WorldWideScience

Sample records for neutron scattering observation

  1. Collective Excitations in Liquid Hydrogen Observed by Coherent Neutron Scattering

    DEFF Research Database (Denmark)

    da Costa Carneiro, Kim; Nielsen, M.; McTague, J. P.

    1973-01-01

    Coherent scattering of neutrons by liquid parahydrogen shows the existence of well-defined collective excitations in this liquid. Qualitative similarity with the scattering from liquid helium is found. Furthermore, in the range of observed wave vectors, 0.7 Å-1 ≤κ≤3.1 Å-1, extending from the firs...... through the third Brillouin zones in the solid, S(κ,ω) is remarkably similar to the scattering law expected from a polycrystal. For κ≤2.3 Å-1 the observed spectra satisfy the one-phonon sum rule with mean square displacement 〈u2〉=1.0 Å2....

  2. Spin observables in proton-neutron scattering at intermediate energy

    International Nuclear Information System (INIS)

    Spinka, H.

    1986-05-01

    A summary of np elastic scattering spin measurements at intermediate energy is given. Preliminary results from a LAMPF experiment to measure free neutron-proton elastic scattering spin-spin correlation parameters are presented. A longitudinally polarized proton target was used. These measurements are part of a program to determine the neutron-proton amplitudes in a model independent fashion at 500, 650, and 800 MeV. Some new proton-proton total cross sections in pure helicity states (Δσ/sub L/(pp)) near 3 GeV/c are also given. 37 refs., 2 figs

  3. Neutron scattering

    International Nuclear Information System (INIS)

    1991-02-01

    The annual report on hand gives an overview of the research work carried out in the Laboratory for Neutron Scattering (LNS) of the ETH Zuerich in 1990. Using the method of neutron scattering, it is possible to examine in detail the static and dynamic properties of the condensed material. In accordance with the multidisciplined character of the method, the LNS has for years maintained a system of intensive co-operation with numerous institutes in the areas of biology, chemistry, solid-state physics, crystallography and materials research. In 1990 over 100 scientists from more than 40 research groups both at home and abroad took part in the experiments. It was again a pleasure to see the number of graduate students present, who were studying for a doctorate and who could be introduced into the neutron scattering during their stay at the LNS and thus were in the position to touch on central ways of looking at a problem in their dissertation using this modern experimental method of solid-state research. In addition to the numerous and interesting ways of formulating the questions to explain the structure, nowadays the scientific programme increasingly includes particularly topical studies in connection with high temperature-supraconductors and materials research

  4. Direct Observation of Neutron Scattering in BC408 Scintillator for Comparison with SImulation

    Science.gov (United States)

    Rogers, W. F.; Boone, J. E.; Wantz, A.; Frank, N.; Kuchera, A. N.; Mosby, S.; Thoennessen, M.; MoNA Collaboration

    2017-09-01

    Monte Carlo simulation provides an important tool for the interpretation of neutron scattering data in the Modular Neutron Array (MoNA) and the Large multi-Institutional Scintillator Array (LISA), each located at the NSCL facility at MSU and consisting of 144 stacked 2-m long organic plastic scintillator bar detectors. Energy and trajectory for unbound state decay neutrons are determined by time of flight and location of first light produced in the array. While most neutrons scattering elastically from protons and inelastically from C nuclei produce light above detector threshold, those scattered elastically from C remain below threshold (``dark scatter''), altering neutron trajectories, thus decreasing energy and momentum resolution. To test the accuracy of our Geant4/MENATE_R simulations, we observed neutrons scattering from 16 MoNA bars arranged in two stack geometries at the LANSCE facility at Los Alamos National Laboratory. Spallation neutrons ranging in energy from 0.5 to 800 MeV emerged from a 3 mm collimator in the 90m shed on WNR flight path 4FP15L and struck the array along a well defined path. Results for neutron hit multiplicity, scattering dynamics, and dark scatter redirection are compared with simulation. Work supported by NSF Grant PHY-1744043.

  5. Direct Observation of Neutron Scattering in MoNA Scintillator Detectors

    Science.gov (United States)

    Rogers, W. F.; Mosby, S.; Frank, N.; Kuchera, A. N.; Thoennessen, M.; MoNA Collaboration

    2017-01-01

    Monte Carlo simulations provide an important tool for the interpretation of neutron scattering data in the MoNA and LISA arrays at NSCL. Neutron energy and trajectory are determined by time of flight and position of first light produced in the array. Neutrons elastically scattered from H and inelastically from C typically produce light above detector threshold, while those elastically scattered from C produce light below threshold (``dark scattering'') and are redirected in flight, thus lowering energy and trajectory resolution. In order to test the effectiveness of our Geant4/MENATE_R simulations, we conducted an experiment at the LANSCE facility at Los Alamos National Laboratory to observe scattering of individual neutrons with well defined energy and trajectory in 16 MoNA detector bars arranged in two different stack geometries. Neutrons with energies ranging from 0.5 to 800 MeV emerged from a 3 mm collimator in the 90m shed on the WNR 4FP15L flight path to enter the array at a well defined point. Several features of neutron scattering are compared with simulation predictions, including hit multiplicity, scattering angle, mean distance between scatters, and the effect of dark scatter redirection. Results to date will be presented. Work supported by NSF Grant PHY-1506402.

  6. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2012-07-01

    The following topics are dealt with: Neutron scattering in contemporary research, neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  7. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2012-01-01

    The following topics are dealt with: Neutron scattering in contemporary research, neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  8. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2013-07-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, nanostructures investigated by small-angle neutron scattering, structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic neutron scattering, strongly correlated electrons, polymer dynamics, applications of neutron scattering. (HSI)

  9. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2013-01-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, nanostructures investigated by small-angle neutron scattering, structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic neutron scattering, strongly correlated electrons, polymer dynamics, applications of neutron scattering. (HSI)

  10. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: Neutron sources, neutron properties and elastic scattering, correlation functions measured by scattering experiments, symmetry of crystals, applications of neutron scattering, polarized-neutron scattering and polarization analysis, structural analysis, magnetic and lattice excitation studied by inelastic neutron scattering, macromolecules and self-assembly, dynamics of macromolecules, correlated electrons in complex transition-metal oxides, surfaces, interfaces, and thin films investigated by neutron reflectometry, nanomagnetism. (HSI)

  11. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: Neutron sources, neutron properties and elastic scattering, correlation functions measured by scattering experiments, symmetry of crystals, applications of neutron scattering, polarized-neutron scattering and polarization analysis, structural analysis, magnetic and lattice excitation studied by inelastic neutron scattering, macromolecules and self-assembly, dynamics of macromolecules, correlated electrons in complex transition-metal oxides, surfaces, interfaces, and thin films investigated by neutron reflectometry, nanomagnetism. (HSI)

  12. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  13. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  14. Observation of events with an energetic forward neutron in deep inelastic scattering at HERA

    International Nuclear Information System (INIS)

    Derrick, M.; Krakauer, D.; Magill, S.

    1996-05-01

    In deep inelastic neutral current scattering of positrons and protons at the center of mass energy of 300 GeV, we observe, with the ZEUS detector, events with a high energy neutron produced at very small scattering angles with respect to the proton direction. The events constitute a fixed fraction of the deep inelastic, neutral current event sample independent of Bjorken x and Q 2 in the range 3.10 -4 BJ -3 and 10 2 2 . (orig.)

  15. Methods of contrast variation by nuclear polarisation in small-angle neutron scattering: Observation of domains of nuclear polarisation by neutron scattering

    International Nuclear Information System (INIS)

    Leymarie, E.

    2002-11-01

    In this thesis we study the theoretical and experimental aspects of Contrast Variation by Nuclear Polarization (CVNP) applied to small-angle neutron scattering. The basics of neutron scattering theory is developed by highlighting the origin of the CVNP method: the strong spin dependence of thermal neutron scattering, especially on protons. We also present the principles of NMR with a special attention on the method of dynamic nuclear polarization by the solid effect which makes it possible to control the proton polarization and therefore the contrast for neutron scattering. We present a theoretical study of the CVNP method called static which supposes that the nuclear polarization is homogeneous in the sample and constant during the experiment. We show that it allows one to obtain partial structure functions of systems with multiple components, by carrying out several acquisitions with different polarizations on a single sample. For this purpose, we tested a simple device to stabilize the nuclear polarization. We describe finally a new application of the CVNP method called dynamic. In a solution of deuterated glycerol-water containing a small concentration of paramagnetic centres, we showed the existence of domains of polarized protons at the onset of dynamic polarization. This reinforces considerably the coherent scattering of paramagnetic centres. We describe the theoretical reasons explaining the appearance of these domains of polarization, as well as the various techniques used to observe them by neutron scattering. (author)

  16. Hidden order in Ce compounds. Direct observation of magnetic octupole order by neutron scattering

    International Nuclear Information System (INIS)

    Kuwahara, Keitaro

    2008-01-01

    Experimental results of single crystal neutron scattering experiments on Ce 0.7 La 0.3 B 6 , which shows a so-called 'hidden order' in phase IV at low temperature, are presented. Below the phase transition temperature 1.5 K of phase IV, weak but distinct superlattice reflections at the scattering vector (h/2,h/2,l/2) (h, l=odd number) have been observed for the first time by neutron scattering. The intensity of the superlattice reflections is stronger for high scattering vectors, which is quite different from the usual magnetic form factor of magnetic dipoles. This result directly evidences that the order parameter of phase IV has a complex magnetization density, consistent with the recent experimental and theoretical prediction in which the order parameter is the magnetic octupoles. Neutron scattering experiments using short wavelength neutrons, as done in this study, could become a general method to study the high-rank multipoles in f electron systems. (author)

  17. Neutron scattering

    International Nuclear Information System (INIS)

    Furrer, A.

    1993-01-01

    This report contains the text of 16 lectures given at the Summer School and the report on a panel discussion entitled ''the relative merits and complementarities of x-rays, synchrotron radiation, steady- and pulsed neutron sources''. figs., tabs., refs

  18. Neutron Scattering

    International Nuclear Information System (INIS)

    Fayer, Michael J.; Gee, Glendon W.

    2005-01-01

    The neutron probe is a standard tool for measuring soil water content. This article provides an overview of the underlying theory, describes the methodology for its calibration and use, discusses example applications, and identifies the safety issues. Soil water makes land-based life possible by satisfying plant water requirements, serving as a medium for nutrient movement to plant roots and nutrient cycling, and controlling the fate and transport of contaminants in the soil environment. Therefore, a successful understanding of the dynamics of plant growth, nutrient cycling, and contaminant behavior in the soil requires knowledge of the soil water content as well as its spatial and temporal variability. After more than 50 years, neutron probes remain the most reliable tool available for field monitoring of soil water content. Neutron probes provide integrated measurements over relatively large volumes of soil and, with proper access, allow for repeated sampling of the subsurface at the same locations. The limitations of neutron probes include costly and time-consuming manual operation, lack of data automation, and costly regulatory requirements. As more non-radioactive systems for soil water monitoring are developed to provide automated profiling capabilities, neutron-probe usage will likely decrease. Until then, neutron probes will continue to be a standard for reliable measurements of field water contents in soils around the globe

  19. Chamber for mechanical testing in H2 with observation by neutron scattering

    Science.gov (United States)

    Connolly, Matthew; Bradley, Peter; Slifka, Andrew; Drexler, Elizabeth

    2017-06-01

    A gas-pressure chamber has been designed, constructed, and tested at a moderate pressure (3.4 MPa, 500 psi) and has the capability of mechanical loading of steel specimens for neutron scattering measurements. The chamber will allow a variety of in situ neutron scattering measurements: in particular, diffraction, quasielastic scattering, inelastic scattering, and imaging. The chamber is compatible with load frames available at the user facilities at the NIST Center for Neutron Research and Oak Ridge National Laboratory Spallation Neutron Source. A demonstration of neutron Bragg edge imaging using the chamber is presented.

  20. Observation of edge refraction in ultra small angle neutron scattering

    International Nuclear Information System (INIS)

    Treimer, W.; Strobl, M.; Hilger, A.

    2002-01-01

    Slits and macroscopic objects such as edges give rise to refraction and diffraction. In this Letter we show the effect of Cd edges and slits if they are inserted between the monochromator and analyser in a double crystal diffractometer. Despite to the use of wavelengths of tens of nanometer and strong absorbing materials refraction is observed which contributes to enhanced wing intensity of the instrumental curve of the double crystal diffractometer

  1. Observation of edge refraction in ultra small angle neutron scattering

    Science.gov (United States)

    Treimer, W.; Strobl, M.; Hilger, A.

    2002-11-01

    Slits and macroscopic objects such as edges give rise to refraction and diffraction. In this Letter we show the effect of Cd edges and slits if they are inserted between the monochromator and analyser in a double crystal diffractometer. Despite to the use of wavelengths of tens of nanometer and strong absorbing materials refraction is observed which contributes to enhanced wing intensity of the instrumental curve of the double crystal diffractometer.

  2. Observation of cross-shaped anisotropy in spin-resolved small-angle neutron scattering

    Science.gov (United States)

    Michels, Andreas; Honecker, Dirk; Döbrich, Frank; Dewhurst, Charles D.; Suzuki, Kiyonori; Heinemann, André

    2012-05-01

    We report the results of spin-resolved small-angle neutron scattering (SANS) experiments on the two-phase nanocrystalline alloy NANOPERM. At a saturating applied magnetic field of 1.27T we observe a cross-shaped angular anisotropy in the non-spin-flip SANS cross section Σ++. This feature—for this class of materials only visible at saturation in Σ++—is attributed to the specific ratio of nuclear to magnetic scattering being smaller than unity. Analysis of the non-spin-flip and spin-flip cross sections provides the nuclear and magnetic SANS and allows us to estimate the magnitude of the respective scattering-length density contrast at the interphase between the nanoparticles and the amorphous magnetic matrix.

  3. Observation of spin-wave dispersion in Nd-Fe-B magnets using neutron Brillouin scattering

    International Nuclear Information System (INIS)

    Ono, K.; Inami, N.; Saito, K.; Takeichi, Y.; Kawana, D.; Yokoo, T.; Itoh, S.; Yano, M.; Shoji, T.; Manabe, A.; Kato, A.; Kaneko, Y.

    2014-01-01

    The low-energy spin-wave dispersion in polycrystalline Nd-Fe-B magnets was observed using neutron Brillouin scattering (NBS). Low-energy spin-wave excitations for the lowest acoustic spin-wave mode were clearly observed. From the spin-wave dispersion, we were able to determine the spin-wave stiffness constant D sw (100.0 ± 4.9 meV.Å 2 ) and the exchange stiffness constant A (6.6 ± 0.3 pJ/m)

  4. Neutron scattering. Experiment manuals

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: The thermal triple axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot single-crystal diffractometer HEiDi for structure analysis with neutrons, the backscattering spectrometer SPHERES, neutron polarization analysis with tht time-of-flight spectrometer DNS, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering with the KWS-1 and KWS-2 diffractometers, the very-small-angle neutron scattering diffractrometer with focusing mirror KWS-3, the resonance spin-echo spectrometer RESEDA, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  5. Neutron scattering. Experiment manuals

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: The thermal triple axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot single-crystal diffractometer HEiDi for structure analysis with neutrons, the backscattering spectrometer SPHERES, neutron polarization analysis with tht time-of-flight spectrometer DNS, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering with the KWS-1 and KWS-2 diffractometers, the very-small-angle neutron scattering diffractrometer with focusing mirror KWS-3, the resonance spin-echo spectrometer RESEDA, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  6. Introduction to neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Fischer, W.E. [Paul Scherrer Inst. (PSI), Villigen (Switzerland)

    1996-11-01

    We give here an introduction to the theoretical principles of neutron scattering. The relationship between scattering- and correlation-functions is particularly emphasized. Within the framework of linear response theory (justified by the weakness of the basic interaction) the relation between fluctuation and dissipation is discussed. This general framework explains the particular power of neutron scattering as an experimental method. (author) 4 figs., 4 refs.

  7. Observation and modeling of biological colloids with neutron scattering techniques and Monte Carlo simulations

    NARCIS (Netherlands)

    Van Heijkamp, L.F.

    2011-01-01

    In this study non-invasive neutron scattering techniques are used on soft condensed matter, probing colloidal length scales. Neutrons penetrate deeply into matter and have a different interaction with hydrogen and deuterium, allowing for tunable contrast using light and heavy water as solvents. The

  8. Polarimetric neutron scattering

    International Nuclear Information System (INIS)

    Tasset, F.

    2001-01-01

    Polarimetric Neutron Scattering in introduced, both by, explaining methodological issues and the corresponding instrumental developments. After a short overview of neutron spin polarization and the neutron polarization 3d-vector a pictorial approach of the microscopic theory is used to show how a polarized beam interacts with lattice and magnetic Fourier components in a crystal. Examples are given of using Spherical Neutron Polarimetry (SNP) and the corresponding Cryopad polarimeter for the investigation of non-collinear magnetic structures. (R.P.)

  9. Outline of Neutron Scattering Formalism

    OpenAIRE

    Berk, N. F.

    1993-01-01

    Neutron scattering formalism is briefly surveyed. Topics touched upon include coherent and incoherent scattering, bound and free cross-sections, the Van Hove formalism, magnetic scattering, elastic scattering, the static approximation, sum rules, small angle scattering, inelastic scattering, thermal diffuse scattering, quasielastic scattering, and neutron optics.

  10. Virtual neutron scattering experiments

    DEFF Research Database (Denmark)

    Overgaard, Julie Hougaard; Bruun, Jesper; May, Michael

    2016-01-01

    We describe how virtual experiments can be utilized in a learning design that prepares students for hands-on experiments at large-scale facilities. We illustrate the design by showing how virtual experiments are used at the Niels Bohr Institute in a master level course on neutron scattering....... In the last week of the course, students travel to a large-scale neutron scattering facility to perform real neutron scattering experiments. Through student interviews and survey answers, we argue, that the virtual training prepares the students to engage more fruitfully with experiments by letting them focus...

  11. Virtual neutron scattering experiments

    DEFF Research Database (Denmark)

    Overgaard, Julie Hougaard; Bruun, Jesper; May, Michael

    2017-01-01

    We describe how virtual experiments can be utilized in a learning design that prepares students for hands-on experiments at large-scale facilities. We illustrate the design by showing how virtual experiments are used at the Niels Bohr Institute in a master level course on neutron scattering....... In the last week of the course, students travel to a large-scale neutron scattering facility to perform real neutron scattering experiments. Through student interviews and survey answers, we argue, that the virtual training prepares the students to engage more fruitfully with experiments by letting them focus...

  12. Neutron scattering. Experiment manuals

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2014-01-01

    The following topics are dealt with: The thermal triple-axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot-single-crystal diffractometer HEiDi, the three-axis spectrometer PANDA, the backscattering spectrometer SPHERES, the DNS neutron-polarization analysis, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering at KWS-1 and KWS-2, a very-small-angle neutron scattering diffractometer with focusing mirror, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  13. Neutron scattering. Experiment manuals

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2014-07-01

    The following topics are dealt with: The thermal triple-axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot-single-crystal diffractometer HEiDi, the three-axis spectrometer PANDA, the backscattering spectrometer SPHERES, the DNS neutron-polarization analysis, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering at KWS-1 and KWS-2, a very-small-angle neutron scattering diffractometer with focusing mirror, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  14. Volume 15. Neutron scattering

    International Nuclear Information System (INIS)

    Kostorz, G.

    1979-01-01

    This volume of the Treatise on Materials Science and Technology shows how neutron scattering methods can be used to obtain important information on materials, by guiding the reader through the principles and describing recent applications. Materials scientists, but also solid state physicists, physical chemists, and metallurgists interested in this field, will find a completely referenced survey of the ''classical topics'' of neutron scattering and a more detailed presentation of methods and techniques that are more specifically related to materials science. After a brief review of the general principles in the first chapter, subsequent chapters concentrate on particular methods and problems. The techniques used in neutron crystallography are presented, and selected applications of nuclear and magnetic scattering are discussed. The measurement of phonons, their role in phase transformations, and their behavior in the presence of crystal defects are considered, and quasi-elastic scattering is given detailed treatment. The methods of small-angle scattering and diffuse scattering have been developed to a considerable perfection in recent years and are presented in detail. The structure and dynamics of hydrogen dissolved in metals and the conformation and dynamics of polymers are two outstanding subjects to which neutron scattering has contributed so much in recent years that separate chapters are devoted to covering these fields. Finally, the choice of the appropriate materials is also becoming increasingly crucial in the design and construction of neutron spectrometers. Therefore, the last chapter deals with special materials problems in neutron devices

  15. Introductory theory of neutron scattering

    International Nuclear Information System (INIS)

    Gunn, J.M.F.

    1986-12-01

    The paper comprises a set of six lecture notes which were delivered to the summer school on 'Neutron Scattering at a pulsed source', Rutherford Laboratory, United Kingdom, 1986. The lectures concern the physical principles of neutron scattering. The topics of the lectures include: diffraction, incoherent inelastic scattering, connection with the Schroedinger equation, magnetic scattering, coherent inelastic scattering, and surfaces and neutron optics. (UK)

  16. Neutron scattering and models: Titanium

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.

    1997-07-01

    Differential neutron elastic-scattering cross sections of elemental titanium were measured from 4.5 {r_arrow} 10.0 MeV in incident energy increments of {approx} 0.5 MeV. At each energy the measurements were made at forty or more scattering angles distributed between {approx} 17 and 160{degree}. Concurrently, differential neutron inelastic-scattering cross sections were measured for observed excitations of 0.975 {+-} 0.034, 1.497 {+-} 0.033, 2.322 {+-} 0.058, 3.252 {+-} 0.043, 3.700 {+-} 0.093, 4.317 {+-} 0.075 and 4.795 {+-} 0.100 MeV. All of the observed inelastically-scattered neutron groups were composites of contributions from several isotopes and/or levels. The experimental results were used to develop energy-average optical, statistical and coupled-channels models.

  17. Phase transitions and neutron scattering

    International Nuclear Information System (INIS)

    Shirane, G.

    1993-01-01

    A review is given of recent advances in neutron scattering studies of solid state physics. I have selected the study of a structural phase transition as the best example to demonstrate the power of neutron scattering techniques. Since energy analysis is relatively easy, the dynamical aspects of a transition can be elucidated by the neutron probe. I shall discuss in some detail current experiments on the 100 K transition in SrTiO 3 , the crystal which has been the paradigm of neutron studies of phase transitions for many years. This new experiment attempts to clarify the relation between the neutron central peak, observed in energy scans, and the two length scales observed in recent x-ray diffraction studies where only scans in momentum space are possible. (author)

  18. Phase transitions and neutron scattering

    International Nuclear Information System (INIS)

    Shirane, G.

    1993-01-01

    A review is given of recent advances in neutron scattering studies of solid state physics. The author has selected the study of a structural phase transition as the best example to demonstrate the power of neutron scattering techniques. Since energy analysis is relatively easy, the dynamical aspects of a transition can be elucidated by the neutron probe. He will discuss in some detail current experiments on the 100K transition in SrTiO 3 , the crystal which has been the paradigm of neutron studies of phase transitions for many years. This new experiment attempts to clarify the relation between the neutron central peak, observed in energy scans, and the two length scales observed in recent x-ray diffraction studies where only scans in momentum space are possible

  19. Neutron scattering from fractals

    DEFF Research Database (Denmark)

    Kjems, Jørgen; Freltoft, T.; Richter, D.

    1986-01-01

    -angle neutron scattering studies of the variation with aggregation rate are presented. These results allow a very detailed comparison to be made with the theoretical scattering curves. Preliminary incoherent inelastic data on the low-frequency dynamics of hydroxylated silica particle aggregates show a clear...

  20. Neutron scattering in ORNL's calibration facility

    International Nuclear Information System (INIS)

    Liu, J.C.; Sims, C.S.; Casson, W.H.; Murakami, H.

    1991-01-01

    Room scattering corrections for several common neutron detectors in a new neutron calibration facility at the Oak Ridge National Laboratory were measured. Results for three radioisotopic sources in ground scattering and enclosed room scattering situations are compared with two model calculations, and the agreement is good. A personnel neutron spectrometer was used to examine further the spectral variation inside the enclosed neutron room. Scattered fluence and scattered dose equivalent results from the spectral measurements indicate that the scattering predictions using models hold only for small-source-to-detector distances. Additional observations from this study are also presented. (author)

  1. MAGNETIC NEUTRON SCATTERING

    International Nuclear Information System (INIS)

    ZALIZNYAK, I.A.; LEE, S.H.

    2004-01-01

    Much of our understanding of the atomic-scale magnetic structure and the dynamical properties of solids and liquids was gained from neutron-scattering studies. Elastic and inelastic neutron spectroscopy provided physicists with an unprecedented, detailed access to spin structures, magnetic-excitation spectra, soft-modes and critical dynamics at magnetic-phase transitions, which is unrivaled by other experimental techniques. Because the neutron has no electric charge, it is an ideal weakly interacting and highly penetrating probe of matter's inner structure and dynamics. Unlike techniques using photon electric fields or charged particles (e.g., electrons, muons) that significantly modify the local electronic environment, neutron spectroscopy allows determination of a material's intrinsic, unperturbed physical properties. The method is not sensitive to extraneous charges, electric fields, and the imperfection of surface layers. Because the neutron is a highly penetrating and non-destructive probe, neutron spectroscopy can probe the microscopic properties of bulk materials (not just their surface layers) and study samples embedded in complex environments, such as cryostats, magnets, and pressure cells, which are essential for understanding the physical origins of magnetic phenomena. Neutron scattering is arguably the most powerful and versatile experimental tool for studying the microscopic properties of the magnetic materials. The magnitude of the cross-section of the neutron magnetic scattering is similar to the cross-section of nuclear scattering by short-range nuclear forces, and is large enough to provide measurable scattering by the ordered magnetic structures and electron spin fluctuations. In the half-a-century or so that has passed since neutron beams with sufficient intensity for scattering applications became available with the advent of the nuclear reactors, they have became indispensable tools for studying a variety of important areas of modern science

  2. MAGNETIC NEUTRON SCATTERING

    Energy Technology Data Exchange (ETDEWEB)

    ZALIZNYAK,I.A.; LEE,S.H.

    2004-07-30

    Much of our understanding of the atomic-scale magnetic structure and the dynamical properties of solids and liquids was gained from neutron-scattering studies. Elastic and inelastic neutron spectroscopy provided physicists with an unprecedented, detailed access to spin structures, magnetic-excitation spectra, soft-modes and critical dynamics at magnetic-phase transitions, which is unrivaled by other experimental techniques. Because the neutron has no electric charge, it is an ideal weakly interacting and highly penetrating probe of matter's inner structure and dynamics. Unlike techniques using photon electric fields or charged particles (e.g., electrons, muons) that significantly modify the local electronic environment, neutron spectroscopy allows determination of a material's intrinsic, unperturbed physical properties. The method is not sensitive to extraneous charges, electric fields, and the imperfection of surface layers. Because the neutron is a highly penetrating and non-destructive probe, neutron spectroscopy can probe the microscopic properties of bulk materials (not just their surface layers) and study samples embedded in complex environments, such as cryostats, magnets, and pressure cells, which are essential for understanding the physical origins of magnetic phenomena. Neutron scattering is arguably the most powerful and versatile experimental tool for studying the microscopic properties of the magnetic materials. The magnitude of the cross-section of the neutron magnetic scattering is similar to the cross-section of nuclear scattering by short-range nuclear forces, and is large enough to provide measurable scattering by the ordered magnetic structures and electron spin fluctuations. In the half-a-century or so that has passed since neutron beams with sufficient intensity for scattering applications became available with the advent of the nuclear reactors, they have became indispensable tools for studying a variety of important areas of modern

  3. Small angle neutron scattering

    International Nuclear Information System (INIS)

    Dasannacharya, B.A.; Goyal, P.S.

    1997-01-01

    Small angle neutron scattering (SANS) is one of the most popular neutron scattering technique both for the basic research and as a tool in the hands of applied scientist. SANS is used for studying the structure of a material on a length scale of 10 - 1000 A. SANS is a diffraction experiment that involves scattering of a monocromatic beam of neutrons in order to obtain structural information about macromolecules and heterogeneities. This paper will discuss the design of SANS spectrometers with a special emphasis on the instruments which are better suited for medium flux reactors. The design of several different types of SANS spectrometers will be given. The optimization procedures and appropriate modifications to suit the budget and the space will be discussed. As an example, the design of a SANS spectrometer at CIRUS reactor Trombay will be given. (author)

  4. Neutron scattering in Australia

    International Nuclear Information System (INIS)

    Knott, R.B.

    1994-01-01

    Neutron scattering techniques have been part of the Australian scientific research community for the past three decades. The High Flux Australian Reactor (HIFAR) is a multi-use facility of modest performance that provides the only neutron source in the country suitable for neutron scattering. The limitations of HIFAR have been recognized and recently a Government initiated inquiry sought to evaluate the future needs of a neutron source. In essence, the inquiry suggested that a delay of several years would enable a number of key issues to be resolved, and therefore a more appropriate decision made. In the meantime, use of the present source is being optimized, and where necessary research is being undertaken at major overseas neutron facilities either on a formal or informal basis. Australia has, at present, a formal agreement with the Rutherford Appleton Laboratory (UK) for access to the spallation source ISIS. Various aspects of neutron scattering have been implemented on HIFAR, including investigations of the structure of biological relevant molecules. One aspect of these investigations will be presented. Preliminary results from a study of the interaction of the immunosuppressant drug, cyclosporin-A, with reconstituted membranes suggest that the hydrophobic drug interdigitated with lipid chains

  5. Observation of oxygen Frenkel disorder in uranium dioxide above 2000 K using neutron scattering techniques

    International Nuclear Information System (INIS)

    Clausen, K.; Hayes, W.; Macdonald, J.E.; Osborn, R.; Hutchings, M.T.

    1983-12-01

    Diffraction and coherent diffuse quasielastic scattering of neutrons have been used to investigate Frenkel disorder of the oxygen sublattice in single crystals of stoichiometric UO 2 . Measurements were made up to 2900 K using a special high-temperature furnace. The results provide the first direct evidence for the occurrence of Frenkel disorder in UO 2 and enable estimates of the defect concentration and activation energy to be made. (author)

  6. Neutron small angle scattering

    International Nuclear Information System (INIS)

    Ibel, K.

    1975-01-01

    The neutron small-angle scattering system at the High-Flux Reactor in Grenoble consists of three major parts: the supply of cold neutrons via bent neutron guides; the small angle camera D11; and the data handling facilities. The camera D11 has an overall length of 80 m. The effective length of the camera is variable. The length of the collimator before the fixed sample position can be reduced by movable neutron guides; the secondary flight path of 40 m full length contains detector sites in various positions. Thus, a large domain of momentum transfers can be exploited. Scattering angles between 5.10 -4 and 0.5 rad and neutron wavelengths from 0.2 to 2.0 nm are available with the same instrument and the same relative resolution. A large-area position-sensitive detector is used which allows simultaneous recording of intensities scattered into different angles; it is a multiwire proportional chamber. 3808 elements of 1 cm 2 are arranged in a two-dimensional matrix. Future development comprises an increase of the limit in the count rate due to the electronic interface between the detector and on-line computer, actually at 5.10 4 per sec. by one order of magnitude

  7. Small angle neutron scattering

    International Nuclear Information System (INIS)

    Gupta, Sanjay

    1982-01-01

    The technique of small angle neutron scattering was first used in Germany less than two decades ago. Since then it has developed very rapidly, and today it is regarded as one of the most powerful techniques in materials, chemical and biological research. During the last decade the combination of high flux reactors and sophisticated instrumentation has revolutionized the technique. This paper endeavours to present a brief but comprehensive review of small angle scattering of neutrons and its applications in solid state research. The domain in which small angle neutron scattering is particularly useful is delineated and some of the methods used in the analysis of data are discussed with special emphasis on recent developments. Typical small angle neutron scattering cameras are described. Finally some experimental results on heterogeneities in metallic systems (both static and dynamic studies), radiation damage in materials, superconductivity, magnetic materials and the technologically very important area of non-destructive testing are reviewed in order to illustrate the wide range of applicability of this technique to problems in solid state research. (author)

  8. Direct Observation Of Nanoparticle-Surfactant Interactions Using Small Angle Neutron Scattering

    Science.gov (United States)

    Kumar, Sugam; Aswal, V. K.

    2010-12-01

    Interactions of anionic silica nanoparticles with anionic, cationic and nonionic surfactants have directly been studied by contrast variation small angle neutron scattering (SANS). The measurements are performed on 1 wt% of both silica nanoparticles and surfactants of anionic sodium dodecyle sulphate (SDS), cationic dodecyltrimethyl ammonium bromide (DTAB) and non-ionic polyoxyethylene 10 lauryl ether (C12E10) in aqueous solution. We show that there is no direct interaction in the case of SDS with silica particles, whereas strong interaction for DTAB leads to the aggregation of silica particles. The interaction of C12E10 is found through the micelles adsorbed on the silica particles.

  9. Small angle neutron scattering

    Directory of Open Access Journals (Sweden)

    Cousin Fabrice

    2015-01-01

    Full Text Available Small Angle Neutron Scattering (SANS is a technique that enables to probe the 3-D structure of materials on a typical size range lying from ∼ 1 nm up to ∼ a few 100 nm, the obtained information being statistically averaged on a sample whose volume is ∼ 1 cm3. This very rich technique enables to make a full structural characterization of a given object of nanometric dimensions (radius of gyration, shape, volume or mass, fractal dimension, specific area… through the determination of the form factor as well as the determination of the way objects are organized within in a continuous media, and therefore to describe interactions between them, through the determination of the structure factor. The specific properties of neutrons (possibility of tuning the scattering intensity by using the isotopic substitution, sensitivity to magnetism, negligible absorption, low energy of the incident neutrons make it particularly interesting in the fields of soft matter, biophysics, magnetic materials and metallurgy. In particular, the contrast variation methods allow to extract some informations that cannot be obtained by any other experimental techniques. This course is divided in two parts. The first one is devoted to the description of the principle of SANS: basics (formalism, coherent scattering/incoherent scattering, notion of elementary scatterer, form factor analysis (I(q→0, Guinier regime, intermediate regime, Porod regime, polydisperse system, structure factor analysis (2nd Virial coefficient, integral equations, characterization of aggregates, and contrast variation methods (how to create contrast in an homogeneous system, matching in ternary systems, extrapolation to zero concentration, Zero Averaged Contrast. It is illustrated by some representative examples. The second one describes the experimental aspects of SANS to guide user in its future experiments: description of SANS spectrometer, resolution of the spectrometer, optimization of

  10. Industrial Uses of Neutron Scattering

    Science.gov (United States)

    Priesmeyer, Hans Georg

    Recent progress in neutron scattering for industrial purposes is reviewed. The relevant fields of interest are small-angle scattering, high-resolution diffraction, texture determination, reflectometry and radiography. Potential users are encouraged to address themselves to one of the neutron scattering centers given in the Appendix.

  11. Neutron scattering in dimers

    DEFF Research Database (Denmark)

    Gudel, H. U.; Furrer, A.; Kjems, Jørgen

    1986-01-01

    Insulating compounds containing dimers of transition metal and rare earth ions have been studied by inelastic neutron scattering (INS). Energy splittings can be directly determined, and the corresponding parameters are easily extracted from the experimental data. The intensities of dimer...... excitations are modulated by an interference term reflecting the distance between the magnetic ions within the dimers. The INS technique is particularly powerful for the study of effects like: temperature dependence of exchange, the role of biquadratic exchange, the combination of crystal-field and exchange...

  12. Neutron scattering from colloids

    International Nuclear Information System (INIS)

    Cebula, D.J.; Thomas, R.K.; Harris, N.M.; Tabony, J.; White, J.W.

    1978-01-01

    This paper appraises the usefulness of neutron diffraction and small angle scattering for determining the structure of dilute and concentrated sols. For monodisperse polystyrene latex, the particle size and density can be readily determined and an upper limit to density fluctuations within the colloid particle set. For the polystyrene latex peptized by the adsorption of laurate, the physical dimensions and packing density of the adsorbed phase can be determined. The effects of polydispersity for unpeptized and peptized graphite sols, and the effects of extreme particle anisotropy using sols of montmorillonite clay minerals have been studied. (author)

  13. Neutron scattering observations on the magnetic phases of rareearth ternary superconductors

    International Nuclear Information System (INIS)

    Moncton, D.E.

    1979-01-01

    A number of ternary compounds become superconducting even though they contain a chemically ordered sublattice of magnetic rare-earth ions. Studies of the physical properties of these materials have revealed anomalies below T/sub c/ which have been attributed to magentic ordering transitions. Usng neutron spectrometers at the Brookhaven National Laboratory, a group of us has demonstrated that simple magnetic structures with long-range order do occur, and we have solved some of the magnetic structures of these superconductors. Specifically, we have found that in DyMo 6 S 8 and TbMo 6 S 8 an antiferromagnetic structure coexists with superconductivity. In two other compounds, ErRh 4 B 4 and HoMo 6 S 8 we have found that the development of ferromagnetism is responsible for the quenching of superconductivity. A study of the critical magnetic neutron scattering near the superconducting → ferromagnetic transitions shows the presence of fluctuations into a state with an oscillatory magnetization of wave length lambda = 100A

  14. Neutron scattering of lanthanide materials

    International Nuclear Information System (INIS)

    Moon, R.M.; Nicklow, R.M.

    1991-01-01

    A selected review of recent neutron scattering results on lanthanide materials is presented. Topics covered include the magnetic structures of the elemental metals, magnetic superlattices, enhanced nuclear magnetism, magnetic excitations and critical scattering. (orig.)

  15. Single Crystal Diffuse Neutron Scattering

    Directory of Open Access Journals (Sweden)

    Richard Welberry

    2018-01-01

    Full Text Available Diffuse neutron scattering has become a valuable tool for investigating local structure in materials ranging from organic molecular crystals containing only light atoms to piezo-ceramics that frequently contain heavy elements. Although neutron sources will never be able to compete with X-rays in terms of the available flux the special properties of neutrons, viz. the ability to explore inelastic scattering events, the fact that scattering lengths do not vary systematically with atomic number and their ability to scatter from magnetic moments, provides strong motivation for developing neutron diffuse scattering methods. In this paper, we compare three different instruments that have been used by us to collect neutron diffuse scattering data. Two of these are on a spallation source and one on a reactor source.

  16. Magnetic neutron and x-ray scattering

    International Nuclear Information System (INIS)

    Vettier, C.

    1999-01-01

    Most of our knowledge about the microscopic properties of magnetic materials comes from neutron scattering experiments owing to the strength of the interaction between the neutron spin and magnetisation densities which is exploited to study the statics and dynamics of magnetic moments. Neutron diffraction is the probe of choice for magnetic structure determinations and inelastic neutron scattering is the only tool to observe the propagation of magnetic excitations. However, neutron scattering suffer from two drawbacks: i) neutron beams have a low flux and a low brilliance; ii) the magnetic neutron scattering amplitude is neither electronic shell sensitive nor species selective. These limitations are easily overcome by the x-ray methods. On the one hand, x-rays are extremely sensitive to electronic distributions and the use of resonant scattering has proven to be extremely sensitive to the symmetry of the site and electronic shell which carries the magnetisation. On the other hand, the high brilliance x-ray beams delivered by the modern synchrotron facilities are perfectly suited to the study of small samples. Furthermore, the recent progress achieved in x-ray instrumentation has stimulated considerable theoretical interest on the use of the x-ray scattering and new phenomena related to magnetism can be directly detected in x-ray scattering experiments. Recent specific examples are presented to underline the complementary use of neutron and x-ray methods. (author)

  17. Observation of soft phonon mode in TbFe3(BO3)4 by inelastic neutron scattering

    Science.gov (United States)

    Pavlovskiy, M. S.; Shaykhutdinov, K. A.; Wu, L. S.; Ehlers, G.; Temerov, V. L.; Gudim, I. A.; Shinkorenko, A. S.; Podlesnyak, A.

    2018-02-01

    The phonon dispersion in terbium iron borate TbFe3(BO3)4 has been measured by inelastic neutron scattering in a temperature range 180 observed at the corner of the Brillouin zone (Λ point) at temperatures T ⪆TS , in full agreement with theoretical calculations. The TA soft mode undergoes considerable broadening at the Λ point near the transition temperature that can be attributed to the anharmonic interference between transverse acoustic and optical modes.

  18. Fast dynamics of Na 0.5Li 0.5PO 3 observed by coherent neutron scattering

    Science.gov (United States)

    Rufflé, B.; Beaufils, S.; Etrillard, J.; Coddens, G.; Toudic, B.; Ecolivet, C.

    1997-02-01

    Experimental results obtained by coherent neutron scattering with the time of flight spectrometer MIBEMOL on the less-fragile glass-forming liquid Na 0.5Li 0.5PO 3 are presented. A qualitative discussion of the susceptibility spectra within the framework of the simplest version of the mode-coupling theory locates a possible crossover temperature Tc near 620 K (∼1.2 Tg) close to the temperature of the decoupling phenomena of the relaxation time scales observed by 31P NMR.

  19. Neutron scattering and models: Silver

    International Nuclear Information System (INIS)

    Smith, A.B.

    1996-07-01

    Differential neutron elastic-scattering cross sections of elemental silver were measured from 1.5 → 10 MeV at ∼ 100 keV intervals up to 3 MeV, at ∼ 200 keV intervals from 3 → 4 MeV, and at ∼ 500 keV intervals above 4 MeV. At ≤ 4 MeV the angular range of the measurements was ∼ 20 0 → 160 0 with 10 measured values below 3 MeV and 20 from 3 → 4 MeV at each incident energy. Above 4 MeV ≥ 40 scattering angles were used distributed between ∼ 17 0 and 16 0 All of the measured elastic distributions included some contributions due to inelastic scattering. Below 4 MeV the measurements determined cross sections for ten inelastically-scattered neutron groups corresponding to observed excitations of 328 ± 13, 419 ± 50, 748 ± 25, 908 ± 26, 115 ± 38, 1286 ± 25, 1507 ± 20, 1632 ± 30, 1835 ± 20 and 1944 ± 26 keV. All of these inelastic groups probably were composites of contributions from the two isotopes 107 Ag and 109 Ag. The experimental results were interpreted in terms of the spherical optical model and of rotational and vibrational coupled-channels models, and physical implications are discussed. In particular, the neutron-scattering results are consistent with a ground-state rotational band with a quadrupole deformation Β 2 = 0.20 ± ∼ 10% for both of the naturally-occurring silver isotopes

  20. Scattering of fast neutrons from elemental molybdenum

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.

    1982-11-01

    Differential broad-resolution neutron-scattering cross sections of elemental molybdenum were measured at 10 to 20 scattering angles distributed between 20 and 160 degrees and at incident-neutron energy intervals of approx. = 50 to 200 keV from 1.5 to 4.0 MeV. Elastically-scattered neutrons were fully resolved from inelastic events. Lumped-level inelastic-neutron-scattering cross sections were determined corresponding to observed excitation energies of; 789 +- 23, 195 +- 23, 1500 +- 34, 1617 +- 12, 1787, 1874, 1991, 2063 +- 24, 2296, 2569 and 2802 keV. An optical-statistical model was deduced from the measured elastic-scattering results. The experimental values were compared with the respective quantities given in ENDF/B-V

  1. In-situ observation of dynamic water behavior in polymer electrolyte fuel cell by combined method of Small-Angle Neutron Scattering and Neutron Radiography

    International Nuclear Information System (INIS)

    Putra, A; Yamaguchi, D; Koizumi, S; Hashimoto, T; Iwase, H; Maekawa, Y; Matsubayashi, M

    2010-01-01

    In-situ observation was conducted on an operating polymer electrolyte fuel cell with a combined method of small-angle neutron scattering (SANS) and neutron radiography (NR). The combined measurement system has been recently developed to visualize water in a wide length scale from nano- to millimeter and successfully detected a spatial distribution of the water generated in individual cell elements; NR macroscopically detected the water in a gas diffusion layer and a flow-field, whereas SANS microscopically did in a membrane electrode assembly. In particular SANS was found to be a strong tool to make a rather precise analysis on the water content inside of ion conducting channels of polymer electrolyte membrane.

  2. Commercial applications of neutron scattering

    International Nuclear Information System (INIS)

    Hutchings, M.T.

    1993-01-01

    The fact that industry is now willing to pay the full commercial cost for certain neutron scattering experiments aimed at solving its urgent materials - related problems is a true testimony to the usefulness of neutrons as microscopic probes. This paper gives examples of such use of three techniques drawn mainly from our experience at AEA Technology Harwell Laboratory. These are diffraction to measure residual stress, small angle neutron scattering to examine hardening precipitates in ferritic steels brought about by irradiation, and reflectivity to study amorphous diamond layers deposited on silicon. In most cases it is the penetrative power of the neutron which proves to be its best asset for commercial industrial applicaitons. (author)

  3. Direct observation of hydrogen trapped by NbC in steel using small-angle neutron scattering

    International Nuclear Information System (INIS)

    Ohnuma, Masato; Suzuki, Jun-ichi; Wei, Fu-Gao; Tsuzaki, Kaneaki

    2008-01-01

    Small-angle neutron scattering has been measured for 97.62Fe-0.23C-0.25Nb-1.90Ni (at.%) steel with and without hydrogen charging. The intensity of the scattering from nanosized NbC is higher for samples with hydrogen than for those without hydrogen. The enhanced scattering intensity for samples with hydrogen disappears after hydrogen desorption heat treatment. This result provides direct structural evidence for the trapping of hydrogen by NbC

  4. Small angle neutron scattering from glassy SiO2

    International Nuclear Information System (INIS)

    Spooner, S.; Hastings, J.B.

    1976-01-01

    The present investigation of neutron scattering from glassy silica was undertaken to resolve whether the small angle scattering observed by Renninger and Uhlmann could also be seen in the bulk samples typically used in neutron-scattering experiments. Within the rather large error bars of this experiment no small angle scattering increase at small angles could be seen. (Auth.)

  5. Superconductivity, antiferromagnetism, and neutron scattering

    International Nuclear Information System (INIS)

    Tranquada, John M.; Xu, Guangyong; Zaliznyak, Igor A.

    2014-01-01

    High-temperature superconductivity in both the copper-oxide and the iron–pnictide/chalcogenide systems occurs in close proximity to antiferromagnetically ordered states. Neutron scattering has been an essential technique for characterizing the spin correlations in the antiferromagnetic phases and for demonstrating how the spin fluctuations persist in the superconductors. While the nature of the spin correlations in the superconductors remains controversial, the neutron scattering measurements of magnetic excitations over broad ranges of energy and momentum transfers provide important constraints on the theoretical options. We present an overview of the neutron scattering work on high-temperature superconductors and discuss some of the outstanding issues. - Highlights: • High-temperature superconductivity is closely associated with antiferromagnetism. • Antiferromagnetic spin fluctuations coexist with the superconductivity. • Neutron scattering is essential for characterising the full spectrum of spin excitations

  6. Bibliography for thermal neutron scattering

    International Nuclear Information System (INIS)

    Sakamoto, M.; Chihara, J.; Nakahara, Y.; Kadotani, H.; Sekiya, T.

    1976-12-01

    It contains bibliographical references to measurements, calculations, reviews and basic studies on thermal neutron scatterings and dynamical properties of condensed matter. About 2,700 documents up to the end of 1975 are covered. (auth.)

  7. Neutron scattering and physisorption

    International Nuclear Information System (INIS)

    Marlow, I.; Thomas, R.K.; Trewern, T.D.

    1977-01-01

    Neutron scattering experiments on methane and ammonia adsorbed on a graphitized carbon black are described. Diffraction from adsorbed deuterated methane shows that, at a coverage of 0.7, it forms an epitaxial layer with a √3x√3 structure. Between 50 and 60 K it undergoes a phase transition from two-dimensional solid to liquid (bulk melting point=89.7 K). Similar results are obtained for deuterated methane on a sample of graphon intercalated with potassium. From the effect of adsorbed methane on the intensities of 001 peaks of both substrates the carbon atom of the methane is estimated to be 3.3+-0.2 A from the surface. Ammonia-d 3 on graphon behaves quite differently from methane. It follows a type III isotherm and at low temperatures desorbs from the surface to form bulk ammonia. This has anomalous melting properties which are shown to be related to adsorption isobars for the system. The detailed interpretation of the results emphasizes the close link between adsorption and heterogeneous nucleation. Quasielastic experiments on the ammonia-graphon system show that the adsorbed ammonia is undergoing translational diffusion on the surface which is much faster than in the bulk. This is attributed to the breaking up of the hydrogen bonded network normally present in t

  8. Superconductivity, Antiferromagnetism, and Neutron Scattering

    OpenAIRE

    Tranquada, John M.; Xu, Guangyong; Zaliznyak, Igor A.

    2013-01-01

    High-temperature superconductivity in both the copper-oxide and the iron-pnictide/chalcogenide systems occurs in close proximity to antiferromagnetically ordered states. Neutron scattering has been an essential technique for characterizing the spin correlations in the antiferromagnetic phases and for demonstrating how the spin fluctuations persist in the superconductors. While the nature of the spin correlations in the superconductors remains controversial, the neutron scattering measurements...

  9. Fast-neutron scattering from elemental cadmium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.

    1982-07-01

    Neutron differential-elastic-scattering cross sections of elemental cadmium are measured from approx. = 1.5 to 4.0 MeV at incident-neutron energy intervals of 50 to 200 keV and at 10 to 20 scattering angles distributed between approx. = 20 and 160 degrees. Concurrently, lumped-level neutron inelastic-excitation cross sections are measured. The experimental results are used to deduce parameters of an optical-statistical model that is descriptive of the observables and are compared with corresponding quantities given in ENDF/B-V

  10. Multiple magnetic scattering in small-angle neutron scattering of Nd?Fe?B nanocrystalline magnet

    OpenAIRE

    Ueno, Tetsuro; Saito, Kotaro; Yano, Masao; Ito, Masaaki; Shoji, Tetsuya; Sakuma, Noritsugu; Kato, Akira; Manabe, Akira; Hashimoto, Ai; Gilbert, Elliot P.; Keiderling, Uwe; Ono, Kanta

    2016-01-01

    We have investigated the influence of multiple scattering on the magnetic small-angle neutron scattering (SANS) from a Nd?Fe?B nanocrystalline magnet. We performed sample-thickness- and neutron-wavelength-dependent SANS measurements, and observed the scattering vector dependence of the multiple magnetic scattering. It is revealed that significant multiple scattering exists in the magnetic scattering rather than the nuclear scattering of Nd?Fe?B nanocrystalline magnet. It is considered that th...

  11. The challenge of observation on livings things by employing an ultra small-angle neutron scattering method

    International Nuclear Information System (INIS)

    Koizumi, Satoshi; Motokawa, Ryuhei; Iwase, Hiroki; Miyamoto, Nobuyoshi; Tanaka, Kazuhiro; Masui, Tomomi; Iida, You; Yue, Zhao; Chiba, Kaori; Kumada, Takayuki; Yamaguchi, Daisuke; Hashimoto, Takeji

    2007-01-01

    To address the question as to how small-angle scattering is effectively applied to the cell, i.e., a hierarchically ordered system comprising multi-components of macro and small molecules, the size of which ranges from 100 μm to several μm, we reconstructed SANS-J (pinhole small-angle neutron scattering spectrometer at research reactor JRR3, Tokai) to focusing and polarized neutron small-angle spectrometer (SANS-J-II), by employing focusing neutron lenses and high resolution photomultiplier. Consequently, an accessible minimum wave number q min was improved from 3x10 -3 A -1 to medium ultra-small angle scattering of 3x10 -4 A -1 . The focusing USANS method, thus developed, is crucial to fill the gap in wave number q between those covered by a double crystal method and by a conventional pin-hole method. (author)

  12. Neutron scatter camera

    Science.gov (United States)

    Mascarenhas, Nicholas; Marleau, Peter; Brennan, James S.; Krenz, Kevin D.

    2010-06-22

    An instrument that will directly image the fast fission neutrons from a special nuclear material source has been described. This instrument can improve the signal to background compared to non imaging neutron detection techniques by a factor given by ratio of the angular resolution window to 4.pi.. In addition to being a neutron imager, this instrument will also be an excellent neutron spectrometer, and will be able to differentiate between different types of neutron sources (e.g. fission, alpha-n, cosmic ray, and D-D or D-T fusion). Moreover, the instrument is able to pinpoint the source location.

  13. Neutron scattering. Experiment manuals

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2012-01-01

    The following topics are dealt with: The thermal triple-axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot single-crystal diffractometer HEiDi for structure analysis with neutrons, the backscattering spectrometer SPHERES, the neutron polarization analyzer DNS, the neutron spin-echo spectrometer J-NSE, the small-angle neutron diffractometers KWS-1/-2, the very-small-angle neutron diffractometer with focusing mirror KWS-3, the resonance spin-echo spectrometer RESEDA, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  14. Critical Magnetic Scattering of Neutrons in Iron

    DEFF Research Database (Denmark)

    Passell, L.; Blinowski, K.; Brun, T.

    1964-01-01

    scattered at small angles in iron and determined the spin correlation range 1∕κ1 and a parameter Λ associated with the lifetime of the fluctuations. Our results confirm the recent observation of Jacrot, Konstantinovic, Parette, and Cribier that the scattering is not elastic even at the Curie temperature. We......The intense small‐angle scattering of low‐energy neutrons by magnetic materials near the Curie temperature has been shown by Van Hove to be directly related to the appearance of large scale fluctuations in the spin density. We have measured the angular and energy distributions of 4.27‐Å neutrons...

  15. New techniques in neutron scattering

    International Nuclear Information System (INIS)

    Hayter, J.B.

    1993-01-01

    New neutron sources being planned, such as the Advanced Neutron Source (ANS) or the European Spallation Source (ESS), will provide an order of magnitude flux increase over what is available today, but neutron scattering will still remain a signal-limited technique. At the same time, the development of new materials, such as polymer and ceramic composites or a variety of complex fluids, will increasingly require neutron-based research. This paper will discuss some of the new techniques which will allow us to make better use of the available neutrons, either through improved instrumentation or through sample manipulation. Discussion will center primarily on unpolarized neutron techniques since polarized neutrons will be the subject of the next paper. (author)

  16. Neutron scattering science in Australia

    International Nuclear Information System (INIS)

    Knott, Robert

    1999-01-01

    Neutron scattering science in Australia is making an impact on a number of fields in the scientific and industrial research communities. The unique properties of the neutron are being used to investigate problems in chemistry, materials science, physics, engineering and biology. The reactor HIFAR at the Australian Nuclear Science and Technology Organisation research laboratories is the only neutron source in Australia suitable for neutron scattering science. A suite of instruments provides a wide range of opportunities for the neutron scattering community that extends throughout universities, government and industrial research laboratories. Plans are in progress to replace the present research reactor with a modern multi-purpose research reactor to offer the most advanced neutron scattering facilities. The experimental and analysis equipment associated with a modern research reactor will permit the establishment of a national centre for world class neutron science research focussed on the structure and functioning of materials, industrial irradiations and analyses in support of Australian manufacturing, minerals, petrochemical, pharmaceuticals and information science industries. (author)

  17. Neutron scattering science in Australia

    Energy Technology Data Exchange (ETDEWEB)

    Knott, Robert [Australian Nuclear Science and Technology Organisation, Menai, NSW (Australia)

    1999-10-01

    Neutron scattering science in Australia is making an impact on a number of fields in the scientific and industrial research communities. The unique properties of the neutron are being used to investigate problems in chemistry, materials science, physics, engineering and biology. The reactor HIFAR at the Australian Nuclear Science and Technology Organisation research laboratories is the only neutron source in Australia suitable for neutron scattering science. A suite of instruments provides a wide range of opportunities for the neutron scattering community that extends throughout universities, government and industrial research laboratories. Plans are in progress to replace the present research reactor with a modern multi-purpose research reactor to offer the most advanced neutron scattering facilities. The experimental and analysis equipment associated with a modern research reactor will permit the establishment of a national centre for world class neutron science research focussed on the structure and functioning of materials, industrial irradiations and analyses in support of Australian manufacturing, minerals, petrochemical, pharmaceuticals and information science industries. (author)

  18. Chemical applications of neutron scattering.

    Science.gov (United States)

    Trouw, F R; Price, D L

    1999-01-01

    Neutron scattering represents a versatile technique for chemists, as it explores the structure and dynamics of materials at the atomic scale. This review gives an outline of the neutron scattering formalism and describes diffraction and inelastic and quasielastic scattering techniques. Applications to chemistry are illustrated by examples from recent work on crystalline and liquid organic materials, including heterogeneous systems, bulk polymers and polymer solutions. There is particular emphasis on systems where hydrogen bonding plays a significant role. With more powerful sources and improved instrumentation in prospect, there is considerable potential for future extension of these methods to increasingly complex materials.

  19. Advances in neutron scattering spectroscopy

    International Nuclear Information System (INIS)

    White, J.W.

    1977-01-01

    Some aspects of the application of neutron scattering to problems in polymer science, surface chemistry, and adsorption phenomena, as well as molecular biology, are reviewed. In all these areas, very significant work has been carried out using the medium flux reactors at Harwell, Juelich and Risoe, even without the use of advanced multidetector techniques or of a neutron cold source. A general tendency can also be distinguished in that, for each of these new fields, a distinct preference for colder neutrons rather than thermal neutron beams can be seen. (author)

  20. Neutron scattering from fractals

    DEFF Research Database (Denmark)

    Kjems, Jørgen; Freltoft, T.; Richter, D.

    1986-01-01

    The scattering formalism for fractal structures is presented. Volume fractals are exemplified by silica particle clusters formed either from colloidal suspensions or by flame hydrolysis. The determination of the fractional dimensionality through scattering experiments is reviewed, and recent small...

  1. Neutron Brillouin scattering in dense fluids

    Energy Technology Data Exchange (ETDEWEB)

    Verkerk, P. [Technische Univ. Delft (Netherlands); FINGO Collaboration

    1997-04-01

    Thermal neutron scattering is a typical microscopic probe for investigating dynamics and structure in condensed matter. In contrast, light (Brillouin) scattering with its three orders of magnitude larger wavelength is a typical macroscopic probe. In a series of experiments using the improved small-angle facility of IN5 a significant step forward is made towards reducing the gap between the two. For the first time the transition from the conventional single line in the neutron spectrum scattered by a fluid to the Rayleigh-Brillouin triplet known from light-scattering experiments is clearly and unambiguously observed in the raw neutron data without applying any corrections. Results of these experiments are presented. (author).

  2. Correlations among observables in the neutron-deuteron elastic scattering at low energies

    International Nuclear Information System (INIS)

    Frederico, T.; Goldman, I.D.

    1984-01-01

    The 2 S amplitude of the n-d elastic scattering appears like function of the dublet ( 2 a) scattering length in the three nucleons calculations. The correlation of Kcotg 2 δ o with 2 a, with separable N-N potential calculations, is obtained and the result is independent of the N-N potential. The 2 δ o (n-d) values obtained with these lines, using 2 a=.65F (experimental value), agree with p-d data. 2 S and 4 S scattering amplitude and tritium energy (E T ) calculations are performed with the zero-range model and an alternative deduction is proposed. These results for the E T and Kcotg 2 δ o correlation with 2 a show the limitations of this model. (L.C.) [pt

  3. Observation of Oxygen Frenkel Disorder in Uranium Dioxide above 2000 K by Use of Neutron-Scattering Techniques

    DEFF Research Database (Denmark)

    Clausen, Kurt Nørgaard; Hayes, W.; Macdonald, J E.

    1984-01-01

    Diffraction and coherent diffuse quasielastic scattering of neutrons have been used to investigate Frenkel disorder of the oxygen sublattice in single crystals of stoichiometric UO2. Measurements were made up to 2900 K using a special high-temperature furnace. The results provide the first direct...

  4. Neutron scattering and absorption properties

    Energy Technology Data Exchange (ETDEWEB)

    Holden, N.E.

    1993-12-01

    The Table in this report presents an evaluated set of values for the experimental quantities, which characterize the properties for scattering and absorption of neutrons. The neutron cross section is given for room temperature neutrons, 20.43{degree}C, corresponds to a thermal neutron energy of 0.0253 electron volts (eV) or a neutron velocity of 2200 meters/second. The neutron resonance integral is defined over the energy range from 0.5 eV to 0.1 {times} 10{sup 6} eV, or 0.1 MeV. A list of the major references used is given below. The literature cutoff data is October 1993. Uncertainties are given in parentheses. Parentheses with two or more numbers indicate values to the excited states(s) and to the ground state of the product nucleus.

  5. Neutron scattering in liquids

    Energy Technology Data Exchange (ETDEWEB)

    Barocchi, F. [Florence Univ. (Italy). Ist. di Fisica

    1996-12-31

    Together with X-rays, thermal neutrons are the ideal probe to study the microscopic structure of condensed matter, however the precision attainable usually with neutrons for the measurement of atomic position correlation functions in liquids is, at least, one order of magnitude better than for X-rays. In order to measure properly the microscopic dynamics a wide range of momentum transfer with corresponding energy transfer must be available in the range of liquid state excitations. This again is only attainable, with good resolution, with neutrons. (author) 7 figs., 3 refs.

  6. Neutron scattering by Dirac multipoles

    Science.gov (United States)

    Lovesey, S. W.; Khalyavin, D. D.

    2017-06-01

    Scattering by magnetic charge formed by Dirac multipoles that are magnetic and polar is examined in the context of materials with properties that challenge conventional concepts. An order parameter composed of Dirac quadrupoles has been revealed in the pseudo-gap phase of ceramic, high-T c superconductors on the basis of Kerr effect and magnetic neutron Bragg diffraction measurements. Construction of Dirac quadrupoles that emerge from centrosymmetric sites used by Cu ions in the ceramic superconductor Hg1201 is illustrated, together with selection rules for excitations that will feature in neutron inelastic scattering, and RIXS experiments. We report magnetic scattering amplitudes for diffraction by polar multipoles that have universal value, because they are not specific to ceramic superconductors. To illustrate this attribute, we consider neutron Bragg diffraction from a magnetically ordered iridate (Sr2IrO4) and discuss shortcomings in published interpretations of diffraction data.

  7. Neutron scattering by Dirac multipoles

    International Nuclear Information System (INIS)

    Lovesey, S W; Khalyavin, D D

    2017-01-01

    Scattering by magnetic charge formed by Dirac multipoles that are magnetic and polar is examined in the context of materials with properties that challenge conventional concepts. An order parameter composed of Dirac quadrupoles has been revealed in the pseudo-gap phase of ceramic, high- T c superconductors on the basis of Kerr effect and magnetic neutron Bragg diffraction measurements. Construction of Dirac quadrupoles that emerge from centrosymmetric sites used by Cu ions in the ceramic superconductor Hg1201 is illustrated, together with selection rules for excitations that will feature in neutron inelastic scattering, and RIXS experiments. We report magnetic scattering amplitudes for diffraction by polar multipoles that have universal value, because they are not specific to ceramic superconductors. To illustrate this attribute, we consider neutron Bragg diffraction from a magnetically ordered iridate (Sr 2 IrO 4 ) and discuss shortcomings in published interpretations of diffraction data. (paper)

  8. The Low-Temperature Inflection Observed in Neutron Scattering Measurements of Proteins Is Due to Methyl Rotation : Direct Evidence Using Isotope Labeling and Molecular Dynamics Simulations

    NARCIS (Netherlands)

    Wood, Kathleen; Tobias, Douglas J.; Kessler, Brigitte; Gabel, Frank; Oesterhelt, Dieter; Mulder, Frans A. A.; Zaccai, Giuseppe; Weik, Martin

    2010-01-01

    There is increasing interest in the contribution of methyl groups to the overall dynamics measured by neutron scattering experiments of proteins. In particular an inflection observed in atomic mean square displacements measured as a function of temperature on high resolution spectrometers (similar

  9. New Techniques in Neutron Scattering

    DEFF Research Database (Denmark)

    Birk, Jonas Okkels

    potential performance than any existing facility, however in order to use this pulse structure optimally many existing neutron scattering instruments will need to be redesigned. This defense will concentrate on the design and optimization of the inverse time-of-flight cold neutron spectrometer CAMEA......, simulations and prototyping to optimize the instrument and ensure that it will deliver the predicted performance when constructed. During the design a new prismatic analyser concept that can be of interest to many other neutron spectrometers was developed. The design work was compiled into an instrument......Neutron scattering is an important experimental technique in amongst others solid state physics, biophysics, and engineering. This year construction of European Spallation Source (ESS) was commenced in Lund, Sweeden. The facility will use a new long pulsed source principle to obtain higher...

  10. Neutron scattering by Dirac multipoles

    OpenAIRE

    Lovesey, S. W.; Khalyavin, D. D.

    2016-01-01

    Ordered magnetic charge created by Dirac multipoles that are magnetic and polar is examined. It has previously been revealed in the pseudo-gap phase of high-Tc materials by use of the Kerr effect and magnetic neutron Bragg diffraction. There are several forms of the polar operator for magnetic neutron scattering built from spin and electric dipole operators of unpaired electrons. Construction of Dirac quadrupoles that emerge from centrosymmetric sites used by Cu ions in the ceramic supercondu...

  11. Bibliography for thermal neutron scattering

    International Nuclear Information System (INIS)

    Sakamoto, Masanobu; Chihara, Junzo; Gotoh, Yorio; Kadotani, Hiroyuki; Sekiya, Tamotsu.

    1979-09-01

    Bibliographic references are given for measurements, calculations, reviews and basic studies of thermal neutron scattering and dynamical properties of condensed matter. This is the sixth edition covering 3,326 articles collected up to 1978. The edition being the final issue of the present bibliography series, a forthcoming edition will be published in a new form of bibliography. (author)

  12. Recent development in magnetic neutron scattering studies

    International Nuclear Information System (INIS)

    Endoh, Yasuo

    1993-01-01

    Neutron scattering results contain many new concepts in modern magnetism. We review here the most recent neutron magnetic scattering studies from so called '214' copper oxide lamellar materials, because a number of important developments in magnetism are condensed in this novel subject. We show that neutron scattering has played crucial role in our understanding of modern magnetism. (author)

  13. Interesting results from neutron-scattering

    International Nuclear Information System (INIS)

    Woods, A.D.B.

    Neutron scattering has been a useful tool in the determination of the lattice dynamics of metals, studies of the physics of magnetism in rare-earth systems, observing changes in the structure of DNA bases after ultraviolet irradiation, looking at plastic crystals, following structural phase changes in ferroelectric materials, and studying liquid He. Both low- and high-flux facilities are useful. (LL)

  14. A small angle neutron scattering study

    Indian Academy of Sciences (India)

    Nanocrystalline nickel oxide powders were calcined at 300, 600 and 900°C and pore structure evolution was followed by small angle neutron scattering (SANS). Pore size distributions at two widely separated size ranges have been revealed. Shrinkage of larger-sized pore with reduction in polydispersity has been observed ...

  15. Fast neutron scattering near shell closures: Scandium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.

    1992-08-01

    Neutron differential elastic- and inelastic-scattering cross sections are measured from ∼ 1.5 to 10 MeV with sufficient detail to define the energy-averaged behavior of the scattering processes. Neutrons corresponding to excitations of 465 ± 23, 737 ± 20, 1017 ± 34, 1251 ± 20, 1432 ± 23 and 1692 ± 25 keV are observed. It is shown that the observables, including the absorption cross section, are reasonably described with a conventional optical-statistical model having energy-dependent geometric parameters. These energy dependencies are alleviated when the model is extended to include the contributions of the dispersion relationship. The model parameters are conventional, with no indication of anomalous behavior of the neutron interaction with 45 Sc, five nucleons from the doubly closed shell at 40 Ca

  16. Artefacts of fast neutron radiography concerned with neutron scattering

    International Nuclear Information System (INIS)

    Mikerov, V.I.; Isakov, A.I.; Tukarev, V.A.; Koshelev, A.P.; Bykov, A.A.; Khodeev, A.I.; Waschkowski, W.

    1999-01-01

    The paper considers peculiarities of fast neutron radiography with a two dimensional detector. Effects produced by scattered neutrons was simulated for various neutron sources. Contribution of γ-rays generated in the sample was estimated for a fission spectrum of fast neutrons. Feasibility of fast neutrons collimating by a honeycomb collimator was considered.(author)

  17. Oxide research using neutron scattering

    International Nuclear Information System (INIS)

    Hunter, B.A.; Howard, C.J.; Kennedy, B.J.

    1998-01-01

    Full text: Oxide materials form a large group of technologically and scientifically important materials, and research on these types of materials is on the forefront of scientific research. The important properties of these materials, such as the electronic, magnetic and mechanical properties, are related to the structure and chemical composition of those materials. As the structure is so important in the understanding of the properties, neutron scattering is playing a key role due to its advantages in characterising the role of the oxygen. We present here some examples of the latest oxide structures studied by neutron powder diffraction at ANSTO

  18. Neutron scattering studies on soft materials

    International Nuclear Information System (INIS)

    Inoue, Rintaro; Kanaya, Toshiji

    2010-01-01

    We review recent progress of neutron scattering studies on soft matters using various techniques such as small angle neutron scattering, neutron spin echo, backscattering, time-of-flight technique, reflectivity and grazing-incident small angle neutron scattering. In the present review, we focus on functionalized polymers such as polyrotaxane, Nafion, polymer/nano composite system, and casein protein thin films, which are of great interest from both scientific and industrial viewpoints. We also state some future experiments at J-PARC. (author)

  19. The low-temperature inflection observed in neutron scattering measurements of proteins is due to methyl rotation: direct evidence using isotope labeling and molecular dynamics simulations.

    Science.gov (United States)

    Wood, Kathleen; Tobias, Douglas J; Kessler, Brigitte; Gabel, Frank; Oesterhelt, Dieter; Mulder, Frans A A; Zaccai, Giuseppe; Weik, Martin

    2010-04-14

    There is increasing interest in the contribution of methyl groups to the overall dynamics measured by neutron scattering experiments of proteins. In particular an inflection observed in atomic mean square displacements measured as a function of temperature on high resolution spectrometers (approximately 1 microeV) was explained by the onset of methyl group rotations. By specifically labeling a non-methyl-containing side-chain in a native protein system, the purple membrane, and performing neutron scattering measurements, we here provide direct experimental evidence that the observed inflection is indeed due to methyl group rotations. Molecular dynamics simulations reproduce the experimental data, and their analysis suggests that the apparent transition is due to methyl group rotation entering the finite instrumental resolution of the spectrometer. Methyl group correlation times measured by solid state NMR in the purple membrane, taken from previous work, support the interpretation.

  20. Quantum entanglement and neutron scattering experiments

    International Nuclear Information System (INIS)

    Cowley, R A

    2003-01-01

    It is shown that quantum entanglement in condensed matter can be observed with scattering experiments if the energy resolution of the experiments enables a clear separation between the elastic scattering and the scattering from the excitations in the system. These conditions are not satisfied in recent deep inelastic neutron scattering experiments from hydrogen-containing systems that have been interpreted as showing the existence of quantum entanglement for short times in, for example, water at room temperature. It is shown that the theory put forward to explain these experiments is inconsistent with the first-moment sum rule for the Van Hove scattering function and we suggest that the theory is incorrect. The experiments were performed using the unique EVS spectrometer at ISIS and suggestions are made about how the data and their interpretation should be re-examined

  1. Progress report on neutron scattering at JAERI

    International Nuclear Information System (INIS)

    Morii, Yukio

    2000-01-01

    Progress in neutron scattering experiments at Japan Atomic Energy Research Institute for the year 1997-1998 is reported in brief. The superconducting gap was discovered in the spin excitation spectra of a heavy fermion superconductor UPd 2 Al 3 , which proved the superconductivity of this compound to be due to magnetic origin. The magnetic and superconducting order parameter was found in UPd 2 Al 3 , UNi 2 Al 3 , UPt 3 and URu 2 Si 2 . It was concluded from this result that the coupling of the order parameter would be a characteristic property in heavy fermion superconductors. The correlation between strong magnetic interaction and the superconducting transition under high pressure was indicated from spin excitation in the strongly correlated electron system of a ladder material (Sr,Ca) 14 Cu 24 O 41 . The magnetic flux structure in a Bi 2 Sr 2 CaCu 2 O 8+δ superconductor was examined by SANS (small angle neutron scattering) to observe the decomposition of the flux lines. A liquid-He-free dilution refrigerator was developed for neutron scattering experiments at ultralow temperature. The coherent scattering length of the 69 Ga and 71 Ga was evaluated by use of the apparatus for precise neutron optics. The structure of hen egg-white Lysozyne was investigated in detail. Detailed research report for the year 1997-1998 was published in the JAERI-Review 99-003. (Y. Kazumata)

  2. Neutron scattering study of dilute supercritical solutions

    International Nuclear Information System (INIS)

    Cochran, H.D.; Wignall, G.D.; Shah, V.M.; Londono, J.D.; Bienkowski, P.R.

    1994-01-01

    Dilute solutions in supercritical solvents exhibit interesting microstructures that are related to their dramatic macroscopic behavior. In typical attractive solutions, solutes are believed to be surrounded by clusters of solvent molecules, and solute molecules are believed to congregate in the vicinity of one another. Repulsive solutions, on the other hand, exhibit a local region of reduced solvent density around the solute with solute-solute congregation. Such microstructures influence solubility, partial molar volume, reaction kinetics, and many other properties. We have undertaken to observe these interesting microstructures directly by neutron scattering experiments on dilute noble gas systems including Ar. The three partial structure factors for such systems and the corresponding pair correlation functions can be determined by using the isotope substitution technique. The systems studied are uniquely suited for our objectives because of the large coherent neutron scattering length of the isotope 36 Ar and because of the accurate potential energy functions that are available for use in molecular simulations and theoretical calculations to be compared with the scattering results. We will describe our experiment, the unique apparatus we have built for it, and the neutron scattering results from our initial allocations of beam time. We will also describe planned scattering experiments to follow those with noble gases, including study of long-chain molecules in supercritical solvents. Such studies will involve hydrocarbon mixtures with and without deuteration to provide contrast

  3. Neutron scattering from polarised proton domains

    CERN Document Server

    Van den Brandt, B; Kohbrecher, J; Konter, J A; Mango, S; Glattli, H; Leymarie, E; Grillo, I; May, R P; Jouve, H; Stuhrmann, H B; Stuhrmann, H B; Zimmer, O

    2002-01-01

    Time-dependent small-angle polarised neutron scattering from domains of polarised protons has been observed at the onset of dynamic nuclear polarisation in a frozen solution of 98% deuterated glycerol-water at 1 K containing a small concentration of paramagnetic centres (EHBA-Cr sup V). Simultaneous NMR measurements show that the observed scattering arises from protons around the Cr sup V -ions which are polarised to approx 10% in a few seconds, much faster than the protons in the bulk. (authors)

  4. Neutron scattering by normal liquids

    Energy Technology Data Exchange (ETDEWEB)

    Gennes, P.G. de [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1961-07-01

    Neutron data on motions in normal liquids well below critical point are reviewed and classified according to the order of magnitude of momentum transfers {Dirac_h}q and energy transfers {Dirac_h}w. For large momentum transfers a perfect gas model is valid. For smaller q and incoherent scattering, the major effects are related to the existence of two characteristic times: the period of oscillation of an atom in its cell, and the average lifetime of the atom in a definite cell. Various interpolation schemes covering both time scales are discussed. For coherent scattering and intermediate q, the energy spread is expected to show a minimum whenever q corresponds to a diffraction peak. For very small q the standard macroscopic description of density fluctuations is applicable. The limits of the various (q) and (w) domains and the validity of various approximations are discussed by a method of moments. The possibility of observing discrete transitions due to internal degrees of freedom in polyatomic molecules, in spite of the 'Doppler width' caused by translational motions, is also examined. (author) [French] L'auteur examine les donnees neutroniques sur les mouvements dans les liquides normaux, bien au-dessous du point critique, et les classe d'apres l'ordre de grandeur des transferts de quantite de mouvement {Dirac_h}q et des transferts d'energie {Dirac_h}w. Pour les grands transferts de, quantite de mouvement, un modele de gaz parfait est valable. En ce qui concerne les faibles valeurs de q et la diffussion incoherente, les principaux effets sont lies a l'existence de deux temps caracteristiques: la periode d'oscillation d'un atome dans sa cellule et la duree moyenne de vie de l'atome dans une cellule determinee. L'auteur etudie divers systemes d'interpolation se rapportant aux deux echelles de temps. Pour la diffusion coherente et les valeurs intermediaires de q, on presume que le spectre d

  5. Instruments and accessories for neutron scattering research

    International Nuclear Information System (INIS)

    Ishii, Yoshinobu; Morii, Yukio

    2000-04-01

    This report describes neutron scattering instruments and accessories installed by four neutron scattering research groups at the ASRC (Advanced Science Research Center) of the JAERI and the recent topics of neutron scattering research using these instruments. The specifications of nine instruments (HRPD, BIX-I, TAS-1 and PNO in the reactor hall, RESA, BIX-II, TAS-2, LTAS and SANS-J in the guide hall of the JRR-3M) are summarized in this booklet. (author)

  6. Neutron scattering studies in the actinide region

    International Nuclear Information System (INIS)

    Beghian, L.E.; Kegel, G.H.R.

    1991-08-01

    During the report period we have investigated the following areas: Neutron elastic and inelastic scattering measurements on 14 N, 181 Ta, 232 Th, 238 U and 239 Pu; Prompt fission spectra for 232 Th, 235 U, 238 U and 239 Pu; Theoretical studies of neutron scattering; Neutron filters; New detector systems; and Upgrading of neutron target assembly, data acquisition system, and accelerator/beam-line apparatus

  7. Alloys studied by neutron scattering

    International Nuclear Information System (INIS)

    Morii, Yukio

    1993-01-01

    Neutron scattering study on the martensitic transformation and spinodal decomposition of alloys is described. Lattice vibration mode [110]TA 1 in various noble metal bcc-based alloys was measured. An analysis of the (110) interplanar force constants revealed a relation between the force constants and the martensite phase at low temperatures. Time resolved experiments of spinodal decomposition of MnCu were carried out to investigate how the separated (decomposed) phase grows in time. In the late regime of the decomposition, the size of the precipitate increased with a power law oft 0.37 while the crystallite grew as t 0.236 . (author)

  8. Fundamentals of neutron scattering by condensed matter

    Energy Technology Data Exchange (ETDEWEB)

    Scherm, R. [Institut Max von Laue - Paul Langevin (ILL), 38 - Grenoble (France)

    1996-12-31

    The purpose of this introductory lecture is to give the basic facts about the scattering of neutrons by condensed matter. This lecture is restricted to nuclear scattering, whereas magnetic scattering will be dealt with in an other course. Most of the formalism, however, can also be easily extended to magnetic scattering. (author) 17 figs., 3 tabs., 10 refs.

  9. Lectures on neutron scattering techniques: 1

    International Nuclear Information System (INIS)

    Carlile, C.J.

    1988-08-01

    The lecture on the production of neutrons was presented at a Summer School on neutron scattering, Rome, 1986. A description is given of the production of neutrons by natural radioactive sources, fission, and particle accelerator sources. Modern neutron sources with high intensities are discussed including the ISIS pulsed neutron source at the Rutherford Appleton Laboratory and the High Flux Reactor at the Institut Laue Langevin. (U.K.)

  10. Neutron scattering on magnetic surfaces

    International Nuclear Information System (INIS)

    Ott, F.

    2007-01-01

    During the early eighties, advanced techniques for the deposition of ultra-thin metal films were developed. The combination of different types of materials gave rise to new physical phenomena such as the magnetic exchange coupling in superlattices or the exchange bias between ferro and anti-ferro layers. New types of heterostructures combining magnetic oxides, insulating oxides or magnetic semiconductors are still being developed. Alongside the fabrication of these new meta-materials made of thin films stacking, polarized neutron reflectometry has emerged as a routine tool for the characterization of magnetic hetero-structures. In the recent years, the new developments of polarized reflectivity have been connected to the study of micro- and nano-structures, especially micro-magnetic structures in multilayers. The technique of off-specular scattering has been developed for the study of the roughness or the micro magnetism at a micro metric scale. For the study of nano-metric structures, in the range below 100 nm, grazing incidence Small Angle Scattering is being considered. In thin films, the volume of magnetic matter is very small but nevertheless, diffraction experiments can be performed owing to the good performances of modern neutron spectrometers

  11. Progress report on neutron scattering at JAERI

    Energy Technology Data Exchange (ETDEWEB)

    Morii, Yukio [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    2000-10-01

    Progress in neutron scattering experiments at Japan Atomic Energy Research Institute for the year 1997-1998 is reported in brief. The superconducting gap was discovered in the spin excitation spectra of a heavy fermion superconductor UPd{sub 2}Al{sub 3}, which proved the superconductivity of this compound to be due to magnetic origin. The magnetic and superconducting order parameter was found in UPd{sub 2}Al{sub 3}, UNi{sub 2}Al{sub 3}, UPt{sub 3} and URu{sub 2}Si{sub 2}. It was concluded from this result that the coupling of the order parameter would be a characteristic property in heavy fermion superconductors. The correlation between strong magnetic interaction and the superconducting transition under high pressure was indicated from spin excitation in the strongly correlated electron system of a ladder material (Sr,Ca){sub 14}Cu{sub 24}O{sub 41}. The magnetic flux structure in a Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+{delta}} superconductor was examined by SANS (small angle neutron scattering) to observe the decomposition of the flux lines. A liquid-He-free dilution refrigerator was developed for neutron scattering experiments at ultralow temperature. The coherent scattering length of the {sup 69}Ga and {sup 71}Ga was evaluated by use of the apparatus for precise neutron optics. The structure of hen egg-white Lysozyne was investigated in detail. Detailed research report for the year 1997-1998 was published in the JAERI-Review 99-003. (Y. Kazumata)

  12. Study of material science by neutron scattering

    International Nuclear Information System (INIS)

    Kim, H.J.; Yoon, B.K.; Cheon, B.C.; Lee, C.Y.; Kim, C.S.

    1980-01-01

    To develop accurate methods of texture measurement in metallic materials by neutron diffraction, (100),(200),(111) and (310) pole figures have been measured for the oriented silicon steel sheet, and currently study of correction methods for neutron absorption and extinction effects are in progress. For quantitative analysis of texture of polycrystalline material with a cubic structure, a software has been developed to calculate inverse pole figures for arbitrary direction specified in the speciman as well as pole figures for arbitrary chosen crystallographic planes from three experimental pole figures. This work is to be extended for the calculation of three dimensional orientation distribution function and for the evaluation of errors in the quantitative analysis of texture. Work is also for the study of N-H...O hydrogen bond in amino acid by observing molecular motions using neutron inelastic scattering. Measurement of neutron inelastic scattering spectrum of L-Serine is completed at 100 0 K and over the energy transfer range of 20-150 meV. (KAERI INIS Section)

  13. Application of neutron scattering in polymers

    International Nuclear Information System (INIS)

    Han, C.C.

    2003-01-01

    Full text: Neutron scattering offers many opportunities in sciences and technology. This is particularly true in the field of polymer sciences and materials. It is mainly because that the scattering length scales (q -1 ) and scattering contrast (scattering cross-sections) makes neutron a perfect tool for polymer studies. Several examples will be used to illustrate the importance of the small angle neutron scattering and the neutron reflection studies in polymer physics. These include the determination of phase diagram, interaction parameter, and spinodal decomposition kinetics by SANS. In the dynamics area, examples will be given to illustrate the critical temperature shift and mixing of polymer blends under shear flow. Also, the confinement effect on the phase separated structure of polymer blend films will be used to demonstrate the importance of the neutron reflectivity measurement

  14. Neutron imaging and small angle neutron scattering instruments at KUR

    International Nuclear Information System (INIS)

    Saito, Yasushi; Oba, Yojiro; Hino, Masahiro

    2015-01-01

    We review the neutron imaging (NI) and small-angle neutron scattering (SANS) instruments at KUR, Kumatori, Osaka, Japan. There are two NI and one SANS instruments. The both instruments are compact and used flexibly. Some challenging experiments taking advantage of low neutron fluence are described. The feature of KUR is also described briefly. (author)

  15. Multiple magnetic scattering in small-angle neutron scattering of Nd–Fe–B nanocrystalline magnet

    Science.gov (United States)

    Ueno, Tetsuro; Saito, Kotaro; Yano, Masao; Ito, Masaaki; Shoji, Tetsuya; Sakuma, Noritsugu; Kato, Akira; Manabe, Akira; Hashimoto, Ai; Gilbert, Elliot P.; Keiderling, Uwe; Ono, Kanta

    2016-01-01

    We have investigated the influence of multiple scattering on the magnetic small-angle neutron scattering (SANS) from a Nd–Fe–B nanocrystalline magnet. We performed sample-thickness- and neutron-wavelength-dependent SANS measurements, and observed the scattering vector dependence of the multiple magnetic scattering. It is revealed that significant multiple scattering exists in the magnetic scattering rather than the nuclear scattering of Nd–Fe–B nanocrystalline magnet. It is considered that the mean free path of the neutrons for magnetic scattering is rather short in Nd–Fe–B magnets. We analysed the SANS data by the phenomenological magnetic correlation model considering the magnetic microstructures and obtained the microstructural parameters. PMID:27321149

  16. Multiple magnetic scattering in small-angle neutron scattering of Nd-Fe-B nanocrystalline magnet.

    Science.gov (United States)

    Ueno, Tetsuro; Saito, Kotaro; Yano, Masao; Ito, Masaaki; Shoji, Tetsuya; Sakuma, Noritsugu; Kato, Akira; Manabe, Akira; Hashimoto, Ai; Gilbert, Elliot P; Keiderling, Uwe; Ono, Kanta

    2016-06-20

    We have investigated the influence of multiple scattering on the magnetic small-angle neutron scattering (SANS) from a Nd-Fe-B nanocrystalline magnet. We performed sample-thickness- and neutron-wavelength-dependent SANS measurements, and observed the scattering vector dependence of the multiple magnetic scattering. It is revealed that significant multiple scattering exists in the magnetic scattering rather than the nuclear scattering of Nd-Fe-B nanocrystalline magnet. It is considered that the mean free path of the neutrons for magnetic scattering is rather short in Nd-Fe-B magnets. We analysed the SANS data by the phenomenological magnetic correlation model considering the magnetic microstructures and obtained the microstructural parameters.

  17. American Conference on Neutron Scattering 2014

    International Nuclear Information System (INIS)

    Dillen, J. Ardie

    2014-01-01

    Scientists from the around the world converged in Knoxville, TN to have share ideas, present technical information and contribute to the advancement of neutron scattering. Featuring over 400 oral/poster presentations, ACNS 2014 offered a strong program of plenary, invited and contributed talks and poster sessions covering topics in soft condensed matter, hard condensed matter, biology, chemistry, energy and engineering applications in neutron physics - confirming the great diversity of science that is enabled by neutron scattering.

  18. American Conference on Neutron Scattering 2014

    Energy Technology Data Exchange (ETDEWEB)

    Dillen, J. Ardie [Materials Research Society, Warrendale, PA (United States)

    2014-12-31

    Scientists from the around the world converged in Knoxville, TN to have share ideas, present technical information and contribute to the advancement of neutron scattering. Featuring over 400 oral/poster presentations, ACNS 2014 offered a strong program of plenary, invited and contributed talks and poster sessions covering topics in soft condensed matter, hard condensed matter, biology, chemistry, energy and engineering applications in neutron physics – confirming the great diversity of science that is enabled by neutron scattering.

  19. Inelastic neutron scattering from superconducting rings

    International Nuclear Information System (INIS)

    Agafonov, A.I.

    2010-01-01

    For the first time the differential cross section for the inelastic magnetic neutron scattering by superconducting rings is derived taking account of the interaction of the neutron magnetic moment with the magnetic field generated by the superconducting current. Calculations of the scattering cross section are carried out for cold neutrons and thin film rings from type-II superconductors with the magnetic fields not exceeding the first critical field.

  20. Neutron scattering in concrete and wood

    International Nuclear Information System (INIS)

    Facure, A.; Silva, A. X.; Falcao, R. C.; Crispim, V. R.

    2006-01-01

    In this work, the energy spectra of photoneutrons, scattered by ordinary, high-density concrete and wood barriers, have been evaluated using the MCNP4B code. These spectra were calculated for different scattering angles, and for incident neutron energies varying between 0.1 and 10 MeV. The results presented are required to simulate typical photoneutron fluence, produced by medical accelerators, which is scattered by the room walls and reaches the door. It was found that the mean energy of the scattered neutrons does not depend on the scattering angle. Furthermore, it was found that the scattered neutron energies are lower in wood and baryte concrete, which indicates that these materials can be used for lining the maze walls in order to reduce neutron dose at the room door. These data will help to estimate the personal dose received by the patient and staff in radiotherapy facilities. (authors)

  1. Neutron scattering equipments in JAERI. Current status

    International Nuclear Information System (INIS)

    Hamaguchi, Yoshikazu; Minakawa, Nobuaki

    2003-01-01

    24 neutron scattering instruments are installed in the JRR-3M research reactor. Among them JAERI has 12 neutron scattering instruments. Those instruments are HRPD for high-resolution structural analysis, TAS-1 and TAS-2 for elastic and inelastic scattering and for magnetic scattering measurements by the polarized neutron, LTAS for elastic and inelastic scattering measurement at a low energy region, and for neutron device development, PNO for topography and for very small angle scattering measurement in a small Q range, NRG for neutron radiography, RESA for internal strain measurements, SANS for the molecule and semi-macroscopic magnetic structural analysis, BIX-2 and BIX-3 for the biological structural analysis research, and PGA for the research of prompt gamma-ray analysis. The university groups have 12 neutron scattering instruments. Since those instruments were installed at the period when JRR-3M was completed, about 10 years have passed. In order to match the old control systems with the progress of recent computer technologies, and peripheral equipment, numbers of instruments are being renewed. In the neutron guide hall of JRR-3M, the Ni mirror guide tube was replaced by a super mirror guide tube to increase neutron flux. The intensity of 2A flux was increased by a factor of about two. (J.P.N.)

  2. Neutron scattering and models: molybdenum

    International Nuclear Information System (INIS)

    Smith, A.B.

    1999-01-01

    A comprehensive interpretation of the fast-neutron interaction with elemental and isotopic molybdenum at energies of le 30 MeV is given. New experimental elemental-scattering information over the incident energy range 4.5 r a rrow 10 MeV is presented. Spherical, vibrational and dispersive models are deduced and discussed, including isospin, energy-dependent and mass effects. The vibrational models are consistent with the ''Lane potential''. The importance of dispersion effects is noted. Dichotomies that exist in the literature are removed. The models are vehicles for fundamental physical investigations and for the provision of data for applied purposes. A ''regional'' molybdenum model is proposed. Finally, recommendations for future work are made

  3. Neutron scattering and models : molybdenum.

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.

    1999-05-26

    A comprehensive interpretation of the fast-neutron interaction with elemental and isotopic molybdenum at energies of {le} 30 MeV is given. New experimental elemental-scattering information over the incident energy range 4.5 {r_arrow} 10 MeV is presented. Spherical, vibrational and dispersive models are deduced and discussed, including isospin, energy-dependent and mass effects. The vibrational models are consistent with the ''Lane potential''. The importance of dispersion effects is noted. Dichotomies that exist in the literature are removed. The models are vehicles for fundamental physical investigations and for the provision of data for applied purposes. A ''regional'' molybdenum model is proposed. Finally, recommendations for future work are made.

  4. German neutron scattering conference. Programme and abstracts

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas (ed.)

    2012-07-01

    The German Neutron Scattering Conference 2012 - Deutsche Neutronenstreutagung DN 2012 offers a forum for the presentation and critical discussion of recent results obtained with neutron scattering and complementary techniques. The meeting is organized on behalf of the German Committee for Research with Neutrons - Komitee Forschung mit Neutronen KFN - by the Juelich Centre for Neutron Science JCNS of Forschungszentrum Juelich GmbH. In between the large European and international neutron scattering conferences ECNS (2011 in Prague) and ICNS (2013 in Edinburgh), it offers the vibrant German and international neutron community an opportunity to debate topical issues in a stimulating atmosphere. Originating from ''BMBF Verbundtreffen'' - meetings for projects funded by the German Federal Ministry of Education and Research - this conference series has a strong tradition of providing a forum for the discussion of collaborative research projects and future developments in the field of research with neutrons in general. Neutron scattering, by its very nature, is used as a powerful probe in many different disciplines and areas, from particle and condensed matter physics through to chemistry, biology, materials sciences, engineering sciences, right up to geology and cultural heritage; the German Neutron Scattering Conference thus provides a unique chance for exploring interdisciplinary research opportunities. It also serves as a showcase for recent method and instrument developments and to inform users of new advances at neutron facilities.

  5. German neutron scattering conference. Programme and abstracts

    International Nuclear Information System (INIS)

    Brueckel, Thomas

    2012-01-01

    The German Neutron Scattering Conference 2012 - Deutsche Neutronenstreutagung DN 2012 offers a forum for the presentation and critical discussion of recent results obtained with neutron scattering and complementary techniques. The meeting is organized on behalf of the German Committee for Research with Neutrons - Komitee Forschung mit Neutronen KFN - by the Juelich Centre for Neutron Science JCNS of Forschungszentrum Juelich GmbH. In between the large European and international neutron scattering conferences ECNS (2011 in Prague) and ICNS (2013 in Edinburgh), it offers the vibrant German and international neutron community an opportunity to debate topical issues in a stimulating atmosphere. Originating from ''BMBF Verbundtreffen'' - meetings for projects funded by the German Federal Ministry of Education and Research - this conference series has a strong tradition of providing a forum for the discussion of collaborative research projects and future developments in the field of research with neutrons in general. Neutron scattering, by its very nature, is used as a powerful probe in many different disciplines and areas, from particle and condensed matter physics through to chemistry, biology, materials sciences, engineering sciences, right up to geology and cultural heritage; the German Neutron Scattering Conference thus provides a unique chance for exploring interdisciplinary research opportunities. It also serves as a showcase for recent method and instrument developments and to inform users of new advances at neutron facilities.

  6. Interaction of methanol with the flexible metal-organic framework MIL-53(Fe) observed by inelastic neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Munn, Alexis S. [Department of Chemistry, University of Warwick, Coventry CV4 7AL (United Kingdom); Ramirez-Cuesta, Anibal J. [ISIS Facility, STFC Rutherford Appleton Laboratory, Chilton OX11 0QX (United Kingdom); Millange, Franck [Institut Lavoisier Versailles, Université de Versailles, UMR 8180, 78035 Versailles (France); Walton, Richard I., E-mail: r.i.walton@warwick.ac.uk [Department of Chemistry, University of Warwick, Coventry CV4 7AL (United Kingdom)

    2013-12-12

    Highlights: • A spectroscopic signature of guest-induced swelling of a flexible MOF has been identified. • Librations of the linker contribute to pore opening of the MOF structure. • Complementary in situ powder XRD shows changes in long-range order during guest uptake. - Abstract: In situ powder X-ray diffraction and thermogravimetry show that the iron(III) carboxylate material MIL-53(Fe) expands in two steps upon exposure to methanol vapour to give a ‘half open’ phase and then a fully expanded structure; these correspond to the uptake of one and two molar equivalents of methanol, respectively. This knowledge allows interpretation of inelastic neutron scattering (INS) spectra, measured using TOSCA at ISIS, of the solid loaded with various amounts of water, methanol or d3-methanol (CD{sub 3}OH), aided also by DFT simulation of INS spectra of the analogous MIL-53(Al) structure. The key signature of the expansion and contraction of the structure is the shift of bands in the 400 cm{sup −1} region: these are assigned as due to the librations of the terephthalate rings, involving motions that result in distortion of the aromatic ring and a rocking motion of the aromatic ring about the bonds to the carboxylate groups.

  7. Interaction of methanol with the flexible metal-organic framework MIL-53(Fe) observed by inelastic neutron scattering

    International Nuclear Information System (INIS)

    Munn, Alexis S.; Ramirez-Cuesta, Anibal J.; Millange, Franck; Walton, Richard I.

    2013-01-01

    Highlights: • A spectroscopic signature of guest-induced swelling of a flexible MOF has been identified. • Librations of the linker contribute to pore opening of the MOF structure. • Complementary in situ powder XRD shows changes in long-range order during guest uptake. - Abstract: In situ powder X-ray diffraction and thermogravimetry show that the iron(III) carboxylate material MIL-53(Fe) expands in two steps upon exposure to methanol vapour to give a ‘half open’ phase and then a fully expanded structure; these correspond to the uptake of one and two molar equivalents of methanol, respectively. This knowledge allows interpretation of inelastic neutron scattering (INS) spectra, measured using TOSCA at ISIS, of the solid loaded with various amounts of water, methanol or d3-methanol (CD 3 OH), aided also by DFT simulation of INS spectra of the analogous MIL-53(Al) structure. The key signature of the expansion and contraction of the structure is the shift of bands in the 400 cm −1 region: these are assigned as due to the librations of the terephthalate rings, involving motions that result in distortion of the aromatic ring and a rocking motion of the aromatic ring about the bonds to the carboxylate groups

  8. Oedometric Small-Angle Neutron Scattering: In Situ Observation of Nanopore Structure During Bentonite Consolidation and Swelling in Dry and Hydrous CO2 Environments.

    Science.gov (United States)

    Dewers, Thomas A; Heath, Jason E; Bryan, Charles R; Mang, Joseph T; Hjelm, Rex P; Ding, Mei; Taylor, Mark

    2018-03-20

    Results of oedometric consolidation experiments linked with small-angle neutron scattering (SANS) measurements are presented, using SWy-2 Wyoming bentonite clay in dry and water-bearing N 2 and CO 2 atmospheres. Oedometric SANS involves deforming a porous sample under uniaxial strain conditions with applied axial force and internal pore pressure control, and combines with SANS for in situ observation of pore structure evolution and interaction. Scattering from both interlayer (clay intra-aggregate) and free (interaggregate) pores is observed, showing decreasing pore size with dry consolidation and interactions between interlayer and free pore types with swelling and consolidation. Introduction of dry liquid CO 2 at zero effective stress (axial stress minus pore pressure) produces large shifts in interlayer scatterers, but is reversible back to pre-CO 2 levels upon decreasing pore pressure and increasing effective stress. Introduction of wet liquid CO 2 , conversely, produces large but irreversible changes in interlayer scatterers, which are interpreted to be the combined result of CO 2 and H 2 O intercalation under hydrostatic conditions, but which diminish with application of effective pressure and consolidation to higher bentonite dry densities. Consideration of CO 2 intercalation in smectite-bearing CO 2 caprocks needs to include effects of both water and nonhydrostatic stress.

  9. Fluence-compensated down-scattered neutron imaging using the neutron imaging system at the National Ignition Facility.

    Science.gov (United States)

    Casey, D T; Volegov, P L; Merrill, F E; Munro, D H; Grim, G P; Landen, O L; Spears, B K; Fittinghoff, D N; Field, J E; Smalyuk, V A

    2016-11-01

    The Neutron Imaging System at the National Ignition Facility is used to observe the primary ∼14 MeV neutrons from the hotspot and down-scattered neutrons (6-12 MeV) from the assembled shell. Due to the strong spatial dependence of the primary neutron fluence through the dense shell, the down-scattered image is convolved with the primary-neutron fluence much like a backlighter profile. Using a characteristic scattering angle assumption, we estimate the primary neutron fluence and compensate the down-scattered image, which reveals information about asymmetry that is otherwise difficult to extract without invoking complicated models.

  10. Neutron scattering on magnetic surfaces

    Science.gov (United States)

    Ott, Frédéric

    2007-09-01

    During the early 1980s, advanced techniques for the deposition of ultra-thin metal films were developed. The combination of different types of materials gave rise to new physical phenomena such as the magnetic exchange coupling in superlattices or the exchange bias between ferro and anti-ferro layers. The field was very active because of the associated industrial applications in magnetic field sensors. New types of heterostructures combining magnetic oxides, insulating oxides or magnetic semiconductors are still being developed. Alongside the fabrication of these new meta-materials made of thin films stacking, polarized neutron reflectometry has emerged as a routine tool for the characterization of magnetic hetero-structures. In the recent years, the new developments of polarized reflectivity have been connected to the study of micro and nanostructures, especially micromagnetic structures in multilayers. The technique of off-specular scattering has been developed for the study of the roughness or the micromagnetism at a micrometric scale. For the study of nanometric structures, in the range below 100 nm, grazing incidence Small Angle Scattering is being considered. To cite this article: F. Ott, C. R. Physique 8 (2007).

  11. Neutron scattering from quantum liquids

    International Nuclear Information System (INIS)

    Cowley, R.A.

    1976-01-01

    Recent neutron scattering measurements on the quantum liquids 4 He and 3 He are described. In the Bose superfluid there is a well-defined excitation for wave vectors less than 3.6 A -1 . In the Fermi liquid measurements are much more difficult because of the large absorption cross section, but measurements at the Institute Laue-Langevin have shown that there are no well-defined excitations at 0.63 0 K for wave vectors between 1.0 and 2.6 A -1 . The difference between these results is due to the existence of particle-hole excitations in the Fermi liquid into which collective excitations can decay. Because of the simplicity of the excitations in 4 He, it has become a testing ground for the effects of the interactions between the excitations. Measurements are described which show that while roton-roton interactions are attractive at small wave vectors they are repulsive at larger wave vectors. The scattering at large momentum transfer in 4 He has been measured, but its interpretation is still open to question

  12. Neutron scattering for polymer science at reactor and spallation sources

    International Nuclear Information System (INIS)

    Koizumi, Satoshi

    2009-01-01

    The neutron, having a variety of intrinsic properties (no charge, mass, spin and magnetic moment), is a marvelous probe to explore the structure of polymer materials. We report characteristic methods of small-angle neutron-neutron scattering (SANS), which are performed at reactor and spallation sources. A time-of-flight method at a spallation source employs neutrons of wide wavelength distribution in order to observe a wide length scale from angstrom to nanometer (from small-angle to wide-angle scattering regions). At a reactor source, on the other hand, a monochromatic neutron is utilized for precise observation of ultra-small-angle scattering, corresponding to a range from nano to micron meters. By combining both facilities, polymer science is further improved into exploring hierarchical structures in polymeric materials. (author)

  13. Neutron scattering in Indonesia. Country report

    International Nuclear Information System (INIS)

    Ikram, Abarrul

    2000-01-01

    Neutron scattering in Indonesia is still alienated due to some reasons and conditions which are discussed. The reactor and its latest operation mode are also described. The neutron beam facilities which include one diffractometer for residual stress measurement, one diffractometer for single crystal structural determination and texture measurement, one high resolution powder diffractometer, one neutron radiography facility, one triple axis spectrometer, one small angle neutron scattering spectrometer and one high resolution small angle neutron scattering spectrometer were presented briefly together with improvements of neutron intensities at some spectrometers in connection with the setting of main beam shutter position. Special attention is given for four instruments mostly related to this workshop. Their performances and problems faced in the past 9 months are presented as well as the future plan for refurbishment and development. (author)

  14. Neutron scattering studies of carbon nanotubes

    International Nuclear Information System (INIS)

    Rols, S.; Anglaret, E.; Sauvajol, J.L.

    1999-01-01

    Complete text of publication follows. Neutron scattering is shown to be a powerful tool for the study of both the structure and the vibrational properties of nanotubes. Comparison between the neutron diffraction data and calculations on finite-size bundles of single wall carbon nanotubes (SWNT) allow to estimate the mean-tube diameter, the tube diameter distribution as well as the mean-size of the bundles. The technique is complementary of x-ray diffraction since it allows a characterization of large amount of samples. A good agreement is found with structural information obtained in electron microscopy and Raman spectroscopy. Recent results probing the evolution of the diffraction spectra of SWNT samples with temperature and pressure will be presented. Moreover, the efficiency of TOF neutron scattering is demonstrated to study the phonon density of states of SWNT. Original features are recorded in the frequency range 6 to 60 meV and assigned to intratube excitations on the basis of calculations for (10,10) SWNT. At lower frequencies (below 6 meV), a peculiar frequency-dependence is observed of the density of states assigned to some contribution due to intratube and intertube excitations with peculiar q-dispersions. Preliminary results on multi-wall nanotubes will also be presented. (author)

  15. Quantum effects in deep inelastic neutron scattering

    International Nuclear Information System (INIS)

    Mayers, J.

    1989-07-01

    In the Impulse Approximation (IA), which is used to interpret deep inelastic neutron scattering (DINS) measurements, it is assumed both that the target system can be treated as a gas of free atoms and that the struck atom recoils freely after the collision with the neutron. Departures from the IA are generally attributed to final state effects (FSE), which are due to the inaccuracy of the latter assumption. However it is shown that even when FSE are neglected, significant departures from the IA occur at low temperatures due to inaccuracies in the former assumption. These are referred to as initial state effects (ISE) and are due to the quantum nature of the initial state. Comparison with experimental data and exactly soluble models shows that ISE largely account for observed asymmetries and peak shifts in the neutron scattering function S(q,ω), compared with the IA prediction. It is shown that when FSE are neglected, ISE can also be neglected when either the momentum transfer or the temperature is high. Finally it is shown that FSE should be negligible at high momentum transfers in systems other than quantum fluids and that therefore in this regime the IA is reached in such systems. (author)

  16. Studies of the dynamic properties of materials using neutron scattering

    International Nuclear Information System (INIS)

    Lovesey, S.W.; Windsor, C.G.

    1985-09-01

    The dynamic properties of materials using the neutron scattering technique is reviewed. The basic properties of both nuclear scattering and magnetic scattering are summarized. The experimental methods used in neutron scattering are described, along with access to neutron sources, and neutron inelastic instruments. Applied materials science using inelastic neutron scattering; rotational tunnelling of a methyl group; molecular diffusion from quasi-elastic scattering; and the diffusion of colloidal particles and poly-nuclear complexes; are also briefly discussed. (U.K.)

  17. Monte Carlo simulations of neutron scattering instruments

    International Nuclear Information System (INIS)

    Aestrand, Per-Olof; Copenhagen Univ.; Lefmann, K.; Nielsen, K.

    2001-01-01

    A Monte Carlo simulation is an important computational tool used in many areas of science and engineering. The use of Monte Carlo techniques for simulating neutron scattering instruments is discussed. The basic ideas, techniques and approximations are presented. Since the construction of a neutron scattering instrument is very expensive, Monte Carlo software used for design of instruments have to be validated and tested extensively. The McStas software was designed with these aspects in mind and some of the basic principles of the McStas software will be discussed. Finally, some future prospects are discussed for using Monte Carlo simulations in optimizing neutron scattering experiments. (R.P.)

  18. High pressure cell for neutron scattering experiments

    International Nuclear Information System (INIS)

    Shinde, A.B.; Krishna, P.S.R.; Paranjpe, S.K.; Vaidya, S.N.

    1997-01-01

    We report here the design and fabrication of a high pressure clamped cell using EN45 steel for neutron scattering experiments up to 15 kbar. The pressure cell geometry allows detection of scattered neutrons in a plane over an angular range of 90 deg. The cell can be used for both elastic and inelastic scattering measurements on polycrystalline materials and disordered materials. The volume of the sample region is about 400 mm 3 . Preliminary results obtained from neutron diffraction of ND 4 I and KNO 3 are presented. (author)

  19. Techniques in high pressure neutron scattering

    CERN Document Server

    Klotz, Stefan

    2013-01-01

    Drawing on the author's practical work from the last 20 years, Techniques in High Pressure Neutron Scattering is one of the first books to gather recent methods that allow neutron scattering well beyond 10 GPa. The author shows how neutron scattering has to be adapted to the pressure range and type of measurement.Suitable for both newcomers and experienced high pressure scientists and engineers, the book describes various solutions spanning two to three orders of magnitude in pressure that have emerged in the past three decades. Many engineering concepts are illustrated through examples of rea

  20. Neutron scattering studies of solid electrolytes

    International Nuclear Information System (INIS)

    Shapiro, S.M.

    1976-01-01

    The role which neutron scattering can play in determining the nature of the disorder and the conducting mechanism in the solid electrolytes is discussed. First, some of the general formalism for elastic and inelastic neutron scattering is reviewed, and the quantities which can be measured are pointed out. Then the application of neutron scattering to the studies of three different problems is examined; the anion disorder in the fluorite system, the dynamical behavior in beta-alumina, and the cation diffusion in αAgI are discussed. 8 figures

  1. Current status of neutron scattering in Thailand

    International Nuclear Information System (INIS)

    Kornduangkaeo, Areeratt; Pongkasem, Somchai; Putchar, Suriya; Ampornrat, Pantip; Kajornrith, Varavuth; Chamchang, Jipawat

    2006-01-01

    The current neutron powder diffractometer at the Thai Research Reactor-1/Modification 1 (TRR-1/M1) has been modified from the obsolete neutron diffractometer which had been used during 1968-1975. The upgraded diffractometer has medium resolution and is appropriate for studying samples with small unit cell dimensions and training university students in the field of neutron scattering. This paper describes the current activities of neutron scattering research in Thailand, the current status of a new research reactor project at Ongkarak for enlarging the perspectives of its utilization in the future as well as the organizational reformation of the Office of Atomic Energy for Peace (OAEP). (author)

  2. Observation of Ortho-III correlations by neutron and hard x-ray scattering in an untwinned YBa2Cu3O6.77 single crystal

    DEFF Research Database (Denmark)

    Schleger, P.; Casalta, H.; Hadfield, R.

    1995-01-01

    We present measurements of Ortho-III phase correlations in an untwinned single crystal of YBa2Cu3O6.77 by neutron scattering and the novel method of hard (95 keV) X-ray scattering. The Ortho-III ordering is essentially two-dimensional, exhibiting Lorentzian peak shapes in the a-b plane. At room...

  3. Phase sensitive small angle neutron scattering

    Science.gov (United States)

    Brok, Erik; Majkrzak, Charles F.; Krycka, Kathryn

    It is a well-known problem that information about the scattered wave is lost in scattering experiments because the measured quantity is the modulus squared of the complex wave function. This ''phase problem'' leads to ambiguity in determining the physical properties of the scattering sample. Small angle neutron scattering (SANS) is a useful technique for determining the structure of biomolecules, in particular proteins that cannot be crystallized and studied with x-ray crystallography. However, because the biomolecules are usually suspended in a liquid the observed scattering is an average of all possible orientations, making it difficult to obtain three dimensional structural information. In a proposed method polarized SANS and magnetic nanoparticle references attached to the sample molecules is used to obtain phase sensitive structural information and simultaneously circumvent the problem of orientational averaging (Majkrzak et al. J. Appl. Cryst. 47, 2014) If realized and perfected the technique is very promising for unambiguous determination of the three dimensional structure of biomolecules. We demonstrate the principles of our method and show the first experimental data obtained on a simple test system consisting of core shell magnetic nanoparticles.

  4. Advantages of neutron scattering for biological structure analysis

    International Nuclear Information System (INIS)

    Schoenborn, B.P.

    1975-01-01

    The advantages and disadvantages of neutron scattering for protein crystallography, scattering from oriented systems, and solution scattering are summarized. Techniques for minimizing the disadvantages are indicated

  5. Observation of subtle dynamic transitions by a combination of neutron scattering, X-ray diffraction and DSC: a case study of the monoclinic L-cysteine.

    Science.gov (United States)

    Bordallo, Heloisa N; Boldyreva, Elena V; Fischer, Jennifer; Koza, Michael Marek; Seydel, Tilo; Minkov, Vasily S; Drebushchak, Valery A; Kyriakopoulos, Antonios

    2010-05-01

    The paper illustrates the benefit of combining several experimental techniques (incoherent elastic and inelastic neutron scattering, DSC, and X-ray diffraction) to study subtle dynamic transitions in a biologically important system, probing a broad time (frequency) range of the molecular motions in a wide temperature interval of 2-300K. As a case study the crystalline form (a monoclinic polymorph) of l-cysteine ((+)NH(3)-CH(CH(2)SH)-COO(-)) - an essential amino acid - has been selected. Crystals of amino acids are widely used to mimic important structural and dynamic features of peptides. The conformational lability of cysteine and the dynamics of the thiol-side chains are known to account for various phase transitions in the crystalline state and for the conformational transitions important for the biological function in the peptides. The effect of temperature on the monoclinic polymorph of l-cysteine, metastable at ambient conditions, has been studied for the first time. A dynamical transition at about 150K, marking a crossover of the molecular fluctuations between harmonic and non-harmonic dynamical regimes, was evidenced by evaluating the evolution of the mean-square displacement obtained from the elastic fixed window approach using the backscattering spectrometer IN10 located at the ILL. Although this transition does not manifest itself in the DSC, it was clearly observed by incoherent inelastic neutron scattering. By analyzing the dynamical susceptibility contribution (chi''(omega)) obtained using IN6 also at ILL we were able to evidence another relaxation process at a different time scale. The disordered soft l-cysteine structure has an excess of inelastic scattering at about 3meV, analogous to the "boson peak" observed in glass-like materials and proteins. High-precision X-ray diffraction has revealed an anomaly in the changes of selected unit cell parameters and volume at about 240K.

  6. Complex Magnetic Systems Studied with Neutron Scattering

    DEFF Research Database (Denmark)

    Jacobsen, Henrik

    was conrmed with further neutron scattering experiments. An apparent discontinuity in the dispersion of the dynamic stripes in the limit of vanishing energy transfer was found in violation of Goldstone's theorem. Detailed simulations of the experiment showed that this eect could not be explained......This thesis presents work done during my PhD jointly at the Niels Bohr Institute and the European Spallation Source. The thesis can be divided into four parts: introduction, magnetic nanoparticles, frustrated materials and superconductivity. The rst part is an introduction to magnetism and neutron....... This leads to absence of long range order even at very low temperatures and to fascinating new states of matter. Neutron scattering is the main experimental tool used in this thesis. The advantage of neutron scattering is that the neutron is sensitive to both magnetic order and magnetic dynamics...

  7. Neutron Scattering studies of magnetic molecular magnets

    International Nuclear Information System (INIS)

    Chaboussant, G.

    2009-01-01

    This work deals with inelastic neutron scattering studies of magnetic molecular magnets and focuses on their magnetic properties at low temperature and low energies. Several molecular magnets (Mn 12 , V 15 , Ni 12 , Mn 4 , etc.) are reviewed. Inelastic neutron scattering is shown to be a perfectly suited spectroscopy tool to -a) probe magnetic energy levels in such systems and -b) provide key information to understand the quantum tunnel effect of the magnetization in molecular spin clusters. (author)

  8. Thermal-neutron multiple scattering: critical double scattering

    International Nuclear Information System (INIS)

    Holm, W.A.

    1976-01-01

    A quantum mechanical formulation for multiple scattering of thermal-neutrons from macroscopic targets is presented and applied to single and double scattering. Critical nuclear scattering from liquids and critical magnetic scattering from ferromagnets are treated in detail in the quasielastic approximation for target systems slightly above their critical points. Numerical estimates are made of the double scattering contribution to the critical magnetic cross section using relevant parameters from actual experiments performed on various ferromagnets. The effect is to alter the usual Lorentzian line shape dependence on neutron wave vector transfer. Comparison with corresponding deviations in line shape resulting from the use of Fisher's modified form of the Ornstein-Zernike spin correlations within the framework of single scattering theory leads to values for the critical exponent eta of the modified correlations which reproduce the effect of double scattering. In addition, it is shown that by restricting the range of applicability of the multiple scattering theory from the outset to critical scattering, Glauber's high energy approximation can be used to provide a much simpler and more powerful description of multiple scattering effects. When sufficiently close to the critical point, it provides a closed form expression for the differential cross section which includes all orders of scattering and has the same form as the single scattering cross section with a modified exponent for the wave vector transfer

  9. Progress report on neutron scattering at JAERI

    Energy Technology Data Exchange (ETDEWEB)

    Morii, Yukio [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1998-10-01

    In the first half of fiscal year 1997, JRR-3M was operated for 97 days followed by a long term shut down for its annual maintenance. Three days were lost out of 100 scheduled operation days, due to a trouble in irradiation facility. Neutron scattering research activities at the JRR-3M have been extended from that of fiscal year 1996. In the Research Group for Quantum Condensed Matter System, experimental study under high pressures, low temperatures and high fields as well as coupling of these conditions were planned to find new quantum condensed matter systems. And, obtained experimental results were immediately provided to theorists for their investigations. In cooperation with new group, Research Group for Neutron Scattering of Strongly Correlated Electron Systems and Research Group for Neutron Scattering at Ultralow Temperatures were carrying neutron scattering experiments at JRR-3M. Research Group for Neutron Crystallography in Biology had opened a way for investigating biomatter neutron diffraction research with high experimental accuracy by growing a millimeter-class large single crystal. In fiscal year 1997, 39 research projects were conducted by these four groups and other staffs in JAERI, 27 projects collaborated with university researchers and 3 projects collaborated with private enterprises were also conducted as complementary researches. 2117 days of machine times were requested to use 8 neutron scattering instruments this year, which corresponded to 1.51 times larger than those planned at its beginning. (G.K.)

  10. SANS-1: Small angle neutron scattering

    Directory of Open Access Journals (Sweden)

    André Heinemann

    2015-08-01

    Full Text Available The new small angle scattering instrument SANS-1, jointly operated by the Technische Universität München and GEMS, Helmholtz-Zentrum Geesthacht, has completed commissioning and is in regular user service (Gilles et al., 2006. SANS-1 is located at the end of neutron guide NL4a in the Neutron Guide Hall West.

  11. SANS-1: Small angle neutron scattering

    OpenAIRE

    Heinemann, André; Mühlbauer, Sebastian

    2015-01-01

    The new small angle scattering instrument SANS-1, jointly operated by the Technische Universität München and GEMS, Helmholtz-Zentrum Geesthacht, has completed commissioning and is in regular user service (Gilles et al., 2006). SANS-1 is located at the end of neutron guide NL4a in the Neutron Guide Hall West.

  12. Lectures on magnetism and neutron scattering

    International Nuclear Information System (INIS)

    Gunn, J.M.F.

    1983-12-01

    The paper contains six lectures given to the Neutron Division of the Rutherford Appleton laboratory in 1983. The aim was to explain fundamental physics of neutron scattering and basic magnetism to the non-specialist scientist. The text includes: origin of neutron's magnetic moment and spin-dependent interactions with electrons and nuclei, why are solids magnetic, magnetic anistropy and domain structure, phenomenological spin waves, magnetic phase transitions and electronic excitations in magnets. (U.K.)

  13. Introduction to neutron scattering. Lecture notes of the introductory course

    Energy Technology Data Exchange (ETDEWEB)

    Furrer, A. [ed.

    1996-12-31

    These proceedings enclose ten papers presented at the 1. European Conference on Neutron scattering (ECNS `96). The aim of the Introductory Course was fourfold: - to learn the basic principles of neutron scattering, - to get introduced into the most important classes of neutron scattering instruments, -to learn concepts and their transformation into neutron scattering experiments in various fields of condensed matter research, - to recognize the limitations of the neutron scattering technique as well as to the complementarity of other methods. figs., tabs., refs.

  14. Introduction to neutron scattering. Lecture notes of the introductory course

    International Nuclear Information System (INIS)

    Furrer, A.

    1996-01-01

    These proceedings enclose ten papers presented at the 1. European Conference on Neutron scattering (ECNS '96). The aim of the Introductory Course was fourfold: - to learn the basic principles of neutron scattering, - to get introduced into the most important classes of neutron scattering instruments, -to learn concepts and their transformation into neutron scattering experiments in various fields of condensed matter research, - to recognize the limitations of the neutron scattering technique as well as to the complementarity of other methods. figs., tabs., refs

  15. Superfluidity, Bose condensation and neutron scattering in liquid 4He

    International Nuclear Information System (INIS)

    Silver, R.N.

    1997-01-01

    The relation between superfluidity and Bose condensation in 4 He provides lessons that may be valuable in understanding the strongly correlated electron system of high T c superconductivity. Direct observation of a Bose condensate in the superfluid by deep inelastic neutron scattering measurements has been attempted over many years. But the impulse approximation, which relates momentum distributions to neutron scattering structure functions, is broadened by final state effects. Nevertheless, the excellent quantitative agreement between ab initio quantum many body theory and high precision neutron experiments provides confidence in the connection between superfluidity and Bose condensation

  16. Grazing incidence polarized neutron scattering in reflection ...

    Indian Academy of Sciences (India)

    During the year 1980, polarized neutron scattering technique came into being as an ana- lytic tool to measure the ... The discovery of antiferromagnetic coupling was critical to the discovery of GMR, pro- viding as it did ..... Here we consider the incident wave vector ki making an angle αi in the x–z plane while the scattered ...

  17. A small-angle neutron scattering study

    Indian Academy of Sciences (India)

    400Da [9]. Low-angle X-ray scattering [10] and neutron scattering [11] also in- dicated serum albumin to be a prolate ellipsoid. However, studies using 1H NMR indicated that a prolate structure was unlikely; rather a heart-shaped structure was proposed [12]. The shape of albumin reveals a heart-shaped molecule that can.

  18. Neutron Scattering in Biology Techniques and Applications

    CERN Document Server

    Fitter, Jörg; Katsaras, John

    2006-01-01

    The advent of new neutron facilities and the improvement of existing sources and instruments world wide supply the biological community with many new opportunities in the areas of structural biology and biological physics. The present volume offers a clear description of the various neutron-scattering techniques currently being used to answer biologically relevant questions. Their utility is illustrated through examples by some of the leading researchers in the field of neutron scattering. This volume will be a reference for researchers and a step-by-step guide for young scientists entering the field and the advanced graduate student.

  19. Neutron scattering: Revealing the structure of matter

    International Nuclear Information System (INIS)

    Zeyher, A.

    1996-01-01

    Neutrons are being used to explore materials and biological molecules in a growing number of applications, such as advanced steels and other materials, polymer films, complex molecular structures, and magnetic behavior. open-quotes Virtually all we know about the structure of the new high-transition temperature superconductors was determined using neutron scattering,close quotes said Bill Appleton, associate director for advanced materials, physical, and neutron sciences at Oak Ridge National Laboratory, in Oak Ridge, Tennessee. Neutrons are the only way to see what happens inside superconductors because of the neutron's penetrating power and its magnetic moment. Penetrating power means that neutrons can look up to several centimetres below the surface of a material without damaging it; the neutron's magnetic moment means that it is sensitive to the magnetic fields inside a material. Research in high-temperature superconductivity is only one example of the power of neutrons to illuminate, without disturbing, the structure and behavior of matter at the atomic or molecular scale. In many applications, neutron scattering serves as a complement to X-ray diffraction. In others, neutrons are the only nondestructive probe for looking inside materials or processes

  20. The hydrogen anomaly problem in neutron Compton scattering

    Science.gov (United States)

    Karlsson, Erik B.

    2018-03-01

    Neutron Compton scattering (also called ‘deep inelastic scattering of neutrons’, DINS) is a method used to study momentum distributions of light atoms in solids and liquids. It has been employed extensively since the start-up of intense pulsed neutron sources about 25 years ago. The information lies primarily in the width and shape of the Compton profile and not in the absolute intensity of the Compton peaks. It was therefore not immediately recognized that the relative intensities of Compton peaks arising from scattering on different isotopes did not always agree with values expected from standard neutron cross-section tables. The discrepancies were particularly large for scattering on protons, a phenomenon that became known as ‘the hydrogen anomaly problem’. The present paper is a review of the discovery, experimental tests to prove or disprove the existence of the hydrogen anomaly and discussions concerning its origin. It covers a twenty-year-long history of experimentation, theoretical treatments and discussions. The problem is of fundamental interest, since it involves quantum phenomena on the subfemtosecond time scale, which are not visible in conventional thermal neutron scattering but are important in Compton scattering where neutrons have two orders of magnitude times higher energy. Different H-containing systems show different cross-section deficiencies and when the scattering processes are followed on the femtosecond time scale the cross-section losses disappear on different characteristic time scales for each H-environment. The last section of this review reproduces results from published papers based on quantum interference in scattering on identical particles (proton or deuteron pairs or clusters), which have given a quantitative theoretical explanation both regarding the H-cross-section reduction and its time dependence. Some new explanations are added and the concluding chapter summarizes the conditions for observing the specific quantum

  1. BUILDING A NETWORK FOR NEUTRON SCATTERING EDUCATION

    International Nuclear Information System (INIS)

    Pynn, Roger; Baker, Shenda Mary; Louca, Despo A.; McGreevy, Robert L.; Ekkebus, Allen E.; Kszos, Lynn A.; Anderson, Ian S.

    2008-01-01

    In a concerted effort supported by the National Science Foundation, the Department of Commerce, and the Department of Energy, the United States is rebuilding its leadership in neutron scattering capability through a significant investment in U.S. neutron scattering user facilities and related instrumentation. These unique facilities provide opportunities in neutron scattering to a broad community of researchers from academic institutions, federal laboratories, and industry. However, neutron scattering is often considered to be a tool for 'experts only' and in order for the U.S. research community to take full advantage of these new and powerful tools, a comprehensive education and outreach program must be developed. The workshop described below is the first step in developing a national program that takes full advantage of modern education methods and leverages the existing educational capacity at universities and national facilities. During March 27-28, 2008, a workshop entitled 'Building a Network for Neutron Scattering Education' was held in Washington, D.C. The goal of the workshop was to define and design a roadmap for a comprehensive neutron scattering education program in the United States. Successful implementation of the roadmap will maximize the national intellectual capital in neutron sciences and will increase the sophistication of research questions addressed by neutron scattering at the nation's forefront facilities. (See Appendix A for the list of attendees, Appendix B for the workshop agenda, Appendix C for a list of references. Appendix D contains the results of a survey given at the workshop; Appendix E contains summaries of the contributed talks.) The workshop brought together U.S. academicians, representatives from neutron sources, scientists who have developed nontraditional educational programs, educational specialists, and managers from government agencies to create a national structure for providing ongoing neutron scattering education. A

  2. BUILDING A NETWORK FOR NEUTRON SCATTERING EDUCATION

    Energy Technology Data Exchange (ETDEWEB)

    Pynn, Roger [ORNL; Baker, Shenda Mary [ORNL; Louca, Despo A [ORNL; McGreevy, Robert L [ORNL; Ekkebus, Allen E [ORNL; Kszos, Lynn A [ORNL; Anderson, Ian S [ORNL

    2008-10-01

    In a concerted effort supported by the National Science Foundation, the Department of Commerce, and the Department of Energy, the United States is rebuilding its leadership in neutron scattering capability through a significant investment in U.S. neutron scattering user facilities and related instrumentation. These unique facilities provide opportunities in neutron scattering to a broad community of researchers from academic institutions, federal laboratories, and industry. However, neutron scattering is often considered to be a tool for 'experts only' and in order for the U.S. research community to take full advantage of these new and powerful tools, a comprehensive education and outreach program must be developed. The workshop described below is the first step in developing a national program that takes full advantage of modern education methods and leverages the existing educational capacity at universities and national facilities. During March 27-28, 2008, a workshop entitled 'Building a Network for Neutron Scattering Education' was held in Washington, D.C. The goal of the workshop was to define and design a roadmap for a comprehensive neutron scattering education program in the United States. Successful implementation of the roadmap will maximize the national intellectual capital in neutron sciences and will increase the sophistication of research questions addressed by neutron scattering at the nation's forefront facilities. (See Appendix A for the list of attendees, Appendix B for the workshop agenda, Appendix C for a list of references. Appendix D contains the results of a survey given at the workshop; Appendix E contains summaries of the contributed talks.) The workshop brought together U.S. academicians, representatives from neutron sources, scientists who have developed nontraditional educational programs, educational specialists, and managers from government agencies to create a national structure for providing ongoing neutron

  3. Ultra-small-angle neutron scattering. History, developments and applications

    International Nuclear Information System (INIS)

    Koizumi, Satoshi; Yamaguchi, Daisuke

    2011-01-01

    Ultra-small-angle neutron scattering (USANS), which is a scattering method observing in a q-region of q=10 -3 nm -1 , was initiated by double crystal (Bonse-Hart) method. Recently, a focusing USANS method was developed by combining a pin-hole type spectrometer and focusing lenses. These two methods, which are complementary to each other, were employed to achieve wide q-observations on microbial cellulose, actin cytoskeleton, tire, and membrane-electrolyte assembly of fuel cell. (author)

  4. Application of eV neutron scattering and eV neutron absorption techniques

    International Nuclear Information System (INIS)

    Ikeda, S.

    1989-01-01

    Intense spallation neutron sources can provide a useful eV neutron flux in the energy range 1-100 eV, which is much more intense than has ever been available from steady state sources, and makes two fruitful techniques possible. One is an eV neutron scattering technique, which allows the impulse approximation limit to be approached. The other is an eV neutron absorption technique. Both have been used to observe the motions of specific atoms in the high temperature superconducting systems La-Cu-O and Y-Ba-Cu-O. The procedure and experimental layout are given. Neutron scattering and neutron absorption spectra are presented for different temperatures. These allowed effective temperatures of atoms in the high T c materials to be found. (author)

  5. Small-angle scattering of neutrons from normal and superfluid liquid helium

    International Nuclear Information System (INIS)

    Tsipenyuk, Yu.M.; Kirichek, O.; Petrenko, O.

    2013-01-01

    The results of experiments on small-angle neutron scattering in liquid helium in the range of temperatures of 1-5 K, performed on a neutron pulse source ISIS (England), are presented. The detailed measurements of angular distribution of scattered neutrons allowed one to observe an essential change in temperature dependence of the second moment of pair correlation function (the first derivative of angular distribution at small angles of scattering). At high temperatures the angular distribution of scattered neutrons follows the classical description of small-angle scattering, but at temperatures below the l-point a quantum behavior is observed neutron-scattering by quantum fluctuations. It is experimentally confirmed that in the whole temperature range the cross-section of neutron scattering at a zero angle is determined by the classical thermodynamic fluctuations of density.

  6. New spectrometers for diffuse scattering of neutrons

    International Nuclear Information System (INIS)

    Just, W.; Schmatz, W.; Bauer, G.

    1975-01-01

    The study of defects in solids can be complemented in many cases by the diffuse scattering of X-rays, neutrons or electrons to draw information about size, symmetry and position of defects. Since defect concentrations are usually very low in order to avoid interactions, the intensity problem is of major concern as well as the distinction between the interesting signal and other sources of scattering. Two neutron spectrometers are described which were specially designed to tackle these problems, one of them operating in Juelich, the other one on the HFR in Grenoble. The second one, also offering the possibility of employing polarized neutrons, is specially suited to the study of diffuse magnetic scattering

  7. Neutron Scattering and High Magnetic Fields

    Energy Technology Data Exchange (ETDEWEB)

    Winn, Barry L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Stone, Matthew B. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2014-11-01

    The workshop “Neutron Scattering and High Magnetic Fields” was held September 4-5, 2014 at the Oak Ridge National Laboratory (ORNL). The workshop was held in response to a recent report by the National Research Council of the National Academy of Sciences entitled “High Magnetic Field Science and Its Application in the United States: Current Status and Future Directions.”1 This report highlights the fact that neutron scattering measurements carried out in high magnetic fields provide important opportunities for new science. The workshop explored the range of the scientific discoveries that could be enabled with neutron scattering measurements at high fields (25 Tesla or larger), the various technologies that might be utilized to build specialized instruments and sample environment equipment to enable this research at ORNL, and possible routes to funding and constructing these facilities and portable high field sample environments.

  8. Neutron small angle scattering of irradiated aluminium-silicon alloys

    International Nuclear Information System (INIS)

    Kostorz, G.

    1976-01-01

    Technically pure aluminium and aluminium-silicon alloys (0.43, 0.83 and 1.2% Si, also containing 0.11 to 0.14 at. % Fe) were investigated by slow neutron small angle scattering after irradiation with fast neutrons at low temperatures. Different irradiation levels, ageing at room temperature and at 60/70 0 C had no measurable effect upon small angle scattering cross-sections. From the experimental precision upper limit for the amount of Si involved in clustering after irradiation can be given. The observed small angle scattering shows a strong dependence on scattering angles and is attributed to large precipitates of Al 12 Fe 3 Si. A surface layer on the as-received samples is identified as another source of low-intensity small angle scattering. (orig.) [de

  9. Inelastic neutron scattering from glass formers

    International Nuclear Information System (INIS)

    Buchenau, U.

    1997-01-01

    Neutron spectra below and above the glass transition temperature show a pronounced difference between strong and fragile glass formers in Angell's fragility scheme. The strong anharmonic increase of the inelastic scattering with increasing temperature in fragile substances is absent in the strongest glass former SiO 2 . That difference is reflected in the temperature dependence of Brillouin sound velocities above the glass transition. Coherent inelastic neutron scattering data indicate a mixture of sound waves and local modes at the low frequency boson peak. A relation between the fragility and the temperature dependence of the transverse hypersound velocity at the glass temperature is derived. (author)

  10. Larmor-precession based neutron scattering instrumentation

    International Nuclear Information System (INIS)

    Ioffe, Alexander

    2009-01-01

    The Larmor precession of the neutron spin in a magnetic field allows the attachment of a Larmor clock to every neutron. Such Larmor labelling opens the possibility for the development of unusual neutron scattering techniques, where the energy (momentum) resolution does not require the initial and final states to be well selected. This principally allows for achievement of very high energy (momentum) resolution that is not feasible at all with conventional neutron scattering techniques, because the required neutron beam monochromatization (collimation) will result in intolerable intensity losses. Such decoupling of resolution and collimation allows, for example, for a significant increase in the luminosity of small-angle scattering or high-resolution diffractometers; the fact that opens new perspectives for their implementation at middle flux neutron sources. Different kinds of Larmor clock-based instrumentation, particularly two alternative NSE techniques using rotating and time-gradient magnetic field arrangements, which can be considered as inexpensive and affordable alternatives to present day NSE techniques, will be discussed and results of simulations and first experiments will be presented. (author)

  11. Neutron scattering of advanced magnetic materials

    Science.gov (United States)

    Yusuf, S. M.; Kumar, Amit

    2017-09-01

    An overview of notable contributions of neutron scattering in the advancement of magnetic materials has been presented. A brief description of static neutron scattering techniques, viz., diffraction, depolarization, small angle scattering, and reflectivity, employed in the studies of advanced magnetic materials, is given. Apart from providing the up-to-date literature, this review highlights the importance of neutron scattering techniques in achieving microscopic as well as mesoscopic understanding of static magnetic properties of the following selective classes of advanced magnetic materials: (i) magnetocaloric materials, (ii) permanent magnets, (iii) multiferroic materials, (iv) spintronic materials, and (v) molecular magnetic materials. In the area of magnetocaloric materials, neutron diffraction studies have greatly improved the understanding of magneto-structural coupling by probing (i) atomic site distribution, (ii) evolution of structural phases and lattice parameters across the TC, and (iii) microscopic details of magnetic ordering in several potential magnetocaloric materials. Such an understanding is vital to enhance the magnetocaloric effect. Structural and magnetic investigations, employing neutron diffraction and allied techniques, have helped to improve the quality of permanent magnets by tailoring (understanding) structural phases, magnetic ordering, crystallinity, microstructure (texture), and anisotropy. The neutron diffraction studies of structural distortions/instabilities and magnetic ordering in multiferroic materials have improved the microscopic understanding of magnetoelectric coupling that allows one to control magnetic order by an electric field and electric order by a magnetic field in multiferroic materials. In the field of molecular magnetic materials, neutron diffraction studies have enhanced the understanding of (i) structural and magnetic ordering, (ii) short-range structural and magnetic correlations, (iii) spin density distribution

  12. Application of eV neutron scattering and eV neutron absorption techniques

    International Nuclear Information System (INIS)

    Ikeda, Susumu

    1989-01-01

    Intense spallation neutron sources can provide a useful eV neutron flux in the energy range 1-100 eV, which is much more intense than has even been available from steady-state sources, and makes two fruitful techniques possible. One is an eV neutron scattering technique. The other is an eV neutron absorption technique. The discovery of superconductivity in the temperature range 30-100 K for the La-Cu-O system and the Y-Ba-Cu-O system is one of the most exciting events in recent solid state physics. Many attempts to explain such extraordinary high Tc values have been made with conventional electron-phonon coupling theory as well as with non-phonon mechanisms. The most direct test for such theories is to look for predicted excitations by using inelastic neutron scattering techniques. The eV neutron scattering and eV neutron absorption experiments can provide new important information for the high Tc mechanism, which has never been obtained by ordinary neutron scattering experiments. For the first time, the author applies these methods to the observation of motions of specific atoms in La-Cu-O and Y-Ba-Cu-O systems. In this paper, he reports a procedure of the application. 17 refs., 8 figs., 1 tab

  13. Determination of the nuclear scattering amplitude of uranium-235 isotope by neutron diffraction method

    International Nuclear Information System (INIS)

    Bayvas, F.

    1980-05-01

    The nuclear scattering amplitude of uranium-235 isotope has been determined by the neutron diffraction method. Although the scattering cross section for slow neutrons of uranium-235 is very small (16.33 barns), the coherent scattering can be observed. The scattering amplitude of this isotope has been calculated from the measured diffraction intensities of the enriched metallic uranium as b=(1.05+-0.05)x10 -12 cm. It may possibly give some more idea about the neutron-nucleus interactions of uranium-235 and some other elements which show the same scattering length for slow neutrons. (author)

  14. Critical Magnetic Scattering of Neutrons in Iron

    DEFF Research Database (Denmark)

    Passell, L.; Blinowski, K.; Brun, T.

    1965-01-01

    Measurements of the angular and energy distributions of 4.28 Å neutrons scattered at small angles from iron at temperatures above the Curie temperature are described. The results are interpreted in terms of Van Hove's theory of critical magnetic scattering and yield information on the range of sp...... to the existence of long-range couplings within the spin system. Details of certain recent modifications of the theory of critical systems are discussed and compared with the experimental results.......Measurements of the angular and energy distributions of 4.28 Å neutrons scattered at small angles from iron at temperatures above the Curie temperature are described. The results are interpreted in terms of Van Hove's theory of critical magnetic scattering and yield information on the range of spin...

  15. Observations of CEF-split intermultiplet transitions in optically opaque EuBa{sub 2}Cu{sub 3}O{sub 7} using inelastic neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Staub, U.; Soderholm, L.; Osborn, R. [Argonne National Lab., IL (United States); Balcar, E. [Atominstitut der Oesterriechischen Universitaeten, Vienna (Austria); Trunov, V. [St. Petersburg Nuclear Physics Institute (Russian Federation)

    1995-02-01

    Inelastic neutron scattering (INS) results on the intermultiplet transitions J=0 {yields} 1 and J=l {yields} 2 in optically opaque EuBa{sub 2}Cu{sub 3}O{sub 7} are reported. Whereas these multiplets are split by the crystalline electric field (CEF), their low J values are influenced to first order only by the 2 second-order (J=l) and additional fourth-order (J=2) CEF parameters. B{sub 0}{sup 2}, B{sub 2}{sup 2} and the spin-orbit coupling parameter were obtained by fitting the splitting of the J=1 multiplet and the energy separation between the J=0 and 1 multiplets. The J=0 to 1 splitting observed here is smaller than previously seen by optical spectroscopic studies on a variety of transparent, ionic compounds, necessitating fitting of the free-ion parameter. Additional spectroscopic information on the J=2 multiplet indicates that additional fitting of free ion parameters must be included to adequately model the observed low energy separation between the two lowest J-multiplets. Preliminary calculation on the Q-dependence of the CEF split J=0 to 1 transitions and the comparison with observations are presented.

  16. Small-angle neutron-scattering experiments

    International Nuclear Information System (INIS)

    Hardy, A.D.; Thomas, M.W.; Rouse, K.D.

    1981-04-01

    A brief introduction to the technique of small-angle neutron scattering is given. The layout and operation of the small-angle scattering spectrometer, mounted on the AERE PLUTO reactor, is also described. Results obtained using the spectrometer are presented for three materials (doped uranium dioxide, Magnox cladding and nitrided steel) of interest to Springfields Nuclear Power Development Laboratories. The results obtained are discussed in relation to other known data for these materials. (author)

  17. Neutron Scattering for the Nuclear Industry

    International Nuclear Information System (INIS)

    Rogge, Ronald B.

    1999-01-01

    The National Research Council's (NRC's) Neutron Program for Materials Research is in the fortunate circumstance of being located at the primary research facility for Canada's nuclear industry, Atomic Energy of Canada Limited (AECL). The National Research Universal (NRU) Reactor located at the Chalk River Laboratories is the source of neutrons for NRC's neutron beam laboratory. The NRC provides access to neutrons in two ways: (a) as an international user facility, participating in collaborative research projects with university, industry, and government laboratories, and (b) on a fee-for-service basis, obtaining proprietary information for Canadian and foreign industries. Consequently, neutron-scattering techniques can be applied to problems that span the range from fundamental research on the properties and behavior of materials to manufacturing processes and failure analysis

  18. Fast-neutron total and scattering cross sections of niobium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-07-01

    Neutron total cross sections of niobium were measured from approx. = 0.7 to 4.5 MeV at intervals of less than or equal to 50 keV with broad resolution. Differential-elastic-scattering cross sections were measured from approx. = 1.5 to 4.0 MeV at intervals of 0.1 to 0.2 MeV and at 10 to 20 scattering angles distributed between approx. = 20 and 160 degrees. Inelastically-scattered neutrons, corresponding to the excitation of levels at: 788 +- 23, 982 +- 17, 1088 +- 27, 1335 +- 35, 1504 +- 30, 1697 +- 19, 1971 +- 22, 2176 +- 28, 2456 +- (.), and 2581 +- (.) keV, were observed. An optical-statistical model, giving a good description of the observables, was deduced from the measured differential-elastic-scattering cross sections. The experimental-results were compared with the respective evaluated quantities given in ENDF/B-V

  19. Fast-neutron total and scattering cross sections of niobium

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-07-01

    Neutron total cross sections of niobium were measured from approx. = 0.7 to 4.5 MeV at intervals of less than or equal to 50 keV with broad resolution. Differential-elastic-scattering cross sections were measured from approx. = 1.5 to 4.0 MeV at intervals of 0.1 to 0.2 MeV and at 10 to 20 scattering angles distributed between approx. = 20 and 160 degrees. Inelastically-scattered neutrons, corresponding to the excitation of levels at: 788 +- 23, 982 +- 17, 1088 +- 27, 1335 +- 35, 1504 +- 30, 1697 +- 19, 1971 +- 22, 2176 +- 28, 2456 +- (.), and 2581 +- (.) keV, were observed. An optical-statistical model, giving a good description of the observables, was deduced from the measured differential-elastic-scattering cross sections. The experimental-results were compared with the respective evaluated quantities given in ENDF/B-V.

  20. Magnetism and magnetic materials probed with neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Velthuis, S.G.E. te, E-mail: tevelthuis@anl.gov [Materials Science Division, Argonne National Laboratory, 9700 S Cass Ave, Argonne, IL 60439 (United States); Pappas, C. [Faculty of Applied Sciences, Delft University of Technology, Mekelweg 15, NL-2629JB Delft (Netherlands)

    2014-01-15

    Neutron scattering techniques are becoming increasingly accessible to a broader range of scientific communities, in part due to the onset of next-generation, high-power spallation sources, high-performance, sophisticated instruments and data analysis tools. These technical advances also advantageously impact research into magnetism and magnetic materials, where neutrons play a major role. In this Current Perspective series, the achievements and future prospects of elastic and inelastic neutron scattering, polarized neutron reflectometry, small angle neutron scattering, and neutron imaging, are highlighted as they apply to research into magnetic frustration, superconductivity and magnetism at the nanoscale. - Highlights: • Introduction to Current Perspective series titled Magnetism and Magnetic Materials probed with Neutron Scattering. • Elastic and inelastic neutron scattering in systems with magnetic frustration and superconductivity. • Small angle neutron scattering and polarized neutron reflectometry in studying magnetism at the nanoscale. • Imaging of magnetic fields and domains.

  1. Magnetism and magnetic materials probed with neutron scattering

    International Nuclear Information System (INIS)

    Velthuis, S.G.E. te; Pappas, C.

    2014-01-01

    Neutron scattering techniques are becoming increasingly accessible to a broader range of scientific communities, in part due to the onset of next-generation, high-power spallation sources, high-performance, sophisticated instruments and data analysis tools. These technical advances also advantageously impact research into magnetism and magnetic materials, where neutrons play a major role. In this Current Perspective series, the achievements and future prospects of elastic and inelastic neutron scattering, polarized neutron reflectometry, small angle neutron scattering, and neutron imaging, are highlighted as they apply to research into magnetic frustration, superconductivity and magnetism at the nanoscale. - Highlights: • Introduction to Current Perspective series titled Magnetism and Magnetic Materials probed with Neutron Scattering. • Elastic and inelastic neutron scattering in systems with magnetic frustration and superconductivity. • Small angle neutron scattering and polarized neutron reflectometry in studying magnetism at the nanoscale. • Imaging of magnetic fields and domains

  2. Diffraction limit of the theory of multiple small-angle neutron scattering by a dense system of scatterers

    Science.gov (United States)

    Dzheparov, F. S.; Lvov, D. V.

    2016-02-01

    Multiple small-angle neutron scattering by a high-density system of inhomogeneities has been considered. A combined approach to the analysis of multiple small-angle neutron scattering has been proposed on the basis of the synthesis of the Zernike-Prince and Moliére formulas. This approach has been compared to the existing multiple small-angle neutron scattering theory based on the eikonal approximation. This comparison has shown that the results in the diffraction limit coincide, whereas differences exist in the refraction limit because the latter theory includes correlations between successive scattering events. It has been shown analytically that the existence of correlations in the spatial position of scatterers results in an increase in the number of unscattered neutrons. Thus, the narrowing of spectra of multiple small-angle neutron scattering observed experimentally and in numerical simulation has been explained.

  3. Instrumental resolution effects in neutron scattering studies of protein dynamics

    Science.gov (United States)

    Nickels, Jonathan D.

    2013-10-01

    In this study, the dynamics of Green Fluorescent protein (GFP) are analyzed using three neutron scattering spectrometers. We focus on the effect of instrumental energy resolution in the analysis of the elastic incoherent structure factor (EISF) and mean square displacement (MSD). This topic still remains a source of controversy. Our data clearly demonstrate the presence of the resolution effect in the dynamic transition for hydrated protein and the onset of translational motions in hydration water consistent with previous results from quasielastic neutron scattering. The 190 K onset of motions in hydration water observed at ∼1 ns is also consistent with a Tg of hydration water below 190 K.

  4. Slow neutron scattering with small angle. 5-6

    International Nuclear Information System (INIS)

    Komura, Shigehiro

    1976-01-01

    The principle, experimental apparatus, and applications of small angle neutron scattering are briefly reviewed. As for the principle, the mathematical expressions for the nuclear and magnetic scattering cross sections of neutrons are given. The advantages of utilizing cold neutrons are also discussed. As for the experimental apparatus, the one at ILL, Grenoble, is introduced with a bird-eye view, a schematic diagram, and the fundamental parameters of the apparatus. The calculated and measured spectra of neutron flux at the exit of a guide tube are also presented. The first example of the small angle neutron scattering is the measurement of void distribution within aluminum single-crystals irradiated with fast neutrons, which was carried out at Juelich. The second problem is the magnetic unevenness in the single crystal of Fe-Ni invar alloy. The third application is the observation of the helical structure of the tobacco mosaic virus in D 2 O. It is suggested that significant informations are expected to be obtained about the conformation of RNA in virus from the results of this observation. (Aoki, K.)

  5. Neutron elastic scattering at very small angles

    CERN Multimedia

    2002-01-01

    This experiment will measure neutron-proton elastic scattering at very small angles and hence very small four-momentum transfer, |t|. The range of |t| depends on the incident neutron momentum of the events but the geometrical acceptance will cover the angular range 0.025 < $\\Theta_{lab}$ < 1.9 mrad. The higher figure could be extended to 8.4 mrad by changing the geometry of the experiment in a later phase. \\\\ \\\\ The neutron beam will be highly collimated and will be derived from a 400 GeV external proton beam of up to $4 \\times 10^{10}$ protons per pulse in the SPS North Area Hall 1. The hydrogen target will be gaseous, operating at 40 atm. pressure and acts as a multiwire proportional chamber to detect the recoil protons. The forward neutron will be detected and located by interaction in a neutron vertex detector and its energy measured by a conventional steel plate calorimeter. \\\\ \\\\ The experiment will cover the angular region of nucleon-nucleon scattering which is dominated by Coulomb scattering ...

  6. Experimental technique of small angle neutron scattering

    International Nuclear Information System (INIS)

    Xia Qingzhong; Chen Bo

    2006-03-01

    The main parts of Small Angle Neutron Scattering (SANS) spectrometer, and their function and different parameters are introduced from experimental aspect. Detailed information is also introduced for SANS spectrometer 'Membrana-2'. Based on practical experiments, the fundamental requirements and working condition for SANS experiments, including sample preparation, detector calibration, standard sample selection and data preliminary process are described. (authors)

  7. Some applications of polarized inelastic neutron scattering

    Indian Academy of Sciences (India)

    A brief account of applications of polarized inelastic neutron scattering in condensed matter research is given. ... the itinerant antiferromagnet chromium we demonstrate that the dynamics of the longitudinal and transverse excitations are very different, resolving a long standing puzzle concerning the slope of their dispersion.

  8. NEUTRON-SCATTERING STUDY OF DCN

    DEFF Research Database (Denmark)

    Mackenzie, Gordon A.; Pawley, G. S.

    1979-01-01

    Phonons in deuterium cyanide have been measured by neutron coherent inelastic scattering. The main subject of study was the transverse acoustic mode in the (110) direction polarised along (110) which is associated with the first-order structural phase transition at 160K. Measurements have shown...

  9. Neutron scattering on hydrides of intermetallic compounds

    International Nuclear Information System (INIS)

    Hempelmann, R.

    1986-11-01

    This review surveys the application of neutron scattering for the investigation of the microscopic behaviour of hydrogen in intermetallic compounds. This concerns the structure as well as the dynamics. Neutron diffraction experiments were performed on Ti 1.2 Mn 1.8 D 3 and LaNi 5 D 7 . In the latter case the dominant nickel scattering could be suppressed by isotope substitution with 60 Ni, and the anisotropic broadening of the Bragg peaks could be modelled in a correspondingly modified Rietveld-profile refinement. For the investigation of hydrogen diffusion in intermetallic hydrides by means of quasielastic neutron scattering an iterative multiple scattering correction procedure has been developped which allows a reliable determination of hydrogen diffusion coefficients. The mechanism of hydrogen diffusion in intermetallic hydrides comprises three types of jumps: escape jumps out of energetically lower interstitials, transport jumps over the energetically higher sites and locally restricted jump processes. For Ti 1.2 Mn 1.8 H 3 the main features of the diffusional behaviour could be described quantitatively in the framework of a three state model. By means of neutron vibrational spectroscopy information about the occupied hydrogen sites and thus about the structure can be extracted from the symmetry splitting of the vibrational modes. In this way we showed that in α-LaNi 5 H x , La 2 Ni 4 -octahedral and La 2 Ni 2 -tetrahedral interstitial sites are occupied. (orig./GG)

  10. A small-angle neutron scattering investigation

    Indian Academy of Sciences (India)

    Hence, the steel is used in aircraft, nuclear reactor, petrochemical plants and many other industries. However, presence of carbide formers such as Mo and Cr war- rants the possibility of carbide precipitates in the structure and in turn affects the mechanical properties. Small-angle neutron scattering (SANS) is an important ...

  11. Magnetic Scattering of Neutrons in Chronium

    DEFF Research Database (Denmark)

    Bjerrum Møller, Hans; Blinowski, K.; Mackintosh, A. R.

    1964-01-01

    The results of a study of the magnetic scattering of neutrons in chromium near the Néel temperature are presented. It is deduced from these results that short range ordering persists in chromium unusually high above the Néel temperature, and that the magnetic structure below the Néel temperature...

  12. Critical scattering of neutrons from terbium

    DEFF Research Database (Denmark)

    Als-Nielsen, Jens Aage; Dietrich, O.W.; Marshall, W.

    1968-01-01

    The inelasticity of the critical scattering of neutrons in terbium has been measured above the Neél temperature at the (0, 0, 2−Q) satellite position. The results show that dynamic slowing down of the fluctuations does occur in a second‐order phase transition in agreement with the general theory...

  13. Neutron scattering (progress report) January - December 1991

    International Nuclear Information System (INIS)

    Buehrer, W.; Fischer, P.; Furrer, A.

    1992-02-01

    Progress made by the Laboratory for Neutron Scattering of the Swiss Federal Institute of Technology during the year 1991 in the fields of high-T c superconductors, materials science, magnetism, structural research, lattice dynamics, phase transitions, instrumental and support activities is reported. figs., tabs., refs

  14. 2016 American Conference on Neutron Scattering (ACNS)

    International Nuclear Information System (INIS)

    Woodward, Patrick

    2017-01-01

    The 8th American Conference on Neutron Scattering (ACNS) was held July 10-14, 2016 in Long Beach California, marking the first time the meeting has been held on the west coast. The meeting was coordinated by the Neutron Scattering Society of America (NSSA), and attracted 285 attendees. The meeting was chaired by NSSA vice president Patrick Woodward (the Ohio State University) assisted by NSSA president Stephan Rosenkranz (Argonne National Laboratory) together with the local organizing chair, Brent Fultz (California Institute of Technology). As in past years the Materials Research Society assisted with planning, logistics and operation of the conference. The science program was divided into the following research areas: (a) Sources, Instrumentation, and Software; (b) Hard Condensed Matter; (c) Soft Matter; (d) Biology; (e) Materials Chemistry and Materials for Energy; (f) Engineering and Industrial Applications; and (g) Neutron Physics.

  15. Resonance effects in neutron scattering lengths

    International Nuclear Information System (INIS)

    Lynn, J.E.

    1989-01-01

    The nature of neutron scattering lengths is described and the nuclear effects giving rise to their variation is discussed. Some examples of the shortcomings of the available nuclear data base, particularly for heavy nuclei, are given. Methods are presented for improving this data base, in particular for obtaining the energy variation of the complex coherent scattering length from long to sub-angstrom wave lengths from the available sources of slow neutron cross section data. Examples of this information are given for several of the rare earth nuclides. Some examples of the effect of resonances in neutron reflection and diffraction are discussed. This report documents a seminar given at Argonne National Laboratory in March 1989. 18 refs., 18 figs

  16. 2016 American Conference on Neutron Scattering (ACNS)

    Energy Technology Data Exchange (ETDEWEB)

    Woodward, Patrick [Materials Research Society, Warrendale, PA (United States)

    2017-02-09

    The 8th American Conference on Neutron Scattering (ACNS) was held July 10-14, 2016 in Long Beach California, marking the first time the meeting has been held on the west coast. The meeting was coordinated by the Neutron Scattering Society of America (NSSA), and attracted 285 attendees. The meeting was chaired by NSSA vice president Patrick Woodward (the Ohio State University) assisted by NSSA president Stephan Rosenkranz (Argonne National Laboratory) together with the local organizing chair, Brent Fultz (California Institute of Technology). As in past years the Materials Research Society assisted with planning, logistics and operation of the conference. The science program was divided into the following research areas: (a) Sources, Instrumentation, and Software; (b) Hard Condensed Matter; (c) Soft Matter; (d) Biology; (e) Materials Chemistry and Materials for Energy; (f) Engineering and Industrial Applications; and (g) Neutron Physics.

  17. The Effect of Anisotropic Scatter on Atmospheric Neutron Transport

    Science.gov (United States)

    2015-03-26

    THE EFFECT OF ANISOTROPIC SCATTER ON ATMOSPHERIC NEUTRON TRANSPORT THESIS MARCH 2015 Nicholas J...iii AFIT-ENP-MS-15-M-085 THE EFFECT OF ANISOTROPIC SCATTER ON ATMOSPHERIC NEUTRON TRANSPORT THESIS Presented to the...EFFECT OF ANISOTROPIC SCATTER ON ATMOSPHERIC NEUTRON TRANSPORT Nicholas J. McIntee, BSE Major, USA Committee Membership: Dr. Kirk A. Mathews

  18. Neutron Scattering Investigations of Correlated Electron Systems and Neutron Instrumentation

    DEFF Research Database (Denmark)

    Holm, Sonja Lindahl

    This PhD work has two main topics; one on neutron instrumentations, and one on correlated electron systems. There have been a total of ten different subprojects. Common to all the projects is the neutron scattering technique that is presented in the first chapters of the thesis. Neutrons are a un......This PhD work has two main topics; one on neutron instrumentations, and one on correlated electron systems. There have been a total of ten different subprojects. Common to all the projects is the neutron scattering technique that is presented in the first chapters of the thesis. Neutrons...... the impact of the time structure (pulse length and repetition frequency) choice for ESS are appended. McStas simulations of a low resolution cold powder diffractometer and high resolution thermal powder diffractometer with wavelength frame multiplication have been carried out for 20 different settings...... of the time structure. The instrument designs were changed to fit each setting with pulse lengths between 1 ms and 2 ms and repetition frequencies between 10 Hz and 25 Hz. The cold powder diffractometer was found to perform well with all the different source settings. The thermal powder diffractometer...

  19. Electrospinning atactic polystyrene: A neutron scattering study

    International Nuclear Information System (INIS)

    Mohan, S; Sen, S; Mitchell, G R; Olley, R H; Davis, F J

    2009-01-01

    Electrospinning is a method used to produce nanoscale to microscale sized polymer fibres. In this study we electrospin 1:1 blends of deuterated and hydrogenated atactic-Polystyrene from N,N-Dimethylformamide for small angle neutron scattering experiments in order to analyse the chain conformation in the electrospun fibres. Small angle neutron scattering was carried out on randomly orientated fibre mats obtained using applied voltages of 10kV-15kV and needle tip to collector distances of 20cm and 30cm. Fibre diameters varied from 3μm - 20μm. Neutron scattering data from fibre samples were compared with bulk samples of the same polymer blend. The scattering data indicates that there are pores and nanovoiding present in the fibres; this was confirmed by scanning electron microscopy. A model that combines the scattering from the pores and the labelled polymer chains was used to extract values for the radius of gyration. The radius of gyration in the fibres is found to vary little with the applied voltage, but varies with the initial solution concentration and fibre diameter. The values for the radius of gyration in the fibres are broadly equivalent to that of the bulk state.

  20. Anomalous inelastic neutron scattering from calcite

    International Nuclear Information System (INIS)

    Dove, M.T.; Harris, M.J.; Winkler, B.; Hagen, M.E.; Keele Univ.; Powell, B.M.; Steigenberger, U.

    1992-01-01

    Inelastic neutron scattering measurements on calcite (CaCO 3 ) in its low temperature phase have revealed the existence of an unusual column of inelastic scattering at the wavevector corresponding to the F point of the high temperature Brillouin zone. At the same wavevector there is also a transverse acoustic soft mode and the column of scattering ranges in energy from zero up to the soft mode. The intensity of the anomalous scattering increases rapidly with temperature, and is consistent with an Arrhenius relation of the form exp(-T * /T), where T * = 1035 K. We speculate that this scattering arises from thermal fluctuations of the calcite structure into a different ordered structure, which is related to an ordering instability at the F point. Evidence for this possibility has also been obtained from lattice energy calculations. (author)

  1. Small angle neutron scattering studies on the interaction of cationic

    Indian Academy of Sciences (India)

    The structure of the protein–surfactant complex of bovine serum albumin (BSA) and cationic surfactants has been studied by small angle neutron scattering. At low concentrations, the CTAB monomers are observed to bind to the protein leading to an increase in its size. On the other hand at high concentrations, surfactant ...

  2. Dynamics of Magnetic Nanoparticles Studied by Neutron Scattering

    DEFF Research Database (Denmark)

    Hansen, Mikkel Fougt; Bødker, Franz; Mørup, Steen

    1997-01-01

    We present the first triple-axis neutron scattering measurements of magnetic fluctuations in nanoparticles using an antiferromagnetic reflection. Both the superparamagnetic relaxation and precession modes in similar to 15 nm hematite particles are: observed. The results have been consistently...... analyzed on the basis of a simple model with uniaxial anisotropy and the Neel-Brown theory for the relaxation....

  3. Neutron scattering studies of nanomagnetism and artificially structured materials

    International Nuclear Information System (INIS)

    Fitzsimmons, M.R.; Bader, S.D.; Borchers, J.A.; Felcher, G.P.; Furdyna, J.K.; Hoffmann, A.; Kortright, J.B.; Schuller, Ivan K.; Schulthess, T.C.; Sinha, S.K.; Toney, M.F.; Weller, D.; Wolf, S.

    2004-01-01

    Nanostructured magnetic materials are intensively investigated due to their unusual properties and promise for possible applications. The key issue for these materials is to understand the limits between their physical properties (transport, magnetism, mechanical, etc.) and their chemical-physical structure. In principle, a detailed knowledge of the chemical and physical structures allows calculation of their physical properties. Theoretical and computational methods are rapidly evolving so that magnetic properties of nanostructured materials might soon be predicted. Success in this endeavor requires detailed quantitative understanding of magnetic structure at the microscopic level. Neutron scattering is a well-developed technique that can determine magnetic structure at the atomic length scale in samples of ever diminishing size. This has opened up the use of neutron scattering to nanostructured materials prepared by thin film and lithographic techniques. Many interesting and unexpected results have emerged from the application of elastic neutron scattering to nanostructured magnetic thin films such as superlattices and multilayers. These include, distinguishing between magnetic and chemical boundaries, observing the spatial dependence of the magnetization vector in nonuniform materials, unusual coupling mechanisms across nonmagnetic materials, unexpected magnetic phase diagrams, etc. Extension of elastic neutron scattering to nanostructured arrays and three-dimensional magnetic composites will allow future determination of magnetic structure with unprecedented resolution. In this review, we discuss the impact of neutron scattering to the study of magnetic nanostructures, i.e., magnetic materials that are artificially structured at nanometer length scales, such as magnetic thin films, multilayers and nanodot arrays. The basic interactions and different length scales relevant to these systems as well as the basic issues and phenomena of interest are briefly

  4. Neutron scattering studies of nanomagnetism and artificially structured materials

    Science.gov (United States)

    Fitzsimmons, M. R.; Bader, S. D.; Borchers, J. A.; Felcher, G. P.; Furdyna, J. K.; Hoffmann, A.; Kortright, J. B.; Schuller, Ivan K.; Schulthess, T. C.; Sinha, S. K.; Toney, M. F.; Weller, D.; Wolf, S.

    2004-04-01

    Nanostructured magnetic materials are intensively investigated due to their unusual properties and promise for possible applications. The key issue for these materials is to understand the limits between their physical properties (transport, magnetism, mechanical, etc.) and their chemical-physical structure. In principle, a detailed knowledge of the chemical and physical structures allows calculation of their physical properties. Theoretical and computational methods are rapidly evolving so that magnetic properties of nanostructured materials might soon be predicted. Success in this endeavor requires detailed quantitative understanding of magnetic structure at the microscopic level. Neutron scattering is a well-developed technique that can determine magnetic structure at the atomic length scale in samples of ever diminishing size. This has opened up the use of neutron scattering to nanostructured materials prepared by thin film and lithographic techniques. Many interesting and unexpected results have emerged from the application of elastic neutron scattering to nanostructured magnetic thin films such as superlattices and multilayers. These include, distinguishing between magnetic and chemical boundaries, observing the spatial dependence of the magnetization vector in nonuniform materials, unusual coupling mechanisms across nonmagnetic materials, unexpected magnetic phase diagrams, etc. Extension of elastic neutron scattering to nanostructured arrays and three-dimensional magnetic composites will allow future determination of magnetic structure with unprecedented resolution. In this review, we discuss the impact of neutron scattering to the study of magnetic nanostructures, i.e., magnetic materials that are artificially structured at nanometer length scales, such as magnetic thin films, multilayers and nanodot arrays. The basic interactions and different length scales relevant to these systems as well as the basic issues and phenomena of interest are briefly

  5. Neutron scattering lengths of molten metals determined by gravity refractometry

    International Nuclear Information System (INIS)

    Reiner, G.; Waschkowski, W.; Koester, L.

    1990-01-01

    Very accurate values of the coherent neutron scattering lengths of the heavy elements Bi and Pb are important quantities for the investigation of the electric interactions of neutrons with atoms. We performed, therefore, a series of experiments to determine accurate scattering lengths by means of neutron gravity refractometry on liquid mirrors of molten metals. The possible perturbations of the necessary reflection measurements have been discussed in details. After taking into account the uncertainties and corrections associated with observable perturbations we obtained the following values for bound atoms: b(Bi)=8.532±0.002 fm, b(Pb)=9.405±0.003 fm, b(Tl)=8.776±0.005 fm, b(Sn)=6.225±0.002 fm and b(Ga)=7.288±0.002 fm. These data are corrected for the local field effect occuring in the reflection on liquids. The recently reported results for the neutron's electric polarizability and the neutron-electron scattering length are supported by the Bi- and Pb-scattering length of this work. (orig.)

  6. Applications of thermal neutron scattering in biology, biochemistry and biophysics

    International Nuclear Information System (INIS)

    Worcester, D.L.

    1977-01-01

    Biological applications of thermal neutron scattering have increased rapidly in recent years. The following categories of biological research with thermal neutron scattering are presently identified: crystallography of biological molecules; neutron small-angle scattering of biological molecules in solution (these studies have already included numerous measurements of proteins, lippoproteins, viruses, ribosomal subunits and chromatin subunit particles); neutron small-angle diffraction and scattering from biological membranes and membrane components; and neutron quasielastic and inelastic scattering studies of the dynamic properties of biological molecules and materials. (author)

  7. Proceedings of the workshop on neutron scattering instrumentation for SNQ

    International Nuclear Information System (INIS)

    Scherm, R.; Stiller, H.

    1984-10-01

    These proceedings contain the articles presented at the named workshop. These concern instrumentation for neutron diffraction with special regards to small angle scattering, diffuse scattering, inelastic scattering, high resolution spectroscopy, and special techniques. (HSI)

  8. Fast-neutron scattering cross sections of elemental silver

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.

    1982-05-01

    Differential neutron elastic- and inelastic-scattering cross sections of elemental silver are measured from 1.5 to 4.0 MeV at intervals of less than or equal to 200 keV and at 10 to 20 scattering angles distributed between 20 and 160 0 . Inelastically-scattered neutron groups are observed corresponding to the excitation of levels at; 328 +- 13, 419 +- 50, 748 +- 25, 908 +- 26, 1150 +- 38, 1286 +- 25, 1507 +- 20, 1623 +- 30, 1835 +- 20 and 1944 +- 26 keV. The experimental results are used to derive an optical-statistical model that provides a good description of the observed cross sections. The measured values are compared with corresponding quantities given in ENDF/B-V

  9. The information bandwidth of neutron scattering instruments

    International Nuclear Information System (INIS)

    Johnson, M.W.

    1995-07-01

    The concept of the information content of a scientific measurement is introduced, and a theory is presented which enables the information that may be obtained by a neutron scattering instrument to be calculated. When combined with the time taken to perform the measurement the bandwidth of the instrument is obtained. This bandwidth is effectively a figure of merit which is of use in three respects: in the design of neutron instrumentation, the optimisation of measurements, and in the comparison of one instrument with another. (author)

  10. High-pressure cell for neutron scattering

    International Nuclear Information System (INIS)

    Onodera, Akifumi; Nakai, Yutaka; Kunitomi, Nobuhiko

    1987-01-01

    We have developed a high-pressure cell for neutron scattering. The cell uses a barrel-shaped support cylinder made of sintered ceramics. Samples 6 mm in diameter and 10 mm long can be accommodated. The cell is suitable for use at low and high temperatures, after a pressure generated at room temperature is locked. The change of pressure on cooling to cryogenic temperatures is estimated by measuring the lattice parameter of NaCl. Besides the pressure locking technique, continuous pressurization can be achieved at room temperature by using a built-in mini-press while the cell is mounted on a goniometer of neutron spectrometer. (author)

  11. Theory of neutron scattering in disordered alloys

    International Nuclear Information System (INIS)

    Yussouff, M.; Mookerjee, A.

    1984-08-01

    A comprehensive theory of thermal neutron scattering in disordered alloys is presented here. We consider in detail the case of substitutional random binary alloy with random changes in mass and force constants; and for all values of the concentration. The cluster CPA formalism in argumented space developed here is free from analytical difficulties for the Green function, performs correct averaging over random atomic scattering lengths and employs a self-consistent medium for the calculations. For easy computation, we describe the graphical representation of the resolvent where the approximation steps can be depicted as closed paths in augmented space. Our results for scattering cross sections, both coherent and incoherent, include new types of terms and these lead to asymmetric line shapes for the coherent scattering. (author)

  12. Neutron scattering in engineering applications

    Science.gov (United States)

    Webster, G. A.; Ezeilo, A. N.

    1997-02-01

    The state of stress generated in engineering components during manufacture and use can significantly influence their load carrying capacity and resistance to fracture. Some manufacturing processes introduce damaging residual tensile stresses whereas others can produce beneficial compression. In order to make reliable estimates of component performance it is necessary to have an accurate knowledge of these stresses. In this paper a technique for measuring residual stresses non-destructively by neutron diffraction is outlined. A representative selection of stress distributions developed by a range of manufacturing processes is examined. Some comparisons are made with strain gauge, X-ray and finite element determinations. It is shown how the results can be of benefit in engineering stress analysis.

  13. Observation of Nonlinear Compton Scattering

    Energy Technology Data Exchange (ETDEWEB)

    Kotseroglou, T.

    2003-12-19

    This experiment tests Quantum Electrodynamics in the strong field regime. Nonlinear Compton scattering has been observed during the interaction of a 46.6 GeV electron beam with a 10{sup 18} W/cm{sup 2} laser beam. The strength of the field achieved was measured by the parameter {eta} = e{var_epsilon}{sub rms}/{omega}mc = 0.6. Data were collected with infrared and green laser photons and circularly polarized laser light. The timing stabilization achieved between the picosecond laser and electron pulses has {sigma}{sub rms} = 2 ps. A strong signal of electrons that absorbed up to 4 infrared photons (or up to 3 green photons) at the same point in space and time, while emitting a single gamma ray, was observed. The energy spectra of the scattered electrons and the nonlinear dependence of the electron yield on the field strength agreed with the simulation over 3 orders of magnitude. The detector could not resolve the nonlinear Compton scattering from the multiple single Compton scattering which produced rates of scattered electrons of the same order of magnitude. Nevertheless, a simulation has studied this difference and concluded that the scattered electron rates observed could not be accounted for only by multiple ordinary Compton scattering; nonlinear Compton scattering processes are dominant for n {ge} 3.

  14. Estimation of scattering neutron intensities of materials for neutron radiography

    International Nuclear Information System (INIS)

    Sato, M.; Watanabe, Y.; Kobayashi, H.

    2004-01-01

    A new database (DBNR) is prepared based on the Nuclear Data from the Joint Evaluated File Library (NDJEF) for use in scattering neutron radiography and ordinal radiography. The new database includes a data handling tool. As a result, users can easily extract nuclear data from a file on a personal computer. The nuclear data are limited to naturally existing stable elements in an energy range from 10 -6 eV to 10 -7 eV. Within the limitation, total scattering (n, γ) and (n, α) cross sections are arbitrary extracted for the desired elements and energy ranges

  15. Neutron scattering at structural phase transformations

    International Nuclear Information System (INIS)

    Plakida, N.M.

    1982-01-01

    The specific fractures of neutron scattering cross sections on crystal lattices at structural phase transformations are considered in the lecture. The analysis of the elastic and inelastic scattering is carried out at different transformations (ordering type, displacement type incommensurable transformations). The experimental study on some transitions are given as an example, namely, transformation at the Brillouin zone edge in cubic perovskite. RbCaF 3 transformation in a quasiunidimensional ferroelectrics CsH 2 PO 4 and CsD 2 PO 4 , phase transformation into an incommensurable phase in diphenyl

  16. Neutron scattering. Annual progress report 1997

    International Nuclear Information System (INIS)

    Allenspach, P.; Boeni, B.; Fischer, P.; Furrer, A.

    1998-02-01

    The present progress report describes the scientific and technical activities obtained by LNS staff members in 1997. It also includes the work performed by external groups at our CRG instruments D1A and IN3 at the ILL Grenoble. Due to the outstanding properties of neutrons and x-rays the research work covered many areas of science and materials research. The highlight of the year 1997 was certainly the production of neutrons at the new spallation neutron source SINQ. From July to November, SINQ was operating for typically two days/week and allowed the commissioning of four instruments at the neutron guide system: - the triple-axis spectrometer Druechal, - the powder diffractometer DMC, - the double-axis diffractometer TOPSI, the polarised triple-axis spectrometer TASP. These instruments are now fully operational and have already been used for condensed matter studies, partly in cooperation with external groups. Five further instruments are in an advanced state, and their commissioning is expected to occur between June and October 1998: - the high-resolution powder diffractometer HRPT, - the single-crystal diffractometer TriCS, - the time-of-flight spectrometer FOCUS, - the reflectometer AMOR, - the neutron optical bench NOB. Together with the small angle neutron scattering facility SANS operated by the spallation source department, all these instruments will be made available to external user groups in the future. (author) figs., tabs., refs

  17. Specimen environments in thermal neutron scattering experiments

    International Nuclear Information System (INIS)

    Cebula, D.J.

    1980-11-01

    This report is an attempt to collect into one place outline information concerning the techniques used and basic design of sample environment apparatus employed in neutron scattering experiments. Preliminary recommendations for the specimen environment programme of the SNS are presented. The general conclusion reached is that effort should be devoted towards improving reliability and efficiency of operation of specimen environment apparatus and developing systems which are robust and easy to use, rather than achieving performance at the limits of technology. (author)

  18. Neutron scattering cross sections of uranium-238

    International Nuclear Information System (INIS)

    Beghian, L.E.; Kegel, G.H.R.; Marcella, T.V.; Barnes, B.K.; Couchell, G.P.; Egan, J.J.; Mittler, A.; Pullen, D.J.; Schier, W.A.

    1979-01-01

    The University of Lowell high-resolution time-of-flight spectrometer was used to measure angular distributions and 90-deg excitation functions for neutrons scattered from 238 U in the energy range from 0.9 to 3.1 MeV. This study was limited to the elastic and the first two inelastic groups, corresponding to states of 238 U at 45 keV (2 + ) and 148 keV (4 + ). Angular distributions were measured at primary neutron energies of 1.1, 1.9, 2.5, and 3.1 MeV for the same three neutron groups. Whereas the elastic data are in fair agreement with the evaluation in the ENDF/B-IV file, there is substantial disagreement between the inelastic measurements and the evaluated cross sections. 12 figures

  19. Inelastic neutron scattering from synthetic and biological polymers

    International Nuclear Information System (INIS)

    White, J.W.

    1976-01-01

    Neutron elastic and inelastic scattering measurements have provided many unique insights into structure, and by reviewing progress on synthetics, important differences likely to arise in biological systems are identified and a direction for studies of the latter is suggested. By neutron inelastic scattering it is possible to measure the frequency of thermally excited interatomic and intermolecular vibrations in crystals. With perfect organic and inorganic crystals the technique is now classical and has given great insight into the crystal forces responsible for the observed structures as well as the phase transitions they undergo. The study of polymer crystals immediately presents two problems of disorder: (1) Macroscopic disorder arises because the sample is a mixture of amorphous and crystalline fractions, and it may be acute enough to inhibit growth of a single crystal large enough for neutron studies. (2) Microscopic disorder in the packing of polymer chains in the ''crystalline'' regions is indicated by broadening of Bragg peaks. Both types of disorder problem arise in biological systems. The methods by which they were partially overcome to allow neutron measurements with synthetic polymers are described but first a classical example of the determination of interatomic forces by inelastic neutron scattering is given

  20. Fast-neutron scattering from vibrational palladium nuclei

    Energy Technology Data Exchange (ETDEWEB)

    Smith, A.B. [Argonne National Lab., IL (United States)]|[Univ. of Arizona, Tucson, AZ (United States); Guenther, P.T. [Argonne National Lab., IL (United States)

    1993-10-01

    Neutron total cross sections of elemental palladium are measured from {approx}0.6--4.5 MeV. These results, combined with others previously reported from this laboratory, provide a detailed knowledge of the neutron total cross sections of palladium from {approx}0.1--20 MeV. Differential neutron elastic-scattering cross sections are measured from {approx}1.5--10 MeV in sufficient energy and angle detail to well define the energy-average behavior. Concurrently, neutron inelastic-scattering cross sections are measured from {approx}1.5--8 MeV. Inelastically-scattered neutron groups are observed corresponding to excitations of: 306 {+-} 14, 411 {+-} 47, {approx}494, 791 {+-} 20, 924 {+-} 20, 1,156 {+-} 24, 1,358 {+-} 35, 1,554 {+-} 47 and 1,706 {+-} 59 keV, with additional tentative groups at 1,938 and 2,059 keV. Particular attention is given to the inelastic excitation of the 2{sup +} yrast states of the even isotopes. This broad data base is examined in the context of optical-statistical and coupled-channels models. The resulting model parameters are consistent with systematic trends in this vibrational mass region previously noted at this laboratory, and provide a suitable vehicle for many applications.

  1. Small-angle scattering from neutron-irradiated amorphous Pd80Si20

    International Nuclear Information System (INIS)

    Doi, K.; Kayano, H.; Masumoto, T.

    1978-01-01

    Small-angle scattering intensities were observed for amorphous Pd 80 Si 20 which was irradiated by fast neutrons to a fluence of 5 X 10 20 neutrons cm -2 . A broad hump was observed at 2 sin theta/lambda = 0.05 A -1 . The structure inhomogeneities produced by the neutron irradiation are discussed with the aid of the results of wide-angle scattering measurements. (Auth.)

  2. Neutron Inelastic Scattering Vol. I. Proceedings of a Symposium on Neutron Inelastic Scattering

    International Nuclear Information System (INIS)

    1968-01-01

    Proceedings of a Symposium convened by the IAEA and held in Copenhagen, 20-25 May 1968. The meeting was attended by 167 participants from 29 Member States and 4 international organizations. These are the fourth IAEA Symposium Proceedings to have neutron inelastic scattering as their main theme, the previous ones being Inelastic Scattering of Neutrons in Solids and Liquids (Vienna), IAEA (1961), Inelastic Scattering of Neutrons in Solids and Liquids (Chalk River), IAEA (1963), and Inelastic Scattering of Neutrons (Bombay), IAEA (1965). Contents: Dynamics of solids, including: lattice vibrations and local modes (6 papers), lattice dynamics in metals (7 papers), lattice dynamics of metals and alloys (13 papers), lattice dynamics of non-metals (11 papers) and review paper; Dynamics of liquids, including: coherent neutron scattering on systems (13 papers and review paper); Molecular dynamics (9 papers); Experimental methods (17 papers); and Summary. Each paper is in its original language (93 English, 2 French, 4 Russian) and is preceded by an abstract in English with one in the original language where this is not English. Discussions are in English. (author)

  3. Neutron scattering study of yttrium iron garnet

    Science.gov (United States)

    Shamoto, Shin-ichi; Ito, Takashi U.; Onishi, Hiroaki; Yamauchi, Hiroki; Inamura, Yasuhiro; Matsuura, Masato; Akatsu, Mitsuhiro; Kodama, Katsuaki; Nakao, Akiko; Moyoshi, Taketo; Munakata, Koji; Ohhara, Takashi; Nakamura, Mitsutaka; Ohira-Kawamura, Seiko; Nemoto, Yuichi; Shibata, Kaoru

    2018-02-01

    The nuclear and magnetic structure and full magnon dispersions of yttrium iron garnet Y3Fe5O12 have been studied using neutron scattering. The refined nuclear structure is distorted to a trigonal space group of R 3 ¯ . The highest-energy dispersion extends up to 86 meV. The observed dispersions are reproduced by a simple model with three nearest-neighbor-exchange integrals between 16 a (octahedral) and 24 d (tetrahedral) sites, Ja a, Ja d, and Jd d, which are estimated to be 0.00 ±0.05 , -2.90 ±0.07 , and -0.35 ±0.08 meV, respectively. The lowest-energy dispersion below 14 meV exhibits a quadratic dispersion as expected from ferromagnetic magnons. The imaginary part of q -integrated dynamical spin susceptibility χ″(E ) exhibits a square-root energy dependence at low energies. The magnon density of state is estimated from χ″(E ) obtained on an absolute scale. The value is consistent with the single chirality mode for the magnon branch expected theoretically.

  4. Neutron scattering applications in structural biology: now and the future

    Energy Technology Data Exchange (ETDEWEB)

    Trewhella, J. [Los Alamos National Lab., NM (United States)

    1996-05-01

    Neutrons have an important role to play in structural biology. Neutron crystallography, small-angle neutron scattering and inelastic neutron scattering techniques all contribute unique information on biomolecular structures. In particular, solution scattering techniques give critical information on the conformations and dispositions of the components of complex assemblies under a wide variety of relevant conditions. The power of these methods is demonstrated here by studies of protein/DNA complexes, and Ca{sup 2+}-binding proteins complexed with their regulatory targets. In addition, we demonstrate the utility of a new structural approach using neutron resonance scattering. The impact of biological neutron scattering to date has been constrained principally by the available fluxes at neutron sources and the true potential of these approaches will only be realized with the development of new more powerful neutron sources. (author)

  5. Development of temperature related thermal neutron scattering database for MCNP

    International Nuclear Information System (INIS)

    Mei Longwei; Cai Xiangzhou; Jiang Dazhen; Chen Jingen; Guo Wei

    2013-01-01

    Based on ENDF/B-Ⅶ neutron library, the thermal neutron scattering library S(α, β) for molten salt reactor moderators was developed. The temperatures of this library were chose as the characteristic temperature of the molten salt reactor. The cross section of the thermal neutron scattering of ACE format was investigated, and this library was also validated by the benchmarks of ICSBEP. The uncertainties shown in the validation were in reasonable range when compared with the thermal neutron scattering library tmccs which included in the MCNP data library. It was proved that the thermal neutron scattering library processed in this study could be used in the molten salt reactor design. (authors)

  6. Silicon Photomultipliers for Compact Neutron Scatter Cameras

    Science.gov (United States)

    Ruch, Marc L.

    The ability to locate and identify special nuclear material (SNM) is critical for treaty verification and emergency response applications. SNM is used as the nuclear explosive in a nuclear weapon. This material emits neutrons, either spontaneously or when interrogated. The ability to form an image of the neutron source can be used for characterization and/or to confirm that the item is a weapon by determining whether its shape is consistent with that of a weapon. Additionally, treaty verification and emergency response applications might not be conducive to non-portable instruments. In future weapons treaties, for example, it is unlikely that host countries will make great efforts to facilitate large, bulky, and/or fragile inspection equipment. Furthermore, inspectors and especially emergency responders may need to access locations not easily approachable by vehicles. Therefore, there is a considerable need for a compact, human-portable neutron imaging system. Of the currently available neutron imaging technologies, only neutron scatter cameras (NSCs) can be made truly compact because aperture-based imagers, and time-encoded imagers, rely on large amounts of materials to modulate the neutron signal. NSCs, in contrast, can be made very small because most of the volume of the imager can be filled with active detector material. Also, unlike other neutron imaging technologies, NSCs have the inherent ability to act as neutron spectrometers which gives them an additional means of identifying a neutron source. Until recently, NSCs have relied on photomultiplier tubes (PMT) readouts, which are bulky and fragile, require high voltage, and are very sensitive to magnetic fields. Silicon photomultipliers (SiPMs) do not suffer from these drawbacks and are comparable to PMTs in many respects such as gain, and cost with better time resolution. Historically, SiPMs have been too noisy for these applications; however, recent advancements have greatly reduced this issue and they have

  7. Neutron scattering treatise on materials science and technology

    CERN Document Server

    Kostorz, G

    1979-01-01

    Treatise on Materials Science and Technology, Volume 15: Neutron Scattering shows how neutron scattering methods can be used to obtain important information on materials. The book discusses the general principles of neutron scattering; the techniques used in neutron crystallography; and the applications of nuclear and magnetic scattering. The text also describes the measurement of phonons, their role in phase transformations, and their behavior in the presence of crystal defects; and quasi-elastic scattering, with its special merits in the study of microscopic dynamical phenomena in solids and

  8. Neutron-scattering studies of chromatin

    International Nuclear Information System (INIS)

    Bradbury, E.M.; Baldwin, J.P.; Carpenter, B.G.; Hjelm, R.P.; Hancock, R.; Ibel, K.

    1976-01-01

    It is clear that a knowledge of the basic molecular structure of chromatin is a prerequisite for any progress toward an understanding of chromosome organization. With a two-component system, protein and nucleic acid, neutrons have a particularly powerful application to studies of the spatial arrangements of these components because of the ability, by contrast matching with H 2 O-D 2 O mixtures, to obtain neutron-scattering data on the individual components. With this approach it has been shown that the neutron diffraction of chromatin is consistent with a ''beads on a string'' model in which the bead consists of a protein core with DNA coiled on the outside. However, because chromatin is a gel and gives limited structural data, confirmation of such a model requires extension of the neutron studies by deuteration of specific chromatin components and the isolation of chromatin subunits. Although these studies are not complete, the neutron results so far obtained support the subunit model described above

  9. Protein dynamics as seen by (quasi) elastic neutron scattering.

    Science.gov (United States)

    Magazù, S; Mezei, F; Falus, P; Farago, B; Mamontov, E; Russina, M; Migliardo, F

    2017-01-01

    Elastic and quasielastic neutron scattering studies proved to be efficient probes of the atomic mean square displacement (MSD), a fundamental parameter for the characterization of the motion of individual atoms in proteins and its evolution with temperature and compositional environment. We present a technical overview of the different types of experimental situations and the information quasi-elastic neutron scattering approaches can make available. In particular, MSD can crucially depend on the time scale over which the averaging (building of the "mean") takes place, being defined by the instrumental resolution. Due to their high neutron scattering cross section, hydrogen atoms can be particularly sensitively observed with little interference by the other atoms in the sample. A few examples, including new data, are presented for illustration. The incoherent character of neutron scattering on hydrogen atoms restricts the information obtained to the self-correlations in the motion of individual atoms, simplifying at the same time the data analysis. On the other hand, the (often overlooked) exploration of the averaging time dependent character of MSD is crucial for unambiguous interpretation and can provide a wealth of information on micro- and nanoscale atomic motion in proteins. By properly exploiting the broad range capabilities of (quasi)elastic neutron scattering techniques to deliver time dependent characterization of atomic displacements, they offer a sensitive, direct and simple to interpret approach to exploration of the functional activity of hydrogen atoms in proteins. Partial deuteration can add most valuable selectivity by groups of hydrogen atoms. "This article is part of a Special Issue entitled "Science for Life" Guest Editor: Dr. Austen Angell, Dr. Salvatore Magazù and Dr. Federica Migliardo". Copyright © 2016 Elsevier B.V. All rights reserved.

  10. Critical Magnetic Scattering of Neutrons in Iron

    DEFF Research Database (Denmark)

    Passell, L.; Blinowski, K.; Brun, T.

    1964-01-01

    scattered at small angles in iron and determined the spin correlation range 1∕κ1 and a parameter Λ associated with the lifetime of the fluctuations. Our results confirm the recent observation of Jacrot, Konstantinovic, Parette, and Cribier that the scattering is not elastic even at the Curie temperature. We...

  11. Neutron Scattering Differential Cross Sections for 12C

    Science.gov (United States)

    Byrd, Stephen T.; Hicks, S. F.; Nickel, M. T.; Block, S. G.; Peters, E. E.; Ramirez, A. P. D.; Mukhopadhyay, S.; McEllistrem, M. T.; Yates, S. W.; Vanhoy, J. R.

    2016-09-01

    Because of the prevalence of its use in the nuclear energy industry and for our overall understanding of the interactions of neutrons with matter, accurately determining the effects of fast neutrons scattering from 12C is important. Previously measured 12C inelastic neutron scattering differential cross sections found in the National Nuclear Data Center (NNDC) show significant discrepancies (>30%). Seeking to resolve these discrepancies, neutron inelastic and elastic scattering differential cross sections for 12C were measured at the University of Kentucky Acceleratory Laboratory for incident neutron energies of 5.58, 5.83, and 6.04 MeV. Quasi mono-energetic neutrons were scattered off an enriched 12C target (>99.99%) and detected by a C6D6 liquid scintillation detector. Time-of-flight (TOF) techniques were used to determine scattered neutron energies and allowed for elastic/inelastic scattering distinction. Relative detector efficiencies were determined through direct measurements of neutrons produced by the 2H(d,n) and 3H(p,n) source reactions, and absolute normalization factors were found by comparing 1H scattering measurements to accepted NNDC values. This experimental procedure has been successfully used for prior neutron scattering measurements and seems well-suited to our current objective. Significant challenges were encountered, however, with measuring the neutron detector efficiency over the broad incident neutron energy range required for these measurements. Funding for this research was provided by the National Nuclear Security Administration (NNSA).

  12. Inelastic neutron scattering on solid and liquid gallium

    International Nuclear Information System (INIS)

    Luzny, W.; Niziol, S.; Mayer, J.; Natkaniec, I.

    1989-01-01

    In order to find a physical property which would be able to distinguish the liquid gallium obtained by melting the α-phase and the liquid gallium annealed at temperatures higher than 333 K, measurements of incoherent inelastic neutron scattering (IINS) spectra were made with the aim to observe changes in the excitation spectrum occuring during the melting and then annealing of liquid gallium. The results of neutron experiments have shown that the diatomic-type structure of α-Ga is destroyed just in the melting point and that the dynamic properties of liquid gallium do not depend on the thermal history of the sample

  13. Polarized neutron scattering on HYSPEC: the HYbrid SPECtrometer at SNS

    Energy Technology Data Exchange (ETDEWEB)

    Zaliznyak, Igor [Brookhaven National Laboratory (BNL); Savici, Andrei T [ORNL; Garlea, Vasile O [ORNL; Winn, Barry L [ORNL; Schneelock, John [Brookhaven National Laboratory (BNL); Tranquada, John M. [Brookhaven National Laboratory (BNL); Gu, G. D. [Brookhaven National Laboratory (BNL); Wang, Aifeng [Brookhaven National Laboratory (BNL); Petrovic, C [Brookhaven National Laboratory (BNL)

    2017-01-01

    We describe some of the first polarized neutron scattering measurements performed at HYSPEC spectrometer at the Spallation Neutron Source, Oak Ridge National Laboratory. We discuss details of the instrument setup and the experimental procedures in the mode with the full polarization analysis. Examples of the polarized neutron diffraction and the polarized inelastic neutron data obtained on single crystal samples are presented.

  14. Neutron scattering studies of premartensitic phenomena

    International Nuclear Information System (INIS)

    Shapiro, S.M.

    1989-01-01

    Elastic neutron diffraction and inelastic neutron scattering are ideal techniques for studying premartensitic behavior in metallic alloys. By necessity, real, bulk samples are probed replete with their intrinsic defects. Also, because of the properties of the neutron it is straightforward to probe the behavior of the phonon modes away from the zone center which is probed in the normal ultrasonic techniques. A wide variety of alloys exhibiting martensitic transformations have been studied. It will be shown that most systems undergoing diffusionless transformations exhibit premartensitic behavior in that precursor effects are seen at temperatures well above the martensitic transformation temperature, T M . This behavior manifests itself in an anomalous temperature dependence of the energy of a particular phonon mode as the temperature approaches T M . The wavevector of this mode is frequently away from the zone center (i.e., q ≠ O). This softening is nearly always accompanied by elastic diffuse scattering at the same wavevector. Particular examples to be discussed are the alkali metals, ω-phase materials and Ni-based alloys. 34 refs., 9 figs

  15. Probing fine magnetic particles with neutron scattering

    International Nuclear Information System (INIS)

    Pynn, R.

    1991-01-01

    Because thermal neutrons are scattered both by nuclei and by unpaired electrons, they provide an ideal probe for studying the atomic and magnetic structures of fine-grained magnetic materials, including nanocrystalline solids, thin epitaxial layers, and colloidal suspensions of magnetic particles, known as ferrofluids. Diffraction, surface reflection, and small angle neutron scattering (SANS) are the techniques used. With the exception of surface reflection, these methods are described in this article. The combination of SANS with refractive-index matching and neutron polarisation analysis is particularly powerful because it allows the magnetic and atomic structures to be determined independently. This technique has been used to study both dilute and concentrated ferrofluid suspensions of relatively monodisperse cobalt particles, subjected to a series of applied magnetic fields. The size of the cobalt particle core and the surrounding surfactant layer were determined. The measured interparticle structure factor agrees well with a recent theory that allows correlations in binary mixtures of magnetic particles to be calculated in the case of complete magnetic alignment. When one of the species in such a binary mixture is a nonmagnetic, cyclindrical macromolecule, application of a magnetic field leads to some degree of alignment of the nonmagnetic species. This result has been demonstrated with tobacco mosaic virus suspended in a water-based ferrofluid

  16. Cryogen free cryostat for neutron scattering experiments

    Science.gov (United States)

    Kirichek, O.; Down, R. B. E.; Manuel, P.; Keeping, J.; Bowden, Z. A.

    2014-12-01

    Most very low temperature (below 1K) experiments at advanced neutron facilities are based on dilution and 3He refrigerator inserts used with Orange cryostats, or similar systems. However recent increases in the cost of liquid helium caused by global helium supply problems, has raised significant concern about the affordability of such cryostats. Here we present the design and test results of a cryogen free top-loading cryostat with a standard KelvinoxVT® dilution refrigerator insert which provides sample environment for neutron scattering experiments in the temperature range 35 mK - 300 K. The dilution refrigerator insert operates in a continuous regime. The cooling time of the insert is similar to one operated in the Orange cryostat. The main performance criteria such as base temperature, cooling power, and circulation rate are compatible with the technical specification of a standard dilution refrigerator. In fact the system offers operating parameters very similar to those of an Orange cryostat, but without the complication of cryogens. The first scientific results obtained in ultra-low temperature neutron scattering experiment with this system are also going to be discussed.

  17. Neutron scattering: properties, status and perspectives

    International Nuclear Information System (INIS)

    Clausen, K.N.; Swygenhoven, H. van; Lehmann, E.

    2008-01-01

    This presentation will start with a short general introduction to neutron scattering, and how the penetrating power, isotope, magnetic and hydrogen sensitivity, and micro to meV spectroscopic energy resolution of this technique can be used to study a multitude of key questions relevant to energy materials, for both nuclear and non nuclear applications. The second part will be a short review of current capabilities and some remarks on what is just around the corner with upcoming new facilities like SNS in the US, JSNS in Japan and hopefully also soon a new next generation neutron scattering facility in Europe - European Spallation Source (ESS). With the new sources and the development in modeling capabilities we will take huge steps towards studying and understanding real materials or systems under real conditions and in real time. The status and perspectives will be illustrated by a few illustrative examples and by no means be a comprehensive list. Superconducting and hydrogen storage materials are essential issues for energy storage and transport that will be covered in detail in other presentations at this symposium, and thus be omitted in this presentation. The main example is on in situ studies of operating fuel cells and how neutron imaging can be used to understand and optimize system performance. (au)

  18. Neutron, x-ray scattering and TEM studies of Ni-Ti multilayers

    International Nuclear Information System (INIS)

    Keem, J.E.; Wood, J.; Grupido, N.; Hart, K.; Nutt, S.; Reichel, D.G.; Yelon, W.B.

    1988-01-01

    The authors present an analysis of Ni-Ti multilayer neutron reflectors and supermirrors undertaken to identify the causes of the lower than expected observed scattering power and critical angle enhancement of Ni-Ti supermirrors. Results of these investigations focus attention on cusp formation in the Ni-Ti bilayers as probable cause for the reduced neutron scattering power. Grazing angle x-ray and neutron scattering, wide angle neutron diffraction and analytical cross sectional TEM have been used. The multilayers were produced by magnetron sputtering and ion-beam deposition on float glass substrates and silicon wafers

  19. Study of scattering in bi-dimensional neutron radiographic images

    International Nuclear Information System (INIS)

    Oliveira, K.A.M. de; Crispim, V.R.; Silva, F.C.

    2009-01-01

    The effect of neutron scattering frequently causes distortions in neutron radiographic images and, thus, reduces the quality. In this project, a type of filter, comprised of cadmium (a neutron absorber), was used in the form of a grid to correct this effect. This device generated image data in the discrete shadow bands of the absorber, components relative to neutron scattering on the test object and surroundings. Scattering image data processing, together with the original neutron radiographic image, resulted in a corrected image with improved edge delineation and, thus, greater definition in the neutron radiographic image of the test object. The objective of this study is to propose a theoretical/experimental methodology that is capable of eliminating the components relative to neutron scattering in neutron radiographic images, coming from the material that composes the test object and the materials that compose the surrounding area. (author)

  20. Annual report on neutron scattering studies in JAERI

    International Nuclear Information System (INIS)

    Sato, Masatoshi; Nishi, Masakazu; Fujishita, Hideshi; Iizumi, Masashi

    1982-07-01

    Neutron scattering studies carried out from September 1979 to August 1981 by Division of Physics, JAERI, and universities with JRR-2 and -3 neutron beam facilities are described: 61 summary reports, and a list of publications. (author)

  1. Fast-neutron scattering cross sections of elemental zirconium

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.

    1982-12-01

    Differential neturon-elastic-scattering cross sections of elemental zirconium are measured from 1.5 to 4.0 MeV at intervals of less than or equal to 200 keV. Inelastic-neutron-scattering cross sections corresponding to the excitation of levels at observed energies of: 914 +- 25, 1476 +- 37, 1787 +- 23, 2101 +- 26, 2221 +- 17, 2363 +- 14, 2791 +- 15 and 3101 +- 25 keV are determined. The experimental results are interpreted in terms of the optical-statistical model and are compared with corresponding quantities given in ENDF/B-V

  2. Significance of collective motions in biopolymers and neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Go, Nobuhiro [Kyoto Univ. (Japan)

    1996-05-01

    Importance of collective variable description of conformational dynamics of biopolymers and the vital role that neutron inelastic scattering phenomena would play in its experimental determination are discussed. (author)

  3. Small-angle neutron scattering technique in liquid crystal studies

    International Nuclear Information System (INIS)

    Shahidan Radiman

    2005-01-01

    The following topics discussed: general principles of SAS (Small-angle Neutron Scattering), liquid crystals, nanoparticle templating on liquid crystals, examples of SAS results, prospects of this studies

  4. Molecular dynamics using quasielastic neutron scattering

    CERN Document Server

    Mitra, S

    2003-01-01

    Quasielastic neutron scattering (QENS) technique is well suited to study the molecular motions (rotations and translations) in solids or liquids. It offers a unique possibility of analysing spatial dimensions of atomic or molecular processes in their development over time. We describe here some of the systems studied using the QENS spectrometer, designed, developed and commissioned at Dhruva reactor in Trombay. We have studied a variety of systems to investigate the molecular motion, for example, simple molecular solids, molecules adsorbed in confined medium like porous systems or zeolites, monolayer-protected nano-sized metal clusters, water in Portland cement as it cures with time, etc. (author)

  5. Neutron scattering on partially deuterated polybutadiene

    CERN Document Server

    Kahle, S; Monkenbusch, M; Richter, D; Arbe, A; Colmenero, J; Frick, B

    2002-01-01

    The molecular nature of the secondary relaxation (Johari-Goldstein relaxation) and its relationship with the alpha relaxation is in most cases still unknown. In order to access these processes on a molecular level, it is necessary to obtain spatial information of the relaxation. Through the momentum-transfer dependence of the dynamic structure factor S(Q,t), this information can be provided by quasielastic neutron scattering techniques. The large difference in scattering lengths between hydrogen and deuterium allows us to accentuate specific correlations between atoms in a polymer melt. Here, we report on recent results on a polybutadiene melt, where the double bond was hydrogeneous, while the methylene groups carried deuterons (d4h2-PB). In this way the correlations between the double bonds are emphasised. We will show that the double bond/double bond correlation function, generated in this way, shows the same temperature dependence as the viscosity at higher temperatures at the structure factor peak maximum...

  6. Small-angle neutron scattering and inelastic neutron scattering studies on β-cyclodextrins and hydroxypropyl-β-cyclodextrins

    International Nuclear Information System (INIS)

    Maccarrone, S.; Magazu, S.; Migliardo, F.; Mondio, F. Mondio

    2004-01-01

    This work reports new experimental neutron scattering results on β-cyclodextrins and hydroxypropyl-β-cyclodextrins. The small angle neutron scattering analysis shows that the typical conformation of the investigated systems in crystalline state is also maintained in aqueous solution. Inelastic neutron scattering results emphasize the more 'crystalline' character of β-cyclodextrins in comparison with hydroxypropyl β-cyclodextrins from the differences in the vibrational spectra of these compounds

  7. Investigations of advanced magnetic materials using neutron scattering

    International Nuclear Information System (INIS)

    Yusuf, S.M.

    2016-01-01

    A wide class of advanced magnetic materials, such as molecular magnets, magnetic nanoparticles, 1-D and 2-D magnetic materials, high magnetocaloric materials, high magnetoresistive materials, and multiferroic materials by using neutron diffraction, neutron depolarization and polarized neutron small angle scattering techniques has been investigated. A detailed understanding of magnetic correlations in mesoscopic and microscopic length scales in such systems has been achieved. The results of some of these recent investigations, and highlight the usefulness of neutron diffraction, neutron depolarization, and polarized neutron small angle scattering techniques for studying advanced magnetic materials have been presented in this talk. The applied aspects of the derived results have been discussed

  8. Magnetic scattering of neutrons by atoms

    International Nuclear Information System (INIS)

    Stassis, C.; Deckman, H.W.

    1976-01-01

    The magnetic scattering of neutrons by an atom or ion possessing both a spin and orbital magnetic moment is examined. For an atom in the 1sup(n) electronic configuration the magnetic scattering amplitude is determined by matrix elements of even-order electric and odd-order magnetic multipoles, whose order of multipolarity k is less than or equal to 21 + 1. The calculation of the matrix elements of these multipoles is separated into evaluating radial matrix elements and matrix elements of the Racah tensors Wsup(0,k) and Wsup(1,k') where k is an even integar less than or equal to 21. The calculation of the matrix elements of these tensors is considerably simplified by selection rules based on the groups Sp(41 + 2), R(21 + 1), R(3) and in the case of f-electrons, the special group G 2 . It is shown that, in the case of elastic scattering by an atom or an ion whose state is a single Russell-Saunders state, the magnetic scattering amplitude can be written in the conventional form p(q)qsub(m).sigma. General expressions for the amplitude p(q) as well as the elastic magnetic form factor are obtained. The evaluation of the coherent magnetic scattering amplitude by an atom in a magnetic field is discussed, and the small-q approximation to the elastic magnetic scattering is considered. The formation is illustrated for the important case of d- and f-electrons. The generalization of the formalism to the case of mixed atomic configurations is examined in some detail. (author)

  9. Observation of pulsed neutron Ramsey resonance

    Energy Technology Data Exchange (ETDEWEB)

    Masuda, Y. [High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba Ibaraki 305-0801 (Japan)]. E-mail: yasuhiro.masuda@kek.jp; Skoy, V. [Joint Institute for Nuclear Reasearch, 141980 Dubna, Moscow Region (Russian Federation); Ino, T. [High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba Ibaraki 305-0801 (Japan); Jeong, S.C. [High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba Ibaraki 305-0801 (Japan); Watanabe, Y. [High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba Ibaraki 305-0801 (Japan)

    2007-07-15

    A Ramsey resonance for pulsed neutrons was observed. The separated oscillatory fields for nuclear magnetic resonance were synchronized with a neutron pulse, and then the Ramsey resonance was observed as a function of the neutron velocity. The phase of one of the oscillatory fields was modulated as a function of the neutron time of flight for a neutron velocity measurement.

  10. Monte Carlo calculation of the slow neutron background in the neutron-neutron scattering experiment at the pulse reactor BIGR

    International Nuclear Information System (INIS)

    Budnik, A.D.; Ososkov, G.A.; Pokotilovskij, Yu.N.; Rogov, A.D.

    1995-01-01

    Slow neutron background calculations were performed for the proposed geometry of the neutron-neutron scattering experiment at the BIGR pulse reactor. The incoming slow neutron space and spectral distributions on the moderator surface were calculated with the MCNP program starting from the exact physical model of the reactor fuel and moderator and shielding geometry. Two elastic scatterings of slow neutrons from the neutron absorbing cover (Cd) inside the collimating and shielding system were taken into account. The calculated thermal neutron background is significantly lower than the estimated n-n scattering effect. 3 refs., 5 figs., 2 tabs

  11. Magnetization reversal of a Nd-Cu-infiltrated Nd-Fe-B nanocrystalline magnet observed with small-angle neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Saito, Kotaro, E-mail: kotaro.saito@kek.jp; Ono, Kanta [Institute of Materials Structure Science, High Energy Accelerator Research Organization, 1-1 Oho, 305-0803 Tsukuba (Japan); Ueno, Tetsuro [Elements Strategy Initiative Center for Magnetic Materials, National Institute for Materials Science, 1-2-1 Sengen, 305-0047 Tsukuba (Japan); Yano, Masao; Shoji, Tetsuya; Sakuma, Noritsugu; Manabe, Akira; Kato, Akira [Toyota Motor Corporation, Toyota, Aichi 471-8571 (Japan); Harada, Masashi [Toyota Central R and D Labs, Inc., Aichi 480-1192 (Japan); Keiderling, Uwe [Helmholtz-Zentrum Berlin für Materialien and Energie, 14109 Berlin (Germany)

    2015-05-07

    The magnetization reversal process of Nd-Fe-B nanocrystalline magnets infiltrated with Nd-Cu alloy was examined using small-angle neutron scattering (SANS). The magnetic-field dependence of SANS intensity revealed a qualitative difference between Nd-Cu-infiltrated samples and as-deformed samples. Insufficient magnetic isolation along the direction perpendicular to the nominal c-axis is expected from comparable SANS intensities for different ranges of q values along this direction. For small q values near the coercivity field, Nd-Cu-infiltrated samples show a noticeable reduction in SANS intensity along the nominal c-axis, which is parallel to the external magnetic field. This indicates less spatial fluctuation of magnetic moments in Nd-Cu-infiltrated samples, owing to magnetically isolated Nd{sub 2}Fe{sub 14}B grains.

  12. Magnetization reversal of a Nd-Cu-infiltrated Nd-Fe-B nanocrystalline magnet observed with small-angle neutron scattering

    International Nuclear Information System (INIS)

    Saito, Kotaro; Ono, Kanta; Ueno, Tetsuro; Yano, Masao; Shoji, Tetsuya; Sakuma, Noritsugu; Manabe, Akira; Kato, Akira; Harada, Masashi; Keiderling, Uwe

    2015-01-01

    The magnetization reversal process of Nd-Fe-B nanocrystalline magnets infiltrated with Nd-Cu alloy was examined using small-angle neutron scattering (SANS). The magnetic-field dependence of SANS intensity revealed a qualitative difference between Nd-Cu-infiltrated samples and as-deformed samples. Insufficient magnetic isolation along the direction perpendicular to the nominal c-axis is expected from comparable SANS intensities for different ranges of q values along this direction. For small q values near the coercivity field, Nd-Cu-infiltrated samples show a noticeable reduction in SANS intensity along the nominal c-axis, which is parallel to the external magnetic field. This indicates less spatial fluctuation of magnetic moments in Nd-Cu-infiltrated samples, owing to magnetically isolated Nd 2 Fe 14 B grains

  13. Malaysia's entry into a neutron-scattering programme

    International Nuclear Information System (INIS)

    Abdul Ghaffar Ramli; Mohamad Deraman.

    1986-10-01

    The neutron-scattering programme in Malaysia had been planned and re-planned since 1982, soom after Malaysia's first research reactor was commissioned. Currently, and most definitely, the neutron-scattering programme will start off with small-angle neutron-scattering (SANS). This seems to be in contrast with other nations' neutron-scattering programmes where the usual activity would first be neutron diffraction. This paper gives the reasons behind the selection of small-angle neutron-scattering (SANS) as a starting point. The design of Malaysia's SANS instrument and its expected applications will be explained. Other matters, especially those related to expected future developments or arrangements will also be discussed. (author)

  14. Current status and future development of neutron scattering in CIAE

    International Nuclear Information System (INIS)

    Chen, D.F.; Gou, C.; Ye, C.T.; Guo, L.P.; Sun, K.

    2003-01-01

    Currently, the 15 MW Heavy Water Research Reactor (HWRR) at China Institute of Atomic Energy (CIAE) in Beijing is the only neutron source available for neutron scattering experiments in China. A 60 MW tank-in-pool inverse neutron trap-type research reactor, China Advanced Research Reactor (CARR), now is being built at CIAE to meet the increasing demand of neutron scattering research in China. According to design, the maximum unperturbed thermal neutron flux would be expected to be 8x10 14 n/cm 2 .s in the reflector region. Seven out of nine tangential horizontal beam tubes will be dedicated for neutron scattering experiments. A cold source, a hot source and a 30x60 m 2 guide tube hall will also be constructed. In this paper, a brief introduction of HWRR, the existing neutron scattering facilities and research activities at HWRR, CARR, and the facilities to be built at CARR are presented. (author)

  15. Investigations of the magnetic materials using neutron scattering

    International Nuclear Information System (INIS)

    Kakurai, Kazuhisa; Takeda, Masayasu

    2010-01-01

    Utilizing the neutron magnetic scattering, one can investigate magnetic materials by looking at their magnetic nano structures. It is not exaggerated to state that nearly all the present microscopic knowledge of solid state magnetism has been obtained by neutron magnetic scattering experiments in the steady state neutron beam facilities at research reactors. In this review, we would like to introduce basics of the neutron magnetic scattering and demonstrate its strength by presenting some recent experiments on magnetic materials performed at the Research Reactor JRR-3 facility in the Nuclear Science Research Center, Tokai, Japan Atomic Energy Agency. The operation of the pulsed neutron source facility in the Materials and Life Science Facility of Japan Proton Accelerator Complex (J-PARC) will make the magnetic neutron scattering techniques even more common place, and the complementary use of both the steady state and pulsed neutron facilities in the near proximity will serve the broad users from academia and industries investigating magnetic materials. (author)

  16. A magneto-elastic model for the relaxation of lanthanide ions in YBa2Cu3O7-δ observed by neutron scattering

    International Nuclear Information System (INIS)

    Lovesey, S.W.; Staub, U.

    1999-01-01

    The 4f electrons attached to a lanthanide ion substituting for Y in YBa 2 Cu 3 O 7-δ are described with a crystal-field potential (symmetry D 2h ) and a magneto-elastic interaction, linear in the normal modes of vibration of the paramagnetic ion and anions. The most significant matrix elements of the interaction are determined using selection rules and wavefunctions for the crystal-field states. Applied to Tb 3+ , Ho 3+ and Tm 3+ , calculations for the ground state and first excited state indicate that the dynamic properties of the lanthanide ions are adequately described by the simple addition of one crystal-field state, leading to a three-state model similar to the one introduced by Orbach for the interpretation of electron paramagnetic resonance signals from a lanthanide ion in dilute concentration in a salt. The cross-section for inelastic scattering of neutrons by an ion is derived by constructing a pseudo-spin model (spin = 1) and treating the magneto-elastic interaction as a perturbation on the three crystal-field states. In the case of Tb 3+ , the energy of the first excited state relative to the ground state is found to be very much smaller than the energy of any other state, the scattering of neutrons is thus a quasi-elastic process and the width in energy or, alternatively, the relaxation rate is proportional to {exp (Δ/k B T) - 1} -1 , where T is the temperature and Δ is the energy of the third, intermediate crystal-field state at which the density of phonon states is very significant. The value of Δ suggested by the calculation and the law predicted for the temperature dependence of the relaxation rate are in accord with measurements, on metallic and non metallic samples. Equally impressive accounts are given of data published on the relaxation rates of Ho 3+ and Tm 3+ in YBa 2 Cu 3 O 7-δ . (author)

  17. Fast neutron inelastic scattering from nuclei

    International Nuclear Information System (INIS)

    Lachkar, J.

    1978-01-01

    The need for accurate values of inelastic scattering cross sections appears when the requests for neutron data for reactors and other applied purposes are considered. These requests are partly related to values for spherical nuclei, well studied over many years. These studies were extensively considered in two review papers presented, in 1976, at the International Conference on the Interactions of Neutrons with nuclei. Other requests are related to vibrational and rotational nuclei, and relevant studies have been recently performed. The quality of these investigations and the large number of recent results have lead to concentration on them as the topic of the present review. The constant improvements of the experimental techniques permits precise measurements of inelastic scattering cross sections to the first excited levels over a range of incident energies, such that different reactions mechanisms are predominant in different parts of that range of energies. Quadrupole, hexadecapole and octupole deformation parameters of the target nuclei can be deduced from the data using phenomenological models. The successful application of the analysis over the range of energies leads to the conclusion that reliable information on the shape of the nuclei has been derived. The validity of the various models, which include direct interaction and compound nucleus reaction mechanisms, is discussed in connection with analyses of recent experiments. (author) [fr

  18. Observation of mesoscopic structure in NdBa sub 2 Cu sub 3 O sub 7 sub - subdelta by small-angle neutron scattering

    CERN Document Server

    Miyata, S; Suzuki, J I; Kuroda, K; Koshizuka, N

    2003-01-01

    In order to clarify the origin of the high critical current density (J sub c) of NdBa sub 2 Cu sub 3 O sub 7 sub - subdelta (Nd123), we investigated the inhomogeneities in this material by small-angle neutron scattering (SANS) experiments. As a result of numerical calculations, it was found that the anisotropic scattering patterns and radial intensity profiles can be explained by the existence of elliptic cylindrical objects of which the cylindrical axis is parallel to the crystallographic c-axis. Long and short elliptic axis lengths and the height of the elliptic cylinders in the high-J sub c sample are about 400, 200 and 100 nm, and those of the low-J sub c sample are about 200, 100 and 50 nm. Since these two samples have been heat-treated in different manners, it is suggested that sizes of the elliptic cylinders are affected by the heat treatments and this change in scale, as a result, increases or decreases the J sub c characteristics of the samples. (author)

  19. INFLUENCE OF SCATTERED NEUTRON RADIATION ON METROLOGICAL CHARACTERISTICS OF АТ140 NEUTRON CALIBRATION FACILITY

    Directory of Open Access Journals (Sweden)

    D. I. Komar

    2017-01-01

    Full Text Available Today facilities with collimated radiation field are widely used as reference in metrological support of devices for neutron radiation measurement. Neutron fields formed by radionuclide neutron sources. The aim of this research was to study characteristics of experimentally realized neutron fields geometries on АТ140 Neutron Calibration Facility using Monte Carlo method.For calibration, we put a device into neutron field with known flux density or ambient equivalent dose rate. We can form neutron beam from radionuclide fast-neutron source in different geometries. In containercollimator of АТ140 Neutron Calibration Facility we can install special inserts to gather fast-neutron geometry or thermal-neutron geometry. We need to consider neutron scattering from air and room’s walls. We can conduct measurements of neutron field characteristics in several points and get the other using Monte Carlo method.Thermal neutron collimator forms a beam from radionuclide source with a significant amount of neutrons with thermal energies. From found relationship between full neutron flux and distance to neutron source we see that inverse square law is violated. Scattered radiation contribution into total flux increases when we are moving away from neutron source and significantly influences neutron fields characteristics. While source is exposed in shadow-cone geometry neutron specter has pronounced thermal component from wall scattering.In this work, we examined main geometry types used to acquire reference neutron radiation using radionuclide sources. We developed Monte Carlo model for 238Pu-Be neutron source and АТ140 Neutron Calibration Facility’s container-collimator. We have shown the most significant neutron energy distribution factor to be scattered radiation from room’s walls. It leads to significant changes of neutron radiation specter at a distance from the source. When planning location, and installing the facility we should consider

  20. Inelastic Scattering of Neutrons. Vol. II. Proceedings of the Symposium on Inelastic Scattering of Neutrons

    International Nuclear Information System (INIS)

    1965-01-01

    The general technique of using neutron interactions - and in particular the inelastic scattering of neutrons - to study the dynamics of matter, and the interatomic forces which determine dynamics, is now well established. This area of physics research is of increasing interest to developing countries as well as to many advanced research centres of the world. Three international symposia have already been devoted to the subject of neutron inelastic scattering: the first was held in Stockholm in 1957; the second and third were convened by the IAEA in Vienna in October 1960, and in Chalk River, Canada, in September 1962. In view of continuing and expanding activity in this field, the IAEA convened the present Symposium at Bombay from 15 to 19 December 1964 on the invitation of the Government of India and the Indian Atomic Energy Commission. A total of 66 papers representing 15 countries and 1 international organization were presented at Bombay. The meeting concentrated on experimental results and interpretation rather than on equipment and techniques; thus neutron inelastic scattering has ''come of age'' and is indeed now fully established as a versatile and powerful research tool. Gratitude is expressed to authors of papers, chairmen of sessions, and discussion participants for their contributions to the success of the Bombay Symposium

  1. Diverse Neutron Scattering Measurements in Unconventional Superconductors

    Science.gov (United States)

    Carr, Scott

    Superconductivity is an amazing phenomena. Beyond the eye-popping demos and promises of floating trains, it is a macroscopic manifestation of pure quantum physics. Where most quantum effects are smothered by thermal energy even at the lowest of temperatures, superconductivity brings the strangeness of quantum mechanics to reasonably accessible temperatures. An while it does have applications in terms of efficient charge transfer and the production of powerful magnetic fields, this is not why we study it. The mystery of its origin, oddness of its effects, and beauty of its consequences drives us to delve into the richness of this amazing phenomena. One key player in the physics of these exotic superconductors appears to be magnetism. Magnetism is a constant presence in the phase diagrams of exotic superconductors and appears to couple to the superconducting transition in some interesting ways. The details of the connection remain unknown, but it is clear that magnetism, either through static order, fluctuations, or both, is an important aspect of the crystalline environments which foster superconductivity. Through the tool of neutron scattering I investigate this connection across an array or different compounds using a variety of techniques. In this thesis, I conclude on the role of phase separation in superconducting K yFe1.6+xSe2 using neutron diffraction, perform a survey of magnetic excitations across the superconducting phase diagram in NaFe1-xCoxAs with neutron time-of-flight spectroscopy, and reveal new magnetic properties of the old heavy fermion superconductor UPt3 via more traditional neutron measurements.

  2. Internal motions in proteins: A combined neutron scattering and ...

    Indian Academy of Sciences (India)

    Abstract. It is well-known that water plays a major role in the stability and catalytic function of proteins. Both the effect of hydration water on the dynamics of proteins and that of proteins on the dynamics of water have been studied using inelastic neutron scatter- ing. Inelastic neutron scattering is the most direct probe of ...

  3. Small angle polarised neutron scattering investigation of magnetic nanoparticles

    International Nuclear Information System (INIS)

    Bergenti, I.; Deriu, A.; Savini, L.; Bonetti, E.; Spizzo, F.; Hoell, H.

    2003-01-01

    Small angle scattering of polarised neutron (SANSPOL) is a powerful technique for the determination of magnetisation, density and compositional profiles of nanostructured particles. We present here some examples of the magnetic profile determination using the SANSPOL technique and we discuss in detail its advantage with respect to the conventional small angle neutron scattering approach

  4. Inelastic neutron scattering and lattice dynamics of minerals

    Indian Academy of Sciences (India)

    We review current research on minerals using inelastic neutron scattering and lattice dynamics calculations. Inelastic neutron scattering studies in combination with first principles and atomistic calculations provide a detailed understanding of the phonon dispersion relations, density of states and their manifestations in ...

  5. Inelastic neutron scattering and lattice dynamics of minerals

    Indian Academy of Sciences (India)

    Abstract. We review current research on minerals using inelastic neutron scattering and lattice dynamics calculations. Inelastic neutron scattering studies in combination with first principles and atomistic calculations provide a detailed understanding of the phonon dispersion relations, density of states and their ...

  6. Neutron quasielastic scattering from molecular liquids and glasses

    International Nuclear Information System (INIS)

    Bermejo, F.J.; Chahid, A.; Garcia-Hernandez, M.; Martinez, J.L.; Mompean, F.J.; Howells, W.S; Enciso, E.

    1992-01-01

    An overview of the present status of the theory of neutron scattering from disordered molecular systems (liquids and glasses), with the main emphasis on the theoretical modelling of spectral lineshapes, is presented. Applications to several specific cases are described in order to illustrate the capabilities of Quasielastic Neutron Scattering (QENS) for obtaining reliable information about the stochastic dynamics of these systems. (orig.)

  7. Ten year's activity in the field of neutron scattering workshop

    International Nuclear Information System (INIS)

    Hamaguchi, Yoshikazu

    2003-01-01

    'Neutron scattering' is in the frame of the 'Utilization of Research Reactor's of the FNCA (Forum for Nuclear Cooperation in Asia) project, which held the workshops from FY 1992. This report is a summary of the results and activities of neutron scattering workshops and sub-workshops since the start in FY 1992. (author)

  8. Elastic and inelastic scattering of neutrons on 238U nucleus

    Directory of Open Access Journals (Sweden)

    Capote R.

    2014-04-01

    Full Text Available Advanced modelling of neutron induced reactions on the 238U nucleus is aimed at improving our knowledge of neutron scattering. Capture and fission channels are well constrained by available experimental data and neutron standard evaluation. A focus of this contribution is on elastic and inelastic scattering cross sections. The employed nuclear reaction model includes – a new rotational-vibrational dispersive optical model potential coupling the low-lying collective bands of vibrational character observed in even-even actinides; – the Engelbrecht-Weidenmüller transformation allowing for inclusion of compound-direct interference effects; – and a multi-humped fission barrier with absorption in the secondary well described within the optical model for fission. Impact of the advanced modelling on elastic and inelastic scattering cross sections including angular distributions and emission spectra is assessed both by comparison with selected microscopic experimental data and integral criticality benchmarks including measured reaction rates (e.g. JEMIMA, FLAPTOP and BIG TEN. Benchmark calculations provided feedback to improve the reaction modelling. Improvement of existing libraries will be discussed.

  9. ``Skew'' Scattering of Cold Unpolarized Neutrons in Ferromagnetic Crystal

    Science.gov (United States)

    Udalov, Oleg Georgievich

    2013-06-01

    The problem of neutron scattering by a single magnetic atom is theoretically considered in the second order perturbation theory. It is demonstrated that the elastic scattering of unpolarized neutron by a magnetic atom is skewed, i.e., it contains a term including the symmetry of a mixed product of the atom magnetic moment and the wave vectors of incident and scattered neutrons ([\\mbi{k}× \\mbi{k}']\\cdot \\mbi{h}). The problem of dynamical diffraction of unpolarized neutrons by a perfect ferromagnetic crystal is investigated. We consider the case when the Bragg condition is satisfied for two reciprocal lattice vectors. In this situation the neutron skew scattering manifests itself as a dependence of the diffracted beam intensity on the sign of the crystal magnetization. The diffraction of unpolarized neutrons by a Co crystal has been calculated. The change in the intensity through the magnetization reversal in this case is estimated at 40%.

  10. Neutron scattering from 12C in the few-MeV region

    International Nuclear Information System (INIS)

    Smith, A.; Holt, R.; Whalen, J.

    1978-09-01

    Neutron total cross sections of natural carbon are deduced from the observed transmission of approximately monoenergetic neutrons through carbon samples of varying thickness. The measurements extend from approximately equal to 0.1 to 4.5 MeV with resolutions of approximately equal to 2 to 100 keV. Neutron differential-elastic-scattering cross sections of natural carbon are measured from 1.5 to 4.0 MeV at incident-neutron energy intervals of approximately less than 100 keV, over an angular range of approximately equal to 20 to 160 0 and with energy resolutions of 20 to 50 keV. The experimental results are interpreted in terms of a multilevel R-function analysis. Results are compared with the large body of measured and evaluated neutron total and scattering cross sections and scattered neutron polarizations reported in the literature. It is suggested that the observed neutron total and scattering cross sections of carbon are physically consistent and suitable for use as a reference standard in experimental studies of neutron processes. The R-function description should provide a convenient description of neutron total and scattering cross sections of carbon as a function of both angle and energy. 88 references

  11. Optimising polarised neutron scattering measurements--XYZ and polarimetry analysis

    International Nuclear Information System (INIS)

    Cussen, L.D.; Goossens, D.J.

    2002-01-01

    The analytic optimisation of neutron scattering measurements made using XYZ polarisation analysis and neutron polarimetry techniques is discussed. Expressions for the 'quality factor' and the optimum division of counting time for the XYZ technique are presented. For neutron polarimetry the optimisation is identified as analogous to that for measuring the flipping ratio and reference is made to the results already in the literature

  12. Optimising polarised neutron scattering measurements--XYZ and polarimetry analysis

    CERN Document Server

    Cussen, L D

    2002-01-01

    The analytic optimisation of neutron scattering measurements made using XYZ polarisation analysis and neutron polarimetry techniques is discussed. Expressions for the 'quality factor' and the optimum division of counting time for the XYZ technique are presented. For neutron polarimetry the optimisation is identified as analogous to that for measuring the flipping ratio and reference is made to the results already in the literature.

  13. Biophysical aspects of neutron scattering from vibrational modes of proteins

    International Nuclear Information System (INIS)

    Martel, P.

    1992-01-01

    This review describes a major portion of the published work on neutron scattering experiments aimed at measuring large scale motions in proteins. The importance of these motions for enzyme function and oxygen transport is indicated. The theory applicable to each type of neutron scattering measurement is given and results are discussed with a view to biological relevance. New experiments are suggested and a comparison of neutron scattering data is made with results from other techniques such as raman scattering, infrared absorption, photolysis and molecular dynamics simulation. (author)

  14. Current status of neutron scattering facilities in Serpong

    International Nuclear Information System (INIS)

    Ikram, Abarrul

    1999-01-01

    Brief explanation of the research reactor as a neutron source is presented together with its current operation mode. The neutron beam facilities include one diffractometer for residual stress measurement, one diffractometer for single crystal structural determination and texture measurement, one high resolution powder diffractometer, one neutron radiography facility, one triple axis spectrometer, one small angle neutron scattering spectrometer and one high resolution small angle neutron scattering spectrometer. Current status of three instruments mostly related to this workshop, their performances and problems faced in the last year are presented as well as the future plan for refurbishment and development. (author)

  15. Inelastic Neutron Scattering Study of Mn

    Energy Technology Data Exchange (ETDEWEB)

    Zhong, Y.; Sarachik, M.P.; Friedman, J.R.; Robinson, R.A.; Kelley, T.M.; Nakotte, H.; Christianson, A.C.; Trouw, F.; Aubin, S.M.J.; Hendrickson, D.N.

    1998-11-09

    The authors report zero-field inelastic neutron scattering experiments on a 14-gram deuterated sample of Mn{sub 12}-Acetate consisting of a large number of identical spin-10 magnetic clusters. Their resolution enables them to see a series of peaks corresponding to transitions between the anisotropy levels within the spin-10 manifold. A fit to the spin Hamiltonian H = {minus}DS{sub z}{sup 2} + {mu}{sub B}B{center_dot}g{center_dot}S-BS{sub z}{sup 4} + C(S{sub +}{sup 4} + S{sub {minus}}{sup 4}) yields an anisotropy constant D = (0.54 {+-} 0.02) K and a fourth-order diagonal anisotropy coefficient B = (1.2 {+-} 0.1) x 10{sup {minus}3}K. Unlike EPR measurements, their experiments do not require a magnetic field and yield parameters that do not require knowledge of the g-value.

  16. Lattice Waves, Spin Waves, and Neutron Scattering

    Science.gov (United States)

    Brockhouse, Bertram N.

    1962-03-01

    Use of neutron inelastic scattering to study the forces between atoms in solids is treated. One-phonon processes and lattice vibrations are discussed, and experiments that verified the existence of the quantum of lattice vibrations, the phonon, are reviewed. Dispersion curves, phonon frequencies and absorption, and models for dispersion calculations are discussed. Experiments on the crystal dynamics of metals are examined. Dispersion curves are presented and analyzed; theory of lattice dynamics is considered; effects of Fermi surfaces on dispersion curves; electron-phonon interactions, electronic structure influence on lattice vibrations, and phonon lifetimes are explored. The dispersion relation of spin waves in crystals and experiments in which dispersion curves for spin waves in Co-Fe alloy and magnons in magnetite were obtained and the reality of the magnon was demonstrated are discussed. (D.C.W)

  17. Surface scattering efficiency of some common materials for shielding pulsed neutron scattering instruments

    International Nuclear Information System (INIS)

    Bartoli, L.; Becherini, F.; Grazzi, F.; Zoppi, M.

    2009-01-01

    We have measured the surface scattering efficiency of a new ceramic composite, based on boron carbide, that was recently proposed for use as a shielding material for pulsed neutron scattering instrumentation. The results show that, due to a relevant presence of clay material in the composite, the surface scattering efficiency is higher than other common shielding materials, which are used on pulsed neutron scattering instrumentation, and suggest revising the material composition.

  18. Neutron scattering for the analysis of biological structures. Brookhaven symposia in biology. Number 27

    Energy Technology Data Exchange (ETDEWEB)

    Schoenborn, B P [ed.

    1976-01-01

    Sessions were included on neutron scattering and biological structure analysis, protein crystallography, neutron scattering from oriented systems, solution scattering, preparation of deuterated specimens, inelastic scattering, data analysis, experimental techniques, and instrumentation. Separate entries were made for the individual papers.

  19. Neutron scattering from the flux lattice in high temperature superconductors

    International Nuclear Information System (INIS)

    Paul, D.McK.; Forgan, E.M.; Cubitt, R.; Lee, S.L.; Mook, H.A.; Timmins, P.

    1992-01-01

    Neutron scattering has been used to observe diffraction from the flux-line lattice in high temperature superconductors. This technique is particularly useful in such system as it allows observations to be made over a wide range of temperature and magnetic field. Experiments on the systems K 0.4 Ba 0.6 BiO 3 and YBa 2 Cu 3 O 7-δ will be described with applied magnetic fields of up to 4 T and for temperatures from 2 K to Tc. (orig.)

  20. Introduction to the theory of thermal neutron scattering

    CERN Document Server

    Squires, G L

    2012-01-01

    Since the advent of the nuclear reactor, thermal neutron scattering has proved a valuable tool for studying many properties of solids and liquids, and research workers are active in the field at reactor centres and universities throughout the world. This classic text provides the basic quantum theory of thermal neutron scattering and applies the concepts to scattering by crystals, liquids and magnetic systems. Other topics discussed are the relation of the scattering to correlation functions in the scattering system, the dynamical theory of scattering and polarisation analysis. No previous knowledge of the theory of thermal neutron scattering is assumed, but basic knowledge of quantum mechanics and solid state physics is required. The book is intended for experimenters rather than theoreticians, and the discussion is kept as informal as possible. A number of examples, with worked solutions, are included as an aid to the understanding of the text.

  1. Zirconium as a standard for long wavelength neutron scattering

    International Nuclear Information System (INIS)

    Meardon, B.H.

    1977-11-01

    In this report a proposal is made for the use of zirconium as a standard cylindrical calibration sample for long wavelength (>4 A) neutron scattering measurements. Scattering data are presented from vanadium and zirconium samples and the expected scattering at 20 A is discussed using Monte-Carlo simulation techniques. (author)

  2. Multiple small-angle neutron scattering studies of anisotropic materials

    CERN Document Server

    Allen, A J; Long, G G; Ilavsky, J

    2002-01-01

    Building on previous work that considered spherical scatterers and randomly oriented spheroidal scatterers, we describe a multiple small-angle neutron scattering (MSANS) analysis for nonrandomly oriented spheroids. We illustrate this with studies of the multi-component void morphologies found in plasma-spray thermal barrier coatings. (orig.)

  3. Small angle neutron scattering in surface-active agents mixtures

    Science.gov (United States)

    Bulavin, L. A.; Garamus, V. M.; Ostanevich, Yu. M.

    The method of study of micelle structure by small angle neutron scattering is studied. The determination of maximum size, radius of gyration, average scattering density of micelles is presented. The way of study of distribution of scattering density in micelle is described. The problem of micelles interaction is discussed.

  4. Multi-Messenger Observations of Neutron Rich Matter

    Energy Technology Data Exchange (ETDEWEB)

    Horowitz, C. J. [UTK/ORNL/Indiana University

    2012-01-01

    At very high densities, electrons react with protons to form neutron rich matter. This material is central to many fundamental questions in nuclear physics and astrophysics. Moreover, neutron rich matter is being studied with an extraordinary variety of new tools such as the Facility for Rare Isotope Beams (FRIB) and the Laser Interferometer Gravitational Wave Observatory (LIGO). We describe the Lead Radius Experiment (PREX) that uses parity violating electron scattering to measure the neutron radius in 208Pb. This has important implications for neutron stars and their crusts. We discuss X-ray observations of neutron star radii. These also have important implications for neutron rich matter. Gravitational waves (GW) open a new window on neutron rich matter. They come from sources such as neutron star mergers, rotating neutron star mountains, and collective r-mode oscillations. Using large scale molecular dynamics simulations, we find neutron star crust to be very strong. It can support mountains on rotating neutron stars large enough to generate detectable gravitational waves. We believe that combing astronomical observations using photons, GW, and neutrinos, with laboratory experiments on nuclei, heavy ion collisions, and radioactive beams will fundamentally advance our knowledge of compact objects in the heavens, the dense phases of QCD, the origin of the elements, and of neutron rich matter.

  5. Effects of Hot-Spot Geometry on Backscattering and Down-Scattering Neutron Spectra

    Science.gov (United States)

    Mohamed, Z. L.; Mannion, O. M.; Forrest, C. J.; Knauer, J. P.; Anderson, K. S.; Radha, P. B.

    2017-10-01

    The measured neutron spectrum produced by a fusion experiment plays a key role in inferring observable quantities. One important observable is the areal density of an implosion, which is inferred by measuring the scattering of neutrons. This project seeks to use particle-transport simulations to model the effects of hot-spot geometry on backscattering and down-scattering neutron spectra along different lines of sight. Implosions similar to those conducted at the Laboratory of Laser Energetics are modeled by neutron transport through a DT plasma and a DT ice shell using the particle transport codes MCNP and IRIS. Effects of hot-spot geometry are obtained by ``detecting'' scattered neutrons along different lines of sight. This process is repeated for various hot-spot geometries representing known shape distortions between the hot spot and the shell. This material is based upon work supported by the Department of Energy National Nuclear Security Administration under Award Number DE-NA0001944.

  6. Small Angle Scattering in Neutron Imaging—A Review

    Directory of Open Access Journals (Sweden)

    Markus Strobl

    2017-12-01

    Full Text Available Conventional neutron imaging utilizes the beam attenuation caused by scattering and absorption through the materials constituting an object in order to investigate its macroscopic inner structure. Small angle scattering has basically no impact on such images under the geometrical conditions applied. Nevertheless, in recent years different experimental methods have been developed in neutron imaging, which enable to not only generate contrast based on neutrons scattered to very small angles, but to map and quantify small angle scattering with the spatial resolution of neutron imaging. This enables neutron imaging to access length scales which are not directly resolved in real space and to investigate bulk structures and processes spanning multiple length scales from centimeters to tens of nanometers.

  7. Neutron scattering and the search for mechanisms of superconductivity

    DEFF Research Database (Denmark)

    Aeppli, G.; Bishop, D.J.; Broholm, C.

    1999-01-01

    Neutron scattering is a direct probe of mass and magnetization density in solids. We start with a brief review of experimental strategies for determining the mechanisms of superconductivity and how neutron scattering contributed towards our understanding of conventional superconductors. The remai......Neutron scattering is a direct probe of mass and magnetization density in solids. We start with a brief review of experimental strategies for determining the mechanisms of superconductivity and how neutron scattering contributed towards our understanding of conventional superconductors....... The remainder of the article gives examples of neutron results with impact on the search for the mechanism of superconductivity in more recently discovered, 'exotic', materials, namely the heavy fermion compounds and the layered cuprates, (C) 1999 Elsevier Science B.V. All rights reserved....

  8. Applications of californium-252 neutron scattering gauges in petrochemical industry

    International Nuclear Information System (INIS)

    de Monchy, A.R.; Kok, C.A.; van Klaveren, J.A.

    1976-01-01

    Neutron scattering has long been known as a useful means of detecting atomic hydrogen, e.g., in soil moisture determinations. More recently the use of neutron scattering in process industry has increased. Part of this increased usage is due to the advent of californium-252 neutron sources which produce at least two orders of magnitude more neutrons than the classical (alpha-emitter)/Be type of the same activity. A number of typical applications of neutron scattering devices in the petrochemical process industry are discussing, including: (1) level detection of hydrocarbon liquids in steel-walled vessels or reactors; (2) measurements of liquid hold-up in two-phase flow in pipelines; and (3) foam density measurements in a large commercial flasher. In all these applications small californium-252 sources of 1 to 2 micrograms, combined with a helium-3 neutron detector, were used

  9. Impact of the Cryogen Free Revolution on Neutron Scattering Laboratories

    Science.gov (United States)

    Kirichek, Oleg

    A global shortage of helium gas can seriously jeopardise the scientific programmes of neutron scattering laboratories due to the use of cryogenic sample environment in the majority of the neutron scattering experiments. Recently developed cryogen-free technology allows a significant reduction or even a complete elimination of liquid helium consumption. Here we review the impact of the cryogen-free revolution on cryogenic equipment used at large neutron facilities, such as cryostats, dilution refrigerators, superconducting magnets and other cryogenic systems. Particular attention is given to the newly developed superconducting magnets for neutron diffraction and spectroscopy experiments. Use of the cryogen-free approach, as well as cutting-edge superconducting magnet technology and advanced neutron optics allows researcher to achieve extraordinary performance in their experiments, opening up new opportunities in neutron scattering research.

  10. Neutron Brillouin scattering experiments with pulsed neutrons on high resolution chopper spectrometer HRC

    International Nuclear Information System (INIS)

    Itoh, S; Yokoo, T; Endoh, Y; Kawana, D; Kaneko, Y; Tokura, Y; Fujita, M; Yoshida, K; Saito, K; Inami, N; Takeichi, Y; Ono, K

    2014-01-01

    We improved the High Resolution Chopper Spectrometer (HRC), which is installed at MLF in J-PARC, in order to perform neutron Brillouin scattering (NBS) experiments, and successfully demonstrated a feasibility of this method. Gapless spin-wave excitations were observed in La 0.8 Sr 0.2 MnO 3 , which were in good agreement with previous results using single crystals, on the other hand, a large energy gap in the ferromagnetic spin waves was found in SrRuO 3 . Spin-wave peaks in a permanent magnet Nd 2 Fe 14 B were on the dispersion curve determined previously using a single crystal. Excitations, so-called fast sound, in liquid D 2 O were in a good agreement with previous inelastic neutron scattering experiments and the dispersion curve were extended to the lower Q region.

  11. Neutron scattering studies of low dimensional magnetic systems

    DEFF Research Database (Denmark)

    Hansen, Ursula Bengård

    CoCl2 · 2D2O have been investigated with neutron scattering experiments.CoCl2 · 2D2O can be considered a quasi one dimensional Ising system. This means, thatit is a near ideal model material for investigating low dimensional magnetic phenomena.The excitation spectrum of CoCl2 · 2D2O has been...... investigated at low temperaturesand in a longitudinal magnetic eld using neutron spectroscopy. Here we observe thehybridisation of the magnon bound states, inherent to the low dimensional nature ofCoCl2 · 2D2O.At higher temperature, signatures which can be attributed to Magnetic Bloch Oscillationsis observed......The results of this thesis can be divided into two parts, one concerning neutron scatteringstudies of low dimensional magnetic systems and one concerning neutron optics for theEuropean Spallation Source (ESS).In the part concerning low dimensional magnetic systems, three aspects of the dynamicsof...

  12. On the theory of ultracold neutrons scattering by Davydov solitons

    International Nuclear Information System (INIS)

    Brizhik, L.S.

    1984-01-01

    Elastic coherent scattering of ultracold neutrons by Davydov solitons in one-dimensional periodic molecular chains without account of thermal oscillations of chain atoms is studied. It is shown that the expression for the differential cross section of the elastic neutron scattering by Davydov soliton breaks down into two components. One of them corresponds to scattering by a resting soliton, the other is proportional to the soliton velocity and has a sharp maximum in the direction of mirror reflection of neutrons from the chain

  13. Neutron total scattering cross sections of elemental antimony

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1982-11-01

    Neutron total cross sections are measured from 0.8 to 4.5 MeV with broad resolutions. Differential-neutron-elastic-scattering cross sections are measured from 1.5 to 4.0 MeV at intervals of 50 to 200 keV and at scattering angles distributed between 20 and 160 degrees. Lumped-level neutron-inelastic-scattering cross sections are measured over the same angular and energy range. The exPerimental results are discussed in terms of an optical-statistical model and are compared with respective values given in ENDF/B-V

  14. LANSCE '90: the Manuel Lujan Jr. Neutron Scattering Center

    International Nuclear Information System (INIS)

    Pynn, Roger

    1991-01-01

    This paper describes progress that has been made at the Manuel Lujan Jr. Neutron Scattering Center (LANSCE) during the past two years. Presently, LANSCE provides a higher peak neutron flux than any other pulsed spallation neutron source. There are seven spectrometers for neutron scattering experiments that are operated for a national user program sponsored by the U.S. Department of Energy. Two more spectrometers are under construction. Plans have been made to raise the number of beam holes available for instrumentation and to improve the efficiency of the target/moderator system. (author)

  15. LANSCE '90: The Manuel Lujan Jr. Neutron Scattering Center

    International Nuclear Information System (INIS)

    Pynn, R.

    1990-01-01

    This paper describes progress that has been made at the Manuel Lujan Jr. Neutron Scattering Center (LANSCE) during the past two years. Presently, LANSCE provides a higher peak neutron flux than any other pulsed spallation neutron source. There are seven spectrometers for neutron scattering experiments that are operated for a national user program sponsored by the US Department of Energy. Two more spectrometers are under construction. Plans have been made to raise the number of beam holes available for instrumentation and to improve the efficiency of the target/moderator system. 9 refs., 4 figs

  16. Early history of neutron scattering at Oak Ridge

    International Nuclear Information System (INIS)

    Wilkinson, M.K.

    1985-07-01

    Most of the early development of neutron scattering techniques utilizing reactor neutrons occurred at the Oak Ridge National Laboratory during the years immediately following World War II. C.G. Shull, E.O. Wollan, and their associates systematically established neutron diffraction as a quantitative research tool and then applied this technique to important problems in nuclear physics, chemical crystallography, and magnetism. This article briefly summarizes the very important research at ORNL during this period, which laid the foundation for the establishment of neutron scattering programs throughout the world. 47 refs., 10 figs

  17. Neutron scattering studies of magnetic molecular spin clusters

    International Nuclear Information System (INIS)

    Chaboussant, G.; Basler, R.; Sieber, A.; Ochsenbein, S.T.; Guedel, H.-U.

    2004-01-01

    Molecular magnets are crystalline materials made up of interacting magnetic centres within each molecule. Each such 'spin-cluster' is magnetically well isolated from its neighbours due to the surrounding ligands. The resulting magnetic properties are governed by exchange interactions between neighbouring spins and magneto-crystalline anisotropy. We present a brief overview of the salient features observed in three very different molecular magnets (Mn 4 , Ni 12 and V 15 ) where magnetic frustration plays a crucial role. It is demonstrated that Inelastic Neutron Scattering (INS) is an excellent technique to elucidate complex behaviour associated with geometrically frustrated molecular magnets

  18. Application of Incoherent Inelastic Neutron Scattering in Pharmaceutical Analysis

    DEFF Research Database (Denmark)

    Bordallo, Heloisa N.; A. Zakharov, Boris; Boidyreva, E.V.

    2012-01-01

    This study centers on the use of inelastic neutron scattering as an alternative tool for physical characterization of solid pharmaceutical drugs. On the basis of such approach, relaxation processes in the pharmaceutical compound phenacetin (p-ethoxyacetanilide, C(10)H(13)NO(2)) were evidenced...... on heating between 2 and 300 K. By evaluating the mean-square displacement obtained from the elastic fixed window approach, using the neutron backscattering technique, a crossover of the molecular fluctuations between harmonic and nonharmonic dynamical regimes around 75 K was observed. From the temperature...... in the harmonic approximation. The overall spectral profile of the calculated partial contributions to the generalized density of states compares satisfactorily to the experimental spectra in the region of the lattice modes where the intermolecular interactions are expected to play an important role. This study...

  19. Order and disorder in solid oxygen: neutron scattering investigations

    International Nuclear Information System (INIS)

    Dunstetter, F.; Duparc, O.H.; Delapalme, A.

    1996-01-01

    Solid oxygen exists at zero pressure in three crystallographic phases, denoted α, β, γ. Various results have been obtained by neutron scattering in the two disordered β and γ phases. Plastic γ-O 2 has a A15 structure with 8 molecules per unit cell. The molecules, located at 2a and 6c sites, exhibit two different types of disorder of molecular axes: a spherical-like disorder for the 6c molecules, and a disc-like disorder for the 6c molecules. A precise diffraction analysis on large single crystals shows that the disorder of molecular axis of the molecules can be interpreted in terms of localized forbidden orientations, or orientational holes, with a wide disorder among the other orientations. An important contribution of the translation-rotation coupling must be taken into account for the 6c molecules. Analysis of diffuse scattering by both an approximate analytical model and molecular dynamics simulation shows an important contribution to the orientational correlations between 6c - 6c and 2a - 6c molecules. Magnetic disorder can be investigated by neutron polarization analysis of the paramagnetic scattering. The 3D long range antiferromagnetic order of the α phase becomes a 2D short range helicoidal order in the β phase, with a very short 0.5 nm correlation range. In the γ phase, one observes, as in the liquid, a strong antiferromagnetic correlation, with a suggestion of a 1D order along the linear chains of 6c molecules. In all the measured phases, the variation of the scattering intensity with scattering vector q cannot be reproduced at high q by the know magnetic form factor. This suggests the need for a better description of the π orbital and the theoretical magnetic form factor of the molecule

  20. An empirical formula for scattered neutron components in fast neutron radiography

    International Nuclear Information System (INIS)

    Dou Haifeng; Tang Bin

    2011-01-01

    Scattering neutrons are one of the key factors that may affect the images of fast neutron radiography. In this paper, a mathematical model for scattered neutrons is developed on a cylinder sample, and an empirical formula for scattered neutrons is obtained. According to the results given by Monte Carlo methods, the parameters in the empirical formula are obtained with curve fitting, which confirms the logicality of the empirical formula. The curve-fitted parameters of common materials such as 6 LiD are given. (authors)

  1. Inelastic Neutron Scattering from Hydrogen Adsorbed in Carbon

    Science.gov (United States)

    Olsen, Raina; Beckner, Matthew; Taub, Haskell; Pfeifer, Peter; Wexler, Carlos

    2011-03-01

    Inelastic neutron scattering (INS) from adsorbed hydrogen offers a powerful tool to probe the local adsorption environment of storage material. We will show recently measured INS spectra of hydrogen adsorbed on four different carbon samples and discuss the interpretation of their spectral features, using previous theoretical calculations. Both rotational and vibrational transitions can be observed, along with free recoil scattering parallel to the adsorption plane. The spectra from carbon nanotubes and activated carbon are well explained by theory. However, the spectra from PVDC carbon is quite unusual. This material is based upon work supported in part by the Department of Energy under Award Nos. DE-FG02-07ER46411, DE-FG36-08GO18142, and DE-AC02-06CH11357.

  2. Neutron and light scattering studies of polymers adsorbed on laponite

    CERN Document Server

    Nelson, A R J

    2002-01-01

    The adsorption of poly(ethylene oxide) (PEO) and various poly(ethylene oxide)-poly(propylene oxide)-poly(ethylene oxide) (Pluronic) copolymers onto the synthetic clay Laponite, was investigated using Small Angle Neutron Scattering (SANS) and Dynamic Light Scattering (DLS). The Laponite particles are anisotropic, with a relatively high aspect ratio; but are the same order of magnitude in size as the polymer radius of gyration. Consequently, the particles present a radically different adsorption geometry compared to a locally planar interface, that is assumed by the majority of adsorption studies. The PEO homo-polymer formed thin layers, with the layer thickness being much smaller on the face than on the edge of the particle. Furthermore, the face thickness remained constant with increasing molecular weight, unlike the edge thickness, which grew with a small power law dependence on the molecular weight. Although the hydrodynamic thicknesses (DLS) were larger than those observed with SANS, the layer thicknesses ...

  3. On the analysis of Deep Inelastic Neutron Scattering Experiments

    International Nuclear Information System (INIS)

    Blostein, J.J.; Dawidowski, J.; Granada, J.R.

    2001-01-01

    We analyze the different steps that must be followed for data processing in Deep Inelastic Neutron Scattering Experiments. Firstly we discuss to what extent multiple scattering effects can affect the measured peak shape, concluding the an accurate calculation of these effects must be performed to extract the desired effective temperature from the experimental data. We present a Monte Carlo procedure to perform these corrections. Next, we focus our attention on experiments performed on light nuclei. We examine cases in which the desired information is obtained from the observed peak areas, and we analyze the procedure to obtain an effective temperature from the experimental peaks. As a consequence of the results emerging from those cases we trace the limits of validity of the convolution formalism usually employed, and propose a different treatment of the experimental data for this kind of measurements. (author)

  4. Inelastic scattering of 275 keV neutrons by silver

    International Nuclear Information System (INIS)

    Litvinsky, L.L.; Zhigalov, Ya.A.; Krivenko, V.G.; Purtov, O.A.; Sabbagh, S.

    1997-01-01

    Neutron total, elastic and inelastic scattering cross-scattering of Ag at the E n = 275 KeV neutron energy were measured by using the filtered neutron beam of the WWR-M reactor in Kiev. The d-neutron strength function S n2 of Ag was determined from the analysis of all available data in the E n ≤ keV energy region on neutron inelastic scattering cross-sections with excitation of the first isomeric levels I π m = 7/2 + , E m ∼ 90 keV of 107,109 Ag: S n2 = (1.03 ± 0.19) · 10 -4 . (author). 10 refs, 3 figs

  5. Some thoughts on the future of neutron scattering

    International Nuclear Information System (INIS)

    Egelstaff, P.A.

    1991-01-01

    Attendance of ICANS meetings believe that neutron scattering has a bright future, but critics of neutron scattering argue that its practitioners are an aging group, that they use a few, very expensive neutron sources and that the interesting science may be done by other techniques. The ICANS committee asked me to comment on the future of neutron scattering in the light of this contrast. Some comments will be made on the age distribution, on the proper distribution of sources, on the convenient availability of neutron instruments and methods, on the expansion into new areas of science, on applications to industry and on the probable impact of synchrotron sources. It is hoped that these comments will lead to an outward looking discussion on the future. (author)

  6. Applications of neutron scattering in molecular biological research

    International Nuclear Information System (INIS)

    Nierhaus, K.H.

    1984-01-01

    The study of the molecular structure of biological materials by neutron scattering is described. As example the results of the study of the components of a ribosome of Escherichia coli are presented. (HSI) [de

  7. 3rd AINSE neutron scattering conference, Lucas Heights -AINSE Theatre

    International Nuclear Information System (INIS)

    1986-01-01

    Abstracts of papers, the conference program and general information is included in the conference handbook. The program is divided into the following sessions: hydrogeneous and biological materials, industrial applications, phase transitions, magnetism, small angle neutron scattering and new developments

  8. Small-angle neutron scattering studies of sodium butyl benzene

    Indian Academy of Sciences (India)

    Na-NBBS), in aqueous solutions is investigated by small-angle neutron scattering (SANS). Nearly ellipsoidal aggregates of Na-NBBS at concentrations well above its minimum hydrotrope concentration were detected by SANS. The hydrotrope ...

  9. Small-angle neutron scattering studies of sodium butyl benzene ...

    Indian Academy of Sciences (India)

    Na-NBBS), in aqueous solutions is investigated by small-angle neutron scattering (SANS). Nearly ellipsoidal aggregates of Na-NBBS at concentrations well above its minimum hydrotrope concentration were detected by SANS. The hydrotrope ...

  10. A new ceramic material for shielding pulsed neutron scattering instruments

    International Nuclear Information System (INIS)

    Celli, M.; Grazzi, F.; Zoppi, M.

    2006-01-01

    We propose a new ceramic composite, based on boron carbide, to use as a shielding material for pulsed neutron scattering instrumentation. The measured transmission data show characteristics equivalent to crispy mix, a common shielding material used at ISIS (UK)

  11. Spectrum of ferromagnetic transition metal magnetic excitations and neutron scattering

    International Nuclear Information System (INIS)

    Kuzemskij, A.L.

    1979-01-01

    Quantum statistical models of ferromagnetic transition metals as well as methods of their solutions are reviewed. The correspondence of results on solving these models and the data on scattering thermal neutrons in ferromagnetic is discussed

  12. Structural observation of amorphous alloys by neutron diffraction

    International Nuclear Information System (INIS)

    Fukunaga, Toshiharu; Itoh, Keiji

    2006-01-01

    Neutron diffraction is a powerful tool to elucidate the atomic arrangement of amorphous alloys because of characteristic scattering lengths of constituent elements. For hydrogen absorption amorphous alloys H/D isotopic substitution was employed to observe the location of deuterium atoms because the neutron coherent scattering length of deuterium is large enough to observe in comparison with those of the constituent atoms. Moreover, Reverse Monte Carlo (RMC) modeling has been recognized to be an excellent method for visualizing the three-dimensional atomic arrangement of amorphous alloys, based on the results of neutron and X-ray diffraction experiments. Therefore, the combination of neutron, X-ray diffraction experiments and the RMC modeling was used to clarify the topological characteristics of the structure of amorphous alloys. (author)

  13. Set of thermal neutron-scattering experiments for the Weapons Neutron Research Facility

    International Nuclear Information System (INIS)

    Brugger, R.M.

    1975-12-01

    Six classes of experiments form the base of a program of thermal neutron scattering at the Weapons Neutron Research (WNR) Facility. Three classes are to determine the average microscopic positions of atoms in materials and three are to determine the microscopic vibrations of these atoms. The first three classes concern (a) powder sample neutron diffraction, (b) small angle scattering, and (c) single crystal Laue diffraction. The second three concern (d) small kappa inelastic scattering, (e) scattering surface phonon measurements, and (f) line widths. An instrument to couple with the WNR pulsed source is briefly outlined for each experiment

  14. The dynamics of physisorbed layers studied by neutron scattering

    International Nuclear Information System (INIS)

    Nielsen, M.; McTague, J.P.

    1978-01-01

    We discuss the neutron scattering technique applied to the study of adsorbed thin films. Despite the fact that neutrons are scattered very weakly by surfaces, recent studies have shown that both structural and dynamical information can be obtained even for submonolayer coverages. Results will be shown for films of Ar, D 2 , H 2 , and O 2 adsorbed on (001) surfaces of graphite and for H 2 molecules adsorbed on activated alumina. (orig.) [de

  15. Neutron Scattering and Its Application to Strongly Correlated Systems

    OpenAIRE

    Zaliznyak, Igor A.; Tranquada, John M.

    2013-01-01

    Neutron scattering is a powerful probe of strongly correlated systems. It can directly detect common phenomena such as magnetic order, and can be used to determine the coupling between magnetic moments through measurements of the spin-wave dispersions. In the absence of magnetic order, one can detect diffuse scattering and dynamic correlations. Neutrons are also sensitive to the arrangement of atoms in a solid (crystal structure) and lattice dynamics (phonons). In this chapter, we provide an ...

  16. Small-angle neutron scattering study of Fe-B and Fe-Ni-B metallic glasses

    International Nuclear Information System (INIS)

    Cser, L.; Kovacs, I.; Lovas, A.; Svab, E.; Zsigmond, G.

    1982-01-01

    Small-angle scattering of neutron (SANS) was analysed on Fe-B and Fe-Ni-B metallic glass ribbons by means of a double crystal small angle device and a neutron diffractometer. The dimensions of magnetic domains and small clusters were determined. An appreciable anisotropy of SANS intensity and surface scattering was observed. (orig.)

  17. Small-angle neutron scattering study of Fe-B and Fe-Ni-B metallic glasses

    International Nuclear Information System (INIS)

    Cser, L.; Kovacs, I.; Lovas, A.; Svab, E.; Zsigmond, Gy.

    1981-01-01

    Small-angle neutron scattering (SANS) on Fe-B and Fe-Ni-B metallic glass ribbons was analysed by means of a double-crystal small-angle device and a neutron diffractometer. The sizes of magnetic domains and small clusters were determined. An appreciable anisotropy of SANS intensity and surface scattering was observed. (author)

  18. Neutron scattering for materials science. Materials Research Society proceedings

    International Nuclear Information System (INIS)

    Shapiro, S.M.; Moss, S.C.; Jorgensen, J.D.

    1990-01-01

    Neutron Scattering is by now a well-established technique which has been used by condensed matter scientists to probe both the structure and the dynamical interactions in solids and liquids. The use of neutron scattering methods in materials science research has in turn increased dramatically in recent years. The symposium presented in this book was assembled to bring together scientists with a wide range of interest, including high-T c superconducting materials, phase transformations, neutron depth profiling, structure and dynamics of glasses and liquids, surfaces and interfaces, porous media, intercalation compounds and lower dimensional systems, structure and dynamics of polymers, residual stress analysis, ordering and phase separation in alloys, and magnetism in alloys and multilayers. The symposium included talks covering the latest advances in broad areas of interest such as Rietveld structure refinement, triple axis spectrometry, quasi elastic scattering and diffusion, small angle scattering and surface scattering

  19. In-situ soil carbon analysis using inelastic neutron scattering

    Science.gov (United States)

    In situ soil carbon analysis using inelastic neutron scattering (INS) is based on the emission of 4.43 MeV gamma rays from carbon nuclei excited by fast neutrons. This in-situ method has excellent potential for easily measuring soil carbon since it does not require soil core sampling and processing ...

  20. Perspectives of extreme sample environment in neutron scattering ...

    Indian Academy of Sciences (India)

    Perspectives of extreme sample environment in neutron scattering and consequences for instrumentation. MICHAEL STEINER. Hahn-Meitner-Institut Berlin. E-mail: steiner@hmi.de. Abstract. Because neutrons can penetrate bulky pieces of matter, increasingly complex sample environment is requested by the users of ...

  1. A high pressure sample facility for neutron scattering

    International Nuclear Information System (INIS)

    Carlile, C.J.; Glossop, B.H.

    1981-06-01

    Commissioning tests involving deformation studies and tests to destruction as well as neutron diffraction measurements of a standard sample have been carried out on the SERC high pressure sample facility for neutron scattering studies. A detailed description of the pressurising equipment is given. (author)

  2. The measurement of neutron scattering cross sections at small angles

    International Nuclear Information System (INIS)

    Qi, H.Q.; Liu, Y.C.; Chen, Z.P.; Wu, X.C.; Wang, W.H.; Zhang, J.

    1985-08-01

    A position sensitive neutron detector was used to measure the scattering cross sections of 14.7 MeV neutrons from Pb between 3 0 and 9 0 . The method to correct the effects of finite positional resolution by unfolding positional spectrum was studied. (author)

  3. Monitoring of Bainite Transformation Using in Situ Neutron Scattering

    Directory of Open Access Journals (Sweden)

    Hikari Nishijima

    2016-01-01

    Full Text Available Bainite transformation behavior was monitored using simultaneous measurements of dilatometry and small angle neutron scattering (SANS. The volume fraction of bainitic ferrite was estimated from the SANS intensity, showing good agreement with the results of the dilatometry measurements. We propose a more advanced monitoring technique combining dilatometry, SANS and neutron diffraction.

  4. Small Angle Neutron Scattering instrument at Malaysian TRIGA reactor

    Energy Technology Data Exchange (ETDEWEB)

    Shukri Mohd; Razali Kassim; Zal Uyun Mahmood [Malaysian Inst. for Nuclear Technology Research (MINT), Bangi, Kajang (Malaysia); Shahidan Radiman

    1998-10-01

    The TRIGA MARK II Research reactor at the Malaysian Institute for Nuclear Research (MINT) was commissioned in July 1982. Since then various works have been performed to utilise the neutrons produced from this steady state reactor. One of the project involved the Small Angle Neutron Scattering (SANS). (author)

  5. Diffuse Neutron Scattering of the High Temperature Phase of Fe3O4

    OpenAIRE

    Siratori , K.; Ishii , Y.; Morii , Y.; Funahashi , S.; Yanase , A.

    1997-01-01

    Diffuse neutron scattering is observed for the high temperature phase of magnetite, Fe3O4, in an extended range in the (001) and (011) plane of the Brillouin zone. Contours of scattered intensity shows a characteristic pattern, discs in the (100) plane around the Γ points, spheres around the X points, etc. The intensity of this diffuse scattering increases with decreasing temperature down to the Verwey point and is attributed to the lattice distortion induced by charge fluctuation in the B si...

  6. Elastic and Inelastic Scattering of Neutrons using a CLYC array

    Science.gov (United States)

    Brown, Tristan; Doucet, E.; Chowdhury, P.; Lister, C. J.; Wilson, G. L.; Devlin, M.; Mosby, S.

    2015-10-01

    CLYC scintillators, which have dual neutron and gamma response, have recently ushered in the possibility of fast neutron spectroscopy without time-of-flight (TOF). A 16-element array of 1'' x 1'' 6Li-depleted CLYC crystals, where pulse-shape-discrimination is achieved via digital pulse processing, has been commissioned at UMass Lowell. In an experiment at LANSCE, high energy neutrons were used to bombard 56Fe and 238U targets, in order to measure elastic and inelastic neutron scattering cross sections as a function of energy and angle with the array. The array is placed very close to the targets for enhanced geometrical solid angles for scattered neutrons compared to standard neutron-TOF measurements. A pulse-height spectrum of scattered neutrons in the detectors is compared to the energy of the incident neutrons, which is measured via the TOF of the pulsed neutrons from the source to the detectors. Recoil corrections are necessary to combine the energy spectra from all the detectors to obtain angle-integrated elastic and inelastic cross-sections. The detection techniques, analysis procedures and results will be presented. Supported by NNSA-SSAA program through DOE Grant DE-NA00013008.

  7. Small angle neutron scattering from nanometer grain sized materials

    Science.gov (United States)

    Epperson, J. E.; Siegel, R. W.

    1991-11-01

    Small angle neutron scattering has been utilized, along with a number of complementary characterization methods suitable to the nanometer size scale, to investigate the structures of cluster-assembled nanophase materials. Results of these investigations are described and problems and opportunities in using small angle scattering for elucidating nanostructures are discussed.

  8. Introduction to the theory of elastic neutron scattering

    International Nuclear Information System (INIS)

    Blume, M.

    1976-01-01

    A theoretical comparison is made of the experimental techniques used in slow neutron scattering from solids and liquids and those of x-ray scattering, in order to see the similarities and the differences in the information they provide about the structure of matter

  9. Small Angle Scattering in Neutron Imaging : A Review

    NARCIS (Netherlands)

    Strobl, Markus; Harti, Ralph P.; Grünzweig, Christian; Woracek, Robin; Plomp, J.

    2017-01-01

    Conventional neutron imaging utilizes the beam attenuation caused by scattering and absorption through the materials constituting an object in order to investigate its macroscopic inner structure. Small angle scattering has basically no impact on such images under the geometrical conditions applied.

  10. Magnetic dynamics of fine particles studied by inelastic neutron scattering

    CERN Document Server

    Hansen, M F; Moerup, S; Lefmann, K; Clausen, K N; Lindgaard, P A

    2000-01-01

    We give an introduction to inelastic neutron scattering and the dynamic scattering function for magnetic nanoparticles. Differences between ferromagnetic and antiferromagnetic nanoparticles are discussed and we give a review of recent results on ferromagnetic Fe nanoparticles and canted antiferromagnetic alpha-Fe sub 2 O sub 3 nanoparticles.

  11. Neutron scattering from an imperfect flux-line lattice

    International Nuclear Information System (INIS)

    Brandt, E.H.

    1978-01-01

    The diffraction of neutrons from the imperfect vortex lattice of a type-II superconductor is investigated. It is found that flux pinning leads not only to a broadening of the Bragg reflections but also to diffuse scattering into the first Brillouin zone, which at high fields exceeds Bragg scattering

  12. Inelastic neutron scattering for materials science and engineering

    International Nuclear Information System (INIS)

    Shapiro, S.M.

    1995-01-01

    The neutron is the ideal probe for studying the positions and motions of atoms in condensed matter. The main advantage of the neutron in inelastic scattering results from its heavy mass when compared to other particles which are used to probe materials such as the photon (light, x-rays, or γ-rays) or the electron. The author discusses the application of neutron scattering to study a number of different materials related problems, including, hard magnets, shape memory effects, and hydrogen distribution in metals

  13. A high temperature high pressure cell for quasielastic neutron scattering.

    Science.gov (United States)

    Yang, F; Kaplonski, J; Unruh, T; Mamontov, E; Meyer, A

    2011-08-01

    We present our recent development of a high temperature high pressure cell for neutron scattering. Combining a water cooled Nb1Zr pressure cell body with an internal heating furnace, the sample environment can reach temperatures of up to 1500 K at a pressure of up to 200 MPa at the sample position, with an available sample volume of about 700 mm(3). The cell material Nb1Zr is specifically chosen due to its reasonable mechanical strength at elevated temperatures and fairly small neutron absorption and incoherent scattering cross sections. With this design, an acceptable signal-to-noise ratio of about 10:1 can be achieved. This opens new possibilities for quasielastic neutron scattering studies on different types of neutron spectrometers under high temperature high pressure conditions, which is particularly interesting for geological research on, e.g., water dynamics in silicate melts.

  14. An introduction to small-angle neutron scattering

    International Nuclear Information System (INIS)

    Windsor, C.G.

    1988-01-01

    Neutron and X-ray small-angle scattering provide, along with electron microscopy and diffraction, the principal techniques for the microscopic characterization of materials. Neutron, X-ray and electron beams each have quite different properties. In fact, each has unique advantages. The penetration of neutrons through most materials is responsible for many applications. The ever-increasing intensity of available X-ray beams is opening new fields. The advantage of electron beams is their ability to work in both real and reciprocal space. The problems of transforming the results of an experiment in reciprocal space to give an interpretation in real space are central to small-angle scattering, and are discussed. Several examples will be given of the successful use of small-angle neutron scattering applied to problems where other techniques have failed to make a decisive contribution. (orig.)

  15. Neutron inelastic scattering measurements on the stable isotopes of titanium

    Science.gov (United States)

    Olacel, A.; Belloni, F.; Borcea, C.; Boromiza, M.; Dessagne, P.; Henning, G.; Kerveno, M.; Negret, A.; Nyman, M.; Pirovano, E.; Plompen, A. J. M.

    2017-07-01

    The results of a neutron inelastic scattering experiment performed at the Geel Electron Linear Accelerator pulsed white neutron source of the European Commission Joint Research Centre are reported. The neutrons with energies up to 18 MeV interacted with a natTi sample and the γ rays resulting from inelastic scattering reactions on the stable isotopes were detected using the Gamma Array for Inelastic Neutron Scattering (GAINS) spectrometer. We were able to measure the γ -production cross sections for 21 transitions in the five stable Ti isotopes. From these, the level cross sections and the total inelastic cross sections were determined. Our experimental results are compared with theoretical calculations performed using the talys 1.8 code, evaluated nuclear data libraries, and also with previously reported results.

  16. Investigation of ferromagnetic domain structures by neutron small angle scattering

    International Nuclear Information System (INIS)

    Schild, L.

    1984-01-01

    The magnetic small angle scattering of thermal neutrons caused by magnetic refraction at domain walls of ferromagnetic materials without texture has been investigated. Experiments on Fe-Si alloys with a twin crystal diffractometer were carried out. It is shown that the mean extension of magnetic basic units (domains as well as parallel wall systems) can be determined. A comparison of grain sizes determined metallographically with domain sizes obtained by neutron small-angle scattering has shown that neither mean grain size nor domain size can be assessed by small-angle scattering experiments

  17. Small angle neutron scattering study of Linde 80 RPV welds

    International Nuclear Information System (INIS)

    Wirth, B.D.; Odette, G.R.; Lucas, G.E.; Spooner, S.E.

    1999-01-01

    Small angle neutron scattering (SANS) results are presented for Linde 80 welds irradiated, as part of the B and W Owners Group Integrated Surveillance Program, at low fluxes ( 15 n/m 2 -s) to fluences from 0.29 to 3.5 x 10 23 n/m 2 (E > 1 MeV) at irradiation temperatures from 276 to 292 C. The welds all contain about 0.6 Ni (all composition units are in wt.%), 0.009 to 0.18 P and 0.05 to 0.28 Cu. In the welds with significant amounts of copper (>0.2 Cu) the measured defect scattering cross sections were consistent with either: (a) copper rich precipitates (CRPs) alloyed with manganese and nickel; or (b) dominant CRP scattering, plus a weak contribution from so-called matrix defect features. Similar weak scattering was observed in a low copper (0.06 Cu) weld. The identity of matrix defect features cannot be determined from the SANS data alone, but the scattering is consistent with the presence of subnanometer vacancy cluster-solute complexes. The general character of the CRPs, and the trends in their number density, volume fraction and average radius as a function of fluence and irradiation temperature, are very similar to those observed in a wide range of pressure vessel-type steels irradiated in test reactors at intermediate to high flux. The SANS data in the surveillance welds is also in unity with: (a) thermodynamic-kinetic radiation enhanced diffusion models of CRP evolution; (b) mechanical property changes, including predictions of the correlations of the surveillance data base; and (c) an atomic scale, atom probe field ion microscopy study into the nanostructure-chemistry of a CRP

  18. Large volume high-pressure cell for inelastic neutron scattering

    International Nuclear Information System (INIS)

    Wang, W.; Kamenev, K. V.; Sokolov, D. A.; Huxley, A. D.

    2011-01-01

    Inelastic neutron scattering measurements typically require two orders of magnitude longer data collection times and larger sample sizes than neutron diffraction studies. Inelastic neutron scattering measurements on pressurised samples are particularly challenging since standard high-pressure apparatus restricts sample volume, attenuates the incident and scattered beams, and contributes background scattering. Here, we present the design of a large volume two-layered piston-cylinder pressure cell with optimised transmission for inelastic neutron scattering experiments. The design and the materials selected for the construction of the cell enable its safe use to a pressure of 1.8 GPa with a sample volume in excess of 400 mm 3 . The design of the piston seal eliminates the need for a sample container, thus providing a larger sample volume and reduced absorption. The integrated electrical plug with a manganin pressure gauge offers an accurate measurement of pressure over the whole range of operational temperatures. The performance of the cell is demonstrated by an inelastic neutron scattering study of UGe 2 .

  19. Large volume high-pressure cell for inelastic neutron scattering.

    Science.gov (United States)

    Wang, W; Sokolov, D A; Huxley, A D; Kamenev, K V

    2011-07-01

    Inelastic neutron scattering measurements typically require two orders of magnitude longer data collection times and larger sample sizes than neutron diffraction studies. Inelastic neutron scattering measurements on pressurised samples are particularly challenging since standard high-pressure apparatus restricts sample volume, attenuates the incident and scattered beams, and contributes background scattering. Here, we present the design of a large volume two-layered piston-cylinder pressure cell with optimised transmission for inelastic neutron scattering experiments. The design and the materials selected for the construction of the cell enable its safe use to a pressure of 1.8 GPa with a sample volume in excess of 400 mm(3). The design of the piston seal eliminates the need for a sample container, thus providing a larger sample volume and reduced absorption. The integrated electrical plug with a manganin pressure gauge offers an accurate measurement of pressure over the whole range of operational temperatures. The performance of the cell is demonstrated by an inelastic neutron scattering study of UGe(2).

  20. Inelastic scattering of fast neutrons on Fe-56; Inelastische Streuung schneller Neutronen an {sup 56}Fe

    Energy Technology Data Exchange (ETDEWEB)

    Beyer, Roland

    2014-11-24

    The relevant reaction cross sections for the nuclear transmutation will be measured at the neutron flight time facility nELBE in Dresden-Rossendorf. Transmutation by fast neutron irradiation is supposed to reduce the radiotoxicity of high-level radioactive wastes. The thesis is aimed to measure the inelastic neutron scattering cross sections of Fe-56 using a new double flight-time method. With combined plastic and BaF2 scintillation detectors for the first time the emitted neutrons and photons are observed in coincidence.

  1. Spin echo small angle neutron scattering using a continuously pumped (3)He neutron polarisation analyser.

    Science.gov (United States)

    Parnell, S R; Washington, A L; Li, K; Yan, H; Stonaha, P; Li, F; Wang, T; Walsh, A; Chen, W C; Parnell, A J; Fairclough, J P A; Baxter, D V; Snow, W M; Pynn, R

    2015-02-01

    We present a new instrument for spin echo small angle neutron scattering (SESANS) developed at the Low Energy Neutron Source at Indiana University. A description of the various instrument components is given along with the performance of these components. At the heart of the instrument are a series of resistive coils to encode the neutron trajectory into the neutron polarisation. These are shown to work well over a broad range of neutron wavelengths. Neutron polarisation analysis is accomplished using a continuously operating neutron spin filter polarised by Rb spin-exchange optical pumping of (3)He. We describe the performance of the analyser along with a study of the (3)He polarisation stability and its implications for SESANS measurements. Scattering from silica Stöber particles is investigated and agrees with samples run on similar instruments.

  2. Data acquisition system for the neutron scattering instruments at the intense pulsed neutron source

    International Nuclear Information System (INIS)

    Crawford, R.K.; Daly, R.T.; Haumann, J.R.; Hitterman, R.L.; Morgan, C.B.; Ostrowski, G.E.; Worlton, T.G.

    1981-01-01

    The Intense Pulsed Neutron Source (IPNS) at Argonne National Laboratory is a major new user-oriented facility which is now coming on line for basic research in neutron scattering and neutron radiation damage. This paper describes the data-acquisition system which will handle data acquisition and instrument control for the time-of-flight neutron-scattering instruments at IPNS. This discussion covers the scientific and operational requirements for this system, and the system architecture that was chosen to satisfy these requirements. It also provides an overview of the current system implementation including brief descriptions of the hardware and software which have been developed

  3. Earth formation pulsed neutron porosity logging system utilizing epithermal neutron and inelastic scattering gamma ray detectors

    International Nuclear Information System (INIS)

    Smith, H.D. Jr.; Smith, M.P.; Schultz, W.E.

    1978-01-01

    An improved pulsed neutron porosity logging system is provided in the present invention. A logging tool provided with a 14 MeV pulsed neutron source, an epithermal neutron detector and an inelastic scattering gamma ray detector is moved through a borehole. The detection of inelastic gamma rays provides a measure of the fast neutron population in the vicinity of the detector. repetitive bursts of neutrons irradiate the earth formation and, during the busts, inelastic gamma rays representative of the fast neutron population is sampled. During the interval between bursts the epithermal neutron population is sampled along with background gamma radiation due to lingering thermal neutrons. the fast and epithermal neutron population measurements are combined to provide a measurement of formation porosity

  4. Quasielastic Neutron Scattering by Superionic Strontium Chloride

    DEFF Research Database (Denmark)

    Dickens, M. H.; Hutchings, M. T.; Kjems, Jørgen

    1978-01-01

    The scattering, from powder and single crystal samples, appears only above the superionic transition temperature, 1000K. The integrated intensity is found to be strongly dependent on the direction and magnitude of the scattering vector, Q, (which suggests the scattering is coherent) but does not ...

  5. 2010 American Conference on Neutron Scattering (ACNS 2010)

    Energy Technology Data Exchange (ETDEWEB)

    Billinge, Simon

    2011-06-17

    The ACNS provides a focal point for the national neutron user community to strengthen ties within this diverse group, while at the same time promoting neutron research among colleagues in related disciplines identified as “would-be” neutron users. The American Conference on Neutron Scattering thus serves a dual role as a national user meeting and a scientific meeting. As a venue for scientific exchange, the ACNS showcases recent results and provides forums for scientific discussion of neutron research in diverse fields such as hard and soft condensed matter, liquids, biology, magnetism, engineering materials, chemical spectroscopy, crystal structure, and elementary excitations, fundamental physics and development of neutron instrumentation through a combination of invited talks, contributed talks and poster sessions. As a “super-user” meeting, the ACNS fulfills the main objectives of users' meetings previously held periodically at individual national neutron facilities, with the advantage of a larger and more diverse audience. To this end, each of the major national neutron facilities (NIST, LANSCE, HFIR and SNS) have an opportunity to exchange information and update users, and potential users, of their facility. This is also an appropriate forum for users to raise issues that relate to the facilities. For many of the national facilities, this super-user meeting should obviate the need for separate user meetings that tax the time, energy and budgets of facility staff and the users alike, at least in years when the ACNS is held. We rely upon strong participation from the national facilities. The NSSA intends that the American Conference on Neutron Scattering (ACNS) will occur approximately every two years, but not in years that coincide with the International or European Conferences on Neutron Scattering. The ACNS is to be held in association with one of the national neutron centers in a rotating sequence, with the host facility providing local

  6. High magnetic field susceptibility and neutron scattering measurements for ZnFe2O4 single crystal

    International Nuclear Information System (INIS)

    Kamazawa, Kazuya; Nakajima, Kenji; Kohn, Key; Tsunoda, Yorihiko

    2004-01-01

    We studied field dependences of magnetic susceptibility and neutron scattering measurements for frustrated normal spinel ZnFe 2 O 4 . Although a peak which is similar to the antiferromagnetic transition is observed at 13 K in the magnetic susceptibility, there is no magnetic long-range order in our neutron scattering measurements. When we measure the magnetic susceptibility under the high magnetic field, the peak position moves toward the high temperature. In the neutron scattering measurements, magnetic diffuse scattering around the nuclear Bragg peaks disappear under the magnetic field of 3 T

  7. Observation of long-range ferromagnetic order in the heavy-fermion compuound URu/sub 1. 2/Re/sub 0. 8/Si/sub 2/ by neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Torikachvili, M.S.; Rebelsky, L.; Motoya, K.; Shapiro, S.M.; Dalichaouch, Y.; Maple, M.B.

    1989-01-01

    We have performed a neutron scattering study of the heavy-fermion compound URu/sub 1.2/Re/sub 0.8/Si/sub 2/, in order to verify the occurrence of long-range ferromagnetic order. This study consisted of measurements of elastic, inelastic, and polarized neutron scattering, measurement of low-angle critical scattering, and the determination of the temperature dependence of the order parameter. We found a sharp peak in the critical scattering at /approx/ 30 K for the wavevector q = 0.08 /angstrom//sup /minus/1/; and an enhancement of the intensity at the position of the (101) nuclear Bragg reflection below the Curie temperature. These measurements suggest the occurrence of long-range magnetic order. The value of the ordered moment is estimated to be /approx/ 0.53 /mu//sub B/ at 10 K. 17 refs., 3 figs.

  8. The use of neutron scattering to determine the functional structure of glycoside hydrolase.

    Science.gov (United States)

    Nakamura, Akihiko; Ishida, Takuya; Samejima, Masahiro; Igarashi, Kiyohiko

    2016-10-01

    Neutron diffraction provides different information from X-ray diffraction, because neutrons are scattered by atomic nuclei, whereas X-rays are scattered by electrons. One of the key advantages of neutron crystallography is the ability to visualize hydrogen and deuterium atoms, making it possible to observe the protonation state of amino acid residues, hydrogen bonds, networks of water molecules and proton relay pathways in enzymes. But, because of technical difficulties, less than 100 enzyme structures have been evaluated by neutron crystallography to date. In this review, we discuss the advantages and disadvantages of neutron crystallography as a tool to investigate the functional structure of glycoside hydrolases, with some examples. Copyright © 2016 Elsevier Ltd. All rights reserved.

  9. Small angle neutron scattering of micro- and nanostructured materials

    International Nuclear Information System (INIS)

    Trinker, M.

    2006-05-01

    In this work studies of micro- and nanostructured materials by means of neutron scattering techniques are presented. The first part contains the theory of neutron scattering by structures in condensed matter necessary for the understanding of the experimental results. The method of small angle neutron scattering (SANS) is applied to a sample of highly irradiated SiC/SiCf composite. These materials play an important role in concepts for future fusion reactors. Radiation induced structural changes after high-dose irradiation in the spallation target of the SINQ neutron source, Switzerland, are analyzed. For testing instruments and methods used in ultra-small angle neutron scattering (USANS) artificial microstructured samples fabricated from silicon are particularly suitable. Because of the known structure parameters and the model-like character of such samples the performance of the instruments involved and the models used for interpretation of the scattering data can be tested. The development and fabrication of a series of such silicon gratings at the Center for Micro- and Nanostructures (ZMNS) of the Vienna University of Technology are described. The following USANS measurements at the instrument S18 of the Institute Laue-Langevin, Grenoble, which is run by the Atomic Institute of the Austrian Universities, and the instrument itself are presented. Subsequently the results are compared to those of the newly developed spinecho small angle neutron scattering technique (SESANS) at the Delft University of Technology. The complementarity of both techniques is demonstrated by means of the scattering data obtained from the silicon gratings. A method for the direct reconstruction of one-dimensional scattering length density distributions is applied to the USANS scattering data of the silicon microstructures. The results are compared to those obtained from scanning electron microscopy and the applicability of the method to USANS scattering data for the reconstruction of one

  10. The liquids nitrogen, oxygen and helium-4 studied by neutron scattering

    International Nuclear Information System (INIS)

    Pedersen, K.S.

    1980-01-01

    The work falls in three parts: Neutron diffraction on liquid nitrogen and liquid oxygen; Neutron inelastic scattering on liquid nitrogen; Neutron inelastic scattering on liquid 4 He. Most of the work has been related to the neutron inelastic scattering experiments on liquid nitrogen. (Auth.)

  11. Experimental studies of the critical scattering of neutrons for large scattering vectors

    International Nuclear Information System (INIS)

    Ciszewski, R.

    1972-01-01

    The most recent results concerned with the critical scattering of neutrons are reviewed. The emphasis is on the so-called thermal shift, that is the shift of the main maximum in the intensity of critically scattered neutrons with temperature changes. Four theories of this phenomenon are described and their shortcomings are shown. It has been concluded that the situation is involved at present and needs further theoretical and experimental study. (S.B.)

  12. Toward a new polyethylene scattering law determined using inelastic neutron scattering

    International Nuclear Information System (INIS)

    Lavelle, C.M.; Liu, C.-Y.; Stone, M.B.

    2013-01-01

    Monte Carlo neutron transport codes such as MCNP rely on accurate data for nuclear physics cross-sections to produce accurate results. At low energy, this takes the form of scattering laws based on the dynamic structure factor, S(Q,E). High density polyethylene (HDPE) is frequently employed as a neutron moderator at both high and low temperatures, however the only cross-sections available are for ambient temperatures (∼300K), and the evaluation has not been updated in quite some time. In this paper we describe inelastic neutron scattering measurements on HDPE at 5 and 294 K which are used to improve the scattering law for HDPE. We review some of the past HDPE scattering laws, describe the experimental methods, and compare computations using these models to the measured S(Q,E). The total cross-section is compared to available data, and the treatment of the carbon secondary scatterer as a free gas is assessed. We also discuss the use of the measurement itself as a scattering law via the one phonon approximation. We show that a scattering law computed using a more detailed model for the Generalized Density of States (GDOS) compares more favorably to this experiment, suggesting that inelastic neutron scattering can play an important role in both the development and validation of new scattering laws for Monte Carlo work. -- Highlights: ► Polyethylene at 5 K and 300 K is measured using inelastic neutron scattering (INS). ► Measurements conducted at the Wide Angular-Range Chopper Spectrometer at SNS. ► Several models for Polyethylene are compared to measurements. ► Improvements to existing models for the polyethylene scattering law are suggested. ► INS is shown to be highly valuable tool for scattering law development

  13. Neutron scattering at the high-flux isotope reactor

    International Nuclear Information System (INIS)

    Cable, J.W. Chakoumakos, B.C.; Dai, P.

    1995-01-01

    The title facilities offer the brightest source of neutrons in the national user program. Neutron scattering experiments probe the structure and dynamics of materials in unique and complementary ways as compared to x-ray scattering methods and provide fundamental data on materials of interest to solid state physicists, chemists, biologists, polymer scientists, colloid scientists, mineralogists, and metallurgists. Instrumentation at the High- Flux Isotope Reactor includes triple-axis spectrometers for inelastic scattering experiments, a single-crystal four diffractometer for crystal structural studies, a high-resolution powder diffractometer for nuclear and magnetic structure studies, a wide-angle diffractometer for dynamic powder studies and measurements of diffuse scattering in crystals, a small-angle neutron scattering (SANS) instrument used primarily to study structure-function relationships in polymers and biological macromolecules, a neutron reflectometer for studies of surface and thin-film structures, and residual stress instrumentation for determining macro- and micro-stresses in structural metals and ceramics. Research highlights of these areas will illustrate the current state of neutron science to study the physical properties of materials

  14. X-ray and Neutron Scattering of Water.

    Science.gov (United States)

    Amann-Winkel, Katrin; Bellissent-Funel, Marie-Claire; Bove, Livia E; Loerting, Thomas; Nilsson, Anders; Paciaroni, Alessandro; Schlesinger, Daniel; Skinner, Lawrie

    2016-07-13

    This review article focuses on the most recent advances in X-ray and neutron scattering studies of water structure, from ambient temperature to the deeply supercooled and amorphous states, and of water diffusive and collective dynamics, in disparate thermodynamic conditions and environments. In particular, the ability to measure X-ray and neutron diffraction of water with unprecedented high accuracy in an extended range of momentum transfers has allowed the derivation of detailed O-O pair correlation functions. A panorama of the diffusive dynamics of water in a wide range of temperatures (from 400 K down to supercooled water) and pressures (from ambient up to multiple gigapascals) is presented. The recent results obtained by quasi-elastic neutron scattering under high pressure are compared with the existing data from nuclear magnetic resonance, dielectric and infrared measurements, and modeling. A detailed description of the vibrational dynamics of water as measured by inelastic neutron scattering is presented. The dependence of the water vibrational density of states on temperature and pressure, and in the presence of biological molecules, is discussed. Results about the collective dynamics of water and its dispersion curves as measured by coherent inelastic neutron scattering and inelastic X-ray scattering in different thermodynamic conditions are reported.

  15. Studies on biological macromolecules by neutron inelastic scattering

    International Nuclear Information System (INIS)

    Fujiwara, Satoru; Nakagawa, Hiroshi

    2013-01-01

    Neutron inelastic scattering techniques, including quasielastic and elastic incoherent neutron scattering, provide unique tools to directly measure the protein dynamics at a picosecond time scale. Since the protein dynamics at this time scale is indispensable to the protein functions, elucidation of the protein dynamics is indispensable for ultimate understanding of the protein functions. There are two complementary directions of the protein dynamics studies: one is to explore the physical basis of the protein dynamics using 'model' proteins, and the other is more biology-oriented. Examples of the studies on the protein dynamics with neutron inelastic scattering are described. The examples of the studies in the former direction include the studies on the dynamical transitions of the proteins, the relationship between the protein dynamics and the hydration water dynamics, and combined analysis of the protein dynamics with molecular dynamics simulation. The examples of the studies in the latter direction include the elastic incoherent and quasielastic neutrons scattering studies of actin. Future prospects of the studies on the protein dynamics with neutron scattering are briefly described. (author)

  16. Development of new methods for studying nanostructures using neutron scattering

    International Nuclear Information System (INIS)

    Pynn, Roger

    2016-01-01

    The goal of this project was to develop improved instrumentation for studying the microscopic structures of materials using neutron scattering. Neutron scattering has a number of advantages for studying material structure but suffers from the well-known disadvantage that neutrons' ability to resolve structural details is usually limited by the strength of available neutron sources. We aimed to overcome this disadvantage using a new experimental technique, called Spin Echo Scattering Angle Encoding (SESAME) that makes use of the neutron's magnetism. Our goal was to show that this innovation will allow the country to make better use of the significant investment it has recently made in a new neutron source at Oak Ridge National Laboratory (ORNL) and will lead to increases in scientific knowledge that contribute to the Nation's technological infrastructure and ability to develop advanced materials and technologies. We were successful in demonstrating the technical effectiveness of the new method and established a baseline of knowledge that has allowed ORNL to start a project to implement the method on one of its neutron beam lines.

  17. Monte Carlo simulation of fast neutron scattering experiments including DD-breakup neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Schmidt, D.; Siebert, B.R.L.

    1993-06-01

    The computational simulation of the deuteron breakup in a scattering experiment has been investigated. Experimental breakup spectra measured at 16 deuteron energies and at 7 angles for each energy served as the data base. Analysis of these input data and of the conditions of the scattering experiment made it possible to reduce the input data. The use of one weighted breakup spectrum is sufficient to simulate the scattering spectra at one incident neutron energy. A number of tests were carried out to prove the validity of this result. The simulation of neutron scattering on carbon, including the breakup, was compared with measured spectra. Differences between calculated and measured spectra were for the most part within the experimental uncertainties. Certain significant deviations can be attributed to erroneous scattering cross sections taken from an evaluation and used in the simulation. Scattering on higher-lying states in [sup 12]C can be analyzed by subtracting the simulated breakup-scattering from the experimental spectra. (orig.)

  18. Monte Carlo simulation of fast neutron scattering experiments including DD-breakup neutrons

    International Nuclear Information System (INIS)

    Schmidt, D.; Siebert, B.R.L.

    1993-06-01

    The computational simulation of the deuteron breakup in a scattering experiment has been investigated. Experimental breakup spectra measured at 16 deuteron energies and at 7 angles for each energy served as the data base. Analysis of these input data and of the conditions of the scattering experiment made it possible to reduce the input data. The use of one weighted breakup spectrum is sufficient to simulate the scattering spectra at one incident neutron energy. A number of tests were carried out to prove the validity of this result. The simulation of neutron scattering on carbon, including the breakup, was compared with measured spectra. Differences between calculated and measured spectra were for the most part within the experimental uncertainties. Certain significant deviations can be attributed to erroneous scattering cross sections taken from an evaluation and used in the simulation. Scattering on higher-lying states in 12 C can be analyzed by subtracting the simulated breakup-scattering from the experimental spectra. (orig.)

  19. Small angle neutron scattering and small angle X-ray scattering ...

    Indian Academy of Sciences (India)

    Abstract. The morphology of carbon nanofoam samples comprising platinum nanopar- ticles dispersed in the matrix was characterized by small angle neutron scattering (SANS) and small angle X-ray scattering (SAXS) techniques. Results show that the structure of pores of carbon matrix exhibits a mass (pore) fractal nature ...

  20. Small angle neutron scattering and small angle X-ray scattering ...

    Indian Academy of Sciences (India)

    Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400 085, India. *Corresponding author ... ticles dispersed in the matrix was characterized by small angle neutron scattering (SANS) and small angle X-ray ... for scattering from rough pore–mass interfaces, α > 3 and the (surface) fractal dimension Ds = 6 ...

  1. Small angle neutron scattering and small angle X-ray scattering ...

    Indian Academy of Sciences (India)

    2015-11-27

    Nov 27, 2015 ... Small angle neutron scattering and small angle X-ray scattering studies of platinum-loaded carbon foams. P U Sastry V K Aswal A G Wagh ... Proceedings of the International Workshop/Conference on Computational Condensed Matter Physics and Materials Science (IWCCMP-2015). Posted on November ...

  2. Data reduction for time-of-flight small-angle neutron scattering with virtual neutrons

    Science.gov (United States)

    Du, Rong; Tian, Haolai; Zuo, Taisen; Tang, Ming; Yan, Lili; Zhang, Junrong

    2017-09-01

    Small-angle neutron scattering (SANS) is an experimental technique to detect material structures in the nanometer to micrometer range. The solution of the structural model constructed from SANS strongly depends on the accuracy of the reduced data. The time-of-flight (TOF) SANS data are dependent on the wavelength of the pulsed neutron source. Therefore, data reduction must be handled very carefully to transform measured neutron events into neutron scattering intensity. In this study, reduction algorithms for TOF SANS data are developed and optimized using simulated data from a virtual neutron experiment. Each possible effect on the measured data is studied systematically, and suitable corrections are performed to obtain high-quality data. This work will facilitate scientific research and the instrument design at China Spallation Neutron Source.

  3. Fragility of complexity biophysical systems by neutron scattering

    International Nuclear Information System (INIS)

    Magazu, Salvatore; Migliardo, Federica; Bellocco, Ersilia; Lagana, Giuseppina; Mondelli, Claudia

    2006-01-01

    Neutron scattering is an exceptional tool to investigate structural and dynamical properties of systems of biophysical interest, such as proteins, enzymes, lipids and sugars. Moreover, elastic neutron scattering enhances the investigation of atomic motions in hydrated proteins in a wide temperature range and on the picosecond timescale. Homologous disaccharides, such as trehalose, maltose and sucrose, are cryptobiotic substances, since they allow to many organisms to undergo in a 'suspended life' state, known as cryptobiosis in extreme environmental conditions. The present paper is aimed to discuss the fragility degree of disaccharides, as evaluated of the temperature dependence of the mean square displacement by elastic neutron scattering, in order to link this feature with their bioprotective functions

  4. Birefringent neutron prisms for spin echo scattering angle measurement

    Science.gov (United States)

    Pynn, Roger; Fitzsimmons, M. R.; Lee, W. T.; Stonaha, P.; Shah, V. R.; Washington, A. L.; Kirby, B. J.; Majkrzak, C. F.; Maranville, B. B.

    2009-09-01

    In the first decade of the 19th century, an English chemist, William Wollaston, invented an arrangement of birefringent prisms that splits a beam of light into two spatially separated beams with orthogonal polarizations. We have constructed similar devices for neutrons using triangular cross-section solenoids and employed them for Spin Echo Scattering Angle Measurement (SESAME). A key difference between birefringent neutron prisms and their optical analogues is that it is hard to embed the former in a medium which has absolutely no birefringence because this implies the removal of all magnetic fields. We have overcome this problem by using the symmetry properties of the Wollaston neutron prisms and of the overall spin echo arrangement. These symmetries cause a cancellation of Larmor phase aberrations and provide robust coding of neutron scattering angles with simple equipment.

  5. Neutron scattering in soft matter physics and chemistry

    International Nuclear Information System (INIS)

    White, J.W.

    1999-01-01

    Recent experiments area of soft matter science show that self assembly on the micron scale as well as the nanometer scale can be directed chemically. This lecture illustrates how such processes can be studied using the contrast variation available in neutron scattering through isotopic replacement and the techniques of neutron small angle scattering and neutron reflectivity. Related dynamical information at nanometer resolution and on time scales between a nanosecond and a few tenths of a picosecond will become accessible with brighter neutron sources. The examples presented concern the template induced crystallisation of zeolites, the liquid crystal template induced synthesis of mesoporous materials and the structure of thin films at the air water interface. (J.P.N.)

  6. Neutron scattering: a necessary tool for understanding engineering materials

    International Nuclear Information System (INIS)

    Zhang Changsheng; Peng Mei; Sun Guang'ai

    2015-01-01

    In engineering materials science, it is extremely challenging to construct the relationship between the 'microstructures and internal stresses' inside materials and the 'macroscopic performance and service life' of components. Up to now, neutrons have been the only probe for bulk materials that allows engineers and material scientists to acquire information nondestructively about the size and density of the microstructures and three-dimensional distribution of internal stresses deep inside materials. Neutron diffraction stress analysis and small angle neutron scattering are recognized to be of essential value. This article reviews briefly the development, applications and future of these techniques. The neutron scattering instrumentation that will be completed in China in the near future will provide a platform for innovative research for multidisciplinary users, and play a lasting fundamental role in the nation's major engineering fields. (authors)

  7. Probing spin frustration in high-symmetry magnetic nanomolecules by inelastic neutron scattering

    DEFF Research Database (Denmark)

    Garlea, V.O.; Nagler, S.E.; Zarestky, J.L.

    2006-01-01

    Low temperature inelastic neutron scattering studies have been performed to characterize the low energy magnetic excitation spectrum of the magnetic nanomolecule {Mo(72)Fe(30)}. This unique highly symmetric cluster features spin frustration and is one of the largest discrete magnetic molecules...... of the temperature dependence of the observed neutron scattering are explained by a quantum model of the frustrated spin cluster. However, no satisfactory theoretical explanation is yet available for the observed magnetic field dependence....... studied to date by inelastic neutron scattering. The 30 s=5/2 Fe(III) ions, embedded in a spherical polyoxomolybdate molecule, occupy the vertices of an icosidodecahedron and are coupled via nearest-neighbor antiferromagnetic interactions. The overall energy scale of the excitation and the gross features...

  8. Neutron scattering study of layered silicates pillared with alkylamnonium ions

    International Nuclear Information System (INIS)

    Neumann, D.A.; Rush, J.J.; Nicol, J.M.; Wada, N.; Fan, Y.; Kim, H.; Solin, S.; Pinnavaia, P.; Trevino, S.F.

    1990-01-01

    Incoherent, inelastic neutron scattering has been used to study the vibrational spectra of tetramethylammonium montmorillonite and trimethylammonium vermiculite in the energy range 20-140 meV. For both systems peaks are observed due to the internal modes of the intercalate and to the excitations of the hydroxyl groups within the host layers. For the montmorillonite sample, it is found that the steric constraints imposed on the tetramethylammonium ion by the bounding clay layers contribute an additional 28 meV to the rational barrier of the methyl groups. This tetramethylammonium ion occupies. For the trimethylammonium vermiculite sample normal mode analysis of the internal modes of the intercalated ion shows that the N-H bond is parallel to the c-axis of the host

  9. Neutron scattering study on amorphous magnetics

    International Nuclear Information System (INIS)

    Toperverg, B.P.

    1982-01-01

    The study on the ferromagnetic metallic glasses by means of neutron ssattering method is reviewed. Disordered ferromagnetics are considered with allowance for exchange interactione anisotropic interaction being neglected. Phase transformations in the systemS are discussed as well as the existence of the spin glass state from the data of various neutron experiments. The validity of the Sherrington-Kirkpatric state diagram is analyzed

  10. Chemical shift of neutron resonances and some ideas on neutron resonances and scattering theory

    International Nuclear Information System (INIS)

    Ignatovich, V.K.; )

    2002-01-01

    The dependence of positions of neutron resonances in nuclei in condensed matter on chemical environment is considered. A possibility of theoretical description of neutron resonances, different from R-matrix theory is investigated. Some contradictions of standard scattering theory are discussed and a new approach without these contradictions is formulated [ru

  11. The neutron spin-echo spectrometer: a new high resolution technique in neutron scattering

    International Nuclear Information System (INIS)

    Nicholson, L.K.

    1981-01-01

    The neutron spin-echo (NSE) spectrometer provides the highest energy resolution available in neutron scattering experiments. The article describes the principles behind the first NSE spectrometer (at the Institute Laue-Langevin, Grenoble, France) and, as an example of one of its applications, some recent results on polymer chain dynamics are presented. (author)

  12. Inelastic neutron scattering facilities at the Budapest Neutron Center

    Energy Technology Data Exchange (ETDEWEB)

    Toeroek, Gy.; Nagy, A. [Research Institute for Solid State Physics and Optics, P.O.B.49, 1525 Budapest (Hungary); Lebedev, V.T.; Gordeev, G.P. [Petersburg Nuclear Physics Institute, 188300 Gatchina (Russian Federation); Zsigmond, G. [Hahn Meitner Institute, Glienicker str 100, 14109 Berlin (Germany)

    2004-11-01

    Two Triple Axis spectrometers are commissioned now at the Budapest Neutron Center. The Thermal Triple Axis Spectrometer (TAST) is installed on the 8-th beam (60 mm diameter) and supplied with a 120 mm-long sapphire crystal placed inside the channel (2 m far from monochromator) to filter fast neutrons. The Eulerian cradle can be placed at the sample position to carry out holographic measurements. Otherwise a normal goniometer (carrying up to 100 kg weight for orientation, e.g. Cryostat/magnet/heavy sample) is used. This spectrometer's resolution was modeled by VITESS program package. The second (cold) neutron spectrometer (ATHOS) on a curved (4200 m) neutron guide is mounted at the 19 m-position from the cold source. The neutron guide 1.5{theta}{sub c}, made of boron glass, is coated with NiTi multilayer. This instrument, developed into the RITA-type spectrometer, is supplied with a 190 x 190 mm{sup 2} position sensitive detector and a polarization option (stacked polarizer). In addition it has the optional COMPACT Neutron Spin Echo setup, based on Larmor precession, for energy analysis with the resolution of 10 {mu}eV. The test measurements are presented. (copyright 2004 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  13. Magnetic nanostructures studied by polarized small angle neutron scattering

    International Nuclear Information System (INIS)

    Wiedenmann, Albrecht; Kammel, Martin; Heinemann, Andre

    2005-01-01

    Small Angle Neutron Scattering using polarised neutrons is introduced as a contrast variation technique for magnetic systems. The potential of this technique is illustrated on diluted Ferrofluids. Composition, magnetization and size distributions of magnetic core-shell composite particles and magnetic aggregates could be precisely evaluated beside non-magnetic micelles and free surfactants of similar sizes. Structure factors have been extracted which revealed a local pseudo-crystalline ordering of the magnetic particles induced by magnetic fields

  14. Thermal neutron scattering studies of condensed matter under high pressures

    International Nuclear Information System (INIS)

    Carlile, C.J.; Salter, D.C.

    1978-01-01

    Although temperature has been used as a thermodynamic variable for samples in thermal neutron scattering experiments since the inception of the neutron technique, it is only in the last decade that high pressures have been utilised for this purpose. In the paper the problems particular to this field of work are outlined and a review is made of the types of high-pressure cells used and the scientific results obtained from the experiments. 103 references. (author)

  15. Some Notes on Neutron Up-Scattering and the Doppler-Broadening of High-Z Scattering Resonances

    Energy Technology Data Exchange (ETDEWEB)

    Parsons, Donald Kent [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-09-28

    When neutrons are scattered by target nuclei at elevated temperatures, it is entirely possible that the neutron will actually gain energy (i.e., up-scatter) from the interaction. This phenomenon is in addition to the more usual case of the neutron losing energy (i.e., down-scatter). Furthermore, the motion of the target nuclei can also cause extended neutron down-scattering, i.e., the neutrons can and do scatter to energies lower than predicted by the simple asymptotic models. In recent years, more attention has been given to temperature-dependent scattering cross sections for materials in neutron multiplying systems. This has led to the inclusion of neutron up-scatter in deterministic codes like Partisn and to free gas scattering models for material temperature effects in Monte Carlo codes like MCNP and cross section processing codes like NJOY. The free gas scattering models have the effect of Doppler Broadening the scattering cross section output spectra in energy and angle. The current state of Doppler-Broadening numerical techniques used at Los Alamos for scattering resonances will be reviewed, and suggestions will be made for further developments. The focus will be on the free gas scattering models currently in use and the development of new models to include high-Z resonance scattering effects. These models change the neutron up-scattering behavior.

  16. A more informative approach for characterization of polymer monolithic phases: small angle neutron scattering/ultrasmall angle neutron scattering.

    Science.gov (United States)

    Ford, Kathleen M; Konzman, Brian G; Rubinson, Judith F

    2011-12-15

    Neutron scattering techniques have been used frequently to characterize geological specimens and to determine the structures of glasses and of polymers as solutions, suspensions, or melts. Little work has been reported on their application in determining polymers' structural properties relevant to separations. Here, we present a comparison of characterization results from nitrogen porosimetry and from combined small angle neutron scattering (SANS) and ultrasmall angle neutron scattering (USANS) experiments. We show that SANS is extremely sensitive to the pore characteristics. Both approaches can provide information about porosity and pore characteristics, but the neutron scattering techniques provide additional information in the form of the surface characteristics of the pores and their length scales. Fits of the scattering data show that cylindrical pores are present with diameters down to 0.6 μm and that, for length scales down to approxmately 20 Å, the material shows self-similar (fractal) slopes of -3.4 to -3.6. Comparison of these characteristics with other examples from the scattering literature indicate that further investigation of their meaning for chromatographic media is required.

  17. Activity report on neutron scattering research. V. 1, 1994

    International Nuclear Information System (INIS)

    Fujii, Y.; Oohara, Y.

    1994-09-01

    In April, 1993, the Neutron Scattering Laboratory attached to the Institute for Solid State Physics, University of Tokyo, was newly established in Tokai, Ibaraki Prefecture, to promote nationwide users' programs for utilizing the university-owned neutron instruments installed at the JRR-3M reactor of Japan Atomic Energy Research Institute. This upgraded reactor (20 MW, the cold source is installed) has drastically expanded the number of users and research areas since 1990 when it became operational. Currently 8 and 3 out of 18 new spectrometers in total at the JRR-3M are owned by ISSP and Tohoku University, respectively, while the remaining 7 spectrometers belong to JAERI. In addition, 3 conventional spectrometers in the 30 years old JRR-2 reactor (10 MW) have also supported research activities. This is the first issue of 'Activity report on neutron scattering research', and it is to be published annually. In this report, the brief history of neutron scattering research, the users' programs, the committees, the neutron scattering instruments available at the JRR-3M and the JRR-2M, the activity reports on structures and excitation, magnetism, superconductors, liquid and glass, material science, polymers, biology and instrumentation, and publication list are reported. (K.I.)

  18. Quasielastic neutron scattering in biology: Theory and applications.

    Science.gov (United States)

    Vural, Derya; Hu, Xiaohu; Lindner, Benjamin; Jain, Nitin; Miao, Yinglong; Cheng, Xiaolin; Liu, Zhuo; Hong, Liang; Smith, Jeremy C

    2017-01-01

    Neutrons scatter quasielastically from stochastic, diffusive processes, such as overdamped vibrations, localized diffusion and transitions between energy minima. In biological systems, such as proteins and membranes, these relaxation processes are of considerable physical interest. We review here recent methodological advances and applications of quasielastic neutron scattering (QENS) in biology, concentrating on the role of molecular dynamics simulation in generating data with which neutron profiles can be unambiguously interpreted. We examine the use of massively-parallel computers in calculating scattering functions, and the application of Markov state modeling. The decomposition of MD-derived neutron dynamic susceptibilities is described, and the use of this in combination with NMR spectroscopy. We discuss dynamics at very long times, including approximations to the infinite time mean-square displacement and nonequilibrium aspects of single-protein dynamics. Finally, we examine how neutron scattering and MD can be combined to provide information on lipid nanodomains. This article is part of a Special Issue entitled "Science for Life" Guest Editor: Dr. Austen Angell, Dr. Salvatore Magazù and Dr. Federica Migliardo. Copyright © 2016 Elsevier B.V. All rights reserved.

  19. Ultra-small-angle scattering with polarized neutrons

    International Nuclear Information System (INIS)

    Jericha, E.; Badurek, G.; Trinker, M.

    2007-01-01

    Ultra-small-angle neutron scattering (USANS) has been established as an effective technique for the study of structures in the micrometre range in recent years. Consequentially this method has been extended to magnetic structures of corresponding size. We present the instrument arrangement and first experimental results. The instrument itself is a double crystal diffractometer in Bonse-Hart configuration which takes advantage of the narrow angular width of the perfect crystal reflection to obtain an extremely high angular resolution of the scattering vector. The neutrons are loss-free polarized by permanent magnetic prisms located between the monochromator crystal and the sample. Neutrons with opposite polarization are separated to a large extent and their different scattering behaviour may be studied in a single measurement without additional manipulation of the neutron spin. In this manner we are able to separate the magnetic and nuclear contribution to the scattering. We present first exemplifying measurements on ferromagnetic rods and wires, and on soft-magnetic ribbons. Related experiments were performed at the USANS facility of the TRIGA reactor at the Vienna University of Technology and at the combined neutron interferometer/USANS instrument S18 at the ILL, Grenoble

  20. Ultra-small-angle scattering with polarized neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Jericha, E. [Atominstitut, Vienna University of Technology, Stadionallee 2, 1020 Vienna (Austria)]. E-mail: jericha@ati.ac.at; Badurek, G. [Atominstitut, Vienna University of Technology, Stadionallee 2, 1020 Vienna (Austria); Trinker, M. [Atominstitut, Vienna University of Technology, Stadionallee 2, 1020 Vienna (Austria)

    2007-07-15

    Ultra-small-angle neutron scattering (USANS) has been established as an effective technique for the study of structures in the micrometre range in recent years. Consequentially this method has been extended to magnetic structures of corresponding size. We present the instrument arrangement and first experimental results. The instrument itself is a double crystal diffractometer in Bonse-Hart configuration which takes advantage of the narrow angular width of the perfect crystal reflection to obtain an extremely high angular resolution of the scattering vector. The neutrons are loss-free polarized by permanent magnetic prisms located between the monochromator crystal and the sample. Neutrons with opposite polarization are separated to a large extent and their different scattering behaviour may be studied in a single measurement without additional manipulation of the neutron spin. In this manner we are able to separate the magnetic and nuclear contribution to the scattering. We present first exemplifying measurements on ferromagnetic rods and wires, and on soft-magnetic ribbons. Related experiments were performed at the USANS facility of the TRIGA reactor at the Vienna University of Technology and at the combined neutron interferometer/USANS instrument S18 at the ILL, Grenoble.

  1. Thermal neutron scattering cross sections of beryllium and magnesium oxides

    International Nuclear Information System (INIS)

    Al-Qasir, Iyad; Jisrawi, Najeh; Gillette, Victor; Qteish, Abdallah

    2016-01-01

    Highlights: • Neutron thermalization in BeO and MgO was studied using Ab initio lattice dynamics. • The BeO phonon density of states used to generate the current ENDF library has issues. • The BeO cross sections can provide a more accurate ENDF library than the current one. • For MgO an ENDF library is lacking: a new accurate one can be built from our results. • BeO is a better filter than MgO, especially when cooled down to 77 K. - Abstract: Alkaline-earth beryllium and magnesium oxides are fundamental materials in nuclear industry and thermal neutron scattering applications. The calculation of the thermal neutron scattering cross sections requires a detailed knowledge of the lattice dynamics of the scattering medium. The vibrational properties of BeO and MgO are studied using first-principles calculations within the frame work of the density functional perturbation theory. Excellent agreement between the calculated phonon dispersion relations and the experimental data have been obtained. The phonon densities of states are utilized to calculate the scattering laws using the incoherent approximation. For BeO, there are concerns about the accuracy of the phonon density of states used to generate the current ENDF/B-VII.1 libraries. These concerns are identified, and their influences on the scattering law and inelastic scattering cross section are analyzed. For MgO, no up to date thermal neutron scattering cross section ENDF library is available, and our results represent a potential one for use in different applications. Moreover, the BeO and MgO efficiencies as neutron filters at different temperatures are investigated. BeO is found to be a better filter than MgO, especially when cooled down, and cooling MgO below 77 K does not significantly improve the filter’s efficiency.

  2. Introduction to nanostructural analyses by small-angle neutron scattering

    International Nuclear Information System (INIS)

    Shibayama, Mitsuhiro

    2010-01-01

    It has already passed more than 30 years since small-angle neutron scattering (SANS) technique was applied in structural analyses. SANS is now one of common tools in structure investigations and SANS instruments can be found in any neutron scattering facilities. In particular, SANS plays an important role in the field of soft matter, such as polymer, micelles, gels, vesicles, as well as biological systems and metallurgy. Here, I give a brief survey on (1) the utility of SANS in structural studies, (2) experimental aspects of SANS, and (3) some results obtained so far. (author)

  3. Inelastic scattering of fast neutrons from $^{56}$Fe

    CERN Document Server

    Beyer, R; Hannaske, R; Junghans, A R; Massarczyk, R; Anders, M; Bemmerer, D; Ferrari, A; Kögler, T; Röder, M; Schmidt, K; Wagner, A

    2014-01-01

    Inelastic scattering of fast neutrons from $^{56}$Fe was studied at the photoneutron source nELBE. The neutron energies were determined on the basis of a timeof- flight measurement. Gamma-ray spectra were measured with a high-purity germanium detector. The total scattering cross sections deduced from the present experiment in an energy range from 0.8 to 9.6 MeV agree within 15% with earlier data and with predictions of the statistical-reaction code Talys.

  4. X-ray and neutron scattering from surface and interface

    International Nuclear Information System (INIS)

    Metoki, Naoto

    1995-01-01

    Recent X-ray and neutron surface scattering studies of magnetic metal thin films and superlattices are reviewed. The Fresnel and Master formula for the specular reflectivity of ideal and real surfaces, respectively, are explained. We show some experimental results of X-ray specular reflectivity of Si, Co thin film, and Co/Cr superlattices as well as spin-polarized neutron reflectivity of a non-colinearly coupled Fe/Cr superlattice. A recent surface scattering study of hcp-bcc structural change of Co layers in Co/Cr (001) superlattices is reviewed as an example of this method. (author)

  5. An inelastic neutron scattering study of hematite nanoparticles

    DEFF Research Database (Denmark)

    Hansen, Mikkel Fougt; Klausen, Stine Nyborg; Lefmann, K

    2003-01-01

    We have studied the magnetic dynamics in nanocrystalline hematite by inelastic neutron scattering at the high-resolution time-of-flight spectrometer IRIS at ISIS. Compared to previous inelastic neutron scattering experiments an improvement of the resolution function is achieved and more detailed...... moment at the antiferromagnetic Bragg reflection. We have studied different weightings of the particle size distribution. The data and their temperature dependence can with good agreement be interpreted on the basis of the Neel-Brown theory for superparamagnetic relaxation and a model for the collective...

  6. Small-angle neutron-scattering experiment, (2)

    International Nuclear Information System (INIS)

    Niimura, Nobuo; Kaji, Harumi.

    1983-01-01

    Elementary explanation is given to the experiment on the small angle scattering using neutrons having long wave-length (3-12A), continued from the previous report. Two types of the apparatus for small angle neutron scattering experiment are described. The first is angle dispersion type, which uses the neutron beam from research reactors, and the second is wavelength dispersion type, which uses pulsed cold neutron sources. The principles of these experiments are explained. Especially the wavelength dispersion is described in detail. The apparatus in the booster facility at the Institute for High Energy Physics is shown as an example for the latter type. The two-dimensional position sensitive detector, which is essential for angle dispersion type, is also used for the wavelength dispersion type, and its data processing is also described. In the small angle neutron scattering experiment for the studies on the structure of living body substances, the techniques that should be taken into account in common are discussed; the proportion of D 2 O-H 2 O in solvent, the measurable range of Q, the size of specimens, the correction of incident neutron spectra, and the analysis of measured data. (Asami, T.)

  7. Methods of Information Processing for Neutron Scattering Data

    Science.gov (United States)

    Nave, Patrick; Jiao, Lin; Mourigal, Martin; Stone, Matthew

    Inferring complex dispersion relations from resolution-limited neutron scattering measurements is a task which has been approached from a variety of perspectives from Monte Carlo (MC) scattering simulations to resolution function methods which convolve an approximate resolution function with a theoretical model dispersion. However, detailed MC simulations require a highly-accurate framework such as MCViNE, which is not available for all neutron scattering facilities and is also time consuming, while resolution function methods are faster yet more dependent on accurate analytical models of the instrument to construct a valid approximation. Our research investigates two methods for analyzing neutron scattering data in a more general context. The first is a numerical covariance method designed to be fast while retaining high enough accuracy to be useful and enough generality to be applicable to any time-of-flight direct geometry neutron spectrometer. The second is a theoretical method based in topological data analysis concepts. In particular, we explore the computation of invariant topological features which may be useful in algorithmically learning from large databases of scattering data and identifying resolution correlations across sets of instrument parameters.

  8. Neutron Scattering from fcc Pr and Pr3Tl

    DEFF Research Database (Denmark)

    Birgeneau, R. J.; Als-Nielsen, Jens Aage; Bucher, E.

    1972-01-01

    Elastic-neutron-scattering measurements on the singlet-ground-state ferromagnets fcc Pr and Pr3 Tl are reported. Both exhibit magnetic phase transitions, possibly to a simple ferromagnetic state at 20 and 11.6 °K, respectively. The transitions appear to be of second order although that in fcc Pr...... is clearly anomalous. Additional information on the inelastic scattering studies of the Γ1-Γ4 excitons in these systems is presented. dhcp Pr is also briefly discussed....

  9. Kartini Research Reactor prospective studies for neutron scattering application

    International Nuclear Information System (INIS)

    Widarto

    1999-01-01

    The Kartini Research Reactor (KRR) is located in Yogyakarta Nuclear Research Center, Yogyakarta - Indonesia. The reactor is operated for 100 kW thermal power used for research, experiments and training of nuclear technology. There are 4 beam ports and 1 column thermal are available at the reactor. Those beam ports have thermal neutron flux around 10 7 n/cm 2 s each other and used for sub critical assembly, neutron radiography studies and Neutron Activation Analysis (NAA). Design of neutron collimator has been done for piercing radial beam port and the calculation result of collimated neutron flux is around 10 9 n/cm 2 s. This paper describes experiment facilities and parameters of the Kartini research reactor, and further more the prospective studies for neutron scattering application. The purpose of this paper is to optimize in utilization of the beam ports facilities and enhance the manpower specialty. The special characteristic of the beam ports and preliminary studies, pre activities regarding with neutron scattering studies for KKR is presented. (author)

  10. Leading Neutron Production In Deep Inelastic Scattering At Hera

    CERN Document Server

    Fagerstroem, C P

    2000-01-01

    The properties of leading neutrons produced in deep inelastic scattering are studied. The neutrons are detected with the Forward Neutron Calorimeter (FNC). The calibration and performance of the FNC are presented. The angular dependence of leading neutrons has been parametrized in the form dN/dp2T=exp- b˙p2T , where p2T is the transverse momentum squared of the neutron. The values of b are found to depend strongly on the energy of the neutron. The cross section for the kinematic region Q2 > 10 GeV2 and &thetas;n < 0.8 mrad is found to be (7.87 ± 0.15 (stat.) ± 0.79 (syst.))% of the inclusive deep inelastic scattering cross section. This fraction is found to be relatively independent of the kinematic variables x and Q2. Using the method of relative cross sections which reduces considerable systematic error, the structure function for leading neutron production FLN32 x,Q2,xL is measured. By assuming a simple model of one pion exchange, the structure function of the pion Fp2x,Q2 is e...

  11. Steel research using neutron beam techniques. In-situ neutron diffraction, small-angle neutron scattering and residual stress analysis

    International Nuclear Information System (INIS)

    Sueyoshi, Hitoshi; Ishikawa, Nobuyuki; Yamada, Katsumi; Sato, Kaoru; Nakagaito, Tatsuya; Matsuda, Hiroshi; Arakaki, Yu; Tomota, Yo

    2014-01-01

    Recently, the neutron beam techniques have been applied for steel researches and industrial applications. In particular, the neutron diffraction is a powerful non-destructive method that can analyze phase transformation and residual stress inside the steel. The small-angle neutron scattering is also an effective method for the quantitative evaluation of microstructures inside the steel. In this study, in-situ neutron diffraction measurements during tensile test and heat treatment were conducted in order to investigate the deformation and transformation behaviors of TRIP steels. The small-angle neutron scattering measurements of TRIP steels were also conducted. Then, the neutron diffraction analysis was conducted on the high strength steel weld joint in order to investigate the effect of the residual stress distribution on the weld cracking. (author)

  12. Latest developments of neutron scattering instrumentation at the Juelich Centre for Neutron Science

    International Nuclear Information System (INIS)

    Ioffe, Alexander

    2013-01-01

    Jülich Centre for Neutron Science (JCNS) is operating a number of world-class neutron scattering instruments situated at the most powerful and advanced neutron sources (FRM II, ILL and SNS) and is continuously undertaking significant efforts in the development and upgrades to keep this instrumentation in line with the continuously changing scientific request. These developments are mostly based upon the latest progress in neutron optics and polarized neutron techniques. For example, the low-Q limit of the suite of small angle-scattering instruments has been extended to 4·10 -5 Å -1 by the successful use of focusing optics. A new generation of correction elements for the neutron spin-echo spectrometer has allowed for the use of the full field integral available, thus pushing further the instrument resolution. A significant progress has been achieved in the developments of 3 He neutron spin filters for purposes of the wide-angle polarization analysis for off-specular reflectometry and (grazing incidence) small-angle neutron scattering, e.g. the on-beam polarization of 3 He in large cells is allowing to achieve a high neutron beam polarization without any degradation in time. The wide Q-range polarization analysis using 3 He neutron spin filters has been implemented for small-angle neutron scattering that lead to the reduction up to 100 times of the intrinsic incoherent background from non-deuterated biological molecules. Also the work on wide-angle XYZ magnetic cavities (Magic PASTIS) will be presented. (author)

  13. High pressure apparatus for neutron scattering at low temperature

    International Nuclear Information System (INIS)

    Munakata, Koji; Uwatoko, Yoshiya; Aso, Naofumi

    2010-01-01

    Effects of pressure on the physical properties are very important for understanding highly correlated electron systems, in which pressure-induced attractive phenomena such as superconductivity and magnetically ordered non-Fermi liquid have been observed. Up to now, many scientists have developed a lot of high pressure apparatus for each purpose. The characteristic features of various materials and pressure transmitting media for use of high pressure apparatus are reported. Then, two kinds of clamp type high-pressure cell designed for low-temperature neutron diffraction measurements are shown; one is a piston cylinder type high-pressure cell which can be attached to the dilution refrigerator, and the other one is a newly-developed cubic anvil type high-pressure cell which can generate pressure above 7GPa. We also introduce the results of magnetic neutron scattering under pressure on a pressure-induced superconducting ferromagnet UGe 2 in use of the piston cylinder type clamp cell, and those on an iron arsenide superconductor SrFe 2 As 2 in use of the cubic anvil type clamp cell. (author)

  14. Small angle neutron scattering from high impact polystyrene

    International Nuclear Information System (INIS)

    Pringle, O.A.

    1981-01-01

    High impact polystyrene (HIPS) is a toughened plastic composed of a polystyrene matrix containing a few percent rubber in the form of dispersed 0.1 to 10 micron diameter rubber particles. Some commercial formulations of HIPS include the addition of a few percent mineral oil, which improves the toughness of the plastic. Little is known about the mechanism by which the mineral oil helps toughen the plastic. It is hypothesized that the oil is distributed only in the rubber particles, but whether this hypothesis is correct was not known prior to this work. The size of the rubber particles in HIPS and their neutron scattering length density contrast with the polystyrene matrix cause HIPS samples to scatter neutrons at small angles. The variation of this small angle neutron scattering (SANS) signal with mineral oil content has been used to determine the location of the oil in HIPS. The SANS spectrometer at the University of Missouri Research Reactor Facility (MURR) was used to study plastic samples similar in composition to commercial HIPS. The MURR SANS spectrometer is used to study the small angle scattering of a vertical beam of 4.75 A neutrons from solid and liquid samples. The scattered neutrons are detected in a 54 x 60 cm 2 position sensitive detector designed and built at MURR. A series of plastic samples of varying rubber and oil content and different rubber domain sizes and shapes were examined on the MURR SANS spectrometer. Analysis of the scattering patterns showed that the mineral oil is about eight to ten times more likely to be found in the rubber particles than in the polystyrene matrix. This result confirmed the hypothesis that the mineral oil is distributed primarily in the rubber particles

  15. Structural characterizaton of deep-submicron lithographic structures using small-angle neutron scattering

    Science.gov (United States)

    Lin, Eric K.; Jones, Ronald L.; Wu, Wen-li; Barker, John G.; Bolton, Patrick J.; Barclay, George G.

    2002-07-01

    As critical dimensions continue to decrease with each technology node, the precise characterization of line width and profile becomes an increasingly challenging task. Small angle neutron scattering (SANS) offers several advantages for the characterization of sub-100 nm structures, particularly as a calibrating measurement method. In this work, SANS is used to characterize three samples prepared with the same mask and focus conditions, but different photoresist formulations. The mask pattern consists of parallel lines with a nominal line width of 180 nm and a 1:2 line to space ratio. Scattering data are taken using both a focused neutron beam instrument (two-dimensional data) and a perfect crystal diffraction ultra-high resolution small angle neutron scattering (USANS) instrument. From the location and intensity of observed diffraction peaks, both the periodicity of each grating pattern and the average line widths are determined from simple analytic expressions with nanometer resolution.

  16. Neutron scattering facilities at China Institute of Atomic Energy. Present and future situations

    Energy Technology Data Exchange (ETDEWEB)

    Ye, C.T.; Gou, C.; Yang, T.H. [China Institute of Atomic Energy, Beijing (China)

    2001-03-01

    The 15 MW Heavy Water Research Reactor (HWRR) at CIAE in Beijing is the only neutron source available for neutron scattering experiments in China at present. So far totally 5 neutron scattering spectrometers are installed at 4 beam tubes. A 60 MW new research reactor, China Advanced Research Reactor (CARR), now is being built at CIAE to meet the increasing demand of neutron scattering research in China. A brief description of HWRR, the presently existing neutron scattering equipments at HWRP, CARR, and the neutron scattering facilities to be installed at CARR are presented. (J.P.N.)

  17. Phase separation and ordering process in Al-Li alloys studied by small-angle neutron scattering and neutron diffraction

    International Nuclear Information System (INIS)

    Furusaka, M.; Fujikawa, S.I.

    1993-01-01

    To study phase separation kinetics of Al-9.5at.%Li polycrystalline alloys in which precipitates have ordered Al 3 Li (δ') structure, profile analysis of small-angle neutron scattering and superlattice reflections (100) and (110) were done. A small-angle scattering instrument and a triple-axis spectrometer in elastic mode were used in the measurements. Strong texture was observed in the reflections. Therefore, measurements were done using the crystal orientation where the intensity of the reflection was at the maximum. Profiles of small-angle scattering and superlattice reflections were almost identical at higher momentum transfer side. At lower momentum transfer side, small-angle scattering showed interference effects, but superlattice reflection did not show any sign of interference. Integrated intensities of superlattice reflections were obtained and compared with small-angle scattering intensity. The order parameter was not saturated in the δ' precipitates at the early stage of the phase separation process

  18. New Insights into Pore Characteristics and Hydrocarbon Generation of Shale Using Small-Angle Neutron Scattering

    Science.gov (United States)

    Ding, M.; Hartl, M.; Wang, Y.; Hjelm, R.

    2014-12-01

    Pore size, distribution, connectivity, and shape as well as hydrocarbon saturation and composition reflect the history of hydrocarbon maturation and migration. However, characterization of the underlying factors and processes controlling hydrocarbons behavior in tight rocks is extremely limited, especially lacking of direct experimental observations. We have studied the pore characteristics of marine and lacustrine shale from the Erdos basin, China during laboratory pyrolysis using small-angle neutron scattering (SANS). Our SANS results show that scattering intensity of smaller pores (industry.

  19. Evolution of Neutron Stars and Observational Constraints

    Directory of Open Access Journals (Sweden)

    Lattimer J.

    2010-10-01

    Full Text Available The structure and evolution of neutron stars is discussed with a view towards constraining the properties of high density matter through observations. The structure of neutron stars is illuminated through the use of several analytical solutions of Einstein’s equations which, together with the maximally compact equation of state, establish extreme limits for neutron stars and approximations for binding energies, moments of inertia and crustal properties as a function of compactness. The role of the nuclear symmetry energy is highlighted and constraints from laboratory experiments such as nuclear masses and heavy ion collisions are presented. Observed neutron star masses and radius limits from several techniques, such as thermal emissions, X-ray bursts, gammaray flares, pulsar spins and glitches, spin-orbit coupling in binary pulsars, and neutron star cooling, are discussed. The lectures conclude with a discusson of proto-neutron stars and their neutrino signatures.

  20. Scattered Neutron Tomography Based on A Neutron Transport Inverse Problem

    International Nuclear Information System (INIS)

    William Charlton

    2007-01-01

    Neutron radiography and computed tomography are commonly used techniques to non-destructively examine materials. Tomography refers to the cross-sectional imaging of an object from either transmission or reflection data collected by illuminating the object from many different directions

  1. Scattered Neutron Tomography Based on A Neutron Transport Inverse Problem

    Energy Technology Data Exchange (ETDEWEB)

    William Charlton

    2007-07-01

    Neutron radiography and computed tomography are commonly used techniques to non-destructively examine materials. Tomography refers to the cross-sectional imaging of an object from either transmission or reflection data collected by illuminating the object from many different directions.

  2. Neutron-scattering studies of magnetic superconductors

    International Nuclear Information System (INIS)

    Sinha, S.K.; Crabtree, G.W.; Hinks, D.G.; Mook, H.A.; Pringle, O.A.

    1982-01-01

    Results obtained in the last few years obtained by neutron diffraction on the nature of the magnetic ordering in magnetic superconductors are reviewed. Emphasis is given to studies of the complex intermediate phase in ferromagnetic superconductors where both superconductivity and ferromagnetism appear to coexist

  3. Optics for Advanced Neutron Imaging and Scattering

    Energy Technology Data Exchange (ETDEWEB)

    Moncton, David E. [Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States); Khaykovich, Boris [Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)

    2016-03-30

    During the report period, we continued the work as outlined in the original proposal. We have analyzed potential optical designs of Wolter mirrors for the neutron-imaging instrument VENUS, which is under construction at SNS. In parallel, we have conducted the initial polarized imaging experiment at Helmholtz Zentrum, Berlin, one of very few of currently available polarized-imaging facilities worldwide.

  4. Grazing incidence polarized neutron scattering in reflection ...

    Indian Academy of Sciences (India)

    along with suppression of training effect in exchange coupled system was microscopically identified using neutron ..... reversal mechanism and suppression of training in an exchange-coupled system by Paul et al are worth ...... density functional calculations based on Korringa–Kohn–Rostoker–Coherent potential-.

  5. Inelastic neutron scattering from high-density fcc 4He

    International Nuclear Information System (INIS)

    Thomlinson, W.; Eckert, J.; Shirane, G.

    1978-01-01

    The phonon dispersion relations in high-density crystals of fcc 4 He have been measured along high-symmetry directions by the neutron-inelastic-scattering technique. A recent study of the lattice dynamics of fcc 4 He by Eckert et al. has been extended to cover the fcc phase diagram at pressures below 5 kbar. Molar volumes of 9.03, 9.43, and 9.97 cm 3 /mole have been studied in the temperature range from near the melting curve to near the fcc-hcp transition line. The phonon dispersion relations are in good agreement with a first-order self-consistent phonon theory calculation by Goldman. The observed phonon-group line shapes at large energy and momentum transfers show evidence for multiphonon scattering in agreement with calculations by Glyde. Eckert et al. reported extremely large anharmonic isochoric temperature shifts of the phonon energies. The present work studied the shifts as a function of molar volume and temperature. Mode-Grueneisen-parameter dispersion curves have been measured using the present data and earlier measurements at lower density in the fcc phase by Traylor et al. Macroscopic Grueneisen parameters have been calculated from the phonon density of states obtained from the data

  6. A Neutron Elastic Diffuse Scattering Study of PMN

    OpenAIRE

    Xu, Guangyong; Shirane, G.; Copley, J. R. D.; Gehring, P. M.

    2003-01-01

    We have performed elastic diffuse neutron scattering studies on the relaxor Pb(Mg$_{1/3}$Nb$_{2/3}$)O$_3$ (PMN). The measured intensity distribution near a (100) Bragg peak in the (hk0) scattering plane assumes the shape of a butterfly with extended intensity in the (110) and (1$\\bar{1}$0) directions. The temperature dependence of the diffuse scattering shows that both the size of the polar nanoregions (PNR) and the integrated diffuse intensity increase with cooling even for temperatures belo...

  7. Theory of quasielastic neutron scattering by water in heterogeneous systems

    International Nuclear Information System (INIS)

    Sposito, G.

    1982-01-01

    The partial differential cross-section is derived for the quasielastic scattering of neutrons by liquid water protons undergoing translational diffusion in a heterogeneous system. It is shown that the incoherent scattering law reflects both molecular averaging via statistical mechanics and local volume averaging over the microscopic heterogeneities in the target sample. A model expression for the incoherent scattering law is derived using the macroscopic differential balance laws for mass and linear momentum as applied to liquid water in a porous medium. The model expression can be used to measure the macroscopic water diffusivity parameter. (author)

  8. Dynamics of liquid N2 studied by neutron inelastic scattering

    DEFF Research Database (Denmark)

    Pedersen, Karen Schou; Carneiro, Kim; Hansen, Flemming Yssing

    1982-01-01

    Neutron inelastic-scattering data from liquid N2 at wave-vector transfer κ between 0.18 and 2.1 Å-1 and temperatures ranging from T=65-77 K are presented. The data are corrected for the contribution from multiple scattering and incoherent scattering. The resulting dynamic structure factor S (κ......,ω) is compared with S (κ,ω) determined by a molecular-dynamics calculation and with that calculated from a linearized Vlasov equation. For κ≤0.3 Å-1 the experimental S (κ,ω) is compared with the values predicted by hydrodynamic theory....

  9. A Neutron Scattering Study of Collective Excitations in Superfluid Helium

    DEFF Research Database (Denmark)

    Graf, E. H.; Minkiewicz, V. J.; Bjerrum Møller, Hans

    1974-01-01

    Extensive inelastic-neutron-scattering experiments have been performed on superfluid helium over a wide range of energy and momentum transfers. A high-resolution study has been made of the pressure dependence of the single-excitation scattering at the first maximum of the dispersion curve over...... of the multiexcitation scattering was also studied. It is shown that the multiphonon spectrum of a simple Debye solid with the phonon dispersion and single-excitation cross section of superfluid helium qualitatively reproduces these data....

  10. Immersive Visual Analytics for Transformative Neutron Scattering Science

    Energy Technology Data Exchange (ETDEWEB)

    Steed, Chad A [ORNL; Daniel, Jamison R [ORNL; Drouhard, Margaret [University of Washington, Seattle; Hahn, Steven E [ORNL; Proffen, Thomas E [ORNL

    2016-01-01

    The ORNL Spallation Neutron Source (SNS) provides the most intense pulsed neutron beams in the world for scientific research and development across a broad range of disciplines. SNS experiments produce large volumes of complex data that are analyzed by scientists with varying degrees of experience using 3D visualization and analysis systems. However, it is notoriously difficult to achieve proficiency with 3D visualizations. Because 3D representations are key to understanding the neutron scattering data, scientists are unable to analyze their data in a timely fashion resulting in inefficient use of the limited and expensive SNS beam time. We believe a more intuitive interface for exploring neutron scattering data can be created by combining immersive virtual reality technology with high performance data analytics and human interaction. In this paper, we present our initial investigations of immersive visualization concepts as well as our vision for an immersive visual analytics framework that could lower the barriers to 3D exploratory data analysis of neutron scattering data at the SNS.

  11. A workshop on enhanced national capability for neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Hurd, Alan J [Los Alamos National Laboratory; Rhyne, James J [Los Alamos National Laboratory; Lewis, Paul S [Los Alamos National Laboratory

    2009-01-01

    This two-day workshop will engage the international neutron scattering community to vet and improve the Lujan Center Strategic Plan 2007-2013 (SP07). Sponsored by the LANL SC Program Office and the University of California, the workshop will be hosted by LANSCE Professor Sunny Sinha (UCSD). Endorsement by the Spallation Neutron Source will be requested. The discussion will focus on the role that the Lujan Center will play in the national neutron scattering landscape assuming full utilization of beamlines, a refurbished LANSCE, and a 1.4-MW SNS. Because the Lujan Strategic Plan is intended to set the stage for the Signature Facility era at LANSCE, there will be some discussion of the long-pulse spallation source at Los Alamos. Breakout groups will cover several new instrument concepts, upgrades to present instruments, expanded sample environment capabilities, and a look to the future. The workshop is in keeping with a request by BES to update the Lujan strategic plan in coordination with the SNS and the broader neutron community. Workshop invitees will be drawn from the LANSCE User Group and a broad cross section of the US, European, and Pacific Rim neutron scattering research communities.

  12. Development of new methods for studying nanostructures using neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Pynn, Roger [Indiana Univ., Bloomington, IN (United States)

    2016-03-18

    The goal of this project was to develop improved instrumentation for studying the microscopic structures of materials using neutron scattering. Neutron scattering has a number of advantages for studying material structure but suffers from the well-known disadvantage that neutrons’ ability to resolve structural details is usually limited by the strength of available neutron sources. We aimed to overcome this disadvantage using a new experimental technique, called Spin Echo Scattering Angle Encoding (SESAME) that makes use of the neutron’s magnetism. Our goal was to show that this innovation will allow the country to make better use of the significant investment it has recently made in a new neutron source at Oak Ridge National Laboratory (ORNL) and will lead to increases in scientific knowledge that contribute to the Nation’s technological infrastructure and ability to develop advanced materials and technologies. We were successful in demonstrating the technical effectiveness of the new method and established a baseline of knowledge that has allowed ORNL to start a project to implement the method on one of its neutron beam lines.

  13. Diffuse neutron scattering from anion-excess strontium chloride

    DEFF Research Database (Denmark)

    Goff, J.P.; Clausen, K.N.; Fåk, B.

    1992-01-01

    The defect structure and diffusional processes have been studied in the anion-excess fluorite (Sr, Y)Cl2.03 by diffuse neutron scattering techniques. Static cuboctahedral clusters found at ambient temperature break up at temperatures below 1050 K, where the anion disorder is highly dynamic. The a...

  14. Inelastic neutron scattering from non-framework species within zeolites

    International Nuclear Information System (INIS)

    Newsam, J.M.; Brun, T.O.; Trouw, F.; Iton, L.E.; Curtiss, L.A.

    1990-01-01

    Inelastic and quasielastic neutron scattering have special advantages for studying certain of the motional properties of protonated or organic species within zeolites and related microporous materials. In this paper these advantages and various experimental methods are outlined, and illustrated by measurements of torsional vibrations and rotational diffusion of tetramethylammonium (TMA) cations occluded within zeolites TMA-sodalite, omega, ZK-4 and SAPO-20

  15. Ultrasound effects and neutron scattering in UPt3

    DEFF Research Database (Denmark)

    Bruls, G.; Weber, D.; Kouroudis, I.

    1993-01-01

    We present results of sound propagation measurements and neutron scattering experiments on one and the same sample of the heavy fermion substance UPt3. From these experiments we deduce a B-T phase diagram of the small-moment spin density wave region in this compound for magnetic field B parallel...

  16. Inelastic neutron scattering and lattice dynamics studies in complex ...

    Indian Academy of Sciences (India)

    At Trombay, lattice dynamics studies employing coherent inelastic neutron scattering (INS) experiments have been carried out at the two research reactors, CIRUS and Dhruva. While the early work at CIRUS involved many elemental solids and ionic molecular solids, recent experiments at Dhruva have focussed on certain ...

  17. Small angle neutron scattering study of mixed micelles of oppositely ...

    Indian Academy of Sciences (India)

    - methylammonium bromide (DTAB) and sodium dodecyl sulphate (SDS) have been studied using small angle neutron scattering. The concentration of one of the components was kept fixed (0.3 M) and that of another varied in the range 0 to ...

  18. Inelastic Neutron Scattering Investigations of the Magnetic Excitations

    DEFF Research Database (Denmark)

    Feile, R; Kjems, Jørgen; Hauser, A.

    1984-01-01

    The magnetic excitations perpendicular to the antiferromagnetic chains in CsVX3 (X = Cl, Br, I) have been measured in the ordered state by inelastic neutron scattering. The dispersion relations and intensity distributions are those expected for ordinary spin waves in a triangular xy-model....

  19. Studies of magnetism with inelastic scattering of cold neutrons

    International Nuclear Information System (INIS)

    Jacrot, B.

    1964-01-01

    Inelastic scattering of cold neutrons can be used to study some aspects of magnetism: spins waves, exchange integrals, vicinity of Curie point. After description of the experimental set-up, several experiments, in the fields mentioned above, are analysed. (author) [fr

  20. Recent neutron scattering research and development in India

    Indian Academy of Sciences (India)

    Recent neutron scattering research and development in India ... The research activities involve various nanoscale structural, dynamical and magnetic investigations on materials of scientific interest and technological importance. ... Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400 085, India ...

  1. A national facility for small angle neutron scattering

    International Nuclear Information System (INIS)

    Buyers, W.J.L.; Katsaras, J.; Mellors, W.; Potter, M.M.; Powell, B.M.; Rogge, R.B.; Root, J.H.; Tennant, D.C.; Tun, Z.

    1995-01-01

    A world-class small angle neutron scattering (SANS) facility is proposed for Canada. It will provide users from the fields of biology, chemistry, physics, materials science and engineering with a uniquely powerful tool for investigating microstructural properties whose length scales lie in the optical to atomic range. (author). 7 refs

  2. Small angle neutron scattering study of two nonionic surfactants in ...

    Indian Academy of Sciences (India)

    cO Indian Academy of Sciences. Vol. 71, No. 5. — journal of. November 2008 physics pp. 1079–1083. Small angle neutron scattering study of two nonionic surfactants in water micellar solutions. RAJEWSKA ALDONA. Institute of Atomic Energy, 05-400 Swierk-Otwock, Poland. E-mail: aldonar@cyf.gov.pl. Abstract.

  3. Small angle neutron scattering study on the aggregation behaviour ...

    Indian Academy of Sciences (India)

    Small angle neutron scattering (SANS) measurements on aqueous solutions of four polyethylene oxide–polypropylene oxide–polyethylene oxide block copolymers (commercially known as Pluronic®)F88, P85, F127 and P123 in the presence of hydrophobic C14Diol (also known as Surfynol® 104) reveal information on ...

  4. Recent neutron scattering research and development in India

    Indian Academy of Sciences (India)

    Neutron scattering; national facility; structure; dynamics; magnetism. PACS Nos 61.12.-q; 78.70.Nx. 1. Introduction. The research activities at the Dhruva reactor involve various nanoscale structural, dynamical and magnetic investigations on materials of scientific interest and tech- nological importance. The main advantages ...

  5. Small angle neutron scattering studies of mixed micelles of sodium

    Indian Academy of Sciences (India)

    The aqueous solutions of sodium cumene sulphonate (NaCS) and its mixtures with each of cetyl trimethylammonium bromide (CTAB) and sodium dodecyl sulphate (SDS) are characterized by small angle neutron scattering (SANS). NaCS when added to CTAB solution leads to the formation of long rod-shaped micelles with ...

  6. Analysis of inelastic neutron scattering results on model compounds ...

    Indian Academy of Sciences (India)

    Keywords. Vibrational spectroscopy; nitrogenous bases; inelastic neutron scattering. PACS No. 63.20. 1. .... Where, Bz[x(y)] implies that this indole mode has x% of the benzene mode number y (after [10]); similarly .... the momentum transfer vector, Q, is essentially parallel to the incident beam for all energy transfers, at least ...

  7. Small-angle neutron scattering from colloidal dispersions

    International Nuclear Information System (INIS)

    Ottewill, R.H.

    1991-01-01

    A survey is given of recent work on the use of small-angle neutron scattering to examine colloidal dispersions. Particular attention is given to the determination of particle size and polydispersity, the determination of particle morphology and the behaviour of concentrated colloidal dispersions, both at rest and under the influence of an applied shear field. (orig.)

  8. Small-angle neutron scattering from micellar solutions

    Indian Academy of Sciences (India)

    The structure (shape and size) and the interaction of these aggregates, referred to as micelles, depend on the molecular architecture of the surfactant molecule, presence of additives and the solution conditions such as temperature, concentration etc. This paper gives the usefulness of small-angle neutron scattering to the ...

  9. Temperature dependent small-angle neutron scattering of CTABr ...

    Indian Academy of Sciences (India)

    Atomic Research Centre, Mumbai 400 085, India. cDepartment of Physics, Bhavnagar University, Bhavnagar 364 002, India. E-mail: ruv@bhavuni.edu. Abstract. Small-angle neutron scattering studies have been carried out to check the structural integrity of ... the surface of the micelle. Micellar solution of CTABr is isotropic ...

  10. Small-angle neutron scattering studies on water soluble complexes ...

    Indian Academy of Sciences (India)

    ... by small-angle neutron scattering. SANS data showed a positive indication of the formation of RCP-SDS complexes. Even though the complete structure of the polyion complexes could not be ascertained, the results obtained give us the information on the local structure in these polymer-surfactant systems. The data were ...

  11. Simulation of a complete inelastic neutron scattering experiment

    DEFF Research Database (Denmark)

    Edwards, H.; Lefmann, K.; Lake, B.

    2002-01-01

    A simulation of an inelastic neutron scattering experiment on the high-temperature superconductor La2-xSrxCuO4 is presented. The complete experiment, including sample, is simulated using an interface between the experiment control program and the simulation software package (McStas) and is compared...

  12. Characterization of alumina using small angle neutron scattering (SANS)

    International Nuclear Information System (INIS)

    Megat Harun Al Rashidn Megat Ahmad; Abdul Aziz Mohamed; Azmi Ibrahim; Che Seman Mahmood; Edy Giri Rachman Putra; Muhammad Rawi Muhammad Zin; Razali Kassim; Rafhayudi Jamro

    2007-01-01

    Alumina powder was synthesized from an aluminium precursor and studied using small angle neutron scattering (SANS) technique and complemented with transmission electron microscope (TEM). XRD measurement confirmed that the alumina produced was high purity and highly crystalline αphase. SANS examination indicates the formation of mass fractals microstructures with fractal dimension of about 2.8 on the alumina powder. (Author)

  13. Temperature dependent small-angle neutron scattering of CTABr ...

    Indian Academy of Sciences (India)

    Micelles are aggregates of surfactant molecules and these aggregates are usually formed in different shapes of spherical, cylindrical, ellipsoidal, disc-like etc. The size and shapes of these micelles are studied using small-angle neutron scattering (SANS) [2]. A preparation of stable emulsion of magnetic fluid with micelles ...

  14. Small-angle neutron scattering studies of nonionic surfactant: Effect

    Indian Academy of Sciences (India)

    Micellar solution of nonionic surfactant -dodecyloligo ethyleneoxide surfactant, decaoxyethylene monododecyl ether [CH3(CH2)11(OCH2CH2)10OH], C12E10 in D2O solution have been analysed by small-angle neutron scattering (SANS) at different temperatures (30, 45 and 60°C) both in the presence and absence of ...

  15. Spin dynamics in Tb studied by critical neutron scattering

    DEFF Research Database (Denmark)

    Dietrich, O. W.; Als-Nielsen, Jens Aage

    1971-01-01

    The inelasticity of the critical neutron scattering in Tb was measured at and above the Neel temperature. In the hydrodynamic region the line width Gamma (q=0, kappa 1)=C kappa z1, with z=1.4+or-0.1 and c=4.3+or-0.3 meVAAz. This result deviates from the conventional theory, which predicts...

  16. Lattice dynamics of solid deuterium by inelastic neutron scattering

    DEFF Research Database (Denmark)

    Nielsen, Mourits; Bjerrum Møller, Hans

    1971-01-01

    The dispersion relations for phonons in solid ortho-deuterium have been measured at 5 °K by inelastic neutron scattering. The results are in good agreement with recent calculations in which quantum effects are taken into account. The data have been fitted to a third-neighbor general force model...

  17. Spin-wave and critical neutron scattering from chromium

    DEFF Research Database (Denmark)

    Als-Nielsen, Jens Aage; Axe, J.D.; Shirane, G.

    1971-01-01

    Chromium and its dilute alloys are unique examples of magnetism caused by itinerant electrons. The magnetic excitations have been studied by inelastic neutron scattering using a high-resolution triple-axis spectrometer. Spin-wave peaks in q scans at constant energy transfer ℏω could, in general...

  18. Small-angle neutron scattering in materials science - an introduction

    Energy Technology Data Exchange (ETDEWEB)

    Fratzl, P. [Vienna Univ., Inst. fuer Materialphysik, Vienna (Austria)

    1996-12-31

    The basic principles of the application of small-angle neutron scattering to materials research are summarized. The text focusses on the classical methods of data evaluation for isotropic and for anisotropic materials. Some examples of applications to the study of alloys, porous materials, composites and other complex materials are given. (author) 9 figs., 38 refs.

  19. Neutron Scattering Experiments with the Unconventional Superconductor Uranium-Platinum

    Science.gov (United States)

    Gannon, William Joseph

    The heavy fermion superconductor UPt3 has been studied extensively for nearly 30 years. Still key questions remain. Here, I report results of crystal growth and neutron scattering experiments on this important compound. Small angle neutron scattering from the superconducting vortex lattice reveals possible evidence for broken time reversal in the superconducting B-phase, and provides direction sensitive measurements of the temperature dependence of the London penetration depth, revealing details of nodes in the superconducting gap consistent with the E2u order parameter model. Measurements of the polarized neutron spin flipping ratio show that the temperature dependence of the spin susceptibility is temperature independent for fields parallel to the crystal c-axis and in the basal plane. Finally, inelastic scattering experiments exploring the coupling of antiferromagnetism and superconductivity reveal that this coupling is quasi elastic, rather than elastic as previously thought. In this thesis, I will describe the efforts to grow large single crystals for these experiments, the different neutron scattering arrangements used to make these measurements, and the experimental results.

  20. Quasi-elastic neutron scattering study of dynamics in condensed ...

    Indian Academy of Sciences (India)

    S MITRA and R MUKHOPADHYAY. Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai 400 085, India. E-mail: smitra@apsara.barc.ernet.in. Abstract. Quasi-elastic neutron scattering (QENS) technique, known to study stochas- tic motions has been successfully used to elucidate the molecular motions ...

  1. Ultra Small-Angle Neutron Scattering Study of Porous Glass

    International Nuclear Information System (INIS)

    Desai, Reshma R.; Desa, J. A. Erwin; Sen, D.; Mazumder, S.

    2011-01-01

    Compacts of silica micro-spheres prepared for different times at sintering temperatures of 640 deg. C and 740 deg. C have been studied by Ultra Small-Angle Neutron Scattering (USANS) and Scanning Electron Microscopy (SEM). Stress versus strain measurements display several breakage points related to a range of nearest neighbour coordination around each microsphere.

  2. Spin-Echo Small-Angle Neutron Scattering Development

    NARCIS (Netherlands)

    Uca, O.

    2003-01-01

    Spin-Echo Small-Angle Neutron Scattering (SESANS) instrument is a novel SANS technique which enables one to characterize distances from a few nanometers up to the micron range. The most striking difference between normal SANS and SESANS is that in SESANS one gets information in real space, whereas

  3. Test of time reversal symmetry with resonance neutron scattering

    International Nuclear Information System (INIS)

    Bowman, J.D.

    1986-01-01

    The possibility of searching for time-reversal symmetry violation in the scattering of epithermal neutrons from nuclei is discussed. Sources of both statistical and systematic errors are reviewed. A qualitative assessment of the size of the time reversal is made and a schematic design of an experiment to test time reversal symmetry is presented. (DWL) 10 refs., 1 fig

  4. Small-angle neutron scattering study of structural evolution of ...

    Indian Academy of Sciences (India)

    Small-angle neutron scattering; biological macromolecules; protein solution. PACS Nos 61.12.Ex; 87.14.Ee; 87.15.Nn. Biological macromolecules such as proteins possess a specific shape and charge, which regulate and ... Figure 1a shows the phase diagram of crystallization of 1 wt% lysozyme protein solution as a ...

  5. Derivation of Inter-Atomic Force Constants of Cu2O from Diffuse Neutron Scattering Measurement

    Directory of Open Access Journals (Sweden)

    T. Makhsun

    2013-04-01

    Full Text Available Neutron scattering intensity from Cu2O compound has been measured at 10 K and 295 K with High Resolution Powder Diffractometer at JRR-3 JAEA. The oscillatory diffuse scattering related to correlations among thermal displacements of atoms was observed at 295 K. The correlation parameters were determined from the observed diffuse scattering intensity at 10 and 295 K. The force constants between the neighboring atoms in Cu2O were estimated from the correlation parameters and compared to those of Ag2O

  6. Neutron Scattering at HIFAR—Glimpses of the Past

    Directory of Open Access Journals (Sweden)

    Margaret Elcombe

    2017-04-01

    Full Text Available This article attempts to give a description of neutron scattering down under for close on forty-six years. The early years describe the fledgling group buying parts and cobbling instruments together to its emergence as a viable neutron scattering group with up to ten working instruments. The second section covers the consolidation of this group, despite tough higher level management. The Australian Science and Technology Council (ASTEC enquiry in 1985 and the Government decision not to replace the HIgh Flux Australian Reactor (HIFAR, led to major expansion and upgrading of the existing neutron beam facilities during the 1990s. Finally, there were some smooth years of operation while other staff were preparing for the replacement reactor. It has concentrated on the instruments as they were built, modified, replaced with new ones, and upgraded at different times.

  7. Diffuse scattering of neutrons and X-rays

    International Nuclear Information System (INIS)

    Novion, C.H. de

    1978-01-01

    Diffuse scattering is used to study defect concentrations of about 10 -4 in the case of X-rays and 10 -3 in the case of neutrons. The foundations of diffuse scattering formalism are given, some experimental devices described and a few applications discussed: study by diffraction on powders of defects in CeOsub(2-x); short-range order study by X-rays on Cusub(0.75) Ausub(0.25); short-range order study by neutrons on Cusub(0.435)Nisub(0.565); short-range order study by electrons TiOx; study of irradiation-induced self-interstitials in Al; study of holes created by neutrons in Al [fr

  8. Neutron Scattering Studies of Thermoelectric Materials for Automotive Applications

    Science.gov (United States)

    Yang, Jihui

    2010-03-01

    Solid-state thermoelectric (TE) technology uses electrons and holes as the working fluid for heat pumping and power generation, and has the virtues of no moving parts and high reliability. Advances in TE materials can lead to high thermal-to-electrical energy conversion efficiency and hence significant energy savings by generating electricity from waste heat. A good TE material should simultaneously possess high thermopower, low electrical resistivity, and low thermal conductivity. Most of the work in the past decade has been focused on lowering materials lattice thermal conductivity. Neutron diffraction and inelastic neutron scattering provide unique opportunities to understand the vibrational properties of thermoelectric materials. I will review some of our recent neutron studies on skutterudites, prospective high efficiency TE materials. Our studies have attempted to elucidate the crucial factors in these compounds relating to the filling-atom sublattices, particularly with respect to composition, nature of mixed fillers, dynamic disorder, phase coherence, and phonon scattering mechanisms.

  9. Development of spin echo small angle neutron scattering

    International Nuclear Information System (INIS)

    Bouwman, W.G.; Uca, O.; Van Oossanen, M.; Kraan, W.H.; Rekveldt, M.T.

    1999-01-01

    A novel kind of small angle neutron scattering (SANS) instrument is being built, based on the Larmor precession of polarised neutrons in a magnetic field. A spin echo of the polarised neutrons is used to detect the scattering. The basis of this instrument is a symmetric set-up with a spin flipper in the centre, which creates a spin echo, even with a divergent beam. The precession regions on either side of the spin flipper are shaped such to produce a very sensitive relation between the vertical angle of the neutron path and the total precession angle on one side. Any SANS of a sample placed in the instrument changes the symmetry of the neutron path and therefore decreases the echo. This amounts to measuring only the difference of the incoming and outgoing angle. This gives a huge increase in intensity of the signal with respect to conventional SANS in which both incoming and outgoing angle are defined. Magnetised foils, which rotate the neutron spin between being parallel to the magnetic field and perpendicular to the field are used to start or terminate the precession. With a preliminary set-up the first spin echo SANS signal have been measured. A full correlation function in samples over distances from 5 to 1000 nm is expected to be measured in some minutes. (author)

  10. Small angle neutron scattering experiment and raw data reduction

    International Nuclear Information System (INIS)

    Wei Guohai; Li Tianfu; Zhang Li; Wang Yu; Wang Hongli; Liu Xiangfeng

    2010-01-01

    Small angle neutron scattering (SANS) technique is a powerful tool for nanometer structural analysis of materials. The process of SANS measurement, and the raw data reduction, is relatively complicated. In order to obtain the absolute SANS intensity, one needs to measure intensities of the incident and scattered beams, the sample transmission, the background, the scattering and transmission of the empty cell etc. If a wide scattering vector range is needed, one has to measure the same sample under different instrument configurations. Also, a large number of data treatments are needed before one obtains the SANS data for further analysis. In this paper, after a short introduction to the SANS basic theory and the experimental system, we focus on the raw data reduction method, in which the averaging and the combination of the isotropically scattered data are discussed in detail. (authors)

  11. Activity report on neutron scattering research

    International Nuclear Information System (INIS)

    Sato, S.; Tawata, N.; Takesue, N.; Yoshizawa, H.

    1999-01-01

    This describes the experiments performed on the 14 university-owned spectrometers installed at the research reactor JRR-3M of Japan Energy Research Institute (JAERI) in Tokai. The report covers the period from April 1998 through March 1999, which is the Japanese Fiscal Year, JFY-1998. The contents are consisted of four parts such as outline, instrumentation, activity reports and publications. Outline describes brief history, users problem and committees. On instrumentation, JRR-3M Neutron Source, Status of Instruments, TAS, PONTA, TOPAN, HQR, KSD, HERMES, FONDER, NDC, HER, SANS-U, ULS, NSE, AGNES, MINE and R and D are explained. In the activity reports, 92 reports and their abstracts are described in eight parts: structures and excitations, magnetism, strongly correlated electronic systems, amorphous and liquid, polymers, biology, fundamental physics and neutron optics and instrumentations. Publications have list of publications and list of dissertations from 1994 to 1999. (S.Y.)

  12. Neutron inelastic scattering studies of crystal hydrates. Part of a coordinated programme on the application of research reactor neutron scattering techniques in the study of solids

    International Nuclear Information System (INIS)

    Amilius, Z.

    1977-12-01

    Using an inverted berillium filter spectrometer, neutrons inelastically scattered from the samples of hydrated and deuterated crystals of Cu Cl 2 .2H 2 O, Cu Cl 2 .2H 2 O and K 2 Cu Cl 2 .2D 2 O were measured, with the objective of determining the librational frequencies of the water molecule. The experiments were performed at room temperature only, permitting to draw only limited conclusions on the assignment of specific librational modes to the peak in the observed neutron spectra

  13. Small angle neutron scattering study on a phase separation in a 3-component microemulsion system

    DEFF Research Database (Denmark)

    Seto, H.; Yokoi, E.; Komura, S.

    1993-01-01

    observed a small change of the water droplet size approaching a phase separation point. In this work, further small angle neutron scattering results are presented obtained at the new SANS equipment in JAERI. The evidences described above were confirmed and a detailed phase diagram has been obtained...

  14. The defect structure of yttria-stabilized zirconia, studied by quasielastic diffuse neutron scattering

    DEFF Research Database (Denmark)

    Andersen, Niels Hessel; Clausen, Kurt Nørgaard; Hackett, M. A.

    1986-01-01

    The static defect structure of the oxygen ion conductor Y2O3 stabilized zirconia has been studied at room temperature by coherent diffuse neutron scattering from single crystal samples containing nominally 9.4, 12, 15 and 18 mol% Y2O3. There are two principal contributions to the observed diffuse...

  15. Small-angle neutron scattering instrument at MINT

    International Nuclear Information System (INIS)

    Mohd Ali Sufi; Yusof Abdullah; Razali Kassim; Hamid; Shahidan Radiman; Mohammad Deraman; Abdul Ghaffar Ramli

    1996-01-01

    The Small Angle Neutron Scattering (SANS) Instrument has been developed at Malaysian Institute for Nuclear Technology Research (MINT) for studying structural properties of materials on the length scale 1 nm to 100 nm. This is the length scale which is relevant for many topics within soft condensed matter, like polymers, colloids, biological macromolecules, etc. The SANS is a complementary technique to X-ray and electron scattering. However, while these later techniques give information on structures near surface, SANS concerns the structure of the bulk. Samples studied by SANS technique are typically bulk materials of the sizes mm's to cm's, or materials dissolved in a liquid. This paper described the general characteristics of SANS instrument as well as the experimental formulation in neutron scattering. The preliminary results obtained by this instrument are shown

  16. The National Facility for Small-Angle Neutron Scattering

    International Nuclear Information System (INIS)

    Koehler, W.C.

    1986-01-01

    On this occasion honoring Professor C.G.Shull, the 30-m small-angle neutron scattering (SANS) instrument of the National Center for Small-Angle Scattering Research (NCSASR) will have been in routine user-mode operation for five years. Professor Shull served the Center as chairman of its first Advisory Committee and in that capacity contributed his expertise to the construction phase of the 30-m machine and to the formulation of operating policy. He has had a long and varied interest in the scientific application of small-angle scattering of X-rays and of neutrons. It is a pleasure for me to dedicate this review to him on his 70th birthday. (orig.)

  17. Neutron detectors for scattering experiments at HANARO

    Indian Academy of Sciences (India)

    Korea Atomic Energy Research Institute (KAERI) has been developing various kinds of PSDs to improve the instrument performance and to develop new scattering instruments. Our development work is initiated with 1-D PSD for residual stress analysis spectrometer and finally the technology is extended to development of ...

  18. Ultra-small angle neutron scattering on structured materials

    International Nuclear Information System (INIS)

    Hainbuchner, M.

    2000-12-01

    In this work investigations of the inner macroscopic structure of various materials using the ultra small angle neutron scattering (USANS) technique are presented. First, the silicon double crystal and pinhole instruments used for the experiments are described. Then the basics of small angle neutron scattering theory are discussed. The treatment of the experimental scattering measurement data and the fitting of theoretical scattering models are thoroughly discussed, in particular the specific effects of the double crystal instrument geometry are considered. The used numerical procedures of the automatic data treatment and model fitting are presented. The quality and the reliability of these procedures and of the ultra small angle scattering experiments, performed on the neutron optical bench instrument S18 at the high flux reactor of the Institute Laue-Langevin, are illustrated by various measurements. The ultra small angle scattering measurements connect seamlessly or overlap with conventional pinhole measurements. For the determination the inner structure of the investigated materials a combination of ultra small and small angle scattering patterns can be used, which cover more than three orders of magnitude in momentum transfer and ten orders of magnitude in macroscopic differential scattering cross section. The specimens were carefully selected in order to represent a wide range of different materials. Artificial periodic silicon gratings were examined in order to prove high order interference effects. Measuring this kind of samples the performance of an USANS instrument can simply be determined. This allows the comparison of different instruments. For the calibration of the instrument and testing of the data treatment routines suspensions of latex spheres of various diameters were examined. In order to demonstrate that the evaluation of samples showing strong multiple scattering can produce meaningful results, measurements on sintered alumina using various

  19. The analysis and correction of neutron scattering effects in neutron imaging

    International Nuclear Information System (INIS)

    Raine, D.A.; Brenizer, J.S.

    1997-01-01

    A method of correcting for the scattering effects present in neutron radiographic and computed tomographic imaging has been developed. Prior work has shown that beam, object, and imaging system geometry factors, such as the L/D ratio and angular divergence, are the primary sources contributing to the degradation of neutron images. With objects smaller than 20--40 mm in width, a parallel beam approximation can be made where the effects from geometry are negligible. Factors which remain important in the image formation process are the pixel size of the imaging system, neutron scattering, the size of the object, the conversion material, and the beam energy spectrum. The Monte Carlo N-Particle transport code, version 4A (MCNP4A), was used to separate and evaluate the effect that each of these parameters has on neutron image data. The simulations were used to develop a correction algorithm which is easy to implement and requires no a priori knowledge of the object. The correction algorithm is based on the determination of the object scatter function (OSF) using available data outside the object to estimate the shape and magnitude of the OSF based on a Gaussian functional form. For objects smaller than 1 mm (0.04 in.) in width, the correction function can be well approximated by a constant function. Errors in the determination and correction of the MCNP simulated neutron scattering component were under 5% and larger errors were only noted in objects which were at the extreme high end of the range of object sizes simulated. The Monte Carlo data also indicated that scattering does not play a significant role in the blurring of neutron radiographic and tomographic images. The effect of neutron scattering on computed tomography is shown to be minimal at best, with the most serious effect resulting when the basic backprojection method is used

  20. Small angle neutron scattering study of nanostructure in permanent magnet materials and coercivity mechanism

    International Nuclear Information System (INIS)

    Kato, Hiroaki

    2008-01-01

    Small angle neutron scattering study was performed in sintered Nd-Fe-B permanent magnets. The 99% enriched 11 B isotope was used to avoid high neutron absorption of 10 B in natural boron. In all the samples examined, the intensity of scattered neutrons was proportional to the q -4 for q -1 , irrespective of the direction of q. For q>0.5 nm -1 , on the other hand, the intensity was markedly higher than that expected from the q -4 dependence. These results show that there exists a neutron scatterer with a dimension of less than 10 nm, which is considered to be a Nd-rich grain boundary phase in the matrix of Nd 2 Fe 14 B phase. In the sample with Al and Cu additives, we observed a small but finite increase of intensity as compared with the sample without Al and Cu additives for the q range of 0.1 -1 . Since Al- and Cu-containing samples have higher coercivity, this result suggests that there is a correlation between the density of neutron scatterer at a Nd-rich grain boundary and the coercivity. (author)

  1. Probing photoinduced spin states in spin-crossover molecules with neutron scattering

    Science.gov (United States)

    Ridier, K.; Craig, G. A.; Damay, F.; Fennell, T.; Murrie, M.; Chaboussant, G.

    2017-03-01

    We report a neutron-scattering investigation of the spin-crossover compound [Fe (ptz) 6] (BF4)2 , which undergoes an abrupt thermal spin transition from high spin (HS), S =2 , to low spin (LS), S =0 , around 135 K. The HS magnetic state can be restored at low temperature under blue/green light irradiation. We have developed a specially designed optical setup for neutron scattering to address the magnetic properties of the light-induced HS state. By using neutron diffraction, we demonstrate that significant HS/LS ratios (of up to 60%) can be obtained with this experimental setup on a sample volume considered large (400 mg), while a complete recovery of the LS state is achieved using near-infrared light. Finally, with inelastic neutron scattering (INS) we have observed magnetic transitions arising from the photo-induced metastable HS S =2 state split by crystal-field and spin-orbit coupling. We interpret the INS data assuming a spin-only model with a zero-field splitting of the S =2 ground state. The obtained parameters are D ≈-1.28 ±0.03 meV and |E |≈0.08 ±0.03 meV. The present results show that in situ magnetic inelastic neutron-scattering investigations on a broad range of photomagnetic materials are now possible.

  2. Studies of molecular dynamics with neutron scattering techniques. Part of a coordinated programme on neutron scattering techniques

    International Nuclear Information System (INIS)

    Vinhas, L.A.

    1980-05-01

    Molecular dynamics was studied in samples of tert-butanol, cyclohexanol and methanol, using neutron inelastic and quasi-elastic techniques. The frequency spectra of cyclohexanol in crystalline phase were interpreted by assigning individual energy peaks to hindered rotation of molecules, lattice vibration, hydrogen bond stretching and ring bending modes. Neutron quasi-elastic scattering measurements permitted the testing of models for molecular diffusion as a function of temperature. The interpretation of neutron incoherent inelastic scattering on methanol indicated the different modes of molecular dynamics in this material; individual inelastic peaks in the spectra could be assigned to vibrations of crystalline lattice, stretching of hydrogen bond and vibrational and torsional modes of CH 3 OH molecule. The results of the experimental work on tertbutanol indicate two distinct modes of motion in this material: individual molecular librations are superposed to a cooperative rotation diffusion which occurs both in solid and in liquid state

  3. Neutron-optical effects at very cold neutrons scattering on the spherical particles of different sizes

    International Nuclear Information System (INIS)

    Grinev, V.G.; Kudinova, O.I.; Novokshonova, L.A.; Kuznetsov, S.P.; Udovenko, A.I.; Shelagin, A.V.

    2006-01-01

    Very cold neutrons (VCN) with the wavelength λ > 4.0 ran are convenient tool for investigating the super molecular structures of different nature. Using a Born approximation (BA) to the analysis of dependencies on the wavelength of the VCN scattering cross sections, it is possible to obtain information about average sizes (R) and concentrations of the scattering particles with R∼ λ. However, with an increasing the sizes of scatterers the conditions for BA applicability can be disrupted. In this work we investigated the possibilities of BA, eikonal and geometric-optical approximations for the analysis of VCN scattering on the spherical particles with R ≥ λ

  4. Small-angle neutron scattering measurement of silicon nanoparticle size

    International Nuclear Information System (INIS)

    Choi, Jonghoon; Tung, Shih-Huang; Wang, Nam Sun; Reipa, Vytas

    2008-01-01

    We have determined the particle size distribution profiles of octane-terminated silicon nanoparticle suspensions, produced using the sonication of electrochemically etched Si wafers. Small-angle neutron scattering data was analyzed separately in high (0.4 nm -1 -1 ) and low (q -1 ) scattering vector ranges. Data in the high q range is consistent with the log-normal distribution of isolated spherical particles with median diameter d = 3 ± 0.2 nm. Particle sizes were also indirectly assessed from photoluminescence and optical transmission spectroscopy using the size/bandgap relation: E g = 3.44d -0.5 , where E g is in eV and d in nm. Both measurements were consistent with the particle size distribution profiles, estimated from ANS data fitting and TEM image analysis. A subpopulation of larger, irregular shape structures in the size range 10-50 nm was also indicated by neutron scattering in the low q range and HRTEM images. However, further studies are warranted to explain a relationship between the slope of scattering intensity versus scattering vector dependence in the intermediate scattering vector range (0.4 nm -1 -1 ) and the role of non-geometrical Si nanoparticle characteristics (mutual interaction forces, surface termination, etc)

  5. A thermal neutron scattering law for yttrium hydride

    Science.gov (United States)

    Zerkle, Michael; Holmes, Jesse

    2017-09-01

    Yttrium hydride (YH2) is of interest as a high temperature moderator material because of its superior ability to retain hydrogen at elevated temperatures. Thermal neutron scattering laws for hydrogen bound in yttrium hydride (H-YH2) and yttrium bound in yttrium hydride (Y-YH2) prepared using the ab initio approach are presented. Density functional theory, incorporating the generalized gradient approximation (GGA) for the exchange-correlation energy, is used to simulate the face-centered cubic structure of YH2 and calculate the interatomic Hellmann-Feynman forces for a 2 × 2 × 2 supercell containing 96 atoms. Lattice dynamics calculations using PHONON are then used to determine the phonon dispersion relations and density of states. The calculated phonon density of states for H and Y in YH2 are used to prepare H-YH2 and Y-YH2 thermal scattering laws using the LEAPR module of NJOY2012. Analysis of the resulting integral and differential scattering cross sections demonstrates adequate resolution of the S(α,β) function. Comparison of experimental lattice constant, heat capacity, inelastic neutron scattering spectra and total scattering cross section measurements to calculated values are used to validate the thermal scattering laws.

  6. A thermal neutron scattering law for yttrium hydride

    Directory of Open Access Journals (Sweden)

    Zerkle Michael

    2017-01-01

    Full Text Available Yttrium hydride (YH2 is of interest as a high temperature moderator material because of its superior ability to retain hydrogen at elevated temperatures. Thermal neutron scattering laws for hydrogen bound in yttrium hydride (H-YH2 and yttrium bound in yttrium hydride (Y-YH2 prepared using the ab initio approach are presented. Density functional theory, incorporating the generalized gradient approximation (GGA for the exchange-correlation energy, is used to simulate the face-centered cubic structure of YH2 and calculate the interatomic Hellmann-Feynman forces for a 2 × 2 × 2 supercell containing 96 atoms. Lattice dynamics calculations using PHONON are then used to determine the phonon dispersion relations and density of states. The calculated phonon density of states for H and Y in YH2 are used to prepare H-YH2 and Y-YH2 thermal scattering laws using the LEAPR module of NJOY2012. Analysis of the resulting integral and differential scattering cross sections demonstrates adequate resolution of the S(α,β function. Comparison of experimental lattice constant, heat capacity, inelastic neutron scattering spectra and total scattering cross section measurements to calculated values are used to validate the thermal scattering laws.

  7. Neutron scattering from a substitutional mass defect

    International Nuclear Information System (INIS)

    Williams, R.D.; Lovesey, S.W.

    1985-06-01

    The dynamic structure factor is calculated for a low concentration of light mass scatterers substituted in a cubic crystal matrix. A new numerical method for the exact calculation is demonstrated. A local density of states for the low momentum transfer limit, and the shifts and widths of the oscillator peaks in the high momentum transfer limit are derived. The limitations of an approximation which decouples the defect from the lattice is discussed. (author)

  8. 2009 International Conference on Neutron Scattering (ICNS 2009)

    Energy Technology Data Exchange (ETDEWEB)

    Gopal Rao, PhD; Gillespie, Donna

    2010-08-05

    The ICNS provides a focal point for the worldwide neutron user community to strengthen ties within this diverse group, while at the same time promoting neutron research among colleagues in related disciplines identified as would-be neutron users. The International Conference on Neutron Scattering thus serves a dual role as an international user meeting and a scientific meeting. As a venue for scientific exchange, the ICNS showcases recent results and provides forums for scientific discussion of neutron research in diverse fields such as hard and soft condensed matter, liquids, biology, magnetism, engineering materials, chemical spectroscopy, crystal structure, and elementary excitations, fundamental physics and development of neutron instrumentation through a combination of invited talks, contributed talks and poster sessions. Each of the major national neutron facilities (NIST, LANSCE, ANL, HFIR and SNS), along with their international counterparts, has an opportunity to exchange information with each other and to update users, and potential users, of their facility. This is also an appropriate forum for users to raise issues that relate to the facilities.

  9. Antiferromagnetism, crystal fields and hybridisation in UxY1-xPd3 studied by neutron scattering

    DEFF Research Database (Denmark)

    Bull, M.J.; McEwen, K.A.; Eccleston, R.S.

    1999-01-01

    We summarise our UxY1-xPd3 inelastic neutron scattering experiments and present new neutron diffraction results for a single crystal of U0.45Y0.55Pd3. Long-range antiferromagnetic order is unambiguously observed below T-N = 22.5 K. in contrast, no long-range order is found in polycrystalline...

  10. Multiple scattering and attenuation corrections in Deep Inelastic Neutron Scattering experiments

    International Nuclear Information System (INIS)

    Dawidowski, J; Blostein, J J; Granada, J R

    2006-01-01

    Multiple scattering and attenuation corrections in Deep Inelastic Neutron Scattering experiments are analyzed. The theoretical basis of the method is stated, and a Monte Carlo procedure to perform the calculation is presented. The results are compared with experimental data. The importance of the accuracy in the description of the experimental parameters is tested, and the implications of the present results on the data analysis procedures is examined

  11. Neutron scattering for analysis of processes in lithium-ion batteries

    Science.gov (United States)

    Balagurov, A. M.; Bobrikov, I. A.; Samoylova, N. Yu; Drozhzhin, O. A.; Antipov, E. V.

    2014-12-01

    The review is concerned with analysis and generalization of information on application of neutron scattering for elucidation of the structure of materials for rechargeable energy sources (mainly lithium-ion batteries) and on structural rearrangements in these materials occurring in the course of electrochemical processes. Applications of the main methods including neutron diffraction, small-angle neutron scattering, inelastic neutron scattering, neutron reflectometry and neutron introscopy are considered. Information on advanced neutron sources is presented and a number of typical experiments are outlined. The results of some studies of lithium-containing materials for lithium-ion batteries, carried out at IBR-2 pulsed reactor, are discussed. The bibliography includes 50 references.

  12. New neutron-based isotopic analytical methods; An explorative study of resonance capture and incoherent scattering

    NARCIS (Netherlands)

    Perego, R.C.

    2004-01-01

    Two novel neutron-based analytical techniques have been treated in this thesis, Neutron Resonance Capture Analysis (NRCA), employing a pulsed neutron source, and Neutron Incoherent Scattering (NIS), making use of a cold neutron source. With the NRCA method isotopes are identified by the

  13. Neutron and light scattering studies of polymers adsorbed on laponite

    International Nuclear Information System (INIS)

    Nelson, Andrew Robert John

    2002-01-01

    The adsorption of poly(ethylene oxide) (PEO) and various poly(ethylene oxide)-poly(propylene oxide)-poly(ethylene oxide) (Pluronic) copolymers onto the synthetic clay Laponite, was investigated using Small Angle Neutron Scattering (SANS) and Dynamic Light Scattering (DLS). The Laponite particles are anisotropic, with a relatively high aspect ratio; but are the same order of magnitude in size as the polymer radius of gyration. Consequently, the particles present a radically different adsorption geometry compared to a locally planar interface, that is assumed by the majority of adsorption studies. The PEO homo-polymer formed thin layers, with the layer thickness being much smaller on the face than on the edge of the particle. Furthermore, the face thickness remained constant with increasing molecular weight, unlike the edge thickness, which grew with a small power law dependence on the molecular weight. Although the hydrodynamic thicknesses (DLS) were larger than those observed with SANS, the layer thicknesses were much smaller than that expected for polymer adsorption on spherical particles. Experimentally determined inter-particle structure factors suggested that the adsorbed PEO layers provided a steric repulsion term to the inter-particle interactions. The autocorrelation functions for aggregating Laponite dispersions were followed with DLS. It was found that the stabilisation provided by the adsorbed layer reduced the aggregation rate, with lower molecular weights being most effective. SANS and DLS measurements on Laponite/Pluronic systems revealed that the thickness of the Pluronic layer was the same on the edge and face of the particle. As the Pluronic anchor fraction decreased, and the PEO block molecular weight increased, a growth in the layer size and adsorbed amount was observed. The low anchor fraction Pluronics had higher adsorbed amounts and thicker layers, than the highest M w homo-polymers, demonstrating the importance of the PPO block in the

  14. Intercalibration of small-angle X-ray and neutron scattering data

    International Nuclear Information System (INIS)

    Russell, T.P.; Lin, J.S.; Spooner, S.; Wignall, G.D.

    1988-01-01

    Absolute calibration forms a valuable diagnostic tool in small-angle scattering experiments and allows the parameters of a given model to be restricted to the set which reproduces the observed intensity. General methods which are available for absolute scaling of small-angle X-ray scattering (SAXS) data are reviewed along with estimates of the degree of internal consistency which may be achieved between the various standards. In order to minimize the time devoted to calibration in a given experimental program, emphasis is placed on developing a set of precalibrated strongly scattering standards for the SAXS facilities of the National Center for Small-Angle Scattering Research (Oak Ridge). Similar standards have been developed previously for calibration of small-angle neutron scattering (SANS) data. Particular attention is given to standards which can be used for either SAXS or SANS experiments where each sample has been independently calibrated for both types of radiation. These calibrations have been tested via the theoretical relationships between the two cross sections. It has been found that specimens best suited for such intercalibration purposes are a glassy carbon specimen where the scattering arises from voids in a carbon matrix and a perdeuterated polyethylene where the scattering arises from periodic arrangement of the crystalline lamellae. In only these two cases could the identical specimen be used for both the neutron and X-ray scattering experiments. (orig.)

  15. Investigation of short range order in Fe-C melts by neutron scattering

    International Nuclear Information System (INIS)

    Weber, M.; Steeb, S.

    1978-01-01

    Neutron diffraction measurements were done with Fe-C-melts (5; 13; and 17 at % C) using the method of isotopic substitution. The neutron small angle scattering effect observed could be explained by magnetic scattering, caused by spin-fluctuations still existing in the molten state far away from the Curie temperature. Total structure factors were calculated from observed intensities taking into account the correction for magnetic scattering. For each carbon concentration two alloys were investigated, one using iron of natural isotopic abundance and the other using enriched 57 Fe. From a comparison of the q-region below the first maximum of the total structure factor as obtained using Fesup(nat) or 57 Fe, respectively, a tendency to the preference of unlike nearest neighbours is concluded, the distance between Fe-C-pairs being 2.2 A. (orig.) [de

  16. DNS: Diffuse scattering neutron time-of-flight spectrometer

    Directory of Open Access Journals (Sweden)

    Yixi Su

    2015-08-01

    Full Text Available DNS is a versatile diffuse scattering instrument with polarisation analysis operated by the Jülich Centre for Neutron Science (JCNS, Forschungszentrum Jülich GmbH, outstation at the Heinz Maier-Leibnitz Zentrum (MLZ. Compact design, a large double-focusing PG monochromator and a highly efficient supermirror-based polarizer provide a polarized neutron flux of about 107 n cm-2 s-1. DNS is used for the studies of highly frustrated spin systems, strongly correlated electrons, emergent functional materials and soft condensed matter.

  17. Quokka: The Small-Angle Neutron Scattering Instrument at OPAL

    International Nuclear Information System (INIS)

    Gilbert, Elliot; Noakes, Terry; Schulz, Jamie; Baxter, Peter; Darmann, Frank; Hauser, Nick; Abbeywick, Peter; Brule, Alain; Imamovic, Eno; Christoforidis, Jason

    2005-01-01

    Full text: A small-angle neutron scattering (SANS) instrument is being designed as part of the initial instrument suite for the 20-MW OPAL Reactor. The new instrument, receiving neutrons from a large liquid-D2 cold source, will be in the spirit of the worlds best facilities and will greatly build upon the Australian Nuclear Science and Technology Organisations existing expertise and facilities. Scheduled for completion in July 2006, it will provide Australian and international researchers with opportunities to access state-of-the-art SANS instrumentation. The details of the new SANS will be presented. (author)

  18. In-situ studies with photons, neutrons and electrons scattering

    International Nuclear Information System (INIS)

    Kannengiesser, Thomas; Babu, Sudarsanam Suresh; Komizo, Yu-ichi; Ramirez, Antonio J.

    2010-01-01

    In-situ scattering and diffraction measurements using synchrotron and neutron beam lines have become a viable tool to look at the non-equilibrium processing of advanced materials. This volume presents the subject from the theoretical and experimental standpoint, in order to provide a closer insight into the different synchrotron and neutron diffraction techniques as well as innovative microscopy techniques. It addresses the following items: - phase detection and quantification - In-situ welding experiments - Stress/strain build-up - model development and Simulation - Analysis tools and programming (orig.)

  19. Investigation of neutron scattering for a multisphere spectrometer

    International Nuclear Information System (INIS)

    Sun, R.K.

    1990-01-01

    Count rates were measured as a function of distance from a planar concrete reflector for a set of eight Bonner-sphere detectors and four isotopic neutron sources. These data can be used to determine the contributions of scattered neutrons to the response of moderated detectors used in environments bounded by concrete. A model based on images of the original source can be developed to produce an equation that describes the data well, if the strengths of the image sources can be treated as variable parameters. Values of the parameters appearing in the equations are given based on least-squares analysis of the experimental results

  20. Investigation of phonon-like excitation in hydrated protein powders by neutron scattering

    Science.gov (United States)

    Chu, Xiang-Qiang (Rosie); Mamontov, Eugene; O'Neill, Hugh; Zhang, Qiu; Kolesnikov, Alexander

    2013-03-01

    Detecting the phonon dispersion relations in proteins is essential for understanding the intra-protein dynamical behavior. Such study has been attempted by X-ray in recent years. However, for such detections, neutrons have significant advantages in resolution and time-efficiency compare to X-rays. Traditionally the collective motions of atoms in protein molecules are hard to detect using neutrons, because of high incoherent scattering background from intrinsic hydrogen atoms in the protein molecules. The recent availability of a fully deuterated green fluorescent protein (GFP) synthesized by the Bio-deuteration Lab at ORNL opens new possibilities to probe collective excitations in proteins using inelastic neutron scattering. Using a direct time-of-flight Fermi chopper neutron spectrometer, we obtained a full map of the meV phonon-like excitations in the fully deuterated protein. The Q range of the observed excitations corresponds to the length scale close to the size of the secondary structures of proteins and reflects the collective intra-protein motions. Our results show that hydration of GFP seems to harden, not soften, the collective motions. This result is counterintuitive but in agreement with the observations by previous neutron scattering experiments. Sample preparation was supported by facilities operated by the Center for Structural Molecular Biology at ORNL which is supported by the U.S. DOE, Office of Science, Office of Biological and Environmental Research Project ERKP291.

  1. Fast-neutron total and scattering cross sections of Cr, Fe and 60Ni

    International Nuclear Information System (INIS)

    Smith, A.B.; Guenther, P.T.; Whalen, J.F.

    1979-01-01

    Neutron total cross sections are measured with broad resolutions (50 to 100 keV) from approx. = 1.0 to 4.5 MeV at intervals of less than or equal to 50 keV and to accuracies of approx. = 1% using a variety of sample thicknesses. Differential elastic-scattering cross sections are measured at greater than or equal to 10 scattering angles distributed between 20 to 160 deg. from approx. = 1.5 to 4.0 MeV at intervals of less than or equal to 50 keV. Angle-integrated elastic scattering cross sections are deduced from the measured values to accuracies greater than or equal to 5%. Inelastic-neutron-scattering cross sections are determined up to incident neutron energies of 4.0 MeV, at scattering angles distributed between 20 to 160 deg., and for 5 observed excitations in Cr, for 7 in Fe and for 6 in 60 Ni. The experimental results are discussed in terms of conventional optical-statistical models with attention to cross section fluctuations and in the context of direct-scattering processes. The experimental and calculational results are compared with the corresponding evaluated quantities given in the ENDF/B file with attention to regions of agreement and inconsistency. 14 references

  2. Neutron spectral modulation as a new thermal neutron scattering technique. Pt. 1

    International Nuclear Information System (INIS)

    Ito, Y.; Nishi, M.; Motoya, K.

    1982-01-01

    A thermal neutron scattering technique is presented based on a new idea of labelling each neutron in its spectral position as well as in time through the scattering process. The method makes possible the simultaneous determination of both the accurate dispersion relation and its broadening by utilizing the resolution cancellation property of zero-crossing points in the cross-correlated time spectrum together with the Fourier transform scheme of the neutron spin echo without resorting to the echoing. The channel Fourier transform applied to the present method also makes possible the determination of the accurate direct energy scan profile of the scattering function with a rather broad incident neutron wavelength distribution. Therefore the intensity sacrifice for attaining high accurarcy is minimized. The technique is used with either a polarized or unpolarized beam at the sample position with no precautions against beam depolarization at the sample for the latter case. Relative time accurarcy of the order of 10 -3 to 10 -4 may be obtained for the general dispersion relation and for the quasi-elastic energy transfers using correspondingly the relative incident neutron wavelength spread of 10 to 1% around an incident neutron energy of a few meV. (orig.)

  3. Neutrons for Catalysis: A Workshop on Neutron Scattering Techniques for Studies in Catalysis

    International Nuclear Information System (INIS)

    Overbury, Steven H.; Coates, Leighton; Herwig, Kenneth W.; Kidder, Michelle

    2011-01-01

    This report summarizes the Workshop on Neutron Scattering Techniques for Studies in Catalysis, held at the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory (ORNL) on September 16 and 17, 2010. The goal of the Workshop was to bring experts in heterogeneous catalysis and biocatalysis together with neutron scattering experimenters to identify ways to attack new problems, especially Grand Challenge problems in catalysis, using neutron scattering. The Workshop locale was motivated by the neutron capabilities at ORNL, including the High Flux Isotope Reactor (HFIR) and the new and developing instrumentation at the SNS. Approximately 90 researchers met for 1 1/2 days with oral presentations and breakout sessions. Oral presentations were divided into five topical sessions aimed at a discussion of Grand Challenge problems in catalysis, dynamics studies, structure characterization, biocatalysis, and computational methods. Eleven internationally known invited experts spoke in these sessions. The Workshop was intended both to educate catalyst experts about the methods and possibilities of neutron methods and to educate the neutron community about the methods and scientific challenges in catalysis. Above all, it was intended to inspire new research ideas among the attendees. All attendees were asked to participate in one or more of three breakout sessions to share ideas and propose new experiments that could be performed using the ORNL neutron facilities. The Workshop was expected to lead to proposals for beam time at either the HFIR or the SNS; therefore, it was expected that each breakout session would identify a few experiments or proof-of-principle experiments and a leader who would pursue a proposal after the Workshop. Also, a refereed review article will be submitted to a prominent journal to present research and ideas illustrating the benefits and possibilities of neutron methods for catalysis research.

  4. Neutrons for Catalysis: A Workshop on Neutron Scattering Techniques for Studies in Catalysis

    Energy Technology Data Exchange (ETDEWEB)

    Overbury, Steven {Steve} H [ORNL; Coates, Leighton [ORNL; Herwig, Kenneth W [ORNL; Kidder, Michelle [ORNL

    2011-10-01

    This report summarizes the Workshop on Neutron Scattering Techniques for Studies in Catalysis, held at the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory (ORNL) on September 16 and 17, 2010. The goal of the Workshop was to bring experts in heterogeneous catalysis and biocatalysis together with neutron scattering experimenters to identify ways to attack new problems, especially Grand Challenge problems in catalysis, using neutron scattering. The Workshop locale was motivated by the neutron capabilities at ORNL, including the High Flux Isotope Reactor (HFIR) and the new and developing instrumentation at the SNS. Approximately 90 researchers met for 1 1/2 days with oral presentations and breakout sessions. Oral presentations were divided into five topical sessions aimed at a discussion of Grand Challenge problems in catalysis, dynamics studies, structure characterization, biocatalysis, and computational methods. Eleven internationally known invited experts spoke in these sessions. The Workshop was intended both to educate catalyst experts about the methods and possibilities of neutron methods and to educate the neutron community about the methods and scientific challenges in catalysis. Above all, it was intended to inspire new research ideas among the attendees. All attendees were asked to participate in one or more of three breakout sessions to share ideas and propose new experiments that could be performed using the ORNL neutron facilities. The Workshop was expected to lead to proposals for beam time at either the HFIR or the SNS; therefore, it was expected that each breakout session would identify a few experiments or proof-of-principle experiments and a leader who would pursue a proposal after the Workshop. Also, a refereed review article will be submitted to a prominent journal to present research and ideas illustrating the benefits and possibilities of neutron methods for catalysis research.

  5. Quasi-elastic neutron scattering studies of protein dynamics

    International Nuclear Information System (INIS)

    Rorschach, H.E.

    1993-01-01

    Results that shed new light on the study of protein dynamics were obtained by quasi-elastic neutron scattering. The triple axis instrument H-9 supplied by the cold source was used to perform a detailed study of the quasi-elastic spectrum and the Debye-Waller factor for trypsin in powder form, in solution, and in crystals. A preliminary study of myoglobin crystals was also done. A new way to view the results of quasi-elastic scattering experiments is sketched, and the data on trypsin are presented and analyze according to this new picture

  6. THERMAL: A routine designed to calculate neutron thermal scattering

    International Nuclear Information System (INIS)

    Cullen, D.E.

    1995-01-01

    THERMAL is designed to calculate neutron thermal scattering that is isotropic in the center of mass system. At low energy thermal motion will be included. At high energies the target nuclei are assumed to be stationary. The point of transition between low and high energies has been defined to insure a smooth transition. It is assumed that at low energy the elastic cross section is constant in the center of mass system. At high energy the cross section can be of any form. You can use this routine for all energies where the elastic scattering is isotropic in the center of mass system. In most materials this will be a fairly high energy

  7. A local dynamic correlation function from inelastic neutron scattering

    International Nuclear Information System (INIS)

    McQueeney, R.J.

    1997-01-01

    Information about local and dynamic atomic correlations can be obtained from inelastic neutron scattering measurements by Fourier transform of the Q-dependent intensity oscillations at a particular frequency. A local dynamic structure function, S(r,ω), is defined from the dynamic scattering function, S(Q,ω), such that the elastic and frequency-integrated limits correspond to the average and instantaneous pair-distribution functions, respectively. As an example, S(r,ω) is calculated for polycrystalline aluminum in a model where atomic motions are entirely due to harmonic phonons

  8. Solution of neutron slowing down equation including multiple inelastic scattering

    International Nuclear Information System (INIS)

    El-Wakil, S.A.; Saad, A.E.

    1977-01-01

    The present work is devoted the presentation of an analytical method for the calculation of elastically and inelastically slowed down neutrons in an infinite non absorbing homogeneous medium. On the basis of the Central limit theory (CLT) and the integral transform technique the slowing down equation including inelastic scattering in terms of the Green function of elastic scattering is solved. The Green function is decomposed according to the number of collisions. A formula for the flux at any lethargy O (u) after any number of collisions is derived. An equation for the asymptotic flux is also obtained

  9. Small-angle neutron scattering in materials science

    International Nuclear Information System (INIS)

    Fratzl, P.

    1999-01-01

    Small-angle scattering (SAS) in an ideal tool for studying the structure of materials in the mesoscopic size range between 1 and about 100 nanometers. The basic principles of the method are reviewed, with particular emphasis on data evaluation and interpretation for isotropic as well as oriented or single-crystalline materials. Examples include metal alloys, composites and porous materials. The last section gives a comparison between the use of neutrons and (synchrotron) x-rays for small-angle scattering in materials physics. (author)

  10. Opportunities for inelastic neutron scattering and residual stress measurements

    International Nuclear Information System (INIS)

    Hagen, M.; Studer, A.J.; Cussen, L.; Kirstein, O.

    2003-01-01

    Full text: The Triple Axis Spectrometer (TAS) at the HIFAR reactor has recently undergone a major refurbishment consisting of the replacement of the motors and motor control system, the construction of a sample table with XYZ translation, modification of the analyser system and the installation of a multiwire position sensitive detector. This has enabled its use for both inelastic neutron scattering and residual stress measurements. This instrument will provide a facility for such fields of work within Australia until the installation of a new state-of-the-art TAS and Residual Stress diffractometer at the Replacement Research Reactor. In this talk we will describe the capabilities of the refurbished TAS and how it fits into the overall picture of neutron scattering facilities available, at present and in the future, to the Australian science community

  11. Neutron and Synchrotron X-Ray Scattering Studies of Superconductors

    International Nuclear Information System (INIS)

    Tranquada, J.M.

    2008-01-01

    Superconductors hold the promise for a more stable and efficient electrical grid, but new isotropic, high-temperature superconductors are needed in order to reduce cable manufacturing costs. The effort to understand high-temperature superconductivity, especially in the layered cuprates, provides guidance to the search for new superconductors. Neutron scattering has long provided an important probe of the collective excitations that are involved in the pairing mechanism. For the cuprates, neutron and x-ray diffraction techniques also provide information on competing types of order, such as charge and spin stripes, that appear to be closely connected to the superconductivity. Recently, inelastic x-ray scattering has become competitive for studying phonons and may soon provide valuable information on electronic excitations. Examples of how these techniques contribute to our understanding of superconductivity are presented

  12. Inelastic neutron scattering and lattice dynamics studies in complex solids

    International Nuclear Information System (INIS)

    Rao, Mala N.; Mittal, R.; Choudhury, Narayani; Chaplot, S.L.

    2004-01-01

    At Trombay, lattice dynamics studies employing coherent inelastic neutron scattering (INS) experiments have been carried out at the two research reactors, CIRUS and Dhruva. While the early work at CIRUS involved many elemental solids and ionic molecular solids, recent experiments at Dhruva have focussed on certain superconductors (cuprates and intermetallics), geophysically important minerals (Al 2 SiO 5 , ZrSiO 4 , MnCO 3 ) and layered halides (BaFCl, ZnCl 2 ). In most of the studies, theoretical modelling of lattice dynamics has played a significant role in the interpretation and analysis of the results from experiments. This talk summarises the developments and current activities in the field of inelastic neutron scattering and lattice dynamics at Trombay. (author)

  13. Inelastic neutron scattering in tetragonal KNbO3

    International Nuclear Information System (INIS)

    Fontana, M.D.; Dolling, G.; Kugel, G.E.; Carabatos, C.

    1979-01-01

    Inelastic neutron scattering experiments in tetragonal KNbO 3 show a high anisotropy in some regions of the phonon dispersion relation and the existence of strong one-dimensional intercell correlations between atomic motions along the [100] and [010] directions, in agreement with x-ray diffuse-scattering measurements in the same phase. The transverse phonon modes propagating normally to these directions of strong correlations, that is, with polarization vectors parallel to them, are relatively soft, not only near the zone center but all the way to the zone boundary. Comparison of these results with the Raman, neutron, and x-ray data obtained in the other phases suggests a description of the ferroelectric phase transition mechanism in KNbO 3 in terms of soft modes and dynamic correlations in each phase. (author)

  14. Sheared liquids explored by means of neutron scattering

    CERN Document Server

    Wolff, M; Frick, B; Zabel, H

    2003-01-01

    Despite its large economic impact, lubrication has not been well understood up to now. The present paper shows the possible impact of quasielastic and inelastic neutron scattering in this field. Liquids under shear have been investigated using the backscattering instrument IN16 (ILL). Macroscopic and microscopic modes, which can be addressed within the same measurement, have been explored. For a commercial motor oil a macroscopic velocity distribution with surface slip has been found. For a polymer solution (P85 in deuterated water) we report diffusion to slow down under shear. Additionally, diffusion becomes anisotropic under shear for both samples. The experimental data are evaluated quantitatively by using computer simulations which show the limitation of this technique: the quasielastic linewidth should not be larger than the inelastic energy shift from Doppler scattered neutrons.

  15. Scattering analysis of LOFAR pulsar observations

    Science.gov (United States)

    Geyer, M.; Karastergiou, A.; Kondratiev, V. I.; Zagkouris, K.; Kramer, M.; Stappers, B. W.; Grießmeier, J.-M.; Hessels, J. W. T.; Michilli, D.; Pilia, M.; Sobey, C.

    2017-09-01

    We measure the effects of interstellar scattering on average pulse profiles from 13 radio pulsars with simple pulse shapes. We use data from the LOFAR High Band Antennas, at frequencies between 110 and 190 MHz. We apply a forward fitting technique, and simultaneously determine the intrinsic pulse shape, assuming single Gaussian component profiles. We find that the constant τ, associated with scattering by a single thin screen, has a power-law dependence on frequency τ ∝ ν-α, with indices ranging from α = 1.50 to 4.0, despite simplest theoretical models predicting α = 4.0 or 4.4. Modelling the screen as an isotropic or extremely anisotropic scatterer, we find anisotropic scattering fits lead to larger power-law indices, often in better agreement with theoretically expected values. We compare the scattering models based on the inferred, frequency-dependent parameters of the intrinsic pulse, and the resulting correction to the dispersion measure (DM). We highlight the cases in which fits of extreme anisotropic scattering are appealing, while stressing that the data do not strictly favour either model for any of the 13 pulsars. The pulsars show anomalous scattering properties that are consistent with finite scattering screens and/or anisotropy, but these data alone do not provide the means for an unambiguous characterization of the screens. We revisit the empirical τ versus DM relation and consider how our results support a frequency dependence of α. Very long baseline interferometry, and observations of the scattering and scintillation properties of these sources at higher frequencies, will provide further evidence.

  16. Neutron Scattering of Aromatic and Aliphatic Liquids.

    Science.gov (United States)

    Falkowska, Marta; Bowron, Daniel T; Manyar, Haresh G; Hardacre, Christopher; Youngs, Tristan G A

    2016-07-04

    Organic solvents, such as cyclohexane, cyclohexene, methylcyclohexane, benzene and toluene, are widely used as both reagents and solvents in industrial processes. Despite the ubiquity of these liquids, the local structures that govern the chemical properties have not been studied extensively. Herein, we report neutron diffraction measurements on liquid cyclohexane, cyclohexene, methylcyclohexane, benzene and toluene at 298 K to obtain a detailed description of the local structure in these compounds. The radial distribution functions of the centres of the molecules, as well as the partial distribution functions for the double bond for cyclohexene and methyl group for methylcyclohexane and toluene have been calculated. Additionally, probability density functions and angular radial distribution functions were extracted to provide a full description of the local structure within the chosen liquids. Structural motifs are discussed and compared for all liquids, referring specifically to the functional group and aromaticity present in the different liquids. ©2016 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA.

  17. Bragg optics computer codes for neutron scattering instrument design

    International Nuclear Information System (INIS)

    Popovici, M.; Yelon, W.B.; Berliner, R.R.; Stoica, A.D.

    1997-01-01

    Computer codes for neutron crystal spectrometer design, optimization and experiment planning are described. Phase space distributions, linewidths and absolute intensities are calculated by matrix methods in an extension of the Cooper-Nathans resolution function formalism. For modeling the Bragg reflection on bent crystals the lamellar approximation is used. Optimization is done by satisfying conditions of focusing in scattering and in real space, and by numerically maximizing figures of merit. Examples for three-axis and two-axis spectrometers are given

  18. SANS [small-angle neutron scattering] from polymers and colloids

    International Nuclear Information System (INIS)

    Hayter, J.B.

    1987-01-01

    Small-angle neutron scattering (SANS) has been remarkably successful in providing detailed quantitative structural information on complex everyday materials, such as polymers and colloids, which are often of considerable industrial as well as academic interest. This paper reviews some recent SANS experiments on polymers and colloids, including ferrofluids, and discusses the use of these apparently complex systems as general physical models of the liquid or solid state

  19. Neutron scattering from amorphous, disordered and nanocrystalline materials

    International Nuclear Information System (INIS)

    Price, D.L.

    1994-10-01

    The author has described the power of neutron diffraction and inelastic scattering techniques for determining the structure and dynamics of disordered systems, using the archetypal glass SiO 2 as a detailed example. Of course the field of amorphous and disordered systems contains a much greater variety of types of materials exhibiting a wide range of possible types of disorder. The author gives a brief review of the varieties of order and disorder exhibited by condensed matter

  20. The single-angle neutron scattering facility at Pelindaba

    International Nuclear Information System (INIS)

    Hofmeyr, C.; Mayer, R.M.; Tillwick, D.L.; Starkey, J.R.

    1978-05-01

    The small-angle neutron scattering facility at the SAFARI-1 reactor is described in detail, and with reference to theoretical and practical design considerations. Inexpensive copper microwave guides used as a guide-pipe for slow neutrons provided the basis for a useful though comparatively simple facility. The neutron-spectrum characteristics of the final facility in different configurations of the guide-pipe (both S and single-curved) agree wel with expected values based on results obtained with a test facility. The design, construction, installation and alignment of various components of the facility are outlined, as well as intensity optimisation. A general description is given of experimental procedures and data-aquisition electronics for the four-position sample holder and counter array of up to 18 3 He detectors and a beam monitor [af