WorldWideScience

Sample records for ir elemental analysis

  1. Ir and Rare Earth's Elements determination by Neutron Activation Analysis and ICP - MS in soil samples

    Science.gov (United States)

    Salvini, A.; Cattadori, C.; Broggini, C.; Cagnazzo, M.; Ori, Gian Gabriele; Nisi, S.; Borio, A.; Manera, S.

    2006-05-01

    The platinum metals depleted in the earth's crust are relative to their cosmic abundance; concentration of these elements in sediments may thus indicate influxes of extraterrestrial material. Analysis of these parameters are done easily by Neutron Activation Analysis (NAA) and comparative results with ICP-MS technique show a good match. Results, adjust parameters and limits of this method will be displayed in tables.

  2. Identification of urushi coated films taken from ancient Buddha images by using PIXE, FT-IR, and organic elemental analysis

    International Nuclear Information System (INIS)

    Kagemori, N.; Umemura, K.; Yoshimura, T.; Inoue, M.; Kawai, S.; Yano, K.; Sera, K.; Futatsugawa, S.; Nakamura, Y.

    1999-01-01

    Six types of samples including urushi, urushi tree and black coating films taken from ancient Buddha images were examined by analyses of PIXE, organic element and FT-IR to identify with urushi or another material. Based on the results of three analytical experiments above mentioned, the coating materials aging over hundreds of years were identified with weathered urushi films mixed with other material. Further investigation may reveal the urushi coating techniques used in the past. (author)

  3. Determination of trace elements in the seeds of fruits using instrumental neutron activation analysis (INAA) in Arak, I.R. Iran

    International Nuclear Information System (INIS)

    Pourimani Reza; Meighani Elham; Fathivand Aliasghar

    2018-01-01

    In this study, four fruit's seed samples as Punica granatum L., Citrus medica var. limonum, Malus domestica L. and Citrus vulgaris Risso were prepared from Arak's markets. They were analyzed using instrumental neutron activation method (INAA). In this method, Tehran research reactor as a neutron source and relative INAA method has been used as the analysis method and to record gamma ray spectrum, the high purity germanium detector was used. Pomegranate seeds had the highest number of essential elements. Apple seeds and sour orange seeds contain the highest levels of Mg and K, Respectively. (author)

  4. IR laser enrichment of light elements isotopes - challenges and prospects

    International Nuclear Information System (INIS)

    Parthasarathy, V.

    2002-01-01

    Full text: Infra-red multiple photon dissociation (IR MPD) of poly-atomic molecules has made considerable progress since its discovery in the early seventies. Since the process was found to be isotopically selective; the possibility of laser isotope separation (LIS) created a lot of initial excitement. While the early investigations were concerned with the fundamental dynamics and potential applications of the phenomenon, serious efforts for the isotope enrichment process have been made only during the last decade. These efforts focussed on aspects to improve both the enrichment factor and throughput in various systems. Many research groups have achieved a good measure of success for scaling up the process for various light elements like carbon, oxygen, silicon and sulphur whose isotopes are quite important in medicine and technology. Significant results have been reported especially for the separation of carbon isotopes wherein macroscopic operating scales have been already realised. This talk will give-a summary of our work carried out at BARC and highlight the current efforts for scaling up the process for carbon isotopes enrichment. This would include the design aspects of a large photochemical reactor with multi-pass, refocusing optics for efficient photon utilization. It will also cover the development of a cryogenic distillation set up and a preparative gas chromatograph for a large scale separation and collection of the isotopically enriched photoproduct in the post irradiation stage. Based on the experience gained and infra structure developed, plans are afoot to separate oxygen and sulphur isotopes using a similar approach

  5. Boundary Element Solution of Geometrical Inverse Heat Conduction Problems for Development of IR CAT Scan

    International Nuclear Information System (INIS)

    Choi, C. Y.; Park, C. T.; Kim, T. H.; Han, K. N.; Choe, S. H.

    1995-01-01

    A geometrical inverse heat conduction problem is solved for the development of Infrared Computerized-Axial-Tomography (IR CAT) Scan by using a boundary element method in conjunction with regularization procedure. In this problem, an overspecified temperature condition by infrared scanning is provided on the surface, and is used together with other conditions to solve the position of an unknown boundary (cavity). An auxiliary problem is introduced in the solution of this problem. By defining a hypothetical inner boundary for the auxiliary problem domain, the cavity is located interior to the domain and its position is determined by solving a potential problem. Boundary element method with regularization procedure is used to solve this problem, and the effects of regularization on the inverse solution method are investigated by means of numerical analysis

  6. Quantitative gas analysis with FT-IR

    DEFF Research Database (Denmark)

    Bak, J.; Larsen, A.

    1995-01-01

    Calibration spectra of CO in the 2.38-5100 ppm concentration range (22 spectra) have been measured with a spectral resolution of 4 cm(-1), in the mid-IR (2186-2001 cm(-1)) region, with a Fourier transform infrared (FT-IR) instrument. The multivariate calibration method partial least-squares (PLS1...

  7. Experimental verification of active IR stealth technology by controlling the surface temperature using a thermoelectric element

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Dong Geon; Han, Kuk Il; Choi, Jun Hyuk; Kim, Tae Kuk [Dept. of Mechanical Engineering, Chung Ang University, Seoul (Korea, Republic of)

    2016-10-15

    In this paper, we propose a technique for IR low-observability that uses an active IR signal tuning through the real time control of the object surface temperature according to the varying background environment. This is achieved by applying the proper object surface temperature obtained to result in the minimum radiance difference between the object and the background. Experimental verification by using the thermoelectric temperature control element shows that the IR radiance contrast between the object and the background can be reduced up to 99% during the night and up to 95% during the day time as compared to the un-tuned original radiance contrast values. The stealth technology demonstrated in this paper may be applied for many military systems needed for the IR stealth performance when a suitable temperature control unit is developed.

  8. Experimental verification of active IR stealth technology by controlling the surface temperature using a thermoelectric element

    International Nuclear Information System (INIS)

    Kim, Dong Geon; Han, Kuk Il; Choi, Jun Hyuk; Kim, Tae Kuk

    2016-01-01

    In this paper, we propose a technique for IR low-observability that uses an active IR signal tuning through the real time control of the object surface temperature according to the varying background environment. This is achieved by applying the proper object surface temperature obtained to result in the minimum radiance difference between the object and the background. Experimental verification by using the thermoelectric temperature control element shows that the IR radiance contrast between the object and the background can be reduced up to 99% during the night and up to 95% during the day time as compared to the un-tuned original radiance contrast values. The stealth technology demonstrated in this paper may be applied for many military systems needed for the IR stealth performance when a suitable temperature control unit is developed

  9. Improvenments in environmental trace analysis by GC-IR and LC-IR.

    NARCIS (Netherlands)

    Visser, T.; Vredenbregt, M.J.; Jong, A.P.J.M.; Somsen, G.W.; Hankemeier, T.; Velthorst, N.H.; Gooijer, C.; Brinkman, U.A.T.

    1997-01-01

    Research has been carried out to enlarge the potential of infrared (IR) spectrometry as a detector in gas and liquid chromatography (GC and LC). The study has been directed to applications in environmental analysis. Examples of recently obtained results are presented. The analyte detectability of

  10. Elements of real analysis

    CERN Document Server

    Sprecher, David A

    2010-01-01

    This classic text in introductory analysis delineates and explores the intermediate steps between the basics of calculus and the ultimate stage of mathematics: abstraction and generalization.Since many abstractions and generalizations originate with the real line, the author has made it the unifying theme of the text, constructing the real number system from the point of view of a Cauchy sequence (a step which Dr. Sprecher feels is essential to learn what the real number system is).The material covered in Elements of Real Analysis should be accessible to those who have completed a course in

  11. Linearly Polarized IR Spectroscopy Theory and Applications for Structural Analysis

    CERN Document Server

    Kolev, Tsonko

    2011-01-01

    A technique that is useful in the study of pharmaceutical products and biological molecules, polarization IR spectroscopy has undergone continuous development since it first emerged almost 100 years ago. Capturing the state of the science as it exists today, "Linearly Polarized IR Spectroscopy: Theory and Applications for Structural Analysis" demonstrates how the technique can be properly utilized to obtain important information about the structure and spectral properties of oriented compounds. The book starts with the theoretical basis of linear-dichroic infrared (IR-LD) spectroscop

  12. Analysis of effect of cable degradation on SPND IR calculation

    International Nuclear Information System (INIS)

    Tamboli, P.K.; Sharma, A.; Prasad, A.D.; Singh, Nita; Antony, J.; Kelkar, M.G.; Kaurav, Reetesh; Pramanik, M.

    2013-01-01

    Neutron flux is the most vital parameter in the nuclear reactor safety against Neutronic over power. The modern days Indian PHWRs with large core size are loosely coupled reactors and hence In-core Self Power Neutron Detectors (SPNDs) are most suitable for monitoring local neutron power for generating Regional Overpower Trip. However the SPNDs and its Mineral Insulation Cable are prone to IR loss due to use of ceramic insulation which are highly hygroscopic. The present paper covers the online analysis of IR f degraded cable as per the surveillance requirement of monitoring the IR to assess the healthiness of SPNDs which are part of SSC/SSE for Reactor Protection Systems. The paper also proposes an alternative method for monitoring IR for startup//low power range when SPND signals are yet to pick up and Reactor Control and Protection are based on out of core Ionization Chambers. (author)

  13. IR spectral analysis for the diagnostics of crust earthquake precursors

    Directory of Open Access Journals (Sweden)

    R. M. Umarkhodgaev

    2012-11-01

    Full Text Available Some possible physical processes are analysed that cause, under the condition of additional ionisation in a pre-breakdown electric field, emissions in the infrared (IR interval. The atmospheric transparency region of the IR spectrum at wavelengths of 7–15 μm is taken into account. This transparency region corresponds to spectral lines of small atmospheric constituents like CH4, CO2, N2O, NO2, NO, and O3. The possible intensities of the IR emissions observable in laboratories and in nature are estimated. The acceleration process of the electrons in the pre-breakdown electrical field before its adhesion to the molecules is analyzed. For daytime conditions, modifications of the adsorption spectra of the scattered solar emissions are studied; for nighttime, variations of emission spectra may be used for the analysis.

  14. METHODOLOGICAL ELEMENTS OF SITUATIONAL ANALYSIS

    Directory of Open Access Journals (Sweden)

    Tetyana KOVALCHUK

    2016-07-01

    Full Text Available The article deals with the investigation of theoretical and methodological principles of situational analysis. The necessity of situational analysis is proved in modern conditions. The notion “situational analysis” is determined. We have concluded that situational analysis is a continuous system study which purpose is to identify dangerous situation signs, to evaluate comprehensively such signs influenced by a system of objective and subjective factors, to search for motivated targeted actions used to eliminate adverse effects of the exposure of the system to the situation now and in the future and to develop the managerial actions needed to bring the system back to norm. It is developed a methodological approach to the situational analysis, its goal is substantiated, proved the expediency of diagnostic, evaluative and searching functions in the process of situational analysis. The basic methodological elements of the situational analysis are grounded. The substantiation of the principal methodological elements of system analysis will enable the analyst to develop adaptive methods able to take into account the peculiar features of a unique object which is a situation that has emerged in a complex system, to diagnose such situation and subject it to system and in-depth analysis, to identify risks opportunities, to make timely management decisions as required by a particular period.

  15. Elements of abstract harmonic analysis

    CERN Document Server

    Bachman, George

    2013-01-01

    Elements of Abstract Harmonic Analysis provides an introduction to the fundamental concepts and basic theorems of abstract harmonic analysis. In order to give a reasonably complete and self-contained introduction to the subject, most of the proofs have been presented in great detail thereby making the development understandable to a very wide audience. Exercises have been supplied at the end of each chapter. Some of these are meant to extend the theory slightly while others should serve to test the reader's understanding of the material presented. The first chapter and part of the second give

  16. Platinum group element enrichments and possible chondritic Ru:Ir across the Frasnian-Famennian boundary, western New York State.

    Science.gov (United States)

    Over, D J; Conaway, C A; Katz, D J; Goodfellow, W D; Gregoire, D C

    1997-08-01

    The Frasnian-Famennian boundary is recognized as the culmination of a global mass extinction in the Late Devonian. In western New York State the boundary is a distinct horizon within a pyritic black shale bed of the upper Hanover Shale defined by the first occurrence of Palmatolepis triangularis in the absence of Frasnian conodonts. The boundary is characterized by a minor disconformity marked by a lag concentration of conodonts. Iridium at the boundary is 0.11-0.24 ng/g, two to five times background levels of <0.05 ng/g; other Ir enrichments of 0.38 ng/g and 0.49 ng/g occur within 50 cm of the conodont-constrained boundary. Numerous Ir enrichments in the boundary interval suggest extraterrestrial accretion and platinum group element (PGE) concentration at disconformities, or mobilization and concentration in organic-rich/pyritic-rich laminations from cosmic or terrestrial sources. PGE ratios of Pt/Pd and Ku/Ir at the boundary horizon approximate chondritic ratios and are suggestive of an unaltered extraterrestrial source. These values do not conclusively establish a single extraterrestrial impact as the ultimate cause of the Frasnian-Famennian mass extinction, especially given the presence of similar Ir enrichments elsewhere in the section and the absence at the boundary of microtektites and shocked mineral grains.

  17. Nanomechanical IR spectroscopy for fast analysis of liquid-dispersed engineered nanomaterials

    OpenAIRE

    Andersen, Alina Joukainen; Yamada, Shoko; Ek, Pramod Kumar; Andresen, Thomas Lars; Boisen, Anja; Schmid, Silvan

    2016-01-01

    The proliferated use of engineered nanomaterials (ENMs), e.g. in nanomedicine, calls for novel techniques allowing for fast and sensitive analysis of minute samples. Here we present nanomechanical IR spectroscopy (NAM-IR) for chemical analysis of picograms of ENMs. ENMs are nebulized directly from dispersion and efficiently collected on nanomechanical string resonators through a non-diffusion limited sampling method. Even very small amounts of sample can convert absorbed IR light into a measu...

  18. US-LHC IR magnet error analysis and compensation

    International Nuclear Information System (INIS)

    Wei, J.; Ptitsin, V.; Pilat, F.; Tepikian, S.; Gelfand, N.; Wan, W.; Holt, J.

    1998-01-01

    This paper studies the impact of the insertion-region (IR) magnet field errors on LHC collision performance. Compensation schemes including magnet orientation optimization, body-end compensation, tuning shims, and local nonlinear correction are shown to be highly effective

  19. "Batch" kinetics in flow: online IR analysis and continuous control.

    Science.gov (United States)

    Moore, Jason S; Jensen, Klavs F

    2014-01-07

    Currently, kinetic data is either collected under steady-state conditions in flow or by generating time-series data in batch. Batch experiments are generally considered to be more suitable for the generation of kinetic data because of the ability to collect data from many time points in a single experiment. Now, a method that rapidly generates time-series reaction data from flow reactors by continuously manipulating the flow rate and reaction temperature has been developed. This approach makes use of inline IR analysis and an automated microreactor system, which allowed for rapid and tight control of the operating conditions. The conversion/residence time profiles at several temperatures were used to fit parameters to a kinetic model. This method requires significantly less time and a smaller amount of starting material compared to one-at-a-time flow experiments, and thus allows for the rapid generation of kinetic data. Copyright © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  20. Nanomechanical IR spectroscopy for fast analysis of liquid-dispersed engineered nanomaterials

    DEFF Research Database (Denmark)

    Andersen, Alina Joukainen; Yamada, Shoko; Ek, Pramod Kumar

    2016-01-01

    The proliferated use of engineered nanomaterials (ENMs), e.g. in nanomedicine, calls for novel techniques allowing for fast and sensitive analysis of minute samples. Here we present nanomechanical IR spectroscopy (NAM-IR) for chemical analysis of picograms of ENMs. ENMs are nebulized directly from...

  1. Downhole Elemental Analysis with LIBS

    Science.gov (United States)

    Moreschini, Paolo; Zacny, Kris; Rickman, Doug

    2011-01-01

    In this paper we discuss a novel instrument, currently under development at Honeybee Robotics with SBIR funding from NASA. The device is designed to characterize elemental composition as a function of depth in non-terrestrial geological formations. The instrument consists of a miniaturized laser-induced breakdown spectrometer (LIBS) analyzer integrated in a 2" diameter drill string. While the drill provides subsurface access, the LIBS analyzer provides information on the elemental composition of the borehole wall. This instrument has a variety of space applications ranging from exploration of the Moon for which it was originally designed, to Mars, as well as a variety of terrestrial applications. Subsurface analysis is usually performed by sample acquisition through a drill or excavator, followed by sample preparation and subsequent sample presentation to an instrument or suite of instruments. An alternative approach consisting in bringing a miniaturized version of the instrument to the sample has many advantages over the traditional methodology, as it allows faster response, reduced probability of cross-contamination and a simplification in the sampling mechanisms. LIBS functions by focusing a high energy laser on a material inducing a plasma consisting of a small fraction of the material under analysis. Optical emission from the plasma, analyzed by a spectrometer, can be used to determine elemental composition. A triangulation sensor located in the sensor head determines the distance of the sensor from the borehole wall. An actuator modifies the position of the sensor accordingly, in order to compensate for changes due to the profile of the borehole walls. This is necessary because LIBS measurements are negatively affected by changes in the relative position of the focus of the laser with respect to the position of the sample (commonly referred to as the "lens to sample distance"). Profiling the borehole is done by adjusting the position of the sensor with a

  2. Trace Element Analysis of Selenium

    International Nuclear Information System (INIS)

    Soliman, M.S.A.

    2010-01-01

    The present thesis divided into four chapters as follows:Chapter (1):This chapter contains an introduction on different oxidation states of organic and inorganic species for selenium in environmental and biological samples, the process for separation of selenium from these samples and the importance of selenium as a component for these samples. Also gives notes about the techniques which are used in the elemental analysis for selenium species and the detection limits for selenium in these techniques, selenium species in human body and the importance of these species in protecting the body from the different types of cancer and the sources of selenium in environmental samples (soil and water) and distribution levels of selenium in these samples.Chapter (2):This chapter is divided into two parts :The first part deals with the sample collection process for environmental samples (underground water, soil) and the wet digestion ( microwave digestion ) process of soil samples. It also contains the theory of work of the closed microwave digestion system.The second part contains detailed information concerning the theoretical considerations of the used analytical techniques. These techniques include Hydride generation - Atomic Absorption Spectrometer (HG-AAS), Inductively Coupled Plasma Mass Spectrometer (ICP-MS) and Neutron Activation Analysis (NAA).Chapter (3): This chapter includes the methods of sampling, sample preparation, and sample digesition. The measures of quality assurance are disscused in this chapter. It describes in details the closed microwave digestion technique and the analytical methods used in this study which are present in Central Laboratory for Elemental and Isotopic Analysis (CLEIA) and the Egypt Second Research Reactor (ETRR-2). The described techniques are Atomic Absorption Spectrometer (AAS 6 vario, Analytical Jena GmbH, Germany), JMS-PLASMAX2 Mass Spectrometer (ICP-MS) and the Egypt Second Research Reactor (NAA).

  3. Zr 2Ir 6B with an eightfold superstructure of the cubic perovskite-like boride ZrIr 3B 0.5: Synthesis, crystal structure and bonding analysis

    Science.gov (United States)

    Hermus, Martin; Fokwa, Boniface P. T.

    2010-04-01

    Single phase powder samples and single crystals of Zr 2Ir 6B were successfully synthesized by arc-melting the elements in a water-cooled copper crucible under an argon atmosphere. Superstructure reflections were observed both on powder and on single crystal diffraction data, leading to an eightfold superstructure of ZrIr 3B x phase. The new phase, which has a metallic luster, crystallizes in space group Fm3¯m (no. 225) with the lattice parameters a=7.9903(4) Å, V=510.14(4) Å 3. Its crystal structure was refined on the basis of powder as well as single crystal data. The single crystal refinement converged to R1=0.0239 and w R2=0.0624 for all 88 unique reflections and 6 parameters. Zr 2Ir 6B is isotypic to Ti 2Rh 6B and its structure can be described as a defect double perovskite, A2BB' O6, where the A site is occupied by zirconium, the B site by boron, the O site by iridium but the B' site is vacant, leading to the formation of empty and boron-filled octahedral Ir 6 clusters. According to the result of tight-binding electronic structure calculations, Ir-B and Ir-Zr interactions are mainly responsible for the structural stability of the phase. According to COHP bonding analysis, the strongest bonding occurs for the Ir-B contacts, and the Ir-Ir bonding within the empty clusters is two times stronger than that in the BIr 6 octahedra.

  4. Nanomechanical IR Spectroscopy for the fast analysis of picogram samples of engineered nanomaterials

    DEFF Research Database (Denmark)

    Andersen, Alina Joukainen; Ek, Pramod Kumar; Andresen, Thomas Lars

    2014-01-01

    The proliferation of engineered nanomaterials (ENMs), e.g. in nanomedicine, demands for novel sensitive techniques allowing for the analysis of minute samples. We present nanoelectromechanical system-based IR spectroscopy (NEMS-IR) of picograms of polymeric micelles. The micelles are nebulized...

  5. IR spectral analysis for the diagnostics of crust earthquake precursors

    Science.gov (United States)

    Umarkhodgaev, R. M.; Liperovsky, V. A.; Mikhailin, V. V.; Meister, C.-V.; Naumov, D. Ju

    2012-04-01

    In regions of future earthquakes, a few days before the seismic shock, the emanation of radon and hydrogen is being observed, which causes clouds of increased ionisation in the atmosphere. In the present work the possible diagnostics of these clouds using infrared (IR) spectroscopy is considered, which may be important and useful for the general geophysical system of earthquake prediction and the observation of industrial emissions of radioactive materials into the atmosphere. Some possible physical processes are analysed, which cause, under the condition of additional ionisation in a pre-breakdown electrical field, emissions in the IR interval. In doing so, the transparency region of the IR spectrum at wavelengths of 7-15 μm is taken into account. This transparency region corresponds to spectral lines of small atmospheric constituents like CH4, CO2, N2O, NO2, NO, and O3. The possible intensities of the IR emissions observable in laboratories and in nature are estimated. The acceleration process of the electrons in the pre-breakdown electrical field before its adhesion to the molecules is analysed. The laboratory equipment for the investigation of the IR absorption spectrum is constructed for the cases of normal and decreased atmospheric pressures. The syntheses of ozone and nitrous oxides are performed in the barrier discharge. It is studied if the products of the syntheses may be used to model atmospheric processes where these components take part. Spectra of products of the syntheses in the wavelength region of 2-10 μm are observed and analysed. A device is created for the syntheses and accumulation of nitrous oxides. Experiments to observe the IR-spectra of ozone and nitrous oxides during the syntheses and during the further evolution of these molecules are performed. For the earthquake prediction, practically, the investigation of emission spectra is most important, but during the laboratory experiments, the radiation of the excited molecules is shifted by a

  6. IR and UV spectroscopic analysis of TBP complexes

    International Nuclear Information System (INIS)

    Azzouz, A.; Berrak, A.; Seridi, L.; Attou, M.

    1985-06-01

    The complexity of TBP molecule and the limited number of references stimulated the elaboration of this report. The spectroscopic of TBP and its complexes in the IR and UV fields permitted to elucidate or to confirm certain aspects concerning the solvation phenomenum. In IR spectroscopy, the stretching band of the P→O bond only is characteristic of the complex formed. The position of this band gives sufficient information about the kind and the stability of a complex. The TBP electronic spectra are characterized by two bands (200-220 nm) 1 and (268-290 nm) 2 whose intensity ratio (2/1) is about 0,13. The solvent nature seems to influence the positions of these bands and that of the inflexion point. The band 2 disappears when the TBP is complexed and the position and the intensity of the band 1 depend upon the complex nature

  7. Elemental analysis of soil and hair sample by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

    2004-03-01

    Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used

  8. Elemental analysis of soil and hair sample by instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

    2004-03-01

    Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used.

  9. FINITE ELEMENT ANALYSIS OF ELEMENT ANALYSIS OF A FREE ...

    African Journals Online (AJOL)

    eobe

    the stairs and to compare the finite element ana ... tual three dimensional behavior of the stair slab system. ..... due to its close relation of output with the propo .... flights. It is best not to consider any open well when .... thermodynamics of solids.

  10. Phytochemical screening, proximate and elemental analysis of ...

    African Journals Online (AJOL)

    Citrus sinensis was screened for its phytochemical composition and was evaluated for the proximate and elemental analysis. The phytochemical analysis indicated the presence of reducing sugar, saponins, cardiac glycosides, tannins and flavonoids. The elemental analysis indicated the presence of the following mineral ...

  11. Hydrogenated fullerenes in space: FT-IR spectra analysis

    International Nuclear Information System (INIS)

    El-Barbary, A. A.

    2016-01-01

    Fullerenes and hydrogenated fullerenes are found in circumstellar and interstellar environments. But the determination structures for the detected bands in the interstellar and circumstellar space are not completely understood so far. For that purpose, the aim of this article is to provide all possible infrared spectra for C 20 and C 60 fullerenes and their hydrogenated fullerenes. Density Functional theory (DFT) is applied using B3LYP exchange-functional with basis set 6–31G(d, p). The Fourier transform infrared spectroscopy (FT-IR) is found to be capable of distinguishing between fullerenes, mono hydrogenated fullerenes and fully hydrogenated fullerenes. In addition, deposition of one hydrogen atom outside the fully hydrogenated fullerenes is found to be distinguished by forming H 2 molecule at peak around 4440 cm −1 . However, deposition of one hydrogen atom inside the fully hydrogenated fullerenes cannot be distinguished. The obtained spectral structures are analyzed and are compared with available experimental results.

  12. FINITE ELEMENT ANALYSIS OF STRUCTURES

    Directory of Open Access Journals (Sweden)

    PECINGINA OLIMPIA-MIOARA

    2015-05-01

    Full Text Available The application of finite element method is analytical when solutions can not be applied for deeper study analyzes static, dynamic or other types of requirements in different points of the structures .In practice it is necessary to know the behavior of the structure or certain parts components of the machine under the influence of certain factors static and dynamic . The application of finite element in the optimization of components leads to economic growth , to increase reliability and durability organs studied, thus the machine itself.

  13. Accurate determination of light elements by charged particle activation analysis

    International Nuclear Information System (INIS)

    Shikano, K.; Shigematsu, T.

    1989-01-01

    To develop accurate determination of light elements by CPAA, accurate and practical standardization methods and uniform chemical etching are studied based on determination of carbon in gallium arsenide using the 12 C(d,n) 13 N reaction and the following results are obtained: (1)Average stopping power method with thick target yield is useful as an accurate and practical standardization method. (2)Front surface of sample has to be etched for accurate estimate of incident energy. (3)CPAA is utilized for calibration of light element analysis by physical method. (4)Calibration factor of carbon analysis in gallium arsenide using the IR method is determined to be (9.2±0.3) x 10 15 cm -1 . (author)

  14. Complex of the equipment for instrumental element analysis

    International Nuclear Information System (INIS)

    Borisov, G.I.; Komkov, M.M.; Kuz'michev, V.A.

    1986-01-01

    Complex of the equipment for instrumental element analysis at the IR-8 reactor is designed, fabricated and taken into operation. The complex is provided with a multichannel system of vacuum pneumatic transport with radiation positions in the reactor horizontal tangential channel for neutron-activation analysis by short-lived isotopes; specialized dry vertical channels in a beryllium reflector of the reactor and remote system of radioactive sample replacement for neutron-activation analysis by long-lived isotopes; a specialized horizontal tangential channel for neutron beam extraction by means of a beryllium converter and remote device for studied sample replacement under radiation and measurement of prompt γ-radiation for neutron-radiation analysis; a measuring center using minicomputers for experimental data accumulation and processing and analysis control

  15. Why do probabilistic finite element analysis ?

    CERN Document Server

    Thacker, Ben H

    2008-01-01

    The intention of this book is to provide an introduction to performing probabilistic finite element analysis. As a short guideline, the objective is to inform the reader of the use, benefits and issues associated with performing probabilistic finite element analysis without excessive theory or mathematical detail.

  16. Hydrogenated fullerenes in space: FT-IR spectra analysis

    Energy Technology Data Exchange (ETDEWEB)

    El-Barbary, A. A. [Physics Department, Faculty of Education, Ain-Shams University, Cairo, Egypt Physics Department, Faculty of Science, Jazan University, Jazan (Saudi Arabia)

    2016-06-10

    Fullerenes and hydrogenated fullerenes are found in circumstellar and interstellar environments. But the determination structures for the detected bands in the interstellar and circumstellar space are not completely understood so far. For that purpose, the aim of this article is to provide all possible infrared spectra for C{sub 20} and C{sub 60} fullerenes and their hydrogenated fullerenes. Density Functional theory (DFT) is applied using B3LYP exchange-functional with basis set 6–31G(d, p). The Fourier transform infrared spectroscopy (FT-IR) is found to be capable of distinguishing between fullerenes, mono hydrogenated fullerenes and fully hydrogenated fullerenes. In addition, deposition of one hydrogen atom outside the fully hydrogenated fullerenes is found to be distinguished by forming H{sub 2} molecule at peak around 4440 cm{sup −1}. However, deposition of one hydrogen atom inside the fully hydrogenated fullerenes cannot be distinguished. The obtained spectral structures are analyzed and are compared with available experimental results.

  17. Elements of stock market analysis

    Directory of Open Access Journals (Sweden)

    Suciu, T.

    2013-12-01

    Full Text Available The paper represents a starting point in the presentation of the two types of stock/market analysis: the fundamental analysis and the technical analysis. The fundamental analysis consist in the assessment of the financial and economic status of the company together with the context and macroeconomic environment where it activates. The technical analysis deals with the demand and supply of securities and the evolution of their trend on the market, using a range of graphics and charts to illustrate the market tendencies for the quick identification of the best moments to buy or sell.

  18. Finite element application to global reactor analysis

    International Nuclear Information System (INIS)

    Schmidt, F.A.R.

    1981-01-01

    The Finite Element Method is described as a Coarse Mesh Method with general basis and trial functions. Various consequences concerning programming and application of Finite Element Methods in reactor physics are drawn. One of the conclusions is that the Finite Element Method is a valuable tool in solving global reactor analysis problems. However, problems which can be described by rectangular boxes still can be solved with special coarse mesh programs more efficiently. (orig.) [de

  19. Finite element analysis of tibial fractures

    DEFF Research Database (Denmark)

    Wong, Christian Nai En; Mikkelsen, Mikkel Peter W; Hansen, Leif Berner

    2010-01-01

    Project. The data consisted of 21,219 3D elements with a cortical shell and a trabecular core. Three types of load of torsion, a direct lateral load and axial compression were applied. RESULTS: The finite element linear static analysis resulted in relevant fracture localizations and indicated relevant...

  20. A CAREM type fuel element dynamic analysis

    International Nuclear Information System (INIS)

    Magoia, J.E.

    1990-01-01

    A first analysis on the dynamic behaviour of a fuel element designed for the CAREM nuclear reactor (Central Argentina de Elementos Modulares) was performed. The model used to represent this dynamic behaviour was satisfactorily evaluated. Using primary estimations for some of its numerical parameters, a first approximation to its natural vibrational modes was obtained. Results obtained from fuel elements frequently used in nuclear power plants of the PWR (Pressurized Water Reactors) type, are compared with values resulting from similar analysis. (Author) [es

  1. Finite element analysis of piezoelectric materials

    International Nuclear Information System (INIS)

    Lowrie, F.; Stewart, M.; Cain, M.; Gee, M.

    1999-01-01

    This guide is intended to help people wanting to do finite element analysis of piezoelectric materials by answering some of the questions that are peculiar to piezoelectric materials. The document is not intended as a complete beginners guide for finite element analysis in general as this is better dealt with by the individual software producers. The guide is based around the commercial package ANSYS as this is a popular package amongst piezoelectric material users, however much of the information will still be useful to users of other finite element codes. (author)

  2. Development of IR Contrast Data Analysis Application for Characterizing Delaminations in Graphite-Epoxy Structures

    Science.gov (United States)

    Havican, Marie

    2012-01-01

    Objective: Develop infrared (IR) flash thermography application based on use of a calibration standard for inspecting graphite-epoxy laminated/honeycomb structures. Background: Graphite/Epoxy composites (laminated and honeycomb) are widely used on NASA programs. Composite materials are susceptible for impact damage that is not readily detected by visual inspection. IR inspection can provide required sensitivity to detect surface damage in composites during manufacturing and during service. IR contrast analysis can provide characterization of depth, size and gap thickness of impact damage. Benefits/Payoffs: The research provides an empirical method of calibrating the flash thermography response in nondestructive evaluation. A physical calibration standard with artificial flaws such as flat bottom holes with desired diameter and depth values in a desired material is used in calibration. The research devises several probability of detection (POD) analysis approaches to enable cost effective POD study to meet program requirements.

  3. Attenuated total reflectance-FT-IR spectroscopy for gunshot residue analysis: potential for ammunition determination.

    Science.gov (United States)

    Bueno, Justin; Sikirzhytski, Vitali; Lednev, Igor K

    2013-08-06

    The ability to link a suspect to a particular shooting incident is a principal task for many forensic investigators. Here, we attempt to achieve this goal by analysis of gunshot residue (GSR) through the use of attenuated total reflectance (ATR) Fourier transform infrared spectroscopy (FT-IR) combined with statistical analysis. The firearm discharge process is analogous to a complex chemical process. Therefore, the products of this process (GSR) will vary based upon numerous factors, including the specific combination of the firearm and ammunition which was discharged. Differentiation of FT-IR data, collected from GSR particles originating from three different firearm-ammunition combinations (0.38 in., 0.40 in., and 9 mm calibers), was achieved using projection to latent structures discriminant analysis (PLS-DA). The technique was cross (leave-one-out), both internally and externally, validated. External validation was achieved via assignment (caliber identification) of unknown FT-IR spectra from unknown GSR particles. The results demonstrate great potential for ATR-FT-IR spectroscopic analysis of GSR for forensic purposes.

  4. Antioxidant activity and FT-IR analysis of Datura innoxia and Datura ...

    African Journals Online (AJOL)

    Materials and Methods: Determination of total phenolic content and total flavonoid content and antioxidant activity in terms of total antioxidant assay, ABTS assay, DPPH assay and in-vitro lipid peroxidation inhibiting activity were determined along with the FT-IR (Fourier transform infrared spectroscopy) analysis of the ...

  5. Determining the degree of grafting for poly (vinylidene fluoride) graft-copolymers using fluorine elemental analysis

    International Nuclear Information System (INIS)

    Yu Yang; Zhang Bowu; Yang Xuanxuan; Deng Bo; Li Linfan; Yu Ming; Li Jingye

    2011-01-01

    Acrylic acid (AAc) and styrene (St) were grafted onto poly (vinylidene fluoride) (PVDF) powder or membrane samples by pre-irradiation graft copolymerization. The grafted chains were proved by FT-IR spectroscopy analysis. The degree of grafting (DG) of the grafted PVDF was determined by fluorine elemental analysis (FEA) method, and was compared with the DGs determined by weighing method, acid-base back titration method and quantitative FT-IR method. The results show that the FEA method is accurate, convenient and universal, especially for the grafted polymer powders. (authors)

  6. ANSYS mechanical APDL for finite element analysis

    CERN Document Server

    Thompson, Mary Kathryn

    2017-01-01

    ANSYS Mechanical APDL for Finite Element Analysis provides a hands-on introduction to engineering analysis using one of the most powerful commercial general purposes finite element programs on the market. Students will find a practical and integrated approach that combines finite element theory with best practices for developing, verifying, validating and interpreting the results of finite element models, while engineering professionals will appreciate the deep insight presented on the program's structure and behavior. Additional topics covered include an introduction to commands, input files, batch processing, and other advanced features in ANSYS. The book is written in a lecture/lab style, and each topic is supported by examples, exercises and suggestions for additional readings in the program documentation. Exercises gradually increase in difficulty and complexity, helping readers quickly gain confidence to independently use the program. This provides a solid foundation on which to build, preparing readers...

  7. Elemental analysis with external-beam PIXE

    Science.gov (United States)

    Lin, E. K.; Wang, C. W.; Teng, P. K.; Huang, Y. M.; Chen, C. Y.

    1992-05-01

    A beamline system and experimental setup has been established for elemental analysis using PIXE with an external beam. Experiments for the study of the elemental composition of ancient Chinese potsherds (the Min and Ching ages) were performed. Continuum X-ray spectra from the samples bombarded by 3 MeV protons have been measured with a Si(Li) detector. From the analysis of PIXE data, the concentration of the main elements (Al, Si, K, and Ca) and of more than ten trace elements in the matrices and glazed surfaces were determined. Results for two different potsherds are presented, and those obtained from the glaze colorants are compared with the results of measurements on a Ching blue-and-white porcelain vase.

  8. Finite elements for analysis and design

    CERN Document Server

    Akin, J E; Davenport, J H

    1994-01-01

    The finite element method (FEM) is an analysis tool for problem-solving used throughout applied mathematics, engineering, and scientific computing. Finite Elements for Analysis and Design provides a thoroughlyrevised and up-to-date account of this important tool and its numerous applications, with added emphasis on basic theory. Numerous worked examples are included to illustrate the material.Key Features* Akin clearly explains the FEM, a numerical analysis tool for problem-solving throughout applied mathematics, engineering and scientific computing* Basic theory has bee

  9. Electrical machine analysis using finite elements

    CERN Document Server

    Bianchi, Nicola

    2005-01-01

    OUTLINE OF ELECTROMAGNETIC FIELDSVector AnalysisElectromagnetic FieldsFundamental Equations SummaryReferencesBASIC PRINCIPLES OF FINITE ELEMENT METHODSIntroductionField Problems with Boundary ConditionsClassical Method for the Field Problem SolutionThe Classical Residual Method (Galerkin's Method)The Classical Variational Method (Rayleigh-Ritz's Method)The Finite Element MethodReferencesAPPLICATIONS OF THE FINITE ELEMENT METHOD TO TWO-DIMENSIONAL FIELDSIntroductionLinear Interpolation of the Function fApplication of the Variational MethodSimple Descriptions of Electromagnetic FieldsAppendix: I

  10. Elemental analysis techniques using proton microbeam

    International Nuclear Information System (INIS)

    Sakai, Takuro; Oikawa, Masakazu; Sato, Takahiro

    2005-01-01

    Proton microbeam is a powerful tool for two-dimensional elemental analysis. The analysis is based on Particle Induced X-ray Emission (PIXE) and Particle Induced Gamma-ray Emission (PIGE) techniques. The paper outlines the principles and instruments, and describes the dental application has been done in JAERI Takasaki. (author)

  11. Trace element analysis of nail polishes

    International Nuclear Information System (INIS)

    Misra, G.; Mittal, V.K.; Sahota, H.S.

    1999-01-01

    Instrumental neutron activation analysis (INAA) technique was used to measure the concentrations of various trace elements in nail polishes of popular Indian and foreign brands. The aim of the present experiment was to see whether trace elements could distinguish nail polishes of different Indian and foreign brands from forensic point of view. It was found that cesium can act as a marker to differentiate foreign and Indian brands. (author)

  12. Chemical analysis of rare earth elements

    International Nuclear Information System (INIS)

    Tsukahara, Ryoichi; Sakoh, Takefumi; Nagai, Iwao

    1994-01-01

    Recently attention has been paid to ICP-AES or ICP-MS, and the reports on the analysis of rare earth elements by utilizing these methods continue to increase. These reports have become to take about 30% of the reports on rare earth analysis, and this is because these methods are highly sensitive to rare earth elements, and also these methods have spread widely. In ICP-AES and ICP-MS, mostly solution samples are measured, therefore, solids must be made into solution. At the time of quantitatively determining the rare earth elements of low concentration, separation and concentration are necessary. Referring to the literatures reported partially in 1990 and from 1991 to 1993, the progress of ICP-AES and ICP-MS is reported. Rare earth oxides and the alloys containing rare earth elements are easily decomposed with acids, but the decomposition of rocks is difficult, and its method is discussed. The separation of the rare earth elements from others in geochemical samples, cation exchange process is frequently utilized. Also solvent extraction process has been studied. For the separation of rare earth elements mutually, chromatography is used. The spectral interference in spectral analysis was studied. The comparison of these methods with other methods is reported. (K.I)

  13. PIXE - a new method for elemental analysis

    International Nuclear Information System (INIS)

    Johansson, S.A.E.

    1983-01-01

    With elemental analysis we mean the determination of which chemical elements are present in a sample and of their concentration. This is an old and important problem in chemistry. The earliest methods were purely chemical and many such methods are still used. However, various methods based on physical principles have gradually become more and more important. One such method is neutron activation. When the sample is bombarded with neutrons it becomes radioactive and the various radioactive isotopes produced can be identified by the radiation they emit. From the measured intensity of the radiation one can calculate how much of a certain element that is present in the sample. Another possibility is to study the light emitted when the sample is excited in various ways. A spectroscopic investigation of the light can identify the chemical elements and allows also a determination of their concentration in the sample. In the same way, if a sample can be brought to emit X-rays, this radiation is also characteristic for the elements present and can be used to determine the elemental concentration. One such X-ray method which has been developed recently is PIXE. The name is an acronym for Particle Induced X-ray Emission and indicates the principle of the method. Particles in this context means heavy, charged particles such as protons and a-particles of rather high energy. Hence, in PIXE-analysis the sample is irradiated in the beam of an accelerator and the emitted X-rays are studied. (author)

  14. Identification of mineral compositions in some renal calculi by FT Raman and IR spectral analysis

    Science.gov (United States)

    Tonannavar, J.; Deshpande, Gouri; Yenagi, Jayashree; Patil, Siddanagouda B.; Patil, Nikhil A.; Mulimani, B. G.

    2016-02-01

    We present in this paper accurate and reliable Raman and IR spectral identification of mineral constituents in nine samples of renal calculi (kidney stones) removed from patients suffering from nephrolithiasis. The identified mineral components include Calcium Oxalate Monohydrate (COM, whewellite), Calcium Oxalate Dihydrate (COD, weddellite), Magnesium Ammonium Phosphate Hexahydrate (MAPH, struvite), Calcium Hydrogen Phosphate Dihydrate (CHPD, brushite), Pentacalcium Hydroxy Triphosphate (PCHT, hydroxyapatite) and Uric Acid (UA). The identification is based on a satisfactory assignment of all the observed IR and Raman bands (3500-400 cm- 1) to chemical functional groups of mineral components in the samples, aided by spectral analysis of pure materials of COM, MAPH, CHPD and UA. It is found that the eight samples are composed of COM as the common component, the other mineral species as common components are: MAPH in five samples, PCHT in three samples, COD in three samples, UA in three samples and CHPD in two samples. One sample is wholly composed of UA as a single component; this inference is supported by the good agreement between ab initio density functional theoretical spectra and experimental spectral measurements of both sample and pure material. A combined application of Raman and IR techniques has shown that, where the IR is ambiguous, the Raman analysis can differentiate COD from COM and PCHT from MAPH.

  15. Identification of mineral compositions in some renal calculi by FT Raman and IR spectral analysis.

    Science.gov (United States)

    Tonannavar, J; Deshpande, Gouri; Yenagi, Jayashree; Patil, Siddanagouda B; Patil, Nikhil A; Mulimani, B G

    2016-02-05

    We present in this paper accurate and reliable Raman and IR spectral identification of mineral constituents in nine samples of renal calculi (kidney stones) removed from patients suffering from nephrolithiasis. The identified mineral components include Calcium Oxalate Monohydrate (COM, whewellite), Calcium Oxalate Dihydrate (COD, weddellite), Magnesium Ammonium Phosphate Hexahydrate (MAPH, struvite), Calcium Hydrogen Phosphate Dihydrate (CHPD, brushite), Pentacalcium Hydroxy Triphosphate (PCHT, hydroxyapatite) and Uric Acid (UA). The identification is based on a satisfactory assignment of all the observed IR and Raman bands (3500-400c m(-1)) to chemical functional groups of mineral components in the samples, aided by spectral analysis of pure materials of COM, MAPH, CHPD and UA. It is found that the eight samples are composed of COM as the common component, the other mineral species as common components are: MAPH in five samples, PCHT in three samples, COD in three samples, UA in three samples and CHPD in two samples. One sample is wholly composed of UA as a single component; this inference is supported by the good agreement between ab initio density functional theoretical spectra and experimental spectral measurements of both sample and pure material. A combined application of Raman and IR techniques has shown that, where the IR is ambiguous, the Raman analysis can differentiate COD from COM and PCHT from MAPH. Copyright © 2015 Elsevier B.V. All rights reserved.

  16. Analysis of light elements by PIGE

    International Nuclear Information System (INIS)

    Kim, Y. S.; Choi, H. W.; Kim, D. K.; Woo, H. J.; Kim, N. B.; Park, K. S.

    2000-01-01

    The PIGE (Proton Induced Gamma ray Emission) method was applied for the measurement of light elements Li - K. A test measurement has been performed for geological, biological, environmental and material samples by using a standard sample for each element. The measurement was performed for the two proton energies of 2.4 and 3.4 MeV, and 3.4MeV was found to yield better result for multielemental analysis. The result shows a fair agreement within 15% for all elements with standard values. The detection limits of Li, B, F and Na are less than 100 ppm, while those of the other elements are from a few hundred ppm to a few percents. (author)

  17. Single cell elemental analysis using nuclear microscopy

    International Nuclear Information System (INIS)

    Ren, M.Q.; Thong, P.S.P.; Kara, U.; Watt, F.

    1999-01-01

    The use of Particle Induced X-ray Emission (PIXE), Rutherford Backscattering Spectrometry (RBS) and Scanning Transmission Ion Microscopy (STIM) to provide quantitative elemental analysis of single cells is an area which has high potential, particularly when the trace elements such as Ca, Fe, Zn and Cu can be monitored. We describe the methodology of sample preparation for two cell types, the procedures of cell imaging using STIM, and the quantitative elemental analysis of single cells using RBS and PIXE. Recent work on single cells at the Nuclear Microscopy Research Centre,National University of Singapore has centred around two research areas: (a) Apoptosis (programmed cell death), which has been recently implicated in a wide range of pathological conditions such as cancer, Parkinson's disease etc, and (b) Malaria (infection of red blood cells by the malaria parasite). Firstly we present results on the elemental analysis of human Chang liver cells (ATTCC CCL 13) where vanadium ions were used to trigger apoptosis, and demonstrate that nuclear microscopy has the capability of monitoring vanadium loading within individual cells. Secondly we present the results of elemental changes taking place in individual mouse red blood cells which have been infected with the malaria parasite and treated with the anti-malaria drug Qinghaosu (QHS)

  18. Orthodontic treatment: Introducing finite element analysis

    NARCIS (Netherlands)

    Driel, W.D. van; Leeuwen, E.J. van

    1998-01-01

    The aim of orthodontic treatment is the displacement of teeth by means ofspecial appliances, like braces and brackets. Through these appliances the orthodontist can apply a set of forces to the teeth which wilt result in its displacement through the jawbone. Finite Element analysis of this process

  19. Uncertainties in elemental quantitative analysis by PIXE

    International Nuclear Information System (INIS)

    Montenegro, E.C.; Baptista, G.B.; Paschoa, A.S.; Barros Leite, C.V.

    1979-01-01

    The effects of the degree of non-uniformity of the particle beam, matrix composition and matrix thickness in a quantitative elemental analysis by particle induced X-ray emission (PIXE) are discussed and a criterion to evaluate the resulting degree of uncertainty in the mass determination by this method is established. (Auth.)

  20. Isogeometric finite element analysis of poroelasticity

    NARCIS (Netherlands)

    Irzal, F.; Remmers, J.J.C.; Verhoosel, C.V.; Borst, de R.

    2013-01-01

    We present an alternative numerical approach for predicting the behaviour of a deformable fluid-saturated porous medium. The conventional finite element technology is replaced by isogeometric analysis that uses non-uniform rational B-splines. The ability of these functions to provide higher-order

  1. Application of FT-IR spectroscopy on breast cancer serum analysis

    Science.gov (United States)

    Elmi, Fatemeh; Movaghar, Afshin Fayyaz; Elmi, Maryam Mitra; Alinezhad, Heshmatollah; Nikbakhsh, Novin

    2017-12-01

    Breast cancer is regarded as the most malignant tumor among women throughout the world. Therefore, early detection and proper diagnostic methods have been known to help save women's lives. Fourier Transform Infrared (FT-IR) spectroscopy, coupled with PCA-LDA analysis, is a new technique to investigate the characteristics of serum in breast cancer. In this study, 43 breast cancer and 43 healthy serum samples were collected, and the FT-IR spectra were recorded for each one. Then, PCA analysis and linear discriminant analysis (LDA) were used to analyze the spectral data. The results showed that there were differences between the spectra of the two groups. Discriminating wavenumbers were associated with several spectral differences over the 950-1200 cm- 1(sugar), 1190-1350 cm- 1 (collagen), 1475-1710 cm- 1 (protein), 1710-1760 cm- 1 (ester), 2800-3000 cm- 1 (stretching motions of -CH2 & -CH3), and 3090-3700 cm- 1 (NH stretching) regions. PCA-LDA performance on serum IR could recognize changes between the control and the breast cancer cases. The diagnostic accuracy, sensitivity, and specificity of PCA-LDA analysis for 3000-3600 cm- 1 (NH stretching) were found to be 83%, 84%, 74% for the control and 80%, 76%, 72% for the breast cancer cases, respectively. The results showed that the major spectral differences between the two groups were related to the differences in protein conformation in serum samples. It can be concluded that FT-IR spectroscopy, together with multivariate data analysis, is able to discriminate between breast cancer and healthy serum samples.

  2. Upstand Finite Element Analysis of Slab Bridges

    OpenAIRE

    O'Brien, Eugene J.; Keogh, D.L.

    1998-01-01

    For slab bridge decks with wide transverse edge cantilevers, the plane grillage analogy is shown to be an inaccurate method of linear elastic analysis due to variations in the vertical position of the neutral axis. The upstand grillage analogy is also shown to give inaccurate results, this time due to inappropriate modelling of in-plane distortions. An alternative method, known as upstand finite element analysis, is proposed which is sufficiently simple to be used on an everyday basis in the ...

  3. Determination of the elemental composition of copper and bronze objects by neutron activation analysis

    International Nuclear Information System (INIS)

    Hoelttae, P.; Rosenberg, R.J.

    1987-01-01

    A method for the elemental analysis of copper and bronze objects is described. Na, Co, Ni, Cu, Zn, As, Ag, Sn, Sb, W, Ir and Au are determined through instrumental neutron activation analysis. Mg, Al, V, Ti and Mn are determined after chemical separation using anionic exchange. The detection limits for a number of other elements are also given. Results for NBS standard reference materials are presented and the results are compared with the recommended values. The agreement is good. The results of the analysis of five ancient bronze and two copper objects are also presented. (author) 3 refs.; 4 tabs

  4. Determination of the elemental composition of copper and bronze objects by neutron activation analysis

    International Nuclear Information System (INIS)

    Hoelttae, P.; Rosenberg, R.J.

    1986-01-01

    A method for the elemental analysis of copper and bronze objects is described. Na, Co, Ni, Cu, Zn, As, Ag, Sn, Sb, W, Ir and Au are determined through instrumental neutron activation analysis. Mg, Al, V, Ti and Mn are determined after chemical separation using anionic exchange. The detection limits for a number of other elements are also given. Results for NBS standard reference materials are presented and the results compared with the recommended values. The agreement is good. The results of the analysis of five ancient bronze and two copper objects are presented. (author)

  5. Platinum-group elements fractionation by selective complexing, the Os, Ir, Ru, Rh-arsenide-sulfide systems above 1020 °C

    Science.gov (United States)

    Helmy, Hassan M.; Bragagni, Alessandro

    2017-11-01

    The platinum-group element (PGE) contents in magmatic ores and rocks are normally in the low μg/g (even in the ng/g) level, yet they form discrete platinum-group mineral (PGM) phases. IPGE (Os, Ir, Ru) + Rh form alloys, sulfides, and sulfarsenides while Pt and Pd form arsenides, tellurides, bismuthoids and antimonides. We experimentally investigate the behavior of Os, Ru, Ir and Rh in As-bearing sulfide system between 1300 and 1020 °C and show that the prominent mineralogical difference between IPGE (+Rh) and Pt and Pd reflects different chemical preference in the sulfide melt. At temperatures above 1200 °C, Os shows a tendency to form alloys. Ruthenium forms a sulfide (laurite RuS2) while Ir and Rh form sulfarsenides (irarsite IrAsS and hollingworthite RhAsS, respectively). The chemical preference of PGE is selective: IPGE + Rh form metal-metal, metal-S and metal-AsS complexes while Pt and Pd form semimetal complexes. Selective complexing followed by mechanical separation of IPGE (and Rh)-ligand from Pt- and Pd-ligand associations lead to PGE fractionation.

  6. The first photometric analysis of the near contact binary IR Cas

    International Nuclear Information System (INIS)

    Li, Kai; Hu, S.-M.; Guo, D.-F.; Jiang, Y.-G.; Gao, D.-Y.; Chen, X.

    2014-01-01

    The first photometric analysis of IR Cas was carried out based on the new observed BVRI light curves. The symmetric light curves and nearly flat secondary minimum indicate that very precise photometric results can be determined. We found that IR Cas is a near contact binary with the primary component filling its Roche lobe. An analysis of the O – C diagram based on all available times of minimum light reveals evidence for a periodic change with a semi-amplitude of 0.0153 days and a period of 39.7 yr superimposed on a secular decrease at a rate of dp/dt = –1.28(± 0.09) × 10 –7 days yr –1 . The most reasonable explanation for the periodic change is the light time-travel effect due to a third body. The period decrease may be caused by mass transfer from the primary component to the secondary. With the decreasing period, IR Cas would eventually evolve into a contact system.

  7. Spatial variation of contaminant elements of roadside dust samples from Budapest (Hungary) and Seoul (Republic of Korea), including Pt, Pd and Ir.

    Science.gov (United States)

    Sager, Manfred; Chon, Hyo-Taek; Marton, Laszlo

    2015-02-01

    Roadside dusts were studied to explain the spatial variation and present levels of contaminant elements including Pt, Pd and Ir in urban environment and around Budapest (Hungary) and Seoul (Republic of Korea). The samples were collected from six sites of high traffic volumes in Seoul metropolitan city and from two control sites within the suburbs of Seoul, for comparison. Similarly, road dust samples were obtained two times from traffic focal points in Budapest, from the large bridges across the River Danube, from Margitsziget (an island in the Danube in the northern part of Budapest, used for recreation) as well as from main roads (no highways) outside Budapest. The samples were analysed for contaminant elements by ICP-AES and for Pt, Pd and Ir by ICP-MS. The highest Pt, Pd and Ir levels in road dusts were found from major roads with high traffic volume, but correlations with other contaminant elements were low, however. This reflects automobile catalytic converter to be an important source. To interpret the obtained multi-element results in short, pollution index, contamination index and geo-accumulation index were calculated. Finally, the obtained data were compared with total concentrations encountered in dust samples from Madrid, Oslo, Tokyo and Muscat (Oman). Dust samples from Seoul reached top level concentrations for Cd-Zn-As-Co-Cr-Cu-Mo-Ni-Sn. Just Pb was rather low because unleaded gasoline was introduced as compulsory in 1993. Concentrations in Budapest dust samples were lower than from Seoul, except for Pb and Mg. Compared with Madrid as another continental site, Budapest was higher in Co-V-Zn. Dust from Oslo, which is not so large, contained more Mn-Na-Sr than dust from other towns, but less other metals.

  8. Modelling optimization involving different types of elements in finite element analysis

    International Nuclear Information System (INIS)

    Wai, C M; Rivai, Ahmad; Bapokutty, Omar

    2013-01-01

    Finite elements are used to express the mechanical behaviour of a structure in finite element analysis. Therefore, the selection of the elements determines the quality of the analysis. The aim of this paper is to compare and contrast 1D element, 2D element, and 3D element used in finite element analysis. A simple case study was carried out on a standard W460x74 I-beam. The I-beam was modelled and analyzed statically with 1D elements, 2D elements and 3D elements. The results for the three separate finite element models were compared in terms of stresses, deformation and displacement of the I-beam. All three finite element models yield satisfactory results with acceptable errors. The advantages and limitations of these elements are discussed. 1D elements offer simplicity although lacking in their ability to model complicated geometry. 2D elements and 3D elements provide more detail yet sophisticated results which require more time and computer memory in the modelling process. It is also found that the choice of element in finite element analysis is influence by a few factors such as the geometry of the structure, desired analysis results, and the capability of the computer

  9. Structural analysis of reactor fuel elements

    International Nuclear Information System (INIS)

    Weeks, R.W.

    1977-01-01

    An overview of fuel-element modeling is presented that traces the development of codes for the prediction of light-water-reactor and fast-breeder-reactor fuel-element performance. It is concluded that although the mathematical analysis is now far advanced, the development and incorporation of mechanistic constitutive equations has not kept pace. The resultant reliance on empirical correlations severely limits the physical insight that can be gained from code extrapolations. Current efforts include modeling of alternate fuel systems, analysis of local fuel-cladding interactions, and development of a predictive capability for off-normal behavior. Future work should help remedy the current constitutive deficiencies and should include the development of deterministic failure criteria for use in design

  10. Introduction to nonlinear finite element analysis

    CERN Document Server

    Kim, Nam-Ho

    2015-01-01

    This book introduces the key concepts of nonlinear finite element analysis procedures. The book explains the fundamental theories of the field and provides instructions on how to apply the concepts to solving practical engineering problems. Instead of covering many nonlinear problems, the book focuses on three representative problems: nonlinear elasticity, elastoplasticity, and contact problems. The book is written independent of any particular software, but tutorials and examples using four commercial programs are included as appendices: ANSYS, NASTRAN, ABAQUS, and MATLAB. In particular, the MATLAB program includes all source codes so that students can develop their own material models, or different algorithms. This book also: ·         Presents clear explanations of nonlinear finite element analysis for elasticity, elastoplasticity, and contact problems ·         Includes many informative examples of nonlinear analyses so that students can clearly understand the nonlinear theory ·    ...

  11. Finite element analysis of nonlinear creeping flows

    International Nuclear Information System (INIS)

    Loula, A.F.D.; Guerreiro, J.N.C.

    1988-12-01

    Steady-state creep problems with monotone constitutive laws are studied. Finite element approximations are constructed based on mixed Petrov-Galerkin formulations for constrained problems. Stability, convergence and a priori error estimates are proved for equal-order discontinuous stress and continuous velocity interpolations. Numerical results are presented confirming the rates of convergence predicted in the analysis and the good performance of this formulation. (author) [pt

  12. Trace-element analysis in environmental sciences

    International Nuclear Information System (INIS)

    Valkovic, V.; Moschini, G.

    1988-01-01

    The use of charged-particle accelerators in trace-element analysis in the field of environmental sciences is described in this article. Nuclear reactions, charged-particle-induced X-ray emission as well as other nuclear and atomic processes can be used individually, or combined, in developing adequate analytical systems. In addition to concentration levels, concentration levels, concentration profiles can be measured, resulting in unique information. Some examples of experiments performed are described together with the suggestions for future measurements [pt

  13. Finite element analysis of inelastic structural behavior

    International Nuclear Information System (INIS)

    Argyris, J.H.; Szimmat, J.; Willam, K.J.

    1977-01-01

    The paper describes recent achievements in the finite element analysis of inelastic material behavior. The main purpose is to examine the interaction of three disciplines; (i) the finite element formulation of large deformation problems in the light of a systematic linearization, (ii) the constitutive modelling of inelastic processes in the rate-dependent and rate-independent response regime and (iii) the numerical solution of nonlinear rate problems via incremental iteration techniques. In the first part, alternative finite element models are developed for the idealization of large deformation problems. A systematic approach is presented to linearize the field equations locally by an incremental procedure. The finite element formulation is then examined for the description of inelastic material processes. In the second part, nonlinear and inelastic material phenomena are classified and illustrated with representative examples of concrete and metal components. In particular, rate-dependent and rate-independent material behavior is examined and representative constitutive models are assessed for their mathematical characterization. Hypoelastic, elastoplastic and endochronic models are compared for the description rate-independent material phenomena. In the third part, the numerial solution of inelastic structural behavior is discussed. In this context, several incremental techniques are developed and compared for tracing the evolution of the inelastic process. The numerical procedures are examined with regard to stability and accuracy to assess the overall efficiency. The 'optimal' incremental technique is then contrasted with the computer storage requirements to retain the data for the 'memory-characteristics' of the constitutive model

  14. Application of synchrotron radiation to elemental analysis

    International Nuclear Information System (INIS)

    Jones, K.W.; Gordon, B.M.; Hanson, A.L.; Hastings, J.B.; Howells, M.R.; Kraner, H.W.; Chen, J.R.

    1983-01-01

    The use of a synchrotron storage ring as a high brightness source for production of monoergic, variable energy, and highly polarized x-ray beams promises to revolutionize the field of elemental analysis. The results of exploratory work using the Cornell synchrotron facility, CHESS, will be described. Design considerations and features of the new X-Ray Microprobe Facility now under construction at the Brookhaven National Synchrotron Light Source will be presented. This facility will be used for bulk analysis and for microanalysis with an initial spatial resolution of the order of 30 μm

  15. Network application of PIXE trace element analysis

    International Nuclear Information System (INIS)

    Niizeki, T.; Kawasaki, K.; Hattori, T.

    2003-01-01

    Particle Induced X-ray Emission (PIXE) is a very sensitive analytical technique for determinations of trace elements. But the number of users is limited because there are not so much accelerators which can be used easily. On the other hand, PIXE is a typical machine analysis which can easily analyze automatically and make online data acquisition system. If there is useful online data handling system then PIXE analysis should be more useful for many persons. Therefore we develop to online PIXE facility at Tokyo Institute of Technology VdG laboratory and use it for environmental educations. (author)

  16. Optical selection of trace elements for discriminant analysis

    International Nuclear Information System (INIS)

    Rasmussen, S.E.; Erasmus, C.S.; Watterson, J.I.W.; Sellschop, J.P.F.

    This report describes different methods of element selection; a combination of stepwise multivariate analysis of variance for primary element selection, and principle component analysis regression for the element interrelationship analysis. These offer a satisfactory solution to the problem of element selection

  17. An assessment of surface emissivity variation effects on plasma uniformity analysis using IR cameras

    Science.gov (United States)

    Greenhalgh, Abigail; Showers, Melissa; Biewer, Theodore

    2017-10-01

    The Prototype-Material Plasma Exposure eXperiment (Proto-MPEX) is a linear plasma device operating at Oak Ridge National Laboratory (ORNL). Its purpose is to test plasma source and heating concepts for the planned Material Plasma Exposure eXperiment (MPEX), which has the mission to test the plasma-material interactions under fusion reactor conditions. In this device material targets will be exposed to high heat fluxes (>10 MW/m2). To characterize the heat fluxes to the target a IR thermography system is used taking up to 432 frames per second videos. The data is analyzed to determine the surface temperature on the target in specific regions of interest. The IR analysis has indicated a low level of plasma uniformity; the plasma often deposits more heat to the edge of the plate than the center. An essential parameter for IR temperature calculation is the surface emissivity of the plate (stainless steel). A study has been performed to characterize the variation in the surface emissivity of the plate as its temperature changes and its surface finish is modified by plasma exposure.

  18. Elements of healthy death: a thematic analysis.

    Science.gov (United States)

    Estebsari, Fatemeh; Taghdisi, Mohammad Hossein; Mostafaei, Davood; Rahimi, Zahra

    2017-01-01

    Background: Death is a natural and frightening phenomenon, which is inevitable. Previous studies on death, which presented a negative and tedious image of this process, are now being revised and directed towards acceptable death and good death. One of the proposed terms about death and dying is "healthy death", which encourages dealing with death positively and leading a lively and happy life until the last moment. This study aimed to explain the views of Iranians about the elements of healthy death. Methods: This qualitative study was conducted for 12 months in two general hospitals in Tehran (capital of Iran), using the thematic analysis method. After conducting 23 in-depth interviews with 21 participants, transcription of content, and data immersion and analysis, themes, as the smallest meaningful units were extracted, encoded and classified. Results: One main category of healthy death with 10 subthemes, including dying at the right time, dying without hassle, dying without cost, dying without dependency and control, peaceful death, not having difficulty at dying, not dying alone and dying at home, inspired death, preplanned death, and presence of a clergyman or a priest, were extracted as the elements of healthy death from the perspective of the participants in this study. Conclusion: The study findings well explained the elements of healthy death. Paying attention to the conditions and factors causing healthy death by professionals and providing and facilitating quality services for patients in the end stage of life make it possible for patients to experience a healthy death.

  19. Dissipation element analysis of turbulent scalar fields

    International Nuclear Information System (INIS)

    Wang Lipo; Peters, Norbert

    2008-01-01

    Dissipation element analysis is a new approach for studying turbulent scalar fields. Gradient trajectories starting from each material point in a scalar field Φ'(x-vector,t) in ascending directions will inevitably reach a maximal and a minimal point. The ensemble of material points sharing the same pair ending points is named a dissipation element. Dissipation elements can be parameterized by the length scale l and the scalar difference Δφ ', which are defined as the straight line connecting the two extremal points and the scalar difference at these points, respectively. The decomposition of a turbulent field into dissipation elements is space-filling. This allows us to reconstruct certain statistical quantities of fine scale turbulence which cannot be obtained otherwise. The marginal probability density function (PDF) of the length scale distribution based on a Poisson random cutting-reconnection process shows satisfactory agreement with the direct numerical simulation (DNS) results. In order to obtain the further information that is needed for the modeling of scalar mixing in turbulence, such as the marginal PDF of the length of elements and all conditional moments as well as their scaling exponents, there is a need to model the joint PDF of l and Δφ ' as well. A compensation-defect model is put forward in this work to show the dependence of Δφ ' on l. The agreement between the model prediction and DNS results is satisfactory, which may provide another explanation of the Kolmogorov scaling and help to improve turbulent mixing models. Furthermore, intermittency and cliff structure can also be related to and explained from the joint PDF.

  20. Finite element analysis of ARPS structures

    International Nuclear Information System (INIS)

    Ruhkamp, J.D.; McDougal, J.R.; Kramer, D.P.

    1998-01-01

    Algor finite element software was used to determine the stresses and deflections in the metallic walls of Advanced Radioisotope Power Systems (ARPS) designs. The preliminary design review of these systems often neglects the structural integrity of the design which can effect fabrication and the end use of the design. Before finite element analysis (FEA) was run on the canister walls of the thermophotovoltaic (TPV) generator, hand calculations were used to approximate the stresses and deflections in a flat plate. These results compared favorably to the FEA results of a similar size flat plate. The AMTEC (Alkali Metal Thermal-to-Electric Conversion) cells were analyzed by FEA and the results compared to two cells that were mechanically tested. The mechanically tested cells buckled in the thin sections, one at the top and one in the lower section. The FEA predicted similar stress and shape results but the critical buckling load was found to be very shape dependent

  1. Reliability analysis of dispersion nuclear fuel elements

    Science.gov (United States)

    Ding, Shurong; Jiang, Xin; Huo, Yongzhong; Li, Lin an

    2008-03-01

    Taking a dispersion fuel element as a special particle composite, the representative volume element is chosen to act as the research object. The fuel swelling is simulated through temperature increase. The large strain elastoplastic analysis is carried out for the mechanical behaviors using FEM. The results indicate that the fission swelling is simulated successfully; the thickness increments grow linearly with burnup; with increasing of burnup: (1) the first principal stresses at fuel particles change from tensile ones to compression ones, (2) the maximum Mises stresses at the particles transfer from the centers of fuel particles to the location close to the interfaces between the matrix and the particles, their values increase with burnup; the maximum Mises stresses at the matrix exist in the middle location between the two particles near the mid-plane along the length (or width) direction, and the maximum plastic strains are also at the above region.

  2. Reliability analysis of dispersion nuclear fuel elements

    Energy Technology Data Exchange (ETDEWEB)

    Ding Shurong [Department of Mechanics and Engineering Science, Fudan University, Shanghai 200433 (China)], E-mail: dsr1971@163.com; Jiang Xin [Department of Mechanics and Engineering Science, Fudan University, Shanghai 200433 (China); Huo Yongzhong [Department of Mechanics and Engineering Science, Fudan University, Shanghai 200433 (China)], E-mail: yzhuo@fudan.edu.cn; Li Linan [Department of Mechanics, Tianjin University, Tianjin 300072 (China)

    2008-03-15

    Taking a dispersion fuel element as a special particle composite, the representative volume element is chosen to act as the research object. The fuel swelling is simulated through temperature increase. The large strain elastoplastic analysis is carried out for the mechanical behaviors using FEM. The results indicate that the fission swelling is simulated successfully; the thickness increments grow linearly with burnup; with increasing of burnup: (1) the first principal stresses at fuel particles change from tensile ones to compression ones, (2) the maximum Mises stresses at the particles transfer from the centers of fuel particles to the location close to the interfaces between the matrix and the particles, their values increase with burnup; the maximum Mises stresses at the matrix exist in the middle location between the two particles near the mid-plane along the length (or width) direction, and the maximum plastic strains are also at the above region.

  3. MicrOmega IR: a new infrared hyperspectral imaging microscope or in situ analysis

    Science.gov (United States)

    Vaitua, Leroi; Bibring, Jean-Pierre; Berthé, Michel

    2017-11-01

    MicrOmega IR is an ultra miniaturized Near Infrared hyperspectral microscope for in situ analysis of samples. It is designed to be implemented on board space planetary vehicles (lander and/or rovers). It acquires images of samples typically some 5 mm in width with a spatial sampling of 20 μm. On each pixel, MicrOmega acquires the spectrum in the spectral range 0.9 - 2.6 μm, with a possibility to extend the sensibility up to 4 μm. The spectrum will be measured in up to 300 contiguous spectral channels (600 in the extended range): given the diagnostic spectral features present in this domain, it provides the composition of each spatially resolved constituent. MicrOmega has thus the potential to identify: minerals, such as pyroxene and olivine, ferric oxides, hydrated phases such as phyllosilicates, sulfates and carbonates, ices and organics. The composition of the various phases within a given sample is a critical record of its formation and evolution. Coupled to the mapping information, it provides unique clues to describe the history of the parent body. In particular, the capability to identify hydrated grains and to characterize their adjacent phases has a huge potential in the search for potential bio-relics in Martian samples. This purely non destructive characterization enables further analyses (e.g. through mass spectrometry) to be performed, and/or to contribute to sample selection to return to Earth. MicrOmega IR is coupled to a visible microscope: MicrOmega VIS. Thus, the MicrOmega instrument is developed by an international consortium: IAS (Orsay, France), LESIA (Meudon, France), CBM (Orléans, France), University Of Bern (Bern, Switzerland), IKI (Moscow, Russia). This instrument (MicrOmega IR, MicrOmega VIS and the electronics) is selected for the ESA Exomars mission (launch scheduled for 2013). MicrOmega IR will be used in a reduced spectral range (0.9 - 2.6 μm), due to power, mass and thermal constraints: however, most minerals and other

  4. Failure analysis for WWER-fuel elements

    International Nuclear Information System (INIS)

    Boehmert, J.; Huettig, W.

    1986-10-01

    If the fuel defect rate proves significantly high, failure analysis has to be performed in order to trace down the defect causes, to implement corrective actions, and to take measures of failure prevention. Such analyses are work-consuming and very skill-demanding technical tasks, which require examination methods and devices excellently developed and a rich stock of experience in evaluation of features of damage. For that this work specifies the procedure of failure analyses in detail. Moreover prerequisites and experimental equipment for the investigation of WWER-type fuel elements are described. (author)

  5. Finite element analysis of permanent magnet motors

    International Nuclear Information System (INIS)

    Boglietti, A.; Chiampi, M.; Tartaglia, M.; Chiarabaglio, D.

    1989-01-01

    The analysis of permanent magnet D.C. brushless motors, supplied by current control inverters, is developed employing a finite element package tailored for such devices. The study is devoted to predicting the performance of a set of four poles machines, under different operating conditions (no-load, rated load). The over-load conditions are also considered including the saturation effect. Moreover the influence of such design parameters, as the tooth shape and the number of magnet segments, is investigated. Computed results are found in satisfactory agreement with experimental ones

  6. Near-IR laser-based spectrophotometer for comparative analysis of isotope content of CO2 in exhale air samples

    International Nuclear Information System (INIS)

    Stepanov, E V; Glushko, A N; Kasoev, S G; Koval', A V; Lapshin, D A

    2011-01-01

    We present a laser spectrophotometer aimed at high-accuracy comparative analysis of content of 12 CO 2 and 13 CO 2 isotope modifications in the exhale air samples and based on a tunable near-IR diode laser (2.05 μm). The two-channel optical scheme of the spectrophotometer and the special digital system for its control are described. An algorithm of spectral data processing aimed at determining the difference in the isotope composition of gas mixtures is proposed. A few spectral regions (near 4880 cm -1 ) are determined to be optimal for analysis of relative content of 12 CO 2 and 13 CO 2 in the exhale air. The use of the proposed spectrophotometer scheme and the developed algorithm makes the results of the analysis less susceptible to the influence of the interference in optical elements, to the absorption in the open atmosphere, to the slow drift of the laser pulse envelope, and to the offset of optical channels. The sensitivity of the comparative analysis of the isotope content of CO 2 in exhale air samples, achieved using the proposed scheme, is estimated to be nearly 0.1‰.

  7. Determination of geochemical distribution of platinum elements in chromites and related minerals using neutron activation analysis technique

    International Nuclear Information System (INIS)

    Agiorgitis, G.

    1978-08-01

    Results of Pt, Pd, Ir, Os and Ru determination in various rocks and minerals using radiochemical neutron activation method are presented and geochemical correlations of the platinum elements studied. The method of analysis was described in detail in 4 progress reports

  8. Trace element analysis: a diagnostic tool

    International Nuclear Information System (INIS)

    Qureshi, I.H.; Cheema, M.N.

    1976-09-01

    The human mody continuously assimilates a variety of elements from the environment, and the concentration of these elements in the blood is regulated by means of various homeostatic mechanisms. Some of the elements, though present in very small amounts, have highly specialized functions in initiating many biochemical reactions. These elements, known as essential trace elements, are closely related to human diseases since their deficiency or excess induces physiological changes. Many diseases such as hypertension, atherosclerosis, diabetes, etc., are related to an imbalance in trace element. The measurement of trace elements in body fluids and tissues can, therefore, be effectively employed for diagnostic tests

  9. Siderophile element concentrations in magnetic spherules from deep sea sediments revealed by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Nogami, Ken-ichi; Shimamura, Tadashi; Tazawa, Yuji; Yamakoshi, Kazuo.

    1980-01-01

    For the purpose of deciding the extraterrestrial origin of the magnetic spherules found in deep sea sediments, the siderophile elements Co, Ni, Ir and/or Au etc., were measured by instrumental neutron activation analysis. Spherules were collected from red clay samples which were dredged from Mid Pacific Ocean. Only spherules which had smooth surfaces and relatively high specific gravities were chosen for analysis. Existence of Co, Ni and Ir in most spherules suggests the possibility of an extraterrestrial origin for these spherules. It is not clear whether these spherules are droplets ablated from iron meteorites entering into the Earth's atmosphere or they are cosmic iron grains themselves. X-ray diffraction analysis suggested that these spherules are the products of rapid cooling materials. (author)

  10. Ames S-32 O-16 O-18 Line List for High-Resolution Experimental IR Analysis

    Science.gov (United States)

    Huang, Xinchuan; Schwenke, David W.; Lee, Timothy J.

    2016-01-01

    By comparing to the most recent experimental data and spectra of the SO2 628 ?1/?3 bands (see Ulenikov et al., JQSRT 168 (2016) 29-39), this study illustrates the reliability and accuracy of the Ames-296K SO2 line list, which is accurate enough to facilitate such high-resolution spectroscopic analysis. The SO2 628 IR line list is computed on a recently improved potential energy surface (PES) refinement, denoted Ames-Pre2, and the published purely ab initio CCSD(T)/aug-cc-pVQZ dipole moment surface. Progress has been made in both energy level convergence and rovibrational quantum number assignments agreeing with laboratory analysis models. The accuracy of the computed 628 energy levels and line list is similar to what has been achieved and reported for SO2 626 and 646, i.e. 0.01-0.03 cm(exp -1) for bands up to 5500 cm(exp -1). During the comparison, we found some discrepancies in addition to overall good agreements. The three-IR-list based feature-by-feature analysis in a 0.25 cm(exp -1) spectral window clearly demonstrates the power of the current Ames line lists with new assignments, correction of some errors, and intensity contributions from varied sources including other isotopologues. We are inclined to attribute part of detected discrepancies to an incomplete experimental analysis and missing intensity in the model. With complete line position, intensity, and rovibrational quantum numbers determined at 296 K, spectroscopic analysis is significantly facilitated especially for a spectral range exhibiting such an unusually high density of lines. The computed 628 rovibrational levels and line list are accurate enough to provide alternatives for the missing bands or suspicious assignments, as well as helpful to identify these isotopologues in various celestial environments. The next step will be to revisit the SO2 828 and 646 spectral analyses.

  11. Finite element analysis of multilayer coextrusion.

    Energy Technology Data Exchange (ETDEWEB)

    Hopkins, Matthew Morgan; Schunk, Peter Randall; Baer, Thomas A. (Proctor & Gamble Company, West Chester, OH); Mrozek, Randy A. (Army Research Laboratory, Adelphi, MD); Lenhart, Joseph Ludlow (Army Research Laboratory, Adelphi, MD); Rao, Rekha Ranjana; Collins, Robert (Oak Ridge National Laboratory); Mondy, Lisa Ann

    2011-09-01

    Multilayer coextrusion has become a popular commercial process for producing complex polymeric products from soda bottles to reflective coatings. A numerical model of a multilayer coextrusion process is developed based on a finite element discretization and two different free-surface methods, an arbitrary-Lagrangian-Eulerian (ALE) moving mesh implementation and an Eulerian level set method, to understand the moving boundary problem associated with the polymer-polymer interface. The goal of this work is to have a numerical capability suitable for optimizing and troubleshooting the coextrusion process, circumventing flow instabilities such as ribbing and barring, and reducing variability in layer thickness. Though these instabilities can be both viscous and elastic in nature, for this work a generalized Newtonian description of the fluid is used. Models of varying degrees of complexity are investigated including stability analysis and direct three-dimensional finite element free surface approaches. The results of this work show how critical modeling can be to reduce build test cycles, improve material choices, and guide mold design.

  12. Trace element analysis of common salt using neutron activation analysis

    International Nuclear Information System (INIS)

    Usman, K.

    1993-01-01

    Instrumental Fast Neutron Activation Analysis (IFNAA) technique has been used in the qualitative and quantitative determination of the impurity elements in common salt. Samples of the different types of common salt processed in Nigeria and some of those imported into the country were used. The type A711 KAMAN neutron generator and a high-purity Germanium (HpGe) gamma spectrometer available at the Centre for Energy Research and Training, Ahmadu Bello University, Zaria has been used. The ORTEC ADCAM 100 Emulation Software (Maestro) was used in the qualitative measurement of the detected elements. The G.R.G Activation Analysis System by G. R. Gilmore, 1987, was used in the quantitative determination of the elements detected by relative method. Aluminium and arsenic were detected and measured

  13. Analysis and Design of Rolling Stock Elements

    Directory of Open Access Journals (Sweden)

    M. V. Chugunov

    2014-01-01

    Full Text Available The work solves the problem of equal-strength design of the rolling stock elements in option of discrete equal-strength. For this purpose, has been developed the software built in SolidWorks and SolidWorks Simulation as an AddIn-application using necessary basic functionality and extending it in the specified part on the basis of API SolidWorks and COM technology.The SolidWorks software is used to develop a 3D-model for general force frame of the wagon as an assembly. As this assembly is quite complicated and includes many elements both standard, and non-standard type, 3D - specification is developed by 3Dvia Composer software, which is included in the article in the form of the gif-animation and via-roller. This means is very useful for the evident analysis of topology and geometrical properties of a design as a whole, facilitates a procedure of adequate formation of the FE model providing accuracy and profitability of computing. From the point of view of profitability and opportunities of definition of concentrators of stresses with a sufficient accuracy for practice the combined model including volume and shell FEM is optimum.In the work the analysis results of stress-strain state of a design are given in two options of static loading in the form of stress diagrams, the main areas of stress concentration are revealed.Results of equal-strength design in the form of thickness distribution on thin-walled elements of a design, considered within FEM as shells, are received. It is shown that the developed software doesn't allow optimum design results, however it is economically viable, simple in use and can be applied to the solution of problems of rational design in design practice.SolidWorks, as well as the majority of similar CADs, possess an open architecture and allow users to apply its functionality. This work continues a series of publications of the author of this paper and other authors concerning the API-based CAD/CAE adaptation and

  14. Nonlinear finite element analysis of concrete structures

    International Nuclear Information System (INIS)

    Ottosen, N.S.

    1980-05-01

    This report deals with nonlinear finite element analysis of concrete structures loaded in the short-term up until failure. A profound discussion of constitutive modelling on concrete is performed; a model, applicable for general stress states, is described and its predictions are compared with experimental data. This model is implemented in the AXIPLANE-program applicable for axisymmetrick and plane structures. The theoretical basis for this program is given. Using the AXIPLANE-program various concrete structures are analysed up until failure and compared with experimental evidence. These analyses include panels pressure vessel, beams failing in shear and finally a specific pull-out test, the Lok-Test, is considered. In these analyses, the influence of different failure criteria, aggregate interlock, dowel action, secondary cracking, magnitude of compressive strenght, magnitude of tensile strenght and of different post-failure behaviours of the concrete are evaluated. Moreover, it is shown that a suitable analysis of the theoretical data results in a clear insight into the physical behaviour of the considered structures. Finally, it is demonstrated that the AXISPLANE-program for widely different structures exhibiting very delicate structural aspects gives predictions that are in close agreement with experimental evidence. (author)

  15. Prediction and phylogenetic analysis of mammalian short interspersed elements (SINEs).

    Science.gov (United States)

    Rogozin, I B; Mayorov, V I; Lavrentieva, M V; Milanesi, L; Adkison, L R

    2000-09-01

    The presence of repetitive elements can create serious problems for sequence analysis, especially in the case of homology searches in nucleotide sequence databases. Repetitive elements should be treated carefully by using special programs and databases. In this paper, various aspects of SINE (short interspersed repetitive element) identification, analysis and evolution are discussed.

  16. FT-IR microscopical analysis with synchrotron radiation: The microscope optics and system performance

    International Nuclear Information System (INIS)

    Reffner, J.A.; Martoglio, P.A.; Williams, G.P.

    1995-01-01

    When a Fourier transform infrared (FT-IR) microspectrometer was first interfaced with the National Synchrotron Light Source (NSLS) in September 1993, there was an instant realization that the performance at the diffraction limit had increased 40-100 times. The synchrotron source transformed the IR microspectrometer into a true IR microprobe, providing high-quality IR spectra for probe diameters at the diffraction limit. The combination of IR microspectroscopy and synchrotron radiation provides a powerful new tool for molecular spectroscopy. The ability to perform IR microspectroscopy with synchrotron radiation is still under development at Brookhaven National Laboratory, but several initial studies have been completed that demonstrate the broad-ranging applications of this technology and its potential for materials characterization

  17. FT-IR microscopical analysis with synchrotron radiation: The microscope optics and system performance

    Energy Technology Data Exchange (ETDEWEB)

    Reffner, J.A.; Martoglio, P.A. [Spectra-Tech, Inc., Shelton, CT (United States); Williams, G.P. [Brookhaven National Lab., Upton, NY (United States)

    1995-01-01

    When a Fourier transform infrared (FT-IR) microspectrometer was first interfaced with the National Synchrotron Light Source (NSLS) in September 1993, there was an instant realization that the performance at the diffraction limit had increased 40-100 times. The synchrotron source transformed the IR microspectrometer into a true IR microprobe, providing high-quality IR spectra for probe diameters at the diffraction limit. The combination of IR microspectroscopy and synchrotron radiation provides a powerful new tool for molecular spectroscopy. The ability to perform IR microspectroscopy with synchrotron radiation is still under development at Brookhaven National Laboratory, but several initial studies have been completed that demonstrate the broad-ranging applications of this technology and its potential for materials characterization.

  18. Quantitative analysis of semivolatile organic compounds in selected fractions of air sample extracts by GC/MI-IR spectrometry

    International Nuclear Information System (INIS)

    Childers, J.W.; Wilson, N.K.; Barbour, R.K.

    1990-01-01

    The authors are currently investigating the capabilities of gas chromatography/matrix isolation infrared (GC/MI-IR) spectrometry for the determination of semivolatile organic compounds (SVOCs) in environmental air sample extracts. Their efforts are focused on the determination of SVOCs such as alkylbenzene positional isomers, which are difficult to separate chromatographically and to distinguish by conventional electron-impact ionization GC/mass spectrometry. They have performed a series of systematic experiments to identify sources of error in quantitative GC/MI-IR analyses. These experiments were designed to distinguish between errors due to instrument design or performance and errors that arise from some characteristic inherent to the GC/MI-IR technique, such as matrix effects. They have investigated repeatability as a function of several aspects of GC/MI IR spectrometry, including sample injection, spectral acquisition, cryogenic disk movement, and matrix deposition. The precision, linearity, dynamic range, and detection limits of a commercial GC/MI-IR system for target SVOCs were determined and compared to those obtained with the system's flame ionization detector. The use of deuterated internal standards in the quantitative GC/MI-IR analysis of selected fractions of ambient air sample extracts will be demonstrated. They will also discuss the current limitations of the technique in quantitative analyses and suggest improvements for future consideration

  19. Structural and physical properties of new uranium and transition element ternary stannides (Fe, Co, Ni, Ru, Rh, Pd, Ir, Pt); Proprietes structurales et physiques de nouveaux stannures ternaires a base d'uranium et d'element de transition (Fe, Co, Ni, Rh, Pd, Ir, Pt)

    Energy Technology Data Exchange (ETDEWEB)

    Mirambet, F

    1993-12-15

    This work is dedicated to the study of ternary stannides based on uranium. The author reviews the structural, magnetic and electric properties of different families of stannides. The study of the U{sub 2}M{sub 2}Sn family where M stands for Fe, Co, Ni, Ru, Rh, Pd, Ir and Pt shows that the magnetic behaviour of uranium in these compounds is strongly influenced by the transition element M, which is explained by the hybridization force 5f(U) - nd(M) that depends on the number of electrons on the d shell of the M element. For instance, for the elements whose d shell is low filled (Fe, Ru), the U{sub 2}M{sub 2}Sn stannides show no magnetic order. On the other hand, when the number of d-electrons increases, a magnetic order appears progressively.

  20. Finite element analysis of plastic recycling machine designed for ...

    African Journals Online (AJOL)

    ... design was evaluated using finite element analysis (FEA) tool in Solid Works Computer ... Also, a minimum factor of safety value of 5.3 was obtained for shredder shaft ... Machine; Design; Recycling; Sustainability; Finite Element; Simulation ...

  1. Stability analysis of artificial synthetic overweight elements

    International Nuclear Information System (INIS)

    Zhou Jian

    1990-01-01

    Stability of artificial synthetic overweight elements has been analysed theoretically using a diagram of nuclear stability. It is indicated that overweight nucleus can be synthesized only when a certain amount of neutrons participate simultaneously in the synthesis. The maximum number of protons in overweight elements is 1002. The proton number of 'extreme overweight' elements of which the neutron star is possibly composed is in the range from 326 to 1002. It is expected that the mass number of the stable overweight elements with proton number 114 is in the range from 299 to 315

  2. Molecular structure, vibrational analysis (IR and Raman) and quantum chemical investigations of 1-aminoisoquinoline

    Science.gov (United States)

    Sivaprakash, S.; Prakash, S.; Mohan, S.; Jose, Sujin P.

    2017-12-01

    Quantum chemical calculations of energy and geometrical parameters of 1-aminoisoquinoline [1-AIQ] were carried out by using DFT/B3LYP method using 6-311G (d,p), 6-311G++(d,p) and cc-pVTZ basis sets. The vibrational wavenumbers were computed for the energetically most stable, optimized geometry. The vibrational assignments were performed on the basis of potential energy distribution (PED) using VEDA program. The NBO analysis was done to investigate the intra molecular charge transfer of the molecule. The frontier molecular orbital (FMO) analysis was carried out and the chemical reactivity descriptors of the molecule were studied. The Mulliken charge analysis, molecular electrostatic potential (MEP), HOMO-LUMO energy gap and the related properties were also investigated at B3LYP level. The absorption spectrum of the molecule was studied from UV-Visible analysis by using time-dependent density functional theory (TD-DFT). Fourier Transform Infrared spectrum (FT-IR) and Raman spectrum of 1-AIQ compound were analyzed and recorded in the range 4000-400 cm-1 and 3500-100 cm-1 respectively. The experimentally determined wavenumbers were compared with those calculated theoretically and they complement each other.

  3. Chromatographic Techniques for Rare Earth Elements Analysis

    Science.gov (United States)

    Chen, Beibei; He, Man; Zhang, Huashan; Jiang, Zucheng; Hu, Bin

    2017-04-01

    The present capability of rare earth element (REE) analysis has been achieved by the development of two instrumental techniques. The efficiency of spectroscopic methods was extraordinarily improved for the detection and determination of REE traces in various materials. On the other hand, the determination of REEs very often depends on the preconcentration and separation of REEs, and chromatographic techniques are very powerful tools for the separation of REEs. By coupling with sensitive detectors, many ambitious analytical tasks can be fulfilled. Liquid chromatography is the most widely used technique. Different combinations of stationary phases and mobile phases could be used in ion exchange chromatography, ion chromatography, ion-pair reverse-phase chromatography and some other techniques. The application of gas chromatography is limited because only volatile compounds of REEs can be separated. Thin-layer and paper chromatography are techniques that cannot be directly coupled with suitable detectors, which limit their applications. For special demands, separations can be performed by capillary electrophoresis, which has very high separation efficiency.

  4. Trace element analysis of soy sauce

    International Nuclear Information System (INIS)

    Tomita, Michio; Haruyama, Yoichi; Saito, Manabu

    1994-01-01

    Trace elements in soy sauce have been measured by means of in-air PIXE. Six kinds of trace elements were detected, such as Mu, Fe, Ni, Zn, Cu and Br. Concentrations of Mn, Fe, Zn and Br which were observed in all samples, have been determined. Each analyzed sample contained considerable amount of bromine about 160 ppm. (author)

  5. Advances in analysis of pre-earthquake thermal anomalies by analyzing IR satellite data

    Science.gov (United States)

    Ouzounov, D.; Bryant, N.; Filizzola, C.; Pergola, N.; Taylor, P.; Tramutoli, V.

    Presented work addresses the possible relationship between tectonic stress, electro-chemical and thermodynamic processes in the atmosphere and increasing infrared (IR) flux as part of a larger family of electromagnetic (EM) phenomena related to earthquake activity. Thermal infra-red (TIR) surveys performed by polar orbiting (NOAA/AVHRR, MODIS) and geosynchronous weather satellites (GOES, METEOSAT) seems to indicate the appearance (from days to weeks before the event) of "anomalous" space-time TIR transients associated with the place (epicentral area, linear structures and fault systems) and the time of occurrence of a number of major earthquakes with M>5 and focal depths no deeper than 50km. As Earth emitted in 8-14 microns range the TIR signal measured from satellite strongly vary depending on meteorological conditions and other factors (space-time changes in atmospheric transmittance, time/season, solar and satellite zenithal angles and etc) independent from seismic activity, a preliminary definition of "anomalous TIR signal" should be given. To provide reliable discrimination of thermal anomalous area from the natural events (seasonal changes, local morphology) new robust approach (RAT) has been recently proposed (and successfully applied in the field of the monitoring of the major environmental risks) that permits to give a statistically based definition of thermal info-red (TIR) anomaly and reduce of false events detection. New techniques also were specifically developed to assure the precise co-registration of all satellite scenes and permit accurate time-series analysis of satellite observations. As final results we present examples of most recent 2000/2004 worldwide strong earthquakes and the techniques used to capture the tracks of thermal emission mid-IR anomalies and methodology for practical future use of such phenomena in the early warning systems.

  6. Wide-band IR imaging in the NIR-MIR-FIR regions for in situ analysis of frescoes

    Science.gov (United States)

    Daffara, C.; Pezzati, L.; Ambrosini, D.; Paoletti, D.; Di Biase, R.; Mariotti, P. I.; Frosinini, C.

    2011-06-01

    Imaging methods offer several advantages in the field of conservation allowing to perform non-invasive inspection of works of art. In particular, non-invasive techniques based on imaging in different infrared (IR) regions are widely used for the investigation of paintings. Using radiation beyond the visible range, different characteristics of the inspected artwork may be revealed according to the bandwidth acquired. In this paper we present the recent results of a joint project among the two research institutes DIMEG and CNR-INO, and the restoration facility Opificio delle Pietre Dure, concerning the wide-band integration of IR imaging techniques, in the spectral ranges NIR 0.8-2.5 μm, MIR 3-5 μm, and FIR 8-12 μm, for in situ analysis of artworks. A joint, multi-mode use of reflection and thermal bands is proposed for the diagnostics of mural paintings, and it is demonstrated to be an effective tool in inspecting the layered structure. High resolution IR reflectography and, to a greater extent, IR imaging in the 3-5 μm band, are effectively used to characterize the superficial layer of the fresco and to analyze the stratigraphy of different pictorial layers. IR thermography in the 8-12 μm band is used to characterize the support deep structure. The integration of all the data provides a multi- layered and multi-spectral representation of the fresco that yields a comprehensive analysis.

  7. Trace element analysis in soy sauce. 2

    International Nuclear Information System (INIS)

    Haruyama, Yoichi; Saito, Manabu; Tomita, Michio; Yoshida, Koji.

    1994-01-01

    Trace elements in four kinds of soybean and three kinds of salt have been measured by means of in-air PIXE. In soybeans, which were made in Japan, America, Canada and China, six kinds of trace elements were detected, such as Mn, Fe, Ni, Cu, Zn and Br. The concentration of these elements varied depending on the place they were made. American soybean showed characteristic feature compared with other soybeans. As to the bromine concentration, American soybean contains ten times as much as Japanese one. In salts Br and Sr were detected. (author)

  8. Elemental content in cigarette components and its distribution as determined by neutron activation analysis

    International Nuclear Information System (INIS)

    Metwally, Y.E.

    2003-01-01

    Cigarette smoking, a world-wide habit. Has a very bad and hazardous effects on the human body. In the present study, different kinds of cigarette brands have been collected from local and foreign markets representing ten countries all over the world. All the selected samples were irradiated in first Inshas reactor (IR-1) in Egypt. A comprehensive study of the elemental contents in cigarette samples under investigation has been carried out by using neutron activation analysis technique. Concentrations of the polluting elements and tracer contents of cigarette tobacco have been determined. The elemental distribution of the component (tobacco. ash. filter before and after smoking and wrapping paper) of some kinds of cigarettes has been studied. The obtained data resulting from the present work were discussed

  9. Elemental Analysis and Biological Activities of Chrysophyllum ...

    African Journals Online (AJOL)

    Sapotaceae) Leaves. ... The plant material could be used as a source of important elements required for the body. In suitable form, the plant could be used in the prevention and treatment of dental caries, oxidative damage, obesity and cancer.

  10. The fire assay preconcentration of the platinum group elements for the neutron activation analysis of geological material

    International Nuclear Information System (INIS)

    Parry, S.J.

    1994-01-01

    This paper describes the work that has been carried out using neutron activation analysis (NAA) to develop a rapid and reliable method for the determination of the platinum group elements (PGE: Pt, Pd, Ir, Ru, Rh, and Os) and Au in geological, environmental and industrial samples. The method is based on the now established method of preconcentration with fire assay, followed by NAA of the separated PGE and Au. Recent developments have seen improvements in the technique to eliminate losses due to dissolution procedures, and complete recovery of the elements prior to analysis. The method is now being used to validate inductively coupled plasma-mass spectroscopy methods for analysis of the PGE

  11. Instrumental trace element analysis of California market milk

    International Nuclear Information System (INIS)

    Ragaini, R.C.; Langhorst, A.L.; Ralston, H.R.; Heft, R.

    1975-01-01

    Trace element analysis for 15 elements (Zn, Na, Br, Rb, Sr, Mg, Al, Ca, Cl, I, K, Fe, Co, Se, Cs) was carried out on 32 samples of California market milk and 6 samples of Colorado milk in a pilot study of toxic and nutrient trace elements in the soil-forage-cow-milk food chain. The techniques of instrumental neutron activation analysis and x-ray fluorescence analysis are described. Sample collection, preparation, analysis, and data reduction procedures are discussed. The mean values and variations of trace element concentrations in milk are compared to data from other studies. (U.S.)

  12. Finite element analysis theory and application with ANSYS

    CERN Document Server

    Moaveni, Saeed

    2015-01-01

    For courses in Finite Element Analysis, offered in departments of Mechanical or Civil and Environmental Engineering. While many good textbooks cover the theory of finite element modeling, Finite Element Analysis: Theory and Application with ANSYS is the only text available that incorporates ANSYS as an integral part of its content. Moaveni presents the theory of finite element analysis, explores its application as a design/modeling tool, and explains in detail how to use ANSYS intelligently and effectively. Teaching and Learning Experience This program will provide a better teaching and learning experience-for you and your students. It will help: *Present the Theory of Finite Element Analysis: The presentation of theoretical aspects of finite element analysis is carefully designed not to overwhelm students. *Explain How to Use ANSYS Effectively: ANSYS is incorporated as an integral part of the content throughout the book. *Explore How to Use FEA as a Design/Modeling Tool: Open-ended design problems help stude...

  13. Minerals from Macedonia. XII. The dependence of quartz and opal color on trace element composition - AAS, FT IR and micro-Raman spectroscopy study

    International Nuclear Information System (INIS)

    Makreski, Petre; Jovanovski, Gligor; Stafilov, Trajce; Boev, Blazho

    2004-01-01

    The dependence of the color of quartz and opal natural minerals, collected from different localities in the Republic of Macedonia (Alinci, Belutche, Budinarci, Mariovo, Sasa, Sazhdevo, Chanishte, Cheshinovo, Zletovo) on their element composition is studied using Fourier transform infrared spectroscopy (FT IR), micro-Raman spectroscopy and atomic absorption spectrometry (AAS). In order to determine the content of different trace elements (Al, Cd, Ca, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb and Zn), 15 quartz and 2 opal mineral samples, using flame atomic absorption spectrometry (FAAS) and Zeeman electrothermal atomic absorption spectrometry (ETAAS) are studied. To avoid matrix interferences, the method for elimination of silicium is proposed. Optimal instrumental parameters for ETAAS determination (temperature and time for drying, pyrolysis and atomizing) are established by extensive testing for each investigated element. It is found that the milky white color of quartz minerals is due to the presence of traces of Ca, the appearance of black color is the result of the existence of Pb, Mn and Al impurities, and the occurrence of Fe and Cr introduce appearance of red and green color, respectively. Preliminary identification of the minerals is based on the comparison of our results, obtained by using the infrared and Raman vibrational spectroscopy, with the corresponding literature data for the analogous mineral species originating all over the world. An overview of the basic morphological and physico-chemical characteristics of the quartz and opal minerals and the geology of the localities is given. The colored pictures of the studied quartz and opal minerals are presented as well. (Author)

  14. NMR and IR Spectroscopy for the Structural Characterization of Edible Fats and Oils: An Instrumental Analysis Laboratory

    Science.gov (United States)

    Crowther, Molly W.

    2008-01-01

    This article describes an upper-level instrumental laboratory for undergraduates that explores the complementary nature of IR and NMR spectroscopy for analysis of several edible fats and oils that are structurally similar but differ in physical properties and health implications. Five different fats and oils are analyzed for average chain length,…

  15. Trace elements in termites by PIXE analysis

    Energy Technology Data Exchange (ETDEWEB)

    Yoshimura, T. E-mail: tsuyoshi@termite.kuwri.kyoto-u.ac.jp; Kagemori, N.; Kawai, S.; Sera, K.; Futatsugawa, S

    2002-04-01

    Trace elements in a Japanese subterranean xylophagous termite, Coptotermes formosanus Shiraki, were analyzed by the PIXE method. The total amount of the 14 predominant elements out of 27 detected in an intact termite was higher in a soldier termite (23 000 {mu}g/g) than in a worker termite (10 000 {mu}g/g). A block of wood (Pinus densiflora Sieb. et Zucc.) for termite feed had a much lower concentration (3600 {mu}g/g) compared with that in an intact termite. This probably relates the functional bio-condensation and/or bio-recycling of trace elements in C. formosanus. When a termite was separated into three anatomical parts, head, degutted body and gut, the worker gut contained the highest total amount of the 14 predominant measured elements (31 000 {mu}g/g). This might be correlated with the higher activity of food digestion and energy production in the worker gut. Moreover, the mandible of the soldier head, with an exoskeleton that is intensely hardened, showed a preferential distribution of Mn and Fe. These results suggest that the characteristic localization of elements will be closely related to the functional role of the individual anatomical part of C. formosanus.

  16. Elemental PIXE analysis of oolong tea

    International Nuclear Information System (INIS)

    Watanabe, M.; Ishii, K.; Matsuyama, S.

    2008-01-01

    The contamination of heavy metals in food becomes a serious problem. We analyzed oolong tea from different production areas by PIXE using very simple sample preparation and examined trace elements contained in these samples. From the results of this experiment, we could know oolong tea which analyzed in this experiment contains various minerals such as K, Ca, P, S, Cl, Fe, Mn, Cu and Cr but not toxic element of As which detection limit of PIXE was lower than the standard values given by the food hygiene law in Japan. (author)

  17. Trace element analysis in soy sauce

    International Nuclear Information System (INIS)

    Haruyama, Yoichi; Saito, Manabu; Tomiya, Michio

    1993-01-01

    Trace elements in soy sauce have been measured by means of in-air PIXE. Six kinds of trace elements were detected, such as Mn, Fe, Ni, Zn, Cu and Br. Concentrations of Mn, Fe, Zn and Br which were observed in all samples, have been determined. Each analyzed sample contained considerable amount of Br about 160 ppm. Comparison of Br content of the imported raw materials with those of the domestic ones suggested that the large amount of Br was the residual fumigation chemicals in the imported raw materials. (author)

  18. Thermodynamic analysis of light-actinide elements

    International Nuclear Information System (INIS)

    Brosh, Eli; Makov, Guy; Shneck, Roni Z.

    2005-01-01

    The thermophysical properties of the alpha phases of the light actinide elements Th, U, Np and Pu were analysed. For each of the analysed elements, the Gibbs free-energy was modelled by an explicit function of temperature T and pressure P over the whole relevant T-P range, in a manner compatible with the CALPHAD (Calculation of Alloy Phase Diagrams) method. Several adjustable model-parameters were fitted to available experimental results. The model is based on a new semi-empirical equation of state, which interpolates with Thomas-Fermi type models for the volume and with the Dulong-Petit value for the heat capacity, at extreme pressures

  19. Finite-element analysis of dynamic fracture

    Science.gov (United States)

    Aberson, J. A.; Anderson, J. M.; King, W. W.

    1976-01-01

    Applications of the finite element method to the two dimensional elastodynamics of cracked structures are presented. Stress intensity factors are computed for two problems involving stationary cracks. The first serves as a vehicle for discussing lumped-mass and consistent-mass characterizations of inertia. In the second problem, the behavior of a photoelastic dynamic tear test specimen is determined for the time prior to crack propagation. Some results of a finite element simulation of rapid crack propagation in an infinite body are discussed.

  20. Sugar and acid content of Citrus prediction modeling using FT-IR fingerprinting in combination with multivariate statistical analysis.

    Science.gov (United States)

    Song, Seung Yeob; Lee, Young Koung; Kim, In-Jung

    2016-01-01

    A high-throughput screening system for Citrus lines were established with higher sugar and acid contents using Fourier transform infrared (FT-IR) spectroscopy in combination with multivariate analysis. FT-IR spectra confirmed typical spectral differences between the frequency regions of 950-1100 cm(-1), 1300-1500 cm(-1), and 1500-1700 cm(-1). Principal component analysis (PCA) and subsequent partial least square-discriminant analysis (PLS-DA) were able to discriminate five Citrus lines into three separate clusters corresponding to their taxonomic relationships. The quantitative predictive modeling of sugar and acid contents from Citrus fruits was established using partial least square regression algorithms from FT-IR spectra. The regression coefficients (R(2)) between predicted values and estimated sugar and acid content values were 0.99. These results demonstrate that by using FT-IR spectra and applying quantitative prediction modeling to Citrus sugar and acid contents, excellent Citrus lines can be early detected with greater accuracy. Copyright © 2015 Elsevier Ltd. All rights reserved.

  1. Elemental analysis of samples of rare earths

    International Nuclear Information System (INIS)

    Lopez M, J.; Ramirez T, J.J.; Sandoval J, R.A.; Aspiazu F, J.; Villasenor S, P.; Lugo L, M.F.

    2003-01-01

    Applying the PIXE technique (Particle Induced X-Ray Emission) it was analyzed the purity of the samples that will be used to measure the production section of X rays with Li and B beams. It is not necessary to determine the concentrations of the pollutant elements. (Author)

  2. Elemental analysis of atmospheric aerosols in Gaborone

    African Journals Online (AJOL)

    ELO

    amount more than 90% were copper, lead, nickel and gold. Key words: Atmospheric particles, elements, ... Selebi-Phikwe area, gold and nickel in Francis town and soda ash in Sowa. Gaborone is the capital of ... a stub three times a week with an exposure time of four hours. The exposed stubs were collected and kept ...

  3. Analysis on the Three Elements in Communication

    Institute of Scientific and Technical Information of China (English)

    李霞

    2014-01-01

    In public communication,people may have no troubles to epress themselves grammatically correctly,but sometimes the sentences just sound not pragmatically proper. Through analyzing and comprehending those Elements in English to avoid the misunderstanding and misusing in the communication is significant.

  4. Analysis on 9 Elements in English Pragmatics

    Institute of Scientific and Technical Information of China (English)

    李霞

    2014-01-01

    College Students may have no troubles to compose grammatically correct sentences to express themselves,but sometimes the sentences just seem not pragmatically proper.Through analyzing and comprehending the 9 Elements in English Pragmatics to avoid the misunderstanding and misusing in the communication is significant for English learners,special to one who intends to use English as a communicating medium.

  5. Analysis on the Three Elements in Communication

    Institute of Scientific and Technical Information of China (English)

    李霞

    2014-01-01

    In public communication,people may have no troubles to epress themselves grammatically correctly,but sometimes the sentences just sound not pragmatically proper.Through analyzing and comprehending those Elements in English to avoid the misunderstanding and misusing in the communication is significant.

  6. Finite Element Analysis of Pipe T-Joint

    OpenAIRE

    P.M.Gedkar; Dr. D.V. Bhope

    2012-01-01

    This paper reports stress analysis of two pressurized cylindrical intersection using finite element method. The different combinations of dimensions of run pipe and the branch pipe are used to investigate thestresses in pipe at the intersection. In this study the stress analysis is accomplished by finite element package ANSYS.

  7. VIRTUAL EXPERIMENTAL ANALYSIS ON CLEANING ELEMENT OF SUGARCANE HARVESTER

    Institute of Scientific and Technical Information of China (English)

    Ma Fanglan; Li Shangping; He Yulin; Meng Yanmei; Chen Weixu

    2005-01-01

    The laws of influence of different factors have been analyzed in order to enhance the working efficiency and fatigue life of the cleaning element in brush shape of the sugarcane harvester.Based on the principle of orthogonal experiment design, the virtual-orthogonal-experimental analysis for the cleaning element is carried out on the finite element analysis (FEA) software-ANSYS after analyzing the nonlinear structural behavior in the working procedure. The results are analyzed with the overall balancing method, and then the optimal combination is got, which is made up of different levels of different factors. Also the optimal combination of design parameters of the cleaning element received from the virtual experimental analysis is conducted an experiment to confirm that the virtual analysis model and results are right, and the effect of factors on the function of the cleaning element is obtained by more analysis and further optimizing.

  8. Finite element reliability analysis of fatigue life

    International Nuclear Information System (INIS)

    Harkness, H.H.; Belytschko, T.; Liu, W.K.

    1992-01-01

    Fatigue reliability is addressed by the first-order reliability method combined with a finite element method. Two-dimensional finite element models of components with cracks in mode I are considered with crack growth treated by the Paris law. Probability density functions of the variables affecting fatigue are proposed to reflect a setting where nondestructive evaluation is used, and the Rosenblatt transformation is employed to treat non-Gaussian random variables. Comparisons of the first-order reliability results and Monte Carlo simulations suggest that the accuracy of the first-order reliability method is quite good in this setting. Results show that the upper portion of the initial crack length probability density function is crucial to reliability, which suggests that if nondestructive evaluation is used, the probability of detection curve plays a key role in reliability. (orig.)

  9. Finite element analysis of human joints

    Energy Technology Data Exchange (ETDEWEB)

    Bossart, P.L.; Hollerbach, K.

    1996-09-01

    Our work focuses on the development of finite element models (FEMs) that describe the biomechanics of human joints. Finite element modeling is becoming a standard tool in industrial applications. In highly complex problems such as those found in biomechanics research, however, the full potential of FEMs is just beginning to be explored, due to the absence of precise, high resolution medical data and the difficulties encountered in converting these enormous datasets into a form that is usable in FEMs. With increasing computing speed and memory available, it is now feasible to address these challenges. We address the first by acquiring data with a high resolution C-ray CT scanner and the latter by developing semi-automated method for generating the volumetric meshes used in the FEM. Issues related to tomographic reconstruction, volume segmentation, the use of extracted surfaces to generate volumetric hexahedral meshes, and applications of the FEM are described.

  10. Finite element analysis of human joints

    International Nuclear Information System (INIS)

    Bossart, P.L.; Hollerbach, K.

    1996-09-01

    Our work focuses on the development of finite element models (FEMs) that describe the biomechanics of human joints. Finite element modeling is becoming a standard tool in industrial applications. In highly complex problems such as those found in biomechanics research, however, the full potential of FEMs is just beginning to be explored, due to the absence of precise, high resolution medical data and the difficulties encountered in converting these enormous datasets into a form that is usable in FEMs. With increasing computing speed and memory available, it is now feasible to address these challenges. We address the first by acquiring data with a high resolution C-ray CT scanner and the latter by developing semi-automated method for generating the volumetric meshes used in the FEM. Issues related to tomographic reconstruction, volume segmentation, the use of extracted surfaces to generate volumetric hexahedral meshes, and applications of the FEM are described

  11. Sensitivity Range Analysis of Infrared (IR) Transmitter and Receiver Sensor to Detect Sample Position in Automatic Sample Changer

    International Nuclear Information System (INIS)

    Syirrazie Che Soh; Nolida Yussup; Nur Aira Abdul Rahman; Maslina Ibrahim

    2016-01-01

    Sensitivity range of IR Transmitter and Receiver Sensor influences the effectiveness of the sensor to detect position of a sample. Then the purpose of this analysis is to determine the suitable design and specification the electronic driver of the sensor to gain appropriate sensitivity range for required operation. The related activities to this analysis cover electronic design concept and specification, calibration of design specification and evaluation on design specification for required application. (author)

  12. Elemental analysis: Reduction to SI units; Rueckfuehrung in der Elementanalytik

    Energy Technology Data Exchange (ETDEWEB)

    Rienitz, O.; Jaehrling, R.; Schiel, D. [PTB-Arbeitsgruppe ' ' Anorganische Analytik' ' , Braunschweig (Germany); Matschat, R.; Kipphardt, H. [Bundesanstalt fuer Materialforschung und -pruefung, Berlin (Germany); Gernand, W.; Oeter, D. [MercK KGaA (Germany)

    2005-12-15

    In a joint project, PTB, BAM and Merck KGaA worked on a metrological reduction system for all elements relevant to analysis. The BAM certified primary pure substances with a relative error of U{sub rel} {<=} 0.01% for the mass of the main element. This was achieved by measuring the mass components of all potential impurities, i.e. practically all elements of the periodic system except the main element. These pure substances are the national reference standards of elemental analysis. From them, PTB produces primary elementa solutions and transfer solutions which are passed on as reference standards. The industrial partner constructed the DKD calibration laboratory, which certifies commercial secondary calibration solutions on the basis of the reference standard solutions produced by PTB. With this final product, measurements in elemental analysis can be reduced to the SI units system as a routine procedure. (orig.)

  13. A Dual Super-Element Domain Decomposition Approach for Parallel Nonlinear Finite Element Analysis

    Science.gov (United States)

    Jokhio, G. A.; Izzuddin, B. A.

    2015-05-01

    This article presents a new domain decomposition method for nonlinear finite element analysis introducing the concept of dual partition super-elements. The method extends ideas from the displacement frame method and is ideally suited for parallel nonlinear static/dynamic analysis of structural systems. In the new method, domain decomposition is realized by replacing one or more subdomains in a "parent system," each with a placeholder super-element, where the subdomains are processed separately as "child partitions," each wrapped by a dual super-element along the partition boundary. The analysis of the overall system, including the satisfaction of equilibrium and compatibility at all partition boundaries, is realized through direct communication between all pairs of placeholder and dual super-elements. The proposed method has particular advantages for matrix solution methods based on the frontal scheme, and can be readily implemented for existing finite element analysis programs to achieve parallelization on distributed memory systems with minimal intervention, thus overcoming memory bottlenecks typically faced in the analysis of large-scale problems. Several examples are presented in this article which demonstrate the computational benefits of the proposed parallel domain decomposition approach and its applicability to the nonlinear structural analysis of realistic structural systems.

  14. Elemental hair analysis: A review of procedures and applications

    International Nuclear Information System (INIS)

    Pozebon, D.; Scheffler, G.L.; Dressler, V.L.

    2017-01-01

    Although exogenous contamination and unreliable reference values have limited the utility of scalp hair as a biomarker of chemical elements exposure, its use in toxicological, clinical, environmental and forensic investigations is growing and becoming more extensive. Therefore, hair elemental analysis is reviewed in the current manuscript which spans articles published in the last 10 years. It starts with a general discussion of history, morphology and possible techniques for elemental analysis, where inductively coupled plasma-mass spectrometry (ICP-MS) is clearly highlighted since this technique is leading quantitative ultra-trace elemental analysis. Emphasis over sampling, quality assurance, washing procedures and sample decomposition is given with detailed protocols compiled in tables as well as the utility of hair to identify human gender, age, diseases, healthy conditions, nutrition status and contamination sites. Isotope ratio information, chemical speciation analysis and analyte preconcentration are also considered for hair. Finally, the potential of laser ablation ICP-MS (LA-ICP-MS) to provide spatial resolution and time-track the monitoring of elements in hair strands instead of conventional bulk analysis is spotlighted as a real future trend in the field. - Highlights: • Elemental analysis of hair is critically reviewed, with focus on ICP-MS employment. • Standards protocols of hair washing and sample decomposition are compiled. • The usefulness of elemental and/or isotopic analysis of hair is demonstrated. • The potential of LA-ICP-MS for elemental time tracking in hair is highlighted.

  15. Insulating phase in Sr{sub 2}IrO{sub 4}: An investigation using critical analysis and magnetocaloric effect

    Energy Technology Data Exchange (ETDEWEB)

    Bhatti, Imtiaz Noor; Pramanik, A.K., E-mail: akpramanik@mail.jnu.ac.in

    2017-01-15

    The nature of insulating phase in 5d based Sr{sub 2}IrO{sub 4} is quite debated as the theoretical as well as experimental investigations have put forward evidences in favor of both magnetically driven Slater-type and interaction driven Mott-type insulator. To understand this insulating behavior, we have investigated the nature of magnetic state in Sr{sub 2}IrO{sub 4} through studying critical exponents, low temperature thermal demagnetization and magnetocaloric effect. The estimated critical exponents do not exactly match with any universality class, however, the values obey the scaling behavior. The exponent values suggest that spin interaction in present material is close to mean-field model. The analysis of low temperature thermal demagnetization data, however, shows dual presence of localized- and itinerant-type of magnetic interaction. Moreover, field dependent change in magnetic entropy indicates magnetic interaction is close to mean-field type. While this material shows an insulating behavior across the magnetic transition, yet a distinct change in slope in resistivity is observed around T{sub c}. We infer that though the insulating phase in Sr{sub 2}IrO{sub 4} is more close to be Slater-type but the simultaneous presence of both Slater- and Mott-type is the likely scenario for this material. - Highlights: • Critical analysis shows Sr{sub 2}IrO{sub 4} has ferromagnetic ordering temperature T{sub c}~225 K. • Obtained critical exponents imply spin interaction is close to mean-field model. • Analysis of magneto-entropy data also supports mean-field type interaction. • However, the presence of both itinerant and localized spin interaction is evident. • Sr{sub 2}IrO{sub 4} has simultaneous presence of both Slater- and Mott-type insulating phase.

  16. Crystallization and diffraction analysis of the serpin IRS-2 from the hard tick Ixodes ricinus

    International Nuclear Information System (INIS)

    Kovářová, Zuzana; Chmelař, Jindřich; Šanda, Miloslav; Brynda, Jiří; Mareš, Michael; Řezáčová, Pavlína

    2010-01-01

    Cleavage of the serpin IRS-2 from the hard tick I. ricinus by contaminating proteolytic activity mimicked the specific processing of the serpin by its target protease and resulted in a more stable form of the serpin which produced crystals that diffracted to 1.8 Å resolution. IRS-2 from the hard tick Ixodes ricinus belongs to the serpin family of protease inhibitors. It is produced in the salivary glands of the tick and its anti-inflammatory activity suggests that it plays a role in parasite–host interaction. Recombinant IRS-2 prepared by heterologous expression in a bacterial system was crystallized using the hanging-drop vapour-diffusion method. The crystals belonged to the primitive tetragonal space group P4 3 and diffracted to 1.8 Å resolution. Mass-spectrometric and electrophoretic analyses revealed that IRS-2 was cleaved by contaminating proteases during crystallization. This processing of IRS-2 mimicked the specific cleavage of the serpin by its target protease and resulted in a more stable form (the so-called relaxed conformation), which produced well diffracting crystals. Activity profiling with specific substrates and inhibitors demonstrated traces of serine and cysteine proteases in the protein stock solution

  17. Neutron-activation analysis of trace elements in thyroids

    International Nuclear Information System (INIS)

    Boulyga, S.F.; Petri, H.; Kanash, N.V.; Malenchenko, A.F.

    1999-01-01

    Neutron activation analysis was used for routine measurement of trace elements in thyroids of inhabitants of Belarus as well as in thyroids of people operated for thyroid cancer. The method chosen allowed the analysis of 28 elements, among them essential and toxic ones, with a good accuracy. The results obtained showed significant differences in the elemental composition of thyroid from the different regions. The changes of elemental composition of thyroids of inhabitants of the Gomel region, where goiter is endemic, seem to be identical to those in the tumor tissue. (author)

  18. On constitutive modelling in finite element analysis

    International Nuclear Information System (INIS)

    Bathe, K.J.; Snyder, M.D.; Cleary, M.P.

    1979-01-01

    This compact contains a brief introduction to the problems involved in constitutive modeling as well as an outline of the final paper to be submitted. Attention is focussed on three important areas: (1) the need for using theoretically sound material models and the importance of recognizing the limitations of the models, (2) the problem of developing stable and effective numerical representations of the models, and (3) the necessity for selection of an appropriate finite element mesh that can capture the actual physical response of the complete structure. In the final paper, we will be presenting our recent research results pertaining to each of these problem areas. (orig.)

  19. SEM and elemental analysis of composite resins

    International Nuclear Information System (INIS)

    Hosoda, H.; Yamada, T.; Inokoshi, S.

    1990-01-01

    Twenty-four chemically cured, 21 light-cured anterior, three light-cured anterior/posterior, and 18 light-cured posterior composite resins were examined using scanning electron microscopy, and the elemental composition of their filler particles was analyzed with an energy dispersive electron probe microanalyzer. According to the results obtained, the composite resins were divided into five groups (traditional, microfilled type, submicrofilled type, hybrid type, and semihybrid), with two additional hypothetical categories (microfilled and hybrid). Characteristics of each type were described with clinical indications for selective guidance of respective composite resins for clinical use

  20. Analysis of the development of missile-borne IR imaging detecting technologies

    Science.gov (United States)

    Fan, Jinxiang; Wang, Feng

    2017-10-01

    Today's infrared imaging guiding missiles are facing many challenges. With the development of targets' stealth, new-style IR countermeasures and penetrating technologies as well as the complexity of the operational environments, infrared imaging guiding missiles must meet the higher requirements of efficient target detection, capability of anti-interference and anti-jamming and the operational adaptability in complex, dynamic operating environments. Missileborne infrared imaging detecting systems are constrained by practical considerations like cost, size, weight and power (SWaP), and lifecycle requirements. Future-generation infrared imaging guiding missiles need to be resilient to changing operating environments and capable of doing more with fewer resources. Advanced IR imaging detecting and information exploring technologies are the key technologies that affect the future direction of IR imaging guidance missiles. Infrared imaging detecting and information exploring technologies research will support the development of more robust and efficient missile-borne infrared imaging detecting systems. Novelty IR imaging technologies, such as Infrared adaptive spectral imaging, are the key to effectively detect, recognize and track target under the complicated operating and countermeasures environments. Innovative information exploring techniques for the information of target, background and countermeasures provided by the detection system is the base for missile to recognize target and counter interference, jamming and countermeasure. Modular hardware and software development is the enabler for implementing multi-purpose, multi-function solutions. Uncooled IRFPA detectors and High-operating temperature IRFPA detectors as well as commercial-off-the-shelf (COTS) technology will support the implementing of low-cost infrared imaging guiding missiles. In this paper, the current status and features of missile-borne IR imaging detecting technologies are summarized. The key

  1. Neutron activation analysis of trace elements in foodstuffs

    International Nuclear Information System (INIS)

    Schelenz, R.; Fischer, E.

    1976-05-01

    A neutron activation method for multielement determination in biological material was developed. The individual steps of the method include radiochemical processing as well as nondestructive techniques. In order to develop a high resolution gamma spectrometric method the indispensable assumptions were the application of Ge(Li)-semiconductor detectors, multi-channel pulse height analyzers and the use of electronic data evaluation with mini-computers for the automatic evaluation of complex gamma spectra. After radiochemical separation (RNAA) 33 elements can be determined in biological materials and by application of nondestructive, purely instrumental techniques (INAA) 25 elements. The time required for the analysis of 33 elements can be determined in biological materials and by application of nondestructive, purely instrumental techniques (INAA) 25 elements. The time required for the analysis of 33 elements is 4 days. The neutron activation method is used routinely for the determination of trace elements in foodstuffs and in the field of nutrition research. (orig.) [de

  2. Alphavirus replicon approach to promoterless analysis of IRES elements.

    Science.gov (United States)

    Kamrud, K I; Custer, M; Dudek, J M; Owens, G; Alterson, K D; Lee, J S; Groebner, J L; Smith, J F

    2007-04-10

    Here we describe a system for promoterless analysis of putative internal ribosome entry site (IRES) elements using an alphavirus (family Togaviridae) replicon vector. The system uses the alphavirus subgenomic promoter to produce transcripts that, when modified to contain a spacer region upstream of an IRES element, allow analysis of cap-independent translation of genes of interest (GOI). If the IRES element is removed, translation of the subgenomic transcript can be reduced >95% compared to the same transcript containing a functional IRES element. Alphavirus replicons, used in this manner, offer an alternative to standard dicistronic DNA vectors or in vitro translation systems currently used to analyze putative IRES elements. In addition, protein expression levels varied depending on the spacer element located upstream of each IRES. The ability to modulate the level of expression from alphavirus vectors should extend the utility of these vectors in vaccine development.

  3. Elemental analysis of biological materials. Current problems and techniques with special reference to trace elements

    International Nuclear Information System (INIS)

    1980-01-01

    Selected techniques were reviewed for the assay of trace and minor elements in biological materials. Other relevant information is also presented on the need for such analyses, sampling, sample preparation and analytical quality control. In order to evaluate and compare the applicability of the various analytical techniques on a meaningful and objective basis, the materials chosen for consideration were intended to be typical of a wide range of biological matrics of different elemental compositions, namely Bowen's kale, representing a plant material, and NBS bovine liver, IAEA animal muscle, and blood serum, representing animal tissues. The subject is reviewed under the following headings: on the need for trace element analyses in the life sciences (4 papers); sampling and sample preparation for trace element analysis (2 papers); analytical techniques for trace and minor elements in biological materials (7 papers); analytical quality control (2 papers)

  4. Finite element analysis of inclined nozzle-plate junctions

    International Nuclear Information System (INIS)

    Dixit, K.B.; Seth, V.K.; Krishnan, A.; Ramamurthy, T.S.; Dattaguru, B.; Rao, A.K.

    1979-01-01

    Estimation of stress concentration at nozzle to plate or shell junctions is a significant problem in the stress analysis of nuclear reactors. The topic is a subject matter of extensive investigations and earlier considerable success has been reported on analysis for the cases when the nozzle is perpendicular to the plate or is radial to the shell. Analytical methods for the estimation of stress concentrations for the practical situations when the intersecting nozzle is inclined to the plate or is non-radial to the shell is rather scanty. Specific complications arise in dealing with the junction region when the nozzle with circular cross-section meets the non-circular cut-out on the plate or shell. In this paper a finite element analysis is developed for inclined nozzles and results are presented for nozzle-plate junctions. A method of analysis is developed with a view to achieving simultaneously accuracy of results and simplicity in the choice of elements and their connectivity. The circular nozzle is treated by axisymmetric conical shell elements. The nozzle portion in the region around the junction and the flat plate is dealt with by triangular flat shell elements. Special transition elements are developed for joining the flat shell elements with the axisymmetric elements under non-axisymmetric loading. A substructure method of analysis is adopted which achieves considerable economy in handling the structure and also conveniently combines the different types of elements in the structure. (orig.)

  5. PIXE methodology of rare earth element analysis and its applications

    International Nuclear Information System (INIS)

    Ma Xinpei

    1992-01-01

    The Proton Induced X-ray Emission (PIXE) methodology of rare earth element (REEs) analysis is discussed, including the significance of REE analysis, the principle of PIXE applied to REE, selection of characteristic X-ray for Lanthanide series elements, deconvolution of highly over lapped PIXE spectrum and minimum detection limit (MDL) of REEs. Some practical applications are presented. And the specialities of PIXE analysis to the high pure REE chemicals are discussed. (author)

  6. A computer program for structural analysis of fuel elements

    International Nuclear Information System (INIS)

    Hayashi, I.M.V.; Perrotta, J.A.

    1988-01-01

    It's presented the code ELCOM for the matrix analysis of tubular structures coupled by rigid spacers, typical of PWR's fuel elements. The code ELCOM makes a static structural analysis, where the displacements and internal forces are obtained for each structure at the joints with the spacers, and also, the natural frequencies and vibrational modes of an equivalent integrated structure are obtained. The ELCOM result is compared to a PWR fuel element structural analysis obtained in published paper. (author) [pt

  7. 2. Methods of elemental analysis of materials

    International Nuclear Information System (INIS)

    Musilek, L.

    1992-01-01

    The principles of activation analysis are outlined including the preparation of samples and reference materials, the choice of suitable activation sources, interfering effects, detection of radiation emitted and analysis of mixtures of emitters, and the potential of activation analysis in various fields of science and technology. The principles of X-ray fluorescence analysis and the associated instrumentation are also dealt with, and examples of applications are given. Described are also the physical nature of the Moessbauer effect, Moessbauer sources and spectrometers, and the applicability of this effect in physical research and in the investigation of iron-containing materials. (Z.S.). 1 tab., 20 figs., 90 refs

  8. Multi-element analysis of small biological samples

    International Nuclear Information System (INIS)

    Rokita, E.; Cafmeyer, J.; Maenhaut, W.

    1983-01-01

    A method combining PIXE and INAA was developed to determine the elemental composition of small biological samples. The method needs virtually no sample preparation and less than 1 mg is sufficient for the analysis. The method was used for determining up to 18 elements in leaves taken from Cracow Herbaceous. The factors which influence the elemental composition of leaves and the possible use of leaves as an environmental pollution indicator are discussed

  9. High accuracy 3D electromagnetic finite element analysis

    International Nuclear Information System (INIS)

    Nelson, E.M.

    1996-01-01

    A high accuracy 3D electromagnetic finite element field solver employing quadratic hexahedral elements and quadratic mixed-order one-form basis functions will be described. The solver is based on an object-oriented C++ class library. Test cases demonstrate that frequency errors less than 10 ppm can be achieved using modest workstations, and that the solutions have no contamination from spurious modes. The role of differential geometry and geometrical physics in finite element analysis will also be discussed

  10. X-ray fluorescent elemental analysis. Ch. 16

    International Nuclear Information System (INIS)

    Baryshev, V.; Kulipanov, G.; Skrinsky, A.

    1991-01-01

    X-ray fluorescence analysis (XFA) is used worldwide to define a quantitative content of the elements as well as to visualize the distribution of elements in different regions (element mapping). Utilization of synchrotron radiation (SR) to excite X-ray fluorescence enables the XFA method to be qualitatively improved. This chapter reviews the experimental work in especially the last decade (author). 71 refs.; 24 figs.; 3 tabs

  11. High accuracy 3D electromagnetic finite element analysis

    International Nuclear Information System (INIS)

    Nelson, Eric M.

    1997-01-01

    A high accuracy 3D electromagnetic finite element field solver employing quadratic hexahedral elements and quadratic mixed-order one-form basis functions will be described. The solver is based on an object-oriented C++ class library. Test cases demonstrate that frequency errors less than 10 ppm can be achieved using modest workstations, and that the solutions have no contamination from spurious modes. The role of differential geometry and geometrical physics in finite element analysis will also be discussed

  12. Nonlinear Finite Element Analysis of Shells with Large Aspect Ratio

    Science.gov (United States)

    Chang, T. Y.; Sawamiphakdi, K.

    1984-01-01

    A higher order degenerated shell element with nine nodes was selected for large deformation and post-buckling analysis of thick or thin shells. Elastic-plastic material properties are also included. The post-buckling analysis algorithm is given. Using a square plate, it was demonstrated that the none-node element does not have shear locking effect even if its aspect ratio was increased to the order 10 to the 8th power. Two sample problems are given to illustrate the analysis capability of the shell element.

  13. Neutron activation analysis of trace elements in IAEA reference materials

    International Nuclear Information System (INIS)

    Cheema, M.N.; Hasany, S.M.; Hanif, I.; Chaudhry, M.S.; Qureshi, I.H.

    1978-09-01

    Analytical Chemistry Group of Nuclear Chemistry Division at PINSTECH has been participating in IAEA Intercomparison programme of analytical quality control since 1972. So far fifteen samples of a variety of materials received from the Agency have been analyzed for different minor and trace elements. Mostly destructive and non-destructive neutron activation analysis techniques have been used for elemental analysis. In this report the description of the samples and the experimental procedures employed have been mentioned. The results of elemental analysis have been reported and compared with IAEA values which are based on the average computed from the results of different participating laboratories. (authors)

  14. Application of trace element analysis to determine trace element concentrations in the field of medicine

    International Nuclear Information System (INIS)

    Kasperek, K.; Feinendegen, L.E.

    1976-01-01

    Applied trace elements research in medicine requires a sensitive and efficient technique of trace elements analysis such as, e.g., neutron activation analysis. Essential trace elements act as stabilisators (iron in haem), structural elements (silicium in fibrous tissue), in hormones (iodine in thyroid hormone), in vitamins (cobalt in vitamin B 12), and in enzymes. Most of the essential trace elements act as coenzymes or in coenzymes or directly as metabolic catalysators. For example, selenium deficiency in PKU and maple syrup patients receiving dietary treatment can be detected by determining the selenium content of the serum, while low selenium values in the whole blood indicate liver cirrhosis. Acrodermatitis enteropathica can be diagnosed by determinig zinc in the serum, and pancreatic insufficiency by determining zinc in the pancreatic juice. Zinc also plays a part in disturbances of growth, in the healing of wounds, and in the insulin metabolism. Cobalt is important in some types of anaemia and in myocardiopathies. Trace elements are also necessary in the treatment of diseases, e.g. iron cobalt in some types of anaemia, and zinc in the delayed healing of wounds in the postoperative phase and in acrodermatitis enteropathica. Chromium is now being tested for the treatment of diabetes mellitus, and fluorides may be of interest in the treatment of osteoporosis. Finally, trace elements are important in the aetiology of acute poisoning, in nutrition, and in environmental protection. (orig./AK) [de

  15. Application of trace element analysis to determine trace element concentrations in the field of medicine. [Neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Kasperek, K; Feinendegen, L E

    1976-01-01

    Applied trace elements research in medicine requires a sensitive and efficient technique of trace elements analysis, such as neutron activation analysis. Essential trace elements act as stabilizators (iron in haem), structural elements (silicon in fibrous tissue), in hormones (iodine in thyroid hormone), in vitamins (cobalt in vitamin B 12), and in enzymes. Most of the essential trace elements act as coenzymes or in coenzymes or directly as metabolic catalyzers. For example, selenium deficiency in PKU and maple syrup patients receiving dietary treatment can be detected by determining the selenium content of the serum, while low selenium values in the whole blood indicate liver cirrhosis. Acrodermatitis enteropathica can be diagnosed by determinig zinc in the serum, and pancreatic insufficiency by determining zinc in the pancreatic juice. Zinc also plays a part in disturbances of growth, in the healing of wounds, and in the insulin metabolism. Cobalt is important in some types of anaemia and in myocardiopathies. Trace elements are also necessary in the treatment of diseases, e.g. iron cobalt in some types of anaemia, and zinc in the delayed healing of wounds in the postoperative phase and in acrodermatitis enteropathica. Chromium is now being tested for the treatment of diabetes mellitus, and fluorides may be of interest in the treatment of osteoporosis. Finally, trace elements are important in the aetiology of acute poisoning, in nutrition, and in environmental protection.

  16. A Rapid Method of Crude Oil Analysis Using FT-IR Spectroscopy

    African Journals Online (AJOL)

    HP USER

    Nigerian Journal of Basic and Applied Science (June,2016), 24(1): 47-55 ... ABSTRACT: This study determines the viability of the use of Fourier Transform ... IR spectra of Crude oil sample containing a mixture of both degraded (sample 151).

  17. Finite element stress analysis of brick-mortar masonry under ...

    African Journals Online (AJOL)

    Stress analysis of a brick-mortar couplet as a substitute for brick wall structure has been performed by finite element method, and algorithm for determining the element stiffness matrix for a plane stress problem using the displacement approach was developed. The nodal displacements were derived for the stress in each ...

  18. Trace elements in Australian opals using neutron activation analysis

    International Nuclear Information System (INIS)

    McOrist, G.D.; Fardy, J.J.

    1994-01-01

    Neutron activation analysis was used to determine the concentration of trace elements in 42 samples of black, grey and white opals taken from a number of recognised Australian field. The results were evaluated to determine if a relationship exited between trace element content and opal colour. (author) 12 refs.; 12 figs.; 3 tabs

  19. Probing Trace-elements in Bitumen by Neutron Activation Analysis

    NARCIS (Netherlands)

    Nahar, S.N.; Schmets, A.J.M.; Scarpas, Athanasios

    Trace elements and their concentrations play an important role in both chemical and physical properties of bitumen. Instrumental Neutron Activation Analysis (INAA) has been applied to determine the concentration of trace elements in bitumen. This method requires irradiation of the material with

  20. A method for the quantitative analysis of heavy elements by X-ray fluorescence

    International Nuclear Information System (INIS)

    Souza Caillaux, Z. de

    1981-01-01

    A study of quantitative analysis methodology by X-ray fluorescence analysis is presented. With no damage to precision it makes possible an analysis of heavy elements in samples with the form and texture as they present themselves. Some binary alloys were examined such as: FeCo; CuNi; CuZn; AgCd; AgPd; AuPt e PtIr. The possibility of application of this method is based on the compromise solutIon of wave lengths and the intensity of the homologous emission and absorption edges of constituents with the quantic efficiency of the detector, the dispersion and the wave lenght resolution of crystal analyser, and the uniformity of the excitation intensity. (Author) [pt

  1. Introduction to finite element analysis using MATLAB and Abaqus

    CERN Document Server

    Khennane, Amar

    2013-01-01

    There are some books that target the theory of the finite element, while others focus on the programming side of things. Introduction to Finite Element Analysis Using MATLAB(R) and Abaqus accomplishes both. This book teaches the first principles of the finite element method. It presents the theory of the finite element method while maintaining a balance between its mathematical formulation, programming implementation, and application using commercial software. The computer implementation is carried out using MATLAB, while the practical applications are carried out in both MATLAB and Abaqus. MA

  2. Shakedown analysis by finite element incremental procedures

    International Nuclear Information System (INIS)

    Borkowski, A.; Kleiber, M.

    1979-01-01

    It is a common occurence in many practical problems that external loads are variable and the exact time-dependent history of loading is unknown. Instead of it load is characterized by a given loading domain: a convex polyhedron in the n-dimensional space of load parameters. The problem is then to check whether a structure shakes down, i.e. responds elastically after a few elasto-plastic cycles, or not to a variable loading as defined above. Such check can be performed by an incremental procedure. One should reproduce incrementally a simple cyclic process which consists of proportional load paths that connect the origin of the load space with the corners of the loading domain. It was proved that if a structure shakes down to such loading history then it is able to adopt itself to an arbitrary load path contained in the loading domain. The main advantage of such approach is the possibility to use existing incremental finite-element computer codes. (orig.)

  3. Optical strain measurements and its finite element analysis of cold ...

    African Journals Online (AJOL)

    International Journal of Engineering, Science and Technology ... Online video images of square grid were recorded during the deformation ... Finite element software ANSYS has been applied for the analysis of the upset forming process.

  4. Elemental analysis of combustion products by neutron activation

    International Nuclear Information System (INIS)

    Heft, R.E.; Koszykowski, R.F.

    1980-01-01

    This paper gives a brief description of the neutron activation analysis method, which is being used to determine the elemental profile of combustion products from coal-fired power plants, oil shale retorting, and underground coal gasification

  5. Finite element analysis of thermal stress distribution in different ...

    African Journals Online (AJOL)

    Nigerian Journal of Clinical Practice • Jan-Feb 2016 • Vol 19 • Issue 1. Abstract ... Key words: Amalgam, finite element method, glass ionomer cement, resin composite, thermal stress ... applications for force analysis and assessment of different.

  6. A study on the nonlinear finite element analysis of reinforced concrete structures: shell finite element formulation

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Sang Jin; Seo, Jeong Moon

    2000-08-01

    The main goal of this research is to establish a methodology of finite element analysis of containment building predicting not only global behaviour but also local failure mode. In this report, we summerize some existing numerical analysis techniques to be improved for containment building. In other words, a complete description of the standard degenerated shell finite element formulation is provided for nonlinear stress analysis of nuclear containment structure. A shell finite element is derived using the degenerated solid concept which does not rely on a specific shell theory. Reissner-Mindlin assumptions are adopted to consider the transverse shear deformation effect. In order to minimize the sensitivity of the constitutive equation to structural types, microscopic material model is adopted. The four solution algorithms based on the standard Newton-Raphson method are discussed. Finally, two numerical examples are carried out to test the performance of the adopted shell medel.

  7. A study on the nonlinear finite element analysis of reinforced concrete structures: shell finite element formulation

    International Nuclear Information System (INIS)

    Lee, Sang Jin; Seo, Jeong Moon

    2000-08-01

    The main goal of this research is to establish a methodology of finite element analysis of containment building predicting not only global behaviour but also local failure mode. In this report, we summerize some existing numerical analysis techniques to be improved for containment building. In other words, a complete description of the standard degenerated shell finite element formulation is provided for nonlinear stress analysis of nuclear containment structure. A shell finite element is derived using the degenerated solid concept which does not rely on a specific shell theory. Reissner-Mindlin assumptions are adopted to consider the transverse shear deformation effect. In order to minimize the sensitivity of the constitutive equation to structural types, microscopic material model is adopted. The four solution algorithms based on the standard Newton-Raphson method are discussed. Finally, two numerical examples are carried out to test the performance of the adopted shell medel

  8. Trace and ultratrace level elemental and speciation analysis

    International Nuclear Information System (INIS)

    Arunachalam, J.

    2012-01-01

    Accurate determination of elements present at parts per million and billion levels in various matrices is a growing requirement in different fields. In environmental sciences various trace elements need to be analyzed so as establish the dispersal models of pollutants or the adequacy of effluent treatment prior to discharge into water bodies. The issues of bioaccumulation and magnification are important in aquatic systems. In nutrition and biochemistry one has to establish the bio-availability of essential and toxic elemental species as toxic elements prevent assimilation of essential elements. Fission and fusion technologies use a variety of structural materials requiring many trace elements to be present at levels strictly below the specified levels. Ultra-pure bulk semiconductor materials are required for fabrication devices. In metallurgy and materials sciences too, various trace elements are known to influence the properties. In the emerging fields like nanotechnology, it is necessary to understand the passage and accumulation of nano-particles inside the cells, through trace analysis. Many analytical techniques exist which can provide the concentration information in the bulk materials with good accuracy. They include ICP-AES, FAAS, and ICP-MS, which are solution based techniques. Direct solid state analytical techniques are Glow Discharge Mass Spectrometry (GDMS) and XRF. Accelerator based ion-beam analysis techniques can provide information on concentration and depth profiles of different elements in layered structures. Hyphenated techniques such as HPLC/lC-ICPMS, are helpful in identifying various chemical oxidation states in which a given element might be present in a matrix, which is termed as speciation analysis. This presentation will include the existing analytical competencies and the laboratory requirements for trace and ultra trace element elemental and speciation analyses and their applications. (author)

  9. Analysis and design of lumped element Marchand baluns

    DEFF Research Database (Denmark)

    Johansen, Tom Keinicke; Krozer, Viktor

    2008-01-01

    In this paper a novel design procedure for lumped element Marchand baluns is proposed. An analysis is performed on the balun structure in order to determine the conditions for ideal balun performance in terms of the lumped element values. The analysis is verified by two broadband designs centered...... around 22.75 GHz and differing only in terms of their impedance transformation ratio. EM simulation results on our proposed lumped element Marchand balun structure predicts an insertion loss of 4 dB and return loss of 40 dB at the design frequency of 22.75 GHz. The amplitude and phase imbalance...

  10. Finite element analysis of tubular joints in offshore structures ...

    African Journals Online (AJOL)

    ... representing a 2-D model of the joint between the brace and the chord walls. This was subsequently followed but finite element analysis of six tubular joints. A global analysis was initially undertaken, then the submodel analysis carried in the areas of stress concentration. Journal of Civil Engineering, JKUAT (2001) Vol 6, ...

  11. ANALYSIS OF DESIGN ELEMENTS IN SKI SUITS

    Directory of Open Access Journals (Sweden)

    Birsen Çileroğlu

    2014-06-01

    Full Text Available Popularity of Ski Sport in 19th century necessitated a new perspective on protective skiing clothing ag ainst the mountain climates and excessive cold. Winter clothing were the basis of ski attire during this period. By the beginning of 20th century lining cloth were used to minimize the wind effect. The difference between the men and women’s ski attire of the time consisted of a knee - length skirts worn over the golf trousers. Subsequent to the First World War, skiing suit models were influenced by the period uniforms and the producers reflected the fashion trends to the ski clothing. In conformance with th e prevailing trends, ski trousers were designed and produced for the women thus leading to reduction in gender differences. Increases in the ski tourism and holding of the first winter olympics in 1924 resulted in variations in ski attires, development of design characteristics, growth in user numbers, and enlargement of production capacities. Designers emphasized in their collections combined presence of elegance and practicality in the skiing attire. In 1930s, the ski suits influenced by pilots’ uniforms included characteristics permitting freedom of motion, and the design elements exhibited changes in terms of style, material and aerodynamics. In time, the ski attires showed varying design features distinguishing professionals from the amateurs. While protective functionality was primary consideration for the amateurs, for professionals the aerodynamic design was also a leading factor. Eventually, the increased differences in design characteristics were exhibited in ski suit collections, World reknown brands were formed, production and sales volumes showed significant rise. During 20th century the ski suits influenced by fashion trends to acquire unique styles reached a position of dominance to impact current fashion trends, and apart from sports attir es they became a style determinant in the clothing of cold climates. Ski suits

  12. Kinetics and evolved gas analysis for pyrolysis of food processing wastes using TGA/MS/FT-IR.

    Science.gov (United States)

    Özsin, Gamzenur; Pütün, Ayşe Eren

    2017-06-01

    The objective of this study was to identify the pyrolysis of different bio-waste produced by food processing industry in a comprehensible manner. For this purpose, pyrolysis behaviors of chestnut shells (CNS), cherry stones (CS) and grape seeds (GS) were investigated by thermogravimetric analysis (TGA) combined with a Fourier-transform infrared (FT-IR) spectrometer and a mass spectrometer (MS). In order to make available theoretical groundwork for biomass pyrolysis, activation energies were calculated with the help of four different model-free kinetic methods. The results are attributed to the complex reaction schemes which imply parallel, competitive and complex reactions during pyrolysis. During pyrolysis, the evolution of volatiles was also characterized by FT-IR and MS. The main evolved gases were determined as H 2 O, CO 2 and hydrocarbons such as CH 4 and temperature dependent profiles of the species were obtained. Copyright © 2017 Elsevier Ltd. All rights reserved.

  13. Finite Element Analysis of Circular Plate using SolidWorks

    International Nuclear Information System (INIS)

    Kang, Yeo Jin; Jhung, Myung Jo

    2011-01-01

    Circular plates are used extensively in mechanical engineering for nuclear reactor internal components. The examples in the reactor vessel internals are upper guide structure support plate, fuel alignment plate, lower support plate etc. To verify the structural integrity of these plates, the finite element analyses are performed, which require the development of the finite element model. Sometimes it is very costly and time consuming to make the model especially for the beginners who start their engineering job for the structural analysis, necessitating a simple method to develop the finite element model for the pursuing structural analysis. Therefore in this study, the input decks are generated for the finite element analysis of a circular plate as shown in Fig. 1, which can be used for the structural analysis such as modal analysis, response spectrum analysis, stress analysis, etc using the commercial program Solid Works. The example problems are solved and the results are included for analysts to perform easily the finite element analysis of the mechanical plate components due to various loadings. The various results presented in this study would be helpful not only for the benchmark calculations and results comparisons but also as a part of the knowledge management for the future generation of young designers, scientists and computer analysts

  14. Analysis of concrete beams using applied element method

    Science.gov (United States)

    Lincy Christy, D.; Madhavan Pillai, T. M.; Nagarajan, Praveen

    2018-03-01

    The Applied Element Method (AEM) is a displacement based method of structural analysis. Some of its features are similar to that of Finite Element Method (FEM). In AEM, the structure is analysed by dividing it into several elements similar to FEM. But, in AEM, elements are connected by springs instead of nodes as in the case of FEM. In this paper, background to AEM is discussed and necessary equations are derived. For illustrating the application of AEM, it has been used to analyse plain concrete beam of fixed support condition. The analysis is limited to the analysis of 2-dimensional structures. It was found that the number of springs has no much influence on the results. AEM could predict deflection and reactions with reasonable degree of accuracy.

  15. Dynamic relaxation method in analysis of reinforced concrete bent elements

    Directory of Open Access Journals (Sweden)

    Anna Szcześniak

    2015-12-01

    Full Text Available The paper presents a method for the analysis of nonlinear behaviour of reinforced concrete bent elements subjected to short-term static load. The considerations in the range of modelling of deformation processes of reinforced concrete element were carried out. The method of structure effort analysis was developed using the finite difference method. The Dynamic Relaxation Method, which — after introduction of critical damping — allows for description of the static behaviour of a structural element, was used to solve the system of nonlinear equilibrium equations. In order to increase the method effectiveness in the range of the post-critical analysis, the Arc Length Parameter on the equilibrium path was introduced into the computational procedure.[b]Keywords[/b]: reinforced concrete elements, physical nonlinearity, geometrical nonlinearity, dynamic relaxation method, arc-length method

  16. Analysis of trace elements in opal using PIXE

    Energy Technology Data Exchange (ETDEWEB)

    Hinrichs, Ruth, E-mail: ruth.hinrichs@ufrgs.br [Instituto de Geociências, Universidade Federal do Rio Grande do Sul, Porto Alegre, RS (Brazil); Programa de Pós-graduação em Física, UFRGS, Porto Alegre, RS (Brazil); Bertol, A.P.L. [Programa de Pós-graduação em Física, UFRGS, Porto Alegre, RS (Brazil); Vasconcellos, M.A.Z. [Programa de Pós-graduação em Física, UFRGS, Porto Alegre, RS (Brazil); Instituto de Física, UFRGS, Porto Alegre, RS (Brazil)

    2015-11-15

    Particle induced X-ray emission (PIXE) analysis is particularly important for the analysis of trace elements of precious samples, being one of the few methods to determine elements with ppm concentration that does not affect sample integrity. A PIXE methodology for trace element analysis in opal was developed. To avoid detector count saturation due to the high number of Si-Kα X-rays generated in the sample, several filters were employed to optimize the reduction of the Si-Kα signal, while maintaining acceptable intensities of the other relevant X-ray lines. Two proton beam energies were tested, to establish the signal to noise ratio in different X-ray energies. Spectra were fitted with the software GUPIX, using a matrix composition determined with electron beam excited energy dispersive X-ray spectrometry. Above the energy of the silicon X-ray, several trace elements were quantified.

  17. Correct use of Membrane Elements in Structural Analysis

    Directory of Open Access Journals (Sweden)

    Rothman Timothy

    2016-01-01

    Full Text Available Structural analysis of consumer electronic devices such as phones and tablets involves Finite Element Analysis (FEA. Dynamic loading conditions such as device dropping and bending dictate accurate FEA models to reduce design risk in many areas. The solid elements typically used in structural analysis do not have integration points on the surface. The outer surface is of most interest because that is where the cracks start. Analysts employ a post processing trick through using membranes to bring accurate stress/strain results to the surface. This paper explains numerical issues with implementation of membranes and recommends a methodology for accurate structural analysis.

  18. Using the ion microprobe mass analyser for trace element analysis

    International Nuclear Information System (INIS)

    Schilling, J.H.

    1978-01-01

    Most techniques for the analysis of trace elements are capable of determining the concentrations in a bulk sample or solution, but without reflecting their distribution. In a bulk analysis therefore elements which occur in high concentration in a few precipitates would still be considered trace elements even though their local concentration greatly exceed the normally accepted trace elements concentration limit. Anomalous distribution is also shown by an oxide layer, a few hundred Angstrom thick, on an aluminium sample. A low oxide concentration would be reported if it were included in the bulk analysis, which contradicts the high surface concentration. The importance of a knowledge of the trace element distribution is therefore demonstrated. Distributional trace element analysis can be carried out using the ion microprobe mass analyser (IMMA). Since the analytical technique used in this instrument, namely secondary ion mass spectrometry (SIMS), is not universally appreciated, the instrument and its features will be described briefly followed by a discussion of quantitative analysis and the related subjects of detection limit and sample consumption. Finally, a few examples of the use of the instrument are given

  19. Elements of stochastic calculus and analysis

    CERN Document Server

    Stroock, Daniel W

    2018-01-01

    This book gives a somewhat unconventional introduction to stochastic analysis. Although most of the material covered here has appeared in other places, this book attempts to explain the core ideas on which that material is based. As a consequence, the presentation is more an extended mathematical essay than a ``definition, lemma, theorem'' text. In addition, it includes several topics that are not usually treated elsewhere. For example, Wiener's theory of homogeneous chaos is discussed, Stratovich integration is given a novel development and applied to derive Wong and Zakai's approximation theorem, and examples are given of the application of Malliavin's calculus to partial differential equations. Each chapter concludes with several exercises, some of which are quite challenging. The book is intended for use by advanced graduate students and research mathematicians who may be familiar with many of the topics but want to broaden their understanding of them.

  20. High sensitivity analysis of atmospheric gas elements

    International Nuclear Information System (INIS)

    Miwa, Shiro; Nomachi, Ichiro; Kitajima, Hideo

    2006-01-01

    We have investigated the detection limit of H, C and O in Si, GaAs and InP using a Cameca IMS-4f instrument equipped with a modified vacuum system to improve the detection limit with a lower sputtering rate We found that the detection limits for H, O and C are improved by employing a primary ion bombardment before the analysis. Background levels of 1 x 10 17 atoms/cm 3 for H, of 3 x 10 16 atoms/cm 3 for C and of 2 x 10 16 atoms/cm 3 for O could be achieved in silicon with a sputtering rate of 2 nm/s after a primary ion bombardment for 160 h. We also found that the use of a 20 K He cryo-panel near the sample holder was effective for obtaining better detection limits in a shorter time, although the final detection limits using the panel are identical to those achieved without it

  1. High sensitivity analysis of atmospheric gas elements

    Energy Technology Data Exchange (ETDEWEB)

    Miwa, Shiro [Materials Analysis Lab., Sony Corporation, 4-16-1 Okata, Atsugi 243-0021 (Japan)]. E-mail: Shiro.Miwa@jp.sony.com; Nomachi, Ichiro [Materials Analysis Lab., Sony Corporation, 4-16-1 Okata, Atsugi 243-0021 (Japan); Kitajima, Hideo [Nanotechnos Corp., 5-4-30 Nishihashimoto, Sagamihara 229-1131 (Japan)

    2006-07-30

    We have investigated the detection limit of H, C and O in Si, GaAs and InP using a Cameca IMS-4f instrument equipped with a modified vacuum system to improve the detection limit with a lower sputtering rate We found that the detection limits for H, O and C are improved by employing a primary ion bombardment before the analysis. Background levels of 1 x 10{sup 17} atoms/cm{sup 3} for H, of 3 x 10{sup 16} atoms/cm{sup 3} for C and of 2 x 10{sup 16} atoms/cm{sup 3} for O could be achieved in silicon with a sputtering rate of 2 nm/s after a primary ion bombardment for 160 h. We also found that the use of a 20 K He cryo-panel near the sample holder was effective for obtaining better detection limits in a shorter time, although the final detection limits using the panel are identical to those achieved without it.

  2. Thermomechanical analysis of nuclear fuel elements

    International Nuclear Information System (INIS)

    Hernandez L, H.

    1997-01-01

    This work presents development of a code to obtain the thermomechanical analysis of fuel rods in the fuel assemblies inserted in the core of BWR reactors. The code uses experimental correlations developed in several laboratories. The development of the code is divided in two parts: a) the thermal part and b) the mechanical part, extending both the fuel and the cladding materials. The thermal part consists of finding the radial distribution of temperatures in the pellet, from the fuel centerline up to the coolant, along the total active length, considering one and two phase flow in the coolant, as a result of the pressure drop in the system. The mechanical part analyzes the effects of temperature gradients, pressure and irradiation, to which the fuel rod is subjected. The strains produced by swelling, creep and thermal stress in the fuel material are analyzed. In the same way the strains in the cladding are analyzed, considering the effects produced by the pressure exerted on the cladding by pellet swelling, by the pressure caused by fission gas release toward the cavities, and by the strain produced on the cladding by the pressure changes of the system. (Author)

  3. Perspectives on clinical possibility: elements of analysis.

    Science.gov (United States)

    Chiffi, Daniele; Zanotti, Renzo

    2016-08-01

    Possibility is one of the most common modalities in reasoning and argumentation. Various kinds of modal concepts have been identified in philosophical and logical discussion of the metaphysics of modality. We focus here on the concept of clinical possibility. A critical analysis of what is intended as clinical possibility has not yet received sufficient examination, although the concept is extensively used in clinical reasoning. We present arguments to emphasize some desirable features associated with the concept of clinical possibility. We argue that almost all clinical possibilities are potentialities, that is, possibilities that may be actualized by effective, appropriate and feasible interventions. However, in some limited cases, even mere possibilities - which may or may not be actualized, since we do not have the required knowledge - may be involved in clinical reasoning, and we present some examples in this paper. We then introduce some basic views on the nature of possibility showing their validity and limitations when applied to the concept of clinical possibility. Lastly, we conjecture that clinical possibility is a normative modality that can be formalized in a multimodal system with epistemic and deontic logical operators. © 2015 John Wiley & Sons, Ltd.

  4. Finite element analysis of an inflatable torus considering air mass structural element

    Science.gov (United States)

    Gajbhiye, S. C.; Upadhyay, S. H.; Harsha, S. P.

    2014-01-01

    Inflatable structures, also known as gossamer structures, are at high boom in the current space technology due to their low mass and compact size comparing to the traditional spacecraft designing. Internal pressure becomes the major source of strength and rigidity, essentially stiffen the structure. However, inflatable space based membrane structure are at high risk to the vibration disturbance due to their low structural stiffness and material damping. Hence, the vibration modes of the structure should be known to a high degree of accuracy in order to provide better control authority. In the past, most of the studies conducted on the vibration analysis of gossamer structures used inaccurate or approximate theories in modeling the internal pressure. The toroidal shaped structure is one of the important key element in space application, helps to support the reflector in space application. This paper discusses the finite-element analysis of an inflated torus. The eigen-frequencies are obtained via three-dimensional small-strain elasticity theory, based on extremum energy principle. The two finite-element model (model-1 and model-2) have cases have been generated using a commercial finite-element package. The structure model-1 with shell element and model-2 with the combination of the mass of enclosed fluid (air) added to the shell elements have been taken for the study. The model-1 is computed with present analytical approach to understand the convergence rate and the accuracy. The convergence study is made available for the symmetric modes and anti-symmetric modes about the centroidal-axis plane, meeting the eigen-frequencies of an inflatable torus with the circular cross section. The structural model-2 is introduced with air mass element and analyzed its eigen-frequency with different aspect ratio and mode shape response using in-plane and out-plane loading condition are studied.

  5. A refined element-based Lagrangian shell element for geometrically nonlinear analysis of shell structures

    Directory of Open Access Journals (Sweden)

    Woo-Young Jung

    2015-04-01

    Full Text Available For the solution of geometrically nonlinear analysis of plates and shells, the formulation of a nonlinear nine-node refined first-order shear deformable element-based Lagrangian shell element is presented. Natural co-ordinate-based higher order transverse shear strains are used in present shell element. Using the assumed natural strain method with proper interpolation functions, the present shell element generates neither membrane nor shear locking behavior even when full integration is used in the formulation. Furthermore, a refined first-order shear deformation theory for thin and thick shells, which results in parabolic through-thickness distribution of the transverse shear strains from the formulation based on the third-order shear deformation theory, is proposed. This formulation eliminates the need for shear correction factors in the first-order theory. To avoid difficulties resulting from large increments of the rotations, a scheme of attached reference system is used for the expression of rotations of shell normal. Numerical examples demonstrate that the present element behaves reasonably satisfactorily either for the linear or for geometrically nonlinear analysis of thin and thick plates and shells with large displacement but small strain. Especially, the nonlinear results of slit annular plates with various loads provided the benchmark to test the accuracy of related numerical solutions.

  6. Geographic identification of Boletus mushrooms by data fusion of FT-IR and UV spectroscopies combined with multivariate statistical analysis

    Science.gov (United States)

    Yao, Sen; Li, Tao; Li, JieQing; Liu, HongGao; Wang, YuanZhong

    2018-06-01

    Boletus griseus and Boletus edulis are two well-known wild-grown edible mushrooms which have high nutrition, delicious flavor and high economic value distributing in Yunnan Province. In this study, a rapid method using Fourier transform infrared (FT-IR) and ultraviolet (UV) spectroscopies coupled with data fusion was established for the discrimination of Boletus mushrooms from seven different geographical origins with pattern recognition method. Initially, the spectra of 332 mushroom samples obtained from the two spectroscopic techniques were analyzed individually and then the classification performance based on data fusion strategy was investigated. Meanwhile, the latent variables (LVs) of FT-IR and UV spectra were extracted by partial least square discriminant analysis (PLS-DA) and two datasets were concatenated into a new matrix for data fusion. Then, the fusion matrix was further analyzed by support vector machine (SVM). Compared with single spectroscopic technique, data fusion strategy can improve the classification performance effectively. In particular, the accuracy of correct classification of SVM model in training and test sets were 99.10% and 100.00%, respectively. The results demonstrated that data fusion of FT-IR and UV spectra can provide higher synergic effect for the discrimination of different geographical origins of Boletus mushrooms, which may be benefit for further authentication and quality assessment of edible mushrooms.

  7. V{sub 1+x}Nb{sub 1-x}IrB{sub 2} (x ∼ 0.1), the first quaternary metal-rich -boride adopting the Mo{sub 2}IrB{sub 2}-type structure: Synthesis, crystal and electronic structure and bonding analysis

    Energy Technology Data Exchange (ETDEWEB)

    Goerens, Christian; Fokwa, Boniface P.T. [Institute of Inorganic Chemistry, RWTH Aachen University (Germany)

    2013-02-15

    Polycrystalline samples and single crystals of the new metal-rich boride V{sub 1+x}Nb{sub 1-x}IrB{sub 2} (x ∼ 0.1), were synthesized by arc-melting the elements in a water-cooled copper crucible under an argon atmosphere and characterized by X-ray diffraction and EDX measurements. The crystal structure was refined on the basis of single crystal data. The new phase adopts the Mo{sub 2}IrB{sub 2}-type structure (space group Pnnm, no. 58) with the lattice parameters a = 7.301(7) Aa, b = 9.388(9) Aa and c = 3.206(5) Aa. It is the first quaternary representative of Mo{sub 2}IrB{sub 2}-type structure. The structure contains zigzag B{sub 4}-fragments with boron-boron distances of 1.83-1.85 Aa. The electronic density of states and crystal orbital Hamilton population (for bonding analysis) were calculated, using the linear muffin-tin orbital atomic sphere approximation (LMTO-ASA) method. According to these calculations, this metal-rich compound should be metallic, as expected. Furthermore, very strong boron-boron interactions are observed in the zigzag B{sub 4}-fragment and two significantly different Ir-B interactions are observed in the new phase and the prototype Mo{sub 2}IrB{sub 2}. (Copyright copyright 2013 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  8. Complex finite element sensitivity method for creep analysis

    International Nuclear Information System (INIS)

    Gomez-Farias, Armando; Montoya, Arturo; Millwater, Harry

    2015-01-01

    The complex finite element method (ZFEM) has been extended to perform sensitivity analysis for mechanical and structural systems undergoing creep deformation. ZFEM uses a complex finite element formulation to provide shape, material, and loading derivatives of the system response, providing an insight into the essential factors which control the behavior of the system as a function of time. A complex variable-based quadrilateral user element (UEL) subroutine implementing the power law creep constitutive formulation was incorporated within the Abaqus commercial finite element software. The results of the complex finite element computations were verified by comparing them to the reference solution for the steady-state creep problem of a thick-walled cylinder in the power law creep range. A practical application of the ZFEM implementation to creep deformation analysis is the calculation of the skeletal point of a notched bar test from a single ZFEM run. In contrast, the standard finite element procedure requires multiple runs. The value of the skeletal point is that it identifies the location where the stress state is accurate, regardless of the certainty of the creep material properties. - Highlights: • A novel finite element sensitivity method (ZFEM) for creep was introduced. • ZFEM has the capability to calculate accurate partial derivatives. • ZFEM can be used for identification of the skeletal point of creep structures. • ZFEM can be easily implemented in a commercial software, e.g. Abaqus. • ZFEM results were shown to be in excellent agreement with analytical solutions

  9. Elemental content of Vietnamese rice. Part 2. Multivariate data analysis.

    Science.gov (United States)

    Kokot, S; Phuong, T D

    1999-04-01

    Rice samples were obtained from the Red River region and some other parts of Vietnam as well as from Yanco, Australia. These samples were analysed for 14 elements (P, K, Mg, Ca, Mn, Zn, Fe, Cu, Al, Na, Ni, As, Mo and Cd) by ICP-AES, ICP-MS and FAAS as described in Part 1. This data matrix was then submitted to multivariate data analysis by principal component analysis to investigate the influences of environmental and crop cultivation variables on the elemental content of rice. Results revealed that geographical location, grain variety, seasons and soil conditions are the most likely significant factors causing changes in the elemental content between the rice samples. To assess rice quality according to its elemental content and physio-biological properties, a multicriteria decision making method (PROMETHEE) was applied. With the Vietnamese rice, the sticky rice appeared to contain somewhat higher levels of nutritionally significant elements such as P, K and Mg than the non-sticky rice. Also, rice samples grown during the wet season have better levels of nutritionally significant mineral elements than those of the dry season, but in general, the wet season seemed to provide better overall elemental and physio-biological rice quality.

  10. A finite-element for the analysis of shell intersections

    International Nuclear Information System (INIS)

    Koves, W.J.; Nair, S.

    1994-01-01

    The analysis of discontinuity stresses at shell intersections is a problem of great importance in several major industries. Some of the major areas of interest are pressure-containing equipment, such as reactors and piping, in the nuclear and fossil power industry; pressure vessels and heat exchangers in the petrochemical industry; bracing in offshore oil platforms; and aerospace structures. A specialized shell-intersection finite element, which is compatible with adjoining shell elements, has been developed that has the capability of physically representing the complex three-dimensional geometry and stress state at shell intersections. The element geometry is a contoured shape that matches a wide variety of practical nozzle configurations used in ASME Code pressure vessel construction, and allows computational rigor. A closed-form theory of elasticity solution was used to compute the stress state and strain energy in the element. The concept of an energy-equivalent nodal displacement and force vector set was then developed to allow complete compatibility with adjoining shell elements and retain the analytical rigor within the element. This methodology provides a powerful and robust computation scheme that maintains the computational efficiency of shell element solutions. The shell-intersection element was then applied to the cylinder-sphere and cylinder-cylinder intersection problems

  11. Hydrothermal analysis in engineering using control volume finite element method

    CERN Document Server

    Sheikholeslami, Mohsen

    2015-01-01

    Control volume finite element methods (CVFEM) bridge the gap between finite difference and finite element methods, using the advantages of both methods for simulation of multi-physics problems in complex geometries. In Hydrothermal Analysis in Engineering Using Control Volume Finite Element Method, CVFEM is covered in detail and applied to key areas of thermal engineering. Examples, exercises, and extensive references are used to show the use of the technique to model key engineering problems such as heat transfer in nanofluids (to enhance performance and compactness of energy systems),

  12. Element analysis of Japanese traditional papers by PIXE method

    International Nuclear Information System (INIS)

    Suzuki, Tatsuya; Yasuda, Keisuke; Tani, Teruhiro

    2000-01-01

    The Japanese papers, 'washi', are made from the bast fibers of the plants. Since washi have the informations of the raw material plants, there is potentiality of the identification of the production place by the element analysis of the washi. Three kinds of washi made of kozo, which have different habitats, were prepared. The elements in their washi were measured by the PIXE. It was confirmed that the amount of elements included in the washi depend on the habitats of their raw material plants. (author)

  13. High accuracy 3D electromagnetic finite element analysis

    International Nuclear Information System (INIS)

    Nelson, E.M.

    1997-01-01

    A high accuracy 3D electromagnetic finite element field solver employing quadratic hexahedral elements and quadratic mixed-order one-form basis functions will be described. The solver is based on an object-oriented C++ class library. Test cases demonstrate that frequency errors less than 10 ppm can be achieved using modest workstations, and that the solutions have no contamination from spurious modes. The role of differential geometry and geometrical physics in finite element analysis will also be discussed. copyright 1997 American Institute of Physics

  14. FT-IR spectroscopic analysis for studying Clostridium cell response to conversion of enzymatically hydrolyzed hay

    Science.gov (United States)

    Grube, Mara; Gavare, Marita; Nescerecka, Alina; Tihomirova, Kristina; Mezule, Linda; Juhna, Talis

    2013-07-01

    Grass hay is one of assailable cellulose containing non-food agricultural wastes that can be used as a carbohydrate source by microorganisms producing biofuels. In this study three Clostridium strains Clostridium acetobutylicum, Clostridium beijerinckii and Clostridium tetanomorphum, capable of producing acetone, butanol and ethanol (ABE) were adapted to convert enzymatically hydrolyzed hay used as a growth media additive. The results of growth curves, substrate degradation kinetics and FT-IR analyses of bacterial biomass macromolecular composition showed diverse strain-specific cell response to the growth medium composition.

  15. Nonlinear nonstationary analysis with the finite element method

    International Nuclear Information System (INIS)

    Vaz, L.E.

    1981-01-01

    In this paper, after some introductory remarks on numerical methods for the integration of initial value problems, the applicability of the finite element method for transient diffusion analysis as well as dynamic and inelastic analysis is discussed, and some examples are presented. (RW) [de

  16. a finite element model for the analysis of bridge decks

    African Journals Online (AJOL)

    Dr Obe

    A FINITE ELEMENT MODEL FOR THE ANALYSIS OF BRIDGE DECKS. NIGERIAN JOURNAL OF TECHNOLOGY, VOL. 27 NO.1, MARCH 2008. 59. (a) Beam-plate system. (b) T-beam structural model. Fig. 1 Beam-plate structure idealisations. The matrix displacement method of analysis is used. The continuum structure is.

  17. PIXE analysis of trace elements in cetacean teeth

    International Nuclear Information System (INIS)

    Mitani, Yoko; Arai, Nobuaki; Sakamoto, Wataru; Yoshida, Koji

    1997-01-01

    PIXE was adopted for analysis of trace elements in teeth of two species of cetaceans, sperm whale (Physeter microcephalus) and pantropical spotted dolphin (Stenella attenuata). The analyses were performed along with the growth layer of the teeth, which is formed annually, suitable for age determination. Mn, Fe, Cu, Zu and Sr were detected in the teeth of sperm whale and pantropical spotted dolphin. Among these trace elements, gradual increase was observed for Zn/Ca ratio in the sperm whale's teeth. (author)

  18. Trace elements in coloured opals using neutron activation analysis

    International Nuclear Information System (INIS)

    McOrist, G.D.; Smallwood, A.

    1995-01-01

    Neutron activation analysis was used to determine the concentration of trace elements in 50 samples of orange, yellow, honey, green, blue and pink opals as well as 18 samples of colourless opals taken from a number of recognised fields in Australia, Peru, Mexico and USA. The results were evaluated to determine the relationship between trace elements content and opal colour. (author). 10 refs., 10 figs., 3 tabs

  19. Integral finite element analysis of turntable bearing with flexible rings

    Science.gov (United States)

    Deng, Biao; Liu, Yunfei; Guo, Yuan; Tang, Shengjin; Su, Wenbin; Lei, Zhufeng; Wang, Pengcheng

    2018-03-01

    This paper suggests a method to calculate the internal load distribution and contact stress of the thrust angular contact ball turntable bearing by FEA. The influence of the stiffness of the bearing structure and the plastic deformation of contact area on the internal load distribution and contact stress of the bearing is considered. In this method, the load-deformation relationship of the rolling elements is determined by the finite element contact analysis of a single rolling element and the raceway. Based on this, the nonlinear contact between the rolling elements and the inner and outer ring raceways is same as a nonlinear compression spring and bearing integral finite element analysis model including support structure was established. The effects of structural deformation and plastic deformation on the built-in stress distribution of slewing bearing are investigated on basis of comparing the consequences of load distribution, inner and outer ring stress, contact stress and other finite element analysis results with the traditional bearing theory, which has guiding function for improving the design of slewing bearing.

  20. Dual emitter IrQ(ppy)2 for OLED applications: Synthesis and spectroscopic analysis

    International Nuclear Information System (INIS)

    Ciobotaru, I.C.; Polosan, S.; Ciobotaru, C.C.

    2014-01-01

    The synthesis of organometallic compound with iridium and two types of ligands, quinoline and phenylpyridine, was done successfully. The absorption spectra of this compound have shown broad peaks in a visible region assigned to metal-to-ligands charge transfer and in UV region assigned to intraligand absorptions. The photoluminescence spectra exhibit dual character in which the red emission is more intense than the green one. In cathodoluminescence measurements, under electron beam, the powder obtained after recrystallization from dichloromethane, shows similar behaviors with photoluminescence spectra. The cathodoluminescence images have shown a luminescent crystalline powder with triclinic structure. This compound exhibits combined vibrational modes, which proves the presence in the same molecule of both ligands. Density Functional Theory calculation was involved in order to identify the main vibrations of this compound. Highlights: • Mixed-ligand of IrQ(ppy) 2 synthesis which gives green and red phosphorescence due to the MCLT processes coming from two types of ligands. • Absorption, photoluminescence, infrared spectroscopy and cathodoluminescence measurements for characterization of IrQ(ppy) 2 organometallic compound. • Experimental results have been compared with the output files obtained from Density Functional Theory by using the Gaussian 03W software

  1. Pan-cancer analysis of somatic copy-number alterations implicates IRS4 and IGF2 in enhancer hijacking

    DEFF Research Database (Denmark)

    Weischenfeldt, Joachim Lütken; Dubash, Taronish; Drainas, Alexandros P

    2017-01-01

    overexpression resulting from CRE reorganization (e.g., enhancer hijacking) by integrating SCNAs, gene expression data and information on topologically associating domains (TADs). Analysis of 7,416 cancer genomes uncovered several pan-cancer candidate genes, including IRS4, SMARCA1 and TERT. We demonstrate...... intersecting with a TAD boundary mediate de novo formation of a 3D contact domain comprising IGF2 and a lineage-specific super-enhancer, resulting in high-level gene activation. Our framework enables systematic inference of CRE rearrangements mediating dysregulation in cancer....

  2. Elemental Study in Soybean and Products by Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Vorapot, Permnamtip; Arporn Busamongkol; Sirinart, Laoharojanaphand

    2009-07-01

    Full text: Elements were analyzed in soybean and products by Instrumental Neutron Activation Analysis (INAA), Pseudo-Cyclic Instrumental Neutron Activation Analysis (PCINAA) and Epithermal Instrumental Neutron Activation Analysis (EINAA). Elements detected in sample were include Al, Br, Ca, Cl, Cu, Fe, I, K, Mg, Mn Na, Se and Zn. The result showed that the nutritional contents changed after food processing. From experiments (n = 2), it was found that after food processing, the concentration of Cl and Na in soy bean curd increased from 0.0045 and 0.0011% to found 0.91 and 0.39 %, respectively. Other elements did not differ from soybean. Limits of detection for Al, Br, Ca, Cl, Cu, Fe, I, K, Mg, Mn Na, Se and Zn were 0.05, 0.2, 50, 6, 10, 15, 0.05, 30, 40, 5, 5, 0.05 and 1 mg.kg - 1, respectively

  3. Probabilistic finite elements for transient analysis in nonlinear continua

    Science.gov (United States)

    Liu, W. K.; Belytschko, T.; Mani, A.

    1985-01-01

    The probabilistic finite element method (PFEM), which is a combination of finite element methods and second-moment analysis, is formulated for linear and nonlinear continua with inhomogeneous random fields. Analogous to the discretization of the displacement field in finite element methods, the random field is also discretized. The formulation is simplified by transforming the correlated variables to a set of uncorrelated variables through an eigenvalue orthogonalization. Furthermore, it is shown that a reduced set of the uncorrelated variables is sufficient for the second-moment analysis. Based on the linear formulation of the PFEM, the method is then extended to transient analysis in nonlinear continua. The accuracy and efficiency of the method is demonstrated by application to a one-dimensional, elastic/plastic wave propagation problem. The moments calculated compare favorably with those obtained by Monte Carlo simulation. Also, the procedure is amenable to implementation in deterministic FEM based computer programs.

  4. Analysis of Brick Masonry Wall using Applied Element Method

    Science.gov (United States)

    Lincy Christy, D.; Madhavan Pillai, T. M.; Nagarajan, Praveen

    2018-03-01

    The Applied Element Method (AEM) is a versatile tool for structural analysis. Analysis is done by discretising the structure as in the case of Finite Element Method (FEM). In AEM, elements are connected by a set of normal and shear springs instead of nodes. AEM is extensively used for the analysis of brittle materials. Brick masonry wall can be effectively analyzed in the frame of AEM. The composite nature of masonry wall can be easily modelled using springs. The brick springs and mortar springs are assumed to be connected in series. The brick masonry wall is analyzed and failure load is determined for different loading cases. The results were used to find the best aspect ratio of brick to strengthen brick masonry wall.

  5. Ring-element analysis of layered orthotropic bodies

    DEFF Research Database (Denmark)

    Jørgensen, O.

    1993-01-01

    For the analysis of arbitrarily laminated circular bodies, a displacement-based ring-element is presented. The analysis is performed in a cylindrical coordinate system. The method of analysis requires the boundary conditions as well as the external forces to be pi-periodic. The element formulation...... accounts for a desired degree of approximation of the displacement field in the direction of the circumference. This is done by a truncated Fourier expansion of the angular dependence of the displacements in terms of trigonometric functions. Thus the Fourier expansion coefficients are the unknowns...... to that of solutions obtained by traditional 3D elements. A scheme for analytical integration of the angular dependence of the stiffness matrix is given....

  6. An improved synthesis, spectroscopic (FT-IR, NMR) study and DFT computational analysis (IR, NMR, UV-Vis, MEP diagrams, NBO, NLO, FMO) of the 1,5-methanoazocino[4,3-b]indole core structure

    Science.gov (United States)

    Uludağ, Nesimi; Serdaroğlu, Goncagül

    2018-03-01

    This study examines the synthesis of azocino[4,3-b]indole structure, which constitutes the tetracyclic framework of uleine, dasycarpidoneand tubifolidineas well as ABDE substructure of the strychnosalkaloid family. It has been synthesized by Fischer indolization of 2 and through the cylization of 4 by 2,3-dichlor-5-6-dicyanobenzoquinone (DDQ). 1H and 1C NMR chemical shifts have been predicted with GIAO approach and the calculated chemical shifts show very good agreement with observed shifts. FT-IR spectroscopy is important for the analysis of functional groups of synthesized compounds and we also supported FT-IR vibrational analysis with computational IR analysis. The vibrational spectral analysis was performed at B3LYP level of the theory in both the gas and the water phases and it was compared with the observed IR values for the important functional groups. The DFT calculations have been conducted to determine the most stable structure of the 1,2,3,4,5,6,7-Hexahydro-1,5-methanoazocino [4,3-b] indole (5). The Frontier Molecular Orbital Analysis, quantum chemical parameters, physicochemical properties have been predicted by using the same theory of level in both gas phase and the water phase, at 631 + g** and 6311++g** basis sets. TD- DFT calculations have been performed to predict the UV- Vis spectral analysis for this synthesized molecule. The Natural Bond Orbital (NBO) analysis have been performed at B3LYP level of theory to elucidate the intra-molecular interactions such as electron delocalization and conjugative interactions. NLO calculations were conducted to obtain the electric dipole moment and polarizability of the title compound.

  7. Finite Element Analysis and Design of Experiments in Engineering Design

    OpenAIRE

    Eriksson, Martin

    1999-01-01

    Projects with the objective of introducing Finite Element Analysis (FEA) into the early phases of the design process have previously been carried out at the Department of Machine Design, see e.g. the Doctoral thesis by Burman [13]. These works clearly highlight the usefulness of introducing design analysis early in the design process. According to Bjärnemo and Burman [10] the most significant advantage of applying design analysis early in the design process was the shift from verification to ...

  8. Determination of mutually interfering elements in activation analysis

    International Nuclear Information System (INIS)

    Figueiredo, A.M.G.

    1979-01-01

    The determination of the elements present in the groups scandium-zinc, mercury-selenium and arsenic-antimony-bromine represents a classical problem in thermal neutron activation analysis because the gamma-ray peaks of the radioisotopes produced from these elements by activation appear very close in the spectrum. A study is made of the possibility of simultaneous instrumental determination of these elements by means of the spectrum stripping technique, using a 400-channel analyser coupled to a Nal(Tl) detector and a 4096-channel analyser coupled to a Ge(Li) detector. Artificial mixtures of the interfering elements in varying proportions are prepared, so as to reproduce possible real samples, where the elements may be present at several concentrations. Radiochemical separation techniques for the cited elements are studied with the use of tracers. For the separation of scadium and zinc, the technique of extraction chromatography is applied. The separation of mercury and selenium is accomplished by means of ion exchange. The technique of coprecipitation is used to separate bromine from arsenic and antimony followed by ion exchange to isolate these two elements from each other. The precision and the accuracy of the results are discussed. (Author) [pt

  9. Chemical analysis of useful trace elements in sea water

    International Nuclear Information System (INIS)

    Katoh, Shunsaku; Fujii, Ayako; Miyai, Yoshitaka; Sakane, Kohji; Ogata, Noboru.

    1983-01-01

    The methods for the analysis of useful trace elements in sea water which have been tried so far are reviewed, and these methods are described briefly from the standpoint of studying the collection of resources. Ag and Au can be determined by concentrating sea water by ion-exchange method, solvent extraction method and electrodeposition method, then the elements are measured quantitatively by activation analysis and atomic absorption spectrochemical analysis. Sr, B and Li, which exist in relatively high concentration in sea water, are determined easily by atomic absorption spectrochemical analysis and absorption spectrometry. U, Mo and V are measured suitably by concentrating the elements by coprecipitation or solvent extraction method, and measuring by fluorescence analysis and arsenazo-3 method for U and through graphite-atomic absorption analysis for Mo and V. It has been revealed that the concentration of Ag and Au in sea water is extremely low, accordingly the recovery study is not conducted recently. On the other hand, the adsorption method using hydrated titanium oxide and amidoxim adsorbents for U, Mo and V, the adsorption method using aluminum adsorbent for Li, and the adsorption method using magnesium oxide and zirconium hydroxide and the solvent extraction method for B are hopeful to recover these elements. (Yoshitake, I.)

  10. Analysis of trace elements in human hair by PIXE

    International Nuclear Information System (INIS)

    Baptista, G.B.; Montenegro, E.C.; Paschoa, A.S.; Barros Leite, C.V. de.

    1980-10-01

    The PIXE method was applied to the analysis of trace elements in scalp hair using two methods for target preparation. In the first method eigth hair strands each with nearly cylindrical geommetry and approximately the same diameter were selected and placed on an aluminum frame. In the second method a given mass of hair was dissolved with nitric acid and a known amount of strontium was added to the solution and dripped on a membrane filter using a micropipet. The results for the concentrations of trace elements in hair obtained by the two methods are compared and several aspects of the analysis is discussed. (Author) [pt

  11. PIXE trace element analysis of a selection of wines

    International Nuclear Information System (INIS)

    Houdayer, A.; Hinrichsen, P.F.; Martin, J.P.; Belhadfa, A.

    1987-01-01

    The University of Montreal EN Tandem accelerator and a Si (Li) X-ray detector were used for a PIXE (Proton Induced X-ray emission) trace element analysis of a selection of wines. Quantitative measurements of the concentrations of the sixteen trace elements Na, Mg, Al, Si, P, S, Cl, K, Ca, Cr, Mn, Fe, Co, Cu, Zn, and Br were made. To optimize the sensitivity, spectra were recorded at 1.0 MeV proton energy for elements with Z 19. The absolute concentrations of the trace elements were determined by doping the samples of wine with 1000 ppm of vanadium for the 1.0 MeV bombardments, and 1000 ppm of yttrium for the 3.0 MeV irradiations. The targets were prepared by depositing a few microliters of the wine onto a Nuclepore filter

  12. Finite element analysis of rotating beams physics based interpolation

    CERN Document Server

    Ganguli, Ranjan

    2017-01-01

    This book addresses the solution of rotating beam free-vibration problems using the finite element method. It provides an introduction to the governing equation of a rotating beam, before outlining the solution procedures using Rayleigh-Ritz, Galerkin and finite element methods. The possibility of improving the convergence of finite element methods through a judicious selection of interpolation functions, which are closer to the problem physics, is also addressed. The book offers a valuable guide for students and researchers working on rotating beam problems – important engineering structures used in helicopter rotors, wind turbines, gas turbines, steam turbines and propellers – and their applications. It can also be used as a textbook for specialized graduate and professional courses on advanced applications of finite element analysis.

  13. TAPIR, Thermal Analysis of HTGR with Graphite Sleeve Fuel Elements

    International Nuclear Information System (INIS)

    Weicht, U.; Mueller, W.

    1983-01-01

    1 - Nature of the physical problem solved: Thermal analysis of a reactor core containing internally and/or externally gas cooled prismatic fuel elements of various geometries, rating, power distribution, and material properties. 2 - Method of solution: A fuel element in this programme is regarded as a sector of a fuelled annulus with graphite sleeves of any shape on either side and optional annular gaps between fuel and graphite and/or within the graphite. It may have any centre angle and the fuelled annulus may become a solid cylindrical rod. Heat generation in the fuel is assumed to be uniform over the cross section and peripheral heat flux into adjacent sectors is ignored. Fuel elements and coolant channels are treated separately, then linked together to fit a specified pattern. 3 - Restrictions on the complexity of the problem: Maxima of: 50 fuel elements; 50 cooled channels; 25 fuel geometries; 25 coolant channel geometries; 10 axial power distributions; 10 graphite conductivities

  14. Analysis of pure and malachite green doped polysulfone sample using FT-IR technique

    Science.gov (United States)

    Nayak, Rashmi J.; Khare, P. K.; Nayak, J. G.

    2018-05-01

    The sample of pure and malachite green doped Polysulfone in the form of foil was prepared by isothermal immersion technique. For the preparation of pure sample 4 gm of Polysulfone was dissolved in 50 ml of Dimethyl farmamide (DMF) solvent, while for the preparation of doped sample 10 mg, 50 mg and 100 mg Malachite Green was mixed with 4 gm of Polysulfone respectively. For the study of structural characterization of these pure and doped sample, Fourier Transform Infra-Red Spectroscopy (FT-IR) technique was used. This study shows that the intensity of transmittance decreases as the ratio of doping increases in pure polysulfone. The reduction in intensity of transmittance is clearly apparent in the present case more over the bands were broader which indicates towards charge transfer interaction between the donar and acceptor molecule.

  15. Safety Analysis Report for Primary Capsule of Ir-192 Radiation Source

    International Nuclear Information System (INIS)

    Lee, J. C.; Bang, K. S.; Choi, W. S.; Seo, K. S.; Son, K. J.; Park, W. J.

    2008-12-01

    All of the source capsules to transport a special form radioactive material should be designed and fabricated in accordance with the design criteria prescribed in IAEA standards and domestic regulations. The objective of this project is to prove the safety of a primary capsule for Ir-192 radiation source which produced in the HANARO. The safety tests of primary capsules were carried out for the impact, percussion and heat conditions. And leakage tests were carried out before and after the each tests. The capsule showed slight scratches and their deformations were not found after each tests. It also met the allowable limits of leakage rate after each test. Therefore, it has been verified that the capsule was designed and fabricated to meet all requirements for the special form radioactive materials

  16. Analysis of cosmetic residues on a single human hair by ATR FT-IR microspectroscopy

    Science.gov (United States)

    Pienpinijtham, Prompong; Thammacharoen, Chuchaat; Naranitad, Suwimol; Ekgasit, Sanong

    2018-05-01

    In this work, ATR FT-IR spectra of single human hair and cosmetic residues on hair surface are successfully collected using a homemade dome-shaped Ge μIRE accessary installed on an infrared microscope. By collecting ATR spectra of hairs from the same person, the spectral patterns are identical and superimposed while different spectral features are observed from ATR spectra of hairs collected from different persons. The spectral differences depend on individual hair characteristics, chemical treatments, and cosmetics on hair surface. The "Contact-and-Collect" technique that transfers remarkable materials on the hair surface to the tip of the Ge μIRE enables an identification of cosmetics on a single hair. Moreover, the differences between un-split and split hairs are also studied in this report. These highly specific spectral features can be employed for unique identification or for differentiation of hairs based on the molecular structures of hairs and cosmetics on hairs.

  17. Biomonitoring of air pollution through trace element analysis

    International Nuclear Information System (INIS)

    Bamford, S.A.; Osae, E.K.; Aboh, I.J.; Serfor-Armah, Y.; Nyarko, B.; Odamtten, G.T.

    1999-01-01

    Studies are being carried out to determine the potential and reliability in the use of local lichen species for biomonitoring air pollution in Ghana. The location of most of the gold mines in forest areas of the country presents the gold mining industry as a suitable setting for such investigations. The nuclear-related techniques being used in the multielement analysis of lichen samples and air filter samples are instrumental neutron activation analysis (Miniature Neutron Source Reactor) and energy dispersive x-ray fluorescence analysis (tube-excitation). Validation of the quantitative methods of the INAA through analysis of standard and certified reference materials of orchard leaves NBS SRM 1571 and BCR-CRM No. 279 gave very good results for most elements analyzed. Elemental analysis of identified lichen samples will be done beating in mind microclimatic factors, specie type and nature of soil. (author)

  18. Biomonitoring of air pollution through trace element analysis

    International Nuclear Information System (INIS)

    Bamford, S.A.; Osae, E.K.; Aboh, I. J.; Serfor-Armah, Y.; Nyarko, B.; Ofosu, F.; Odamtten, G.T.

    1999-04-01

    Studies are being carried out to determine the potential and reliability in the use of local lichen species for biomonitoring air pollution in Ghana. The location of most of the gold mines in forest areas of the country presents the gold mining industry as a suitable setting for such investigations. The nuclear-related techniques being used in the multielement analysis of lichen samples and air filter samples are instrumental neutron activation analysis (Miniature Neutron Source Reactor) and energy dispersive x-ray fluorescence analysis (tube-excitation). Validation of the quantitative methods of the INAA through analysis of standard certified reference materials of orchard leaves NBS SRM 1571 and BCR-CRM No. 279 gave very good results for most elements analyzed. Elemental analysis of identified lichen samples will be done bearing in mind microclimatic factors, specie type and nature of soil. (author)

  19. Elemental analysis of hair using PIXE-tomography and INAA

    International Nuclear Information System (INIS)

    Beasley, D.; Gomez-Morilla, I.; Spyrou, N.

    2008-01-01

    3D quantitative elemental maps of a section of a strand of hair were produced using a combination of PIXE-Tomography and simultaneous On/Off Axis STIM-Tomography at the University of Surrey Ion Beam Centre. The distributions of S, K, Cl, Ca, Fe and Zn were determined using the PIXE-T reconstruction package DISRA. The results were compared with conventional bulk PIXE analysis of tomographic data as determined using Dan32. The overall concentrations determined by PIXE were compared with elemental concentrations held in the University of Surrey Hair Database. All the entries currently in the database were produced using INAA. The merits and possible contributions of tomographic PIXE analysis to analysis of hair are discussed. The conclusions drawn from the PIXE-Tomography analysis can be used to argue for more stringent procedures for hair analysis at the University of Surrey. (author)

  20. Elemental analysis of cotton by laser-induced breakdown spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Schenk, Emily R.; Almirall, Jose R.

    2010-05-01

    Laser-induced breakdown spectroscopy (LIBS) has been applied to the elemental characterization of unprocessed cotton. This research is important in forensic and fraud detection applications to establish an elemental fingerprint of U.S. cotton by region, which can be used to determine the source of the cotton. To the best of our knowledge, this is the first report of a LIBS method for the elemental analysis of cotton. The experimental setup consists of a Nd:YAG laser that operates at the fundamental wavelength as the LIBS excitation source and an echelle spectrometer equipped with an intensified CCD camera. The relative concentrations of elements Al, Ba, Ca, Cr, Cu, Fe, Mg, and Sr from both nutrients and environmental contributions were determined by LIBS. Principal component analysis was used to visualize the differences between cotton samples based on the elemental composition by region in the U.S. Linear discriminant analysis of the LIBS data resulted in the correct classification of >97% of the cotton samples by U.S. region and >81% correct classification by state of origin.

  1. Finite element analysis of FRP-strengthened RC beams

    Directory of Open Access Journals (Sweden)

    Teeraphot Supaviriyakit

    2004-05-01

    Full Text Available This paper presents a non-linear finite element analysis of reinforced concrete beam strengthened with externally bonded FRP plates. The finite element modeling of FRP-strengthened beams is demonstrated. Concrete and reinforcing bars are modeled together as 8-node isoparametric 2D RC element. The FRP plate is modeled as 8-node isoparametric 2D elastic element. The glue is modeled as perfect compatibility by directly connecting the nodes of FRP with those of concrete since there is no failure at the glue layer. The key to the analysis is the correct material models of concrete, steel and FRP. Cracks and steel bars are modeled as smeared over the entire element. Stress-strain properties of cracked concrete consist of tensile stress model normal to crack, compressive stress model parallel to crack and shear stress model tangential to crack. Stressstrain property of reinforcement is assumed to be elastic-hardening to account for the bond between concrete and steel bars. FRP is modeled as elastic-brittle material. From the analysis, it is found that FEM can predict the load-displacement relation, ultimate load and failure mode of the beam correctly. It can also capture the cracking process for both shear-flexural peeling and end peeling modes similar to the experiment.

  2. Three dimensional finite element linear analysis of reinforced concrete structures

    International Nuclear Information System (INIS)

    Inbasakaran, M.; Pandarinathan, V.G.; Krishnamoorthy, C.S.

    1979-01-01

    A twenty noded isoparametric reinforced concrete solid element for the three dimensional linear elastic stress analysis of reinforced concrete structures is presented. The reinforcement is directly included as an integral part of the element thus facilitating discretization of the structure independent of the orientation of reinforcement. Concrete stiffness is evaluated by taking 3 x 3 x 3 Gauss integration rule and steel stiffness is evaluated numerically by considering three Gaussian points along the length of reinforcement. The numerical integration for steel stiffness necessiates the conversion of global coordiantes of the Gaussian points to nondimensional local coordinates and this is done by Newton Raphson iterative method. Subroutines for the above formulation have been developed and added to SAP and STAP routines for solving the examples. The validity of the reinforced concrete element is verified by comparison of results from finite element analysis and analytical results. It is concluded that this finite element model provides a valuable analytical tool for the three dimensional elastic stress analysis of concrete structures like beams curved in plan and nuclear containment vessels. (orig.)

  3. Qualitative PIXE analysis of mineral elements in some phytopharmaceutic drugs

    International Nuclear Information System (INIS)

    Preoteasa, E.A.; Harangus, Livia; Gugiu, M; Iordan, Andreea; Ciortea, C.

    2002-01-01

    A large number of phytopharmaceutic drugs are being developed, due to positive effects in various diseases and to high tolerance by the organism. While their medicinally active compounds have been identified, little attention has been paid to their mineral micro- and trace elements. The mineral elements in the drug may have therapeutic or toxic effects which should be properly assessed. Nuclear and atomic methods allow sensitive multielement detection and we previously performed nuclear activation analysis of some Romanian drugs made by plants. Despite this method's high sensitivity, its use is limited by the availability of a nuclear reactor. Particle-induced X-ray emission (PIXE) provides an alternative, and here we examined its potential for the analysis of mineral elements in three commercial phytopharmaceutical preparations, namely, Liv52, Mentat, and Geriforte. The PIXE measurements were performed with 3 MeV protons at the 8.5 MV NIPNE-HH tandem accelerator, using a hyper pure Ge detector, normally oriented and connected to a multichannel analyzer and to a computer; the drug pills were fixed at 45 angle with respect to the beam. In all drugs PIXE detected mineral elements with Z > 16 down to trace levels. Major elements included K, Ca, Fe, Cu, and Zn, and minor/trace amounts of S, Cl, Ti, Cr, Mn, Ni, Ga, Br, Rb, Sr, Hg, and As/Pb were detected. Some differences were seen between the three drugs. Although at trace levels Ga, As, Hg and Pb are not toxic, one should consider that their accumulation might be harmful and caution seems recommendable on long-term cure. Most of the other elements are known to exert a positive biological role, and both in major and trace levels they may contribute to the therapeutic action. Thus PIXE analysis of mineral elements in phytopharmaceutic drugs, even qualitative, is useful for evaluating the benefits and risks in the therapy. (authors)

  4. Finite element analysis of degraded concrete structures - Workshop proceedings

    International Nuclear Information System (INIS)

    1999-09-01

    This workshop is related to the finite element analysis of degraded concrete structures. It is composed of three sessions. The first session (which title is: the use of finite element analysis in safety assessments) comprises six papers which titles are: Historical Development of Concrete Finite Element Modeling for Safety Evaluation of Accident-Challenged and Aging Concrete Structures; Experience with Finite Element Methods for Safety Assessments in Switzerland; Stress State Analysis of the Ignalina NPP Confinement System; Prestressed Containment: Behaviour when Concrete Cracking is Modelled; Application of FEA for Design and Support of NPP Containment in Russia; Verification Problems of Nuclear Installations Safety Software of Strength Analysis (NISS SA). The second session (title: concrete containment structures under accident loads) comprises seven papers which titles are: Two Application Examples of Concrete Containment Structures under Accident Load Conditions Using Finite Element Analysis; What Kind of Prediction for Leak rates for Nuclear Power Plant Containments in Accidental Conditions; Influence of Different Hypotheses Used in Numerical Models for Concrete At Elevated Temperatures on the Predicted Behaviour of NPP Core Catchers Under Severe Accident Conditions; Observations on the Constitutive Modeling of Concrete Under Multi-Axial States at Elevated Temperatures; Analyses of a Reinforced Concrete Containment with Liner Corrosion Damage; Program of Containment Concrete Control During Operation for the Temelin Nuclear Power Plant; Static Limit Load of a Deteriorated Hyperbolic Cooling Tower. The third session (concrete structures under extreme environmental load) comprised five papers which titles are: Shear Transfer Mechanism of RC Plates After Cracking; Seismic Back Calculation of an Auxiliary Building of the Nuclear Power Plant Muehleberg, Switzerland; Seismic Behaviour of Slightly Reinforced Shear Wall Structures; FE Analysis of Degraded Concrete

  5. Isotope dilution inductively coupled plasma quadrupole mass spectrometry in connection with a chromatographic separation for ultra trace determinations of platinum group elements (Pt, Pd, Ru, Ir) in environmental samples.

    Science.gov (United States)

    Müller, M; Heumann, K G

    2000-09-01

    An isotope dilution inductively coupled plasma quadrupole mass spectrometric (ID-ICP-QMS) method was developed for the simultaneous determination of the platinum group elements Pt, Pd, Ru, and Ir in environmental samples. Spike solutions, enriched with the isotopes 194Pt, 108Pd, 99Ru, and 191Ir, were used for the isotope dilution step. Interfering elements were eliminated by chromatographic separation using an anion-exchange resin. Samples were dissolved with aqua regia in a high pressure asher. Additional dissolution of possible silicate portions by hydrofluoric acid was usually not necessary. Detection limits of 0.15 ng x g(-1), 0.075 ng x g(-1), and 0.015 ng x g(-1) were achieved for Pt, Pd, Ru, and Ir, respectively, using sample weights of only 0.2 g. The reliability of the ID-ICP-QMS method was demonstrated by analyzing a Canadian geological reference material and by participating in an interlaboratory study for the determination of platinum and palladium in a homogenized road dust sample. Surface soil, sampled at different distances from a highway, showed concentrations in the range of 0.1-87 ng x g(-1). An exponential decrease of the platinum and palladium concentration with increasing distance and a small anthropogenic contribution to the natural background concentration of ruthenium and iridium was found in these samples.

  6. Neutron activation analysis for bulk and trace elements in urine

    International Nuclear Information System (INIS)

    Cornelis, R.; Speecke, A.; Hoste, J.

    1975-01-01

    Problems in sampling urine for trace element analysis by neutron activation are systematically examined. Collection, storage, sample preparation and contamination hazards during irradiation are studied in detail. Three different sizes of urine samples are prepared for analysis, depending on the concentration and nuclear properties of the elements, and suitable multielement doped urine standards are used. As, Br, Ca, Cl, Co, Cr, Cs, Cu, Hg, I, K, Mg, Mn, Na, Rb, Se and Zn are determined. The extreme care given to sample collection, use of ''ultra-clean'' vials, and work in a dust-free room allows consistent values to be obtained over long periods of time. A literature review of the amounts of forty elements present in urine per day is also given

  7. Adaptive finite-element ballooning analysis of bipolar ionized fields

    International Nuclear Information System (INIS)

    Al-Hamouz, Z.M.

    1995-01-01

    This paper presents an adaptive finite-element iterative method for the analysis of the ionized field around high-voltage bipolar direct-current (HVDC) transmission line conductors without resort to Deutsch's assumption. A new iterative finite-element ballooning technique is proposed to solve Poisson's equation wherein the commonly used artificial boundary around the transmission line conductors is simulated at infinity. Unlike all attempts reported in the literature for the solution of ionized field, the constancy of the conductors' surface field at the corona onset value is directly implemented in the finite-element formulation. In order to investigate the effectiveness of the proposed method, a laboratory model was built. It has been found that the calculated V-I characteristics and the ground-plane current density agreed well with those measured experimentally. The simplicity in computer programming in addition to the low number of iterations required to achieve convergence characterize this method of analysis

  8. Analysis of Printing Substrate, Ink Age and Number of IR Drying Influence on Electrical Resistance of Conductive Inks

    Directory of Open Access Journals (Sweden)

    Josip Jerić

    2015-05-01

    Full Text Available As a result of availability of new technologies, functional printing as a segment has become one of the most interesting directions of research and development in graphic technology. Conductive inks are not a novelty and they already have broad possibilities in production of everyday products. There is still a big market for the broadening of their use, as well as a possibility of further enhancing their properties. This paper analyzes the influence of printing substrate, age of ink and the number of IR drying on the electrical resistance of the conductive inks. In the paper, subject of analysis was the change of electrical resistance in the line that was 9 cm long and 10 typographic points wide. The semi-automated screen-printing machine was used for printing. Three types of printing substrates were used; uncoated, coated and recycled paper. Two types of inks were used; newly opened ink and ink that was out of date for half year. After the printing, prints were dried using the IR dryer. Prints were dried once, and then additional three times. After the first and last drying, multimeter was used to measure electrical resistance of the lines. Analysis of the data shows that the older ink produces prints with higher electrical resistance. There are also notable differences in the electrical resistance based on the printing substrate.

  9. Contribution to the analysis of light elements using x fluorescence excited by radio-elements

    International Nuclear Information System (INIS)

    Robert, A.

    1964-01-01

    In order to study the possibilities of using radioactive sources for the X-fluorescence analysis of light elements, the principle is given, after a brief description of X-fluorescence, of the excitation of this phenomenon by X, β and α emission from radio-elements. The operation and use of the proportional gas counter for X-ray detection is described. A device has been studied for analysing the elements of the 2. and 3. periods of the Mendeleev table. It makes it possible to excite the fluorescence with a radioactive source emitting X-rays or a particles; the X-ray fluorescence penetrates into a window-less proportional counter, this being made possible by the use of an auxiliary electric field in the neighbourhood of the sample. The gas detection pressure leading to the maximum detection yield is given. The spectra are given for the K α lines of 3. period elements excited by 55 Fe, 3 H/Zr and 210 Po sources; for the 2. period the K α spectra of carbon and of fluorine excited by the α particles of 210 Po. (author) [fr

  10. Trace elements in coloured opals using neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    McOrist, G.D.; Smallwood, A. [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1996-12-31

    Neutron activation analysis (NAA) is a technique particularly suited to analysing opals since it is non-destructive and the silica matrix of opals is not prone to significant activation. It was used to determine the concentration of trace elements in 50 samples of orange, yellow, green, blue and pink opals as well as 18 samples of colourless opals taken from a number of recognised fields in Australia, Peru, Mexico and USA. The results were then evaluated to determine if a relationship existed between trace element content and opal colour. The mean concentration of most of the elements found in orange, yellow and colourless opals were similar with few exceptions. This indicated that, for these samples, colour is not related to the trace elements present. However, the trace element profile of the green, pink and blue opals was found to be significantly different with each colour having a much higher concentration of certain trace elements when compared with all other opals analysed. 7 refs.

  11. Trace elements in coloured opals using neutron activation analysis

    International Nuclear Information System (INIS)

    McOrist, G.D.; Smallwood, A.

    1996-01-01

    Neutron activation analysis (NAA) is a technique particularly suited to analysing opals since it is non-destructive and the silica matrix of opals is not prone to significant activation. It was used to determine the concentration of trace elements in 50 samples of orange, yellow, green, blue and pink opals as well as 18 samples of colourless opals taken from a number of recognised fields in Australia, Peru, Mexico and USA. The results were then evaluated to determine if a relationship existed between trace element content and opal colour. The mean concentration of most of the elements found in orange, yellow and colourless opals were similar with few exceptions. This indicated that, for these samples, colour is not related to the trace elements present. However, the trace element profile of the green, pink and blue opals was found to be significantly different with each colour having a much higher concentration of certain trace elements when compared with all other opals analysed. 7 refs

  12. Trace elements in coloured opals using neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    McOrist, G D; Smallwood, A [Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW (Australia)

    1997-12-31

    Neutron activation analysis (NAA) is a technique particularly suited to analysing opals since it is non-destructive and the silica matrix of opals is not prone to significant activation. It was used to determine the concentration of trace elements in 50 samples of orange, yellow, green, blue and pink opals as well as 18 samples of colourless opals taken from a number of recognised fields in Australia, Peru, Mexico and USA. The results were then evaluated to determine if a relationship existed between trace element content and opal colour. The mean concentration of most of the elements found in orange, yellow and colourless opals were similar with few exceptions. This indicated that, for these samples, colour is not related to the trace elements present. However, the trace element profile of the green, pink and blue opals was found to be significantly different with each colour having a much higher concentration of certain trace elements when compared with all other opals analysed. 7 refs.

  13. Nonlinear Finite Element Analysis of Pull-Out Test

    DEFF Research Database (Denmark)

    Saabye Ottesen, N

    1981-01-01

    A specific pull-out test used to determine in-situ concrete compressive strength is analyzed. This test consists of a steel disc that is extracted from the structure. The finite element analysis considers cracking as well as strain hardening and softening in the pre- and post-failure region...

  14. Trace element analysis of archaeological artefacts from Pella, Jordan

    International Nuclear Information System (INIS)

    Clayton, E.

    1985-01-01

    A brief history of the site at Pella, Jordan is presented, as a prelude to an analysis of the element composition of 82 pottery sherds. Statistical results from this data support the archaeological evidence for occupation during the Late Bronze and Early Iron Age

  15. Neutron activation analysis as an element of sculpture provenance establishing

    International Nuclear Information System (INIS)

    Panczyk, E.; Rowinska, L.; Walis, L.; Ligeza, M.; Nalepa, B.

    1998-01-01

    Investigation was carried out on the subject named ''Madonna Jackowa'' (XV cent.). The investigation object was to answer whether ''Madonna Jackowa'' was made of a native alabaster. Alabaster derived from five carious mines situated at the Cracow - Lvov line and ''Madonna Jackowa'' were analysed and the trace elements contents were compared. Instrumental neutron activation method was used for analysis of the trace. (author)

  16. Multivariate statistical analysis of major and trace element data for ...

    African Journals Online (AJOL)

    Multivariate statistical analysis of major and trace element data for niobium exploration in the peralkaline granites of the anorogenic ring-complex province of Nigeria. PO Ogunleye, EC Ike, I Garba. Abstract. No Abstract Available Journal of Mining and Geology Vol.40(2) 2004: 107-117. Full Text: EMAIL FULL TEXT EMAIL ...

  17. Microlocal methods in the analysis of the boundary element method

    DEFF Research Database (Denmark)

    Pedersen, Michael

    1993-01-01

    The application of the boundary element method in numerical analysis is based upon the use of boundary integral operators stemming from multiple layer potentials. The regularity properties of these operators are vital in the development of boundary integral equations and error estimates. We show...

  18. Three-dimensional wake field analysis by boundary element method

    International Nuclear Information System (INIS)

    Miyata, K.

    1987-01-01

    A computer code HERTPIA was developed for the calculation of electromagnetic wake fields excited by charged particles travelling through arbitrarily shaped accelerating cavities. This code solves transient wave problems for a Hertz vector. The numerical analysis is based on the boundary element method. This program is validated by comparing its results with analytical solutions in a pill-box cavity

  19. Analysis of Trace Elements in South African Clinkers using Latent ...

    African Journals Online (AJOL)

    The trace element content of clinkers (and possibly of cements) can be used to identify the manufacturing factory. The Mg, Sr, Ba, Mn, Ti, Zr, Zn and V content of clinkers give detailed information for the determination of the origin of clinkers produced in different factories. However, for the analysis of such complex data there ...

  20. GRIZ: Visualization of finite element analysis results on unstructured grids

    International Nuclear Information System (INIS)

    Dovey, D.; Loomis, M.D.

    1994-01-01

    GRIZ is a general-purpose post-processing application that supports interactive visualization of finite element analysis results on three-dimensional unstructured grids. GRIZ includes direct-to-videodisc animation capabilities and is being used as a production tool for creating engineering animations

  1. Advanced chemical analysis service for elements, radionuclides and phases

    International Nuclear Information System (INIS)

    Sansoni, B.

    1986-01-01

    A review is given on the structure, organisation and performance of the chemical analysis service of the Central Department for Chemical Analysis at the Kernforschungsanlage Juelich GmbH. The research and development programs together with the infrastructure of the Centre afford to analyse almost all stable elements of the periodical table in almost any material. The corresponding chemical analysis service has been organized according to a new modular system of analytical steps. According to this, the most complicated and, therefore, most general case of an analytical scheme for element and radionuclide analysis in any type of material can be differentiated into about 14 different steps, the modules. They are more or less independent of the special problem. The laboratory is designed and organized according to these steps. (orig./PW) [de

  2. Developments in Dynamic Analysis for quantitative PIXE true elemental imaging

    International Nuclear Information System (INIS)

    Ryan, C.G.

    2001-01-01

    Dynamic Analysis (DA) is a method for projecting quantitative major and trace element images from PIXE event data-streams (off-line or on-line) obtained using the Nuclear Microprobe. The method separates full elemental spectral signatures to produce images that strongly reject artifacts due to overlapping elements, detector effects (such as escape peaks and tailing) and background. The images are also quantitative, stored in ppm-charge units, enabling images to be directly interrogated for the concentrations of all elements in areas of the images. Recent advances in the method include the correction for changing X-ray yields due to varying sample compositions across the image area and the construction of statistical variance images. The resulting accuracy of major element concentrations extracted directly from these images is better than 3% relative as determined from comparisons with electron microprobe point analysis. These results are complemented by error estimates derived from the variance images together with detection limits. This paper provides an update of research on these issues, introduces new software designed to make DA more accessible, and illustrates the application of the method to selected geological problems.

  3. Biological reference materials and analysis of toxic elements

    Energy Technology Data Exchange (ETDEWEB)

    Subramanian, R; Sukumar, A

    1988-12-01

    Biological monitoring of toxic metal pollution in the environment requires quality control analysis with use of standard reference materials. A variety of biological tissues are increasingly used for analysis of element bioaccumulation, but the available Certified Reference Materials (CRMs) are insufficient. An attempt is made to review the studies made using biological reference materials for animal and human tissues. The need to have inter-laboratory studies and CRM in the field of biological monitoring of toxic metals is also discussed.

  4. Combining FT-IR spectroscopy and multivariate analysis for qualitative and quantitative analysis of the cell wall composition changes during apples development.

    Science.gov (United States)

    Szymanska-Chargot, M; Chylinska, M; Kruk, B; Zdunek, A

    2015-01-22

    The aim of this work was to quantitatively and qualitatively determine the composition of the cell wall material from apples during development by means of Fourier transform infrared (FT-IR) spectroscopy. The FT-IR region of 1500-800 cm(-1), containing characteristic bands for galacturonic acid, hemicellulose and cellulose, was examined using principal component analysis (PCA), k-means clustering and partial least squares (PLS). The samples were differentiated by development stage and cultivar using PCA and k-means clustering. PLS calibration models for galacturonic acid, hemicellulose and cellulose content from FT-IR spectra were developed and validated with the reference data. PLS models were tested using the root-mean-square errors of cross-validation for contents of galacturonic acid, hemicellulose and cellulose which was 8.30 mg/g, 4.08% and 1.74%, respectively. It was proven that FT-IR spectroscopy combined with chemometric methods has potential for fast and reliable determination of the main constituents of fruit cell walls. Copyright © 2014 Elsevier Ltd. All rights reserved.

  5. Piezoelectric Analysis of Saw Sensor Using Finite Element Method

    Directory of Open Access Journals (Sweden)

    Vladimír KUTIŠ

    2013-06-01

    Full Text Available In this contribution modeling and simulation of surface acoustic waves (SAW sensor using finite element method will be presented. SAW sensor is made from piezoelectric GaN layer and SiC substrate. Two different analysis types are investigated - modal and transient. Both analyses are only 2D. The goal of modal analysis, is to determine the eigenfrequency of SAW, which is used in following transient analysis. In transient analysis, wave propagation in SAW sensor is investigated. Both analyses were performed using FEM code ANSYS.

  6. Analysis of Tire Tractive Performance on Deformable Terrain by Finite Element-Discrete Element Method

    Science.gov (United States)

    Nakashima, Hiroshi; Takatsu, Yuzuru

    The goal of this study is to develop a practical and fast simulation tool for soil-tire interaction analysis, where finite element method (FEM) and discrete element method (DEM) are coupled together, and which can be realized on a desktop PC. We have extended our formerly proposed dynamic FE-DE method (FE-DEM) to include practical soil-tire system interaction, where not only the vertical sinkage of a tire, but also the travel of a driven tire was considered. Numerical simulation by FE-DEM is stable, and the relationships between variables, such as load-sinkage and sinkage-travel distance, and the gross tractive effort and running resistance characteristics, are obtained. Moreover, the simulation result is accurate enough to predict the maximum drawbar pull for a given tire, once the appropriate parameter values are provided. Therefore, the developed FE-DEM program can be applied with sufficient accuracy to interaction problems in soil-tire systems.

  7. Development of a diamond waveguide sensor for sensitive protein analysis using IR quantum cascade lasers

    Science.gov (United States)

    Piron, P.; Vargas Catalan, E.; Haas, J.; Österlund, L.; Nikolajeff, F.; Andersson, P. O.; Bergström, J.; Mizaikoff, B.; Karlsson, M.

    2018-02-01

    Microfabricated diamond waveguides, between 5 and 20 μm thick, manufactured by chemical vapor deposition of diamond, followed by standard lithographic techniques and inductively coupled plasma etching of diamond, are used as bio-chemical sensors in the mid infrared domain: 5-11 μm. Infrared light, emitted from a broadly tunable quantum cascade laser with a wavelength resolution smaller than 20 nm, is coupled through the diamond waveguides for attenuated total reflection spectroscopy. The expected advantages of these waveguides are a high sensitivity due to the high number of internal reflections along the propagation direction, a high transmittance in the mid-IR domain, the bio-compatibility of diamond and the possibility of functionalizing the surface layer. The sensor will be used for analyzing different forms of proteins such as α-synuclein which is relevant in understanding the mechanism behind Parkinson's disease. The fabrication process of the waveguide, its characteristics and several geometries are introduced. The optical setup of the biosensor is described and our first measurements on two analytes to demonstrate the principle of the sensing method will be presented. Future use of this sensor includes the functionalization of the diamond waveguide sensor surface to be able to fish out alpha-synuclein from cerebrospinal fluid.

  8. Analysis of cosmetic residues on a single human hair by ATR FT-IR microspectroscopy.

    Science.gov (United States)

    Pienpinijtham, Prompong; Thammacharoen, Chuchaat; Naranitad, Suwimol; Ekgasit, Sanong

    2018-05-15

    In this work, ATR FT-IR spectra of single human hair and cosmetic residues on hair surface are successfully collected using a homemade dome-shaped Ge μIRE accessary installed on an infrared microscope. By collecting ATR spectra of hairs from the same person, the spectral patterns are identical and superimposed while different spectral features are observed from ATR spectra of hairs collected from different persons. The spectral differences depend on individual hair characteristics, chemical treatments, and cosmetics on hair surface. The "Contact-and-Collect" technique that transfers remarkable materials on the hair surface to the tip of the Ge μIRE enables an identification of cosmetics on a single hair. Moreover, the differences between un-split and split hairs are also studied in this report. These highly specific spectral features can be employed for unique identification or for differentiation of hairs based on the molecular structures of hairs and cosmetics on hairs. Copyright © 2018 Elsevier B.V. All rights reserved.

  9. Elemental characterization of Brazilian beans using neutron activation analysis

    International Nuclear Information System (INIS)

    Lilian Seiko Kato; Nadai Fernandes, E.A. De; Marcio Arruda Bacchi; Gabriel Adrian Sarries; Andres Enrique Lai Reyes

    2015-01-01

    Beans are important for many developing countries as a source of protein and mineral nutrients. Here, ten commercial types of Brazilian beans, from the species Phaseolus vulgaris (common beans) and Vigna unguiculata (cowpeas), were analyzed by neutron activation analysis for the determination of Br, Ca, Co, Cs, Fe, K, Mo, Na, Rb, Sc and Zn. There were statistical differences (p/0.05) amongst the commercial types, except for Br, Rb and Sc. In general, non-essential elements showed high variability, indicating that the origin of beans had a strong influence on the mass fraction of such elements. (author)

  10. Fast XRF analysis of mineral elements in dental composites

    International Nuclear Information System (INIS)

    Preoteasa, E. A.; Constantinescu, B.; Preoteasa, E.

    2001-01-01

    Dental composites, made of particles of glass, ceramics or quartz embedded in an organic polymer matrix, extensively replaced silver amalgam in tooth fillings and enabled new applications for restorative dentistry. Long-term alteration of dental fillings together with market pressure motivates the development of composites at a high rate, largely by progress of materials forming their mineral phase. Therefore, dental composites constantly bring at the interface with enamel and dentine new elements foreign to the organism, whose biological action has not been studied. Atomic and nuclear methods for surface multielemental analysis have been used in dental research but not for composites. X-ray fluorescence (XRF) is suited for the fast microanalytical screening of the elements and of their changes at the biomaterial's surface. The potential of radioisotope-excited XRF for the analysis of dental composites has been examined. Flat disk-shaped samples of composites have been prepared and polymerized chemically or by irradiation with intense 420-500 nm light. The measurements were performed with a spectrometric chain containing a 30 mCi source of 241 Am, a Si(Li) detector, and a multichannel analyzer. The spectra were built up for 2000-6000 sec. The characteristic X lines were integrated and normalized to source lines. The following Z ≥ 20 elements were detected in the studied composites: Ba only in Charisma (Kulzer) and Pekafill (Bayer); Zr, Ba, Yb in Tetric Ceram, and Ca, Ba, Yb together with traces of possibly Ti and Fe in Ariston (both from Vivadent); Zr, Hf in Valux Plus (3M Dental); and Sr, Ba together with some trace element, seemingly Cu, in F2000 Compomer (3M Dental) and with other trace elements like Ca, Fe in Surefil (Dentsply). Among older materials, Concise (3M Dental) contained only light (Z 3 that releases F for protection of enamel and dentine. Yb, Zr, Ba, Hf improve the radiological opacity of the materials. Some elements may accompany others as

  11. Analytical and statistical analysis of elemental composition of lichens

    International Nuclear Information System (INIS)

    Calvelo, S.; Baccala, N.; Bubach, D.; Arribere, M.A.; Riberio Guevara, S.

    1997-01-01

    The elemental composition of lichens from remote southern South America regions has been studied with analytical and statistical techniques to determine if the values obtained reflect species, growth forms or habitat characteristics. The enrichment factors are calculated discriminated by species and collection site and compared with data available in the literature. The elemental concentrations are standardized and compared for different species. The information was statistically processed, a cluster analysis was performed using the three first principal axes of the PCA; the three groups formed are presented. Their relationship with the species, collection sites and the lichen growth forms are interpreted. (author)

  12. Finite elements for non-linear analysis of pipelines

    International Nuclear Information System (INIS)

    Benjamim, A.C.; Ebecken, N.F.F.

    1982-01-01

    The application of a three-dimensional lagrangian formulation for the great dislocations analysis and great rotation of pipelines systems is studied. This formulation is derived from the soil mechanics and take into account the shear stress effects. Two finite element models are implemented. The first, of right axis, uses as interpolation functions the conventional gantry functions, defined in relation to mobile coordinates. The second, of curve axis and variable cross sections, is obtained from the degeneration of the three-dimensional isoparametric element, and uses as interpolation functions third degree polynomials. (E.G.) [pt

  13. Trace element analysis in rheumatoid arthritis under chrysotherapy

    International Nuclear Information System (INIS)

    Lecomte, R.; Paradis, P.; Monaro, S.; Barrette, M.; Lamoureux, G.; Menard, H.A.

    1981-01-01

    Proton induced X-ray emission (PIXE) analysis is used to measure trace element concentrations in blood serum from patients with rheumatoid arthritis. Initially trace element contaminations in blood-collecting and storing devices are determined. Then mean values and nyctemeral cycles are measured both in normal subjects and patients with rheumatoid arthritis and other similar pathologies. Abnormal concentrations of Cu and Zn and anomalies in the nyctemeral cycle are found in the patients. In the second phase of the project, the special case of chrysotherapeutically treated (gold salt treatment) rheumatoid arthritis patients is studied for extended periods of time (up to 53 weeks). (orig.)

  14. Analysis of Piezoelectric Solids using Finite Element Method

    Science.gov (United States)

    Aslam, Mohammed; Nagarajan, Praveen; Remanan, Mini

    2018-03-01

    Piezoelectric materials are extensively used in smart structures as sensors and actuators. In this paper, static analysis of three piezoelectric solids is done using general-purpose finite element software, Abaqus. The simulation results from Abaqus are compared with the results obtained using numerical methods like Boundary Element Method (BEM) and meshless point collocation method (PCM). The BEM and PCM are cumbersome for complex shape and complicated boundary conditions. This paper shows that the software Abaqus can be used to solve the governing equations of piezoelectric solids in a much simpler and faster way than the BEM and PCM.

  15. Stress analysis of heated concrete using finite elements

    International Nuclear Information System (INIS)

    Majumdar, P.; Gupta, A.; Marchertas, A.

    1994-01-01

    Described is a finite element analysis of concrete, which is subjected to rapid heating. Using thermal mass transport calculation, the moisture content, temperature and pore pressure distribution over space and time is obtained first. From these effects, stress at various points of the concrete are computed using the finite element method. Contribution to the stress formulation comes from three components, namely the thermal expansion, pore pressure, and the shrinkage of concrete due to moisture loss (from dehydration). The material properties of concrete are assumed to be homogeneous, elastic, and cracking is not taken into consideration. (orig.)

  16. Fourier analysis of finite element preconditioned collocation schemes

    Science.gov (United States)

    Deville, Michel O.; Mund, Ernest H.

    1990-01-01

    The spectrum of the iteration operator of some finite element preconditioned Fourier collocation schemes is investigated. The first part of the paper analyses one-dimensional elliptic and hyperbolic model problems and the advection-diffusion equation. Analytical expressions of the eigenvalues are obtained with use of symbolic computation. The second part of the paper considers the set of one-dimensional differential equations resulting from Fourier analysis (in the tranverse direction) of the 2-D Stokes problem. All results agree with previous conclusions on the numerical efficiency of finite element preconditioning schemes.

  17. Finite element analysis of structures through unified formulation

    CERN Document Server

    Carrera, Erasmo; Petrolo, Marco; Zappino, Enrico

    2014-01-01

    The finite element method (FEM) is a computational tool widely used to design and analyse  complex structures. Currently, there are a number of different approaches to analysis using the FEM that vary according to the type of structure being analysed: beams and plates may use 1D or 2D approaches, shells and solids 2D or 3D approaches, and methods that work for one structure are typically not optimized to work for another. Finite Element Analysis of Structures Through Unified Formulation deals with the FEM used for the analysis of the mechanics of structures in the case of linear elasticity. The novelty of this book is that the finite elements (FEs) are formulated on the basis of a class of theories of structures known as the Carrera Unified Formulation (CUF). It formulates 1D, 2D and 3D FEs on the basis of the same ''fundamental nucleus'' that comes from geometrical relations and Hooke''s law, and presents both 1D and 2D refined FEs that only have displacement variables as in 3D elements. It also covers 1D...

  18. Analysis of IRS-1-mediated phosphatidylinositol 3-kinase activation in the adipose tissue of polycystic ovary syndrome patients complicated with insulin resistance

    Energy Technology Data Exchange (ETDEWEB)

    Yongli, Chu [Yantai Yuhuangding Hospital, Yantai (China). Dept. of Obstetrics and Gynecology; Hongyu, Qiu; Yongyu, Sun; Min, Li; Hongfa, Li

    2004-04-01

    Objective: To investigate the insulin receptor substance-1 (IRS-1)-mediated phosphatidylinositol-3 (PI-3) kinase activity in adipose tissue of polycystic ovary syndrome (PCOS) patients, and to explore molecular mechanisms of insulin resistance of PCOS. Methods: Blood and adipose tissue samples from patients with PCOS with insulin resistance (n=19), PCOS without insulin resistance (n=10) and controls (n=15) were collected. Serum luteinizing hormone (LH), follicle stimulating hormone (FSH), testosterone (T) were measured by chemiluminescence assay. Fasting insulin (FIN) was measured by radioimmunoassay. Fasting plasma glucose (FPG) was measured by oxidase assay. Insulin resistance index (IR) was calculated using homeostasis model assessment (HOMA) to analyze the relationship between these markers and insulin resistance. The tyrosine phosphorylation of IRS-1 was measured by immunoprecipitation and enhanced chemiluminescent immunoblotting technique. PI-3 kinase activity was detected by immunoprecipitation, thin-layer chromatography and gamma scintillation counting. The results were analyzed by statistical methods. Results: 1) The levels of serum LH, LH/FSH, T, FIN and HOMA-IR in PCOS without insulin resistance were significantly higher than those of control group (all P<0.05); the levels of serum LH, LH/FSH, T, FIN and HOMA-IR in PCOS with insulin resistance were significantly higher than those of PCOS without insulin resistance (all P<0.05). 2) The tyrosine phosphorylation analysis of IRS-1 showed that IRS-1 tyrosine phosphorylation was significantly decreased in PCOS with insulin resistance compared to that of PCOS without insulin resistance and control groups (P<0.01). 3) PI-3 kinase activity was significantly decreased (P<0.01) and negatively correlated with HOMA-IR. Conclusion: In consequence of the weaker signal caused by the change of upper stream signal molecule IRS-1 tyrosine phosphorylation, PI-3 kinase activity decreased, it affects the insulin signal

  19. Analysis of IRS-1-mediated phosphatidylinositol 3-kinase activation in the adipose tissue of polycystic ovary syndrome patients complicated with insulin resistance

    International Nuclear Information System (INIS)

    Chu Yongli; Qiu Hongyu; Sun Yongyu; Li Min; Li Hongfa

    2004-01-01

    Objective: To investigate the insulin receptor substance-1 (IRS-1)-mediated phosphatidylinositol-3 (PI-3) kinase activity in adipose tissue of polycystic ovary syndrome (PCOS) patients, and to explore molecular mechanisms of insulin resistance of PCOS. Methods: Blood and adipose tissue samples from patients with PCOS with insulin resistance (n=19), PCOS without insulin resistance (n=10) and controls (n=15) were collected. Serum luteinizing hormone (LH), follicle stimulating hormone (FSH), testosterone (T) were measured by chemiluminescence assay. Fasting insulin (FIN) was measured by radioimmunoassay. Fasting plasma glucose (FPG) was measured by oxidase assay. Insulin resistance index (IR) was calculated using homeostasis model assessment (HOMA) to analyze the relationship between these markers and insulin resistance. The tyrosine phosphorylation of IRS-1 was measured by immunoprecipitation and enhanced chemiluminescent immunoblotting technique. PI-3 kinase activity was detected by immunoprecipitation, thin-layer chromatography and gamma scintillation counting. The results were analyzed by statistical methods. Results: 1) The levels of serum LH, LH/FSH, T, FIN and HOMA-IR in PCOS without insulin resistance were significantly higher than those of control group (all P<0.05); the levels of serum LH, LH/FSH, T, FIN and HOMA-IR in PCOS with insulin resistance were significantly higher than those of PCOS without insulin resistance (all P<0.05). 2) The tyrosine phosphorylation analysis of IRS-1 showed that IRS-1 tyrosine phosphorylation was significantly decreased in PCOS with insulin resistance compared to that of PCOS without insulin resistance and control groups (P<0.01). 3) PI-3 kinase activity was significantly decreased (P<0.01) and negatively correlated with HOMA-IR. Conclusion: In consequence of the weaker signal caused by the change of upper stream signal molecule IRS-1 tyrosine phosphorylation, PI-3 kinase activity decreased, it affects the insulin signal

  20. Temperature-dependent IR-transition moment orientational analysis applied to thin supported films of poly-ε-caprolactone.

    Science.gov (United States)

    Kossack, Wilhelm; Schulz, Martha; Thurn-Albrecht, Thomas; Reinmuth, Jörg; Skokow, Viktor; Kremer, Friedrich

    2017-12-13

    A novel experimental setup is described which enables one to carry out infrared transition moment orientational analysis (IR-TMOA) depending on temperature. By this, three dimensional molecular order parameter tensors of IR-active transition dipole moments with respect to the sample coordinate system can be determined in their thermal evolution (35 °C < T < 59 °C). As an example crystallinity and macroscopic order of poly-ε-caprolcatone are monitored. Both remain largely unaltered up to T ∼ 50 °C, above which they decrease. These reductions are explained as the melting of flat-on crystalline lamellae that make up about 34% of the crystalline material. The remaining crystallites are arranged into bulk-like, confined spherulitic structures and do not melt by more than (3 ± 3)%. Therefore, flat-on oriented lamellae are supposed to be kinetically favored by confinement during melt crystallization but are thermodynamically less stable than two-dimensionally confined bulk-like spherulites.

  1. Sample preparation procedure for PIXE elemental analysis on soft tissues

    International Nuclear Information System (INIS)

    Kubica, B.; Kwiatek, W.M.; Dutkiewicz, E.M.; Lekka, M.

    1997-01-01

    Trace element analysis is one of the most important field in analytical chemistry. There are several instrumental techniques which are applied for determinations of microscopic elemental content. The PIXE (Proton Induced X-ray Emission) technique is one of the nuclear techniques that is commonly applied for such purpose due to its multielemental analysis possibilities. The aim of this study was to establish the optimal conditions for target preparation procedure. In this paper two different approaches to the topic are presented and widely discussed. The first approach was the traditional pellet technique and the second one was mineralization procedure. For the analysis soft tissue such as liver was used. Some results are also presented on water samples. (author)

  2. OXYGEN PRESSURE REGULATOR DESIGN AND ANALYSIS THROUGH FINITE ELEMENT MODELING

    Directory of Open Access Journals (Sweden)

    Asterios KOSMARAS

    2017-05-01

    Full Text Available Oxygen production centers produce oxygen in high pressure that needs to be defused. A regulator is designed and analyzed in the current paper for medical use in oxygen production centers. This study aims to design a new oxygen pressure regulator and perform an analysis using Finite Element Modeling in order to evaluate its working principle. In the design procedure,the main elements and the operating principles of a pressure regulator are taking into account. The regulator is designed and simulations take place in order to assessthe proposed design. Stress analysis results are presented for the main body of the regulator, as well as, flow analysis to determine some important flow characteristics in the inlet and outlet of the regulator.

  3. Finite Element Residual Stress Analysis of Planetary Gear Tooth

    Directory of Open Access Journals (Sweden)

    Jungang Wang

    2013-01-01

    Full Text Available A method to simulate residual stress field of planetary gear is proposed. In this method, the finite element model of planetary gear is established and divided to tooth zone and profile zone, whose different temperature field is set. The gear's residual stress simulation is realized by the thermal compression stress generated by the temperature difference. Based on the simulation, the finite element model of planetary gear train is established, the dynamic meshing process is simulated, and influence of residual stress on equivalent stress of addendum, pitch circle, and dedendum of internal and external meshing planetary gear tooth profile is analyzed, according to non-linear contact theory, thermodynamic theory, and finite element theory. The results show that the equivalent stresses of planetary gear at both meshing and nonmeshing surface are significantly and differently reduced by residual stress. The study benefits fatigue cracking analysis and dynamic optimization design of planetary gear train.

  4. Probabilistic finite elements for fracture and fatigue analysis

    Science.gov (United States)

    Liu, W. K.; Belytschko, T.; Lawrence, M.; Besterfield, G. H.

    1989-01-01

    The fusion of the probabilistic finite element method (PFEM) and reliability analysis for probabilistic fracture mechanics (PFM) is presented. A comprehensive method for determining the probability of fatigue failure for curved crack growth was developed. The criterion for failure or performance function is stated as: the fatigue life of a component must exceed the service life of the component; otherwise failure will occur. An enriched element that has the near-crack-tip singular strain field embedded in the element is used to formulate the equilibrium equation and solve for the stress intensity factors at the crack-tip. Performance and accuracy of the method is demonstrated on a classical mode 1 fatigue problem.

  5. Trace elemental analysis of the aerosol particulates in northern Punjab

    International Nuclear Information System (INIS)

    Iqbal, M.Z.

    2002-01-01

    Trace elemental analysis of the aerosol particulates was studied in the atmosphere of Lahore, Faisalabad, Islamabad, Sheikhupura, Wah Cantt. And Khanispur. The amount of the aerosol particulates in the above mentioned areas was compared to the U.S. EPA maximum permissible limits. Scavenging mechanism of the aerosol particulates through precipitation was studied in the atmosphere of Lahore and Sheikhupura by using HPLC and ICP-AES techniques. The site distribution and morphological structure of the aerosol particulates was studied by using Scanning Electron Microscope model JSM-35CF. Trace elemental composition of the aerosol particulates in the atmosphere of the selected areas of Pakistan was carried out by using NAA. The elements thus studied were Ce, Yb, Se, Cr, Hf, Cs, Sc, Fe, Co, Eu, Sb, Mo, Ba, Zn, Hg, Br, Na, Gd, Sm, Nd and In while Pb and Cd were estimated by using ASS technique. (author)

  6. Investigation on trace elements in crude oil and organic matter extracted from rocks with instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Ding Zuguo; Chai Zhifang

    1990-01-01

    Solvent extraction, column chromatography and instrumental neutron activation analysis(INAA) have been used to investigate the trace elements in crude oil, organic matter extracted from rocks and their related fractions. With these methods, about 70 crude oil samples from eight different oil fields in China and 6 extracted asphaltene samples of the lower paleozoic from the upper Yangtze region have been analyzed, and about 40 elements of interest have been determined. Those elements include Al, As, Au, Ba, Br, Cl, Co, Cr, Cs, Cu, Fe, Hf, I, Ir, Mg, Mn, Mo, Na, Ni, Rb, Re, S, Sb, Sc, Se, Sr, Th, Zn, V and parts of REE. The experimental results show that the method possesses several advantages, i.e. non-destructive, multi-elements, sensitive, precise and accurate. Without ashing samples, the loss of volatile elements such as Cl, S, Se and Sb are avoided. The column chromatography makes it possible to study the distributions of trace elements in different fractions of crude oil and organic matter extracted. Meanwhile, the characters of trace elements in them have also been discussed

  7. Elemental misinterpretation in automated analysis of LIBS spectra.

    Science.gov (United States)

    Hübert, Waldemar; Ankerhold, Georg

    2011-07-01

    In this work, the Stark effect is shown to be mainly responsible for wrong elemental allocation by automated laser-induced breakdown spectroscopy (LIBS) software solutions. Due to broadening and shift of an elemental emission line affected by the Stark effect, its measured spectral position might interfere with the line position of several other elements. The micro-plasma is generated by focusing a frequency-doubled 200 mJ pulsed Nd/YAG laser on an aluminum target and furthermore on a brass sample in air at atmospheric pressure. After laser pulse excitation, we have measured the temporal evolution of the Al(II) ion line at 281.6 nm (4s(1)S-3p(1)P) during the decay of the laser-induced plasma. Depending on laser pulse power, the center of the measured line is red-shifted by 130 pm (490 GHz) with respect to the exact line position. In this case, the well-known spectral line positions of two moderate and strong lines of other elements coincide with the actual shifted position of the Al(II) line. Consequently, a time-resolving software analysis can lead to an elemental misinterpretation. To avoid a wrong interpretation of LIBS spectra in automated analysis software for a given LIBS system, we recommend using larger gate delays incorporating Stark broadening parameters and using a range of tolerance, which is non-symmetric around the measured line center. These suggestions may help to improve time-resolving LIBS software promising a smaller probability of wrong elemental identification and making LIBS more attractive for industrial applications.

  8. Nonlinear Finite Element Analysis of Reinforced Concrete Shells

    Directory of Open Access Journals (Sweden)

    Mustafa K. Ahmed

    2013-05-01

    Full Text Available This investigation is to develop a numerical model suitable for nonlinear analysis of reinforced concrete shells. A nine-node Lagrangian element Figure (1 with enhanced shear interpolation will be used in this study. Table (1 describes shape functions and their derivatives of this element.An assumed transverse shear strain is used in the formulation of this element to overcome shear locking. Degenerated quadratic thick plate elements employing a layered discrelization through the thickness will be adopted. Different numbers of layers for different thickness can be used per element. A number of layers between (6 and 10 have proved to be appropriate to represent the nonlinear material behavior in structures. In this research 8 layers will be adequate. Material nonlinearities due to cracking of concrete, plastic flow or crushing of concrete in compression and yield condition of reinforcing steel are considered. The maximum tensile strength is used as a criterion for crack initiation. Attention is given to the tension stiffening phenomenon and the degrading effect of cracking on the compressive and shear strength of concrete. Perfect bond between concrete and steel is assumed. Attention is given also to geometric nonlinearities. An example have been chosen in order to demonstrate the suitability of the models by comparing the predicted behaviour with the experimental results for shell exhibiting various modes of failure.

  9. Finite element elastic-plastic analysis of LMFBR components

    International Nuclear Information System (INIS)

    Levy, A.; Pifko, A.; Armen, H. Jr.

    1978-01-01

    The present effort involves the development of computationally efficient finite element methods for accurately predicting the isothermal elastic-plastic three-dimensional response of thick and thin shell structures subjected to mechanical and thermal loads. This work will be used as the basis for further development of analytical tools to be used to verify the structural integrity of liquid metal fast breeder reactor (LMFBR) components. The methods presented here have been implemented into the three-dimensional solid element module (HEX) of the Grumman PLANS finite element program. These methods include the use of optimal stress points as well as a variable number of stress points within an element. This allows monitoring the stress history at many points within an element and hence provides an accurate representation of the elastic-plastic boundary using a minimum number of degrees of freedom. Also included is an improved thermal stress analysis capability in which the temperature variation and corresponding thermal strain variation are represented by the same functional form as the displacement variation. Various problems are used to demonstrate these improved capabilities. (Auth.)

  10. Medical and health-related trace element analysis by TXRF

    International Nuclear Information System (INIS)

    Greaves, E.D.

    2000-01-01

    The advantages offered with TXRF analysis by direct irradiation with monochromatic X-rays of tissue homogenates and body fluids make the technique appropriate for a number of medical and health related applications. The ability to detect low levels of toxic heavy elements is being used as an aid in accidental poisoning diagnosis and treatment, in treatment-induced toxicity control and as an accessory in medical and health research. Thus lead-in-whole-blood analysis is used in confirmation of diagnosis of victims of poisoning, or monitoring the evolution and efficiency of the clinical treatment. Measurement and control of plasma platinum levels of cancer patients undergoing chemotherapy with Pt-containing drugs includes: establishment of the drug level-tumor remission response, measurement of Pt plasma level curves and establishment of optimum dosage to minimize the nephrotoxicity of platinum, and bioequivalence comparisons of different commercially available platinum containing anticancer drugs. Analysis as an aid in clinical research applications includes: trace element determination of amniotic fluid in fetus malformation studies; analysis of brain specimens and cerebrospinal fluid in diagnosis of central nervous system disorders; the influence of trace elements in cataract genesis and the influence of heavy elements in semen quality in human reproduction studies. Human body samples require the use of monochromatized beams of x-rays in order to derive the special advantage of its use: i) The reduction in the spectrum background allowing direct irradiation of organic matter specimens. Hence human tissue and body fluids are prepared by simple procedures involving dilution, homogenization and standard addition avoiding the need for specimen digestion. This results in faster, cheaper methods that decrease sample contamination problems. ii) The presence of a large Compton scattered signal in the spectrum and its use as an internal standard reference allows further

  11. PHARMACOPOEIA METHODS FOR ELEMENTAL ANALYSIS OF MEDICINES: A COMPARATIVE STUDY

    Directory of Open Access Journals (Sweden)

    Tetiana M. Derkach

    2018-01-01

    Full Text Available The article is devoted to the problem of quality assurance of medicinal products, namely the determination of elemental impurity concentration compared to permitted daily exposures for and the correct choice analytical methods that are adequate to the formulated tasks. The paper goal is to compare characteristics of four analytical methods recommended by the Pharmacopoeia of various countries to control the content of elemental impurities in medicines, including medicinal plant raw materials and herbal medicines. Both advantages and disadvantages were described for atomic absorption spectroscopy with various atomising techniques, as well as atomic emission spectroscopy and mass spectrometry with inductively coupled plasma. The choice of the most rational analysis method depends on a research task and is reasoned from the viewpoint of analytical objectives, possible complications, performance attributes, and economic considerations. The methods of ICP-MS and GFAAS were shown to provide the greatest potential for determining the low and ultra-low concentrations of chemical elements in medicinal plants and herbal medicinal products. The other two methods, FAAS and ICP-AES, are limited to the analysis of the main essential elements and the largest impurities. The ICP-MS is the most efficient method for determining ultra-low concentrations. However, the interference of mass peaks is typical for ICP-MS. It is formed not only by impurities but also by polyatomic ions with the participation of argon, as well as atoms of gases from the air (C, N and O or matrices (O, N, H, P, S and Cl. Therefore, a correct sample preparation, which guarantees minimisation of impurity contamination and loss of analytes becomes the most crucial stage of analytical applications of ICP-MS. The detections limits for some chemical elements, which content is regulated in modern Pharmacopoeia, were estimated for each method and analysis conditions of medicinal plant raw

  12. Qualitative PIXE analysis of mineral elements in some dental composites

    International Nuclear Information System (INIS)

    Preoteasa, E.A.; Iordan, Andreea; Harangus, Livia; Ciortea, C.; Gugiu, M.; Moldovan, Maria

    2002-01-01

    Dental composites, made by particles of glass, ceramics and quartz embedded in an organic polymer, develop at a high rate. However, commercial composites are expensive and recently the 'Restacril' biomaterials company became prepared to offer a low-cost alternative. The durability of dental fillings depends not only on biomaterial's gross chemical composition, but also on impurities. These may influence the chemical, mechanical and surface properties of the inorganic particles and modify the composites' clinical behavior. Thus elemental analysis is necessary to improve the biomaterials' quality. Nuclear and atomic methods allow sensitive multielement detection, and we previously analyzed some commercial composites by particle-induced X-ray emission (PIXE). Here we applied PIXE in the qualitative analysis of six new Romanian biomaterials, aiming to compare their nominal and detected composition and paying attention to the impurities. The PIXE measurements were performed with 3 MeV protons at the 8.5 MV NIPNE-HH tandem accelerator, using a hyper pure Ge detector, normal to the beam and connected to a multichannel analyzer and to a computer. Solid samples of composites with a flat surface were fixed at 45 angle, absorber foil of Al 30 mm thick was used, and integration of beam current was done. In all composites PIXE detected mineral elements with Z > 19 down to trace levels. All major nominal elements with Z > 20 - Ca, Sr, Zr, Ba, and Yb - were detected by PIXE. In addition, many minor and trace elements absent from the nominal formulations were seen, including K, Ti, Mn, Fe, Ni, Cu, Zn, Ga, Ag, Cd, Hf, and As/Pb. Such impurities may come from rough materials and preparative technologies. The impurities in Romanian composites are comparable to those in some commercial biomaterials but higher than in other ones. Thus PIXE analysis of mineral elements in Romanian composites, even qualitative, appears useful for quality control and improvement. (authors)

  13. XRF analysis of portland cement for major and trace elements

    International Nuclear Information System (INIS)

    Abdunnabi, A. R.

    2012-12-01

    Libyan portland cement produced in several factories around the country, in Lip tis, Zoltan, Souq-Elkamis, Dernah and El-Fatach, were analyzed for quantitative major and trace elements and mineral content, which were compered with those imported from Spain, Romania, Cyprus, and Egypt. X-ray fluorescence spectro X lab 2000 spectrometer equipped with Rh-and X-ray tube was used for the analysis of various samples. The detector Si(Li) with a resolution of 148 eV at Mn K-a=5.9 keV facilitates the determination of a wide range of elements from sodium to uranium, with a detection limit at sub levels. Cement samples in the powder form were analyzed using the pellet-technique. The pellets were prepared by mixing 4g of the cement powder with 0.9 g of binder (HWC) and pressed at high pressure. A ful analysis including, background counting, matrix correction and all relevant corrections were achieved automatically by XLAB 2000 software package. For major and trace elements X RF results were higher for most of the elements than those analyzed with atomic absorption spectrometry. The mineral content showed that Libyan cement is comparable to the imported ones, also the Libyan cement meets the requirements of the international specifications of the portland cement. (Author)

  14. Electromagnetic analysis of control element drive mechanism for KSNP

    International Nuclear Information System (INIS)

    Kim, H. M.; Kim, I. G.; Kim, I. Y.

    2002-01-01

    The magnetic jack type Control Element Drive Mechanism (CEDM) for Korean Standard Nuclear Power Plant (KSNP) is an electromechanical device which provides controlled linear motion to the Control Element Assembly (CEA) through the Extension Shaft Assembly (ESA) in response to operational signals received from the Control Element Drive Mechanism Control System (CEDMCS). The CEDM is operated by applying localized magnetic flux fields to movable latch and lift magnets, which are in the coolant pressure boundary. The CEDM design had been developed through electromechanical testing of the system including the magnetic force lifting the ESA. But it will be inefficient if parametric studies should be performed to improve the CEDM by test due to the consumption of high cost and long duration. So it becomes necessary to develop a computational model to simulate the electromagnetic characteristics of the CEDM to improve the CEDM design efficiently. In this paper, the electromagnetic analysis using a 2D finite element model has been carried out to simulate magnetic force of the lift magnet of the CEDM, to provide effective evaluation between leakage flux and lift force and to compare with test results. Analysis results show the lift force satisfied the test results and design requirement and the lift force depend on the shape of the components, leakage flux and B-H curve

  15. Characteristic and analysis of structural elements of corporate social responsibility

    Directory of Open Access Journals (Sweden)

    J. S. Bilonog

    2015-04-01

    Full Text Available In this article attention is focused on social responsibility of business and on necessity to estimate its condition in Ukraine. Materials regarding elements and the principles of corporate social responsibility are structured. On this basis unification of quantitative elements of business social responsibility is offered according to which it is possible to carry out the analysis of the non­financial reporting. It is proposed to use not only quantitative techniques of data analysis but also refer to the qualitative ones. As a result of this, the analysis of social reports will be more productive and would minimize subjectivity of the researcher or representatives of the company which are responsible for presenting the information to the general public. The basic principles by which the companies can realize the strategy of corporate social responsibility are considered. Due to the empirical analysis of corporate reports expediency to use specified elements is proved. Reports of the companies in producing and non­productive sector are analyzed in more detail; features of displaying information on corporate social responsibility are defined. The attention to need of carrying out monitoring researches in the sphere of the corporate social reporting is updated.

  16. PIXE analysis of caries related trace elements in tooth enamel

    International Nuclear Information System (INIS)

    Annegarn, H.J.; Jodaikin, A.; Cleaton-Jones, P.E.; Sellschop, J.P.F.; Madiba, C.C.P.; Bibby, D.; University of the Witwatersrand, Johannesburg

    1981-01-01

    PIXE analysis has been applied to a set of twenty human teeth to determine trace element concentration in enamel from areas suceptible to dental caries (mesial and distal contact points) and in areas less susceptible to the disease (buccal surface), with the aim of determining the possible roles of trace elements in the carious process. The samples were caries-free anterior incisors extracted for periodontal reasons from subjects 10-30 years of age. Prior to extraction of the sample teeth, a detailed dental history and examination was carried out in each individual. PIXE analysis, using a 3 MeV proton beam of 1 mm diameter, allowed the determination of Ca, Mn, Fe, Cu, Zn, Sr and Pb above detection limits. As demonstrated in this work, the enhanced sensitivity of PIXE analysis over electron microprobe analysis, and capability of localised surface analysis compared with the pooled samples require for neutron activation analysis, makes it a powerful and useful technique in dental analysis. (orig.)

  17. PIXE analysis of caries related trace elements in tooth enamel

    Energy Technology Data Exchange (ETDEWEB)

    Annegarn, H J; Jodaikin, A; Cleaton-Jones, P E; Sellschop, J P.F.; Madiba, C C.P.; Bibby, D [University of the Witwatersrand, Johannesburg (South Africa). Nuclear Physics Research Unit; University of the Witwatersrand, Johannesburg (South Africa). Dental Research Unit)

    1981-03-01

    PIXE analysis has been applied to a set of twenty human teeth to determine trace element concentration in enamel from areas suceptible to dental caries (mesial and distal contact points) and in areas less susceptible to the disease (buccal surface), with the aim of determining the possible roles of trace elements in the carious process. The samples were caries-free anterior incisors extracted for periodontal reasons from subjects 10-30 years of age. Prior to extraction of the sample teeth, a detailed dental history and examination was carried out in each individual. PIXE analysis, using a 3 MeV proton beam of 1 mm diameter, allowed the determination of Ca, Mn, Fe, Cu, Zn, Sr and Pb above detection limits. As demonstrated in this work, the enhanced sensitivity of PIXE analysis over electron microprobe analysis, and capability of localised surface analysis compared with the pooled samples require for neutron activation analysis, makes it a powerful and useful technique in dental analysis.

  18. Proposal for element size and time increment selection guideline by 3-D finite element method for elastic waves propagation analysis

    International Nuclear Information System (INIS)

    Ishida, Hitoshi; Meshii, Toshiyuki

    2008-01-01

    This paper proposes a guideline for selection of element size and time increment by 3-D finite element method, which is applied to elastic wave propagation analysis for a long distance of a large structure. An element size and a time increment are determined by quantitative evaluation of strain, which must be 0 on the analysis model with a uniform motion, caused by spatial and time discretization. (author)

  19. AN ANALYSIS OF THE SHAPES OF INTERSTELLAR EXTINCTION CURVES. VI. THE NEAR-IR EXTINCTION LAW

    International Nuclear Information System (INIS)

    Fitzpatrick, E. L.; Massa, D.

    2009-01-01

    We combine new observations from the Hubble Space Telescope's Advanced Camera of Survey with existing data to investigate the wavelength dependence of near-IR (NIR) extinction. Previous studies suggest a power law form for NIR extinction, with a 'universal' value of the exponent, although some recent observations indicate that significant sight line-to-sight line variability may exist. We show that a power-law model for the NIR extinction provides an excellent fit to most extinction curves, but that the value of the power, β, varies significantly from sight line to sight line. Therefore, it seems that a 'universal NIR extinction law' is not possible. Instead, we find that as β decreases, R(V) ≡ A(V)/E(B - V) tends to increase, suggesting that NIR extinction curves which have been considered 'peculiar' may, in fact, be typical for different R(V) values. We show that the power-law parameters can depend on the wavelength interval used to derive them, with the β increasing as longer wavelengths are included. This result implies that extrapolating power-law fits to determine R(V) is unreliable. To avoid this problem, we adopt a different functional form for NIR extinction. This new form mimics a power law whose exponent increases with wavelength, has only two free parameters, can fit all of our curves over a longer wavelength baseline and to higher precision, and produces R(V) values which are consistent with independent estimates and commonly used methods for estimating R(V). Furthermore, unlike the power-law model, it gives R(V)s that are independent of the wavelength interval used to derive them. It also suggests that the relation R(V) = -1.36 E(K-V)/(E(B-V)) - 0.79 can estimate R(V) to ±0.12. Finally, we use model extinction curves to show that our extinction curves are in accord with theoretical expectations, and demonstrate how large samples of observational quantities can provide useful constraints on the grain properties.

  20. Sensitivity analysis overlaps of friction elements in cartridge seals

    Directory of Open Access Journals (Sweden)

    Žmindák Milan

    2018-01-01

    Full Text Available Cartridge seals are self-contained units consisting of a shaft sleeve, seals, and gland plate. The applications of mechanical seals are numerous. The most common example of application is in bearing production for automobile industry. This paper deals with the sensitivity analysis of overlaps friction elements in cartridge seal and their influence on the friction torque sealing and compressive force. Furthermore, it describes materials for the manufacture of sealings, approaches usually used to solution of hyperelastic materials by FEM and short introduction into the topic wheel bearings. The practical part contains one of the approach for measurement friction torque, which results were used to specifying the methodology and precision of FEM calculation realized by software ANSYS WORKBENCH. This part also contains the sensitivity analysis of overlaps friction elements.

  1. Forensic Comparison of Soil Samples Using Nondestructive Elemental Analysis.

    Science.gov (United States)

    Uitdehaag, Stefan; Wiarda, Wim; Donders, Timme; Kuiper, Irene

    2017-07-01

    Soil can play an important role in forensic cases in linking suspects or objects to a crime scene by comparing samples from the crime scene with samples derived from items. This study uses an adapted ED-XRF analysis (sieving instead of grinding to prevent destruction of microfossils) to produce elemental composition data of 20 elements. Different data processing techniques and statistical distances were evaluated using data from 50 samples and the log-LR cost (C llr ). The best performing combination, Canberra distance, relative data, and square root values, is used to construct a discriminative model. Examples of the spatial resolution of the method in crime scenes are shown for three locations, and sampling strategy is discussed. Twelve test cases were analyzed, and results showed that the method is applicable. The study shows how the combination of an analysis technique, a database, and a discriminative model can be used to compare multiple soil samples quickly. © 2016 American Academy of Forensic Sciences.

  2. Optimization of sample absorbance for quantitative analysis in the presence of pathlength error in the IR and NIR regions

    International Nuclear Information System (INIS)

    Hirschfeld, T.; Honigs, D.; Hieftje, G.

    1985-01-01

    Optical absorbance levels for quantiative analysis in the presence of photometric error have been described in the past. In newer instrumentation, such as FT-IR and NIRA spectrometers, the photometric error is no longer limiting. In these instruments, pathlength error due to cell or sampling irreproducibility is often a major concern. One can derive optimal absorbance by taking both pathlength and photometric errors into account. This paper analyzes the cases of pathlength error >> photometric error (trivial) and various cases in which the pathlength errors and the photometric error are of the same order: adjustable concentration (trivial until dilution errors are considered), constant relative pathlength error (trivial), and constant absolute pathlength error. The latter, in particular, is analyzed in detail to give the behavior of the error, the behavior of the optimal absorbance in its presence, and the total error levels attainable

  3. Twenty years of analysis of light elements at the LARN

    International Nuclear Information System (INIS)

    Demortier, G.

    1992-01-01

    We review the applications of ion beam analysis of light elements performed in the LARN during the last twenty years. The works mainly concern: helium bubbles in aluminum foils, Li in aluminum alloys, carbon in high purity MgO crystals and in olivines, nitrogen bubbles in glass and implanted nitrogen in iron and aluminum, oxygen in YBaCuO superconductors, fluorine in tooth enamel and implanted fluorine in metals. (orig.)

  4. Instrumental neutron activation analysis in environmental studies of trace elements

    International Nuclear Information System (INIS)

    Salmon, L.

    1975-06-01

    The application of a routine instrumental nuclear method is described in relation to environmental surveys and studies. A working rather than formal review is made of the techniques applied with particular reference to the data processing methods involved. The elements measured by instrumental activation analysis were: Ag, Al, As, Au, Ba, Br, Ca, Ce, Cl, Cd, Co, Cr, Cs, Cu, Fe, Hg, I, In, La, Mn, Na, Ni, Pb, Rb, Sb, Sc, Se, Th, Ti, U, V, W, Zn. (author)

  5. Three dimensional mathematical model of tooth for finite element analysis

    Directory of Open Access Journals (Sweden)

    Puškar Tatjana

    2010-01-01

    Full Text Available Introduction. The mathematical model of the abutment tooth is the starting point of the finite element analysis of stress and deformation of dental structures. The simplest and easiest way is to form a model according to the literature data of dimensions and morphological characteristics of teeth. Our method is based on forming 3D models using standard geometrical forms (objects in programmes for solid modeling. Objective. Forming the mathematical model of abutment of the second upper premolar for finite element analysis of stress and deformation of dental structures. Methods. The abutment tooth has a form of a complex geometric object. It is suitable for modeling in programs for solid modeling SolidWorks. After analyzing the literature data about the morphological characteristics of teeth, we started the modeling dividing the tooth (complex geometric body into simple geometric bodies (cylinder, cone, pyramid,.... Connecting simple geometric bodies together or substricting bodies from the basic body, we formed complex geometric body, tooth. The model is then transferred into Abaqus, a computational programme for finite element analysis. Transferring the data was done by standard file format for transferring 3D models ACIS SAT. Results. Using the programme for solid modeling SolidWorks, we developed three models of abutment of the second maxillary premolar: the model of the intact abutment, the model of the endodontically treated tooth with two remaining cavity walls and the model of the endodontically treated tooth with two remaining walls and inserted post. Conclusion Mathematical models of the abutment made according to the literature data are very similar with the real abutment and the simplifications are minimal. These models enable calculations of stress and deformation of the dental structures. The finite element analysis provides useful information in understanding biomechanical problems and gives guidance for clinical research.

  6. Preparation of hair and nail samples for trace element analysis

    International Nuclear Information System (INIS)

    Scoble, H.A.; Litman, R.

    1978-01-01

    The method of washing of human hair and nail samples is examined by neutron activation and γ-ray analysis. The amounts of Na, K, Br, Au, Zn, and La that are removed by successive washings determine the optimum number of washing for removing these trace elements as surface contaminants. A total solution contact time with the nails is 5 minutes, and leaching effcts are observed after 6 washings

  7. IR spectroscopy together with multivariate data analysis as a process analytical tool for in-line monitoring of crystallization process and solid-state analysis of crystalline product

    DEFF Research Database (Denmark)

    Pöllänen, Kati; Häkkinen, Antti; Reinikainen, Satu-Pia

    2005-01-01

    -ray powder diffraction (XRPD) as a reference technique. In order to fully utilize DRIFT, the application of multivariate techniques are needed, e.g., multivariate statistical process control (MSPC), principal component analysis (PCA) and partial least squares (PLS). The results demonstrate that multivariate...... Fourier transform infra red (ATR-FTIR) spectroscopy provides valuable information on process, which can be utilized for more controlled crystallization processes. Diffuse reflectance Fourier transform infra red (DRIFT-IR) is applied for polymorphic characterization of crystalline product using X......Crystalline product should exist in optimal polymorphic form. Robust and reliable method for polymorph characterization is of great importance. In this work, infra red (IR) spectroscopy is applied for monitoring of crystallization process in situ. The results show that attenuated total reflection...

  8. Elemental analysis of sub-hourly ambient aerosol collections

    Energy Technology Data Exchange (ETDEWEB)

    Kidwell, C.B.; Ondov, J.M. [University of Maryland, College Park, MD (USA). Dept. of Chemical & Biochemistry

    2004-03-01

    Simultaneous multielement graphite furnace atomic absorption spectrometry was used to determine Al, As, Cd, Cr, Cu, Fe, Mn, Ni, Pb, Sb, Se, and Zn in ambient air sampled at 170 L.min{sup -1} for 30 min and collected as a slurry after dynamic preconcentration. Analyses of slurries of NIST SRM 1648, Urban Particulate Matter, were typically within 10% of expected values for all elements except Al, Cr, and Fe, elements for which deviations were mostly due to difficulties in transferring large particles. This problem will be reduced for urban fine particulate matter samples (PM2.5). Trends in the concentrations of elemental source markers were readily correlated with wind direction and other meteorological factors to identify the influences of local industrial emissions, including motor vehicle traffic, coal- and oil-fired power plants, and municipal incinerators. Factor analysis was applied to the 88-sample data set to extract 7 factors: urban dust, meteorological factors, incinerators, coal- fired power plants, Tour Bus emission, unknown As source, and oil-fired power plants. Factor analysis was also applied to an 18-sample data set representing 2.5 h averages of the 30 min data to simulate the effect of longer sample collection times. Only 6 factors were extracted from this data set, which shows that increased temporal resolution enhances the power of factor analysis to resolve sources. These results indicate that a wealth of detailed information is revealed at this level of temporal resolution.

  9. Finite element analysis of the cyclic indentation of bilayer enamel

    International Nuclear Information System (INIS)

    Jia, Yunfei; Xuan, Fu-zhen; Chen, Xiaoping; Yang, Fuqian

    2014-01-01

    Tooth enamel is often subjected to repeated contact and often experiences contact deformation in daily life. The mechanical strength of the enamel determines the biofunctionality of the tooth. Considering the variation of the rod arrangement in outer and inner enamel, we approximate enamel as a bilayer structure and perform finite element analysis of the cyclic indentation of the bilayer structure, to mimic the repeated contact of enamel during mastication. The dynamic deformation behaviour of both the inner enamel and the bilayer enamel is examined. The material parameters of the inner and outer enamel used in the analysis are obtained by fitting the finite element results with the experimental nanoindentation results. The penetration depth per cycle at the quasi-steady state is used to describe the depth propagation speed, which exhibits a two-stage power-law dependence on the maximum indentation load and the amplitude of the cyclic load, respectively. The continuous penetration of the indenter reflects the propagation of the plastic zone during cyclic indentation, which is related to the energy dissipation. The outer enamel serves as a protective layer due to its great resistance to contact deformation in comparison to the inner enamel. The larger equivalent plastic strain and lower stresses in the inner enamel during cyclic indentation, as calculated from the finite element analysis, indicate better crack/fracture resistance of the inner enamel. (paper)

  10. Finite element analysis of the cyclic indentation of bilayer enamel

    Science.gov (United States)

    Jia, Yunfei; Xuan, Fu-zhen; Chen, Xiaoping; Yang, Fuqian

    2014-04-01

    Tooth enamel is often subjected to repeated contact and often experiences contact deformation in daily life. The mechanical strength of the enamel determines the biofunctionality of the tooth. Considering the variation of the rod arrangement in outer and inner enamel, we approximate enamel as a bilayer structure and perform finite element analysis of the cyclic indentation of the bilayer structure, to mimic the repeated contact of enamel during mastication. The dynamic deformation behaviour of both the inner enamel and the bilayer enamel is examined. The material parameters of the inner and outer enamel used in the analysis are obtained by fitting the finite element results with the experimental nanoindentation results. The penetration depth per cycle at the quasi-steady state is used to describe the depth propagation speed, which exhibits a two-stage power-law dependence on the maximum indentation load and the amplitude of the cyclic load, respectively. The continuous penetration of the indenter reflects the propagation of the plastic zone during cyclic indentation, which is related to the energy dissipation. The outer enamel serves as a protective layer due to its great resistance to contact deformation in comparison to the inner enamel. The larger equivalent plastic strain and lower stresses in the inner enamel during cyclic indentation, as calculated from the finite element analysis, indicate better crack/fracture resistance of the inner enamel.

  11. Carrier Dynamics Analysis in Metal-SemiconductorMetal Device for mid-IR Silicon Photonics

    DEFF Research Database (Denmark)

    Hui, Alvin Tak Lok; Ding, Yunhong; Hu, Hao

    A modelling platform for active carrier removal based on metal-semiconductor-metal structure is reported on analysis of carrier dynamics. The analysis reveals electric current hot spots exist in geometric singularities and curly trajectory of carriers should be considered when accurately estimati...

  12. Carrier dynamics analysis in metal-semiconductor-metal device for mid-IR silicon photonics

    DEFF Research Database (Denmark)

    Hui, Alvin Tak Lok; Ding, Yunhong; Hu, Hao

    2017-01-01

    A modelling platform for active carrier removal based on metal-semiconductor-metal structure is reported on analysis of carrier dynamics. The analysis reveals electric current hot spots exist in geometric singularities and curly trajectory of carriers should be considered when accurately estimati...

  13. Impaired Insulin Signaling is Associated with Hepatic Mitochondrial Dysfunction in IR+/−-IRS-1+/− Double Heterozygous (IR-IRS1dh Mice

    Directory of Open Access Journals (Sweden)

    Andras Franko

    2017-05-01

    Full Text Available Mitochondria play a pivotal role in energy metabolism, but whether insulin signaling per se could regulate mitochondrial function has not been identified yet. To investigate whether mitochondrial function is regulated by insulin signaling, we analyzed muscle and liver of insulin receptor (IR+/−-insulin receptor substrate-1 (IRS-1+/− double heterozygous (IR-IRS1dh mice, a well described model for insulin resistance. IR-IRS1dh mice were studied at the age of 6 and 12 months and glucose metabolism was determined by glucose and insulin tolerance tests. Mitochondrial enzyme activities, oxygen consumption, and membrane potential were assessed using spectrophotometric, respirometric, and proton motive force analysis, respectively. IR-IRS1dh mice showed elevated serum insulin levels. Hepatic mitochondrial oxygen consumption was reduced in IR-IRS1dh animals at 12 months of age. Furthermore, 6-month-old IR-IRS1dh mice demonstrated enhanced mitochondrial respiration in skeletal muscle, but a tendency of impaired glucose tolerance. On the other hand, 12-month-old IR-IRS1dh mice showed improved glucose tolerance, but normal muscle mitochondrial function. Our data revealed that deficiency in IR/IRS-1 resulted in normal or even elevated skeletal muscle, but impaired hepatic mitochondrial function, suggesting a direct cross-talk between insulin signaling and mitochondria in the liver.

  14. A proposal for a determination method of element division on an analytical model for finite element elastic waves propagation analysis

    International Nuclear Information System (INIS)

    Ishida, Hitoshi; Meshii, Toshiyuki

    2010-01-01

    This study proposes an element size selection method named the 'Impact-Meshing (IM) method' for a finite element waves propagation analysis model, which is characterized by (1) determination of element division of the model with strain energy in the whole model, (2) static analysis (dynamic analysis in a single time step) with boundary conditions which gives a maximum change of displacement in the time increment and inertial (impact) force caused by the displacement change. In this paper, an example of application of the IM method to 3D ultrasonic wave propagation problem in an elastic solid is described. These examples showed an analysis result with a model determined by the IM method was convergence and calculation time for determination of element subdivision was reduced to about 1/6 by the IM Method which did not need determination of element subdivision by a dynamic transient analysis with 100 time steps. (author)

  15. Fourier Transform Infrared (FT-IR) and Laser Ablation Inductively Coupled Plasma-Mass Spectrometry (LA-ICP-MS) Imaging of Cerebral Ischemia: Combined Analysis of Rat Brain Thin Cuts Toward Improved Tissue Classification.

    Science.gov (United States)

    Balbekova, Anna; Lohninger, Hans; van Tilborg, Geralda A F; Dijkhuizen, Rick M; Bonta, Maximilian; Limbeck, Andreas; Lendl, Bernhard; Al-Saad, Khalid A; Ali, Mohamed; Celikic, Minja; Ofner, Johannes

    2018-02-01

    Microspectroscopic techniques are widely used to complement histological studies. Due to recent developments in the field of chemical imaging, combined chemical analysis has become attractive. This technique facilitates a deepened analysis compared to single techniques or side-by-side analysis. In this study, rat brains harvested one week after induction of photothrombotic stroke were investigated. Adjacent thin cuts from rats' brains were imaged using Fourier transform infrared (FT-IR) microspectroscopy and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS). The LA-ICP-MS data were normalized using an internal standard (a thin gold layer). The acquired hyperspectral data cubes were fused and subjected to multivariate analysis. Brain regions affected by stroke as well as unaffected gray and white matter were identified and classified using a model based on either partial least squares discriminant analysis (PLS-DA) or random decision forest (RDF) algorithms. The RDF algorithm demonstrated the best results for classification. Improved classification was observed in the case of fused data in comparison to individual data sets (either FT-IR or LA-ICP-MS). Variable importance analysis demonstrated that both molecular and elemental content contribute to the improved RDF classification. Univariate spectral analysis identified biochemical properties of the assigned tissue types. Classification of multisensor hyperspectral data sets using an RDF algorithm allows access to a novel and in-depth understanding of biochemical processes and solid chemical allocation of different brain regions.

  16. Volatility-dependent 2D IR correlation analysis of traditional Chinese medicine ‘Red Flower Oil’ preparation from different manufacturers

    Science.gov (United States)

    Wu, Yan-Wen; Sun, Su-Qin; Zhou, Qun; Tao, Jia-Xun; Noda, Isao

    2008-06-01

    As a traditional Chinese medicine (TCM), 'Red Flower Oil' preparation is widely used as a household remedy in China and Southeast Asia. Usually, the preparation is a mixture of several plant essential oils with different volatile features, such as wintergreen oil, turpentine oil and clove oil. The proportions of these plant essential oils in 'Red Flower Oil' vary from different manufacturers. Thus, it is important to develop a simple and rapid evaluation method for quality assurance of the preparations. Fourier transform infrared (FT-IR) was applied and two-dimensional correlation infrared spectroscopy (2D IR) based on the volatile characteristic of samples was used to enhance the resolution of FT-IR spectra. 2D IR technique could, not only easily provide the composition and their volatile sequences in 'Red flower Oil' preparations, but also rapidly discriminate the subtle differences in products from different manufacturers. Therefore, FT-IR combined with volatility-dependent 2D IR correlation analysis provides a very fast and effective method for the quality control of essential oil mixtures in TCM.

  17. Validation of Correction Algorithms for Near-IR Analysis of Human Milk in an Independent Sample Set-Effect of Pasteurization.

    Science.gov (United States)

    Kotrri, Gynter; Fusch, Gerhard; Kwan, Celia; Choi, Dasol; Choi, Arum; Al Kafi, Nisreen; Rochow, Niels; Fusch, Christoph

    2016-02-26

    Commercial infrared (IR) milk analyzers are being increasingly used in research settings for the macronutrient measurement of breast milk (BM) prior to its target fortification. These devices, however, may not provide reliable measurement if not properly calibrated. In the current study, we tested a correction algorithm for a Near-IR milk analyzer (Unity SpectraStar, Brookfield, CT, USA) for fat and protein measurements, and examined the effect of pasteurization on the IR matrix and the stability of fat, protein, and lactose. Measurement values generated through Near-IR analysis were compared against those obtained through chemical reference methods to test the correction algorithm for the Near-IR milk analyzer. Macronutrient levels were compared between unpasteurized and pasteurized milk samples to determine the effect of pasteurization on macronutrient stability. The correction algorithm generated for our device was found to be valid for unpasteurized and pasteurized BM. Pasteurization had no effect on the macronutrient levels and the IR matrix of BM. These results show that fat and protein content can be accurately measured and monitored for unpasteurized and pasteurized BM. Of additional importance is the implication that donated human milk, generally low in protein content, has the potential to be target fortified.

  18. Validation of Correction Algorithms for Near-IR Analysis of Human Milk in an Independent Sample Set—Effect of Pasteurization

    Science.gov (United States)

    Kotrri, Gynter; Fusch, Gerhard; Kwan, Celia; Choi, Dasol; Choi, Arum; Al Kafi, Nisreen; Rochow, Niels; Fusch, Christoph

    2016-01-01

    Commercial infrared (IR) milk analyzers are being increasingly used in research settings for the macronutrient measurement of breast milk (BM) prior to its target fortification. These devices, however, may not provide reliable measurement if not properly calibrated. In the current study, we tested a correction algorithm for a Near-IR milk analyzer (Unity SpectraStar, Brookfield, CT, USA) for fat and protein measurements, and examined the effect of pasteurization on the IR matrix and the stability of fat, protein, and lactose. Measurement values generated through Near-IR analysis were compared against those obtained through chemical reference methods to test the correction algorithm for the Near-IR milk analyzer. Macronutrient levels were compared between unpasteurized and pasteurized milk samples to determine the effect of pasteurization on macronutrient stability. The correction algorithm generated for our device was found to be valid for unpasteurized and pasteurized BM. Pasteurization had no effect on the macronutrient levels and the IR matrix of BM. These results show that fat and protein content can be accurately measured and monitored for unpasteurized and pasteurized BM. Of additional importance is the implication that donated human milk, generally low in protein content, has the potential to be target fortified. PMID:26927169

  19. Multidimensional elemental analysis with the Sandia nuclear microprobe

    International Nuclear Information System (INIS)

    Doyle, B.L.

    1988-01-01

    It is well known that many of the ion beam analysis techniques such as Rutherford backscattering spectrometry, elastic recoil detection, resonant and nonresonant nuclear reaction analysis can be used to nondestructively obtain concentration depth profiles of elements in solids. When these techniques are combined with the small beam spot capabilities of a scanned nuclear microprobe, sample composition can be determined in up to three dimensions. This paper will review the various procedures used to collect and analyze multidimensional data using the Sandia nuclear microprobe. In addition, examples of how these data are being used in the study of materials will be shown. (author)

  20. FT-IR spectroscopy and multivariate analysis as an auxiliary tool for diagnosis of mental disorders: Bipolar and schizophrenia cases

    Science.gov (United States)

    Ogruc Ildiz, G.; Arslan, M.; Unsalan, O.; Araujo-Andrade, C.; Kurt, E.; Karatepe, H. T.; Yilmaz, A.; Yalcinkaya, O. B.; Herken, H.

    2016-01-01

    In this study, a methodology based on Fourier-transform infrared spectroscopy and principal component analysis and partial least square methods is proposed for the analysis of blood plasma samples in order to identify spectral changes correlated with some biomarkers associated with schizophrenia and bipolarity. Our main goal was to use the spectral information for the calibration of statistical models to discriminate and classify blood plasma samples belonging to bipolar and schizophrenic patients. IR spectra of 30 samples of blood plasma obtained from each, bipolar and schizophrenic patients and healthy control group were collected. The results obtained from principal component analysis (PCA) show a clear discrimination between the bipolar (BP), schizophrenic (SZ) and control group' (CG) blood samples that also give possibility to identify three main regions that show the major differences correlated with both mental disorders (biomarkers). Furthermore, a model for the classification of the blood samples was calibrated using partial least square discriminant analysis (PLS-DA), allowing the correct classification of BP, SZ and CG samples. The results obtained applying this methodology suggest that it can be used as a complimentary diagnostic tool for the detection and discrimination of these mental diseases.

  1. Thermal Analysis, FT-IR Spectroscopy and Optical Microscopy as a Tool for Characterization of Marble

    Czech Academy of Sciences Publication Activity Database

    Plevová, Eva; Kožušníková, Alena; Vaculíková, Lenka

    2009-01-01

    Roč. 5, č. 9 (2009), s. 149-150 ISSN 1336-7242. [Zjazd chemikov /61./. 07.09.2009-11.09.2009, Tatranské Matliare] R&D Projects: GA ČR GP105/07/P416; GA ČR GA105/08/1398 Institutional research plan: CEZ:AV0Z30860518 Keywords : marbles * thermal analysis * thermomechanical analysis Subject RIV: CB - Analytical Chemistry, Separation

  2. Macro elemental analysis of food samples by nuclear analytical technique

    Science.gov (United States)

    Syahfitri, W. Y. N.; Kurniawati, S.; Adventini, N.; Damastuti, E.; Lestiani, D. D.

    2017-06-01

    Energy-dispersive X-ray fluorescence (EDXRF) spectrometry is a non-destructive, rapid, multi elemental, accurate, and environment friendly analysis compared with other detection methods. Thus, EDXRF spectrometry is applicable for food inspection. The macro elements calcium and potassium constitute important nutrients required by the human body for optimal physiological functions. Therefore, the determination of Ca and K content in various foods needs to be done. The aim of this work is to demonstrate the applicability of EDXRF for food analysis. The analytical performance of non-destructive EDXRF was compared with other analytical techniques; neutron activation analysis and atomic absorption spectrometry. Comparison of methods performed as cross checking results of the analysis and to overcome the limitations of the three methods. Analysis results showed that Ca found in food using EDXRF and AAS were not significantly different with p-value 0.9687, whereas p-value of K between EDXRF and NAA is 0.6575. The correlation between those results was also examined. The Pearson correlations for Ca and K were 0.9871 and 0.9558, respectively. Method validation using SRM NIST 1548a Typical Diet was also applied. The results showed good agreement between methods; therefore EDXRF method can be used as an alternative method for the determination of Ca and K in food samples.

  3. A Study on the Effect of Cohesive Laws on Finite Element Analysis of Crack Propagation Using Cohesive Elements

    Energy Technology Data Exchange (ETDEWEB)

    Seo, Hyeongseok; Baek, Hyungchan; Kim, Hyungyu [Seoul Nat' l Univ. of Sci. and Tech., Seoul (Korea, Republic of)

    2014-04-15

    In this paper, the effect of cohesive laws on the finite element analysis of crack propagation using cohesive elements is investigated through three-point bending and double cantilever beam problems. The cohesive elements are implemented into ABAQUS/Standard user subroutines(UEL), and the shape of cohesive law is varied by changing parameters in polynomial functions of cohesive traction-separation relations. In particular, crack propagation behaviors are studied by comparing load-displacement curves of the analysis models which have different shapes of cohesive laws with the same values of fracture energy and cohesive strength. Furthermore, the influence of the element size on crack propagation is discussed in this study.

  4. An IR Sounding-Based Analysis of the Saharan Air Layer in North Africa

    Science.gov (United States)

    Nicholls, Stephen D.; Mohr, Karen I.

    2018-01-01

    Intense daytime surface heating over barren-to-sparsely vegetated surfaces results in dry convective mixing. In the absence of external forcing such as mountain waves, the dry convection can produce a deep, well-mixed, nearly isentropic boundary layer that becomes a well-mixed residual layer in the evening. These well-mixed layers (WML) retain their unique mid-tropospheric thermal and humidity structure for several days. To detect the SAL and characterize its properties, AIRS Level 2 Ver. 6 temperature and humidity products (2003-Present) are evaluated against rawinsondes and compared to model analysis at each of the 55 rawinsonde stations in northern Africa. To distinguish WML from Saharan air layers (WMLs of Saharan origin), the detection involved a two-step process: 1) algorithm-based detection of WMLs in dry environments (less than 7 g per kilogram mixing ratio) 2) identification of Sahara air layers (SAL) by applying Hybrid Single Particle Lagrangian Integrated Trajectory (HYSPLIT) back trajectories to determine the history of each WML. WML occurrence rates from AIRS closely resemble that from rawinsondes, yet rates from model analysis were up to 30% higher than observations in the Sahara due to model errors. Despite the overly frequent occurrence of WMLs from model analysis, HYSPLIT trajectory analysis showed that SAL occurrence rates (given a WML exists) from rawinsondes, AIRS, and model analysis were nearly identical. Although the number of WMLs varied among the data sources, the proportion of WMLs which were classified as SAL was nearly the same. The analysis of SAL bulk properties showed that AIRS and model analysis exhibited a slight warm and moist bias relative to rawinsondes in non-Saharan locations, but model analysis was notably warmer than rawinsondes and AIRS within the Sahara. The latter result is likely associated with the dearth of available data assimilated by model analysis in the Sahara. The variability of SAL thicknesses was reasonably

  5. Finansinių ataskaitų elementų įvertinimo būdai viešojo ir privataus sektoriaus apskaitoje

    OpenAIRE

    Rudžionienė, Kristina

    2009-01-01

    Financial accounting is not only a historical cost accounting in XX-XXI centuries. It is a need to use other methods of evaluation of financial statements' elements seeking the main purpose of financial accounting - to disclose true and fair value of public sector assets, net assets/equity, liabilities, results of activity. One of the most important choices is the choice of an evaluation method which influence financial statement elements values. This problem was not analysed in Lithuanian sc...

  6. Thermal buckling comparative analysis using Different FE (Finite Element) tools

    Energy Technology Data Exchange (ETDEWEB)

    Banasiak, Waldemar; Labouriau, Pedro [INTECSEA do Brasil, Rio de Janeiro, RJ (Brazil); Burnett, Christopher [INTECSEA UK, Surrey (United Kingdom); Falepin, Hendrik [Fugro Engineers SA/NV, Brussels (Belgium)

    2009-12-19

    High operational temperature and pressure in offshore pipelines may lead to unexpected lateral movements, sometimes call lateral buckling, which can have serious consequences for the integrity of the pipeline. The phenomenon of lateral buckling in offshore pipelines needs to be analysed in the design phase using FEM. The analysis should take into account many parameters, including operational temperature and pressure, fluid characteristic, seabed profile, soil parameters, coatings of the pipe, free spans etc. The buckling initiation force is sensitive to small changes of any initial geometric out-of-straightness, thus the modeling of the as-laid state of the pipeline is an important part of the design process. Recently some dedicated finite elements programs have been created making modeling of the offshore environment more convenient that has been the case with the use of general purpose finite element software. The present paper aims to compare thermal buckling analysis of sub sea pipeline performed using different finite elements tools, i.e. general purpose programs (ANSYS, ABAQUS) and dedicated software (SAGE Profile 3D) for a single pipeline resting on an the seabed. The analyses considered the pipeline resting on a flat seabed with a small levels of out-of straightness initiating the lateral buckling. The results show the quite good agreement of results of buckling in elastic range and in the conclusions next comparative analyses with sensitivity cases are recommended. (author)

  7. In-vivo elemental analysis at Birmingham 1968-1981

    International Nuclear Information System (INIS)

    Chettle, D.R.; Scott, M.C.

    1986-01-01

    Techniques have been developed to measure a number of elements in-vivo. Some have been measured by producing a radioactive isotope in the body by neutron bombardment and subsequently counting γ-rays given off during its decay. Measurements of calcium and sodium have been those most frequently used; copper, iron and phosphorus have also been measured in this way. Gamma-rays emitted 10 -18 s-10 -12 s following neutron capture have also been used for elemental analysis. This method, which involved detectors being in position by the subject during the neutron irradiation, has been widely applied to measurements of both nitrogen and cadmium. Preliminary studies of nuclear resonance scattering have suggested that this could be used for in-vivo elemental analysis, provided technical difficulties in source preparation could be overcome. Recently the use of X-ray fluorescence has been investigated for in-vivo analyses of lead in bone; the extension of this technique to measure mercury in the kidney is under consideration. (author)

  8. Optimization of deformation monitoring networks using finite element strain analysis

    Science.gov (United States)

    Alizadeh-Khameneh, M. Amin; Eshagh, Mehdi; Jensen, Anna B. O.

    2018-04-01

    An optimal design of a geodetic network can fulfill the requested precision and reliability of the network, and decrease the expenses of its execution by removing unnecessary observations. The role of an optimal design is highlighted in deformation monitoring network due to the repeatability of these networks. The core design problem is how to define precision and reliability criteria. This paper proposes a solution, where the precision criterion is defined based on the precision of deformation parameters, i. e. precision of strain and differential rotations. A strain analysis can be performed to obtain some information about the possible deformation of a deformable object. In this study, we split an area into a number of three-dimensional finite elements with the help of the Delaunay triangulation and performed the strain analysis on each element. According to the obtained precision of deformation parameters in each element, the precision criterion of displacement detection at each network point is then determined. The developed criterion is implemented to optimize the observations from the Global Positioning System (GPS) in Skåne monitoring network in Sweden. The network was established in 1989 and straddled the Tornquist zone, which is one of the most active faults in southern Sweden. The numerical results show that 17 out of all 21 possible GPS baseline observations are sufficient to detect minimum 3 mm displacement at each network point.

  9. The platinum group elements and gold: analysis by radiochemical and instrumental neutron activation analysis and relevance to geological exploration and related problems

    Energy Technology Data Exchange (ETDEWEB)

    Reeves, S.; Plimer, I. R. [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1996-12-31

    This paper presents an overview of research conducted with the support of the Australian Institute of Nuclear Science and Engineering, at the University of Melbourne, School of Earth Sciences, Radiochemical Neutron Activation Laboratory. The primary objective of this research is to realize the high potential of the platinum group elements (PGE) and gold to the solution of petrogenetic problems, the study of magma generation and magmatic processes in mafic/ultramafic rock suites, as tracers in hydrothermal ore formation. The PGEs (Os, Ru, Ir, Pt, Pd and Rh) are among the least abundant of all elements on earth with unique properties such as high melting points, high electrical and thermal conductivity, high density, strength and toughness as alloys. They exhibit both siderophile and chalcophile characteristics and are valuable tools in providing information about magmatic processes, in particular S-saturation, as well as crystal fractionation trends. Two distinct groups of PGEs are discerned; the IPGEs (Ru, Os, Ir) and the PPGEs (Pt, Pd, Rh, Au) on the basis of their behaviour during fractionation processes. Using chondrite normalized PGE patterns it is possible to distinguish between sulphides that segregated from primitive magmas, such as komatiites, and sulphides which segregated from more fractionated magmas, such as tholeiites. It is critical to the understanding of these processes to be able to analyse key elements, such as the PGE and gold, in the parts per billion to parts per trillion range. Platinum group elements and Au were determined by radiochemical neutron activation analysis using a modified NiS fire-assay preconcentration technique, adapted from procedures first used by Robert, R.V. D. and van Wyk, E. (1975) . Detection limits are generally 0.005-0.01 ppb (Au and Ir), 0.1-0.2 ppb (Pd and Pt), and 0.1-0.5 ppb for Ru. 9 refs.

  10. The platinum group elements and gold: analysis by radiochemical and instrumental neutron activation analysis and relevance to geological exploration and related problems

    International Nuclear Information System (INIS)

    Reeves, S.; Plimer, I. R.

    1996-01-01

    This paper presents an overview of research conducted with the support of the Australian Institute of Nuclear Science and Engineering, at the University of Melbourne, School of Earth Sciences, Radiochemical Neutron Activation Laboratory. The primary objective of this research is to realize the high potential of the platinum group elements (PGE) and gold to the solution of petrogenetic problems, the study of magma generation and magmatic processes in mafic/ultramafic rock suites, as tracers in hydrothermal ore formation. The PGEs (Os, Ru, Ir, Pt, Pd and Rh) are among the least abundant of all elements on earth with unique properties such as high melting points, high electrical and thermal conductivity, high density, strength and toughness as alloys. They exhibit both siderophile and chalcophile characteristics and are valuable tools in providing information about magmatic processes, in particular S-saturation, as well as crystal fractionation trends. Two distinct groups of PGEs are discerned; the IPGEs (Ru, Os, Ir) and the PPGEs (Pt, Pd, Rh, Au) on the basis of their behaviour during fractionation processes. Using chondrite normalized PGE patterns it is possible to distinguish between sulphides that segregated from primitive magmas, such as komatiites, and sulphides which segregated from more fractionated magmas, such as tholeiites. It is critical to the understanding of these processes to be able to analyse key elements, such as the PGE and gold, in the parts per billion to parts per trillion range. Platinum group elements and Au were determined by radiochemical neutron activation analysis using a modified NiS fire-assay preconcentration technique, adapted from procedures first used by Robert, R.V. D. and van Wyk, E. (1975) . Detection limits are generally 0.005-0.01 ppb (Au and Ir), 0.1-0.2 ppb (Pd and Pt), and 0.1-0.5 ppb for Ru. 9 refs

  11. The platinum group elements and gold: analysis by radiochemical and instrumental neutron activation analysis and relevance to geological exploration and related problems

    Energy Technology Data Exchange (ETDEWEB)

    Reeves, S; Plimer, I R [Melbourne Univ., Parkville, VIC (Australia). School of Physics

    1997-12-31

    This paper presents an overview of research conducted with the support of the Australian Institute of Nuclear Science and Engineering, at the University of Melbourne, School of Earth Sciences, Radiochemical Neutron Activation Laboratory. The primary objective of this research is to realize the high potential of the platinum group elements (PGE) and gold to the solution of petrogenetic problems, the study of magma generation and magmatic processes in mafic/ultramafic rock suites, as tracers in hydrothermal ore formation. The PGEs (Os, Ru, Ir, Pt, Pd and Rh) are among the least abundant of all elements on earth with unique properties such as high melting points, high electrical and thermal conductivity, high density, strength and toughness as alloys. They exhibit both siderophile and chalcophile characteristics and are valuable tools in providing information about magmatic processes, in particular S-saturation, as well as crystal fractionation trends. Two distinct groups of PGEs are discerned; the IPGEs (Ru, Os, Ir) and the PPGEs (Pt, Pd, Rh, Au) on the basis of their behaviour during fractionation processes. Using chondrite normalized PGE patterns it is possible to distinguish between sulphides that segregated from primitive magmas, such as komatiites, and sulphides which segregated from more fractionated magmas, such as tholeiites. It is critical to the understanding of these processes to be able to analyse key elements, such as the PGE and gold, in the parts per billion to parts per trillion range. Platinum group elements and Au were determined by radiochemical neutron activation analysis using a modified NiS fire-assay preconcentration technique, adapted from procedures first used by Robert, R.V. D. and van Wyk, E. (1975) . Detection limits are generally 0.005-0.01 ppb (Au and Ir), 0.1-0.2 ppb (Pd and Pt), and 0.1-0.5 ppb for Ru. 9 refs.

  12. Simultaneous speciation neutron activation analysis for trace elements

    International Nuclear Information System (INIS)

    Chatt, A.; Kiceniuk, J.W.; Menendez Sanchez, W.; Bottaro, C.

    2006-01-01

    Among the various forms of neutron activation technique being developed in our laboratory, much emphasis has been placed over the last ten years or so on the development of simultaneous speciation neutron activation analysis (SSNAA). This technique can now be used for the simultaneous determination of various species of a number of elements. Almost all speciation techniques consist of two steps. The first step involves the separation of species from the sample followed by the second step of element-specific detection. A number of characteristic features of NAA, which other techniques normally do not possess, can be advantageously exploited in SSNAA. For example, SSNAA can be used for: (i) multielement speciation with high specificity, (ii) speciation of chemically dissimilar elements such as Cd, Mn and Se, (iii) speciation of elements such as Cl, Br and I which are rather difficult to determine by most other techniques, etc. We have developed SSNAA methods for assaying various arsenic species, namely As(III), As(V), dimethyl arsonic acid (DMA), monomethylarsinic acid (MMA), arsenobetaine (AsB), organically bound arsenic (OBAs), and lipid-soluble arsenic (LSAs) in marine fish samples. We have extended these methods to include simultaneous determination of various species of As, Sb and Se in water. We have also developed SSNAA methods employing biochemical techniques for the simultaneous separation, preconcentration and characterization of metalloproteins and protein-bound trace element species of As, Br, Cd, Cu, Mn, Se, and Zn. We have developed methods for the simultaneous separation and characterization of organohalogen compounds in fish. An overview of the SSNAA methods being developed in our laboratory will be presented. (author)

  13. Structural optimisation of cage induction motors using finite element analysis

    Science.gov (United States)

    Palko, S.

    The current trend in motor design is to have highly efficient, low noise, low cost, and modular motors with a high power factor. High torque motors are useful in applications like servo motors, lifts, cranes, and rolling mills. This report contains a detailed review of different optimization methods applicable in various design problems. Special attention is given to the performance of different methods, when they are used with finite element analysis (FEA) as an objective function, and accuracy problems arising from the numerical simulations. Also an effective method for designing high starting torque and high efficiency motors is presented. The method described in this work utilizes FEA combined with algorithms for the optimization of the slot geometry. The optimization algorithm modifies the position of the nodal points in the element mesh. The number of independent variables ranges from 14 to 140 in this work.

  14. Grouping and analysis of chair quality and their basic elements

    Directory of Open Access Journals (Sweden)

    Skakić Dušan

    2009-01-01

    Full Text Available Both the scientific experience and the engineering practice indicate that the decision making processes in the course of solving complex designing problems require an analysis of a great number of different construction variants. These types of decision-making processes are time consuming and do not always result in the selection of an optimal solution. That is why the methods of numerical optimization are applied in a wide range of technical sciences to assist in the selection of the best solution. The first step in solving the problem by using the Finite element method is to determine the type of chair earmarked for modeling, and to determine the dimensions of the chair elements.

  15. Elemental analysis of Kuwaiti petroleum and combustion products

    Energy Technology Data Exchange (ETDEWEB)

    Reid, J.S.; Cahill, T.A.; Gearhart, E.A.; Flocchini, R.G. (California Univ., Davis, CA (United States). Crocker Nuclear Lab.); Schweitzer, J.S.; Peterson, C.A. (Schlumberger-Doll Research Center, Ridgefield, CT (United States))

    1993-03-01

    Crude oil from eight Kuwaiti fields and aerosols generated by their combustion in the laboratory have been analyzed by composition and particulate size. Liquid petroleum and petroleum combustion products were subjected to elemental analysis by proton induced x-ray techniques and by x-ray fluorescence techniques. The mean sulfur content of the burning wells was weighted by their production rates to obtain the mean sulfur content of the burning oil, 2.66%. The liquid samples were also analyzed by neutron activation analyses. Results show that Kuwaiti oil and smoke aerosols from laboratory combustion generally contain very low amounts of chlorine, contrary to what is found in airborne samples above Kuwait. Trace element signatures were developed to aid in tracing smoke from the oil fires. (Author).

  16. Study on Tourist Carrying Capacity Based on Matter Element Analysis

    Institute of Scientific and Technical Information of China (English)

    LiuYunguo; FanTing; LiXin; ZhouMing; WangXianhai

    2005-01-01

    This paper proposes that it is necessary to implement the concept of tourist carrying capacity to facilitate the tourism planning, and presents a method to evaluate the carrying capacity. The method called matter element analysis can solve the uncertain and incompatible problem of the evaluated factors in assessing carrying capacity.The current state of a destination's carrying capacity can be determined by establishing the standard indexes and the matter element model. Through the evaluating of the travel industry zones of the Autonomous Prefecture of Western Hunan, the method is proved to be simple and feasible, and it is improved to be significant for the tourism planning and determination as well as the sustainable development of the regional tourism.

  17. Probabilistic finite elements for fatigue and fracture analysis

    Science.gov (United States)

    Belytschko, Ted; Liu, Wing Kam

    1993-04-01

    An overview of the probabilistic finite element method (PFEM) developed by the authors and their colleagues in recent years is presented. The primary focus is placed on the development of PFEM for both structural mechanics problems and fracture mechanics problems. The perturbation techniques are used as major tools for the analytical derivation. The following topics are covered: (1) representation and discretization of random fields; (2) development of PFEM for the general linear transient problem and nonlinear elasticity using Hu-Washizu variational principle; (3) computational aspects; (4) discussions of the application of PFEM to the reliability analysis of both brittle fracture and fatigue; and (5) a stochastic computational tool based on stochastic boundary element (SBEM). Results are obtained for the reliability index and corresponding probability of failure for: (1) fatigue crack growth; (2) defect geometry; (3) fatigue parameters; and (4) applied loads. These results show that initial defect is a critical parameter.

  18. Nonlinear dynamic analysis using Petrov-Galerkin natural element method

    International Nuclear Information System (INIS)

    Lee, Hong Woo; Cho, Jin Rae

    2004-01-01

    According to our previous study, it is confirmed that the Petrov-Galerkin Natural Element Method (PG-NEM) completely resolves the numerical integration inaccuracy in the conventional Bubnov-Galerkin Natural Element Method (BG-NEM). This paper is an extension of PG-NEM to two-dimensional nonlinear dynamic problem. For the analysis, a constant average acceleration method and a linearized total Lagrangian formulation is introduced with the PG-NEM. At every time step, the grid points are updated and the shape functions are reproduced from the relocated nodal distribution. This process enables the PG-NEM to provide more accurate and robust approximations. The representative numerical experiments performed by the test Fortran program, and the numerical results confirmed that the PG-NEM effectively and accurately approximates the nonlinear dynamic problem

  19. Fingerprint elements scatter analysis on ancient chinese Ru porcelains samples

    International Nuclear Information System (INIS)

    Gao Zhengyao; Wang Jie; Chen Xiande

    1997-01-01

    Altogether 28 samples, mainly including glazes and bodies of ancient Chinese Ru porcelain, were analyzed by NAA technique and the contents of 36 elements were compared. The scatter analysis for nine fingerprint-elements indicates that almost all ancient Chinese Ru porcelain samples had nearly identical and long-term stable source of raw materials although they were fired in different kilns, at varying time and with distinct colors, and moreover, the source of raw materials for modern Ru porcelain seems to approach that for ancient one. The close provenance relation between ancient Jun porcelain and ancient Ru porcelain is also preliminarily verified. The glaze material of Jingdezhen white porcelain is totally different from all other samples. It shows that the former came from a separate source

  20. Simultaneous multi-element analysis of some edible pulses using neutron activation analysis

    International Nuclear Information System (INIS)

    El-Sweify, F.H.; Metwally, E.; Abdel-Khalik, H.

    2007-01-01

    This paper comprises the application of instrumental neutron activation analysis (INAA) for multi-element determination in some edible pulse samples. These edible pulses are usually daily used in the Egyptian kitchen. These were: anise, cumin, coriander, caraway, black cumin, white kidney bean, lupine, lentil, chickpea, broad bean, peanut, almond, and fenugreek. The pulses have been analyzed as dehulled pulses, in the case of legume and oil pulses with simultaneous analysis of their respective skins. The determined elements were: Ce, Co, Cr, Cs, Eu, Fe, Hf, Rb, Sb, Sc, Sr, Th and Zn. The element content in the dehulled pulses and their respective skins has been compared. Some elements were major or minor elements where others were trace elements. Standard reference materials were used to assure quality control, accuracy and precision of the technique. (author)

  1. The genetic analysis of heading time in hybrid rice IR54 and its early-maturity mutant-5460

    International Nuclear Information System (INIS)

    Zhou Yuanchang; Cai Junmai; Li Weiming

    1994-01-01

    V 20 A, IR 54 and its early mutant line 5460 were used as parents in three crosses. The heading time of radiation induced 5460 was 35(1986)∼40(1989) days earlier than that of IR 54 , and the F 1 plants of 5460/IR 54 showed a heading time close to that of their middle-parent. The segregation ratio of early-, intermediate- and late heading plants are given. From the segregation patterns, it may be assumed that three dominant genes, A,B and C, are involved and when they are combined, their complementary interaction expresses a late-heading phenotype which is strongly sensitive to photo-period. As V 20 A is previously suggested to have abC, it is expected that IR 54 has ABc, and 5460 has Abc. This means that gene b in 5460 is a single locus recessive mutation for early-maturity from gene B in IR 54

  2. Quantitative analysis of light elements in aerosol samples by PIGE

    International Nuclear Information System (INIS)

    Mateus, R.; Reis, M.A.; Jesus, A.P.; Ribeiro, J.P.

    2006-01-01

    Quantitative PIGE analysis of aerosol samples collected on nuclepore polycarbonate filters was performed by a method that avoids the use of comparative standards. Nuclear cross sections and calibration parameters established before in an extensive work on thick and intermediate samples were employed. For these samples, the excitation functions of nuclear reactions, induced by the incident protons on target's light elements, were used as input for a code that evaluates the gamma-ray yield integrating along the depth of the sample. In the present work we apply the same code to validate the use of an effective energy for thin sample analysis. Results pertaining to boron, fluorine and sodium concentrations are presented. In order to establish a correlation with sodium values, PIXE results related to chlorine are also presented, giving support to the reliability of this PIGE method for thin film analysis

  3. Storage and pre-neutron-activation-analysis treatment for trace-element analysis in urine

    International Nuclear Information System (INIS)

    Blotcky, A.J.; Rack, E.P.

    1985-01-01

    The problems regarding storage and pre-neutron-activation-analysis treatment for the elements aluminum, calcium, vanadium, selenium, copper, iodine, zinc, manganese, and magnesium in a urine matrix are reviewed. The type of collection and storage procedure and pre-neutron activation analysis treatment of urine depend on the specific trace element; that is, its inherent physical and chemical properties. Specifically polyethylene in teflon containers are the most suitable for general determinations. Whether any preservative is added would depend upon the stability of the trace element and its tendency for surface adsorption. Preferably, preservatives should contain no radioactivatable elements for maximum efficacy. Freeze drying or packing urine shipments under dry ice needs to be explored on an individual basis. Each pre- or post-neutron activation analysis treatment is specific and optimized for the trace element analyzed

  4. Strength Analysis on Ship Ladder Using Finite Element Method

    Science.gov (United States)

    Budianto; Wahyudi, M. T.; Dinata, U.; Ruddianto; Eko P., M. M.

    2018-01-01

    In designing the ship’s structure, it should refer to the rules in accordance with applicable classification standards. In this case, designing Ladder (Staircase) on a Ferry Ship which is set up, it must be reviewed based on the loads during ship operations, either during sailing or at port operations. The classification rules in ship design refer to the calculation of the structure components described in Classification calculation method and can be analysed using the Finite Element Method. Classification Regulations used in the design of Ferry Ships used BKI (Bureau of Classification Indonesia). So the rules for the provision of material composition in the mechanical properties of the material should refer to the classification of the used vessel. The analysis in this structure used program structure packages based on Finite Element Method. By using structural analysis on Ladder (Ladder), it obtained strength and simulation structure that can withstand load 140 kg both in static condition, dynamic, and impact. Therefore, the result of the analysis included values of safety factors in the ship is to keep the structure safe but the strength of the structure is not excessive.

  5. Tube Bulge Process : Theoretical Analysis and Finite Element Simulations

    International Nuclear Information System (INIS)

    Velasco, Raphael; Boudeau, Nathalie

    2007-01-01

    This paper is focused on the determination of mechanics characteristics for tubular materials, using tube bulge process. A comparative study is made between two different models: theoretical model and finite element analysis. The theoretical model is completely developed, based first on a geometrical analysis of the tube profile during bulging, which is assumed to strain in arc of circles. Strain and stress analysis complete the theoretical model, which allows to evaluate tube thickness and state of stress, at any point of the free bulge region. Free bulging of a 304L stainless steel is simulated using Ls-Dyna 970. To validate FE simulations approach, a comparison between theoretical and finite elements models is led on several parameters such as: thickness variation at the free bulge region pole with bulge height, tube thickness variation with z axial coordinate, and von Mises stress variation with plastic strain. Finally, the influence of geometrical parameters deviations on flow stress curve is observed using analytical model: deviations of the tube outer diameter, its initial thickness and the bulge height measurement are taken into account to obtain a resulting error on plastic strain and von Mises stress

  6. Distributed Finite Element Analysis Using a Transputer Network

    Science.gov (United States)

    Watson, James; Favenesi, James; Danial, Albert; Tombrello, Joseph; Yang, Dabby; Reynolds, Brian; Turrentine, Ronald; Shephard, Mark; Baehmann, Peggy

    1989-01-01

    The principal objective of this research effort was to demonstrate the extraordinarily cost effective acceleration of finite element structural analysis problems using a transputer-based parallel processing network. This objective was accomplished in the form of a commercially viable parallel processing workstation. The workstation is a desktop size, low-maintenance computing unit capable of supercomputer performance yet costs two orders of magnitude less. To achieve the principal research objective, a transputer based structural analysis workstation termed XPFEM was implemented with linear static structural analysis capabilities resembling commercially available NASTRAN. Finite element model files, generated using the on-line preprocessing module or external preprocessing packages, are downloaded to a network of 32 transputers for accelerated solution. The system currently executes at about one third Cray X-MP24 speed but additional acceleration appears likely. For the NASA selected demonstration problem of a Space Shuttle main engine turbine blade model with about 1500 nodes and 4500 independent degrees of freedom, the Cray X-MP24 required 23.9 seconds to obtain a solution while the transputer network, operated from an IBM PC-AT compatible host computer, required 71.7 seconds. Consequently, the $80,000 transputer network demonstrated a cost-performance ratio about 60 times better than the $15,000,000 Cray X-MP24 system.

  7. Optimized elemental analysis of fluorescence lamp shredder waste.

    Science.gov (United States)

    Hobohm, Julia; Kuchta, Kerstin; Krüger, Oliver; van Wasen, Sebastian; Adam, Christian

    2016-01-15

    Fluorescence lamps contain considerable amounts of rare earth elements (REE). Several recycling procedures for REE recovery from spent lamps have been established. However, despite their economic importance, the respective recycling is scarce so far, with an REE recovery rate of less than 1%. A reliable analysis of REE and other relevant metals like Yttrium is crucial for a thorough and complete recovery process. This applies both to the solid matter and aqueous phase, since most of the recycling processes include wet-chemical steps. We tested seven different reagent mixtures for microwave-assisted digestion of fluorescent lamp shredder, including hydrofluoric acid, perchloric acid, and hydrogen peroxide. We determined the concentrations of 25 of the most relevant rare earth and other trace elements (Al, P, Ti, V, Cr, Fe, Ni, Cu, Ga, Ge, As, Y, Ag, Cd, Sn, Sb, La, Ce, Eu, Gd, Tb, W, Au, Hg, and Pb) in the respective dilutions. Two independent digestions, one a mixture of perchlorid/nitric/hydrofluoric acid and the other aqua regia, showed the highest concentrations of 23 of these elements, excluding only Sn and Tb. The REE concentrations in the tested lamp shredder sample (stated in g/kg) were 10.2 (Y), 12.1 (La), 7.77 (Ce), 6.91 (Eu), 1.90 (Gd), and 4.11 (Tb). Copyright © 2015 Elsevier B.V. All rights reserved.

  8. Head of detector for multi-element analysis

    International Nuclear Information System (INIS)

    Frynta, Z.

    1983-01-01

    The detector head mounted on the scintillation counter consists of a hollow hexagonal rotary support axially arranged with the photomultiplier of the scintillation counter. In the walls of the hexagonal rotary support there are openings in which are inserted absorption filters. The mounting of the absorption filters on the rotary support allows the analysis of a greater number of elements without the dismantling of the head and the replacement of filters. The suitable geometry of the head is retained so that it is possible to insert the head into the hollows similarly as the scintillation counter. (J.P.)

  9. Neutron activation analysis of trace elements in rain water

    International Nuclear Information System (INIS)

    Luten, J.B.

    1977-01-01

    In this thesis the principles and practical aspects of activation analysis which are of direct importance in the analysis of rain water, are presented together with recent literature data on other techniques. Problems due to the storage of rain water samples are discussed. A multi-element method for the determination of trace elements in rain water by instrumental neutron activation analysis is described. Gamma ray spectrometry using Ge(Li) detectors offers the possibility to determine Na, Al, Cl, V, Mn, Co, Cu, Br and I in rain water samples of 2.5 ml after a 4-min irradiation in a thermal neutron flux of 5 x 10 13 n cm -2 s -1 . In residues of rain water samples of 100 ml, irradiated during 2 days in a thermal neutron flux of >5 x 10 13 n cm -2 s -1 Cr, Fe, Co, Zn and Sb can be determined after a cooling period of approximately 21 days. The detection limits are lower than those reported in previous investigations except for Cu. The precision is about 10% or better, except for Co, Cu and I. A routine method for the determination of bromine and iodine in rain water by n.a.a. is presented. The elements are isolated by isotope exchange between the irradiated sample and a solution of Br 2 or I 2 in CCl 4 . The method is not sensitive to the chemical species in which the halogen is present. Irradiation of solutions of iodine compounds in a high thermal neutron flux gives rise to the formation of iodate. Results of a further investigation of this phenomenon are given, as well as the determination of iodate in rain water by n.a.a. Iodate is separated by anion exchange. The combination of n.a.a. and solvent extraction is used for the determination of five trace elements (V, Co, Cu, Zn and In) in 10-ml rain water samples. For V, Co and Cu this method is more sensitive and reproducible than instrumental n.a.a. The results of the analysis of eleven sequential 30-ml samples from the beginning of the shower are presented as an illustration of possible applications of the

  10. Applications of finite-element scaling analysis in primatology.

    Science.gov (United States)

    Richtsmeier, J T

    1989-01-01

    The study of biological shape in three dimensions using landmark data can now be accomplished using several alternative methods. This report focuses on the use of finite-element scaling analysis in primate craniofacial morphology. The method is particularly useful in its ability to localize the differences between forms, thereby indicating those loci that differ most between specimens. Several examples of this feature are provided from primatological research. Particulars of the methods are also discussed in an attempt to provide the reader with cautionary knowledge for prudent application of the method in future research.

  11. Finite element analysis of reticulated ceramics under compression

    International Nuclear Information System (INIS)

    D’Angelo, Claudio; Ortona, Alberto; Colombo, Paolo

    2012-01-01

    Graphical abstract: - Abstract: This paper shows how finite element analysis can be used to study the effect of the morphological features of reticulated ceramics on their mechanical properties under compression. Quantitative morphological data, obtained by X-ray computed tomography (XCT) for a commercially available Si–SiC foam produced by the replica method, have been linked to a set of computer generated cells in which one morphological parameter was varied at a time. The findings indicate how the modification of some morphological features, which depend on the careful selection of appropriate and specific processing parameters, would enable the production of ceramic foams possessing higher strength for a given total porosity value.

  12. Eddy current analysis by the finite element circuit method

    International Nuclear Information System (INIS)

    Kameari, A.; Suzuki, Y.

    1977-01-01

    The analysis of the transient eddy current in the conductors by ''Finite Element Circuit Method'' is developed. This method can be easily applied to various geometrical shapes of thin conductors. The eddy currents on the vacuum vessel and the upper and lower support plates of JT-60 machine (which is now being constructed by Japan Atomic Energy Research Institute) are calculated by this method. The magnetic field induced by the eddy current is estimated in the domain occupied by the plasma. And the force exerted to the vacuum vessel is also estimated

  13. Sorption of redox-sensitive elements: critical analysis

    International Nuclear Information System (INIS)

    Strickert, R.G.

    1980-12-01

    The redox-sensitive elements (Tc, U, Np, Pu) discussed in this report are of interest to nuclear waste management due to their long-lived isotopes which have a potential radiotoxic effect on man. In their lower oxidation states these elements have been shown to be highly adsorbed by geologic materials occurring under reducing conditions. Experimental research conducted in recent years, especially through the Waste Isolation Safety Assessment Program (WISAP) and Waste/Rock Interaction Technology (WRIT) program, has provided extensive information on the mechanisms of retardation. In general, ion-exchange probably plays a minor role in the sorption behavior of cations of the above three actinide elements. Formation of anionic complexes of the oxidized states with common ligands (OH - , CO -- 3 ) is expected to reduce adsorption by ion exchange further. Pertechnetate also exhibits little ion-exchange sorption by geologic media. In the reduced (IV) state, all of the elements are highly charged and it appears that they form a very insoluble compound (oxide, hydroxide, etc.) or undergo coprecipitation or are incorporated into minerals. The exact nature of the insoluble compounds and the effect of temperature, pH, pe, other chemical species, and other parameters are currently being investigated. Oxidation states other than Tc (IV,VII), U(IV,VI), Np(IV,V), and Pu(IV,V) are probably not important for the geologic repository environment expected, but should be considered especially when extreme conditions exist (radiation, temperature, etc.). Various experimental techniques such as oxidation-state analysis of tracer-level isotopes, redox potential measurement and control, pH measurement, and solid phase identification have been used to categorize the behavior of the various valence states

  14. Sorption of redox-sensitive elements: critical analysis

    Energy Technology Data Exchange (ETDEWEB)

    Strickert, R.G.

    1980-12-01

    The redox-sensitive elements (Tc, U, Np, Pu) discussed in this report are of interest to nuclear waste management due to their long-lived isotopes which have a potential radiotoxic effect on man. In their lower oxidation states these elements have been shown to be highly adsorbed by geologic materials occurring under reducing conditions. Experimental research conducted in recent years, especially through the Waste Isolation Safety Assessment Program (WISAP) and Waste/Rock Interaction Technology (WRIT) program, has provided extensive information on the mechanisms of retardation. In general, ion-exchange probably plays a minor role in the sorption behavior of cations of the above three actinide elements. Formation of anionic complexes of the oxidized states with common ligands (OH/sup -/, CO/sup - -//sub 3/) is expected to reduce adsorption by ion exchange further. Pertechnetate also exhibits little ion-exchange sorption by geologic media. In the reduced (IV) state, all of the elements are highly charged and it appears that they form a very insoluble compound (oxide, hydroxide, etc.) or undergo coprecipitation or are incorporated into minerals. The exact nature of the insoluble compounds and the effect of temperature, pH, pe, other chemical species, and other parameters are currently being investigated. Oxidation states other than Tc (IV,VII), U(IV,VI), Np(IV,V), and Pu(IV,V) are probably not important for the geologic repository environment expected, but should be considered especially when extreme conditions exist (radiation, temperature, etc.). Various experimental techniques such as oxidation-state analysis of tracer-level isotopes, redox potential measurement and control, pH measurement, and solid phase identification have been used to categorize the behavior of the various valence states.

  15. Multi-element analysis of unidentified fallen objects from Tatale in ...

    African Journals Online (AJOL)

    A multi-element analysis has been carried out on two fallen objects, # 01 and # 02, using instrumental neutron activation analysis technique. A total of 17 elements were identified in object # 01 while 21 elements were found in object # 02. The two major elements in object # 01 were Fe and Mg, which together constitute ...

  16. Evaluation of oil thickness by neural network analysis of IR imagery

    International Nuclear Information System (INIS)

    Wood, P.; Strachan, I.; Davies, L.; Lunel, T.

    1997-01-01

    The feasibility of using neural network analysis of conventional thermal infra-red data gathered from surveillance aircraft to determine the thickness of oil at sea, was examined. Sea trial data was examined using Multi-Layer Perceptron neural network architecture, based on indications that it was the most appropriate configuration for determining oil thickness. Core input variables included oil brightness, time of day, sea brightness, wind speed, oil type, and sea temperature. Other variables, such as altitude, wave height, air temperature, camera gain, and others, did not appear to produce any significant difference in the prediction performance. By using only a restricted sea trial data set in training the network, it was found that it was possible to correctly classify about 80 per cent of the data into one of four thickness classes. Since there was no additional data available to validate the network, these results were considered encouraging, but not definitive. Additional data will be collected in planned future sea trials to further evaluate the accuracy of the trained network. 4 refs., 6 tabs., 4 figs

  17. IR thermographic observation and shear bands plasticity analysis in Fe-based metallic glass

    International Nuclear Information System (INIS)

    Bouzakher, B.; Benameur, T.; Sidhom, H.

    2009-01-01

    Infrared thermography observation and in situ atomic force microscopy characterization were carried out to investigate the mechanical damage processes at the edge-notch region of large ribbons of Fe 78 Si 10 B 12 metallic glass. An obvious thermoelastic and inelastic degradation phenomenon was observed ahead at the notched region of the specimens, which probably result from free volume accumulation process and shear band activity during plane stress solicitations. Moreover, AFM topographic and frictional analysis of changes in the crack path during stable crack propagation regime revealed a periodic morphology evolution, formation of nanoscale damage cavity in the range of 20-140 nm and a maximum temperature rise ahead of the pre-crack tip was found in the order of 1.5 deg. C. The nanometer scaled shear offset, discreteness and shear bands density were determined. While these key parameters play a role in observing a large plastic zone in front of the crack, however they are unable to explain the distinct intrinsic ductility of some monolithic metallic glasses. A general Mohr-Coulomb-type constitutive description was used to deduce analytic expressions for prediction of the variation of hydrostatic component of the applied stress to the shear stress ratio as function of Poisson's ratio.

  18. Rapid discrimination of sea buckthorn berries from different H. rhamnoides subspecies by multi-step IR spectroscopy coupled with multivariate data analysis

    Science.gov (United States)

    Liu, Yue; Zhang, Ying; Zhang, Jing; Fan, Gang; Tu, Ya; Sun, Suqin; Shen, Xudong; Li, Qingzhu; Zhang, Yi

    2018-03-01

    As an important ethnic medicine, sea buckthorn was widely used to prevent and treat various diseases due to its nutritional and medicinal properties. According to the Chinese Pharmacopoeia, sea buckthorn was originated from H. rhamnoides, which includes five subspecies distributed in China. Confusion and misidentification usually occurred due to their similar morphology, especially in dried and powdered forms. Additionally, these five subspecies have vital differences in quality and physiological efficacy. This paper focused on the quick classification and identification method of sea buckthorn berry powders from five H. rhamnoides subspecies using multi-step IR spectroscopy coupled with multivariate data analysis. The holistic chemical compositions revealed by the FT-IR spectra demonstrated that flavonoids, fatty acids and sugars were the main chemical components. Further, the differences in FT-IR spectra regarding their peaks, positions and intensities were used to identify H. rhamnoides subspecies samples. The discrimination was achieved using principal component analysis (PCA) and partial least square-discriminant analysis (PLS-DA). The results showed that the combination of multi-step IR spectroscopy and chemometric analysis offered a simple, fast and reliable method for the classification and identification of the sea buckthorn berry powders from different H. rhamnoides subspecies.

  19. Analysis of TRU waste for RCRA-listed elements

    International Nuclear Information System (INIS)

    Mahan, C.; Gerth, D.; Yoshida, T.

    1996-01-01

    Analytical methods for RCRA listed elements on Portland cement type waste have been employed using both microwave and open hot plate digestions with subsequent analysis by inductively coupled plasma atomic emission spectroscopy (ICP-AES), inductively coupled plasma mass spectrometry (ICP-AES), inductively coupled plasma mass spectrometry (ICP-MS), graphite furnace atomic absorption (GFAA) and cold vapor atomic absorption and fluorescence (CVAA/CVAFS). Four different digestion procedures were evaluated including an open hot plate nitric acid digestion, EPA SW-846 Method 3051, and 2 methods using modifications to Method 3051. The open hot plate and the modified Method 3051, which used aqua regia for dissolution, were the only methods which resulted in acceptable data quality for all 14 RCRA-listed elements. Results for the nitric acid open hot plate digestion were used to qualify the analytical methods for TRU waste characterization, and resulted in a 99% passing score. Direct chemical analysis of TRU waste is being developed at Los Alamos National Laboratory in an attempt to circumvent the problems associated with strong acid digestion methods. Technology development includes laser induced breakdown spectroscopy (LIBS), laser ablation inductively coupled plasma mass spectrometry (LA-ICPMS), dc arc CID atomic emission spectroscopy (DC-AES), and glow discharge mass spectrometry (GDMS). Analytical methods using the Portland cement matrix are currently being developed for each of the listed techniques. Upon completion of the development stage, blind samples will be distributed to each of the technology developers for RCRA metals characterization

  20. Thermomechanical finite element analysis of hot water boiler structure

    Directory of Open Access Journals (Sweden)

    Živković Dragoljub S.

    2012-01-01

    Full Text Available The paper presents an application of the Finite Elements Method for stress and strain analysis of the hot water boiler structure. The aim of the research was to investigate the influence of the boiler scale on the thermal stresses and strains of the structure of hot water boilers. Results show that maximum thermal stresses appear in the zone of the pipe carrying wall of the first reversing chamber. This indicates that the most critical part of the boiler are weld spots of the smoke pipes and pipe carrying plate, which in the case of significant scale deposits can lead to cracks in the welds and water leakage from the boiler. The nonlinear effects were taken into account by defining the bilinear isotropic hardening model for all boiler elements. Temperature dependency was defined for all relevant material properties, i. e. isotropic coefficient of thermal expansion, Young’s modulus, and isotropic thermal conductivity. The verification of the FEA model was performed by comparing the measured deformations of the hot water boiler with the simulation results. As a reference object, a Viessmann - Vitomax 200 HW boiler was used, with the installed power of 18.2 MW. CAD modeling was done within the Autodesk Inventor, and stress and strain analysis was performed in the ANSYS Software.

  1. Investigation of Apple Vibration Characteristics Using Finite Element Modal Analysis

    Directory of Open Access Journals (Sweden)

    R Mirzaei

    2013-02-01

    Full Text Available The most important quality indicator of fruits is the flesh firmness which is well correlated to their young’s modulus. In this research variation of vibration characteristics (shape modes, natural frequency of apple due to change of material characteristics (density, young's models, Poisson ratio and apple volume was investigated using Finite Element simulation. An image processing technique was used to obtain an unsymmetrical and non-spherical geometric model of apple. The exact three-dimensional shape of the fruit was created by determining the coordinates of apple surface and forming uneven rotational curvatures. Modal analysis with no boundary constraints has been applied. The first 20 Eigen frequencies and the corresponding mode shape were determined. Six rigid body modes possess zero resonant frequency which is related to the degree of freedom of a rigid body in space indicated the validity of finite element model. The modal analysis results showed that resonant frequency increased by increasing young's modulus of the fruit, while it decreased by increasing apple density. First mode torsion has a mean resonant frequency of 584 Hz. Variations of natural frequency due to change in young's modulus, density, and Poisson ratio were 80%, 11% and 4%, respectively. Coefficient of variation of resonant frequency in response to changing young's modulus was 2-3 times of that of density which shows the greatest effect of young modulus changes on natural frequency of fruits. Consequently with determination of fruits' natural frequency, their young modulus and firmness can be estimated.

  2. X-ray trace element analysis with positive ion beams

    International Nuclear Information System (INIS)

    Davis, R.H.

    1973-01-01

    A new trace element analysis having the advantage that many elements may be detected in a single measurement, based on positive charged particle induced X-ray florescence and on the production of X-rays by heavy ions, is described. Because of the large cross-sections for the production of discrete X-ray and the low yield of continuum radiation, positive charged particle X-ray florescence is a competitive, fast, analytic tool. In the experiment a beam of positive charged particles from an accelerator was directed toward a target. X-rays induced by the bombardment were detected by a Si(Li) detector the ouput from which was amplified and sorted in a multichannel analyzer. For rapid data handling and analysis, the multichannel analyzer or ADC unit was connected to an on-line computer. A large variety of targets prepared in collaboration with the oceanographers have been studied and spectra obtained for different particles having the same velocity are presented to show that the yield of discrete X-rays increases at least as rapidly as Z 2 . While protons of several MeV appear to be already competitive further advantage may be gained by heavy ions at lower energies since the continuum is reduced while the peak ''signals'' retain strength due to the Z 2 dependence. (S.B.)

  3. Multi-element neutron activation analysis of Brazilian coal samples

    International Nuclear Information System (INIS)

    Atalla, L.T.; Requejo, C.S.

    1982-09-01

    The elements U, Th, La, Ce, Nd, Sm, Eu, Dy, Tb, Yb, Lu, Sc, Ta, Hf, Co, Ni, Cr, Mo, Ti, V, W, In, Ga, Mn, Ba, Sr, Mg, Rb, Cs, K, Cl, Br, As, Sb, Au, Ca, Al and Fe were determined in coal samples by instrumental neutron activation analysis, by using both thermal and epithermal neutron irradiations. The irradiation times were 10 minutes and 8 or 16 hours in a position where the thermal neutron flux was about 10 12 n.cm - 2 .s - 1 and 72 non-consecutive hours for epithermal irradiation at a flux of about 10 11 n.Cm - 2 .s - 1 . After the instrumental analysis of the above mentioned elements, Zn and Se were determined with chemical separation. The relative standard deviation of, at least, 4 determinations was about + - 10% for the majority of the results. The coal samples analysed were supplied by: Cia. Estadual da Tecnologia e Saneamento Basico (CETESB-SP), Cia. de Pesquisas e Lavras Minerais (COPELMI-RS), Cia. Carbonifera Urussunga (SC), Cia. Carbonifera Prospera (SC), Cia. Carbonifera Treviso (SC), Cia. Nacional de Mineracao de Carvao do Barro Branco (SC) and Comissao Nacional de Energia Nuclear (CNEN-RJ). (Author) [pt

  4. Elemental analysis by IBA and NAA — A critical comparison

    Science.gov (United States)

    Watterson, J. I. W.

    1988-12-01

    In this review neutron activation analysis (NAA) and ion beam analysis (IBA) have been compared in the context of the entire field of analytical science using the discipline of scientometrics, as developed by Braun and Lyon. This perspective on the relative achievements of the two methods is modified by considering and comparing their particular attributes and characteristics, particularly in relation to their differing degree of maturity. This assessment shows that NAA, as the more mature method, is the most widely applied nuclear technique, but the special capabilities of IBA give it the ability to provide information about surface composition and elemental distribution that is unique, while it is still relatively immature and it is not yet possible to define its ultimate role with any confidence.

  5. Finite element analysis of elasto-plastic tee joints

    International Nuclear Information System (INIS)

    Powell, G.H.

    1974-09-01

    The theory and computational procedures used in the computer program B169TJ/EP for the analysis of elasto-plastic tee joints are described, and detailed user's guide is presented. The program is particularly applicable to joints conforming to the ANSI B16.9 Manufacturing Standard, but can also be applied to other joint geometries. The joint may be loaded by internal pressure and by arbitrary combinations of applied forces and moments at the ends of the branch and run pipes, and the loading sequence may be arbitrary. The joint material is assumed to yield according to the von Mises criterion, and to exhibit either linear kinematic hardening or nonlinear isotropic hardening after yield. The program makes use of the finite element and mesh generation procedures previously applied in the elastic stress analysis program B16.9TJ/ SA, with minor modifications. (U.S.)

  6. Biomonitoring of air pollution through trace element analysis

    International Nuclear Information System (INIS)

    Akoto Bamford, Samuel; Osae, E.K.; Serfor-Armah, Y.; Nyarko, B.; Ofosu, F.; Aboh, I.J.; Odamtten, G.T.

    2001-01-01

    Research work is currently going on to determine the suitability in the use of local lichen species for biomonitoring air pollution in Ghana. The study areas being investigated are the gold-mining areas situated in the Moist Evergreen and Semi-Deciduous forests in Ghana. The nuclear analytical techniques being used in this work are instrumental neutron activation analysis and tube-excited x-ray fluorescence spectrometry. The present report covers results of quality control exercise carried out to validate the quantitative methods being used. This includes our participation in an intercomparison exercise carried out among participants of the IAEA coordinated research project. The samples analyzed were two lichen samples from two completely different areas using neutron activation analysis. Only short- and medium-lived irradiations were carried out. Satisfactory results were obtained for most of the elements identified and quantified. (author)

  7. Development of environmental education system using online element analysis

    International Nuclear Information System (INIS)

    Niizeki, T.; Yoshihara, T.; Tsuchiya, K.; Kawasaki, K.; Komiya, K.

    2007-01-01

    We have constructed a network system which enables one to access and analyze environmental data obtained at different and distant laboratories. As a preliminary feasibility test of the system, we studied the elements in the water of the Tesio River using PIXE and ion chromatography. Students used the data online to carry out analysis via internet. We found two factors with different features in calcium from the factor analysis. The comparison of the specific result and relevant geology information has revealed a remarkable presence of Ca 2+ which might come from dissolution of limestone in the upper Tesio River. PIXE data gave crucial information to draw such a conclusion. The present system has been found useful in environmental education in universities, online sharing of PIXE data in particular. (author)

  8. Automatic measurement system for light element isotope analysis

    International Nuclear Information System (INIS)

    Satake, Hiroshi; Ikegami, Kouichi.

    1990-01-01

    The automatic measurement system for the light element isotope analysis was developed by installing the specially designed inlet system which was controlled by a computer. The microcomputer system contains specific interface boards for the inlet system and the mass spectrometer, Micromass 602 E. All the components of the inlet and the computer system installed are easily available in Japan. Ten samples can be automatically measured as a maximum of. About 160 minutes are required for 10 measurements of δ 18 O values of CO 2 . Thus four samples can be measured per an hour using this system, while usually three samples for an hour using the manual operation. The automatized analysis system clearly has an advantage over the conventional method. This paper describes the details of this automated system, such as apparatuses used, the control procedure and the correction for reliable measurement. (author)

  9. Seismic Analysis of Concrete Dam by Using Finite Element Method

    Directory of Open Access Journals (Sweden)

    Rozaina Ismail

    2017-01-01

    Full Text Available This paper reports a brief study on linear seismic analysis of Sg. Kinta Concrete Dam. The analysis was conducted in order to determine the performance and behaviour of the dam under seismic excitation. The dam was modelled as two-dimensional and developed based on the design drawing that is obtained from Angkasa Consulting Services Sdn. Bhd. The seismic analysis of the dam is conducted using finite element analysis software package LUSAS 14.3 and the dam has been analyse as a plain stress problem with a linear consideration. A set of historic data, with E1 Centro earthquake acceleration of about 0.50g is used as an earthquake excitation. The natural frequency and mode shape up to fifth mode of the dam has been obtained from the analysis to show the differences of the stress and deformation between each mode. The maximum horizontal and vertical stress of Sg. Kinta dam was found and the distribution of them was discussed in form of contours. The deformation of the dam were also been discussed by comparing the maximum displacement for each mode shaped.

  10. Toenail elemental analysis of Korean young adults by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Lee, O.

    2016-01-01

    The element contents in toenail clippings of healthy Korean young adults were measured using an instrumental neutron activation analysis. The average contents of elements such as Na, K, Cl, Ca, Fe, Se, and Zn are 449, 474, 1024, 1677, 66, 0.7 and 94 mg/kg in men, whereas those contents in women respectively 332, 476, 836, 1097, 66, 0.8 and 104 mg/kg. The correlation analysis of toenail elements with chronic disease risks showed positive associations between Na and serum HDL-cholesterol, blood pressure, and negative associations between Se and Hs-CRP, between Zn and hemoglobin level. (author)

  11. Multi-element analysis of emeralds and associated rocks by k0 neutron activation analysis

    International Nuclear Information System (INIS)

    Acharya, R.N.; Mondal, R.K.; Burte, P.P.; Nair, A.G.C.; Reddy, N.B.Y.; Reddy, L.K.; Reddy, A.V.R.; Manohar, S.B.

    2000-01-01

    Multi-element analysis was carried out in natural emeralds, their associated rocks and one sample of beryl obtained from Rajasthan, India. The concentrations of 21 elements were assayed by Instrumental Neutron Activation Analysis using the k 0 method (k 0 INAA method) and high-resolution gamma ray spectrometry. The data reveal the segregation of some elements from associated (trapped and host) rocks to the mineral beryl forming the gemstones. A reference rock standard of the US Geological Survey (USGS BCR-1) was also analysed as a control of the method

  12. A simplification of the deuterium oxide dilution technique using FT-IR analysis of plasma, for estimating piglet milk intake

    International Nuclear Information System (INIS)

    Glencross, B.D.; Tuckey, R.C.; Hartmann, P.E.; Mullan, B.P.

    1997-01-01

    Previous studies estimating milk intake using deuterium oxide (D 2 O) as a tracer have required sublimation of the sample fluid (usually plasma) to remove solids and retrieve total water. This procedure has been simplified by directly measuring the D 2 O content of plasma with a Fourier transform-infrared (FT-IR) spectrometer, removing the requirement for sample sublimation. Comparisons of samples that were split and then analysed as water of sublimation and as total plasma were performed. It was found that the direct analysis of the plasma could be achieved without a loss in fidelity of the results (sublimated v. plasma, r 2 = 0.976; n = 26). Linearity of assay standards was very high (r 2 > 0.997). The modified technique was used to determine the milk intake by piglets from litters of 7 sows during established lactation (Days 10-15). Water turnover (WTO) was shown to be the primary point by which differences in the piglet milk intakes were influenced. Differences in the milk composition had minimal effect on the milk intake determinations. Milk intake by each piglet was shown to be strongly correlated to piglet growth (r 2 = 0.59, P 2 = 0.84, P < 0.01). Copyright (1997) CSIRO Australia

  13. Fourier Transform Infrared Spectroscopy (FT-IR) and Simple Algorithm Analysis for Rapid and Non-Destructive Assessment of Developmental Cotton Fibers.

    Science.gov (United States)

    Liu, Yongliang; Kim, Hee-Jin

    2017-06-22

    With cotton fiber growth or maturation, cellulose content in cotton fibers markedly increases. Traditional chemical methods have been developed to determine cellulose content, but it is time-consuming and labor-intensive, mostly owing to the slow hydrolysis process of fiber cellulose components. As one approach, the attenuated total reflection Fourier transform infrared (ATR FT-IR) spectroscopy technique has also been utilized to monitor cotton cellulose formation, by implementing various spectral interpretation strategies of both multivariate principal component analysis (PCA) and 1-, 2- or 3-band/-variable intensity or intensity ratios. The main objective of this study was to compare the correlations between cellulose content determined by chemical analysis and ATR FT-IR spectral indices acquired by the reported procedures, among developmental Texas Marker-1 (TM-1) and immature fiber ( im ) mutant cotton fibers. It was observed that the R value, CI IR , and the integrated intensity of the 895 cm -1 band exhibited strong and linear relationships with cellulose content. The results have demonstrated the suitability and utility of ATR FT-IR spectroscopy, combined with a simple algorithm analysis, in assessing cotton fiber cellulose content, maturity, and crystallinity in a manner which is rapid, routine, and non-destructive.

  14. Finite element analysis of car hood for impact test by using ...

    African Journals Online (AJOL)

    Finite element analysis of car hood for impact test by using solidworks software ... high safety and at the same time can be built according to market demands. ... Keywords: finite element analysis; impact test; Solidworks; automation, car hood.

  15. Isolated Gramicidin Peptides Probed by IR Spectroscopy

    NARCIS (Netherlands)

    Rijs, A. M.; Kabelac, M.; Abo-Riziq, A.; Hobza, P.; de Vries, M. S.

    2011-01-01

    We report double-resonant IR/UV ion-dip spectroscopy of neutral gramicidin peptides in the gas phase. The IR spectra of gramicidin A and C, recorded in both the 1000 cm(-1) to 1800 cm(-1) and the 2700 to 3750 cm(-1) region, allow structural analysis. By studying this broad IR range, various local

  16. Trace element analysis of silicate rocks by XRF. Pt. 2

    International Nuclear Information System (INIS)

    Orihashi, Yuji; Yuhara, Masaki; Kagami, Hiroo; Honma, Hiroji

    1993-01-01

    Quantitative X-ray fluorescence analysis of six trace elements (Ce, Ba, Ga, Co, Cr, V) in silicate rocks has been investigated, using pressed powder pellets. Ga analysis was performed using a Cr tube, whereas a Au tube was used for the remaining five elements. Corrections were made for the interference of BaKα on CeKα, FeKβ on CoKα, CrKα on VKβ and VKα on TiKβ. Mass absorption functions were estimated from background intensities at 2θ=35.5deg and that of FeKα at wavelengths longer than the iron absorption edge for a Au tube, and from the value of net intensity/background one for a Cr tube. Calibration lines were constructed using twenty-four U.S. Geological Survey and Geological Survey of Japan igneous rock reference samples. For each line, the correction coefficient is greater than 0.993 except for Ga and Ce (>0.985), indicating that the correction and calibration procedures are appropriate for accurate analysis over a wide compositional range. Analytical results for igneous, sedimentary and metamorphic reference samples (U. S. Geological Survey, Institute of Geophysical and Geochemical Exploration, South-African Bureau of Standards) accord well with recommended or proposed values, respectively. The results of this study and those of Orihashi et al. (1993) show Ce, Ba, Nb, Zr, Y, Sr, Rb, Th, Ga, Zn, Cu, Ni, Co, Cr and V in silicate rocks can be quantitatively determined by XRF at ISEI. (author)

  17. Quantitative analysis of light elements in thick samples by PIGE

    International Nuclear Information System (INIS)

    Mateus, R.; Jesus, A.P.; Ribeiro, J.P.

    2004-01-01

    PIGE analysis of thick and intermediate samples is usually performed with the help of standards, but this method gives only good results when the standard is very similar to the sample to be analysed. In this work, we present an alternative method for PIGE analysis of light elements in thick samples. This method is based on a code that integrates the nuclear reaction excitation function along the depth of the sample. For the integration procedure the sample is divided in sublayers, defined by the energy steps that were used to measure accurately the excitation function. This function is used as input. Within each sublayer the stopping power cross-sections may be assumed as constant. With these two conditions the calculus of the contribution of each sublayer for the total yield becomes an easy task. This work presents results for the analysis of lithium, boron, fluorine and sodium in thick samples. For this purpose, excitation functions of the reactions 7 Li(p,p ' γ) 7 Li, 19 F(p,p ' γ) 19 F, 10 B(p,αγ) 7 Be and 23 Na(p,p ' γ) 23 Na were employed. Calculated γ-ray yields were compared, at several proton energy values, with experimental yields for thick samples made of inorganic compounds of the referred elements. The agreement is better than 7.5%. Taking into consideration the experimental uncertainty of the measured yields and the errors related to the stopping power values used, this agreement shows that effects as the beam energy straggling, ignored in the calculation, seem to play a minor role

  18. Finite element analysis of prestressed concrete reactor vessels

    International Nuclear Information System (INIS)

    Smith, P.D.; Cook, W.A.; Anderson, C.A.

    1977-01-01

    This paper discusses the development of a finite element code suitable for the safety analysis of prestressed concrete reactor vessels. The project has involved modification of a general purpose computer code to handle reinforced concrete structures as well as comparison of results obtained with the code against published experimental data. The NONSAP nonlinear structural analysis program was selected for the ease with which it can be modified to encompass problems peculiar to nuclear reactors. Pre- and post-processors have been developed for mesh generation and for graphical display of response variables. An out-of-core assembler and solver have been developed for the analysis of large three dimensional problems. The constitutive model for short term loads forms an orthotropic stress-strain relationship in which the concrete and the reinforcing steel are treated as a composite. The variation of stiffness and strength of concrete under multiaxial stress states is accounted for. Cracks are allowed to form at element integration points based on a three dimensional failure envelope in stress space. Composite tensile and shear properties across a crack are modified to account for bond degradation and for dowel action of the reinforcement. The constitutive law for creep is base on the expansion of the usual creep compliance function in the form of a Dirichlet exponential series. Empirical creep data are then fit to the Dirichlet series approximation by means of a least squares procedure. The incremental deformation process is subsequently reduced to a series of variable stiffness elasticity problems in which the past stress history is represented by a finite number of hidden material variables

  19. Neutron activation analysis for uranium and associated elements

    International Nuclear Information System (INIS)

    Bowman, W.W.

    1977-01-01

    The samples obtained by the Savannah River Laboratory as part of the National Uranium Resource Evaluation program are activated in the intense neutron flux from a Savannah River Plant production reactor. A pilot-scale facility was installed at the reactor site to provide analyses of samples through the initial phase of the program and to develop design data for a full-scale facility. Sediments are analyzed by direct activation of 0.5-g samples. However, to analyze ground or surface water samples, mineral elements from 1-liter samples are concentrated on ion exchange resin and then approximately 5-g samples of resin are activated. Uranium concentration is determined by counting neutrons emitted from specific short-lived products of fission induced in 235 U by the primary neutron flux. Repetitive short cycles of irradiation and counting permit detection and determination of <0.1 μg of uranium. Elements associated with uranium are determined by spectral analysis of the gamma ray activities induced by the cyclic and subsequent longer irradiations. The pilot facility consists of four irradiation positions (plus 2 spare positions), a sample loader and unloader, and counting stations with neutron and gamma ray detectors, all interconnected with a pneumatic sample transport system. A computer controls both the transport system and the data acquisition devices. Gamma ray counting data are stored on magnetic tape for further processing by a large central computer. Facility hardware and software are described. Repetitive analyses of standards have shown an accuracy within +-10% for uranium values and within +-25% for associated elements. A quality assurance program has been developed to maintain these levels of reliability

  20. PIXE-quantified AXSIA: Elemental mapping by multivariate spectral analysis

    International Nuclear Information System (INIS)

    Doyle, B.L.; Provencio, P.P.; Kotula, P.G.; Antolak, A.J.; Ryan, C.G.; Campbell, J.L.; Barrett, K.

    2006-01-01

    Automated, nonbiased, multivariate statistical analysis techniques are useful for converting very large amounts of data into a smaller, more manageable number of chemical components (spectra and images) that are needed to describe the measurement. We report the first use of the multivariate spectral analysis program AXSIA (Automated eXpert Spectral Image Analysis) developed at Sandia National Laboratories to quantitatively analyze micro-PIXE data maps. AXSIA implements a multivariate curve resolution technique that reduces the spectral image data sets into a limited number of physically realizable and easily interpretable components (including both spectra and images). We show that the principal component spectra can be further analyzed using conventional PIXE programs to convert the weighting images into quantitative concentration maps. A common elemental data set has been analyzed using three different PIXE analysis codes and the results compared to the cases when each of these codes is used to separately analyze the associated AXSIA principal component spectral data. We find that these comparisons are in good quantitative agreement with each other

  1. Finite element analysis of 2-Station hip himulator

    Science.gov (United States)

    Fazli, M. I. M.; Yahya, A.; Shahrom, A.; Nawawi, S. W.; Zainudin, M. R.; Nazarudin, M. S.

    2017-10-01

    This paper presented the analysis of materials and design architecture of 2-station hip simulator. Hip simulator is a machine used to conduct the joint and wear test of hip prosthetic. In earlier work, the hip simulator was modified and some improvement were made by using SolidWorks software. The simulator consists of 3DOF which controlled by separate stepper motor and a static load that set up by manual method in each station. In this work, finite element analysis (FEA) of hip simulator was implemented to analyse the structure of the design and selected materials used for simulator component. The analysis is completed based on two categories which are safety factor and stress tests. Both design drawing and FEA was done using SolidWorks software. The study of the two categories is performed by applying the peak load up to 4000N on the main frame that is embedded with metal-on-metal hip prosthesis. From FEA, the value of safety factor and degree of stress formation are successfully obtained. All the components exceed the value of 2 for safety factor analysis while the degree of stress formation shows higher value compare to the yield strength of the material. With this results, it provides information regarding part of simulator which are susceptible to destruct. Besides, the results could be used for design improvement and certify the stability of the hip simulator in real application.

  2. Storage element performance optimization for CMS analysis jobs

    International Nuclear Information System (INIS)

    Behrmann, G; Dahlblom, J; Guldmyr, J; Happonen, K; Lindén, T

    2012-01-01

    Tier-2 computing sites in the Worldwide Large Hadron Collider Computing Grid (WLCG) host CPU-resources (Compute Element, CE) and storage resources (Storage Element, SE). The vast amount of data that needs to processed from the Large Hadron Collider (LHC) experiments requires good and efficient use of the available resources. Having a good CPU efficiency for the end users analysis jobs requires that the performance of the storage system is able to scale with I/O requests from hundreds or even thousands of simultaneous jobs. In this presentation we report on the work on improving the SE performance at the Helsinki Institute of Physics (HIP) Tier-2 used for the Compact Muon Experiment (CMS) at the LHC. Statistics from CMS grid jobs are collected and stored in the CMS Dashboard for further analysis, which allows for easy performance monitoring by the sites and by the CMS collaboration. As part of the monitoring framework CMS uses the JobRobot which sends every four hours 100 analysis jobs to each site. CMS also uses the HammerCloud tool for site monitoring and stress testing and it has replaced the JobRobot. The performance of the analysis workflow submitted with JobRobot or HammerCloud can be used to track the performance due to site configuration changes, since the analysis workflow is kept the same for all sites and for months in time. The CPU efficiency of the JobRobot jobs at HIP was increased approximately by 50 % to more than 90 %, by tuning the SE and by improvements in the CMSSW and dCache software. The performance of the CMS analysis jobs improved significantly too. Similar work has been done on other CMS Tier-sites, since on average the CPU efficiency for CMSSW jobs has increased during 2011. Better monitoring of the SE allows faster detection of problems, so that the performance level can be kept high. The next storage upgrade at HIP consists of SAS disk enclosures which can be stress tested on demand with HammerCloud workflows, to make sure that the I

  3. In-situ elemental analysis of coal by neutron activation

    International Nuclear Information System (INIS)

    Mikesell, J.L.; Senftle, F.E.; Tanner, A.B.

    1986-01-01

    The U.S. Geological Survey (USGS) has worked to develop neutron techniques for the borehole measurement of the elemental composition of ores since 1969, and first demonstrated a borehole ultimate analysis of coal in 1977. Borehole measurements such as these permit real-time evaluation of coal quality without the expense of coring or the delays associated with laboratory analyses. Two technological innovations make such measurements possible: the availability, from Savannah River Operations Office, DOE, of small californium-252 (/sup 252/Cf) fission neutron sources, and the development, by USGS and Princeton Gamma-Techn, of the melting-cryogen-cooled high-purity germanium borehole gamma-ray detector. A technique of relating mass fractions to measured gamma-ray intensities, which eliminates the need for detailed knowledge of the geometry of the neutron distribution, is used to calculate elemental compositions without resorting to the test pits or computer borehole modeling. In coal, all of the major constituents (C, H, N, S, Si, Al, Fe, Ti) except oxygen can be determined quantitatively by thermal neutron capture gamma-ray spectroscopy

  4. Essential trace elements in edible mushrooms by Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Moura, Patricia L.C.; Maihara, Vera A.; Castro, Lilian P. de [Instituto de Pesquisa e Energetica e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)]. E-mail: patricialandim@ig.com.br; vmaihara@ipen.br; lilian.Pavanelli@terra.com.br; Figueira, Rubens C.L. [Universidade Cruzeiro do Sul, Sao Paulo, SP (Brazil)]. E-mail: figueiraru@yahoo.com.br

    2007-07-01

    Mushrooms are excellent nutritional sources since they provide proteins, fibers and mineral, such as K, P, Fe. They have also been the focus of medical research. In Brazil mushrooms are not consumed in large quantities by the general population since people know little about the nutritional and medicinal benefits that mushrooms offer. Hence, this study intends to contribute to a better understanding of the essential element content in edible mushrooms, which are currently commercialized in Sao Paulo state. Br Fe, K, Na and Zn concentrations were determined by Instrumental Neutron Activation Analysis in the following mushroom species: Shitake (Lentinus edodes), Shimeji (Pleurotus ssp), Paris Champignon (Agaricus bisporus), Hiratake ( Pleurotus ssp) and Eringue (Pleurotus Eryngu. The mushroom samples were acquired from commercial establishments in the city of Sao Paulo and directly from the producers. Essential element contents in mushrooms varied between Br 0.03 to 4.1 mg/kg; Fe 20 to 267 mg/kg; K 1.2 to 5.3 g/kg, Na 10 to 582 mg/kg and Zn 60 to 120 mg/kg. The results confirm that mushrooms can be considered a good source of K, Fe and Zn. The low Na level is a good nutritional benefit for the consumer. (author)

  5. Two-Dimensional Nonlinear Finite Element Analysis of CMC Microstructures

    Science.gov (United States)

    Mital, Subodh K.; Goldberg, Robert K.; Bonacuse, Peter J.

    2012-01-01

    A research program has been developed to quantify the effects of the microstructure of a woven ceramic matrix composite and its variability on the effective properties and response of the material. In order to characterize and quantify the variations in the microstructure of a five harness satin weave, chemical vapor infiltrated (CVI) SiC/SiC composite material, specimens were serially sectioned and polished to capture images that detailed the fiber tows, matrix, and porosity. Open source quantitative image analysis tools were then used to isolate the constituents, from which two dimensional finite element models were generated which approximated the actual specimen section geometry. A simplified elastic-plastic model, wherein all stress above yield is redistributed to lower stress regions, is used to approximate the progressive damage behavior for each of the composite constituents. Finite element analyses under in-plane tensile loading were performed to examine how the variability in the local microstructure affected the macroscopic stress-strain response of the material as well as the local initiation and progression of damage. The macroscopic stress-strain response appeared to be minimally affected by the variation in local microstructure, but the locations where damage initiated and propagated appeared to be linked to specific aspects of the local microstructure.

  6. Obtaining local reciprocal lattice vectors from finite-element analysis.

    Science.gov (United States)

    Sutter, John P; Connolley, Thomas; Hill, Tim P; Huang, Houcheng; Sharp, Doug W; Drakopoulos, Michael

    2008-11-01

    Finite-element analysis is frequently used by engineers at synchrotron beamlines to calculate the elastic deformation of a single crystal undergoing mechanical bending or thermal load. ANSYS Workbench software is widely used for such simulations. However, although ANSYS Workbench software provides useful information on the displacements, strains and stresses within the crystal, it does not yield the local reciprocal lattice vectors that would be required for X-ray diffraction calculations. To bridge this gap, a method based on the shape functions and interpolation procedures of the software itself has been developed. An application to the double-crystal bent Laue monochromator being designed for the I12 (JEEP) wiggler beamline at the Diamond Light Source is presented.

  7. Elements of Constitutive Modelling and Numerical Analysis of Frictional Soils

    DEFF Research Database (Denmark)

    Jakobsen, Kim Parsberg

    of a constitutive model for soil is based on a profound knowledge of the soil behaviour upon loading. In the present study it is attempted to get a better understanding of the soil behaviour bv performing a number of triaxial compression tests on sand. The stress-strain behaviour of sand depends strongly......This thesis deals with elements of elasto-plastic constitutive modelling and numerical analysis of frictional soils. The thesis is based on a number of scientific papers and reports in which central characteristics of soil behaviour and applied numerical techniques are considered. The development...... and subsequently dilates during shear. The change in the volumetric behaviour of the soil skeleton is commonly referred to as the characteristic state. The stress ratio corresponding to the characteristic state is independent of the mean normal effective stress and the relative density, but depends on the stress...

  8. Finite element analysis of mechanical stability of coarsened nanoporous gold

    International Nuclear Information System (INIS)

    Cho, Hoon-Hwe; Chen-Wiegart, Yu-chen Karen; Dunand, David C.

    2016-01-01

    The mechanical stability of nanoporous gold (np-Au) at various stages of thermal coarsening is studied via finite element analysis under volumetric compression using np-Au architectures imaged via X-ray nano-tomography. As the np-Au is coarsened thermally over ligament sizes ranging from 185 to 465 nm, the pore volume fraction is determinant for the mechanical stability of the coarsened np-Au, unlike the curvature and surface orientation of the ligaments. The computed Young's modulus and yield strength of the structures are compared with the Gibson–Ashby model. The geometry of the structures determines the locations where stress concentrations occur at the onset of yielding.

  9. Neutron activation analysis of trace elements in biological tissue

    Energy Technology Data Exchange (ETDEWEB)

    Velandia, J A; Perkons, A K

    1974-01-01

    Thermal Neutron Activation Analysis with Instrumental Ge(Li) Gamma Spectrometry was used to determine the amounts of more than 30 trace constituents in heart tissue of rats and kidney tissue of rabbits. The results were confirmed by a rapid ion-exchange group separation method in the initial stages of the experiments. The samples were exposed to thermal neutrons for periods between 3 minutes and 14 hours. Significant differences in the amounts and types of trace elements in the two different tissue types are apparent, however, are probably due to specific diets. Tables of relevant nuclear data, standard concentrations, radiochemical separation recoveries, and quantitative analytical results are presented. The ion-exchange group separation scheme and typical examples of the instrumental gamma ray spectra are shown. The techniques developed in this study are being used for a large scale constituent survey of various diseased and healthy human tissues.

  10. Studying apple bruise using a finite element method analysis

    Science.gov (United States)

    Pascoal-Faria, P.; Alves, N.

    2017-07-01

    Apple bruise damage from harvesting, handling, transporting and sorting is considered to be the major source of reduced fruit quality, resulting in a loss of profits for the entire fruit industry. Bruising is defined as damage and discoloration of fruit flesh, usually with no breach of the skin. The three factors which can physically cause fruit bruising are vibration, compression load and impact. The last one is the main source of bruise damage. Therefore, prediction of the level of damage, stress distribution and deformation of the fruits under external force has become a very important task. To address these problems a finite element analysis has been developed for studying Portuguese Royal Gala apple bruise. The results obtained will be suitable to apple distributors and sellers and will allow a reduction of the impact caused by bruise damage in apple annual production.

  11. Model order reduction techniques with applications in finite element analysis

    CERN Document Server

    Qu, Zu-Qing

    2004-01-01

    Despite the continued rapid advance in computing speed and memory the increase in the complexity of models used by engineers persists in outpacing them. Even where there is access to the latest hardware, simulations are often extremely computationally intensive and time-consuming when full-blown models are under consideration. The need to reduce the computational cost involved when dealing with high-order/many-degree-of-freedom models can be offset by adroit computation. In this light, model-reduction methods have become a major goal of simulation and modeling research. Model reduction can also ameliorate problems in the correlation of widely used finite-element analyses and test analysis models produced by excessive system complexity. Model Order Reduction Techniques explains and compares such methods focusing mainly on recent work in dynamic condensation techniques: - Compares the effectiveness of static, exact, dynamic, SEREP and iterative-dynamic condensation techniques in producing valid reduced-order mo...

  12. Finite element analysis on badminton racket design parameters

    CERN Document Server

    Nasruddin, Fakhrizal Azmy; Syahrom, Ardiyansyah; Abdul Kadir, Mohammed Rafiq; Omar, Abdul Hafidz; Öchsner, Andreas

    2016-01-01

    This work identifies the characteristics of racket design parameters that influence racket performance.  It presents the finite element analysis of several designs of badminton rackets and compares them to experimental results for validation. Designing a racket requires a comprehensive understanding of racket performance characteristics. Essentially, racket performance is related to the sweet spot, which is the spot on the racket head that produces the most power and control when it strikes a shuttlecock. Determining a coefficient of restitution can help to identify the sweet spot on a racket. By analyzing several head shape designs, it becomes apparent that isometric head shape rackets produce better coefficients of restitution compared to oval and round ones. It is recommended that the racket design consist of low string tension, stiffer racket shafts and bigger head size in order to produce higher shuttlecock speed.

  13. Instrumental Neutron Activation Analysis in archaeology interpretation beyond elemental abundance

    International Nuclear Information System (INIS)

    Bishop, Ronald L.

    2001-01-01

    Application of instrumental neutron activation analysis to the study of archaeological ceramics involves the determination of the source or sources used to produce pottery. Groups of relatively homogeneous elemental abundances are shown to be statically distinct from one another often leading to the assesment of what was locally produced and what was imported to a site. These assesment, however are among the most preliminary interpretations. Archaeology is concerned with the reasons for artificial distributions and how and why the distribution varied through time 3 reasons that include the social and political basis of ancient economics and how these responded to other factors, such as ideology. These objectives are addressed through the increasing refinement of compositional groups leading toward greater specificity of attribution. In so doing the role of analytical precision among other considerations groves in importance. This paper illustration some of these considerations with examples from the U.S. southwest, the Maya region of southern mexico, and lower central America

  14. Heterogeneous modelling and finite element analysis of the femur

    Directory of Open Access Journals (Sweden)

    Zhang Binkai

    2017-01-01

    Full Text Available As the largest and longest bone in the human body, the femur has important research value and application prospects. This paper introduces a fast reconstruction method with Mimics and ANSYS software to realize the heterogeneous modelling of the femur according to Hu distribution of the CT series, and simulates it in various situations by finite element analysis to study the mechanical characteristics of the femur. The femoral heterogeneous model shows the distribution of bone mineral density and material properties, which can be used to assess the diagnosis and treatment of bone diseases. The stress concentration position of the femur under different conditions can be calculated by the simulation, which can provide reference for the design and material selection of prosthesis.

  15. Elemental analysis of artefacts - establishing external beam PIXE

    International Nuclear Information System (INIS)

    Alves, A.; Johnston, P.; Short, R.; Bubb, I.

    1999-01-01

    The development of an external PIXE facility on the 1 MV Tandetron accelerator at RMIT has led to a wide range of research possibilities. A proton beam, generated inside a vacuum is brought into air via an Au coated Kapton foil exit window (thickness 8μm, diameter 0.35mm). Monitoring of the beam intensity is achieved by detecting backscattered protons from the inside Au coating on the window. Artefacts, which may be too large to be placed inside the vacuum, are positioned in the beamline opposite the exit window. An optical system consisting of a CCD camera, alignment laser and two mirrors allows viewing of a region of the target 10mm x 10mm. This technique provides quantitative analysis of elements in the pigments used in paintings and on ceramics, which is a valuable tool in art conservation and authentication. Application of the technique to a ceramic sample from the historic house 'Viewbank' is described

  16. Overview of adaptive finite element analysis in computational geodynamics

    Science.gov (United States)

    May, D. A.; Schellart, W. P.; Moresi, L.

    2013-10-01

    The use of numerical models to develop insight and intuition into the dynamics of the Earth over geological time scales is a firmly established practice in the geodynamics community. As our depth of understanding grows, and hand-in-hand with improvements in analytical techniques and higher resolution remote sensing of the physical structure and state of the Earth, there is a continual need to develop more efficient, accurate and reliable numerical techniques. This is necessary to ensure that we can meet the challenge of generating robust conclusions, interpretations and predictions from improved observations. In adaptive numerical methods, the desire is generally to maximise the quality of the numerical solution for a given amount of computational effort. Neither of these terms has a unique, universal definition, but typically there is a trade off between the number of unknowns we can calculate to obtain a more accurate representation of the Earth, and the resources (time and computational memory) required to compute them. In the engineering community, this topic has been extensively examined using the adaptive finite element (AFE) method. Recently, the applicability of this technique to geodynamic processes has started to be explored. In this review we report on the current status and usage of spatially adaptive finite element analysis in the field of geodynamics. The objective of this review is to provide a brief introduction to the area of spatially adaptive finite analysis, including a summary of different techniques to define spatial adaptation and of different approaches to guide the adaptive process in order to control the discretisation error inherent within the numerical solution. An overview of the current state of the art in adaptive modelling in geodynamics is provided, together with a discussion pertaining to the issues related to using adaptive analysis techniques and perspectives for future research in this area. Additionally, we also provide a

  17. A Finite Element Analysis of Optimal Variable Thickness Sheets

    DEFF Research Database (Denmark)

    Petersson, Joakim S

    1996-01-01

    A quasimixed Finite Element (FE) method for maximum stiffness of variablethickness sheets is analysed. The displacement is approximated with ninenode Lagrange quadrilateral elements and the thickness is approximated aselementwise constant. One is guaranteed that the FE displacement solutionswill ...

  18. Analysis of trace elements in chicken embryo cells

    International Nuclear Information System (INIS)

    Qiu Zhijun; Wang Jiqing; Guo Panlin; Li Xiaolin; Zhu Jieqing; Lu Rongrong

    2002-01-01

    A scanning proton microprobe (SPM) with high resolution and high sensitivity was applied to analyze trace elements in chicken embryo forebrain neutron cell and skeletal muscle myotube cell. The absorption of the two different cells to zinc ions, correlation of elements and trace elemental distributions in the cells were studied. The results indicate that the absorptive capacity of the chicken embryo forebrain neuron cell to zinc ions is larger than that of the chicken embryo skeletal muscle myotube cell, and the concentrations of intracellular trace elements such as Cr, Fe, Ni are explicitly higher. The correlations of elements such as S and Zn or Fe and Zn are positive, but the correlations of P and Ni or Cr and Fe are negative. From the maps of cellular elemental distribution the contents of the different elements are different in the intracellular parts, for example, the contents of the elements phosphorus, sulfur, potassium in the cell membranes are higher than that in the cells

  19. Finite element analysis of a crankshaft of diesel engine

    International Nuclear Information System (INIS)

    Bannikiv, M.G.

    2005-01-01

    This research was a part of the project aimed at the increase in power of the direct injection turbocharged twelve- cylinder V-type diesel engine. Crankshaft of a high power high speed diesel engine is subjected to complex loading conditions and undergoes high cyclic loads of the order of 107 to 108 cycles. Therefore, durability of this component is of critical importance. Strength analysis was based on the assessment of factor of safety (FOS) of the engine augmented by brake mean effective pressure (bmep) and/or engine speed. In the first part of the study, mechanical loads due to gas pressure and inertia forces were obtained from engine cycle simulation. Relationships for displacement, velocity and acceleration of an articulated connecting rod piston as a function of engine geometry and crank angle were derived. In the second part, the range of bmep and engine speed was determined over which engine performance is satisfactory on the basis of fatigue. It was shown that with limitations imposed (unchanged design and material of the crankshaft) the crankshaft of the given engine can withstand increase in power up to 15%. It was recommended, that required increase in engine power should be realized by the increase in bmep, since the increase in engine speed would deteriorate combustion efficiency. Finite Element Analysis was used to verify stresses calculations. New features of procedure used and relationships obtained in this research apply to strength analysis of other types of internal combustion engines. (author)

  20. Comparative analysis of regulatory elements in different germin-like ...

    African Journals Online (AJOL)

    It was observed that these promoters have important regulatory elements, which are involved in various important functions. These elements have been compared on the basis of location, copy number, and distributed on positive and negative strands. It was also observed that some of these elements are common and ...

  1. Analysis of elements present in beers and brewing waters by neutron activation analysis

    International Nuclear Information System (INIS)

    Krausova, Ivana; Kucera, Jan; Dostalek, Pavel; Potesil, Vaclav

    2011-01-01

    Neutron activation analysis (NAA) was used for determination of Si, Na, K, Ca, Sc, V, Cr, Mn, Fe, Co, Zn, Rb, Cs, and La in Czech beers and brewing waters. The Si concentration in beer determined by the reaction 29 Si(n,p) 29 Al with fast neutrons confirmed that beer is an important Si source in human diet. Determination of other trace elements by NAA with the whole spectrum of reactor neutrons aimed at the feasibility of identification of Gambrinus beers brewed in various breweries. The elements Ca and V appeared to be the best candidates for this purpose. The concentrations of elements determined by NAA were also compared with the recommended daily element intake for humans. The accuracy of the method was proved by analysis of reference materials, specifically NIST SRM 2704 Buffalo River Sediment, NIST SRM 1633b Coal Fly Ash, and NIST SRM 1515 Apple Leaves. (author)

  2. Elemental analysis of two Egyptian iron ores and produced industrial iron samples by neutron activation analysis

    International Nuclear Information System (INIS)

    Sroor, A.; Abdel-Basset, N.; Abdel-Haleem, A.S.; Hassan, A.M.

    2001-01-01

    Elemental analysis of two iron ores and initial industrial iron production prepared by the Egyptian Iron and Steel Company of Helwan near Cairo were performed by the instrumental neutron activation analysis technique. Five samples of each type were irradiated for 48 h in a thermal neutron flux of 4x10 12 n/cm 2 s in the first Egyptian research reactor ET-RR-1. Also, the Pneumatic Irradiation Rabbit System (PIRS), attached to the reactor ET-RR-1 in Inshass, was used to measure short-life elements. The γ-ray spectra were obtained with a hyper pure germanium detection system. The concentration percentage values of major, minor and trace elements are presented. Implications of the elemental concentration values obtained are presented

  3. Neutron activation analysis as applied to instrumental analysis of trace elements from seawater

    International Nuclear Information System (INIS)

    Boniforti, R.; Moauro, A.; Madaro, M.

    1983-01-01

    Particulate matter collected from the coastal area delimited by the mouth of the river Volturno and the Sabaudia lake has been analyzed by instrumental neutron activation analysis for its content of twenty-two trace elements. The results for surface water and bottom water are reported separately, thus evidencing the effect of sampling depth on the concentration of many elements. The necessity of accurately 'cleaning' the filters before use is stressed

  4. Elemental analysis of Uranouchi bay seabed sludge using PIXE

    International Nuclear Information System (INIS)

    Kabir, M. Hasnat; Narusawa, Tadashi; Nishiyama, Fumitaka; Sumi, Katsuhiro

    2006-01-01

    Elemental analyses were carried out for the seabed sludge collected from Uranouchi bay (Kochi, Japan) using Particle Induced X-ray Emission (PIXE). Seabed-sludge contamination with heavy metals as well as toxic elements becomes one of the most serious environmental problems. The aim of the present study is to investigate the polluted areas in the bay by heavy and toxic elements. As a results of analyses of samples collected from eleven different places in the bay, seventeen elements including toxic ones were detected. The results suggest that the center region of the bay is seriously contaminated by heavy and toxic elements in comparison with the other areas in the bay. (author)

  5. [Principal component analysis and cluster analysis of inorganic elements in sea cucumber Apostichopus japonicus].

    Science.gov (United States)

    Liu, Xiao-Fang; Xue, Chang-Hu; Wang, Yu-Ming; Li, Zhao-Jie; Xue, Yong; Xu, Jie

    2011-11-01

    The present study is to investigate the feasibility of multi-elements analysis in determination of the geographical origin of sea cucumber Apostichopus japonicus, and to make choice of the effective tracers in sea cucumber Apostichopus japonicus geographical origin assessment. The content of the elements such as Al, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Mo, Cd, Hg and Pb in sea cucumber Apostichopus japonicus samples from seven places of geographical origin were determined by means of ICP-MS. The results were used for the development of elements database. Cluster analysis(CA) and principal component analysis (PCA) were applied to differentiate the sea cucumber Apostichopus japonicus geographical origin. Three principal components which accounted for over 89% of the total variance were extracted from the standardized data. The results of Q-type cluster analysis showed that the 26 samples could be clustered reasonably into five groups, the classification results were significantly associated with the marine distribution of the sea cucumber Apostichopus japonicus samples. The CA and PCA were the effective methods for elements analysis of sea cucumber Apostichopus japonicus samples. The content of the mineral elements in sea cucumber Apostichopus japonicus samples was good chemical descriptors for differentiating their geographical origins.

  6. Neutron activation analysis of trace elements in foodstuffs

    International Nuclear Information System (INIS)

    Schelenz, R.; Bayat, I.; Fischer, E.

    1976-05-01

    For the determination of trace elements in foodstuffs with the aid of neutron activation analysis the separation of volatile radionuclides after digestion of the sample is of special interest for radiochemical processing. A distillation procedure was developed to give reproducable results, however optimal conditions were not found for all volatile radionuclides studied. The required selective separation of Br-82 from the distillate was best achieved by the application of an ion-exchange column-chromatography technique. The computer programs for the evaluation of complex gamma spectra have been developed further. The automatic peak search and peak area determination is based on a computer program using the correlation technique and carried out with a mini-computer coupled with a multi-channel gamma spectrometer. The results, which are presented in 3 earlier reports relating to this research program, reveal the advantages and disadvantages of the individual steps of the radiochemical separation scheme. Before neutron activation analysis can be introduced on a routine basis, some aspects of the radiochemical process remain to be tested; these studies will be published in a fourth and final report. (orig.) [de

  7. Finite Element Analysis of Patella Alta: A Patellofemoral Instability Model.

    Science.gov (United States)

    Watson, Nicole A; Duchman, Kyle R; Grosland, Nicole M; Bollier, Matthew J

    2017-01-01

    This study aims to provide biomechanical data on the effect of patella height in the setting of medial patellofemoral ligament (MPFL) reconstruction using finite element analysis. The study will also examine patellofemoral joint biomechanics using variable femoral insertion sites for MPFL reconstruction. A previously validated finite element knee model was modified to study patella alta and baja by translating the patella a given distance to achieve each patella height ratio. Additionally, the models were modified to study various femoral insertion sites of the MPFL (anatomic, anterior, proximal, and distal) for each patella height model, resulting in 32 unique scenarios available for investigation. In the setting of patella alta, the patellofemoral contact area decreased, resulting in a subsequent increase in maximum patellofemoral contact pressures as compared to the scenarios with normal patellar height. Additionally, patella alta resulted in decreased lateral restraining forces in the native knee scenario as well as following MPFL reconstruction. Changing femoral insertion sites had a variable effect on patellofemoral contact pressures; however, distal and anterior femoral tunnel malpositioning in the setting of patella alta resulted in grossly elevated maximum patellofemoral contact pressures as compared to other scenarios. Patella alta after MPFL reconstruction results in decreased lateral restraining forces and patellofemoral contact area and increased maximum patellofemoral contact pressures. When the femoral MPFL tunnel is malpositioned anteriorly or distally on the femur, the maximum patellofemoral contact pressures increase with severity of patella alta. When evaluating patients with patellofemoral instability, it is important to recognize patella alta as a potential aggravating factor. Failure to address patella alta in the setting of MPFL femoral tunnel malposition may result in even further increases in patellofemoral contact pressures, making it

  8. Nitinol Embolic Protection Filters: Design Investigation by Finite Element Analysis

    Science.gov (United States)

    Conti, Michele; de Beule, Matthieu; Mortier, Peter; van Loo, Denis; Verdonck, Pascal; Vermassen, Frank; Segers, Patrick; Auricchio, Ferdinando; Verhegghe, Benedict

    2009-08-01

    The widespread acceptance of carotid artery stenting (CAS) to treat carotid artery stenosis and its effectiveness compared with surgical counterpart, carotid endarterectomy (CEA), is still a matter of debate. Transient or permanent neurological deficits may develop in patients undergoing CAS due to distal embolization or hemodynamic changes. Design, development, and usage of embolic protection devices (EPDs), such as embolic protection filters, appear to have a significant impact on the success of CAS. Unfortunately, some drawbacks, such as filtering failure, inability to cross tortuous high-grade stenoses, malpositioning and vessel injury, still remain and require design improvement. Currently, many different designs of such devices are available on the rapidly growing dedicated market. In spite of such a growing commercial interest, there is a significant need for design tools as well as for careful engineering investigations and design analyses of such nitinol devices. The present study aims to investigate the embolic protection filter design by finite element analysis. We first developed a parametrical computer-aided design model of an embolic filter based on micro-CT scans of the Angioguard™ XP (Cordis Endovascular, FL) EPD by means of the open source pyFormex software. Subsequently, we used the finite element method to simulate the deployment of the nitinol filter as it exits the delivery sheath. Comparison of the simulations with micro-CT images of the real device exiting the catheter showed excellent correspondence with our simulations. Finally, we evaluated circumferential basket-vessel wall apposition of a 4 mm size filter in a straight vessel of different sizes and shape. We conclude that the proposed methodology offers a useful tool to evaluate and to compare current or new designs of EPDs. Further simulations will investigate vessel wall apposition in a realistic tortuous anatomy.

  9. Phosphogypsum analysis: total content and extractable element concentrations

    International Nuclear Information System (INIS)

    Gennari, Roseli F.; Medina, Nilberto H.; Garcia, Isabella; Silveira, Marcilei A.G.

    2011-01-01

    Phosphogypsum stand for the chemical origin gypsum generated in fertilizers production, in which phosphate rock is attacked by sulfuric acid resulting in phosphoric acid (H 3 PO 4 ) and phosphate fertilizers. Phosphogypsum is not a commercial product and it is stocked in large open areas or accumulated in lakes inducing to a major environmental problem due to the presence of toxic and radioactive elements. The increasing world agricultural demand is the real responsible for the severity of this environmental problem. Nevertheless, there are some possibilities for the application of this reject material, such as civil construction, waste water treatment, and in cultivated lands, etc. In the agriculture the phosphogypsum is commonly used as a nutrient source due to its large amounts of phosphorus, calcium and sulfur. However, there are still some environmental questions related to the use of this by-product since phosphogypsum is classified as TENORM (Technologically Enhanced Naturally Occurring Radioactive Material), which is a solid waste containing heavy metals and naturally occurring radioactive elements from the rock matrix. In this work, Plasma Mass Spectrometry (ICP-MS) was used to study phosphogypsum samples. Several acid solutions for samples digestion were evaluated in order to be feasible the chemical analysis. BCR sequential extractions were also performed. The results showed analyte concentrations are highly dependent on the acid solution used. The BCR guidelines could not be applied as used for soil, since the phosphogypsum solubility is different. So, it would be necessary to use different mass aliquots in the extractions, to be feasible an environmental evaluation. (author)

  10. Investigation of faulted tunnel models by combined photoelasticity and finite element analysis

    International Nuclear Information System (INIS)

    Ladkany, S.G.; Huang, Yuping

    1994-01-01

    Models of square and circular tunnels with short faults cutting through their surfaces are investigated by photoelasticity. These models, when duplicated by finite element analysis can predict the stress states of square or circular faulted tunnels adequately. Finite element analysis, using gap elements, may be used to investigate full size faulted tunnel system

  11. The nonlinear finite element analysis program NUCAS (NUclear Containment Analysis System) for reinforced concrete containment building

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Sang Jin; Lee, Hong Pyo; Seo, Jeong Moon [Korea Atomic Energy Research Institute, Taejeon (Korea)

    2002-03-01

    The maim goal of this research is to develop a nonlinear finite element analysis program NUCAS to accurately predict global and local failure modes of containment building subjected to internal pressure. In this report, we describe the techniques we developed throught this research. An adequate model to the analysis of containment building such as microscopic material model is adopted and it applied into the development Reissner-Mindlin degenerated shell element. To avoid finite element deficiencies, the substitute strains based on the assumed strain method is used in the shell formulation. Arc-length control method is also adopted to fully trace the peak load-displacement path due to crack formation. In addition, a benchmark test suite is developed to investigate the performance of NUCAS and proposed as the future benchmark tests for nonlinear analysis of reinforced concrete. Finally, the input format of NUCAS and the examples of input/output file are described. 39 refs., 65 figs., 8 tabs. (Author)

  12. Infinite elements for soil-structure interaction analysis in multi-layered halfspaces

    International Nuclear Information System (INIS)

    Yun, Chung Bang; Kim, Jae Min; Yang, Shin Chu

    1994-01-01

    This paper presents the theoretical aspects of a computer code (KIESSI) for soil-structure interaction analysis in a multi-layered halfspace using infinite elements. The shape functions of the infinite elements are derived from approximate expressions of the analytical solutions. Three different infinite elements are developed. They are the horizontal, the vertical and the comer infinite elements (HIE, VIE and CIE). Numerical example analyses are presented for demonstrating the effectiveness of the proposed infinite elements

  13. Identification of Serine Conformers by Matrix-Isolation IR Spectroscopy Aided by Near-Infrared Laser Induced Conformational Change, 2D Correlation Analysis, and Quantum Mechanical Anharmonic Computations

    Science.gov (United States)

    Najbauer, Eszter E.; Bazsó, Gábor; Apóstolo, Rui; Fausto, Rui; Biczysko, Malgorzata; Barone, Vincenzo; Tarczay, György

    2018-01-01

    The conformers of α-serine were investigated by matrix-isolation IR spectroscopy combined with NIR laser irradiation. This method, aided by 2D correlation analysis, enabled unambiguously grouping the spectral lines to individual conformers. On the basis of comparison of at least nine experimentally observed vibrational transitions of each conformer with empirically scaled (SQM) and anharmonic (GVPT2) computed IR spectra, 6 conformers were identified. In addition, the presence of at least one more conformer in Ar matrix was proved, and a short-lived conformer with a half-live of (3.7±0.5)·103 s in N2 matrix was generated by NIR irradiation. The analysis of the NIR laser induced conversions revealed that the excitation of the stretching overtone of both the side-chain and the carboxylic OH groups can effectively promote conformational changes, but remarkably different paths were observed for the two kinds of excitations. PMID:26201050

  14. Sensitivity analysis of the Galerkin finite element method neutron diffusion solver to the shape of the elements

    Energy Technology Data Exchange (ETDEWEB)

    Hosseini, Seyed Abolfaz [Dept. of Energy Engineering, Sharif University of Technology, Tehran (Iran, Islamic Republic of)

    2017-02-15

    The purpose of the present study is the presentation of the appropriate element and shape function in the solution of the neutron diffusion equation in two-dimensional (2D) geometries. To this end, the multigroup neutron diffusion equation is solved using the Galerkin finite element method in both rectangular and hexagonal reactor cores. The spatial discretization of the equation is performed using unstructured triangular and quadrilateral finite elements. Calculations are performed using both linear and quadratic approximations of shape function in the Galerkin finite element method, based on which results are compared. Using the power iteration method, the neutron flux distributions with the corresponding eigenvalue are obtained. The results are then validated against the valid results for IAEA-2D and BIBLIS-2D benchmark problems. To investigate the dependency of the results to the type and number of the elements, and shape function order, a sensitivity analysis of the calculations to the mentioned parameters is performed. It is shown that the triangular elements and second order of the shape function in each element give the best results in comparison to the other states.

  15. The TX-model - a quantitative heat loss analysis of district heating pipes by means of IR surface temperature measurements

    Energy Technology Data Exchange (ETDEWEB)

    Zinki, Heimo [ZW Energiteknik, Nykoeping (Sweden)

    1996-11-01

    The aim of this study was to investigate the possibility of analysing the temperature profile at the ground surface above buried district heating pipes in such a way that would enable the quantitative determination of heat loss from the pair of pipes. In practical applications, it is supposed that this temperature profile is generated by means of advanced IR-thermography. For this purpose, the principle of the TX - model has been developed, based on the fact that the heat losses from pipes buried in the ground have a temperature signature on the ground surface. Qualitative analysis of this temperature signature is very well known and in practical use for detecting leaks from pipes. These techniques primarily make use of relative changes of the temperature pattern along the pipe. In the quantitative heat loss analysis, however, it is presumed that the temperature profile across the pipes is related to the pipe heat loss per unit length. The basic idea is that the integral of the temperature profile perpendicular to the pipe, called TX, is a function of the heat loss, but is also affected by other parameters such as burial depth, heat diffusivity, wind, precipitation and so on. In order to analyse the parameters influencing the TX- factor, a simulation model for the energy balance at the ground surface has been developed. This model includes the heat flow from the pipe to the surface and the heat exchange at the surface with the environment due to convection, latent heat change, solar and long wave radiation. The simulation gives the surprising result that the TX factor is by and large unaffected during the course of a day even when the sun is shining, as long as other climate conditions are relatively stable (low wind, no rain, no shadows). The results from the simulations were verified at different sites in Denmark, Finland, Sweden and USA through a co-operative research program organised and partially financed by the IEA District Heating Programme, Task III, and

  16. Soil-Framed Structure Interaction Analysis - A New Interface Element

    Directory of Open Access Journals (Sweden)

    M. Dalili Shoaei

    Full Text Available AbstractInterfacial behavior between soil and shallow foundation has been found so influential to combined soil-footing performance and redistribution of forces in the superstructure. This study introduces a new thin-layer interface element formulated within the context of finite element method to idealize interfacial behavior of soil-framed structure interaction with new combination of degrees of freedom at top and bottom sides of the interface element, compatible with both isoparametric beam and quadrilateral element. This research also tends to conduct a parametric study on respective parameters of the new joint element. Presence of interface element showed considerable changes in the performance of the framed structure under quasi-static loading.

  17. Finite Element Analysis of Composite Aircraft Fuselage Frame

    Science.gov (United States)

    Dandekar, Aditya Milind

    Composites have been introduced in aircraft industries, for their stronger, stiffer, and lighter properties than their metal-alloys counterparts. The general purpose of an aircraft is to transport commercial or military payload. Aircraft frames primarily maintains the shape of fuselage and prevent instability of the structure. Fuselage is similar as wing in construction which consist of longitudinal elements (longerons and stringers), transverse elements (frames and bulkheads) and its external skin. The fuselage is subjected to forces such as the wing reactions, landing gear reaction, empennage reaction, inertia forces subjected due to size and weight, internal pressure forces due to high altitude. Frames also ensure fail-safe design against skin crack propagation due to hoops stress. Ideal fuselage frames cross section is often circular ring shape with a frame cap of Z section. They are mainly made up of light alloy commonly used is aluminium alloys such as Al-2024, Al-7010, Al-7050, Al-7175. Aluminium alloys have good strength to density ratios in compression and bending of thin plate. A high strength to weight ratio of composite materials can result in a lighter aircraft structure or better safety factor. This research focuses on analysis of fuselage frame under dynamic load condition with change in material. Composites like carbon fibre reinforced plastics [CFRP] and glass fibre reinforced plastics [GFRP] are compared with traditional aluminium alloy Al-7075. The frame is subjected to impact test by dropping it at a velocity of 30 ft. / secs from a height of 86 inch from its centre of gravity. These parameters are considered in event of failure of landing gear, and an aircraft is subject to belly landing or gear-up landing. The shear flow is calculated due to impact force which acts in radial direction. The frame is analysed under static structural and explicit dynamic load conditions. Geometry is created in ANSYS Design Modeler. Analysis setup is created using

  18. Analysis of toxical element in the whitening cream cosmetic samples using neutron activation analysis (NAA)

    International Nuclear Information System (INIS)

    Th Rina M; Sunarko

    2007-01-01

    Neutron activation analysis has been done to analyze of toxical elements that is not allowed in the whitening cream cosmetic. These samples have been randomly selected from the cosmetic market. The samples were irradiated at thermal neutron flux of 10"1"33n.cm"-"2s"-"1 in the irradiation facility of rabbit system in the RSG-GAS reactor Serpong. Counting of irradiated samples have been done by a high resolution HPGe detector couple to multichannel analyzer. Data have been analyzed by GENIE 2000. The sample have been qualitatively determined up to 19 elements. These elements are: As, Br, Ce, Co, Cr, Cs, Eu, Fe, Hg, K, La, Na, Rb, Sb, Se, Sc, Rb, Th, IV, and Zn. The result of qualitative analysis showed that the toxical elements present in the samples are Hg, As, Cr and Sb with the following concentration ranges in μg/g 25.2-65.1, 1.0-6.3, 30.5-89.1 and 2.9-5.3, respectively and these element not allowed in the whitening cream cosmetic. Besides that, the others elements have been detected in the samples are Br, Fe, Zn, Sc and Co, with concentration ranges, 13.1-36.4, 65.6-159.3, 0.79-77.1, 0.5-19.5, and 6.8-31.7 μg/g, respectively, in the sample whitening cream cosmetic. (author)

  19. Nonconforming axisymmetric elements for the analysis of containment structures

    International Nuclear Information System (INIS)

    Choi, C.K.; Kim, S.Y.

    1989-01-01

    In this study, the behaviors of the conforming isoparametric quadrilateral 4-node and triangular 3-nod axisymmetric solid elements are improved by adding nonconforming displacement modes. The convergence tests and the irregular mesh tests have been established through the analyses of a primary shield wall typed structure. For example study, a containment wall with internal pressure of 60 ksi has been analyzed. It shows that the nonconforming elements behave better than the conforming elements, especially, in the structurally discontinuous regions

  20. Neutron activation analysis of trace elements in Japanese hormesis cosmetics

    International Nuclear Information System (INIS)

    Furuta, E.; Nakahara, H.; Hatsukawa, Y.; Matsue, H.; Sakane, H.

    2008-01-01

    In Japan, cosmetics claiming hormesis effect are available through Internet. Although these cosmetics show the contents, they never mention the minor elements and radioactive sources. The existence of radioisotopes, however, was observed by measurements of the gamma-rays with a HPGe detector. In this study, in order to clarify the contents of trace elements, the hormesis cosmetics including radioactive sources were analyzed using INAA, PGAA and NAA with multiple gamma-ray detection (NAAMG). Nineteen elements were analyzed quantitatively in hormesis cosmetics by INAA, PGAA and NAAMG and 16 elements were detected qualitatively by SEM-EPMA. (author)

  1. Instrumental neutron activation analysis of a nickel sulfide fire assay button to determine the platinum group elements and gold

    Energy Technology Data Exchange (ETDEWEB)

    Asif, M.; Parry, S.J.; Malik, H. (Imperial College of Science, Technology and Medicine, Silwood Park, Ascot (United Kingdom). Centre for Analytical Research in the Environment)

    1992-08-01

    Platinum group elements and gold were determined in reference materials SARM 7 and MA 1b using fire assay with 0.5 g of nickel prior to neutron activation analysis. The method is simple and rapid, avoiding the dissolution step where losses occur, particularly of gold. The problem of standardizing the button mass was overcome by using a spiking technique. The method is best suited to samples with little or no copper, when the detection limits can be as low as 0.002, 0.025, 0.018, 0.0002, 0.002, 0.020 and 0.2 mg kg[sup -1] for Rh, Pd, Pt, Ir, Au, Os and Ru, respectively. (author).

  2. Sensitivity analysis of bridge health index to element failure and element conditions.

    Science.gov (United States)

    2009-11-01

    Bridge Health Index (BHI) is a bridge performance measure based on the condition of the bridge elements. It : is computed as the ratio of remaining value of the bridge structure to the initial value of the structure. Since it : is expressed as a perc...

  3. Stress and Deformation Analysis in Base Isolation Elements Using the Finite Element Method

    Directory of Open Access Journals (Sweden)

    Claudiu Iavornic

    2011-01-01

    Full Text Available In Modern tools as Finite Element Method can be used to study the behavior of elastomeric isolation systems. The simulation results obtained in this way provide a large series of data about the behavior of elastomeric isolation bearings under different types of loads and help in taking right decisions regarding geometrical optimizations needed for improve such kind of devices.

  4. Containment penetration design and analysis by finite element methods

    International Nuclear Information System (INIS)

    Perry, R.F.; Rigamonti, G.; Dainora, J.

    1975-01-01

    Containment penetration designs which provide complete support to process piping containing high pressure and high temperature fluids and which do not employ cooling coils, require special provisions to sustain loadings associated with normal/abnormal conditions and to limit maximum temperature transmitted to the containment concrete wall. In order to accomodate piping loads and fluid temperatures within code and regulatory limitations, the containment penetration designs require careful analysis of two critical regions: 1) the portion of the penetration sleeve which is exposed to containment ambient conditions and 2) the portion of the penetration which connects the sleeve to process piping (flued head). Analytical models using finite element representation of process piping, penetration flued head, and exposed sleeve were employed to investigate the penetration assembly design. By application of flexible multi-step analyses, different penetration configurations were evaluated to determine the effects of key design parameters. Among the parameters studied were flued head angles with the process piping, sleeve length and wall thickness. Special designs employing fins welded to the sleeve to further lower the temperature at the concrete wall interface were also investigated and fin geometry effects reported. (Auth.)

  5. Elemental analysis of brazing alloy samples by neutron activation technique

    International Nuclear Information System (INIS)

    Eissa, E.A.; Rofail, N.B.; Hassan, A.M.; El-Shershaby, A.; Walley El-Dine, N.

    1996-01-01

    Two brazing alloy samples (C P 2 and C P 3 ) have been investigated by Neutron activation analysis (NAA) technique in order to identify and estimate their constituent elements. The pneumatic irradiation rabbit system (PIRS), installed at the first egyptian research reactor (ETRR-1) was used for short-time irradiation (30 s) with a thermal neutron flux of 1.6 x 10 1 1 n/cm 2 /s in the reactor reflector, where the thermal to epithermal neutron flux ratio is 106. Long-time irradiation (48 hours) was performed at reactor core periphery with thermal neutron flux of 3.34 x 10 1 2 n/cm 2 /s, and thermal to epithermal neutron flux ratio of 79. Activation by epithermal neutrons was taken into account for the (1/v) and resonance neutron absorption in both methods. A hyper pure germanium detection system was used for gamma-ray acquisitions. The concentration values of Al, Cr, Fe, Co, Cu, Zn, Se, Ag and Sb were estimated as percentages of the sample weight and compared with reported values. 1 tab

  6. Fluid-film bearings: a finite element method of analysis

    International Nuclear Information System (INIS)

    Pururav, T.; Soni, R.S.; Kushwaha, H.S.; Mahajan, S.C.

    1995-01-01

    Finite element method (FEM) has become a very popular technique for the analysis of fluid-film bearings in the last few years. These bearings are extensively used in nuclear industry applications such as in moderator pumps and main coolant pumps. This report gives the methodology for the solution of Reynold's equation using FEM and its implementation in FE software LUBAN developed in house. It also deals with the mathematical basis and algorithm to account for the cavitation phenomena which makes these problems non-linear in nature. The dynamic coefficients of bearings are evaluated by one-step approach using variational principles. These coefficients are useful for the dynamic characterisation of fluid-film bearings. Several problems have been solved using this code including two real life problems, a circumferentially grooved journal bearing for which experimental results are available and the bearing of moderator pump of 500 MWe PHWR, have been solved. The results obtained for sample problems are in good agreement with the published literature. (author). 9 refs., 14 figs., 5 tabs., 2 ills

  7. PIXE analysis for bioaccumulation studies of trace elements

    International Nuclear Information System (INIS)

    Iwata, Y.; Satoh, A.; Sasaki, Y.; Ito, R.; Kuramachi, K.

    2005-01-01

    Bioaccumulation by micro-alga in the ocean was simulated in nutritive seawater containing known amounts of trace metals, and the concentration factors for Fe, Zn and Cd were measured by PIXE. Trace transition metals in nearshore seawater were removed by Chelex-100. Then a culture solution was prepared by adding known amounts of trace metals and nutritive salts to the purified seawater. Marine micro-algae (Nannochloropsis sp., and Phaeodactylum sp.,) were purely cultured in the culture solution. An interested metal ion was added to the culture solution (0.01-5.0 mg/l). Alga in 10 ml of the culture solution was collected on a polycarbonate filter (pore size: 1.0 ) by suction filtration and subjected to 2.9 MeV proton bombardment. Na, Mg, Al, Si, P, S, Cl, K, Ca, Cr, Mn, Fe, Zn and Cd were simultaneously determined. PIXE multi-element analysis was possible using less than 1 mg of analytical sample. The quantity of the metal in the alga was increased in proportion to the concentration in the culture solution. The concentration factors for Zn, Fe and Cd were measured, e.g., 10200 ± 300 ml/g to Zn for Phaeodactylum. The trend of the affinity for the trace metals in the case of Nannochloropsis was Fe 3+ > Zn 2+ > Pb 2+ > Cd 2+ . (author)

  8. Application of cyclic activation to in vivo elemental analysis

    International Nuclear Information System (INIS)

    Spyrou, N.M.

    1984-01-01

    Experience over the past seven years with a prototype cyclic system, based on an oscillating 5Ci AmBe neutron source, suggests that multielemental in vivo analysis is possible and more specifically indicates that the determination of selenium and cadmium in liver may allow the examination of the interaction of the two elements at acceptable doses. Detection limits obtained for selenium and cadmium, in the same experiment but through different modes of detection i.e. the measurement of delayed gamma-rays from short-lived Se-77m (17.6 s) and prompt gamma-rays from Cd-114, in a cyclic sequence of irradiations, are 0.4 ppm and 6 ppm respectively, for a total irradiation period of 1800s and an equivalent dose to the irradiated region of 5mSv. The redesigning of the prototype system is being considered in order to decrease the detection limit of selenium to a value of 0.1 ppm or less and the effect of increasing the neutron flux tenfold is investigated. This could result in an improvement by a factor of 4 to 5 in detection, for the same dose. 36 references, 6 figures

  9. Elemental analysis of brazing alloy samples by neutron activation technique

    Energy Technology Data Exchange (ETDEWEB)

    Eissa, E A; Rofail, N B; Hassan, A M [Reactor and Neutron physics Department, Nuclear Research Centre, Atomic Energy Authority, Cairo (Egypt); El-Shershaby, A; Walley El-Dine, N [Physics Department, Faculty of Girls, Ain Shams Universty, Cairo (Egypt)

    1997-12-31

    Two brazing alloy samples (C P{sup 2} and C P{sup 3}) have been investigated by Neutron activation analysis (NAA) technique in order to identify and estimate their constituent elements. The pneumatic irradiation rabbit system (PIRS), installed at the first egyptian research reactor (ETRR-1) was used for short-time irradiation (30 s) with a thermal neutron flux of 1.6 x 10{sup 1}1 n/cm{sup 2}/s in the reactor reflector, where the thermal to epithermal neutron flux ratio is 106. Long-time irradiation (48 hours) was performed at reactor core periphery with thermal neutron flux of 3.34 x 10{sup 1}2 n/cm{sup 2}/s, and thermal to epithermal neutron flux ratio of 79. Activation by epithermal neutrons was taken into account for the (1/v) and resonance neutron absorption in both methods. A hyper pure germanium detection system was used for gamma-ray acquisitions. The concentration values of Al, Cr, Fe, Co, Cu, Zn, Se, Ag and Sb were estimated as percentages of the sample weight and compared with reported values. 1 tab.

  10. Finite element analysis of CFRP reinforced silo structure design method

    Science.gov (United States)

    Yuan, Long; Xu, Xinsheng

    2017-11-01

    Because of poor construction, there is a serious problem of concrete quality in the silo project, which seriously affects the safe use of the structure. Concrete quality problems are mainly seen in three aspects: concrete strength cannot meet the design requirements, concrete cracking phenomenon is serious, and the unreasonable concrete vibration leads to a lot of honeycombs and surface voids. Silos are usually reinforced by carbon fiber cloth in order to ensure the safe use of silos. By the example of an alumina silo in a fly ash plant in Binzhou, Shandong Province, the alumina silo project was tested and examined on site. According to filed test results, the actual concrete strength was determined, and the damage causes of the silo was analysed. Then, a finite element analysis model of this silo was established, the CFRP cloth reinforcement method was adopted to strengthen the silo, and other technology like additional reinforcement, rebar planting, carbon fiber bonding technology was also expounded. The research of this paper is of great significance to the design and construction of silo structure.

  11. Analysis of gear reducer housing using the finite element method

    Science.gov (United States)

    Miklos, I. Zs; Miklos, C. C.; Alic, C. I.; Raţiu, S.

    2018-01-01

    The housing is an important component in the construction of gear reducers, having the role of fixing the relative position of the shafts and toothed wheels. At the same time, the housing takes over, via the bearings, the shaft loads resulting when the toothed wheel is engaging another toothed mechanism (i.e. power transmission through belts or chains), and conveys them to the foundation on which it is anchored. In this regard, in order to ensure the most accurate gearing, a high stiffness of the housing is required. In this paper, we present the computer-aided 3D modelling of the housing (in cast version) of a single stage cylindrical gear reducer, using the Autodesk Inventor Professional software, on the principle of constructive sizing. For the housing resistance calculation, we carried out an analysis using the Autodesk Simulation Mechanical software to apply the finite element method, based on the actual loads, as well as a comparative study of the stress and strain distribution, for several tightening values of the retaining bolts that secure the cover and the foundation housing.

  12. Theoretical basis for a transient thermal elastic-plastic stress analysis of nuclear reactor fuel elements

    International Nuclear Information System (INIS)

    Hsu, T.R.; Bertels, A.W.M.; Banerjee, S.; Harrison, W.C.

    1976-07-01

    This report presents the theoretical basis for a transient thermal elastic-plastic stress analysis of a nuclear reactor fuel element subject to severe transient thermo-mechanical loading. A finite element formulation is used for both the non-linear stress analysis and thermal analysis. These two major components are linked together to form an integrated program capable of predicting fuel element transient behaviour in two dimensions. Specific case studies are presented to illustrate capabilities of the analysis. (author)

  13. Trace element analysis in silicon by accelerator SIMS

    Energy Technology Data Exchange (ETDEWEB)

    Ender, R.M.; Suter, M. [Eidgenoessische Technische Hochschule, Zurich (Switzerland); Doebeli, M.; Synal, H.A. [Paul Scherrer Inst. (PSI), Villigen (Switzerland)

    1997-09-01

    The accelerator SIMS technique has been applied to Si samples implanted with different elements. It has been shown that concentrations of several trace elements can be analysed down to about 1 ppb in depth profiling mode. (author) 2 figs., 1 ref.

  14. Analysis of Tube Drawing Process – A Finite Element Approach ...

    African Journals Online (AJOL)

    In this paper the effect of die semi angle on drawing load in cold tube drawing has been investigated numerically using the finite element method. The equation governing the stress distribution was derived and solved using Galerkin finite element method. An isoparametric formulation for the governing equation was utilized ...

  15. Convergence analysis of spectral element method for electromechanical devices

    NARCIS (Netherlands)

    Curti, M.; Jansen, J.W.; Lomonova, E.A.

    2017-01-01

    This paper concerns the comparison of the performance of the Spectral Element Method (SEM) and the Finite Element Method (FEM) for a magnetostatic problem. The convergence of the vector magnetic potential, the magnetic flux density, and the total stored energy in the system is compared with the

  16. Stress distributions in finite element analysis of concrete gravity dam ...

    African Journals Online (AJOL)

    Gravity dams are solid structures built of mass concrete material; they maintain their stability against the design loads from the geometric shape, the mass, and the strength of the concrete. The model was meshed with an 8-node biquadratic plane strain quadrilateral (CPE8R) elements, using ABAQUS, a finite element ...

  17. Convergence analysis of spectral element method for magnetic devices

    NARCIS (Netherlands)

    Curti, M.; Jansen, J.W.; Lomonova, E.A.

    2018-01-01

    This paper concerns the comparison of the performance of the Spectral Element Method (SEM) and the Finite Element Method (FEM) for modeling a magnetostatic problem. The convergence of the vector magnetic potential, the magnetic flux density, and the total stored energy in the system is compared with

  18. Modelling Convergence of Finite Element Analysis of Cantilever Beam

    African Journals Online (AJOL)

    Convergence studies are carried out by investigating the convergence of numerical results as the number of elements is increased. If convergence is not obtained, the engineer using the finite element method has absolutely no indication whether the results are indicative of a meaningful approximation to the correct solution ...

  19. THE PRACTICAL ANALYSIS OF FINITE ELEMENTS METHOD ERRORS

    Directory of Open Access Journals (Sweden)

    Natalia Bakhova

    2011-03-01

    Full Text Available Abstract. The most important in the practical plan questions of reliable estimations of finite elementsmethod errors are considered. Definition rules of necessary calculations accuracy are developed. Methodsand ways of the calculations allowing receiving at economical expenditures of computing work the best finalresults are offered.Keywords: error, given the accuracy, finite element method, lagrangian and hermitian elements.

  20. Analysis of Content of Selected Critical Elements in Fly Ash

    Directory of Open Access Journals (Sweden)

    Makowska Dorota

    2016-03-01

    Full Text Available Pursuant to the new mineral policy of the European Union, searching for new sources of raw materials is required. Coal fly ash has long been considered as a potential source of a number of critical elements. Therefore, it is important to monitor the contents of the critical elements in fly ash from coal combustion. The paper presents the results of examinations of the contents of selected elements, i.e. beryllium, cobalt, chromium and germanium in fly ash from Polish power plants. The results of the conducted investigations indicate that the examined ash samples from bituminous coal combustion cannot be treated as a potential source of the analysed critical elements. The content of these elements in ash, though slightly higher than their average content in the sedimentary rocks, is, however, not high enough to make their recovery technologically and economically justified at this moment.

  1. Vibration Analysis of Circular Arch Element Using Curvature

    Directory of Open Access Journals (Sweden)

    H. Saffari

    2008-01-01

    Full Text Available In this paper, a finite element technique was used to determine the natural frequencies, and the mode shapes of a circular arch element was based on the curvature, which can fully represent the bending energy and by the equilibrium equations, the shear and axial strain energy were incorporated into the formulation. The treatment of general boundary conditions dose need a consideration when the element is incorporated by the curvature-based formula. This can be obtained by the introduction of a transformation matrix between nodal curvatures and nodal displacements. The equation of the motion for the element was obtained by the Lagrangian equation. Four examples are presented in order to verify the element formulation and its analytical capability.

  2. FT-IR-cPAS—New Photoacoustic Measurement Technique for Analysis of Hot Gases: A Case Study on VOCs

    Science.gov (United States)

    Hirschmann, Christian Bernd; Koivikko, Niina Susanna; Raittila, Jussi; Tenhunen, Jussi; Ojala, Satu; Rahkamaa-Tolonen, Katariina; Marbach, Ralf; Hirschmann, Sarah; Keiski, Riitta Liisa

    2011-01-01

    This article describes a new photoacoustic FT-IR system capable of operating at elevated temperatures. The key hardware component is an optical-readout cantilever microphone that can work up to 200 °C. All parts in contact with the sample gas were put into a heated oven, incl. the photoacoustic cell. The sensitivity of the built photoacoustic system was tested by measuring 18 different VOCs. At 100 ppm gas concentration, the univariate signal to noise ratios (1σ, measurement time 25.5 min, at highest peak, optical resolution 8 cm−1) of the spectra varied from minimally 19 for o-xylene up to 329 for butyl acetate. The sensitivity can be improved by multivariate analyses over broad wavelength ranges, which effectively co-adds the univariate sensitivities achievable at individual wavelengths. The multivariate limit of detection (3σ, 8.5 min, full useful wavelength range), i.e., the best possible inverse analytical sensitivity achievable at optimum calibration, was calculated using the SBC method and varied from 2.60 ppm for dichloromethane to 0.33 ppm for butyl acetate. Depending on the shape of the spectra, which often only contain a few sharp peaks, the multivariate analysis improved the analytical sensitivity by 2.2 to 9.2 times compared to the univariate case. Selectivity and multi component ability were tested by a SBC calibration including 5 VOCs and water. The average cross selectivities turned out to be less than 2% and the resulting inverse analytical sensitivities of the 5 interfering VOCs was increased by maximum factor of 2.2 compared to the single component sensitivities. Water subtraction using SBC gave the true analyte concentration with a variation coefficient of 3%, although the sample spectra (methyl ethyl ketone, 200 ppm) contained water from 1,400 to 100k ppm and for subtraction only one water spectra (10k ppm) was used. The developed device shows significant improvement to the current state-of-the-art measurement methods used in industrial

  3. An implementation analysis of the linear discontinuous finite element method

    International Nuclear Information System (INIS)

    Becker, T. L.

    2013-01-01

    This paper provides an implementation analysis of the linear discontinuous finite element method (LD-FEM) that spans the space of (l, x, y, z). A practical implementation of LD includes 1) selecting a computationally efficient algorithm to solve the 4 x 4 matrix system Ax = b that describes the angular flux in a mesh element, and 2) choosing how to store the data used to construct the matrix A and the vector b to either reduce memory consumption or increase computational speed. To analyze the first of these, three algorithms were selected to solve the 4 x 4 matrix equation: Cramer's rule, a streamlined implementation of Gaussian elimination, and LAPACK's Gaussian elimination subroutine dgesv. The results indicate that Cramer's rule and the streamlined Gaussian elimination algorithm perform nearly equivalently and outperform LAPACK's implementation of Gaussian elimination by a factor of 2. To analyze the second implementation detail, three formulations of the discretized LD-FEM equations were provided for implementation in a transport solver: 1) a low-memory formulation, which relies heavily on 'on-the-fly' calculations and less on the storage of pre-computed data, 2) a high-memory formulation, which pre-computes much of the data used to construct A and b, and 3) a reduced-memory formulation, which lies between the low - and high-memory formulations. These three formulations were assessed in the Jaguar transport solver based on relative memory footprint and computational speed for increasing mesh size and quadrature order. The results indicated that the memory savings of the low-memory formulation were not sufficient to warrant its implementation. The high-memory formulation resulted in a significant speed advantage over the reduced-memory option (10-50%), but also resulted in a proportional increase in memory consumption (5-45%) for increasing quadrature order and mesh count; therefore, the practitioner should weigh the system memory constraints against any

  4. An implementation analysis of the linear discontinuous finite element method

    Energy Technology Data Exchange (ETDEWEB)

    Becker, T. L. [Bechtel Marine Propulsion Corporation, Knolls Atomic Power Laboratory, P.O. Box 1072, Schenectady, NY 12301-1072 (United States)

    2013-07-01

    This paper provides an implementation analysis of the linear discontinuous finite element method (LD-FEM) that spans the space of (l, x, y, z). A practical implementation of LD includes 1) selecting a computationally efficient algorithm to solve the 4 x 4 matrix system Ax = b that describes the angular flux in a mesh element, and 2) choosing how to store the data used to construct the matrix A and the vector b to either reduce memory consumption or increase computational speed. To analyze the first of these, three algorithms were selected to solve the 4 x 4 matrix equation: Cramer's rule, a streamlined implementation of Gaussian elimination, and LAPACK's Gaussian elimination subroutine dgesv. The results indicate that Cramer's rule and the streamlined Gaussian elimination algorithm perform nearly equivalently and outperform LAPACK's implementation of Gaussian elimination by a factor of 2. To analyze the second implementation detail, three formulations of the discretized LD-FEM equations were provided for implementation in a transport solver: 1) a low-memory formulation, which relies heavily on 'on-the-fly' calculations and less on the storage of pre-computed data, 2) a high-memory formulation, which pre-computes much of the data used to construct A and b, and 3) a reduced-memory formulation, which lies between the low - and high-memory formulations. These three formulations were assessed in the Jaguar transport solver based on relative memory footprint and computational speed for increasing mesh size and quadrature order. The results indicated that the memory savings of the low-memory formulation were not sufficient to warrant its implementation. The high-memory formulation resulted in a significant speed advantage over the reduced-memory option (10-50%), but also resulted in a proportional increase in memory consumption (5-45%) for increasing quadrature order and mesh count; therefore, the practitioner should weigh the system memory

  5. The use of synchrotron radiation for trace element analysis and element mapping by scanning X-ray fluorescence

    International Nuclear Information System (INIS)

    Davies, S.T.

    1983-01-01

    Synchrotron Radiation excited X-Ray Fluorescence is a potentially powerful tool for the routine quantitative chemical analysis of materials, with minimum detection limits typically of the order of a tenth of a ppm, and with the added advantages of simultaneous multi-element detection capability, spatial resolution on a micron scale, large signal to noise ratios and short analysis times. This paper presents a brief review of the use of Synchrotron Radiation in Trace Element Analysis and discusses the requirements for a microprobe for chemical analysis utilising SR. Data obtained at the Synchrotron Radiation Source, Daresbury Laboratory include XRF spectra of standard reference materials and an application of the technique to the study of ion implanted layers in semiconductors is outlined. (author)

  6. Simulation Analysis of Tilted Polyhedron-Shaped Thermoelectric Elements

    Science.gov (United States)

    Meng, Xiangning; Suzuki, Ryosuke O.

    2015-06-01

    The generation of thermoelectricity is considered a promising approach to harness the waste heat generated in industries, automobiles, gas fields, and other man-made processes. The waste heat can be converted to electricity via a thermoelectric (TE) generator. In this light, the generator performance depends on the geometric configuration of its constituent elements as well as their material properties. Our previous work reported TE behaviors for modules consisting of parallelogram-shaped elements, because elements with tilted laminate structures provide increased mechanical stability and efficient heat-transferring ability from the hot surface to the cold surface. Here, we study TE elements in the shape of a polyhedron that is obtained by mechanically truncating the edges of a parallelogram element in order to further enhance the generator performance and reduce TE material usage. The TE performance of the modules consisting of these polyhedron elements is numerically simulated by using the finite-volume method. The output power, voltage, and current of the polyhedral TE module are greater than those of the parallelogram-element module. The polyhedron shape positively affects heat transfer and the flow of electric charges in the light of increasing the efficiency of conversion from heat to electricity. By varying the shape of the truncated portions, we determine the optimal shape that enables homogeneous heat flux distribution and slow diffusion of thermal energy to obtain the better efficiency of conversion of heat into electricity. We believe that the findings of our study can significantly contribute to the design policy in TE generation.

  7. Characterizing floodplain evolution by joint analysis of SAR, GOES IR and local precipitation data: Case study of Rio Colorado, Bolivia

    Science.gov (United States)

    Koenders, R.; Oyen, A. M.; Weltje, G.; Sarna, K.; Donselaar, R.

    2013-12-01

    Dryland rivers in an endorheic basin experience downstream decrease of channel width and depth as the consequence of transmission losses by percolation and evapo-transpiration. Major changes in the river morphology take place during short peak discharge periods when the volume of water and sediment by far exceeds the river capacity and, as a consequence, meander bends are cut off, and the river path may change position by avulsion. Successive avulsions create a complex network of cross-cutting abandoned river channels. The Río Colorado, located in the southeast part of the Altiplano basin in Bolivia, is such a river system. This system consists of a very low-gradient lacustrine coastal plain onto which is deposited a 400 km2 sheet of fluvial sediment over the last 4000 year. Traditional studies to monitor the morphological changes at the terminus of the river system are based on field data acquisition of the fluvial sediments. This is time consuming and only covers a small area of the total fluvial morphology. The combination of field measurements and remote sensing imagery allows for the analysis of the development of the entire river system terminus at a longer temporal scale. Changes of alluvial surfaces affect the reflectance of objects and patterns on the ground, which is recorded by satellite images. In this study we show the response of the delta to rainfall events of various intensities in the Rio Colorado watershed. We combine precipitation data in the watershed with spaceborne synthetic aperture radar (SAR) data. We use two data sets that contain precipitation information: rainfall estimates based on Geostationary Operational Environmental Satellite (GOES) weather satellite IR window brightness temperatures and direct measures of rainfall from rain gauges in the vicinity of the delta. To detect changes on the surface water content we use the backscatter intensity or amplitude images from the European Remote Sensing Satellite (ERS) Synthetic Aperture

  8. Containment penetration design and analysis by finite element methods

    International Nuclear Information System (INIS)

    Perry, R.F.; Rigamonti, G.; Dainora, J.

    1975-01-01

    Containment penetration designs which provide complete support to process piping containing high pressure and high temperature fluids and which do not employ cooling coils, require special provisions to sustain loadings associated with normal/abnormal conditions and to limit maximum temperature transmitted to the containment concrete wall. In order to accommodate piping imposed loads and fluid temperatures within code and regulatory limitations, the containment penetration designs require careful analysis of two critical regions: the portion of the penetration sleeve which is exposed to containment ambient conditions and the portion of the penetration which connects the sleeve to process piping (flued head). The length and thickness of the sleeve must be designed to provide maximum heat dissipation to the atmosphere and minimum heat conduction through the sleeve to meet concrete temperature limitations. The sleeve must have the capability to transmit the postulated piping loads to concrete embedments in the containment shell. The penetration flued head design must be strong enough to transfer high mechanical loads and be flexible enough to accommodate the thermal stresses generated by the high temperature fluid. Analytical models using finite element representations of process piping, penetration flued head, and exposed sleeve were employed to investigate the penetration assembly design. By application of flexible multi-step analyses, different penetration configurations were evaluated to determine the effects of key design parameters. Among the parameters studied were flued head profiles, flued head angles with the process piping, sleeve length and wall thickness. Special designs employing fins welded to the sleeve to lower the temperature at the concrete wall interface were investigated and fin geometry effects reported

  9. Nuclear reaction analysis (NRA) for trace element detection

    Energy Technology Data Exchange (ETDEWEB)

    Doebeli, M. [Paul Scherrer Inst. (PSI), Villigen (Switzerland); Noll, K. [Bern Univ. (Switzerland)

    1997-09-01

    Ion beam induced nuclear reactions can be used to analyse trace element concentrations in materials. The method is especially suited for the detection of light contaminants in heavy matrices. (author) 3 figs., 2 refs.

  10. Fluid-structure finite-element vibrational analysis

    Science.gov (United States)

    Feng, G. C.; Kiefling, L.

    1974-01-01

    A fluid finite element has been developed for a quasi-compressible fluid. Both kinetic and potential energy are expressed as functions of nodal displacements. Thus, the formulation is similar to that used for structural elements, with the only differences being that the fluid can possess gravitational potential, and the constitutive equations for fluid contain no shear coefficients. Using this approach, structural and fluid elements can be used interchangeably in existing efficient sparse-matrix structural computer programs such as SPAR. The theoretical development of the element formulations and the relationships of the local and global coordinates are shown. Solutions of fluid slosh, liquid compressibility, and coupled fluid-shell oscillation problems which were completed using a temporary digital computer program are shown. The frequency correlation of the solutions with classical theory is excellent.

  11. Comparative analysis of vitamin C, crude protein, elemental nitrogen ...

    African Journals Online (AJOL)

    Yomi

    2011-12-21

    Dec 21, 2011 ... greens (Brassica napus L.) and kale (Brassica oleracea var. acephala) ... Nitrogen is essential for protein production, for proper growth of ... Brassica crops. ..... the effect of trace element-amended fertilizers on their Co, Se, and.

  12. STATISTICAL ANALYSIS OF THE DEMOLITION OF THE HITCH DEVICES ELEMENTS

    Directory of Open Access Journals (Sweden)

    V. V. Artemchuk

    2009-03-01

    Full Text Available The results of statistical research of wear of automatic coupler body butts and thrust plates of electric locomotives are presented in the article. Due to the increased wear the mentioned elements require special attention.

  13. Finite element analysis of thermal stress distribution in different ...

    African Journals Online (AJOL)

    Nigerian Journal of Clinical Practice. Journal Home ... Von Mises and thermal stress distributions were evaluated. Results: In all ... distribution. Key words: Amalgam, finite element method, glass ionomer cement, resin composite, thermal stress ...

  14. Elemental analysis of bottom ash from municipal incinerator by neutron activation analysis

    International Nuclear Information System (INIS)

    Kim, S. H.; Jang, S. H.; Moon, J. H.; Jung, Y. S.; Kim, Y. J.

    2003-01-01

    Elemental analysis of bottom ash generated from municipal solid waste incinerator was performed by neutron activation analysis. For this study, ash samples monthly collected from incinerator in D city were sieved with 5 mm mesh size, dried, pulverized by agate mortar and finally re-sieved with 200μ mesh size. Prepared samples were irradiated by neutrons using NAA No.1 irradiation hole in Korea Atomic Energy Research Institute. Activated samples were measured by gamma-ray spectrometer according to the relevant nuclear properties of target nuclides and the concentration of 33 elements were determined from the collected ash samples. Quality control was conducted by comparative analysis with two NIST standard reference materials simultaneously. Mean values and standard deviations of hazardous elements such as As, Cr, Cu, Fe, Mn, Sb and Zn among the determined elements were 3.8±6.9mg/kg, 620±0.12 %, 4.76±0.37 %, 0.26±0.10 %, 115±29 mg/kg and 0.71±0.19 %, respectively

  15. Neutron activation analysis for environmental trace element research determination of elemental composition of sediments in the Sea of Galillee, Israel

    Energy Technology Data Exchange (ETDEWEB)

    Lavi, N; Ne` eman, E; Brenner, S; Butenko, V [Tel Aviv Univ. (Israel). Medical School

    1996-12-01

    The aims of this work were to: a) demonstrate the effectiveness of instrumental neutron activation analysis for determining the background concentrations of trace elements in the sediments collected from the Sea of Gallile. b) determine the advantage factors for epithermal neutron irradiation. c) determine the contribution of silicon to the total {sup 28}Al activity by the {sup 28}Si(n,p){sup 28}Al reaction. c) check the validity of the method by determining the elemental content of U.S. NBS Standard Reference Material SRM-1633a (fly ash). d) calculate the average enrichment factors for the elements in sediments . e) determine the concentrations of the artificial radionuclides {sup 134}Cs, {sup 137}Cs and the naturally occurring radionuclides {sup 40}K, {sup 226}Ra and {sup 232}Th (authors).

  16. The role of neutron activation analysis for trace elements characterization, analysis and certification in atmospheric particulates

    International Nuclear Information System (INIS)

    Rizzio, Enrico; Gallorini, Mario

    2002-01-01

    The Neutron Activation Analysis (NAA) owns these requirements and is universally accepted as one of the most reliable analytical tools for trace and ultratrace elements determination. Its use in trace elements atmospheric pollution related studies has been and is still extensive as can be demonstrate by several specific works and detailed reviews. In this work, the application of this nuclear technique, in solving a series of different analytical problems related to trace elements in air pollution processes is reported. Examples and results are given on the following topics: characterization of urban and rural airborne particulate samples; particles size distribution in the different inhalable and respirable fractions (PM10 and PM 2.5); certification of related Standard Reference Materials for data quality assurance. (author)

  17. Instrumental photoactivation analysis of some elements in steel

    International Nuclear Information System (INIS)

    Galatanu, V.; Timus, D.; Catana, D.

    1985-01-01

    Photoactivation determination of Cr, Ni and Mo had been performed in large representative samples of steel. The disc samples (40 mm diameter and 3,5 mm thickness) were irradiated in the bremstrahlung beam of a 25 MeV betatron, at 0.5 m from the Pt target in order to insure a fairly uniform irradiation. The gamma-rays were detected with a 40 cm Ge(Li) detector coupled to an IR 90 programmable analyser. The concentration determined were between 0,1% and 9% for Ni, 0,4% and 18% for Cr and 0,05% and 1,50% for Mo. The accuracy of the determinations was 10% for lower consentrations and 3% for higher concentrations

  18. Multi-element analysis for environmental characterization and its future trends

    International Nuclear Information System (INIS)

    Sansoni, B.

    1987-04-01

    Before starting to characterize the environment by its elemental composition, it may be useful to ask about the objective of these efforts. This includes questions about the scope of environmental protection, the definition of the environment and the limitations of its characterization by elemental composition alone. In the second part of this lecture, examples are given of the elemental composition of well analysed samples from the atmosphere, hydrosphere, lithosphere and biosphere. The third part introduces the principle of multi-element analysis and the fourth part gives examples. Finally, future aspects of modern chemical analysis are outlined with respect to the multi-element principle. (orig.)

  19. Forensic identification of trunk mat by trace element analysis of single fiber with laser ablation ICP-MS

    International Nuclear Information System (INIS)

    Hiroma, Yuki; Nakai, Izumi; Hokura, Akiko

    2010-01-01

    The application of LA-ICP-MS (laser ablation inductively coupled plasma mass spectrometry) to the chemical characterization of single trunk mat fibers made of PET was investigated in order to establish a forensic analytical method for the discrimination of samples of different origins. The analytical conditions of LA-ICP-MS equipped with a 213 nm Nd : YAG laser were optimized to analyze trace elements, such as Cu, Sb, and Ba at ppm levels. A total of 31 samples produced by 7 car manufactures in Japan were used for analysis. The concentrations of Li, Mg, Al, P, Ca, Ti, Co, Cu, Ge, Nb, Sb, Ta, and Pb were successfully measured from a single fiber sample with a diameter of ca. 20 μm. It was possible to discriminate all 31 samples based on the analytical results of a single fiber by LA-ICP-MS combined with those of FT-IR and SEM-EDS. LA-ICP-MS has good analytical sensitivity, and requires a much shorter preparation time and a smaller sample size than any other conventional element analysis methods. This paper demonstrates for the first time that this method is practically useful as a powerful tool for the forensic identification of a single trunk mat fiber. (author)

  20. Determination of toxic elements in tobacco products by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Ahmad, S.; Chaudhry, M.S.; Qureshi, I.H.

    1979-01-01

    The concentration of 15 elements in various brands of cigarette tobacco and cigarette wrapping paper were determined using instrumental neutron activation analysis. The paper of some of the brands contains higher concentrations of toxic elements than the tobacco. The cigarette filter and the ash were also analyzed to determine the adsorption of toxic elements on the filter and their transference in smoke. The toxic effects of some of the elements have been briefly discussed. (author)

  1. Seismic analysis of the APR1400 nuclear reactor system using a verified beam element model

    International Nuclear Information System (INIS)

    Park, Jong-beom; Park, No-Cheol; Lee, Sang-Jeong; Park, Young-Pil; Choi, Youngin

    2017-01-01

    Highlights: • A simplified beam element model is constructed based on the real dynamic characteristics of the APR1400. • Time history analysis is performed to calculate the seismic responses of the structures. • Large deformations can be observed at the in-phase mode of reactor vessel and core support barrel. - Abstract: Structural integrity is the first priority in the design of nuclear reactor internal structures. In particular, nuclear reactor internals should be designed to endure external forces, such as those due to earthquakes. Many researchers have performed finite element analyses to meet these design requirements. Generally, a seismic analysis model should reflect the dynamic characteristics of the target system. However, seismic analysis based on the finite element method requires long computation times as well as huge storage space. In this research, a beam element model was developed and confirmed based on the real dynamic characteristics of an advanced pressurized water nuclear reactor 1400 (APR1400) system. That verification process enhances the accuracy of the finite element analysis using the beam elements, remarkably. Also, the beam element model reduces seismic analysis costs. Therefore, the beam element model was used to perform the seismic analysis. Then, the safety of the APR1400 was assessed based on a seismic analysis of the time history responses of its structures. Thus, efficient, accurate seismic analysis was demonstrated using the proposed beam element model.

  2. Seismic analysis of the APR1400 nuclear reactor system using a verified beam element model

    Energy Technology Data Exchange (ETDEWEB)

    Park, Jong-beom [Department of Mechanical Engineering, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722 (Korea, Republic of); Park, No-Cheol, E-mail: pnch@yonsei.ac.kr [Department of Mechanical Engineering, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722 (Korea, Republic of); Lee, Sang-Jeong; Park, Young-Pil [Department of Mechanical Engineering, Yonsei University, 50 Yonsei-ro, Seodaemun-gu, Seoul 03722 (Korea, Republic of); Choi, Youngin [Korea Institute of Nuclear Safety, 62 Gwahak-ro, Yuseong-gu, Daejeon 34142 (Korea, Republic of)

    2017-03-15

    Highlights: • A simplified beam element model is constructed based on the real dynamic characteristics of the APR1400. • Time history analysis is performed to calculate the seismic responses of the structures. • Large deformations can be observed at the in-phase mode of reactor vessel and core support barrel. - Abstract: Structural integrity is the first priority in the design of nuclear reactor internal structures. In particular, nuclear reactor internals should be designed to endure external forces, such as those due to earthquakes. Many researchers have performed finite element analyses to meet these design requirements. Generally, a seismic analysis model should reflect the dynamic characteristics of the target system. However, seismic analysis based on the finite element method requires long computation times as well as huge storage space. In this research, a beam element model was developed and confirmed based on the real dynamic characteristics of an advanced pressurized water nuclear reactor 1400 (APR1400) system. That verification process enhances the accuracy of the finite element analysis using the beam elements, remarkably. Also, the beam element model reduces seismic analysis costs. Therefore, the beam element model was used to perform the seismic analysis. Then, the safety of the APR1400 was assessed based on a seismic analysis of the time history responses of its structures. Thus, efficient, accurate seismic analysis was demonstrated using the proposed beam element model.

  3. Assessment of non-linear analysis finite element program (NONSAP) for inelastic analysis

    International Nuclear Information System (INIS)

    Chang, T.Y.; Prachuktam, S.; Reich, M.

    1976-11-01

    An assessment on a nonlinear structural analysis finite element program called NONSAP is given with respect to its inelastic analysis capability for pressure vessels and components. The assessment was made from the review of its theoretical basis and bench mark problem runs. It was found that NONSAP has only limited capability for inelastic analysis. However, the program was written flexible enough that it can be easily extended or modified to suit the user's need. Moreover, some of the numerical difficulties in using NONSAP are pointed out

  4. Leaf elemental analysis in mycorrhizal post oak seedlings

    Energy Technology Data Exchange (ETDEWEB)

    Boling, B.C. [Department of Biology, University of North Texas, P.O. Box 305220, Denton, TX 76203-5220 (United States); Naab, F.U. [Ion Beam Modification and Analysis Laboratory, Department of Physics, University of North Texas, P.O. Box 311427, Denton, TX 76203-1427 (United States)]. E-mail: fun001@unt.edu; Smith, D. [Department of Biology, University of North Texas, P.O. Box 305220, Denton, TX 76203-5220 (United States); Duggan, J.L. [Ion Beam Modification and Analysis Laboratory, Department of Physics, University of North Texas, P.O. Box 311427, Denton, TX 76203-1427 (United States); McDaniel, F.D. [Ion Beam Modification and Analysis Laboratory, Department of Physics, University of North Texas, P.O. Box 311427, Denton, TX 76203-1427 (United States)

    2006-09-15

    Growth and element assimilation was investigated in the leaves of post oak seedlings exposed to four different treatment combinations of fertilization and ectomycorrhizal inoculation. Element concentration was analyzed via particle-induced X-ray emission spectrometry (PIXE). PIXE detected 10 of the 13 essential macro and micronutrients: P, S, Mg, Ca, K, Cu, Zn, Mn, Fe and Cl. Mean growth and dry weight was significantly different across the treatment groups as well as the mean concentration of Mg, Al, S, K, Ca, Fe, Cu and Zn. The data suggest that fertilization rather than mycorrhizal inoculation had a stronger influence on nutrient uptake. This study is the first to analyze element concentration in post oak and to investigate the potential benefits of mycorrhizal symbiosis in post oak seedlings in terms of nutrient uptake.

  5. Non destructive SXRF analysis of heavy elements in lichens

    International Nuclear Information System (INIS)

    Ramos, M.T.; Figueiredo, M.O.; Pereira da Silva, T.; Basto, M.J.; Chevallier, P.

    2000-01-01

    Various species incrusting granitic and calcareous rocks were collected at different places covering a large span of atmospheric conditions. They were chemically studied by synchrotron- induced X-ray fluorescence (SXRF), a nondestructive technique of outmost importance in the field, allowing for a future use of the same lichen fragments in further tests. This study proved that lichens - at least the saxicolous species - concentrate heavy elements recognized as strong pollutants, like lead and bromine, irrespective the environmental availability of these elements, either in the atmosphere or in the rock substrate, partially frustrating the use of saxicolous lichens as pollution monitors. (author)

  6. Design element analysis on juice market Case study: Prigat

    Directory of Open Access Journals (Sweden)

    Nicoleta Andreea NEACŞU

    2015-06-01

    Full Text Available : If at the beginning package was considered simply a package that contained a product, now due to the development and modernization of the trade, it is a very valuable component of the marketing policy, being a carrier of messages to the consumer. Classic design elements that are included in any packaging refer to shape, color and graphics. The Romanian Juices Market was marked by originality and innovation in terms of packaging design elements. Thus, from 1998 until now the following have appeared: the first wide mouth square bottle, the first sport opening head PET bottle for Prigat Active, the first opening gable top box produced in our country.

  7. AMS advances in the geosciences and heavy-element analysis

    International Nuclear Information System (INIS)

    Rucklidge, J.C.; Wilson, G.C.; Kilius, L.R.

    1990-01-01

    Until recently small accelerators, such as the 2 MV Tandetron, have been used only for the lighter elements such as 10 Be, 14 C and 26 Al, while the heavier isotopes such as 36 Cl, 41 Ca and 129 I have been perceived to need the higher energies only available on large machines. We describe the use of a Tandetron for measurement of 129 I/ 127 I at natural levels, and the in situ assay of some heavy elements of interest in economic geology at detection levels superior to those of more widely used techniques. A few recently described novel applications of AMS are also given. (orig.)

  8. Model Reduction in Dynamic Finite Element Analysis of Lightweight Structures

    DEFF Research Database (Denmark)

    Flodén, Ola; Persson, Kent; Sjöström, Anders

    2012-01-01

    models may be created by assembling models of floor and wall structures into large models of complete buildings. When assembling the floor and wall models, the number of degrees of freedom quickly increases to exceed the limits of computer capacity, at least in a reasonable amount of computational time...... Hz. Three different methods of model reduction were investigated; Guyan reduction, component mode synthesis and a third approach where a new finite element model was created with structural elements. Eigenvalue and steady-state analyses were performed in order to compare the errors...

  9. Qualitative analysis of the rare earth element by simulation of inductively coupled plasma emission spectra

    International Nuclear Information System (INIS)

    Hashimoto, M.S.; Tobishima, Taeko; Kamitake, Seigo; Yasuda, Kazuo.

    1985-01-01

    The emission lines for qualitative analysis of rare earth elements by a simulation technique of ICP spectra were proposed. The spectra were simulated by employing a Gaussian (or a Lorentzian at high concentrations) profile. The simulated spectra corresponded quite well with the observed ones. The emission lines were selected so that the interference was as small as possible. The present qualitative analysis is based on a pattern recognition method where observed intensity ratios of the emission lines in each element are compared with those of a single analyte element. The qualitative analysis was performed for twelve standard solutions containing a single rare earth element and for eight standard solutions containing an element other than rare earth elements. The selection of the emission lines and the algorithm of the present qualitative analysis were justified. (author)

  10. A General Finite Element Scheme for Limit State Analysis and Optimization

    DEFF Research Database (Denmark)

    Damkilde, Lars

    1999-01-01

    Limit State analysis which is based on a perfect material behaviour is used in many different applications primarily within Structural Engineering and Geotechnics. The calculation methods have not reached the same level of automation such as Finite Element Analysis for elastic structures....... The computer based systems are more ad hoc based and are typically not well-integrated with pre- and postprocessors well-known from commercial Finite Element codes.A finite element based formulation of limit state analysis is presented which allows an easy integration with standard Finite Element codes...... for elastic analysis. In this way the user is able to perform a limit state analysis on the same model used for elastic analysis only adding data for the yield surface.The method is based on the lower-bound theorem and uses stress-based elements with a linearized yield surface. The mathematical problem...

  11. Elemental analysis of Taiwanese areca nut and limes with INAA

    International Nuclear Information System (INIS)

    Wei, Y.Y.; Chung, C.

    1997-01-01

    The popular areca nuts were sampled and their stuffed white and red lime were collected simultaneously from four marketplaces in Taiwan in different growing seasons. Samples of areca nut were treated via homogenizer prior to freeze drying, about 100-150 mg each of the areca nut and lime were packed into PE bag. Samples were irradiated with neutron flux about 10 12 n x cm -2 x s -1 . A total of 17, 18, and 13 elements was analyzed with INAA for white lime, red lime, and areca nut, respectively. The results indicated that Ca have the highest concentration in both limes. Most elements in collected samples have wide range of concentrations among different seasons and marketplaces. It is suggested that the elemental concentration of areca nut and limes exists in divergence originated from various farms in Taiwan. In addition, four elements of Ca, Fe, Mg, and Sc are probably overtaken by persons having chewing habit of areca nut and their effects on oral cancer are discussed. (author)

  12. Woody tissue analysis using an element ratio technique (DRIS)

    Science.gov (United States)

    Kurt H. Riitters; L.F. Ohmann; D.F. Grigal

    1991-01-01

    The diagnosis and recommendation integrated system (DRIS) was used to describe the variation of 12 elements in woody tree tissue and balsam fir (Abies balsamae (L.) Mill.), sugar maple (Acer saccharum Marsh.), jack pine (Pinus banksiana Lamb.), red pine (Pinus resinosa alt.), and aspen (

  13. A Comparative Analysis of Nutrients and Mineral Elements Content ...

    African Journals Online (AJOL)

    (Mg), Iron (Fe), Copper (Cu) and Zinc (Zn) content, while P. pedicellatum has high ... INTRODUCTION ... central to animal production and productivity. .... for growth and serve as structural element in all plant ... the animal's body, it ensured correct maintenance of ... Ash content because Ash is the approximation of total.

  14. Theoretical analysis of the alloying element effect on decarburization

    International Nuclear Information System (INIS)

    Elanskij, G.N.; Kudrin, V.A.; Akinfiev, S.I.

    1978-01-01

    On the basis of the laws of physical chemistry the alloying element (Ni, Cr, Mo, W, Co, Mn) effect on the kinetics and degree of decarburizing in iron melt with low carbon concentrations has been determined. The calculation of alloying element effect on the value of carbon diffusion coefficient and on the velocity changes in carbon oxidation rate has been carried out. It is shown that carbon diffusion coefficient and decarburization rate are detemined by two factors: thermodynamic, carbon activity change in the presence of alloying elements being accounted for and structural, dependending on the liquid metal structure and being determined by the viscosity activity of impurity. Experimental data are given, testifying that the introduction in the melt of such elements as Ni, Co, Cu, promotes a decrease in carbon content, as well as accelerates the decarburization process. W and Mo produce a poor effect, and Cr and Mn abruptly increase the value of minimum carbon content. Mo, Cr and W reduce the decarburization rate in the melt

  15. Elemental Analysis of Galium incanum SM subsp Centrale Ehrend ...

    African Journals Online (AJOL)

    . centrale Ehrend. Methods: The air-dried aerial parts of the plant material were used and its water extract (2 % w/v infusion) was analysed for trace elements using x-ray fluorescence (XRF ) spectrometry. Results: The aqueous extract depicted ...

  16. Analysis of Essential and Toxic Elements in Jujube Fruits Collected ...

    African Journals Online (AJOL)

    Purpose: To develop a simple and precise method for the determination of the levels of both essential and toxic elements in jujube collected from different locations in China. Methods: Dried jujube fruits collected were digested by optimized microwave procedure. Inductively coupled plasma atomic emission spectrometry ...

  17. A comparative phylogenetic analysis of full-length mariner elements

    Indian Academy of Sciences (India)

    Mariner like elements (MLEs) are widely distributed type II transposons with an open reading frame (ORF) for transposase. We studied comparative phylogenetic evolution and inverted terminal repeat (ITR) conservation of MLEs from Indian saturniid silkmoth, Antheraea mylitta with other full length MLEs submitted in the ...

  18. Instrumental methods for analysis of some elements in flour

    International Nuclear Information System (INIS)

    Zagrodzki, P.; Dutkiewicz, E.M.; Malec, P.; Krosniak, M.; Knap, W.

    1993-10-01

    For ten various brands of flour contents of chosen (heavy) elements were determined by means of ICP, GF-AAS, PIXE and ASV/CSV methods. General performance of participating laboratories as well as pros and cons of different analytical methods were compared and discussed. (author). 6 refs, 6 figs, 7 tabs

  19. Appendix F : finite element analysis of end region.

    Science.gov (United States)

    2013-03-01

    FE (finite element) modeling was conducted to 1) provide a better understanding of the : elastic behavior of the end region prior to cracking and 2) to evaluate the effects of bearing pad : stiffness and width on end region elastic stresses. The FEA ...

  20. Structural weights analysis of advanced aerospace vehicles using finite element analysis

    Science.gov (United States)

    Bush, Lance B.; Lentz, Christopher A.; Rehder, John J.; Naftel, J. Chris; Cerro, Jeffrey A.

    1989-01-01

    A conceptual/preliminary level structural design system has been developed for structural integrity analysis and weight estimation of advanced space transportation vehicles. The system includes a three-dimensional interactive geometry modeler, a finite element pre- and post-processor, a finite element analyzer, and a structural sizing program. Inputs to the system include the geometry, surface temperature, material constants, construction methods, and aerodynamic and inertial loads. The results are a sized vehicle structure capable of withstanding the static loads incurred during assembly, transportation, operations, and missions, and a corresponding structural weight. An analysis of the Space Shuttle external tank is included in this paper as a validation and benchmark case of the system.

  1. Investigation of the Behavior of Steel Shear Walls Using Finite Elements Analysis

    OpenAIRE

    Abubakri, K.; Veladi, H.

    2016-01-01

    Currently, steel shear walls are considered by engineers as an economic method against lateral loads imposed by wind and earthquake in tall structures. Accordingly, there is a growing need to develop accurate methods alongside approximation methods to estimate the behavior of these structural elements. The finite element technique is one of the strongest numerical methods in analysis of solid mechanics problems. Finite element analysis however requires high technical knowledge of the behavior...

  2. GC-MS and FI-IR analysis of the bio-oil with addition of ethyl acetate during storage

    Directory of Open Access Journals (Sweden)

    Le eZhang

    2014-01-01

    Full Text Available Different mass fractions (0%, 3%, 6%, 9%, 12%, and 15% of ethyl acetate were added to bio-oil for improving its storage stability during storage at 40℃ for 35d. For different bio-oils during storage, physical properties were characterized and chemical components were determined by GC-MS and FT-IR. The results of properties characterization showed that, addition of ethyl acetate could instantly lower bio-oil viscosity, water content, and dramatically decrease the rate of aging. pH value of bio-oil can be instantly improved by adding ethyl acetate. GC-MS results revealed that addition of various content of ethyl acetate into bio-oil and its storage at 40℃ for 35d could both lead to disappearance of previous compounds and generation of new compounds. FT-IR results showed that addition of various content of ethyl acetate into bio-oils and its storage at 40℃ for 35d could slightly change the wavenumbers of substantial functional groups in bio-oils.

  3. Analysis of the ATR fuel element swaging process

    International Nuclear Information System (INIS)

    Richins, W.D.; Miller, G.K.

    1995-12-01

    This report documents a detailed evaluation of the swaging process used to connect fuel plates to side plates in Advanced Test Reactor (ATR) fuel elements. The swaging is a mechanical process that begins with fitting a fuel plate into grooves in the side plates. Once a fuel plate is positioned, a lip on each of two side plate grooves is pressed into the fuel plate using swaging wheels to form the joints. Each connection must have a specified strength (measured in terms, of a pullout force capacity) to assure that these joints do not fail during reactor operation. The purpose of this study is to analyze the swaging process and associated procedural controls, and to provide recommendations to assure that the manufacturing process produces swaged connections that meet the minimum strength requirement. The current fuel element manufacturer, Babcock and Wilcox (B ampersand W) of Lynchburg, Virginia, follows established procedures that include quality inspections and process controls in swaging these connections. The procedures have been approved by Lockheed Martin Idaho Technologies and are designed to assure repeatability of the process and structural integrity of each joint. Prior to July 1994, ATR fuel elements were placed in the Hydraulic Test Facility (HTF) at the Idaho National Engineering Laboratory (AGNAIL), Test Reactor Area (TRA) for application of Boehmite (an aluminum oxide) film and for checking structural integrity before placement of the elements into the ATR. The results presented in this report demonstrate that the pullout strength of the swaged connections is assured by the current manufacturing process (with several recommended enhancements) without the need for- testing each element in the HTF

  4. Analysis of elements in human blood of patients with chronic kidney disease using neutron activation analysis

    International Nuclear Information System (INIS)

    Metairon, S.; Zamboni, C.B.; Kovacs, L.; Genezini, F.A.; Santos, N.F.; Vilela, E.C.

    2009-01-01

    Neutron activation analysis has been used to determine Br, Ca, Cl, K, Mg and Na concentrations in whole blood of patients with chronic kidney disease (CKD) as well as in whole blood of normal individuals (control group). The dependence of the elements concentration in function of sex, age, time and type of treatment were investigated. The similarities and differences between healthy individuals and CKD are discussed. (author)

  5. Elemental analysis of coal by proton-induced x-ray emission analysis

    International Nuclear Information System (INIS)

    Cronch, S.M.; Ehmann, W.D.; Laumer, H.W.; Gabbard, F.

    1976-01-01

    Proton-induced x-ray emission was used to determine elemental concentrations in solid coal samples. The coal samples were irradiated with 2.5 to 5.5 MeV protons. Concentrations were determined from characteristic x-ray yields taking into account matrix absorption. The precision is shown by replicate analysis and the accuracy by comparison with results obtained by other laboratories using different techniques

  6. Imaging of lipids in atherosclerotic lesion in aorta from ApoE/LDLR-/- mice by FT-IR spectroscopy and Hierarchical Cluster Analysis.

    Science.gov (United States)

    P Wrobel, Tomasz; Mateuszuk, Lukasz; Chlopicki, Stefan; Malek, Kamilla; Baranska, Malgorzata

    2011-12-21

    Spectroscopy-based approaches can provide an insight into the biochemical composition of a tissue sample. In the present work Fourier transform infrared (FT-IR) spectroscopy was used to develop a reliable methodology to study the content of free fatty acids, triglycerides, cholesteryl esters as well as cholesterol in aorta from mice with atherosclerosis (ApoE/LDLR(-/-) mice). In particular, distribution and concentration of palmitic, oleic and linoleic acid derivatives were analyzed. Spectral analysis of pure compounds allowed for clear discrimination between free fatty acids and other similar moieties based on the carbonyl band position (1699-1710 cm(-1) range). In order to distinguish cholesteryl esters from triglycerides a ratio of carbonyl band to signal at 1010 cm(-1) was used. Imaging of lipids in atherosclerotic aortic lesions in ApoE/LDLR(-/-) mice was followed by Hierarchical Cluster Analysis (HCA). The aorta from C57Bl/6J control mice (fed with chow diet) was used for comparison. The measurements were completed with an FT-IR spectrometer equipped with a 128 × 128 FPA detector. In cross-section of aorta from ApoE/LDLR(-/-) mice a region of atherosclerotic plaque was clearly identified by HCA, which was later divided into 2 sub-regions, one characterized by the higher content of cholesterol, while the other by higher contents of cholesteryl esters. HCA of tissues deposited on normal microscopic glass, hence limited to the 2200-3800 cm(-1) spectral range, also identified a region of atherosclerotic plaque. Importantly, this region correlates with the area stained by standard histological staining for atherosclerotic plaque (Oil Red O). In conclusion, the use of FT-IR and HCA may provide a novel tool for qualitative and quantitative analysis of contents and distribution of lipids in atherosclerotic plaque.

  7. Elemental composition of platelets. Part I. Sampling and sample preparation of platelets for trace-element analysis

    International Nuclear Information System (INIS)

    Iyengar, G.V.; Borberg, H.; Kasperek, K.; Kiem, J.; Siegers, M.; Feinendegen, L.E.; Gross, R.

    1979-01-01

    Sampling of platelets for trace-element analysis poses special problems: obtaining adequate sample materials, achieving a sufficient cell purity, preserving viability (integrity), correcting for trapped plasma, and controlling contamination. We used a blood-cell separator for the primary isolation of platelets from blood, and differential centrifugation in natural plasma to further isolate them. The pyrimidopyrimidine RA233 was used as a stabilizer to maintain viability. 131 I-labeled human serum albumin was used to estimate trapped plasma. Contamination was controlled by using five-times-distilled water to simulate donor's blood in the system and by comparing three fractions: the serum, the first portion of the platelet-rich plasma, and the supernatant plasma after the final centrifugation. Neutron activation analysis was used for the elemental analysis. A single differential centrifugation of the platelet-rich plasma from the blood-cell separator at 400 x g for 8 min was optimum (mean mass fractions: erythrocytes/platelets < 5 mg/g and leukocytes/platelets < 20 mg/g). The trapped plasma in the wet platelet samples amounted to about 0.40 g/g. No appreciable contamination from the sampling system was found for the elements Ag, Cd, Co, Cr, Cs, Cu, Fe, Mo, Rb, Sb, Se, and Zn. 2 figures, 3 tables

  8. Bioinformatic analysis of Entamoeba histolytica SINE1 elements

    Directory of Open Access Journals (Sweden)

    Butcher Sarah A

    2010-05-01

    Full Text Available Abstract Background Invasive amoebiasis, caused by infection with the human parasite Entamoeba histolytica remains a major cause of morbidity and mortality in some less-developed countries. Genetically E. histolytica exhibits a number of unusual features including having approximately 20% of its genome comprised of repetitive elements. These include a number of families of SINEs - non-autonomous elements which can, however, move with the help of partner LINEs. In many eukaryotes SINE mobility has had a profound effect on gene expression; in this study we concentrated on one such element - EhSINE1, looking in particular for evidence of recent transposition. Results EhSINE1s were detected in the newly reassembled E. histolytica genome by searching with a Hidden Markov Model developed to encapsulate the key features of this element; 393 were detected. Examination of their sequences revealed that some had an internal structure showing one to four 26-27 nt repeats. Members of the different classes differ in a number of ways and in particular those with two internal repeats show the properties expected of fairly recently transposed SINEs - they are the most homogeneous in length and sequence, they have the longest (i.e. the least decayed target site duplications and are the most likely to show evidence (in a cDNA library of active transcription. Furthermore we were able to identify 15 EhSINE1s (6 pairs and one triplet which appeared to be identical or very nearly so but inserted into different sites in the genome; these provide good evidence that if mobility has now ceased it has only done so very recently. Conclusions Of the many families of repetitive elements present in the genome of E. histolytica we have examined in detail just one - EhSINE1. We have shown that there is evidence for waves of transposition at different points in the past and no evidence that mobility has entirely ceased. There are many aspects of the biology of this parasite which

  9. Statistical Energy Analysis (SEA) and Energy Finite Element Analysis (EFEA) Predictions for a Floor-Equipped Composite Cylinder

    Science.gov (United States)

    Grosveld, Ferdinand W.; Schiller, Noah H.; Cabell, Randolph H.

    2011-01-01

    Comet Enflow is a commercially available, high frequency vibroacoustic analysis software founded on Energy Finite Element Analysis (EFEA) and Energy Boundary Element Analysis (EBEA). Energy Finite Element Analysis (EFEA) was validated on a floor-equipped composite cylinder by comparing EFEA vibroacoustic response predictions with Statistical Energy Analysis (SEA) and experimental results. Statistical Energy Analysis (SEA) predictions were made using the commercial software program VA One 2009 from ESI Group. The frequency region of interest for this study covers the one-third octave bands with center frequencies from 100 Hz to 4000 Hz.

  10. Radiochemical neutron activation analysis based multi-elemental analysis of high purity gallium

    International Nuclear Information System (INIS)

    Tashimova, F.A.; Sadikov, I.I; Salimov, M.I.; Zinov'ev, V.G.

    2006-01-01

    Full text: Gallium is one of the widely used materials in semiconductor and optoelectronics industry. Gallium is used to produce infrared detectors, piezoelectric sensors, high- and low-temperature transistors for space and defense technology. One of the most important requirements for semiconductor materials of gallium compounds is an excessive high purity for layers and films. Information on impurities (type of an impurity, concentration, character of distribution) is important as for better understanding of the physical and chemical processes taking place in formed semiconductor structures and for the 'know-how' of devices on their basis. The object of this work is to develop radiochemical neutron activation technique for analysis of high purity gallium. Irradiation of 0.1 g of gallium sample in neutron flux of 5·10 13 cm -2 s -1 for 5 hours will result in induced activity of more than 10 8 Bq, due to 72 Ga radionuclide, half-life of which is 14.1 hours. Therefore to perform instrumental NAA of gallium long period (10 day) cooling is required, and high sensitive determination of elements producing short- and long-lived radionuclides (T 1/2 72 Ga. We have studied the behavior of gallium in extraction-chromatographic system 'TBP-HCl'. The experiments have shown that higher factor of distribution (D) and capacity on gallium can be achieved when 'TBP-4M HCl' system is used. However more than 10 trace elements have high D and thus they cannot be separated from 72 Ga. To resolve the problem and increase the number of separated trace elements we have used preliminary satisfaction of chromatographic column with tellurium, which has D higher than the most of elements in 'TBP-4M HCl' system and thus suppresses extraction of elements. Distribution profile of gallium along the column and elution curve of 25 trace elements have been measured. Chemical yields of separated elements measured by using radiotracers are more than 93%. On the basis of the carried out researches

  11. Preconcentration and Speciation of Trace Elements and Trace-Element Analogues of Radionuclides by Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Chatt, A.

    1999-01-01

    We have developed a number of preconcentration neutron activation analysis (PNAA) methods in our laboratory for the determination of trace elements in a variety of complex sample matrices. We developed a number of cocrystallization and coprecipitation methods for the determination of trace elements in water samples. We developed several methods for the determination of I in foods and diets. We have developed a number of PNAA methods in our laboratory We determined As and Sb in geological materials and natural waters by coprecipitation with Se and Au in silicate rocks and ores by coprecipitation with Te followed by NAA. We developed an indirect NAA method for the determination of B in leachates of borosilicate glass. We have been interested in studying the speciation of Am, Tc, and Np in simulated vitrified groundwater leachates of high-level wastes under oxid and anoxic conditions using a number of techniques. We then used PNAA methods to study speciation of trace-element analogues of radionuclides. We have been able to apply biochemical techniques and NAA for the separation, preconcentration, and characterization of metalloprotein and protein-bound trace-element species in subcellular fractions of bovine kidneys. Lately, we have concentrated our efforts to develop chemical and biochemical methods in conjunction with NAA, NMR, and MS for the separation and identification of extractable organohalogens (EOX) in tissues of beluga whales, cod, and northern pink shrimp

  12. Analysis of tracer elements in human hair using XRF

    International Nuclear Information System (INIS)

    Hou Jing; Gao Deyu; Zhao Li; Li Hong

    2004-01-01

    Using chemical addition method to calibrate absorption effect, trace element in human hair are analyzed with X-ray fluorescence (XRF). Based on practical samples of human hair, the relative matrix absorption efficienty is determined, and the relation ship between which and the most important componet Ca is fitted. The contents of Ca, Cu, Fe, Zn in the human hair are analyzed using the calibrated constants. A group of standard human hair samples are analyzed and the results are compared with the recommended value of the National Standard. The measured values show a good coincidence with the recommended values. Comparing to the GB, the deviations are Ca 0.28%, Fe 0.99%, Cu 2.6%, Zn 0; the relative errors are Ca 2.2%, Fe 1.7%, Cu 2.2%, Zn 1.1%, and the sensitivity is ≤2.2%. This method may be used to determine the tracing elements in human hair. (authors)

  13. Elemental analysis of river sediments by PIXE and PIGE

    International Nuclear Information System (INIS)

    Kennedy, V.J.; Augusthy, A.; Varier, K.M.; Magudapathy, P.; Panchapakesan, S.; Nair, K.G.M.; Vijayan, V.

    1999-01-01

    The Chaliyar river, located in Kerala, India has shown preoccupying pollution levels, that constitute a threat to public health and the ecological system. PIXE and PIGE techniques have been employed to measure the elemental concentrations in the river sediment samples. Thick targets were prepared out of the sediment samples collected from various sites along the course of the river. The measurements were carried out using 3 MeV proton beam obtained from 3 MV Tandem pelletron accelerator at Institute of Physics, Bhubaneswar. The elemental concentrations, especially that of heavy metals, at different sites are discussed in detail. Our results show that sediments from a site where the industrial activities are high are significantly high in concentrations of heavy metals (Cr, Ni, Cu, Zn, Hg and Pb) than those collected from non-industrial sites. The measured values are compared with the average composition of unpolluted river sediments and other national and international river sediments. (author)

  14. Elemental analysis using temporal gating of a pulsed neutron generator

    Energy Technology Data Exchange (ETDEWEB)

    Mitra, Sudeep

    2018-02-20

    Technologies related to determining elemental composition of a sample that comprises fissile material are described herein. In a general embodiment, a pulsed neutron generator periodically emits bursts of neutrons, and is synchronized with an analyzer circuit. The bursts of neutrons are used to interrogate the sample, and the sample outputs gamma rays based upon the neutrons impacting the sample. A detector outputs pulses based upon the gamma rays impinging upon the material of the detector, and the analyzer circuit assigns the pulses to temporally-based bins based upon the analyzer circuit being synchronized with the pulsed neutron generator. A computing device outputs data that is indicative of elemental composition of the sample based upon the binned pulses.

  15. Finite-element analysis of flawed and unflawed pipe tests

    International Nuclear Information System (INIS)

    James, R.J.; Nickell, R.E.; Sullaway, M.F.

    1989-12-01

    Contemporary versions of the general purpose, nonlinear finite element program ABAQUS have been used in structural response verification exercises on flawed and unflawed austenitic stainless steel and ferritic steel piping. Among the topics examined, through comparison between ABAQUS calculations and test results, were: (1) the effect of using variations in the stress-strain relationship from the test article material on the calculated response; (2) the convergence properties of various finite element representations of the pipe geometry, using shell, beam and continuum models; (3) the effect of test system compliance; and (4) the validity of ABAQUS J-integral routines for flawed pipe evaluations. The study was culminated by the development and demonstration of a ''macroelement'' representation for the flawed pipe section. The macroelement can be inserted into an existing piping system model, in order to accurately treat the crack-opening and crack-closing static and dynamic response. 11 refs., 20 figs., 1 tab

  16. Finite Element Method for Analysis of Material Properties

    DEFF Research Database (Denmark)

    Rauhe, Jens Christian

    and the finite element method. The material microstructure of the heterogeneous material is non-destructively determined using X-ray microtomography. A software program has been generated which uses the X-ray tomographic data as an input for the mesh generation of the material microstructure. To obtain a proper...... which are used for the determination of the effective properties of the heterogeneous material. Generally, the properties determined using the finite element method coupled with X-ray microtomography are in good agreement with both experimentally determined properties and properties determined using......The use of cellular and composite materials have in recent years become more and more common in all kinds of structural components and accurate knowledge of the effective properties is therefore essential. In this wok the effective properties are determined using the real material microstructure...

  17. Analysis of trace elements in serum from human eating irradiated food

    International Nuclear Information System (INIS)

    Huang Zongzhi; Zhou Hongdi; Chen Shijie; Gao Sumei

    1987-01-01

    A method of trace element analysis by Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AEC) in serum from human eating food preserved by irradiation is described. Trace element analysis in human serum is one of the research projects concerning the wholesomeness. 78 serum samples of the human eating food preserved by irradiation were collected. After ashing and solving ICP-AES analysis of serum is performed for detecting 12 trace elements in specimen solution. The detection limitations are in the range of 10 -2 - 10 -3 ppm for differemt elements. The recoveries of elements are over 73%. Concentrations of 12 trace elements in 78 human serum has been calculated with F and t tests at PDP 11/70 computer and it was concluded that there is no significant difference between testing group and control group

  18. PIXE and neutron activation analysis: intercomparison in the elemental concentration of airborne particulate matter

    International Nuclear Information System (INIS)

    Cassorla, V.; Rojas, X.; Gras, N.; Chuaqui, L.; Dinator, M.I.; Morales, J.R.; Llona, F.; Romo-Kroeger, C.

    1993-01-01

    Two nuclear analytical techniques, neutron activation analysis (NAA) and proton induced X-ray emission (PIXE), were used to determine major and trace elements in airborne particulate matter collected during the first fortnight of June 1991 at the La Reina Nuclear Center. NAA detected the presence of 15 elements in the samples. PIXE, for the same samples, allowed the detection of 12 elements. The elements determined by both techniques were Al, Ca, Mn, Fe, Cu, and Zn. A good correlation between results for these elements for each of the two techniques was demonstrated. (author)

  19. Trace element evaluation of different varieties of chewing gum by radiochemical neutron activation analysis

    International Nuclear Information System (INIS)

    Zaidi, J.H.; Arif, M.; Fatima, I.; Ahmad, S.; Qureshi, I.H.

    2000-01-01

    Extensive use of chewing gums, by children in particular, entails the evaluation of trace element contents in them. Radiochemical neutron activation analysis (RNAA) was successfully employed to determine the concentration of 35 trace elements (essential, toxic and nonessential) in eight different brands of chewing gum generally consumed in Rawalpindi/Islamabad area. Comparison of trace element data of our work with literature has been presented. None of the elements detected in the brands of chewing gum examined was found to be present at a level representing a substantial contribution to the total dietary intake of the element. (author)

  20. The Development of Piezoelectric Accelerometers Using Finite Element Analysis

    DEFF Research Database (Denmark)

    Liu, Bin

    1999-01-01

    This paper describes the application of Finite Element (FE) approach for the development of piezoelectric accelerometers. An accelerometer is simulated using the FE approach as an example. Good agreement is achieved between simulated results and calibrated results. It is proved that the FE modeling...... can be effectively used to predict the specifications of the accelerometer, especially when modification of the accelerometer is required. The FE developing technology forms the bases of fast responsiveness and flexible customized design of piezoelectric accelerometers....

  1. Elements that contribute to boost female entrepreneurship: A prospective analysis

    Directory of Open Access Journals (Sweden)

    Pilar Ortiz García

    2016-06-01

    Full Text Available This paper aims to identify what environmental modulators elements favor and contribute to enhance female entrepreneurship from a gender perspective. The qualitative study draws on 10 interviews in depth after being tested on their contents, from a relational perspective, allow a set of conclusions and recommendations that contribute to the empowerment of women entrepreneurs figure. The results highlight the importance of social support and comprehensive training in creating a culture that promotes and makes visible the role of women entrepreneurs.

  2. Glow discharge depth analysis of metallic elements in steels

    International Nuclear Information System (INIS)

    Berneron, R.

    The glow discharge lamp designed by Grimm gives new possibilities in the optical spectrometry. The plasma produced is a cool emissive source and its advantages are the following: low spectral background, no reabsorption, linear calibration, very stable emission, very high yield. The sputtering produced by ionic bombardment of the sample enables the depth repartition of several elements to be made in the same run [fr

  3. Thermohydraulic analysis in pipelines using the finite element method

    International Nuclear Information System (INIS)

    Costa, L.E.; Idelsohn, S.R.

    1984-01-01

    The Finite Element Method (FEM) is employed for the numerical solution of fluid flow problems with combined heat transfer mechanisms. Boussinesq approximations are used for the solution of the governing equations. The application of the FEM leads to a set of simultaneous nonlinear equations. The development of the method, for the solution of bidimensional and axisymmetric problems, is presented. Examples of fluid flow in pipes, including natural and forced convection, are solved with the proposed method and discussed in the paper. (Author) [pt

  4. Piezoelectric theory for finite element analysis of ultrasonic motors

    Energy Technology Data Exchange (ETDEWEB)

    Emery, J.D.; Mentesana, C.P.

    1997-06-01

    The authors present the fundamental equations of piezoelectricity and references. They show how a second form of the equations and a second set of coefficients can be found, through inversions involving the elasticity tensor. They show how to compute the clamped permittivity matrix from the unclamped matrix. The authors list the program pzansys.ftn and present examples of its use. This program does the conversions and calculations needed by the finite element program ANSYS.

  5. Multivariate analysis of attenuated total reflection Fourier transform infrared (ATR FT-IR) spectroscopic data to confirm phase partitioning in methacrylate-based dentin adhesive.

    Science.gov (United States)

    Ye, Qiang; Parthasarathy, Ranganathan; Abedin, Farhana; Laurence, Jennifer S; Misra, Anil; Spencer, Paulette

    2013-12-01

    Water is ubiquitous in the mouths of healthy individuals and is a major interfering factor in the development of a durable seal between the tooth and composite restoration. Water leads to the formation of a variety of defects in dentin adhesives; these defects undermine the tooth-composite bond. Our group recently analyzed phase partitioning of dentin adhesives using high-performance liquid chromatography (HPLC). The concentration measurements provided by HPLC offered a more thorough representation of current adhesive performance and elucidated directions to be taken for further improvement. The sample preparation and instrument analysis using HPLC are, however, time-consuming and labor-intensive. The objective of this work was to develop a methodology for rapid, reliable, and accurate quantitative analysis of near-equilibrium phase partitioning in adhesives exposed to conditions simulating the wet oral environment. Analysis by Fourier transform infrared (FT-IR) spectroscopy in combination with multivariate statistical methods, including partial least squares (PLS) regression and principal component regression (PCR), were used for multivariate calibration to quantify the compositions in separated phases. Excellent predictions were achieved when either the hydrophobic-rich phase or the hydrophilic-rich phase mixtures were analyzed. These results indicate that FT-IR spectroscopy has excellent potential as a rapid method of detection and quantification of dentin adhesives that experience phase separation under conditions that simulate the wet oral environment.

  6. Finite-element pre-analysis for pressurized thermoshock tests

    International Nuclear Information System (INIS)

    Keinaenen, H.; Talja, H.; Lehtonen, M.; Rintamaa, R.; Bljumin, A.; Timofeev, B.

    1992-05-01

    The behaviour of a model pressure vessel is studied in a pressurized thermal shock loading. The tests were performed at the Prometey Institute in St. Petersburg. The calculations were performed at the Technical Research Centre of Finland. The report describes the preliminary finite-element analyses for the fourth, fifth and sixth thermoshock tests with the first model pressure vessel. Seven pressurized thermoshock tests were made with the same model using five different flaw geometries. In the first three tests the flaw was actually a blunt notch. In the two following tests (tests 4 and 5) a sharp pre-crack was produced before the test. In the last two test (tests 6 and 7) the old crack was used. According to the measurements and post-test ultrasonic examination of the crack front, the sixth test led to significant crack extension. Both temperatures and stresses were calculated using the finite-element method. The calculations were made using the idealized initial flaw geometry and preliminary material data. Both two-and three-dimensional models were used in the calculations. J-integral values were calculated from the elastic-plastic finite-element results. The stress intensity factor values were evaluated on the basis of the calculated J-integrals and compared with the preliminary material fracture toughness data obtained from the Prometey Institute

  7. Elemental analysis and nutritional value of edible Trifolium (clover) species.

    Science.gov (United States)

    Gounden, Thaveshan; Moodley, Roshila; Jonnalagadda, Sreekantha B

    2018-04-30

    Trifolium species, commonly known as clover species, have a cosmopolitan distribution and, as such, are used in many different traditional systems of medicine and consumed by many communities all over the world. In this study, the elemental distribution and nutritional value of five edible Trifolium species, namely, Trifolium africanum, Trifolium burchellianum, Trifolium repens, Trifolium dubium and Trifolium pratense were investigated to evaluate the potential of these plant species to alleviate malnutrition, thereby contributing toward the fight against food insecurity. Trifolium species were found to be a rich alternate source of essential nutrients with concentrations of elements being in decreasing order of Ca > Mg > Fe > Mn > Zn > Se > Cu > Cr > Pb > Ni > Co > Cd > As and with adequate levels of lipids (4.2 to 8.6%), proteins (35.1 to 45.4%) and carbohydrates (26.7 to 47.0%). Trifolium species were found to be rich in Se (contributing greater than 516% toward its RDA) with T. dubium having a concentration of 0.53 mg 10 g -1 , dry mass, which is higher than Brazil nuts. T. pratense was found to be the most suitable species for human consumption due to it having low levels of toxic metals (As, Cd and Pb) while being rich in macro- and micro-elements, especially Fe (7.84 mg 10 g -1 , dry mass) and Se (0.36 mg 10 g -1 , dry mass).

  8. [Determination and correlation analysis of trace elements in Boletus tomentipes].

    Science.gov (United States)

    Li, Tao; Wang, Yuan-zhong; Zhang, Ji; Zhao, Yan-li; Liu, Hong-gao

    2011-07-01

    The contents of eleven trace elements in Boletus tomentipes were determined by inductively coupled plasma atomic emission spectroscopy (ICP-AES). The results showed that the fruiting bodies of B. tomentipes were very rich in Mg and Fe (>100 mg x kg(-1)) and rich in Mn, Zn and Cu (>10 mg x kg(-1)). Cr, Pb, Ni, Cd, and As were relatively minor contents (0.1-10.0 mg x kg(-1)) of this species, while Hg occurred at the smallest content (< 0.1 mg x kg(-1)). Among the determined 11 trace elements, Zn-Cu had significantly positive correlation (r = 0.659, P < 0.05), whereas, Hg-As, Ni-Fe, and Zn-Mg had significantly negative correlation (r = -0.672, -0.610, -0.617, P < 0.05). This paper presented the trace elements properties of B. tomentipes, and is expected to be useful for exploitation and quality evaluation of this species.

  9. Elements affecting wound healing time: An evidence based analysis.

    Science.gov (United States)

    Khalil, Hanan; Cullen, Marianne; Chambers, Helen; Carroll, Matthew; Walker, Judi

    2015-01-01

    The purpose of this study was to identify the predominant client factors and comorbidities that affected the time taken for wounds to heal. A prospective study design used the Mobile Wound Care (MWC) database to capture and collate detailed medical histories, comorbidities, healing times and consumable costs for clients with wounds in Gippsland, Victoria. There were 3,726 wounds documented from 2,350 clients, so an average of 1.6 wounds per client. Half (49.6%) of all clients were females, indicating that there were no gender differences in terms of wound prevalence. The clients were primarily older people, with an average age of 64.3 years (ranging between 0.7 and 102.9 years). The majority of the wounds (56%) were acute and described as surgical, crush and trauma. The MWC database categorized the elements that influenced wound healing into 3 groups--factors affecting healing (FAH), comorbidities, and medications known to affect wound healing. While there were a multitude of significant associations, multiple linear regression identified the following key elements: age over 65 years, obesity, nonadherence to treatment plan, peripheral vascular disease, specific wounds associated with pressure/friction/shear, confirmed infection, and cerebrovascular accident (stroke). Wound healing is a complex process that requires a thorough understanding of influencing elements to improve healing times.© 2015 by the Wound Healing Society. © 2015 by the Wound Healing Society.

  10. Advances in dynamic relaxation techniques for nonlinear finite element analysis

    International Nuclear Information System (INIS)

    Sauve, R.G.; Metzger, D.R.

    1995-01-01

    Traditionally, the finite element technique has been applied to static and steady-state problems using implicit methods. When nonlinearities exist, equilibrium iterations must be performed using Newton-Raphson or quasi-Newton techniques at each load level. In the presence of complex geometry, nonlinear material behavior, and large relative sliding of material interfaces, solutions using implicit methods often become intractable. A dynamic relaxation algorithm is developed for inclusion in finite element codes. The explicit nature of the method avoids large computer memory requirements and makes possible the solution of large-scale problems. The method described approaches the steady-state solution with no overshoot, a problem which has plagued researchers in the past. The method is included in a general nonlinear finite element code. A description of the method along with a number of new applications involving geometric and material nonlinearities are presented. They include: (1) nonlinear geometric cantilever plate; (2) moment-loaded nonlinear beam; and (3) creep of nuclear fuel channel assemblies

  11. Roughness analysis of graphite surfaces of casting elements

    Directory of Open Access Journals (Sweden)

    M. Wieczorowski

    2010-01-01

    Full Text Available In the paper profilometric measurements of graphite casting elements were described. Basic topics necessary to assess roughness of their surfaces and influence of asperities on various properties related to manufacturing and use were discussed. Stylus profilometer technique of surface irregularities measurements including its limits resulting from pickup geometry and its contact with measured object were ana-lyzed. Working principle of tactile profilometer and phenomena taking place during movement of a probe on a measured surface were shown. One of the important aspects is a flight phenomenon, which means movement of a pickup without contact with a surface during inspection resulting from too high scanning speed. results of comparison research for graphite elements of new and used mould and pin composing a set were presented. Using some surface roughness, waviness and primary profile parameters (arithmetical mean of roughness profile heights Ra, biggest roughness profile height Rz, maximum primary profile height Pt as well as maximum waviness profile height Wt a possibility of using surface asperities parameters as a measure of wear of chill graphite elements was proved. The most often applied parameter is Ra, but with a help of parameters from W and P family it was shown, that big changes occur not only for roughness but also for other components of surface irregularities.

  12. Thermal analysis of cracked bodies using finite element techniques

    International Nuclear Information System (INIS)

    Hellen, T.K.; Price, R.H.; Harrison, R.P.

    1975-01-01

    The paper develops the potential energy equation in terms of finite element theory including thermal loads. Following this, the energy release rate and consequently the stress intensity factors are derived. Considerations of the classical near crack tip equations are made and deficiencies with the popular substitution methods are highlighted. A method of removing these deficiencies is described. Various energy methods are reconsidered in terms of the role of the thermal energy contribution to the potential energy. These methods include work of crack closure, energy compliance and virtual crack extensions with no other change in nodal geometry, and therefore only requires the recalculation of the stiffness matrices of the crack tip elements. An example of a quadratic temperature gradient parallel to the crack plane in an edge cracked plate is described. Comparisons of the various finite element methods are made and generally show good agreement. A second application compares the virtual crack extension method with an approximate analytical solution in determining stress intensity factors for a thick hollow cylinder with an axial crack for various depths through the wall thickness and for different times. Initially the cylinder is at a uniform high temperature and is then subjected to a sustained cooling shock. Analytical solutions are available for temperature and stress distributions in the uncracked pipe. The stress intensity for a shallow crack in the early stages of the transient has been determined using a superposition procedure. Comparison of the analytical and computed results shows good agreement between the methods

  13. Power flow as a complement to statistical energy analysis and finite element analysis

    Science.gov (United States)

    Cuschieri, J. M.

    1987-01-01

    Present methods of analysis of the structural response and the structure-borne transmission of vibrational energy use either finite element (FE) techniques or statistical energy analysis (SEA) methods. The FE methods are a very useful tool at low frequencies where the number of resonances involved in the analysis is rather small. On the other hand SEA methods can predict with acceptable accuracy the response and energy transmission between coupled structures at relatively high frequencies where the structural modal density is high and a statistical approach is the appropriate solution. In the mid-frequency range, a relatively large number of resonances exist which make finite element method too costly. On the other hand SEA methods can only predict an average level form. In this mid-frequency range a possible alternative is to use power flow techniques, where the input and flow of vibrational energy to excited and coupled structural components can be expressed in terms of input and transfer mobilities. This power flow technique can be extended from low to high frequencies and this can be integrated with established FE models at low frequencies and SEA models at high frequencies to form a verification of the method. This method of structural analysis using power flo and mobility methods, and its integration with SEA and FE analysis is applied to the case of two thin beams joined together at right angles.

  14. Comparison of neutron activation analysis with other instrumental methods for elemental analysis of airborne particulate matter

    International Nuclear Information System (INIS)

    Regge, P. de; Lievens, F.; Delespaul, I.; Monsecour, M.

    1976-01-01

    A comparison of instrumental methods, including neutron activation analysis, X-ray fluorescence spectrometry, atomic absorption spectrometry and emission spectrometry, for the analysis of heavy metals in airborne particulate matter is described. The merits and drawbacks of each method for the routine analysis of a large number of samples are discussed. The sample preparation technique, calibration and statistical data relevant to each method are given. Concordant results are obtained by the different methods for Co, Cu, Ni, Pb and Zn. Less good agreement is obtained for Fe, Mn and V. The results are not in agreement for the elements Cd and Cr. Using data obtained on the dust sample distributed by Euratom-ISPRA within the framework of an interlaboratory comparison, the accuracy of each method for the various elements is estimated. Neutron activation analysis was found to be the most sensitive and accurate of the non-destructive analysis methods. Only atomic absorption spectrometry has a comparable sensitivity, but requires considerable preparation work. X-ray fluorescence spectrometry is less sensitive and shows biases for Cr and V. Automatic emission spectrometry with simultaneous measurement of the beam intensities by photomultipliers is the fastest and most economical technique, though at the expense of some precision and sensitivity. (author)

  15. OH/IR stars in the Galaxy

    International Nuclear Information System (INIS)

    Baud, B.

    1978-01-01

    Radio astronomical observations leading to the discovery of 71 OH/IR sources are described in this thesis. These OH/IR sources are characterized by their double peaked OH emission profile at a wavelength of 18 cm and by their strong IR infrared emission. An analysis of the distribution and radial velocities of a number of previously known and new OH/IR sources was performed. The parameter ΔV (the velocity separation between two emission peaks of the 18 cm line profile) was found to be a good criterion for a population classification with respect to stellar age

  16. Energy Finite Element Analysis Developments for Vibration Analysis of Composite Aircraft Structures

    Science.gov (United States)

    Vlahopoulos, Nickolas; Schiller, Noah H.

    2011-01-01

    The Energy Finite Element Analysis (EFEA) has been utilized successfully for modeling complex structural-acoustic systems with isotropic structural material properties. In this paper, a formulation for modeling structures made out of composite materials is presented. An approach based on spectral finite element analysis is utilized first for developing the equivalent material properties for the composite material. These equivalent properties are employed in the EFEA governing differential equations for representing the composite materials and deriving the element level matrices. The power transmission characteristics at connections between members made out of non-isotropic composite material are considered for deriving suitable power transmission coefficients at junctions of interconnected members. These coefficients are utilized for computing the joint matrix that is needed to assemble the global system of EFEA equations. The global system of EFEA equations is solved numerically and the vibration levels within the entire system can be computed. The new EFEA formulation for modeling composite laminate structures is validated through comparison to test data collected from a representative composite aircraft fuselage that is made out of a composite outer shell and composite frames and stiffeners. NASA Langley constructed the composite cylinder and conducted the test measurements utilized in this work.

  17. Analysis of pipe mitred bends using beam models - by finite element method

    International Nuclear Information System (INIS)

    Salles, A.C.S.L. de.

    1984-01-01

    The formulation of a recently proposed displacement based straight pipe element for the analysis of pipe mitred bends is summarized in this work. The element kinematics includes axial, bending, torsional and ovalisation displacements, all varying cubically along the axis of the element. Interaction effects between angle adjoined straight pipe section are modeled including the appropriate additional strain terms in the stiffness matrix formulation and by using a penalty procedure to enforce continuity of pipe skin flexural rotations at the common helical edge. The element model capabilities are ilustrated in some sample analysis and the results are compared with other available experimental, analytical or more complex numerical models. (Author) [pt

  18. 3-dimensional earthquake response analysis of embedded reactor building using hybrid model of boundary elements and finite elements

    International Nuclear Information System (INIS)

    Muto, K.; Motosaka, M.; Kamata, M.; Masuda, K.; Urao, K.; Mameda, T.

    1985-01-01

    In order to investigate the 3-dimensional earthquake response characteristics of an embedded structure with consideration for soil-structure interaction, the authors have developed an analytical method using 3-dimensional hybrid model of boundary elements (BEM) and finite elements (FEM) and have conducted a dynamic analysis of an actual nuclear reactor building. This paper describes a comparative study between two different embedment depths in soil as elastic half-space. As the results, it was found that the earthquake response intensity decreases with the increase of the embedment depth and that this method was confirmed to be effective for investigating the 3-D response characteristics of embedded structures such as deflection pattern of each floor level, floor response spectra in high frequency range. (orig.)

  19. Advanced neutron source reactor conceptual safety analysis report, three-element-core design: Chapter 15, accident analysis

    International Nuclear Information System (INIS)

    Chen, N.C.J.; Wendel, M.W.; Yoder, G.L.; Harrington, R.M.

    1996-02-01

    In order to utilize reduced enrichment fuel, the three-element-core design for the Advanced Neutron Source has been proposed. The proposed core configuration consists of inner, middle, and outer elements, with the middle element offset axially beneath the inner and outer elements, which are axially aligned. The three-element-core RELAP5 model assumes that the reactor hardware is changed only within the core region, so that the loop piping, heat exchangers, and pumps remain as assumed for the two-element-core configuration. To assess the impact of changes in the core region configuration and the thermal-hydraulic steady-state conditions, the safety analysis has been updated. This report gives the safety margins for the loss-of-off-site power and pressure-boundary fault accidents based on the RELAP5 results. AU margins are greater for the three-element-core simulations than those calculated for the two-element core

  20. Computer analysis with the CEASEMT finite element system

    International Nuclear Information System (INIS)

    Bung, H.; Clement, G.; Hoffmann, A.; Jakubowicz, H.

    1979-01-01

    This section presents results for the analyses of all three international Piping Benchmark Problems. An inelastic analysis of each problem was performed using a full three-dimensional shell analysis (TRICO code) and a simplified piping analysis based on beam theory (TEDEL code)