEM codes. We $9 have difficulties to understand rather large transmutation rates observed experimentally when they are compared with computer simulations. There seems to be a rather fundamental problem understanding the large transmutation rates as $9 observed experimentally in Dubna and CERN, as compared to those theoretical computer simulations mentioned above. (10 refs).

  3. Dendrimer Nanoscaffolds for Potential Theranostics of Prostate Cancer with a Focus on Radiochemistry

    Science.gov (United States)

    Lo, Su-Tang; Kumar, Amit; Hsieh, Jer-Tsong; Sun, Xiankai

    2013-01-01

    Dendrimers are a class of structurally defined macromolecules featured with a central core, a low-density interior formed by repetitive branching units, and a high-density exterior terminated with surface functional groups. In contrast to their polymeric counterparts, dendrimers are nano-sized and symmetrically shaped, which can be reproducibly synthesized in a large scale with monodispersity. These unique features have made dendrimers of increasing interest for drug delivery and other biomedical applications as a nanoscaffold system. Intended to address the potential use of dendrimers for the development of theranostic agents, which combines therapeutics and diagnostics in a single entity for personalized medicine, this review focuses on the reported methodologies of using dendrimer nanoscaffolds for targeted imaging and therapy of prostate cancer. Of particular interest, relevant chemistry strategies are discussed due to their important roles in the design and synthesis of diagnostic and therapeutic dendrimer-based nanoconjugates and potential theranostic agents, targeted or non-targeted. Given the developing status of nanoscaffolded theranostics, major challenges and potential hurdles are discussed along with the examples representing current advances. PMID:23294202

  4. A novel, microcomputer-based process control scheme for radiochemistry autosynthesizers

    International Nuclear Information System (INIS)

    Feliu, A.L.

    1989-01-01

    With the continuing development of positron emission tomography, increasing emphasis is being given to the design of reliable autosynthesizers to supply routinely-used radiopharmaceuticals. In order to reduce the time required to automate the synthesis of new radiotracers, a software scheme is proposed which includes: a generic control program supporting a standard set of components, end-user customization of the video display, mouse-driven remote control of individual components (components are presented on screen as icons), and a batch language for completely automating synthetic operations. This strategy is illustrated in a chemist-friendly microcomputer softward package running under MS-DOS which exploits the features and full flexibility of the CTI/Siemens Chemical Process Control Unit. To facilitate system expansion, the program, written in Microsoft QuickBASIC, contains generic executive-level code with calls to component-specific GOSUBs, and is designed to accommodate operation or hardware modifications in response to improvements in synthetic art without a rewrite. Two user-generated configuration files detail synthesis-specific parameters, providing a customized interface

  5. Radiochemistry of iodine

    Energy Technology Data Exchange (ETDEWEB)

    Kahn, M.; Kleinberg, J.

    1977-09-01

    The preparation of isotopes of the element, with selected procedures for its determination in or separation from various media is described along with the separating of iodine species from each other. Each part of the introductory section is referenced separately from the remainder of the monograph. For the preparative and analytical sections there is an extensive, indexed bibliography which was developed from the indexes of Volumes 19 to 30 inclusive (1965-1974) of Nuclear Science Abstracts (NSA). From these indexes the NSA abstracts of possible pertinent references were selected for examination and a choice was made of those references which were to be included in the bibliography. The bibliography has both primary and secondary references. Although the monograph does not cover hot atom chemistry, the kinetics of exchange reactions, decay schemes, or physiological applications, papers in these areas were examined as possible sources of useful preparative and analytical procedures. (JRD)

  6. Radiochemistry of astatine

    International Nuclear Information System (INIS)

    Ruth, T.J.; Dombsky, M.; D'Auria, J.M.; Ward, T.E.

    1988-01-01

    This monograph is a review of the literature through 1987 and covers the methods of producing the radioisotopes of astatine and the inorganic, nuclear, and organic chemistry of astatine. The discussion is limited to chemical and physical chemical properties of astatine. The monograph, after the introduction, is divided into chapters titled: production methods, nuclear spectroscopy, chemistry of astatine, separation and isolation (dry and wet), and selected procedures. 209 refs., 15 figs., 7 tabs

  7. Radiochemistry of iodine

    International Nuclear Information System (INIS)

    Kahn, M.; Kleinberg, J.

    1977-09-01

    The preparation of isotopes of the element, with selected procedures for its determination in or separation from various media is described along with the separating of iodine species from each other. Each part of the introductory section is referenced separately from the remainder of the monograph. For the preparative and analytical sections there is an extensive, indexed bibliography which was developed from the indexes of Volumes 19 to 30 inclusive (1965-1974) of Nuclear Science Abstracts (NSA). From these indexes the NSA abstracts of possible pertinent references were selected for examination and a choice was made of those references which were to be included in the bibliography. The bibliography has both primary and secondary references. Although the monograph does not cover hot atom chemistry, the kinetics of exchange reactions, decay schemes, or physiological applications, papers in these areas were examined as possible sources of useful preparative and analytical procedures

  8. Introduction to radiochemistry

    International Nuclear Information System (INIS)

    Malcolme-Lawes, D.J.

    1979-01-01

    This book provides an up-to-date account of radiochemical techniques for the student chemist new to the field. Among the topics covered are the major types of radioactive decay and the principal sources of radioisotopes, basic techniques for the detection and measurement of the most important classes of radioactivity and the elements of statistics needed for counting radioactivity. Further chapters are devoted to liquid scintillation counting, elements of γ-spectrometry, the principles of modern radiochromatography, a description of the most commonly used analytical applications of radiochemical techniques, the preparation of radiolabelled compounds from readily available radioactive materials, and aspects of the purity and stability of labelled compounds along with the most important features of how conditions of storage affect these properties. The final chapter introduces the basic principles of safe working with radioactive materials. (author)

  9. Radiochemistry of ruthenium

    Energy Technology Data Exchange (ETDEWEB)

    Schulz, W W; Metcalf, S G; Barney, G S

    1984-06-01

    Information on ruthenium is presented. Topics include the following; isotopes and nuclear properties of ruthenium; review of the chemistry of ruthenium including metal and alloys, compounds of ruthenium, and solution chemistry; separation methods including volatilization of RuO{sub 4}, precipitation and coprecipitation, solvent extraction, chromatographic techniques, and analysis for radioruthenium. 445 refs., 7 figs., 23 tabs.

  10. Radiochemistry of ruthenium

    International Nuclear Information System (INIS)

    Schulz, W.W.; Metcalf, S.G.; Barney, G.S.

    1984-01-01

    Information on ruthenium is presented. Topics include the following; isotopes and nuclear properties of ruthenium; review of the chemistry of ruthenium including metal and alloys, compounds of ruthenium, and solution chemistry; separation methods including volatilization of RuO 4 , precipitation and coprecipitation, solvent extraction, chromatographic techniques, and analysis for radioruthenium. 445 refs., 7 figs., 23 tabs

  11. Electromigration method in radiochemistry

    International Nuclear Information System (INIS)

    Makarova, T.P.; Stepanov, A.V.

    1977-01-01

    Investigations are reviewd of the period 1969-1975 accomplished by such methods as zonal electrophoresis in countercurrent, focusing electrophoresis, isotachophoresis, electrophoresis with elution, continuous two-dimensional electrophoresis. Since the methods considered are based on the use of porous fillers for stabilizing the medium, some attention is given to the effect of the solid-solution interface on the shape and rate of motion of the zones of the rare-earth elements investigated, Sr and others. The trend of developing electrophoresis as a method for obtaining high-purity elements is emphasized

  12. Qualilty, isotopes, and radiochemistry of water sampled from the Upper Moenkopi Village water-supply wells, Coconino County, Arizona

    Science.gov (United States)

    Carruth, Rob; Beisner, Kimberly; Smith, Greg

    2013-01-01

    The Hopi Tribe Water Resources Program has granted contracts for studies to evaluate water supply conditions for the Moenkopi villages in Coconino County, Arizona. The Moenkopi villages include Upper Moenkopi Village and the village of Lower Moencopi, both on the Hopi Indian Reservation south of the Navajo community of Tuba City. These investigations have determined that water supplies are limited and vulnerable to several potential sources of contamination, including the Tuba City Landfill and a former uranium processing facility known as the Rare Metals Mill. Studies are ongoing to determine if uranium and other metals in groundwater beneath the landfill are greater than regional groundwater concentrations. The source of water supply for the Upper Moenkopi Village is three public-supply wells. The wells are referred to as MSW-1, MSW-2, and MSW-3 and all three wells obtain water from the regionally extensive N aquifer. The N aquifer is the principal aquifer in this region of northern Arizona and consists of thick beds of sandstone between less permeable layers of siltstone and mudstone. The relatively fine-grained character of the N aquifer inhibits rapid movement of water and large yields to wells. In recent years, water levels have declined in the three public-supply wells, causing concern that the current water supply will not be able to accommodate peak demand and allow for residential and economic growth. Analyses of major ions, nutrients, selected trace metals, stable and radioactive isotopes, and radiochemistry were performed on the groundwater samples from the three public-supply wells to describe general water-quality conditions and groundwater ages in and immediately surrounding the Upper Moenkopi Village area. None of the water samples collected from the public-supply wells exceeded the U.S. Environmental Protection Agency primary drinking water standards. The ratios of the major dissolved ions from the samples collected from MSW-1 and MSW-2 indicate

  13. Condensate and feedwater systems, pumps, and water chemistry. Volume seven

    International Nuclear Information System (INIS)

    Anon.

    1986-01-01

    Subject matter includes condensate and feedwater systems (general features of condensate and feedwater systems, condenser hotwell level control, condensate flow, feedwater flow), pumps (principles of fluid flow, types of pumps, centrifugal pumps, positive displacement pumps, jet pumps, pump operating characteristics) and water chemistry (water chemistry fundamentals, corrosion, scaling, radiochemistry, water chemistry control processes, water pretreatment, PWR water chemistry, BWR water chemistry, condenser circulating water chemistry

  14. YoungRad-seminar. Proceedings. Seminar for young scientists in the fields of radiophysics, radiochemistry, radioecology, radiation protection and related fields

    International Nuclear Information System (INIS)

    Straelberg, E.; Sidhu, R.; Petersen, R.; Salminen, S.

    2007-09-01

    To provide an inspiring working environment for young students and scientists, it is important that they at an early stage can take part in a network of scientists working in their fields of interest. However, within each of the five Nordic countries the network of people involved in the fields of radiophysics, radiochemistry, radioecology, radiation protection and other related fields is rather small. Educational networking is a key factor in keeping young researchers motivated to continue working within these fields, and to recruit new students. For that reason the first YoungRad-seminar was held in Helsinki 14-15 December 2006. 43 young participants including MSc and PhD students at universities, researchers at different institutes and personnel from Nordic authorities took part in the seminar. All Nordic countries except Iceland were represented. The seminar was divided into four sessions including oral and poster presentations. In addition two senior researchers were invited to speak about Nordic radioecology and NKS. This report contains the abstracts and presentations made at the seminar. (au)

  15. Automated radiosynthesis of no-carrier-added 4-[18F]fluoroiodobenzene: a versatile building block in 18F radiochemistry.

    Science.gov (United States)

    Way, Jenilee Dawn; Wuest, Frank

    2014-02-01

    4-[18F]Fluoroiodobenzene ([18F]FIB) is a versatile building block in 18F radiochemistry used in various transition metal-mediated C-C and C-N cross-coupling reactions and [18F]fluoroarylation reactions. Various synthesis routes have been described for the preparation of [18F]FIB. However, to date, no automated synthesis of [18F]FIB has been reported to allow access to larger amounts of [18F]FIB in high radiochemical and chemical purity. Herein, we describe an automated synthesis of no-carrier-added [18F]FIB on a GE TRACERlab™ FX automated synthesis unit starting from commercially available(4-iodophenyl)diphenylsulfonium triflate as the labelling precursor. [18F]FIB was prepared in high radiochemical yields of 89 ± 10% (decay-corrected, n = 7) within 60 min, including HPLC purification. The radiochemical purity exceeded 95%, and specific activity was greater than 40 GBq/μmol. Typically, from an experiment, 6.4 GBq of [18F]FIB could be obtained starting from 10.4 GBq of [18F]fluoride.

  16. YoungRad-seminar. Proceedings. Seminar for young scientists in the fields of radiophysics, radiochemistry, radioecology, radiation protection and related fields

    Energy Technology Data Exchange (ETDEWEB)

    Straelberg, E; Sidhu, R [Institute for Energy Technology (Norway); Petersen, R [Technological Univ. of Denmark (Denmark); Salminen, S [Univ. of Helsinki (Finland)

    2007-09-15

    To provide an inspiring working environment for young students and scientists, it is important that they at an early stage can take part in a network of scientists working in their fields of interest. However, within each of the five Nordic countries the network of people involved in the fields of radiophysics, radiochemistry, radioecology, radiation protection and other related fields is rather small. Educational networking is a key factor in keeping young researchers motivated to continue working within these fields, and to recruit new students. For that reason the first YoungRad-seminar was held in Helsinki 14-15 December 2006. 43 young participants including MSc and PhD students at universities, researchers at different institutes and personnel from Nordic authorities took part in the seminar. All Nordic countries except Iceland were represented. The seminar was divided into four sessions including oral and poster presentations. In addition two senior researchers were invited to speak about Nordic radioecology and NKS. This report contains the abstracts and presentations made at the seminar. (au)

  17. Design of compact system with wide electron beam for radiation technologies

    International Nuclear Information System (INIS)

    Korolyov, A.N.; Simonov, K.G.; Pirozhenko, V.M.

    2001-01-01

    Design of a compact system for radiation processing of products and materials has been developed. The system provides two modes of irradiation, i.e. irradiation of continuously moving tapes and fixed samples. The irradiation is performed in a hermetically sealed chamber filled by nitrogen. This ecologically pure system includes the radiation protection,autonomous water cooling system and automated PC-control. It can be placed in any production or clinical room

  18. Design of compact system with wide electron beam for radiation technologies

    CERN Document Server

    Korolyov, A N; Pirozhenko, Vitaly M

    2001-01-01

    Design of a compact system for radiation processing of products and materials has been developed. The system provides two modes of irradiation, i.e. irradiation of continuously moving tapes and fixed samples. The irradiation is performed in a hermetically sealed chamber filled by nitrogen. This ecologically pure system includes the radiation protection,autonomous water cooling system and automated PC-control. It can be placed in any production or clinical room.

  19. Performance characterization of the PET-CT tomograph at the PET-cyclotron-radiochemistry site of Messina University

    Directory of Open Access Journals (Sweden)

    Andrea F. Abate

    2015-11-01

    Full Text Available The paper presents a face recognition system based on 3D features with the aim of verifying the identity of subjects accessing a controlled Ambient Intelligence Environment and customizing all the services accordingly. The proposed approach relies on stereoscopic face acquisition and 3D mesh reconstruction avoiding non-automated and expensive 3D scanners, unsuitable for real time applications in general. A bidimensional feature descriptor is extracted from each 3D mesh. It consists in a color image transferring face's 3D features in a 2D space. An automatic weighting mask of each authorized person improves the robustness of recognition in presence of diverse facial expressions and beard. The experiments conducted show high average recognition rate and a measurable effectiveness of both flesh mask and expression weighting mask.

  20. Synthesis, radiochemistry and biological evaluation of a new somatostatin analogue (SDZ 219-387) labelled with technetium-99m

    International Nuclear Information System (INIS)

    Maina, T.; Stolz, B.; Albert, R.; Bruns, C.; Koch, P.; Maecke, H.

    1994-01-01

    A new derivative of octreotide SDZ 219-387 [PnAO-(D)Phe 1 -octreotide] was synthesized, which binds specifically and with high affinity to somatostatin receptors in vitro (pK i =9.79±0.16). This new somatostatin analogue chelates technetium-99m under mild labelling conditions in good yields. The resulting [ 99m Tc]SDZ 219-387 was stable up to 6 h after labelling and could be isolated in a pure radiochemical and chemical form by high-perfomance liquid chromatographic purification. The intravenous administration of purified [ 99m Tc]SDZ 219-387 revealed that the radioligand was rapidly cleared from circulation, and tumour uptake of 0.38% ID/g was observed at 1.5 h post injection. [ 99m Tc]SDZ 219-387 specifically interacted with somatostatin binding sites on the tumour. However, the radioligand is highly lipophilic and excreted mainly through the hepatobiliary system. As a consequence, [ 99m Tc]SDZ 219-387 exhibits increased background activity and therefore is not appropriate for the in vivo visualization of somatostatin receptor-positive tumours and/or their metastases in the abdomen. (orig.)

  1. The dynamics of Cs-137 and Sr-90 pollution of surface water systems of Belarus of Chernobyl origin

    Energy Technology Data Exchange (ETDEWEB)

    Datskevich, P.O.; Dolgov, V.M.; Golikov, Yu.N.; Zemskov, V.N.; Komissarov, F.D.; Khvaley, O.D.

    1995-12-31

    The Belarus water ecosystems have been the object of investigation concerning currents and reservoirs affected by the Chernobyl APS catastrophe. The radio monitoring of samples of water systems components was implemented with the use of modern methods of radiochemistry and ionizing radiations registration. The factual material of water ecosystems sites observation presented its analysis is done and the regularities, tendencies and anomalies are revealed in the Cs-137 and Sr-90 distribution, transport and accumulation for water components.

  2. Development of theme in radiochemistry

    International Nuclear Information System (INIS)

    Homma, Yoshio; Morita-Murase, Yuko

    2001-01-01

    The disintegration rates of 222 Rn and its daughters in natural water were determined successfully by the use of the integral counting method with a liquid scintillation spectrometer. A significant advantage of this method is its freedom from the quenching effect. Moreover, when plural α, and β-emitters are present, their total amounts can be determined. The simple extrapolation of integral counting curve to zero pulse-height, however, do not give the true disintegration rate for the soft β-emitters (Emax 3 H samples, and a modified integral counting method which extrapolates the integral counting curve to the zero detection threshold was proposed. The method has been successfully applied to various β-emitters, 222 Rn samples, and coloured samples of β-emitters, giving more accurate absolute disintegration rate than the conventional integral counting method and the efficiency tracing method. In the course of the study determining 222 Rn by liquid scintillation counting, we observed unexpected phenomena; the air luminescence from gaseous space above LS, and the temperature dependence of pulse-height spectra. As for the former phenomenon, we proposed a method for correcting errors due to air luminescence, a method for determining α-emitters by the air luminescence, and a rapid calibration method for 222 Rn detectors. As for the latter phenomenon, we observed that the pulse-height spectra for α, and β-emitters in LS are shifted toward higher pulse-height with decreasing temperature. We found that the fluorescence intensities of the solvent of LS (toluene) is promoted at lower temperatures, and that not only toluene, but also the fluorescence intensity of a number of aromatic hydrocarbons and aliphatic hydrocarbons show the same effect as toluene. Other unexpected results are existence of metals in umber of enzymes, and discrepancies between the experimental value for Kurie plot of allowed β-emitters and the value which would be expected according to Fermi's theory, the results of which would affect the transmission probability of potential barrier for α-particles. (author)

  3. Radiochemistry in nuclear medicine. Radiopharmaceuticals

    International Nuclear Information System (INIS)

    Samochocka, K.

    1999-01-01

    Radionuclides and radiopharmaceuticals play a kay role in nuclear medicine, both in diagnostics and therapy. Incorporation of radionuclides into biomolecules, and syntheses of radiolabelled compounds of high biological selectivity are a task for radiochemists working in the multidisciplinary field of radiopharmaceutical chemistry. The most commonly used radionuclide, 99m Tc, owes this popularity to its both nearly ideal nuclear properties in respect to medical imaging, and availability from inexpensive radionuclide generators. Also numerous other radionuclides are widely used for medical imaging and therapy. Labelling of biomolecules with radioiodine and various positron emitters is getting increasingly important. This review describes some chemical and radiochemical problems we meet while synthesizing and using 99m Tc-radiopharmaceuticals and radioiodine-labelled biomolecules. Also represented are the recent developments in the design and use of the second generation radiopharmaceuticals based on bifunctional radiochelates. Several principal routes of fast chemical synthesis concerning incorporation of short-lived positron emitters into biomolecules are outlined as well. The search for chemical structures of high biological selectivity, which would be activated by slow neutrons, is related to the method of Neutron Capture Therapy, an interesting option in nuclear medicine. (author)

  4. The suicidal success of radiochemistry

    International Nuclear Information System (INIS)

    Badash, L.

    1979-01-01

    An historical account is given of the work carried out between about 1911 and 1922 on the chemistry and radioactive decay of the radioelements; in particular the studies by Soddy and others leading to the interpretation of the group displacement laws of decay, the acceptance of the theory of isotopy and the comparison of atomic weights of lead from radioactive and from non-radioactive sources. (U.K.)

  5. Radiochemistry and radiopolymerization of polysaccharides

    International Nuclear Information System (INIS)

    Raffi, J.

    1980-03-01

    The effects of gamma radiation on dry state polysaccharides (example: starch) are presented in an overall manner by order of quantitative importance: recombination of radicals to recover the initial macromolecule (cage effect) or smaller molecules which are chemically identical (radiopolymerization) and evolution of radicals to give secondary reactions (formation of radiolysis products). The effect of the botanical origin of the starch studied is briefly discussed, applications and extensions to the case of radiochemically induced modifications to foodstuffs being envisaged [fr

  6. Forty years of radiochemistry education

    International Nuclear Information System (INIS)

    Preiss, I.L.

    1990-01-01

    Overman and Clark began filling the need for the formal education of nuclear scientists versed in chemistry, at the Oak Ridge Institute. In 1947 Clark began the program at Rensselaer that has continued through to today. The evolution of course content, the laboratory programs and complementary course work in other disciplines will be discussed. Educational and logistical concerns will be addressed. The prospects for continuation of both theory and laboratory programs, the student interest and financial support for course development and equipment needs are concerns that will be presented

  7. Management of radioactive waste gases from PET radiopharmaceutical synthesis using cost effective capture systems integrated with a cyclotron safety system.

    Science.gov (United States)

    Stimson, D H R; Pringle, A J; Maillet, D; King, A R; Nevin, S T; Venkatachalam, T K; Reutens, D C; Bhalla, R

    2016-09-01

    The emphasis on the reduction of gaseous radioactive effluent associated with PET radiochemistry laboratories has increased. Various radioactive gas capture strategies have been employed historically including expensive automated compression systems. We have implemented a new cost-effective strategy employing gas capture bags with electronic feedback that are integrated with the cyclotron safety system. Our strategy is suitable for multiple automated 18 F radiosynthesis modules and individual automated 11 C radiosynthesis modules. We describe novel gas capture systems that minimize the risk of human error and are routinely used in our facility.

  8. Software framework developed for the slice test of the ATLAS endcap muon trigger system

    CERN Document Server

    Komatsu, S; Ishida, Y; Tanaka, K; Hasuko, K; Kano, H; Matsumoto, Y; Yakamura, Y; Sakamoto, H; Ikeno, M; Nakayoshi, K; Sasaki, O; Yasu, Y; Hasegawa, Y; Totsuka, M; Tsuji, S; Maeno, T; Ichimiya, R; Kurashige, H

    2002-01-01

    A sliced system test of the ATLAS end cap muon level 1 trigger system has been done in 2001 and 2002 separately. We have developed an own software framework for property and run controls for the slice test in 2001. The system is described in C++ throughout. The multi-PC control system is accomplished using the CORBA system. We have then restructured the software system on top of the ATLAS online software framework, and used this one for the slice test in 2002. In this report we discuss two systems in detail with emphasizing the module property configuration and run control. (8 refs).

  9. Pneumatic transport systems for TRIGA reactors

    International Nuclear Information System (INIS)

    Bolton, John A.

    1970-01-01

    Main parameters and advantages of pneumatically operated systems, primarily those operated by gas pressure are discussed. The special irradiation ends for the TRIGA reactor are described. To give some idea of the complexity of some modern systems, the author presents the large system currently operating at the National Bureau of Standards in Washington. In this system, 13 stations are located throughout the radiochemistry laboratories and three irradiation ends are located in the reactor, which is a 14-megawatt unit. The system incorporates practically every fail-safe device possible, including ball valves located on all capsule lines entering the reactor area, designed to close automatically in the event of a reactor scram, and at that time capsules within the reactor would be diverted by means of switches located on the inside of the reactor wall. The whole system is under final control of a permission control panel located in the reactor control room. Many other safety accessories of the system are described

  10. Welding technology transfer task/laser based weld joint tracking system for compressor girth welds

    Science.gov (United States)

    Looney, Alan

    1991-01-01

    Sensors to control and monitor welding operations are currently being developed at Marshall Space Flight Center. The laser based weld bead profiler/torch rotation sensor was modified to provide a weld joint tracking system for compressor girth welds. The tracking system features a precision laser based vision sensor, automated two-axis machine motion, and an industrial PC controller. The system benefits are elimination of weld repairs caused by joint tracking errors which reduces manufacturing costs and increases production output, simplification of tooling, and free costly manufacturing floor space.

  11. Version 1.00 programmer's tools used in constructing the INEL RML/analytical radiochemistry sample tracking database and its user interface

    International Nuclear Information System (INIS)

    Femec, D.A.

    1995-09-01

    This report describes two code-generating tools used to speed design and implementation of relational databases and user interfaces: CREATE-SCHEMA and BUILD-SCREEN. CREATE-SCHEMA produces the SQL commands that actually create and define the database. BUILD-SCREEN takes templates for data entry screens and generates the screen management system routine calls to display the desired screen. Both tools also generate the related FORTRAN declaration statements and precompiled SQL calls. Included with this report is the source code for a number of FORTRAN routines and functions used by the user interface. This code is broadly applicable to a number of different databases

  12. Spatial Trends and Variability of Vertical Accretion Rates in the Barataria Basin, Louisiana, U.S.A. using Pb-210 and Cs-137 radiochemistry

    Science.gov (United States)

    Shrull, S.; Wilson, C.; Snedden, G.; Bentley, S. J.

    2017-12-01

    Barataria Basin on the south Louisiana coast is experiencing some of the greatest amounts of coastal land loss in the United States with rates as high as 23.1 km2 lost per year. In an attempt to help slow or reverse land loss, millions of dollars are being spent to create sediment diversions to increase the amount of available inorganic sediments to these vulnerable coastal marsh areas. A better understanding of the spatial trends and patterns of background accretion rates needs to be established in order to effectively implement such structures. Core samples from 25 Coastwide Reference Monitoring System (CRMS) sites spanning inland freshwater to coastal saline areas within the basin were extracted, and using vertical accretion rates from Cs-137 & Pb-210 radionuclide detection, mineral versus organic sediment composition, grain size distribution, and spatial trends of bulk densities, the controls on the accretion rates of the marsh soils will be constrained. Initial rates show a range from 0.31 cm/year to 1.02 cm/year with the average being 0.79 cm/year. Preliminary results suggest that location and proximity to an inorganic sediment source (i.e. river/tributary or open water) have a stronger influence on vertical accretion rates than marsh classification and salinity, with no clear relationship between vertical accretion and salinity. Down-core sediment composition and bulk density analyses observed at a number of the sites likely suggest episodic sedimentation and show different vertical accretion rates through time. Frequency and length of inundation (i.e. hydroperiod), and land/marsh classification from the CRMS data set will be further investigated to constrain the spatial variability in vertical accretion for the basin.

  13. Analytical and Radiochemistry for Nuclear Forensics

    Energy Technology Data Exchange (ETDEWEB)

    Steiner, Robert Ernest [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Dry, Donald E. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Kinman, William Scott [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Podlesak, David [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Tandon, Lav [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2015-05-26

    Information about nonproliferation nuclear forensics, activities in forensics at Los Alamos National Laboratory, radio analytical work at LANL, radiochemical characterization capabilities, bulk chemical and materials analysis capabilities, and future interests in forensics interactions.

  14. Radiochemistry Division annual progress report 1989

    International Nuclear Information System (INIS)

    1990-01-01

    The research and development activities of the Division during 1989 are briefly described in the form of individual summaries arranged under the headings: (1)Nuclear chemistry, (2)Actinide chemistry, and (3)Spectroscopy. In the field of nuclear chemistry, main emphasis is on studies in fission chemistry. R and D work in actinide chemistry area is oriented towards study of solvent extraction behaviour of actinide ions from aqueous solutions. The spectroscpoic studies are mainly concerned with EPR investigations. A list of publications by the scientist of the division is given at the end. (author). 22 figs., 39 tabs

  15. Frederick Soddy: Early pioneer in radiochemistry

    International Nuclear Information System (INIS)

    Kauffman, G.B.

    1985-01-01

    It is only by careful study of the lives, works and writings of some of the principal figures in the early period of research into radioactivity that historians can reconstruct the actual events leading up to our modern-day understanding of complex phenomena. One such leading figure was Frederick Soddy (1877-1956), whose life and work are examined here by internationally recognized authorities in the history of science. The reception of Soddy's ideas in Japan and the U.S.S.R. is also considered, providing insight into the international commerce of ideas in the inter-war period. The articles collected in this book, complemented by Soddy's own keynote papers, form a rounded picture of Soddy the man, his life, his work and the impact he had on the society of his time

  16. Radiochemistry and its application to nuclear medicine

    International Nuclear Information System (INIS)

    Welch, J.J.

    1990-01-01

    The role of the radiochemist in Nuclear Medicine has increased since the early 1960's. At that time the first medical 99 Mo/ 99m /Tc generator was developed at Brookhaven National Laboratory and the first hospital based cyclotron installed at Washington University. Radiochemists have been involved in both the development and application of generator and accelerator based radiopharmaceuticals. The development of oxygen-15, nitrogen 13, carbon-11 and fluorine-18 simple compound and synthetic precursors will be discussed. In recent years new high current accelerators have been proposed from Nuclear Medicine isotope production. Generator produced radiopharmaceuticals continue to play a major role in Nuclear Medicine. Problems in the development of targetry to produce parent nuclides as well as challenges in generator development will be described

  17. Advanced facilities for radiochemistry at Harwell

    International Nuclear Information System (INIS)

    1985-01-01

    The leaflets in this folder describe the latest addition to Harwell's active handling capability. This is a high level alpha, beta, gamma facility designed specifically for undertaking chemical research and development work. It is based on using high integrity containment boxes which are housed in concrete shielded enclosures. The active boxes can be removed and transferred remotely to a support area where they, and any associated equipment, can be decontaminated and serviced whilst a new fully commissioned box can be readily brought into service. The facility fulfills the principle of ALARA and is sufficiently flexible to accommodate a wide range of active handling requirements. It is supported by a suite of medium active handling cells, radiochemical laboratories and, as necessary, facilities of other scientific and engineering disciplines. The leaflets are: report on conceptual aspects; Techsheet 'Remote handling facility - Salient information'; Techsheet 'Project capabilities'; and 4 sheets of diagrams showing details of the facility. (U.K.)

  18. Nuclear Forensics and Radiochemistry: Reaction Networks

    Energy Technology Data Exchange (ETDEWEB)

    Rundberg, Robert S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-11-22

    In the intense neutron flux of a nuclear explosion the production of isotopes may occur through successive neutron induced reactions. The pathway to these isotopes illustrates both the complexity of the problem and the need for high quality nuclear data. The growth and decay of radioactive isotopes can follow a similarly complex network. The Bateman equation will be described and modified to apply to the transmutation of isotopes in a high flux reactor. A alternative model of growth and decay, the GD code, that can be applied to fission products will also be described.

  19. Nuclear and radiochemistry, 3rd edition

    International Nuclear Information System (INIS)

    Friedlander, G.; Kennedy, J.W.; Macias, E.S.; Miller, J.M.

    1981-01-01

    A broad coverage of radioactivity and nuclear phenomena fundamentals is presented, followed by discussions of applications in such fields as basic chemistry, biology, medicine, earth and space sciences. Following an introductory historical chapter, the basic fundamentals of nuclear properties, radioactive growth and decay, and nuclear reactions are covered in the first five chapters. Chapters 6-10 deal mainly with topics essential to the practicing radiochemist. They include discussion of interactions of radiation with matter, radiation detection and measurement, techniques in nuclear chemistry, statistics and radioactivity and nuclear models. Applications of these disciplines in the various fields noted above together with chapters on nuclear energy and sources of nuclear bombarding particles complete the 15 chapters of the book

  20. Nuclear Forensics and Radiochemistry: Radiation Detection

    Energy Technology Data Exchange (ETDEWEB)

    Rundberg, Robert S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-11-08

    Radiation detection is necessary for isotope identification and assay in nuclear forensic applications. The principles of operation of gas proportional counters, scintillation counters, germanium and silicon semiconductor counters will be presented. Methods for calibration and potential pitfalls in isotope quantification will be described.

  1. Collected radiochemical procedures (radiochemistry group CNC-11)

    Energy Technology Data Exchange (ETDEWEB)

    Smith, H.L. (ed.)

    1975-04-01

    Separation techniques are given for: Am, Sb, As, Ba, Be, Bi, C, Cd, Ca, Ce, Cs, Cl, Cr, Co, Cm, Ge, Au, In, Fe, lanthanides, Pb, Mg, Mn, Mo, Np, Ni, Nb, Pd, P, Pu, Pa, Rh, Ru, Sc, Ag, Na, Sr, sulfate, Ta, Te, Tl, Th, Sn, transactinides, tritium, W, U, Y, and Zr. Combined procedures and group separations of the heavy elements are also included. (DLC)

  2. Experimental nuclear and radiochemistry. Progress report, 1981

    International Nuclear Information System (INIS)

    Karol, P.J.

    1981-09-01

    Research progress is reported on the following topics: (1) the importance of classical nucleon-nucleon spatial correlations on nuclear interactions; (2) mathematical development of properly behaved skewed Gaussian function; (3) cluster interactions and true pion absorption; and (4) anomalous relativistic heavy-ion projectile fragments

  3. Nuclear Forensics and Radiochemistry: Radiation Detection

    International Nuclear Information System (INIS)

    Rundberg, Robert S.

    2017-01-01

    Radiation detection is necessary for isotope identification and assay in nuclear forensic applications. The principles of operation of gas proportional counters, scintillation counters, germanium and silicon semiconductor counters will be presented. Methods for calibration and potential pitfalls in isotope quantification will be described.

  4. Collected radiochemical procedures (radiochemistry group CNC-11)

    International Nuclear Information System (INIS)

    Smith, H.L.

    1975-04-01

    Separation techniques are given for: Am, Sb, As, Ba, Be, Bi, C, Cd, Ca, Ce, Cs, Cl, Cr, Co, Cm, Ge, Au, In, Fe, lanthanides, Pb, Mg, Mn, Mo, Np, Ni, Nb, Pd, P, Pu, Pa, Rh, Ru, Sc, Ag, Na, Sr, sulfate, Ta, Te, Tl, Th, Sn, transactinides, tritium, W, U, Y, and Zr. Combined procedures and group separations of the heavy elements are also included

  5. Nuclear Forensics and Radiochemistry: Cross Sections

    Energy Technology Data Exchange (ETDEWEB)

    Rundberg, Robert S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-11-08

    The neutron activation of components in a nuclear device can provide useful signatures of weapon design or sophistication. This lecture will cover some of the basics of neutron reaction cross sections. Nuclear reactor cross sections will also be presented to illustrate the complexity of convolving neutron energy spectra with nuclear excitation functions to calculate useful effective reactor cross sections. Deficiencies in the nuclear database will be discussed along with tools available at Los Alamos to provide new neutron cross section data.

  6. 7. Methods of work in radiochemistry

    International Nuclear Information System (INIS)

    Majer, V.

    1981-01-01

    Radiochemical operating techniques are briefly characterized and the basic differences are shown in handling chemical and radioactive materials. Radiochemical techniques are determined by the aspect of operation where the criterium consists either of the quantity of material, activity or the properties of the radionuclide. Main principles are shown of trace techniques, microchemical techniques and techniques of work with high-level radioactive material. The basic hygienic principles are also shown of handling radioactive materials. (B.S.)

  7. Frontiers of heavy element nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Hoffman, D.C.

    1999-01-01

    The production and half-lives of the heaviest chemical elements, now known through Z=112, are reviewed. Recent experimental evidence for the stabilization of heavy element isotopes due to proximity to deformed nuclear shells at Z=108 and N=162 is compared with the theoretical predictions. The possible existence of isotopes of elements 107-110 with half-lives of seconds or longer, and production reactions and experimental techniques for increasing the overall yields of such isotopes in order to study both their nuclear and chemical properties are discussed. The present status of studies of the chemical properties of Rf, Ha, and Sg is briefly summarized and prospects for extending chemical studies beyond Sg are considered. (author)

  8. Radiochemistry Division: annual progress report: 1987

    International Nuclear Information System (INIS)

    1989-01-01

    The progress of Research and Development (R and D) activities during the year 1987 are reported in the form of summaries, which are presented under the headings (1) Actinide Chemistry, (2) Nuclear Chemistry, and (3) Spectroscopy. Microwave absorption studies of the high Tsub(c) oxide superconductor YBa 2 Cu 3 Osub(7-x) using electron paramagnetic resonance techniques are the new feature during the report year. Radioanalytical services and radiation sources in the form of electrodeposited sources or standard soluti ons were also given to the other Divisions, other units of the Department of Atomic Energy, and other organisations in the country. A list of papers by the members of the Division published in various journals and presented at various symposia, conferences etc. is given at the end of the report. (M.G.B.). refs., 51 tabs., 33 figs

  9. Nuclear- and radiochemistry. Vol. 2. Modern applications

    International Nuclear Information System (INIS)

    Roesch, Frank

    2016-01-01

    This work is conceived to meet the demand of state-of-the-art literature to teach the fundamentals as well as the modern applications of nuclear chemistry. The work will consist of two volumes: the first one covering the basics of nuclear chemistry such as the relevant parameters of instable atomic nuclei, the various modi of radioactive transmutations, the corresponding types of radiation including their detection and dosimetry, and finally the mechanisms of nuclear reactions. The second volume addresses relevant fields of nuclear chemistry, such as the chemistry of radioactive elements, application of radioactive nuclei in life sciences, nuclear energy, waste managements and environmental aspects, radiochemical separations, radioanalytical and spectroscopic methods, etc. Here, leading experts will contribute up-to-date knowledge on the most important application of nuclear chemistry.

  10. The research on algorithms for optoelectronic tracking servo control systems

    Science.gov (United States)

    Zhu, Qi-Hai; Zhao, Chang-Ming; Zhu, Zheng; Li, Kun

    2016-10-01

    The photoelectric servo control system based on PC controllers is mainly used to control the speed and position of the load. This paper analyzed the mathematical modeling and the system identification of the servo system. In the aspect of the control algorithm, the IP regulator, the fuzzy PID, the Active Disturbance Rejection Control (ADRC) and the adaptive algorithms were compared and analyzed. The PI-P control algorithm was proposed in this paper, which not only has the advantages of the PI regulator that can be quickly saturated, but also overcomes the shortcomings of the IP regulator. The control system has a good starting performance and the anti-load ability in a wide range. Experimental results show that the system has good performance under the guarantee of the PI-P control algorithm.

  11. A 7MeV S-Band 2998MHz Variable Pulse Length Linear Accelerator System

    CERN Document Server

    Hernandez, Michael; Mishin, Andrey V; Saverskiy, Aleksandr J; Skowbo, Dave; Smith, Richard

    2005-01-01

    American Science and Engineering High Energy Systems Division (AS&E HESD) has designed and commissioned a variable pulse length 7 MeV electron accelerator system. The system is capable of delivering a 7 MeV electron beam with a pulse length of 10 nS FWHM and a peak current of 1 ampere. The system can also produce electron pulses with lengths of 20, 50, 100, 200, 400 nS and 3 uS FWHM with corresponding lower peak currents. The accelerator system consists of a gridded electron gun, focusing coil, an electrostatic deflector system, Helmholtz coils, a standing wave side coupled S-band linac, a 2.6 MW peak power magnetron, an RF circulator, a fast toroid, vacuum system and a PLC/PC control system. The system has been operated at repetition rates up to 250pps. The design, simulations and experimental results from the accelerator system are presented in this paper.

  12. Development of remote control integrator system on Tokamak

    International Nuclear Information System (INIS)

    Wu Yichun; Wang Lingzhi; Shu Shuangbao

    2014-01-01

    In order to meet with the requirement of electromagnetic diagnosis to the J-TEXT Tokamak, a remote control integrator system was developed. With modular design method, the integrator system is composed of the integrator cards, a control card, a linear power card and the BNC interface cards, and it uses the PC control soft- ware to conduct network control. An integrator system provides 32 integrator channels, and all integral channels have four kinds of integral time constants for remote selection and provide three kinds of integrator running control methods. According to laboratory and J-TEXT field testing, it shows that the output voltage range is -10-10 V, output noise is not more than 5 mV, and for the four kinds of integral time constants, the integral output drifts are all less than 5 mV within 100 s for each integrator channel. (authors)

  13. Development of computer-controlled ultrasonic image processing system for severe accidents research

    International Nuclear Information System (INIS)

    Koo, Kil Mo; Kang, Kyung Ho; Kim, Jong Tai; Kim, Jong Whan; Cho, Young Ro; Ha, Kwang Soon; Park, Rae Jun; Kim, Sang Baik; Kim, Hee Dong; Sim, Chul Moo

    2000-07-01

    In order to verify in-vessel corium cooling mechanism, LAVA(Lower-plenum Arrested Vessel Attack) experiment is being performed as a first stage proof of principle test. The aims of this study are to find a gap formation between corium melt and reactor lower head vessel, to verify the principle of the gap formation and to analyze the effect of the gap formation on the thermal behavior of corium melt and the lower plenum. This report aims at developing a computer controlled image signal processing system which is able to improve visualization and to measure the gap distribution with 3-dimensional planar image using a time domain signal analysis method as a part of the ultrasonic pulse echo methods and a computerized position control system. An image signal processing system is developed by independently developing an ultrasonic image signal processing technique and a PC controlled position control system and then combining both systems

  14. Development of computer-controlled ultrasonic image processing system for severe accidents research

    Energy Technology Data Exchange (ETDEWEB)

    Koo, Kil Mo; Kang, Kyung Ho; Kim, Jong Tai; Kim, Jong Whan; Cho, Young Ro; Ha, Kwang Soon; Park, Rae Jun; Kim, Sang Baik; Kim, Hee Dong; Sim, Chul Moo

    2000-07-01

    In order to verify in-vessel corium cooling mechanism, LAVA(Lower-plenum Arrested Vessel Attack) experiment is being performed as a first stage proof of principle test. The aims of this study are to find a gap formation between corium melt and reactor lower head vessel, to verify the principle of the gap formation and to analyze the effect of the gap formation on the thermal behavior of corium melt and the lower plenum. This report aims at developing a computer controlled image signal processing system which is able to improve visualization and to measure the gap distribution with 3-dimensional planar image using a time domain signal analysis method as a part of the ultrasonic pulse echo methods and a computerized position control system. An image signal processing system is developed by independently developing an ultrasonic image signal processing technique and a PC controlled position control system and then combining both systems.

  15. Development of an automated modular system for the synthesis of [11C]acetate.

    Science.gov (United States)

    Felicini, Chiara; Någren, Kjell; Berton, Andrea; Pascali, Giancarlo; Salvadori, Piero Alberto

    2010-12-01

    Carboxylation reactions offer a straightforward method for the synthesis of carbon-11 labelled carboxylic acids. Among these, the preparation of carbon-11 (C)-acetate is receiving increasing attention because of diagnostic applications in oncology in addition to its well-established use as a probe for myocardial oxidative metabolism. Although a number of dedicated modules are commercially available, the development of the synthesis on flexible platforms would be beneficial to widen the number of tracers, in particular for preclinical assessment and testing. In this study, the carboxylation reaction was implemented for the synthesis of sodium 1-[C]acetate after the classic route of carboxylation of methylmagnesium chloride by [C]carbon dioxide, followed by the acidic hydrolysis, purification and sterile filtration. This was performed using a commercially available kit of preassembled hardware units and fully compatible components of radiochemistry automation (VarioSystem). The system proved be to highly versatile and inexpensive and allowed a quick translation of the radiochemistry project into a working system even by less experienced personnel, because of predefined interfaces between electronic parts and operating software (preloaded on a laptop and included in the kit). The automatic module proved to be a simple and reliable system for the production of 1-[C]acetate that was prepared in 24 min (total synthesis time) with stable radiochemical yields (20% nondecay corrected) and high radiochemical purity (>97%). The module is used routinely to produce 1-[C]acetate for preclinical studies and is being implemented for the production of the labelled fatty acids.

  16. Development of portable phased array UT system for real-time flaw imaging

    International Nuclear Information System (INIS)

    Goto, M.

    1995-01-01

    Many functions and features of phased array UT technology must be useful for NDE in the industrial field. Some phased array UT systems have been developed for the inspection of nuclear pressure vessel and turbine components. However, phased array UT is still a special NDE technique and it has not been used widely in the past. The reasons of that are system size, cost, operator performance, equipment design and others. TOSHIBA has newly developed PC controlled portable phased array system to solve those problems. The portable phased array UT system is very compact and light but it is able to drive up to 32-channel linear array probe, to display real-time linear/sector B-scan, to display accumulated B-scan with an encoder and to display profile overlaid B-scan. The first applications were turbine component inspections for precise flaw investigation and flaw image data recording

  17. Experiments with polymer coated microspheres irradiated by the Shiva laser system

    International Nuclear Information System (INIS)

    Auerbach, J.M.; Manes, K.R.; Matthews, D.L.

    1979-01-01

    Polymer coated spherical targets have been irradiated by the Shiva laser system in an effort to compress the contained 10 mg/cc DT fuel to super liquid densities. Glass microspheres of 140 μm ID and 5 μm wall thickness with polymer coatings 15 μm to 100 μm thick have been irradiated with laser pulses of 4 kilojoules in 200 psec FWHM. Target performance was diagnosed with neutron yield measurements, radiochemistry, Argon line imaging, and x-ray imaging techniques. Ball in plate targets achieved greater implosion symmetry than free-standing ball targets. With yields of 10 7 to 10 8 neutrons, targets reached DT fuel compressions of several times liquid density

  18. Systems

    International Nuclear Information System (INIS)

    Anon.

    1980-01-01

    Papers in this session describe the concept of mined geologic disposal system and methods for ensuring that the system, when developed, will meet all technical requirements. Also presented in the session are analyses of system parameters, such as cost and nuclear criticality potential, as well as a technical analysis of a requirement that the system permit retrieval of the waste for some period of time. The final paper discusses studies under way to investigate technical alternatives or complements to the mined geologic disposal system. Titles of the presented papers are: (1) Waste Isolation System; (2) Waste Isolation Economics; (3) BWIP Technical Baseline; (4) Criticality Considerations in Geologic Disposal of High-Level Waste; (5) Retrieving Nuclear Wastes from Repository; (6) NWTS Programs for the Evaluation of Technical Alternatives or Complements to Mined Geologic Repositories - Purpose and Objectives

  19. systems

    Directory of Open Access Journals (Sweden)

    Alexander Leonessa

    2000-01-01

    Full Text Available A nonlinear robust control-system design framework predicated on a hierarchical switching controller architecture parameterized over a set of moving nominal system equilibria is developed. Specifically, using equilibria-dependent Lyapunov functions, a hierarchical nonlinear robust control strategy is developed that robustly stabilizes a given nonlinear system over a prescribed range of system uncertainty by robustly stabilizing a collection of nonlinear controlled uncertain subsystems. The robust switching nonlinear controller architecture is designed based on a generalized (lower semicontinuous Lyapunov function obtained by minimizing a potential function over a given switching set induced by the parameterized nominal system equilibria. The proposed framework robustly stabilizes a compact positively invariant set of a given nonlinear uncertain dynamical system with structured parametric uncertainty. Finally, the efficacy of the proposed approach is demonstrated on a jet engine propulsion control problem with uncertain pressure-flow map data.

  20. Forschungszentrum Rossendorf, Institute of Radiochemistry. Annual report 1995

    International Nuclear Information System (INIS)

    Nitsche, H.

    1996-02-01

    The activities of the institute in the year 1995 are described by short communications. The themes of the chapters are: Speciation and migration of radionuclides; behaviour of colloids and aerosols; organic matter and their interaction with radionuclides; application of x-ray absorption spectroscopy; chemistry of heaviest elements. (SR)

  1. International conference on nuclear and radiochemistry (ICNR' 86)

    International Nuclear Information System (INIS)

    1986-11-01

    This publication contains the abstracts of the papers presented at the conference. A total of 288 abstracts are divided in the four areas: 1. Nuclear Reaction Chemistry; 2. Actinide Chemistry and Chemistry of Nuclear Fuel Cycle; 3. Radioanalytical Chemistry; 4. Radiopharmceuticals and Radiolabelled Compounds; and a General Session

  2. Marie Sklodowska-Curie, polonium, radium and radiochemistry

    International Nuclear Information System (INIS)

    Guillaumont, R.

    2011-01-01

    In this work, the author describes how the methodology developed by Marie Curie in discovering polonium and radium has contributed to greater scientific discoveries and how these discoveries have played a great part in the development of science in general and have particularly enriched chemistry. (O.M.)

  3. Integrated Manhattan Project for Excellence in Radiochemistry (IMPER)

    Energy Technology Data Exchange (ETDEWEB)

    Lewis, Jason

    2014-03-27

    Accomplishments are reported in these areas: single step radiolabeling of peptides with fluorine-18; photoreduction of 99Tc pertechnetate by nanometer-sized metal oxides for environmental remediation; synthesis and characterization of multi-modal CNT imaging constructs.

  4. An operating environment with multitasking capabilities for radiochemistry autosynthesizers

    International Nuclear Information System (INIS)

    Feliu, A.L.

    1991-01-01

    The proliferation of positron emission tomography centers during recent years has stimulated intensive efforts to develop reliable and efficient devices for automating radiopharmaceutical syntheses. In order to expedite the design and operation of fully automated synthesizers, a graphical process control scheme featuring a simple method for the end-user to reconfigure the software was recently suggested. The flexibility and user-friendliness of this scheme were demonstrated with an application package to operate a commercially-available autosynthesizer. This methodology is now extended to include multitasking capabilities. To evaluate the multitasking concept, the demonstration program AUTOMATE was created to simulate independent operation of four autosynthesizers. With AUTOMATE, a chemist could easily supervise one routine synthesis whole ''warming up'' another synthesizer or conducting a research experiment. The graphical approach provides the simplicity of manual control, instant status information, and a choice between ''hands-on'' or unattended operations. The potential utility of AUTOMATE in the laboratory is discussed. (author)

  5. Fuel failure assessments based on radiochemistry. Experience feedback and challenges

    International Nuclear Information System (INIS)

    Petit, C.; Ziabletsev, D.; Zeh, P.

    2015-01-01

    Significant improvements have been observed in LWR nuclear fuel reliability over the past years. As a result, the number of fuel failures in PWRs and BWRs has recently dramatically decreased. Nevertheless, a few remaining challenges still exist. One of them is that the industry has recently started seeing a relatively new type of fuel failure, so-called 'weak leak failures', which could be characterized by a very small release of gaseous fission products and essentially almost zero release of iodines or any other soluble fission products in the reactor coolant. Correspondingly, the behavior of these weak leakers does not follow typical behavior of a conventional leaker characterized by a proportionality of the amount of released Xe 133 related to the failed rod power. Instead, for a weak leaker, the activity of Xe 133 is directly correlated to the size of the cladding defects of the leaker. The presence of undetected weak leaker in the core may lead to carryover of a leaker into the subsequent cycle. Even if the presence of weak leaker in the core is suspected, it typically requires more effort to identify the leaker which could result in extended duration of the outage and ultimately to economic losses to the utility operating the reactor. To effectively deal with this issue the industry has been facing, several changes have been recently realized, which are different from the methodology of dealing with conventional leaker. These changes include new assessment methods, the need for improved sipping techniques to better identify low release leakers, and correspondingly better equipment to be able to locate small clad defects associated with weak leaker, such as sensitive localization device of failed rods, sensitive eddy current coil for the failed rod, ultra high definition cameras for the failed rod examination and experienced fuel reliability engineers performing cause of failure and rood cause research and analyses. Ultimately, the destructive methods of analysis such as hot cell examinations are also beneficial when non-destructive testing methods fail to identify the weak leaks

  6. Forschungszentrum Rossendorf, Institute of Radiochemistry. Annual report 1993

    International Nuclear Information System (INIS)

    Nitsche, H.; Bernhard, G.

    1994-06-01

    Since the founding of the Institute, a reorientation of the scientific direction was initiated: From the production and application of radioisotopes during the period before 1992 toward the new focus of radioecological research for risk assessment and remediation of radionuclide contaminations. The research relates to contamination problems from uranium mining in the German states of Saxony and Thuringia and in the neighboring Czech Republic, and from nuclear weapons production, testing, and accidents in the former Soviet Union. The new research direction of the Institute covers the essential aspects of radionuclide transport in the geo- and biosphere. It includes the distribution of radioactivity in ground- and surface waters and in air. We are studying the interaction of radioactive materials (a) at the interface between aqueous phase and rocks, minerals and soils, (b) the formation and distribution of colloids and aerosols, and (c) the mobilization and retardation of radionuclides through the interaction with organic contaminants and biological decay products. Our studies are essential for the successful development of environmental decontamination and remediation strategies. This report reflects the scientific transition of the Institute. The contributions to the section on ''Ecological Research'' are already focused toward the new challenge. The research that is summarized as ''General Research'' and ''Chemistry of the Heavy Elements'' clearly bear the elements of aerosol science. (orig.)

  7. Radiochemistry Results from the IER-163 COMET Irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Jackman, Kevin R. [Los Alamos National Laboratory; Bredeweg, Todd Allen [Los Alamos National Laboratory; Schake, Ann R. [Los Alamos National Laboratory; Oldham, Warren J. [Los Alamos National Laboratory; Bounds, John Alan [Los Alamos National Laboratory; Sanchez, Rene Gerardo [Los Alamos National Laboratory; Attrep, Moses [C-NR: NUCLEAR & RADIOCHEMISTRY; Rundberg, Robert S. [Los Alamos National Laboratory

    2015-08-07

    The COMET assembly at the National Criticality Experiments Research Center (NCERC) at the Nevada National Security Site (NNSS) was used to irradiate twelve foils in September 2011. The intention of this irradiation was to measure 'peak yield' fission product activities, activation products, and so-called 'endpoint R values' for different foil materials in a non-thermal neutron spectrum. After irradiation, several of the foils were shipped to Los Alamos National Laboratory (LANL) for radiochemical analysis. The results from the non-destructive and radiochemical analyses of six of these foils are presented.

  8. Summer school in nuclear and radiochemistry at Brookhaven National Laboratory

    International Nuclear Information System (INIS)

    Kolsky, K.L.

    2005-01-01

    The U.S. Department of Energy supports 24 fellowships for students to attend six-week programs at either San Jose State University in California, or Brookhaven National Laboratory (BNL) in New York. The American Chemical Society through the Division of Nuclear Science and Technology operates both schools. The twelve students at the BNL program are enrolled in the State University of New York at Stony Brook (SUNYSB) and receive 3 college credits for the lecture course (CHE-361) and 3 additional credits for the laboratory course (CHE-362). In addition to lectures and laboratories, students tour various nuclear facilities offsite, at BNL, and at SUNYSB. Opportunities are given the students to interact with faculty and scientists within the profession through the Guest Lecture Program. Further details are discussed along with results of student surveys for the years 1999 through 2002. (author)

  9. Regulatory requirements for radiopharmaceutical radiochemistry and radiation dosimetry

    International Nuclear Information System (INIS)

    Bonnyman, J.

    1985-01-01

    The Australian Department of Health is responsible for ensuring that radiopharmaceuticals are safe and effective and that their use does not result in unnecessary radiation exposure. Section B1 requirements of New Drug Form 4 (NDF4) fall into the following sections - manufacture, product specifications, quality assurance testing, stability studies and expiry dating. It covers ready to inject pharmaceuticals, radioactive formulations used to prepare a radiopharmaceutical, generators and cold kits

  10. Investigative radiochemistry. A key element in nuclear forensics

    International Nuclear Information System (INIS)

    Mayer, K.; Wallenius, M.; Varga, Z.; Wiss, T.; Fanghaenel, T.

    2011-01-01

    Since the fall of the Iron Curtain illicit trafficking of nuclear and radioactive material has become an issue of concern both on the political and the scientific level. Seized material may be analysed in order to obtain clues on its origin and intended use and to prevent diversion of material from the same source in the future. Nuclear materials (uranium or plutonium) are of particular worry due to the nuclear proliferation risk associated with the material. Nuclear forensic investigations are aimed at the fact that nuclear material carries (inherent) information on its history, including on its origin and the processes applied for its production. Important conclusions can be drawn from decay products, activation products and fission products. Chemical impurities and the isotopic composition of certain major and minor constituents may provide additional information. Comparison of the measured results with nuclear material databases may yield evidence on the production site. The paper will describe the methodologies developed for addressing the above issues, focussing on radiochemical methods. Examples of nuclear forensic casework will illustrate the experience gathered in these areas. (orig.)

  11. Nuclide migration and the environmental radiochemistry of Florida phosphogypsum

    International Nuclear Information System (INIS)

    Burnett, W.C.; Elzerman, A.W.

    2002-01-01

    Phosphogypsum, a waste by-product derived from the wet process production of phosphoric acid, represents one of the most serious problems facing the phosphate industry today. This by-product gypsum precipitates during the reaction of sulfuric acid with phosphate rock and is stored at a rate of about 40 million tons per year on several stacks in central and northern Florida. The main problem associated with this material concerns the relatively high levels of natural uranium-series radionuclides and other impurities which could impact the environment and which makes its commercial use impossible. We have studied the potential release of radionuclides from phosphogypsum by: (i) analysis of stack fluids, groundwaters, and soils associated with gypsum stacks; and (ii) geochemical modeling via MINTEQA2. Stack fluids were observed to be very high in dissolved uranium and 210 Pb with only moderate concentrations of 226 Ra. Underlying soils tend to be enriched in U and 210 Pb indicating precipitation when acidic stack fluids enter a buffered environment. Modeling results showed significant increases in radionuclide complexes with sulfate and phosphate, resulting in relatively mobile uncharged or negatively charged solution species within the stacks. On the other hand, precipitation of multicomponent solids would be expected with increasing pH below the stack. Our evidence thus suggests that while phosphogypsum stacks do contain significant quantities of dissolved radionuclides, removal mechanisms appear to prevent large scale migration of radionuclides to the underlying aquifer. (author)

  12. A mobile automatic gas chromatograph system to measure CO2, CH4 and N2O fluxes from soil in the field

    International Nuclear Information System (INIS)

    Silvola, J.; Martikainen, P.; Nykaenen, H.

    1992-01-01

    A caravan has been converted into mobile laboratory for measuring fluxes of CO 2 , CH 4 and N 2 O from the soil in the field. The caravan was equipped with a gas chromatograph fitted with TC-, FI- and EC-detectors, and a PC controlled data logger. The gas collecting chambers can be used up to 50 m from the caravan. The closing and opening of the chambers, as well as the flows of sample gases from chambers to the gas chromatograph. is pneumatically regulated. Simultaneous recordings of temperature, light intensity and the depth of water table are made. The system has been used for two months in 1992, and some preliminary results are presented

  13. SYSTEM

    Directory of Open Access Journals (Sweden)

    K. Swarnalatha

    2013-01-01

    Full Text Available Risk analysis of urban aquatic systems due to heavy metals turns significant due to their peculiar properties viz. persis tence, non-degradab ility, toxicity, and accumulation. Akkulam Veli (AV, an urba n tropical lake in south India is subjected to various environmental stresses due to multiple waste discharge, sand mining, developmental activities, tour ism related activitie s etc. Hence, a comprehensive approach is adopted for risk assessment using modified degree of contamination factor, toxicity units based on numerical sediment quality guidelines (SQGs, and potentialecological risk indices. The study revealed the presence of toxic metals such as Cr, C d, Pb and As and the lake is rated under ‘low ecological risk’ category.

  14. Separation systems for the nuclear industry: from system elaboration to its validation in radioactive environment

    International Nuclear Information System (INIS)

    Draye, Micheline

    2004-01-01

    -Particle Induced Desorption Mass Spectrometry (TOF-PDMS). This was its first use for the analysis of structural modifications of an organic material subjected to photonic type stress. The described research project illustrates the importance of examining and understanding the fundamental mechanisms of the ageing of organic materials under chemical, radiochemical and thermal stress, and its application to the nuclear industry. To this respect, the research program plans to bring to the fore and to explain fundamental mechanisms of degradation by developing and using analytical techniques and methods. It will enable to obtain information concerning the degraded material, the nature, the composition, the structure of its 'metabolite' compounds and data critical from modeling. It will require approaching various area of knowledge; its interdisciplinary aspect will pull my radiochemistry and separations based research into novel experimental areas as well as introduce others to the subject of radiochemistry and the nuclear fuel cycle. The research project I propose being dependent of a multidisciplinary approach, it will be carried out in the framework of collaborations. These collaborations will be internal to the laboratory as well as national and international. The results from my research area, physico-chemistry of organic Systems under chemical, thermal and radiolytic stress, will not only positively impact the scientific community by will also have important applications to the nuclear industry. (author) [fr

  15. Chemistry monitoring and diagnostic system at NPP Jaslovske Bohunice

    International Nuclear Information System (INIS)

    Smiesko, Ivan; Figedy, Stefan

    2012-09-01

    This paper provides a description of water chemistry monitoring and diagnostic system installed at Slovak NPP Jaslovske Bohunice. System has complex architecture and covers laboratory data, chemistry and radiochemistry on-line monitoring data, process data acquisition and processing and diagnostics. Pre-filtered data from process computer and chemistry on-line monitors are recorded together with laboratory data in the ORACLE-based information system CHEMIS with many presentation and processing features. Brief information is given about the basic features of a newly developed diagnostic system for early detection and identification of anomalies incoming in the water chemistry regime of the primary and secondary circuit of VVER-440 type unit. This system, called SACHER (System of Analysis of Chemical Regime) has been installed within the major modernization project at the NPP Bohunice in the Slovak Republic. System SACHER has been developed fully in MATLAB environment. Diagnostic system works exclusively with available on-line data as an operation personnel support application allowing effective response to adverse chemistry events/trends. The availability of prompt information about the chemical conditions of the primary and secondary circuit is very important in order to prevent the undue corrosion and deposit build-up processes within the plant systems. The typical chemical information systems that exist and work at the NPPs give the user values of the measured quantities together with their time trends and other derived values. It is then the experienced user's role to recognize the situation the monitored process is in and make the subsequent decisions and take the measures. The SACHER system, based on the computational intelligence techniques, inserts the elements of intelligence into the overall chemical information system. It has the modular structure with the following most important modules: - normality module- its aim is to recognize that the process

  16. Microfluidic technology platforms for synthesizing, labeling and measuring the kinetics of transport and biochemical reactions for developing molecular imaging probes

    Energy Technology Data Exchange (ETDEWEB)

    Phelps, Michael E. [Univ. of California, Los Angeles, CA (United States)

    2009-09-01

    Radiotracer techniques are used in environmental sciences, geology, biology and medicine. Radiotracers with Positron Emission Tomography (PET) provided biological examinations of ~3 million patients 2008. Despite the success of positron labeled tracers in many sciences, there is limited access in an affordable and convenient manner to develop and use new tracers. Integrated microfluidic chips are a new technology well matched to the concentrations of tracers. Our goal is to develop microfluidic chips and new synthesis approaches to enable wide dissemination of diverse types of tracers at low cost, and to produce new generations of radiochemists for which there are many unfilled jobs. The program objectives are to: 1. Develop an integrated microfluidic platform technology for synthesizing and 18F-labeling diverse arrays of different classes of molecules. 2. Incorporate microfluidic chips into small PC controlled devices (“Synthesizer”) with a platform interfaced to PC for electronic and fluid input/out control. 3. Establish a de-centralized model with Synthesizers for discovering and producing molecular imaging probes, only requiring delivery of inexpensive [18F]fluoride ion from commercial PET radiopharmacies vs the centralized approach of cyclotron facilities synthesizing and shipping a few different types of 18F-probes. 4. Develop a position sensitive avalanche photo diode (PSAPD) camera for beta particles embedded in a microfluidic chip for imaging and measuring transport and biochemical reaction rates to valid new 18F-labeled probes in an array of cell cultures. These objectives are met within a research and educational program integrating radio-chemistry, synthetic chemistry, biochemistry, engineering and biology in the Crump Institute for Molecular Imaging. The Radiochemistry Training Program exposes PhD and post doctoral students to molecular imaging in vitro in cells and microorganisms in microfluidic chips and in vivo with PET, from new technologies

  17. Emittance measurements at the new UNILAC-pre-stripper using a pepper-pot with a PC-controlled CCD-camera

    CERN Document Server

    Dolinska, M E; Forck, P; Hoffmann, T; Liakin, D; Peters, A; Strehl, P

    2000-01-01

    The complex mathematical algorithms and procedures to extract emittance data from intensity distributions measured with a single shot pepper-pot device are described. First results of mathematical evaluation from the commissioning of the new GSI pre-stripper linac structures are presented.

  18. Nuclear medicine 2009. Abstracts; NuklearMedizin 2009. Vortraege

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2009-07-01

    The journal contains the abstracts of 188 lectures and the abstracts of 103 poster contributions concerning the following topics: systemic therapy; oncology: PET/therapy; physics: device technology; oncology: PET/new pharmaceuticals; neurology: receptors; motion correction methods; oncology: PET/FDG; cardiology; malign thyroid tumors; neuroendocrine tumors; radiochemistry {sup 1}8F, oncology: pre-clinic PET; neurology-oncology-activation; physics: quantification; various topics; radiochemistry: radioactive metals; benign thyroid tumors; therapeutical studies; neurology: neurodegeneration; oncology: SPECT/planar scintigraphy; local therapy; inflammation; dosimetry - radiation protection; radiochemistry: halogens.

  19. The new area monitoring system and the fuel database of the TRIGA Mark II reactor in Vienna

    International Nuclear Information System (INIS)

    Villa, M.; Boeck, H.; Hofbauer, M.; Schwarz, V.

    2004-01-01

    The 250 kW TRIGA Mark-II reactor operates since March 1962 at the Atominstitut, Vienna, Austria. Its main tasks are nuclear education and training in the fields of neutron- and solid state physics, nuclear technology, reactor safety, radiochemistry, radiation protection and dosimetry, and low temperature physics and fusion research. Academic research is carried out by students in the above mentioned fields coordinated and supervised by about 70 staff members with the aim of a masters- or PhD degree in one of the above mentioned areas. After 25 years of successful operation, it was necessary to exchange the old area monitoring system with a new digital one. The purpose of the new system is the permanent control of the reactor hall, the primary and secondary cooling system and the monitoring of the ventilation system. The paper describes the development and implementation of the new area monitoring system. The second topic in this paper describes the development of the new fuel database. Since March 7th, 1962, the TRIGA Mark II reactor Vienna operates with an average of 263 MWh per year, which corresponds to a uranium burn-up of 13.7 g per year. Presently we have 81 TRIGA fuel elements in the core, 55 of them are old aluminium clad elements from the initial criticality while the rest are stainless steel clad elements which had been added later to compensate the uranium consumption. Because 67 % of the elements are older than 40 years, it was necessary to put the history of every element in a database, to get an easy access to all the relevant data for every element in our facility. (author)

  20. Laboratory-scale shielded cell for 252Cf

    International Nuclear Information System (INIS)

    Anderl, R.A.; Cargo, C.H.

    1979-01-01

    A shielded-cell facility for storing and handling remotely up to 2 milligram quantities of unencapsulated 252 Cf has been built in a radiochemistry laboratory at the Test Reactor Area of the Idaho National Engineering Laboratory. Unique features of this facility are its compact bulk radiation shield of borated gypsum and transfer lines which permit the transport of fission product activity from 252 Cf fission sources within the cell to a mass separator and to a fast radiochemistry system in nearby rooms

  1. Performance of PC-based charged particle multi-channel spectrometer utilising particle identification

    International Nuclear Information System (INIS)

    Palla, G.; Sziklai, J.; Trajber, Cs.

    1993-12-01

    A collaterally expandable charged particle spectrometer based on PC control and particle identification is described. A typical system configuration consisting of two channels are used to test the system performance. (author) 7 refs.; 5 figs

  2. A digital data acquisition system for a time of flight neutron diffuse scattering instrument

    International Nuclear Information System (INIS)

    Venegas, Rafael; Bacza, Lorena; Navarro, Gustavo

    1998-01-01

    Full text. We describe the design of a digital data acquisition system built for acquiring and storing the information produced by a neutron diffuse scattering apparatus. This instrument is based on the analysis of pulsed subthermal neutron which are scattered by a solid or liquid sample, measured as function of the scattered neutron wavelength and momentum direction. The time of flight neutron intensities on 14 different angular detector positions and two fission chambers must be analyzed simultaneously for each neutron burst. A PC controlled data acquisition board system was built based on two parallel multiscannning units, each with its own add-one counting unit, and a common base time generator. The unit plugs onto the ISA bus through an interface card. Two separate counting units were designed, to avoid possible access competition between low counting rate counters at off-axis positions and the higher rate frontal 0 deg and beam monitoring counters. the first unit contains logic for 14 independent and simultaneous multi scaling inputs, with 128 time channels and dwell time per channel of 5, 10 or 20 microseconds. Sweep trigger is synchronized with an electric signal from a coil sensing the rotor. The second unit contains logic for four additional multi scalers using the same external synchronizing signal, similar in all others details to the previously described multi scalers. Basic control routines for the acquisitions were written in C and a program for spectrum display and user interface was written in C ++ for a Windows 3.1 OS. A block diagram of the system is presented

  3. A broad-application microchannel-plate detector system for advanced particle or photon detection tasks large area imaging, precise multi-hit timing information and high detection rate

    CERN Document Server

    Jagutzki, O; Mergel, V; Schmidt-Böcking, H; Spielberger, L; Spillmann, U; Ullmann-Pfleger, K

    2002-01-01

    New applications for single particle and photon detection in many fields require both large area imaging performance and precise time information on each detected particle. Moreover, a very high data acquisition rate is desirable for most applications and eventually the detection and imaging of more than one particle arriving within a microsecond is required. Commercial CCD systems lack the timing information whereas other electronic microchannel plate (MCP) read-out schemes usually suffer from a low acquisition rate and complicated and sometimes costly read-out electronics. We have designed and tested a complete imaging system consisting of an MCP position readout with helical wire delay-lines, single-unit amplifier box and PC-controlled time-to-digital converter (TDC) readout. The system is very flexible and can detect and analyse position and timing information at single particle rates beyond 1 MHz. Alternatively, multi-hit events can be collected and analysed at about 20 kHz rate. We discuss the advantage...

  4. Automated PET Radiotracer Manufacture on the BG75 System and Imaging Validation Studies of [18F]fluoromisonidazole ([18F]FMISO).

    Science.gov (United States)

    Yuan, Hong; Frank, Jonathan E; Merrill, Joseph R; Hillesheim, Daniel A; Khachaturian, Mark H; Anzellotti, Atilio I

    2016-01-01

    The hypoxia PET tracer, 1-[18F]fluoro-3-(2-nitro-1Himidazol- 1-yl)-propan-2-ol ([18F]FMISO) is the first radiotracer developed for hypoxia PET imaging and has shown promising for cancer diagnosis and prognosis. However, access to [18F]FMISO radiotracer is limited due to the needed cyclotron and radiochemistry expertise. The study aimed to develop the automated production method on the [18F]FMISO radiotracer with the novel fully automated platform of the BG75 system and validate its usage on animal tumor models. [18F]FMISO was produced with the dose synthesis cartridge automatically on the BG75 system. Validation of [18F]FMISO hypoxia imaging functionality was conducted on two tumor mouse models (FaDu/U87 tumor). The distribution of [18F]FMISO within tumor was further validated by the standard hypoxia marker EF5. The average radiochemical purity was (99±1) % and the average pH was 5.5±0.2 with other quality attributes passing standard criteria (n=12). Overall biodistribution for [18F]FMISO in both tumor models was consistent with reported studies where bladder and large intestines presented highest activity at 90 min post injection. High spatial correlation was found between [18F]FMISO autoradiography and EF5 hypoxia staining, indicating high hypoxia specificity of [18MF]FMISO. This study shows that qualified [18F]FMISO can be efficiently produced on the BG75 system in an automated "dose-on-demand" mode using single dose disposable cards. The possibilities of having a low-cost, automated system manufacturing ([18F]Fluoride production + synthesis + QC) different radiotracers will greatly enhance the potential for PET technology to reach new geographical areas and underserved patient populations. Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.org.

  5. The integrated proactive surveillance system for prostate cancer.

    Science.gov (United States)

    Wang, Haibin; Yatawara, Mahendra; Huang, Shao-Chi; Dudley, Kevin; Szekely, Christine; Holden, Stuart; Piantadosi, Steven

    2012-01-01

    In this paper, we present the design and implementation of the integrated proactive surveillance system for prostate cancer (PASS-PC). The integrated PASS-PC is a multi-institutional web-based system aimed at collecting a variety of data on prostate cancer patients in a standardized and efficient way. The integrated PASS-PC was commissioned by the Prostate Cancer Foundation (PCF) and built through the joint of efforts by a group of experts in medical oncology, genetics, pathology, nutrition, and cancer research informatics. Their main goal is facilitating the efficient and uniform collection of critical demographic, lifestyle, nutritional, dietary and clinical information to be used in developing new strategies in diagnosing, preventing and treating prostate cancer.The integrated PASS-PC is designed based on common industry standards - a three tiered architecture and a Service- Oriented Architecture (SOA). It utilizes open source software and programming languages such as HTML, PHP, CSS, JQuery, Drupal and MySQL. We also use a commercial database management system - Oracle 11g. The integrated PASS-PC project uses a "confederation model" that encourages participation of any interested center, irrespective of its size or location. The integrated PASS-PC utilizes a standardized approach to data collection and reporting, and uses extensive validation procedures to prevent entering erroneous data. The integrated PASS-PC controlled vocabulary is harmonized with the National Cancer Institute (NCI) Thesaurus. Currently, two cancer centers in the USA are participating in the integrated PASS-PC project.THE FINAL SYSTEM HAS THREE MAIN COMPONENTS: 1. National Prostate Surveillance Network (NPSN) website; 2. NPSN myConnect portal; 3. Proactive Surveillance System for Prostate Cancer (PASS-PC). PASS-PC is a cancer Biomedical Informatics Grid (caBIG) compatible product. The integrated PASS-PC provides a foundation for collaborative prostate cancer research. It has been built to

  6. Test specification for decant pump and winch assembly

    International Nuclear Information System (INIS)

    Staehr, T.W.

    1994-01-01

    This specification provides the requirements for testing of the vertical turbine decant pump including the floating suction arm with load sensing winch control, instrumentation and the associated PLC/PC control system

  7. Radiochemistry Lab Decommissioning and Dismantlement. AECL, Chalk River Labs, Ontario, Canada

    International Nuclear Information System (INIS)

    Kenny, Stephen

    2008-01-01

    Atomic Energy of Canada (AECL) was originally founded in the mid 1940's to perform research in radiation and nuclear areas under the Canadian Defense Department. In the mid 50's The Canadian government embarked on several research and development programs for the development of the Candu Reactor. AECL was initially built as a temporary site and is now faced with many redundant buildings. Prior to 2004 small amounts of Decommissioning work was in progress. Many reasons for deferring decommissioning activities were used with the predominant ones being: 1. Reduction in radiation doses to workers during the final dismantlement, 2. Development of a long-term solution for the management of radioactive wastes in Canada, 3. Financial constraints presented by the number of facilities shutdown that would require decommissioning funds and the absence of an approved funding strategy. This has led to the development of a comprehensive decommissioning plan that is all inclusive of AECL's current and legacy liabilities. Canada does not have a long-term disposal site; therefore waste minimization becomes the driving factor behind decontamination for decommissioning before and during dismantlement. This decommissioning job was a great learning experience for decommissioning and the associated contractors who worked on this project. Throughout the life of the project there was a constant focus on waste minimization. This focus was constantly in conflict with regulatory compliance primarily with respect to fire regulations and protecting the facility along with adjacent facilities during the decommissioning activities. Discrepancies in historical documents forced the project to treat every space as a contaminated space until proven differently. Decommissioning and dismantlement within an operating site adds to the complexity of the tasks especially when it is being conducted in the heart of the plant. This project was very successful with no lost time accidents in over one hundred thousand hours worked, on schedule and under budget despite some significant changes throughout the decommissioning phases. The actual cost to decommission this building will come in under 9 million dollars vs. an estimated 14.5 million dollars. This paper will cover some of the unique aspects of dismantling a radioactive building that has seen pretty much every element of the periodic table pass through it with the client requirement focused on minimization of radioactive waste volumes

  8. Identification of cadmium in biological samples using neutron activation analysis with radiochemistry separations

    International Nuclear Information System (INIS)

    Munoz A, Luis; Gras R, Nuri

    2002-01-01

    Chile's 7500 km coastline of the Southern Pacific ocean, with about 4500 km of continental coastline that contains a variety of different geographical zones. This variety means that there is a great diversity of marine resources such as fish, shellfish and seaweeds. The utilization of these resources has been increasing in recent years making this sector an economically important one. The catch as of May 2002 came to 1.9 million tons and exports of the different species amounted to US$611.5 million as of April. But this important economic resource is being threatened by the technical demands imposed by importing countries, mainly the specific requirements for sanitary certification for fishery export products, depending on the markets of destination. The chemical element cadmium is one of the most strictly controlled elements due some shellfish accumulate a large amount of this element and to its high toxicity. The Chilean standard's analytical procedures for cadmium determination in hydro biological products, which must be met by laboratories that certify and control these products for export, are now being evaluated. Through its Chemical Metrology Unit, the Chilean Nuclear Energy Commission is strongly supporting this sector by preparing the secondary reference or control materials, and it has developed and implemented nuclear analytical methods for the certification of these materials, which will be used mostly in collaborative studies. This work describes the methodology developed for the determination of cadmium in biological samples, particularly in shellfish and fish. The method is based on neutron activation analysis with radiochemical separations, using the radioisotopes 115 Cd and 115m In, generated in the samples by bombarding with neutrons in a nuclear reactor. The samples were digested at 110 o C with H 2 SO 4 and H 2 O 2 and then the radioactive cadmium element was separated from the other elements present in the samples using a Bio Rad AG 2-X8 resin. The isolated radioisotope was analyzed with high resolution gamma spectrometry. The yield from the separation was evaluated using a 115 Cd radioactive tracer and the methodology was validated using the reference materials Oyster Tissue 1566A from the NIST, United States and DOLT-2 from the NRC, Canada. This methodology is being applied as a reference technique to support the certification of export fishery products and in environmental studies (LM)

  9. PET radiochemistry: synthesis of 2-[18 F]-fluorine-2-deoxy-D-glucose

    International Nuclear Information System (INIS)

    Lopez D, F.A.; Flores M, A.; Zarate M, A.; Romo, E.

    2005-01-01

    The present work describes the method for the synthesis of the 2-[ 18 F]-fluorine-2-deoxy-D-glucose, the radiopharmaceutical of more use in nuclear medicine for the diagnosis of cancer at world level. (Author)

  10. Contribution of the radiochemistry to the radiological protection in the influence zones of the nuclear facilities

    International Nuclear Information System (INIS)

    Archundia, C.; Araico, E.; Ortiz M, R.

    1991-01-01

    Among the regulatory requirements to satisfy in one first stage, before the beginning of the construction of a nuclear facility, it should be carried out a radiological analytic theoretical study that, with base in the technological characteristics of the power station proposal and making use of the environmental parameters, determine the ecological routes that can carry out to groups of population considered as critical those radionuclides with possibility to be liberated. Also, this study understands the estimate of the equivalent doses for external and internal exhibition that those critical groups would receive real or potentially as a consequence of the normal activity of the power station

  11. Evaluation of radiochemistry purity and p H of radiopharmaceuticals in nuclear medicine services at Pernambuco, Brazil

    International Nuclear Information System (INIS)

    Andrade, Wellington; Lima, Fabiana Farias de; Santos, Poliane A.L.; Lima, Fernando Roberto de Andrade; Lima, Fabiana Farias de

    2011-01-01

    Radiopharmaceuticals are cellular or molecular structures that have a radionuclide in its composition and they are used for diagnosing or treating diseases. The evaluation of the radiochemical purity of radiopharmaceuticals is essential to produce images with artifacts free, as well as avoid unnecessary absorbed dose to the patient. Since they are administered in humans is important and necessary that they undergo rigorous quality control. Due to this fact, the norm in ANVISA RDC 38/2008 declaring the mandatory completion of a minimum of tests in routine nuclear medicine services before human administration. (author)

  12. Start, Stop, Restart: The Recent History of Federal Funding for Radiochemistry Education

    International Nuclear Information System (INIS)

    Williamson, R. Craig

    2009-01-01

    Over the course of the 2009, Federal Fiscal Year the U.S. Departments of Homeland Security and Defense will introduce university programs designed to provide the U.S. national laboratories with a highly qualified workforce in nuclear forensics. These programs are designed to recruit the best and brightest students, develop universities research and education activities, and to enhance university/laboratory(s) interactions nuclear forensics. The approach will be comprehensive in that it will target undergraduate and graduate students, faculty members and institutions. This will include an undergraduate research program designed to encourage emerging seniors to perform research at designated national laboratories throughout the United States. In addition to the undergraduate program, a nationally competitive graduate fellowship program in nuclear forensics was established in 2008. This program provides a four-year appointment with a monthly stipend, full payment of tuition and fees, the establishment of participating universities, and required post-graduate positions in nuclear forensics. A Nuclear Forensics Education Award program will also be introduced. This broad-based program will have an impact on university programs interested in developing nuclear forensics capabilities. This will include funds for instrumentation and equipment, faculty members, students, and curriculum.

  13. Post-Fukushima situation on radiation awareness activities and nuclear and radiochemistry education in Japan

    International Nuclear Information System (INIS)

    Yokoyama, Akihiko

    2013-01-01

    The accident at Fukushima Daiichi Nuclear Power Plant in 2011 altered the working environment for radiochemists in Japan, who are supposed to be in charge of several problems such as radioactive contamination and nuclear wastes from reactors. Under the circumstances, we are compelled to reexamine the education relating to such matters. I discuss the effect of the accident on some aspects of education of the field. (author)

  14. Evaluation of controls for the assurance of quality data in a radiochemistry laboratory

    International Nuclear Information System (INIS)

    Morton, J.S.

    1993-01-01

    The paper describes the controls implemented by the U.S. Department of Energy (DOE) at the Radiological and Environmental Sciences Laboratory (RESL) to secure data quality. A description of the analytical instrumentation and methodology employed by RESL is provided. The results of the intercomparison program with the National Institute of Standards and Technology (NIST) are provided to demonstrate traceability to a primary source. A description of the methods and techniques used to ensure quality control on a daily basis is given. The techniques used to evaluate the sources of uncertainty are reviewed and specific examples cited. The intercomparison programs operated by RESL are discussed

  15. 9. International symposium on nuclear chemistry, radiochemistry and radiation chemistry. Abstracts

    International Nuclear Information System (INIS)

    1992-01-01

    The report presents the abstracts of 30 contributions covering mainly photochemical reactions, irradiation of organic chemicals, gamma-radiation in wastewater treatment, PIXE analysis, and some aspects of nuclear spectroscopic instrumentation in radiochemical analysis

  16. Evaluation of controls for the assurance of quality data in a radiochemistry laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Morton, J.S. [Radiological and Environmental Sciences Lab., Idaho Falls, ID (United States)

    1993-12-31

    The paper describes the controls implemented by the U.S. Department of Energy (DOE) at the Radiological and Environmental Sciences Laboratory (RESL) to secure data quality. A description of the analytical instrumentation and methodology employed by RESL is provided. The results of the intercomparison program with the National Institute of Standards and Technology (NIST) are provided to demonstrate traceability to a primary source. A description of the methods and techniques used to ensure quality control on a daily basis is given. The techniques used to evaluate the sources of uncertainty are reviewed and specific examples cited. The intercomparison programs operated by RESL are discussed.

  17. The radiochemistry of [18 F]-FDG: the first experience in Mexico

    International Nuclear Information System (INIS)

    Lopez D, F.A.

    2004-01-01

    The present work describes the more used method for the synthesis of 2 - [ 18 F] - fluorine-2-deoxy-D-glucose that is the more used radiopharmaceutical in the nuclear medicine in the cancer diagnostic. The process consists on two chemical reactions: i) [ 18 F - ] - nucleophilic radio fluorination and i i) a hydrolysis catalyzed by acid. The first reaction incorporates to the [ 18 F]- fluorine labelled inside the organic precursor 1,3,4,6-tetra- O -acetil-2- O-trifluoromethanesulfonyl- β-D-mannopyranose (triflate of mannose). The mechanism of this reaction is a bimolecular nucleophilic substitution (SN 2 ) with the ion [ 18 F - ] - fluoride; in the second reaction, the hydrolysis of those protective acetyl groups generate the hydroxyl groups free of the [ 18 F]-FDG. The process includes an azeotropic distillation and several purification steps. (Author)

  18. New radiochemistry techniques monograph: open-quotes Ultrafast chemical separationsclose quotes

    International Nuclear Information System (INIS)

    Ypsilanti, M.I.; Meyer, R.A.; Rengan, K.

    1992-01-01

    Study of decay characteristics of short-lived nuclides has fascinated nuclear chemists ever since the discovery of radioactivity. In the last two decades nuclides with half-lives in the range of several seconds to several tens of seconds have been explored. In addition to manual procedures, several automatic batch (autobatch) as well as continuous separation procedures have been developed for the study of these nuclides. The first part of the radiochemical techniques monograph entitled open-quotes Ultrafast Chemical Separationsclose quotes reviews the techniques used in fast separations. A collection of known fast procedures, arranged according to the name of the element, is presented in the second part. A total of 316 procedures for 75 elements are included

  19. Radiochemistry - Applications in the study of radical mechanisms of biological interest

    International Nuclear Information System (INIS)

    Foos, Jacques

    1982-01-01

    In biology, oxygen reducing processes give rise to the formation of intermediate radicals. One of the major breakthroughs of radiation chemistry of aqueous solutions is the identification of these compounds. The author describes the techniques used to study the reaction of these radicals (of radiolytic origin) with biological molecules [fr

  20. Report on results of research and development work in 1980 of the Institute for Radiochemistry

    International Nuclear Information System (INIS)

    1981-02-01

    Reported are the investigations of the Institute with the main points of analysis, nuclear chemistry and water chemistry. The analytical and nuclear chemical topics are included in the projects PWA, PNS, PSB and KMUe. The KMUe-project is performed in close co-operation with the European Institute for Transuranic Elements. The analytical investigations concentrate on fuel- and burn-up tests, on analyses of epipolar rays and neutron activations as well as on methodical development and automation of test methods. The 'Isotope-place' does preparatory works and effects irradiations in the FR2, Cyclotron and Co-60-γ-source. The radiochemical group prepares weekly several hundreds of Curie fission molybdenum 99 for nuclear medical purposes. The institute-internal project 'Drinkwater treatment and technology' treats in close co-operation with the 'Engler-Bunte-Institute' the clearing of water impurities and the analytical determination of persistent noxious substances in waters like the Rhine, the Danube and the lake Constance. (orig./HK) [de

  1. Positron-emitting isotopes in nuclear medicine: a new challenge for radiochemistry and radiotherapy

    International Nuclear Information System (INIS)

    Lars, J.; Nilsson, G.; Ehrin, E.; Stone-Elander, S.

    1980-01-01

    Positron emission tomography and the positron camera are described and their applications in medical diagnostics outlined. The incorporation of positron emitting isotopes into other molecules which can participate biochemically in cell metabolisms and accumulate in cells with increased activity, is discussed. (C.F.)

  2. Determination of radiochemistry purity and pH of radiopharmaceutical in Northeast nuclear medicine services

    International Nuclear Information System (INIS)

    Andrade, Wellington; Santos, Poliane; Lima, Fernando de Andrade; Lima, Fabiana Farias de

    2013-01-01

    The radiopharmaceutical is a chemical compound associated with a radionuclide, which is selected so that meets the need cf diagnosis and capable of producing quality images. Drugs labeled with 99m Tc radionuclide kits consist of lyophilized, and be handled by the nuclear medicine services (NMS) must pass tests as the resolution of ANVISA (RDC 38) published in 2008. Among these tests are those of radiochemical purity and pH determination. This study evaluated the radiochemical purity of radiopharmaceuticals and pH SMN manipulated in the Northeast. The radiochemical purity (RCP) was determined by thin layer chromatography, which were used Whatman ® and silica gel, with dimensions of 1 x 10 cm, as stationary phase, and solvents indicated in the inserts of manufacturers. The chromatographic strips were placed in sealed containers so as not to touch the walls thereof. After the chromatographic run, the tape was cut every centimeter and the activities determined in doses of each calibrator NMS. The pH of the radiopharmaceutical was assessed through the use of universal pH paper (Merck®) and obtained staining compared with its color scale. The results showed (hat 82.6% and 100% of the radiopharmaceuticals of the samples were within the limits recommended by international pharmacopoeias for radiochemical purity and pl-l, respectively. There is then the need to include in routine tests indicated SMN by ANVISA. Well, they can detect possible problems in the marking of radiopharmaceuticals administered to the patient and avoid inappropriate material. (author)

  3. Optimization of a radiochemistry method for plutonium determination in biological samples

    International Nuclear Information System (INIS)

    Cerchetti, Maria L.; Arguelles, Maria G.

    2005-01-01

    Plutonium has been widely used for civilian an military activities. Nevertheless, the methods to control work exposition have not evolved in the same way, remaining as one of the major challengers for the radiological protection practice. Due to the low acceptable incorporation limit, the usual determination is based on indirect methods in urine samples. Our main objective was to optimize a technique used to monitor internal contamination of workers exposed to Plutonium isotopes. Different parameters were modified and their influence on the three steps of the method was evaluated. Those which gave the highest yield and feasibility were selected. The method involves: 1-) Sample concentration (coprecipitation); 2-) Plutonium purification; and 3-) Source preparation by electrodeposition. On the coprecipitation phase, changes on temperature and concentration of the carrier were evaluated. On the ion-exchange separation, changes on the type of the resin, elution solution for hydroxylamine (concentration and volume), length and column recycle were evaluated. Finally, on the electrodeposition phase, we modified the following: electrolytic solution, pH and time. Measures were made by liquid scintillation counting and alpha spectrometry (PIPS). We obtained the following yields: 88% for coprecipitation (at 60 C degree with 2 ml of CaHPO 4 ), 71% for ion-exchange (resins AG 1x8 Cl - 100-200 mesh, hydroxylamine 0.1N in HCl 0.2N as eluent, column between 4.5 and 8 cm), and 93% for electrodeposition (H 2 SO 4 -NH 4 OH, 100 minutes and pH from 2 to 2.8). The expand uncertainty was 30% (NC 95%), the decision threshold (Lc) was 0.102 Bq/L and the minimum detectable activity was 0.218 Bq/L of urine. We obtained an optimized method to screen workers exposed to Plutonium. (author)

  4. Radiochemistry on chip : towards dose-on-demand synthesis of PET radiopharmaceuticals

    NARCIS (Netherlands)

    Arima, V.; Pascali, G.; Lade, O.; Kretschmer, H.R.; Bernsdorf, I.; Hammond, V.; Watts, P.; De Leonardis, F.; Tarn, M.D.; Pamme, N.; Cvetkovic, B.Z.; Dittrich, P.S.; Vasovic, N.; Duane, R.; Jaksic, A.; Zacheo, A.; Zizzari, A.; Marra, L.; Perrone, E.; Salvadori, P.A.; Rinaldi, R.

    2013-01-01

    We have developed an integrated microfluidic platform for producing 2-[18F]-fluoro-2-deoxy-D-glucose (18F-FDG) in continuous flow from a single bolus of radioactive isotope solution, with constant product yields achieved throughout the operation that were comparable to those reported for

  5. Physical chemistry and radiochemistry characterization of sediment dust in Colonia and Soriano provinces in Uruguay

    International Nuclear Information System (INIS)

    Odino, R.; Gabrielli, A.; Piuma, L.; Reina, E.; Suarez, R.

    2010-01-01

    In the present work is characterized dust settled in the Departments of Colon ia and Soriano in Uruguay as a result of unusual events that occurred in July 2010. In order to identify the dust settled physicochemical characterization was carried out an analysis by X-ray fluorescence energy dispersive (EDXRF) spectrometry and analysis by High Resolution Gamma. With the results obtained by EDXRF was calculated using the enrichment factor matrix Mason. Macroscopic analysis indicated that this is a homogeneous sample of ocher-beige. The microscopic analysis showed the presence of sediment sandy silt with clasts of quartz and feldspar. The chemical composition indicated the presence of an inorganic material composed mainly of Al and Si, Fe, Mn and Ca lesser percentage was observed the presence of S, Cl, P, V, Cr, Ni, Cu, Zn, Ga, As , Br, Rb, Sr, Y, Zr, Nb, Ba, Pb, Th. The enrichment factor calculation showed that the elements As and Zn are enriched by a factor greater than 40. Gamma spectrometry analysis of high resolution and natural radionuclides were identified including the presence of high concentrations of 7Be activity, indicating that such material has been transported by air. Digital simulations were performed using the back trajectory model - Noaa HYSPLIT Model attempt to identify the source of the event. [es

  6. Emerging trends in forensic science with special emphasis on nuclear and radiochemistry

    International Nuclear Information System (INIS)

    Krishnamurthy, Rukmani

    2011-01-01

    Forensic science uses the basic principles of all physical and natural science and have evolved many domain of its owns, like Anthropometry, fingerprint, Foot print, ballistics, documentation, Forensic Biology and Serology, Forensic Chemistry, Nuclear forensic science, Forensic Physic, Toxicology, Odontology, Forensic DNA, Cyber Forensic, Forensic Psychology, Forensic engineering etc., which provides a fool prove scientific aid to criminal justice administration. Nuclear forensic science is a fairly young discipline and only a small number of laboratories are active practitioners. However, the number of incidents of illicit trafficking reported and furthermore, the threat of nuclear terrorism calls for preparedness and for effective tools providing hints on the origin of the material and thus on the perpetrator. The determination of characteristic parameters is subject to ongoing research and development work in a number of nuclear measurement laboratories. Parameters like isotopic composition, chemical impurities, age of the material, macroscopic parameters and microstructure provide clues on the origin and on the intended use of the material. Today, nuclear forensics has reached a high degree of maturity and it is highly relevant in the areas of non-proliferation and of nuclear security. Continued development activities and strengthened international cooperation will be of key importance for the perfection of the discipline of nuclear forensics

  7. Radiochemistry research: Progress report, October 1, 1974 to September 30, 1975

    International Nuclear Information System (INIS)

    Rowland, F.S.

    1987-01-01

    A major effort has been made this year to pursue details of the effects of the chlorofluoromethanes in the environment. The AEC report written in September, 1974, was revised and published as a review article in Reviews of Geophysics and Space Physics. A shorter description was published in the New Scientist in December, 1974. Three additional papers were published on the stratospheric chlorine problem. Testimony was provided at various hearings

  8. Karlsruhe Nuclear Research Center, Institute of Radiochemistry. Progress report on research and development work in 1993

    International Nuclear Information System (INIS)

    1994-03-01

    The IRCH microsystems technology activities are dedicated to the development of chemical sensors and probes which meet the practical sensitivity, selectivity or specificity and stability requirements. The devices are miniaturized for integration into microsystems technology solutions and are designed for a wide range of process management, process control and process analysis uses including, e.g. pollution monitoring and medical diagnosis. The nuclear fusion project focuses on investigations into chemical and technical tritium technology problems which may occur, e.g. during tritium recovery from tritiated compounds in the internal and external fusion reactor fuel cycles. Additional efforts go into the physico-ceramic characterization of ceramic breeder materials, the extraction of bred tritium from the blanket, and the development of the necessary process analysis methods. (orig.) [de

  9. Institute for Radiochemistry. Progress report on research and development in 1994

    International Nuclear Information System (INIS)

    1995-01-01

    The IRCH microsystems technology activities are dedicated to the development of chemical sensors and probes which meet the practical sensitivity, selectivity or specificity and stability requirements. The devices are miniaturized for integration into microsystems technology solutions and are designed for a wide range of process management, process control and process analysis uses including, e.g. pollution monitoring and medical diagnosis. The nuclear fusion project focuses on investigations into chemical and technical tritium technology problems which may occur, e.g. during tritium recovery from tritiated compounds in the internal and external fusion reactor fuel cycles. Additional efforts go into the physico-ceramic characterization of bred tritium from the blanket, and the development of the necessary process analysis methods. (orig.) [de

  10. System Budgets

    DEFF Research Database (Denmark)

    Jeppesen, Palle

    1996-01-01

    The lecture note is aimed at introducing system budgets for optical communication systems. It treats optical fiber communication systems (six generations), system design, bandwidth effects, other system impairments and optical amplifiers.......The lecture note is aimed at introducing system budgets for optical communication systems. It treats optical fiber communication systems (six generations), system design, bandwidth effects, other system impairments and optical amplifiers....

  11. Ventilation systems

    International Nuclear Information System (INIS)

    Gossler

    1980-01-01

    The present paper deals with - controlled area ventilation systems - ventilation systems for switchgear-building and control-room - other ventilation systems for safety equipments - service systems for ventilation systems. (orig./RW)

  12. Embedded Systems

    Indian Academy of Sciences (India)

    Embedded system, micro-con- troller ... Embedded systems differ from general purpose computers in many ... Low cost: As embedded systems are extensively used in con- .... operating systems for the desktop computers where scheduling.

  13. Thermal systems; Systemes thermiques

    Energy Technology Data Exchange (ETDEWEB)

    Lalot, S. [Valenciennes Univ. et du Hainaut Cambresis, LME, 59 (France); Lecoeuche, S. [Ecole des Mines de Douai, Dept. GIP, 59 - Douai (France)]|[Lille Univ. des Sciences et Technologies, 59 - Villeneuve d' Ascq (France); Ahmad, M.; Sallee, H.; Quenard, D. [CSTB, 38 - Saint Martin d' Heres (France); Bontemps, A. [Universite Joseph Fourier, LEGI/GRETh, 38 - Grenoble (France); Gascoin, N.; Gillard, P.; Bernard, S. [Laboratoire d' Energetique, Explosion, Structure, 18 - Bourges (France); Gascoin, N.; Toure, Y. [Laboratoire Vision et Robotique, 18 - Bourges (France); Daniau, E.; Bouchez, M. [MBDA, 18 - Bourges (France); Dobrovicescu, A.; Stanciu, D. [Bucarest Univ. Polytechnique, Faculte de Genie Mecanique (Romania); Stoian, M. [Reims Univ. Champagne Ardenne, Faculte des Sciences, UTAP/LTM, 51 (France); Bruch, A.; Fourmigue, J.F.; Colasson, S. [CEA Grenoble, Lab. Greth, 38 (France); Bontemps, A. [Universite Joseph Fourier, LEGI/GRETh, 38 - Grenoble (France); Voicu, I.; Mare, T.; Miriel, J. [Institut National des Sciences Appliquees (INSA), LGCGM, IUT, 35 - Rennes (France); Galanis, N. [Sherbrooke Univ., Genie Mecanique, QC (Canada); Nemer, M.; Clodic, D. [Ecole des Mines de Paris, Centre Energetique et Procedes, 75 (France); Lasbet, Y.; Auvity, B.; Castelain, C.; Peerhossaini, H. [Nantes Univ., Ecole Polytechnique, Lab. de Thermocinetiquede Nantes, UMR-CNRS 6607, 44 (France)

    2005-07-01

    This session about thermal systems gathers 26 articles dealing with: neural model of a compact heat exchanger; experimental study and numerical simulation of the thermal behaviour of test-cells with walls made of a combination of phase change materials and super-insulating materials; hydraulic and thermal modeling of a supercritical fluid with pyrolysis inside a heated channel: pre-dimensioning of an experimental study; energy analysis of the heat recovery devices of a cryogenic system; numerical simulation of the thermo-hydraulic behaviour of a supercritical CO{sub 2} flow inside a vertical tube; mixed convection inside dual-tube exchangers; development of a nodal approach with homogenization for the simulation of the brazing cycle of a heat exchanger; chaotic exchanger for the cooling of low temperature fuel cells; structural optimization of the internal fins of a cylindrical generator; a new experimental approach for the study of the local boiling inside the channels of exchangers with plates and fins; experimental study of the flow regimes of boiling hydrocarbons on a bundle of staggered tubes; energy study of heat recovery exchangers used in Claude-type refrigerating systems; general model of Carnot engine submitted to various operating constraints; the free pistons Stirling cogeneration system; natural gas supplied cogeneration system with polymer membrane fuel cell; influence of the CRN coating on the heat flux inside the tool during the wood unrolling process; transport and mixture of a passive scalar injected inside the wake of a Ahmed body; control of a laser welding-brazing process by infrared thermography; 2D self-adaptative method for contours detection: application to the images of an aniso-thermal jet; exergy and exergy-economical study of an 'Ericsson' engine-based micro-cogeneration system; simplified air-conditioning of telephone switching equipments; parametric study of the 'low-energy' individual dwelling; brief synthesis of

  14. Sediment lithology and radiochemistry from the back-barrier environments along the northern Chandeleur Islands, Louisiana—March 2012

    Science.gov (United States)

    Marot, Marci E.; Smith, Christopher G.; Adams, C. Scott; Richwine, Kathryn A.

    2017-04-11

    Scientists from the U.S. Geological Survey (USGS) St. Petersburg Coastal and Marine Science Center collected a set of 8 sediment cores from the back-barrier environments along the northern Chandeleur Islands, Louisiana, in March 2012. The sampling efforts were part of a larger USGS study to evaluate effects on the geomorphology of the Chandeleur Islands following the construction of an artificial sand berm to reduce oil transport onto federally managed lands. The objective of this study was to evaluate the response of the back-barrier tidal and wetland environments to the berm. This report serves as an archive for sedimentological and radiochemical data derived from the sediment cores. The data described in this report are available for download on the data downloads page.

  15. Progress report on research and development activities in 1992. Annual report of the Institute of Radiochemistry (IRCH)

    International Nuclear Information System (INIS)

    1993-03-01

    The report summarizes the R and D work carried out in 1992 by the IRCH within the scope of the three projects: (1) low-waste and low-pollutant cleaning methods (PSA project), covering analytical and technical aspects of polluted water and soil. (2) Thermonuclear fusion project (blanket development, tritium technology). (3) Microsystems technology (chemical microsensor development). Other work accomplished by the institute is reported in chapter 4, 'Other research projects', and the publications prepared by institute members are listed in an annex. (BBR) [de

  16. Radioactive Environment Contamination and Abilities of the Modern Radiochemistry in the Field of Nuclear Waste Disposal and Monitoring

    International Nuclear Information System (INIS)

    Myasoedov, B.F.; Novikov, A.P.

    1999-01-01

    The study of environmental contamination caused by anthropogenic impacts and, primarily, by radioactive nuclides is one of the main scientific problems facing contemporary science. This is known as Radioecological monitoring. Decisions regarding the remediation of polluted areas require detailed information about the distribution of radioactive nuclides in terrestrial and aquatic ecosystems, as well as, knowledge about radionuclides occurrence forms and migration patterns. Different sources of radionuclides penetration into the environment appoint their interaction with nature matrices in different ways and should be considered accordingly. An overview is given of the present radioecological situation around the reprocessing plant M ayak , which was constructed more than 40 years ago for the production of plutonium for military purposes. Some new approaches, methods and tools developed at the Vernadsky Institute of Geochemistry and Analytical Chemistry for the isolation, concentration and determination of radionuclides in various environmental samples are discussed. Data regarding the distribution, occurrence, and migration processes of radionuclides 90 Sr, 137 Cs, 239 Pu and 241 Am, in aquatic and terrestrial ecosystems of the impact zone of the Mayak plant, are presented

  17. Data Systems vs. Information Systems

    OpenAIRE

    Amatayakul, Margret K.

    1982-01-01

    This paper examines the current status of “hospital information systems” with respect to the distinction between data systems and information systems. It is proposed that the systems currently existing are incomplete data dystems resulting in ineffective information systems.

  18. EXPERT SYSTEMS

    OpenAIRE

    Georgiana Marin; Mihai Catalin Andrei

    2011-01-01

    In recent decades IT and computer systems have evolved rapidly in economic informatics field. The goal is to create user friendly information systems that respond promptly and accurately to requests. Informatics systems evolved into decision assisted systems, and such systems are converted, based on gained experience, in expert systems for creative problem solving that an organization is facing. Expert systems are aimed at rebuilding human reasoning on the expertise obtained from experts, sto...

  19. Multibody Systems

    DEFF Research Database (Denmark)

    Wagner, Falko Jens

    1999-01-01

    Multibody Systems is one area, in which methods for solving DAEs are of special interst. This chapter is about multibody systems, why they result in DAE systems and what kind of problems that can arise when dealing with multibody systems and formulating their corresponding DAE system....

  20. 10th European TRIGA users conference

    International Nuclear Information System (INIS)

    Anon.

    1988-01-01

    Abstracts of 46 papers on various aspects of Triga reactors (mainly Triga Mark 2 reactors) are given, according to the main headings: reactor operation and maintenance experience; new developments and improvements of Triga components and systems, including instrumentation; fuel and fuel management; safety aspects, licensing and radiation protection; experiments with Triga reactors; radiochemistry, radioisotope production and NAA; reactor physics. (qui)

  1. Solid targetry for compact cyclotrons

    International Nuclear Information System (INIS)

    Comor, J.

    2004-01-01

    In this presentation authors present experimental results of solid targetry for compact cyclotrons. It is concluded: Solid targetry is not restricted to large accelerator centers anymore; Small and medium scale radioisotope production is feasible with compact cyclotrons; The availability of versatile solid target systems is expected to boost the radiochemistry of 'exotic' positron emitters

  2. Annual Report 2003 of the Institute of Nuclear Chemistry and Technology

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2004-07-01

    The INCT 2003 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies, nucleonic control systems and accelerators.

  3. Proceedings of the seventh scientific meeting at San Rafael, 6-10 november 1978

    International Nuclear Information System (INIS)

    1980-01-01

    Compilation of 68 papers on a variety of aspects and problems arising from the maintenace, commissioning and operation of Argentina's nuclear power plants and reactors. The subjects are referred, in particular, to reactor components and accesories,including fuel elements and chemical treatment of water, as well as the respective control systems and radiochemistry. (R.J.S.) [es

  4. Activities in nuclear and high energy physics

    Energy Technology Data Exchange (ETDEWEB)

    1983-01-01

    High energy and nuclear physics research concerning bubble chamber investigations, European hybrid system ACCMOR, WA 18, PETRA, PEP, VA 4, SING, LENA, LEP 3 and DELPHI experiments is summarized. Experiments with electron beams, and in pions and muons physics, and radiochemistry are reported on.

  5. Annual Report 2003 of the Institute of Nuclear Chemistry and Technology

    International Nuclear Information System (INIS)

    2004-01-01

    The INCT 2003 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies, nucleonic control systems and accelerators

  6. Annual Report of Institute of Nuclear Chemistry and Technology 2002

    International Nuclear Information System (INIS)

    2003-06-01

    The INCT 2002 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology, Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics, nucleonic control systems and accelerators

  7. Annual Report of Institute of Nuclear Chemistry and Technology 2002

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2003-06-01

    The INCT 2002 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology, Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics, nucleonic control systems and accelerators.

  8. System dynamics

    International Nuclear Information System (INIS)

    Kim, Do Hun; Mun, Tae Hun; Kim, Dong Hwan

    1999-02-01

    This book introduces systems thinking and conceptual tool and modeling tool of dynamics system such as tragedy of single thinking, accessible way of system dynamics, feedback structure and causal loop diagram analysis, basic of system dynamics modeling, causal loop diagram and system dynamics modeling, information delay modeling, discovery and application for policy, modeling of crisis of agricultural and stock breeding products, dynamic model and lesson in ecosystem, development and decadence of cites and innovation of education forward system thinking.

  9. Coupling component systems towards systems of systems

    OpenAIRE

    Autran , Frédéric; Auzelle , Jean-Philippe; Cattan , Denise; Garnier , Jean-Luc; Luzeaux , Dominique; Mayer , Frédérique; Peyrichon , Marc; Ruault , Jean-René

    2008-01-01

    International audience; Systems of systems (SoS) are a hot topic in our "fully connected global world". Our aim is not to provide another definition of what SoS are, but rather to focus on the adequacy of reusing standard system architecting techniques within this approach in order to improve performance, fault detection and safety issues in large-scale coupled systems that definitely qualify as SoS, whatever the definition is. A key issue will be to secure the availability of the services pr...

  10. Systems effectiveness

    CERN Document Server

    Habayeb, A R

    1987-01-01

    Highlights three principal applications of system effectiveness: hardware system evaluation, organizational development and evaluation, and conflict analysis. The text emphasizes the commonality of the system effectiveness discipline. The first part of the work presents a framework for system effectiveness, partitioning and hierarchy of hardware systems. The second part covers the structure, hierarchy, states, functions and activities of organizations. Contains an extended Appendix on mathematical concepts and also several project suggestions.

  11. Auxiliary systems

    International Nuclear Information System (INIS)

    Meyer, P.J.

    1981-01-01

    Systems included under the heading ''Reactor Auxillary Systems'' are those immediately involved with the reactor operation. These include the systems for dosing and letdown of reactor coolant, as well as for the chemical dosing, purification and treatment of the reactor coolant and the cooling system in the controlled area. The ancillary systems are mainly responsible for liquid and gaseous treatment and the waste treatment for final storage. (orig.)

  12. Improvement of A.E.S System, using a 188Re-radiolabeled hapten

    International Nuclear Information System (INIS)

    Morandeau, L.

    2002-01-01

    Full text: Feasibility of two-step radioimmunotherapy (RIT) of cancer by the Affinity Enhancement System (AES) has been demonstrated in experimental and clinical studies. This technique, associating a bispecific antibody (BsAb) and a radiolabeled bivalent peptide, reduces toxicity and improves therapeutic efficacy of the treatment compared to the one step targeting method. The formation of a cyclic complex (antigen-BsAb- hapten-BsAb-antigen) observed on the tumor allows good tumoral fixation. This is associated with low non-specific uptake, due to the fast clearance of the hapten from the organism. Iodine 131, used currently in clinical applications, has however several disadvantages. These include the mean energy of □ . particles, strong y emission and long physical half-life. Rhenium-188 is the radionuclide of choice to replace iodine-131; its low cost, its availability from a W-188/Re-188 generator and its very favorable radiophysical properties (t 1/2 =16.9h; E□=2.118 MeV; Ey (15%)=155keV) make it a very interesting radionuclide for radioimmunotherapy applications. Unlike the case of iodine-131, the radiolabelling of the peptide by rhenium-188 requires the preliminary coupling of a bifunctional chelating agent. This ensures the formation of an in vivo stable complex with the radionuclide. The object of this post-doctoral project is to obtain a rhenium-188 radiolabeled bivalent hapten. To do this, a monovalent hapten will be coupled to a chelating agent that involves two or three patterns to complex the radionuclide, leading to a bivalent or trivalent radiolabeled hapten, suitable for applications in A.E.S. system. The monovalent hapten used, called HSGL (histaminosuccinylglycyllysine) is a small heteropeptide composed of a chain of four molecules which are histamine, succinic acid, glycine, lysine. It is recognised by the antibody anti-HSG. Two kinds of chelating agents, dithiocarbamates and dithiobenzoates will be studied. They have been synthesised at

  13. Bitcoin System

    Directory of Open Access Journals (Sweden)

    Jan Lánský

    2017-06-01

    Full Text Available Cryptocurrency systems are purely digital and decentralized systems that use cryptographic principles to confirm transactions. Bitcoin is the first and also the most widespread cryptocurrency. The aim of this article is to introduce Bitcoin system using a language understandable also to readers without computer science education. This article captures the Bitcoin system from three perspectives: internal structure, network and users. Emphasis is placed on brief and clear definitions (system components and their mutual relationships. A new system view of the stated terms constitutes author’s own contribution.

  14. JOSHUA system

    International Nuclear Information System (INIS)

    Honeck, H.C.

    1975-04-01

    A major computational system called JOSHUA has been under development at the Savannah River Laboratory since 1968. The JOSHUA System has two major parts: the Operating System and the Application System. The Operating System has been in production use since 1970 and provides data management, terminal, and job execution facilities. The Application System uses these facilities in solving problems in reactor physics and engineering. Features of the Application System are the two-dimensional lattice physics and three-dimensional transient reactor physics capabilities, which have been in use since 1971 and 1974, respectively. The capabilities of the JOSHUA System are summarized, and statistics on size, use, and development effort are provided. (U.S.)

  15. Systems thinking.

    Science.gov (United States)

    Cabrera, Derek; Colosi, Laura; Lobdell, Claire

    2008-08-01

    Evaluation is one of many fields where "systems thinking" is popular and is said to hold great promise. However, there is disagreement about what constitutes systems thinking. Its meaning is ambiguous, and systems scholars have made diverse and divergent attempts to describe it. Alternative origins include: von Bertalanffy, Aristotle, Lao Tsu or multiple aperiodic "waves." Some scholars describe it as synonymous with systems sciences (i.e., nonlinear dynamics, complexity, chaos). Others view it as taxonomy-a laundry list of systems approaches. Within so much noise, it is often difficult for evaluators to find the systems thinking signal. Recent work in systems thinking describes it as an emergent property of four simple conceptual patterns (rules). For an evaluator to become a "systems thinker", he or she need not spend years learning many methods or nonlinear sciences. Instead, with some practice, one can learn to apply these four simple rules to existing evaluation knowledge with transformative results.

  16. Cognitive Systems

    DEFF Research Database (Denmark)

    The tutorial will discuss the definition of cognitive systems as the possibilities to extend the current systems engineering paradigm in order to perceive, learn, reason and interact robustly in open-ended changing environments. I will also address cognitive systems in a historical perspective...... to be modeled within a limited set of predefined specifications. There will inevitably be a need for robust decisions and behaviors in novel situations that include handling of conflicts and ambiguities based on the capability and knowledge of the artificial cognitive system. Further, there is a need...... in cognitive systems include e.g. personalized information systems, sensor network systems, social dynamics system and Web2.0, and cognitive components analysis. I will use example from our own research and link to other research activities....

  17. Crystal Systems.

    Science.gov (United States)

    Schomaker, Verner; Lingafelter, E. C.

    1985-01-01

    Discusses characteristics of crystal systems, comparing (in table format) crystal systems with lattice types, number of restrictions, nature of the restrictions, and other lattices that can accidently show the same metrical symmetry. (JN)

  18. Filter systems

    International Nuclear Information System (INIS)

    Vanin, V.R.

    1990-01-01

    The multidetector systems for high resolution gamma spectroscopy are presented. The observable parameters for identifying nuclides produced simultaneously in the reaction are analysed discussing the efficiency of filter systems. (M.C.K.)

  19. Microfluidic Radiometal Labeling Systems for Biomolecules

    Energy Technology Data Exchange (ETDEWEB)

    Reichert, D E; Kenis, P J. A.

    2011-12-29

    In a typical labeling procedure with radiometals, such as Cu-64 and Ga-68; a very large (~ 100-fold) excess of the non-radioactive reactant (precursor) is used to promote rapid and efficient incorporation of the radioisotope into the PET imaging agent. In order to achieve high specific activities, careful control of reaction conditions and extensive chromatographic purifications are required in order to separate the labeled compounds from the cold precursors. Here we propose a microfluidic approach to overcome these problems, and achieve high specific activities in a more convenient, semi-automated fashion and faster time frame. Microfluidic reactors, consisting of a network of micron-sized channels (typical dimensions in the range 10 - 300¼m), filters, separation columns, electrodes and reaction loops/chambers etched onto a solid substrate, are now emerging as an extremely useful technology for the intensification and miniaturization of chemical processes. The ability to manipulate, process and analyze reagent concentrations and reaction interfaces in both space and time within the channel network of a microreactor provides the fine level of reaction control that is desirable in PET radiochemistry practice. These factors can bring radiometal labeling, specifically the preparation of radio-labeled biomolecules such as antibodies, much closer to their theoretical maximum specific activities.

  20. Expert systems

    International Nuclear Information System (INIS)

    Haldy, P.A.

    1988-01-01

    The definitions of the terms 'artificial intelligence' and 'expert systems', the methodology, areas of employment and limits of expert systems are discussed. The operation of an expert system is described, especially the presentation and organization of knowledge as well as interference and control. Methods and tools for expert system development are presented and their application in nuclear energy are briefly addressed. 7 figs., 2 tabs., 6 refs

  1. Expert System

    DEFF Research Database (Denmark)

    Hildebrandt, Thomas Troels; Cattani, Gian Luca

    2016-01-01

    An expert system is a computer system for inferring knowledge from a knowledge base, typically by using a set of inference rules. When the concept of expert systems was introduced at Stanford University in the early 1970s, the knowledge base was an unstructured set of facts. Today the knowledge b...... for the application of expert systems, but also raises issues regarding privacy and legal liability....

  2. Retrofitting Systems

    DEFF Research Database (Denmark)

    Rose, Jørgen

    1997-01-01

    This report gives an overview of the different retrofitting possibilities that are available today. The report looks at both external and internal systems for external wall constructions, roof constructions, floor constructions and foundations. All systems are described in detail in respect to use...... and methods, and the efficiency of the different systems are discussed....

  3. Multifunction system

    International Nuclear Information System (INIS)

    Wauthier, J.; Fiori, R.

    1990-01-01

    The development, the characteristics and the applications of a multifunction system are presented. The system is used on the RBES laboratory pipes, at Marcoule. The system was developed in order to allow, without time loss, the modification of the circuit function by replacing only one component. The following elements form the multifunction system: a fixed base, which is part of the tube, a removable piece, which is inserted into the base, a cover plate and its locking system. The material, chosen among commercial trade marks, required small modifications in order to be used in the circuit [fr

  4. Operating systems

    CERN Document Server

    Tsichritzis, Dionysios C; Rheinboldt, Werner

    1974-01-01

    Operating Systems deals with the fundamental concepts and principles that govern the behavior of operating systems. Many issues regarding the structure of operating systems, including the problems of managing processes, processors, and memory, are examined. Various aspects of operating systems are also discussed, from input-output and files to security, protection, reliability, design methods, performance evaluation, and implementation methods.Comprised of 10 chapters, this volume begins with an overview of what constitutes an operating system, followed by a discussion on the definition and pr

  5. Systems integration.

    Science.gov (United States)

    Siemieniuch, C E; Sinclair, M A

    2006-01-01

    The paper presents a view of systems integration, from an ergonomics/human factors perspective, emphasising the process of systems integration as is carried out by humans. The first section discusses some of the fundamental issues in systems integration, such as the significance of systems boundaries, systems lifecycle and systems entropy, issues arising from complexity, the implications of systems immortality, and so on. The next section outlines various generic processes for executing systems integration, to act as guides for practitioners. These address both the design of the system to be integrated and the preparation of the wider system in which the integration will occur. Then the next section outlines some of the human-specific issues that would need to be addressed in such processes; for example, indeterminacy and incompleteness, the prediction of human reliability, workload issues, extended situation awareness, and knowledge lifecycle management. For all of these, suggestions and further readings are proposed. Finally, the conclusions section reiterates in condensed form the major issues arising from the above.

  6. Ternary systems

    International Nuclear Information System (INIS)

    Kagan, D.N.; Hubberstey, P.; Barker, M.G.

    1985-01-01

    The paper reviews the experimental and theoretical studies carried out on multicomponent alkali metal systems. Solid-liquid phase equilibria studies are mainly concerned with the systems Na-K-Rb and Na-K-Cs, and data on the liquidus temperatures in these systems are presented. The thermodynamic properties of the ternary Na-K-Cs eutectic system have been determined experimentally, and the enthalpy, heat capacity and excess functions of the alloy are given. An analysis of calculational methods used in determining thermodynamic functions of ternary liquid metals systems is described. Finally, data are tabulated for the density, compressibility, saturated vapour pressure, viscosity and thermal conductivity of the ternary Na-K-Cs eutectic system. (UK)

  7. Recommender systems

    CERN Document Server

    Kembellec, Gérald; Saleh, Imad

    2014-01-01

    Acclaimed by various content platforms (books, music, movies) and auction sites online, recommendation systems are key elements of digital strategies. If development was originally intended for the performance of information systems, the issues are now massively moved on logical optimization of the customer relationship, with the main objective to maximize potential sales. On the transdisciplinary approach, engines and recommender systems brings together contributions linking information science and communications, marketing, sociology, mathematics and computing. It deals with the understan

  8. Material Systems

    DEFF Research Database (Denmark)

    Jensen, Mads Brath; Mortensen, Henrik Rubæk; Mullins, Michael

    2009-01-01

    This paper describes and reflects upon the results of an investigative project which explores the setting up of a material system - a parametric and generative assembly consisting of and taking into consideration material properties, manufacturing constraints and geometric behavior. The project...... approaches the subject through the construction of a logic-driven system aiming to explore the possibilities of a material system that fulfills spatial, structural and performative requirements concurrently and how these are negotiated in situations where they might be conflicting....

  9. Systems Engineering

    OpenAIRE

    Vaughan, William W.

    2016-01-01

    The term “systems engineering” when entered into the Google search page, produces a significant number of results, evidence that systems engineering is recognized as being important for the success of essentially all products. Since most readers of this item will be rather well versed in documents concerning systems engineering, I have elected to share some of the points made on this subject in a document developed by the European Cooperation for Space Standardization (ECSS), a component of t...

  10. Energetic Systems

    Data.gov (United States)

    Federal Laboratory Consortium — The Energetic Systems Division provides full-spectrum energetic engineering services (project management, design, analysis, production support, in-service support,...

  11. Intelligent systems

    CERN Document Server

    Irwin, J David

    2011-01-01

    Technology has now progressed to the point that intelligent systems are replacing humans in the decision making processes as well as aiding in the solution of very complex problems. In many cases intelligent systems are already outperforming human activities. Artificial neural networks are not only capable of learning how to classify patterns, such images or sequence of events, but they can also effectively model complex nonlinear systems. Their ability to classify sequences of events is probably more popular in industrial applications where there is an inherent need to model nonlinear system

  12. Systemic darwinism.

    Science.gov (United States)

    Winther, Rasmus Grønfeldt

    2008-08-19

    Darwin's 19th century evolutionary theory of descent with modification through natural selection opened up a multidimensional and integrative conceptual space for biology. We explore three dimensions of this space: explanatory pattern, levels of selection, and degree of difference among units of the same type. Each dimension is defined by a respective pair of poles: law and narrative explanation, organismic and hierarchical selection, and variational and essentialist thinking. As a consequence of conceptual debates in the 20th century biological sciences, the poles of each pair came to be seen as mutually exclusive opposites. A significant amount of 21st century research focuses on systems (e.g., genomic, cellular, organismic, and ecological/global). Systemic Darwinism is emerging in this context. It follows a "compositional paradigm" according to which complex systems and their hierarchical networks of parts are the focus of biological investigation. Through the investigation of systems, Systemic Darwinism promises to reintegrate each dimension of Darwin's original logical space. Moreover, this ideally and potentially unified theory of biological ontology coordinates and integrates a plurality of mathematical biological theories (e.g., self-organization/structure, cladistics/history, and evolutionary genetics/function). Integrative Systemic Darwinism requires communal articulation from a plurality of perspectives. Although it is more general than these, it draws on previous advances in Systems Theory, Systems Biology, and Hierarchy Theory. Systemic Darwinism would greatly further bioengineering research and would provide a significantly deeper and more critical understanding of biological reality.

  13. Caste System

    OpenAIRE

    Hoff, Karla

    2016-01-01

    In standard economics, individuals are rational actors and economic forces undermine institutions that impose large inefficiencies. The persistence of the caste system is evidence of the need for psychologically more realistic models of decision-making in economics. The caste system divides South Asian society into hereditary groups whose lowest ranks are represented as innately polluted. ...

  14. Recommender systems

    OpenAIRE

    Lu L.; Medo M.; Yeung C.H.; Zhang Y.-C.; Zhang Z.-K.; Zhou T.

    2012-01-01

    The ongoing rapid expansion of the Internet greatly increases the necessity of effective recommender systems for filtering the abundant information. Extensive research for recommender systems is conducted by a broad range of communities including social and computer scientists, physicists, and interdisciplinary researchers. Despite substantial theoretical and practical achievements, unification and comparison of different approaches are lacking, which impedes further advances. In this article...

  15. GEOMASS system

    International Nuclear Information System (INIS)

    Ohyama, Takuya; Saegusa, Hiromitsu

    2009-03-01

    As a part of the research and development regarding characterisation of deep geological environment, the GEOMASS (GEOLOGICAL MODELLING ANALYSIS AND SIMULATION SOFTWARE) system has been developed by the Japan Atomic Energy Agency in order to carry out geological and hydrogeological modelling and groundwater flow simulation and so on. The GEOMASS system integrates a commercial geological interpretation system (EarthVision), which is used for geological modelling and visualisation, with a proprietary code for groundwater flow (FracAffinity). This integrated system allows users to make rapid improvement of models as data increases. Also, it is possible to perform more realistic groundwater flow simulation due to the capability of modelling the rock mass as a continuum with discrete hydro-structural features in the rock mass. This paper consists of 'Overview of GEOMASS system', FracAffinity Theoretical Background' and 'FracAffinity User Guide' and is edited as a GEOMASS system manual. 'Overview of GEOMASS system' describes the outline of this system. 'FracAffinity Theoretical Background' describes the information of technical background of FracAffinity software. FracAffinity User Guide' describes the structure of the FracAffinity input files, the usage of FracAffinity Interface and flow-solver. Updating of the FracAffinity has been continued as needed and FracAffinity version3.3 is the latest version at present (July 2008). (author)

  16. Systems integration (automation system). System integration (automation system)

    Energy Technology Data Exchange (ETDEWEB)

    Fujii, K; Komori, T; Fukuma, Y; Oikawa, M [Nippon Steal Corp., Tokyo (Japan)

    1991-09-26

    This paper introduces business activities on an automation systems integration (SI) started by a company in July,1988, and describes the SI concepts. The business activities include, with the CIM (unified production carried out on computers) and AMENITY (living environment) as the mainstays, a single responsibility construction ranging from consultation on structuring optimal systems for processing and assembling industries and intelligent buildings to system design, installation and after-sales services. With an SI standing on users {prime} position taken most importantly, the business starts from a planning and consultation under close coordination. On the conceptual basis of structuring optimal systems using the ompany {prime}s affluent know-hows and tools and adapting and applying with multi-vendors, open networks, centralized and distributed systems, the business is promoted with the accumulated technologies capable of realizing artificial intelligence and neural networks in its background, and supported with highly valuable business results in the past. 10 figs., 1 tab.

  17. Creative Systems

    DEFF Research Database (Denmark)

    Manelius, Anne-Mette; Beim, Anne

    2007-01-01

    Opsamling af diskussioner på konferencen og udstillingen Creative Systems i september/oktober 2007. Konferencen og Udstillingen Creative Systems sætter fokus på systemer som en positiv drivkraft i den kreative skabelsesproces. CINARK inviterede fire internationale kapaciteter, som indenfor hver...... deres felt har beskæftiget sig med udviklingen af systemer. Kieran Timberlake, markant amerikansk tegnestue; Mark West, Professor på University of Manitoba, Canada, og pioner indenfor anvendelse af tekstilforskalling til betonstøbninger; Matilda McQuaid, Arkitekturhistoriker og kurator på udstillingen...... om Extreme Textiles på amerikanske Cooper Hewit Design Museum, samt Professor Ludger Hovestadt, ved ETH, Zürich der fokuserer på udvikling og anvendelse af logaritmiske systemtilgange. Udstillingen diskuterede ud fra deres meget forskellige arbejder, det kreative potentiale i anvendelsen af systemer...

  18. Reactive Systems

    DEFF Research Database (Denmark)

    Aceto, Luca; Ingolfsdottir, Anna; Larsen, Kim Guldstrand

    A reactive system comprises networks of computing components, achieving their goals through interaction among themselves and their environment. Thus even relatively small systems may exhibit unexpectedly complex behaviours. As moreover reactive systems are often used in safety critical systems......, the need for mathematically based formal methodology is increasingly important. There are many books that look at particular methodologies for such systems. This book offers a more balanced introduction for graduate students and describes the various approaches, their strengths and weaknesses, and when...... they are best used. Milner's CCS and its operational semantics are introduced, together with the notions of behavioural equivalences based on bisimulation techniques and with recursive extensions of Hennessy-Milner logic. In the second part of the book, the presented theories are extended to take timing issues...

  19. Upgraded RECOVER system - CASDAC system

    International Nuclear Information System (INIS)

    Yamamoto, Yoichi; Koyama, Kinji

    1992-03-01

    The CASDAC (Containment And Surveillance Data Authenticated Communication) system has been developed by JAERI for nuclear safeguards and physical protection of nuclear material. This system was designed and constructed as an upgraded RECOVER system, design concept of which was based on the original RECOVER system and also the TRANSEAVER system. Both of them were developed several years ago as a remote monitoring system for continual verification of security and safeguards status of nuclear material. The system consists of two subsystems, one of them is a Grand Command Center (GCC) subsystem and the other is a facility subsystem. Communication between the two subsystems is controlled through the international telephone line network. Therefore all communication data are encrypted to prevent access by an unauthorized person who may intend to make a falsification, or tapping. The facility subsystem has an appropriate measure that ensure data security and reliable operation under unattended mode of operator. The software of this system is designed so as to be easily used in other different types of computers. This report describes the outline of the CASDAC system and the results of its performance test. This work has been carried out in the framework of Japan Support Programme for Agency Safeguards (JASPAS) as a project, JA-1. (author)

  20. Watchdog System

    DEFF Research Database (Denmark)

    Madsen, Tanja Kidholm Osmann; Bahnsen, Chris Holmberg; Jensen, Morten Bornø

    This deliverable is part of WP4. Overall WP4 is motivated by the need for automatic systems that can ease the task of annotating massive amounts of traffic data. Concretely this deliverable is related to WP4.2 - the watchdog system. The idea with the watchdog is to develop a system that can remov...... huge chunks of video data where no events/interactions of interest are occurring and hence let a user focus on manually annotation of only the interesting stuff....

  1. Dynamical systems

    CERN Document Server

    Sternberg, Shlomo

    2010-01-01

    Celebrated mathematician Shlomo Sternberg, a pioneer in the field of dynamical systems, created this modern one-semester introduction to the subject for his classes at Harvard University. Its wide-ranging treatment covers one-dimensional dynamics, differential equations, random walks, iterated function systems, symbolic dynamics, and Markov chains. Supplementary materials offer a variety of online components, including PowerPoint lecture slides for professors and MATLAB exercises.""Even though there are many dynamical systems books on the market, this book is bound to become a classic. The the

  2. Water systems

    International Nuclear Information System (INIS)

    Riess, R.

    1980-01-01

    The present paper describes the coolant chemistry and its consequences for 1300 MWsub(e) KWU PWR plants. Some selected systems, i.e. primary heat transport system, steam water cycle and cooling water arrangements, are chosen for this description. Various aspects of coolant chemistry regarding general corrosion, selective types of corrosion and deposits on heat transfer surfaces have been discussed. The water supply systems necessary to fulfill the requirements of the coolant chemistry are discussed as well. It has been concluded that a good operating performance can only be achieved when - beside other factors - the water chemistry has been given sufficient consideration. (orig./RW)

  3. Water systems

    International Nuclear Information System (INIS)

    Riess, R.

    1981-01-01

    The present paper describes the coolant chemistry and its consequences for 1300 MWsub(e) KWU PWR plants. Some selected systems, i.e. primary heat transport system, steam water cycle and cooling water arrangements, are chosen for this description. Various aspects of coolant chemistry regarding general corrosion, selective types of corrosion and deposits on heat transfer surface have been discussed. The water supply systems necessary to fulfill the requirements of the coolant chemistry are discussed as well. It has been concluded that a good operating performance can only be achieved when - beside other factors - the water chemistry has been given sufficient consideration. (orig./RW)

  4. Imaging system

    International Nuclear Information System (INIS)

    Froggatt, R.J.

    1981-01-01

    The invention provides a two dimensional imaging system in which a pattern of radiation falling on the system is detected to give electrical signals for each of a plurality of strips across the pattern. The detection is repeated for different orientations of the strips and the whole processed by compensated back projection. For a shadow x-ray system a plurality of strip x-ray detectors are rotated on a turntable. For lower frequencies the pattern may be rotated with a Dove prism and the strips condensed to suit smaller detectors with a cylindrical lens. (author)

  5. Kaonic systems

    Directory of Open Access Journals (Sweden)

    Oset E.

    2012-12-01

    Full Text Available I make a short review of the situation of the kaonic systems, with novel information supporting the two Λ(1405 states from the K-d → nπΣ reaction. A review is made of the K¯$ar K$NN system with recent calculations converging to smaller bindings and larger widths. Novel systems involving two kaons and one nucleon or three kaons are also reported and finally a short discussion is made of the analogous state DNN for which recent studies find a large binding and a small width.

  6. The systems integration modeling system

    International Nuclear Information System (INIS)

    Danker, W.J.; Williams, J.R.

    1990-01-01

    This paper discusses the systems integration modeling system (SIMS), an analysis tool for the detailed evaluation of the structure and related performance of the Federal Waste Management System (FWMS) and its interface with waste generators. It's use for evaluations in support of system-level decisions as to FWMS configurations, the allocation, sizing, balancing and integration of functions among elements, and the establishment of system-preferred waste selection and sequencing methods and other operating strategies is presented. SIMS includes major analysis submodels which quantify the detailed characteristics of individual waste items, loaded casks and waste packages, simulate the detailed logistics of handling and processing discrete waste items and packages, and perform detailed cost evaluations

  7. A novel fractional sliding mode control configuration for ...

    Indian Academy of Sciences (India)

    Karima Rabah

    2017-09-09

    Sep 9, 2017 ... for synchronizing disturbed fractional-order chaotic systems. KARIMA RABAH1, SAMIR ... duced to realize chaos synchronization, such as PC control [19] .... where t0 is the initial time, α ∈ (0,1), λ > 0, b > 0, m(0) = 0, m(x) ≥ 0 .... where k = k2/k1 is a positive real number. Choosing .... operating conditions.

  8. ring system

    African Journals Online (AJOL)

    1,3,2-DIAZABORACYCLOALKANE. RING SYSTEM. Negussie Retta" and Robert H. Neilson. 'Department of Chemistry, Addis Ababa University, P.O. Box 1176, Addis Ababa, Ethiopia. Department of Chemistry, Texas Christian University.

  9. Septic Systems

    Science.gov (United States)

    The web site provides guidance and technical assistance for homeowners, government officials, industry professionals, and EPA partners about how to properly develop and manage individual onsite and community cluster systems that treat domestic wastewater.

  10. Respiratory system

    Science.gov (United States)

    Bartlett, R. G., Jr.

    1973-01-01

    The general anatomy and function of the human respiratory system is summarized. Breathing movements, control of breathing, lung volumes and capacities, mechanical relations, and factors relevant to respiratory support and equipment design are discussed.

  11. Bubble systems

    CERN Document Server

    Avdeev, Alexander A

    2016-01-01

    This monograph presents a systematic analysis of bubble system mathematics, using the mechanics of two-phase systems in non-equilibrium as the scope of analysis. The author introduces the thermodynamic foundations of bubble systems, ranging from the fundamental starting points to current research challenges. This book addresses a range of topics, including description methods of multi-phase systems, boundary and initial conditions as well as coupling requirements at the phase boundary. Moreover, it presents a detailed study of the basic problems of bubble dynamics in a liquid mass: growth (dynamically and thermally controlled), collapse, bubble pulsations, bubble rise and breakup. Special emphasis is placed on bubble dynamics in turbulent flows. The analysis results are used to write integral equations governing the rate of vapor generation (condensation) in non-equilibrium flows, thus creating a basis for solving a number of practical problems. This book is the first to present a comprehensive theory of boil...

  12. Systems Biology

    Indian Academy of Sciences (India)

    IAS Admin

    study and understand the function of biological systems, particu- larly, the response of such .... understand the organisation and behaviour of prokaryotic sys- tems. ... relationship of the structure of a target molecule to its ability to bind a certain ...

  13. Bricks / Systems

    DEFF Research Database (Denmark)

    At first glance, this book may appear eclectic. It contains writings from architectural practice in a language and structure based on subjective views and experiences, combined with research contributions based on systematic design investigations of discrete computational systems. Discussions range......, and it aims to illustrate and identify new modes of working in architecture, particularly with regards to brickwork and other complex systems of modular assemblies, whether physical or digital....

  14. Expert Systems

    OpenAIRE

    Lucas, P.J.F.

    2005-01-01

    Expert systems mimic the problem-solving activity of human experts in specialized domains by capturing and representing expert knowledge. Expert systems include a knowledge base, an inference engine that derives conclusions from the knowledge, and a user interface. Knowledge may be stored as if-then rules, orusing other formalisms such as frames and predicate logic. Uncertain knowledge may be represented using certainty factors, Bayesian networks, Dempster-Shafer belief functions, or fuzzy se...

  15. Nanorobotic Systems

    Directory of Open Access Journals (Sweden)

    Lixin Dong

    2008-11-01

    Full Text Available Two strategies towards the realization of nanotechnology have been presented, i.e., top-down and bottom up. The former one is mainly based on nanofabrication and includes technologies such as nano-lithography, nano-imprint, and etching. Presently, they are still 2D fabrication processes with low resolution. The later one is an assembly-based technique. At present, it includes such items as self-assembly, dip-pen lithography, and directed self-assembly. These techniques can generate regular nano patterns in large scales. To fabricate 3D complex nano devices there are still no effective ways by so far. Here we show our effort on the development of a nano laboratory, a prototype nanomanufacturing system, based on nanorobotic manipulations. In which, we take a hybrid strategy as shown in Fig. 1. In this system, nano fabrication and nano assembly can be performed in an arbitrary order to construct nano building blocks and finally nano devices. The most important feature in this system is that the products can be fed back into the system to shrink the system part by part leading to nanorobots. Property characterization can be performed in each intermediate process. Due to the nanorobotic manipulation system, dynamic measurement can be performed rather than conventional static observations.

  16. Fiscal system analysis - contractual systems

    International Nuclear Information System (INIS)

    Kaiser, M.J.

    2006-01-01

    Production sharing contracts are one of the most popular forms of contractual system used in petroleum agreements around the world, but the manner in which the fiscal terms and contract parameters impact system measures is complicated and not well understood. The purpose of this paper is to quantify the influence of private and market uncertainty in contractual fiscal systems. A meta-modelling approach is employed that couples the results of a simulation model with regression analysis to construct numerical functionals that quantify the fiscal regime. Relationships are derived that specify how the present value, rate of return, and take statistics vary as a function of the system parameters. The deepwater Girassol field development in Angola is taken as a case study. (author)

  17. Reactor system

    International Nuclear Information System (INIS)

    Miyano, Hiroshi; Narabayashi, Naoshi.

    1990-01-01

    The represent invention concerns a reactor system with improved water injection means to a pressure vessel of a BWR type reactor. A steam pump is connected to a heat removing system pipeline, a high pressure water injection system pipeline and a low pressure water injection system pipeline for injecting water into the pressure vessel. A pump actuation pipeline is disposed being branched from a main steam pump or a steam relieaf pipeline system, through which steams are supplied to actuate the steam pump and supply cooling water into the pressure vessel thereby cooling the reactor core. The steam pump converts the heat energy into the kinetic energy and elevates the pressure of water to a level higher than the pressure of the steams supplied by way of a pressure-elevating diffuser. Cooling water can be supplied to the pressure vessel by the pressure elevation. This can surely inject cooling water into the pressure vessel upon loss of coolant accident or in a case if reactor scram is necessary, without using an additional power source. (I.N.)

  18. ARAC system

    International Nuclear Information System (INIS)

    Kelly, M.F.; Wyman, R.H.

    1975-01-01

    In spite of the remarkable safety record of the nuclear industry as a whole, recent public concern over the potential impact of the industry's accelerated growth has prompted ERDA to expand its emergency response procedures. The Atmospheric Release Advisory Capability, ARAC, is a computer communications system designed to enhance the existing emergency response capability of ERDA nuclear facilities. ARAC will add at least two new functions to this capability: centralized, real-time data acquisition and storage, and simulation of the long range atmospheric transport of hazardous materials. To perform these functions, ARAC employs four major sub-systems or facilities: the site facility, the central facility, the global weather center and the regional model. The system has been under development for the past two years at the Lawrence Livermore Laboratory of the University of California

  19. Microbiology System

    Science.gov (United States)

    1992-01-01

    Technology originating in a NASA-sponsored study of the measurement of microbial growth in zero gravity led to the development of Biomerieux Vitek, Inc.'s VITEK system. VITEK provides a physician with accurate diagnostic information and identifies the most effective medication. Test cards are employed to identify organisms and determine susceptibility to antibiotics. A photo-optical scanner scans the card and monitors changes in the growth of cells contained within the card. There are two configurations - VITEK and VITEK JR as well as VIDAS, a companion system that detects bacteria, viruses, etc. from patient specimens. The company was originally created by McDonnell Douglas, the NASA contractor.

  20. Spin systems

    CERN Document Server

    Caspers, W J

    1989-01-01

    This book is about spin systems as models for magnetic materials, especially antiferromagnetic lattices. Spin-systems are well-defined models, for which, in special cases, exact properties may be derived. These special cases are for the greater part, one- dimensional and restricted in their applicability, but they may give insight into general properties that also exist in higher dimension. This work pays special attention to qualitative differences between spin lattices of different dimensions. It also replaces the traditional picture of an (ordered) antiferromagnetic state of a Heisenberg sy

  1. Distributed systems

    CERN Document Server

    Van Steen, Maarten

    2017-01-01

    For this third edition of "Distributed Systems," the material has been thoroughly revised and extended, integrating principles and paradigms into nine chapters: 1. Introduction 2. Architectures 3. Processes 4. Communication 5. Naming 6. Coordination 7. Replication 8. Fault tolerance 9. Security A separation has been made between basic material and more specific subjects. The latter have been organized into boxed sections, which may be skipped on first reading. To assist in understanding the more algorithmic parts, example programs in Python have been included. The examples in the book leave out many details for readability, but the complete code is available through the book's Website, hosted at www.distributed-systems.net.

  2. Research Projects for Interrogations of Biological Systems: Training for the Development of Novel Radiotracers

    Energy Technology Data Exchange (ETDEWEB)

    Jurisson, Silvia S. [Univ. of Missouri, Columbia, MO (United States); Lever, Susan Z. [Univ. of Missouri, Columbia, MO (United States); Robertson, J. David [Univ. of Missouri, Columbia, MO (United States)

    2016-10-04

    This grant was situated at the University of Missouri to train Ph.D. scientists in radiochemistry and synthetic chemistry in conjunction with Faculty from the Interdisciplinary Plant Group, Division of Biological Sciences, the MU Research Reactor Center, Molecular Biology and the Radiopharmaceutical Sciences Institute. This project was collaborative with Brookhaven National Laboratory (Richard Ferrieri, PI). Projects for the Ph.D. candidates included novel probe development for peptides, nucleosides, small molecules or radiometals, the direct use of radiometals as probes, or nuclear techniques for analysis. The projects for the postdoctoral fellow involved synthetic chemistry for the preparation of precursors for novel tracers that will be radiolabeled with 18F or other appropriate radionuclides. The skill sets of our team members allowed us to prepare probes with positron or single photon emitters, as well as ones that are dual-labeled (fluorescent and radiolabeled). We focused our technical advances to those that will be broadly applicable to any research field.

  3. Research Projects for Interrogations of Biological Systems: Training for the Development of Novel Radiotracers

    International Nuclear Information System (INIS)

    Jurisson, Silvia S.; Lever, Susan Z.; Robertson, J. David

    2016-01-01

    This grant was situated at the University of Missouri to train Ph.D. scientists in radiochemistry and synthetic chemistry in conjunction with Faculty from the Interdisciplinary Plant Group, Division of Biological Sciences, the MU Research Reactor Center, Molecular Biology and the Radiopharmaceutical Sciences Institute. This project was collaborative with Brookhaven National Laboratory (Richard Ferrieri, PI). Projects for the Ph.D. candidates included novel probe development for peptides, nucleosides, small molecules or radiometals, the direct use of radiometals as probes, or nuclear techniques for analysis. The projects for the postdoctoral fellow involved synthetic chemistry for the preparation of precursors for novel tracers that will be radiolabeled with "1"8F or other appropriate radionuclides. The skill sets of our team members allowed us to prepare probes with positron or single photon emitters, as well as ones that are dual-labeled (fluorescent and radiolabeled). We focused our technical advances to those that will be broadly applicable to any research field.

  4. Radioecological state of some surface water systems of contaminated areas of both Gomel and Mogilev Regions

    International Nuclear Information System (INIS)

    Datskevich, P. I.; Komissariv, F. D.; Khvale', O. D.; Basharina, L. P.; Lobach, I. L.

    1997-01-01

    The radioecological situation of different ecosystems of Belarus and their components has been analysed. Such components of the surface water ecosystems as water, suspensions, sediments and soils of water-collection areas were used for the investigation of the content of cesium 137 and strontium 90. The received data were given since 1990. The content of cesium 137 and strontium 90 in the components of water ecosystems was counted in the laboratory conditions by means of standard methods of beta radiometry, semiconductor gamma spectrometry and radiochemistry. The error of measurement of radioactivity was not higher than 25 and 35% for cesium 137 and strontium 90 accordingly. Water ecosystems were distinguished by the state of contamination of water-collection areas and hydrological parameters. These and some other reasons considered in the article influence on the character of cesium 137 and strontium 90 behaviour in water ecosystems

  5. Immune System

    Science.gov (United States)

    ... of the Immune System Print en español El sistema inmunitario Whether you're stomping through the showers ... of Use Notice of Nondiscrimination Visit the Nemours Web site. Note: All information on TeensHealth® is for ...

  6. Operating Systems

    Indian Academy of Sciences (India)

    areas in which this type is useful are multimedia, virtual reality, and advanced scientific projects such as undersea exploration and planetary rovers. Because of the expanded uses for soft real-time functionality, it is finding its way into most current operating systems, including major versions of Unix and Windows NT OS.

  7. Barrier Systems

    NARCIS (Netherlands)

    Heteren, S. van

    2015-01-01

    Barrier-system dynamics are a function of antecedent topography and substrate lithology, Relative sea-level (RSL) changes, sediment availability and type, climate, vegetation type and cover, and various aero- and hydrodynamic processes during fair-weather conditions and extreme events. Global change

  8. Systems Science

    Science.gov (United States)

    Christakis, Alexander; Hammond, Debora; Jackson, Michael; Laszlo, Alexander; Mitroff, Ian; Snowden, Dave; Troncale, Len; Carr-Chellman, Alison; Spector, J. Michael; Wilson, Brent

    2013-01-01

    Scholars representing the field of systems science were asked to identify what they considered to be the most exciting and imaginative work currently being done in their field, as well as how that work might change our understanding. The scholars included Alexander Christakis, Debora Hammond, Michael Jackson, Alexander Laszlo, Ian Mitroff, Dave…

  9. Transport system

    NARCIS (Netherlands)

    Drenth, K.F.

    1999-01-01

    The transport system comprises at least one road surface (2) and at least one vehicle (4) on wheels (6). The road surface (2) has a substantially bowl-shaped cross section and the vehicle (4) is designed so that the wheels (6) run directly on the road surface (2) while the road surface (2) acts as a

  10. Quorum Systems

    DEFF Research Database (Denmark)

    Wattenhofer, Roger; Förster, Klaus-Tycho

    2016-01-01

    What happens if a single server is no longer powerful enough to service all your customers? The obvious choice is to add more servers and to use the majority approach (e.g. Paxos, Chapter 2) to guarantee consistency. However, even if you buy one million servers, a client still has to access more ...... study the theory behind overlapping sets, known as quorum systems....

  11. System Dynamics

    Science.gov (United States)

    Morecroft, John

    System dynamics is an approach for thinking about and simulating situations and organisations of all kinds and sizes by visualising how the elements fit together, interact and change over time. This chapter, written by John Morecroft, describes modern system dynamics which retains the fundamentals developed in the 1950s by Jay W. Forrester of the MIT Sloan School of Management. It looks at feedback loops and time delays that affect system behaviour in a non-linear way, and illustrates how dynamic behaviour depends upon feedback loop structures. It also recognises improvements as part of the ongoing process of managing a situation in order to achieve goals. Significantly it recognises the importance of context, and practitioner skills. Feedback systems thinking views problems and solutions as being intertwined. The main concepts and tools: feedback structure and behaviour, causal loop diagrams, dynamics, are practically illustrated in a wide variety of contexts from a hot water shower through to a symphony orchestra and the practical application of the approach is described through several real examples of its use for strategic planning and evaluation.

  12. System Description:

    DEFF Research Database (Denmark)

    Schürmann, Carsten; Poswolsky, Adam

    2009-01-01

    Delphin is a functional programming language [Adam Poswolsky and Carsten Schürmann. Practical programming with higher-order encodings and dependent types. In European Symposium on Programming (ESOP), 2008] utilizing dependent higher-order datatypes. Delphin's two-level type-system cleanly separates...

  13. Immune System

    Science.gov (United States)

    A properly functioning immune system is essential to good health. It defends the body against infectious agents and in some cases tumor cells. Individuals with immune deficiencies resulting from genetic defects, diseases (e.g., AIDS, leukemia), or drug therapies are more suscepti...

  14. Bioenergy systems

    International Nuclear Information System (INIS)

    Mitchell, C.P.

    1997-01-01

    The objective of this paper is to demonstrate that a bioenergy system has to be considered as an integrated process in which each stage or step interacts with other steps in the overall process. There are a number of stages in the supply and conversion of woody biomass for energy. Each step in the chain has implications for the next step and for overall system efficiency. The resource can take many forms and will have varying physical and chemical characteristics which will influence the efficiency and cost of conversion. The point in the supply chain at which size and moisture content is reduced and the manner in which it is done is influential in determining feedstock delivered cost and overall system costs. To illustrate the interactions within the overall system, the influence of the nature, size and moisture content of delivered feedstocks on costs of generating electricity via thermal conversion processes is examined using a model developed to investigate the inter-relationships between the stages in the supply chain. (author)

  15. Urogenital system

    International Nuclear Information System (INIS)

    Hamm, B.; Asbach, P.; Beyersdorff, D.; Hein, P.; Zaspel, U.

    2007-01-01

    The book is focussed on the radiological diagnostics of diseases in the urogential system. The description of the specific diseases, the identification by modern imaging techniques, the interpretation of examinatory results and therapeutic options are systematically treated in 4 chapters: kidney and adrenal glands, urinary tract, male genitals, female genitals

  16. Mirror systems.

    Science.gov (United States)

    Fogassi, Leonardo; Ferrari, Pier Francesco

    2011-01-01

    Mirror neurons are a class of visuomotor neurons, discovered in the monkey premotor cortex and in an anatomically connected area of the inferior parietal lobule, that activate both during action execution and action observation. They constitute a circuit dedicated to match actions made by others with the internal motor representations of the observer. It has been proposed that this matching system enables individuals to understand others' behavior and motor intentions. Here we will describe the main features of mirror neurons in monkeys. Then we will present evidence of the presence of a mirror system in humans and of its involvement in several social-cognitive functions, such as imitation, intention, and emotion understanding. This system may have several implications at a cognitive level and could be linked to specific social deficits in humans such as autism. Recent investigations addressed the issue of the plasticity of the mirror neuron system in both monkeys and humans, suggesting also their possible use in rehabilitation. WIREs Cogn Sci 2011 2 22-38 DOI: 10.1002/wcs.89 For further resources related to this article, please visit the WIREs website. Copyright © 2010 John Wiley & Sons, Ltd.

  17. Systemic Planning

    DEFF Research Database (Denmark)

    Leleur, Steen

    This book presents principles and methodology for planning in a complex world. It sets out a so-called systemic approach to planning, among other things, by applying “hard” and “soft” methodologies and methods in combination. The book is written for Ph.D and graduate students in engineering...

  18. Implementasi Penggunaan Smartphone Android untuk Control PC (Personal Computer

    Directory of Open Access Journals (Sweden)

    Imam Solikin

    2018-05-01

    Full Text Available The purpose of this research is to simplify the control of personal computer (PC such as control pointer, keyboard control and make it easier to do the presentation by controlling the slide remotely using smartphone through wifi connections facility. The smartphone is a multimedia phone that combines PC functionality with microprocessor, memory, and built-in modem to produce smart smartphone gadgets. Problems that occur when performing a presentation such as PC control, control pointer and keyboard control for input should be close to the PC so it is less than optimal in explaining the material. The model used in implementing the use of Android Smartphone for PC control is a conceptual model consisting of several stages: potential and problems, data collection, system testing, test results, and system implementation or implementation. From the results of PC control research can be done by connecting the Smartphone with a PC via wifi network so that PC can be controlled remotely. PC control application is an application that can control PC remotely connected via wifi network connection. Benefits derived from this research make it easy to mengedalikan PC remotely such as facilitate in the percentage and control pointer and control Keyboard for input process.

  19. Energy systems

    International Nuclear Information System (INIS)

    Haefele, W.

    1974-01-01

    Up to the present the production, transmission and distribution of energy has been considered mostly as a fragmented problem; at best only subsystems have been considered. Today the scale of energy utilization is increasing rapidly, and correspondingly, the reliance of societies on energy. Such strong quantitative increases influence the qualitative nature of energy utilization in most of its aspects. Resources, reserves, reliability and environment are among the key words that may characterize the change in the nature of the energy utilization problem. Energy can no longer be considered an isolated technical and economical problem, rather it is embedded in the ecosphere and the society-technology complex. Restraints and boundary conditions have to be taken into account with the same degree of attention as in traditional technical problems, for example a steam turbine. This results in a strong degree of interweaving. Further, the purpose of providing energy becomes more visible, that is, to make survival possible in a civilized and highly populated world on a finite globe. Because of such interweaving and finiteness it is felt that energy should be considered as a system and therefore the term 'energy systems' is used. The production of energy is only one component of such a system; the handling of energy and the embedding of energy into the global and social complex in terms of ecology, economy, risks and resources are of similar importance. he systems approach to the energy problem needs more explanation. This paper is meant to give an outline of the underlying problems and it is hoped that by so doing the wide range of sometimes confusing voices about energy can be better understood. Such confusion starts already with the term 'energy crisis'. Is there an energy crisis or not? Much future work is required to tackle the problems of energy systems. This paper can only marginally help in that respect. But it is hoped that it will help understand the scope of the

  20. Energy systems

    Energy Technology Data Exchange (ETDEWEB)

    Haefele, W [Nuclear Research Centre, Applied Systems Analysis and Reactor Physics, Karlsruhe (Germany); International Institute for Applied Systems Analysis, Laxenburg (Austria)

    1974-07-01

    Up to the present the production, transmission and distribution of energy has been considered mostly as a fragmented problem; at best only subsystems have been considered. Today the scale of energy utilization is increasing rapidly, and correspondingly, the reliance of societies on energy. Such strong quantitative increases influence the qualitative nature of energy utilization in most of its aspects. Resources, reserves, reliability and environment are among the key words that may characterize the change in the nature of the energy utilization problem. Energy can no longer be considered an isolated technical and economical problem, rather it is embedded in the ecosphere and the society-technology complex. Restraints and boundary conditions have to be taken into account with the same degree of attention as in traditional technical problems, for example a steam turbine. This results in a strong degree of interweaving. Further, the purpose of providing energy becomes more visible, that is, to make survival possible in a civilized and highly populated world on a finite globe. Because of such interweaving and finiteness it is felt that energy should be considered as a system and therefore the term 'energy systems' is used. The production of energy is only one component of such a system; the handling of energy and the embedding of energy into the global and social complex in terms of ecology, economy, risks and resources are of similar importance. he systems approach to the energy problem needs more explanation. This paper is meant to give an outline of the underlying problems and it is hoped that by so doing the wide range of sometimes confusing voices about energy can be better understood. Such confusion starts already with the term 'energy crisis'. Is there an energy crisis or not? Much future work is required to tackle the problems of energy systems. This paper can only marginally help in that respect. But it is hoped that it will help understand the scope of the

  1. TUBO system

    International Nuclear Information System (INIS)

    Barbosa, H.J.C.; Guerreiro, J.N.C.; Toledo, E.M.

    1980-01-01

    Proceedings recently incorporated to TUBO system like the seismic analysis and the stress verification acccording to ASME-Boiler Rule and Pressure Vessel Code-section III are presented. The seismic analysis comprehend the consideration of uniform motion of the support, its multiple excitation, and the attainment of the spectral response for both cases. The module for stress verification uses stresses resulting fromthe combination of the loads specified by the user, in the automatic verification of permissible stresses for the pipings class 1 and 2, based on criteria NB-3650 and NC-3650 of ASME. The implementation of these proceedings in the TUBO system are discussed and a numerical example that covers the different phases of a stress analysis in a piping is presented [pt

  2. Solar Systems

    Science.gov (United States)

    1979-01-01

    The solar collectors shown are elements of domestic solar hot water systems produced by Solar One Ltd., Virginia Beach, Virginia. Design of these systems benefited from technical expertise provided Solar One by NASA's Langley Research Center. The company obtained a NASA technical support package describing the d e sign and operation of solar heating equipment in NASA's Tech House, a demonstration project in which aerospace and commercial building technology are combined in an energy- efficient home. Solar One received further assistance through personal contact with Langley solar experts. The company reports that the technical information provided by NASA influenced Solar One's panel design, its selection of a long-life panel coating which increases solar collection efficiency, and the method adopted for protecting solar collectors from freezing conditions.

  3. Bilateral system. The ABACC system

    International Nuclear Information System (INIS)

    Nicolas, Ruben O.

    2001-01-01

    After relating the antecedents of the creation of the Brazilian-Argentine Agency for the Accounting and Control of Nuclear Materials (ABACC), the paper describes the common system of accounting and control set up by Argentina and Brazil. The organization of ABACC is also outlined

  4. Physical system requirements: Overall system

    International Nuclear Information System (INIS)

    1992-01-01

    The Nuclear Waste Policy Act (NWPA) of 1982 assigned to the Department of Energy (DOE) the responsibility for managing the disposal of spent nuclear fuel and high-level radioactive waste and established the Office of Civilian Radioactive Waste Management (OCRWM) for that purpose. The Secretary of Energy, in his November 1989 report to Congress (DOE/RW-0247), announced three new initiatives for conduct of the Civilian Radioactive Waste Management (CRWM) program. One of these initiatives was to establish improved management structure and procedures. In response, OCRWM performed a management study and the Direct subsequently issued the Management Systems Improvement Strategy (MSIS) on August 10, 1990, calling for a rigorous implementation of systems engineering principles with a special emphasis on functional analysis. This approach establishes a framework for integrating the program management efforts with the technical requirements analysis into a single, unified, and consistent program. The functional analysis approach recognizes that just the facilities and equipment comprising the physical waste management system must perform certain functions, so must certain programmatic and management functions be performed within the program in order to successfully bring the physical system into being

  5. Security system

    Science.gov (United States)

    Baumann, Mark J.; Kuca, Michal; Aragon, Mona L.

    2016-02-02

    A security system includes a structure having a structural surface. The structure is sized to contain an asset therein and configured to provide a forceful breaching delay. The structure has an opening formed therein to permit predetermined access to the asset contained within the structure. The structure includes intrusion detection features within or associated with the structure that are activated in response to at least a partial breach of the structure.

  6. Cardiovascular system

    International Nuclear Information System (INIS)

    Soulen, R.L.; Grosh, J.

    1984-01-01

    Invasive cardiovascular diagnostic procedures involve a finite risk and therefore can be recommended only when the benefit appears to exceed the risk by a substantial margin. The risk/benefit ratio varies not only with the procedure concerned but with the status of the vascular system, concomitant diseases, and the risks of both the suspected illness and its treatment. The risks inherent in the procedures per se are detailed in the sections to follow

  7. Priority Systems

    OpenAIRE

    Gössler , Gregor; Sifakis , Joseph

    2004-01-01

    Projet POP_ART; We present a framework for the incremental construction of deadlock-free systems meeting given safety properties. The framework borrows concepts and basic results from the controller synthesis paradigm by considering a step in the construction process as a controller synthesis problem. We show that priorities are expressive enough to represent restrictions induced by deadlock-free controllers preserving safety properties. We define a correspondence between such restrictions an...

  8. Imaging system

    International Nuclear Information System (INIS)

    Rushbrooke, J.G.; Ansorge, R.E.

    1987-01-01

    A moving object such as a container on a conveyor belt is imaged by an optical system onto a charge coupled device array in which the lines of the array are arranged perpendicular to the direction of motion of the object. The speed of movement of the object is sensed to generate electrical signals which are processed to provide shift signals enabling the shifting of data row to row in the array in synchronism with the movement of the container. The electrical charge associated with a given point on the array is transferred from one line to the other until it appears at the last line of the array, from which it is read out in known manner in conjunction with all other electrical charges associated with the row of charge coupled devices in the last line of the array. Due to the integrating effect achieved, the aperture of the imaging system can be much smaller than otherwise would be required, and/or the level of light illumination can be reduced. The imaging system can be applied to X-ray inspection devices, aerial surveillance or scanning of moving documents in copying processes. (author)

  9. Braking system

    Science.gov (United States)

    Norgren, D.U.

    1982-09-23

    A balanced braking system comprising a plurality of braking assemblies located about a member to be braked. Each of the braking assemblies consists of a spring biased piston of a first material fitted into a body of a different material which has a greater contraction upon cooling than the piston material. The piston is provided with a recessed head portion over which is positioned a diaphragm and forming a space therebetween to which is connected a pressurized fluid supply. The diaphragm is controlled by the fluid in the space to contact or withdraw from the member to be braked. A cooling means causes the body within which the piston is fitted to contract more than the piston, producing a tight shrink fit therebetween. The braking system is particularly applicable for selectively braking an arbor of an electron microscope which immobilizes, for example, a vertically adjustable low temperature specimen holder during observation. The system provides balanced braking forces which can be easily removed and re-established with minimal disturbance to arbor location.

  10. Protecting information in systems of systems

    NARCIS (Netherlands)

    Trivellato, D.

    2012-01-01

    Systems of systems are coalitions of autonomous and heterogeneous systems that collaborate to achieve a common goal. The component systems of a system of systems often belong to different security domains, which are governed by different authorities (hereafter called parties). Furthermore, systems

  11. Streamlining and automation of radioanalytical methods at a commercial laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Harvey, J.T.; Dillard, J.W. [IT Corp., Knoxville, TN (United States)

    1993-12-31

    Through the careful planning and design of laboratory facilities and incorporation of modern instrumentation and robotics systems, properly trained and competent laboratory associates can efficiently and safely handle radioactive and mixed waste samples. This paper addresses the potential improvements radiochemistry and mixed waste laboratories can achieve utilizing robotics for automated sample analysis. Several examples of automated systems for sample preparation and analysis will be discussed.

  12. Activation analysis course experiments with a 14-MeV neutron generator

    International Nuclear Information System (INIS)

    Miller, D.A.; Miller, G.E.

    1976-01-01

    The use of a 14 MeV neutron generator system in the radiochemistry teaching program of the Chemistry Department of the University of California at Irvine is described. Several different types of experiment are outlined to indicate the broad applicability of such a system to an instructional program in Chemistry. The program has encompassed instruction of undergraduates, graduate students and a Summer Institute Workshop for College Professors

  13. Streamlining and automation of radioanalytical methods at a commercial laboratory

    International Nuclear Information System (INIS)

    Harvey, J.T.; Dillard, J.W.

    1993-01-01

    Through the careful planning and design of laboratory facilities and incorporation of modern instrumentation and robotics systems, properly trained and competent laboratory associates can efficiently and safely handle radioactive and mixed waste samples. This paper addresses the potential improvements radiochemistry and mixed waste laboratories can achieve utilizing robotics for automated sample analysis. Several examples of automated systems for sample preparation and analysis will be discussed

  14. Dynamical systems

    CERN Document Server

    Birkhoff, George D

    1927-01-01

    His research in dynamics constitutes the middle period of Birkhoff's scientific career, that of maturity and greatest power. -Yearbook of the American Philosophical Society The author's great book€¦is well known to all, and the diverse active modern developments in mathematics which have been inspired by this volume bear the most eloquent testimony to its quality and influence. -Zentralblatt MATH In 1927, G. D. Birkhoff wrote a remarkable treatise on the theory of dynamical systems that would inspire many later mathematicians to do great work. To a large extent, Birkhoff was writing about his o

  15. Nuclear systems

    CERN Document Server

    Todreas, Neil E

    2011-01-01

    Principal Characteristics of Power ReactorsIntroductionPower CyclesPrimary Coolant SystemsReactor CoresFuel AssembliesAdvanced Water- and Gas-Cooled Reactors (Generation III And III+)Advanced Thermal and Fast Neutron Spectrum Reactors (Generation IV)ReferencesProblemsThermal Design Principles and ApplicationIntroductionOverall Plant Characteristics Influenced by Thermal Hydraulic ConsiderationsEnergy Production and Transfer ParametersThermal Design LimitsThermal Design MarginFigures of Merit for Core Thermal PerformanceThe Inverted Fuel ArrayThe Equivalent Annulus ApproximationReferencesProble

  16. Videobasierte Systeme

    Science.gov (United States)

    Knoll, Peter

    Videosensoren spielen für Fahrerassistenz systeme eine zentrale Rolle, da sie die Interpretation visueller Informationen (Objektklassifikation) gezielt unterstützen. Im Heckbereich kann die Video sensorik in der einfachsten Variante die ultraschallbasierte Einparkhilfe bei Einpark- und Rangiervorgängen unterstützen. Beim Nachtsichtsystem NightVision wird das mit Infrarotlicht angestrahlte Umfeld vor dem Fahrzeug mit einer Frontkamera aufgenommen und im Fahrzeugcockpit auf einem Display dem Fahrer angezeigt (s. Nachtsichtsysteme). Andere Fahrerassistenzsysteme verarbeiten die Videosignale und generieren daraus gezielt Informationen, die für eigenständige Funktionen (z. B. Spurverlassenswarner) oder aber als Zusatzinformation für andere Funktionen ausgewertet werden (Sensordatenfusion).

  17. Relaxation System

    Science.gov (United States)

    1987-01-01

    Environ Corporation's relaxation system is built around a body lounge, a kind of super easy chair that incorporates sensory devices. Computer controlled enclosure provides filtered ionized air to create a feeling of invigoration, enhanced by mood changing aromas. Occupant is also surrounded by multidimensional audio and the lighting is programmed to change colors, patterns, and intensity periodically. These and other sensory stimulators are designed to provide an environment in which the learning process is stimulated, because research has proven that while an individual is in a deep state of relaxation, the mind is more receptive to new information.

  18. Bearing system

    Science.gov (United States)

    Kapich, Davorin D.

    1987-01-01

    A bearing system includes backup bearings for supporting a rotating shaft upon failure of primary bearings. In the preferred embodiment, the backup bearings are rolling element bearings having their rolling elements disposed out of contact with their associated respective inner races during normal functioning of the primary bearings. Displacement detection sensors are provided for detecting displacement of the shaft upon failure of the primary bearings. Upon detection of the failure of the primary bearings, the rolling elements and inner races of the backup bearings are brought into mutual contact by axial displacement of the shaft.

  19. Propulsion Systems

    Science.gov (United States)

    2011-03-31

    stand.    CV CS x dAvvdVov dt d F   (18-1) Where  denotes density and vx is the velocity in the x-direction. The first term on the...by  but to avoid confusion with  from Eqs. 18-7 to 10, it is denoted k in this formula . Ru is the universal gas constant (8.314472 J/mol K), pe is...Russian Federation Used on Phobos spacecraft as main engines 74 1.03 NTO/ UDMH 13.73-19.61 316-325 Orbital Maneuvering System 1 Aerojet Shuttle

  20. Expert Systems: What Is an Expert System?

    Science.gov (United States)

    Duval, Beverly K.; Main, Linda

    1994-01-01

    Describes expert systems and discusses their use in libraries. Highlights include parts of an expert system; expert system shells; an example of how to build an expert system; a bibliography of 34 sources of information on expert systems in libraries; and a list of 10 expert system shells used in libraries. (Contains five references.) (LRW)

  1. System analysis and design

    International Nuclear Information System (INIS)

    Son, Seung Hui

    2004-02-01

    This book deals with information technology and business process, information system architecture, methods of system development, plan on system development like problem analysis and feasibility analysis, cases for system development, comprehension of analysis of users demands, analysis of users demands using traditional analysis, users demands analysis using integrated information system architecture, system design using integrated information system architecture, system implementation, and system maintenance.

  2. Posting system

    International Nuclear Information System (INIS)

    Hackney, S.

    1983-01-01

    A system for posting hazardous materials into and out of an enclosure, such as a glovebox, through a port in a wall of the enclosure. The port is normally closed by a door which cooperates with a removable end closure, on a container or the like when the latter is presented to and secured at the port. The container is secured in position at the port by means of a rotatable coupling ring. A single interlock ensures that the door cannot be opened in the absence of a container at the port and also that the container cannot be removed from the port when the door is open. In place of the container, a glove secured to a rigid sleeve may be used to enable the operator to perform a work function within the glovebox. (author)

  3. hydrothermal systems

    Directory of Open Access Journals (Sweden)

    L. Bayón

    2002-01-01

    Full Text Available In this paper, we revise the classical formulation of the problem depriving it of the concepts that are superfluous from the mathematical point of view. We observe that a number of power stations can be substituted by a single one that behaves equivalently to the entire set. Proceeding in this way, we obtain a variational formulation in its purest sense (without restrictions. This formulation allows us to employ the theory of calculus of variations to the highest degree. We then calculate the equivalent minimizer in the case where the cost functions are second-order polynomials. We prove that the equivalent minimizer is a second-order polynomial with piece-wise constant coefficients. Moreover, it belongs to the class C1. Finally, we present various examples prompted by real systems and perform the proposed algorithms using Mathematica.

  4. Nonlinear systems

    CERN Document Server

    Palmero, Faustino; Lemos, M; Sánchez-Rey, Bernardo; Casado-Pascual, Jesús

    2018-01-01

    This book presents an overview of the most recent advances in nonlinear science. It provides a unified view of nonlinear properties in many different systems and highlights many  new developments. While volume 1 concentrates on mathematical theory and computational techniques and challenges, which are essential for the study of nonlinear science, this second volume deals with nonlinear excitations in several fields. These excitations can be localized and transport energy and matter in the form of breathers, solitons, kinks or quodons with very different characteristics, which are discussed in the book. They can also transport electric charge, in which case they are known as polarobreathers or solectrons. Nonlinear excitations can influence function and structure in biology, as for example, protein folding. In crystals and other condensed matter, they can modify transport properties, reaction kinetics and interact with defects. There are also engineering applications in electric lattices, Josephson junction a...

  5. Posting system

    International Nuclear Information System (INIS)

    Jones, E.L.

    1983-01-01

    A posting system for the movement of equipment, such as a manipulator, into and out of an enclosure e.g. a cell or glovebox, for toxic or radioactive materials has the manipulator arranged within a collapsible bellows-like container with an end of the container cooperating with a port entry to the enclosure. The collapsible container isolates the manipulator from the environment outside the enclosure and allows the manipulator to enter and leave the contaminated enclosure without breach of the containment. A particular construction of cell for use with radioactive material is described, having a thick wall of shielding material such as concrete provided with a door normally closed by a Pb shutter and having a cylindrical gamma shield block located over the shutter on the exterior of the wall. (author)

  6. Systems engineering simplified

    CERN Document Server

    Cloutier, Robert; Bone, Mary Alice

    2015-01-01

    IntroductionOverviewDiscussion of Common TerminologyThe Case for Systems EngineeringA Brief History of Systems EngineeringSystem ExamplesSummaryThe System Life CycleManaging System Development-The Vee ModelSystem ProductionSystem Utilization and SupportSystem Retirement and DisposalOther Systems Engineering Development ModelsSpiral ModelAgile Model for Systems EngineeringSystem of InterestAbstraction and DecompositionIntegrationDeveloping and Managing RequirementsCyclone Requiremen

  7. NJOY system

    International Nuclear Information System (INIS)

    Gil, Choong Sup; Kim, Jung Do

    1998-01-01

    The NJOY Nuclear Data Processing System is used to convert evaluated nuclear data in ENDF format into forms useful for applications. The NJOY code is a modular computer code designed to read evaluated data in ENDF format, transform the data in various ways, and output the results as libraries designed to be used in various applications. The modules are essentially independent programs, and they communicate with each other using input and output files, plus a very few common variables. The NJOY code can work with neutrons, photons, and charged particles. The evaluated nuclear data are reconstructed to pointwise cross sections from ENDF resonance parameters and interpolation schemes. The pointwise data can be Doppler broadened to the temperatures requested by users. The data in unresolved energy range can be computed to effective self-shielded pointwise cross sections. The cross sections and scattering matrices for free or bound scatterers in the thermal energy range are able to be produced. The self-shielded multigroup cross sections, group-to-group scattering matrices, photon-production matrices, and charged-particle cross sections from pointwise data can be generated for various application codes

  8. Chem systems

    International Nuclear Information System (INIS)

    Anon.

    1992-01-01

    This paper reports that world styrene demand, paced by a near doubling of combined requirements in East Asia and Oceania, could reach 19.3 million metric tons by 2000, an average growth rate of 3.7%/year. So concludes Chem Systems Inc., Tarrytown, N.Y., in a study of world styrene markets through the end of the century. Pacific Rim styrene production and consumption throughout the 1990s are predicted to make up increasingly larger shares of world markets, while demand and production lag in the U.S. and western Europe. Demand and capacity in other parts of the world will grow in real terms, increasing combined market shares only slightly. Most of the increase will be driven by demand in East Asia and Oceania, where consumption by century's end is expected to increase 4.48 million metric tons from 2.25 million tons in 1991. Meantime, Japan's styrene demand in 2000 is projected at 2.64 million tons, a 500,000 ton increase from 1991 demand but a net market loss of 1.9%

  9. 10. European TRIGA users conference. Papers and abstracts

    International Nuclear Information System (INIS)

    1988-01-01

    The Tenth European TRIGA Users Conference was held in Vienna, September 14-16, 1988 under the sponsorship of the Atominstitut. The main areas of discussions were: Reactor operation and maintenance experiences; New developments and improvements of TRIGA components and systems, including instrumentation; Fuel and fuel management; Safety aspects, licensing and radiation protection; Experiments with TRIGA reactors; Radiochemistry, radioisotope production and NAA; and Reactor physics

  10. A Simple Apparatus for Fast Ion Exchange Separations

    International Nuclear Information System (INIS)

    Samsahl, K.

    1964-09-01

    An apparatus suitable for very fast ion exchange group separations in radiochemistry has been elaborated. The apparatus which consists of a system of glass tubes with pistons driven by the same force, allows the exact adjustment of influent solutions to a long series of ion-exchange columns. The practical application of the apparatus to the simultaneous separation of six groups of trace elements in the neutron activation analysis of biological material is described

  11. Research programs carried out at the TRIGA Mark II reactor Vienna

    International Nuclear Information System (INIS)

    Bock, H.

    1978-01-01

    During the period July 1976 to July 1978 approximately 170 papers have been published by staff members of the Atominstitute in scientific journals covering the main research fields which are: radiation physics; nuclear physics; reactor technology; neutron solid state physics; radiochemistry; health physics. In the department of reactor technology research work was is done on in-core instrumentation, failed fuel element detection systems and neutron radiography

  12. 10. European TRIGA users conference. Papers and abstracts

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1988-07-01

    The Tenth European TRIGA Users Conference was held in Vienna, September 14-16, 1988 under the sponsorship of the Atominstitut. The main areas of discussions were: Reactor operation and maintenance experiences; New developments and improvements of TRIGA components and systems, including instrumentation; Fuel and fuel management; Safety aspects, licensing and radiation protection; Experiments with TRIGA reactors; Radiochemistry, radioisotope production and NAA; and Reactor physics.

  13. Annual Report of Institute of Nuclear Chemistry and Technology 2001

    International Nuclear Information System (INIS)

    2002-06-01

    The INCT 2001 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology in Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics, nucleonic control systems and accelerators and nuclear analytical methods

  14. Annual Report of the Institute of Nuclear Chemistry and Technology 2000

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2001-06-01

    The INCT 2000 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics and nucleonic control systems and accelerators.

  15. Annual Report of the Institute of Nuclear Chemistry and Technology 2000

    International Nuclear Information System (INIS)

    2001-06-01

    The INCT 2000 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics and nucleonic control systems and accelerators

  16. A Simple Apparatus for Fast Ion Exchange Separations

    Energy Technology Data Exchange (ETDEWEB)

    Samsahl, K

    1964-09-15

    An apparatus suitable for very fast ion exchange group separations in radiochemistry has been elaborated. The apparatus which consists of a system of glass tubes with pistons driven by the same force, allows the exact adjustment of influent solutions to a long series of ion-exchange columns. The practical application of the apparatus to the simultaneous separation of six groups of trace elements in the neutron activation analysis of biological material is described.

  17. Quantitative studies in radiopharmaceutical science. Progress report, April 1-August 31, 1986

    International Nuclear Information System (INIS)

    Cooper, M.

    1986-09-01

    This report covers progress made during the first reporting period since the redirection of the project. In radiochemistry, achievements in fluorine-18 tracer studies including purification and reaction kinetics of 2-fluorodeoxyglucose and production of 6-fluoroDOPA. Radiopharmaceuticals have been prepared and tested for studies on CNS dopaminergic systems. By use of dynamic positron emission tomography the cerebral transport and metabolism of glucose continues to be studied. 6 figs

  18. Automation of (64)Cu production at Turku PET Centre.

    Science.gov (United States)

    Elomaa, Viki-Veikko; Jurttila, Jori; Rajander, Johan; Solin, Olof

    2014-07-01

    At Turku PET Centre automation for handling solid targets for the production of (64)Cu has been built. The system consists of a module for moving the target from the irradiation position into a lead transport shield and a robotic-arm assisted setup for moving the target within radiochemistry laboratory. The main motivation for designing automation arises from radiation hygiene. Copyright © 2014 Elsevier Ltd. All rights reserved.

  19. Work on the hot atom chemistry at the Institute of Nuclear Sciences Boris Kidric, Vinca, Yugoslavia

    International Nuclear Information System (INIS)

    Veljkovic, S.

    1969-01-01

    A survey of work on hot atom chemistry from the establishment of the Institute up to now, where the role of Prof. P. Savic, should be specially emphasized, is given. The investigations in this domain during the first period, were directed to solve various problems in production of radioactive isotopes. Today these investigations are closely associated with the work in radiochemistry, physical chemistry of liquid and solid systems and fast reaction kinetics improving the development of these branches (author) [sr

  20. Annual Report 2004 of Institute of Nuclear Chemistry and Technology

    Energy Technology Data Exchange (ETDEWEB)

    Michalik, J; Smulek, W; Godlewska-Para, E [eds.

    2005-06-01

    The INCT 2004 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics, nucleonic control systems and accelerators, radiobiology and nuclear analytical methods.

  1. Annual Report of Institute of Nuclear Chemistry and Technology 2001

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2002-06-01

    The INCT 2001 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology in Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics, nucleonic control systems and accelerators and nuclear analytical methods.

  2. Annual Report of Institute of Nuclear Chemistry and Technology 1999

    International Nuclear Information System (INIS)

    2000-06-01

    The INCT 1999 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology, Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics and nucleonic control systems and accelerators

  3. Annual Report 2004 of Institute of Nuclear Chemistry and Technology

    International Nuclear Information System (INIS)

    Michalik, J.; Smulek, W.; Godlewska-Para, E.

    2005-06-01

    The INCT 2004 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics, nucleonic control systems and accelerators, radiobiology and nuclear analytical methods

  4. Annual Report of Institute of Nuclear Chemistry and Technology 1999

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2000-06-01

    The INCT 1999 Annual Report is the review of scientific activities in all branches being developed in the Institute of Nuclear Chemistry and Technology, Warsaw. The studies are connected in general with the following fields: radiation chemistry and physics, radiation technologies, radiochemistry, stable isotopes, nuclear analytical methods, chemistry in general, radiobiology, process engineering, material engineering, structural studies and diagnostics and nucleonic control systems and accelerators.

  5. System safety education focused on system management

    Science.gov (United States)

    Grose, V. L.

    1971-01-01

    System safety is defined and characteristics of the system are outlined. Some of the principle characteristics include role of humans in hazard analysis, clear language for input and output, system interdependence, self containment, and parallel analysis of elements.

  6. Systems Biology and Health Systems Complexity in;

    NARCIS (Netherlands)

    Donald Combs, C.; Barham, S.R.; Sloot, P.M.A.

    2016-01-01

    Systems biology addresses interactions in biological systems at different scales of biological organization, from the molecular to the cellular, organ, organism, societal, and ecosystem levels. This chapter expands on the concept of systems biology, explores its implications for individual patients

  7. Airport Information Retrieval System (AIRS) System Design

    Science.gov (United States)

    1974-07-01

    This report presents the system design for a prototype air traffic flow control automation system developed for the FAA's Systems Command Center. The design was directed toward the immediate automation of airport data for use in traffic load predicti...

  8. Organic chemistry and radiochemistry: study of chemical interactions between iodine and paint of French nuclear reactor in a severe accident situation

    International Nuclear Information System (INIS)

    Aujollet, Y.

    2005-01-01

    In Phebus (French in pile facility; PWR scale 1/5000) experiments, performed by the Institut de Radioprotection et de Surete Nucleaire, few quantities of organic iodides were registered after interaction between iodine and reactor containment paint. This study concerns all mechanisms of chemical reactions between iodine and the polymer of the paint in order to estimate the organic iodides released from the paint. At first, all the paint components had been identified. Several models of chemical sites of the polymer were synthesized and tested with iodine in different conditions of temperature and radiation. These experiments showed interactions between iodine and secondary or tertiary amines by charge transfer. In few cases, the complex of tertiary amines creates oxidation reactions. (author)

  9. The radiochemistry of [{sup 18} F]-FDG: the first experience in Mexico; La radioquimica del [{sup 18} F]-FDG: la primera experiencia en Mexico

    Energy Technology Data Exchange (ETDEWEB)

    Lopez D, F A [Unidad PET-Ciclotron, Facultad de Medicina, UNAM, Av. Universidad 3000, Ciudad Universitaria, Coyoacan, 04500 Mexico, D. F. (Mexico)

    2004-07-01

    The present work describes the more used method for the synthesis of 2 - [{sup 18} F] - fluorine-2-deoxy-D-glucose that is the more used radiopharmaceutical in the nuclear medicine in the cancer diagnostic. The process consists on two chemical reactions: i) [{sup 18} F{sup -}] - nucleophilic radio fluorination and i i) a hydrolysis catalyzed by acid. The first reaction incorporates to the [{sup 18} F]- fluorine labelled inside the organic precursor 1,3,4,6-tetra- O -acetil-2- O-trifluoromethanesulfonyl- {beta}-D-mannopyranose (triflate of mannose). The mechanism of this reaction is a bimolecular nucleophilic substitution (SN{sub 2}) with the ion [{sup 18} F{sup -}] - fluoride; in the second reaction, the hydrolysis of those protective acetyl groups generate the hydroxyl groups free of the [{sup 18} F]-FDG. The process includes an azeotropic distillation and several purification steps. (Author)

  10. Evaluation of the production capabilities of 18F, 11C, 13N and 15O PET isotopes at the PET-cyclotron-radiochemistry site of Messina University

    OpenAIRE

    Auditore, Lucrezia; Amato, Ernesto; Italiano, Antonio; Pagano, Benedetta; Baldari, Sergio

    2017-01-01

    The production of 18F, 11C, 13N, and 15O positron emitting radionuclides for PET imaging is usually accomplished in Nuclear Medicine Departments through direct nuclear reactions induced by protons accelerated by compact medical cyclotrons on liquid or gaseous targets. Messina University has funded the construction of a PET-cyclotron-radio-chemistry plant at the Messina University Hospital, equipped with a 11 MeV self-shielded cyclotron. We estimated the expected production yields of these nuc...

  11. Evaluation of the production capabilities of 18F, 11C, 13N and 15O PET isotopes at the PET-cyclotron-radiochemistry site of Messina University

    Directory of Open Access Journals (Sweden)

    Lucrezia Auditore

    2017-02-01

    Full Text Available The production of 18F, 11C, 13N, and 15O positron emitting radionuclides for PET imaging is usually accomplished in Nuclear Medicine Departments through direct nuclear reactions induced by protons accelerated by compact medical cyclotrons on liquid or gaseous targets. Messina University has funded the construction of a PET-cyclotron-radio-chemistry plant at the Messina University Hospital, equipped with a 11 MeV self-shielded cyclotron. We estimated the expected production yields of these nuclides, accounting for target thickness, production of other radioactive nuclides, and time effects on the irradiated target purity. To this aim, both TALYS code (v. 1.8 and an analytical approach based on EXFOR experimental data were used. The general agreement between the two approaches, and with the available literature data, allows to assess the expected yields at the End of Bombardment, and relative target purities, to be used for further radiopharmaceutical preparation steps.

  12. Establishment of an Undergraduate Research and Training Program in Radiochemistry at Florida Memorial University, a Historically Black College or University (HBCU)

    International Nuclear Information System (INIS)

    Tamalis, Dimitri; Stiffin, Rose; Elliott, Michael; Huisso, Ayivi; Biegalski, Steven; Landsberger, Sheldon

    2009-01-01

    With the passing of the Energy Policy Act of 2005, the United States is experiencing for the first time in over two decades, what some refer to as the ''Nuclear Renaissance''. The US Nuclear Regulatory Commission (NRC) recognizes this surge in application submissions and is committed to reviewing these applications in a timely manner to support the country's growing energy demands. Notwithstanding these facts, it is understood that the nuclear industry requires appropriately trained and educated personnel to support the growing needs of the nuclear industry and the US NRC. Equally important is the need to educate the next generation of students in nuclear non-proliferation, nuclear forensics and various aspects of homeland security for the national laboratories and the Department of Defense. From mechanical engineers educated and experienced in materials, thermal/fluid dynamics, and component failure analysis, to physicists using advanced computing techniques to design the next generation of nuclear reactor fuel elements, the need for new engineers, scientists, and health physicist has never been greater.

  13. Radiochemistry, pre-clinical studies and first clinical investigation of 90Y-labeled hydroxyapatite (HA) particles prepared utilizing 90Y produced by (n,γ) route

    International Nuclear Information System (INIS)

    Vimalnath, K.V.; Chakraborty, Sudipta; Rajeswari, A.; Sarma, H.D.; Nuwad, Jitendra; Pandey, Usha; Kamaleshwaran, K.; Shinto, Ajit; Dash, Ashutosh

    2015-01-01

    Introduction: The scope of using no carrier added (NCA) 90 Y [T 1/2 = 64.1 h, E β(max) = 2.28 MeV] obtained from 90 Sr/ 90 Y generator in radiation synovectomy (RSV) is widely accepted. In the present study, the prospect of using 90 Y produced by (n,γ) route in a medium flux research reactor for use in RSV was explored. Methods: Yttrium-90 was produced by thermal neutron irradiation of Y 2 O 3 target at a neutron flux of ~ 1 × 10 14 n/cm 2 .s for 14 d. The influence of various experimental parameters were systematically investigated and optimized to arrive at the most favorable conditions for the formulation of 90 Y labeled hydroxyapatite (HA) using HA particles of 1–10 μm size range. An optimized kit formulation strategy was developed for convenient one-step compounding of 90 Y-HA, which is easily adaptable at hospital radiopharmacy. The pre-clinical biological evaluation of 90 Y-HA particles was studied by carrying out biodistribution and bioluminiscence imaging studies in Wistar rats. The first clinical investigation using the radiolabeled preparation was performed on a patient suffering from chronic arthritis in knee joint by administering 185 MBq 90 Y-HA formulated at the hospital radiopharmacy deploying the proposed strategy. Results: Yttrium-90 was produced with a specific activity of 851 ± 111 MBq/mg and radionuclidic purity of 99.95 ± 0.02%. 90 Y-labeled HA particles (185 ± 10 MBq doses) were formulated in high radiochemical purity (> 99%) and excellent in vitro stability. The preparation showed promising results in pre-clinical studies carried out in Wistar rats. The preliminary results of the first clinical investigation of 90 Y-HA preparation in a patient with rheumatoid arthritis in knee joints demonstrated the effectiveness of the formulation prepared using 90 Y produced via (n,γ) route in the management of the disease. Conclusion: The studies revealed that effective utilization of 90 Y produced via (n,γ) route in a medium flux research reactor coupled with the developed strategy of using HA kits for convenient formulation of 90 Y-HA at the hospital radiopharmacy can contribute to sustainable growth in the clinical utilization of 90 Y in RSV in the foreseeable future

  14. Evaluation of the Radiochemistry of Near-Field Water Samples at the Nevada Test Site Applied to the Definition of a Hydrologic Source Term

    International Nuclear Information System (INIS)

    Smith, D K

    2002-01-01

    Effective management of available groundwater resources and strategies for remediation of water impacted by past nuclear testing practices depend on knowledge about the migration of radionuclides in groundwater away from the sites of the explosions. A primary concern is to assess the relative mobilities of the different radionuclide species found near sites of underground nuclear tests and to determine the concentration, extent, and speed of this movement. Ultimately the long term transport behavior of radionuclides with half-lives long enough that they will persist for decades, their interaction with groundwater, and the resulting flux of these contaminants is of paramount importance. As part of a comprehensive approach to these assessments, more than three decades of site-specific sites studies have been undertaken at the Nevada Test Site (NTS) which have focused on the means responsible for the observed or suspected movement of radionuclides away from underground nuclear tests (RNM, 1983). More recently regional and local models of groundwater flow and radionuclide transport have been developed as part of a federal and state of Nevada program to assess the long-term effects of underground nuclear testing on human health and environment (e.g., U.S. DOE/NV, 1997a; Tompson et al., 1999; Pawloski et al., 2001). Necessary to these efforts is a reliable measure of the hydrologic source term which is defined as those radionuclides dissolved in or otherwise transported by groundwater (Smith et al., 1995). Measurement of radionuclides in waters sampled near the sites of underground nuclear test provides arguably the best opportunity to bound the hydrologic source term. This empirical approach was recognized early and concentration data has been collected annually since mid-1970's. Initially three sites were studied at the NTS; over the years the program has been expanded to include more than fifteen study locations. As part of various field programs, Lawrence Livermore National Laboratory and Los Alamos National Laboratory have annually returned water samples from wells in near-field locations at the NTS for radiochemical analyses. This report makes the distinction between samples taken in the near-field and the far field. The near-field includes the area extending radially ∼300 meters from surface ground zero (the firing point of an underground nuclear test projected upwards on ground surface). Over the years this sampling program has also been refereed to as the ''hot-well monitoring program'' because these water samples contained concentrations of tritium above natural background (tritium concentrations in southern Nevada precipitation are 0.5 to 2.0 Bq/L, Farmer et al., 1998). A majority of the hot wells contain tritium in excess of the 741 Bq/L (20,000 pCi/L) drinking water standard (Smith et al., 1996a; Smith et al., 1997). The sites which comprise our current hot well sampling network are plotted on a map of the NTS in Figure 1

  15. Optimization of a radiochemistry method for plutonium determination in biological samples; Optimizacion del metodo radioquimico para determinar plutonio en muestras biologicas

    Energy Technology Data Exchange (ETDEWEB)

    Cerchetti, Maria L; Arguelles, Maria G [Comision Nacional de Energia Atomica, Ezeiza (Argentina). Laboratorio de Dosimetria Personal y de Area

    2005-07-01

    Plutonium has been widely used for civilian an military activities. Nevertheless, the methods to control work exposition have not evolved in the same way, remaining as one of the major challengers for the radiological protection practice. Due to the low acceptable incorporation limit, the usual determination is based on indirect methods in urine samples. Our main objective was to optimize a technique used to monitor internal contamination of workers exposed to Plutonium isotopes. Different parameters were modified and their influence on the three steps of the method was evaluated. Those which gave the highest yield and feasibility were selected. The method involves: 1-) Sample concentration (coprecipitation); 2-) Plutonium purification; and 3-) Source preparation by electrodeposition. On the coprecipitation phase, changes on temperature and concentration of the carrier were evaluated. On the ion-exchange separation, changes on the type of the resin, elution solution for hydroxylamine (concentration and volume), length and column recycle were evaluated. Finally, on the electrodeposition phase, we modified the following: electrolytic solution, pH and time. Measures were made by liquid scintillation counting and alpha spectrometry (PIPS). We obtained the following yields: 88% for coprecipitation (at 60 C degree with 2 ml of CaHPO{sub 4}), 71% for ion-exchange (resins AG 1x8 Cl{sup -} 100-200 mesh, hydroxylamine 0.1N in HCl 0.2N as eluent, column between 4.5 and 8 cm), and 93% for electrodeposition (H{sub 2}SO{sub 4}-NH{sub 4}OH, 100 minutes and pH from 2 to 2.8). The expand uncertainty was 30% (NC 95%), the decision threshold (Lc) was 0.102 Bq/L and the minimum detectable activity was 0.218 Bq/L of urine. We obtained an optimized method to screen workers exposed to Plutonium. (author)

  16. On different experimental behaviour of fast secondary particles produced in 12C interactions at relativistic energies as studied with radiochemistry and in a propane chamber

    International Nuclear Information System (INIS)

    Kulakov, B.A.; Karachuk, J.; Gelovani, L.K.; Gridnev, T.G.; Sosnin, A.N.; Brandt, R.

    1998-01-01

    Energetic secondary fragments produced in the interaction of (41-44) GeV 12 C ions with copper exhibit experimentally a broader angular distribution as compared to energetic secondary fragments produced in the interactions at a lower 12 C-energy (15-25) GeV when studied with radiochemical techniques. Such a different experimental behaviour of secondary fragments produced by 12 C ions of the same two energy groups is not observed, when these secondary fragments are investigated with a propane bubble chamber. Separation of secondary particles is described

  17. Study by X-ray photoelectron spectroscopy (XPS) and radiochemistry (Cl36) of the interaction of chloride ions with a passive film formed on nickel

    International Nuclear Information System (INIS)

    Herbelin, Jean-Marc

    1990-01-01

    This research thesis reports the study of the influence of chlorides on nickel passivation by using a radiochemical method based on the use of the Cl 36 isotope and the X-ray photoelectron spectroscopy (XPS). The first one allows the in-situ determination of the adsorption of chlorides on the surface, or their inclusion in surface films during the electrochemical treatment. The XPS analysis allows the characterization of modifications induced by chlorides in passive films. The obtained results allow a better understanding in the interpretation of the mechanisms of corrosion induced by chloride ions [fr

  18. Bulk Scale Formulation of Therapeutic Doses of Clinical Grade Ready-to-Use 177Lu-DOTA-TATE: The Intricate Radiochemistry Aspects.

    Science.gov (United States)

    Mathur, Anupam; Prashant, Vrinda; Sakhare, Navin; Chakraborty, Sudipta; Vimalnath, K V; Mohan, Repaka Krishna; Arjun, Chanda; Karkhanis, Barkha; Seshan, Ravi; Basu, Sandip; Korde, Aruna; Banerjee, Sharmila; Dash, Ashutosh; Sachdev, Satbir Singh

    2017-09-01

    177 Lu-DOTA-TATE is a clinically useful and promising therapeutic radiopharmaceutical for peptide receptor radionuclide therapy of neuroendocrine tumors (NETs) overexpressing somatostatin receptors. Currently, the radiopharmaceutical is prepared in-house at nuclear medicine centers, thereby restricting its use to limited centers only. In this article, the authors describe systematic studies toward bulk scale formulation of "ready-to-use" 177 Lu-DOTA-TATE using medium specific activity 177 Lu (740-1110 GBq/mg) at a centralized radiopharmacy facility. In an optimized protocol, 177 Lu-DOTA-TATE synthesis was carried out by direct heating of 177 LuCl 3 (Sp. act. 740-1110 GBq/mg) with DOTA-TATE peptide (1.5-3.0 equivalents) in ammonium acetate buffer (0.2 M) containing 2,5-dihydroxy benzoic acid (gentisic acid). Thereafter, the crude labeled product was purified using a Sep-Pak ® C18 column and diluted with acetate buffer-gentisic acid (1.5% w/v) solution to final radioactive concentration of 740 MBq/mL. This was further sterilized and dispensed as 7.4 GBq patient dose/vial with 2 days postformulation calibration. A peptide/metal ratio of 1.5-3.0 is essential for complexation wherein radiolabeling yields >90% are obtained minimizing free 177 Lu waste. For formulation of 7.4 GBq patient dose (2 days postproduction), even specific activity of about 555 GBq/mg was found to be adequate for the radiometal. The ready-to-use 740 MBq/mL 177 Lu-DOTA-TATE formulation with gentisic acid (1.5% w/v) is observed to be safe for human use for more than 1 week (radiochemical purity >98%) from the day of production when stored at -70°C. However, the target specificity may get affected beyond 2 days as the total peptide content for 7.4 GBq dose may exceed the critical peptide limit of 300 μg. Patient treatment carried with several batches of present formulation in diseased NET patients exhibited desired distribution at the tumor and its metastatic site. A ready-to-use formulation of 177 Lu-DOTA-TATE was successfully prepared and optimized for regular bulk scale production and supply to distant nuclear medicine centers.

  19. System specifications for the NDS Dictionary System

    International Nuclear Information System (INIS)

    Attree, P.M.; Smith, P.M.

    1979-09-01

    The NDS Dictionary System is a computerized system for maintaining and distributing the EXFOR dictionaries and for preparing internal versions of these dictionaries for use in the NDS EXFOR System and other NDS systems. This document is an internal manual for the system specifications of the NDS Dictionary System. It includes flow charts, system and program summaries, input and output specifications and file and record descriptions. This manual is updated from time to time when system modifications are made; this is the version of January 1979

  20. Quality management system

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Mu Sung

    2009-08-15

    This book deals with ISO9001 quality management system which includes summary of this system such as classification of quality, principle of quality management, and definition, requirement and procedure of quality management system, introduction of ISO9001 system like model of ISO9001 quality management system, ISO certificate system, structure of ISO9001 standard, requirement of ISO9001 quality management system, process approach and documentation of system, propel cases of ISO9001 quality management system.

  1. Quality management system

    International Nuclear Information System (INIS)

    Lee, Mu Sung

    2009-08-01

    This book deals with ISO9001 quality management system which includes summary of this system such as classification of quality, principle of quality management, and definition, requirement and procedure of quality management system, introduction of ISO9001 system like model of ISO9001 quality management system, ISO certificate system, structure of ISO9001 standard, requirement of ISO9001 quality management system, process approach and documentation of system, propel cases of ISO9001 quality management system.

  2. Protecting Information in Systems of Systems

    NARCIS (Netherlands)

    Trivellato, Daniel; Zannone, Nicola; Etalle, Sandro

    2011-01-01

    Systems of Systems (SoS) are dynamic, distributed coalitions of autonomous and heterogeneous systems that collaborate to achieve a common goal. While offering several advantages in terms of scalability and flexibility, the SoS paradigm has a strong impact on system interoperability and on the

  3. A security framework for systems of systems

    NARCIS (Netherlands)

    Trivellato, D.; Zannone, N.; Etalle, S.

    2011-01-01

    Systems of systems consist of a wide variety of dynamic, distributed coalitions of autonomous and heterogeneous systems that collaborate to achieve a common goal. While offering several advantages in terms of scalability and flexibility, this new paradigm has a strong impact on system

  4. A Security Framework for Systems of Systems

    NARCIS (Netherlands)

    Trivellato, Daniel; Zannone, Nicola; Etalle, Sandro

    2011-01-01

    Systems of systems consist of a wide variety of dynamic, distributed coalitions of autonomous and heterogeneous systems that collaborate to achieve a common goal. While offering several advantages in terms of scalability and flexibility, this new paradigm has a strong impact on system

  5. Systems theory of interconnected port contact systems

    NARCIS (Netherlands)

    Eberard, D.; Maschke, B.M.; Schaft, A.J. van der

    2005-01-01

    Port-based network modeling of a large class of complex physical systems leads to dynamical systems known as port-Hamiltonian systems. The key ingredient of any port-Hamiltonian system is a power-conserving interconnection structure (mathematically formalized by the geometric notion of a Dirac

  6. Digital processing data communication systems (bus systems)

    International Nuclear Information System (INIS)

    Fleck, K.

    1980-01-01

    After an introduction to the technology of digital processing data communication systems there are the following chapters: digital communication of processing data in automation technology, the technology of biserial communication, the implementaiton of a bus system, the data transmission of the TDC-2000 system of Honeywell's and the process bus CS 275 in the automation system TELEPERM M of Siemens AG. (WB) [de

  7. Networked control of microgrid system of systems

    Science.gov (United States)

    Mahmoud, Magdi S.; Rahman, Mohamed Saif Ur; AL-Sunni, Fouad M.

    2016-08-01

    The microgrid has made its mark in distributed generation and has attracted widespread research. However, microgrid is a complex system which needs to be viewed from an intelligent system of systems perspective. In this paper, a network control system of systems is designed for the islanded microgrid system consisting of three distributed generation units as three subsystems supplying a load. The controller stabilises the microgrid system in the presence of communication infractions such as packet dropouts and delays. Simulation results are included to elucidate the effectiveness of the proposed control strategy.

  8. D0 Cryo System Control System Autodialer

    Energy Technology Data Exchange (ETDEWEB)

    Urbin, J.; /Fermilab

    1990-04-17

    The DO cryogenic system is controlled by a TI565-PLC based control system. This allows the system to be unmanned when in steady state operation. System experts will need to be contacted when system parameters exceed normal operating points and reach alarm setpoints. The labwide FIRUS system provides one alarm monitor and communication link. An autodialer provides a second and more flexible alarm monitor and communication link. The autodialer monitors contact points in the control system and after receiving indication of an alarm accesses a list of experts which it calls until it receives an acknowledgement. There are several manufacturers and distributors of autodialer systems. This EN explains the search process the DO cryo group used to fmd an autodialer system that fit the cryo system's needs and includes information and specs for the unit we chose.

  9. Superspeed Maglev system Transrapid. System decription

    Energy Technology Data Exchange (ETDEWEB)

    Miller, L [Thyssen Henschel AG,, Maglev Transportation Technology, Muenchen (Germany)

    1996-12-31

    The superspeed maglev system Transrapid is a track-bound transportation system for passengern and priority freight transport. The transrapid trainsets are composed of self-sufficient vehicle section coupled together. The superspeed maglev system Transrapid is capable of revenue operation at speeds of 100 to 500 km/h. Besides the description of the system concept and system characteristics safety and availability are discussed. (HW)

  10. System design specification Brayton Isotope Power System (BIPS) Flight System (FS), and Ground Demonstration System (GDS)

    International Nuclear Information System (INIS)

    1976-01-01

    The system design specification for ground demonstration, development, and flight qualification of a Brayton Isotope Power System (BIPS) is presented. The requirements for both a BIPS conceptual Flight System (FS) and a Ground Demonstration System (GDS) are defined

  11. Situation awareness with systems of systems

    CERN Document Server

    Tretmans, Jan; Borth, Michael

    2013-01-01

    This book discusses various aspects, challenges, and solutions for developing systems-of-systems for situation awareness, using applications in the domain of maritime safety and security.  Topics include advanced, multi-objective visualization methods for situation awareness, stochastic outlier selection, rule-based anomaly detection, an ontology-based event model for semantic reasoning, new methods for semi-automatic generation of adapters bridging communication gaps, security policies for systems-of-systems, trust assessment, and methods to deal with the dynamics of systems-of-systems in run-time monitoring, testing, and diagnosis. Architectural considerations for designing information-centric systems-of-systems such as situation awareness systems, and an integrated demonstrator implementing many of the investigated aspects, complete the book.

  12. System specifications for the NDS EXFOR System

    International Nuclear Information System (INIS)

    Attree, P.M.; Smith, P.M.

    1979-07-01

    EXFOR is the agreed exchange format for the magnetic-tape exchange of nuclear reaction data between national and international nuclear data centres for the benefit of nuclear data users in all countries. The NDS EXFOR System is a computerized system for the storage and retrieval of EXFOR information compiled or received by the IAEA. This document is an internal manual for the system specifications of the NDS EXFOR System. It includes flow charts, system and program summaries, input and output specifications and file and record descriptions. The manual is updated from time to time when system modifications are made

  13. System specifications for the NDS EXFOR System

    Energy Technology Data Exchange (ETDEWEB)

    Attree, P M; Smith, P M

    1982-06-01

    EXFOR is the agreed exchange format for the magnetic-tape exchange of nuclear reaction data between national and international nuclear data centers for the benefit of nuclear data users in all countries. The NDS EXFOR System is a computerized system for the storage and retrieval of EXFOR information compiled or received of the IAEA. This document is an internal manual for the system specifications of the NDS EXFOR System. It includes flow charts, system and program summaries, input and output specifications and file and record descriptions. The manual is updated from time to time when system modifications are made; the first version was issued in July 1979. (author)

  14. Computer System Design System-on-Chip

    CERN Document Server

    Flynn, Michael J

    2011-01-01

    The next generation of computer system designers will be less concerned about details of processors and memories, and more concerned about the elements of a system tailored to particular applications. These designers will have a fundamental knowledge of processors and other elements in the system, but the success of their design will depend on the skills in making system-level tradeoffs that optimize the cost, performance and other attributes to meet application requirements. This book provides a new treatment of computer system design, particularly for System-on-Chip (SOC), which addresses th

  15. Smart electromechanical systems the central nervous system

    CERN Document Server

    Kurbanov, Vugar

    2017-01-01

    This book describes approaches to solving the problems of developing the central nervous system of robots (CNSR) based on smart electromechanical systems (SEMS) modules, principles of construction of the various modules of the central nervous system and variants of mathematical software CNSR in control systems for intelligent robots. It presents the latest advances in theory and practice at the Russian Academy of Sciences. Developers of intelligent robots to solve modern problems in robotics are increasingly addressing the use of the bionic approach to create robots that mimic the complexity and adaptability of biological systems. These have smart electromechanical system (SEMS), which are used in various cyber-physical systems (CPhS), and allow the functions of calculation, control, communications, information storage, monitoring, measurement and control of parameters and environmental parameters to be integrated. The behavior of such systems is based on the information received from the central nervous syst...

  16. Multiobjective Collaborative Optimization of Systems of Systems

    National Research Council Canada - National Science Library

    Wolf, Robert A

    2005-01-01

    ...; in other words an inefficient design of the system of systems. This thesis examines the simultaneous design of several ships using the sea base concept as an example application of a network of ships working together...

  17. Situation Awareness with Systems of Systems

    NARCIS (Netherlands)

    Laar, P. van de; Tretmans, J.; Borth, M.

    2013-01-01

    This book discusses various aspects, challenges, and solutions for developing systems-of-systems for situation awareness, using applications in the domain of maritime safety and security. Topics include advanced, multi-objective visualization methods for situation awareness, stochastic outlier

  18. Linking Political Systems and War Systems

    DEFF Research Database (Denmark)

    Harste, Gorm

    2009-01-01

    Decisive parts of the Western political system have demonstrated a seemingly surprising misinterpretation of military might. As Madelaine Albright has suggested, the mighty perceived themselves as "almighty". Political power seems to have invested in instrumental coercive power relations and found...... military coercion to be the appropriate mean. Using the system theory and the theory of systemic risks displayed by the German sociologist Niklas Luhmann the article demonstrates how military systems due to their own autonomy and autopoiesis do not fit into the idea of political government....... The Clausewitzian ideal of a political system that could continue its power games by means of war was moderated by Clausewitz' own analysis of "friction". How can a political system be so blind towards the possibilities of another system? What are the risks of systemic blind spots? The argument of the paper...

  19. Designing information systems

    CERN Document Server

    Blethyn, Stanley G

    2014-01-01

    Designing Information Systems focuses on the processes, methodologies, and approaches involved in designing information systems. The book first describes systems, management and control, and how to design information systems. Discussions focus on documents produced from the functional construction function, users, operators, analysts, programmers and others, process management and control, levels of management, open systems, design of management information systems, and business system description, partitioning, and leveling. The text then takes a look at functional specification and functiona

  20. Cognitive Medical Multiagent Systems

    OpenAIRE

    Barna Iantovics

    2010-01-01

    The development of efficient and flexible agent-based medical diagnosis systems represents a recent research direction. Medical multiagent systems may improve the efficiency of traditionally developed medical computational systems, like the medical expert systems. In our previous researches, a novel cooperative medical diagnosis multiagent system called CMDS (Contract Net Based Medical Diagnosis System) was proposed. CMDS system can solve flexibly a large variety of medical diagnosis problems...