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Sample records for csitl crystal array

  1. Experimental studies on radiation damages of CsI(Tl) crystals

    International Nuclear Information System (INIS)

    He Jingtang; Mao Yufang; Dong Xiaoli; Chen Duanbao; Li Zuhao

    1997-01-01

    The results of experimental studies on radiation damage of CsI(Tl) crystal were reported. There are radiation damage effects on CsI(Tl) crystal. Experimental studies on recovery of damaged CsI(Tl) crystals were made. It seems that after heating at 200 degree C for 4 hours, the damaged crystals could be recovered completely

  2. Comparison of functional parameters of CsI:Tl crystals and thick films

    International Nuclear Information System (INIS)

    Fedorov, A.; Gektin, A.; Lebedynskiy, A.; Mateychenko, P.; Shkoropatenko, A.

    2013-01-01

    500 mkm thick CsI:Tl columnar films can be produced using thermal evaporation in vacuum by sublimation of the same bulk crystal. Comparison of afterglow and radiation stability of deposited CsI:Tl films with source crystal was the aim of current work. It is shown that the afterglow in the films is always below its level in initial single crystal. It was ascertained that the annealing atmospheres influence the processes leading to the activator depletion of the films during the thermal processing. -- Highlights: ► Thick CsI:Tl columnar films were obtained by thermal evaporation in vacuum. ► Radiation stability of such CsI:Tl films appears to be better than that of crystal. ► CsI:Tl film parameters can be modified by annealing in different atmospheres

  3. Color centers in heavily irradiated CsI(Tl) crystals

    International Nuclear Information System (INIS)

    Yakovlev, V.; Meleshko, A.; Trefilova, L.

    2008-01-01

    The absorption and luminescence properties of CsI(Tl) crystals colored by irradiation are studied by the method of the time-resolved spectroscopy. The scheme of the electron transitions in CsI(Tl) crystal is suggested to explain the appearance of the color centers under exposure to the near-UV light. It is established that either of the two types activator color centers holds the charge carrier with opposite sign. The model of the hole Tl 2+ v c - activator color center is suggested. According to the model the positive charge of Tl 2+ ion is compensated by the negative charge of a close cation vacancy v c - . The color center emission reveals in the cathode-luminescence spectrum of the colored CsI(Tl) crystal. The high-dose irradiation of CsI(Tl) crystal results in the reduction of the decay time of the near-thallium self-trapped excitons (STE) emission. The decay kinetics of Tl 2+ v c - emission contains the time components typical for the decay kinetics of near-thallium STE emission. The reason of the observed effects is the energy transfer from the near-thallium STE excitons to the color centers via the inductive-resonant mechanism

  4. Novel laser-processed CsI:Tl detector for SPECT

    Energy Technology Data Exchange (ETDEWEB)

    Sabet, H., E-mail: hsabet@mgh.harvard.edu; Uzun-Ozsahin, D.; El-Fakhri, G. [Massachusetts General Hospital, Harvard Medical School, Boston, Massachusetts 02129 (United States); Bläckberg, L. [Massachusetts General Hospital, Harvard Medical School, Boston, Massachusetts 02129 and Department of Physics and Astronomy, Uppsala University, Uppsala 75120 (Sweden)

    2016-05-15

    Purpose: The aim of this work is to demonstrate the feasibility of a novel technique for fabrication of high spatial resolution CsI:Tl scintillation detectors for single photon emission computed tomography systems. Methods: The scintillators are fabricated using laser-induced optical barriers technique to create optical microstructures (or optical barriers) inside the CsI:Tl crystal bulk. The laser-processed CsI:Tl crystals are 3, 5, and 10 mm in thickness. In this work, the authors focus on the simplest pattern of optical barriers in that the barriers are created in the crystal bulk to form pixel-like patterns resembling mechanically pixelated scintillators. The monolithic CsI:Tl scintillator samples are fabricated with optical barrier patterns with 1.0 × 1.0 mm{sup 2} and 0.625 × 0.625 mm{sup 2} pixels. Experiments were conducted to characterize the fabricated arrays in terms of pixel separation and energy resolution. A 4 × 4 array of multipixel photon counter was used to collect the scintillation light in all the experiments. Results: The process yield for fabricating the CsI:Tl arrays is 100% with processing time under 50 min. From the flood maps of the fabricated detectors exposed to 122 keV gammas, peak-to-valley (P/V) ratios of greater than 2.3 are calculated. The P/V values suggest that regardless of the crystal thickness, the pixels can be resolved. Conclusions: The results suggest that optical barriers can be considered as a robust alternative to mechanically pixelated arrays and can provide high spatial resolution while maintaining the sensitivity in a high-throughput and cost-effective manner.

  5. Novel laser-processed CsI:Tl detector for SPECT

    International Nuclear Information System (INIS)

    Sabet, H.; Uzun-Ozsahin, D.; El-Fakhri, G.; Bläckberg, L.

    2016-01-01

    Purpose: The aim of this work is to demonstrate the feasibility of a novel technique for fabrication of high spatial resolution CsI:Tl scintillation detectors for single photon emission computed tomography systems. Methods: The scintillators are fabricated using laser-induced optical barriers technique to create optical microstructures (or optical barriers) inside the CsI:Tl crystal bulk. The laser-processed CsI:Tl crystals are 3, 5, and 10 mm in thickness. In this work, the authors focus on the simplest pattern of optical barriers in that the barriers are created in the crystal bulk to form pixel-like patterns resembling mechanically pixelated scintillators. The monolithic CsI:Tl scintillator samples are fabricated with optical barrier patterns with 1.0 × 1.0 mm"2 and 0.625 × 0.625 mm"2 pixels. Experiments were conducted to characterize the fabricated arrays in terms of pixel separation and energy resolution. A 4 × 4 array of multipixel photon counter was used to collect the scintillation light in all the experiments. Results: The process yield for fabricating the CsI:Tl arrays is 100% with processing time under 50 min. From the flood maps of the fabricated detectors exposed to 122 keV gammas, peak-to-valley (P/V) ratios of greater than 2.3 are calculated. The P/V values suggest that regardless of the crystal thickness, the pixels can be resolved. Conclusions: The results suggest that optical barriers can be considered as a robust alternative to mechanically pixelated arrays and can provide high spatial resolution while maintaining the sensitivity in a high-throughput and cost-effective manner.

  6. Radiation Hardness Study of CsI(Tl) Crystals for Belle II Calorimeter

    CERN Document Server

    Matvienko, D V; Sedov, E V; Shwartz, B A

    2017-01-01

    The Belle II calorimeter (at least, its barrel part) consists of CsI(Tl) scintillation crystals which have been used at the Belle experiment. We perform the radiation hardness study of some typical Belle crystals and conclude their light output reductions are acceptable for Belle II experiment where the absorption dose can reach 10 krad during the detector operation. CsI(Tl) crystals have high stablity and low maintenance cost and are considered as possible option for the calorimeter of the future Super-Charm-Tau factory (SCT) in Novosibirsk. Our study demonstrates sufficiently high radiation hardness of CsI(Tl) crystals for SCT conditions.

  7. Development of low-background CsI(Tl) crystals for WIMP search

    International Nuclear Information System (INIS)

    Lee, H.S.; Bhang, H.; Hahn, I.S.; Hwang, M.J.; Kim, H.J.; Kim, S.C.; Kim, S.K.; Kim, S.Y.; Kim, T.Y.; Kim, Y.D.; Kwak, J.W.; Kwon, Y.J.; Lee, J.; Lee, J.I.; Lee, M.J.; Li, J.; Myung, S.S.; Park, H.; Zhu, J.J.

    2007-01-01

    Search for weakly interacting massive particles (WIMPs) is being carried out at the underground laboratory, Yangyang, Korea. Characteristics and internal background of CsI(Tl) crystal have been investigated. In our extensive R and D, we reduced internal background in the CsI(Tl) crystal. With the latest, we have achieved 5.50+/-0.10cpd (counts/keV/kg/day) at 10-15keV low-energy region. Further reduction of internal background is foreseen with the CsI powder lately produced

  8. Silicon drift detectors coupled to CsI(Tl) scintillators for spaceborne gamma-ray detectors

    International Nuclear Information System (INIS)

    Marisaldi, M.; Fiorini, C.; Labanti, C.; Longoni, A.; Perotti, F.; Rossi, E.; Soltau, H.

    2006-01-01

    Silicon Drift Detectors (SDDs), thanks to their peculiar low noise characteristics, have proven to be excellent photodetectors for CsI(Tl) scintillation light detection. Two basic detector configurations have been developed: either a single SDD or a monolithic array of SDDs coupled to a single CsI(Tl) crystal. A 16 independent detectors prototype is under construction, designed to work in conjunction with the MEGA Compton telescope prototype under development at MPE, Garching, Germany. A single SDD coupled to a CsI(Tl) crystal has also been tested as a monolithic detector with an extended energy range between 1.5 keV and 1 MeV. The SDD is used as a direct X-ray detector for low energy photons interacting in silicon and as a scintillation light photodetector for photons interacting in the crystal. The type of interaction is identified by means of pulse shape discrimination technique. Detectors based on an array of SDDs coupled to a single CsI(Tl) crystal have also been built. The readout of these detectors is based on the Anger camera technique, and submillimeter spatial resolution can be achieved. The two detectors' approaches and their applications will be described

  9. Development of low background CsI(Tl) and NaI(Tl) crystals for WIMP search

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Hyun Su [Department of Physics, Ewha Womans University, Seoul 120-750 (Korea, Republic of)

    2015-08-17

    We have developed low background CsI(Tl) and NaI(Tl) crystals to search for weakly interacting massive particles as well as to verify the origin of the annual modulation signal observed by the DAMA/LIBRA experiment. Extensive studies about the contamination mechanisim of {sup 137}Cs in CsI powder lead to the growth of ultra-low-background CsI(Tl) crystals. Similar approaches for NaI(Tl) crystals have been applied to reduce internal backgrounds to less than 0.5 counts/kg/day/keV. Status and understanding of backgrounds and background reduction in NaI(Tl) crystals will be discussed.

  10. Hadronic vs. electromagnetic pulse shape discrimination in CsI(Tl) for high energy physics experiments

    Science.gov (United States)

    Longo, S.; Roney, J. M.

    2018-03-01

    Pulse shape discrimination using CsI(Tl) scintillators to perform neutral hadron particle identification is explored with emphasis towards application at high energy electron-positron collider experiments. Through the analysis of the pulse shape differences between scintillation pulses from photon and hadronic energy deposits using neutron and proton data collected at TRIUMF, it is shown that the pulse shape variations observed for hadrons can be modelled using a third scintillation component for CsI(Tl), in addition to the standard fast and slow components. Techniques for computing the hadronic pulse amplitudes and shape variations are developed and it is shown that the intensity of the additional scintillation component can be computed from the ionization energy loss of the interacting particles. These pulse modelling and simulation methods are integrated with GEANT4 simulation libraries and the predicted pulse shape for CsI(Tl) crystals in a 5 × 5 array of 5 × 5 × 30 cm3 crystals is studied for hadronic showers from 0.5 and 1 GeV/c KL0 and neutron particles. Using a crystal level and cluster level approach for photon vs. hadron cluster separation we demonstrate proof-of-concept for neutral hadron detection using CsI(Tl) pulse shape discrimination in high energy electron-positron collider experiments.

  11. Light yield of a CsI(Tl) crystal under irradiation by protons with the energy from 3 to 15 MeV

    International Nuclear Information System (INIS)

    Dorchoman, D.; Konstantin, M.; Lazarovich, D.; Muntyanu, I.; Oganesyan, K.O.; Porokhovoj, S.Yu.

    1976-01-01

    Measurement results are presented of light yield in CsI(Tl) crystals at the irradiation by protons with the energy from 3 to 15 MeV. Plates of 100x100x2 mm size are used as CsI(Tl) scintillator samples. A brief analysis of possible sistematic errors is given which allows to estimate the total error upon the light yield valve determination equal to 0,5%. Measurement results of crystal light yield show that the dependence of CsI(Tl) light yield on proton energy is described by the straight line passing through the origin

  12. Scintillation detector composed by new type of avalanche photodiode and CsI(Tl) crystal

    International Nuclear Information System (INIS)

    He Jingtang; Chen Duanbao; Li Zuhao; Mao Yufang; Dong Xiaoli

    1996-01-01

    Using S5345 type of avalanche photodiode produced by Hamamatsu for the CsI(Tl) crystal readout, the spectrum of γ ray were measured. Energy resolution of 6.8% for 1.27 MeV γ ray from 22 Na source was obtained. The relation between energy resolution and coupling area, dimension of crystal, shaping time and bias were measured

  13. Experimental studies on using silicon photodiode as read-out component of CsI(Tl) crystal

    International Nuclear Information System (INIS)

    He Jingtang; Chen Duanbao; Li Zuhao; Mao Yufang; Dong Xiaoli

    1996-01-01

    Experimental studies on using silicon photodiode as the read-out component of CsI(Tl) crystal are reported. The read-out properties of two different types of silicon photodiode produced by Hamamatsu were measured, including relations between energy resolution and bias, shaping time, sensitive area of photodiode and the dimension of the crystal

  14. Impact of precursor purity on optical properties and radiation detection of CsI:Tl scintillators

    Energy Technology Data Exchange (ETDEWEB)

    Saengkaew, Phannee; Cheewajaroen, Kulthawat; Yenchai, Chadet; Thong-aram, Decho [Chulalongkorn University, Department of Nuclear Engineering, Faculty of Engineering, Bangkok (Thailand); Sanorpim, Sakuntam [Chulalongkorn University, Department of Physics, Faculty of Science, Bangkok (Thailand); Jitpukdee, Manit [Kasetsart University, Department of Applied Radiation and Isotope, Faculty of Science, Bangkok (Thailand); Yordsri, Visittapong; Thanachayanont, Chanchana [Ministry of Science and Technology, National Metal and Materials Technology Center, National Science and Technology Development Agency, Pathumthani (Thailand); Nuntawong, Noppadon [Ministry of Science and Technology, National Electronic and Computer Technology Center, National Science and Technology Development Agency, Pathumthani (Thailand)

    2016-08-15

    Cesium iodide doped with thallium (CsI:Tl) crystals was grown to develop the gamma-ray detectors by using low-cost raw materials. Effect of impurities on optical properties and radiation detection performance was investigated. By a modified homemade Bridgman-Stockbarger technique, CsI:Tl samples were grown in two levels of CsI and TlI reactant materials, i.e., having as a very high purity of 99.999 % and a high purity of 99.9 %. XRD measurements indicate CsI:Tl crystals having a good quality with a dominant (110) plane. Having a cubic structure, a lattice constant of CsI crystals of 0.4574 nm and a crystallite size of 43.539 nm were obtained. From the lower-purity raw materials, calcite was found in an orange crystal with a lattice constant of 0.4560 nm and a crystallite size of 43.089 nm. By PL measurements, the optical properties of the CsI:Tl crystals were analyzed. ∝540-nm-wavelength PL peak was observed from the colorless high-purity crystal, and ∝600-nm-wavelength PL peak was observed from the orange crystal. The brighter PL emission was obtained from the orange crystals suggesting impurities. CsI:Tl surface morphology by SEM exhibited a smooth surface with some parallel crystal facets. For electrical properties of high-quality CsI:Tl crystals, the electrical resistances were 230 ± 16 MΩ in cross-sectional direction and 714 ± 136 MΩ in vertical direction with respect to more homogeneous crystal quality in cross-sectional direction than that in vertical direction. TEM measurement was applied to evaluate the microstructure of colorless CsI:Tl crystal with different patterns of a cubic structure. Both CsI:Tl crystals show good efficiencies and good resolutions. Maintaining the same electronic conditions and amplifications, the colorless CsI:Tl scintillators represented a higher detection efficiency at 122 keV of Co-57 of 78.4 % and the energy resolution of 23.3 % compared to the detection efficiency of 75.9 % and the energy resolution of 34.6 % of the

  15. Development of surgical gamma probes with TlBr semiconductors and CsI(Tl) scintillators crystals

    International Nuclear Information System (INIS)

    Costa, Fabio Eduardo da

    2006-01-01

    Radio guided surgery, using probes with radiation detectors, has been prominence in the medical area in the last decade. This technique consists in injecting a radioactive substance to concentrate in tumour and assist the localization during the surgical procedure. The radio guided surgeries allowing the identification of lymph node has revolutioned the behavior of tumour in initial stadium when are being spread by lymphatic way. The conditions imposed to the surgery due the proximity between some lymph nodes, demands of the probes, a small diameters and capacity of individual identification of these lymph nodes radiolabelled by a specific tracer. The international market supplies these probes with CdTe semiconductors and scintillators, but there is some time lack a promptly technical assistance in the Brazilian market. This work developed probes with national technology, using CsI(Tl) scintillators crystals and, in substitution to CdTe crystals semiconductors, the TlBr crystal, that is a new semiconductor detector in a world-wide development, with advantages in relation to the CdTe. Both crystals have been grown in IPEN. All the necessary electronics, specially, the preamplifier, that was also a restrictive factor for development of these types of probe in the country, have been developed with components found in the national market. Systematic measures of spatial resolution, spatial selectivity, maximum sensitivity and quality of the shielding have been carried the probes development. The results have shown that the probes, one with the CsI(Tl) crystal and another with TlBr semiconductor presented the requested performance in the international literature for radio guided probes. (author)

  16. Comparison of CsI(Tl) and CsI(Na) partially slotted crystals for high-resolution SPECT imaging

    International Nuclear Information System (INIS)

    Giokaris, N.; Loudos, G.; Maintas, D.; Karabarbounis, A.; Lembesi, M.; Spanoudaki, V.; Stiliaris, E.; Boukis, S.; Sakellios, N.; Karakatsanis, N.; Gektin, A.; Boyarintsev, A.; Pedash, V.; Gayshan, V.

    2006-01-01

    Dedicated systems based on Position Sensitive Photomultiplier Tubes (PSPMTs) coupled to scintillators, have been used over the past years for the construction of compact systems, suitable for applications such as small animal imaging and small organs imaging. Most of the proposed systems are based on fully pixelized scintillators. Previous studies have shown that partially slotted scintillators offer a good compromise between cost, energy resolution and spatial resolution. In this work, the performance of two sets of CsI(Tl) and CsI(Na) partially slotted crystals is compared. Initial results show that CsI(Tl) scintillators are more suitable for gamma-ray detection, since their performance in terms of sensitivity, spatial and energy resolution is superior than that of CsI(Na)

  17. A study of the impact of radiation exposure on the uniformity of large CsI(Tl) crystals for the BaBar detector

    International Nuclear Information System (INIS)

    Hryn'ova, Tetiana; Kim, Peter; Kocian, Martin; Perl, Martin; Rogers, Howard; Schindler, Rafe H.; Wisniewski, William J.

    2004-01-01

    We describe an apparatus that allows simultaneous exposure of large CsI(Tl) crystals to ionizing radiation and precise measurement of the longitudinal changes in light yield of the crystals. We present herein the results from this device for exposures up to 10krad

  18. Search for solar axions with CsI(Tl) crystal detectors

    Energy Technology Data Exchange (ETDEWEB)

    Yoon, Y.S. [Center for Underground Physics, Institute for Basic Science (IBS), Daejon 34047 (Korea, Republic of); Park, H.K. [Center for Underground Physics, Institute for Basic Science (IBS), Daejon 34047 (Korea, Republic of); Basic Science, IBS-UST School, Daejeon 34047 (Korea, Republic of); Bhang, H.; Choi, J.H. [Department of Physics and Astronomy, Seoul National University, Seoul 08826 (Korea, Republic of); Collaboration: The KIMS collaboration

    2016-06-01

    The results of a search for solar axions from the Korea Invisible Mass Search (KIMS) experiment at the Yangyang Underground Laboratory are presented. Low-energy electron-recoil events would be produced by conversion of solar axions into electrons via the axio-electric effect in CsI(Tl) crystals. Using data from an exposure of 34,596 kg⋅days, we set a 90 % confidence level upper limit on the axion-electron coupling, g{sub ae}, of 1.39×10{sup −11} for an axion mass less than 1 keV/c{sup 2}. This limit is lower than the indirect solar neutrino bound, and fully excludes QCD axions heavier than 0.48 eV/c{sup 2} and 140.9 eV/c{sup 2} for the DFSZ and KSVZ models respectively.

  19. Pulse shape discrimination properties of Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12}:Ce,B single crystal in comparison with CsI:Tl

    Energy Technology Data Exchange (ETDEWEB)

    Rawat, S. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Department of Physics, Indian Institute of Technology, Roorkee 247667 (India); Tyagi, Mohit [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Netrakanti, P.K.; Kashyap, V.K.S.; Mitra, A. [Nuclear Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Singh, A.K.; Desai, D.G. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India); Kumar, G. Anil [Department of Physics, Indian Institute of Technology, Roorkee 247667 (India); Gadkari, S.C. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai 400085 (India)

    2016-12-21

    Single crystals of Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12}:Ce,B and CsI:Tl were grown by Czochralski and Bridgman techniques, respectively. While both the crystals exhibited similar emission at about 550 nm, their scintillation decay times showed significantly different characteristics. The average scintillation decay time of Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12}:Ce,B crystal was found to be about 284 ns for alpha excitation compared to 108 ns measured for a gamma source. On the other hand in CsI:Tl crystals, the alpha excitation resulted in a lower average decay time of 600 ns compared to 1200 ns with gamma excitation. Their pulse shape discrimination (PSD) for gamma and alpha radiations were studied by coupling the scintillators with photomultiplier tube or SiPM and employing an advanced digitizer as well as a conventional zero-crossing setup. In spite of having a poor α/γ light yield ratio, the PSD figure of merit and the difference of zero-crossing time in Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12}:Ce,B crystals were found to be superior in comparison to CsI:Tl crystals.

  20. Structure and scintillation properties of CsI(Tl) films on Si single crystal substrates

    Energy Technology Data Exchange (ETDEWEB)

    Guo, Lina [State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Information, University of Electronic Science and Technology of China, Chengdu 610054 (China); Liu, Shuang, E-mail: shuangliu@uestc.edu.cn [State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Information, University of Electronic Science and Technology of China, Chengdu 610054 (China); Chen, Dejun; Zhang, Shangjian; Liu, Yong; Zhong, Zhiyong [State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Information, University of Electronic Science and Technology of China, Chengdu 610054 (China); Falco, Charles M. [University of Arizona, College of Optical Sciences, AZ 85721 (United States)

    2016-10-30

    Highlights: • We obtained the desired micro-columnar structure of CsI(Tl) films on the orienting Si substrates. • We improved the micro-columnar structure of CsI(Tl) films under the relatively large deposition rate through using the substrate with a pre-deposited CsI nanolayer. • We modeled the interface structures between the CsI(Tl) films with (200) and (310) orientation and Si(111) substrates to explain the preferred orientation of film under the influence of the orienting substrate significantly. • We gained a new spectrum of the CsI(Tl) films peaked at 740 nm wavelength. - Abstract: CsI(Tl) scintillation films fabricated on glass substrates are widely applied for X-ray imaging because their ability to grow in micro-columnar structure and proper emission wavelength matching CCD cameras. But the coupling process between the CsI(Tl) films and Si-based photo detector would cause coupling loss. In this work, CsI(Tl) films were deposited on the orienting Si substrates and the Si substrates covered by the pre-deposited CsI nanolayers. Structure and scintillation properties of films were examined by using scanning electron microscopy, X-ray diffraction, photoluminescence and radioluminescent spectrum. The films deposited on the orienting Si substrates show the micro-columnar morphology with perfect single crystalline structure and the photoluminescence spectra with bimodal distribution. The performances of the films prepared on the pre-deposited CsI nanolayer, containing micro-columns structure and the light yield are improved.

  1. Structure and scintillation properties of CsI(Tl) films on Si single crystal substrates

    International Nuclear Information System (INIS)

    Guo, Lina; Liu, Shuang; Chen, Dejun; Zhang, Shangjian; Liu, Yong; Zhong, Zhiyong; Falco, Charles M.

    2016-01-01

    Highlights: • We obtained the desired micro-columnar structure of CsI(Tl) films on the orienting Si substrates. • We improved the micro-columnar structure of CsI(Tl) films under the relatively large deposition rate through using the substrate with a pre-deposited CsI nanolayer. • We modeled the interface structures between the CsI(Tl) films with (200) and (310) orientation and Si(111) substrates to explain the preferred orientation of film under the influence of the orienting substrate significantly. • We gained a new spectrum of the CsI(Tl) films peaked at 740 nm wavelength. - Abstract: CsI(Tl) scintillation films fabricated on glass substrates are widely applied for X-ray imaging because their ability to grow in micro-columnar structure and proper emission wavelength matching CCD cameras. But the coupling process between the CsI(Tl) films and Si-based photo detector would cause coupling loss. In this work, CsI(Tl) films were deposited on the orienting Si substrates and the Si substrates covered by the pre-deposited CsI nanolayers. Structure and scintillation properties of films were examined by using scanning electron microscopy, X-ray diffraction, photoluminescence and radioluminescent spectrum. The films deposited on the orienting Si substrates show the micro-columnar morphology with perfect single crystalline structure and the photoluminescence spectra with bimodal distribution. The performances of the films prepared on the pre-deposited CsI nanolayer, containing micro-columns structure and the light yield are improved.

  2. Pulse shape analysis using CsI(Tl) Crystals

    International Nuclear Information System (INIS)

    Silva, J.; Fiori, E.; Loher, B.; Savran, D.; Wirth, R.; Vencelj, M.

    2013-06-01

    The decay time of CsI(Tl) scintillating material consists of more than a single exponential component. The ratio between the intensity of these components varies as a function of the ionizing power of the absorbed particles, such as γ -rays or protons, and the temperature. This property can therefore be used for particle discrimination and for temperature monitoring, using pulse shape analysis. An unsupervised method that uses fuzzy clustering algorithms for particle identification based on pulse shape analysis is presented. The method is applied to discriminate between photon and proton-induced signals in CsI(Tl) scintillator detectors. The first results of a method that uses pulse shape analysis for correcting the temperature-dependent gain effect of the detector are also presented. The method aims at conserving a good energy resolution in a temperature varying environment without the need to measure the temperature of the detector externally (authors)

  3. Limits on Interactions between Weakly Interacting Massive Particles and Nucleons Obtained with CsI(Tl) Crystal Detectors

    International Nuclear Information System (INIS)

    Lee, H. S.; Bhang, H. C.; Choi, J. H.; Kim, D. W.; Kim, S. C.; Kim, S. K.; Kwak, J. W.; Lee, J.; Lee, J. H.; Lee, M. J.; Lee, S. J.; Myung, S. S.; Ryu, S.; Dao, H.; Li, J.; Li, X.; Li, Y. J.; Yue, Q.; Zhu, J. J.; Hahn, I. S.

    2007-01-01

    The Korea Invisible Mass Search (KIMS) experiment presents new limits on the weakly interacting massive particle (WIMP)-nucleon cross section using data from an exposure of 3409 kg·d taken with low-background CsI(Tl) crystals at the Yangyang Underground Laboratory. The most stringent limit on the spin-dependent interaction for a pure proton case is obtained. The DAMA signal region for both spin-independent and spin-dependent interactions for the WIMP masses greater than 20 GeV/c 2 is excluded by the single experiment with crystal scintillators

  4. Temperature dependence of CsI(Tl) gamma-ray excited scintillation characteristics

    International Nuclear Information System (INIS)

    1993-01-01

    Gamma-ray excited emission spectrum, absolute scintillation yield, rise and decay time constants, and thermoluminescence emissions of CsI(Tl) were measured at -100 to +50 C, for crystals from 4 different vendors. The thermoluminescence glow curves were the only property that varied significantly from crystal to crystal; room temperature operation in current mode could be susceptible to temperature fluctuations. The CsI(Tl) emission spectrum has emission bands peaking around 400 and 560 nm; the former band disappears between -50 and -75 C. The RT absolute scintillation yield was calculated to be 65,500±4,100 photons/MeV. The two primary decay time constants increases about exponentially with inverse temperature. An ultra-fast decay component was confirmed. Applications are discussed

  5. Studies of scintillation light nonproportionality of ZnSe(Te), CsI(Tl) and YAP(Ce) crystals using heavy ions

    CERN Document Server

    Klamra, W; Kapusta, M; Kérek, A; Moszynski, M; Norlin, L O; Novák, D; Possnert, G

    2002-01-01

    The scintillation light yield for ZnSe(Te), CsI(Tl) and YAP(Ce) crystals have been studied with alpha particles, sup 1 sup 2 C and sup 8 sup 1 Br in the energy region 2.8-42.2 MeV. A nonproportional behavior was observed, mostly pronounced for alpha particles on YAP(Ce). The results are understood in terms of delta-rays effect.

  6. Results from an investigation of the physical origins of nonproportionality in CsI(Tl)

    Science.gov (United States)

    Asztalos, S.; Hennig, W.; Warburton, W. K.

    2011-10-01

    The relative scintillation response per energy deposited by Compton electrons, or nonproportionality, has traditionally been considered an intrinsic scintillator property. However, such an interpretation is inconsistent with recent results that show nonproportionality to depend on external factors such as shaping time, temperature and supplier. Apparently, at least some of the overall nonproportionality has an extrinsic origin. In this work we describe the results from a suite of measurements designed to test the hypothesis that nonproportionality in CsI(Tl) material has an extrinsic component that correlates with impurity levels. Our choice of material was motivated by the excellent energy resolution observed in one bulk crystal (6.4%)—a marked departure from that measured with conventional CsI(Tl) stock (8-8.5%). Six bulk CsI(Tl) crystals were procured and diced into 44 wafers. Using X-ray fluorescence techniques no conclusive evidence for impurities was found in any of the wafers at the 1-50 ppm level. One crystal exhibited a distinct correlation among energy resolution, decay lifetimes, nonproportionality and a very low level of Tl doping.

  7. Results from an investigation of the physical origins of nonproportionality in CsI(Tl)

    International Nuclear Information System (INIS)

    Asztalos, S.; Hennig, W.; Warburton, W.K.

    2011-01-01

    The relative scintillation response per energy deposited by Compton electrons, or nonproportionality, has traditionally been considered an intrinsic scintillator property. However, such an interpretation is inconsistent with recent results that show nonproportionality to depend on external factors such as shaping time, temperature and supplier. Apparently, at least some of the overall nonproportionality has an extrinsic origin. In this work we describe the results from a suite of measurements designed to test the hypothesis that nonproportionality in CsI(Tl) material has an extrinsic component that correlates with impurity levels. Our choice of material was motivated by the excellent energy resolution observed in one bulk crystal (6.4%)-a marked departure from that measured with conventional CsI(Tl) stock (8-8.5%). Six bulk CsI(Tl) crystals were procured and diced into 44 wafers. Using X-ray fluorescence techniques no conclusive evidence for impurities was found in any of the wafers at the 1-50 ppm level. One crystal exhibited a distinct correlation among energy resolution, decay lifetimes, nonproportionality and a very low level of Tl doping.

  8. The 8{pi} miniball charged-particle detector array

    Energy Technology Data Exchange (ETDEWEB)

    Ball, G C; Galindo-Uribarri, A; Andrews, H R; Bray, N C; Lori, J D; Radford, D C; Smith, L V; Tapp, G A; Ward, D [Atomic Energy of Canada Ltd., Chalk River, ON (Canada). Chalk River Nuclear Labs.; Drake, T E [Toronto Univ., ON (Canada). Dept. of Physics; Waddington, J C [McMaster Univ., Hamilton, ON (Canada). Dept. of Physics

    1992-08-01

    A modular miniature array of 24 CsI(Tl) crystals (0.5 cm) thick coupled to large area photodiodes has been constructed to operate inside the 8{pi} spectrometer. The array was designed to have good resolution, high efficiency, and adequate granularity for detecting light charged particles emitted in coincidence with the gamma rays from the decay of high-spin states populated in heavy-ion fusion-evaporation reactions. 17 refs., 2 tabs., 3 figs.

  9. Pulse shaper for scintillation detectors with NaI(Tl) or CsI(Tl) crystals

    International Nuclear Information System (INIS)

    Novisov, B.S.; Maksimenko, A.S.; Baryshev, A.V.; Zhukov, A.V.

    1978-01-01

    The basic circuit of a signal shaper for scintillation detectors with NaI(Tl) and CsI(Tl) crystals is described. To increase amplitude resolution, it is suggested to integrate not the whole charge at the photomultiplier output, but a part of the charge during the initial 100 ns of the current pulse; the remaining part of the current signal is compensated directly at the photomultiplier anode by means of an electric circuit. The principal elements of the spectrometric signal shaper include an input transistor amplifier, a compensation circuit, a key element, a shaper amplifier of time pulses, a shaper of signal duration for controlling the key element, and an output spectrometric amplifier. This device, being used, one can shape pulses at durations of 100 ns and more. The shaper restoration time does not exceed 50 ns. When the shaper operates with NaI(Tl) crystals and at counting rate of 10 6 pulse/s, the amplitude resolution with and without the compensation circuit is 17% and 21% respectively

  10. Investigating the origins of double photopeaks in CsI:Tl samples through activator mapping

    Science.gov (United States)

    Onken, Drew R.; Gridin, Sergii; Williams, Richard T.; Williams, Charles B.; Donati, George L.; Gayshan, Vadim; Vasyukov, Sergey; Gektin, Alex

    2018-06-01

    Careful examination of the origins of double photopeaks in CsI:Tl provides a foundation for exploring the relationship between activator homogeneity and photopeak resolution in scintillators. In rare cases, certain CsI:Tl crystals exhibit a second photopeak in the pulse-height spectrum. A combination of optical mapping and ICP-MS measurements reveals the presence of two distinct regions with differing Tl concentrations in these crystals. The oscillator strength of the 299 nm absorption A-band of Tl in CsI was measured to be 0.0526 ± 0.0008; this parameter can be used to quantify activator concentration from the optical absorption. Using published measurements of luminescence intensity versus Tl concentration, the distributions of Tl measured from optical absorption maps of the samples were reconstructed into photopeaks in good agreement with experiment. The distribution of Tl concentrations in these particular crystals allowed examining luminescence pulse shape as a function of Tl concentration.

  11. A compact, discrete CsI(Tl) scintillator/Si photodiode gamma camera for breast cancer imaging

    Energy Technology Data Exchange (ETDEWEB)

    Gruber, Gregory J. [Univ. of California, Berkeley, CA (United States)

    2000-01-01

    Recent clinical evaluations of scintimammography (radionuclide breast imaging) are promising and suggest that this modality may prove a valuable complement to X-ray mammography and traditional breast cancer detection and diagnosis techniques. Scintimammography, however, typically has difficulty revealing tumors that are less than 1 cm in diameter, are located in the medial part of the breast, or are located in the axillary nodes. These shortcomings may in part be due to the use of large, conventional Anger cameras not optimized for breast imaging. In this thesis I present compact single photon camera technology designed specifically for scintimammography which strives to alleviate some of these limitations by allowing better and closer access to sites of possible breast tumors. Specific applications are outlined. The design is modular, thus a camera of the desired size and geometry can be constructed from an array (or arrays) of individual modules and a parallel hole lead collimator for directional information. Each module consists of: (1) an array of 64 discrete, optically-isolated CsI(Tl) scintillator crystals 3 x 3 x 5 mm3 in size, (2) an array of 64 low-noise Si PIN photodiodes matched 1-to-1 to the scintillator crystals, (3) an application-specific integrated circuit (ASIC) that amplifies the 64 photodiode signals and selects the signal with the largest amplitude, and (4) connectors and hardware for interfacing the module with a motherboard, thereby allowing straightforward computer control of all individual modules within a camera.

  12. A compact, discrete CsI(Tl) scintillator/Si photodiode gamma camera for breast cancer imaging

    International Nuclear Information System (INIS)

    Gruber, Gregory J.

    2000-01-01

    Recent clinical evaluations of scintimammography (radionuclide breast imaging) are promising and suggest that this modality may prove a valuable complement to X-ray mammography and traditional breast cancer detection and diagnosis techniques. Scintimammography, however, typically has difficulty revealing tumors that are less than 1 cm in diameter, are located in the medial part of the breast, or are located in the axillary nodes. These shortcomings may in part be due to the use of large, conventional Anger cameras not optimized for breast imaging. In this thesis I present compact single photon camera technology designed specifically for scintimammography which strives to alleviate some of these limitations by allowing better and closer access to sites of possible breast tumors. Specific applications are outlined. The design is modular, thus a camera of the desired size and geometry can be constructed from an array (or arrays) of individual modules and a parallel hole lead collimator for directional information. Each module consists of: (1) an array of 64 discrete, optically-isolated CsI(Tl) scintillator crystals 3 x 3 x 5 mm 3 in size, (2) an array of 64 low-noise Si PIN photodiodes matched 1-to-1 to the scintillator crystals, (3) an application-specific integrated circuit (ASIC) that amplifies the 64 photodiode signals and selects the signal with the largest amplitude, and (4) connectors and hardware for interfacing the module with a motherboard, thereby allowing straightforward computer control of all individual modules within a camera

  13. Studies of the performance of different front-end systems for flat-panel multi-anode PMTs with CsI(Tl) scintillator arrays

    International Nuclear Information System (INIS)

    Sekiya, H.; Hattori, K.; Kubo, H.; Miuchi, K.; Nagayoshi, T.; Nishimura, H.; Okada, Y.; Orito, R.; Takada, A.; Takeda, A.; Tanimori, T.; Ueno, K.

    2006-01-01

    We have studied the performance of two different types of front-end systems for our gamma camera based on Hamamatsu H8500 (flat-panel 64 channels multi-anode PSPMT) with a CsI(Tl) scintillator array. The array consists of 64 pixels of 6x6x20mm 3 which corresponds to the anode pixels of H8500. One of the system is based on commercial ASIC chips in order to read out every anode. The others are based on resistive charge divider network between anodes to reduce readout channels. In both systems, each pixel (6mm) was clearly resolved by flood field irradiation of 137 Cs. We also investigated the energy resolution of these systems and showed the performance of the cascade connection of resistive network between some PMTs for large area detectors

  14. Near threshold pulse shape discrimination techniques in scintillating CsI(Tl) crystals

    International Nuclear Information System (INIS)

    Wu, S.C.; Yue, Q.; Lai, W.P.; Li, H.B.; Li, J.; Lin, S.T.; Liu, Y.; Singh, V.; Wang, M.Z.; Wong, H.T.; Xin, B.; Zhou, Z.Y.

    2004-01-01

    There are recent interests with CsI(Tl) scintillating crystals for Dark Matter experiments. The key merit is the capability to differentiate nuclear recoil (nr) signatures from the background β/γ-events due to ambient radioactivity on the basis of their different pulse shapes. One of the major experimental challenges is to perform such pulse shape analysis in the statistics-limited domain where the light output is close to the detection threshold. Using data derived from measurements with low-energy γ's and nuclear recoils due to neutron elastic scatterings, it was verified that the pulse shapes between β/γ-events are different. Several methods of pulse shape discrimination (PSD) are studied, and their relative merits are compared. Full digitization of the pulse shapes is crucial to achieve good discrimination. Advanced software techniques with mean time, neural network and likelihood ratios give rise to satisfactory performance, and are superior to the conventional Double Charge method commonly applied at higher energies. PSD becomes effective starting at a light yield of about 20 photo-electrons. This corresponds to a detection threshold of about 5 keV electron-equivalence energy, or 40-50 keV recoil kinetic energy, in realistic experiments

  15. Timing characteristics of Ce doped Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12} single crystals in comparison with CsI(Tl) scintillators

    Energy Technology Data Exchange (ETDEWEB)

    Tyagi, M.; Singh, A.K.; Singh, S.G.; Sen, S.; Gadkari, S.C. [Technical Physics Division, Bhabha Atomic Research Centre, Mumbai, 400085 (India); Desai, V.V.; Nayak, B.K. [Nuclear Physics Division, Bhabha Atomic Research Centre, Mumbai, 400085 (India)

    2015-10-15

    Single crystals of Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12}:Ce with B codopants were successfully grown using the Czochralski technique. The timing characteristics of the crystal was measured by coupling the crystal to photomultiplier tubes (PMT) or silicon photodiodes [Si(PIN)]. The two prompt γ-rays emitted in a cascade from {sup 60}Co or {sup 22}Na source were detected in coincidence using Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12}:Ce,B crystal detectors and a BaF{sub 2} detector. The time resolution of these crystals are observed to be better than that measured for CsI:Tl crystal coupled to PMT or Si(PIN) in an identical measurement setup. (copyright 2015 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

  16. Effects of film thickness on scintillation characteristics of columnar CsI:Tl films exposed to high gamma radiation doses

    Energy Technology Data Exchange (ETDEWEB)

    Shinde, Seema; Singh, S.G.; Sen, S.; Gadkari, S.C., E-mail: gadkari@barc.gov.in

    2016-02-21

    Oriented columnar films of Tl doped CsI (CsI:Tl) of varying thicknesses from 50 µm to 1000 µm have been deposited on silica glass substrates by a thermal evaporation technique. The SEM micrographs confirmed the columnar structure of the film while the powder X-ray diffraction pattern recorded for the films revealed a preferred orientation of the grown columns along the <200> direction. Effects of high energy gamma exposure up to 1000 Gy on luminescence properties of the films were investigated. Results of radio-luminescence, photo-luminescence and scintillation studies on the films are compared with those of a CsI:Tl single crystal with similar thickness. A possible correlation between the film thicknesses and radiation damage in films has been observed. - Highlights: • CsI:Tl films of different thicknesses deposited for γ and α detection. • Pulse-height spectra found to degrade with increasing thickness. • Radiation damage is found more in films than single crystal of comparable thickness. • Detection efficiency increases for γ while it is invariant for α beyond 50 µm.

  17. Effects of film thickness on scintillation characteristics of columnar CsI:Tl films exposed to high gamma radiation doses

    International Nuclear Information System (INIS)

    Shinde, Seema; Singh, S.G.; Sen, S.; Gadkari, S.C.

    2016-01-01

    Oriented columnar films of Tl doped CsI (CsI:Tl) of varying thicknesses from 50 µm to 1000 µm have been deposited on silica glass substrates by a thermal evaporation technique. The SEM micrographs confirmed the columnar structure of the film while the powder X-ray diffraction pattern recorded for the films revealed a preferred orientation of the grown columns along the direction. Effects of high energy gamma exposure up to 1000 Gy on luminescence properties of the films were investigated. Results of radio-luminescence, photo-luminescence and scintillation studies on the films are compared with those of a CsI:Tl single crystal with similar thickness. A possible correlation between the film thicknesses and radiation damage in films has been observed. - Highlights: • CsI:Tl films of different thicknesses deposited for γ and α detection. • Pulse-height spectra found to degrade with increasing thickness. • Radiation damage is found more in films than single crystal of comparable thickness. • Detection efficiency increases for γ while it is invariant for α beyond 50 µm.

  18. Neutron calibration facility with an Am-Be source for pulse shape discrimination measurement of CsI(Tl) crystals

    International Nuclear Information System (INIS)

    Lee, H.S.; Bhang, H.; Choi, J.H.; Choi, S.; Joo, H.W.; Kim, G.B.; Kim, K.W.; Kim, S.C.; Kim, S.K.; Lee, J.H.; Lee, J.K.; Myung, S.S.; Hahn, I.S.; Jeon, E.J.; Kang, W.G.; Kim, Y.D.; Kim, Y.H.; Li, J.; Kim, H.J.; Leonard, D.S.

    2014-01-01

    We constructed a neutron calibration facility based on a 300-mCi Am-Be source in conjunction with a search for weakly interacting massive particle candidates for dark matter. The facility is used to study the response of CsI(Tl) crystals to nuclear recoils induced by neutrons from the Am-Be source and comparing them with the response to electron recoils produced by Compton scattering of 662-keV γ-rays from a 137 Cs source. The measured results on pulse shape discrimination (PSD) between nuclear- and electron-recoil events are quantified in terms of quality factors. A comparison with our previous result from a neutron generator demonstrate the feasibility of performing calibrations of PSD measurements using neutrons from a Am-Be source

  19. Photonic Crystal Nanocavity Arrays

    National Research Council Canada - National Science Library

    Altug, Hatice; Vuckovic, Jelena

    2006-01-01

    We recently proposed two-dimensional coupled photonic crystal nanocavity arrays as a route to achieve a slow-group velocity of light in all crystal directions, thereby enabling numerous applications...

  20. Composite detector for mixed radiations based on CsI(Tl) and dispersions of small ZnSe(Te) crystals

    International Nuclear Information System (INIS)

    Ryzhikov, V.; Gal'chinetskii, L.; Katrunov, K.; Lisetskaya, E.; Gavriluk, V.; Zelenskaya, O.; Starzhynskiy, N.; Chernikov, V.

    2005-01-01

    A new large area detector of high-energy X-ray and β-radiation has been designed and studied. A composite material based on small-crystalline ZnSe(Te) was applied onto the wide surface of a light guide. An experimental specimen has been prepared, which showed β-sensitivity C β =5.5cm 2 . The spectrograms of a 90 Sr+ 90 Y β-source obtained with the specimen under study make it possible to evaluate the age of the source by the ratio of low- and high-energy regions of the spectrum. The combined detector (CD) comprises a single crystalline plate of ZnSe(Te) placed onto the output window of a scintillating transparent light guide made of CsI(Tl) in the shape of a truncated pyramid. The CsI(Tl) light guide is used to create an additional channel for detection of γ-radiation, as well as for protecting the photodiode from the penetrating radiation. It is shown that introduction of the light guide does not worsen the energy resolution characteristics of ZnSe(Te). Separate detection of α- and γ-radiation has been achieved under simultaneous excitation by 239 Pu (ZnSe(Te), R α =6%) and 241 Am (CsI(Tl), R γ =20%). The use of selective optical filters allows separation of the peaks of total absorption (p.t.a.) in the case of their superposition

  1. Effect of crystal shape, size and reflector type on operation characteristics of gamma-radiation detectors based on CsI(Tl) and CsI(Na) scintillators

    International Nuclear Information System (INIS)

    Globus, M.E.; Grinyov, B.V.; Ratner, M.A.

    1996-01-01

    Operation characteristics of CsI(Tl) and CsI(Na) scintillation detectors, to a large degree connected with light collection in crystals, are calculated for various shapes, sizes and reflecting surface types. Allowance is made for the true light reflection indicatrix which is characterized by the effective mirror constituent of the reflected light, p. Its value , averaged over incidence angle, is used for the classification of reflecting surfaces. Operation characteristics (in particular, spectrometric ones) are found to be essentially dependent on . Tables of operation characteristics, given below, permit one to make inferential conclusions on an optimal combination of the shape, sizes an the reflecting surface version

  2. Particle gamma correlations in {sup 12}C measured with the CsI(Tl) based detector array CHIMERA

    Energy Technology Data Exchange (ETDEWEB)

    Cardella, G., E-mail: cardella@ct.infn.it [INFN - Sezione di Catania, Via S. Sofia, 95123 Catania (Italy); Acosta, L. [INFN - Sezione di Catania, Via S. Sofia, 95123 Catania (Italy); Amorini, F. [INFN - Laboratori Nazionali del Sud, Via S. Sofia, Catania (Italy); Auditore, L. [INFN Gruppo collegato di Messina and Dip. di Fisica e Scienze della Terra, Università di Messina (Italy); Berceanu, I. [Institute for Physics and Nuclear Engineering, Bucharest (Romania); Castoldi, A. [INFN Sezione di Milano e Politecnico Milano (Italy); De Filippo, E. [INFN - Sezione di Catania, Via S. Sofia, 95123 Catania (Italy); Dell' Aquila, D. [Dipartimento di scienze Fisiche, Università Federico II and INFN Sezione di Napoli (Italy); Francalanza, L. [INFN - Laboratori Nazionali del Sud, Via S. Sofia, Catania (Italy); Dip. di Fisica e Astronomia, Università di Catania, Via S. Sofia, Catania (Italy); Gnoffo, B. [INFN - Sezione di Catania, Via S. Sofia, 95123 Catania (Italy); Guazzoni, C. [INFN Sezione di Milano e Politecnico Milano (Italy); Lanzalone, G. [INFN - Laboratori Nazionali del Sud, Via S. Sofia, Catania (Italy); Facoltà di Ingegneria e Architettura, Università Kore, Enna (Italy); Lombardo, I. [Dipartimento di scienze Fisiche, Università Federico II and INFN Sezione di Napoli (Italy); Minniti, T.; Morgana, E.; Norella, S. [INFN Gruppo collegato di Messina and Dip. di Fisica e Scienze della Terra, Università di Messina (Italy); Pagano, A. [INFN - Sezione di Catania, Via S. Sofia, 95123 Catania (Italy); Pagano, E.V. [INFN - Laboratori Nazionali del Sud, Via S. Sofia, Catania (Italy); Dip. di Fisica e Astronomia, Università di Catania, Via S. Sofia, Catania (Italy); Papa, M.; Pirrone, S. [INFN - Sezione di Catania, Via S. Sofia, 95123 Catania (Italy); and others

    2015-11-01

    The gamma decay of the first excited 4.44 MeV 2+level of {sup 12}C, populated by inelastic scattering of proton and {sup 16}O beams at various energies was studied in order to test γ-ray detection efficiency and the quality of angular distribution information given by the CsI(Tl) detectors of the 4π CHIMERA array. The γ-decay was measured in coincidence with ejectile scattered particles in an approximately 4π geometry allowing to extract the angular distribution in the reference frame of recoiling {sup 12}C target. The typical sin{sup 2} (2θ) behavior of angular distribution was observed in the case of {sup 16}O beam. Besides that, for the proton beam, in order to explain the observed distribution, the addition of an incoherent flat contribution was required. This latter is the effect of proton spin flip events allowing the population of M=±1 magnetic substates, that is not possible in reactions induced by {sup 16}O beam. A comparison with previously collected data, obtained measuring only in and out of plane proton-γ-ray coincidences, confirms the good quality of the angular distribution information given by the apparatus. Possible applications with radioactive beams are outlined.

  3. Alpha-gamma pulse shape discrimination in CsI:Tl, CsI:Na and BaF sub 2 scintillators

    CERN Document Server

    Dinca, L E; Haas, J; Bom, V R; Eijk, C W E

    2002-01-01

    Some scintillating materials offer the possibility of measuring well separated alpha and gamma scintillation response using a single crystal. Eventually aiming at thermal neutron detection using sup 6 Li or sup 1 sup 0 B admixture, pulse shape discrimination measurements were made on three scintillators: CsI:Tl, CsI:Na and pure BaF sub 2 crystals. A very good alpha/gamma discrimination was obtained using sup 2 sup 2 Na, sup 2 sup 4 sup 1 Am (gamma) and sup 2 sup 4 sup 4 Cm (alpha) radioactive sources.

  4. A cadmium-zinc-telluride crystal array spectrometer

    International Nuclear Information System (INIS)

    McHugh, H. R.; Quam, W.; DeVore, T.; Vogle, R.; Weslowski, J.

    2003-01-01

    This paper describes a gamma detector employing an array of eight cadmium-zinc-telluride (CZT) crystals configured as a high resolution gamma ray spectrometer. This detector is part of a more complex instrument that identifies the isotope,displays this information, and records the gamma spectrum. Various alarms and other operator features are incorporated in this battery operated rugged instrument. The CZT detector is the key component of this instrument and will be described in detail in this paper. We have made extensive spectral measurements of the usual laboratory gamma sources, common medical isotopes, and various Special Nuclear Materials (SNM) with this detector. Some of these data will be presented as spectra. We will also present energy resolution and detection efficiency for the basic 8-crystal array. Additional data will also be presented for a 32-crystal array. The basic 8-crystal array development was completed two years ago, and the system electronic design has been imp roved recently. This has resulted in significantly improved noise performance. We expect to have a much smaller detector package, using 8 crystals, in a few months. This package will use flip-chip packaging to reduce the electronics physical size by a factor of 5

  5. Scintillation response of CsI: Tl crystal under neutron, gamma, alpha particles and beta excitations

    Energy Technology Data Exchange (ETDEWEB)

    Pereira, Maria da Conceicao Costa; Madi Filho, Tufic; Lopes, Valdir Maciel; Berretta, Jose Roberto; Cardenas, Jose Patricio Nahuel, E-mail: macoper@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2015-07-01

    Among the converters of X and gamma radiation in light photons, known as scintillators, the one which is the most efficient emits photons with a wavelength near 400 nm. Particularly, among them, the cesium iodine doped with thallium (CsI:Tl) crystal is that which matches better between the light emission spectrum (peak at 540 nm) and the quantum sensitivity curve of the photodiodes and CCD (Charge Coupled Device). This explains the renewed interest in using this crystal as scintillator. Although the CsI:Tl crystal is commercially available, its local development would give the possibility to obtain it in different geometric configurations and coupling. Moreover, there is a special interest in studying new conditions that will alter the properties of this crystal in order to achieve a optimal level of its functional characteristics. Having an efficient national scintillator with low cost is a strategic opportunity to study the response of a detector applied to different types of radiation. The crystal of cesium iodide activated with thallium (CsI:Tl) has a high gamma detection efficiency per unit volume. In this paper, the CsI:Tl crystal, grown by the vertical Bridgman technique in evacuated silica ampoules and with the purpose of use as radiation detectors, is described. To evaluate the scintillator, measures of the thallium distribution in the crystal volume were taken, with overall efficiency score. The scintillator response was studied through gamma radiation from sources of {sup 137}Cs, {sup 60}Co, {sup 22}Na, {sup 54}Mn, {sup 131}I and {sup 99m}Tc; the beta radiation from source of {sup 90}Sr/{sup 90}Y, alpha particles from {sup 241}Am source and the scintillator response to neutrons from Am/Be source. The energetic resolution for {sup 137}Cs gamma rays (662 keV) was 10%. The results showed the validity of using the CsI:Tl crystal developed in our laboratory, in many applications in the area of radiation detectors. (author)

  6. Development of a PET detector module incorporating a silicon photodiode array

    International Nuclear Information System (INIS)

    Rosenfeld, A.B.; Takacs, G.J.; Lerch, M.L.F.; Simmonds, P.E.

    2000-01-01

    Full text: We are developing a new Positron Emission Tomography (PET) detection sub-module with depth of interaction capability. The new sub-module is simple and robust to minimise module assembly complications and is completely independent of photomultiplier tubes. The new sub-module has also been designed to maximise its flexibility for easy sub-module coupling so as to form a complete, customised, detection module to be used in PET scanners dedicated to human brain and breast, and small animal studies. Blue enhanced, silicon 8x8 detector arrays are used to read out the scintillation crystals, and form the basis of the new module. The new detectors were designed by the Centre for Medical Radiation Physics (CMRP) at the University of Wollongong in collaboration with the High Energy Physics Department, University of Melbourne and produced by SPO D etector , Ukraine. Complementing the work on the silicon photodetectors, we have also carried out simulations of the propagation of the scintillation light in the crystals, and the effect of crystal dimensions and surface treatment on the distribution of light detected by the photodiode array. The distribution of light over the photodiodes has then been used to test various algorithms for calculating the point of interaction of the gamma ray in the crystal. Simulations of the light propagation show that for a crystal of dimensions 25mm x 25mm x 3mm, it is possible to determine the point of interaction in 2 dimensions with an average accuracy of just over 0.5mm. The resulting photon distribution detected by the array. The surface treatment, while having a large effect on the light output, does not have a great effect on the accuracy. If these dimensions change to 25mm x 25mm x 6mm then the surface conditions have a greater effect on the accuracy. It is possible however, with careful surface treatment, to achieve an accuracy of around 0.6mm, only marginally worse than the case for the 3mm thick crystal. Gamma ray

  7. Theoretical analysis and experimental evaluation of a CsI(Tl) based electronic portal imaging system

    International Nuclear Information System (INIS)

    Sawant, Amit; Zeman, Herbert; Samant, Sanjiv; Lovhoiden, Gunnar; Weinberg, Brent; DiBianca, Frank

    2002-01-01

    This article discusses the design and analysis of a portal imaging system based on a thick transparent scintillator. A theoretical analysis using Monte Carlo simulation was performed to calculate the x-ray quantum detection efficiency (QDE), signal to noise ratio (SNR) and the zero frequency detective quantum efficiency [DQE(0)] of the system. A prototype electronic portal imaging device (EPID) was built, using a 12.7 mm thick, 20.32 cm diameter, CsI(Tl) scintillator, coupled to a liquid nitrogen cooled CCD TV camera. The system geometry of the prototype EPID was optimized to achieve high spatial resolution. The experimental evaluation of the prototype EPID involved the determination of contrast resolution, depth of focus, light scatter and mirror glare. Images of humanoid and contrast detail phantoms were acquired using the prototype EPID and were compared with those obtained using conventional and high contrast portal film and a commercial EPID. A theoretical analysis was also carried out for a proposed full field of view system using a large area, thinned CCD camera and a 12.7 mm thick CsI(Tl) crystal. Results indicate that this proposed design could achieve DQE(0) levels up to 11%, due to its order of magnitude higher QDE compared to phosphor screen-metal plate based EPID designs, as well as significantly higher light collection compared to conventional TV camera based systems

  8. Coupled Photonic Crystal Cavity Array Laser

    DEFF Research Database (Denmark)

    Schubert, Martin

    in the quadratic lattice. Processing techniques are developed and optimized in order fabricate photonic crystals membranes in gallium arsenide with quantum dots as gain medium and in indium gallium arsenide phosphide with quantum wells as gain medium. Several key issues in process to ensure good quality....... The results are in good agreement with standard coupled mode theory. Also a novel type of photonic crystal structure is proposed called lambda shifted cavity which is a twodimensional photonic crystal laser analog of a VCSEL laser. Detailed measurements of the coupled modes in the photonic crystals...... with quantum dots are carried out. In agreement with a simple gain model the structures do not show stimulated emission. The spectral splitting due to the coupling between single cavities as well as arrays of cavities is studied theoretically and experimentally. Lasing is observed for photonic crystal cavity...

  9. A new hybrid photomultiplier tube as detector for scintillating crystals

    International Nuclear Information System (INIS)

    De Notaristefani, F.; Vittori, F.; Puertolas, D.

    2002-01-01

    In this work, we have attentively studied the performance of a new hybrid photomultiplier tube (HPMT) as detector for photons from scintillating crystals. The HPMT is equipped with a YAP window in order to improve light collection and increase measured light response from scintillating crystals. Several measurements have been performed on BGO, LSO, CsI(Tl) and NaI(Tl) planar crystals having three different surface treatments as well as on YAP : Ce and CsI(Tl) matrices. Such crystals have been coupled to two HPMTs, one equipped with a YAP window (Y-HPMT) and the other with a conventional quartz window (Q-HPMT). Measurements on crystals coupled to the Y-HPMT have shown a consistent improvement of the light response, thanks to the presence of the YAP window. Indeed, the light response measured with the Y-HPMT was on average equal to 1.5, 2.1 and 2.6 times that obtained with the Q-HPMT for planar crystals with white painted (diffusive), fine ground and polished rear surfaces, respectively. With regards to crystal matrices, we measured a light response increase of about 1.2 times

  10. Radiation damage of CsI(Tl) scintillators: blocking of energy transfer process of V sub k centers to Tl sup + activators

    CERN Document Server

    Hamada, M M; Shimizu, S; Kubota, S

    2002-01-01

    This paper reports the emission spectra, light output, transmission and decay curves of CsI(Tl) crystals irradiated with gamma rays at different doses, ranging from 1x10 sup 5 to 5x10 sup 5 Gy. The crystals were coated with black or white tapes. Significant decreases in the emission spectra and light output values were observed for the crystals coated with white tape as the radiation dose increased. The decrease in the degree of the rising part of the decay curve in the irradiated crystals is attributed to the blocking of the energy transfer processes of V sub k lattice disorders, which were produced in irradiated crystals. The scintillation mechanism is affected in the crystal irradiated at 5x10 sup 5 Gy. However for crystals irradiated below 10 sup 5 Gy the mechanism process is not altered, and the decrease in the light output is due to internal transmission loss. It was also observed that the damage for irradiation is not permanent and it obeys a bi-exponential function.

  11. Experimental evidence of infrared scintillation in crystals

    CERN Document Server

    Belogurov, S; Carugno, Giovanni; Conti, E; Iannuzzi, D; Meneguzzo, Anna Teresa

    2000-01-01

    We present experimental results on infrared emission induced by protons in some solid-state samples. Infrared scintillation occurs in many crystals, with different yield values and time-response behaviours. A rough measurement of the emission wavelength of CsI(Tl) is also reported.

  12. Low-cost scalable quartz crystal microbalance array for environmental sensing

    Energy Technology Data Exchange (ETDEWEB)

    Anazagasty, Cristain [University of Puerto Rico; Hianik, Tibor [Comenius University, Bratislava, Slovakia; Ivanov, Ilia N [ORNL

    2016-01-01

    Proliferation of environmental sensors for internet of things (IoT) applications has increased the need for low-cost platforms capable of accommodating multiple sensors. Quartz crystal microbalance (QCM) crystals coated with nanometer-thin sensor films are suitable for use in high-resolution (~1 ng) selective gas sensor applications. We demonstrate a scalable array for measuring frequency response of six QCM sensors controlled by low-cost Arduino microcontrollers and a USB multiplexer. Gas pulses and data acquisition were controlled by a LabVIEW user interface. We test the sensor array by measuring the frequency shift of crystals coated with different compositions of polymer composites based on poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) while films are exposed to water vapor and oxygen inside a controlled environmental chamber. Our sensor array exhibits comparable performance to that of a commercial QCM system, while enabling high-throughput 6 QCM testing for under $1,000. We use deep neural network structures to process sensor response and demonstrate that the QCM array is suitable for gas sensing, environmental monitoring, and electronic-nose applications.

  13. Energy calibration of CsI(Tl) scintillator in pulse-shape identification technique

    CERN Document Server

    Avdeichikov, V; Golubev, P; Jakobsson, B; Colonna, N

    2003-01-01

    A batch of 16 CsI(Tl) scintillator crystals, supplied by the Bicron Company, has been studied with respect to precise energy calibration in pulse-shape identification technique. The light corresponding to pulse integration within the time interval 1.6-4.5 mu s (long gate) and 0.0-4.5 mu s (extra-long gate) exhibits a power law relation, L(E,Z,A)=a1(Z,A)E sup a sup 2 sup ( sup Z sup , sup A sup ) , for sup 1 sup , sup 2 sup , sup 3 H isotopes in the measured energy range 5-150 MeV. For the time interval 0.0-0.60 mu s (short gate), a significant deviation from the power law relation is observed, for energy greater than approx 30 MeV. The character of the a2(p)-a2(d) and a2(p)-a2(t) correlations for protons, deuterons and tritons, reveals 3 types of crystals in the batch. These subbatches differ in the value of the extracted parameter a2 for protons, and in the value of the spread of a2 for deuterons and tritons. This may be explained by the difference in the energy dependence of the fast decay time component an...

  14. Method and apparatus for enhancing vortex pinning by conformal crystal arrays

    Science.gov (United States)

    Janko, Boldizsar; Reichhardt, Cynthia; Reichhardt, Charles; Ray, Dipanjan

    2015-07-14

    Disclosed is a method and apparatus for strongly enhancing vortex pinning by conformal crystal arrays. The conformal crystal array is constructed by a conformal transformation of a hexagonal lattice, producing a non-uniform structure with a gradient where the local six-fold coordination of the pinning sites is preserved, and with an arching effect. The conformal pinning arrays produce significantly enhanced vortex pinning over a much wider range of field than that found for other vortex pinning geometries with an equivalent number of vortex pinning sites, such as random, square, and triangular.

  15. The design and performance of a large-volume spherical CsI(Tl) scintillation counter for gamma-ray spectroscopy

    CERN Document Server

    Meng, L J; Chirkin, V M; Potapov, V N; Ivanov, O P; Ignatov, S M

    2002-01-01

    This paper presents details of the design and performance of a prototype large-volume scintillation detector used for gamma-ray spectroscopy. In this detector, a spherical CsI(Tl) scintillation crystal having a diameter of 5.7 cm was polished and packed in dry MgO powder. The scintillation light from the crystal was viewed using a single 1x1 cm sup 2 silicon PIN diode. A low-noise preamplifier was also integrated within the detector housing. The measured noise level was equivalent to approx 800 electrons (FWHM). Such a configuration provided a very good light collection efficiency, which resulted in an average of 20 electrons being generated per keV of energy deposited in the crystal. One of the key features of the detector design is that it minimises spatial variations in the light collection efficiency throughout the detector. Compared with a standard 3 in. NaI scintillation counter, this feature leads to a much-improved energy resolution, particularly for photon energies above 1 MeV. The results presented ...

  16. Two-dimensional diced scintillator array for innovative, fine-resolution gamma camera

    International Nuclear Information System (INIS)

    Fujita, T.; Kataoka, J.; Nishiyama, T.; Ohsuka, S.; Nakamura, S.; Yamamoto, S.

    2014-01-01

    We are developing a technique to fabricate fine spatial resolution (FWHM<0.5mm) and cost-effective photon counting detectors, by using silicon photomultipliers (SiPMs) coupled with a finely pixelated scintillator plate. Unlike traditional X-ray imagers that use a micro-columnar CsI(Tl) plate, we can pixelate various scintillation crystal plates more than 1 mm thick, and easily develop large-area, fine-pitch scintillator arrays with high precision. Coupling a fine pitch scintillator array with a SiPM array results in a compact, fast-response detector that is ideal for X-ray, gamma-ray, and charged particle detection as used in autoradiography, gamma cameras, and photon counting CTs. As the first step, we fabricated a 2-D, cerium-doped Gd 3 Al 2 Ga 3 O 12 (Ce:GAGG) scintillator array of 0.25 mm pitch, by using a dicing saw to cut micro-grooves 50μm wide into a 1.0 mm thick Ce:GAGG plate. The scintillator plate is optically coupled with a 3.0×3.0mm pixel 4×4 SiPM array and read-out via the resistive charge-division network. Even when using this simple system as a gamma camera, we obtained excellent spatial resolution of 0.48 mm (FWHM) for 122 keV gamma-rays. We will present our plans to further improve the signal-to-noise ratio in the image, and also discuss a variety of possible applications in the near future

  17. A BaF2 crystal array for high energy -ray measurements

    Indian Academy of Sciences (India)

    A very well-known such array is called two-arm-photon- spectrometer (TAPS) [1]. It consists of large (25 cm long) hexagonal BaF¾ crystals ar- ranged in packs of 64 crystals. ... light which may not reach the photomultiplier tube. A sketch of the ...

  18. Particle identification method in the CsI(Tl) scintillator used for the CHIMERA 4 pi detector

    CERN Document Server

    Alderighi, M; Basssini, R; Berceanu, I; Blicharska, J; Boiano, C; Borderie, B; Bougault, R; Bruno, M; Cali, C; Cardella, G; Cavallaro, S; D'Agostino, M; D'andrea, M; Dayras, R; De Filippo, E; Fichera, F; Geraci, E; Giustolisi, F; Grzeszczuk, A; Guardone, N; Guazzoni, P; Guinet, D; Iacono-Manno, M; Kowalski, S; La Guidara, E; Lanchais, A L; Lanzalone, G; Lanzanò, G; Le Neindre, N; Li, S; Maiolino, C; Majka, Z; Manfredi, G; Nicotra, D; Paduszynski, T; Pagano, A; Papa, M; Petrovici, C M; Piasecki, E; Pirrone, S; Politi, G; Pop, A; Porto, F; Rivet, M F; Rosato, E; Sacca, G; Sechi, G; Simion, V; Sperduto, M L; Steckmeyer, J C; Trifiró, A; Trimarchi, M; Urso, S; Vannini, G; Vigilante, M; Wilczynski, J; Wu, H; Xiao, Z; Zetta, L; Zipper, W

    2002-01-01

    The charged particle identification obtained by the analysis of signals coming from the CsI(Tl) detectors of the CHIMERA 4 pi heavy-ion detector is presented. A simple double-gate integration method, with the use of the cyclotron radiofrequency as reference time, results in low thresholds for isotopic particle identification. The dependence of the identification quality on the gate generation timing is discussed. Isotopic identification of light ions up to Beryllium is clearly seen. For the first time also the identification of Z=5 particles is observed. The identification of neutrons interacting with CsI(Tl) by (n,alpha) and (n,gamma) reactions is also discussed.

  19. Liquid crystal-based hydrophone arrays

    Science.gov (United States)

    Brodzeli, Zourab; Silvestri, Leonardo; Michie, Andrew; Chigrinov, Vladimir G.; Guo, Qi; Pozhidaev, Eugene P.; Kiselev, Alexei D.; Ladouceur, Francois

    2012-09-01

    We describe a fiber optic hydrophone array system that could be used for underwater acoustic surveillance applications (e.g. military, counter terrorist, and customs authorities in protecting ports and harbors), offshore production facilities or coastal approaches as well as various marine applications. In this paper, we propose a new approach to underwater sonar systems using the voltage-controlled liquid crystals and simple multiplexing method. The proposed method permits measurement of sound under water at multiple points along an optical fiber using the low cost components and standard single mode fiber, without complex interferometric measurement techniques, electronics or demodulation software.

  20. A theoretical study of CsI:Tl columnar scintillator image quality parameters by analytical modeling

    Energy Technology Data Exchange (ETDEWEB)

    Kalyvas, N., E-mail: nkalyvas@teiath.gr; Valais, I.; Michail, C.; Fountos, G.; Kandarakis, I.; Cavouras, D.

    2015-04-11

    Medical X-ray digital imaging systems such as mammography, radiography and computed tomography (CT), are composed from efficient radiation detectors, which can transform the X-rays to electron signal. Scintillators are materials that emit light when excited by X-rays and incorporated in X-ray medical imaging detectors. Columnar scintillator, like CsI:T1 is very often used for X-ray detection due to its higher performance. The columnar form limits the lateral spread of the optical photons to the scintillator output, thus it demonstrates superior spatial resolution compared to granular scintillators. The aim of this work is to provide an analytical model for calculating the MTF, the DQE and the emission efficiency of a columnar scintillator. The model parameters were validated against published Monte Carlo data. The model was able to predict the overall performance of CsI:Tl scintillators and suggested an optimum thickness of 300 μm for radiography applications. - Highlights: • An analytical model for calculating MTF, DQE and Detector Optical Gain (DOG) of columnar phosphors was developed. • The model was fitted to published efficiency and MTF Monte Carlo data. • A good fit was observed for 300 µm columnar CsI:Tl thickness. • The performance of the 300 µm column thickness CsI:Tl was better in terms of MTF and DOG for radiographic applications.

  1. Validation of the GATE Monte Carlo simulation platform for modelling a CsI(Tl) scintillation camera dedicated to small-animal imaging

    International Nuclear Information System (INIS)

    Lazaro, D; Buvat, I; Loudos, G; Strul, D; Santin, G; Giokaris, N; Donnarieix, D; Maigne, L; Spanoudaki, V; Styliaris, S; Staelens, S; Breton, V

    2004-01-01

    Monte Carlo simulations are increasingly used in scintigraphic imaging to model imaging systems and to develop and assess tomographic reconstruction algorithms and correction methods for improved image quantitation. GATE (GEANT4 application for tomographic emission) is a new Monte Carlo simulation platform based on GEANT4 dedicated to nuclear imaging applications. This paper describes the GATE simulation of a prototype of scintillation camera dedicated to small-animal imaging and consisting of a CsI(Tl) crystal array coupled to a position-sensitive photomultiplier tube. The relevance of GATE to model the camera prototype was assessed by comparing simulated 99m Tc point spread functions, energy spectra, sensitivities, scatter fractions and image of a capillary phantom with the corresponding experimental measurements. Results showed an excellent agreement between simulated and experimental data: experimental spatial resolutions were predicted with an error less than 100 μm. The difference between experimental and simulated system sensitivities for different source-to-collimator distances was within 2%. Simulated and experimental scatter fractions in a [98-82 keV] energy window differed by less than 2% for sources located in water. Simulated and experimental energy spectra agreed very well between 40 and 180 keV. These results demonstrate the ability and flexibility of GATE for simulating original detector designs. The main weakness of GATE concerns the long computation time it requires: this issue is currently under investigation by the GEANT4 and the GATE collaborations

  2. A new avalanche photo diode based readout for the crystal barrel calorimeter

    Energy Technology Data Exchange (ETDEWEB)

    Urban, Martin [Helmholtz-Institut fuer Strahlen- und Kernphysik, Nussallee 14-16, 53115 Bonn (Germany); Collaboration: CBELSA/TAPS-Collaboration

    2015-07-01

    The CBELSA/TAPS experiment at ELSA has proven successful in the measurement of double polarization observables in meson photoproduction off protons and neutrons. To be able to measure purely neutral reactions on a polarized neutron target with high efficiency, the main calorimeter consisting of 1320 CsI(Tl) crystals has to be integrated into the first level trigger. Key requirement to achieve this goal is an exchange of the existing PIN photo diode by a new avalanche photo diode (APD) readout. The main advantage of the new readout system is that it will provide timing information which allows a fast trigger signal. The energy resolution will remain compatible to the previous system. Besides the development of automated test routines for the front end electronics, the characterization of all APDs was successfully accomplished in Bonn. After tests with a 3 x 3 CsI(Tl) crystal matrix at the tagged photon beam facilities at ELSA and MAMI the first half of the Crystal Barrel was upgraded in 2014. This talk shows the result of the latest test measurements including the gain stabilization of the new APD readout electronics and presents the progress of the ongoing upgrade.

  3. Epitaxial Ge-crystal arrays for X-ray detection

    International Nuclear Information System (INIS)

    Kreiliger, T; Falub, C V; Müller, E; Känel, H von; Isa, F; Isella, G; Chrastina, D; Bergamaschini, R; Marzegalli, A; Miglio, L; Kaufmann, R; Niedermann, P; Neels, A; Dommann, A; Meduňa, M

    2014-01-01

    Monolithic integration of an X-ray absorber layer on a Si CMOS chip might be a potentially attractive way to improve detector performance at acceptable costs. In practice this requires, however, the epitaxial growth of highly mismatched layers on a Si-substrate, both in terms of lattice parameters and thermal expansion coefficients. The generation of extended crystal defects, wafer bowing and layer cracking have so far made it impossible to put the simple concept into practice. Here we present a way in which the difficulties of fabricating very thick, defect-free epitaxial layers may be overcome. It consists of an array of densely packed, three-dimensional Ge-crystals on a patterned Si(001) substrate. The finite gap between neighboring micron-sized crystals prevents layer cracking and substrate bowing, while extended defects are driven to the crystal sidewalls. We show that the Ge-crystals are indeed defect-free, despite the lattice misfit of 4.2%. The electrical characteristics of individual Ge/Si heterojunction diodes are obtained from in-situ measurements inside a scanning electron microscope. The fabrication of monolithically integrated detectors is shown to be compatible with Si-CMOS processing

  4. YAP:Ce and CsI(Tl) detectors for dielectronic recombination experiment at the CSRm

    International Nuclear Information System (INIS)

    Wen, W.Q.; Ma, X.; Xu, W.Q.; Meng, L.J.; Zhu, X.L.; Gao, Y.; Wang, S.L.; Zhang, P.J.; Zhao, D.M.; Liu, H.P.; Zhu, L.F.; Yang, X.D.; Li, J.; Ma, X.M.; Yan, T.L.; Yang, J.C.; Yuan, Y.J.; Xia, J.W.; Xu, H.S.; Xiao, G.Q.

    2013-01-01

    Highlights: • YAP:Ce and CsI(Tl) scintillation detectors are developed to detect heavy ions at the storage ring. • A high count rate of ∼10 7 s −1 is obtained with the YAP:Ce detector for heavy ion detection. • YAP:Ce detector shows good performance for DR experiment with 3.7 MeV/u 112 Sn 35+ . -- Abstract: The storage ring CSRm in Lanzhou provides good possibilities for electron-ion collision studies with cooled ion beams. To carry on the recombination experiment at the CSRm, a scintillation detector CsI(Tl) to detect the recombined ions was developed and tested. In addition, a YAP:Ce detector has been developed and installed at CSRm and capability of handling a high count rate of ∼10 7 s −1 has been obtained which is sufficient for the future dielectronic recombination experiment at the CSRm. The comparison of the characteristics of these two detectors is presented

  5. Sub-threshold wavelength splitting in coupled photonic crystal cavity arrays

    DEFF Research Database (Denmark)

    Schubert, Martin; Frandsen, Lars Hagedorn; Skovgård, Troels Suhr

    Coupled photonic crystal (PhC) cavity arrays have recently been found to increase the output power of nanocavity lasers by coherent coupling of a large number of cavities [1]. We have measured the sub-threshold behaviour of such structures in order to gain better understanding of the mode structure....... PhC structures defined by circular holes placed in a quadratic lattice with pitch a=280 nm were fabricated in a GaAs membrane and cavity arrays were realized by introducing single missing holes with intracavity hole distances of two, three, five and seven holes. Arrays with different number...... of coupled cavities were fabricated and characterized using photoluminescence measurements of quantum dots embedded in the GaAs PhC membrane. Since the collection spot size was ~2.5 μm and therefore small compared to the arrays, spectra were taken at several positions of each array....

  6. Scalable gamma-ray camera for wide-area search based on silicon photomultipliers array

    Science.gov (United States)

    Jeong, Manhee; Van, Benjamin; Wells, Byron T.; D'Aries, Lawrence J.; Hammig, Mark D.

    2018-03-01

    Portable coded-aperture imaging systems based on scintillators and semiconductors have found use in a variety of radiological applications. For stand-off detection of weakly emitting materials, large volume detectors can facilitate the rapid localization of emitting materials. We describe a scalable coded-aperture imaging system based on 5.02 × 5.02 cm2 CsI(Tl) scintillator modules, each partitioned into 4 × 4 × 20 mm3 pixels that are optically coupled to 12 × 12 pixel silicon photo-multiplier (SiPM) arrays. The 144 pixels per module are read-out with a resistor-based charge-division circuit that reduces the readout outputs from 144 to four signals per module, from which the interaction position and total deposited energy can be extracted. All 144 CsI(Tl) pixels are readily distinguishable with an average energy resolution, at 662 keV, of 13.7% FWHM, a peak-to-valley ratio of 8.2, and a peak-to-Compton ratio of 2.9. The detector module is composed of a SiPM array coupled with a 2 cm thick scintillator and modified uniformly redundant array mask. For the image reconstruction, cross correlation and maximum likelihood expectation maximization methods are used. The system shows a field of view of 45° and an angular resolution of 4.7° FWHM.

  7. 2D director calculation for liquid crystal optical phased array

    International Nuclear Information System (INIS)

    Xu, L; Zhang, J; Wu, L Y

    2005-01-01

    A practical numerical model for a liquid crystal cell is set up based on the geometrical structure of liquid crystal optical phased arrays. Model parameters include width and space of electrodes, thickness of liquid crystal layer, alignment layers and glass substrates, pre-tilted angles, dielectric constants, elastic constants and so on. According to electrostatic field theory and Frank-Oseen elastic continuum theory, 2D electric potential distribution and 2D director distribution are calculated by means of the finite difference method on non-uniform grids. The influence of cell sizes on director distribution is analyzed. The fringe field effect between electrodes is also discussed

  8. Gamma-ray detection with an UV-enhanced photodiode and scintillation crystals emitting at short wavelengths

    International Nuclear Information System (INIS)

    Johansen, G.A.

    1997-01-01

    A low-noise ion implanted photodiode with high spectral response in the deep blue/UV region has been tested as read-out device for scintillation crystals with matching emission spectra (YAP(Ce), GSO(Ce), BGO and CsI(Tl)). This gamma-ray detector concept is attractive in many industrial applications where compactness, reliability and ambient temperature operation are important. The results show that the amount of detected scintillation light energy falls rapidly off as the wavelength of the scintillation light decreases. It is concluded that the dynamic spectral response of the photodiode, due to increasing carrier collection times, is considerably less than the DC response at short wavelengths. The diode is not useful in pulse mode operation with scintillation crystals emitting at wavelengths below about 400 nm. For read-out of CsI(Tl) with 661.6 keV gamma-radiation, however, the photodiode concept shows better energy resolution (7.1%) than other detectors. (orig.)

  9. Fabrication and Characterization of Vertically Aligned ZnO Nanorod Arrays via Inverted Monolayer Colloidal Crystals Mask

    Science.gov (United States)

    Chen, Cheng; Ding, Taotao; Qi, Zhiqiang; Zhang, Wei; Zhang, Jun; Xu, Juan; Chen, Jingwen; Dai, Jiangnan; Chen, Changqing

    2018-04-01

    The periodically ordered ZnO nanorod (NR) arrays have been successfully synthesized via a hydrothermal approach on the silicon substrates by templating of the TiO2 ring deriving from the polystyrene (PS) nanosphere monolayer colloidal crystals (MCC). With the inverted MCC mask, sol-gel-derived ZnO seeds could serve as the periodic nucleation positions for the site-specific growth of ZnO NRs. The large-scale patterned arrays of single ZnO NR with good side-orientation can be readily produced. According to the experimental results, the as-integrated ZnO NR arrays showed an excellent crystal quality and optical property, very suitable for optoelectronic applications such as stimulated emitters and ZnO photonic crystal devices.

  10. Systematics in the light response of BGO, CsI(Tl) and GSO(Ce) scintillators to charged particles

    CERN Document Server

    Avdeichikov, V; Nikitin, V A; Nomokonov, V P; Wegner, A

    2002-01-01

    The light response of a BGO crystal has been measured for particles Z=1-8, A=1-16 in the energy range approx 2-60 A MeV. The reaction products are identified by a DELTA E(Si)-E(Sci/PD) telescope. The position of the jump in the value of the signal from the PD at the punch-through points is used to calibrate both the DELTA E(Si) and E(Sci/PD) scales in MeV. The dependence of the light output on the energy E, ion atomic number Z and mass A is parameterized by the power law relation, L(Z,A,E)=a sub 1 (Z,A)E sup a sup sub 2 sup ( sup Z sup , sup A sup ). The parameters a sub 1 and a sub 2 have a smooth dependence on Z for all three crystals. The mass dependence of a sub 1 ,a sub 2 is deduced as a simple analytical expression. The systematics of these parameters is presented for BGO, CsI(Tl) and GSO(Ce) scintillators as a function of Z,A. Calculations of the response function, based on the Murray-Mayer model provide an excellent description of the shape of L(Z,A,E) versus E dependence, but show some deviations in ...

  11. Automated preparation method for colloidal crystal arrays of monodisperse and binary colloid mixtures by contact printing with a pintool plotter.

    Science.gov (United States)

    Burkert, Klaus; Neumann, Thomas; Wang, Jianjun; Jonas, Ulrich; Knoll, Wolfgang; Ottleben, Holger

    2007-03-13

    Photonic crystals and photonic band gap materials with periodic variation of the dielectric constant in the submicrometer range exhibit unique optical properties such as opalescence, optical stop bands, and photonic band gaps. As such, they represent attractive materials for the active elements in sensor arrays. Colloidal crystals, which are 3D gratings leading to Bragg diffraction, are one potential precursor of such optical materials. They have gained particular interest in many technological areas as a result of their specific properties and ease of fabrication. Although basic techniques for the preparation of regular patterns of colloidal crystals on structured substrates by self-assembly of mesoscopic particles are known, the efficient fabrication of colloidal crystal arrays by simple contact printing has not yet been reported. In this article, we present a spotting technique used to produce a microarray comprising up to 9600 single addressable sensor fields of colloidal crystal structures with dimensions down to 100 mum on a microfabricated substrate in different formats. Both monodisperse colloidal crystals and binary colloidal crystal systems were prepared by contact printing of polystyrene particles in aqueous suspension. The array morphology was characterized by optical light microscopy and scanning electron microscopy, which revealed regularly ordered crystalline structures for both systems. In the case of binary crystals, the influence of the concentration ratio of the large and small particles in the printing suspension on the obtained crystal structure was investigated. The optical properties of the colloidal crystal arrays were characterized by reflection spectroscopy. To examine the stop bands of the colloidal crystal arrays in a high-throughput fashion, an optical setup based on a CCD camera was realized that allowed the simultaneous readout of all of the reflection spectra of several thousand sensor fields per array in parallel. In agreement with

  12. Using the combination CsI(Tl) + photodiode for identification and energy measurement of light particles

    International Nuclear Information System (INIS)

    Guinet, D.; Chambon, B.; Cheynis, B.; Demeyer, A.; Drain, D.; Hu, X.C.; Pastor, C.; Vagneron, L.; Zaid, K.; Giorni, A.; Heuer, D.; Lleres, A.; Viano, J.B.

    1989-01-01

    The feasibility of discriminating light charged particles in charge and mass using the CsI(Tl) + photodiode combination is demonstrated. Experiment layout and results for a test using a beam of 30 MeV/nucleon α particles impinging on self-supporting gold and aluminium targets are shown

  13. A new DOI detector design using discrete crystal array with depth-dependent reflector patterns and single-ended readout

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Seung-Jae; Lee, Chaeyeong [Department of Radiological Science, Yonsei University, Wonju 26493 (Korea, Republic of); Kang, Jihoon, E-mail: ray.jihoon.kang@gmail.com [Department of Biomedical Engineering, Chonnam National University, 50 Daehak-ro, Yeosu, Jeonnam 59626 (Korea, Republic of); Chung, Yong Hyun, E-mail: ychung@yonsei.ac.kr [Department of Radiological Science, Yonsei University, Wonju 26493 (Korea, Republic of)

    2017-01-21

    We developed a depth of interaction (DOI) positron emission tomography (PET) detector using depth-dependent reflector patterns in a discrete crystal array. Due to the different reflector patterns at depth, light distribution was changed relative to depth. As a preliminary experiment, we measured DOI detector module crystal identification performance. The crystal consisted of a 9×9 array of 2 mmx2 mmx20 mm lutetium-yttrium oxyorthosilicate (LYSO) crystals. The crystal array was optically coupled to a 64-channel position-sensitive photomultiplier tube with a 2 mmx2 mm anode size and an 18.1 mmx18.1 mm effective area. We obtained the flood image with an Anger-type calculation. DOI layers and 9×9 pixels were well distinguished in the obtained images. Preclinical PET scanners based on this detector design offer the prospect of high and uniform spatial resolution.

  14. A new DOI detector design using discrete crystal array with depth-dependent reflector patterns and single-ended readout

    International Nuclear Information System (INIS)

    Lee, Seung-Jae; Lee, Chaeyeong; Kang, Jihoon; Chung, Yong Hyun

    2017-01-01

    We developed a depth of interaction (DOI) positron emission tomography (PET) detector using depth-dependent reflector patterns in a discrete crystal array. Due to the different reflector patterns at depth, light distribution was changed relative to depth. As a preliminary experiment, we measured DOI detector module crystal identification performance. The crystal consisted of a 9×9 array of 2 mmx2 mmx20 mm lutetium-yttrium oxyorthosilicate (LYSO) crystals. The crystal array was optically coupled to a 64-channel position-sensitive photomultiplier tube with a 2 mmx2 mm anode size and an 18.1 mmx18.1 mm effective area. We obtained the flood image with an Anger-type calculation. DOI layers and 9×9 pixels were well distinguished in the obtained images. Preclinical PET scanners based on this detector design offer the prospect of high and uniform spatial resolution.

  15. Range-energy relation, range straggling and response function of CsI(Tl), BGO and GSO(Ce) scintillators for light ions

    CERN Document Server

    Avdeichikov, V; Jakobsson, B; Rodin, A M; Ter-Akopian, G M

    2000-01-01

    Range-energy relations and range straggling of sup 1 sup , sup 2 sup , sup 3 H and sup 4 sup , sup 6 He isotopes with the energy approx 50A MeV are measured for the CsI(Tl), BGO and GSO(Ce) scintillators with an accuracy better than 0.2% and 5%, respectively. The Si-Sci/PD telescope was exposed to secondary beams from the mass separator ACCULINNA. The experimental technique is based on the registration of the 'jump' in the amplitude of the photodiode signal for ions passing through the scintillation crystal. Light response of the scintillators for ions 1<=Z<=4 is measured in energy range (5-50)A MeV, the results are in good agreement with calculations based on Birks model. The energy loss straggling for particles with DELTA E/E=0.01-0.50 and mass up to A=10 in 286 mu m DELTA E silicon detector is studied and compared with theoretical prescriptions. The results allow a precise absolute calibration of the scintillation crystal and to optimize the particle identification by the DELTA E-E(Sci/PD) method.

  16. Crystal scintillators for use in check-light source for thermoluminescent systems

    Science.gov (United States)

    Nagpal, J. S.; Sabharwal, S. C.; Chougaonkar, M. P.; Godbole, S. V.

    1999-08-01

    Beta ( 63Ni, Emax 0.063 MeV) excited radioluminescence of indigenously grown crystal scintillators CsI(Tl), Bi 4Ge 3O 12 and CdWO 4 has been studied for its use in check-light source needed for thermoluminescence systems. Temperature coefficient of the light output over 298-323 K and the beta-induced TL of the scintillators over 298-553 K are reported.

  17. Refractive index dispersion sensing using an array of photonic crystal resonant reflectors

    DEFF Research Database (Denmark)

    Hermannsson, Pétur Gordon; Vannahme, Christoph; Smith, Cameron

    2015-01-01

    Refractive index sensing plays a key role in various environmental and biological sensing applications. Here, a method is presented for measuring the absolute refractive index dispersion of liquids using an array of photonic crystal resonant reflectors of varying periods. It is shown that by cove......Refractive index sensing plays a key role in various environmental and biological sensing applications. Here, a method is presented for measuring the absolute refractive index dispersion of liquids using an array of photonic crystal resonant reflectors of varying periods. It is shown...... that by covering the array with a sample liquid and measuring the resonance wavelength associated with transverse electric polarized quasi guided modes as a function of period, the refractive index dispersion of the liquid can be accurately obtained using an analytical expression. This method is compact, can...... perform measurements at arbitrary number of wavelengths, and requires only a minute sample volume. The ability to sense a material's dispersion profile offers an added dimension of information that may be of benefit to optofluidic lab-on-a-chip applications. © 2015 AIP Publishing LLC....

  18. Optimization of a large-area detector-block based on SiPM and pixelated LYSO crystal arrays.

    Science.gov (United States)

    Calva-Coraza, E; Alva-Sánchez, H; Murrieta-Rodríguez, T; Martínez-Dávalos, A; Rodríguez-Villafuerte, M

    2017-10-01

    We present the performance evaluation of a large-area detector module based on the ArrayC-60035-64P, an 8×8 array of tileable, 7.2mm pitch, silicon photomultipliers (SiPM) by SensL, covering a total area of 57.4mm×57.4mm. We characterized the ArrayC-60035-64P, operating at room temperature, using LYSO pixelated crystal arrays of different pitch sizes (1.075, 1.430, 1.683, 2.080 and 2.280mm) to determine the resolvable crystal size. After an optimization process, a 7mm thick coupling light guide was used for all crystal pitches. To identify the interaction position a 16-channel (8 columns, 8 rows) symmetric charge division (SCD) readout board together with a center-of-gravity algorithm was used. Based on this, we assembled the detector modules using a 40×40 LYSO, 1.43mm pitch array, covering the total detector area. Calibration was performed using a 137 Cs source resulting in excellent crystal maps with minor geometric distortion, a mean 4.1 peak-to-valley ratio and 9.6% mean energy resolution for 662keV photons in the central region. The resolvability index was calculated in the x and y directions with values under 0.42 in all cases. We show that these large area SiPM arrays, combined with a 16-channel SCD readout board, can offer high spatial resolution, without processing a big number of signals, attaining excellent energy resolution and detector uniformity. Copyright © 2017 Associazione Italiana di Fisica Medica. Published by Elsevier Ltd. All rights reserved.

  19. Spatially resolved single crystal x-ray spectropolarimetry of wire array z-pinch plasmas.

    Science.gov (United States)

    Wallace, M S; Haque, S; Neill, P; Pereira, N R; Presura, R

    2018-01-01

    A recently developed single-crystal x-ray spectropolarimeter has been used to record paired sets of polarization-dependent and axially resolved x-ray spectra emitted by wire array z-pinches. In this measurement, two internal planes inside a suitable crystal diffract the x-rays into two perpendicular directions that are normal to each other, thereby separating incident x-rays into their linearly polarized components. This paper gives considerations for fielding the instrument on extended sources. Results from extended sources are difficult to interpret because generally the incident x-rays are not separated properly by the crystal. This difficulty is mitigated by using a series of collimating slits to select incident x-rays that propagate in a plane of symmetry between the polarization-splitting planes. The resulting instrument and some of the spatially resolved polarized x-ray spectra recorded for a 1-MA aluminum wire array z-pinch at the Nevada Terawatt Facility at the University of Nevada, Reno will be presented.

  20. Study on the property of the avalanche photodiode as the readout component for scintillation crystals

    International Nuclear Information System (INIS)

    He Jingtang; Chen Duanbao; Zhu Guoyi; Mao Yufang; Dong Xiaoli; Li Zuhao

    1996-01-01

    The new avalanche photodiode (APD) and a CsI(Tl) crystal formed a scintillation detector. The energy spectrum of γ rays was measured by this detector. The measured results were compared with that measured by photomultiplier. Our plan is to use APD as PbWO 4 readout component for forward luminosity electromagnetic calorimeter at τ-C factory

  1. Two-dimensional photonic crystal arrays for polymer:fullerene solar cells.

    Science.gov (United States)

    Nam, Sungho; Han, Jiyoung; Do, Young Rag; Kim, Hwajeong; Yim, Sanggyu; Kim, Youngkyoo

    2011-11-18

    We report the application of two-dimensional (2D) photonic crystal (PC) array substrates for polymer:fullerene solar cells of which the active layer is made with blended films of poly(3-hexylthiophene) (P3HT) and [6,6]-phenyl-C61-butyric acid methyl ester (PCBM). The 2D PC array substrates were fabricated by employing a nanosphere lithography technique. Two different hole depths (200 and 300 nm) were introduced for the 2D PC arrays to examine the hole depth effect on the light harvesting (trapping). The optical effect by the 2D PC arrays was investigated by the measurement of optical transmittance either in the direction normal to the substrate (direct transmittance) or in all directions (integrated transmittance). The results showed that the integrated transmittance was higher for the 2D PC array substrates than the conventional planar substrate at the wavelengths of ca. 400 nm, even though the direct transmittance of 2D PC array substrates was much lower over the entire visible light range. The short circuit current density (J(SC)) was higher for the device with the 2D PC array (200 nm hole depth) than the reference device. However, the device with the 2D PC array (300 nm hole depth) showed a slightly lower J(SC) value at a high light intensity in spite of its light harvesting effect proven at a lower light intensity.

  2. Comparison of SensL and Hamamatsu 4×4 channel SiPM arrays in gamma spectrometry with scintillators

    Energy Technology Data Exchange (ETDEWEB)

    Grodzicka-Kobylka, M., E-mail: m.grodzicka@ncbj.gov.pl; Szczesniak, T.; Moszyński, M.

    2017-06-01

    The market of Silicon Photomultipliers (SiPMs) consists of many manufacturers that produce their detectors in different technology. Hamamatsu (Japan) and SensL (Ireland) seems to be the most popular companies that produce large SiPM arrays. The aim of this work is characterization and comparison of 4×4 channel SiPM arrays produced by these two producers. Both of the tested SiPMs are made in through-silicon via (TSV) technology, consist of 16, 3×3 mm avalanche photodiode (APD) cells and have fill factor slightly above 60%. The largest difference is a single APD cell size and hence total number of APD cells (55,424 for Hamamatsu, 76,640 for SensL). In the case of SensL SiPM, its spectral response characteristics is shifted slightly toward shorter wavelengths with maximum at 420 nm (450 nm for Hamamatsu). The presented measurements cover selection of the SiPM optimum operating voltage (in respect to energy resolution), verification of the excess noise factor and check of the linearity characteristics. Moreover, the gamma spectrometry with LSO, BGO and CsI:Tl scintillators together with pulse characteristics for these crystals (rise time and fall time) is reported, as well as temperature dependence. The presented measurements show better performance of the SensL array comparing to the Hamamatsu detector.

  3. Calibrating the CsI(Tl) detectors of the GARFIELD apparatus

    CERN Document Server

    Abbondanno, U; Casini, G; Cavaletti, R; Cavallaro, S; Chiari, M; D'Agostino, M; Gramegna, F; Lanchais, A; Margagliotti, G V; Mastinu, P F; Milazzo, P M; Moroni, A; Nannini, A; Ordine, A; Vannini, G; Vannucci, L

    2002-01-01

    The energy and charge dependence of the light output of the CsI(Tl) detectors of the GARFIELD apparatus has been investigated for heavy ions with 5<=Z<=16 in the energy range from 2.2 to 8.3 A MeV. The results have been compared to an analytical expression successfully used in previous calibration procedures at higher energies, and a rather good agreement was obtained between measured and calculated quantities. The resulting parameter set was successfully applied to another set of experimental data. The overall result demonstrates the validity of the above mentioned calibration procedure in a wide range of incident ion energies and masses.

  4. Crystal scintillators for use in check-light source for thermoluminescent systems

    Energy Technology Data Exchange (ETDEWEB)

    Nagpal, J.S.; Sabharwal, S.C.; Chougaonkar, M.P.; Godbole, S.V

    1999-08-11

    Beta ({sup 63}Ni, E{sub max} 0.063 MeV) excited radioluminescence of indigenously grown crystal scintillators CsI(Tl), Bi{sub 4}Ge{sub 3}O{sub 12} and CdWO{sub 4} has been studied for its use in check-light source needed for thermoluminescence systems. Temperature coefficient of the light output over 298-323 K and the beta-induced TL of the scintillators over 298-553 K are reported. (author)

  5. A BaF2 crystal array for high energy-ray measurements

    Indian Academy of Sciences (India)

    Abstract. We shall discuss about the scientific motivation and construction of a 7 × 7 BaF2 crystal array at Variable Energy Cyclotron Centre, Calcutta. This detector would be used to measure high energy -ray photons from GDR decay and proton–neutron bremsstrahlung reactions at the present 88'' cyclotron and upcoming ...

  6. Performance of a PET detector module utilizing an array of silicon photodiodes to identify the crystal of interaction

    International Nuclear Information System (INIS)

    Moses, W.W.; Derenzo, S.E.; Nutt, R.; Digby, W.M.; Williams, C.W.; Andreaco, M.

    1993-01-01

    The authors initial performance results for a new multi-layer PET detector module consisting of an array of 3 mm square by 30 mm deep BGO crystals coupled on one end to a single photomultiplier tube and on the opposite end to an array of 3 mm square silicon photodiodes. The photomultiplier tube provides an accurate timing pulse and energy discrimination for all the crystals in the module, while the silicon photodiodes identify the crystal of interaction. When a single BGO crystal at +25 C is excited with 511 keV photons, the authors measure a photodiode signal centered at 700 electrons (e - ) with noise of 375 e - fwhm. When a four crystal/photodiode module is excited with a collimated line source of 511 keV photons, the crystal of interaction is correctly identified 82% of the time. The misidentification rate can be greatly reduced and an 8 x 8 crystal/photodiode module constructed by using thicker depletion layer photodiodes or cooling to 0 C

  7. Development of a model for on-line control of crystal growth by the AHP method

    Science.gov (United States)

    Gonik, M. A.; Lomokhova, A. V.; Gonik, M. M.; Kuliev, A. T.; Smirnov, A. D.

    2007-05-01

    The possibility to apply a simplified 2D model for heat transfer calculations in crystal growth by the axial heat close to phase interface (AHP) method is discussed in this paper. A comparison with global heat transfer calculations with the CGSim software was performed to confirm the accuracy of this model. The simplified model was shown to provide adequate results for the shape of the melt-crystal interface and temperature field in an opaque (Ge) and a transparent crystal (CsI:Tl). The model proposed is used for identification of the growth setup as a control object, for synthesis of a digital controller (PID controller at the present stage) and, finally, in on-line simulations of crystal growth control.

  8. 'Optical' soft x-ray arrays for fluctuation diagnostics in magnetic fusion energy experiments

    International Nuclear Information System (INIS)

    Delgado-Aparicio, L.F.; Stutman, D.; Tritz, K.; Finkenthal, M.; Kaita, R.; Roquemore, L.; Johnson, D.; Majeski, R.

    2004-01-01

    We are developing large pixel count, fast (≥100 kHz) and continuously sampling soft x-ray (SXR) array for the diagnosis of magnetohydrodynamics (MHD) and turbulent fluctuations in magnetic fusion energy plasmas. The arrays are based on efficient scintillators, high thoughput multiclad fiber optics, and multichannel light amplification and integration. Compared to conventional x-ray diode arrays, such systems can provide vastly increased spatial coverage, and access to difficult locations with small neutron noise and damage. An eight-channel array has been built using columnar CsI:Tl as an SXR converter and a multianode photomultiplier tube as photoamplifier. The overall system efficiency is measured using laboratory SXR sources, while the time response and signal-to-noise performance have been evaluated by recording MHD activity from the spherical tori (ST) Current Drive Experiment-Upgrade and National Spherical Torus Experiment, both at Princeton Plasma Physics Laboratory

  9. Simulation studies of crystal-photodetector assemblies for the Turkish accelerator center particle factory electromagnetic calorimeter

    Energy Technology Data Exchange (ETDEWEB)

    Kocak, F., E-mail: fkocak@uludag.edu.tr

    2015-07-01

    The Turkish Accelerator Center Particle Factory detector will be constructed for the detection of the produced particles from the collision of a 1 GeV electron beam against a 3.6 GeV positron beam. PbWO{sub 4} and CsI(Tl) crystals are considered for the construction of the electromagnetic calorimeter part of the detector. The generated optical photons in these crystals are detected by avalanche or PIN photodiodes. Geant4 simulation code has been used to estimate the energy resolution of the calorimeter for these crystal–photodiode assemblies.

  10. Diamond turning of small Fresnel lens array in single crystal InSb

    International Nuclear Information System (INIS)

    Jasinevicius, R G; Duduch, J G; Cirino, G A; Pizani, P S

    2013-01-01

    A small Fresnel lens array was diamond turned in a single crystal (0 0 1) InSb wafer using a half-radius negative rake angle (−25°) single-point diamond tool. The machined array consisted of three concave Fresnel lenses cut under different machining sequences. The Fresnel lens profiles were designed to operate in the paraxial domain having a quadratic phase distribution. The sample was examined by scanning electron microscopy and an optical profilometer. Optical profilometry was also used to measure the surface roughness of the machined surface. Ductile ribbon-like chips were observed on the cutting tool rake face. No signs of cutting edge wear was observed on the diamond tool. The machined surface presented an amorphous phase probed by micro Raman spectroscopy. A successful heat treatment of annealing was carried out to recover the crystalline phase on the machined surface. The results indicated that it is possible to perform a ‘mechanical lithography’ process in single crystal semiconductors. (paper)

  11. Distributed hydrophone array based on liquid crystal cell

    Science.gov (United States)

    Brodzeli, Zourab; Ladouceur, Francois; Silvestri, Leonardo; Michie, Andrew; Chigrinov, Vladimir; Guo, Grace Qi; Pozhidaev, Eugene P.; Kiselev, Alexei D.

    2012-02-01

    We describe a fibre optic hydrophone array system that could be used for underwater acoustic surveillance applications e.g. military, counter terrorist and customs authorities in protecting ports and harbors, offshore production facilities or coastal approaches as well as various marine applications. In this paper we propose a new approach to underwater sonar systems using voltage-controlled Liquid Crystals (LC) and simple multiplexing method. The proposed method permits measurements of sound under water at multiple points along an optical fibre using low cost components (LC cells), standard single mode fibre, without complex interferometric measurement techniques, electronics or demodulation software.

  12. Concentration dependence of the light yield and energy resolution of NaI:Tl and CsI:Tl crystals excited by gamma, soft X-rays and alpha particles

    CERN Document Server

    Trefilova, L N; Kovaleva, L V; Zaslavsky, B G; Zosim, D I; Bondarenko, S K

    2002-01-01

    Based on the analysis of light yield dependence on activator concentration for NaI:Tl and CsI:Tl excited by gamma-rays, soft X-rays and alpha-particles, an explanation of the effect of energy resolution enhancement with the rise of Tl content has been proposed. Based on the concept regarding the electron track structure, we proposed an alternative explanation of the intrinsic resolution value. The concept does not take into account the non-proportional response to electrons of different energies and is based on the statistic fluctuation of scintillation photon number formed outside and inside the regions of higher ionization density.

  13. Equivalent thermal history reconstruction from a partially crystallized glass-ceramic sensor array

    Science.gov (United States)

    Heeg, Bauke

    2015-11-01

    The basic concept of a thermal history sensor is that it records the accumulated exposure to some unknown, typically varying temperature profile for a certain amount of time. Such a sensor is considered to be capable of measuring the duration of several (N) temperature intervals. For this purpose, the sensor deploys multiple (M) sensing elements, each with different temperature sensitivity. At the end of some thermal exposure for a known period of time, the sensor array is read-out and an estimate is made of the set of N durations of the different temperature ranges. A potential implementation of such a sensor was pioneered by Fair et al. [Sens. Actuators, A 141, 245 (2008)], based on glass-ceramic materials with different temperature-dependent crystallization dynamics. In their work, it was demonstrated that an array of sensor elements can be made sensitive to slight differences in temperature history. Further, a forward crystallization model was used to simulate the variations in sensor array response to differences in the temperature history. The current paper focusses on the inverse aspect of temperature history reconstruction from a hypothetical sensor array output. The goal of such a reconstruction is to find an equivalent thermal history that is the closest representation of the true thermal history, i.e., the durations of a set of temperature intervals that result in a set of fractional crystallization values which is closest to the one resulting from the true thermal history. One particular useful simplification in both the sensor model as well as in its practical implementation is the omission of nucleation effects. In that case, least squares models can be used to approximate the sensor response and make reconstruction estimates. Even with this simplification, sensor noise can have a destabilizing effect on possible reconstruction solutions, which is evaluated using simulations. Both regularization and non-negativity constrained least squares

  14. Fibre Coupled Photonic Crystal Cavity Arrays on Transparent Substrates for Spatially Resolved Sensing

    Directory of Open Access Journals (Sweden)

    Mark G. Scullion

    2014-11-01

    Full Text Available We introduce a photonic crystal cavity array realised in a silicon thin film and placed on polydimethlysiloxane (PDMS as a new platform for the in-situ sensing of biomedical processes. Using tapered optical fibres, we show that multiple independent cavities within the same waveguide can be excited and their resonance wavelength determined from camera images without the need for a spectrometer. The cavity array platform combines sensing as a function of location with sensing as a function of time.

  15. Resonant absorption in semiconductor nanowires and nanowire arrays: Relating leaky waveguide modes to Bloch photonic crystal modes

    Energy Technology Data Exchange (ETDEWEB)

    Fountaine, Katherine T., E-mail: kfountai@caltech.edu [Department of Chemistry and Chemical Engineering, California Institute of Technology, 1200 E. California Blvd., Pasadena, California 91125 (United States); Joint Center for Artificial Photosynthesis, California Institute of Technology, 1200 E. California Blvd., Pasadena, California 91125 (United States); Whitney, William S. [Joint Center for Artificial Photosynthesis, California Institute of Technology, 1200 E. California Blvd., Pasadena, California 91125 (United States); Department of Physics, California Institute of Technology, 1200 E. California Blvd., Pasadena, California 91125 (United States); Atwater, Harry A. [Joint Center for Artificial Photosynthesis, California Institute of Technology, 1200 E. California Blvd., Pasadena, California 91125 (United States); Department of Applied Physics and Materials Science, California Institute of Technology, 1200 E. California Blvd., Pasadena, California 91125 (United States)

    2014-10-21

    We present a unified framework for resonant absorption in periodic arrays of high index semiconductor nanowires that combines a leaky waveguide theory perspective and that of photonic crystals supporting Bloch modes, as array density transitions from sparse to dense. Full dispersion relations are calculated for each mode at varying illumination angles using the eigenvalue equation for leaky waveguide modes of an infinite dielectric cylinder. The dispersion relations along with symmetry arguments explain the selectivity of mode excitation and spectral red-shifting of absorption for illumination parallel to the nanowire axis in comparison to perpendicular illumination. Analysis of photonic crystal band dispersion for varying array density illustrates that the modes responsible for resonant nanowire absorption emerge from the leaky waveguide modes.

  16. The development of a single-crystal fiber-array scintillator area detector

    International Nuclear Information System (INIS)

    Loong, Chun; Vitt, Richard; Sayir, Ali; Sayir, Haluk

    2001-01-01

    The scientific output of a neutron instrument is directly proportional to the effectiveness of its detector system-coverage of scattering area, pixel resolution, counting efficiency, signal-to-noise ratio, life time and cost. The current neutron scintillator detectors employ mainly 6 Li-doped glass and ZnS, both of which present well-know limitations such as low light output, high gamma sensitivity in the case of 6 Li-glass and optical opacity in the case of ZnS. We aim to develop a position-sensitive, flight-time differentiable, efficient and cost-effective neutron detector system based on single-crystal scintillator fiber-arrays. The laser-heated melt modulation fiber growth technology developed at NASA provides the means to grow high-purity single-crystal fibers or rods of variable diameters (200 μm to 5 mm) and essentially unlimited length. Arrays of such fibers can be tailored to meet the requirements of pixel size, geometric configuration, and coverage area for a detector system. We report a plan in the growth and characterization of scintillators based on lithium silicates and boron aluminates using Ce as activator. (author)

  17. Evaluation of polymer-coated CsI:Tl as an alpha/beta pulse shape discriminating flow-cell

    International Nuclear Information System (INIS)

    Branton, S.D.; Fjeld, R.A.; DeVol, T.A.

    1996-01-01

    A pulse shape discriminating flow-cell radiation detection system constructed with polymer coated CsI:Tl was evaluated for simultaneous gross alpha/gross beta quantification. The CsI:TI scintillator was crushed and sieved to 63-90 μm particle size and microencapsulated with Parylene C to reduce its rate of dissolution. Averaged over the first hour of use, the pulse shape discrimination figure-of-merit was 1.4 and the detection efficiencies were 64.9 ± 5.7 %, 52.5 ± 4.5 % and 4.5 ± 0.2 % for 233 U, 90 Sr/ 90 Y and 14 C , respectively. The typical background count rate in the alpha and beta pulse shape window was 0.17 and 0.004 cps, respectively. The resultant minimum detectable activity for a 30 second count time was calculated to be 0.19 ± 0.01 Bq, 0.9 ± 0.1 Bq and 11.4 ± 0.6 Bq for 233 U, 90 Sr/ 90 Y and 14 C, respectively. Although the 3 μm thick microencapsulation reduced CsI:Tl dissolution, the detection efficiency declined by a factor of two after 4.8 hours while the pulse shape resolution degraded slightly

  18. A study on light collection of small scintillating crystals

    CERN Document Server

    Vittori, F; Malatesta, T; Puertolas, D

    2000-01-01

    Measurements are described concerning the light collection efficiency of YAP:Ce and CsI(Tl) crystals pillars with thicknesses ranging between 3 and 28 mm and cross-sections of 0.6 x 0.6 and 1 x 1 mm sup 2. These measurements have shown that the light collection is strongly dependent on the length of the pillar rather than on its cross-sectional area. A Monte Carlo code has been developed in order to evaluate the light collection efficiency as a function of the pillar geometry and surface treatment. Particular attention has been paid to the light transition through the crystal-photocathode window interface. The possibility to improve light detection by using a new photon detector provided with a YAP photocathode window has been verified.

  19. Sliding three-phase contact line of printed droplets for single-crystal arrays

    International Nuclear Information System (INIS)

    Kuang, Minxuan; Wu, Lei; Li, Yifan; Gao, Meng; Zhang, Xingye; Jiang, Lei; Song, Yanlin

    2016-01-01

    Controlling the behaviours of printed droplets is an essential requirement for inkjet printing of delicate three-dimensional (3D) structures or high-resolution patterns. In this work, molecular deposition and crystallization are regulated by manipulating the three-phase contact line (TCL) behaviour of the printed droplets. The results show that oriented single-crystal arrays are fabricated based on the continuously sliding TCL. Owing to the sliding of the TCL on the substrate, the outward capillary flow within the evaporating droplet is suppressed and the molecules are brought to the centre of the droplet, resulting in the formation of a single crystal. This work provides a facile strategy for controlling the structures of printed units by manipulating the TCL of printed droplets, which is significant for realizing high-resolution patterns and delicate 3D structures. (paper)

  20. Air-Coupled Low Frequency Ultrasonic Transducers and Arrays with PMN-32%PT Piezoelectric Crystals

    Directory of Open Access Journals (Sweden)

    Rymantas J. Kazys

    2017-01-01

    Full Text Available Air-coupled ultrasonic techniques are being increasingly used for material characterization, non-destructive evaluation of composite materials using guided waves as well as for distance measurements. Application of those techniques is mainly limited by the big losses of ultrasonic signals due to attenuation and mismatch of the acoustic impedances of ultrasonic transducers and air. One of the ways to solve this problem is by application of novel more efficient piezoelectric materials like lead magnesium niobate-lead titanate (PMN-PT type crystals. The objective of this research was the development and investigation of low frequency (<50 kHz wide band air-coupled ultrasonic transducers and arrays with an improved performance using PMN-32%PT crystals. Results of finite element modelling and experimental investigations of the developed transducers and arrays are presented. For improvement of the performance strip-like matching elements made of low acoustic impedance, materials such as polystyrene foams were applied. It allowed to achieve transduction losses for one single element transducer −11.4 dB, what is better than of commercially available air-coupled ultrasonic transducers. Theoretical and experimental investigations of the acoustic fields radiated by the eight element ultrasonic array demonstrated not only a good performance of the array in a pulse mode, but also very good possibilities to electronically focus and steer the ultrasonic beam in space.

  1. Studies of an array of PbF2 Cherenkov crystals with large-area SiPM readout

    Energy Technology Data Exchange (ETDEWEB)

    Fienberg, A. T.; Alonzi, L. P.; Anastasi, A.; Bjorkquist, R.; Cauz, D.; Fatemi, R.; Ferrari, C.; Fioretti, A.; Frankenthal, A.; Gabbanini, C.; Gibbons, L. K.; Giovanetti, K.; Goadhouse, S. D.; Gohn, W. P.; Gorringe, T. P.; Hertzog, D. W.; Iacovacci, M.; Kammel, P.; Kaspar, J.; Kiburg, B.; Li, L.; Mastroianni, S.; Pauletta, G.; Peterson, D. A.; Počanić, D.; Smith, M. W.; Sweigart, D. A.; Tishchenko, V.; Venanzoni, G.; Van Wechel, T. D.; Wall, K. B.; Winter, P.; Yai, K.

    2015-05-01

    The electromagnetic calorimeter for the new muon (g-2) experiment at Fermilab will consist of arrays of PbF2 Cherenkov crystals read out by large-area silicon photo-multiplier (SiPM) sensors. We report here on measurements and simulations using 2.0 -- 4.5 GeV electrons with a 28-element prototype array. All data were obtained using fast waveform digitizers to accurately capture signal pulse shapes versus energy, impact position, angle, and crystal wrapping. The SiPMs were gain matched using a laser-based calibration system, which also provided a stabilization procedure that allowed gain correction to a level of 1e-4 per hour. After accounting for longitudinal fluctuation losses, those crystals wrapped in a white, diffusive wrapping exhibited an energy resolution sigma/E of (3.4 +- 0.1) % per sqrt(E/GeV), while those wrapped in a black, absorptive wrapping had (4.6 +- 0.3) % per sqrt(E/GeV). The white-wrapped crystals---having nearly twice the total light collection---display a generally wider and impact-position-dependent pulse shape owing to the dynamics of the light propagation, in comparison to the black-wrapped crystals, which have a narrower pulse shape that is insensitive to impact position.

  2. Design and simulation of a novel method for determining depth-of-interaction in a PET scintillation crystal array using a single-ended readout by a multi-anode PMT

    International Nuclear Information System (INIS)

    Ito, Mikiko; Sim, Kwang-Souk; Lee, Jae Sung; Park, Min-Jae; Hong, Seong Jong

    2010-01-01

    PET detectors with depth-of-interaction (DOI) encoding capability allow high spatial resolution and high sensitivity to be achieved simultaneously. To obtain DOI information from a mono-layer array of scintillation crystals using a single-ended readout, the authors devised a method based on light spreading within a crystal array and performed Monte Carlo simulations with individual scintillation photon tracking to prove the concept. A scintillation crystal array model was constructed using a grid method. Conventional grids are constructed using comb-shaped reflector strips with rectangular teeth to isolate scintillation crystals optically. However, the authors propose the use of triangularly shaped teeth, such that scintillation photons spread only in the x-direction in the upper halves of crystals and in the y-direction in lower halves. DOI positions can be estimated by considering the extent of two-dimensional light dispersion, which can be determined from the multiple anode outputs of a position-sensitive PMT placed under the crystal array. In the main simulation, a crystal block consisting of a 29 x 29 array of 1.5 mm x 1.5 mm x 20 mm crystals and a multi-anode PMT with 16 x 16 pixels were used. The effects of crystal size and non-uniform PMT output gain were also explored by simulation. The DOI resolution estimated for 1.5 x 1.5 x 20 mm 3 crystals was 2.16 mm on average. Although the flood map was depth dependent, each crystal was well identified at all depths when a corner of the crystal array was irradiated with 511 keV gamma rays (peak-to-valley ratio ∼9:1). DOI resolution was better than 3 mm up to a crystal length of 28 mm with a 1.5 x 1.5 mm 2 or 2.0 x 2.0 mm 2 crystal surface area. The devised light-sharing method allowed excellent DOI resolutions to be obtained without the use of dual-ended readout or multiple crystal arrays.

  3. Performance of A Compact Multi-crystal High-purity Germanium Detector Array for Measuring Coincident Gamma-ray Emissions

    Energy Technology Data Exchange (ETDEWEB)

    Howard, Chris [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Daigle, Stephen [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Buckner, Matt [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Erikson, Luke E. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Runkle, Robert C. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Stave, Sean C. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Champagne, Art [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Cooper, Andrew [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Downen, Lori [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Glasgow, Brian D. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Kelly, Keegan [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Sallaska, Anne [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States)

    2015-02-18

    The Multi-sensor Airborne Radiation Survey (MARS) detector is a 14-crystal array of high-purity germanium (HPGe) detectors housed in a single cryostat. The array was used to measure the astrophysical S-factor for the 14N(p,γ)15O* reaction for several transition energies at an effective center of mass energy of 163 keV. Owing to the segmented nature of the MARS detector, the effect of gamma-ray summing was greatly reduced in comparison to past experiments which utilized large, single-crystal detectors. The new S-factor values agree within the uncertainties with the past measurements. Details of the analysis and detector performance will be presented.

  4. Performance of a compact multi-crystal high-purity germanium detector array for measuring coincident gamma-ray emissions

    Energy Technology Data Exchange (ETDEWEB)

    Howard, Chris; Daigle, Stephen; Buckner, Matt [University of North Carolina at Chapel Hill, Chapel Hill, NC 27599 (United States); Triangle Universities Nuclear Laboratory, Durham, NC 27708 (United States); Erikson, Luke E.; Runkle, Robert C. [Pacific Northwest National Laboratory, Richland, WA 99352 (United States); Stave, Sean C., E-mail: Sean.Stave@pnnl.gov [Pacific Northwest National Laboratory, Richland, WA 99352 (United States); Champagne, Arthur E.; Cooper, Andrew; Downen, Lori [University of North Carolina at Chapel Hill, Chapel Hill, NC 27599 (United States); Triangle Universities Nuclear Laboratory, Durham, NC 27708 (United States); Glasgow, Brian D. [Pacific Northwest National Laboratory, Richland, WA 99352 (United States); Kelly, Keegan; Sallaska, Anne [University of North Carolina at Chapel Hill, Chapel Hill, NC 27599 (United States); Triangle Universities Nuclear Laboratory, Durham, NC 27708 (United States)

    2015-05-21

    The Multi-sensor Airborne Radiation Survey (MARS) detector is a 14-crystal array of high-purity germanium (HPGe) detectors housed in a single cryostat. The array was used to measure the astrophysical S-factor for the {sup 14}N(p,γ){sup 15}O{sup ⁎} reaction for several transition energies at an effective center-of-mass energy of 163 keV. Owing to the granular nature of the MARS detector, the effect of gamma-ray summing was greatly reduced in comparison to past experiments which utilized large, single-crystal detectors. The new S-factor values agree within their uncertainties with the past measurements. Details of the analysis and detector performance are presented.

  5. The Milano-Gran Sasso double beta decay experiment: toward a 20-crystal array

    International Nuclear Information System (INIS)

    Alessandrello, A.; Brofferio, C.; Bucci, C.; Cremonesi, O.; Fiorini, E.; Giuliani, A.; Nucciotti, A.; Pavan, M.; Pessina, G.; Previtali, E.; Zanotti, L.

    1996-01-01

    TeO 2 thermal detectors are being used by the Milano group to search for neutrinoless double beta decay of 130 Te. An upper limit for neutrinoless decay half life of 2.1 x 10 22 yr at 90% CL obtained with a 334 g TeO 2 detector has been previously reported. To improve the sensitivity of the experiment an array of twenty 340 g TeO 2 crystals will be realised in the next future. As a first step toward the realisation of that experiment a 4 crystal detector has been tested in the Gran Sasso refrigerator. Detector performances, data acquisition and analysis are discussed. (orig.)

  6. An electrically tunable plenoptic camera using a liquid crystal microlens array

    International Nuclear Information System (INIS)

    Lei, Yu; Tong, Qing; Zhang, Xinyu; Sang, Hongshi; Ji, An; Xie, Changsheng

    2015-01-01

    Plenoptic cameras generally employ a microlens array positioned between the main lens and the image sensor to capture the three-dimensional target radiation in the visible range. Because the focal length of common refractive or diffractive microlenses is fixed, the depth of field (DOF) is limited so as to restrict their imaging capability. In this paper, we propose a new plenoptic camera using a liquid crystal microlens array (LCMLA) with electrically tunable focal length. The developed LCMLA is fabricated by traditional photolithography and standard microelectronic techniques, and then, its focusing performance is experimentally presented. The fabricated LCMLA is directly integrated with an image sensor to construct a prototyped LCMLA-based plenoptic camera for acquiring raw radiation of targets. Our experiments demonstrate that the focused region of the LCMLA-based plenoptic camera can be shifted efficiently through electrically tuning the LCMLA used, which is equivalent to the extension of the DOF

  7. Design and performance of modularized NaI(Tl) detectors with rectangular crystal elements: An array of 49 and the Crystal Box

    International Nuclear Information System (INIS)

    Wilson, S.L.; Hofstadter, R.; Hughes, E.B.; Lin, Y.C.; Parks, R.; Rolfe, J.; Bolton, R.D.; Bowman, J.D.; Cooper, M.D.; Hoffman, C.M.; Hogan, G.E.; Mariam, F.G.; Mischke, R.E.; Nagle, D.E.; Piilonen, L.E.; Sandberg, V.D.; Sanders, G.H.; Werbeck, R.; Williams, R.A.; Frank, J.S.; Hallin, A.L.; Matis, H.S.; Sennhauser, U.; Wright, S.C.

    1988-01-01

    An array of 49 NaI(Tl) modules each 20 inch in depth and 2.5 inch x 2.5 inch in cross section has been constructed and its properties, especially energy resolution, explored for positrons in the range 20 MeV - 18 GeV. A subsequent much larger detector, the Crystal Box, has also been constructed from 396 modules of the same cross section, but mostly 12 inch in depth, and operated as a γ-ray and positron detector in a search for rare muon decays. The calibration procedure used for the Crystal Box and its characteristic resolutions in energy, impact point and time are described. (orig.)

  8. CsI(Tl) with photodiodes for identifying subsurface radionuclide contamination

    International Nuclear Information System (INIS)

    Stromswold, D.C.; Meisner, J.E.; Nicaise, W.F.

    1994-10-01

    At the US Department of Energy's Hanford Site near Richland, Washington, underground radioactive contamination exists as the result of leaks, spills, and intentional disposal of waste products from plutonium-production operations. Characterizing these contaminants in preparation for environmental remediation is a major effort now in progress. In this paper, a cylindrical (15 x 61 mm) CsI(Tl) scintillation detector with two side-mounted photodiodes has been developed to collect spectral gamma-ray data in subsurface contaminated formations at the U.S. Department of Energy's Hanford Site. It operates inside small-diameter, thick-wall steel pipes pushed into the ground to depths up to 20 m by a cone penetrometer. The detector provides a rugged, efficient, magnetic-field-insensitive means for identifying gamma-ray-emitting contaminants (mainly 137 Cs and 60 Co). Mounting two 3 x 30-mm photodiodes end-to-end on a flat area along the detector's side provides efficient light collection over the length of the detector

  9. SPAD array chips with full frame readout for crystal characterization

    Energy Technology Data Exchange (ETDEWEB)

    Fischer, Peter; Blanco, Roberto; Sacco, Ilaria; Ritzert, Michael [Heidelberg University (Germany); Weyers, Sascha [Fraunhofer Institute for Microelectronic Circuits and Systems (Germany)

    2015-05-18

    We present single photon sensitive 2D camera chips containing 88x88 avalanche photo diodes which can be read out in full frame mode with up to 400.000 frames per second. The sensors have an imaging area of ~5mm x 5mm covered by square pixels of ~56µm x 56µm with a ~55% fill factor in the latest chip generation. The chips contain a self triggering logic with selectable (column) multiplicities of up to >=4 hits within an adjustable coincidence time window. The photon accumulation time window is programmable as well. First prototypes have demonstrated low dark count rates of <50kHz/mm2 (SPAD area) at 10 degree C for 10% masked pixels. One chip version contains an automated readout of the photon cluster position. The readout of the detailed photon distribution for single events allows the characterization of light sharing, optical crosstalk etc., in crystals or crystal arrays as they are used in PET instrumentation. This knowledge could lead to improvements in spatial or temporal resolution.

  10. On the elimination of the afterglow of CsI(Tl) scintillation detector

    International Nuclear Information System (INIS)

    Alfassi, Z.B.; Ifergan, Y.; Wengrowicz, U.; Weinstein, Marcelo

    2009-01-01

    The use of CsI(Tl) in survey meters is limited to low dose-rate fields due to the afterglow effect, which can take up to 20 min in case of 120 s exposure to 4 R/h field. Even mixtures of low and high dose-rate fields are prohibited since the afterglow effect of the high dose-rate field prevents the use of the meter in the low dose-rate field. It was found that heating the scintillation detector to 60 deg. C shortened considerably the time of the afterglow effect to 3 s, even after exposure of 120 s to fields of 4 R/h. It is suggested to start heating the detector immediately when reaching high dose-rate field and adjusting the calibration to the measured temperature.

  11. Design, instrumentation and response characteristics of a 2 pi multi-detector of CsI(Tl) scintillators mounted inside the Plastic Ball spectrometer

    NARCIS (Netherlands)

    Joulaeizadeh, L.; Gasparic, I.; Bacelar, J.; Caplar, R.; Löhner, H.

    2010-01-01

    A 2 pi hemispherical detector consisting of 64 CsI(Tl) scintillator modules covering the angular range of 80 degrees -160 degrees has been constructed. This detector is employed as the Inner Shell of the Plastic Ball detector and was used in two experimental programs concerning the study of pionic

  12. Frequency-addressed tunable transmission in optically thin metallic nanohole arrays with dual-frequency liquid crystals

    International Nuclear Information System (INIS)

    Hao Qingzhen; Zhao Yanhui; Juluri, Bala Krishna; Kiraly, Brian; Huang, Tony Jun; Liou, Justin; Khoo, Iam Choon

    2011-01-01

    Frequency-addressed tunable transmission is demonstrated in optically thin metallic nanohole arrays embedded in dual-frequency liquid crystals (DFLCs). The optical properties of the composite system are characterized by the transmission spectra of the nanoholes, and a prominent transmission peak is shown to originate from the resonance of localized surface plasmons at the edges of the nanoholes. An ∼17 nm shift in the transmission peak is observed between the two alignment configurations of the liquid crystals. This DFLC-based active plasmonic system demonstrates excellent frequency-dependent switching behavior and could be useful in future nanophotonic applications.

  13. Spherical porphyrin sensor array based on encoded colloidal crystal beads for VOC vapor detection.

    Science.gov (United States)

    Xu, Hua; Cao, Kai-Di; Ding, Hai-Bo; Zhong, Qi-Feng; Gu, Hong-Cheng; Xie, Zhuo-Ying; Zhao, Yuan-Jin; Gu, Zhong-Ze

    2012-12-01

    A spherical porphyrin sensor array using colloidal crystal beads (CCBs) as the encoding microcarriers has been developed for VOC vapor detection. Six different porphyrins were coated onto the CCBs with distinctive encoded reflection peaks via physical adsorption and the sensor array was fabricated by placing the prepared porphyrin-modified CCBs together. The change in fluorescence color of the porphyrin-modified CCBs array serves as the detection signal for discriminating between different VOC vapors and the reflection peak of the CCBs serves as the encoding signal to distinguish between different sensors. It was demonstrated that the VOC vapors detection using the prepared sensor array showed excellent discrimination: not only could the compounds from the different chemical classes be easily differentiated (e.g., alcohol vs acids vs ketones) but similar compounds from the same chemical family (e.g., methanol vs ethanol) and the same compound with different concentration ((e.g., Sat. ethanol vs 60 ppm ethanol vs 10 ppm ethanol) could also be distinguished. The detection reproducibility and the humidity effect were also investigated. The present spherical sensor array, with its simple preparation, rapid response, high sensitivity, reproducibility, and humidity insensitivity, and especially with stable and high-throughput encoding, is promising for real applications in artificial olfactory systems.

  14. Improvement of crystal identification performance for a four-layer DOI detector composed of crystals segmented by laser processing

    Science.gov (United States)

    Mohammadi, Akram; Inadama, Naoko; Yoshida, Eiji; Nishikido, Fumihiko; Shimizu, Keiji; Yamaya, Taiga

    2017-09-01

    We have developed a four-layer depth of interaction (DOI) detector with single-side photon readout, in which segmented crystals with the patterned reflector insertion are separately identified by the Anger-type calculation. Optical conditions between segmented crystals, where there is no reflector, affect crystal identification ability. Our objective of this work was to improve crystal identification performance of the four-layer DOI detector that uses crystals segmented with a recently developed laser processing technique to include laser processed boundaries (LPBs). The detector consisted of 2 × 2 × 4mm3 LYSO crystals and a 4 × 4 array multianode photomultiplier tube (PMT) with 4.5 mm anode pitch. The 2D position map of the detector was calculated by the Anger calculation method. At first, influence of optical condition on crystal identification was evaluated for a one-layer detector consisting of a 2 × 2 crystal array with three different optical conditions between the crystals: crystals stuck together using room temperature vulcanized (RTV) rubber, crystals with air coupling and segmented crystals with LPBs. The crystal array with LPBs gave the shortest distance between crystal responses in the 2D position map compared with the crystal array coupled with RTV rubber or air due to the great amount of cross-talk between segmented crystals with LPBs. These results were used to find optical conditions offering the optimum distance between crystal responses in the 2D position map for the four-layer DOI detector. Crystal identification performance for the four-layer DOI detector consisting of an 8 × 8 array of crystals segmented with LPBs was examined and it was not acceptable for the crystals in the first layer. The crystal identification was improved for the first layer by changing the optical conditions between all 2 × 2 crystal arrays of the first layer to RTV coupling. More improvement was observed by combining different optical conditions between all

  15. Enhanced columnar structure in CsI layer by substrate patterning

    Energy Technology Data Exchange (ETDEWEB)

    Jing, T.; Cho, G.; Drewery, J.; Kaplan, S.N.; Mireshghi, A.; Perez-Mendez, V.; Wildermuth, D. [Lawrence Berkeley Lab., CA (United States); Fujieda, I. [Xerox Palo Alto Research Center, CA (United States)

    1991-10-01

    Columnar structure in evaporated CsI layers can be controlled by patterning substrates as well as varying evaporation conditions. Mesh-patterned substrates with various dimensions were created by spin-coating polyimide on glass or amorphous silicon substrates and defining patterns with standard photolithography technique. CsI(Tl) layers 200--1000 {mu}m were evaporated. Scintillation properties of these evaporated layers, such as light yield and speed, were equivalent to those of the source materials. Spatial resolution of X-ray detectors consisting of these layers and a linear array of X-ray detectors consisting of these layers and a linear array of Si photodiodes was evaluated by exposing them to a 25{mu}m narrow beam of X-ray. The results obtained with 200{mu}m thick CsI layers coupled to a linear photodiode array with 20 dots/mm resolution showed that the spatial resolution of CsI(Tl) evaporated on patterned substrates was about 75 {mu}m FWHM, whereas that on CsI(Tl) on flat substrates was about 230 {mu}m FWHM. Micrographs taken by SEM revealed that these layers retained the well-defined columnar structure originating from substrate patterns. Adhesion and light transmission of CsI(Tl) were also improved by patterning the substrate.

  16. A novel intra-operative positron imager for rapid localization of tumor margins

    Science.gov (United States)

    Sabet, Hamid; Stack, Brendan C.; Nagarkar, Vivek V.

    2014-03-01

    We have developed an intra-operative and compact imaging tool for surgeons to detect PET- positive lesions. Currently, most such probes on the market are non-imaging, and provide no ancillary information of surveyed areas, such as clear delineations of malignant tissues. Our probe consists of a novel hybrid scintillator coupled to a compact silicon photomultiplier (SiPM) array with associated front-end electronics encapsulated in an ergonomic housing. Pulse shape discrimination electronics has been implemented and integrated into the downstream data acquisition system. The hybrid scintillator consists of a 0.4 mm thick layer of CsI:Tl scintillator coupled to a 1 mm thick LYSO crystal. To achieve high spatial resolution, CsI:Tl is pixelated to 0.5×0.5 mm2 pixels using laser ablation technique. While CsI:Tl act as beta-sensitive scintillator, LYSO senses the gamma radiation and can be used to navigate the probe to the locations of interest. The gamma response is also subtracted from the beta image for improved SNR and contrast. To achieve accurate centroid position estimation and uniform beta sensitivity over the entire imaging area, the LYSO thickness is optimized such that it acts as scintillation light diffuser by spreading CsI:Tl light over multiple SiPM pixels. The results show that the response of the two scintillators exposed to radiation could be easily distinguished based on their pulse shapes. The probe's spatial resolution is beta radiation even in presence of strong gamma background.

  17. Amorphous silicon pixel layers with cesium iodide converters for medical radiography

    International Nuclear Information System (INIS)

    Jing, T.; Cho, G.; Goodman, C.A.

    1993-11-01

    We describe the properties of evaporated layers of Cesium Iodide (Thallium activated) deposited on substrates that enable easy coupling to amorphous silicon pixel arrays. The CsI(Tl) layers range in thickness from 65 to 220μm. We used the two-boat evaporator system to deposit CsI(Tl) layers. This system ensures the formation of the scintillator film with homogenous thallium concentration which is essential for optimizing the scintillation light emission efficiency. The Tl concentration was kept to 0.1--0.2 mole percent for the highest light output. Temperature annealing can affect the microstructure as well as light output of the CsI(Tl) film. 200--300C temperature annealing can increase the light output by a factor of two. The amorphous silicon pixel arrays are p-i-n diodes approximately lμm thick with transparent electrodes to enable them to detect the scintillation light produced by X-rays incident on the CsI(Tl). Digital radiography requires a good spatial resolution. This is accomplished by making the detector pixel size less then 50μm. The light emission from the CsI(Tl) is collimated by techniques involving the deposition process on pattered substrates. We have measured MTF of greater than 12 line pairs per mm at the 10% level

  18. Time walk correction for TOF-PET detectors based on a monolithic scintillation crystal coupled to a photosensor array

    International Nuclear Information System (INIS)

    Vinke, R.; Loehner, H.; Schaart, D.R.; Dam, H.T. van; Seifert, S.; Beekman, F.J.; Dendooven, P.

    2010-01-01

    When optimizing the timing performance of a time-of-flight positron emission tomography (TOF-PET) detector based on a monolithic scintillation crystal coupled to a photosensor array, time walk as a function of annihilation photon interaction location inside the crystal needs to be considered. In order to determine the 3D spatial coordinates of the annihilation photon interaction location, a maximum likelihood estimation algorithm was developed, based on a detector characterization by a scan of a 511 keV photon beam across the front and one of the side surfaces of the crystal. The time walk effect was investigated using a 20 mmx20 mmx12 mm LYSO crystal coupled to a fast 4x4 multi-anode photomultiplier tube (MAPMT). In the plane parallel to the photosensor array, a spatial resolution of 2.4 mm FWHM is obtained. In the direction perpendicular to the MAPMT (depth-of-interaction, DOI), the resolution ranges from 2.3 mm FWHM near the MAPMT to 4 mm FWHM at a distance of 10 mm. These resolutions are uncorrected for the ∼1mm beam diameter. A coincidence timing resolution of 358 ps FWHM is obtained in coincidence with a BaF 2 detector. A time walk depending on the 3D annihilation photon interaction location is observed. Throughout the crystal, the time walk spans a range of 100 ps. Calibration of the time walk vs. interaction location allows an event-by-event correction of the time walk.

  19. Theoretical model and experimental verification on the PID tracking method using liquid crystal optical phased array

    Science.gov (United States)

    Wang, Xiangru; Xu, Jianhua; Huang, Ziqiang; Wu, Liang; Zhang, Tianyi; Wu, Shuanghong; Qiu, Qi

    2017-02-01

    Liquid crystal optical phased array (LC-OPA) has been considered with great potential on the non-mechanical laser deflector because it is fabricated using photolithographic patterning technology which has been well advanced by the electronics and display industry. As a vital application of LC-OPA, free space laser communication has demonstrated its merits on communication bandwidth. Before data communication, ATP (acquisition, tracking and pointing) process costs relatively long time to result in a bottle-neck of free space laser communication. Meanwhile, dynamic real time accurate tracking is sensitive to keep a stable communication link. The electro-optic medium liquid crystal with low driving voltage can be used as the laser beam deflector. This paper presents a fast-track method using liquid crystal optical phased array as the beam deflector, CCD as a beacon light detector. PID (Proportion Integration Differentiation) loop algorithm is introduced as the controlling algorithm to generate the corresponding steering angle. To achieve the goal of fast and accurate tracking, theoretical analysis and experimental verification are demonstrated that PID closed-loop system can suppress the attitude random vibration. Meanwhile, theoretical analysis shows that tracking accuracy can be less than 6.5μrad, with a relative agreement with experimental results which is obtained after 10 adjustments that the tracking accuracy is less than12.6μrad.

  20. Development of radiation detection and measurement system - Development of scintillation radiation sensor

    Energy Technology Data Exchange (ETDEWEB)

    Kang, Hee Dong; Kim, Wan [Kyungpook National University, Taegu (Korea); Kim, Do Sung [Taegu University, Taegu (Korea)

    2000-03-01

    We have been fabricated CsI(Tl) scintillation crystals and plastic scintillators for radiation-based measuring equipment. CsI (Tl) single crystals doped with thallium as an activator were grown using the Czochralski method. The crystal structure of grown CsI(Tl) was bcc, and it was confirmed that its lattice constant was 4,568 A. The spectral range of luminescence of CsI(Tl) was 350 {approx} 700 nm independent of thallium concentration, and the fast component of the luminescence was decreased with increasing thallium concentration. The energy resolution of CsI(Tl) scintillator doped with 0.1 mole% thallium was about 9% for 137 Cs {gamma}-rays. The relation formula of {gamma}-ray energy versus energy resolution was ln(FWHM%)=-0.705ln({epsilon})+6.75. The radiation damage of CsI(Tl) increased in proportion to thallium concentration and radiation damage of CsI(Tl) increased in proportion to thallium concentration and radiation dosage, and the irradiated crystals were colored reddish. The radiation induced absorption bands appeared around 355, 425, 520 and 555 nm, and their energy level were about 3.50, 2.88, 2.39 and 2.21 eV. Plastic scintillators were fabricated thermal polymerization method. Those were polymerizing at 120 deg. C, during 72 hours, and annealing at 75 deg. C, during 24 hours. When the concentration of 1st solute was 1.5 wt% and concentration of 2nd solute was 0.01 wt%, the characteristics of scintillation were very excellent. Also 3.0 wt% tetraphenyl lead were loaded to improve the detection efficiency of {gamma}-ray. The range of emission spectrum was 400 {approx} 450nm, and the central peak was 415 nm. The radiation damage was not appear under 1*10{sup 3}Gy, but the color of plastic scintillator was changed to brown, over 1*10{sup 4}Gy exposured. 84 refs., 39 figs. (Author)

  1. Development of high-resolution gamma detector using sub-mm GAGG crystals coupled to TSV-MPPC array

    International Nuclear Information System (INIS)

    Lipovec, A.; Shimazoe, K.; Takahashi, H.

    2016-01-01

    In this study a high-resolution gamma detector based on an array of sub-millimeter Ce:GAGG (Cerium doped Gd 3 Al 2 Ga 3 O 12 ) crystals read out by an array of surface-mount type of TSV-MPPC was developed. MPPC sensor from Hamamatsu which has a 26 by 26 mm 2 detector area with 64 channels was used. One channel has a 3 by 3 mm 2 photosensitive area with 50 μ m pitch micro cells. MPPC sensor provides 576 mm 2 sensing area and was used to decode 48 by 48 array with 0.4 by 0.4 by 20 mm 3 Ce:GAGG crystals of 500 μ m pitch. The base of the detector with the crystal module was mounted to a read out board which consists of charge division circuit, thus allowing for a read out of four channels to identify the position of the incident event on the board. The read out signals were amplified using charge sensitive amplifiers. The four amplified signals were digitized and analyzed to produce a position sensitive event. For the performance analysis a 137 Cs source was used. The produced events were used for flood histogram and energy analysis. The effects of the glass thickness between the Ce:GAGG and MPPC were analyzed using the experimental flood diagrams and Geant4 simulations. The glass between the scintillator and the detector allows the spread of the light over different channels and is necessary if the channel's sensitive area is bigger than the scintillator's area. The initial results demonstrate that this detector module is promising and could be used for applications requiring compact and high-resolution detectors. Experimental results show that the detectors precision increases using glass guide thickness of 1.35 mm and 1.85 mm; however the precision using 2.5 mm are practically the same as if using 0.8 mm or 1.0 mm glass guide thicknesses. In addition, simulations using Geant4 indicate that the light becomes scarcer if thicker glass is used, thus reducing the ability to indicate which crystal was targeted. When 2.5 mm glass thickness is used, the scarce

  2. Design and construction of a multi-layer CsI(Tl) telescope for high-energy reaction studies

    International Nuclear Information System (INIS)

    Yan, D.; Sun, Z.Y.; Yue, K.; Wang, S.T.; Zhang, X.H.; Yu, Y.H.; Chen, J.L.; Tang, S.W.; Fang, F.; Zhou, Y.; Sun, Y.; Wang, Z.M.; Sun, Y.Z.

    2017-01-01

    A prototype of a new CsI(Tl) telescope, which will be used in the reaction studies of light isotopes with energy of several hundred AMeV, was constructed and tested at the Institute of Modern Physics, Chinese Academy of Sciences. The telescope has a multi-layer structure, and the range information was obtained to improve the particle identification performance. This prototype has seven layers of different thickness. An energy resolution of 5.0% (FWHM) was obtained for one of the layers in a beam test experiment. Positive improvement for the identification of 14 O and 15 O isotopes was achieved using the range information.

  3. Design and construction of a multi-layer CsI(Tl) telescope for high-energy reaction studies

    Energy Technology Data Exchange (ETDEWEB)

    Yan, D.; Sun, Z.Y. [Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Yue, K., E-mail: yueke@impcas.ac.cn [Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Wang, S.T.; Zhang, X.H.; Yu, Y.H.; Chen, J.L.; Tang, S.W.; Fang, F. [Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Zhou, Y.; Sun, Y. [Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); University of Chinese Academy of Sciences, Beijing 100049 (China); Lanzhou University, Lanzhou 730000 (China); Wang, Z.M.; Sun, Y.Z. [Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); University of Chinese Academy of Sciences, Beijing 100049 (China)

    2017-01-21

    A prototype of a new CsI(Tl) telescope, which will be used in the reaction studies of light isotopes with energy of several hundred AMeV, was constructed and tested at the Institute of Modern Physics, Chinese Academy of Sciences. The telescope has a multi-layer structure, and the range information was obtained to improve the particle identification performance. This prototype has seven layers of different thickness. An energy resolution of 5.0% (FWHM) was obtained for one of the layers in a beam test experiment. Positive improvement for the identification of {sup 14}O and {sup 15}O isotopes was achieved using the range information.

  4. Depth-of-interaction measurement in a single-layer crystal array with a single-ended readout using digital silicon photomultiplier

    International Nuclear Information System (INIS)

    Lee, Min Sun; Lee, Jae Sung

    2015-01-01

    We present the first experimental evaluation of a depth-of-interaction (DOI) positron emission tomography (PET) detector using a digital silicon photomultiplier (dSiPM). To measure DOI information from a mono-layer array of scintillation crystals with a single-ended readout, our group has previously proposed and developed a new method based on light spread using triangular reflectors. Since this method relies on measurement of the light distribution, dSiPM, which has a fully digital interface, has several merits for our DOI measurement. The DOI PET detector comprised of a dSiPM sensor (DPC-3200-22-44) coupled with a 14   ×   14 array of 2 mm  ×  2 mm  ×  20 mm unpolished LGSO crystals. All crystals were covered with triangular reflectors. To obtain a good performance of the DOI PET detector, several parameters of detector were selected as a preliminary experiment. Detector performance was evaluated with the selected parameters and the optimal experimental setup, and a DOI measurement was conducted by irradiating the crystal block at five DOI positions spaced at intervals of 4 mm. Maximum-likelihood estimation was employed for DOI positioning and the optimal DOI estimation scheme was also investigated in this study. As a result, the DOI PET detector showed clear crystal identification. The energy resolution (full-width at half-maximum (FWHM)) averaged over all depths was 10.21%  ±  0.15% at 511 keV, and time resolution averaged over all depths was 1198.61   ±   39.70 ps FWHM. The average DOI positioning accuracy for all depths was 74.22%  ±  6.77%, which equates to DOI resolution of 4.67 mm. Energy and DOI resolutions were uniform over all crystal positions except for the back parts of the array. Furthermore, additional simulation studies were conducted to verify the results of our DOI measurement method that is combined with dSiPM technology. In conclusion, our continuous DOI PET detector

  5. Three-dimensional imaging through turbid media based on polarization-difference liquid-crystal microlens array

    Science.gov (United States)

    Xin, Zhaowei; Wei, Dong; Li, Dapeng; Xie, Xingwang; Chen, Mingce; Zhang, Xinyu; Wang, Haiwei; Xie, Changsheng

    2018-02-01

    In this paper, a polarization difference liquid-crystal microlens array (PD-LCMLA) for three dimensional imaging application through turbid media is fabricated and demonstrated. This device is composed of a twisted nematic liquidcrystal cell (TNLCC), a polarizer and a liquid-crystal microlens array. The polarizer is sandwiched between the TNLCC and LCMLA to help the polarization difference system achieving the orthogonal polarization raw images. The prototyped camera for polarization difference imaging has been constructed by integrating the PD-LCMLA with an image sensor. The orthogonally polarized light-field images are recorded by switching the working state of the TNLCC. Here, by using a special microstructure in conjunction with the polarization-difference algorithm, we demonstrate that the three-dimensional information in the scattering media can be retrieved from the polarization-difference imaging system with an electrically tunable PD-LCMLA. We further investigate the system's potential function based on the flexible microstructure. The microstructure provides a wide operation range in the manipulation of incident beams and also emerges multiple operation modes for imaging applications, such as conventional planar imaging, polarization imaging mode, and polarization-difference imaging mode. Since the PD-LCMLA demonstrates a very low power consumption, multiple imaging modes and simple manufacturing, this kind of device presents a potential to be used in many other optical and electro-optical systems.

  6. High sensitive photonic crystal multiplexed biosensor array using H0 sandwiched cavities

    Directory of Open Access Journals (Sweden)

    Arafa Safia

    2017-01-01

    Full Text Available We theoretically investigate a high sensitive photonic crystal integrated biosensor array structure which is potentially used for label-free multiplexed sensing. The proposed device consists of an array of three sandwiched H0 cavities patterned above silicon on insulator (SOI substrate; each cavity has been designed for different cavity spacing and different resonant wavelength. Results obtained by performing finite-difference time-domain (FDTD simulations, indicate that the response of each detection unit shifts independently in terms of refractive index variations. The optimized design makes possible the combination of sensing as a function of location, as well as a function of time in the same platform. A refractive index sensitivity of 520nm/RIU and a quality factor over 104 are both achieved with an accompanied crosstalk of less than -26 dB. In addition, the device presents an improved detection limit (DL of 1.24.10-6 RIU and a wide measurement range. These features make the designed device a promising element for performing label-free multiplexed detection in monolithic substrate for medical diagnostics and environmental monitoring.

  7. A flexible liquid crystal polymer MEMS pressure sensor array for fish-like underwater sensing

    International Nuclear Information System (INIS)

    Kottapalli, A G P; Asadnia, M; Miao, J M; Barbastathis, G; Triantafyllou, M S

    2012-01-01

    In order to perform underwater surveillance, autonomous underwater vehicles (AUVs) require flexible, light-weight, reliable and robust sensing systems that are capable of flow sensing and detecting underwater objects. Underwater animals like fish perform a similar task using an efficient and ubiquitous sensory system called a lateral-line constituting of an array of pressure-gradient sensors. We demonstrate here the development of arrays of polymer microelectromechanical systems (MEMS) pressure sensors which are flexible and can be readily mounted on curved surfaces of AUV bodies. An array of ten sensors with a footprint of 60 (L) mm × 25 (W) mm × 0.4 (H) mm is fabricated using liquid crystal polymer (LCP) as the sensing membrane material. The flow sensing and object detection capabilities of the array are illustrated with proof-of-concept experiments conducted in a water tunnel. The sensors demonstrate a pressure sensitivity of 14.3 μV Pa −1 . A high resolution of 25 mm s −1 is achieved in water flow sensing. The sensors can passively sense underwater objects by transducing the pressure variations generated underwater by the movement of objects. The experimental results demonstrate the array’s ability to detect the velocity of underwater objects towed past by with high accuracy, and an average error of only 2.5%. (paper)

  8. A new spectroscopic imager for X-rays from 0.5 keV to 150 keV combining a pnCCD and a columnar CsI(Tl) scintillator

    Science.gov (United States)

    Schlosser, D. M.; Hartmann, R.; Kalok, D.; Bechteler, A.; Abboud, A.; Shokr, M.; Çonka, T.; Pietsch, U.; Strüder, L.

    2017-04-01

    By combining a low noise fully depleted pnCCD detector with a columnar CsI(Tl) scintillator an energy dispersive spatial resolving detector can be realized with a high quantum efficiency in the range from below 0.5 keV to above 150 keV. The used scintillator system increases the pulse height of gamma-rays converted in the CsI(Tl), due to focusing properties of the columnar scintillator structure by reducing the event size in indirect detection mode (conversion in the scintillator). In case of direct detection (conversion in the silicon of the pnCCD) the relative energy resolution is 0.7% at 122 keV (FWHM = 850 eV) and the spatial resolution is less than 75 μm. In case of indirect detection the relative energy resolution, integrated over all event sizes is about 9% at 122 keV with an expected spatial precision of below 75 μm.

  9. Factors which define the α/γ ratio in CsI:Tl crystals

    International Nuclear Information System (INIS)

    Kudin, Alexander M.; Sysoeva, Elena P.; Sysoeva, Elena V.; Trefilova, Larisa N.; Zosim, Dmitry I.

    2005-01-01

    Dependences of light yield and α/γ ratio on the Tl concentration have been studied within a wide range of shaping times. It is shown that the α/γ ratio essentially depends on the Tl concentration. Proper combination of the Tl concentration and optimum shaping time in electronics allows to obtain detectors with rather high light output for γ-rays, α-particles and α/γ ratio values. It has been shown that both the light yield at α-excitation and the α/γ-ratio depend on the time of crystal storage after polishing. On the basis of the idea of the formation of deformation-induced point defects in a thin surface-adjacent layer, the causes of the temporary increasing in light yield for α-particle are explained. An explanation is given of the results obtained by Gwin and Murray concerning the fact that the α/γ ratio is practically independent on Tl concentration

  10. Strong photonic crystal behavior in regular arrays of core-shell and quantum disc InGaN/GaN nanorod light-emitting diodes

    Energy Technology Data Exchange (ETDEWEB)

    Lewins, C. J., E-mail: c.j.lewins@bath.ac.uk; Le Boulbar, E. D.; Lis, S. M.; Shields, P. A.; Allsopp, D. W. E., E-mail: d.allsopp@bath.ac.uk [Department of Electronic and Electrical Engineering, University of Bath, Claverton Down, Bath BA2 7AY (United Kingdom); Edwards, P. R.; Martin, R. W. [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom)

    2014-07-28

    We show that arrays of emissive nanorod structures can exhibit strong photonic crystal behavior, via observations of the far-field luminescence from core-shell and quantum disc InGaN/GaN nanorods. The conditions needed for the formation of directional Bloch modes characteristic of strong photonic behavior are found to depend critically upon the vertical shape of the nanorod sidewalls. Index guiding by a region of lower volume-averaged refractive index near the base of the nanorods creates a quasi-suspended photonic crystal slab at the top of the nanorods which supports Bloch modes. Only diffractive behavior could be observed without this region. Slab waveguide modelling of the vertical structure shows that the behavioral regime of the emissive nanorod arrays depends strongly upon the optical coupling between the nanorod region and the planar layers below. The controlled crossover between the two regimes of photonic crystal operation enables the design of photonic nanorod structures formed on planar substrates that exploit either behavior depending on device requirements.

  11. Scintillation crystal mounting apparatus

    International Nuclear Information System (INIS)

    Engdahl, L.W.; Deans, A.J.

    1982-01-01

    An improved detector head for a gamma camera is disclosed. The detector head includes a housing and a detector assembly mounted within the housing. Components of the detector assembly include a crystal sub-assembly, a phototube array, and a light pipe between the phototube array and crystal sub-assembly. The invention provides a unique structure for maintaining the phototubes in optical relationship with the light pipe and preventing the application of forces that would cause the camera's crystal to crack

  12. Electrically pumped all photonic crystal 2nd order DFB lasers arrays emitting at 2.3 μm

    Directory of Open Access Journals (Sweden)

    B. Adelin

    2017-03-01

    Full Text Available Single-mode, widely tunable laser diodes in the mid-infrared range are highly interesting for demanding spectroscopic applications involving multi-species discrimination. We report on an alternative approach using single frequency laser arrays. Single-mode laser arrays were fabricated using all-photonic-crystal electrically pumped distributed feedback cavities on GaSb. The fabricated lasers exhibit thresholds in the 3.2 kA/cm2 range in a continuous wave regime at room temperature. The maximum output power reaches 1 mW and single mode operation with a side-mode suppression ratio of 30 dB is demonstrated. These lasers were used to perform tunable diode laser absorption spectroscopy of several gases in standard gas cells. Continuous spectral coverage of a 40 nm band using 10 lasers seems an achievable goal using laser arrays with PhC lattice constant variations of 1 nm from laser to laser.

  13. A novel gamma-ray detector with submillimeter resolutions using a monolithic MPPC array with pixelized Ce:LYSO and Ce:GGAG crystals

    Energy Technology Data Exchange (ETDEWEB)

    Kato, T., E-mail: katou.frme.8180@asagi.waseda.jp [Research Institute for Science and Engineering, Waseda University, 3-4-1, Ohkubo, Shinjuku, Tokyo (Japan); Kataoka, J.; Nakamori, T.; Miura, T.; Matsuda, H.; Kishimoto, A. [Research Institute for Science and Engineering, Waseda University, 3-4-1, Ohkubo, Shinjuku, Tokyo (Japan); Sato, K.; Ishikawa, Y.; Yamamura, K.; Nakamura, S.; Kawabata, N. [Solid State Division, Hamamatsu Photonics K. K., 1126-1, Ichino-cho, Hamamatsu, Shizuoka (Japan); Ikeda, H. [ISAS/JAXA, 3-1-1, Yoshinodai, Chuo-ku, Sagamihara-shi, Kanagawa (Japan); Yamamoto, S. [Kobe City College of Technology, 8-3, Gakuenhigashimati, Nishi-ku, Kobe-shi, Hyougo 651-2194 (Japan); Kamada, K. [Materials Research Laboratory, Furukawa Co., Ltd., 1-25-13, Kannondai, Tsukuba, Ibaraki 305-0856 (Japan)

    2013-01-21

    We have developed a large-area monolithic Multi-Pixel Photon Counter (MPPC) array consisting of 4×4 channels with a three-side buttable package. Each channel has a photosensitive area of 3×3 mm{sup 2} and 3600 Geiger mode avalanche photodiodes (APDs). For typical operational gain of 7.5×10{sup 5} at +20 °C, gain fluctuation over the entire MPPC device is only ±5.6%, and dark count rates (as measured at the 1 p.e. level) amount to ≤400kcps per channel. We first fabricated a gamma-ray camera consisting of the MPPC array with one-to-one coupling to a Ce-doped (Lu,Y){sub 2}(SiO{sub 4})O (Ce:LYSO) crystal array (4×4 array of 3×3×10 mm{sup 3} crystals). Energy and time resolutions of 11.5±0.5% (FWHM at 662 keV) and 493±22ps were obtained, respectively. When using the charge division resistor network, which compiles signals into four position-encoded analog outputs, the ultimate positional resolution is estimated as 0.19 mm in both X and Y directions, while energy resolution of 10.2±0.4% (FWHM) was obtained. Finally, we fabricated submillimeter Ce:LYSO and Ce-doped Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12} (Ce:GGAG) scintillator matrices each consisting of 1.0×1.0, 0.7×0.7 and 0.5×0.5 mm{sup 2} pixels, to further improve the spatial resolution. In all types of Ce:LYSO and Ce:GGAG matrices, each crystal was clearly resolved in the position histograms when irradiated by a {sup 137}Cs source. The energy resolutions for 662 keV gamma-rays for each Ce:LYSO and Ce:GGAG scintillator matrix were ≤14.3%. These results suggest excellent potential for its use as a high spatial medical imaging device, particularly in positron emission tomography (PET). -- Highlights: ► We developed a newly designed large-area monolithic MPPC array. ► We obtained fine gain uniformity, and good energy and time resolutions when coupled to the LYSO scintillator. ► We fabricated gamma-ray camera consisting of the MPPC array and submillimeter pixelized LYSO and GGAG scintillators. ► In

  14. Detector-counter scintillator with data acquisition system for industrial processes control

    International Nuclear Information System (INIS)

    Costa, Fabio Eduardo da; Hamada, Margarida Mizue; mmhamada@net@ipen.br

    2000-01-01

    Detectors using silicon photodiodes coupled to CsI(Tl) crystals are a technically feasible option for portable detection systems for ionizing radiation. The photodiodes are advantageous because they are not sensitive to magnetic fields, may be operated by low bias and their efficiency spectrum has a good match with the CsI(Tl) crystals spectrum. With this technology, a two channel detection system was developed, associated to a laptop or notebook computer. This system constitutes an autonomous unit to count radioactive, in real time, at two sites, which may be up to 60 meters far from each other. (author)

  15. A SiPM-based isotropic-3D PET detector X'tal cube with a three-dimensional array of 1 mm{sup 3} crystals

    Energy Technology Data Exchange (ETDEWEB)

    Yamaya, Taiga; Mitsuhashi, Takayuki; Inadama, Naoko; Nishikido, Fumihiko; Yoshida, Eiji; Murayama, Hideo [Molecular Imaging Center, National Institute of Radiological Sciences, 4-9-1 Anagawa, Inage-ku, Chiba 263-8555 (Japan); Matsumoto, Takahiro; Kawai, Hideyuki; Suga, Mikio [Chiba University, 1-33 Yayoicho, Inage-ku, Chiba 263-8522 (Japan); Watanabe, Mitsuo, E-mail: taiga@nirs.go.jp [Central Research Laboratory, Hamamatsu Photonics K.K., 5000 Hirakuchi, Hamakita-ku, Hamamatsu 434-8601 (Japan)

    2011-11-07

    We are developing a novel, general purpose isotropic-3D PET detector X'tal cube which has high spatial resolution in all three dimensions. The research challenge for this detector is implementing effective detection of scintillation photons by covering six faces of a segmented crystal block with silicon photomultipliers (SiPMs). In this paper, we developed the second prototype of the X'tal cube for a proof-of-concept. We aimed at realizing an ultimate detector with 1.0 mm{sup 3} cubic crystals, in contrast to our previous development using 3.0 mm{sup 3} cubic crystals. The crystal block was composed of a 16 x 16 x 16 array of lutetium gadolinium oxyorthosilicate (LGSO) crystals 0.993 x 0.993 x 0.993 mm{sup 3} in size. The crystals were optically glued together without inserting any reflector inside and 96 multi-pixel photon counters (MPPCs, S10931-50P, i.e. six faces each with a 4 x 4 array of MPPCs), each having a sensitive area of 3.0 x 3.0 mm{sup 2}, were optically coupled to the surfaces of the crystal block. Almost all 4096 crystals were identified through Anger-type calculation due to the finely adjusted reflector sheets inserted between the crystal block and light guides. The reflector sheets, which formed a belt of 0.5 mm width, were placed to cover half of the crystals of the second rows from the edges in order to improve identification performance of the crystals near the edges. Energy resolution of 12.7% was obtained at 511 keV with almost uniform light output for all crystal segments thanks to the effective detection of the scintillation photons.

  16. Development of an application specific scintimammography detector based on a crystal scintillator array and a PSPMT

    CERN Document Server

    Majewski, S; Goode, A; Kross, B J; Steinbach, D; Weisenberger, A; Williams, M; Wojci, R

    1998-01-01

    We report the results of studies conducted with small field of view scintimammography camera based on a position-sensitive photomultiplier tube (5'' Hamamatsu R3292) and several pixelized crystal scintillator arrays made of YAP, CsI(Na) and NaI(Tl) scintillators. Laboratory tests and pre-clinical phantom studies were conducted to compare and optimize the performances of the prototypes with special emphasis on spatial resolution (approx 2-3mm) and sufficient energy resolution for scatter rejection.

  17. Liquid-crystal microlens array with swing and adjusting focus and constructed by dual patterned ITO-electrodes

    Science.gov (United States)

    Dai, Wanwan; Xie, Xingwang; Li, Dapeng; Han, Xinjie; Liu, Zhonglun; Wei, Dong; Xin, Zhaowei; Zhang, Xinyu; Wang, Haiwei; Xie, Changsheng

    2018-02-01

    Under the condition of existing intense turbulence, the object's wavefront may be severely distorted. So, the wavefront sensors based on the traditional microlens array (MLA) with a fixed focal length can not be used to measure the wavefront effectively. In order to obtain a larger measurement range and higher measurement accuracy, we propose a liquid-crystal microlens array (LCMLA) with needed ability of swing focus over the focal plane and further adjusting focal length, which is constructed by a dual patterned ITO electrodes. The main structure of the LCMLA is divided into two layers, which are made of glass substrate with ITO transparent electrodes. The top layer of each liquid-crystal microlens consists of four rectangular electrodes, and the bottom layer is a circular electrode. In common optical measurements performed, the operations are carried out such as adding the same signal voltage over four electrodes of each microlens to adjust the focal length of the lens cell and adding a signal voltage with different RMS amplitude to adjust the focus position on the focal plane. Experiments show that the LCMLA developed by us demonstrate a desired focal length adjustable function and dynamic swing ability, so as to indicate that the method can be used not only to measure wavefront but also correct the wavefront with strong distortion.

  18. Cosmic ray effect on the X-ray Trigger Telescope of UFFO/Lomonosov using YSO scintillation crystal array in space

    DEFF Research Database (Denmark)

    Kim, M. B.; Jeong, S.; Jeong, H. M.

    2017-01-01

    UFFO Burst Alert and Trigger telescope (UBAT) is the X-ray trigger telescope of UFFO/Lomonosov to localize X-ray source with coded mask method and X-ray detector. Its X-ray detector is made up of 36 8×8 pixels Yttrium OxyorthoSilicate (Y2SiO5:Ce, YSO) scintillation crystal arrays and 36 64-channe...

  19. Improvement on the light yield of a high-Z inorganic scintillator GSO(Ce)

    CERN Document Server

    Kamae, T; Isobe, N; Kokubun, M; Kubota, A; Osone, S; Takahashi, T; Tsuchida, N; Ishibashi, H

    2002-01-01

    Cerium-doped gadolinium silicic dioxide crystal, GSO(Ce), is a high-Z non-hydroscopic scintillator that gives higher light yield than BGO, and can potentially replace NaI(Tl), CsI(Tl) and BGO in many applications. Its production cost, however, has been substantially higher than any of them, while its energy resolution has been worse than that of NaI(Tl) or CsI(Tl). The merit did not overcome these deficiencies except in limited applications. We developed a low background phoswich counter (the well-type phoswich counter) for the Hard X-ray Detector of the Astro-E project based on GSO scintillator. In the developmental work, we have succeeded in improving the light yield of GSO(Ce) by 40-50%. For energies above 500 keV, a large GSO(Ce) crystal (4.5 cmx4.5phi cm) now gives energy resolution comparable to or better than the best NaI(Tl) when read out with a phototube. With a small GSO(Ce) crystal (5x5x5 mm sup 3) and a photodiode, an energy resolution comparable to or better than the best CsI(Tl) has been obtaine...

  20. The control of the growth orientations of electrodeposited single-crystal nanowire arrays: a case study for hexagonal CdS

    Energy Technology Data Exchange (ETDEWEB)

    Sun Hongyu; Li Xiaohong; Chen Yan; Li Wei; Zhang Xiangyi [State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, 066004 Qinhuangdao (China); Li Feng; Liu Baoting [College of Physics Science and Technology, Hebei University, 071002 Baoding (China)], E-mail: xyzh66@ysu.edu.cn

    2008-06-04

    The controllable growth of highly aligned and ordered semiconductor nanowire arrays is crucial for their potential applications in nanodevices. In the present study, both the growth orientation and the microstructure of hexagonal CdS nanowire arrays electrodeposited in a porous alumina template with 40 nm diameter pores have been controlled by simply tuning the deposition current density. An extremely low current density of 0.05 mA cm{sup -2} is favorable for the growth of single-crystal CdS nanowires along the normal direction of the intrinsic low-surface-energy (103) face. This can be understood well by a modified critical dimension model given in the present work.

  1. The control of the growth orientations of electrodeposited single-crystal nanowire arrays: a case study for hexagonal CdS

    International Nuclear Information System (INIS)

    Sun Hongyu; Li Xiaohong; Chen Yan; Li Wei; Zhang Xiangyi; Li Feng; Liu Baoting

    2008-01-01

    The controllable growth of highly aligned and ordered semiconductor nanowire arrays is crucial for their potential applications in nanodevices. In the present study, both the growth orientation and the microstructure of hexagonal CdS nanowire arrays electrodeposited in a porous alumina template with 40 nm diameter pores have been controlled by simply tuning the deposition current density. An extremely low current density of 0.05 mA cm -2 is favorable for the growth of single-crystal CdS nanowires along the normal direction of the intrinsic low-surface-energy (103) face. This can be understood well by a modified critical dimension model given in the present work

  2. Laser direct-write and crystallization of FeSi II micro-dot array for NIR light-emitting device application

    Science.gov (United States)

    Narazaki, Aiko; Kurosaki, Ryozo; Sato, Tadatake; Kawaguchi, Yoshizo; Niino, Hiroyuki

    2007-02-01

    We printed FeSi II micro-dot array on various kinds of substrates utilizing laser-induced forward transfer (LIFT). An amorphous FeSi II was deposited by sputtering on a transparent plate as a source film. A single KrF excimer laser pulse through a mask-projection system was imaged with a small micrometer-sized grid pattern onto a film/plate interface, resulting in the deposition of FeSi II micro-dot array on a facing substrate with a high number density of 10 4 mm -2. FeSi II in the β crystalline phase is a promising eco-friendly semiconductor because of NIR electroluminescence used for optical networking as well as abundant components reserve on the earth and non-toxicity. However, the β-FeSi II film fabrication generally required high-temperature multi-processes which hamper its integration and performance reproducibility. Using the LIFT of micro-dot array, we succeeded in room-temperature preparation of β-FeSi II. Micro-Raman spectroscopy confirmed the β crystalline phase in the micro-dots deposited on an unheated silica glass substrate. Thus, the LIFT is useful for integrating functional micro-dot array accompanied by the crystallization at lower temperatures.

  3. Ultra compact spectrometer apparatus and method using photonic crystals

    Science.gov (United States)

    Ting, David Z. (Inventor); Hill, Cory J. (Inventor); Bandara, Sumith V. (Inventor); Gunapala, Sarath D. (Inventor)

    2009-01-01

    The present invention is directed to methods of photonic crystal formation, and to methods and apparatus for using such photonic crystals, particularly in conjunction with detector arrays. Photonic crystal parameters and detector array parameters are compared to optimize the selection and orientation of a photonic crystal shape. A photonic crystal is operatively positioned relative to a plurality of light sensors. The light sensors can be separated by a pitch distance and positioned within one half of the pitch distance of an exit surface of the photonic crystals.

  4. Recent progress in the development of CsI(Tl) crystal-Si-photodiode spectrometric detection assemblies

    International Nuclear Information System (INIS)

    Semynozhenko, V.P.; Grinyov, B.V.; Nekrasov, V.V.; Borodenko, Yu.A.

    2005-01-01

    Highly sensitive spectrometric γ-detection assemblies are developed using a comprehensive approach (optimization of crystal growth conditions as well as of treatment and packing of scintillators, creation of low-noise charge-sensitive preamplifiers and shapers). The detection assemblies with CsI(Tl)≤100 cm 3 have a sensitivity of about 20 pulse/s(mcR/h), their energy resolution with respect to 137 Cs γ-line being ≤8.5%. The assemblies with lesser scintillator volumes (1-5 cm 3 ) provide a resolution lower than 6% with respect to 137 Cs and ≤40% with respect to 241 Am

  5. The X'tal cube PET detector with a monolithic crystal processed by the 3D sub-surface laser engraving technique: Performance comparison with glued crystal elements

    Energy Technology Data Exchange (ETDEWEB)

    Yoshida, Eiji, E-mail: rush@nirs.go.jp [Molecular Imaging Center, National Institute of Radiological Sciences, 4-9-1 Anagawa, Inage-ku, Chiba 263-8555 (Japan); Hirano, Yoshiyuki; Tashima, Hideaki; Inadama, Naoko; Nishikido, Fumihiko [Molecular Imaging Center, National Institute of Radiological Sciences, 4-9-1 Anagawa, Inage-ku, Chiba 263-8555 (Japan); Moriya, Takahiro; Omura, Tomohide; Watanabe, Mitsuo [Hamamatsu Photonics K.K., 5000 Hirakuchi, Hamakita-ku, Hamamatsu, Shizuoka 434-8601 (Japan); Murayama, Hideo; Yamaya, Taiga [Molecular Imaging Center, National Institute of Radiological Sciences, 4-9-1 Anagawa, Inage-ku, Chiba 263-8555 (Japan)

    2013-09-21

    The X'tal cube is a depth-of-interaction (DOI)-PET detector which is aimed at obtaining isotropic resolution by effective readout of scintillation photons from six sides of the crystal block. The X'tal cube is composed of a 3D crystal block with isotropic segments. Each face of the 3D crystal block is covered with a 4×4 array of multi-pixel photon counters (MPPCs). Previously, in order to fabricate the 3D crystal block efficiently and precisely, we applied a sub-surface laser engraving technique to a monolithic crystal block instead of gluing segmented small crystals. A dense arrangement of multiple micro-cracks carved by the laser beam works efficiently as a scattering wall for the scintillation photons. The X'tal cube with the laser-processed block showed excellent performance with respect to crystal identification and energy resolution. In this work, for characteristics comparison between the laser-processed block and the conventional segmented array block, we made the laser-processed block and two types of segmented array blocks, one with air gaps and the other with glued segmented small crystals. All crystal blocks had 3D grids of 2 mm pitch. The 4×4 MPPC arrays were optically coupled to each surface of the crystal block. When performance was evaluated using a uniform irradiation of 511 keV, we found that the X'tal cubes with the laser-processed block could easily achieve 2 mm{sup 3} uniform crystal identification. Also, the average energy resolution of each 3D grid was 11.1±0.7%. On the other hand, the glued segmented array block had a pinched distribution and crystals could not be separated clearly. The segmented array block with air gaps had satisfactory crystal identification performance; however, the laser-processed block had higher crystal identification performance. Also, the energy resolution of the laser-processed block was better than for the segmented array blocks. In summary, we found the laser-processed X'tal cube had

  6. Construction of a test stand for the measurement of the light output uniformity of CALIFA crystals

    Energy Technology Data Exchange (ETDEWEB)

    Susenburger, Markus; Ignatov, Alexander; Kroell, Thorsten [Technische Universitaet Darmstadt, Darmstadt (Germany)

    2016-07-01

    Currently, the Facility for Antiproton and Ion Research (FAIR) at GSI in Darmstadt is under construction. One experiment at GSI and FAIR is called Reactions with Relativistic Radioactive Beams (R{sup 3}B). A key component of the R{sup 3}B is the CALorimeter for In Flight detection of γ-rays and light charged pArticles (CALIFA), which will surround the R{sup 3}B target chamber and will be capable of the detection of γ-rays in a wide energy range from 100 keV to 30 MeV as well as of light charged particles. CALIFA is built out of two parts, the so called CALIFA barrel and CALIFA endcap. The barrel consists of 1952 CsI(Tl) detector crystals which have to fulfill several specifications. One of these specifications is the uniformity of the light output. Depending on the location of the deposited energy, the crystal's light output varies due to optical focusing effects. This behavior can be manipulated by lapping the crystal's surface. The aim of this work is the development of a test stand which will check if the crystals match the requirements according to the light output uniformity. Because of the large number of crystals needed to be tested, the stand automates the test procedure, which guarantees comparable test measurement for all crystals. The development and construction of this stand is reported.

  7. Proceedings of the Flat-Plate Solar Array Project Workshop on Crystal Gowth for High-Efficiency Silicon Solar Cells

    Science.gov (United States)

    Dumas, K. A. (Editor)

    1985-01-01

    A Workshop on Crystal Growth for High-Efficiency Silicon Solar Cells was held December 3 and 4, 1984, in San Diego, California. The Workshop offered a day and a half of technical presentations and discussions and an afternoon session that involved a panel discussion and general discussion of areas of research that are necessary to the development of materials for high-efficiency solar cells. Topics included the theoretical and experimental aspects of growing high-quality silicon crystals, the effects of growth-process-related defects on photovoltaic devices, and the suitability of various growth technologies as cost-effective processes. Fifteen invited papers were presented, with a discussion period following each presentation. The meeting was organized by the Flat-Plate Solar Array Project of the Jet Propulsion Laboratory. These Proceedings are a record of the presentations and discussions, edited for clarity and continuity.

  8. High Performance Relaxor-Based Ferroelectric Single Crystals for Ultrasonic Transducer Applications

    Directory of Open Access Journals (Sweden)

    Yan Chen

    2014-07-01

    Full Text Available Relaxor-based ferroelectric single crystals Pb(Mg1/3Nb2/3O3-PbTiO3 (PMN-PT have drawn much attention in the ferroelectric field because of their excellent piezoelectric properties and high electromechanical coupling coefficients (d33~2000 pC/N, kt~60% near the morphotropic phase boundary (MPB. Ternary Pb(In1/2Nb1/2O3-Pb(Mg1/3Nb2/3O3-PbTiO3 (PIN-PMN-PT single crystals also possess outstanding performance comparable with PMN-PT single crystals, but have higher phase transition temperatures (rhombohedral to tetragonal Trt, and tetragonal to cubic Tc and larger coercive field Ec. Therefore, these relaxor-based single crystals have been extensively employed for ultrasonic transducer applications. In this paper, an overview of our work and perspectives on using PMN-PT and PIN-PMN-PT single crystals for ultrasonic transducer applications is presented. Various types of single-element ultrasonic transducers, including endoscopic transducers, intravascular transducers, high-frequency and high-temperature transducers fabricated using the PMN-PT and PIN-PMN-PT crystals and their 2-2 and 1-3 composites are reported. Besides, the fabrication and characterization of the array transducers, such as phased array, cylindrical shaped linear array, high-temperature linear array, radial endoscopic array, and annular array, are also addressed.

  9. Miniature quartz crystal-resonator-based thermogravimetric detector.

    Science.gov (United States)

    Sai, N; Tagawa, Y; Sohgawa, M; Abe, T

    2014-09-01

    In this work, a new design for a microheater combined with a quartz crystal microbalance (QCM) array for thermogravimetric analysis is presented. Each QCM consists of two electrodes to excite thickness-shear-mode vibrations and one microheater to increase the temperature on the crystal backside. In addition, all the electrode pads are patterned on the crystal backside, making the design of the QCM compact and user-friendly. Finally, the proposed QCM array was employed to separate ethanol from methanol. This was successfully achieved via thermal desorption spectra calculated by differentiating the frequency changes.

  10. Development of a detector-counter for teaching purposes in nuclear instrumentation

    International Nuclear Information System (INIS)

    Costa, Fabio E. da; Hamada, Margarida M.; Pereira, Maria Conceicao C. Pereira; Mesquita, Carlos H.

    2000-01-01

    A detector system constituted of a monochannel analyzer with digital counter, amplifier, charge sensitive preamplifier and CsI(Tl) scintillator detector coupled to photodiode PIN was developed to gamma radiation detection. The crystal was grown by Bridgman Method. The crystal luminescence spectra has good match with the photodiode efficiency spectrum. The combination CsI(Tl)- photodiode made at possible to obtain a compact and rugged detector, insensitive to magnetic fields and may be operated at low voltages. This detector system has a baseline for 1 MeV and 2 MeV selected by the use, with two discriminators (inferior and superior) for advancements 10 or 20 KeV division. The system showed good energy linearity in the range from 122 to 1440 KeV. (author)

  11. The BaBar Light Pulser System

    Energy Technology Data Exchange (ETDEWEB)

    Clark, P

    2004-03-18

    The BABAR experiment and the PEP-II e{sup +}e{sup -} collider at SLAC in California started taking data in May 1999. The aim of the experiment is to study CP violation in the B meson system. A central part of the BABAR detector is the CsI(Tl) electromagnetic calorimeter. To make precision measurements with a calorimeter in a high luminosity environment requires that the crystals are well calibrated and continually monitored for radiation damage. However, this should not impact the total integrated luminosity. To achieve this goal a fiber-optic light pulser system was designed. The light sources chosen were xenon flash lamps. A novel light distribution method was developed using an array of graded index microlenses. Initial results from performance studies are presented.

  12. Tunable ultra-wideband terahertz filter based on three-dimensional arrays of H-shaped plasmonic crystals

    International Nuclear Information System (INIS)

    Yuan Cai; Xu Shi-Lin; Yao Jian-Quan; Zhao Xiao-Lei; Cao Xiao-Long; Wu Liang

    2014-01-01

    A face-to-face system of double-layer three-dimensional arrays of H-shaped plasmonic crystals is proposed, and its transmission and filtering properties are investigated in the terahertz regime. Simulation results show that our design has excellent filtering properties. It has an ultra-wide bandgap and passband with steep band-edges, and the transmittance of the passband and the forbidden band are very close to 1 and 0, respectively. As the distance between the two face-to-face plates increases, the resonance frequency exhibits a gradual blueshift from 0.88 THz to 1.30 THz. Therefore, we can dynamically control the bandwidths of bandgap and passband by adding a piezoelectric ceramic plate between the two crystal plates. Furthermore, the dispersion relations of modes and electric field distributions are presented to analyze the generation mechanisms of bandgaps and to explain the location of bandgaps and the frequency shift phenomenon. Due to the fact that our design can provide many resonant modes, the bandwidth of the bandgaps can be greatly broadened. This paper can serve as a valuable reference for the design of terahertz functional devices and three-dimensional terahertz metamaterials. (interdisciplinary physics and related areas of science and technology)

  13. Understanding internal backgrounds in NaI(Tl) crystals toward a 200 kg array for the KIMS-NaI experiment

    Energy Technology Data Exchange (ETDEWEB)

    Adhikari, P.; Adhikari, G.; Oh, S.Y. [Sejong University, Department of Physics, Seoul (Korea, Republic of); Choi, S.; Joo, H.W.; Kim, K.W.; Kim, S.K. [Seoul National University, Department of Physics and Astronomy, Seoul (Korea, Republic of); Ha, C.; Jeon, E.J.; Kang, W.G.; Kim, H.O.; Kim, N.Y.; Lee, H.S.; Lee, J.H.; Lee, M.H.; Leonard, D.S.; Li, J.; Olsen, S.L.; Park, H.K.; Park, K.S.; So, J.H.; Yoon, Y.S. [Institute for Basic Science, Center for Underground Physics, Daejeon (Korea, Republic of); Hahn, I.S. [Ewha Womans University, Department of Science Education, Seoul (Korea, Republic of); Kim, H.J. [Kyungpook National University, Department of Physics, Daegu (Korea, Republic of); Kim, Y.D. [Sejong University, Department of Physics, Seoul (Korea, Republic of); Institute for Basic Science, Center for Underground Physics, Daejeon (Korea, Republic of); Kim, Y.H. [Institute for Basic Science, Center for Underground Physics, Daejeon (Korea, Republic of); Korea Research Institute of Standards and Science, Daejeon (Korea, Republic of); Park, H.S. [Korea Research Institute of Standards and Science, Daejeon (Korea, Republic of)

    2016-04-15

    The Korea Invisible Mass Search (KIMS) collaboration has developed low-background NaI(Tl) crystals that are suitable for the direct detection of WIMP dark matter. Building on experience accumulated during the KIMS-CsI programs, the KIMS-NaI experiment will consist of a 200 kg NaI(Tl) crystal array surrounded by layers of shielding structures and will be operated at the Yangyang underground laboratory. The goal is to provide an unambiguous test of the DAMA/LIBRA annual modulation signature. Measurements of six prototype crystals show progress in the reduction of internal contamination from radioisotopes. Based on our understanding of these measurements, we expect to achieve a background level in the final detector configuration that is less than 1 count/day/keV/kg for recoil energies around 2 keV. The annual modulation sensitivity for the KIMS-NaI experiment shows that an unambiguous 7σ test of the DAMA/LIBRA signature would be possible with a 600 kg year exposure with this system. (orig.)

  14. Graphene-based photonic crystal

    International Nuclear Information System (INIS)

    Berman, Oleg L.; Boyko, Vladimir S.; Kezerashvili, Roman Ya.; Kolesnikov, Anton A.; Lozovik, Yurii E.

    2010-01-01

    A novel type of photonic crystal formed by embedding a periodic array of constituent stacks of alternating graphene and dielectric discs into a background dielectric medium is proposed. The photonic band structure and transmittance of such photonic crystal are calculated. The graphene-based photonic crystals can be used effectively as the frequency filters and waveguides for the far infrared region of electromagnetic spectrum. Due to substantial suppression of absorption of low-frequency radiation in doped graphene the damping and skin effect in the photonic crystal are also suppressed. The advantages of the graphene-based photonic crystal are discussed.

  15. In-phased second harmonic wave array generation with intra-Talbot-cavity frequency-doubling.

    Science.gov (United States)

    Hirosawa, Kenichi; Shohda, Fumio; Yanagisawa, Takayuki; Kannari, Fumihiko

    2015-03-23

    The Talbot cavity is one promising method to synchronize the phase of a laser array. However, it does not achieve the lowest array mode with the same phase but the highest array mode with the anti-phase between every two adjacent lasers, which is called out-phase locking. Consequently, their far-field images exhibit 2-peak profiles. We propose intra-Talbot-cavity frequency-doubling. By placing a nonlinear crystal in a Talbot cavity, the Talbot cavity generates an out-phased fundamental wave array, which is converted into an in-phase-locked second harmonic wave array at the nonlinear crystal. We demonstrate numerical calculations and experiments on intra-Talbot-cavity frequency-doubling and obtain an in-phase-locked second harmonic wave array for a Nd:YVO₄ array laser.

  16. Enhancement in photo-electrochemical efficiency by reducing recombination rate in branched TiO2 nanotube array on functionalizing with ZnO micro crystals

    Science.gov (United States)

    Boda, Muzaffar Ahmad; Ashraf Shah, Mohammad

    2018-06-01

    In this study, branched TiO2 nanotube array were fabricated through electrochemical anodization process at constant voltage using third generation electrolyte. On account of morphological advantage, these nanotubes shows significant enhancement in photo-electrochemical property than compact or conventional titania nanotube array. However, their photo-electrochemical efficiency intensifies on coating with ZnO micro-crystals. ZnO coated branched TiO2 nanotube array shows a photocurrent density of 27.8 mA cm‑2 which is 1.55 times the photocurrent density (17.2 mA cm‑2) shown by bare branched titania nanotubes. The significant enhancement in photocurrent density shown by the resulting ZnO/TiO2 hybrid structure is attributed to suppression in electron–hole recombination phenomenon by offering smooth pathway to photo generated excitons on account of staggered band edge positions in individual semiconductors.

  17. A LSO scintillator array for a PET detector module with depth of interaction measurement

    International Nuclear Information System (INIS)

    Huber, J.S.; Moses, W.W.; Andreaco, M.S.; Petterson, O.

    2000-01-01

    We present construction methods and performance results for a production scintillator array of 64 optically isolated, 3 mm x 3 mm x 30 mm sized LSO crystals. This scintillator array has been developed for a PET detector module consisting of the 8x8 LSO array coupled on one end to a single photomultiplier tube (PMT) and on the opposite end to a 64 pixel array of silicon photodiodes (PD). The PMT provides an accurate timing pulse and initial energy discrimination, the PD identifies the crystal of interaction, the sum provides a total energy signal, and the PD/(PD+PMT) ratio determines the depth of interaction (DOI). Unlike the previous LSO array prototypes, we now glue Lumirror reflector material directly onto 4 sides of each crystal to obtain an easily manufactured, mechanically rugged array with our desired depth dependence. With 511 keV excitation, we obtain a total energy signal of 3600 electrons, pulse-height resolution of 25% fwhm, and 6-15 mm fwhm DOI resolution

  18. Seed-mediated growth of patterned graphene nanoribbon arrays

    Science.gov (United States)

    Arnold, Michael Scott; Way, Austin James; Jacobberger, Robert Michael

    2017-09-12

    Graphene nanoribbon arrays, methods of growing graphene nanoribbon arrays, and electronic and photonic devices incorporating the graphene nanoribbon arrays are provided. The graphene nanoribbons in the arrays are formed using a seed-mediated, bottom-up, chemical vapor deposition (CVD) technique in which the (001) facet of a semiconductor substrate and the orientation of the seed particles on the substrate are used to orient the graphene nanoribbon crystals preferentially along a single [110] direction of the substrate.

  19. Hanging drop crystal growth apparatus

    Science.gov (United States)

    Naumann, Robert J. (Inventor); Witherow, William K. (Inventor); Carter, Daniel C. (Inventor); Bugg, Charles E. (Inventor); Suddath, Fred L. (Inventor)

    1990-01-01

    This invention relates generally to control systems for controlling crystal growth, and more particularly to such a system which uses a beam of light refracted by the fluid in which crystals are growing to detect concentration of solutes in the liquid. In a hanging drop apparatus, a laser beam is directed onto drop which refracts the laser light into primary and secondary bows, respectively, which in turn fall upon linear diode detector arrays. As concentration of solutes in drop increases due to solvent removal, these bows move farther apart on the arrays, with the relative separation being detected by arrays and used by a computer to adjust solvent vapor transport from the drop. A forward scattering detector is used to detect crystal nucleation in drop, and a humidity detector is used, in one embodiment, to detect relative humidity in the enclosure wherein drop is suspended. The novelty of this invention lies in utilizing angular variance of light refracted from drop to infer, by a computer algorithm, concentration of solutes therein. Additional novelty is believed to lie in using a forward scattering detector to detect nucleating crystallites in drop.

  20. Applications of a pnCCD detector coupled to columnar structure CsI(Tl) scintillator system in ultra high energy X-ray Laue diffraction

    Science.gov (United States)

    Shokr, M.; Schlosser, D.; Abboud, A.; Algashi, A.; Tosson, A.; Conka, T.; Hartmann, R.; Klaus, M.; Genzel, C.; Strüder, L.; Pietsch, U.

    2017-12-01

    Most charge coupled devices (CCDs) are made of silicon (Si) with typical active layer thicknesses of several microns. In case of a pnCCD detector the sensitive Si thickness is 450 μm. However, for silicon based detectors the quantum efficiency for hard X-rays drops significantly for photon energies above 10 keV . This drawback can be overcome by combining a pixelated silicon-based detector system with a columnar scintillator. Here we report on the characterization of a low noise, fully depleted 128×128 pixels pnCCD detector with 75×75 μm2 pixel size coupled to a 700 μm thick columnar CsI(Tl) scintillator in the photon range between 1 keV to 130 keV . The excellent performance of the detection system in the hard X-ray range is demonstrated in a Laue type X-ray diffraction experiment performed at EDDI beamline of the BESSY II synchrotron taken at a set of several GaAs single crystals irradiated by white synchrotron radiation. With the columnar structure of the scintillator, the position resolution of the whole system reaches a value of less than one pixel. Using the presented detector system and considering the functional relation between indirect and direct photon events Laue diffraction peaks with X-ray energies up to 120 keV were efficiently detected. As one of possible applications of the combined CsI-pnCCD system we demonstrate that the accuracy of X-ray structure factors extracted from Laue diffraction peaks can be significantly improved in hard X-ray range using the combined CsI(Tl)-pnCCD system compared to a bare pnCCD.

  1. Surface modification of YIG by magnet array

    International Nuclear Information System (INIS)

    Atalay, S.; Kolat, V.S.; Bakır, H.G.; Izgi, T.; Kaya, A.O.; Kaya, O.A.; Gencer, H.

    2015-01-01

    Highlights: • The surface of YIG films were magnetically modulated by magnet array. • The surface modulated YIG films formed sharp band gaps. • A very small magnetic field change leads a large change in the peak value of band gap frequency. - Abstract: In this work, magnetostatic surface spin waves (MSSW) were propagated along the single crystal YIG (Y_3Fe_5O_1_2) film grown on GGG substrate. In order to obtain magnonic crystals, unlike the conventional methods, the surface of YIG films were magnetically modulated by magnet array in one and two-dimensions. The surface modulated YIG films formed sharp band gaps at approximately 6.55 GHz and 6.58 GHz at 1600 Oe magnetic field for one and two-dimensional magnonic crystals, respectively. It was found that a very small magnetic field change leads a large change in the peak value of band gap frequency.

  2. Surface modification of YIG by magnet array

    Energy Technology Data Exchange (ETDEWEB)

    Atalay, S., E-mail: satalay@inonu.edu.tr [Inonu University, Science and Art Faculty, Physics Department, 44280 Malatya (Turkey); Kolat, V.S. [Inonu University, Science and Art Faculty, Physics Department, 44280 Malatya (Turkey); Bakır, H.G. [Inonu University, Science and Art Faculty, Astronomy Department, 44280 Malatya (Turkey); Izgi, T.; Kaya, A.O. [Inonu University, Science and Art Faculty, Physics Department, 44280 Malatya (Turkey); Kaya, O.A. [Inonu University, Education Faculty, Computer Education and Educational Technology Department, 44280 Malatya (Turkey); Gencer, H. [Inonu University, Science and Art Faculty, Physics Department, 44280 Malatya (Turkey)

    2015-11-01

    Highlights: • The surface of YIG films were magnetically modulated by magnet array. • The surface modulated YIG films formed sharp band gaps. • A very small magnetic field change leads a large change in the peak value of band gap frequency. - Abstract: In this work, magnetostatic surface spin waves (MSSW) were propagated along the single crystal YIG (Y{sub 3}Fe{sub 5}O{sub 12}) film grown on GGG substrate. In order to obtain magnonic crystals, unlike the conventional methods, the surface of YIG films were magnetically modulated by magnet array in one and two-dimensions. The surface modulated YIG films formed sharp band gaps at approximately 6.55 GHz and 6.58 GHz at 1600 Oe magnetic field for one and two-dimensional magnonic crystals, respectively. It was found that a very small magnetic field change leads a large change in the peak value of band gap frequency.

  3. Photonic Crystals with Large Complete Bandgap Composed of an Approximately Ordered Array of Laurel-Crown-Like Structures Fabricated by Employing Anodic Aluminum Oxide Template

    Science.gov (United States)

    Chan, Der-Sheng; Chau, Yuan-Fong

    2013-01-01

    An innovative fabrication processes of a photonic crystal composed of an approximately ordered array of laurel-crown-like structures by employing an anodic aluminum oxide (AAO) template is presented. We found that the intensity of the electric field is affected by the microstructure and surface morphology of aluminum foil after etching the scalloped barrier oxide layer (BOL). In addition, the electric current is strongly dependent on the electric field distribution in the scalloped BOL at the pore bottoms. By using a different step potential (DSP) of 30-60 V in series, the proposed photonic crystal is fabricated and possesses a large complete photonic bandgap.

  4. An Optimized Design of Single-Channel Beta-Gamma Coincidence Phoswich Detector by Geant4 Monte Carlo Simulations

    Directory of Open Access Journals (Sweden)

    Weihua Zhang

    2011-01-01

    Full Text Available An optimized single-channel phoswich well detector design has been proposed and assessed in order to improve beta-gamma coincidence measurement sensitivity of xenon radioisotopes. This newly designed phoswich well detector consists of a plastic beta counting cell (BC404 embedded in a CsI(Tl crystal coupled to a photomultiplier tube. The BC404 is configured in a cylindrical pipe shape to minimise light collection deterioration. The CsI(Tl crystal consists of a rectangular part and a semicylindrical scintillation part as a light reflector to increase light gathering. Compared with a PhosWatch detector, the final optimized detector geometry showed 15% improvement in the energy resolution of a 131mXe 129.4 keV conversion electron peak. The predicted beta-gamma coincidence efficiencies of xenon radioisotopes have also been improved accordingly.

  5. ISPA (imaging silicon pixel array) experiment

    CERN Document Server

    Patrice Loïez

    2002-01-01

    Application components of ISPA tubes are shown: the CERN-developed anode chip, special windows for gamma and x-ray detection, scintillating crystal and fibre arrays for imaging and tracking of ionizing particles.

  6. High figure of merit ultra-compact 3-channel parallel-connected photonic crystal mini-hexagonal-H1 defect microcavity sensor array

    Science.gov (United States)

    Wang, Chunhong; Sun, Fujun; Fu, Zhongyuan; Ding, Zhaoxiang; Wang, Chao; Zhou, Jian; Wang, Jiawen; Tian, Huiping

    2017-08-01

    In this paper, a photonic crystal (PhC) butt-coupled mini-hexagonal-H1 defect (MHHD) microcavity sensor is proposed. The MHHD microcavity is designed by introducing six mini-holes into the initial H1 defect region. Further, based on a well-designed 1 ×3 PhC Beam Splitter and three optimal MHHD microcavity sensors with different lattice constants (a), a 3-channel parallel-connected PhC sensor array on monolithic silicon on insulator (SOI) is proposed. Finite-difference time-domain (FDTD) simulations method is performed to demonstrate the high performance of our structures. As statistics show, the quality factor (Q) of our optimal MHHD microcavity attains higher than 7×104, while the sensitivity (S) reaches up to 233 nm/RIU(RIU = refractive index unit). Thus, the figure of merit (FOM) >104 of the sensor is obtained, which is enhanced by two orders of magnitude compared to the previous butt-coupled sensors [1-4]. As for the 3-channel parallel-connected PhC MHHD microcavity sensor array, the FOMs of three independent MHHD microcavity sensors are 8071, 8250 and 8250, respectively. In addition, the total footprint of the proposed 3-channel parallel-connected PhC sensor array is ultra-compactness of 12.5 μm ×31 μm (width × length). Therefore, the proposed high FOM sensor array is an ideal platform for realizing ultra-compact highly parallel refractive index (RI) sensing.

  7. Fold distributions at clover, crystal and segment levels for segmented clover detectors

    International Nuclear Information System (INIS)

    Kshetri, R; Bhattacharya, P

    2014-01-01

    Fold distributions at clover, crystal and segment levels have been extracted for an array of segmented clover detectors for various gamma energies. A simple analysis of the results based on a model independant approach has been presented. For the first time, the clover fold distribution of an array and associated array addback factor have been extracted. We have calculated the percentages of the number of crystals and segments that fire for a full energy peak event

  8. Compact CsI(Tl)-PIN detectors for nuclear physics applications

    International Nuclear Information System (INIS)

    Bhattacharjee, T.; Basu, S.K.; Bhattacharyya, S.; Chanda, S.; Chowdhury, A.; Mukhopadhyay, P.; Chatterjee, M.B.; Dey, C.C.; Mukherjee, Anjali

    2005-01-01

    Prototype detector elements, based on CsI(Tl) - Si PIN diodes, have been fabricated and optimized for use in a near 4p charged particle multiplicity filter array. The important aspects of fabrication of such compact detector elements along with the off-line and on-line performance test results will be reported. An early implementation of the proposed multiplicity filter array will be described. The planned use of the array in conjunction with the Indian National Gamma Array (INGA) as a reaction filter in high spin spectroscopic studies would be stressed. (author)

  9. Hydroxyapatite coatings with oriented nanoplate and nanorod arrays: Fabrication, morphology, cytocompatibility and osteogenic differentiation

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Wei [The Education Ministry Key Lab of Resource Chemistry and Shanghai Key Laboratory of Rare Earth Functional Materials, Shanghai Normal University, Shanghai 200234 (China); Tian, Bo [Shanghai Key Laboratory of Orthopedic Implant, Department of Orthopedic Surgery, Shanghai Ninth People' s Hospital, Shanghai Jiao Tong University School of Medicine, Shanghai 200011 (China); Lei, Yong; Ke, Qin-Fei [The Education Ministry Key Lab of Resource Chemistry and Shanghai Key Laboratory of Rare Earth Functional Materials, Shanghai Normal University, Shanghai 200234 (China); Zhu, Zhen-An, E-mail: zhuzhenan2006@126.com [Shanghai Key Laboratory of Orthopedic Implant, Department of Orthopedic Surgery, Shanghai Ninth People' s Hospital, Shanghai Jiao Tong University School of Medicine, Shanghai 200011 (China); Guo, Ya-Ping, E-mail: ypguo@shnu.edu.cn [The Education Ministry Key Lab of Resource Chemistry and Shanghai Key Laboratory of Rare Earth Functional Materials, Shanghai Normal University, Shanghai 200234 (China)

    2016-10-01

    Hydroxyapatite (HA) crystals exhibit rod-like shape with c-axis orientation and plate-like shape with a(b)-axis orientation in vertebrate bones and tooth enamel surfaces, respectively. Herein, we report the synthesis of HA coatings with the oriented nanorod arrays (RHACs) and HA coatings with oriented nanoplate arrays (PHACs) by using bioglass coatings as sacrificial templates. After soaking in simulated body fluid (SBF) at 120 °C, the bioglass coatings are hydrothermally converted into the HA coatings via a dissolution-precipitation reaction. If the Ca/P ratios in SBF are 2.50 and 1.25, the HA crystals on the coatings are oriented nanorod arrays and oriented nanoplate arrays, respectively. Moreover, the bioglass coatings are treated with SBF at 37 °C, plate-like HA coatings with a low crystallinity (SHACs) are prepared. As compared with the Ti6Al4V and SHACs, the human bone marrow stromal cells (hBMSCs) on the RHACs and PHACs have better cell adhesion, spreading, proliferation and osteogenic differentiation because of their moderately hydrophilic surfaces and similar chemical composition, morphology and crystal orientation to human hard tissues. Notably, the morphologies of HA crystals have no obvious effects on cytocompatibility and osteogenic differentiation. Hence, the HA coatings with oriented nanoplate arrays or oriented nanorod arrays have a great potential for orthopedic applications. - Highlights: • We prepare hydroxyapatite coatings with oriented nanoplate and nanorod arrays. • Hydroxyapatite coatings are in situ converted from bioglass coatings. • Hydroxyapatite coatings have good cytocompatibility and osteogenic differentiation. • Oriented hydroxyapatite coatings are used for orthopedic implants.

  10. Hydroxyapatite coatings with oriented nanoplate and nanorod arrays: Fabrication, morphology, cytocompatibility and osteogenic differentiation

    International Nuclear Information System (INIS)

    Chen, Wei; Tian, Bo; Lei, Yong; Ke, Qin-Fei; Zhu, Zhen-An; Guo, Ya-Ping

    2016-01-01

    Hydroxyapatite (HA) crystals exhibit rod-like shape with c-axis orientation and plate-like shape with a(b)-axis orientation in vertebrate bones and tooth enamel surfaces, respectively. Herein, we report the synthesis of HA coatings with the oriented nanorod arrays (RHACs) and HA coatings with oriented nanoplate arrays (PHACs) by using bioglass coatings as sacrificial templates. After soaking in simulated body fluid (SBF) at 120 °C, the bioglass coatings are hydrothermally converted into the HA coatings via a dissolution-precipitation reaction. If the Ca/P ratios in SBF are 2.50 and 1.25, the HA crystals on the coatings are oriented nanorod arrays and oriented nanoplate arrays, respectively. Moreover, the bioglass coatings are treated with SBF at 37 °C, plate-like HA coatings with a low crystallinity (SHACs) are prepared. As compared with the Ti6Al4V and SHACs, the human bone marrow stromal cells (hBMSCs) on the RHACs and PHACs have better cell adhesion, spreading, proliferation and osteogenic differentiation because of their moderately hydrophilic surfaces and similar chemical composition, morphology and crystal orientation to human hard tissues. Notably, the morphologies of HA crystals have no obvious effects on cytocompatibility and osteogenic differentiation. Hence, the HA coatings with oriented nanoplate arrays or oriented nanorod arrays have a great potential for orthopedic applications. - Highlights: • We prepare hydroxyapatite coatings with oriented nanoplate and nanorod arrays. • Hydroxyapatite coatings are in situ converted from bioglass coatings. • Hydroxyapatite coatings have good cytocompatibility and osteogenic differentiation. • Oriented hydroxyapatite coatings are used for orthopedic implants.

  11. A prototype high-resolution animal positron tomograph with avalanche photodiode arrays and LSO crystals

    International Nuclear Information System (INIS)

    Ziegler, S.I.; Pichler, B.J.; Rafecas, M.; Schwaiger, M.

    2001-01-01

    rats and mice showed the feasibility of in vivo imaging using this PET scanner. The first LSO-APD prototype tomograph has been successfully introduced for in vivo animal imaging. APD arrays in combination with LSO crystals offer new design possibilities for positron tomographs with finely granulated detector channels. (orig.)

  12. Inorganic-organic rubbery scintillators

    CERN Document Server

    Gektin, A V; Pogorelova, N; Neicheva, S; Sysoeva, E; Gavrilyuk, V

    2002-01-01

    Spectral-kinetic luminescence properties of films, containing homogeneously dispersed scintillation particles of CsI, CsI:Tl, CsI:Na, and NaI:Tl in optically transparent organosiloxane matrix, are presented. Material is flexible and rubbery and in consequence the detectors of convenient shapes can be produced. It is found that luminescence spectra of the received films are identical whereas decay times are much shorter compared to the same ones of the corresponding single crystals. Layers with pure CsI demonstrate only the fast UV emission (307 nm, 10 ns) without blue microsecond afterglow typical for crystals. The films containing NaI:Tl are non-hygroscopic and preserve scintillation properties for a long time in humid atmosphere unlike single crystals. Organosiloxane layers with CsI:Tl particles provide high light output with good energy resolution for sup 5 sup 5 Fe, sup 1 sup 0 sup 9 Cd, sup 2 sup 4 sup 1 Am sources, and are capable of detecting both X-rays and alpha-, beta-particles.

  13. Transfer-free synthesis of highly ordered Ge nanowire arrays on glass substrates

    Energy Technology Data Exchange (ETDEWEB)

    Nakata, M.; Toko, K., E-mail: toko@bk.tsukuba.ac.jp; Suemasu, T. [Institute of Applied Physics, University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8573 (Japan); Jevasuwan, W.; Fukata, N. [National Institute for Materials Science, 1-1 Namiki, Tsukuba 305-0044 (Japan); Saitoh, N.; Yoshizawa, N. [Electron Microscope Facility, TIA, AIST, 16-1 Onogawa, Tsukuba 305-8569 (Japan)

    2015-09-28

    Vertically aligned Ge nanowires (NWs) are directly synthesized on glass via vapor-liquid-solid (VLS) growth using chemical-vapor deposition. The use of the (111)-oriented Ge seed layer, formed by metal-induced crystallization at 325 °C, dramatically improved the density, uniformity, and crystal quality of Ge NWs. In particular, the VLS growth at 400 °C allowed us to simultaneously achieve the ordered morphology and high crystal quality of the Ge NW array. Transmission electron microscopy demonstrated that the resulting Ge NWs had no dislocations or stacking faults. Production of high-quality NW arrays on amorphous insulators will promote the widespread application of nanoscale devices.

  14. Quantum mechanical cluster calculations of critical scintillation processes

    International Nuclear Information System (INIS)

    Derenzo, Stephen E.; Klintenberg, Mattias K.; Weber, Marvin J.

    2000-01-01

    This paper describes the use of commercial quantum chemistry codes to simulate several critical scintillation processes. The crystal is modeled as a cluster of typically 50 atoms embedded in an array of typically 5,000 point charges designed to reproduce the electrostatic field of the infinite crystal. The Schrodinger equation is solved for the ground, ionized, and excited states of the system to determine the energy and electron wave function. Computational methods for the following critical processes are described: (1) the formation and diffusion of relaxed holes, (2) the formation of excitons, (3) the trapping of electrons and holes by activator atoms, (4) the excitation of activator atoms, and (5) thermal quenching. Examples include hole diffusion in CsI, the exciton in CsI, the excited state of CsI:Tl, the energy barrier for the diffusion of relaxed holes in CaF2 and PbF2, and prompt hole trapping by activator atoms in CaF2:Eu and CdS:Te leading to an ultra-fast (<50ps) scintillation rise time.

  15. Status of the development of a HPGe-BGO pair spectrometer for ELI-NP

    Energy Technology Data Exchange (ETDEWEB)

    Homm, Ilja; Ignatov, Alexander; Ilieva, Stoyanka; Kroell, Thorsten [Technische Universitaet Darmstadt, Darmstadt (Germany)

    2016-07-01

    At the moment, the new European research facility called ELI-NP (The Extreme Light Infrastructure - Nuclear Physics) is being built in Bucharest-Magurele, Romania. It is one of three parts of the ELI project and offers applications for the investigation of questions concerning nuclear physics. The 8 HPGe (High-Purity Germanium) CLOVER detectors of ELIADE (ELI-NP Array of DEtectors) with four crystals each and high resolution are important components for the gamma spectroscopic study of photonuclear reactions. These detectors are surrounded by standard anti-Compton shields (AC shield). We investigate the possibility to operate for two of the ELIADE CLOVERS an advanced version of an AC shield as escape γ-rays pair spectrometers to extend the high-resolution spectroscopy to photon energies of several MeV where the pair production process dominates. The main tasks in this work are to develop and test such an AC shield: a pair spectrometer with BGO and CsI(Tl) crystals with APD (avalanche photodiode) or SPM (silicon photomultiplier) readout. The results of prototype testing are reported.

  16. Single-Crystal Diffraction from Two-Dimensional Block Copolymer Arrays

    International Nuclear Information System (INIS)

    Stein, G. E.; Kramer, E. J.; Li, X.; Wang, J.

    2007-01-01

    The structure of oriented 2D block copolymer single crystals is characterized by grazing-incidence small-angle x-ray diffraction, demonstrating long-range sixfold orientational order. From line shape analysis of the higher-order Bragg diffraction peaks, we determine that translational order decays algebraically with a decay exponent η=0.2, consistent with the Kosterlitz-Thouless-Halperin-Nelson-Young theory for a 2D crystal with a shear modulus μ=2x10 -4 N/m

  17. Mesoscale martensitic transformation in single crystals of topological defects

    Energy Technology Data Exchange (ETDEWEB)

    Li, Xiao; Martínez-González, José A.; Hernández-Ortiz, Juan P.; Ramírez-Hernández, Abelardo; Zhou, Ye; Sadati, Monirosadat; Zhang, Rui; Nealey, Paul F.; de Pablo, Juan J.

    2017-09-05

    Liquid crystal blue phases (BPs) are highly ordered at two levels. Molecules exhibit orientational order at nanometer length scales, while chirality leads to ordered arrays of doubletwisted cylinders over micrometer scales. Past studies of polycrystalline BPs were challenged by grain boundaries between randomly oriented crystalline nanodomains. Here, the nucleation of BPs is controlled with considerable precision by relying on chemically nano-patterned surfaces, leading to macroscopic single-crystal BP specimens where the dynamics of meso-crystal formation can be directly observed. Theory and experiments show that transitions between two BPs having a different network structure proceed through local re-organization of the crystalline array, without diffusion of the double twisted cylinders. In solid crystals, martensitic transformations between crystal structures involve the concerted motion of a few atoms, without diffusion. The transformation between BPs, where crystal features arise in the sub-micron regime, is found to be martensitic in nature, with the diffusion-less feature associated to the collective behavior of the double twist cylinders. Single-crystal BPs are shown to offer fertile grounds for the study of directed crystal-nucleation and the controlled growth of soft matter.

  18. Observation of a commensurate array of flux chains in tilted flux lattices in Bi-Sr-Ca-Cu-O single crystals

    International Nuclear Information System (INIS)

    Bolle, C.A.; Gammel, P.L.; Grier, D.G.; Murray, C.A.; Bishop, D.J.; Mitzi, D.B.; Kapitulnik, A.

    1991-01-01

    We report the observation of a novel flux-lattice structure, a commensurate array of flux-line chains. Our experiments consist of the magnetic decoration of the flux lattices in single crystals of Ba-Sr-Ca-Cu-O where the magnetic field is applied at an angle with respect to the conducting planes. For a narrow range of angles, the equilibrium structure is one with uniformly spaced chains with a higher line density of vortices than the background lattice. Our observations are in qualitative agreement with theories which suggest that, in strongly anisotropic materials the vortices develop an attractive interaction in tilted magnetic fields

  19. Sound absorption enhancement of nonwoven felt by using coupled membrane - sonic crystal inclusion

    Science.gov (United States)

    Fitriani, M. C.; Yahya, I.; Harjana; Ubaidillah; Aditya, F.; Siregar, Y.; Moeliono, M.; Sulaksono, S.

    2016-11-01

    The experimental results from laboratory test on the sound absorption performance of nonwoven felt with an array thin tubes and sonic crystal inclusions reported in this paper. The nonwoven felt sample was produced by a local company with 15 mm in its thickness and 900 gsm. The 6.4 mm diameter plastic straw was used to construct the thin tubes array while the sonic crystal is arranged in a 4 × 4 lattice crystal formation. It made from a PVC cylinder with 17 mm and 50 mm in diameter and length respectively. All cylinders have two holes positioned on 10 mm and 25 mm from the base. The results show that both treatments, array of thin tube and sonic crystal inclusions are effectively increased the sound absorption coefficient of the nonwoven felt significantly especially in the low frequency range starting from 200Hz.

  20. Visual detection of 2,4,6-trinitrotolune by molecularly imprinted colloidal array photonic crystal

    International Nuclear Information System (INIS)

    Lu, Wei; Asher, Sanford A.; Meng, Zihui; Yan, Zequn; Xue, Min; Qiu, Lili; Yi, Da

    2016-01-01

    Graphical abstract: Molecularly imprinted colloidal array (MICA) was explored for the selective visual detection of TNT with color changing from green to red. And molecularly imprinted colloidal particles (MICs) were evaluated for the adsorption capacity and the imprinting efficiency. The MICA had excellent flexibility, reversibility and stability. It promised high potential for the visual semi-quantitative detection of other explosives. - Highlights: • Molecularly imprinted colloidal array (MICA) was used to visually detect TNT. • The relationship of particle size, diffracted wavelength and color was discussed. • The adsorption capacity and imprinting efficiency of MICs were calculated. • MICA had short response time, high selectivity, good reversibility and stability. • MICA had high potential to be used in other customed visual explosive detection. - Abstract: We developed a photonic crystal (PhC) sensor for the quantification of 2,4,6-trinitrotoluene (TNT) in solution. Monodisperse (210 nm in diameter) molecularly imprinted colloidal particles (MICs) for TNT were prepared by the emulsion polymerization of methyl methacrylate and acrylamide in the presence of TNT as a template. The MICs were then self-assembled into close-packed opal PhC films. The adsorption capacity of the MICs for TNT was 64 mg TNT/g. The diffraction from the PhC depended on the TNT concentration in a methanol/water (3/2, v/v) potassium dihydrogen phosphate buffer solution (pH = 7.0, 30 mM). The limit of detection (LOD) of the sensor was 1.03 μg. The color of the molecularly imprinted colloidal array (MICA) changed from green to red with an 84 nm diffraction red shift when the TNT concentration increased to 20 mM. The sensor response time was 3 min. The PhC sensor was selective for TNT compared to similar compounds such as 2,4,6-trinitrophenol, 2,4-dinitrotoluene, 2,6-dinitrotoluene, 2-nitromesitylene, 4-nitrotoluene, 2-nitrotoluene, 1,3-dinitrobenzene, methylbenzene, 4-nitrophenol

  1. Visual detection of 2,4,6-trinitrotolune by molecularly imprinted colloidal array photonic crystal

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Wei [School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, 100081 (China); Asher, Sanford A., E-mail: asher@pitt.edu [Department of Chemistry, University of Pittsburgh, Pittsburgh, PA 15260 (United States); Meng, Zihui, E-mail: m_zihui@yahoo.com [School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, 100081 (China); Yan, Zequn [School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, 100081 (China); Xue, Min, E-mail: minxue@bit.edu.cn [School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, 100081 (China); Qiu, Lili, E-mail: qiulili@bit.edu.cn [School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, 100081 (China); Yi, Da [School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, 100081 (China)

    2016-10-05

    Graphical abstract: Molecularly imprinted colloidal array (MICA) was explored for the selective visual detection of TNT with color changing from green to red. And molecularly imprinted colloidal particles (MICs) were evaluated for the adsorption capacity and the imprinting efficiency. The MICA had excellent flexibility, reversibility and stability. It promised high potential for the visual semi-quantitative detection of other explosives. - Highlights: • Molecularly imprinted colloidal array (MICA) was used to visually detect TNT. • The relationship of particle size, diffracted wavelength and color was discussed. • The adsorption capacity and imprinting efficiency of MICs were calculated. • MICA had short response time, high selectivity, good reversibility and stability. • MICA had high potential to be used in other customed visual explosive detection. - Abstract: We developed a photonic crystal (PhC) sensor for the quantification of 2,4,6-trinitrotoluene (TNT) in solution. Monodisperse (210 nm in diameter) molecularly imprinted colloidal particles (MICs) for TNT were prepared by the emulsion polymerization of methyl methacrylate and acrylamide in the presence of TNT as a template. The MICs were then self-assembled into close-packed opal PhC films. The adsorption capacity of the MICs for TNT was 64 mg TNT/g. The diffraction from the PhC depended on the TNT concentration in a methanol/water (3/2, v/v) potassium dihydrogen phosphate buffer solution (pH = 7.0, 30 mM). The limit of detection (LOD) of the sensor was 1.03 μg. The color of the molecularly imprinted colloidal array (MICA) changed from green to red with an 84 nm diffraction red shift when the TNT concentration increased to 20 mM. The sensor response time was 3 min. The PhC sensor was selective for TNT compared to similar compounds such as 2,4,6-trinitrophenol, 2,4-dinitrotoluene, 2,6-dinitrotoluene, 2-nitromesitylene, 4-nitrotoluene, 2-nitrotoluene, 1,3-dinitrobenzene, methylbenzene, 4-nitrophenol

  2. 3D DNA Crystals and Nanotechnology

    Directory of Open Access Journals (Sweden)

    Paul J. Paukstelis

    2016-08-01

    Full Text Available DNA’s molecular recognition properties have made it one of the most widely used biomacromolecular construction materials. The programmed assembly of DNA oligonucleotides has been used to create complex 2D and 3D self-assembled architectures and to guide the assembly of other molecules. The origins of DNA nanotechnology are rooted in the goal of assembling DNA molecules into designed periodic arrays, i.e., crystals. Here, we highlight several DNA crystal structures, the progress made in designing DNA crystals, and look at the current prospects and future directions of DNA crystals in nanotechnology.

  3. A LaBr{sub 3}: Ce fast-timing array for DESPEC at FAIR

    Energy Technology Data Exchange (ETDEWEB)

    Roberts, Oliver J., E-mail: O.J.Roberts@brighton.ac.uk [School of Computing, Engineering and Mathematics, University of Brighton, Brighton BN2 4GJ (United Kingdom); Bruce, Alison M. [School of Computing, Engineering and Mathematics, University of Brighton, Brighton BN2 4GJ (United Kingdom); Regan, Patrick H. [Department of Physics, University of Surrey, Guildford GU2 7XH (United Kingdom); National Physics Laboratory, Teddington, TW11 0LW (United Kingdom); Podolyák, Zsolt; Townsley, Christopher M. [Department of Physics, University of Surrey, Guildford GU2 7XH (United Kingdom); Smith, John F.; Mulholland, Kieran F. [School of Engineering, The University of the West of Scotland, Paisley PA1 2BE (United Kingdom); Smith, Andrew [The University of Manchester, Oxford Road, Manchester, M13 9PL (United Kingdom)

    2014-06-01

    The design of a fast-timing γ-ray detection array aimed at measuring sub-nanosecond half-lives using LaBr{sub 3}:Ce scintillation crystals is presented. This array will complement novel and existing charged particle and neutron detector arrays at the low-energy branch of a fragment separator (Super-FRS) to be built within the NuSTAR collaboration as part of the future Facility for Anti-proton and Ion Research (FAIR). The array will be used in conjunction with the Advanced Implantation Detector Array (AIDA), to measure implant-decay correlations. Monte-Carlo simulations have been performed to determine the design of the proposed fast-timing array around a localised implantation point. In particular, simulations were used to determine the full-energy peak efficiencies for single cylindrical, conical and ‘hybrid’ detector geometries, as well as complete array configurations of ‘hybrid’ and ∅1.5 in.×2 in. cylindrical crystals. Timing precision calculations were then used to determine the timing response for each configuration based on its simulated efficiency. An informed decision based on the simulated efficiencies and timing precision calculations allowed the optimum configuration for the array to be determined.

  4. Effects of reflector and crystal surface on the performance of a depth-encoding PET detector with dual-ended readout

    International Nuclear Information System (INIS)

    Ren, Silin; Yang, Yongfeng; Cherry, Simon R.

    2014-01-01

    Purpose: Depth encoding detectors are required to improve the spatial resolution and spatial resolution uniformity of small animal positron emission tomography (PET) scanners, as well as dedicated breast and brain scanners. Depth of interaction (DOI) can be measured by using dual-ended readout of lutetium oxyorthosilicate (LSO) scintillator arrays with position-sensitive avalanche photodiodes. Inter-crystal reflectors and crystal surface treatments play important roles in determining the performance of dual-ended detectors. In this paper, the authors evaluated five LSO arrays made with three different intercrystal reflectors and with either polished or unpolished crystal surfaces. Methods: The crystal size in all arrays was 1.5 mm, which is typical of the detector size used in small animal and dedicated breast scanners. The LSO arrays were measured with dual-ended readout and were compared in terms of flood histogram, energy resolution, and DOI resolution performance. Results: The four arrays using enhanced specular reflector (ESR) and Toray reflector provided similar quality flood histograms and the array using Crystal Wrap reflector gave the worst flood histogram. The two arrays using ESR reflector provided the best energy resolution and the array using Crystal Wrap reflector yielded the worst energy resolution. All arrays except the polished ESR array provided good DOI resolution ranging from 1.9 mm to 2.9 mm. DOI resolution improved as the gradient in light collection efficiency with depth (GLCED) increased. The geometric mean energies were also calculated for these dual-ended readout detectors as an alternative to the conventional summed total energy. It was shown that the geometric mean energy is advantageous in that it provides more uniform photopeak amplitude at different depths for arrays with high GLCED, and is beneficial in event selection by allowing a fixed energy window independent of depth. A new method of DOI calculation that improved the linearity

  5. A 90 element CdTe array detector

    Energy Technology Data Exchange (ETDEWEB)

    Iwase, Y.; Onozuka, A.; Ohmori, M. (Nippon Mining Co. Ltd., Toda, Saitama (Japan). Electronic Material and Components Labs.); Funaki, M. (Nippon Mining Co. Ltd., Toda, Saitama (Japan). Materials Development Research Labs.)

    1992-11-15

    The fabrication of a CdTe array radiation detector and its radiation detection characteristics are described. In order to obtain high efficiency of charge collection and realize uniform detection sensitivity, current-voltage characteristics with the combination of large and small barrier height contacts and three kinds of CdTe crystals have been investigated. It was found that the Schottky barrier height of electroless Pt deposition was 0.97 eV, which effectively suppressed electron injection. By using the crystal grown by the travelling heater method with a Cl concentration of 2 ppm, carrier lifetimes for electrons and holes of 1.0 and 0.5 [mu]s, respectively, were achieved. A 90 element array detector exhibited an energy resolution as low as 4.5 keV and a count rate variation of less than 5% for 60 keV [gamma]-rays. (orig.).

  6. A 90 element CdTe array detector

    Science.gov (United States)

    Iwase, Y.; Funaki, M.; Onozuka, A.; Ohmori, M.

    1992-11-01

    The fabrication of a CdTe array radiation detector and its radiation detection characteristics are described. In order to obtain high efficiency of charge collection and realize uniform detection sensitivity, current-voltage characteristics with the combination of large and small barrier height contacts and three kinds of CdTe crystals have been investigated. It was found that the Schottky barrier height of electroless Pt deposition was 0.97 eV, which effectively suppressed electron injection. By using the crystal grown by the travelling heater method with a Cl concentration of 2 ppm, carrier lifetimes for electrons and holes of 1.0 and 0.5 μs, respectively, were achieved. A 90 element array detector exhibited an energy resolution as low as 4.5 keV and a count rate variation of less than 5% for 60 keV γ-rays.

  7. PS-HEMA latex fractionation by sedimentation and colloidal crystallization

    Directory of Open Access Journals (Sweden)

    Cardoso André H.

    1999-01-01

    Full Text Available A poly(styrene-co-hydroxyethylmethacrylate latex underwent sedimentation under gravity followed by an spontaneous and extensive colloidal crystallization. It was then fractionated in three visually distinguishable layers. Latex aliquots layers were sampled at different heigths and the particles were characterized by PCS, microelectrophoresis, infrared spectra and analytical electron microscopy. The major fraction was opalescent and contained the colloidal crystals settled in the bottom of the liquid. Two other latex fractions were obtained, which differed in their chemical compositions, particle sizes and topochemical features from the self-arraying particles. Macrocrystallization of the fractionated latex yielded high quality crystals with a low frequency of defects, which confirms that particle chemical homogeneity is an important factor for particle self-arraying.

  8. Tunneling effect in cavity-resonator-coupled arrays

    International Nuclear Information System (INIS)

    Ma Hua; Xu Zhuo; Qu Shao-Bo; Zhang Jie-Qiu; Wang Jia-Fu; Liang Chang-Hong

    2013-01-01

    The quantum tunneling effect (QTE) in a cavity-resonator-coupled (CRC) array was analytically and numerically investigated. The underlying mechanism was interpreted by treating electromagnetic waves as photons, and then was generalized to acoustic waves and matter waves. It is indicated that for the three kinds of waves, the QTE can be excited by cavity resonance in a CRC array, resulting in sub-wavelength transparency through the narrow splits between cavities. This opens up opportunities for designing new types of crystals based on CRC arrays, which may find potential applications such as quantum devices, micro-optic transmission, and acoustic manipulation. (condensed matter: electronic structure, electrical, magnetic, and optical properties)

  9. Patterned solid state growth of barium titanate crystals

    Science.gov (United States)

    Ugorek, Michael Stephen

    An understanding of microstructure evolution in ceramic materials, including single crystal development and abnormal/enhanced grain growth should enable more controlled final ceramic element structures. In this study, two different approaches were used to control single crystal development in a patterned array. These two methods are: (1) patterned solid state growth in BaTiO 3 ceramics, and (2) metal-mediated single crystal growth in BaTiO 3. With the patterned solid state growth technique, optical photolithography was used to pattern dopants as well as [001] and [110] BaTiO3 single crystal template arrays with a 1000 microm line pattern array with 1000 microm spacings. These patterns were subsequently used to control the matrix grain growth evolution and single crystal development in BaTiO3. It was shown that the growth kinetics can be controlled by a small initial grain size, atmosphere conditions, and the introduction of a dopant at selective areas/interfaces. By using a PO2 of 1x10-5 atm during high temperature heat treatment, the matrix coarsening has been limited (to roughly 2 times the initial grain size), while retaining single crystal boundary motion up to 0.5 mm during growth for dwell times up to 9 h at 1300°C. The longitudinal and lateral growth rates were optimized at 10--15 microm/h at 1300°C in a PO2 of 1x10 -5 atm for single crystal growth with limited matrix coarsening. Using these conditions, a patterned microstructure in BaTiO3 was obtained. With the metal-mediated single crystal growth technique, a novel approach for fabricating 2-2 single crystal/polymer composites with a kerf texture development were studied using both [001] and [110] BaTiO3 single crystals templates. By using a PO 2 of 1x10-11 atm during high temperature heat treatment, matrix coarsening was limited while enabling single crystal boundary motion up to 0.35 mm during growth between 1250°C and 1300°C with growth rates ˜ 3--4 microm/h for both single crystal orientations. By

  10. Real-Time Hand-Held Magnetometer Array

    Science.gov (United States)

    2016-04-01

    measurements, we swung a target, pendulum-style, from the ceiling above the array. We could easily observe that the height of the target was varying... crystal oscillator clock signal. The Microblaze processor boots up with the program already present in its RAM at startup. MR-2104 Real-Time

  11. Characterization and quality control of avalanche photodiode arrays for the Clear-PEM detector modules

    International Nuclear Information System (INIS)

    Abreu, Conceicao; Amaral, Pedro; Carrico, Bruno; Ferreira, Miguel; Luyten, Joan; Moura, Rui; Ortigao, Catarina; Rato, Pedro; Varela, Joao

    2007-01-01

    Clear-PEM is a Positron Emission Mammography (PEM) prototype being developed in the framework of the Crystal Clear Collaboration at CERN. This device is a dedicated PET camera for mammography, based on LYSO:Ce scintillator crystals, Avalanche PhotoDiodes (APD) and a fast, low-noise electronics readout system, designed to examine both the breast and the axillary lymph node areas, and aiming at the detection of tumors down to 2 mm in diameter. The prototype has two planar detector heads, each composed of 96 detector modules. The Clear-PEM detector module is composed of a matrix of 32 identical 2x2x20 mm 3 LYSO:Ce crystals read at both ends by Hamamatsu S8550 APD arrays (4x8) for Depth-of-Interaction (DoI) capability. The APD arrays were characterized by the measurement of gain and dark current as a function of bias voltage, under controlled temperature conditions. Two independent setups were used. The full set of 398 APD arrays followed a well-defined quality control (QC) protocol, aiming at the rejection of arrays not complying within defined specifications. From a total of 398 arrays, only 2 (0.5%) were rejected, reassuring the trust in these detectors for prototype assembly and future developments

  12. Monolithic, High-Speed Fiber-Optic Switching Array for Lidar

    Science.gov (United States)

    Suckow, Will; Roberts, Tony; Switzer, Gregg; Terwilliger, Chelle

    2011-01-01

    Current fiber switch technologies use mechanical means to redirect light beams, resulting in slow switch time, as well as poor reliability due to moving parts wearing out quickly at high speeds. A non-mechanical ability to switch laser output into one of multiple fibers within a fiber array can provide significant power, weight, and costs savings to an all-fiber system. This invention uses an array of crystals that act as miniature prisms to redirect light as an electric voltage changes the prism s properties. At the heart of the electro-optic fiber-optic switch is an electro- optic crystal patterned with tiny prisms that can deflect the beam from the input fiber into any one of the receiving fibers arranged in a linear array when a voltage is applied across the crystal. Prism boundaries are defined by a net dipole moment in the crystal lattice that has been poled opposite to the surrounding lattice fabricated using patterned, removable microelectrodes. When a voltage is applied across the crystal, the resulting electric field changes the index of refraction within the prism boundaries relative to the surrounding substrate, causing light to deflect slightly according to Snell s Law. There are several materials that can host the necessary monolithic poled pattern (including, but not limited to, SLT, KTP, LiNbO3, and Mg:LiNbO3). Be cause this is a solid-state system without moving parts, it is very fast, and does not wear down easily. This invention is applicable to all fiber networks, as well as industries that use such networks. The unit comes in a compact package, can handle both low and high voltages, and has a high reliability (100,000 hours without maintenance).

  13. Assessment of array scintillation detector for follicle thyroid 2-d image acquisition using Monte Carlo simulation

    International Nuclear Information System (INIS)

    Silva, Carlos Borges da; Braz, Delson

    2008-01-01

    Full text: This work presents an innovative study to find out the adequate scintillation inorganic detector array to be used coupled to a specific light photo sensor, a charge coupled device (CCD), through a fiber optic plate. The goal is to choose the type of detector that fits a 2-dimensional imaging acquisition of a cell thyroid tissue application with high resolution and detection efficiency in order to map a follicle image using gamma radiation emission. A point or volumetric source-detector simulation by using a MCNP4B general code, considering different source energies, detector materials and geometry including pixel sizes and reflector types was performed. In this study, simulations were performed for 7 x 7, 31 x 31 and 127 x 127 arrays using CsI(Tl), BGO, CdWO 4 , LSO, GOS and GSO scintillation detectors with pixel dimensions ranging from 1 x 1 cm 2 to 10 x 10 μm 2 and radiation thickness ranging from 1 mm to 10 mm. The effect of all these parameters was investigated to find the best source-detector system that results in an image with the best contrast details. The results showed that it is possible to design a specific imaging system that allows searching for in-vitro studies, specifically in radiobiology applied to endocrine physiology. A 2D image of two thyroid follicles simulated by using MCNP4B code is shown

  14. Programmable and coherent crystallization of semiconductors

    KAUST Repository

    Yu, Liyang

    2017-03-04

    The functional properties and technological utility of polycrystalline materials are largely determined by the structure, geometry, and spatial distribution of their multitude of crystals. However, crystallization is seeded through stochastic and incoherent nucleation events, limiting the ability to control or pattern the microstructure, texture, and functional properties of polycrystalline materials. We present a universal approach that can program the microstructure of materials through the coherent seeding of otherwise stochastic homogeneous nucleation events. The method relies on creating topographic variations to seed nucleation and growth at designated locations while delaying nucleation elsewhere. Each seed can thus produce a coherent growth front of crystallization with a geometry designated by the shape and arrangement of seeds. Periodic and aperiodic crystalline arrays of functional materials, such as semiconductors, can thus be created on demand and with unprecedented sophistication and ease by patterning the location and shape of the seeds. This approach is used to demonstrate printed arrays of organic thin-film transistors with remarkable performance and reproducibility owing to their demonstrated spatial control over the microstructure of organic and inorganic polycrystalline semiconductors.

  15. Structural control of ultra-fine CoPt nanodot arrays via electrodeposition process

    Energy Technology Data Exchange (ETDEWEB)

    Wodarz, Siggi [Department of Applied Chemistry, Waseda University, Shinjuku, Tokyo 169-8555 (Japan); Hasegawa, Takashi; Ishio, Shunji [Department of Materials Science, Akita University, Akita City 010-8502 (Japan); Homma, Takayuki, E-mail: t.homma@waseda.jp [Department of Applied Chemistry, Waseda University, Shinjuku, Tokyo 169-8555 (Japan)

    2017-05-15

    CoPt nanodot arrays were fabricated by combining electrodeposition and electron beam lithography (EBL) for the use of bit-patterned media (BPM). To achieve precise control of deposition uniformity and coercivity of the CoPt nanodot arrays, their crystal structure and magnetic properties were controlled by controlling the diffusion state of metal ions from the initial deposition stage with the application of bath agitation. Following bath agitation, the composition gradient of the CoPt alloy with thickness was mitigated to have a near-ideal alloy composition of Co:Pt =80:20, which induces epitaxial-like growth from Ru substrate, thus resulting in the improvement of the crystal orientation of the hcp (002) structure from its initial deposition stages. Furthermore, the cross-sectional transmission electron microscope (TEM) analysis of the nanodots deposited with bath agitation showed CoPt growth along its c-axis oriented in the perpendicular direction, having uniform lattice fringes on the hcp (002) plane from the Ru underlayer interface, which is a significant factor to induce perpendicular magnetic anisotropy. Magnetic characterization of the CoPt nanodot arrays showed increase in the perpendicular coercivity and squareness of the hysteresis loops from 2.0 kOe and 0.64 (without agitation) to 4.0 kOe and 0.87 with bath agitation. Based on the detailed characterization of nanodot arrays, the precise crystal structure control of the nanodot arrays with ultra-high recording density by electrochemical process was successfully demonstrated. - Highlights: • Ultra-fine CoPt nanodot arrays were fabricated by electrodeposition. • Crystallinity of hcp (002) was improved with uniform composition formation. • Uniform formation of hcp lattices leads to an increase in the coercivity.

  16. Taub-Nut Crystal

    Science.gov (United States)

    Imazato, Harunobu; Mizoguchi, Shun'ya; Yata, Masaya

    We consider the Gibbons-Hawking metric for a three-dimensional periodic array of multi-Taub-NUT centers, containing not only centers with a positive NUT charge but also ones with a negative NUT charge. The latter are regarded as representing the asymptotic form of the Atiyah-Hitchin metric. The periodic arrays of Taub-NUT centers have close parallels with ionic crystals, where the Gibbons-Hawking potential plays the role of the Coulomb static potential of the ions, and are similarly classified according to their space groups. After a periodic identification and a Z2 projection, the array is transformed by T-duality to a system of NS5-branes with the SU(2) structure, and a further standard embedding yields, though singular, a half-BPS heterotic 5-brane background with warped compact transverse dimensions. A discussion is given on the possibility of probing the singular geometry by two-dimensional gauge theories.

  17. Graphene-based one-dimensional photonic crystal

    OpenAIRE

    Berman, Oleg L.; Kezerashvili, Roman Ya.

    2011-01-01

    A novel type of one-dimensional (1D) photonic crystal formed by the array of periodically located stacks of alternating graphene and dielectric stripes embedded into a background dielectric medium is proposed. The wave equation for the electromagnetic wave propagating in such structure solved in the framework of the Kronig-Penney model. The frequency band structure of 1D graphene-based photonic crystal is obtained analytically as a function of the filling factor and the thickness of the diele...

  18. Frequency shift of a crystal quartz resonator in thickness-shear modes induced by an array of hemispherical material units.

    Science.gov (United States)

    Yuantai Hu; Huiliang Hu; Bin Luo; Huan Xue; Jiemin Xie; Ji Wang

    2013-08-01

    A two-dimensional model was established to study the dynamic characteristics of a quartz crystal resonator with the upper surface covered by an array of hemispherical material units. A frequency-dependent equivalent mass ratio was proposed to simulate the effect of the covered units on frequency shift of the resonator system. It was found that the equivalent mass ratio alternately becomes positive or negative with change of shear modulus and radius of each material unit, which indicates that the equivalent mass ratio is strongly related to the vibration mode of the covered loadings. The further numerical results show the cyclical feature in the relationship of frequency shift and shear modulus/radius as expected. The solutions are useful in the analysis of frequency stability of quartz resonators and acoustic wave sensors.

  19. A sub-millimeter resolution PET detector module using a multi-pixel photon counter array

    International Nuclear Information System (INIS)

    Song, Tae Yong; Wu Heyu; Komarov, Sergey; Tai, Yuan-Chuan; Siegel, Stefan B

    2010-01-01

    A PET block detector module using an array of sub-millimeter lutetium oxyorthosilicate (LSO) crystals read out by an array of surface-mount, semiconductor photosensors has been developed. The detector consists of a LSO array, a custom acrylic light guide, a 3 x 3 multi-pixel photon counter (MPPC) array (S10362-11-050P, Hamamatsu Photonics, Japan) and a readout board with a charge division resistor network. The LSO array consists of 100 crystals, each measuring 0.8 x 0.8 x 3 mm 3 and arranged in 0.86 mm pitches. A Monte Carlo simulation was used to aid the design and fabrication of a custom light guide to control distribution of scintillation light over the surface of the MPPC array. The output signals of the nine MPPC are multiplexed by a charge division resistor network to generate four position-encoded analog outputs. Flood image, energy resolution and timing resolution measurements were performed using standard NIM electronics. The linearity of the detector response was investigated using gamma-ray sources of different energies. The 10 x 10 array of 0.8 mm LSO crystals was clearly resolved in the flood image. The average energy resolution and standard deviation were 20.0% full-width at half-maximum (FWHM) and ±5.0%, respectively, at 511 keV. The timing resolution of a single MPPC coupled to a LSO crystal was found to be 857 ps FWHM, and the value for the central region of detector module was 1182 ps FWHM when ±10% energy window was applied. The nonlinear response of a single MPPC when used to read out a single LSO was observed among the corner crystals of the proposed detector module. However, the central region of the detector module exhibits significantly less nonlinearity (6.5% for 511 keV). These results demonstrate that (1) a charge-sharing resistor network can effectively multiplex MPPC signals and reduce the number of output signals without significantly degrading the performance of a PET detector and (2) a custom light guide to permit light sharing

  20. A BGO detector array and its application in intermediate energy heavy ion experiments

    International Nuclear Information System (INIS)

    Li Zuyu; Jin Genming; He Zhiyong; Duan Limin; Wu Heyu; Qi Yujin; Luo Qingzheng; Zhang Baoguo; Wen Wanxin; Dai Guangxi

    1996-01-01

    A BGO crystal (Bi 4 Ge 3 O 12 ) as the E detector of ΔE-E for identification of reaction products has been used for detecting the charged particles emitting from the 25 MeV 40 Ar induced reaction. The responses of the BGO crystal to various light charged particles were measured. A close-packed hexagonal array consisting of thirteen ΔE-E telescopes (Si-BGO) has been developed to detect the light charged particles interfering with each other in intermediate-energy heavy-ion induced reactions. Some applications of this telescope array are also described. (orig.)

  1. The Mu2e undoped CsI crystal calorimeter

    Science.gov (United States)

    Atanov, N.; Baranov, V.; Budagov, J.; Cervelli, F.; Colao, F.; Cordelli, M.; Corradi, G.; Davydov, Y. I.; Di Falco, S.; Diociaiuti, E.; Donati, S.; Donghia, R.; Echenard, B.; Giovannella, S.; Glagolev, V.; Grancagnolo, F.; Happacher, F.; Hitlin, D. G.; Martini, M.; Miscetti, S.; Miyashita, T.; Morescalchi, L.; Murat, P.; Pedreschi, E.; Pezzullo, G.; Porter, F.; Raffaelli, F.; Ricci, M.; Saputi, A.; Sarra, I.; Spinella, F.; Tassielli, G.; Tereshchenko, V.; Usubov, Z.; Zhu, R. Y.

    2018-02-01

    The Mu2e experiment at Fermilab will search for Charged Lepton Flavor Violating conversion of a muon to an electron in an atomic field. The Mu2e detector is composed of a tracker, an electromagnetic calorimeter and an external system, surrounding the solenoid, to veto cosmic rays. The calorimeter plays an important role to provide: a) excellent particle identification capabilities; b) a fast trigger filter; c) an easier tracker track reconstruction. Two disks, located downstream of the tracker, contain 674 pure CsI crystals each. Each crystal is read out by two arrays of UV-extended SiPMs. The choice of the crystals and SiPMs has been finalized after a thorough test campaign. A first small scale prototype consisting of 51 crystals and 102 SiPM arrays has been exposed to an electron beam at the BTF (Beam Test Facility) in Frascati. Although the readout electronics were not final, results show that the current design is able to meet the timing and energy resolution required by the Mu2e experiment.

  2. Development of a hard x-ray focal plane compton polarimeter: a compact polarimetric configuration with scintillators and Si photomultipliers

    Science.gov (United States)

    Chattopadhyay, T.; Vadawale, S. V.; Goyal, S. K.; Mithun, N. P. S.; Patel, A. R.; Shukla, R.; Ladiya, T.; Shanmugam, M.; Patel, V. R.; Ubale, G. P.

    2016-02-01

    X-ray polarization measurement of cosmic sources provides two unique parameters namely degree and angle of polarization which can probe the emission mechanism and geometry at close vicinity of the compact objects. Specifically, the hard X-ray polarimetry is more rewarding because the sources are expected to be intrinsically highly polarized at higher energies. With the successful implementation of Hard X-ray optics in NuSTAR, it is now feasible to conceive Compton polarimeters as focal plane detectors. Such a configuration is likely to provide sensitive polarization measurements in hard X-rays with a broad energy band. We are developing a focal plane hard X-ray Compton polarimeter consisting of a plastic scintillator as active scatterer surrounded by a cylindrical array of CsI(Tl) scintillators. The scatterer is 5 mm diameter and 100 mm long plastic scintillator (BC404) viewed by normal PMT. The photons scattered by the plastic scatterer are collected by a cylindrical array of 16 CsI(Tl) scintillators (5 mm × 5 mm × 150 mm) which are read by Si Photomultiplier (SiPM). Use of the new generation SiPMs ensures the compactness of the instrument which is essential for the design of focal plane detectors. The expected sensitivity of such polarimetric configuration and complete characterization of the plastic scatterer, specially at lower energies have been discussed in [11, 13]. In this paper, we characterize the CsI(Tl) absorbers coupled to SiPM. We also present the experimental results from the fully assembled configuration of the Compton polarimeter.

  3. A quick responding quartz crystal microbalance sensor array based on molecular imprinted polyacrylic acids coating for selective identification of aldehydes in body odor.

    Science.gov (United States)

    Jha, Sunil K; Hayashi, Kenshi

    2015-03-01

    In present work, a novel quartz crystal microbalance (QCM) sensor array has been developed for prompt identification of primary aldehydes in human body odor. Molecularly imprinted polymers (MIP) are prepared using the polyacrylic acid (PAA) polymer matrix and three organic acids (propenoic acid, hexanoic acid and octanoic acid) as template molecules, and utilized as QCM surface coating layer. The performance of MIP films is characterized by 4-element QCM sensor array (three coated with MIP layers and one with pure PAA for reference) dynamic and static responses to target aldehydes: hexanal, heptanal, and nonanal in single, binary, and tertiary mixtures at distinct concentrations. The target aldehydes were selected subsequent to characterization of body odor samples with solid phase-micro extraction gas chromatography mass spectrometer (SPME-GC-MS). The hexanoic acid and octanoic acid imprinted PAA exhibit fast response, and better sensitivity, selectivity and reproducibility than the propenoic acid, and non-imprinted PAA in array. The response time and recovery time for hexanoic acid imprinted PAA are obtained as 5 s and 12 s respectively to typical concentrations of binary and tertiary mixtures of aldehydes using the static response. Dynamic sensor array response matrix has been processed with principal component analysis (PCA) for visual, and support vector machine (SVM) classifier for quantitative identification of target odors. Aldehyde odors were identified successfully in principal component (PC) space. SVM classifier results maximum recognition rate 79% for three classes of binary odors and 83% including single, binary, and tertiary odor classes in 3-fold cross validation. Copyright © 2014 Elsevier B.V. All rights reserved.

  4. Measuring Light Reflectance of BGO Crystal Surfaces

    Science.gov (United States)

    Janecek, Martin; Moses, William W.

    2008-10-01

    A scintillating crystal's surface reflectance has to be well understood in order to accurately predict and optimize the crystal's light collection through Monte Carlo simulations. In this paper, we measure the inner surface reflectance properties for BGO. The measurements include BGO crystals with a mechanically polished surface, rough-cut surface, and chemically etched surface, and with various reflectors attached, both air-coupled and with coupling compound. The measurements are performed with a laser aimed at the center of a hemispherical shaped BGO crystal. The hemispherical shape eliminates any non-perpendicular angles for light entering and exiting the crystal. The reflected light is collected with an array of photodiodes. The laser can be set at an arbitrary angle, and the photodiode array is rotated to fully cover 2pi of solid angle. The current produced in the photodiodes is readout with a digital multimeter connected through a multiplexer. The two rows of photodiodes achieve 5-degree by 4-degree resolution, and the current measurement has a dynamic range of 105:1. The acquired data was not described by the commonly assumed linear combination of specular and diffuse (Lambertian) distributions, except for a very few surfaces. Surface roughness proved to be the most important parameter when choosing crystal setup. The reflector choice was of less importance and of almost no consequence for rough-cut surfaces. Pure specular reflection distribution for all incidence angles was measured for polished surfaces with VM2000 film, while the most Lambertian distribution for any surface finish was measured for titanium dioxide paint. The distributions acquired in this paper will be used to create more accurate Monte Carlo models for light reflection distribution within BGO crystals.

  5. Dual-energy radiography of bone tissues using ZnSe-based scintielectronic detectors

    International Nuclear Information System (INIS)

    Grinyov, B.; Ryzhikov, V.; Lecoq, P.; Naydenov, S.; Opolonin, A.; Lisetskaya, E.; Galkin, S.; Shumeiko, N.

    2007-01-01

    Detectors of the scintillator-photodiode type were obtained on the basis of CsI(Tl), CdWO 4 and ZnSe(Te) crystals, and their comparative study was carried out, aiming at their use in X-ray computer tomography (CT). Because of their low afterglow level (10 ppm after 10 ms), CWO and ZnSe crystals are preferable for this application. A drawback of CWO is its lower (by 3 times) light output as compared with CsI(Tl). ZnSe has low transparence to intrinsic radiation; however, up to energies of 60-70 keV it is superior, as for the whole complex of its parameter, to materials traditionally used for CT detectors. The use of a dual-energy receiving-detecting circuit with a detector pair ZnSe/CsI or ZnSe/CdWO allows efficient distinction between muscular and bone tissues, which supports our earlier theoretical assumptions that this method could be successfully used for separate detection of materials differing in their effective atomic number Z eff and local density (e.g., calcium contents in bone densitometry)

  6. Multiple matching scheme for broadband 0.72Pb(Mg(13)Nb(23))O(3)-0.28PbTiO(3) single crystal phased-array transducer.

    Science.gov (United States)

    Lau, S T; Li, H; Wong, K S; Zhou, Q F; Zhou, D; Li, Y C; Luo, H S; Shung, K K; Dai, J Y

    2009-05-01

    Lead magnesium niobate-lead titanate single crystal 0.72Pb(Mg(13)Nb(23))O(3)-0.28PbTiO(3) (abbreviated as PMN-PT) was used to fabricate high performance ultrasonic phased-array transducer as it exhibited excellent piezoelectric properties. In this paper, we focus on the design and fabrication of a low-loss and wide-band transducer for medical imaging applications. A KLM model based simulation software PiezoCAD was used for acoustic design of the transducer including the front-face matching and backing. The calculated results show that the -6 dB transducer bandwidth can be improved significantly by using double lambda8 matching layers and hard backing. A 4.0 MHz PMN-PT transducer array (with 16 elements) was fabricated and tested in a pulse-echo arrangement. A -6 dB bandwidth of 110% and two-way insertion loss of -46.5 dB were achieved.

  7. Characterization of ParTI Phoswiches Using Charged Pion Beams

    Science.gov (United States)

    Churchman, Emily; Zarrella, Andrew; Youngs, Michael; Yennello, Sherry

    2017-09-01

    The Partial Truncated Icosahedron (ParTI) detector array consists of 15 phoswiches. Each phoswich is made of two scintillating components - a thallium-doped cesium iodide (CsI(Tl)) crystal and an EJ-212 scintillating plastic - coupled to a photomultiplier tube. Both materials have different scintillation times and are sensitive to both charged and neutral particles. The type of particle and amount of energy deposited determine the shape of the scintillation pulse as a function of time. By integrating the fast and slow signals of the scintillation pulses, a ``Fast vs. Slow Integration'' plot can be created that produces particle identification lines based on the energy deposited in the scintillating materials. Four of these phoswiches were taken to the Paul Scherrer Institute (PSI) in Switzerland where π + , π-, and proton beams were scattered onto the phoswiches to demonstrate their particle identification (PID) capabilities. Using digitizers to record the detector response waveforms, pions can also be identified by the characteristic decay pulse of the muon daughters.

  8. A front-end electronic system for large arrays of bolometers

    Science.gov (United States)

    Arnaboldi, C.; Carniti, P.; Cassina, L.; Gotti, C.; Liu, X.; Maino, M.; Pessina, G.; Rosenfeld, C.; Zhu, B. X.

    2018-02-01

    CUORE is an array of thermal calorimeters composed of 988 crystals held at about 10 mK, whose absorbed energy is read out with semiconductor thermistors. The composition of the crystal is TeO2, and the aim is the study of the double beta decay of 130Te on very long and stable runs. CUPID-0 is an array of 26 Zn82Se crystals with double thermistor readout to study the double beta decay of 82Se. In the present paper, we present an overview of the entire front-end electronic readout chain, from the preamplifier to the anti-aliasing filter. This overview includes motivations, design strategies, circuit implementation and performance results of the electronic system, including other auxiliary yet important elements like power supplies and the slow control communication system. The stringent requirements of stability on the very long experimental runs that are foreseen during CUORE and CUPID-0 operation, are achieved thanks to novel solutions of the front-end preamplifier and of the detector bias circuit setup.

  9. Development and performance of charged particle detectors applied to the study of heavy ion reactions; Developpement et performances de detecteurs de particules chargees appliques a l`etude des reactions avec ions lourds

    Energy Technology Data Exchange (ETDEWEB)

    Gourde, M; Beaulieu, L; Dore, D; Laforest, R; Pouliot, J; Roy, R; St-Pierre, C [Laval Univ., Quebec City, PQ (Canada). Dept. de Physique

    1994-12-31

    The new type of charged particle detector described comprises a thin layer of plastic scintillator over a much thicker CsI(Tl) crystal, an optical guide, and a photomultiplier. Results obtained at Chalk River Laboratories for the identification of particles with Z = 1-6 from the {sup 12}C + {sup 197}Au reaction are shown. 12 refs., 4 figs.

  10. CaloCube: a novel calorimeter for high-energy cosmic rays in space

    Directory of Open Access Journals (Sweden)

    Rappoldi A.

    2017-01-01

    Full Text Available CaloCube is an R&D project borne to develop a novel calorimeter design, optimized for high-energy cosmic ray measurements in space. A small prototype made of CsI(Tl elements has been built and tested on particle beams. A final version, made of 5×5×18 crystals and with dual readout (two photodiodes for each crystal, to cover the full required dynamic range, is under construction and will be tested at CERN SPS in Summer 2016. The dual readout compensation technique were developed and the feasibility to extract Čerenkov signals from CsI crystals verified.

  11. An algorithm for automatic crystal identification in pixelated scintillation detectors using thin plate splines and Gaussian mixture models.

    Science.gov (United States)

    Schellenberg, Graham; Stortz, Greg; Goertzen, Andrew L

    2016-02-07

    A typical positron emission tomography detector is comprised of a scintillator crystal array coupled to a photodetector array or other position sensitive detector. Such detectors using light sharing to read out crystal elements require the creation of a crystal lookup table (CLUT) that maps the detector response to the crystal of interaction based on the x-y position of the event calculated through Anger-type logic. It is vital for system performance that these CLUTs be accurate so that the location of events can be accurately identified and so that crystal-specific corrections, such as energy windowing or time alignment, can be applied. While using manual segmentation of the flood image to create the CLUT is a simple and reliable approach, it is both tedious and time consuming for systems with large numbers of crystal elements. In this work we describe the development of an automated algorithm for CLUT generation that uses a Gaussian mixture model paired with thin plate splines (TPS) to iteratively fit a crystal layout template that includes the crystal numbering pattern. Starting from a region of stability, Gaussians are individually fit to data corresponding to crystal locations while simultaneously updating a TPS for predicting future Gaussian locations at the edge of a region of interest that grows as individual Gaussians converge to crystal locations. The algorithm was tested with flood image data collected from 16 detector modules, each consisting of a 409 crystal dual-layer offset LYSO crystal array readout by a 32 pixel SiPM array. For these detector flood images, depending on user defined input parameters, the algorithm runtime ranged between 17.5-82.5 s per detector on a single core of an Intel i7 processor. The method maintained an accuracy above 99.8% across all tests, with the majority of errors being localized to error prone corner regions. This method can be easily extended for use with other detector types through adjustment of the initial

  12. An algorithm for automatic crystal identification in pixelated scintillation detectors using thin plate splines and Gaussian mixture models

    International Nuclear Information System (INIS)

    Schellenberg, Graham; Goertzen, Andrew L; Stortz, Greg

    2016-01-01

    A typical positron emission tomography detector is comprised of a scintillator crystal array coupled to a photodetector array or other position sensitive detector. Such detectors using light sharing to read out crystal elements require the creation of a crystal lookup table (CLUT) that maps the detector response to the crystal of interaction based on the x–y position of the event calculated through Anger-type logic. It is vital for system performance that these CLUTs be accurate so that the location of events can be accurately identified and so that crystal-specific corrections, such as energy windowing or time alignment, can be applied. While using manual segmentation of the flood image to create the CLUT is a simple and reliable approach, it is both tedious and time consuming for systems with large numbers of crystal elements. In this work we describe the development of an automated algorithm for CLUT generation that uses a Gaussian mixture model paired with thin plate splines (TPS) to iteratively fit a crystal layout template that includes the crystal numbering pattern. Starting from a region of stability, Gaussians are individually fit to data corresponding to crystal locations while simultaneously updating a TPS for predicting future Gaussian locations at the edge of a region of interest that grows as individual Gaussians converge to crystal locations. The algorithm was tested with flood image data collected from 16 detector modules, each consisting of a 409 crystal dual-layer offset LYSO crystal array readout by a 32 pixel SiPM array. For these detector flood images, depending on user defined input parameters, the algorithm runtime ranged between 17.5–82.5 s per detector on a single core of an Intel i7 processor. The method maintained an accuracy above 99.8% across all tests, with the majority of errors being localized to error prone corner regions. This method can be easily extended for use with other detector types through adjustment of the initial

  13. An algorithm for automatic crystal identification in pixelated scintillation detectors using thin plate splines and Gaussian mixture models

    Science.gov (United States)

    Schellenberg, Graham; Stortz, Greg; Goertzen, Andrew L.

    2016-02-01

    A typical positron emission tomography detector is comprised of a scintillator crystal array coupled to a photodetector array or other position sensitive detector. Such detectors using light sharing to read out crystal elements require the creation of a crystal lookup table (CLUT) that maps the detector response to the crystal of interaction based on the x-y position of the event calculated through Anger-type logic. It is vital for system performance that these CLUTs be accurate so that the location of events can be accurately identified and so that crystal-specific corrections, such as energy windowing or time alignment, can be applied. While using manual segmentation of the flood image to create the CLUT is a simple and reliable approach, it is both tedious and time consuming for systems with large numbers of crystal elements. In this work we describe the development of an automated algorithm for CLUT generation that uses a Gaussian mixture model paired with thin plate splines (TPS) to iteratively fit a crystal layout template that includes the crystal numbering pattern. Starting from a region of stability, Gaussians are individually fit to data corresponding to crystal locations while simultaneously updating a TPS for predicting future Gaussian locations at the edge of a region of interest that grows as individual Gaussians converge to crystal locations. The algorithm was tested with flood image data collected from 16 detector modules, each consisting of a 409 crystal dual-layer offset LYSO crystal array readout by a 32 pixel SiPM array. For these detector flood images, depending on user defined input parameters, the algorithm runtime ranged between 17.5-82.5 s per detector on a single core of an Intel i7 processor. The method maintained an accuracy above 99.8% across all tests, with the majority of errors being localized to error prone corner regions. This method can be easily extended for use with other detector types through adjustment of the initial

  14. Review of aragonite and calcite crystal morphogenesis in thermal spring systems

    Science.gov (United States)

    Jones, Brian

    2017-06-01

    Aragonite and calcite crystals are the fundamental building blocks of calcareous thermal spring deposits. The diverse array of crystal morphologies found in these deposits, which includes monocrystals, mesocrystals, skeletal crystals, dendrites, and spherulites, are commonly precipitated under far-from-equilibrium conditions. Such crystals form through both abiotic and biotic processes. Many crystals develop through non-classical crystal growth models that involve the arrangement of nanocrystals in a precisely controlled crystallographic register. Calcite crystal morphogenesis has commonly been linked to a ;driving force;, which is a conceptual measure of the distance of the growth conditions from equilibrium conditions. Essentially, this scheme indicates that increasing levels of supersaturation and various other parameters that produce a progressive change from monocrystals and mesocrystals to skeletal crystals to crystallographic and non-crystallographic dendrites, to dumbbells, to spherulites. Despite the vast amount of information available from laboratory experiments and natural spring systems, the precise factors that control the driving force are open to debate. The fact that calcite crystal morphogenesis is still poorly understood is largely a reflection of the complexity of the factors that influence aragonite and calcite precipitation. Available information indicates that variations in calcite crystal morphogenesis can be attributed to physical and chemical parameters of the parent water, the presence of impurities, the addition of organic or inorganic additives to the water, the rate of crystal growth, and/or the presence of microbes and their associated biofilms. The problems in trying to relate crystal morphogenesis to specific environmental parameters arise because it is generally impossible to disentangle the controlling factor(s) from the vast array of potential parameters that may act alone or in unison with each other.

  15. Performance analysis of solar cell arrays in concentrating light intensity

    International Nuclear Information System (INIS)

    Xu Yongfeng; Li Ming; Lin Wenxian; Wang Liuling; Xiang Ming; Zhang Xinghua; Wang Yunfeng; Wei Shengxian

    2009-01-01

    Performance of concentrating photovoltaic/thermal system is researched by experiment and simulation calculation. The results show that the I-V curve of the GaAs cell array is better than that of crystal silicon solar cell arrays and the exergy produced by 9.51% electrical efficiency of the GaAs solar cell array can reach 68.93% of the photovoltaic/thermal system. So improving the efficiency of solar cell arrays can introduce more exergy and the system value can be upgraded. At the same time, affecting factors of solar cell arrays such as series resistance, temperature and solar irradiance also have been analyzed. The output performance of a solar cell array with lower series resistance is better and the working temperature has a negative impact on the voltage in concentrating light intensity. The output power has a -20 W/V coefficient and so cooling fluid must be used. Both heat energy and electrical power are then obtained with a solar trough concentrating photovoltaic/thermal system. (semiconductor devices)

  16. Waveguiding in supported phononic crystal plates

    International Nuclear Information System (INIS)

    Vasseur, J; Hladky-Hennion, A-C; Deymier, P; Djafari-Rouhani, B; Duval, F; Dubus, B; Pennec, Y

    2007-01-01

    We investigate, with the help of the finite element method, the existence of absolute band gaps in the band structure of a free-standing phononic crystal plate and of a phononic crystal slab deposited on a substrate. The two-dimensional phononic crystal is constituted by a square array of holes drilled in an active piezoelectric (PZT5A or AlN) matrix. For both matrix materials, an absolute band gap occurs in the band structure of the free-standing plate provided the thickness of the plate is on the order of magnitude of the lattice parameter. When the plate is deposited on a Si substrate, the absolute band gap still remains when the matrix of the phononic crystal is made of PZT5A. The AlN phononic crystal plate losses its gap when supported by the Si substrate. In the case of the PZT5A matrix, we also study the possibility of localized modes associated with a linear defect created by removing one row of air holes in the deposited phononic crystal plate

  17. Self-organized TiO2 nanotubular arrays for photoelectrochemical hydrogen generation: effect of crystallization and defect structures

    International Nuclear Information System (INIS)

    Mahajan, V K; Misra, M; Raja, K S; Mohapatra, S K

    2008-01-01

    The effect of crystallization and surface chemistry of nanotubular titanium dioxide (TiO 2 ) in connection with the photoelectrochemical process is reported in this investigation. TiO 2 nanotubular arrays were synthesized by a simple anodization process in an acidified fluoride electrolyte at room temperature. The TiO 2 nanotubes were amorphous in as-anodized condition; their transformation to crystalline phases was a function of annealing temperature and gaseous environment. The anatase phase was observed predominantly after annealing in non-oxidizing atmospheres, whereas annealing in an oxygen environment showed a mixture of anatase and rutile phases. X-ray photoelectron spectroscopy was used to determine the chemical environment of the surface, which revealed the presence of phosphate, oxygen vacancies and pentacoordinated Ti in hydrogen annealed samples. Diffuse reflectance photospectrometry of non-oxygen annealed samples showed long absorption tails extending in the visible region. The photoelectrochemical response of the TiO 2 nanotubes annealed in different conditions was investigated. Photoelectrochemical performance under simulated solar light was improved by annealing the nanotubular TiO 2 samples in non-oxidizing environment

  18. ZnO nanorod arrays grown under different pressures and their photoluminescence properties

    Energy Technology Data Exchange (ETDEWEB)

    Meng Xiuqing [Key Laboratory of Excited State Processes, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, 16 East Nan-Hu Road, Open Economic ZoneChangchun 130033 (China); Graduate School of the Chinese Academy of Sciences (China); Zhao Dongxu [Key Laboratory of Excited State Processes, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, 16 East Nan-Hu Road, Open Economic ZoneChangchun 130033 (China)]. E-mail: dxzhao2000@yahoo.com.cn; Shen Dezhen [Key Laboratory of Excited State Processes, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, 16 East Nan-Hu Road, Open Economic ZoneChangchun 130033 (China); Zhang Jiying [Key Laboratory of Excited State Processes, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, 16 East Nan-Hu Road, Open Economic ZoneChangchun 130033 (China); Li Binghui [Key Laboratory of Excited State Processes, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, 16 East Nan-Hu Road, Open Economic ZoneChangchun 130033 (China); Wang Xiaohua [National Key Laboratory of High Power Semiconductor Laser, Changchun University of Science and technology, 7089 Weixing Road Changchun (China); Fan Xiwu [Key Laboratory of Excited State Processes, Changchun Institute of Optics, Fine Mechanics and Physics, Chinese Academy of Sciences, 16 East Nan-Hu Road, Open Economic ZoneChangchun 130033 (China)

    2007-01-15

    The ZnO nanorod arrays were synthesized via a simple vapor deposition method on Si (1 1 1) substrates at a low growth temperature of 520 deg. C. By selecting different source materials under different growth pressures, well-aligned hexagonal-shaped ZnO nanorod arrays were obtained under both conditions. X-ray diffraction (XRD) analysis confirmed the nanorods are c-axis orientated. Selected area electron diffraction (SAED) and transmission electron microscopy (TEM) analysis demonstrated the individual nanorod is single crystal. Photoluminescence (PL) analyses show the superior optical properties of the nanorod arrays.

  19. ZnO nanorod arrays grown under different pressures and their photoluminescence properties

    International Nuclear Information System (INIS)

    Meng Xiuqing; Zhao Dongxu; Shen Dezhen; Zhang Jiying; Li Binghui; Wang Xiaohua; Fan Xiwu

    2007-01-01

    The ZnO nanorod arrays were synthesized via a simple vapor deposition method on Si (1 1 1) substrates at a low growth temperature of 520 deg. C. By selecting different source materials under different growth pressures, well-aligned hexagonal-shaped ZnO nanorod arrays were obtained under both conditions. X-ray diffraction (XRD) analysis confirmed the nanorods are c-axis orientated. Selected area electron diffraction (SAED) and transmission electron microscopy (TEM) analysis demonstrated the individual nanorod is single crystal. Photoluminescence (PL) analyses show the superior optical properties of the nanorod arrays

  20. Improved Light Extraction Efficiency by Photonic Crystal Arrays on Transparent Contact Layer Using Focused Ion Beams

    International Nuclear Information System (INIS)

    Wu, G.M.; Tsai, B.H.; Kung, S.F.; Wu, C.F.

    2011-01-01

    Nitride-based thin-film materials have become increasingly important for the high brightness light-emitting diode applications. The improvements in light extraction and lower power consumption are highly desired. Although the internal quantum efficiency of GaN-based LED has been relatively high, only a small fraction of light can be extracted. In this study, a new design of two-dimensional photonic crystal array has been prepared on the top transparent contact layer of indium-tin oxide film to improve the light extraction efficiency using focused ion beam. The acceleration voltage of the Ga dual-beam nanotechnology system SMI 3050 was 30 kV and the ion beam current was 100 pA. The cylindrical air holes had the diameter of 150 nm and depth of 100 nm. The micro photoluminescence analysis results showed that the light output intensity could be 1.5 times of that of the non-patterned control sample. In addition, the structural damage from the focused ion beam drilling of GaN step could be eliminated. The excellent I-V characteristics have been maintained, and the external light extraction efficiency would be still improved for the LED devices. (author)

  1. Dispersive photonic crystals from the plane wave method

    Energy Technology Data Exchange (ETDEWEB)

    Guevara-Cabrera, E.; Palomino-Ovando, M.A. [Facultad de Ciencias Físico Matemáticas, Benemérita Universidad Autónoma de Puebla, Apdo. Post. 165, Puebla, Pue. 72000, México (Mexico); Flores-Desirena, B., E-mail: bflores@fcfm.buap.mx [Facultad de Ciencias Físico Matemáticas, Benemérita Universidad Autónoma de Puebla, Apdo. Post. 165, Puebla, Pue. 72000, México (Mexico); Gaspar-Armenta, J.A. [Departamento de Investigación en Física de la Universidad de Sonora Apdo, Post 5-088, Hermosillo Sonora 83190, México (Mexico)

    2016-03-01

    Nowadays photonic crystals are widely used in many different applications. One of the most used methods to compute their band structure is the plane wave method (PWM). However, it can only be applied directly to non-dispersive media and be extended to systems with a few model dielectric functions. We explore an extension of the PWM to photonic crystals containing dispersive materials, that solves an eigenvalue equation for the Bloch wave vectors. First we compare our calculation with analytical results for one dimensional photonic crystals containing Si using experimental values of its optical parameters, and obtainig very well agreement, even for the spectrum region with strong absorption. Then, using the same method, we computed the band structure for a two dimensional photonic crystal without absorption, formed by an square array of MgO cylinders in air. The optical parameters for MgO were modeled with the Lorentz dielectric function. Finally, we studied an array of MgO cylinders in a metal, using Drude model without absorption, for the metal dielectric function. For this last case, we study the gap–midgap ratio as a function of the filling fraction for both the square and triangular lattice. The gap–midgap ratio is larger for the triangular lattice, with a maximum value of 10% for a filling fraction of 0.6. Our results show that the method can be applied to dispersive materials, and then to a wide range of applications where photonic crystals can be used.

  2. Superhydrophobic hierarchical arrays fabricated by a scalable colloidal lithography approach.

    Science.gov (United States)

    Kothary, Pratik; Dou, Xuan; Fang, Yin; Gu, Zhuxiao; Leo, Sin-Yen; Jiang, Peng

    2017-02-01

    Here we report an unconventional colloidal lithography approach for fabricating a variety of periodic polymer nanostructures with tunable geometries and hydrophobic properties. Wafer-sized, double-layer, non-close-packed silica colloidal crystal embedded in a polymer matrix is first assembled by a scalable spin-coating technology. The unusual non-close-packed crystal structure combined with a thin polymer film separating the top and the bottom colloidal layers render great versatility in templating periodic nanostructures, including arrays of nanovoids, nanorings, and hierarchical nanovoids. These different geometries result in varied fractions of entrapped air in between the templated nanostructures, which in turn lead to different apparent water contact angles. Superhydrophobic surfaces with >150° water contact angles and <5° contact angle hysteresis are achieved on fluorosilane-modified polymer hierarchical nanovoid arrays with large fractions of entrapped air. The experimental contact angle measurements are complemented with theoretical predictions using the Cassie's model to gain insights into the fundamental microstructure-dewetting property relationships. The experimental and theoretical contact angles follow the same trends as determined by the unique hierarchical structures of the templated periodic arrays. Copyright © 2016 Elsevier Inc. All rights reserved.

  3. Fabrication and characterization of nano-gas sensor arrays

    International Nuclear Information System (INIS)

    Hassan, H. S.; Kashyout, A. B.; Morsi, I.; Nasser, A. A. A.; Raafat, A.

    2015-01-01

    A novel structures of Nanomaterials gas sensors array constructed using ZnO, and ZnO doped with Al via sol-gel technique. Two structure arrays are developed; the first one is a double sensor array based on doping with percentages of 1% and 5%. The second is a quadrature sensor array based on several doping ratios concentrations (0%, 1%, 5% and 10%). The morphological structures of prepared ZnO were revealed using scanning electron microscope (SEM). X-ray diffraction (XRD) patterns reveal a highly crystallized wurtzite structure and used for identifying phase structure and chemical state of both ZnO and ZnO doped with Al under different preparation conditions and different doping ratios. Chemical composition of Al-doped ZnO nanopowders was performed using energy dispersive x-ray (EDS) analysis. The electrical characteristics of the sensor are determined by measuring the two terminal sensor’s output resistance for O 2 , H 2 and CO 2 gases as a function of temperature

  4. Fabrication and characterization of nano-gas sensor arrays

    Energy Technology Data Exchange (ETDEWEB)

    Hassan, H. S., E-mail: hassan.shokry@gmail.com; Kashyout, A. B., E-mail: hady8@yahoo.com [Electronic Materials Researches Department, Advanced Technology and New Materials Research Institute, City of Scientific Researches and technological applications, New Borg El-Arab City, Alexandria (Egypt); Morsi, I., E-mail: drimanmorsi@yahoo.com; Nasser, A. A. A., E-mail: menem-1954@yahoo.com; Raafat, A., E-mail: abrs-218@yahoo.com [Arab Academy for Science and Technology, and Maritime Transport, Alexandria, 21936 (Egypt)

    2015-03-30

    A novel structures of Nanomaterials gas sensors array constructed using ZnO, and ZnO doped with Al via sol-gel technique. Two structure arrays are developed; the first one is a double sensor array based on doping with percentages of 1% and 5%. The second is a quadrature sensor array based on several doping ratios concentrations (0%, 1%, 5% and 10%). The morphological structures of prepared ZnO were revealed using scanning electron microscope (SEM). X-ray diffraction (XRD) patterns reveal a highly crystallized wurtzite structure and used for identifying phase structure and chemical state of both ZnO and ZnO doped with Al under different preparation conditions and different doping ratios. Chemical composition of Al-doped ZnO nanopowders was performed using energy dispersive x-ray (EDS) analysis. The electrical characteristics of the sensor are determined by measuring the two terminal sensor’s output resistance for O{sub 2}, H{sub 2} and CO{sub 2} gases as a function of temperature.

  5. Evaluation of digital detector arrays systems for industrial radiography

    International Nuclear Information System (INIS)

    Silva, Aline S.S.; Oliveira, Davi F.; Gomes, Célio S.; Azeredo, Soraia R.; Lopes, Ricardo T.

    2017-01-01

    Digital Detector Arrays (DDA) or Flat Panel Detector (FPD) is a highly efficient technique that is used in nondestructive testing of internal features of an object. The evaluation of DDA systems for industrial radiography is important to ensure the image quality and to enables long-term stability of this system. This evaluation is specified by ASTM E2737 - 10, which describes the fundamental parameters of DDA systems to be measured. The tests require the usage of either the five-groove wedge or the duplex plate phantom with separate Image Quality Indicators (IQIs). The purpose of this work was evaluate the radiographic performance achieved using both techniques in two DDA systems manufactured by GEIT: DXR250P and DXR250V, which have thallium-doped cesium iodide (CsI:Tl) and terbium-doped gadolinium oxysulfide (Gd 2 O 2 S:Tb - GOS) scintillators, respectively. For this purpose, it was used an X-ray equipment as radiation source. The image quality parameters analyzed were Image Lag (IL), Offset Level (OL), Bad Pixel distribution, Burn In (BI), Spatial Resolution (SR), Material Thickness Range (MTR), Contrast Sensitivity (CS), Signal Level (SL) and Signal-to-Noise Ratio (SNR). As result of this study, has been observed that the use of the five-groove wedge phantom made the measurements to become easier to execute. Regarding the DDA system, the DXR250P presented more IL and BI, but produced images with better CS and SNR and needed a dose almost twice smaller than the DXR250V to achieve a similar SL. (author)

  6. Evaluation of digital detector arrays systems for industrial radiography

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Aline S.S.; Oliveira, Davi F.; Gomes, Célio S.; Azeredo, Soraia R.; Lopes, Ricardo T., E-mail: aline@lin.ufrj.br, E-mail: davi@lin.ufrj.br.br, E-mail: celio@lin.ufrj.br, E-mail: soraia@lin.ufrj.br, E-mail: ricardo@lin.ufrj.br, E-mail: davi.oliveira@uerj.br [Coordenacao de Pos-Graduacao e Pesquisa de Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Lab. de Instrumentação Nuclear

    2017-07-01

    Digital Detector Arrays (DDA) or Flat Panel Detector (FPD) is a highly efficient technique that is used in nondestructive testing of internal features of an object. The evaluation of DDA systems for industrial radiography is important to ensure the image quality and to enables long-term stability of this system. This evaluation is specified by ASTM E2737 - 10, which describes the fundamental parameters of DDA systems to be measured. The tests require the usage of either the five-groove wedge or the duplex plate phantom with separate Image Quality Indicators (IQIs). The purpose of this work was evaluate the radiographic performance achieved using both techniques in two DDA systems manufactured by GEIT: DXR250P and DXR250V, which have thallium-doped cesium iodide (CsI:Tl) and terbium-doped gadolinium oxysulfide (Gd{sub 2}O{sub 2}S:Tb - GOS) scintillators, respectively. For this purpose, it was used an X-ray equipment as radiation source. The image quality parameters analyzed were Image Lag (IL), Offset Level (OL), Bad Pixel distribution, Burn In (BI), Spatial Resolution (SR), Material Thickness Range (MTR), Contrast Sensitivity (CS), Signal Level (SL) and Signal-to-Noise Ratio (SNR). As result of this study, has been observed that the use of the five-groove wedge phantom made the measurements to become easier to execute. Regarding the DDA system, the DXR250P presented more IL and BI, but produced images with better CS and SNR and needed a dose almost twice smaller than the DXR250V to achieve a similar SL. (author)

  7. Optimized orientation of 0.71Pb(Mg1/3Nb2/3)O3-0.29PbTiO3 single crystal for applications in medical ultrasonic arrays

    Science.gov (United States)

    Zhou, Dan; Chen, Jing; Luo, Laihui; Zhao, Xiangyong; Luo, Haosu

    2008-08-01

    In order to extend the potential applications of medical ultrasonic array transducers, two optimized directions with the maximal electromechanical coefficient k33' and minimal k31 are determined for [001] and [110] poled 0.71Pb(Mg1/3Nb2/3)O3-0.29PbTiO3 single crystals using the experimental method. The maximum values of k33' can reach 92.8% and 93.3%, respectively, corresponding to [001]W/[110]L and [110]W/[1-11]L cuts. Furthermore, we simulate the performances of three 3.5 MHz linear array transducers based on the determined directions by PIEZOCAD. Results indicate that under the [001]W/[110]L direction, 25% broader bandwidth, 40% shorter pulse length, and 3 dB higher sensitivity can be obtained compared to the traditional Pb(Zr1-xTix)O3 transducers.

  8. Four-layer DOI PET detectors using a multi-pixel photon counter array and the light sharing method

    Energy Technology Data Exchange (ETDEWEB)

    Nishikido, Fumihiko, E-mail: funis@nirs.go.jp; Inadama, Naoko; Yoshida, Eiji; Murayama, Hideo; Yamaya, Taiga

    2013-11-21

    Silicon photomultipliers (SiPMs) provide many advantages for PET detectors, such as their high internal gain, high photon detection efficiency and insensitivity to magnetic fields. The number of detectable scintillation photons of SiPMs, however, is limited by the number of microcells. Therefore, pulse height of PET detectors using SiPMs is saturated when large numbers of scintillation photons enter the SiPM pixels. On the other hand, we previously presented a depth-of-interaction (DOI) encoding method that is based on the light sharing method. Since our encoding method detects scintillation photons with multiple readout pixels, the saturation effect can be suppressed. We constructed two prototype four-layer DOI detectors using a SiPM array and evaluated their performances. The two prototype detectors consisted of four layers of a 6×6 array of Lu{sub 2(1−x)}Y{sub 2x}SiO{sub 5} (LYSO) crystals and a SiPM (multi-pixel photon detector, MPPC, Hamamatsu Photonics K.K.) array of 4×4 pixels. The size of each LYSO crystal element was 1.46 mm×1.46 mm×4.5 mm and all surfaces of the crystal elements were chemically etched. We used two types of MPPCs. The first one had 3600 microcells and high photon detection efficiency (PDE). The other one had 14,400 microcells and lower PDE. In the evaluation experiment, all the crystals of the detector using the MPPC which had the high PDE were clearly identified. The respective energy and timing resolutions of lower than 15% and 1.0 ns were achieved for each crystal element. No saturation of output signals was observed in the 511 keV energy region due to suppression of the saturation effect by detecting scintillation photons with several MPPC pixels by the light sharing method. -- Highlights: •We constructed and evaluated four-layer DOI detectors by the light sharing method using a MPPC array. •The detectors using two types of the MPPC array were compared. •The energy and timing resolutions of lower than 15% and 1.0 ns were

  9. Four-layer DOI PET detectors using a multi-pixel photon counter array and the light sharing method

    International Nuclear Information System (INIS)

    Nishikido, Fumihiko; Inadama, Naoko; Yoshida, Eiji; Murayama, Hideo; Yamaya, Taiga

    2013-01-01

    Silicon photomultipliers (SiPMs) provide many advantages for PET detectors, such as their high internal gain, high photon detection efficiency and insensitivity to magnetic fields. The number of detectable scintillation photons of SiPMs, however, is limited by the number of microcells. Therefore, pulse height of PET detectors using SiPMs is saturated when large numbers of scintillation photons enter the SiPM pixels. On the other hand, we previously presented a depth-of-interaction (DOI) encoding method that is based on the light sharing method. Since our encoding method detects scintillation photons with multiple readout pixels, the saturation effect can be suppressed. We constructed two prototype four-layer DOI detectors using a SiPM array and evaluated their performances. The two prototype detectors consisted of four layers of a 6×6 array of Lu 2(1−x) Y 2x SiO 5 (LYSO) crystals and a SiPM (multi-pixel photon detector, MPPC, Hamamatsu Photonics K.K.) array of 4×4 pixels. The size of each LYSO crystal element was 1.46 mm×1.46 mm×4.5 mm and all surfaces of the crystal elements were chemically etched. We used two types of MPPCs. The first one had 3600 microcells and high photon detection efficiency (PDE). The other one had 14,400 microcells and lower PDE. In the evaluation experiment, all the crystals of the detector using the MPPC which had the high PDE were clearly identified. The respective energy and timing resolutions of lower than 15% and 1.0 ns were achieved for each crystal element. No saturation of output signals was observed in the 511 keV energy region due to suppression of the saturation effect by detecting scintillation photons with several MPPC pixels by the light sharing method. -- Highlights: •We constructed and evaluated four-layer DOI detectors by the light sharing method using a MPPC array. •The detectors using two types of the MPPC array were compared. •The energy and timing resolutions of lower than 15% and 1.0 ns were achieved for

  10. Instruments and detectors on the base of scintillator crystals ZnSe(Te), CWO, CsI(Tl) for systems of security and customs inspection systems

    International Nuclear Information System (INIS)

    Ryzhikov, V.D.; Opolonin, A.D.; Pashko, P.V.; Svishch, V.M.; Volkov, V.G.; Lysetskaya, E.K.; Kozin, D.N.; Smith, C.

    2005-01-01

    Results of experimental studies of detector arrays scintillator-photodiode (S-PD) and scintillator-photoreceiving device (S-PRD) used for X-ray digital radiography have shown that there exist further possibilities to increase spatial resolution of this system up to 2-3 line pairs per mm. Theoretical analysis and experimental studies show that the two-energy detection method not only allows one to detect organics on the background of metal, but also substantially increases (by 3-5 times) the detection ability of the system as a whole, especially if parameters of the S-PD pair are optimized, in particular, when ZnSe(Te) is used in the low-energy circuit. A possibility to distinguish, in principle, between substances with insignificant differences in atomic number has been theoretically proven--by transition to multi-energy radiography. 3D-imaging has been realized using S-PD detector arrays. On base of theoretical and experimental search was installation of several types of inspection systems for control objects with square size 0.4x0.6-2.5x3.5 m

  11. Design, development and evaluation of a resistor-based multiplexing circuit for a 20×20 SiPM array

    International Nuclear Information System (INIS)

    Wang, Zhonghai; Sun, Xishan; Lou, Kai; Meier, Joseph; Zhou, Rong; Yang, Chaowen; Zhu, Xiaorong; Shao, Yiping

    2016-01-01

    One technical challenge in developing a large-size scintillator detector with multiple Silicon Photomultiplier (SiPM) arrays is to read out a large number of detector output channels. To achieve this, different signal multiplexing circuits have been studied and applied with different performances and cost-effective tradeoffs. Resistor-based multiplexing circuits exhibit simplicity and signal integrity, but also present the disadvantage of timing shift among different channels. In this study, a resistor-based multiplexing circuit for a large-sized SiPM array readout was developed and evaluated by simulation and experimental studies. Similarly to a multiplexing circuit used for multi-anode PMT, grounding and branching resistors were connected to each SiPM output channel. The grounding resistor was used to simultaneously reduce the signal crosstalk among different channels and to improve timing performance. Both grounding and branching resistor values were optimized to maintain a balanced performance of the event energy, timing, and positioning. A multiplexing circuit was implemented on a compact PCB and applied for a flat-panel detector which consisted of a 32×32 LYSO scintillator crystals optically coupled to 5×5 SiPM arrays for a total 20×20 output channels. Test results showed excellent crystal identification for all 1024 LYSO crystals (each with 2×2×30 mm"3 size) with "2"2Na flood-source irradiation. The measured peak-to-valley ratio from typical crystal map profile is around 3:1 to 6.6:1, an average single crystal energy resolution of about 17.3%, and an average single crystal timing resolution of about 2 ns. Timing shift among different crystals, as reported in some other resistor-based multiplexing circuit designs, was not observed. In summary, we have designed and implemented a practical resistor-based multiplexing circuit that can be readily applied for reading out a large SiPM array with good detector performance.

  12. Design, development and evaluation of a resistor-based multiplexing circuit for a 20×20 SiPM array

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Zhonghai [College of Physical Science and Technology, Key Laboratory of Radiation Physics and Technology, Ministry of Education, Sichuan University, Chengdu (China); Department of Radiation Oncology, University of Texas Southwestern Medical Center, Dallas, Tx (United States); Sun, Xishan [Department of Radiation Oncology, University of Texas Southwestern Medical Center, Dallas, Tx (United States); Lou, Kai [Department of Electrical and Computer Engineering, Rice University, Houston, Tx (United States); Meier, Joseph [Department of Imaging Physics, The University of Texas MD Anderson Cancer Center, Houston, Tx (United States); Zhou, Rong; Yang, Chaowen [College of Physical Science and Technology, Key Laboratory of Radiation Physics and Technology, Ministry of Education, Sichuan University, Chengdu (China); Zhu, Xiaorong [Department of Radiation Physics, The University of Texas MD Anderson Cancer Center, Houston, Tx (United States); Shao, Yiping [Department of Radiation Oncology, University of Texas Southwestern Medical Center, Dallas, Tx (United States)

    2016-04-21

    One technical challenge in developing a large-size scintillator detector with multiple Silicon Photomultiplier (SiPM) arrays is to read out a large number of detector output channels. To achieve this, different signal multiplexing circuits have been studied and applied with different performances and cost-effective tradeoffs. Resistor-based multiplexing circuits exhibit simplicity and signal integrity, but also present the disadvantage of timing shift among different channels. In this study, a resistor-based multiplexing circuit for a large-sized SiPM array readout was developed and evaluated by simulation and experimental studies. Similarly to a multiplexing circuit used for multi-anode PMT, grounding and branching resistors were connected to each SiPM output channel. The grounding resistor was used to simultaneously reduce the signal crosstalk among different channels and to improve timing performance. Both grounding and branching resistor values were optimized to maintain a balanced performance of the event energy, timing, and positioning. A multiplexing circuit was implemented on a compact PCB and applied for a flat-panel detector which consisted of a 32×32 LYSO scintillator crystals optically coupled to 5×5 SiPM arrays for a total 20×20 output channels. Test results showed excellent crystal identification for all 1024 LYSO crystals (each with 2×2×30 mm{sup 3} size) with {sup 22}Na flood-source irradiation. The measured peak-to-valley ratio from typical crystal map profile is around 3:1 to 6.6:1, an average single crystal energy resolution of about 17.3%, and an average single crystal timing resolution of about 2 ns. Timing shift among different crystals, as reported in some other resistor-based multiplexing circuit designs, was not observed. In summary, we have designed and implemented a practical resistor-based multiplexing circuit that can be readily applied for reading out a large SiPM array with good detector performance.

  13. Pseudo-time-reversal symmetry and topological edge states in two-dimensional acoustic crystals

    KAUST Repository

    Mei, Jun

    2016-09-02

    We propose a simple two-dimensional acoustic crystal to realize topologically protected edge states for acoustic waves. The acoustic crystal is composed of a triangular array of core-shell cylinders embedded in a water host. By utilizing the point group symmetry of two doubly degenerate eigenstates at the Î

  14. Pseudo-time-reversal symmetry and topological edge states in two-dimensional acoustic crystals

    KAUST Repository

    Mei, Jun; Chen, Zeguo; Wu, Ying

    2016-01-01

    We propose a simple two-dimensional acoustic crystal to realize topologically protected edge states for acoustic waves. The acoustic crystal is composed of a triangular array of core-shell cylinders embedded in a water host. By utilizing the point group symmetry of two doubly degenerate eigenstates at the Î

  15. Nonlinear coherent structures in granular crystals

    Science.gov (United States)

    Chong, C.; Porter, Mason A.; Kevrekidis, P. G.; Daraio, C.

    2017-10-01

    The study of granular crystals, which are nonlinear metamaterials that consist of closely packed arrays of particles that interact elastically, is a vibrant area of research that combines ideas from disciplines such as materials science, nonlinear dynamics, and condensed-matter physics. Granular crystals exploit geometrical nonlinearities in their constitutive microstructure to produce properties (such as tunability and energy localization) that are not conventional to engineering materials and linear devices. In this topical review, we focus on recent experimental, computational, and theoretical results on nonlinear coherent structures in granular crystals. Such structures—which include traveling solitary waves, dispersive shock waves, and discrete breathers—have fascinating dynamics, including a diversity of both transient features and robust, long-lived patterns that emerge from broad classes of initial data. In our review, we primarily discuss phenomena in one-dimensional crystals, as most research to date has focused on such scenarios, but we also present some extensions to two-dimensional settings. Throughout the review, we highlight open problems and discuss a variety of potential engineering applications that arise from the rich dynamic response of granular crystals.

  16. Multiple matching scheme for broadband 0.72Pb(Mg1/3Nb2/3)O3-0.28PbTiO3 single crystal phased-array transducer

    Science.gov (United States)

    Lau, S. T.; Li, H.; Wong, K. S.; Zhou, Q. F.; Zhou, D.; Li, Y. C.; Luo, H. S.; Shung, K. K.; Dai, J. Y.

    2009-05-01

    Lead magnesium niobate-lead titanate single crystal 0.72Pb(Mg1/3Nb2/3)O3-0.28PbTiO3 (abbreviated as PMN-PT) was used to fabricate high performance ultrasonic phased-array transducer as it exhibited excellent piezoelectric properties. In this paper, we focus on the design and fabrication of a low-loss and wide-band transducer for medical imaging applications. A KLM model based simulation software PiezoCAD was used for acoustic design of the transducer including the front-face matching and backing. The calculated results show that the -6 dB transducer bandwidth can be improved significantly by using double λ /8 matching layers and hard backing. A 4.0 MHz PMN-PT transducer array (with 16 elements) was fabricated and tested in a pulse-echo arrangement. A -6 dB bandwidth of 110% and two-way insertion loss of -46.5 dB were achieved.

  17. Ordered arrays of embedded Ga nanoparticles on patterned silicon substrates

    International Nuclear Information System (INIS)

    Bollani, M; Bietti, S; Sanguinetti, S; Frigeri, C; Chrastina, D; Reyes, K; Smereka, P; Millunchick, J M; Vanacore, G M; Tagliaferri, A; Burghammer, M

    2014-01-01

    We fabricate site-controlled, ordered arrays of embedded Ga nanoparticles on Si, using a combination of substrate patterning and molecular-beam epitaxial growth. The fabrication process consists of two steps. Ga droplets are initially nucleated in an ordered array of inverted pyramidal pits, and then partially crystallized by exposure to an As flux, which promotes the formation of a GaAs shell that seals the Ga nanoparticle within two semiconductor layers. The nanoparticle formation process has been investigated through a combination of extensive chemical and structural characterization and theoretical kinetic Monte Carlo simulations. (papers)

  18. Photonic crystal resonator integrated in a microfluidic system

    DEFF Research Database (Denmark)

    Rodrigues de Sousa Nunes, Pedro André; Mortensen, Niels Asger; Kutter, Jörg Peter

    2008-01-01

    We report on a novel optofluidic system consisting of a silica-based 1D photonic crystal, integrated planar waveguides, and electrically insulated fluidic channels. An array of pillars in a microfluidic channel designed for electrochromatography is used as a resonator for on-column label...

  19. 1- to 10-keV x-ray backlighting of annular wire arrays on the Sandia Z-machine using bent-crystal imaging techniques

    International Nuclear Information System (INIS)

    Rambo, Patrick K.; Wenger, David Franklin; Bennett, Guy R.; Sinars, Daniel Brian; Smith, Ian Craig; Porter, John Larry Jr.; Cuneo, Michael Edward; Rovang, Dean Curtis; Anderson, Jessica E.

    2003-01-01

    Annular wire array implosions on the Sandia Z-machine can produce >200 TW and 1-2 MJ of soft x rays in the 0.1-10 keV range. The x-ray flux and debris in this environment present significant challenges for radiographic diagnostics. X-ray backlighting diagnostics at 1865 and 6181 eV using spherically-bent crystals have been fielded on the Z-machine, each with a ∼0.6 eVspectral bandpass, 10 (micro)m spatial resolution, and a 4 mm by 20mm field of view. The Z-Beamlet laser, a 2-TW, 2-kJ Nd:glass laser(λ = 527 nm), is used to produce 0.1-1 J x-ray sources for radiography. The design, calibration, and performance of these diagnostics is presented.

  20. Density of states functions for photonic crystals

    International Nuclear Information System (INIS)

    McPhedran, R.C.; McOrist, J.; Sterke, C.M. de; Nicorovici, N.A.; Botten, L.C.; Asatryan, A.A.

    2004-01-01

    We discuss density of states functions for photonic crystals, in the context of the two-dimensional problem for arrays of cylinders of arbitrary cross section. We introduce the mutual density of states (MDOS), and show that this function can be used to calculate both the local density of states (LDOS), which gives position information for emission of radiation from photonic crystals, and the spectral density of states (SDOS), which gives angular information. We establish the connection between MDOS, LDOS, SDOS and the conventional density of states, which depends only on frequency. We relate all four functions to the band structure and propagating states within the crystal, and give numerical examples of the relation between band structure and density of states functions

  1. Simulation and design of the photonic crystal microwave accelerating structure

    International Nuclear Information System (INIS)

    Song Ruiying; Wu Congfeng; He Xiaodong; Dong Sai

    2007-01-01

    The authors have derived the global band gaps for general two-dimensional (2D) photonic crystal microwave accelerating structures formed by square or triangular arrays of metal posts. A coordinate-space, finite-difference code was used to calculate the complete dispersion curves for the lattices. The fundamental and higher frequency global photonic band gaps were determined numerically. The structure formed by triangular arrays of metal posts with a missing rod at the center has advantages of higher-order-modes (HOM) suppression and main mode restriction under the condition of a/b<0.2. The relationship between the RF properties and the geometrical parameters have been studied for the 9.37 GHz photonic crystal accelerating structure. The Rs, Q, Rs/Q of the new structure may be comparable to the disk-loaded accelerating structure. (authors)

  2. Direct observation of two-step crystallization in nanoparticle superlattice formation

    Energy Technology Data Exchange (ETDEWEB)

    Park, Jungwon; Zheng, Haimei; Lee, Won Chul; Geissler, Phillip L.; Rabani, Eran; Alivisatos, A. Paul

    2011-10-06

    Direct imaging of nanoparticle solutions by liquid phase transmission electron microscopy has enabled unique in-situ studies of nanoparticle motion and growth. In the present work, we report on real-time formation of two-dimensional nanoparticle arrays in the very low diffusive limit, where nanoparticles are mainly driven by capillary forces and solvent fluctuations. We find that superlattice formation appears to be segregated into multiple regimes. Initially, the solvent front drags the nanoparticles, condensing them into an amorphous agglomerate. Subsequently, the nanoparticle crystallization into an array is driven by local fluctuations. Following the crystallization event, superlattice growth can also occur via the addition of individual nanoparticles drawn from outlying regions by different solvent fronts. The dragging mechanism is consistent with simulations based on a coarse-grained lattice gas model at the same limit.

  3. Optical properties of titanium dioxide nanotube arrays

    Energy Technology Data Exchange (ETDEWEB)

    Abdelmoula, Mohamed [Department of Physics, Northeastern University, Boston, Massachusetts 02115 (United States); Department of Materials Science, Carnegie Mellon University, Pittsburgh, PA 15213 (United States); Sokoloff, Jeffrey; Lu, Wen-Tao; Menon, Latika [Department of Physics, Northeastern University, Boston, Massachusetts 02115 (United States); Close, Thomas; Richter, Christiaan, E-mail: christiaan.richter@rit.edu [Department of Chemical Engineering, Rochester Institute of Technology, Rochester, New York, 14623 (United States)

    2014-01-07

    We present experimental measurements and a theoretical analysis of the near UV to NIR optical properties of free standing titania nanotube arrays. An improved understanding of the optical physics of this type of nanostructure is important to several next generation solar energy conversion technologies. We measured the transmission, reflection, and absorption of the electromagnetic spectrum from 300 nm to 1000 nm (UV to NIR) of titania nanotube arrays. We measured the total, specular, and diffuse reflection and transmission using both single point detection and an integrating sphere spectrometer. We find that the transmission, but not the reflection, of light (UV to NIR) through the nanotube array is well-explained by classic geometric optics using an effective medium model taking into account the conical geometry of the nanotubes. For wavelengths shorter than ∼500 nm, we find the surprising result that the reflection coefficient for light incident on the open side of the nanotube array is greater than the reflection coefficient for light incident on the closed “floor” of the nanotube array. We consider theoretical models based on the eikonal approximation, photonic crystal band theory, and a statistical treatment of scattering to explain the observed data. We attribute the fact that light with wavelengths shorter than 500 nm is more highly reflected from the open than the closed tube side as being due to disorder scattering inside the nanotube array.

  4. Band structures of two dimensional solid/air hierarchical phononic crystals

    International Nuclear Information System (INIS)

    Xu, Y.L.; Tian, X.G.; Chen, C.Q.

    2012-01-01

    The hierarchical phononic crystals to be considered show a two-order “hierarchical” feature, which consists of square array arranged macroscopic periodic unit cells with each unit cell itself including four sub-units. Propagation of acoustic wave in such two dimensional solid/air phononic crystals is investigated by the finite element method (FEM) with the Bloch theory. Their band structure, wave filtering property, and the physical mechanism responsible for the broadened band gap are explored. The corresponding ordinary phononic crystal without hierarchical feature is used for comparison. Obtained results show that the solid/air hierarchical phononic crystals possess tunable outstanding band gap features, which are favorable for applications such as sound insulation and vibration attenuation.

  5. Band structures of two dimensional solid/air hierarchical phononic crystals

    Energy Technology Data Exchange (ETDEWEB)

    Xu, Y.L.; Tian, X.G. [State Key Laboratory for Mechanical Structure Strength and Vibration, Xi' an Jiaotong University, Xi' an 710049 (China); Chen, C.Q., E-mail: chencq@tsinghua.edu.cn [Department of Engineering Mechanics, AML and CNMM, Tsinghua University, Beijing 100084 (China)

    2012-06-15

    The hierarchical phononic crystals to be considered show a two-order 'hierarchical' feature, which consists of square array arranged macroscopic periodic unit cells with each unit cell itself including four sub-units. Propagation of acoustic wave in such two dimensional solid/air phononic crystals is investigated by the finite element method (FEM) with the Bloch theory. Their band structure, wave filtering property, and the physical mechanism responsible for the broadened band gap are explored. The corresponding ordinary phononic crystal without hierarchical feature is used for comparison. Obtained results show that the solid/air hierarchical phononic crystals possess tunable outstanding band gap features, which are favorable for applications such as sound insulation and vibration attenuation.

  6. Control of magnonic spectra in cobalt nanohole arrays: the effects of density, symmetry and defects

    International Nuclear Information System (INIS)

    Barman, Anjan

    2010-01-01

    Magnetic nanohole arrays are important systems for propagation of magnetic excitations and are among the potential candidates for magnonic crystals. A thorough investigation of magnonic band structures and the effect of the geometry of the array on them are important. Here, we present a systematic micromagnetic simulation study of magnonic modes in cobalt nanohole (antidot) arrays. In particular, we investigate the effects of the areal density and symmetry of the array and defects introduced in the array. The magnonic modes are strongly dependent on the density and the symmetry of the array but are weakly dependent on the defects. We have further investigated the modes in a tailored array consisting of equally wide hexagonal arrays with varying density. The magnonic spectrum of the tailored array contains additional modes above the modes of the constituent arrays due to the appearance of irregular domain structures at the regions joining arrays of two different types. This opens up the possibility of tuning the magnonic bands in magnetic nanohole arrays by careful design of the structure of the array.

  7. Preparation and electrochemical performance of bramble-like ZnO array as anode materials for lithium-ion batteries

    International Nuclear Information System (INIS)

    Yan, Junfeng; Wang, Gang; Wang, Hui; Zhang, Zhiyong; Ruan, Xiongfei; Zhao, Wu; Yun, Jiangni; Xu, Manzhang

    2015-01-01

    A bramble-like ZnO array with a special three-dimensional (3D) nanostructure was successfully fabricated on Zn foil through a facile two-step hydrothermal process. A possible growth mechanism of the bramble-like ZnO array was proposed. In the first step of hydrothermal process, the crystal nucleus of Zn(OH) 4 2− generated by the zinc atoms and OH − ions fold together preferentially along the positive polar (0001) to form the needle-like ZnO array. In the second step of hydrothermal process, the crystal nuclei of Zn(OH) 4 2− adjust their posture to keep their c-axes vertical to the perching sites due to the sufficient environmental force and further grow preferentially along the (0001) direction so as to form bramble-like ZnO array. The electrochemical properties of the needle- and bramble-like ZnO arrays as anode materials for lithium-ion batteries were investigated and compared. The results show that the bramble-like ZnO material exhibits much better lithium storage properties than the needle-like ZnO sample. Reasons for the enhanced electrochemical performance of the bramble-like ZnO material were investigated

  8. Growth of GaN micro/nanolaser arrays by chemical vapor deposition.

    Science.gov (United States)

    Liu, Haitao; Zhang, Hanlu; Dong, Lin; Zhang, Yingjiu; Pan, Caofeng

    2016-09-02

    Optically pumped ultraviolet lasing at room temperature based on GaN microwire arrays with Fabry-Perot cavities is demonstrated. GaN microwires have been grown perpendicularly on c-GaN/sapphire substrates through simple catalyst-free chemical vapor deposition. The GaN microwires are [0001] oriented single-crystal structures with hexagonal cross sections, each with a diameter of ∼1 μm and a length of ∼15 μm. A possible growth mechanism of the vertical GaN microwire arrays is proposed. Furthermore, we report room-temperature lasing in optically pumped GaN microwire arrays based on the Fabry-Perot cavity. Photoluminescence spectra exhibit lasing typically at 372 nm with an excitation threshold of 410 kW cm(-2). The result indicates that these aligned GaN microwire arrays may offer promising prospects for ultraviolet-emitting micro/nanodevices.

  9. Broadband sound blocking in phononic crystals with rotationally symmetric inclusions.

    Science.gov (United States)

    Lee, Joong Seok; Yoo, Sungmin; Ahn, Young Kwan; Kim, Yoon Young

    2015-09-01

    This paper investigates the feasibility of broadband sound blocking with rotationally symmetric extensible inclusions introduced in phononic crystals. By varying the size of four equally shaped inclusions gradually, the phononic crystal experiences remarkable changes in its band-stop properties, such as shifting/widening of multiple Bragg bandgaps and evolution to resonance gaps. Necessary extensions of the inclusions to block sound effectively can be determined for given incident frequencies by evaluating power transmission characteristics. By arraying finite dissimilar unit cells, the resulting phononic crystal exhibits broadband sound blocking from combinational effects of multiple Bragg scattering and local resonances even with small-numbered cells.

  10. Plasmonic photonic crystals realized through DNA-programmable assembly.

    Science.gov (United States)

    Park, Daniel J; Zhang, Chuan; Ku, Jessie C; Zhou, Yu; Schatz, George C; Mirkin, Chad A

    2015-01-27

    Three-dimensional dielectric photonic crystals have well-established enhanced light-matter interactions via high Q factors. Their plasmonic counterparts based on arrays of nanoparticles, however, have not been experimentally well explored owing to a lack of available synthetic routes for preparing them. However, such structures should facilitate these interactions based on the small mode volumes associated with plasmonic polarization. Herein we report strong light-plasmon interactions within 3D plasmonic photonic crystals that have lattice constants and nanoparticle diameters that can be independently controlled in the deep subwavelength size regime by using a DNA-programmable assembly technique. The strong coupling within such crystals is probed with backscattering spectra, and the mode splitting (0.10 and 0.24 eV) is defined based on dispersion diagrams. Numerical simulations predict that the crystal photonic modes (Fabry-Perot modes) can be enhanced by coating the crystals with a silver layer, achieving moderate Q factors (∼10(2)) over the visible and near-infrared spectrum.

  11. The new FPGA based discriminator board for the CBELSA/TAPS experiment

    Energy Technology Data Exchange (ETDEWEB)

    Fix, Eugenia [HISKP, Universitaet Bonn (Germany); Collaboration: CBELSA/TAPS-Collaboration

    2016-07-01

    The Crystal Barrel calorimeter at ELSA, which consists of 1320 CsI(Tl) crystals has been upgraded by a new Avalanche Photo Diode (APD) crystal readout.The APD readout electronics will provide a fast trigger signal down to 10 MeV energy deposit per single crystal. The processing of these trigger signals requires the development of a previously not existent timing branch of the readout chain of the Crystal Barrel calorimeter. Core component of the timing branch is a newly developed, FPGA based discriminator board. Its firmware contains modules for time to digital conversion, rise time compensation and parts of a cluster finder. In addition the reference voltages and discriminator thresholds are controlled and monitored. This poster presents the design and the achievable accuracy of the new discriminator.

  12. A composite hydrogels-based photonic crystal multi-sensor

    International Nuclear Information System (INIS)

    Chen, Cheng; Zhu, Zhigang; Zhu, Xiangrong; Yu, Wei; Liu, Mingju; Ge, Qiaoqiao; Shih, Wei-Heng

    2015-01-01

    A facile route to prepare stimuli-sensitive poly(vinyl alcohol)/poly(acrylic acid) (PVA/PAA) gelated crystalline colloidal array photonic crystal material was developed. PVA was physically gelated by utilizing an ethanol-assisted method, the resulting hydrogel/crystal composite film was then functionalized with PAA to form an interpenetrating hydrogel film. This sensor film is able to efficiently diffract the visible light and rapidly respond to various environmental stimuli such as solvent, pH and strain, and the accompanying structural color shift can be repeatedly changed and easily distinguished by naked eye. (paper)

  13. Effect of process parameters on crystal size and morphology of lactose in ultrasound-assisted crystallization

    Energy Technology Data Exchange (ETDEWEB)

    Patel, S.R.; Murthy, Z.V.P. [Chemical Engineering Department, S.V. National Institute of Technology, Surat - 395 007, Gujarat (India)

    2011-03-15

    {alpha}-lactose monohydrate is widely used as a pharmaceutical excipient. Drug delivery system requires the excipient to be of narrow particle size distribution with regular particle shape. Application of ultrasound is known to increase or decrease the growth rate of certain crystal faces and controls the crystal size distribution. In the present paper, effect of process parameters such as sonication time, anti-solvent concentration, initial lactose concentration and initial pH of sample on lactose crystal size, shape and thermal transition temperature was studied. The parameters were set according to the L{sub 9}-orthogonal array method at three levels and recovered lactose from whey by sonocrystallization. The recovered lactose was analyzed by particle size analyzer, scanning electron microscopy and differential scanning calorimeter. It was found that the morphology of lactose crystal was rod/needle like shape. Crystal size distribution of lactose was observed to be influenced by different process parameters. From the results of analysis of variance, the sonication time interval was found to be the most significant parameter affecting the volume median diameter of lactose with the highest percentage contribution (74.28%) among other parameters. (copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  14. Large-scale membrane transfer process: its application to single-crystal-silicon continuous membrane deformable mirror

    International Nuclear Information System (INIS)

    Wu, Tong; Sasaki, Takashi; Hane, Kazuhiro; Akiyama, Masayuki

    2013-01-01

    This paper describes a large-scale membrane transfer process developed for the construction of large-scale membrane devices via the transfer of continuous single-crystal-silicon membranes from one substrate to another. This technique is applied for fabricating a large stroke deformable mirror. A bimorph spring array is used to generate a large air gap between the mirror membrane and the electrode. A 1.9 mm × 1.9 mm × 2 µm single-crystal-silicon membrane is successfully transferred to the electrode substrate by Au–Si eutectic bonding and the subsequent all-dry release process. This process provides an effective approach for transferring a free-standing large continuous single-crystal-silicon to a flexible suspension spring array with a large air gap. (paper)

  15. EUROGAM: A high efficiency escape suppressed spectrometer array

    Energy Technology Data Exchange (ETDEWEB)

    Nolan, P J [Liverpool Univ. (United Kingdom). Oliver Lodge Lab.

    1992-08-01

    EUROGAM is a UK-France collaboration to develop and build a high efficiency escape suppressed spectrometer array. The project has involved the development of both germanium (Ge) and bismuth germanate (BGO) detectors to produce crystals which are both bigger and have a more complex geometry. As a major investment for the future, the collaboration has developed a new electronics and data acquisition system based on the VXI and VME standards. The array will start its experimental programme in mid 1992 at the Nuclear Structure Facility at Daresbury, U.K. At this stage it will have a total photopeak efficiency (for 1.33 MeV gamma-rays) of {approx} 4.5%. This will give an improvement in sensitivity (relative to presently operating arrays) of a factor of about 10. When EUROGAM moves to France in mid 1993 its photopeak efficiency will have increased to about 8.5% which will result in an increase in sensitivity of a further factor of about 10. In this article I will concentrate on the array which will operate at Daresbury in 1992 and only briefly cover the developments which will take place for the full array before it is used in France in 1993. (author). 13 refs., 2 tabs., 10 figs.

  16. EUROGAM: A high efficiency escape suppressed spectrometer array

    International Nuclear Information System (INIS)

    Nolan, P.J.

    1992-01-01

    EUROGAM is a UK-France collaboration to develop and build a high efficiency escape suppressed spectrometer array. The project has involved the development of both germanium (Ge) and bismuth germanate (BGO) detectors to produce crystals which are both bigger and have a more complex geometry. As a major investment for the future, the collaboration has developed a new electronics and data acquisition system based on the VXI and VME standards. The array will start its experimental programme in mid 1992 at the Nuclear Structure Facility at Daresbury, U.K. At this stage it will have a total photopeak efficiency (for 1.33 MeV gamma-rays) of ∼ 4.5%. This will give an improvement in sensitivity (relative to presently operating arrays) of a factor of about 10. When EUROGAM moves to France in mid 1993 its photopeak efficiency will have increased to about 8.5% which will result in an increase in sensitivity of a further factor of about 10. In this article I will concentrate on the array which will operate at Daresbury in 1992 and only briefly cover the developments which will take place for the full array before it is used in France in 1993. (author). 13 refs., 2 tabs., 10 figs

  17. Tunable diffraction and self-defocusing in liquid-filled photonic crystal fibers

    DEFF Research Database (Denmark)

    Rosberg, Christian Romer; Bennet, Francis H.; Neshev, Dragomir N.

    2007-01-01

    We suggest and demonstrate a novel platform for the study of tunable nonlinear light propagation in two-dimensional discrete systems, based on photonic crystal fibers filled with high index nonlinear liquids. Using the infiltrated cladding region of a photonic crystal fiber as a nonlinear waveguide...... array, we experimentally demonstrate highly tunable beam diffraction and thermal self-defocusing, and realize a compact all-optical power limiter based on a tunable nonlinear response....

  18. One-dimensional ferromagnetic array compound [Co3(SBA)2(OH)2(H2O)2]n, (SBA = 4-sulfobenzoate)

    Science.gov (United States)

    Honda, Zentaro; Nomoto, Naoyuki; Fujihara, Takashi; Hagiwara, Masayuki; Kida, Takanori; Sawada, Yuya; Fukuda, Takeshi; Kamata, Norihiko

    2018-06-01

    We report on the syntheses, crystal structure, and magnetic properties of the transition metal coordination polymer [Co3(SBA)2(OH)2(H2O)2]n, (SBA = 4-sulfobenzoate) in which CoO6 octahedra are linked through their edges, forming one-dimensional (1D) Co(II) arrays running along the crystal a-axis. These arrays are further perpendicularly bridged by SBA ligand to construct a three-dimensional framework. Its magnetic properties have been investigated, and ferromagnetic interactions within the arrays have been found. From heat capacity measurements, we have found that this compound exhibits a three-dimensional ferromagnetic phase transition at TC = 1.54 K, and the specific heat just above TC shows a Schottky anomaly which originates from an energy gap caused by uniaxial magnetic anisotropy. These results suggest that [Co3(SBA)2(OH)2(H2O)2]n consists of weakly coupled 1D ferromagnetic Ising arrays.

  19. The measurement of temperature effect of light output of scintillators

    International Nuclear Information System (INIS)

    Ji Changsong; Zhou Zaiping; Zhang Longfang

    1999-01-01

    The author describes a experiment equipment used for measurement of temperature effect of light output of scintillators; gives some measurement results of temperature effect of light output for NaI(Tl), CsI(Tl), plastic scintillator, ZnS(Ag), anthracene crystal glass scintillator; analyzes the error factors affecting the measurement results. The total uncertainty of the temperature effect measurement for NaI(Tl) and plastic scintillator is 11%

  20. Colorimetric sensor arrays based on pattern recognition for the detection of nitroaromatic molecules

    Energy Technology Data Exchange (ETDEWEB)

    Lu, Wei; Dong, Xiao [School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing, 100081 (China); Qiu, Lili, E-mail: qiulili@bit.edu.cn [School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing, 100081 (China); Yan, Zequn [School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing, 100081 (China); Meng, Zihui, E-mail: m_zihui@yahoo.com [School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing, 100081 (China); Xue, Min [School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing, 100081 (China); He, Xuan; Liu, Xueyong [Institute of Chemical Materials, China Academy of Engineering Physics, Mianyang, Sichuan, 621900 (China)

    2017-03-15

    Graphical abstract: A colorimetric sensor array based on four kinds molecularly imprinted photonic crystal (MIPC) was explored for the selective visual detection of TNT, 2,6-DNT, 2,4-DNT and 4-MNT. The color of individual sensor changed with the increasing concentration of the analytes, and a cross-responsive platform was evaluated by a “radar” pattern. With the assistance of principal component analysis (PCA), a separate response region contained 95.25% of significant characteristics for the detection of nitroaromatics was generated, which also promised high potential for the customized visual detection system of other harmful chemicals. - Highlights: • Nitroaromatics were visually detected by molecularly imprinted photonic crystal. • The adsorption capacity was calculated. • The cross responsive platform of sensor array was established and discussed. • The discrimination capability was promoted by principal component analysis. • This system had high potential to be used in other customed visual detection. - Abstract: This research demonstrated that, in a colorimetric sensor array, 2,4,6-trinitrotoluene (TNT), 2,6-dinitrotoluene (2,6-DNT), 2,4-dinitrotoluene (2,4-DNT) and 4-nitrotoluene (4-MNT) were identifiable through a unique pattern in a qualitative and semi-quantitative manner. The adsorption capacity of the molecularly imprinted colloidal particles (MICs) for their corresponding templates was 0.27 mmol TNT/g, 0.22 mmol 2,6-DNT/g, 0.31 mmol 2,4-DNT/g and 0.16 mmol 4-MNT/g, respectively. Every optical sensor utilized in the arrays contained three-dimensional molecularly imprinted photonic crystal (MIPC) sensor with different imprinted templates. The intelligent materials can display different colors from green to red to 20 mM corresponding nitroaromatics with varying diffraction red shifts of 84 nm (TNT), 46 nm (2,6-DNT), 54 nm (2,4-DNT) and 35 nm (4-MNT), respectively. With the assistance of principal component analysis (PCA) and rational design

  1. Colorimetric sensor arrays based on pattern recognition for the detection of nitroaromatic molecules

    International Nuclear Information System (INIS)

    Lu, Wei; Dong, Xiao; Qiu, Lili; Yan, Zequn; Meng, Zihui; Xue, Min; He, Xuan; Liu, Xueyong

    2017-01-01

    Graphical abstract: A colorimetric sensor array based on four kinds molecularly imprinted photonic crystal (MIPC) was explored for the selective visual detection of TNT, 2,6-DNT, 2,4-DNT and 4-MNT. The color of individual sensor changed with the increasing concentration of the analytes, and a cross-responsive platform was evaluated by a “radar” pattern. With the assistance of principal component analysis (PCA), a separate response region contained 95.25% of significant characteristics for the detection of nitroaromatics was generated, which also promised high potential for the customized visual detection system of other harmful chemicals. - Highlights: • Nitroaromatics were visually detected by molecularly imprinted photonic crystal. • The adsorption capacity was calculated. • The cross responsive platform of sensor array was established and discussed. • The discrimination capability was promoted by principal component analysis. • This system had high potential to be used in other customed visual detection. - Abstract: This research demonstrated that, in a colorimetric sensor array, 2,4,6-trinitrotoluene (TNT), 2,6-dinitrotoluene (2,6-DNT), 2,4-dinitrotoluene (2,4-DNT) and 4-nitrotoluene (4-MNT) were identifiable through a unique pattern in a qualitative and semi-quantitative manner. The adsorption capacity of the molecularly imprinted colloidal particles (MICs) for their corresponding templates was 0.27 mmol TNT/g, 0.22 mmol 2,6-DNT/g, 0.31 mmol 2,4-DNT/g and 0.16 mmol 4-MNT/g, respectively. Every optical sensor utilized in the arrays contained three-dimensional molecularly imprinted photonic crystal (MIPC) sensor with different imprinted templates. The intelligent materials can display different colors from green to red to 20 mM corresponding nitroaromatics with varying diffraction red shifts of 84 nm (TNT), 46 nm (2,6-DNT), 54 nm (2,4-DNT) and 35 nm (4-MNT), respectively. With the assistance of principal component analysis (PCA) and rational design

  2. Crystallization Behavior of Poly(ethylene oxide) in Vertically Aligned Carbon Nanotube Array.

    Science.gov (United States)

    Sheng, Jiadong; Zhou, Shenglin; Yang, Zhaohui; Zhang, Xiaohua

    2018-03-27

    We investigate the effect of the presence of vertically aligned multiwalled carbon nanotubes (CNTs) on the orientation of poly(ethylene oxide) (PEO) lamellae and PEO crystallinity. The high alignment of carbon nanotubes acting as templates probably governs the orientation of PEO lamellae. This templating effect might result in the lamella planes of PEO crystals oriented along a direction parallel to the long axis of the nanotubes. The presence of aligned carbon nanotubes also gives rise to the decreases in PEO crystallinity, crystallization temperature, and melting temperature due to the perturbation of carbon nanotubes to the crystallization of PEO. These effects have significant implications for controlling the orientation of PEO lamellae and decreasing the crystallinity of PEO and thickness of PEO lamellae, which have significant impacts on ion transport in PEO/CNT composite and the capacitive performance of PEO/CNT composite. Both the decreased PEO crystallinity and the orientation of PEO lamellae along the long axes of vertically aligned CNTs give rise to the decrease in the charge transfer resistance, which is associated with the improvements in the ion transport and capacitive performance of PEO/CNT composite.

  3. A flow-free droplet-based device for high throughput polymorphic crystallization.

    Science.gov (United States)

    Yang, Shih-Mo; Zhang, Dapeng; Chen, Wang; Chen, Shih-Chi

    2015-06-21

    Crystallization is one of the most crucial steps in the process of pharmaceutical formulation. In recent years, emulsion-based platforms have been developed and broadly adopted to generate high quality products. However, these conventional approaches such as stirring are still limited in several aspects, e.g., unstable crystallization conditions and broad size distribution; besides, only simple crystal forms can be produced. In this paper, we present a new flow-free droplet-based formation process for producing highly controlled crystallization with two examples: (1) NaCl crystallization reveals the ability to package saturated solution into nanoliter droplets, and (2) glycine crystallization demonstrates the ability to produce polymorphic crystallization forms by controlling the droplet size and temperature. In our process, the saturated solution automatically fills the microwell array powered by degassed bulk PDMS. A critical oil covering step is then introduced to isolate the saturated solution and control the water dissolution rate. Utilizing surface tension, the solution is uniformly packaged in the form of thousands of isolating droplets at the bottom of each microwell of 50-300 μm diameter. After water dissolution, individual crystal structures are automatically formed inside the microwell array. This approach facilitates the study of different glycine growth processes: α-form generated inside the droplets and γ-form generated at the edge of the droplets. With precise temperature control over nanoliter-sized droplets, the growth of ellipsoidal crystalline agglomerates of glycine was achieved for the first time. Optical and SEM images illustrate that the ellipsoidal agglomerates consist of 2-5 μm glycine clusters with inner spiral structures of ~35 μm screw pitch. Lastly, the size distribution of spherical crystalline agglomerates (SAs) produced from microwells of different sizes was measured to have a coefficient variation (CV) of less than 5%, showing

  4. Anodic Fabrication of Ti-Ni-O Nanotube Arrays on Shape Memory Alloy

    Directory of Open Access Journals (Sweden)

    Qiang Liu

    2014-04-01

    Full Text Available Surface modification with oxide nanostructures is one of the efficient ways to improve physical or biomedical properties of shape memory alloys. This work reports a fabrication of highly ordered Ti-Ni-O nanotube arrays on Ti-Ni alloy substrates through pulse anodization in glycerol-based electrolytes. The effects of anodization parameters and the annealing process on the microstructures and surface morphology of Ti-Ni-O were studied using scanning electron microscope and Raman spectroscopy. The electrolyte type greatly affected the formation of nanotube arrays. A formation of anatase phase was found with the Ti-Ni-O nanotube arrays annealed at 450 °C. The oxide nanotubes could be crystallized to rutile phase after annealing treatment at 650 °C. The Ti-Ni-O nanotube arrays demonstrated an excellent thermal stability by keeping their nanotubular structures up to 650 °C.

  5. Measurement of the point spread function of a pixelated detector array

    Energy Technology Data Exchange (ETDEWEB)

    Ritzer, Christian; Hallen, Patrick; Schug, David; Schulz, Volkmar [Department of Physics of Molecular Imaging Systems, Institute for Experimental Molecular Imaging, RWTH Aachen University, Aachen (Germany)

    2015-05-18

    In order to further understand the PET/MRI scanner of our group, we measured the point spread function of a preclinical scintillation crystal array with a pitch of 1 mm and a total size of 30 mm ~ 30 mm ~ 12 mm. It is coupled via a lightguide to a dSiPM from Philips Digital Photon Counting, used on the TEK-setup. Crystal identification is done with a centre of gravity algorithm and the whole data analysis is performed with the same processing software as for the PET insert, giving comparable results. The beam is created with a 22 NA-Point-Source and a lead collimator, with 0.5 mm bore diameter. The algorithm sorted 62 % of the coincidences into the correct crystal.

  6. Measurement of the point spread function of a pixelated detector array

    International Nuclear Information System (INIS)

    Ritzer, Christian; Hallen, Patrick; Schug, David; Schulz, Volkmar

    2015-01-01

    In order to further understand the PET/MRI scanner of our group, we measured the point spread function of a preclinical scintillation crystal array with a pitch of 1 mm and a total size of 30 mm ~ 30 mm ~ 12 mm. It is coupled via a lightguide to a dSiPM from Philips Digital Photon Counting, used on the TEK-setup. Crystal identification is done with a centre of gravity algorithm and the whole data analysis is performed with the same processing software as for the PET insert, giving comparable results. The beam is created with a 22 NA-Point-Source and a lead collimator, with 0.5 mm bore diameter. The algorithm sorted 62 % of the coincidences into the correct crystal.

  7. On-beam calibration of the ΔE(Si)-Sci/PD charged particle telescope

    International Nuclear Information System (INIS)

    Avdeichikov, V.; Jakobsson, B.; Nikitin, V.A.; Nomokonov, P.V.; Veldhuizen, E.J. van

    2001-01-01

    The reaction products emitted in the 14 N(45A MeV)+(CH 2 /CD 2 ) interactions are identified by a ΔE(Si)-E(Scintillator/Photodiode) telescope by the conventional ΔE-E method. The position of 'jumps' in the amplitude of the photodiode signal for ions passing through the scintillator (Sci) is used to calibrate on-beam both the ΔE and the Sci/PD scales in MeV. The accuracy of an absolute energy calibration is better than 2.3% and 1.8% for CsI(Tl) and GSO(Ce) detectors, respectively. It is defined mostly by the correctness of the range-energy relations of ions in the Si and Sci crystals. The light response function, L(E,Z,A), of isotopes up to Z(A)=8(16) in the range of energy ∼(2.5-60)A MeV is extracted. The effects of doping concentration and pulse shaping on the light response are analyzed. The validity of the existing empirical light-energy relations is checked in a wide interval of ion energies and a new power law relation is proposed. Calculations of the response function based on the Murray-Mayer model are found to be in excellent agreement with experimental data for the CsI(Tl) crystal

  8. 3D Dewetting for Crystal Patterning: Toward Regular Single-Crystalline Belt Arrays and Their Functionality.

    Science.gov (United States)

    Wu, Yuchen; Feng, Jiangang; Su, Bin; Jiang, Lei

    2016-03-16

    Arrays of unidirectional dewetting behaviors can be generated by using 3D-wettability-difference micropillars, yielding highly ordered organic single-crystalline belt arrays. These patterned organic belts show an improved mobility record and can be used as flexible pressure sensors with high sensitivity. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  9. Multiple matching scheme for broadband 0.72Pb(Mg1∕3Nb2∕3)O3−0.28PbTiO3 single crystal phased-array transducer

    OpenAIRE

    Lau, S. T.; Li, H.; Wong, K. S.; Zhou, Q. F.; Zhou, D.; Li, Y. C.; Luo, H. S.; Shung, K. K.; Dai, J. Y.

    2009-01-01

    Lead magnesium niobate–lead titanate single crystal 0.72Pb(Mg1∕3Nb2∕3)O3−0.28PbTiO3 (abbreviated as PMN-PT) was used to fabricate high performance ultrasonic phased-array transducer as it exhibited excellent piezoelectric properties. In this paper, we focus on the design and fabrication of a low-loss and wide-band transducer for medical imaging applications. A KLM model based simulation software PiezoCAD was used for acoustic design of the transducer including the front-face matching and back...

  10. Angular dependence of the coercivity in arrays of ferromagnetic nanowires

    International Nuclear Information System (INIS)

    Holanda, J.; Silva, D.B.O.; Padrón-Hernández, E.

    2015-01-01

    We present a new magnetic model for polycrystalline nanowires arrays in porous anodic aluminum oxide. The principal consideration here is the crystalline structure and the morphology of the wires and them the dipolar interactions between the crystals into the wire. Other aspect here is the direct calculation of the dipolar energy for the interaction of one wire with the others in the array. The free energy density was formulated for polycrystalline nanowires arrays in order to determinate the anisotropy effective field. It was using the microstructure study by scanning and transmission electron microscopy for the estimation of the real structure of the wires. After the structural analysis we used the angular dependences for the coercivity field and for the remnant magnetization to determine the properties of the wires. All analysis were made by the theory treatment proposed by Stoner and Wohlfarth

  11. Angular dependence of the coercivity in arrays of ferromagnetic nanowires

    Energy Technology Data Exchange (ETDEWEB)

    Holanda, J. [Departamento de Física, Universidade Federal de Pernambuco, Recife 50670-901, PE (Brazil); Silva, D.B.O. [Pós-Graduação em Ciência de Materiais, Universidade Federal de Pernambuco, Recife 50670-901, PE (Brazil); Padrón-Hernández, E., E-mail: padron@df.ufpe.br [Departamento de Física, Universidade Federal de Pernambuco, Recife 50670-901, PE (Brazil); Pós-Graduação em Ciência de Materiais, Universidade Federal de Pernambuco, Recife 50670-901, PE (Brazil)

    2015-03-15

    We present a new magnetic model for polycrystalline nanowires arrays in porous anodic aluminum oxide. The principal consideration here is the crystalline structure and the morphology of the wires and them the dipolar interactions between the crystals into the wire. Other aspect here is the direct calculation of the dipolar energy for the interaction of one wire with the others in the array. The free energy density was formulated for polycrystalline nanowires arrays in order to determinate the anisotropy effective field. It was using the microstructure study by scanning and transmission electron microscopy for the estimation of the real structure of the wires. After the structural analysis we used the angular dependences for the coercivity field and for the remnant magnetization to determine the properties of the wires. All analysis were made by the theory treatment proposed by Stoner and Wohlfarth.

  12. Growth of Horizonatal ZnO Nanowire Arrays on Any Substrate

    KAUST Repository

    Qin, Yong

    2008-12-04

    A general method is presented for growing laterally aligned and patterned ZnO nanowire (NW) arrays on any substrate as long as it is flat. The orientation control is achieved using the combined effect from ZnO seed layer and the catalytically inactive Cr (or Sn) layer for NW growth. The growth temperature (< 100 °C) is so low that the method can be applied to a wide range of substrates that can be inorganic, organic, single crystal, polycrystal, or amorphous. The laterally aligned ZnO NW arrays can be employed for various applications, such as gas sensor, field effect transistor, nanogenerator, and flexible electronics. © 2008 American Chemical Society.

  13. Collection of scintillation light from small BGO crystals

    International Nuclear Information System (INIS)

    Cherry, S.R.; Shao, Y.; Tornai, M.P.; Siegel, S.; Ricci, A.R.; Phelps, M.E.

    1995-01-01

    The authors propose to develop a high resolution positron emission tomography (PET) detector designed for animal imaging. The detector consists of a 2-D array of small bismuth germanate (BGO) crystals coupled via optical fibers to a multi-channel photomultiplier tube (MC-PMT). Though this approach offers several advantages over the conventional BGO block design, it does require that a sufficient number of scintillation photons be transported from the crystal, down the fiber and into the PMT. In this study the authors use simulations and experimental data to determine how to maximize the signal reaching the PMT. This involves investigating factors such as crystal geometry, crystal surface treatment, the use of reflectors, choice of optical fiber, coupling of crystals to the optical fiber and optical fiber properties. Their results indicate that using 2 x 2 x 10 mm BGO crystals coupled to 30 cm of clad optical fiber, roughly 50 photoelectrons are produced at the PMT photocathode for a 511 keV interaction. This is sufficient to clearly visualize the photopeak and provide adequate timing resolution for PET. Based on these encouraging results, a prototype detector will now be constructed

  14. Microprocessor system to recover data from a self-scanning photodiode array

    International Nuclear Information System (INIS)

    Koppel, L.N.; Gadd, T.J.

    1975-01-01

    A microprocessor system developed at Lawrence Livermore Laboratory has expedited the recovery of data describing the low energy x-ray spectra radiated by laser-fusion targets. An Intel microprocessor controls the digitization and scanning of the data stream of an x-ray-sensitive self-scanning photodiode array incorporated in a crystal diffraction spectrometer

  15. New Insights into the Origins of Sb-Induced Effects on Self-Catalyzed GaAsSb Nanowire Arrays.

    Science.gov (United States)

    Ren, Dingding; Dheeraj, Dasa L; Jin, Chengjun; Nilsen, Julie S; Huh, Junghwan; Reinertsen, Johannes F; Munshi, A Mazid; Gustafsson, Anders; van Helvoort, Antonius T J; Weman, Helge; Fimland, Bjørn-Ove

    2016-02-10

    Ternary semiconductor nanowire arrays enable scalable fabrication of nano-optoelectronic devices with tunable bandgap. However, the lack of insight into the effects of the incorporation of Vy element results in lack of control on the growth of ternary III-V(1-y)Vy nanowires and hinders the development of high-performance nanowire devices based on such ternaries. Here, we report on the origins of Sb-induced effects affecting the morphology and crystal structure of self-catalyzed GaAsSb nanowire arrays. The nanowire growth by molecular beam epitaxy is changed both kinetically and thermodynamically by the introduction of Sb. An anomalous decrease of the axial growth rate with increased Sb2 flux is found to be due to both the indirect kinetic influence via the Ga adatom diffusion induced catalyst geometry evolution and the direct composition modulation. From the fundamental growth analyses and the crystal phase evolution mechanism proposed in this Letter, the phase transition/stability in catalyst-assisted ternary III-V-V nanowire growth can be well explained. Wavelength tunability with good homogeneity of the optical emission from the self-catalyzed GaAsSb nanowire arrays with high crystal phase purity is demonstrated by only adjusting the Sb2 flux.

  16. Beam-Mode Piezoelectric Properties of Ternary Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3 Single Crystals for Medical Linear Array Applications

    Science.gov (United States)

    Wang, Wei; Wang, Sheng; Zhang, Yaoyao; Zhao, Xiangyong; Luo, Haosu

    2011-11-01

    In this work, the dielectric and beam-mode piezoelectric properties of ternary 0.35Pb(In1/2Nb1/2)O3-0.35Pb(Mg1/3Nb2/3)O3-0.30PbTiO3 (PIMNT35/35/30) piezoelectric single crystals were investigated. The Curie temperature ( T C) and rhombohedral-to-tetragonal phase-transition temperature ( T rt) are 187°C and 127°C, about 30°C higher than those of PMNT crystals. The beam-mode coupling coefficient k {33/ w } was found to be 90.3%. Furthermore, 3.5-MHz linear arrays based on PIMNT35/35/30 crystals and Pb(Zr1- x Ti x )O3 ceramic (PZT-5H) were simulated using PiezoCAD software. The results indicate that the sensitivity and -6 dB bandwidth of a PIMNT35/35/30 transducer would be approximately 4 dB and 20% higher, respectively, compared with a traditional PZT transducer.

  17. Crystal Nucleation Using Surface-Energy-Modified Glass Substrates.

    Science.gov (United States)

    Nordquist, Kyle A; Schaab, Kevin M; Sha, Jierui; Bond, Andrew H

    2017-08-02

    Systematic surface energy modifications to glass substrates can induce nucleation and improve crystallization outcomes for small molecule active pharmaceutical ingredients (APIs) and proteins. A comparatively broad probe for function is presented in which various APIs, proteins, organic solvents, aqueous media, surface energy motifs, crystallization methods, form factors, and flat and convex surface energy modifications were examined. Replicate studies ( n ≥ 6) have demonstrated an average reduction in crystallization onset times of 52(4)% (alternatively 52 ± 4%) for acetylsalicylic acid from 91% isopropyl alcohol using two very different techniques: bulk cooling to 0 °C using flat surface energy modifications or microdomain cooling to 4 °C from the interior of a glass capillary having convex surface energy modifications that were immersed in the solution. For thaumatin and bovine pancreatic trypsin, a 32(2)% reduction in crystallization onset times was demonstrated in vapor diffusion experiments ( n ≥ 15). Nucleation site arrays have been engineered onto form factors frequently used in crystallization screening, including microscope slides, vials, and 96- and 384-well high-throughput screening plates. Nucleation using surface energy modifications on the vessels that contain the solutes to be crystallized adds a layer of useful variables to crystallization studies without requiring significant changes to workflows or instrumentation.

  18. Multiple matching scheme for broadband 0.72Pb(Mg1∕3Nb2∕3)O3−0.28PbTiO3 single crystal phased-array transducer

    Science.gov (United States)

    Lau, S. T.; Li, H.; Wong, K. S.; Zhou, Q. F.; Zhou, D.; Li, Y. C.; Luo, H. S.; Shung, K. K.; Dai, J. Y.

    2009-01-01

    Lead magnesium niobate–lead titanate single crystal 0.72Pb(Mg1∕3Nb2∕3)O3−0.28PbTiO3 (abbreviated as PMN-PT) was used to fabricate high performance ultrasonic phased-array transducer as it exhibited excellent piezoelectric properties. In this paper, we focus on the design and fabrication of a low-loss and wide-band transducer for medical imaging applications. A KLM model based simulation software PiezoCAD was used for acoustic design of the transducer including the front-face matching and backing. The calculated results show that the −6 dB transducer bandwidth can be improved significantly by using double λ∕8 matching layers and hard backing. A 4.0 MHz PMN-PT transducer array (with 16 elements) was fabricated and tested in a pulse-echo arrangement. A −6 dB bandwidth of 110% and two-way insertion loss of −46.5 dB were achieved. PMID:19657405

  19. Tunable photonic crystals with partial bandgaps from blue phase colloidal crystals and dielectric-doped blue phases.

    Science.gov (United States)

    Stimulak, Mitja; Ravnik, Miha

    2014-09-07

    Blue phase colloidal crystals and dielectric nanoparticle/polymer doped blue phases are demonstrated to combine multiple components with different symmetries in one photonic material, creating a photonic crystal with variable and micro-controllable photonic band structure. In this composite photonic material, one contribution to the band structure is determined by the 3D periodic birefringent orientational profile of the blue phases, whereas the second contribution emerges from the regular array of the colloidal particles or from the dielectric/nanoparticle-doped defect network. Using the planewave expansion method, optical photonic bands of the blue phase I and II colloidal crystals and related nanoparticle/polymer doped blue phases are calculated, and then compared to blue phases with no particles and to face-centred-cubic and body-centred-cubic colloidal crystals in isotropic background. We find opening of local band gaps at particular points of Brillouin zone for blue phase colloidal crystals, where there were none in blue phases without particles or dopants. Particle size and filling fraction of the blue phase defect network are demonstrated as parameters that can directly tune the optical bands and local band gaps. In the blue phase I colloidal crystal with an additionally doped defect network, interestingly, we find an indirect total band gap (with the exception of one point) at the entire edge of SC irreducible zone. Finally, this work demonstrates the role of combining multiple - by symmetry - differently organised components in one photonic crystal material, which offers a novel approach towards tunable soft matter photonic materials.

  20. Optimization of planar self-collimating photonic crystals.

    Science.gov (United States)

    Rumpf, Raymond C; Pazos, Javier J

    2013-07-01

    Self-collimation in photonic crystals has received a lot of attention in the literature, partly due to recent interest in silicon photonics, yet no performance metrics have been proposed. This paper proposes a figure of merit (FOM) for self-collimation and outlines a methodical approach for calculating it. Performance metrics include bandwidth, angular acceptance, strength, and an overall FOM. Two key contributions of this work include the performance metrics and identifying that the optimum frequency for self-collimation is not at the inflection point. The FOM is used to optimize a planar photonic crystal composed of a square array of cylinders. Conclusions are drawn about how the refractive indices and fill fraction of the lattice impact each of the performance metrics. The optimization is demonstrated by simulating two spatially variant self-collimating photonic crystals, where one has a high FOM and the other has a low FOM. This work gives optical designers tremendous insight into how to design and optimize robust self-collimating photonic crystals, which promises many applications in silicon photonics and integrated optics.

  1. Propagative selection of tilted array patterns in directional solidification

    Science.gov (United States)

    Song, Younggil; Akamatsu, Silvère; Bottin-Rousseau, Sabine; Karma, Alain

    2018-05-01

    We investigate the dynamics of tilted cellular/dendritic array patterns that form during directional solidification of a binary alloy when a preferred-growth crystal axis is misoriented with respect to the temperature gradient. In situ experimental observations and phase-field simulations in thin samples reveal the existence of a propagative source-sink mechanism of array spacing selection that operates on larger space and time scales than the competitive growth at play during the initial solidification transient. For tilted arrays, tertiary branching at the diverging edge of the sample acts as a source of new cells with a spacing that can be significantly larger than the initial average spacing. A spatial domain of large spacing then invades the sample propagatively. It thus yields a uniform spacing everywhere, selected independently of the initial conditions, except in a small region near the converging edge of the sample, which acts as a sink of cells. We propose a discrete geometrical model that describes the large-scale evolution of the spatial spacing profile based on the local dependence of the cell drift velocity on the spacing. We also derive a nonlinear advection equation that predicts the invasion velocity of the large-spacing domain, and sheds light on the fundamental nature of this process. The models also account for more complex spacing modulations produced by an irregular dynamics at the source, in good quantitative agreement with both phase-field simulations and experiments. This basic knowledge provides a theoretical basis to improve the processing of single crystals or textured polycrystals for advanced materials.

  2. Tunable absorption resonances in the ultraviolet for InP nanowire arrays.

    Science.gov (United States)

    Aghaeipour, Mahtab; Anttu, Nicklas; Nylund, Gustav; Samuelson, Lars; Lehmann, Sebastian; Pistol, Mats-Erik

    2014-11-17

    The ability to tune the photon absorptance spectrum is an attracting way of tailoring the response of devices like photodetectors and solar cells. Here, we measure the reflectance spectra of InP substrates patterned with arrays of vertically standing InP nanowires. Using the reflectance spectra, we calculate and analyze the corresponding absorptance spectra of the nanowires. We show that we can tune absorption resonances for the nanowire arrays into the ultraviolet by decreasing the diameter of the nanowires. When we compare our measurements with electromagnetic modeling, we generally find good agreement. Interestingly, the remaining differences between modeled and measured spectra are attributed to a crystal-phase dependence in the refractive index of InP. Specifically, we find indication of significant differences in the refractive index between the modeled zinc-blende InP nanowires and the measured wurtzite InP nanowires in the ultraviolet. We believe that such crystal-phase dependent differences in the refractive index affect the possibility to excite optical resonances in the large wavelength range of 345 InP nanowire-based solar cells and photodetectors.

  3. The Use of Calixarene Thin Films in the Sensor Array for VOCs Detection and Olfactory Navigation

    Directory of Open Access Journals (Sweden)

    Alan F. Holloway

    2010-02-01

    Full Text Available This work is dedicated to the development of a sensor array for detection of volatile organic chemicals (VOCs in pre-explosive concentrations as well as for olfactory robotic navigation in the frame of two EU projects. A QCM (quartz crystal microbalance sensor array was built utilising quartz crystals spun-coated with thin films of different amphiphilic calixarene molecules to provide a base for pattern recognition of different volatile organic chemicals (VOCs. Commercial Metal-oxide semiconductor (MOS sensors were also used in the same array for the benefit of comparison. The sensor array was tested with a range of organic vapours, such as hydrocarbons, alcohols, ketones, aromatics, etc, in concentrations below LEL and up to UEL (standing for lower and upper explosion limit, respectively; the sensor array proved to be capable of identification and concentration evaluation of a range of VOCs. Comparison of QCM and MOS sensors responses to VOCs in the LEL-UEL range showed the advantage of the former. In addition, the sensor array was tested on the vapours of camphor from cinnamon oil in order to prove the concept of using the "scent marks" for robotic navigation. The results showed that the response signature of QCM coated with calixarenes to camphor is very much different from those of any other VOCs used. Adsorption and de-sorption rates of camphor are also much slower comparing to VOCs due to a high viscosity of the compound. Our experiments demonstrated the suitability of calixarene sensor array for the task and justified the use of camphor as a "scent mark" for olfactory navigation.

  4. Wafer-scale high-throughput ordered arrays of Si and coaxial Si/Si(1-x)Ge(x) wires: fabrication, characterization, and photovoltaic application.

    Science.gov (United States)

    Pan, Caofeng; Luo, Zhixiang; Xu, Chen; Luo, Jun; Liang, Renrong; Zhu, Guang; Wu, Wenzhuo; Guo, Wenxi; Yan, Xingxu; Xu, Jun; Wang, Zhong Lin; Zhu, Jing

    2011-08-23

    We have developed a method combining lithography and catalytic etching to fabricate large-area (uniform coverage over an entire 5-in. wafer) arrays of vertically aligned single-crystal Si nanowires with high throughput. Coaxial n-Si/p-SiGe wire arrays are also fabricated by further coating single-crystal epitaxial SiGe layers on the Si wires using ultrahigh vacuum chemical vapor deposition (UHVCVD). This method allows precise control over the diameter, length, density, spacing, orientation, shape, pattern and location of the Si and Si/SiGe nanowire arrays, making it possible to fabricate an array of devices based on rationally designed nanowire arrays. A proposed fabrication mechanism of the etching process is presented. Inspired by the excellent antireflection properties of the Si/SiGe wire arrays, we built solar cells based on the arrays of these wires containing radial junctions, an example of which exhibits an open circuit voltage (V(oc)) of 650 mV, a short-circuit current density (J(sc)) of 8.38 mA/cm(2), a fill factor of 0.60, and an energy conversion efficiency (η) of 3.26%. Such a p-n radial structure will have a great potential application for cost-efficient photovoltaic (PV) solar energy conversion. © 2011 American Chemical Society

  5. Large displacement bi-directional out-of-plane Lorentz actuator array for surface manipulation

    International Nuclear Information System (INIS)

    Park, Byoungyoul; Afsharipour, Elnaz; Chrusch, Dwayne; Shafai, Cyrus; Andersen, David; Burley, Greg

    2017-01-01

    This paper presents a large displacement out-of-plane Lorentz actuator array for surface manipulation. Actuators are formed from single crystal silicon flexible serpentine springs on either side of a rigid crossbar containing a narrow contact pillar. A rigid mounting rail system was employed to enable a 5  ×  5 array, which offers scalability of the array size. Analytical and finite element models were used to optimize actuator design. Individual actuators were tested to show linear deflection response of  ±150 µ m motion, using a  ±14.7 mA current in the presence of a 0.48 T magnetic field. This actuator array is suitable for various 2D surface modification applications due to its large deformation with low current and temperature of operation, and narrow contact area to a target surface. (paper)

  6. Experimental study of a depth-encoding PET detector inserting horizontal-striped glass between crystal layers

    Science.gov (United States)

    Yang, J.; Kim, K. B.; Choi, Y.; Kang, J.

    2018-04-01

    A depth-encoding positron emission tomography (PET) detector inserting a horizontal-striped glass between pixilated scintillation crystal layers was developed and experimentally evaluated. The detector consists of 2-layers of 4×4 LYSO array arranged with a 3.37 mm pitch. Horizontal-striped glasses with 1×4 array with different thickness of 3, 4 and 5 mm were inserted between top- and bottom-crystal layers. Bottom surface of bottom-layer was optically coupled to a 4×4 GAPD array. Sixteen output signals from DOI-PET detector were multiplexed by modified resistive charge division (RCD) networks and multiplexed signals were fed into custom-made charge-sensitive preamplifiers. The four amplified signals were digitized and recorded by the custom-made DAQ system based on FPGA. The four digitized outputs were post-processed and converted to flood histograms for each interaction event. Experimental results revealed that all crystal pixels were clearly identified on the 2D flood histogram without overlapping. Patterns of the 2D flood histogram were constituted with arrangements of [bottom–top–bottom–top–\\ldots–top–bottom–top–bottom] crystal responses in X-direction. These could be achieved by employing horizontal-striped glass that controlled the extent of light dispersion towards the X-direction in crystal layers for generation of a different position mapping for each layer and the modified RCD network that controls degree of charge sharing in readout electronics for reduction of identification error. This study demonstrated the proposed DOI-PET detector can extract the 3D γ-ray interaction position without considerable performance degradation of PET detector from the 2D flood histogram.

  7. All-dielectric rod antenna array for terahertz communications

    Science.gov (United States)

    Withayachumnankul, Withawat; Yamada, Ryoumei; Fujita, Masayuki; Nagatsuma, Tadao

    2018-05-01

    The terahertz band holds a potential for point-to-point short-range wireless communications at sub-terabit speed. To realize this potential, supporting antennas must have a wide bandwidth to sustain high data rate and must have high gain and low dissipation to compensate for the free space path loss that scales quadratically with frequency. Here we propose an all-dielectric rod antenna array with high radiation efficiency, high gain, and wide bandwidth. The proposed array is integral to a low-loss photonic crystal waveguide platform, and intrinsic silicon is the only constituent material for both the antenna and the feed to maintain the simplicity, compactness, and efficiency. Effective medium theory plays a key role in the antenna performance and integrability. An experimental validation with continuous-wave terahertz electronic systems confirms the minimum gain of 20 dBi across 315-390 GHz. A demonstration shows that a pair of such identical rod array antennas can handle bit-error-free transmission at the speed up to 10 Gbit/s. Further development of this antenna will build critical components for future terahertz communication systems.

  8. Reflectivity quenching of ESR multilayer polymer film reflector in optically bonded scintillator arrays

    Science.gov (United States)

    Loignon-Houle, Francis; Pepin, Catherine M.; Charlebois, Serge A.; Lecomte, Roger

    2017-04-01

    The 3M-ESR multilayer polymer film is a widely used reflector in scintillation detector arrays. As specified in the datasheet and confirmed experimentally by measurements in air, it is highly reflective (> 98 %) over the entire visible spectrum (400-1000 nm) for all angles of incidence. Despite these outstanding characteristics, it was previously found that light crosstalk between pixels in a bonded LYSO scintillator array with ESR reflector can be as high as ∼30-35%. This unexplained light crosstalk motivated further investigation of ESR optical performance. Analytical simulation of a multilayer structure emulating the ESR reflector showed that the film becomes highly transparent to incident light at large angles when surrounded on both sides by materials of refractive index higher than air. Monte Carlo simulations indicate that a considerable fraction (∼25-35%) of scintillation photons are incident at these leaking angles in high aspect ratio LYSO scintillation crystals. The film transparency was investigated experimentally by measuring the scintillation light transmission through the ESR film sandwiched between a scintillation crystal and a photodetector with or without layers of silicone grease. Strong light leakage, up to nearly 30%, was measured through the reflector when coated on both sides with silicone, thus elucidating the major cause of light crosstalk in bonded arrays. The reflector transparency was confirmed experimentally for angles of incidence larger than 60 ° using a custom designed setup allowing illumination of the bonded ESR film at selected grazing angles. The unsuspected ESR film transparency can be beneficial for detector arrays exploiting light sharing schemes, but it is highly detrimental for scintillator arrays designed for individual pixel readout.

  9. Photonic crystal geometry for organic solar cells.

    Science.gov (United States)

    Ko, Doo-Hyun; Tumbleston, John R; Zhang, Lei; Williams, Stuart; DeSimone, Joseph M; Lopez, Rene; Samulski, Edward T

    2009-07-01

    We report organic solar cells with a photonic crystal nanostructure embossed in the photoactive bulk heterojunction layer, a topography that exhibits a 3-fold enhancement of the absorption in specific regions of the solar spectrum in part through multiple excitation resonances. The photonic crystal geometry is fabricated using a materials-agnostic process called PRINT wherein highly ordered arrays of nanoscale features are readily made in a single processing step over wide areas (approximately 4 cm(2)) that is scalable. We show efficiency improvements of approximately 70% that result not only from greater absorption, but also from electrical enhancements. The methodology is generally applicable to organic solar cells and the experimental findings reported in our manuscript corroborate theoretical expectations.

  10. Performance of a monolithic LaBr{sub 3}:Ce crystal coupled to an array of silicon photomultipliers

    Energy Technology Data Exchange (ETDEWEB)

    Ulyanov, Alexei, E-mail: alexey.uliyanov@ucd.ie [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Morris, Oran [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Department of Computer Science & Applied Physics, Galway-Mayo Institute of Technology, Galway (Ireland); Hanlon, Lorraine; McBreen, Sheila; Foley, Suzanne; Roberts, Oliver J.; Tobin, Isaac; Murphy, David; Wade, Colin [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Nelms, Nick; Shortt, Brian [European Space Agency, ESTEC, 2200 AG Noordwijk (Netherlands); Slavicek, Tomas; Granja, Carlos; Solar, Michael [Institute of Experimental and Applied Physics, Czech Technical University in Prague, 12800 Prague 2 (Czech Republic)

    2016-02-21

    A gamma-ray detector composed of a single 28×28×20 mm{sup 3} LaBr{sub 3}:Ce crystal coupled to a custom built 4×4 array of silicon photomultipliers was tested over an energy range of 30 keV to 9.3 MeV. The silicon photomultipliers were initially calibrated using 20 ns light pulses generated by a light emitting diode. The photodetector responses measured as a function of the number of incident photons were found to be non-linear and consistent with model predictions. Using corrections for the non-linearity of the silicon photomultipliers, the detector showed a linear response to gamma-rays with energies from 100 keV to the maximum available energy of 9.3 MeV. The energy resolution was found to be 4% FWHM at 662 keV. Despite the large thickness of the scintillator (20 mm) and a 5 mm thick optical window, the detector was capable of measuring the positions of the gamma-ray interaction points. The position resolution was measured at 356 keV and was found to be 8 mm FWHM in the detector plane and 11 mm FWHM for the depth of interaction. The detector can be used as a building block of a larger calorimeter system that is capable of measuring gamma-ray energies up to tens of MeV.

  11. Diode array pumped, non-linear mirror Q-switched and mode-locked

    Indian Academy of Sciences (India)

    A non-linear mirror consisting of a lithium triborate crystal and a dichroic output coupler are used to mode-lock (passively) an Nd : YVO4 laser, pumped by a diode laser array. The laser can operate both in cw mode-locked and simultaneously Q-switched and mode-locked (QML) regime. The peak power of the laser while ...

  12. Dynamic Diffraction Studies on the Crystallization, Phase Transformation, and Activation Energies in Anodized Titania Nanotubes

    OpenAIRE

    Hani Albetran; Victor Vega; Victor M. Prida; It-Meng Low

    2018-01-01

    The influence of calcination time on the phase transformation and crystallization kinetics of anodized titania nanotube arrays was studied using in-situ isothermal and non-isothermal synchrotron radiation diffraction from room temperature to 900 °C. Anatase first crystallized at 400 °C, while rutile crystallized at 550 °C. Isothermal heating of the anodized titania nanotubes by an increase in the calcination time at 400, 450, 500, 550, 600, and 650 °C resulted in a slight reduction in anatase...

  13. Multiband Photonic Phased-Array Antenna

    Science.gov (United States)

    Tang, Suning

    2015-01-01

    A multiband phased-array antenna (PAA) can reduce the number of antennas on shipboard platforms while offering significantly improved performance. Crystal Research, Inc., has developed a multiband photonic antenna that is based on a high-speed, optical, true-time-delay beamformer. It is capable of simultaneously steering multiple independent radio frequency (RF) beams in less than 1,000 nanoseconds. This high steering speed is 3 orders of magnitude faster than any existing optical beamformer. Unlike other approaches, this technology uses a single controlling device per operation band, eliminating the need for massive optical switches, laser diodes, and fiber Bragg gratings. More importantly, only one beamformer is needed for all antenna elements.

  14. The electronics of the INDRA 4π detection array

    International Nuclear Information System (INIS)

    Pouthas, J.; Bertaut, A.; Bourgault, P.; Martina, L.; Olivier, L.; Piquet, B.; Plagnol, E.; Raine, B.; Saint-Laurent, F.; Spitaels, C.

    1995-01-01

    The INDRA multidetector is composed of 96 ionization chambers, 196 silicon detectors, 324 CsI(Tl) scintillators and 12 NE102/NE115 phoswich detectors. The associated electronics is presented. The signal treatment is performed through specifically designed modules, most of which are in the new VXIbus standard. The large dynamic range required for the silicon detectors is reached by means of a low noise amplifier providing a unipolar signal which is charge integrated and converted on two dynamic ranges. The trigger system relies on a new working mode called 'asynchronous mode' and performs event selections based on multiplicity functions which are built up from subgroups of detectors. The performances of the data acquisition and the graphical software packages are also presented. (author)

  15. Two-dimensional analytic modeling of acoustic diffraction for ultrasonic beam steering by phased array transducers.

    Science.gov (United States)

    Wang, Tiansi; Zhang, Chong; Aleksov, Aleksandar; Salama, Islam; Kar, Aravinda

    2017-04-01

    Phased array ultrasonic transducers enable modulating the focal position of the acoustic waves, and this capability is utilized in many applications, such as medical imaging and non-destructive testing. This type of transducers also provides a mechanism to generate tilted wavefronts in acousto-optic deflectors to deflect laser beams for high precision advanced laser material processing. In this paper, a theoretical model is presented for the diffraction of ultrasonic waves emitted by several phased array transducers into an acousto-optic medium such as TeO 2 crystal. A simple analytic expression is obtained for the distribution of the ultrasonic displacement field in the crystal. The model prediction is found to be in good agreement with the results of a numerical model that is based on a non-paraxial multi-Gaussian beam (NMGB) model. Published by Elsevier B.V.

  16. Synthesis and crystal structures of three new benzotriazolylpropanamides

    Directory of Open Access Journals (Sweden)

    Donna S. Amenta

    2017-06-01

    Full Text Available The base-catalyzed Michael addition of 2-methylacrylamide to benzotriazole afforded 3-(1H-benzotriazol-1-yl-2-methylpropanamide, C10H12N4O (1, in 32% yield in addition to small amounts of isomeric 3-(2H-benzotriazol-2-yl-2-methylpropanamide, C10H12N4O (2. In a similar manner, 3-(1H-benzotriazol-1-yl-N,N-dimethylpropanamide, C11H14N4O (3, was prepared from benzotriazole and N,N-dimethylacrylamide. All three products have been structurally characterized by single-crystal X-ray diffraction. The crystal structures of 1 and 2 comprise infinite arrays formed by N—H...O and N—H...N bridges, as well as π–π interactions, while the molecules of 3 are aggregated to simple π-dimers in the crystal.

  17. Optical properties of anisotropic 3D nanoparticles arrays

    Science.gov (United States)

    Santiago, E. Y.; Esquivel-Sirvent, R.

    2017-07-01

    The optical properties of 3D periodic arrays of spheroidal Au nanoparticles are calculated using a Bruggeman effective medium approximation. The optical response of the supra-crystal depends on the volume fraction of the nanoparticles and their aspect or size ratio (major/minor axis). All the nanoparticles have the same orientation, and this defines an anisotropic dielectric function of the crystal. As a function of the filling fraction, while keeping the size ratio fixed, the maximum in the extinction spectra along the major and minor axes does not show a significant change. However, for a fixed filling fraction, varying the aspect ratio of the particles induces a shift of several hundred of nanometers in the maximum of the extinction spectra along the major axis and almost no changes along the minor axis. Depending on the aspect ratio and the filling fraction, we show that the supra-crystal has three regimes with different values of an effective plasma frequency. Contribution to the Focus Issue Self-assemblies of Inorganic and Organic Nanomaterials edited by Marie-Paule Pileni.

  18. Evaluation of Matrix9 silicon photomultiplier array for small-animal PET

    Science.gov (United States)

    Du, Junwei; Schmall, Jeffrey P.; Yang, Yongfeng; Di, Kun; Roncali, Emilie; Mitchell, Gregory S.; Buckley, Steve; Jackson, Carl; Cherry, Simon R.

    2015-01-01

    Purpose: The MatrixSL-9-30035-OEM (Matrix9) from SensL is a large-area silicon photomultiplier (SiPM) photodetector module consisting of a 3 × 3 array of 4 × 4 element SiPM arrays (total of 144 SiPM pixels) and incorporates SensL’s front-end electronics board and coincidence board. Each SiPM pixel measures 3.16 × 3.16 mm2 and the total size of the detector head is 47.8 × 46.3 mm2. Using 8 × 8 polished LSO/LYSO arrays (pitch 1.5 mm) the performance of this detector system (SiPM array and readout electronics) was evaluated with a view for its eventual use in small-animal positron emission tomography (PET). Methods: Measurements of noise, signal, signal-to-noise ratio, energy resolution, flood histogram quality, timing resolution, and array trigger error were obtained at different bias voltages (28.0–32.5 V in 0.5 V intervals) and at different temperatures (5 °C–25 °C in 5 °C degree steps) to find the optimal operating conditions. Results: The best measured signal-to-noise ratio and flood histogram quality for 511 keV gamma photons were obtained at a bias voltage of 30.0 V and a temperature of 5 °C. The energy resolution and timing resolution under these conditions were 14.2% ± 0.1% and 4.2 ± 0.1 ns, respectively. The flood histograms show that all the crystals in the 1.5 mm pitch LSO array can be clearly identified and that smaller crystal pitches can also be resolved. Flood histogram quality was also calculated using different center of gravity based positioning algorithms. Improved and more robust results were achieved using the local 9 pixels for positioning along with an energy offset calibration. To evaluate the front-end detector readout, and multiplexing efficiency, an array trigger error metric is introduced and measured at different lower energy thresholds. Using a lower energy threshold greater than 150 keV effectively eliminates any mispositioning between SiPM arrays. Conclusions: In summary, the Matrix9 detector system can resolve

  19. Evaluation of Matrix9 silicon photomultiplier array for small-animal PET

    International Nuclear Information System (INIS)

    Du, Junwei; Schmall, Jeffrey P.; Yang, Yongfeng; Di, Kun; Roncali, Emilie; Mitchell, Gregory S.; Buckley, Steve; Jackson, Carl; Cherry, Simon R.

    2015-01-01

    Purpose: The MatrixSL-9-30035-OEM (Matrix9) from SensL is a large-area silicon photomultiplier (SiPM) photodetector module consisting of a 3 × 3 array of 4 × 4 element SiPM arrays (total of 144 SiPM pixels) and incorporates SensL’s front-end electronics board and coincidence board. Each SiPM pixel measures 3.16 × 3.16 mm 2 and the total size of the detector head is 47.8 × 46.3 mm 2 . Using 8 × 8 polished LSO/LYSO arrays (pitch 1.5 mm) the performance of this detector system (SiPM array and readout electronics) was evaluated with a view for its eventual use in small-animal positron emission tomography (PET). Methods: Measurements of noise, signal, signal-to-noise ratio, energy resolution, flood histogram quality, timing resolution, and array trigger error were obtained at different bias voltages (28.0–32.5 V in 0.5 V intervals) and at different temperatures (5 °C–25 °C in 5 °C degree steps) to find the optimal operating conditions. Results: The best measured signal-to-noise ratio and flood histogram quality for 511 keV gamma photons were obtained at a bias voltage of 30.0 V and a temperature of 5 °C. The energy resolution and timing resolution under these conditions were 14.2% ± 0.1% and 4.2 ± 0.1 ns, respectively. The flood histograms show that all the crystals in the 1.5 mm pitch LSO array can be clearly identified and that smaller crystal pitches can also be resolved. Flood histogram quality was also calculated using different center of gravity based positioning algorithms. Improved and more robust results were achieved using the local 9 pixels for positioning along with an energy offset calibration. To evaluate the front-end detector readout, and multiplexing efficiency, an array trigger error metric is introduced and measured at different lower energy thresholds. Using a lower energy threshold greater than 150 keV effectively eliminates any mispositioning between SiPM arrays. Conclusions: In summary, the Matrix9 detector system can

  20. Signal encoding method for a time-of-flight PET detector using a silicon photomultiplier array

    Science.gov (United States)

    Kwon, Sun Il; Lee, Jae Sung

    2014-10-01

    The silicon photomultiplier (SiPM) is a promising photosensor for magnetic resonance (MR) compatible time-of-flight (TOF) positron emission tomography (PET) scanners. The compact size of the SiPM allows direct one-to-one coupling between the scintillation crystal and the photosensor, yielding better timing and energy resolutions than the light sharing methods that have to be used in photomultiplier tube (PMT) PET systems. However, the one-to-one coupling scheme requires a huge volume of readout and processing electronics if no electric signal multiplexing or encoding scheme is properly applied. In this paper, we develop an electric signal encoding scheme for SiPM array based TOF PET detector blocks with the aim of reducing the complexity and volume of the signal readout and processing electronics. In an M×N SiPM array, the output signal of each channel in the SiPM array is divided into two signal lines. These output lines are then tied together in row and column lines. The row and column signals are used to measure the energy and timing information (or vice versa) of each incident gamma-ray event, respectively. Each SiPM channel was directly coupled to a 3×3×20 mm3 LGSO crystal. The reference detector, which was used to measure timing, consisted of an R9800 PMT and a 4×4×10 mm3 LYSO crystal and had a single time resolution of ~200 ps (FWHM). Leading edge discriminators were used to determine coincident events. Dedicated front-end electronics were developed, and the timing and energy resolutions of SiPM arrays with different array sizes (4×4, 8×8, and 12×12) were compared. Breakdown voltage of each SiPM channel was measured using energy spectra within various bias voltages. Coincidence events were measured using a 22Na point source. The average coincidence time resolution of 4×4, 8×8, and 12×12 SiPM arrays were 316 ps, 320 ps, and 335 ps (FWHM), respectively. The energy resolution of 4×4, 8×8, and 12×12 SiPM arrays were 11.8%, 12.5%, and 12.8% (FWHM

  1. Array capabilities and future arrays

    International Nuclear Information System (INIS)

    Radford, D.

    1993-01-01

    Early results from the new third-generation instruments GAMMASPHERE and EUROGAM are confirming the expectation that such arrays will have a revolutionary effect on the field of high-spin nuclear structure. When completed, GAMMASHPERE will have a resolving power am order of magnitude greater that of the best second-generation arrays. When combined with other instruments such as particle-detector arrays and fragment mass analysers, the capabilites of the arrays for the study of more exotic nuclei will be further enhanced. In order to better understand the limitations of these instruments, and to design improved future detector systems, it is important to have some intelligible and reliable calculation for the relative resolving power of different instrument designs. The derivation of such a figure of merit will be briefly presented, and the relative sensitivities of arrays currently proposed or under construction presented. The design of TRIGAM, a new third-generation array proposed for Chalk River, will also be discussed. It is instructive to consider how far arrays of Compton-suppressed Ge detectors could be taken. For example, it will be shown that an idealised open-quote perfectclose quotes third-generation array of 1000 detectors has a sensitivity an order of magnitude higher again than that of GAMMASPHERE. Less conventional options for new arrays will also be explored

  2. Study of a large BGO crystal in a charged particle beam

    International Nuclear Information System (INIS)

    Zhang, N.; Ding, Z.; Wu, Y.; Salomon, M.

    1990-01-01

    We have studied two large crystals of Bismuth Germanate (BGO) with sources and in a pion beam. The response and uniformity have been investigated with several types of reflectors. The temperature dependance of the emitted light was determined, as well as the timing resolution. As the crystal is intended to be part of a large array with very good energy resolution in the detection of high energy gamma rays and electrons, uniformities of better than 0.5% are required. Various methods to achieve this will be discussed

  3. Quality Assurance on Undoped CsI Crystals for the Mu2e Experiment

    Science.gov (United States)

    Atanov, N.; Baranov, V.; Budagov, J.; Davydov, Yu. I.; Glagolev, V.; Tereshchenko, V.; Usubov, Z.; Cervelli, F.; Di Falco, S.; Donati, S.; Morescalchi, L.; Pedreschi, E.; Pezzullo, G.; Raffaelli, F.; Spinella, F.; Colao, F.; Cordelli, M.; Corradi, G.; Diociaiuti, E.; Donghia, R.; Giovannella, S.; Happacher, F.; Martini, M.; Miscetti, S.; Ricci, M.; Saputi, A.; Sarra, I.; Echenard, B.; Hitlin, D. G.; Hu, C.; Miyashita, T.; Porter, F.; Zhang, L.; Zhu, R.-Y.; Grancagnolo, F.; Tassielli, G.; Murat, P.

    2018-02-01

    The Mu2e experiment is constructing a calorimeter consisting of 1,348 undoped CsI crystals in two disks. Each crystal has a dimension of 34 x 34 x 200 mm, and is readout by a large area silicon PMT array. A series of technical specifications was defined according to physics requirements. Preproduction CsI crystals were procured from three firms: Amcrys, Saint-Gobain and Shanghai Institute of Ceramics. We report the quality assurance on crystal's scintillation properties and their radiation hardness against ionization dose and neutrons. With a fast decay time of 30 ns and a light output of more than 100 p.e./MeV measured with a bi-alkali PMT, undoped CsI crystals provide a cost-effective solution for the Mu2e experiment.

  4. High Resolution Displays Using NCAP Liquid Crystals

    Science.gov (United States)

    Macknick, A. Brian; Jones, Phil; White, Larry

    1989-07-01

    Nematic curvilinear aligned phase (NCAP) liquid crystals have been found useful for high information content video displays. NCAP materials are liquid crystals which have been encapsulated in a polymer matrix and which have a light transmission which is variable with applied electric fields. Because NCAP materials do not require polarizers, their on-state transmission is substantially better than twisted nematic cells. All dimensional tolerances are locked in during the encapsulation process and hence there are no critical sealing or spacing issues. By controlling the polymer/liquid crystal morphology, switching speeds of NCAP materials have been significantly improved over twisted nematic systems. Recent work has combined active matrix addressing with NCAP materials. Active matrices, such as thin film transistors, have given displays of high resolution. The paper will discuss the advantages of NCAP materials specifically designed for operation at video rates on transistor arrays; applications for both backlit and projection displays will be discussed.

  5. A scintillating bolometer array for double beta decay studies: The LUCIFER experiment

    Energy Technology Data Exchange (ETDEWEB)

    Gironi, L., E-mail: luca.gironi@mib.infn.it [Università degli Studi di Milano-Bicocca, Milano (Italy); INFN – Sezione di Milano-Bicocca, Milano (Italy)

    2016-07-11

    The main goal of the LUCIFER experiment is to study the neutrinoless double beta decay, a rare process allowed if neutrinos are Majorana particles. Although aiming at a discovery, in the case of insufficient sensitivity the LUCIFER technique will be the demonstrator for a higher mass experiment able to probe the entire inverted hierarchy region of the neutrino mass. In order to achieve this challenging result, high resolution detectors with active background discrimination capability are required. This very interesting possibility can be largely fulfilled by scintillating bolometers thanks to the simultaneous read-out of heat and light emitted by the interactions in the detector or by pulse shape analysis. - Highlights: • The LUCIFER technique will be the demonstrator for a higher mass experiment. • Scintillating bolometers allow high energy resolution and background discrimination. • The first choice for the LUCIFER tower are ZnSe crystals. • The LUCIFER setup will consist of an array of 30 individual single module detectors. • An array of ZnMoO4 crystals allowed the bolometric observation of the 2vDBD of {sup 100}Mo.

  6. Local polarization phenomena in In-doped CdTe x-ray detector arrays

    International Nuclear Information System (INIS)

    Sato, Toshiyuki; Sato, Kenji; Ishida, Shinichiro; Kiri, Motosada; Hirooka, Megumi; Yamada, Masayoshi; Kanamori, Hitoshi

    1995-01-01

    Local polarization phenomena have been studied in detector arrays with the detector element size of 500 microm x 500 microm, which are fabricated from high-resistivity In-doped CdTe crystals grown by the vertical Bridgman technique. It has been found for the first time that a polarization effect, which is characterized by a progressive decrease of the pulse counting rate with increasing photon fluence, strongly depends on the detector elements, that is, the portion of crystals used. The influence of several parameters, such as the applied electric field strength, time, and temperature, on this local polarization effect is also investigated. From the photoluminescence measurements of the inhomogeneity of In dopant, it is concluded that the local polarization effect observed here originates from a deep level associated with In dopant in CdTe crystals

  7. Pilot tests of a PET detector using the TOF-PET ASIC based on monolithic crystals and SiPMs

    International Nuclear Information System (INIS)

    Aguilar, A.; González-Montoro, A.; González, A.J.; Hernández, L.; Monzó, J.M.; Benlloch, J.M.; Bugalho, R.; Ferramacho, L.

    2016-01-01

    In this work we show pilot tests of PET detector blocks using the TOF-PET ASIC, coupled to SiPM detector arrays and different crystal configurations. We have characterized the main ASIC features running calibration processes to compensate the time dispersion among the different ASIC/SiPM paths as well as for the time walk on the arrival of optical photons. The aim of this work is to use of LYSO monolithic crystals and explore their photon Depth of Interaction (DOI) capabilities, keeping good energy and spatial resolutions. First tests have been carried out with crystal arrays. Here we made it possible to reach a coincidence resolving times (CRT) of 370 ps FWHM, with energy resolutions better than 20% and resolving well 2 mm sized crystal elements. When using monolithic crystals, a single-pixel LYSO reference crystal helped to explore the CRT performance. We studied different strategies to provide the best timestamp determination in the monolithic scintillator. Times around 1 ns FWHM have been achieved in these pilot studies. In terms of spatial and energy resolution, values of about 3 mm and better than 30% were found, respectively. We have also demonstrated the capability of this system (monolithic and ASIC) to return accurate DOI information.

  8. Electron cryomicroscopy of two-dimensional crystals of the H+-ATPase from chloroplasts

    NARCIS (Netherlands)

    Böttcher, Bettina; Gräber, Peter; Boekema, Egbert J.; Lücken, Uwe

    1995-01-01

    The H+-ATPase from spinach chloroplasts was isolated and purified. Two-dimensional crystals were obtained from the protein/lipid/detergent micelles by treatment with phospholipase and simultaneous removal of detergent and fatty acids by Biobeads. The resulting two-dimensionally ordered arrays were

  9. ELECTRON CRYOMICROSCOPY OF 2-DIMENSIONAL CRYSTALS OF THE H+-ATPASE FROM CHLOROPLASTS

    NARCIS (Netherlands)

    BOTTCHER, B; GRABER, P; BOEKEMA, EJ; LUCKEN, U

    1995-01-01

    The H+-ATPase from spinach chloroplasts was isolated and purified, Two-dimensional crystals were obtained from the protein/lipid/detergent micelles by treatment with phospholipase and simultaneous removal of detergent and fatty acids by Biobeads. The resulting two-dimensionally ordered arrays were

  10. Copper-encapsulated vertically aligned carbon nanotube arrays.

    Science.gov (United States)

    Stano, Kelly L; Chapla, Rachel; Carroll, Murphy; Nowak, Joshua; McCord, Marian; Bradford, Philip D

    2013-11-13

    A new procedure is described for the fabrication of vertically aligned carbon nanotubes (VACNTs) that are decorated, and even completely encapsulated, by a dense network of copper nanoparticles. The process involves the conformal deposition of pyrolytic carbon (Py-C) to stabilize the aligned carbon-nanotube structure during processing. The stabilized arrays are mildly functionalized using oxygen plasma treatment to improve wettability, and they are then infiltrated with an aqueous, supersaturated Cu salt solution. Once dried, the salt forms a stabilizing crystal network throughout the array. After calcination and H2 reduction, Cu nanoparticles are left decorating the CNT surfaces. Studies were carried out to determine the optimal processing parameters to maximize Cu content in the composite. These included the duration of Py-C deposition and system process pressure as well as the implementation of subsequent and multiple Cu salt solution infiltrations. The optimized procedure yielded a nanoscale hybrid material where the anisotropic alignment from the VACNT array was preserved, and the mass of the stabilized arrays was increased by over 24-fold because of the addition of Cu. The procedure has been adapted for other Cu salts and can also be used for other metal salts altogether, including Ni, Co, Fe, and Ag. The resulting composite is ideally suited for application in thermal management devices because of its low density, mechanical integrity, and potentially high thermal conductivity. Additionally, further processing of the material via pressing and sintering can yield consolidated, dense bulk composites.

  11. Formation of a silicon micropore array of a two-dimension electron multiplier by photo electrochemical etching

    International Nuclear Information System (INIS)

    Gao Yanjun; Duanmu Qingduo; Wang Guozheng; Li Ye; Tian Jingquan

    2009-01-01

    A semiconductor PEC etching method is applied to fabricate the n-type silicon deep micropore channel array. In this method, it is important to arrange the direction of the micropore array along the crystal orientation of the Si substrate. Otherwise, serious lateral erosion will happen. The etching process is also relative to the light intensity and HF concentration. 5% HF concentration and 10-15 cm distance between the light source and the silicon wafer are demonstrated to be the best in our experiments. The n-type silicon deep micropore channel array with aperture of 3 μm and aspect ratio of 40-60, whose inner walls are smooth, is finally obtained.

  12. Dispersion relation of electromagnetic waves in one-dimensional plasma photonic crystals

    International Nuclear Information System (INIS)

    Hojo, Hitoshi; Mase, Atsushi

    2004-01-01

    The dispersion relation of electromagnetic waves in one-dimensional plasma photonic crystals is studied. The plasma photonic crystal is a periodic array composed of alternating thin plasma and dielectric material. The dispersion relation is obtained by solving a Maxwell wave equation using a method analogous to Kronig-Penny's problem in quantum mechanics, and it is found that the frequency gap and cut-off appear in the dispersion relation. The frequency gap is shown to become larger with the increase of the plasma density as well as plasma width. (author)

  13. Direct and indirect signal detection of 122 keV photons with a novel detector combining a pnCCD and a CsI(Tl) scintillator

    Energy Technology Data Exchange (ETDEWEB)

    Schlosser, D.M., E-mail: dieter.schlosser@pnsensor.de [PNSensor GmbH, Sckellstraße 3, 81667 München (Germany); Huth, M.; Hartmann, R. [PNSensor GmbH, Sckellstraße 3, 81667 München (Germany); Abboud, A.; Send, S. [Universität Siegen, Walter-Flex-Straße 3, 57072 Siegen (Germany); Conka-Nurdan, T. [Türkisch-Deutsche Universität, Sakinkaya Cad. 86, Beykoz, 34820 Istanbul (Turkey); Shokr, M.; Pietsch, U. [Universität Siegen, Walter-Flex-Straße 3, 57072 Siegen (Germany); Strüder, L. [PNSensor GmbH, Sckellstraße 3, 81667 München (Germany); Universität Siegen, Walter-Flex-Straße 3, 57072 Siegen (Germany)

    2016-01-01

    By combining a low noise fully depleted pnCCD detector with a CsI(Tl) scintillator, an energy-dispersive area detector can be realized with a high quantum efficiency (QE) in the range from below 1 keV to above 100 keV. In direct detection mode the pnCCD exhibits a relative energy resolution of 1% at 122 keV and spatial resolution of less than 75 µm, the pixel size of the pnCCD. In the indirect detection mode, i.e. conversion of the incoming X-rays in the scintillator, the measured energy resolution was about 9–13% at 122 keV, depending on the depth of interaction in the scintillator, while the position resolution, extracted with the help of simulations, was 30 µm only. We show simulated data for incident photons of 122 keV and compare the various interaction processes and relevant physical parameters to experimental results obtained with a radioactive {sup 57}Co source. - Highlights: • Position and energy resolving pnCCD+CsI(Tl) detector for energies from 1-150 keV • Detection in the pnCCD (122keV): 1% energy and <75µm spatial resolution • Detection in the scintillator (122keV): 9-12% energy and ~30µm spatial resolution.

  14. Highly Uniform Epitaxial ZnO Nanorod Arrays for Nanopiezotronics

    Directory of Open Access Journals (Sweden)

    Nagata T

    2009-01-01

    Full Text Available Abstract Highly uniform and c-axis-aligned ZnO nanorod arrays were fabricated in predefined patterns by a low temperature homoepitaxial aqueous chemical method. The nucleation seed patterns were realized in polymer and in metal thin films, resulting in, all-ZnO and bottom-contacted structures, respectively. Both of them show excellent geometrical uniformity: the cross-sectional uniformity according to the scanning electron micrographs across the array is lower than 2%. The diameter of the hexagonal prism-shaped nanorods can be set in the range of 90–170 nm while their typical length achievable is 0.5–2.3 μm. The effect of the surface polarity was also examined, however, no significant difference was found between the arrays grown on Zn-terminated and on O-terminated face of the ZnO single crystal. The transmission electron microscopy observation revealed the single crystalline nature of the nanorods. The current–voltage characteristics taken on an individual nanorod contacted by a Au-coated atomic force microscope tip reflected Schottky-type behavior. The geometrical uniformity, the designable pattern, and the electrical properties make the presented nanorod arrays ideal candidates to be used in ZnO-based DC nanogenerator and in next-generation integrated piezoelectric nano-electromechanical systems (NEMS.

  15. Transition between metamaterial and photonic-crystal behavior in arrays of dielectric rods

    Czech Academy of Sciences Publication Activity Database

    Dominec, Filip; Kadlec, Christelle; Němec, Hynek; Kužel, Petr; Kadlec, Filip

    2014-01-01

    Roč. 22, č. 25 (2014), s. 30492-30503 ISSN 1094-4087 R&D Projects: GA ČR(CZ) GA14-25639S Institutional support: RVO:68378271 Keywords : metamaterials * photonic crystals * negative refractive index * dielectrics Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.488, year: 2014

  16. CsI calorimeter with 3-D position resolution

    CERN Document Server

    Schopper, Herwig Franz; Shaw, H; Nefzger, C; Zoglauer, A; Schönfelder, V; Kanbach, G

    2000-01-01

    New gamma-ray calorimeter have been developed for the MEGA Compton camera. They consist of arrays of small CsI(Tl) scintillator bars read out by Silicon PIN-diodes and low noise, self-triggering frontend electronics. The length of the bars (the thickness of the calorimeter) can be varied for different applications to fit the stopping power needed and the light loss tolerable. In this paper we present calibration results from 2 cm long bars with diodes on one side, and 8 cm long bars with diodes on two opposite sides. Double-sided readout gives 3-D information of interactions which will be used to overcome the limited position resolution in Anger-cameras at high energies. Simpler detection devices like Anger-cameras might finally resolve only the centre of gravity. As events from gamma-rays with energies of MeV do extend over several cm, it is a prerequisite for an imaging device to resolve the interaction structure in detail. Combining CsI(Tl) scintillators, Silicon PIN-photodiodes and frontend electronics in...

  17. Electrically driven light emission from an array of Si nanoclusters

    International Nuclear Information System (INIS)

    Mazzitello, K I; Martin, H O; Aldao, C M; Roman, H E

    2004-01-01

    Charge transport and light emission properties of an array of silicon nanoclusters (NCs), sandwiched between a p-type and an n-type doped silicon crystal, are studied theoretically by assuming that electrons and holes enter from the opposite sides of the array in response to an applied electric field. The size of the NCs considered ranges from 16 nm down to 3.6 nm and their spatial distribution is optimized so that light emission, resulting from radiative recombinations, is peaked in the visible red around 1.8 eV. The light emission efficiency is limited by the carrier hopping times and is found to be in the range 2-0.5%, for fields ranging from 100 kV cm -1 to 500 kV cm -1 , respectively

  18. On-beam calibration of the {delta}E(Si)-Sci/PD charged particle telescope

    Energy Technology Data Exchange (ETDEWEB)

    Avdeichikov, V. E-mail: vladimir.Avdeichikov@kosufy.lu.se; Jakobsson, B.; Nikitin, V.A.; Nomokonov, P.V.; Veldhuizen, E.J. van

    2001-07-11

    The reaction products emitted in the {sup 14}N(45A MeV)+(CH{sub 2}/CD{sub 2}) interactions are identified by a {delta}E(Si)-E(Scintillator/Photodiode) telescope by the conventional {delta}E-E method. The position of 'jumps' in the amplitude of the photodiode signal for ions passing through the scintillator (Sci) is used to calibrate on-beam both the {delta}E and the Sci/PD scales in MeV. The accuracy of an absolute energy calibration is better than 2.3% and 1.8% for CsI(Tl) and GSO(Ce) detectors, respectively. It is defined mostly by the correctness of the range-energy relations of ions in the Si and Sci crystals. The light response function, L(E,Z,A), of isotopes up to Z(A)=8(16) in the range of energy {approx}(2.5-60)A MeV is extracted. The effects of doping concentration and pulse shaping on the light response are analyzed. The validity of the existing empirical light-energy relations is checked in a wide interval of ion energies and a new power law relation is proposed. Calculations of the response function based on the Murray-Mayer model are found to be in excellent agreement with experimental data for the CsI(Tl) crystal.

  19. Transparently wrap-gated semiconductor nanowire arrays for studies of gate-controlled photoluminescence

    Energy Technology Data Exchange (ETDEWEB)

    Nylund, Gustav; Storm, Kristian; Torstensson, Henrik; Wallentin, Jesper; Borgström, Magnus T.; Hessman, Dan; Samuelson, Lars [Solid State Physics, Nanometer Structure Consortium, Lund University, Box 118, S-221 00 Lund (Sweden)

    2013-12-04

    We present a technique to measure gate-controlled photoluminescence (PL) on arrays of semiconductor nanowire (NW) capacitors using a transparent film of Indium-Tin-Oxide (ITO) wrapping around the nanowires as the gate electrode. By tuning the wrap-gate voltage, it is possible to increase the PL peak intensity of an array of undoped InP NWs by more than an order of magnitude. The fine structure of the PL spectrum reveals three subpeaks whose relative peak intensities change with gate voltage. We interpret this as gate-controlled state-filling of luminescing quantum dot segments formed by zincblende stacking faults in the mainly wurtzite NW crystal structure.

  20. Investigation on the Photoelectrocatalytic Activity of Well-Aligned TiO2 Nanotube Arrays

    Directory of Open Access Journals (Sweden)

    Xiaomeng Wu

    2012-01-01

    Full Text Available Well-aligned TiO2 nanotube arrays were fabricated by anodizing Ti foil in viscous F− containing organic electrolytes, and the crystal structure and morphology of the TiO2 nanotube array were characterized and analyzed by XRD, SEM, and TEM, respectively. The photocatalytic activity of the TiO2 nanotube arrays was evaluated in the photocatalytic (PC and photoelectrocatalytic (PEC degradation of methylene blue (MB dye in different supporting solutions. The excellent performance of ca. 97% for color removal was reached after 90 min in the PEC process compared to that of PC process which indicates that a certain external potential bias favors the promotion of the electrode reaction rate on TiO2 nanotube array when it is under illumination. In addition, it is found that PEC process conducted in supporting solutions with low pH and containing Cl− is also beneficial to accelerate the degradation rate of MB.

  1. Fabrication of non-hexagonal close packed colloidal array on a substrate by transfer

    Science.gov (United States)

    Banik, Meneka; Mukherjee, Rabibrata

    Self-organized colloidal arrays find application in fabrication of solar cells with advanced light management strategies. We report a simple spincoating based approach for fabricating two dimensional colloidal crystals with hexagonal and non-hexagonal close packed assembly on flat and nanopatterned substrates. The non-HCP arrays were fabricated by spin coating the particles onto soft lithographically fabricated substrates. The substrate patterns impose directionality to the particles by confining them within the grooves. We have developed a technique by which the HCP and non-HCP arrays can be transferred to any surface. For this purpose the colloidal arrays were fabricated on a UV degradable PMMA layer, resulting in transfer of the particles on UV exposure. This allows the colloidal structures to be transported across substrates irrespective of their surface energy, wettability or morphology. Since the particles are transferred without exposing it to any kind of chemical or thermal environment, it can be utilized for placing particles on top of thin film solar cells for improving their absorption efficiency.

  2. Fabrication of titanium dioxide nanotube arrays using organic electrolytes

    Science.gov (United States)

    Yoriya, Sorachon

    anodization rates are relatively slower in DEG electrolyte; as a result, the nanotube length is typically less than 10 microm. Pore size of nanotubes grown in DEG has been extended from 150 nm up to approximately 400 nm. The approach to pore widening could be achieved by using a specific condition of low HF concentration and prolonged anodization time. The study of evolution of nanotubes grown in DEG electrolytes showed that a fibrous layer was formed in the early growth stages and then was chemically and gradually removed after a long duration, leaving behind the nanotubes with large pore size. In DEG electrolyte, the closer spacing between Ti and Pt electrodes resulted in the larger nanotube morphological parameters due to the enhanced electrode kinetics facilitating the electrode reactions. Furthermore, this dissertation showed possibilities to crystallize the titania nanotube array films at room temperature via anodization in either DMSO or DEG electrolytes. The partially crystallized films could be achieved specifically in the optimum slow growth process conditions. Due to partial crystallization of the as-anodized samples, the high temperature annealing study revealed that the temperatures of phase transformation are 260 ºC and 430°C for respectively amorphous to anatase and anatase to rutile, which are accounted as the lowest phase transformation temperatures reported to date (2010). Finally, the photoelectrochemical properties of the DMSO fabricated nanotubes were investigated. The maximum photocurrent density of ~ 11 mA cm--2 was achieved by using the 46-microm long nanotube array sample with completely open pores, and photoconversion efficiencies of 5.425 % (+/- 0.087) (under UV light) and 0.197 % (+/- 0.001) (under solar spectrum AM 1.5) have been demonstrated. Biomedical applications of the DEG fabricated nanotube arrays films such as blood clotting, hemocompatibility, and drug delivery were investigated. The titania nanotube arrays showed a significant platelet

  3. The electronics of the INDRA 4{pi} detection array

    Energy Technology Data Exchange (ETDEWEB)

    Pouthas, J.; Bertaut, A.; Bourgault, P.; Martina, L.; Olivier, L.; Piquet, B.; Plagnol, E.; Raine, B.; Saint-Laurent, F.; Spitaels, C. [and others

    1995-12-31

    The INDRA multidetector is composed of 96 ionization chambers, 196 silicon detectors, 324 CsI(Tl) scintillators and 12 NE102/NE115 phoswich detectors. The associated electronics is presented. The signal treatment is performed through specifically designed modules, most of which are in the new VXIbus standard. The large dynamic range required for the silicon detectors is reached by means of a low noise amplifier providing a unipolar signal which is charge integrated and converted on two dynamic ranges. The trigger system relies on a new working mode called `asynchronous mode` and performs event selections based on multiplicity functions which are built up from subgroups of detectors. The performances of the data acquisition and the graphical software packages are also presented. (author). 22 refs. Submitted to Nuclear Instruments and Methods (NL).

  4. TiO2 Nanotube Arrays Composite Film as Photoanode for High-Efficiency Dye-Sensitized Solar Cell

    Directory of Open Access Journals (Sweden)

    Jinghua Hu

    2014-01-01

    Full Text Available A double-layered photoanode made of hierarchical TiO2 nanotube arrays (TNT-arrays as the overlayer and commercial-grade TiO2 nanoparticles (P25 as the underlayer is designed for dye-sensitized solar cells (DSSCs. Crystallized free-standing TNT-arrays films are prepared by two-step anodization process. For photovoltaic applications, DSSCs based on double-layered photoanodes produce a remarkably enhanced power conversion efficiency (PCE of up to 6.32% compared with the DSSCs solely composed of TNT-arrays (5.18% or nanoparticles (3.65% with a similar thickness (24 μm at a constant irradiation of 100 mW cm−2. This is mainly attributed to the fast charge transport paths and superior light-scattering ability of TNT-arrays overlayer and good electronic contact with F-doped tin oxide (FTO glass provided from P25 nanoparticles as a bonding layer.

  5. Iron Fibers Arrays Prepared by Electrodepositing in Reverse Liquid Crystalline

    Institute of Scientific and Technical Information of China (English)

    ZHAO Suling; LIN Dong; GUAN Jianguo; ZHANG Lianmeng

    2006-01-01

    Ordered iron fiber arrays were electrodeposited on the surface of zinc foils using "FeSO4 solution-sodium caprylate-Decanol" 3-component reverse hexagonal liquid crystal as soft templates. The structure of the soft templates and the synthesized iron fibers were characterized by polarizing microscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray microanalysis etc. The experimental results show that the synthesized iron fibers with α crystal phase grew up in the form of fiber clusters of about 200 nm along the direction perpendicular to the cathode surface. Each cluster was composed of several tens of fibers. The fibers had almost the same length of more than 10 μm with a diameter of about 50 nm.

  6. Self-assembled hierarchical nanostructures for high-efficiency porous photonic crystals.

    Science.gov (United States)

    Passoni, Luca; Criante, Luigino; Fumagalli, Francesco; Scotognella, Francesco; Lanzani, Guglielmo; Di Fonzo, Fabio

    2014-12-23

    The nanoscale modulation of material properties such as porosity and morphology is used in the natural world to mold the flow of light and to obtain structural colors. The ability to mimic these strategies while adding technological functionality has the potential to open up a broad array of applications. Porous photonic crystals are one such technological candidate, but have typically underachieved in terms of available materials, structural and optical quality, compatibility with different substrates (e.g., silicon, flexible organics), and scalability. We report here an alternative fabrication method based on the bottom-up self-assembly of elementary building blocks from the gas phase into high surface area photonic hierarchical nanostructures at room temperature. Periodic refractive index modulation is achieved by stacking layers with different nanoarchitectures. High-efficiency porous Bragg reflectors are successfully fabricated with sub-micrometer thick films on glass, silicon, and flexible substrates. High diffraction efficiency broadband mirrors (R≈1), opto-fluidic switches, and arrays of photonic crystal pixels with size<10 μm are demonstrated. Possible applications in filtering, sensing, electro-optical modulation, solar cells, and photocatalysis are envisioned.

  7. Towards UV imaging sensors based on single-crystal diamond chips for spectroscopic applications

    Energy Technology Data Exchange (ETDEWEB)

    De Sio, A. [Department of Astronomy and Space Science, University of Firenze, Largo E. Fermi 2, 50125 Florence (Italy)], E-mail: desio@arcetri.astro.it; Bocci, A. [Department of Astronomy and Space Science, University of Firenze, Largo E. Fermi 2, 50125 Florence (Italy); Bruno, P.; Di Benedetto, R.; Greco, V.; Gullotta, G. [INAF-Astrophysical Observatory of Catania (Italy); Marinelli, M. [INFN-Department of Mechanical Engineering, University of Roma ' Tor Vergata' (Italy); Pace, E. [Department of Astronomy and Space Science, University of Firenze, Largo E. Fermi 2, 50125 Florence (Italy); Rubulotta, D.; Scuderi, S. [INAF-Astrophysical Observatory of Catania (Italy); Verona-Rinati, G. [INFN-Department of Mechanical Engineering, University of Roma ' Tor Vergata' (Italy)

    2007-12-11

    The recent improvements achieved in the Homoepitaxial Chemical Vapour Deposition technique have led to the production of high-quality detector-grade single-crystal diamonds. Diamond-based detectors have shown excellent performances in UV and X-ray detection, paving the way for applications of diamond technology to the fields of space astronomy and high-energy photon detection in harsh environments or against strong visible light emission. These applications are possible due to diamond's unique properties such as its chemical inertness and visible blindness, respectively. Actually, the development of linear array detectors represents the main issue for a full exploitation of diamond detectors. Linear arrays are a first step to study bi-dimensional sensors. Such devices allow one to face the problems related to pixel miniaturisation and of signal read-out from many channels. Immediate applications would be in spectroscopy, where such arrays are preferred. This paper reports on the development of imaging detectors made by our groups, starting from the material growth and characterisation, through the design, fabrication and packaging of 2xn pixel arrays, to their electro-optical characterisation in terms of UV sensitivity, uniformity of the response and to the development of an electronic circuit suitable to read-out very low photocurrent signals. The detector and its electronic read-out were then tested using a 2x5 pixel array based on a single-crystal diamond. The results will be discussed in the framework of the development of an imager device for X-UV astronomy applications in space missions.

  8. Direct Writing of Three-Dimensional Macroporous Photonic Crystals on Pressure-Responsive Shape Memory Polymers.

    Science.gov (United States)

    Fang, Yin; Ni, Yongliang; Leo, Sin-Yen; Wang, Bingchen; Basile, Vito; Taylor, Curtis; Jiang, Peng

    2015-10-28

    Here we report a single-step direct writing technology for making three-dimensional (3D) macroporous photonic crystal patterns on a new type of pressure-responsive shape memory polymer (SMP). This approach integrates two disparate fields that do not typically intersect: the well-established templating nanofabrication and shape memory materials. Periodic arrays of polymer macropores templated from self-assembled colloidal crystals are squeezed into disordered arrays in an unusual shape memory "cold" programming process. The recovery of the original macroporous photonic crystal lattices can be triggered by direct writing at ambient conditions using both macroscopic and nanoscopic tools, like a pencil or a nanoindenter. Interestingly, this shape memory disorder-order transition is reversible and the photonic crystal patterns can be erased and regenerated hundreds of times, promising the making of reconfigurable/rewritable nanooptical devices. Quantitative insights into the shape memory recovery of collapsed macropores induced by the lateral shear stresses in direct writing are gained through fundamental investigations on important process parameters, including the tip material, the critical pressure and writing speed for triggering the recovery of the deformed macropores, and the minimal feature size that can be directly written on the SMP membranes. Besides straightforward applications in photonic crystal devices, these smart mechanochromic SMPs that are sensitive to various mechanical stresses could render important technological applications ranging from chromogenic stress and impact sensors to rewritable high-density optical data storage media.

  9. Application of Piezocomposite Twin, Side by Side, Phased Array UT Probes for the Inspection of Stainless Steel

    International Nuclear Information System (INIS)

    Delaide, M.; Dumas, Ph

    2005-01-01

    UT probes to be used for the examination of coarse-grain structure must allow to detect and size cracks, with a high reliability level. The combination of TRL probes, with phased array and piezocomposite technologies allows to improve probes performances and inspection speed. Single element crystals are replaced by matrix arrays, allowing to deflect and skew the beams, to change the inspection depth. This paper describes the designing, the manufacturing and the characterisation of several probes

  10. Tailoring nonlinearity and dispersion of photonic crystal fibers using hybrid cladding

    International Nuclear Information System (INIS)

    Zhao-lun, Liu; Lan-tian, Hou; Wei, Wang

    2009-01-01

    We present a hybrid cladding photonic crystal fiber for shaping high nonlinear and flattened dispersion in a wide range of wavelengths. The new structure adopts hybrid cladding with different pitches, air-holes diameters and air-holes arrayed fashions. The full-vector finite element method with perfectly matched layer is used to investigate the characteristics of the hybrid cladding photonic crystal fiber such as nonlinearity and dispersion properties. The influence of the cladding structure parameters on the nonlinear coefficient and geometric dispersion is analyzed. High nonlinear coefficient and the dispersion properties of fibers are tailored by adjusting the cladding structure parameters. A novel hybrid cladding photonic crystal fiber with high nonlinear coefficient and dispersion flattened which is suited for super continuum generation is designed. (author)

  11. Design and construction of hierarchical TiO2 nanorod arrays by combining layer-by-layer and hydrothermal crystallization techniques for electrochromic application

    Science.gov (United States)

    Chen, Yongbo; Li, Xiaomin; Bi, Zhijie; He, Xiaoli; Li, Guanjie; Xu, Xiaoke; Gao, Xiangdong

    2018-05-01

    The hierarchical TiO2 (H-TiO2) nanorod arrays (NRAs) composed of single-crystalline nanorods and nanocrystals were finely designed and successfully constructed for electrochromic (EC) application. By combining layer-by-layer (LBL) method and hydrothermal crystallization technique, the superfine nanocrystals (5-7 nm), which can provide abundant active sites and facilitate ion insertion/extraction during EC reactions, were uniformly and conformally assembled on the surface of single-crystalline TiO2 (SC-TiO2) NRAs. The as-formed H-TiO2 NRAs integrate the advantages of one-dimensional NRAs with fast kinetics and superfine nanocrystals with high ion capacity, showing highly enhanced EC performance. Large optical contrast (40.3%), shorter coloring/bleaching time (22/4 s), high coloration efficiency (11.2 cm2 C-1), and excellent cycling stability can be achieved in H-TiO2 NRAs, superior to the pristine SC-TiO2 NRAs and nanocrystalline TiO2 films. This work provides a feasible and well-designed strategy to explore high-performance materials for EC application.

  12. Ethanol-assisted multi-sensitive poly(vinyl alcohol) photonic crystal sensor.

    Science.gov (United States)

    Chen, Cheng; Zhu, Yihua; Bao, Hua; Shen, Jianhua; Jiang, Hongliang; Peng, Liming; Yang, Xiaoling; Li, Chunzhong; Chen, Guorong

    2011-05-21

    An ethanol-assisted method is utilized to generate a robust gelated crystalline colloidal array (GCCA) photonic crystal sensor. The functionalized sensor efficiently diffracts the visible light and responds to various stimuli involving solvent, pH, cation, and compressive strain; the related color change can be easily distinguished by the naked eye. © The Royal Society of Chemistry 2011

  13. Multilayer Photonic Crystal for Spectral Narrowing of Emission

    Directory of Open Access Journals (Sweden)

    Zhanfang LIU

    2017-08-01

    Full Text Available Multilayer colloidal crystal has been prepared by the layer-by-layer deposition of silica microspheres on a glass slide. Each layer is a slab consisting of a fcc close-packed colloidal arrays. By properly choosing the sizes of spheres, the whole spectral feature of multilayer colloidal crystal can be tuned. Here, we engineered a multilayer superlattice structure with an effective passband between two stop bands. This gives a strong narrowing effect on emission spectrum. With the stop bands at the shortwave and longwave edges of emission spectrum, the passband in the central wavelength region can be regarded as a strong decrease of suppression effect and enhancement of a narrow wavelength region of emission. The spectral narrowing modification effect of suitably engineered colloidal crystals shows up their importance in potential application as optical filters and lasing devices.DOI: http://dx.doi.org/10.5755/j01.ms.23.3.16320

  14. Radioanalytical Chemistry for Automated Nuclear Waste Process Monitoring

    International Nuclear Information System (INIS)

    Devol, Timothy A.

    2005-01-01

    Comparison of different pulse shape discrimination methods was performed under two different experimental conditions and the best method was identified. Beta/gamma discrimination of 90Sr/90Y and 137Cs was performed using a phoswich detector made of BC400 (2.5 cm OD x 1.2 cm) and BGO (2.5 cm O.D. x 2.5 cm ) scintillators. Alpha/gamma discrimination of 210Po and 137Cs was performed using a CsI:Tl (2.8 x 1.4 x 1.4 cm3) scintillation crystal. The pulse waveforms were digitized with a DGF-4c (X-Ray Instrumentation Associates) and analyzed offline with IGOR Pro software (Wavemetrics, Inc.). The four pulse shape discrimination methods that were compared include: rise time discrimination, digital constant fraction discrimination, charge ratio, and constant time discrimination (CTD) methods. The CTD method is the ratio of the pulse height at a particular time after the beginning of the pulse to the time at the maximum pulse height. The charge comparison method resulted in a Figure of Merit (FoM) of 3.3 (9.9 % spillover) and 3.7 (0.033 % spillover) for the phoswich and the CsI:Tl scintillator setups, respectively. The CTD method resulted in a FoM of 3.9 (9.2 % spillover) and 3.2 (0.25 % spillover), respectively. Inverting the pulse shape data typically resulted in a significantly higher FoM than conventional methods, but there was no reduction in % spillover values. This outcome illustrates that the FoM may not be a good scheme for the quantification of a system to perform pulse shape discrimination. Comparison of several pulse shape discrimination (PSD) methods was performed as a means to compare traditional analog and digital PSD methods on the same scintillation pulses. The X-ray Instrumentation Associates DGF-4C (40 Msps, 14-bit) was used to digitize waveforms from a CsI:Tl crystal and BC400/BGO phoswich detector

  15. SU-D-206-06: Task-Specific Optimization of Scintillator Thickness for CMOS-Detector Based Cone-Beam Breast CT

    Energy Technology Data Exchange (ETDEWEB)

    Vedantham, S; Shrestha, S; Shi, L; Vijayaraghavan, G; Karellas, A [University of Massachusetts Medical School, Worcester, MA (United States)

    2016-06-15

    Purpose: To optimize the cesium iodide (CsI:Tl) scintillator thickness in a complimentary metal-oxide semiconductor (CMOS)-based detector for use in dedicated cone-beam breast CT. Methods: The imaging task considered was the detection of a microcalcification cluster comprising six 220µm diameter calcium carbonate spheres, arranged in the form of a regular pentagon with 2 mm spacing on its sides and a central calcification, similar to that in ACR-recommended mammography accreditation phantom, at a mean glandular dose of 4.5 mGy. Generalized parallel-cascades based linear systems analysis was used to determine Fourier-domain image quality metrics in reconstructed object space, from which the detectability index inclusive of anatomical noise was determined for a non-prewhitening numerical observer. For 300 projections over 2π, magnification-associated focal-spot blur, Monte Carlo derived x-ray scatter, K-fluorescent emission and reabsorption within CsI:Tl, CsI:Tl quantum efficiency and optical blur, fiberoptic plate transmission efficiency and blur, CMOS quantum efficiency, pixel aperture function and additive noise, and filtered back-projection to isotropic 105µm voxel pitch with bilinear interpolation were modeled. Imaging geometry of a clinical prototype breast CT system, a 60 kV Cu/Al filtered x-ray spectrum from 0.3 mm focal spot incident on a 14 cm diameter semi-ellipsoidal breast were used to determine the detectability index for 300–600 µm thick (75µm increments) CsI:Tl. The CsI:Tl thickness that maximized the detectability index was considered optimal. Results: The limiting resolution (10% modulation transfer function, MTF) progressively decreased with increasing CsI:Tl thickness. The zero-frequency detective quantum efficiency, DQE(0), in projection space increased with increasing CsI:Tl thickness. The maximum detectability index was achieved with 525µm thick CsI:Tl scintillator. Reduced MTF at mid-to-high frequencies for 600µm thick CsI:Tl lowered

  16. LC-lens array with light field algorithm for 3D biomedical applications

    Science.gov (United States)

    Huang, Yi-Pai; Hsieh, Po-Yuan; Hassanfiroozi, Amir; Martinez, Manuel; Javidi, Bahram; Chu, Chao-Yu; Hsuan, Yun; Chu, Wen-Chun

    2016-03-01

    In this paper, liquid crystal lens (LC-lens) array was utilized in 3D bio-medical applications including 3D endoscope and light field microscope. Comparing with conventional plastic lens array, which was usually placed in 3D endoscope or light field microscope system to record image disparity, our LC-lens array has higher flexibility of electrically changing its focal length. By using LC-lens array, the working distance and image quality of 3D endoscope and microscope could be enhanced. Furthermore, the 2D/3D switching ability could be achieved if we turn off/on the electrical power on LClens array. In 3D endoscope case, a hexagonal micro LC-lens array with 350um diameter was placed at the front end of a 1mm diameter endoscope. With applying electric field on LC-lens array, the 3D specimen would be recorded as from seven micro-cameras with different disparity. We could calculate 3D construction of specimen with those micro images. In the other hand, if we turn off the electric field on LC-lens array, the conventional high resolution 2D endoscope image would be recorded. In light field microscope case, the LC-lens array was placed in front of the CMOS sensor. The main purpose of LC-lens array is to extend the refocusing distance of light field microscope, which is usually very narrow in focused light field microscope system, by montaging many light field images sequentially focusing on different depth. With adjusting focal length of LC-lens array from 2.4mm to 2.9mm, the refocusing distance was extended from 1mm to 11.3mm. Moreover, we could use a LC wedge to electrically shift the optics axis and increase the resolution of light field.

  17. Improvements in 130Te double beta decay search with cryogenic TeO2 array detectors

    International Nuclear Information System (INIS)

    Alessandrello, A.; Brofferio, C.; Bucci, C.; Caspani, P.; Cremonesi, O.; Fiorini, E.; Giuliani, A.; Nucciotti, A.; Pavan, M.; Pessina, G.; Previtali, E.; Zanotti, L.

    1996-01-01

    Single crystal TeO 2 bolometers have been used since 5 years ago to search for neutrinoless DBD of 130 Te. During the last year, our group has been studying and preparing the first array of 4 crystals, 340 g each, opening this technique to new frontiers in rare events' physics. The results and perspectives of this second generation cryogenic detectors are here reported and discussed, with particular emphasis on the peculiarities which make them feasible for a consistent upgrading of our previous result in DBD search. (orig.)

  18. Lumped model for rotational modes in phononic crystals

    KAUST Repository

    Peng, Pai

    2012-10-16

    We present a lumped model for the rotational modes induced by the rotational motion of individual scatterers in two-dimensional phononic crystals comprised of square arrays of solid cylindrical scatterers in solid hosts. The model provides a physical interpretation of the origin of the rotational modes, reveals the important role played by the rotational motion in determining the band structure, and reproduces the dispersion relations in a certain range. The model increases the possibilities of manipulating wave propagation in phononic crystals. In particular, expressions derived from the model for eigenfrequencies at high symmetry points unambiguously predict the presence of a new type of Dirac-like cone at the Brillouin center, which is found to be the result of accidental degeneracy of the rotational and dipolar modes.

  19. Lumped model for rotational modes in phononic crystals

    KAUST Repository

    Peng, Pai; Mei, Jun; Wu, Ying

    2012-01-01

    We present a lumped model for the rotational modes induced by the rotational motion of individual scatterers in two-dimensional phononic crystals comprised of square arrays of solid cylindrical scatterers in solid hosts. The model provides a physical interpretation of the origin of the rotational modes, reveals the important role played by the rotational motion in determining the band structure, and reproduces the dispersion relations in a certain range. The model increases the possibilities of manipulating wave propagation in phononic crystals. In particular, expressions derived from the model for eigenfrequencies at high symmetry points unambiguously predict the presence of a new type of Dirac-like cone at the Brillouin center, which is found to be the result of accidental degeneracy of the rotational and dipolar modes.

  20. Ultra-thin g-C{sub 3}N{sub 4} nanosheets wrapped silicon nanowire array for improved chemical stability and enhanced photoresponse

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Beibei; Yu, Hongtao; Quan, Xie, E-mail: quanxie@dlut.edu.cn; Chen, Shuo

    2014-11-15

    Highlights: • g-C{sub 3}N{sub 4}, as an oxygen free and metal free protective material for Si, was proposed. • g-C{sub 3}N{sub 4} nanosheets wrapped Si nanowire array was synthesized. • SiNW/g-C{sub 3}N{sub 4} exhibited enhancement of photoelectrochemical stability and photocurrent. - Abstract: In order to inhibit the oxidation of Si materials in aqueous solution, Si nanowire array was wrapped by ultra-thin g-C{sub 3}N{sub 4} nanosheets via an electrophoresis process. Scanning electron microscopy and transmission electron microscopy images showed that g-C{sub 3}N{sub 4} nanosheets were evenly distributed on the surface of Si nanowire array. X-ray diffraction patterns indicated that Si nanowire array/g-C{sub 3}N{sub 4} nanosheets were composed of Si (4 0 0 crystal plane) and g-C{sub 3}N{sub 4} (0 0 2 and 1 0 0 crystal planes). The cyclic voltammetry curves revealed that the corrosion of Si nanowire array was restrained under the protection of g-C{sub 3}N{sub 4} nanosheets. Furthermore, the photocurrent density of Si nanowire array/g-C{sub 3}N{sub 4} nanosheets increased by nearly 3 times compared to that of bare Si nanowire array due to the effective charge separation caused by the built-in electric field at the interface. This work will facilitate the applications of Si materials in aqueous solution, such as solar energy harvest and photocatalytic pollution control.

  1. Evaluation of a SiPM array detector coupled to a LFS-3 pixellated scintillator for PET/MR applications

    International Nuclear Information System (INIS)

    David, Stratos; Fysikopoulos, Eleftherios; Georgiou, Maria; Loudos, George

    2015-01-01

    SiPM arrays are insensitive to magnetic fields and thus good candidates for hybrid PET/MR imaging systems. Moreover, due to their small size and flexibility can be used in dedicated small field of view small animal imaging detectors and especially in head PET/MR studies in mice. Co-doped LFS-3 scintillator crystals have higher light yield and slightly faster response than that of LSO:Ce mainly due to the co-doped activation of emission centers with varying materials such as Ce, Gd, Sc, Y, La, Tb, or Ca distributed at the molecular scale through the lutetium silicate crystal host. The purpose of this study is to investigate the behavior of the SensL ArraySL-4 (4x4 element array of 3x3 mm 2 silicon photomultipliers) optical detector coupled to a 6x6 LFS-3 scintillator array, with 2x2x5 mm 3 crystal size elements, for possible applications in small field of view PET/MR imaging detectors. We have designed a symmetric resistive charge division circuit to read out the signal outputs of 4x4 pixel SiPM array reducing the 16 pixel outputs of the photodetector to 4 position signals. The 4 position signals were digitized using free running Analog to Digital Converters. The ADCs sampling rate was 50 MHz. An FPGA (Spartan 6 LX150T) was used for triggering and digital signal processing of the pulses. Experimental evaluation was carried out with 22 Na radioactive source and the parameters studied where energy resolution and peak to valley ratio. The first preliminary results of the evaluation shows a clear visualization of the discrete 2x2x5 mm 3 LFS-3 scintillator elements. The mean peak to valley ratio of the horizontal profiles on the raw image was measured equal to 11 while the energy resolution was calculated equal to 30% at the central pixels.

  2. Evaluation of a SiPM array detector coupled to a LFS-3 pixellated scintillator for PET/MR applications

    Energy Technology Data Exchange (ETDEWEB)

    David, Stratos; Fysikopoulos, Eleftherios [Technological Educational Institute of Athens (Greece); Georgiou, Maria [Technological Educational Institute of Athens (Greece); Department of Medical School, University of Thessaly, Larissa (Greece); Loudos, George [Technological Educational Institute of Athens (Greece)

    2015-05-18

    SiPM arrays are insensitive to magnetic fields and thus good candidates for hybrid PET/MR imaging systems. Moreover, due to their small size and flexibility can be used in dedicated small field of view small animal imaging detectors and especially in head PET/MR studies in mice. Co-doped LFS-3 scintillator crystals have higher light yield and slightly faster response than that of LSO:Ce mainly due to the co-doped activation of emission centers with varying materials such as Ce, Gd, Sc, Y, La, Tb, or Ca distributed at the molecular scale through the lutetium silicate crystal host. The purpose of this study is to investigate the behavior of the SensL ArraySL-4 (4x4 element array of 3x3 mm{sup 2} silicon photomultipliers) optical detector coupled to a 6x6 LFS-3 scintillator array, with 2x2x5 mm{sup 3} crystal size elements, for possible applications in small field of view PET/MR imaging detectors. We have designed a symmetric resistive charge division circuit to read out the signal outputs of 4x4 pixel SiPM array reducing the 16 pixel outputs of the photodetector to 4 position signals. The 4 position signals were digitized using free running Analog to Digital Converters. The ADCs sampling rate was 50 MHz. An FPGA (Spartan 6 LX150T) was used for triggering and digital signal processing of the pulses. Experimental evaluation was carried out with {sup 22}Na radioactive source and the parameters studied where energy resolution and peak to valley ratio. The first preliminary results of the evaluation shows a clear visualization of the discrete 2x2x5 mm{sup 3} LFS-3 scintillator elements. The mean peak to valley ratio of the horizontal profiles on the raw image was measured equal to 11 while the energy resolution was calculated equal to 30% at the central pixels.

  3. Flexible nanomembrane photonic-crystal cavities for tensilely strained-germanium light emission

    Energy Technology Data Exchange (ETDEWEB)

    Yin, Jian; Wang, Xiaowei; Paiella, Roberto [Department of Electrical and Computer Engineering and Photonics Center, Boston University, 8 Saint Mary' s Street, Boston, Massachusetts 02215 (United States); Cui, Xiaorui; Sookchoo, Pornsatit; Lagally, Max G. [Department of Materials Science and Engineering, University of Wisconsin – Madison, 1509 University Avenue, Madison, Wisconsin 53706 (United States)

    2016-06-13

    Flexible photonic-crystal cavities in the form of Si-column arrays embedded in polymeric films are developed on Ge nanomembranes using direct membrane assembly. The resulting devices can sustain large biaxial tensile strain under mechanical stress, as a way to enhance the Ge radiative efficiency. Pronounced emission peaks associated with photonic-crystal cavity resonances are observed in photoluminescence measurements. These results show that ultrathin nanomembrane active layers can be effectively coupled to an optical cavity, while still preserving their mechanical flexibility. Thus, they are promising for the development of strain-enabled Ge lasers, and more generally uniquely flexible optoelectronic devices.

  4. A high resolution germanium detector array for hypernuclear studies at PANDA

    Energy Technology Data Exchange (ETDEWEB)

    Bleser, Sebastian; Sanchez Lorente, Alicia; Steinen, Marcell [Helmholtz-Institut Mainz (Germany); Gerl, Juergen; Kojouharova, Jasmina; Kojouharov, Ivan [GSI Darmstadt (Germany); Iazzi, Felice [Politecnico, Torino (Italy); INFN, Torino (Italy); Pochodzalla, Josef; Rittgen, Kai; Sahin, Cihan [Institute for Nuclear Physics, JGU Mainz (Germany)

    2014-07-01

    The PANDA experiment, planned at the FAIR facility in Darmstadt, aims at the high resolution γ-spectroscopy of double Λ hypernuclei. For this purpose a devoted detector setup is required, consisting of a primary nuclear target, an active secondary target and a germanium detector array for the γ-spectroscopy. Due to the limited space within the PANDA detector a compact design is required. In particular the conventional LN{sub 2} cooling system must be replaced by an electro mechanical device and a new arrangement of the crystals is needed. This presentation shows the progress in the development of the germanium detectors. First results of in-beam measurements at COSY with a new electro mechanically cooled single crystal prototype are presented. Digital pulse shape analysis is used to disentangle pile up events due to the high event rate. This analysis technique also allows to recover the high original energy resolution in case of neutron damage. Finally the status of the new triple crystal detector prototype is given.

  5. Performance of an electromagnetic calorimeter with lead-tungstate crystals

    International Nuclear Information System (INIS)

    Kohara, R.; Sugitate, T.; Sugita, N.; Tsuchimoto, Y.; Toyoda, D.; Homma, K.; Yamazaki, H.

    2003-01-01

    The performance of an electromagnetic calorimeter with lead-tungstate (PWO) crystals was tested by using 1 GeV photons. The calorimeter consisted of nine crystals of 20 x 20 x 200 mm in size arranged in a 3 x 3 array. The energy resolution was obtained to be σ E /E = (2.50 ± 0.75%) / √E + (1.25 ± 0.34%) with a photomultiplier tube (PMT) reading all signals. Another setup, reading the central cell with an avalanche photo diode (APD) and the surrounding 8 cells with the PMT, was also studied, however, its energy resolution was not scaled with the stochastic function and we found the resolution of about 10% around 1 GeV. (author)

  6. Studies on an automated gain stabilisation for the new APD read-out of the crystal barrel calorimeter

    Energy Technology Data Exchange (ETDEWEB)

    Pauli, Peter [HISKP Bonn (Germany); Collaboration: CBELSA/TAPS-Collaboration

    2016-07-01

    For the investigation of the nucleon spectrum it is not enough to measure only cross sections because of the large overlap of resonances. To disentangle these resonances, a partial wave analysis is needed. To find unambiguous solutions it is necessary to measure (double) polarisation observables. The CBELSA/TAPS experiment is an important tool to measure these observables in meson photoproduction off nucleons. To achieve a high efficiency in purely neutral reactions it is important to implement the main calorimeter into the first level trigger. To do so it is necessary to replace the current PIN photo diodes with new avalanche photo diodes (APDs). The new read-out is able to provide a timing signal that is fast enough to use it as a trigger while it does not impair the energy resolution of the calorimeter compared to the previous system. A drawback of APDs is their temperature dependency. To provide a stable gain throughout varying running conditions it is vital to monitor the temperature change and correct it if necessary. The poster shows an approach to ensure temperature stability where the temperature is monitored via a temperature sensitive NTC thermistor and the gain is adjusted via changes of the high voltage supply of the APDs. This method proved successful while it is easy to implement in all 1320 CsI(Tl) crystals of the calorimeter.

  7. Angle- and strain-independent coloured free-standing films incorporating non-spherical colloidal photonic crystals.

    Science.gov (United States)

    Yeo, Seon Ju; Tu, Fuquan; Kim, Seung-hyun; Yi, Gi-Ra; Yoo, Pil J; Lee, Daeyeon

    2015-02-28

    Colloidal photonic crystals (CPCs) provide a convenient way to generate structural colour with high stability against degradation under environmental factors. For a number of applications including flexible electronic and energy devices, it is important to generate flexible structural colour that maintains its colour regardless of the angle of observation and the extent of mechanical deformation. However, it is challenging to simultaneously achieve these goals because anisotropy in typical CPC structures (e.g., CPC films) tends to lead to angle-dependent photonic properties and also changes in the lattice constant due to mechanical deformation lead to changes in the photonic properties of CPCs. To overcome these challenges, we present a means of fabricating large-area free-standing films of CPC structures that exhibit angle- and strain-independent photonic characteristics. First, monodisperse double emulsions encapsulating colloidal crystal arrays are prepared using a microfluidic device. By inducing crystallization of highly charged polystyrene particles in the core of double emulsions using osmotic annealing, we generate angle independent colloidal photonic crystal (CPC) supraparticles. Moreover, the shape and crystallinity of the CPC supraparticles can be tuned by changing the concentration of salt in the solution used for osmotic annealing. Subsequently, an array of CPC supraparticles is embedded inside an elastomeric matrix to form a flexible free-standing film, which exhibits structural colours that are independent of viewing angles and externally applied strain.

  8. Photonic Crystal Waveguides in Triangular Lattice of Nanopillars

    DEFF Research Database (Denmark)

    Chigrin, Dmitry N.; Lavrinenko, Andrei

    2004-01-01

    Photonic nanopillars waveguides have been analysed. Dielectric nanopillars are arranged in such way that they from a tringular lattice of 2D photonic crystal. Dispersion of the modes depends on the direction of the triangular lattice, Ã-J or Ã-X, in which nanopillars arrays are extended. Light fi....... Transmission spectra calculated by FDTD method completely reflect peculiarities of modes dispersion, showing up to 80% transmission for a realistic SOI nanopillar structure....

  9. Test of GET Electronics for the CHIMERA and FARCOS multi-detectors

    Science.gov (United States)

    De Luca, S.; Acosta, L.; Auditore, L.; Boiano, C.; Cardella, G.; Castoldi, A.; D'Andrea, M.; De Filippo, E.; Dell'Aquila, D.; Fichera, F.; Gnoffo, B.; Guazzoni, C.; Lanzalone, G.; Lombardo, I.; Martorana, N. S.; Minniti, T.; Norella, S.; Pagano, A.; Pagano, E. V.; Papa, M.; Pirrone, S.; Politi, G.; Quattrocchi, L.; Rizzo, F.; Russotto, P.; Saccà, G.; Trifirò, A.; Trimarchi, M.; Verde, G.; Vigilante, M.

    2017-11-01

    In this paper we present the results of the tests on the new digital electronics GET (General Electronics for Tpc), which will be used for the readout of the CsI(Tl) detectors of CHIMERA (Charged Heavy Ion Mass and Energy Resolving Array) and for the new correlator FARCOS (Femtoscope ARray for COrrelations and Spectroscopy). The new electronics allows us to digitize the full waveform of the signals produced by the detector. Among its features it is worth noticing the compactness and low power consumption (5W for 256 channels). Tests have been performed with pulsers, radioactive sources and ion beams. With such electronics very good results in energy resolution and isotope separation of the detected fragments were obtained, by using both hardware and software filters.

  10. Phase instability in crystals under irradiation

    International Nuclear Information System (INIS)

    Martin, G.

    1975-01-01

    A diffusion term is introduced in the standard chemical rate model of the defect population in crystals under irradiation. For point defect generation rates larger than a critical value (g*), the uniform point defect population is shown to be unstable with respect to spatial fluctuations of the point defect concentration. g* is temperature dependent. Severala effects including the nucleation of arrays of point defect clusters, or radiation induced precipitation may occur above the instability threshold. Defect-defect interaction potentials play a crucial role in the numerical value of this threshold [fr

  11. Valley Topological Phases in Bilayer Sonic Crystals

    Science.gov (United States)

    Lu, Jiuyang; Qiu, Chunyin; Deng, Weiyin; Huang, Xueqin; Li, Feng; Zhang, Fan; Chen, Shuqi; Liu, Zhengyou

    2018-03-01

    Recently, the topological physics in artificial crystals for classical waves has become an emerging research area. In this Letter, we propose a unique bilayer design of sonic crystals that are constructed by two layers of coupled hexagonal array of triangular scatterers. Assisted by the additional layer degree of freedom, a rich topological phase diagram is achieved by simply rotating scatterers in both layers. Under a unified theoretical framework, two kinds of valley-projected topological acoustic insulators are distinguished analytically, i.e., the layer-mixed and layer-polarized topological valley Hall phases, respectively. The theory is evidently confirmed by our numerical and experimental observations of the nontrivial edge states that propagate along the interfaces separating different topological phases. Various applications such as sound communications in integrated devices can be anticipated by the intriguing acoustic edge states enriched by the layer information.

  12. Nanofabrication of Arrays of Silicon Field Emitters with Vertical Silicon Nanowire Current Limiters and Self-Aligned Gates

    Science.gov (United States)

    2016-08-19

    limiters, MEMS, NEMS, field emission, cold cathodes (Some figures may appear in colour only in the online journal) 1. Introduction Dense arrays of silicon... attention has been given to densely packed, highly ordered, top-down fabricated, single crystal vertical silicon nanowire devices that are embedded

  13. Peptide modified ZnO nanoparticles as gas sensors array for volatile organic compounds (VOCs)

    Science.gov (United States)

    Mascini, Marcello; Gaggiotti, Sara; Della Pelle, Flavio; Di Natale, Corrado; Qakala, Sinazo; Iwuoha, Emmanuel; Pittia, Paola; Compagnone, Dario

    2018-04-01

    In this work a peptide based gas sensor array based of ZnO nanoparticles (ZnONPs) has been realized. Four different pentapeptides molecularly modelled for alcohols and esters having cysteine as a common spacer have been immobilized onto ZnONPs. ZnONPs have been morphologically and spectroscopically characterized. Modified nanoparticles have been then deposited onto quartz crystal microbalances (QCMs) and used as gas sensors with nitrogen as carrier gas. Analysis of the pure compounds modelled demonstrated a nice fitting of modelling with real data. The peptide based ZnONPs had very low sensitivity to water, compared to previously studied AuNPs peptide based gas sensors allowing the use of the array on samples with high water content. Real samples of fruit juices have been assayed; stability of the signal, good repeatability and discrimination ability of the array was achieved.

  14. Peptide Modified ZnO Nanoparticles as Gas Sensors Array for Volatile Organic Compounds (VOCs

    Directory of Open Access Journals (Sweden)

    Marcello Mascini

    2018-04-01

    Full Text Available In this work a peptide based gas sensor array based of ZnO nanoparticles (ZnONPs has been realized. Four different pentapeptides molecularly modeled for alcohols and esters having cysteine as a common spacer have been immobilized onto ZnONPs. ZnONPs have been morphologically and spectroscopically characterized. Modified nanoparticles have been then deposited onto quartz crystal microbalances (QCMs and used as gas sensors with nitrogen as carrier gas. Analysis of the pure compounds modeled demonstrated a nice fitting of modeling with real data. The peptide based ZnONPs had very low sensitivity to water, compared to previously studied AuNPs peptide based gas sensors allowing the use of the array on samples with high water content. Real samples of fruit juices have been assayed; stability of the signal, good repeatability, and discrimination ability of the array was achieved.

  15. Improving emission uniformity and linearizing band dispersion in nanowire arrays using quasi-aperiodicity

    Energy Technology Data Exchange (ETDEWEB)

    Anderson, P. Duke [Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States); Univ. of Southern California, Los Angeles, CA (United States). Ming Hsieh Dept. of Electrical Engineering; Koleske, Daniel D. [Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States); Povinelli, Michelle L. [Univ. of Southern California, Los Angeles, CA (United States). Ming Hsieh Dept. of Electrical Engineering; Subramania, Ganapathi [Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)

    2017-10-01

    For this study, we experimentally investigate a new class of quasi-aperiodic structures for improving the emission pattern in nanowire arrays. Efficient normal emission, as well as lasing, can be obtained from III-nitride photonic crystal (PhC) nanowire arrays that utilize slow group velocity modes near the Γ-point in reciprocal space. However, due to symmetry considerations, the emitted far-field pattern of such modes are often ‘donut’-like. Many applications, including lighting for displays or lasers, require a more uniform beam profile in the far-field. Previous work has improved far-field beam uniformity of uncoupled modes by changing the shape of the emitting structure. However, in nanowire systems, the shape of nanowires cannot always be arbitrarily changed due to growth or etch considerations. Here, we investigate breaking symmetry by instead changing the position of emitters. Using a quasi-aperiodic geometry, which changes the emitter position within a photonic crystal supercell (2x2), we are able to linearize the photonic bandstructure near the Γ-point and greatly improve emitted far-field uniformity. We realize the III-nitride nanowires structures using a top-down fabrication procedure that produces nanowires with smooth, vertical sidewalls. Comparison of room-temperature micro-photoluminescence (µ-PL) measurements between periodic and quasi-aperiodic nanowire arrays reveal resonances in each structure, with the simple periodic structure producing a donut beam in the emitted far-field and the quasi-aperiodic structure producing a uniform Gaussian-like beam. We investigate the input pump power vs. output intensity in both systems and observe the simple periodic array exhibiting a non-linear relationship, indicative of lasing. We believe that the quasi-aperiodic approach studied here provides an alternate and promising strategy for shaping the emission pattern of nanoemitter systems.

  16. An Electrochemical Quartz Crystal Microbalance Multisensor System Based on Phthalocyanine Nanostructured Films: Discrimination of Musts

    Directory of Open Access Journals (Sweden)

    Celia Garcia-Hernandez

    2015-11-01

    Full Text Available An array of electrochemical quartz crystal electrodes (EQCM modified with nanostructured films based on phthalocyanines was developed and used to discriminate musts prepared from different varieties of grapes. Nanostructured films of iron, nickel and copper phthalocyanines were deposited on Pt/quartz crystals through the Layer by Layer technique by alternating layers of the corresponding phthalocyanine and poly-allylamine hydrochloride. Simultaneous electrochemical and mass measurements were used to study the mass changes accompanying the oxidation of electroactive species present in must samples obtained from six Spanish varieties of grapes (Juan García, Prieto Picudo, Mencía Regadío, Cabernet Sauvignon, Garnacha and Tempranillo. The mass and voltammetric outputs were processed using three-way models. Parallel Factor Analysis (PARAFAC was successfully used to discriminate the must samples according to their variety. Multi-way partial least squares (N-PLS evidenced the correlations existing between the voltammetric data and the polyphenolic content measured by chemical methods. Similarly, N-PLS showed a correlation between mass outputs and parameters related to the sugar content. These results demonstrated that electronic tongues based on arrays of EQCM sensors can offer advantages over arrays of mass or voltammetric sensors used separately.

  17. Detector characterization and first coincidence tests of a Compton telescope based on LaBr3 crystals and SiPMs

    International Nuclear Information System (INIS)

    Llosá, G.; Barrio, J.; Cabello, J.; Crespo, A.; Lacasta, C.; Rafecas, M.; Callier, S.; La Taille, C. de; Raux, L.

    2012-01-01

    A Compton telescope for dose monitoring in hadron therapy consisting of several layers of continuous LaBr 3 crystals coupled to silicon photomultiplier (SiPM) arrays is under development within the ENVISION project. In order to test the possibility of employing such detectors for the telescope, a detector head consisting of a continuous 16 mm×18 mm×5 mm LaBr 3 crystal coupled to a SiPM array has been assembled and characterized, employing the SPIROC1 ASIC as readout electronics. The best energy resolution obtained at 511 keV is 6.5% FWHM and the timing resolution is 3.1 ns FWHM. A position determination method for continuous crystals is being tested, with promising results. In addition, the detector has been operated in time coincidence with a second detector layer, to determine the coincidence capabilities of the system. The first tests are satisfactory, and encourage the development of larger detectors that will compose the telescope prototype.

  18. Interspace modification of titania-nanorod arrays for efficient mesoscopic perovskite solar cells

    Science.gov (United States)

    Chen, Peng; Jin, Zhixin; Wang, Yinglin; Wang, Meiqi; Chen, Shixin; Zhang, Yang; Wang, Lingling; Zhang, Xintong; Liu, Yichun

    2017-04-01

    Morphology of electron transport layers (ETLs) has an important influence on the device architecture and electronic processes of mesostructured solar cells. In this work, we thoroughly investigated the effect of the interspace of TiO2 nanorod (NR) arrays on the photovoltaic performance of the perovskite solar cells (PSCs). Along with the interspace in TiO2-NR arrays increasing, the thickness as well as the crystal size of perovskite capping layer are reduced accordingly, and the filling of perovskite in the channel becomes incomplete. Electrochemical impedance spectroscopy measurements reveal that this variation of perovskite absorber layer, induced by interspace of TiO2 NR arrays, causes the change of charge recombination process at the TiO2/perovskite interface, suggesting that a balance between capping layer and the perovskite filling is critical to obtain high charge collection efficiency of PSCs. A power conversion efficiency of 10.3% could be achieved through careful optimization of interspace in TiO2-NR arrays. Our research will shed light on the morphology control of ETLs with 1D structure for heterojunction solar cells fabricated by solution-deposited method.

  19. Spatial Control of Photoemitted Electron Beams using a Micro-Lens-Array Transverse-Shaping Technique

    Energy Technology Data Exchange (ETDEWEB)

    Halavanau, A. [Northern Illinois U.; Qiang, G. [Tsinghua U., Beijing, Dept. Eng. Phys.; Ha, G. [POSTECH; Wisniewski, E. [Argonne (main); Piot, P. [NIU, DeKalb; Power, J. G. [Argonne (main); Gai, W. [Argonne (main)

    2017-07-24

    A common issue encountered in photoemission electron sources used in electron accelerators is the transverse inhomogeneity of the laser distribution resulting from the laser-amplification process and often use of frequency up conversion in nonlinear crystals. A inhomogeneous laser distribution on the photocathode produces charged beams with lower beam quality. In this paper, we explore the possible use of microlens arrays (fly-eye light condensers) to dramatically improve the transverse uniformity of the drive laser pulse on UV photocathodes. We also demonstrate the use of such microlens arrays to generate transversely-modulated electron beams and present a possible application to diagnose the properties of a magnetized beam.

  20. Photonic crystal borax competitive binding carbohydrate sensing motif†

    Science.gov (United States)

    Cui, Qingzhou; Muscatello, Michelle M. Ward; Asher, Sanford A.

    2009-01-01

    We developed a photonic crystal sensing method for diol containing species such as carbohydrates based on a poly(vinyl alcohol) (PVA) hydrogel containing an embedded crystalline colloidal array (CCA). The polymerized CCA (PCCA) diffracts visible light. We show that in the presence of borax the diffraction wavelength shifts as the concentration of glucose changes. The diffraction shifts result from the competitive binding of glucose to borate, which reduces the concentration of borate bound to the PVA diols. PMID:19381378

  1. Photonic crystal borax competitive binding carbohydrate sensing motif.

    Science.gov (United States)

    Cui, Qingzhou; Ward Muscatello, Michelle M; Asher, Sanford A

    2009-05-01

    We developed a photonic crystal sensing method for diol containing species such as carbohydrates based on a poly(vinyl alcohol) (PVA) hydrogel containing an embedded crystalline colloidal array (CCA). The polymerized CCA (PCCA) diffracts visible light. We show that in the presence of borax the diffraction wavelength shifts as the concentration of glucose changes. The diffraction shifts result from the competitive binding of glucose to borate, which reduces the concentration of borate bound to the PVA diols.

  2. A novel, SiPM-array-based, monolithic scintillator detector for PET

    International Nuclear Information System (INIS)

    Schaart, Dennis R; Dam, Herman T van; Seifert, Stefan; Beekman, Freek J; Vinke, Ruud; Dendooven, Peter; Loehner, Herbert

    2009-01-01

    Silicon photomultipliers (SiPMs) are of great interest to positron emission tomography (PET), as they enable new detector geometries, for e.g., depth-of-interaction (DOI) determination, are MR compatible, and offer faster response and higher gain than other solid-state photosensors such as avalanche photodiodes. Here we present a novel detector design with DOI correction, in which a position-sensitive SiPM array is used to read out a monolithic scintillator. Initial characterization of a prototype detector consisting of a 4 x 4 SiPM array coupled to either the front or back surface of a 13.2 mm x 13.2 mm x 10 mm LYSO:Ce 3+ crystal shows that front-side readout results in significantly better performance than conventional back-side readout. Spatial resolutions 2 detector, equals 960 ps FWHM.

  3. Optical simulation of quantum algorithms using programmable liquid-crystal displays

    International Nuclear Information System (INIS)

    Puentes, Graciana; La Mela, Cecilia; Ledesma, Silvia; Iemmi, Claudio; Paz, Juan Pablo; Saraceno, Marcos

    2004-01-01

    We present a scheme to perform an all optical simulation of quantum algorithms and maps. The main components are lenses to efficiently implement the Fourier transform and programmable liquid-crystal displays to introduce space dependent phase changes on a classical optical beam. We show how to simulate Deutsch-Jozsa and Grover's quantum algorithms using essentially the same optical array programmed in two different ways

  4. Precision machining and polishing of scintillating crystals for large calorimeters and hodoscopes

    International Nuclear Information System (INIS)

    Wuest, C.R.; Fuchs, B.A.; Holdener, F.R.; Heck, J.L. Jr.

    1994-04-01

    New machining and polishing techniques have been developed for large scintillating crystal arrays such as the Barium Fluoride Electromagnetic Calorimeter for the GEM Detector at SSCL, the Crystal Clear Collaboration's cerium fluoride or lead tungstenate calorimeter at the proposed LHC and CERN, the PHENIX Detector at RHIC (barium fluoride), and the cesium iodide Calorimeter for the BaBar Detector at PEP-2 B Factory at SLAC. The machining and polishing methods to be presented in this paper provide crystalline surfaces without sub-surface damage or deformation as verified by Rutherford Back-scattering (RBS) analysis. Surface roughness of about 10--20 angstroms and sub-micron mechanical tolerances have been demonstrated on large barium fluoride crystal samples. Mass production techniques have also been developed for machining the proper angled surfaces and polishing up to five 50 cm long crystals at one time. These techniques utilize kinematic mount technology developed at LLNL to allow precision machining and polishing of complex surfaces. They will present this technology along with detailed surface studies of barium fluoride and cerium fluoride crystals polished with this technique

  5. All-optical image processing with nonlinear liquid crystals

    Science.gov (United States)

    Hong, Kuan-Lun

    Liquid crystals are fascinating materials because of several advantages such as large optical birefringence, dielectric anisotropic, and easily compatible to most kinds of materials. Compared to the electro-optical properties of liquid crystals widely applied in displays and switching application, transparency through most parts of wavelengths also makes liquid crystals a better candidate for all-optical processing. The fast response time of liquid crystals resulting from multiple nonlinear effects, such as thermal and density effect can even make real-time processing realized. In addition, blue phase liquid crystals with spontaneously self-assembled three dimensional cubic structures attracted academic attention. In my dissertation, I will divide the whole contents into six parts. In Chapter 1, a brief introduction of liquid crystals is presented, including the current progress and the classification of liquid crystals. Anisotropy and laser induced director axis reorientation is presented in Chapter 2. In Chapter 3, I will solve the electrostrictive coupled equation and analyze the laser induced thermal and density effect in both static and dynamic ways. Furthermore, a dynamic simulation of laser induced density fluctuation is proposed by applying finite element method. In Chapter 4, two image processing setups are presented. One is the intensity inversion experiment in which intensity dependent phase modulation is the mechanism. The other is the wavelength conversion experiment in which I can read the invisible image with a visible probe beam. Both experiments are accompanied with simulations to realize the matching between the theories and practical experiment results. In Chapter 5, optical properties of blue phase liquid crystals will be introduced and discussed. The results of grating diffractions and thermal refractive index gradient are presented in this chapter. In addition, fiber arrays imaging and switching with BPLCs will be included in this chapter

  6. Multiplex detection of tumor markers with photonic suspension array

    Energy Technology Data Exchange (ETDEWEB)

    Zhao Yuanjin; Zhao Xiangwei [State Key Laboratory of Bioelectronics, School of Biological Science and Medical Engineering, Southeast University, Nanjing 210096 (China); Pei Xiaoping [Department of Hematology, Affiliated Zhongda Hospital, Southeast University, Nanjing 210009 (China); Hu Jing; Zhao Wenju [State Key Laboratory of Bioelectronics, School of Biological Science and Medical Engineering, Southeast University, Nanjing 210096 (China); Chen Baoan [Department of Hematology, Affiliated Zhongda Hospital, Southeast University, Nanjing 210009 (China); Gu Zhongze [State Key Laboratory of Bioelectronics, School of Biological Science and Medical Engineering, Southeast University, Nanjing 210096 (China); Laboratory of Environment and Biosafety, Research Institute of Southeast University in Suzhou, Dushu Lake Higher Education Town, Suzhou 215123 (China)], E-mail: gu@seu.edu.cn

    2009-02-02

    A novel photonic suspension array was developed for multiplex immunoassay. The carries of this array were silica colloidal crystal beads (SCCBs). The codes of these carriers are the characteristic reflection peak originated from their structural periodicity, and therefore they do not suffer from fading, bleaching, quenching, and chemical instability. In addition, because no dyes or materials related with fluorescence are included, the fluorescence background of SCCBs is very low. With a sandwich format, the proposed suspension array was used for simultaneous multiplex detection of tumor markers in one test tube. The results showed that the four tumor markers, {alpha}-fetoprotein (AFP), carcinoembryonic antigen (CEA), carcinoma antigen 125 (CA 125) and carcinoma antigen 19-9 (CA 19-9) could be assayed in the ranges of 1.0-500 ng mL{sup -1}, 1.0-500 ng mL{sup -1}, 1.0-500 U mL{sup -1} and 3.0-500 U mL{sup -1} with limits of detection of 0.68 ng mL{sup -1}, 0.95 ng mL{sup -1}, 0.99 U mL{sup -1} and 2.30 U mL{sup -1} at 3{sigma}, respectively. The proposed array showed acceptable accuracy, detection reproducibility, storage stability and the results obtained were in acceptable agreement with those from parallel single-analyte test of practical clinical sera. This technique provides a new strategy for low cost, automated, and simultaneous multiplex immunoassay.

  7. Quartz substrate infrared photonic crystal

    Science.gov (United States)

    Ghadiri, Khosrow; Rejeb, Jalel; Vitchev, Vladimir N.

    2003-01-01

    This paper presents the fabrication of a planar photonic crystal (p2c) made of a square array of dielectric rods embedded in air, operating in the infrared spectrum. A quartz substrate is employed instead of the commonly used silicon or column III-V substrate. Our square structure has a normalized cylinder radius-to-pitch ratio of r/a = 0.248 and dielectric material contrast ɛr of 4.5. We choose a Z-cut synthetic quartz for its cut (geometry), and etching properties. Then a particular Z-axis etching process is employed in order to ensure the sharp-edged verticality of the rods and fast etching speed. We also present the computer simulations that allowed the establishment of the photonic band gaps (PBG) of our photonic crystal, as well as the actual measurements. An experimental measurement have been carried out and compared with different simulations. It was found that experimental results are in good agreement with different simulation results. Finally, a frequency selective device for optical communication based on the introduction of impurity sites in the photonic crystal is presented. With our proposed structure Optical System on a Chip (OsoC) with micro-cavity based active devices such as lasers, diodes, modulators, couplers, frequency selective emitters, add-drop filters, detectors, mux/demuxes and polarizers connected by passive waveguide links can be realized.

  8. Focal plane array with modular pixel array components for scalability

    Science.gov (United States)

    Kay, Randolph R; Campbell, David V; Shinde, Subhash L; Rienstra, Jeffrey L; Serkland, Darwin K; Holmes, Michael L

    2014-12-09

    A modular, scalable focal plane array is provided as an array of integrated circuit dice, wherein each die includes a given amount of modular pixel array circuitry. The array of dice effectively multiplies the amount of modular pixel array circuitry to produce a larger pixel array without increasing die size. Desired pixel pitch across the enlarged pixel array is preserved by forming die stacks with each pixel array circuitry die stacked on a separate die that contains the corresponding signal processing circuitry. Techniques for die stack interconnections and die stack placement are implemented to ensure that the desired pixel pitch is preserved across the enlarged pixel array.

  9. Radiation damage in undoped CsI and CsI(Tl)

    International Nuclear Information System (INIS)

    Woody, C.L.; Kierstead, J.A.; Levy, P.W.; Stoll, S.

    1992-01-01

    Radiation damage has been studied in undoped CsI and CsI(TI) crystals using 60 Co gamma radiation for doses up to ∼ 4.2 x 10 6 . Samples from various manufacturers were measured ranging in size from 2.54 cm long cylinders to a 30 cm long block. Measurements were made on the change in optical transmission and scintillation light output as a function of dose. Although some samples showed a small change in transmission, a significant change in light output was observed for all samples. Recovery from damage was also studied as a function of time and exposure to UV light. A short lived phosphorescence was observed in undoped CsI, similar to the phosphorescence seen in CsI(TI)

  10. Interspace modification of titania-nanorod arrays for efficient mesoscopic perovskite solar cells

    International Nuclear Information System (INIS)

    Chen, Peng; Jin, Zhixin; Wang, Yinglin; Wang, Meiqi; Chen, Shixin; Zhang, Yang; Wang, Lingling; Zhang, Xintong; Liu, Yichun

    2017-01-01

    Highlights: • The fabrication of perovskite solar cells utilizing TiO_2 NR arrays. • Investigation of the interspace effect of TiO_2 NR on perovskite layer. • Understanding of the balance between perovskite capping layer and pore filling. - Abstract: Morphology of electron transport layers (ETLs) has an important influence on the device architecture and electronic processes of mesostructured solar cells. In this work, we thoroughly investigated the effect of the interspace of TiO_2 nanorod (NR) arrays on the photovoltaic performance of the perovskite solar cells (PSCs). Along with the interspace in TiO_2-NR arrays increasing, the thickness as well as the crystal size of perovskite capping layer are reduced accordingly, and the filling of perovskite in the channel becomes incomplete. Electrochemical impedance spectroscopy measurements reveal that this variation of perovskite absorber layer, induced by interspace of TiO_2 NR arrays, causes the change of charge recombination process at the TiO_2/perovskite interface, suggesting that a balance between capping layer and the perovskite filling is critical to obtain high charge collection efficiency of PSCs. A power conversion efficiency of 10.3% could be achieved through careful optimization of interspace in TiO_2-NR arrays. Our research will shed light on the morphology control of ETLs with 1D structure for heterojunction solar cells fabricated by solution-deposited method.

  11. Acoustic pressure in cavity of variously sized two-dimensional sonic crystals with various filling fractions

    International Nuclear Information System (INIS)

    Wu Liangyu; Chen Lienwen; Liu Chiaming

    2009-01-01

    This study theoretically and experimentally investigates the acoustic pressure in the cavity of a 2D sonic crystal. Such crystals are composed of polymethyl methacrylate cylinders with a square array embedded in air background. The plane wave expansion method and the supercell calculation are employed to calculate the band structure and obtain the defect band. The finite element method is adopted to simulate the pressure field in the sonic crystal and calculate the pressure in the middle of the cavity as a function of frequency. The effects of sizes and filling fractions are investigated, and the quality factor of the cavity is discussed. The measured spectra and pressures in the defect of the sonic crystal demonstrate that the acoustic waves can be localized in the defect at the resonant frequency

  12. CsI calorimeter with 3-D position resolution

    International Nuclear Information System (INIS)

    Schopper, F.; Andritschke, R.; Shaw, H.; Nefzger, C.; Zoglauer, A.; Schoenfelder, V.; Kanbach, G.

    2000-01-01

    New γ-ray calorimeter have been developed for the MEGA Compton camera. They consist of arrays of small CsI(Tl) scintillator bars read out by Silicon PIN-diodes and low noise, self-triggering frontend electronics. The length of the bars (the thickness of the calorimeter) can be varied for different applications to fit the stopping power needed and the light loss tolerable. In this paper we present calibration results from 2 cm long bars with diodes on one side, and 8 cm long bars with diodes on two opposite sides. Double-sided readout gives 3-D information of interactions which will be used to overcome the limited position resolution in Anger-cameras at high energies. Simpler detection devices like Anger-cameras might finally resolve only the centre of gravity. As events from γ-rays with energies of MeV do extend over several cm, it is a prerequisite for an imaging device to resolve the interaction structure in detail. Combining CsI(Tl) scintillators, Silicon PIN-photodiodes and frontend electronics inside the housing results in a cheap rugged design. While the development in our institute is mainly done for the Compton camera prototype, many other applications are conceivable

  13. Effects of electric fields on the photonic crystal formation from block copolymers

    Science.gov (United States)

    Lee, Taekun; Ju, Jin-wook; Ryoo, Won

    2012-03-01

    Effects of electric fields on the self-assembly of block copolymers have been investigated for thin films of polystyrene-bpoly( 2-vinyl pyridine); PS-b-P2VP, 52 kg/mol-b-57 kg/mol and 133 kg/mol-b-132 kg/mol. Block copolymers of polystyrene and poly(2-vinyl pyridine) have been demonstrated to form photonic crystals of 1D lamellar structure with optical band gaps that correspond to UV-to-visible light. The formation of lamellar structure toward minimum freeenergy state needs increasing polymer chain mobility, and the self-assembly process is accelerated usually by annealing, that is exposing the thin film to solvent vapor such as chloroform and dichloromethane. In this study, thin films of block copolymers were spin-coated on substrates and placed between electrode arrays of various patterns including pin-points, crossing and parallel lines. As direct or alternating currents were applied to electrode arrays during annealing process, the final structure of thin films was altered from the typical 1D lamellae in the absence of electric fields. The formation of lamellar structure was spatially controlled depending on the shape of electrode arrays, and the photonic band gap also could be modulated by electric field strength. The spatial formation of lamellar structure was examined with simulated distribution of electrical potentials by finite difference method (FDM). P2VP layers in self-assembled film were quaternized with methyl iodide vapor, and the remaining lamellar structure was investigated by field emission scanning electron microscope (FESEM). The result of this work is expected to provide ways of fabricating functional structures for display devices utilizing photonic crystal array.

  14. Timed arrays wideband and time varying antenna arrays

    CERN Document Server

    Haupt, Randy L

    2015-01-01

    Introduces timed arrays and design approaches to meet the new high performance standards The author concentrates on any aspect of an antenna array that must be viewed from a time perspective. The first chapters briefly introduce antenna arrays and explain the difference between phased and timed arrays. Since timed arrays are designed for realistic time-varying signals and scenarios, the book also reviews wideband signals, baseband and passband RF signals, polarization and signal bandwidth. Other topics covered include time domain, mutual coupling, wideband elements, and dispersion. The auth

  15. A pilot experiment with reactor neutrinos in Taiwan

    International Nuclear Information System (INIS)

    Wong, Henry T.; Li Jin

    1999-01-01

    A Collaboration comprising scientists from Taiwan, mainland China and the United States has been built up since 1996 to pursue an experimental program in neutrino and astro-particle physics in Taiwan. A pilot experiment to be performed at the Nuclear Power Station II in Taiwan is now under intense preparation. It will make use of a 500 kg CsI(Tl) crystal calorimeter to study various neutrino interactions. Various possible future directions will also be explored. The conceptual design and the physics to be addressed by the pilot experiment are discussed

  16. Plasmonic Photovoltaic Cells with Dual-Functional Gold, Silver, and Copper Half-Shell Arrays.

    Science.gov (United States)

    Wu, Ling; Kim, Gyu Min; Nishi, Hiroyasu; Tatsuma, Tetsu

    2017-09-12

    Solid-state photovoltaic cells based on plasmon-induced charge separation (PICS) have attracted growing attention during the past decade. However, the power conversion efficiency (PCE) of the previously reported devices, which are generally loaded with dispersed metal nanoparticles as light absorbers, has not been sufficiently high. Here we report simpler plasmonic photovoltaic cells with interconnected Au, Ag, and Cu half-shell arrays deposited on SiO 2 @TiO 2 colloidal crystals, which serve both as a plasmonic light absorber and as a current collector. The well-controlled and easily prepared plasmonic structure allows precise comparison of the PICS efficiency between different plasmonic metal species. The cell with the Ag half-shell array has higher photovoltaic performance than the cells with Au and Cu half-shell arrays because of the high population of photogenerated energetic electrons, which gives a high electron injection efficiency and suppressed charge recombination probability, achieving the highest PCE among the solid-state PICS devices even without a hole transport layer.

  17. A high resolution germanium detector array for hypernuclear studies at PANDA

    Energy Technology Data Exchange (ETDEWEB)

    Bleser, Sebastian; Sanchez Lorente, Alicia; Steinen, Marcell [Helmholtz-Institut Mainz (Germany); Gerl, Juergen; Kojouharov, Ivan [GSI, Darmstadt (Germany); Iazzi, Felice [Politecnico, Torino, Turin (Italy); INFN, Torino, Turin (Italy); Pochodzalla, Josef; Rittgen, Kai; Sahin, Cihan [Institute for Nuclear Physics, JGU Mainz (Germany); Collaboration: PANDA-Collaboration

    2013-07-01

    The PANDA experiment, planned at the FAIR facility in Darmstadt, aims at the high resolution γ-spectroscopy of double Λ hypernuclei. For this purpose a devoted detector setup is required, consisting of a primary nuclear target, an active secondary target and a germanium detector array for the γ-spectroscopy. Due to the limited space within the PANDA detector a compact design is required. In particular the conventional LN{sub 2} cooling system must be replaced by an electro-mechanical device and a new arrangement of the crystals is needed. This poster shows the ongoing development of the germanium detectors. Test measurements of a single crystal prototype with an improved cooling concept are shown. Thermal simulations for a triple crystal detector are presented. Aditionally studies of the optimization of the detector arrangement inside the PANDA barrel spectrometer are shown. Finally the status on digital pulse shape analysis is presented which will be necessary to deal with high counting rates and to recover the high original energy resolution in case of neutron damage.

  18. Self-Organization of +-Crown Ether Derivatives into Double-Columnar Arrays Controlled by Supramolecular Isomers of Hydrogen-Bonded Anionic Biimidazolate Ni Complexes

    Directory of Open Access Journals (Sweden)

    Makoto Tadokoro

    2012-01-01

    Full Text Available Anionic tris (biimidazolate nickelate (II ([Ni(Hbim3]−, which is a hydrogen-bonding (H-bonding molecular building block, undergoes self-organization into honeycomb-sheet superstructures connected by complementary intermolecular H-bonds. The crystal obtained from the stacking of these sheets is assembled into channel frameworks, approximately 2 nm wide, that clathrate two cationic K+-crown ether derivatives organised into one-dimensional (1D double-columnar arrays. In this study, we have shown that all five cationic guest-included crystals form nanochannel structures that clathrate the 1-D double-columnar arrays of one of the four types of K+-crown ether derivatives, one of which induces a polymorph. This is accomplished by adaptably fitting two types of anionic [Ni(Hbim3]− host arrays. One is a ΔΛ−ΔΛ−ΔΛ⋯ network with H-bonded linkages alternating between the two different optical isomers of the Δ and Λ types with flexible H-bonded [Ni(Hbim3]−. The other is a ΔΔΔ−ΛΛΛ⋯ network of a racemate with 1-D H-bonded arrays of the same optical isomer for each type. Thus, [Ni(Hbim3]− can assemble large cations such as K+ crown-ether derivatives into double-columnar arrays by highly recognizing flexible H-bonding arrangements with two host networks of ΔΛ−ΔΛ−ΔΛ⋯ and ΔΔΔ−ΛΛΛ⋯.

  19. ArrayBridge: Interweaving declarative array processing with high-performance computing

    Energy Technology Data Exchange (ETDEWEB)

    Xing, Haoyuan [The Ohio State Univ., Columbus, OH (United States); Floratos, Sofoklis [The Ohio State Univ., Columbus, OH (United States); Blanas, Spyros [The Ohio State Univ., Columbus, OH (United States); Byna, Suren [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Prabhat, Prabhat [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Wu, Kesheng [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Brown, Paul [Paradigm4, Inc., Waltham, MA (United States)

    2017-05-04

    Scientists are increasingly turning to datacenter-scale computers to produce and analyze massive arrays. Despite decades of database research that extols the virtues of declarative query processing, scientists still write, debug and parallelize imperative HPC kernels even for the most mundane queries. This impedance mismatch has been partly attributed to the cumbersome data loading process; in response, the database community has proposed in situ mechanisms to access data in scientific file formats. Scientists, however, desire more than a passive access method that reads arrays from files. This paper describes ArrayBridge, a bi-directional array view mechanism for scientific file formats, that aims to make declarative array manipulations interoperable with imperative file-centric analyses. Our prototype implementation of ArrayBridge uses HDF5 as the underlying array storage library and seamlessly integrates into the SciDB open-source array database system. In addition to fast querying over external array objects, ArrayBridge produces arrays in the HDF5 file format just as easily as it can read from it. ArrayBridge also supports time travel queries from imperative kernels through the unmodified HDF5 API, and automatically deduplicates between array versions for space efficiency. Our extensive performance evaluation in NERSC, a large-scale scientific computing facility, shows that ArrayBridge exhibits statistically indistinguishable performance and I/O scalability to the native SciDB storage engine.

  20. Topological features of engineered arrays of adsorbates in honeycomb lattices

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez-Arraga, Luis A., E-mail: ludovici83@gmail.com [IMDEA Nanociencia, Calle de Faraday, 9, Cantoblanco, 28049 Madrid (Spain); Lado, J.L. [International Iberian Nanotechnology Laboratory (INL), Av. Mestre Jose Veiga, 4715-330 Braga (Portugal); Guinea, Francisco [IMDEA Nanociencia, Calle de Faraday, 9, Cantoblanco, 28049 Madrid (Spain); School of Physics and Astronomy, University of Manchester, Oxford Road, Manchester M13 9PL (United Kingdom)

    2016-09-01

    Hydrogen adatoms are one of the most the promising proposals for the functionalization of graphene. The adatoms induce narrow resonances near the Dirac energy, which lead to the formation of magnetic moments. Furthermore, they also create local lattice distortions which enhance the spin–orbit coupling. The combination of magnetism and spin–orbit coupling allows for a rich variety of phases, some of which have non-trivial topological features. We analyze the interplay between magnetism and spin–orbit coupling in ordered arrays of adsorbates on honeycomb lattice monolayers, and classify the different phases that may arise. We extend our model to consider arrays of adsorbates in graphene-like crystals with stronger intrinsic spin–orbit couplings. We also consider a regime away from half-filling in which the Fermi level is at the bottom of the conduction band, we find a Berry curvature distribution corresponding to a Valley–Hall effect.

  1. High-throughput controllable generation of droplet arrays with low consumption

    Science.gov (United States)

    Lin, Yinyin; Wu, Zhongsheng; Gao, Yibo; Wu, Jinbo; Wen, Weijia

    2018-06-01

    We describe a controllable sliding method for fabricating millions of isolated femto- to nanoliter-sized droplets with defined volume, geometry and position and a speed of up to 375 kHz. In this work, without using a superhydrophobic or superoleophobic surface, arrays of droplets are instantly formed on the patterned substrate by sliding a strip of liquid, including water, low-surface-tension organic solvents and solution, along the substrate. To precisely control the volume of the droplets, we systemically investigate the effects of the size of the wettable pattern, the viscosity of the liquid and sliding speed, which were found to vary independently to tune the height and volume of the droplets. Through this method, we successfully fabricated an oriented single metal-organic framework crystal array with control over their XY positioning on the surface, as characterized by microscopy and X-ray diffraction (XRD) techniques.

  2. Simple, Fast, and Cost-Effective Fabrication of Wafer-Scale Nanohole Arrays on Silicon for Antireflection

    Directory of Open Access Journals (Sweden)

    Di Di

    2014-01-01

    Full Text Available A simple, fast, and cost-effective method was developed in this paper for the high-throughput fabrication of nanohole arrays on silicon (Si, which is utilized for antireflection. Wafer-scale polystyrene (PS monolayer colloidal crystal was developed as templates by spin-coating method. Metallic shadow mask was prepared by lifting off the oxygen etched PS beads from the deposited chromium film. Nanohole arrays were fabricated by Si dry etching. A series of nanohole arrays were fabricated with the similar diameter but with different depth. It is found that the maximum depth of the Si-hole was determined by the diameter of the Cr-mask. The antireflection ability of these Si-hole arrays was investigated. The results show that the reflection decreases with the depth of the Si-hole. The deepest Si-hole arrays show the best antireflection ability (reflection 600 nm, which was about 28 percent of the nonpatterned silicon wafer’s reflection. The proposed method has the potential for high-throughput fabrication of patterned Si wafer, and the low reflectivity allows the application of these wafers in crystalline silicon solar cells.

  3. Performance of a high-resolution depth-encoding PET detector module using linearly-graded SiPM arrays

    Science.gov (United States)

    Du, Junwei; Bai, Xiaowei; Gola, Alberto; Acerbi, Fabio; Ferri, Alessandro; Piemonte, Claudio; Yang, Yongfeng; Cherry, Simon R.

    2018-02-01

    The goal of this study was to exploit the excellent spatial resolution characteristics of a position-sensitive silicon photomultiplier (SiPM) and develop a high-resolution depth-of-interaction (DOI) encoding positron emission tomography (PET) detector module. The detector consists of a 30  ×  30 array of 0.445  ×  0.445  ×  20 mm3 polished LYSO crystals coupled to two 15.5  ×  15.5 mm2 linearly-graded SiPM (LG-SiPM) arrays at both ends. The flood histograms show that all the crystals in the LYSO array can be resolved. The energy resolution, the coincidence timing resolution and the DOI resolution were 21.8  ±  5.8%, 1.23  ±  0.10 ns and 3.8  ±  1.2 mm, respectively, at a temperature of -10 °C and a bias voltage of 35.0 V. The performance did not degrade significantly for event rates of up to 130 000 counts s-1. This detector represents an attractive option for small-bore PET scanner designs that simultaneously emphasize high spatial resolution and high detection efficiency, important, for example, in preclinical imaging of the rodent brain with neuroreceptor ligands.

  4. Dual-array valence emission spectrometer (DAVES): A new approach for hard x-ray photon-in photon-out spectroscopies

    Energy Technology Data Exchange (ETDEWEB)

    Finkelstein, K. D., E-mail: kdf1@cornell.edu; Lyndaker, A.; Krawcyk, T.; Conrad, J. [CHESS Wilson Lab, Cornell University, Ithaca, NY 14853 (United States); Pollock, C. J. [Dept. of Chemistry, The Pennsylvania State University, University Park, Pennsylvania 16802 (United States)

    2016-07-27

    CHESS has developed and successfully deployed a novel Dual Array Valence Emission Spectrometer (DAVES) for high energy resolution, hard x-ray spectroscopy. DAVES employs the simplest method for scanning multiple spherical crystals along a Rowland Circle. The new design achieves unique 2-color collection capability and is built to take special advantage of pixel array detectors. Our initial results show why these detectors greatly improve data quality. The presentation emphasizes flexibility of experimental design offered by DAVES. Prospects and benefits of 2-color spectroscopy are illustrated and discussed.

  5. Shape evolution in the superdeformed A≅80-90 mass region

    International Nuclear Information System (INIS)

    Lagergren, K.; Cederwall, B.; Issa, T.; Johnson, A.; Milechina, L.; Wyss, R.; Clark, R.M.; Fallon, P.; Goergen, A.; Macchiavelli, A.O.; Janssens, R.V.F.; Sarantites, D.G.

    2003-01-01

    Superdeformed bands in 88 Mo, 89 Tc, and 91 Tc were populated using a 40 Ca beam with an energy of 185 MeV, impinging on a backed 58 Ni target. γ rays and charged particles emitted in the reactions were detected using the Gammasphere Ge detector array and the CsI(Tl) array Microball. Average transition quadrupole moments Q t , with significantly improved accuracy compared to earlier work, were deduced for the bands using the residual doppler shift technique. The experimental results were included into a systematic study of the Q t values throughout the superdeformed mass 80-90 region. The superdeformed shell gaps are predicted to move towards larger deformations with increasing Z and N in this mass region. This trend is confirmed by the experimental Q t values

  6. Detector block based on arrays of 144 SiPMs and monolithic scintillators: A performance study

    International Nuclear Information System (INIS)

    González, A.J.; Conde, P.; Iborra, A.; Aguilar, A.; Bellido, P.; García-Olcina, R.; Hernández, L.; Moliner, L.; Rigla, J.P.; Rodríguez-Álvarez, M.J.; Sánchez, F.; Seimetz, M.; Soriano, A.; Torres, J.; Vidal, L.F.; Benlloch, J.M.

    2015-01-01

    We have developed a detector block composed by a monolithic LYSO scintillator coupled to a custom made 12×12 SiPMs array. The design is mainly focused to applications such as Positron Emission Tomography. The readout electronics is based on 3 identical and scalable Application Specific Integrated Circuits (ASIC). We have determined the main performance of the detector block namely spatial, energy, and time resolution but also the system capability to determine the photon depth of interaction, for different crystal surface treatments. Intrinsic detector spatial resolution values as good as 1.7 mm FWHM and energies of 15% for black painted crystals were measured

  7. Disentangling nonradiative recombination processes in Ge micro-crystals on Si substrates

    Energy Technology Data Exchange (ETDEWEB)

    Pezzoli, Fabio, E-mail: fabio.pezzoli@unimib.it; Giorgioni, Anna; Gatti, Eleonora; Grilli, Emanuele; Bonera, Emiliano; Miglio, Leo [LNESS and Dipartimento di Scienza dei Materiali, Università degli Studi di Milano-Bicocca, via Cozzi 55, I-20125 Milano (Italy); Gallacher, Kevin; Millar, Ross W.; Paul, Douglas J. [School of Engineering, University of Glasgow, Rankine Building, Oakfield Avenue, Glasgow G12 8LT (United Kingdom); Isa, Fabio [LNESS, Dipartimento di Fisica del Politecnico di Milano and IFN-CNR, Polo Territoriale di Como, Via Anzani 42, I-22100 Como (Italy); Laboratory for Solid State Physics, ETH Zurich, Otto-Stern-Weg 1, CH-8093 Zürich (Switzerland); Biagioni, Paolo [LNESS, Dipartimento di Fisica del Politecnico di Milano and IFN-CNR, Piazza Leonardo da Vinci 32, I-20133 Milano (Italy); Isella, Giovanni [LNESS, Dipartimento di Fisica del Politecnico di Milano and IFN-CNR, Polo Territoriale di Como, Via Anzani 42, I-22100 Como (Italy)

    2016-06-27

    We address nonradiative recombination pathways by leveraging surface passivation and dislocation management in μm-scale arrays of Ge crystals grown on deeply patterned Si substrates. The time decay photoluminescence (PL) at cryogenic temperatures discloses carrier lifetimes approaching 45 ns in band-gap engineered Ge micro-crystals. This investigation provides compelling information about the competitive interplay between the radiative band-edge transitions and the trapping of carriers by dislocations and free surfaces. Furthermore, an in-depth analysis of the temperature dependence of the PL, combined with capacitance data and finite difference time domain modeling, demonstrates the effectiveness of GeO{sub 2} in passivating the surface of Ge and thus in enhancing the room temperature PL emission.

  8. Disentangling nonradiative recombination processes in Ge micro-crystals on Si substrates

    International Nuclear Information System (INIS)

    Pezzoli, Fabio; Giorgioni, Anna; Gatti, Eleonora; Grilli, Emanuele; Bonera, Emiliano; Miglio, Leo; Gallacher, Kevin; Millar, Ross W.; Paul, Douglas J.; Isa, Fabio; Biagioni, Paolo; Isella, Giovanni

    2016-01-01

    We address nonradiative recombination pathways by leveraging surface passivation and dislocation management in μm-scale arrays of Ge crystals grown on deeply patterned Si substrates. The time decay photoluminescence (PL) at cryogenic temperatures discloses carrier lifetimes approaching 45 ns in band-gap engineered Ge micro-crystals. This investigation provides compelling information about the competitive interplay between the radiative band-edge transitions and the trapping of carriers by dislocations and free surfaces. Furthermore, an in-depth analysis of the temperature dependence of the PL, combined with capacitance data and finite difference time domain modeling, demonstrates the effectiveness of GeO_2 in passivating the surface of Ge and thus in enhancing the room temperature PL emission.

  9. Disentangling nonradiative recombination processes in Ge micro-crystals on Si substrates

    Science.gov (United States)

    Pezzoli, Fabio; Giorgioni, Anna; Gallacher, Kevin; Isa, Fabio; Biagioni, Paolo; Millar, Ross W.; Gatti, Eleonora; Grilli, Emanuele; Bonera, Emiliano; Isella, Giovanni; Paul, Douglas J.; Miglio, Leo

    2016-06-01

    We address nonradiative recombination pathways by leveraging surface passivation and dislocation management in μm-scale arrays of Ge crystals grown on deeply patterned Si substrates. The time decay photoluminescence (PL) at cryogenic temperatures discloses carrier lifetimes approaching 45 ns in band-gap engineered Ge micro-crystals. This investigation provides compelling information about the competitive interplay between the radiative band-edge transitions and the trapping of carriers by dislocations and free surfaces. Furthermore, an in-depth analysis of the temperature dependence of the PL, combined with capacitance data and finite difference time domain modeling, demonstrates the effectiveness of GeO2 in passivating the surface of Ge and thus in enhancing the room temperature PL emission.

  10. A Portable Diode Array Spectrophotometer.

    Science.gov (United States)

    Stephenson, David

    2016-05-01

    A cheap portable visible light spectrometer is presented. The spectrometer uses readily sourced items and could be constructed by anyone with a knowledge of electronics. The spectrometer covers the wavelength range 450-725 nm with a resolution better than 5 nm. The spectrometer uses a diffraction grating to separate wavelengths, which are detected using a 128-element diode array, the output of which is analyzed using a microprocessor. The spectrum is displayed on a small liquid crystal display screen and can be saved to a micro SD card for later analysis. Battery life (2 × AAA) is estimated to be 200 hours. The overall dimensions of the unit are 120 × 65 × 60 mm, and it weighs about 200 g. © The Author(s) 2016.

  11. Dual curved photonic crystal ring resonator based channel drop filter using two-dimensional photonic crystal structure

    Energy Technology Data Exchange (ETDEWEB)

    Chhipa, Mayur Kumar, E-mail: mayurchhipa1@gmail.com [Deptt. of Electronics and Communication Engineering, Government Engineering College Ajmer Rajasthan INDIA (India); Dusad, Lalit Kumar [Rajasthan Technical University Kota, Rajasthan (India)

    2016-05-06

    In this paper channel drop filter (CDF) is designed using dual curved photonic crystal ring resonator (PCRR). The photonic band gap (PBG) is calculated by plane wave expansion (PWE) method and the photonic crystal (PhC) based on two dimensional (2D) square lattice periodic arrays of silicon (Si) rods in air structure have been investigated using finite difference time domain (FDTD) method. The number of rods in Z and X directions is 21 and 20 respectively with lattice constant 0.540 nm and rod radius r = 0.1 µm. The channel drop filter has been optimized for telecommunication wavelengths λ = 1.591 µm with refractive indices 3.533. In the designed structure further analysis is also done by changing whole rods refractive index and it has been observed that this filter may be used for filtering several other channels also. The designed structure is useful for CWDM systems. This device may serve as a key component in photonic integrated circuits. The device is ultra compact with the overall size around 123 µm{sup 2}.

  12. Spin-wave dispersion of nanostructured magnonic crystals with periodic defects

    Directory of Open Access Journals (Sweden)

    V. L. Zhang

    2016-11-01

    Full Text Available The spin-wave dispersions in nanostructured magnonic crystals with periodic defects have been mapped by Brillouin light scattering. The otherwise perfect crystals are one-dimensional arrays of alternating 460nm-wide Ni80Fe20 stripes and 40nm-wide air gaps, where one in ten Ni80Fe20 stripes is a defect of width other than 460 nm. Experimentally, the defects are manifested as additional Brillouin peaks, lying within the first and second bandgaps of the perfect crystal, whose frequencies decrease with increasing defect stripe width. Finite-element calculations, based on a supercell comprising one defect and nine perfect Py stripes, show that the defect modes are localized about the defects, with the localization exhibiting an approximate U-shaped dependence on defect size. Calculations also reveal extra magnon branches and the opening of mini-bandgaps, within the allowed bands of the perfect crystal, arising from Bragg reflections at the boundaries of the shorter supercell Brillouin zone. Simulated magnetization profiles of the band-edge modes of the major and mini-bandgaps reveal their different symmetries and localization properties. The findings could find application in microwave magnonic devices like single-frequency passband spin-wave filters.

  13. Dual parameter analysis of CsI:Tl/PMT with a digital oscilloscope

    CERN Document Server

    Devol, T A; Fjeld, R A

    1999-01-01

    Scintillation pulses from alpha-particle and gamma-ray excited CsI:Tl were recorded with a photomultiplier tube and digital oscilloscope card in single parameter (pulse shape or pulse height) and dual parameter (simultaneous pulse shape and pulse height) modes. A 2.8x1.3x1.3 cm sup 3 CsI:Tl crystal was coupled to a Burle 8850 photomultiplier tube (PMT) and excited with sup 1 sup 4 sup 8 Gd (E subalpha=3.18 MeV) and sup 1 sup 3 sup 7 Cs (E subgamma=0.662 MeV). The timing pulses (50 OMEGA terminated dynode signal) from the PMT base were directly input to a GaGe CompuScope 8012A/PCI sup T sup M (12-bit, 50 MHz dual channel digital oscilloscope card) that resided in a P6-300 MHz personal computer. Individual digitized pulses were processed via a LabVIEW sup T sup M V 4.1 interface to the oscilloscope. The ratio of the charge collected over a short time interval to the total charge collected was used for the single parameter pulse shape spectrum while the total charge collected was used for the single parameter pu...

  14. Two inorganic-organic hybrid materials based on polyoxometalate anions and methylene blue: Preparations, crystal structures and properties

    International Nuclear Information System (INIS)

    Nie Shanshan; Zhang Yaobin; Liu Bin; Li Zuoxi; Hu Huaiming; Xue Ganglin; Fu Feng; Wang Jiwu

    2010-01-01

    Two novel inorganic-organic hybrid materials based on an organic dye cation methylene blue (MB) and Lindqvist-type POM polyanions, [C 22 H 18 N 3 S] 2 Mo 6 O 19 2DMF (1) and [C 22 H 18 N 3 S] 2 W 6 O 19 2DMF (2) were synthesized under ambient conditions and characterized by CV, IR spectroscopy, solid diffuse reflectance spectrum, UV-vis spectra in DMF solution, luminescent spectrum and single crystal X-ray diffraction. Crystallographic data reveal that compounds 1 and 2 are isostructural and both crystallize in the triclinic space group P1-bar . Their crystal structures present that the layers of organic molecules and inorganic anions array alternatively, and there exist strong π...π stacking interactions between dimeric MB cations and near distance interactions among organic dye cations, Lindqvist-type POM polyanions and DMF molecules. The solid diffuse reflectance spectra and UV-vis spectra in DMF solution appear new absorption bands ascribed to the charge-transfer transition between the cationic MB donor and the POM acceptors. Studies of the photoluminescent properties show that the formation of 1 and 2 lead to the fluorescence quenching of starting materials. -- Graphical abstract: Their crystal structures present that the layers of organic molecules and inorganic anions array alternatively, and there exist strong π...π stacking interactions between dimeric MB cations. Display Omitted

  15. Enhancement of the fluorescence intensity of DNA intercalators using nano-imprinted 2-dimensional photonic crystal

    International Nuclear Information System (INIS)

    Endo, Tatsuro; Ueda, China; Hisamoto, Hideaki; Kajita, Hiroshi; Okuda, Norimichi; Tanaka, Satoru

    2013-01-01

    We have fabricated polymer-based 2-dimensional photonic crystals that play a key role in enhancing the fluorescence of DNA intercalators. Highly ordered 2-dimensional photonic crystals possessing triangle-shaped and nm-sized hole arrays were fabricated on a 100 μm thick polymer film using nano-imprint lithography. Samples of double-stranded DNAs (sizes: 4361 and 48502 bp; concentration: 1 pM to 10 nM) were adsorbed on the surface of the 2-dimensional photonic crystal by electrostatic interactions and then treated with intercalators. It is found that the fluorescence intensity of the intercalator is enhanced by a factor of up to 10 compared to the enhancement in the absence of the 2-dimensional photonic crystal. Fluorescence intensity increases with increasing length and concentration of the DNAs. If the 2-dimensional photonic crystal is used as a Bragg reflection mirror, the enhancement of fluorescence intensity can be easily observed using a conventional spectrofluorometer. These results suggest that the printed photonic crystal offers a great potential for highly sensitive intercalator-based fluorescent detection of DNAs. (author)

  16. Enhanced density of optical data storage using near-field concept: fabrication and test of nanometric aperture array

    International Nuclear Information System (INIS)

    Cha, J.; Park, J. H.; Kim, Myong R.; Jhe, W.

    1999-01-01

    We have tried to enhance the density of the near-field optical memory and to improve the recording/readout speed. The current optical memory has the limitation in both density and speed. This barrier due to the far-field nature can be overcome by the use of near-field. The optical data storage density can be increased by reducing the size of the nanometric aperture where the near-field is obtained. To fabricate the aperture in precise dimension, we applied the orientation-dependent / anisotropic etching property of crystal Si often employed in the field of MEMS. And so we fabricated the 10 x 10 aperture array. This array will be also the indispensable part for speeding up. One will see the possibility of the multi-tracking pickup in the phase changing type memory through this array. This aperture array will be expected to write the bit-mark whose size is about 100 nm. We will show the recent result obtained. (author)

  17. Modelling of the thermal parameters of high-power linear laser-diode arrays. Two-dimensional transient model

    International Nuclear Information System (INIS)

    Bezotosnyi, V V; Kumykov, Kh Kh

    1998-01-01

    A two-dimensional transient thermal model of an injection laser is developed. This model makes it possible to analyse the temperature profiles in pulsed and cw stripe lasers with an arbitrary width of the stripe contact, and also in linear laser-diode arrays. This can be done for any durations and repetition rates of the pump pulses. The model can also be applied to two-dimensional laser-diode arrays operating quasicontinuously. An analysis is reported of the influence of various structural parameters of a diode array on the thermal regime of a single laser. The temperature distributions along the cavity axis are investigated for different variants of mounting a crystal on a heat sink. It is found that the temperature drop along the cavity length in cw and quasi-cw laser diodes may exceed 20%. (lasers)

  18. Ultrasound Flow Mapping for the Investigation of Crystal Growth.

    Science.gov (United States)

    Thieme, Norman; Bonisch, Paul; Meier, Dagmar; Nauber, Richard; Buttner, Lars; Dadzis, Kaspars; Patzold, Olf; Sylla, Lamine; Czarske, Jurgen

    2017-04-01

    A high energy conversion and cost efficiency are keys for the transition to renewable energy sources, e.g., solar cells. The efficiency of multicrystalline solar cells can be improved by enhancing the understanding of its crystallization process, especially the directional solidification. In this paper, a novel measurement system for the characterization of flow phenomena and solidification processes in low-temperature model experiments on the basis of ultrasound (US) Doppler velocimetry is described. It captures turbulent flow phenomena in two planes with a frame rate of 3.5 Hz and tracks the shape of the solid-liquid interface during multihour experiments. Time-resolved flow mapping is performed using four linear US arrays with a total of 168 transducer elements. Long duration measurements are enabled through an online, field-programmable gate array (FPGA)-based signal processing. Nine single US transducers allow for in situ tracking of a solid-liquid interface. Results of flow and solidification experiments in the model experiment are presented and compared with numerical simulation. The potential of the developed US system for measuring turbulent flows and for tracking the solidification front during a directional crystallization process is demonstrated. The results of the model experiments are in good agreement with numerical calculations and can be used for the validation of numerical models, especially the selection of the turbulence model.

  19. Cells containing aragonite crystals mediate responses to gravity in Trichoplax adhaerens (Placozoa), an animal lacking neurons and synapses.

    Science.gov (United States)

    Mayorova, Tatiana D; Smith, Carolyn L; Hammar, Katherine; Winters, Christine A; Pivovarova, Natalia B; Aronova, Maria A; Leapman, Richard D; Reese, Thomas S

    2018-01-01

    Trichoplax adhaerens has only six cell types. The function as well as the structure of crystal cells, the least numerous cell type, presented an enigma. Crystal cells are arrayed around the perimeter of the animal and each contains a birefringent crystal. Crystal cells resemble lithocytes in other animals so we looked for evidence they are gravity sensors. Confocal microscopy showed that their cup-shaped nuclei are oriented toward the edge of the animal, and that the crystal shifts downward under the influence of gravity. Some animals spontaneously lack crystal cells and these animals behaved differently upon being tilted vertically than animals with a typical number of crystal cells. EM revealed crystal cell contacts with fiber cells and epithelial cells but these contacts lacked features of synapses. EM spectroscopic analyses showed that crystals consist of the aragonite form of calcium carbonate. We thus provide behavioral evidence that Trichoplax are able to sense gravity, and that crystal cells are likely to be their gravity receptors. Moreover, because placozoans are thought to have evolved during Ediacaran or Cryogenian eras associated with aragonite seas, and their crystals are made of aragonite, they may have acquired gravity sensors during this early era.

  20. Optimization of processing parameters on the controlled growth of c-axis oriented ZnO nanorod arrays

    Energy Technology Data Exchange (ETDEWEB)

    Malek, M. F., E-mail: mfmalek07@gmail.com; Rusop, M., E-mail: rusop@salam.uitm.my [NANO-ElecTronic Centre (NET), Faculty of Electrical Engineering, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor (Malaysia); NANO-SciTech Centre (NST), Institute of Science (IOS), Universiti Teknologi MARA - UiTM, 40450 Shah Alam, Selangor (Malaysia); Mamat, M. H., E-mail: hafiz-030@yahoo.com [NANO-ElecTronic Centre (NET), Faculty of Electrical Engineering, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor (Malaysia); Musa, M. Z., E-mail: musa948@gmail.com [NANO-ElecTronic Centre (NET), Faculty of Electrical Engineering, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor (Malaysia); Faculty of Electrical Engineering, Universiti Teknologi MARA (UiTM) Pulau Pinang, Jalan Permatang Pauh, 13500 Permatang Pauh, Pulau Pinang (Malaysia); Saurdi, I., E-mail: saurdy788@gmail.com; Ishak, A., E-mail: ishak@sarawak.uitm.edu.my [NANO-ElecTronic Centre (NET), Faculty of Electrical Engineering, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor (Malaysia); Faculty of Electrical Engineering, Universiti Teknologi MARA (UiTM) Sarawak, Kampus Kota Samarahan, Jalan Meranek, 94300 Kota Samarahan, Sarawak (Malaysia); Alrokayan, Salman A. H., E-mail: dr.salman@alrokayan.com; Khan, Haseeb A., E-mail: khan-haseeb@yahoo.com [Chair of Targeting and Treatment of Cancer Using Nanoparticles, Deanship of Scientific Research, King Saud University (KSU), Riyadh 11451 (Saudi Arabia)

    2016-07-06

    Optimization of the growth time parameter was conducted to synthesize high-quality c-axis ZnO nanorod arrays. The effects of the parameter on the crystal growth and properties were systematically investigated. Our studies confirmed that the growth time influence the properties of ZnO nanorods where the crystallite size of the structures was increased at higher deposition time. Field emission scanning electron microsope analysis confirmed the morphologies structure of the ZnO nanorods. The ZnO nanostructures prepared under the optimized growth conditions showed an intense XRD peak which reveal a higher c-axis oriented ZnO nanorod arrays thus demonstrating the formation of defect free structure.

  1. Interspace modification of titania-nanorod arrays for efficient mesoscopic perovskite solar cells

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Peng; Jin, Zhixin; Wang, Yinglin, E-mail: wangyl100@nenu.edu.cn; Wang, Meiqi; Chen, Shixin; Zhang, Yang; Wang, Lingling; Zhang, Xintong, E-mail: xtzhang@nenu.edu.cn; Liu, Yichun, E-mail: ycliu@nenu.edu.cn

    2017-04-30

    Highlights: • The fabrication of perovskite solar cells utilizing TiO{sub 2} NR arrays. • Investigation of the interspace effect of TiO{sub 2} NR on perovskite layer. • Understanding of the balance between perovskite capping layer and pore filling. - Abstract: Morphology of electron transport layers (ETLs) has an important influence on the device architecture and electronic processes of mesostructured solar cells. In this work, we thoroughly investigated the effect of the interspace of TiO{sub 2} nanorod (NR) arrays on the photovoltaic performance of the perovskite solar cells (PSCs). Along with the interspace in TiO{sub 2}-NR arrays increasing, the thickness as well as the crystal size of perovskite capping layer are reduced accordingly, and the filling of perovskite in the channel becomes incomplete. Electrochemical impedance spectroscopy measurements reveal that this variation of perovskite absorber layer, induced by interspace of TiO{sub 2} NR arrays, causes the change of charge recombination process at the TiO{sub 2}/perovskite interface, suggesting that a balance between capping layer and the perovskite filling is critical to obtain high charge collection efficiency of PSCs. A power conversion efficiency of 10.3% could be achieved through careful optimization of interspace in TiO{sub 2}-NR arrays. Our research will shed light on the morphology control of ETLs with 1D structure for heterojunction solar cells fabricated by solution-deposited method.

  2. Influence of miscut on crystal truncation rod scattering

    International Nuclear Information System (INIS)

    Munkholm, A.; Brennan, S.

    1999-01-01

    X-rays can be used to measure the roughness of a surface by the study of crystal truncation rod scattering. It is shown that for a simple cubic lattice the presence of a miscut surface with a regular step array has no effect on the scattered intensity of a single rod and that a distribution of terrace widths on the surface is shown to have the same effect as adding roughness to the surface. For a perfect crystal without miscut, the scattered intensity is the sum of the intensity from all the rods with the same in-plane momentum transfer. For all real crystals, the scattered intensity is better described as that from a single rod. It is shown that data-collection strategies must correctly account for the sample miscut or there is a potential for improperly measuring the rod intensity. This can result in an asymmetry in the rod intensity above and below the Bragg peak, which can be misinterpreted as being due to a relaxation of the surface. The calculations presented here are compared with data for silicon (001) wafers with 0.1 and 4 miscuts. (orig.)

  3. Crystal structure of core streptavidin determined from multi-wavelength anomalous diffraction of synchrotron radiation

    International Nuclear Information System (INIS)

    Hendrickson, W.A.; Paehler, A.; Smith, J.L.; Satow, Y.; Merritt, E.A.; Phizackerley, R.P.

    1989-01-01

    A three-dimensional crystal structure of the biotin-binding core of streptavidin has been determined at 3.1-angstrom resolution. The structure was analyzed from diffraction data measured at three wavelengths from a single crystal of the selenobiotinyl complex with streptavidin. Streptavidin is a tetramer with subunits arrayed in D 2 symmetry. Each protomer is an 8-stranded β-barrel with simple up-down topology. Biotin molecules are bound at one end of each barrel. This study demonstrates the effectiveness of multi-wavelength anomalous diffraction (MAD) procedures for macromolecular crystallography and provides a basis for detailed study of biotin-avidin interactions

  4. Multistability in planar liquid crystal wells

    KAUST Repository

    Luo, Chong

    2012-06-08

    A planar bistable liquid crystal device, reported in Tsakonas, is modeled within the Landau-de Gennes theory for nematic liquid crystals. This planar device consists of an array of square micrometer-sized wells. We obtain six different classes of equilibrium profiles and these profiles are classified as diagonal or rotated solutions. In the strong anchoring case, we propose a Dirichlet boundary condition that mimics the experimentally imposed tangent boundary conditions. In the weak anchoring case, we present a suitable surface energy and study the multiplicity of solutions as a function of the anchoring strength. We find that diagonal solutions exist for all values of the anchoring strength W≥0, while rotated solutions only exist for W≥W c>0, where W c is a critical anchoring strength that has been computed numerically. We propose a dynamic model for the switching mechanisms based on only dielectric effects. For sufficiently strong external electric fields, we numerically demonstrate diagonal-to-rotated and rotated-to-diagonal switching by allowing for variable anchoring strength across the domain boundary. © 2012 American Physical Society.

  5. Multistability in planar liquid crystal wells

    KAUST Repository

    Luo, Chong; Majumdar, Apala; Erban, Radek

    2012-01-01

    A planar bistable liquid crystal device, reported in Tsakonas, is modeled within the Landau-de Gennes theory for nematic liquid crystals. This planar device consists of an array of square micrometer-sized wells. We obtain six different classes of equilibrium profiles and these profiles are classified as diagonal or rotated solutions. In the strong anchoring case, we propose a Dirichlet boundary condition that mimics the experimentally imposed tangent boundary conditions. In the weak anchoring case, we present a suitable surface energy and study the multiplicity of solutions as a function of the anchoring strength. We find that diagonal solutions exist for all values of the anchoring strength W≥0, while rotated solutions only exist for W≥W c>0, where W c is a critical anchoring strength that has been computed numerically. We propose a dynamic model for the switching mechanisms based on only dielectric effects. For sufficiently strong external electric fields, we numerically demonstrate diagonal-to-rotated and rotated-to-diagonal switching by allowing for variable anchoring strength across the domain boundary. © 2012 American Physical Society.

  6. Investigation of 2D photonic crystal structure based channel drop filter using quad shaped photonic crystal ring resonator for CWDM system

    Energy Technology Data Exchange (ETDEWEB)

    Chhipa, Mayur Kumar, E-mail: mayurchhipa1@gmail.com; Dusad, Lalit Kumar [Government Engineering College Ajmer, Rajasthan (India); Rajasthan Technical University, Kota, Rajasthan (India)

    2016-05-06

    In this paper, the design & performance of two dimensional (2-D) photonic crystal structure based channel drop filter is investigated using quad shaped photonic crystal ring resonator. In this paper, Photonic Crystal (PhC) based on square lattice periodic arrays of Gallium Indium Phosphide (GaInP) rods in air structure have been investigated using Finite Difference Time Domain (FDTD) method and photonic band gap is being calculated using Plane Wave Expansion (PWE) method. The PhC designs have been optimized for telecommunication wavelength λ= 1571 nm by varying the rods lattice constant. The number of rods in Z and X directions is 21 and 20, with lattice constant 0.540 nm it illustrates that the arrangement of Gallium Indium Phosphide (GaInP) rods in the structure which gives the overall size of the device around 11.4 µm × 10.8 µm. The designed filter gives good dropping efficiency using 3.298, refractive index. The designed structure is useful for CWDM systems. This device may serve as a key component in photonic integrated circuits. The device is ultra compact with the overall size around 123 µm{sup 2}.

  7. Microwave-assisted self-doping of TiO2 photonic crystals for efficient photoelectrochemical water splitting

    KAUST Repository

    Zhang, Zhonghai; Yang, Xiulin; Hedhili, Mohamed N.; Ahmed, Elaf S.; Shi, Le; Wang, Peng

    2014-01-01

    In this article, we report that the combination of microwave heating and ethylene glycol, a mild reducing agent, can induce Ti3+ self-doping in TiO2. A hierarchical TiO2 nanotube array with the top layer serving as TiO2 photonic crystals (TiO2 NTPCs

  8. Crystallization mechanisms of acicular crystals

    Science.gov (United States)

    Puel, François; Verdurand, Elodie; Taulelle, Pascal; Bebon, Christine; Colson, Didier; Klein, Jean-Paul; Veesler, Stéphane

    2008-01-01

    In this contribution, we present an experimental investigation of the growth of four different organic molecules produced at industrial scale with a view to understand the crystallization mechanism of acicular or needle-like crystals. For all organic crystals studied in this article, layer-by-layer growth of the lateral faces is very slow and clear, as soon as the supersaturation is high enough, there is competition between growth and surface-activated secondary nucleation. This gives rise to pseudo-twinned crystals composed of several needle individuals aligned along a crystallographic axis; this is explained by regular over- and inter-growths as in the case of twinning. And when supersaturation is even higher, nucleation is fast and random. In an industrial continuous crystallization, the rapid growth of needle-like crystals is to be avoided as it leads to fragile crystals or needles, which can be partly broken or totally detached from the parent crystals especially along structural anisotropic axis corresponding to weaker chemical bonds, thus leading to slower growing faces. When an activated mechanism is involved such as a secondary surface nucleation, it is no longer possible to obtain a steady state. Therefore, the crystal number, size and habit vary significantly with time, leading to troubles in the downstream processing operations and to modifications of the final solid-specific properties. These results provide valuable information on the unique crystallization mechanisms of acicular crystals, and show that it is important to know these threshold and critical values when running a crystallizer in order to obtain easy-to-handle crystals.

  9. Finite element method analysis of band gap and transmission of two-dimensional metallic photonic crystals at terahertz frequencies.

    Science.gov (United States)

    Degirmenci, Elif; Landais, Pascal

    2013-10-20

    Photonic band gap and transmission characteristics of 2D metallic photonic crystals at THz frequencies have been investigated using finite element method (FEM). Photonic crystals composed of metallic rods in air, in square and triangular lattice arrangements, are considered for transverse electric and transverse magnetic polarizations. The modes and band gap characteristics of metallic photonic crystal structure are investigated by solving the eigenvalue problem over a unit cell of the lattice using periodic boundary conditions. A photonic band gap diagram of dielectric photonic crystal in square lattice array is also considered and compared with well-known plane wave expansion results verifying our FEM approach. The photonic band gap designs for both dielectric and metallic photonic crystals are consistent with previous studies obtained by different methods. Perfect match is obtained between photonic band gap diagrams and transmission spectra of corresponding lattice structure.

  10. Study of the reaction {sup 22}O(p,p') with MUST detector. Development of the Cs(Tl) part of MUST-2 detector; Etude de la reaction {sup 22}O(p,p') avec le detecteur MUST. Developpement de l'etage CsI(Tl) de l'ensemble MUST 2

    Energy Technology Data Exchange (ETDEWEB)

    Becheva, E

    2004-11-01

    Elastic and inelastic proton scattering on the unstable nuclei {sup 22}O was measured in inverse kinematics at the GANIL facility. A secondary beam of {sup 22}O at 46.6 MeV/A with intensity of {approx} 1000 pps, impinged on a (CH{sub 2}){sub n} target. Recoiling protons were detected in the silicon strip array MUST. We measured the angular distributions of the ground and 2{sub 1}{sup +} states of {sup 22}O. Phenomenological and microscopic analysis of the data were performed. The phenomenological analysis using a global potential parameterization of Becchetti and Greenlees and CH89 yields a value of the deformation parameter {beta}{sub p,p}, = 0.23{+-}0.04 for {sup 22}O, much lower than that of {sup 20}O. The ratio of neutron and proton matrix element M{sub n}/M{sub p} is found equal to 1.46{+-}0.50. The microscopic analysis used of densities and transition densities calculated within HFB and QRPA models respectively. Optical potential were obtained through both folding and JLM procedures. A ratio M{sub n}/M{sub p}=2.5{+-}1.0 is deduced. Contrary of {sup 20}O, {sup 22}O behaviours like a doubly magic nucleus, suggesting a pronounced sub-shell closure at N=14. To develop the study of direct reactions induced by radioactive beams, we have developed and built, a new multi-detector MUST II devoted to light charged particle detection. In this work we established the requirements for the CsI(Tl) detector stage, and test four CsI detector prototypes, constructed by the SCIONIX company. (author)

  11. The performance of prototype vacuum phototriodes in the first full sized supercrystal array for the CMS ECAL endcaps

    Energy Technology Data Exchange (ETDEWEB)

    Apollonio, M; Barber, G; Britton, D; Davies, G; Mcleod, E; Seez, C [Imperial College, London (United Kingdom); Bell, K W; Brown, R M; Imrie, D C; Lintern, A; Lodge, A; Smith, B; Sproston, M [Rutherford Appleton Laboratory, Chilton, Didcot, Oxon OX11 0QX (United Kingdom); Brooke, J [University of Bristol, Bristol (United Kingdom); Bourotte, J [LLR, Ecole Polytechnique, Palaiseau (France); Camanzi, B [Brunel University, Uxbridge (United Kingdom); Cockerill, D J.A. . [Rutherford Appleton Laboratory, Chilton, Didcot, Oxon OX11 0QX (United Kingdom); Devitsin, E [P.N. Lebedev Physical Institute, Moscow (Russian Federation); Ergun, G [Brunel University, Uxbridge (United Kingdom); Gninenko, S [INR, Moscow (Russian Federation); Golubev, N [INR, Moscow (Russian Federation); Goussev, Y [Petersburg Nuclear Physics Institute, Gatchina (Russian Federation); Haguenauer, M [LLR, Ecole Polytechnique, Palaiseau (France); Head, R [University of Bristol, Bristol (United Kingdom); Heath, H [University of Bristol, Bristol (United Kingdom); Hobson, P R [Brunel University, Uxbridge (United Kingdom); Inyakin, A [INR, Moscow (Russian Federation); Katchanov, V [INR, Moscow (Russian Federation); Kirsanov, M [INR, Moscow (Russian Federation); Nash, S [University of Bristol, Bristol (United Kingdom); Newbold, D [University of Bristol, Bristol (United Kingdom); Ukhanov, M [Protvino, Moscow (Russian Federation); Postoev, V [Protvino, Moscow (Russian Federation); Patalakha, D [Protvino, Moscow (Russian Federation); Presland, A [University of Bristol, Bristol (United Kingdom); Probert, M [University of Bristol, Bristol (United Kingdom); Semeniouk, I [INR, Moscow (Russian Federation); Seliverstov, D [Petersburg Nuclear Physics Institute, Gatchina (Russian Federation); Tapper, R [University of Bristol, Bristol (United Kingdom); Tchuiko, B [Protvino, Moscow (Russian Federation)

    2004-10-21

    The performance of prototype vacuum phototriodes is presented from the first full sized supercrystal array for the CMS ECAL endcaps. The array was exposed to high-energy electrons and tested in magnetic fields of up to 3 T, in the CERN North area, in July and August 1999. The mean VPT electron yield, normalised to a naked crystal light yield of 8 photoelectrons/MeV into an HPMT, was found to be 25 electrons/MeV at 3 T for devices from Research Institute Electron, 35 electrons/MeV for devices from Hamamatsu and 18/23 electrons/MeV from Electron Tubes.

  12. Opal-like Multicolor Appearance of Self-Assembled Photonic Array.

    Science.gov (United States)

    Arnon, Zohar A; Pinotsi, Dorothea; Schmidt, Matthias; Gilead, Sharon; Guterman, Tom; Sadhanala, Aditya; Ahmad, Shahab; Levin, Aviad; Walther, Paul; Kaminski, Clemens F; Fändrich, Marcus; Kaminski Schierle, Gabriele S; Adler-Abramovich, Lihi; Shimon, Linda J W; Gazit, Ehud

    2018-06-20

    Molecular self-assembly of short peptide building blocks leads to the formation of various material architectures that may possess unique physical properties. Recent studies had confirmed the key role of biaromaticity in peptide self-assembly, with the diphenylalanine (FF) structural family as an archetypal model. Another significant direction in the molecular engineering of peptide building blocks is the use of fluorenylmethoxycarbonyl (Fmoc) modification, which promotes the assembly process and may result in nanostructures with distinctive features and macroscopic hydrogel with supramolecular features and nanoscale order. Here, we explored the self-assembly of the protected, noncoded fluorenylmethoxycarbonyl-β,β-diphenyl-Ala-OH (Fmoc-Dip) amino acid. This process results in the formation of elongated needle-like crystals with notable aromatic continuity. By altering the assembly conditions, arrays of spherical particles were formed that exhibit strong light scattering. These arrays display vivid coloration, strongly resembling the appearance of opal gemstones. However, unlike the Rayleigh scattering effect produced by the arrangement of opal, the described optical phenomenon is attributed to Mie scattering. Moreover, by controlling the solution evaporation rate, i.e., the assembly kinetics, we were able to manipulate the resulting coloration. This work demonstrates a bottom-up approach, utilizing self-assembly of a protected amino acid minimal building block, to create arrays of organic, light-scattering colorful surfaces.

  13. Thermal detection of single e-h pairs in a biased silicon crystal detector

    Science.gov (United States)

    Romani, R. K.; Brink, P. L.; Cabrera, B.; Cherry, M.; Howarth, T.; Kurinsky, N.; Moffatt, R. A.; Partridge, R.; Ponce, F.; Pyle, M.; Tomada, A.; Yellin, S.; Yen, J. J.; Young, B. A.

    2018-01-01

    We demonstrate that individual electron-hole pairs are resolved in a 1 cm2 by 4 mm thick silicon crystal (0.93 g) operated at ˜35 mK. One side of the detector is patterned with two quasiparticle-trap-assisted electro-thermal-feedback transition edge sensor arrays held near ground potential. The other side contains a bias grid with 20% coverage. Bias potentials up to ±160 V were used in the work reported here. A fiber optic provides 650 nm (1.9 eV) photons that each produce an electron-hole (e- h+) pair in the crystal near the grid. The energy of the drifting charges is measured with a phonon sensor noise σ ˜0.09 e- h+ pair. The observed charge quantization is nearly identical for h+s or e-s transported across the crystal.

  14. Insights Into the Solution Crystallization of Oriented Alq3 and Znq2 Microprisms and Nanorods.

    Science.gov (United States)

    Boulet, Joel; Mohammadpour, Arash; Shankar, Karthik

    2015-09-01

    Optimized solution-based methods to grow high quality micro- and nanocrystals of organic semi-conductors with defined size, shape and orientation are important to a variety of optoelectronic applications. In this context, we report the growth of single crystal micro- and nanostructures of the organic semiconductors Tris(8-hydroxyquinoline)aluminum (Alq3) and bis(8-hydroxyquinoline)zinc (Znq2) terminating in flat crystal planes using a combination of evaporative and antisolvent crystallization. By controlling substrate-specific nucleation and optimizing the conditions of growth, we generate vertically-oriented hexagonal prism arrays of Alq3, and vertical half-disks and sharp-edged rectangular prisms of Znq2. The effect of process variables such as ambient vapour pressure, choice of anti-solvent and temperature on the morphology and crystal habit of the nanostructures were studied and the results of varying them catalogued to gain a better understanding of the mechanism of growth.

  15. Deterministic patterned growth of high-mobility large-crystal graphene: a path towards wafer scale integration

    Science.gov (United States)

    Miseikis, Vaidotas; Bianco, Federica; David, Jérémy; Gemmi, Mauro; Pellegrini, Vittorio; Romagnoli, Marco; Coletti, Camilla

    2017-06-01

    We demonstrate rapid deterministic (seeded) growth of large single-crystals of graphene by chemical vapour deposition (CVD) utilising pre-patterned copper substrates with chromium nucleation sites. Arrays of graphene single-crystals as large as several hundred microns are grown with a periodicity of up to 1 mm. The graphene is transferred to target substrates using aligned and contamination- free semi-dry transfer. The high quality of the synthesised graphene is confirmed by Raman spectroscopy and transport measurements, demonstrating room-temperature carrier mobility of 21 000 cm2 V-1 s-1 when transferred on top of hexagonal boron nitride. By tailoring the nucleation of large single-crystals according to the desired device geometry, it will be possible to produce complex device architectures based on single-crystal graphene, thus paving the way to the adoption of CVD graphene in wafer-scale fabrication.

  16. A region segmentation based algorithm for building a crystal position lookup table in a scintillation detector

    International Nuclear Information System (INIS)

    Wang Haipeng; Fan Xin; Yun Mingkai; Liu Shuangquan; Cao Xuexiang; Chai Pei; Shan Baoci

    2015-01-01

    In a scintillation detector, scintillation crystals are typically made into a 2-dimensional modular array. The location of incident gamma-ray needs be calibrated due to spatial response nonlinearity. Generally, position histograms-the characteristic flood response of scintillation detectors-are used for position calibration. In this paper, a position calibration method based on a crystal position lookup table which maps the inaccurate location calculated by Anger logic to the exact hitting crystal position has been proposed. Firstly, the position histogram is preprocessed, such as noise reduction and image enhancement. Then the processed position histogram is segmented into disconnected regions, and crystal marking points are labeled by finding the centroids of regions. Finally, crystal boundaries are determined and the crystal position lookup table is generated. The scheme is evaluated by the whole-body positron emission tomography (PET) scanner and breast dedicated single photon emission computed tomography scanner developed by the Institute of High Energy Physics, Chinese Academy of Sciences. The results demonstrate that the algorithm is accurate, efficient, robust and applicable to any configurations of scintillation detector. (authors)

  17. Formation of 3D cholesterol crystals from 2D nucleation sites in lipid bilayer membranes: implications for atherosclerosis.

    Science.gov (United States)

    Varsano, Neta; Fargion, Iael; Wolf, Sharon G; Leiserowitz, Leslie; Addadi, Lia

    2015-02-04

    Atherosclerosis is the major precursor of cardiovascular disease. The formation of cholesterol crystals in atherosclerotic plaques is associated with the onset of acute pathology. The cholesterol crystals induce physical injury in the plaque core, promoting cell apoptosis and triggering an increased inflammatory response. Herein we address the question of how cholesterol crystal formation occurs in atherosclerosis. We demonstrate that three-dimensional (3D) cholesterol crystals can undergo directed nucleation from bilayer membranes containing two-dimensional (2D) cholesterol crystalline domains. We studied crystal formation on supported lipid bilayers loaded with exogenous cholesterol and labeled using a monoclonal antibody that specifically recognizes ordered cholesterol arrays. Our findings show that 3D crystals are formed exclusively on the bilayer regions where there are segregated 2D cholesterol crystalline domains and that they form on the domains. This study has potentially significant implications for our understanding of the crucial step in the mechanism by which atherosclerotic lesions form.

  18. SNP Arrays

    Directory of Open Access Journals (Sweden)

    Jari Louhelainen

    2016-10-01

    Full Text Available The papers published in this Special Issue “SNP arrays” (Single Nucleotide Polymorphism Arrays focus on several perspectives associated with arrays of this type. The range of papers vary from a case report to reviews, thereby targeting wider audiences working in this field. The research focus of SNP arrays is often human cancers but this Issue expands that focus to include areas such as rare conditions, animal breeding and bioinformatics tools. Given the limited scope, the spectrum of papers is nothing short of remarkable and even from a technical point of view these papers will contribute to the field at a general level. Three of the papers published in this Special Issue focus on the use of various SNP array approaches in the analysis of three different cancer types. Two of the papers concentrate on two very different rare conditions, applying the SNP arrays slightly differently. Finally, two other papers evaluate the use of the SNP arrays in the context of genetic analysis of livestock. The findings reported in these papers help to close gaps in the current literature and also to give guidelines for future applications of SNP arrays.

  19. Synthesis of ZnO nanowire arrays on ZnO−TiO{sub 2} mixed oxide seed layer for dye sensitized solar cell applications

    Energy Technology Data Exchange (ETDEWEB)

    Marimuthu, T. [Advanced Materials and Thin Film Physics Lab, Department of Physics, Alagappa University, Karaikudi (India); Anandhan, N., E-mail: anandhan_kn@rediffmail.com [Advanced Materials and Thin Film Physics Lab, Department of Physics, Alagappa University, Karaikudi (India); Thangamuthu, R. [Electrochemical Materials Science Division, CSIR-Central Electrochemical Research Institute, Karaikudi (India); Mummoorthi, M. [Advanced Materials and Thin Film Physics Lab, Department of Physics, Alagappa University, Karaikudi (India); Ravi, G. [Photonic Crystal Lab, Department of Physics, Alagappa University, Karaikudi (India)

    2016-08-25

    ZnO nanowire arrays (NWAs) were synthesized on ZnO−TiO{sub 2} mixed oxide seeded FTO conducting glass plate by two-step sol-gel and hydrothermal method, respectively. X-ray diffraction patterns reveal the presence of mixed and hexagonal phases in seed layer and NWAs, respectively. Scanning electron microscope images showed that the FTO glass plate is uniformly covered with grains and a few nanorods in seed layer and dense NWAs are vertically grown on the seed layer. The hexagonal structure and high crystal quality have been confirmed by micro Raman spectra. Photoluminescence spectra also present that NWAs have high crystal quality and less atomic defects. UV spectra indicate that NWAs are absorbed more dye molecules and it has the band gap equal to bulk material. The efficiency of ZnO−TiO{sub 2} mixed oxide seed layer and ZnO NWAs is found to be 0.56 and 0.84% respectively. Electrochemical impedance spectra reveal that NWAs DSSC has high charge transfer recombination resistance than the seed layer DSSC. - Highlights: • ZnO nanowire arrays were synthesized by two-step sol-gel and hydrothermal method. • The crystal structure and crystalline quality of films are confirmed by Raman spectra. • The emission properties of films are investigated by photoluminescence spectra. • ZnO nanowire arrays (NWAs) have higher charge transfer recombination resistance. • The conversion efficiency of the seed layer and NWAs is to be 0.56 and 0.84%.

  20. Wurtzite InP nanowire arrays grown by selective area MOCVD

    International Nuclear Information System (INIS)

    Chu, Hyung-Joon; Stewart, Lawrence; Yeh, Ting-Wei; Dapkus, P.D.

    2010-01-01

    InP nanowires are a unique material phase because this normally zincblende material forms in the wurtzite crystal structure below a critical diameter owing to the contribution of sidewalls to the total formation energy. This may allow control of the carrier transport and optical properties of InP nanowires for applications such as nano scale transistors, lasers and detectors. In this work, we describe the fabrication of InP nanowire arrays by selective area growth using MOCVD in the diameter range where the wurtzite structure is formed. The spatial growth rate in selective area growth is modeled by a diffusion model for the precursors. The proposed model achieves an average error of 9%. Electron microscopy shows that the grown InP nanowires are in the wurtzite crystal phase with many stacking faults. The threshold diameter of the crystal phase transition of InP nanowires is larger than the thermodynamic estimation. In order to explain this tendency, we propose a surface kinetics model based on a 2 x 2 reconstruction. This model can explain the increased tendency for wurtzite nanowire formation on InP (111)A substrates and the preferred growth direction of binary III-V compound semiconductor nanowires. (copyright 2010 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  1. Distribution of calcium oxalate crystals in floral organs of Araceae in relation to pollination strategy.

    Science.gov (United States)

    Coté, Gary G; Gibernau, Marc

    2012-07-01

    Many flowers are pollinated by potentially hungry insects, yet flowers also contain gametes and embryos which must be protected from predation. Microscopic calcium oxalate crystals in plant tissues have been proposed to protect against herbivory. Aroids, which have an unusual diversity of such crystals, also exhibit diverse pollination strategies. Many species have pollinators that do not feed while visiting the flowers, while other species, especially those pollinated by beetles, offer sterile staminodia as food rewards. We examined flowers of 21 aroid species with various pollination strategies to test the hypothesis that crystals protect vital gametes and embryos while allowing consumption of food bribes. Aroid inflorescences collected from the field or from greenhouse material were sectioned, cleared, and examined by bright field and polarization microscopy. All species examined, regardless of pollination strategy, arrayed crystals around unshed pollen and ovules. Less vital tissues, such as odoriferous appendages, had few crystals. Staminodia offered as food to beetle pollinators, however, differed greatly between species in their crystal contents. Some had minimal crystals; some had crystals in patterns suggesting they limit beetle feeding; still others had abundant crystals in no obvious pattern. The results are consistent with crystals protecting against insect predation of gametes and embryos. However, the role of crystals in food-bribe staminodia is unclear. They may limit and direct feeding by beetles in some species, while in others they might have no protective role.

  2. A novel method to design sparse linear arrays for ultrasonic phased array.

    Science.gov (United States)

    Yang, Ping; Chen, Bin; Shi, Ke-Ren

    2006-12-22

    In ultrasonic phased array testing, a sparse array can increase the resolution by enlarging the aperture without adding system complexity. Designing a sparse array involves choosing the best or a better configuration from a large number of candidate arrays. We firstly designed sparse arrays by using a genetic algorithm, but found that the arrays have poor performance and poor consistency. So, a method based on the Minimum Redundancy Linear Array was then adopted. Some elements are determined by the minimum-redundancy array firstly in order to ensure spatial resolution and then a genetic algorithm is used to optimize the remaining elements. Sparse arrays designed by this method have much better performance and consistency compared to the arrays designed only by a genetic algorithm. Both simulation and experiment confirm the effectiveness.

  3. Using CHIMERA detector at LNS for gamma-particle coincidences

    Directory of Open Access Journals (Sweden)

    Cardella G.

    2016-01-01

    Full Text Available We have recently evaluated the quality of γ-ray angular distributions that can be extracted in particle-gamma coincidence measurements using the CHIMERA detector at LNS. γ-rays have been detected using the CsI(Tl detectors of the spherical part of the CHIMERA array. Very clean γ-rays angular distributions were extracted in reactions induced by different stable beams impinging on 12C thin targets. The results evidenced an effect of projectile spin flip on the γ-rays angular distributions. γ-particle coincidence measurements were also performed in reactions induced by neutron rich exotic beams produced through in-flight fragmentation at LNS. In recent experiments also the Farcos array was used to improve energy and angular resolution measurements of the detected charged particles. Results obtained with both stable and radioactive beams are reported.

  4. Isolation and Identification of Myo-Inositol Crystals from Dragon Fruit (Hylocereus polyrhizus

    Directory of Open Access Journals (Sweden)

    Chandran Somasundram

    2012-04-01

    Full Text Available Crystals isolated from Hylocereus polyrhizus were analyzed using four different approaches—X-ray Crystallography, High Performance Liquid Chromatography (HPLC, Liquid Chromatography Tandem Mass Spectrometry (LC-MS/MS and Nuclear Magnetic Resonance (NMR and identified as myo-inositol. The X-ray crystallography analysis showed that the unit-cell parameters were: a = 6.6226 (3 Å, b = 12.0462 (5 Å, c = 18.8942 (8 Å, α = 90.00, β = 93.98, δ = 90.00. The purity of the crystals were checked using HPLC, whereupon a clean single peak was obtained at 4.8 min with a peak area of 41232 μV*s. The LC-MS/MS technique, which is highly sensitive and selective, was used to provide a comparison of the isolated crystals with a myo-inositol standard where the results gave an identical match for both precursor and product ions. NMR was employed to confirm the molecular structure and conformation of the crystals, and the results were in agreement with the earlier results in this study. The discovery of myo-inositol crystals in substantial amount in H. polyrhizus has thus far not been reported and this is an important finding which will increase the marketability and importance of H. polyrhizus as a crop with a wide array of health properties.

  5. High energy, widely tunable Si-prism-array coupled terahertz-wave parametric oscillator with a deformed pump and optimal crystal location for angle tuning.

    Science.gov (United States)

    Zhang, Ruiliang; Qu, Yanchen; Zhao, Weijiang; Chen, Zhenlei

    2017-03-20

    A high energy, widely tunable Si-prism-array coupled terahertz-wave parametric oscillator (TPO) has been demonstrated by using a deformed pump. The deformed pump is cut from a beam spot of 2 mm in diameter by a 1-mm-wide slit. In comparison with a small pump spot (1-mm diameter), the THz-wave coupling area for the deformed pump is increased without limitation to the low-frequency end of the tuning range. Besides, the crystal location is specially designed to eliminate the alteration of the output position of the pump during angle tuning, so the initially adjusted nearest pumped region to the THz-wave exit surface is maintained throughout the tuning range. The tuning range is 0.58-2.5 THz for the deformed pump, while its low frequency end is limited at approximately 1.2 THz for the undeformed pump with 2 mm diameter. The highest THz-wave output of 2 μJ, which is 2.25 times as large as that from the pump of 1 mm in diameter, is obtained at 1.15 THz under 38 mJ (300  MW/cm2) pumping. The energy conversion efficiency is 5.3×10-5.

  6. Light-assisted, templated self-assembly using a photonic-crystal slab.

    Science.gov (United States)

    Jaquay, Eric; Martínez, Luis Javier; Mejia, Camilo A; Povinelli, Michelle L

    2013-05-08

    We experimentally demonstrate the technique of light-assisted, templated self-assembly (LATS). We excite a guided-resonance mode of a photonic-crystal slab with 1.55 μm laser light to create an array of optical traps. We demonstrate assembly of a square lattice of 520 nm diameter polystyrene particles spaced by 860 nm. Our results demonstrate how LATS can be used to fabricate reconfigurable structures with symmetries different from traditional colloidal self-assembly, which is limited by free energetic constraints.

  7. Dynamic Diffraction Studies on the Crystallization, Phase Transformation, and Activation Energies in Anodized Titania Nanotubes

    Directory of Open Access Journals (Sweden)

    Hani Albetran

    2018-02-01

    Full Text Available The influence of calcination time on the phase transformation and crystallization kinetics of anodized titania nanotube arrays was studied using in-situ isothermal and non-isothermal synchrotron radiation diffraction from room temperature to 900 °C. Anatase first crystallized at 400 °C, while rutile crystallized at 550 °C. Isothermal heating of the anodized titania nanotubes by an increase in the calcination time at 400, 450, 500, 550, 600, and 650 °C resulted in a slight reduction in anatase abundance, but an increase in the abundance of rutile because of an anatase-to-rutile transformation. The Avrami equation was used to model the titania crystallization mechanism and the Arrhenius equation was used to estimate the activation energies of the titania phase transformation. Activation energies of 22 (10 kJ/mol for the titanium-to-anatase transformation, and 207 (17 kJ/mol for the anatase-to-rutile transformation were estimated.

  8. Dynamic Diffraction Studies on the Crystallization, Phase Transformation, and Activation Energies in Anodized Titania Nanotubes.

    Science.gov (United States)

    Albetran, Hani; Vega, Victor; Prida, Victor M; Low, It-Meng

    2018-02-23

    The influence of calcination time on the phase transformation and crystallization kinetics of anodized titania nanotube arrays was studied using in-situ isothermal and non-isothermal synchrotron radiation diffraction from room temperature to 900 °C. Anatase first crystallized at 400 °C, while rutile crystallized at 550 °C. Isothermal heating of the anodized titania nanotubes by an increase in the calcination time at 400, 450, 500, 550, 600, and 650 °C resulted in a slight reduction in anatase abundance, but an increase in the abundance of rutile because of an anatase-to-rutile transformation. The Avrami equation was used to model the titania crystallization mechanism and the Arrhenius equation was used to estimate the activation energies of the titania phase transformation. Activation energies of 22 (10) kJ/mol for the titanium-to-anatase transformation, and 207 (17) kJ/mol for the anatase-to-rutile transformation were estimated.

  9. Scintillation properties of semiconducting {sup 6}LiInSe{sub 2} crystals to ionizing radiation

    Energy Technology Data Exchange (ETDEWEB)

    Wiggins, Brenden [Y-12 National Security Complex, Oak Ridge, TN (United States); Vanderbilt University, Nashville, TN (United States); Groza, Michael; Tupitsyn, Eugene [Fisk University, Nashville, TN (United States); Lukosi, Eric [University of Tennessee, Knoxville, TN (United States); Stassun, Keivan; Burger, Arnold [Vanderbilt University, Nashville, TN (United States); Fisk University, Nashville, TN (United States); Stowe, Ashley [Y-12 National Security Complex, Oak Ridge, TN (United States); Vanderbilt University, Nashville, TN (United States); University of Tennessee, Knoxville, TN (United States)

    2015-11-21

    {sup 6}LiInSe{sub 2} has gained attention recently as a semiconducting thermal neutron detector. As presented herein, the chalcogenide compound semiconductor also detects incident neutrons via scintillation, making {sup 6}LiInSe{sub 2} the only lithium containing semiconductor to respond to neutrons via both detection mechanisms. Both yellow and red crystals, which appear in the literature, were investigated. Only the yellow crystal responded favorably to ionizing radiation, similar to the semiconducting operation utilizing electrodes. The obtained light yield for yellow crystals is 4400 photons/MeV, referenced to Bi{sub 4}Ge{sub 3}O{sub 12} (BGO).The estimated thermal neutron light yield was 21,000 photons/thermal neutron. The two measured decay time components were found to be 31±1 ns (49%) and 143±9 ns (51%).This crystal provides efficient, robust detection of neutrons via scintillation with respectable light yield and rapid response, enabling its use for a broad array of neutron detection applications.

  10. Solar cell array for driving MOS type FET gate. MOS gata EFT gate kudoyo taiyo denchi array

    Energy Technology Data Exchange (ETDEWEB)

    Murakami, S; Yoshida, K; Yoshiki, T; Yamaguchi, Y; Nakayama, T; Owada, Y

    1990-03-12

    There has been a semiconductor relay utilizing MOS type FET (field effect transistor). Concerning the solar cells used for a semiconductor relay, it is required to separate the cells by forming insulating oxide films first and to form semiconductor layers by using many mask patterns, since a crystal semiconductor is used. Thereby its manufacturing process becomes complicated and laminification as well as thin film formation are difficult, In view of the above, this invention proposes a solar cell array for driving a MOS type FET gate consisting of amorphous silicon semiconductor cells, which are used for a semiconductor relay with solar cells generating electromotive power by the light of a light emitting diode and a MOS type FET that the power output of the above solar cells is supplied to its gate, and which are connected in series with many steps. 9 figs.

  11. All-carbon multi-electrode array for real-time in vitro measurements of oxidizable neurotransmitters

    Science.gov (United States)

    Picollo, Federico; Battiato, Alfio; Bernardi, Ettore; Plaitano, Marilena; Franchino, Claudio; Gosso, Sara; Pasquarelli, Alberto; Carbone, Emilio; Olivero, Paolo; Carabelli, Valentina

    2016-02-01

    We report on the ion beam fabrication of all-carbon multi electrode arrays (MEAs) based on 16 graphitic micro-channels embedded in single-crystal diamond (SCD) substrates. The fabricated SCD-MEAs are systematically employed for the in vitro simultaneous amperometric detection of the secretory activity from populations of chromaffin cells, demonstrating a new sensing approach with respect to standard techniques. The biochemical stability and biocompatibility of the SCD-based device combined with the parallel recording of multi-electrodes array allow: i) a significant time saving in data collection during drug screening and/or pharmacological tests over a large number of cells, ii) the possibility of comparing altered cell functionality among cell populations, and iii) the repeatition of acquisition runs over many cycles with a fully non-toxic and chemically robust bio-sensitive substrate.

  12. Optimization of Compton-suppression and summing schemes for the TIGRESS HPGe detector array

    Science.gov (United States)

    Schumaker, M. A.; Svensson, C. E.; Andreoiu, C.; Andreyev, A.; Austin, R. A. E.; Ball, G. C.; Bandyopadhyay, D.; Boston, A. J.; Chakrawarthy, R. S.; Churchman, R.; Drake, T. E.; Finlay, P.; Garrett, P. E.; Grinyer, G. F.; Hackman, G.; Hyland, B.; Jones, B.; Maharaj, R.; Morton, A. C.; Pearson, C. J.; Phillips, A. A.; Sarazin, F.; Scraggs, H. C.; Smith, M. B.; Valiente-Dobón, J. J.; Waddington, J. C.; Watters, L. M.

    2007-04-01

    Methods of optimizing the performance of an array of Compton-suppressed, segmented HPGe clover detectors have been developed which rely on the physical position sensitivity of both the HPGe crystals and the Compton-suppression shields. These relatively simple analysis procedures promise to improve the precision of experiments with the TRIUMF-ISAC Gamma-Ray Escape-Suppressed Spectrometer (TIGRESS). Suppression schemes will improve the efficiency and peak-to-total ratio of TIGRESS for high γ-ray multiplicity events by taking advantage of the 20-fold segmentation of the Compton-suppression shields, while the use of different summing schemes will improve results for a wide range of experimental conditions. The benefits of these methods are compared for many γ-ray energies and multiplicities using a GEANT4 simulation, and the optimal physical configuration of the TIGRESS array under each set of conditions is determined.

  13. Tri-component phononic crystals for underwater anechoic coatings

    International Nuclear Information System (INIS)

    Zhao, Honggang; Liu, Yaozong; Wen, Jihong; Yu, Dianlong; Wen, Xisen

    2007-01-01

    Localized resonance in phononic crystal, composed of three-dimensional arrays of composite units, has been discovered recently. The composite unit is a high-density sphere coated by soft silicon rubber. In this Letter, the absorptive properties induced by the localized resonance are systemically investigated. The mode conversions during the Mie scattering of a single coated lead sphere in unbounded epoxy are analyzed by referring the elements of the scattering matrix. Then the anechoic properties of a slab containing a plane of such composite scatterers are investigated with the multiple-scattering method by accounting the effects of the multiple scattering and the viscous dissipation. The results show that the longitudinal to transverse mode conversion nearby the locally resonant region is an effective way to enhance the anechoic performance of the finite slab of phononic crystal. Then, the influences of the viscoelasticity of the silicon rubber and the coating thickness on the acoustic properties of the finite slab are investigated for anechoic optimization. Finally, we synthetically consider the destructive scattering in the finite slab of phononic crystal and the backing, and design an anechoic slab composed of bi-layer coated spheres. The results show that the most of the incident energy is absorbed at the desired frequency band

  14. LYSO crystal testing for an EDM polarimeter

    Science.gov (United States)

    Müller, F.; Keshelashvili, I.; Mchedlishvili, D.; JEDI Collaboration

    2017-11-01

    Four detector modules, built from three different LYSO crystals and two different types of light sensors (PMTs and SiPM arrays), have been tested with a deuteron beam from 100 MeV - 270 MeV at the COSY accelerator facility for the srEDM project at the Forschungszentrum Jülich in Germany. The detector modules were arranged in a cluster hand mounted on a positioning table. The deuteron beam was targeted at the center of each individual crystal for data analysis. The signals were digitized using a 14 bit, 250 MS/s flash ADC. Further, the energy spectra were calibrated using the known beam energies from the accelerator. From the calibrated spectra, the energy resolution was calculated. A resolution of 3% for the low energies and down to 1% for the high energy of 270 MeV was achieved. A deuteron reconstruction efficiency of almost 100% for low energies and around 70% for high energies was achieved. The SiPM light sensor showed a very good performance and will be used for the next generation of detector modules.

  15. High Density Silver Nanowire Arrays using Self-ordered Anodic Aluminum Oxide (AAO) Membrane

    OpenAIRE

    Han, Young-Hwan

    2008-01-01

    High density silver nanowire arrays were synthesized through the self-ordered Anodic Aluminum Oxide (AAO) template. The pore size in the AAO membrane was confirmed by processing the widening porosity with a honeycomb structure with cross sections of 20nm, 50nm, and 100nm, by SEM. Pore numbers by unit area were consistent; only pore size changed. The synthesized silver nanowire, which was crystallized, was dense in the cross sections of the amorphous AAO membrane. The synthesized silver nanowi...

  16. Large-area 2D periodic crystalline silicon nanodome arrays on nanoimprinted glass exhibiting photonic band structure effects

    International Nuclear Information System (INIS)

    Becker, C; Lockau, D; Sontheimer, T; Rech, B; Schubert-Bischoff, P; Rudigier-Voigt, E; Bockmeyer, M; Schmidt, F

    2012-01-01

    Two-dimensional silicon nanodome arrays are prepared on large areas up to 50 cm 2 exhibiting photonic band structure effects in the near-infrared and visible wavelength region by downscaling a recently developed fabrication method based on nanoimprint-patterned glass, high-rate electron-beam evaporation of silicon, self-organized solid phase crystallization and wet-chemical etching. The silicon nanodomes, arranged in square lattice geometry with 300 nm lattice constant, are optically characterized by angular resolved reflection measurements, allowing the partial determination of the photonic band structure. This experimentally determined band structure agrees well with the outcome of three-dimensional optical finite-element simulations. A 16% photonic bandgap is predicted for an optimized geometry of the silicon nanodome arrays. By variation of the duration of the selective etching step, the geometry as well as the optical properties of the periodic silicon nanodome arrays can be controlled systematically. (paper)

  17. Disposable micro-fluidic biosensor array for online parallelized cell adhesion kinetics analysis on quartz crystal resonators

    DEFF Research Database (Denmark)

    Cama, G.; Jacobs, T.; Dimaki, Maria

    2010-01-01

    among all the sensors of the array. As well, dedicated sensor interface electronics were developed and optimized for fast spectra acquisition of all 16 QCRs with a miniaturized impedance analyzer. This allowed performing cell cultivation experiments for the observation of fast cellular reaction kinetics...

  18. Coupling in reflector arrays

    DEFF Research Database (Denmark)

    Appel-Hansen, Jørgen

    1968-01-01

    In order to reduce the space occupied by a reflector array, it is desirable to arrange the array antennas as close to each other as possible; however, in this case coupling between the array antennas will reduce the reflecting properties of the reflector array. The purpose of the present communic......In order to reduce the space occupied by a reflector array, it is desirable to arrange the array antennas as close to each other as possible; however, in this case coupling between the array antennas will reduce the reflecting properties of the reflector array. The purpose of the present...

  19. Improving solar-pumped laser efficiency by a ring-array concentrator

    Science.gov (United States)

    Tibúrcio, Bruno D.; Liang, Dawei; Almeida, Joana; Matos, Rodrigo; Vistas, Cláudia R.

    2018-01-01

    We report here a compact pumping scheme for achieving large improvement in collection and conversion efficiency of a Nd:YAG solar-pumped laser by an innovative ring-array solar concentrator. An aspheric fused silica lens was used to further concentrate the solar radiation from the focal region of the 1.5-m-diameter ring-array concentrator to a 5.0-mm-diameter, 20-mm-length Nd:YAG single-crystal rod within a conical-shaped pump cavity, enabling multipass pumping to the laser rod. 67.3-W continuous-wave solar laser power was numerically calculated, corresponding to 38.2-W / m2 solar laser collection efficiency, being 1.22 and 1.27 times more than the state-of-the-art records by both heliostat-parabolic mirror and Fresnel lens solar laser systems, respectively. 4.0% conversion efficiency and 0.021-W brightness figure of merit were also numerically obtained, corresponding to 1.25 and 1.62 times enhancement over the previous records, respectively. The influence of tracking error on solar laser output power was also analyzed.

  20. Development and testing of bio-inspired microelectromechanical pressure sensor arrays for increased situational awareness for marine vehicles

    International Nuclear Information System (INIS)

    Dusek, J; Triantafyllou, M S; Kottapalli, A G P; Asadnia, M; Miao, J; Woo, M E; Lang, J H

    2013-01-01

    The lateral line found on most species of fish is a sensory organ without analog in humans. Using sensory feedback from the lateral line, fish are able to track prey, school, avoid obstacles, and detect vortical flow structures. Composed of both a superficial component, and a component contained within canals beneath the fish’s skin, the lateral line acts in a similar fashion to an array of differential pressure sensors. In an effort to enhance the situational and environmental awareness of marine vehicles, lateral-line-inspired pressure sensor arrays were developed to mimic the enhanced sensory capabilities observed in fish. Three flexible and waterproof pressure sensor arrays were fabricated for use as a surface-mounted ‘smart skin’ on marine vehicles. Two of the sensor arrays were based around the use of commercially available piezoresistive sensor dies, with innovative packaging schemes to allow for flexibility and underwater operation. The sensor arrays employed liquid crystal polymer and flexible printed circuit board substrates with metallic circuits and silicone encapsulation. The third sensor array employed a novel nanocomposite material set that allowed for the fabrication of a completely flexible sensor array. All three sensors were surface mounted on the curved hull of an autonomous kayak vehicle, and tested in both pool and reservoir environments. Results demonstrated that all three sensors were operational while deployed on the autonomous vehicle, and provided an accurate means for monitoring the vehicle dynamics. (paper)

  1. Basic study of single crystal fibers of Pr:Lu3Al5O12 scintillator for gamma-ray imaging applications

    International Nuclear Information System (INIS)

    Yanagida, Takayuki; Kamada, Kei; Kawaguchi, Noriaki; Fujimoto, Yutaka; Fukuda, Kentaro; Yokota, Yuui; Chani, Valery; Yoshikawa, Akira

    2011-01-01

    Single-crystalline fibers were grown from 0.25, 0.70, and 1.50 mol% Pr-doped Lu 3 Al 5 O 12 (LuAG) melts by the micro-pulling down (μ-PD) method with a diameter of 0.3-0.5 mm and a length of about 200 mm. They were cut to 10 mm long specimens, and their scintillation properties, including light yield and decay time profile, were examined. These results were compared with corresponding properties of the specimens (0.8x0.8x10 mm 3 ) cut from the bulk crystals produced by conventional Czochralski (CZ) growth. The μ-PD-grown fibers demonstrated relatively low light yield and had the same decay time constant when compared with those of the samples cut from the CZ-grown crystals. The fiber crystals were used to assemble scintillating arrays with dimensions of O 0.5x10 mm 2 x20 pixels and O 0.3x10 mm 2 x30 pixels coated by a BaSO 4 reflector. After optical coupling with a position sensitive photomultiplier tube, the fiber-based arrays demonstrated acceptable imaging capability with a spatial resolution of about 0.5 mm.

  2. Wavelength shifter strips and G-APD arrays for the read-out of the z-coordinate in axial PET modules

    CERN Document Server

    Braem, André; Joram, C; Rudge, A; Séguinot, Jacques; Weilhammer, P; De Leo, R; Nappi, E; Lustermann, W; Schinzel, D; Johnson, I; Renker, D; Albrecht, S

    2008-01-01

    The measurements presented in this paper are related to the development of a PET camera based on a 3-D axial geometry with excellent 3-D spatial, timing and energy resolution. The detector modules consist of matrices of long axially oriented scintillation crystal bars, which are individually coupled to photodetectors. The axial coordinate is derived from wavelength shifting (WLS) plastic strips orthogonally interleaved between the crystal bars and readout by G-APD arrays. We report on results from measurements with two LYSO crystal bars, read with PMTs, and two WLS strips readout with G-APD devices from Hamamatsu (called MPPC). The WLS strips are positioned orthogonally underneath the LYSO bars. Yields of about 80 photoelectrons from the WLS strips for an energy deposition in the LYSO crystals equivalent to the absorption of 511 keV photons are observed. The axial coordinate in the LYSO bars is reconstructed with a precision of about 1.9 mm (FWHM) using a digital reconstruction method. The resolution of an an...

  3. A photonic crystal hydrogel suspension array for the capture of blood cells from whole blood

    Science.gov (United States)

    Zhang, Bin; Cai, Yunlang; Shang, Luoran; Wang, Huan; Cheng, Yao; Rong, Fei; Gu, Zhongze; Zhao, Yuanjin

    2016-02-01

    Diagnosing hematological disorders based on the separation and detection of cells in the patient's blood is a significant challenge. We have developed a novel barcode particle-based suspension array that can simultaneously capture and detect multiple types of blood cells. The barcode particles are polyacrylamide (PAAm) hydrogel inverse opal microcarriers with characteristic reflection peak codes that remain stable during cell capture on their surfaces. The hydrophilic PAAm hydrogel scaffolds of the barcode particles can entrap various plasma proteins to capture different cells in the blood, with little damage to captured cells.Diagnosing hematological disorders based on the separation and detection of cells in the patient's blood is a significant challenge. We have developed a novel barcode particle-based suspension array that can simultaneously capture and detect multiple types of blood cells. The barcode particles are polyacrylamide (PAAm) hydrogel inverse opal microcarriers with characteristic reflection peak codes that remain stable during cell capture on their surfaces. The hydrophilic PAAm hydrogel scaffolds of the barcode particles can entrap various plasma proteins to capture different cells in the blood, with little damage to captured cells. Electronic supplementary information (ESI) available. See DOI: 10.1039/c5nr06368j

  4. Tuning the Cavity Size and Chirality of Self-Assembling 3D DNA Crystals

    Energy Technology Data Exchange (ETDEWEB)

    Simmons, Chad R.; Zhang, Fei; MacCulloch, Tara; Fahmi, Noureddine; Stephanopoulos, Nicholas; Liu, Yan; Seeman, Nadrian C. [Department; Yan, Hao

    2017-08-02

    The foundational goal of structural DNA nanotechnology—the field that uses oligonucleotides as a molecular building block for the programmable self-assembly of nanostructured systems—was to use DNA to construct three-dimensional (3D) lattices for solving macromolecular structures. The programmable nature of DNA makes it an ideal system for rationally constructing self-assembled crystals and immobilizing guest molecules in a repeating 3D array through their specific stereospatial interactions with the scaffold. In this work, we have extended a previously described motif (4 × 5) by expanding the structure to a system that links four double-helical layers; we use a central weaving oligonucleotide containing a sequence of four six-base repeats (4 × 6), forming a matrix of layers that are organized and dictated by a series of Holliday junctions. In addition, we have assembled mirror image crystals (l-DNA) with the identical sequence that are completely resistant to nucleases. Bromine and selenium derivatives were obtained for the l- and d-DNA forms, respectively, allowing phase determination for both forms and solution of the resulting structures to 3.0 and 3.05 Å resolution. Both right- and left-handed forms crystallized in the trigonal space groups with mirror image 3-fold helical screw axes P32 and P31 for each motif, respectively. The structures reveal a highly organized array of discrete and well-defined cavities that are suitable for hosting guest molecules and allow us to dictate a priori the assembly of guest–DNA conjugates with a specified crystalline hand.

  5. Propagation of long-range surface plasmon polaritons in photonic crystals

    DEFF Research Database (Denmark)

    Boltasseva, Alexandra; Søndergaard, Thomas; Nikolajsen, T.

    2005-01-01

    We study the interaction of long-range surface plasmon polaritons (LR-SPPs), excited at telecommunication wavelengths, with photonic crystals (PCs) formed by periodic arrays of gold bumps that are arranged in a triangular lattice and placed symmetrically on both sides of a thin gold film embedded...... structures, is rather weak, so that the photonic bandgap effect might be expected to take place only for some particular propagation directions. Preliminary experiments on LR-SPP bending and splitting at large angles are reported, and further research directions are discussed....

  6. Concurrent array-based queue

    Science.gov (United States)

    Heidelberger, Philip; Steinmacher-Burow, Burkhard

    2015-01-06

    According to one embodiment, a method for implementing an array-based queue in memory of a memory system that includes a controller includes configuring, in the memory, metadata of the array-based queue. The configuring comprises defining, in metadata, an array start location in the memory for the array-based queue, defining, in the metadata, an array size for the array-based queue, defining, in the metadata, a queue top for the array-based queue and defining, in the metadata, a queue bottom for the array-based queue. The method also includes the controller serving a request for an operation on the queue, the request providing the location in the memory of the metadata of the queue.

  7. Wire number dependence of the implosion dynamics, stagnation, and radiation output of tungsten wire arrays at Z driver

    Energy Technology Data Exchange (ETDEWEB)

    Mazarakis, Michael G.; Stygar, William A.; Sinars, Daniel B.; Cuneo, Michael E.; Nash, Thomas J.; Chandler, Gordon A.; Keith Matzen, M.; Porter, John L.; Struve, Kenneth W.; McDaniel, Dillon H. [Sandia National Laboratories, P.O. Box 5800, Albuquerque, New Mexico 87185 (United States); Deeney, Christopher E. [National Nuclear Security Administration, Washington, D.C. 20585 (United States); Douglas, Melissa R. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Chittenden, Jerry [Imperial College, London, SW and 2BW (United Kingdom)

    2011-11-15

    We report results of the experimental campaign, which studied the initiation, implosion dynamics, and radiation yield of tungsten wire arrays as a function of the wire number. The wire array dimensions and mass were those of interest for the Z-pinch driven Inertial Confinement Fusion (ICF) program. An optimization study of the x-ray emitted peak power, rise time, and full width at half maximum was effectuated by varying the wire number while keeping the total array mass constant and equal to {approx}5.8 mg. The driver utilized was the {approx}20-MA Z accelerator before refurbishment in its usual short pulse mode of 100 ns. We studied single arrays of 20-mm diameter and 1-cm height. The smaller wire number studied was 30 and the largest 600. It appears that 600 is the highest achievable wire number with present day's technology. Radial and axial diagnostics were utilized including crystal monochromatic x-ray backlighter. An optimum wire number of {approx}375 was observed which was very close to the routinely utilized 300 for the ICF program in Sandia.

  8. Wire number dependence of the implosion dynamics, stagnation, and radiation output of tungsten wire arrays at Z driver

    International Nuclear Information System (INIS)

    Mazarakis, Michael G.; Stygar, William A.; Sinars, Daniel B.; Cuneo, Michael E.; Nash, Thomas J.; Chandler, Gordon A.; Keith Matzen, M.; Porter, John L.; Struve, Kenneth W.; McDaniel, Dillon H.; Deeney, Christopher E.; Douglas, Melissa R.; Chittenden, Jerry

    2011-01-01

    We report results of the experimental campaign, which studied the initiation, implosion dynamics, and radiation yield of tungsten wire arrays as a function of the wire number. The wire array dimensions and mass were those of interest for the Z-pinch driven Inertial Confinement Fusion (ICF) program. An optimization study of the x-ray emitted peak power, rise time, and full width at half maximum was effectuated by varying the wire number while keeping the total array mass constant and equal to ∼5.8 mg. The driver utilized was the ∼20-MA Z accelerator before refurbishment in its usual short pulse mode of 100 ns. We studied single arrays of 20-mm diameter and 1-cm height. The smaller wire number studied was 30 and the largest 600. It appears that 600 is the highest achievable wire number with present day's technology. Radial and axial diagnostics were utilized including crystal monochromatic x-ray backlighter. An optimum wire number of ∼375 was observed which was very close to the routinely utilized 300 for the ICF program in Sandia.

  9. Characterization studies of Silicon Photomultipliers and crystals matrices for a novel time of flight PET detector

    CERN Document Server

    Auffray, Etiennette; Cortinovis, Daniele; Doroud, Katayoun; Garutti, Erika; Lecoq, Paul; Liu, Zheng; Martinez, Rosana; Paganoni, Marco; Pizzichemi, Marco; Silenzi, Alessandro; Xu, Chen; Zvolský, Milan

    2015-01-01

    This paper describes the characterization of crystal matrices and silicon photomultiplier arrays for a novel Positron Emission Tomography (PET) detector, namely the external plate of the EndoTOFPET-US system. The EndoTOFPET-US collaboration aims to integrate Time-Of-Flight PET with ultrasound endoscopy in a novel multimodal device, capable to support the development of new biomarkers for prostate and pancreatic tumors. The detector consists in two parts: a PET head mounted on an ultrasound probe and an external PET plate. The challenging goal of 1 mm spatial resolution for the PET image requires a detector with small crystal size, and therefore high channel density: 4096 LYSO crystals individually readout by Silicon Photomultipliers (SiPM) make up the external plate. The quality and properties of these components must be assessed before the assembly. The dark count rate, gain, breakdown voltage and correlated noise of the SiPMs are measured, while the LYSO crystals are evaluated in terms of light yield and en...

  10. Readout and characterisation of new silicon pixel photodiode array for use in PET

    International Nuclear Information System (INIS)

    Hooper, P.; Ward, G.; Lerch, R.; Rozenfeld, A.

    2002-01-01

    Full text: Positron emission tomography (PET) is a functional imaging tool, which is able to quantify physiological, and biochemical processes in vivo using short-lived cyclotron-produced radiotracers. The main physical principle of PET is the simultaneous measurement of two 511 keV photons which are emitted in opposite directions following the annihilation of a positron in tissue. The accuracy of tracking these photons determines the accuracy of localising the radiotracer in the body, which is referred to as the spatial resolution of the system. Compared with conventional single photon imaging with gamma cameras, PET provides superior spatial resolution and sensitivity. However, compared with anatomical imaging techniques, the spatial resolution remains relatively poor at approximately 4-6 mm full width at half maximum (FWHM), compared with 1 mm FWHM for MRI. The Centre for Medical Radiation Physics at the University of Wollongong is developing a new Positron Emission Tomography (PET) detection sub-module that will significantly improve the spatial resolution of PET. The new sub-module design is simple and robust to minimise module assembly complications and is completely independent of photomultiplier tubes. The new sub-module has also been designed to maximise its flexibility for easy sub-module coupling so as to form a complete, customised, detection module to be used in PET scanners dedicated to human brain and breast, and small animal studies. A new computer controlled gantry allows the system to be used for PET and SPECT applications. Silicon 8x8 detector arrays have been developed by CMRP and will be optically coupled scintillation crystals and readout using the VIKING tM hybrid preamplifier chip to form the basis of the new module Characterisation of the pixel photodiode array has been performed to check the uniformity of the response of the array. This characterisation has been done using a pulsed, near infra-red laser diode system and alpha particles

  11. Structural coloration of chitosan-cationized cotton fabric using photonic crystals

    Science.gov (United States)

    Yavuz, G.; Zille, A.; Seventekin, N.; Souto, A. P.

    2017-10-01

    In this work, poly (styrene-methyl methacrylate-acrylic acid) P(St-MMA-AA) composite nanospheres were deposited onto chitosan-cationized woven cotton fabrics followed by a second layer of chitosan. The deposited photonic crystals (PCs) on the fabrics were evaluated for coating efficiency and resistance, chemical analysis and color variation by optical and SEM microscopy, ATR-FTIR, diffuse reflectance spectroscopy and washing fastness. Chitosan deposition on cotton fabric provided cationic groups on the fiber surface promoting electrostatic interaction with photonic crystals. SEM images of the washed samples indicate that the PCs are firmly coated on the cotton surface only in the chitosan treated sample. The photonic nanospheres show an average diameter of 280 nm and display a face-centered cubic closepacking structure with an average thickness of 10 μm. A further chitosan post-treatment enhances color yield of the samples due to the chitosan transparent covering layer that induce bright reflections where the angles of incidence and reflection are the same. After washing, no photonic crystal can be detected on control fabric surface. However, the sample that received a chitosan post-treatment showed a good washing fastness maintaining a reasonable degree of iridescence. Chitosan fills the spaces between the polymer spheres in the matrix stabilizing the photonic structure. Sizeable variations in lattice spacing will allow color variations using more flexible non-close-packed photonic crystal arrays in chitosan hydrogels matrices.

  12. A semi-Dirac point and an electromagnetic topological transition in a dielectric photonic crystal

    KAUST Repository

    Wu, Ying

    2014-01-01

    Accidental degeneracy in a photonic crystal consisting of a square array of elliptical dielectric cylinders leads to both a semi-Dirac point at the center of the Brillouin zone and an electromagnetic topological transition (ETT). A perturbation method is deduced to affirm the peculiar linear-parabolic dispersion near the semi-Dirac point. An effective medium theory is developed to explain the simultaneous semi-Dirac point and ETT and to show that the photonic crystal is either a zero-refractive-index material or an epsilon-near-zero material at the semi-Dirac point. Drastic changes in the wave manipulation properties at the semi-Dirac point, resulting from ETT, are described.©2014 Optical Society of America.

  13. High resolution phoswich gamma-ray imager utilizing monolithic MPPC arrays with submillimeter pixelized crystals

    International Nuclear Information System (INIS)

    Kato, T; Kataoka, J; Nakamori, T; Kishimoto, A; Yamamoto, S; Sato, K; Ishikawa, Y; Yamamura, K; Kawabata, N; Ikeda, H; Kamada, K

    2013-01-01

    We report the development of a high spatial resolution tweezers-type coincidence gamma-ray camera for medical imaging. This application consists of large-area monolithic Multi-Pixel Photon Counters (MPPCs) and submillimeter pixelized scintillator matrices. The MPPC array has 4 × 4 channels with a three-side buttable, very compact package. For typical operational gain of 7.5 × 10 5 at + 20 °C, gain fluctuation over the entire MPPC device is only ± 5.6%, and dark count rates (as measured at the 1 p.e. level) amount to ≤ 400 kcps per channel. We selected Ce-doped (Lu,Y) 2 (SiO 4 )O (Ce:LYSO) and a brand-new scintillator, Ce-doped Gd 3 Al 2 Ga 3 O 12 (Ce:GAGG) due to their high light yield and density. To improve the spatial resolution, these scintillators were fabricated into 15 × 15 matrices of 0.5 × 0.5 mm 2 pixels. The Ce:LYSO and Ce:GAGG scintillator matrices were assembled into phosphor sandwich (phoswich) detectors, and then coupled to the MPPC array along with an acrylic light guide measuring 1 mm thick, and with summing operational amplifiers that compile the signals into four position-encoded analog outputs being used for signal readout. Spatial resolution of 1.1 mm was achieved with the coincidence imaging system using a 22 Na point source. These results suggest that the gamma-ray imagers offer excellent potential for applications in high spatial medical imaging.

  14. Self-assembly of charged microclusters of CdSe/ZnS core/shell nanodots and nanorods into hierarchically ordered colloidal arrays

    International Nuclear Information System (INIS)

    Sukhanova, Alyona; Baranov, Alexander V; Klinov, Dmitriy; Oleinikov, Vladimir; Berwick, Kevin; Cohen, Jacques H M; Pluot, Michel; Nabiev, Igor

    2006-01-01

    A thermodynamically driven self-organization of microclusters of semiconductor nanocrystals with a narrow size distribution into periodic two-dimensional (2D) arrays is an attractive low-cost technique for the fabrication of 2D photonic crystals. We have found that CdSe/ZnS core/shell quantum dots or quantum rods, transferred in aqueous phase after capping with the bifunctional surface-active agent DL-cysteine, form on a poly-L-lysine coated surface homogeneously sized micro-particles, droplet-like spheroid clusters and hexagon-like colloidal crystals self-organized into millimetre-sized 2D hexagonal assemblies. The presence of an organic molecular layer around the micro-particles prevents immediate contact between them, forming an interstitial space which may be varied in thickness by changing the origin of the molecular layer capping nanocrystals. Due to the high refractive index of CdSe and the low refractive index of the interstitial spaces, these structures are expected to have deep gaps in their photonic band, forming hierarchically ordered 2D arrays of potentially photonic materials

  15. Programmable cellular arrays. Faults testing and correcting in cellular arrays

    International Nuclear Information System (INIS)

    Cercel, L.

    1978-03-01

    A review of some recent researches about programmable cellular arrays in computing and digital processing of information systems is presented, and includes both combinational and sequential arrays, with full arbitrary behaviour, or which can realize better implementations of specialized blocks as: arithmetic units, counters, comparators, control systems, memory blocks, etc. Also, the paper presents applications of cellular arrays in microprogramming, in implementing of a specialized computer for matrix operations, in modeling of universal computing systems. The last section deals with problems of fault testing and correcting in cellular arrays. (author)

  16. A Novel Self-aligned and Maskless Process for Formation of Highly Uniform Arrays of Nanoholes and Nanopillars

    Directory of Open Access Journals (Sweden)

    Wu Wei

    2008-01-01

    Full Text Available AbstractFabrication of a large area of periodic structures with deep sub-wavelength features is required in many applications such as solar cells, photonic crystals, and artificial kidneys. We present a low-cost and high-throughput process for realization of 2D arrays of deep sub-wavelength features using a self-assembled monolayer of hexagonally close packed (HCP silica and polystyrene microspheres. This method utilizes the microspheres as super-lenses to fabricate nanohole and pillar arrays over large areas on conventional positive and negative photoresist, and with a high aspect ratio. The period and diameter of the holes and pillars formed with this technique can be controlled precisely and independently. We demonstrate that the method can produce HCP arrays of hole of sub-250 nm size using a conventional photolithography system with a broadband UV source centered at 400 nm. We also present our 3D FDTD modeling, which shows a good agreement with the experimental results.

  17. Electrically Tunable Reflective Terahertz Phase Shifter Based on Liquid Crystal

    Science.gov (United States)

    Yang, Jun; Xia, Tianyu; Jing, Shuaicheng; Deng, Guangsheng; Lu, Hongbo; Fang, Yong; Yin, Zhiping

    2018-02-01

    We present a reflective spatial phase shifter which operates at terahertz regime above 325 GHz. The controllable permittivity of the nematic liquid crystals was utilized to realize a tunable terahertz (THz) reflective phase shifter. The reflective characteristics of the terahertz electromagnetic waves and the liquid crystal parameters were calculated and analyzed. We provide the simulation results for the effect of the incident angle of the plane wave on the reflection. The experiment was carried out considering an array consisting of 30 × 30 patch elements, printed on a 20 × 20 mm quartz substrate with 1-mm thickness. The phase shifter provides a tunable phase range of 300° over the frequency range of 325 to 337.6 GHz. The maximum phase shift of 331° is achieved at 330 GHz. The proposed phase shifter is a potential candidate for THz applications, particularly for reconfigurable reflectarrays.

  18. Low temperature preparation of Ag-doped ZnO nanowire arrays for sensor and light-emitting diode applications

    Science.gov (United States)

    Lupan, O.; Viana, B.; Cretu, V.; Postica, V.; Adelung, R.; Pauporté, T.

    2016-02-01

    Transition metal doped-oxide semiconductor nanostructures are important to achieve enhanced and new properties for advanced applications. We describe the low temperature preparation of ZnO:Ag nanowire/nanorod (NW/NR) arrays by electrodeposition at 90 °C. The NWs have been characterized by SEM, EDX, transmittance and photoluminescence (PL) measurements. The integration of Ag in the crystal is shown. Single nanowire/nanorod of ZnO:Ag was integrated in a nanosensor structure leading to new and enhanced properties. The ultraviolet (UV) response of the nanosensor was investigated at room temperature. Experimental results indicate that ZnO:Ag (0.75 μM) nanosensor possesses faster response/recovery time and better response to UV light than those reported in literature. The sensor structure has been also shown to give a fast response for the hydrogen detection with improved performances compared to pristine ZnO NWs. ZnO:Ag nanowire/nanorod arrays electrochemically grown on p-type GaN single crystal layer is also shown to act as light emitter in LED structures. The emission wavelength is red-shifted compared to pristine ZnO NW array. At low Ag concentration a single UV-blue emission is found whereas at higher concentration of dopant the emission is broadened and extends up to the red wavelength range. Our study indicates that high quality ZnO:Ag NW/NR prepared at low temperature by electrodeposition can serve as building nanomaterials for new sensors and light emitting diodes (LEDs) structures with low-power consumption.

  19. Use of a low energy proton accelerator for calibrating a large NaI(Tl) array in a high energy physics experiment

    International Nuclear Information System (INIS)

    Kirkbride, G.I.; O'Reilly, J.G.; Tompkins, J.C.

    1978-01-01

    The use of a 500 keV Van de Graaff proton accelerator to produce γ-rays in the range 4 - 18 MeV via nuclear reactions for the purpose of calibrating a large NaI(Tl) crystal array is reported. Data analysis indicates an energy calibration to approx. 1% over this range

  20. The crystal zero degree detector for ISR tagging at BES III

    Energy Technology Data Exchange (ETDEWEB)

    Denig, Achim; Redmer, Christoph [Johannes Gutenberg Universitaet Mainz (Germany); Koch, Leonard; Kuehn, Wolfgang; Lange, Soeren; Liang, Yutie; Wagner, Milan [Justus-Liebig-Universitaet Giessen (Germany); Collaboration: BESIII-Collaboration

    2016-07-01

    The BES III experiment at the BEPCII electron positron collider in Beijing is collecting data in the charm-τ mass region. Being strongly peaked towards small polar angles, photons from initial state radiation (ISR) are detected with limited efficiency. In order to increase the detection efficiency of these photons, we propose a small detector comprised of two arrays of scintillating crystals separated by a small gap to be placed in the very forward and backward region. The crystals will be read out by SiPMs and the signal will be digitized by a feature extracting flash ADC. This data stream is correlated with the BESIII trigger in realtime on FPGA based hardware. The detectors response has been simulated using GEANT4 and the energy resolution has been obtained. A beam test of a prototype has demonstrated the stably running of the DAQ.

  1. Methods for growth of relatively large step-free SiC crystal surfaces

    Science.gov (United States)

    Neudeck, Philip G. (Inventor); Powell, J. Anthony (Inventor)

    2002-01-01

    A method for growing arrays of large-area device-size films of step-free (i.e., atomically flat) SiC surfaces for semiconductor electronic device applications is disclosed. This method utilizes a lateral growth process that better overcomes the effect of extended defects in the seed crystal substrate that limited the obtainable step-free area achievable by prior art processes. The step-free SiC surface is particularly suited for the heteroepitaxial growth of 3C (cubic) SiC, AlN, and GaN films used for the fabrication of both surface-sensitive devices (i.e., surface channel field effect transistors such as HEMT's and MOSFET's) as well as high-electric field devices (pn diodes and other solid-state power switching devices) that are sensitive to extended crystal defects.

  2. Integration of the GET electronics for the CHIMERA and FARCOS devices

    Science.gov (United States)

    De Filippo, E.; Acosta, L.; Auditore, L.; Boiano, C.; Cardella, G.; Castoldi, A.; D’Andrea, M.; De Luca, S.; Favela, F.; Fichera, F.; Giudice, N.; Gnoffo, B.; Grimaldi, A.; Guazzoni, C.; Lanzalone, G.; Librizzi, F.; Litrico, P.; Maiolino, C.; Maffesanti, S.; Martorana, NS; Pagano, A.; Pagano, EV; Papa, M.; Parsani, T.; Passaro, G.; Pirrone, S.; Politi, G.; Previdi, F.; Quattrocchi, L.; Rizzo, F.; Russotto, P.; Saccà, G.; Salemi, G.; Sciliberto, D.; Trifirò, A.; Trimarchi, M.

    2018-05-01

    A new front-end based on digital GET electronics has been adopted for the readout of the CsI(Tl) detectors of the CHIMERA 4π multi-detector and for the new modular Femtoscopy Array for Correlation and Spectroscopy (FARCOS). It is expected that the coupling of CHIMERA with the FARCOS array, featuring high angular and energy resolution, and the adoption of the new digital electronics will be well suited for improving specific future data analysis, with the full shape storage of the signals, in the field of heavy ion reactions with stable and exotic beams around the Fermi energies domain. Integration of the GET electronics with CHIMERA and FARCOS devices and with the local analog data acquisition will be briefly discussed. We present some results from previous experimental tests and from the first in-beam experiment (Hoyle-Gamma) with the coupled GET+CHIMERA data acquisition.

  3. Fabrication and optical properties of TiO sub 2 nanowire arrays made by sol-gel electrophoresis deposition into anodic alumina membranes

    CERN Document Server

    Lin, Y; Yuan, X Y; Xie, T; Zhang, L D

    2003-01-01

    Ordered TiO sub 2 nanowire arrays have been successfully fabricated into the nanochannels of a porous anodic alumina membrane by sol-gel electrophoretic deposition. After annealing at 500 deg. C, the TiO sub 2 nanowire arrays and the individual nanowires were characterized using scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and x-ray diffraction (XRD). SEM and TEM images show that these nanowires are dense and continuous with a uniform diameter throughout their entire length. XRD and SAED analysis together indicate that these TiO sub 2 nanowires crystallize in the anatase polycrystalline structure. The optical absorption band edge of TiO sub 2 nanowire arrays exhibits a blue shift with respect of that of the bulk TiO sub 2 owing to the quantum size effect.

  4. INFLUENCE OF IONIZING IRRADIATION ON THE PARAMETERS OF ZN NANOTUBES ARRAYS FOR DESIGN OF FLEXIBLE ELECTRONICS ELEMENTS

    Directory of Open Access Journals (Sweden)

    D. B. Kadyrzhanov

    2018-01-01

    Full Text Available The aim of the study is establishing the possibility of using Zn nanotube arrays as a basis for design compact and lightweight elements of flexible electronics, including operating under influence of ionizing irradiation.The paper presents the results of the synthesis of Zn nanotubes obtained by electrochemical deposition in the pores of polymer matrices and the study of their structural and electrophysical properties after directional modification by ionizing radiation with different doses. Using the methods of scanning electron microscopy, X-ray diffraction and energy dispersive analysis, the structure of nanotubes having a polycrystalline structure and completely consisting of zinc was studied and it was demonstrated that irradiation with Ar8+ ions with a dose from 1 × 109 to 5 × 1011 ion/cm2 and energy 1.75 MeV/nucleon has an effect on the crystal structure of nanotubes.At high doses, localized highly defect zones arise, leading to a critical change in the structure and physical properties of the nanotubes, respectively. It is shown that the consequence of the modification of the crystal structure is a change in the electrical conductivity of nanotubes: at low doses the electrical conductivity increases, but when the threshold value is reached, it sharply decreases. The change in the crystal structure and the corresponding changes in the conductive properties of Zn nanotubes due to irradiation determine the mechanism of ionizing radiation influence on nanomaterials and determine the possibility of using Zn nanotubes arrays as a basis for creating compact and lightweight elements of flexible electronics.

  5. Collective electronic excitations in C60 crystals

    International Nuclear Information System (INIS)

    Wu, X.; Ulloa, S.E.

    1994-01-01

    We present a theoretical study of the electronic excitations in fullerene crystals by calculating the density-density correlation function in a fully nonlocal linear response theory. Our results indicate that the collective features associates with the π→π * transitions show strong anisotropic properties, with peaks changing by as much as 0.7 eV in different directions. Meanwhile, the calculated mode dispersion exhibits rather weak wave-number dependence along a given direction, in general agreement with experimental results. The oscillator strength also shows anisotropic behavior, with significant weight redistribution for different directions. We also analyze this system in terms of a classical point-dipole array model, and show that this simple model approximates well the quantum results

  6. Convolving optically addressed VLSI liquid crystal SLM

    Science.gov (United States)

    Jared, David A.; Stirk, Charles W.

    1994-03-01

    We designed, fabricated, and tested an optically addressed spatial light modulator (SLM) that performs a 3 X 3 kernel image convolution using ferroelectric liquid crystal on VLSI technology. The chip contains a 16 X 16 array of current-mirror-based convolvers with a fixed kernel for finding edges. The pixels are located on 75 micron centers, and the modulators are 20 microns on a side. The array successfully enhanced edges in illumination patterns. We developed a high-level simulation tool (CON) for analyzing the performance of convolving SLM designs. CON has a graphical interface and simulates SLM functions using SPICE-like device models. The user specifies the pixel function along with the device parameters and nonuniformities. We discovered through analysis, simulation and experiment that the operation of current-mirror-based convolver pixels is degraded at low light levels by the variation of transistor threshold voltages inherent to CMOS chips. To function acceptable, the test SLM required the input image to have an minimum irradiance of 10 (mu) W/cm2. The minimum required irradiance can be further reduced by adding a photodarlington near the photodetector or by increasing the size of the transistors used to calculate the convolution.

  7. X-ray crystal spectroscopy of JET - a design study

    International Nuclear Information System (INIS)

    Bateman, J.E.; Hobby, M.G.; Peacock, N.J.

    1980-02-01

    This study describes the design and specification of a diagnostic system to measure the space- and time-resolved x-ray spectrum from JET discharges with high-resolution crystal spectrometers operating in the wavelength region 1 - 15A. The specification is given in terms of sensitivity, resolving power, detector, and data handling requirements, special attention being given to the problems encountered in interfacing the spectrometer arrays to the torus vacuum system and in their disposition to the machine. Shielding requirements during the active mode are evaluated and a staged diagnostic is proposed to accommodate D - T operation. (U.K.)

  8. Ag nanoparticles-decorated ZnO nanorod array on a mechanical flexible substrate with enhanced optical and antimicrobial properties

    Science.gov (United States)

    Chen, Yi; Tse, Wai Hei; Chen, Longyan; Zhang, Jin

    2015-03-01

    Heteronanostructured zinc oxide nanorod (ZnO NR) array are vertically grown on polydimethylsiloxane (PDMS) through a hydrothermal method followed by an in situ deposition of silver nanoparticles (Ag NPs) through a photoreduction process. The Ag-ZnO heterostructured nanorods on PDMS are measured with an average diameter of 160 nm and an average length of 2 μm. ZnO NRs measured by high-resolution transmission electron microscope (HRTEM) shows highly crystalline with a lattice fringe of 0.255 nm, which corresponds to the (0002) planes in ZnO crystal lattice. The average diameter of the Ag NPs in situ deposited on the ZnO NRs is estimated at 22 ± 2 nm. As compared to the bare ZnO NRs, the heterostructured Ag-ZnO nanorod array shows enhanced ultraviolet (UV) absorption at 440 nm, and significant emission in the visible region (λem = 542 nm). In addition, the antimicrobial efficiency of Ag-ZnO heterostructured nanorod array shows obvious improvement as compared to bare ZnO nanorod array. The cytotoxicity of ZnO nanorod array with and without Ag NPs was studied by using 3 T3 mouse fibroblast cell line. No significant toxic effect is imposed on the cells.

  9. Determining ice water content from 2D crystal images in convective cloud systems

    Science.gov (United States)

    Leroy, Delphine; Coutris, Pierre; Fontaine, Emmanuel; Schwarzenboeck, Alfons; Strapp, J. Walter

    2016-04-01

    Cloud microphysical in-situ instrumentation measures bulk parameters like total water content (TWC) and/or derives particle size distributions (PSD) (utilizing optical spectrometers and optical array probes (OAP)). The goal of this work is to introduce a comprehensive methodology to compute TWC from OAP measurements, based on the dataset collected during recent HAIC (High Altitude Ice Crystals)/HIWC (High Ice Water Content) field campaigns. Indeed, the HAIC/HIWC field campaigns in Darwin (2014) and Cayenne (2015) provide a unique opportunity to explore the complex relationship between cloud particle mass and size in ice crystal environments. Numerous mesoscale convective systems (MCSs) were sampled with the French Falcon 20 research aircraft at different temperature levels from -10°C up to 50°C. The aircraft instrumentation included an IKP-2 (isokinetic probe) to get reliable measurements of TWC and the optical array probes 2D-S and PIP recording images over the entire ice crystal size range. Based on the known principle relating crystal mass and size with a power law (m=α•Dβ), Fontaine et al. (2014) performed extended 3D crystal simulations and thereby demonstrated that it is possible to estimate the value of the exponent β from OAP data, by analyzing the surface-size relationship for the 2D images as a function of time. Leroy et al. (2015) proposed an extended version of this method that produces estimates of β from the analysis of both the surface-size and perimeter-size relationships. Knowing the value of β, α then is deduced from the simultaneous IKP-2 TWC measurements for the entire HAIC/HIWC dataset. The statistical analysis of α and β values for the HAIC/HIWC dataset firstly shows that α is closely linked to β and that this link changes with temperature. From these trends, a generalized parameterization for α is proposed. Finally, the comparison with the initial IKP-2 measurements demonstrates that the method is able to predict TWC values

  10. Preventing Crystal Agglomeration of Pharmaceutical Crystals Using Temperature Cycling and a Novel Membrane Crystallization Procedure for Seed Crystal Generation

    Directory of Open Access Journals (Sweden)

    Elena Simone

    2018-01-01

    Full Text Available In this work, a novel membrane crystallization system was used to crystallize micro-sized seeds of piroxicam monohydrate by reverse antisolvent addition. Membrane crystallization seeds were compared with seeds produced by conventional antisolvent addition and polymorphic transformation of a fine powdered sample of piroxicam form I in water. The membrane crystallization process allowed for a consistent production of pure monohydrate crystals with narrow size distribution and without significant agglomeration. The seeds were grown in 350 g of 20:80 w/w acetone-water mixture. Different seeding loads were tested and temperature cycling was applied in order to avoid agglomeration of the growing crystals during the process. Focused beam reflectance measurement (FBRM; and particle vision and measurement (PVM were used to monitor crystal growth; nucleation and agglomeration during the seeded experiments. Furthermore; Raman spectroscopy was used to monitor solute concentration and estimate the overall yield of the process. Membrane crystallization was proved to be the most convenient and consistent method to produce seeds of highly agglomerating compounds; which can be grown via cooling crystallization and temperature cycling.

  11. Optical studies of metallo-dielectric photonic crystals

    Science.gov (United States)

    Kamaev, Vladimir

    2007-12-01

    Metallo-dielectric photonic crystals (MDPCs) are characterized by a large difference between the dielectric constants of the constituents. Owing to their high DC conductivity a broad omnidirectional band gap is formed at low frequencies. At the same time there exist numerous propagating electromagnetic modes at frequencies above a cutoff. This gives a possibility of creating a "transparent" metal: a crystal transparent in the visible spectral range and simultaneously having high DC conductivity. Since the cutoff wavelength linearly scales with the crystal periodicity, in order to make an MDPC with propagating modes in the visible range the crystal periodicity has to be around a quarter micrometer. Fabrication of such a crystal is a challenging task. One of the feasible choices is natural or artificial opals, structures made of silica balls arranged into a close packed fcc lattice. The ball diameters could vary from 200 nm to several microns, allowing the desired optical features to be in the visible spectral range. In the present work we studied metal-infiltrated opals numerically, analytically, and experimentally (Chapters 1 and 4). Both theory and experiment revealed high reflectance of the samples at large wavelengths associated with the low frequency metallic band gap formation, and low reflectance at short wavelengths that has characteristic wiggles. Contrarily, the absorbance is low in the IR region and goes up towards the UV end, which is due to low group velocity of light and high metal absorption in the region. Numerical analysis of thin metal-infiltrated opals (˜3-5 layers) did show a transmission peak around the first reflectance minimum and cutoff frequency. In Chapter 5 we present transmission experiments on thin metal films perforated with periodic arrays of holes or deposited on an opal monolayer. Both types of 2D MDPCs exhibited anomalous transmission peaks associated with surface plasma excitations. It was shown that the phenomenon could be

  12. Wave Propagation From Electrons to Photonic Crystals and Left-Handed Materials

    CERN Document Server

    Markos, Peter

    2010-01-01

    This textbook offers the first unified treatment of wave propagation in electronic and electromagnetic systems and introduces readers to the essentials of the transfer matrix method, a powerful analytical tool that can be used to model and study an array of problems pertaining to wave propagation in electrons and photons. It is aimed at graduate and advanced undergraduate students in physics, materials science, electrical and computer engineering, and mathematics, and is ideal for researchers in photonic crystals, negative index materials, left-handed materials, plasmonics, nonlinear effects,

  13. Developing 1D nanostructure arrays for future nanophotonics

    Directory of Open Access Journals (Sweden)

    Cooke DG

    2006-01-01

    Full Text Available AbstractThere is intense and growing interest in one-dimensional (1-D nanostructures from the perspective of their synthesis and unique properties, especially with respect to their excellent optical response and an ability to form heterostructures. This review discusses alternative approaches to preparation and organization of such structures, and their potential properties. In particular, molecular-scale printing is highlighted as a method for creating organized pre-cursor structure for locating nanowires, as well as vapor–liquid–solid (VLS templated growth using nano-channel alumina (NCA, and deposition of 1-D structures with glancing angle deposition (GLAD. As regards novel optical properties, we discuss as an example, finite size photonic crystal cavity structures formed from such nanostructure arrays possessing highQand small mode volume, and being ideal for developing future nanolasers.

  14. Application of the ultrasonic phased array technique to alloy 182 weld inspection in PWR

    International Nuclear Information System (INIS)

    Hsiao, Chu Chung; Shie, Namg Chian; Chu, Shyr Liang; Lee, Sou See; Toung, Jean Chung; Su, Liang Chun; Yang, Hai Ming

    2006-01-01

    Cracks were found in nickel-based welds frequently in some nuclear power plants. The development of inspection technique capability of finding these cracks is thus in great demand. The difficulties of inspection and evaluation for nickel-based welds include ultrasonic reflection of interface of dissimilar materials, ultrasonic distortion of anisotropic microstructure, and signal-to-noise ratio reduction of coarse grain. In this study, an Alloy 182 mock-up with the same size and material properties as in the field is designed and fabricated. The Alloy 182 mock-up specimen contains various cracks and notches for calibration. Phased array UT and other ultrasonic inspection techniques are used in this study. Based on the experiment results, the phased array probe with 2D dual crystals and low frequency (1.5MHz) longitudinal wave is found to perform well. Finally, phased array ultrasonic testing technique has been approved to be an effectively nondestructive test method for DMW with real size testing block involved. Typically, phased array probe can generate sharp tip diffraction signal and thus reliable and accurate result can be obtained for sizing the defect. Furthermore, phased array probe can also generate various angles and focal lengths and thus combinatorial effect can be achieved for several traditional probes. With a full understanding of the beam behavior and an optimized delay laws, the phased away ultrasonic technique integrated with an automatic scanner will achieve not only to save scanning time but also to reduce the amount of radiation exposure on field inspection.

  15. Cyclotron-Resonance-Maser Arrays

    International Nuclear Information System (INIS)

    Kesar, A.; Lei, L.; Dikhtyar, V.; Korol, M.; Jerby, E.

    1999-01-01

    The cyclotron-resonance-maser (CRM) array [1] is a radiation source which consists of CRM elements coupled together under a common magnetic field. Each CRM-element employs a low-energy electron-beam which performs a cyclotron interaction with the local electromagnetic wave. These waves can be coupled together among the CRM elements, hence the interaction is coherently synchronized in the entire array. The implementation of the CRM-array approach may alleviate several technological difficulties which impede the development of single-beam gyro-devices. Furthermore, it proposes new features, such as the phased-array antenna incorporated in the CRM-array itself. The CRM-array studies may lead to the development of compact, high-power radiation sources operating at low-voltages. This paper introduces new conceptual schemes of CRM-arrays, and presents the progress in related theoretical and experimental studies in our laboratory. These include a multi-mode analysis of a CRM-array, and a first operation of this device with five carbon-fiber cathodes

  16. The Role of Coulomb Interactions for Spin Crossover Behaviors and Crystal Structural Transformation in Novel Anionic Fe(III Complexes from a π-Extended ONO Ligand

    Directory of Open Access Journals (Sweden)

    Suguru Murata

    2016-05-01

    Full Text Available To investigate the π-extension effect on an unusual negative-charged spin crossover (SCO FeIII complex with a weak N2O4 first coordination sphere, we designed and synthesized a series of anionic FeIII complexes from a π-extended naphthalene derivative ligand. Acetonitrile-solvate tetramethylammonium (TMA salt 1 exhibited an SCO conversion, while acetone-solvate TMA salt 2 was in a high-spin state. The crystal structural analysis for 2 revealed that two-leg ladder-like cation-anion arrays derived from π-stacking interactions between π-ligands of the FeIII complex anion and Coulomb interactions were found and the solvated acetone molecules were in one-dimensional channels between the cation-anion arrays. A desolvation-induced single-crystal-to-single-crystal transformation to desolvate compound 2’ may be driven by Coulomb energy gain. Furthermore, the structural comparison between quasi-polymorphic compounds 1 and 2 revealed that the synergy between Coulomb and π-stacking interactions induces a significant distortion of coordination structure of 2.

  17. Degree-of-Freedom Strengthened Cascade Array for DOD-DOA Estimation in MIMO Array Systems.

    Science.gov (United States)

    Yao, Bobin; Dong, Zhi; Zhang, Weile; Wang, Wei; Wu, Qisheng

    2018-05-14

    In spatial spectrum estimation, difference co-array can provide extra degrees-of-freedom (DOFs) for promoting parameter identifiability and parameter estimation accuracy. For the sake of acquiring as more DOFs as possible with a given number of physical sensors, we herein design a novel sensor array geometry named cascade array. This structure is generated by systematically connecting a uniform linear array (ULA) and a non-uniform linear array, and can provide more DOFs than some exist array structures but less than the upper-bound indicated by minimum redundant array (MRA). We further apply this cascade array into multiple input multiple output (MIMO) array systems, and propose a novel joint direction of departure (DOD) and direction of arrival (DOA) estimation algorithm, which is based on a reduced-dimensional weighted subspace fitting technique. The algorithm is angle auto-paired and computationally efficient. Theoretical analysis and numerical simulations prove the advantages and effectiveness of the proposed array structure and the related algorithm.

  18. Saturation and stability of nonlinear photonic crystals

    International Nuclear Information System (INIS)

    Franco-Ortiz, M; Corella-Madueño, A; Rosas-Burgos, R A; Adrian Reyes, J; Avendaño, Carlos G

    2017-01-01

    We consider a one-dimensional photonic crystal made by an infinite set of nonlinear nematic films immersed in a linear dielectric medium. The thickness of each equidistant film is negligible and its refraction index depends continuously on the electric field intensity, giving rise to all the involved nonlinear terms, which joints from a starting linear index for negligible amplitudes to a final saturation index for extremely large field intensities. We show that the nonlinear exact solutions of this system form an intensity-dependent band structure which we calculate and analyze. Next, we ponder a finite version of this system; that is, we take a finite array of linear dielectric stacks of the same size separated by the same nonlinear extremely thin nematic slabs and find the reflection coefficients for this arrangement and obtain the dependence on the wave number and intensity of the incident wave. As a final step we analyze the stability of the analytical solutions of the nonlinear crystal by following the evolution of an additive amplitude to the analytical nonlinear solution we have found here. We discuss our results and state our conclusions. (paper)

  19. Evidence of hexatic phase formation in two-dimensional Lennard-Jones binary arrays

    International Nuclear Information System (INIS)

    Li, M.; Johnson, W.L.; Goddard, W.A. III

    1996-01-01

    We report evidence of the hexatic phase formation in Lennard-Jones binary substitutional random arrays from isothermal-isobaric molecular-dynamics simulations. The hexatic phase is analogous to those predicted in Kosterlitz-Thouless theory of melting that is characterized by short-range translational order and quasi-long-range orientational order. At the crystal to hexatic phase transition, dislocation pairs are observed to unbind into isolated dislocations. Further disordering of the hexatic phase, however, does not lead to dissociation of dislocations into disclinations. Instead, the dislocations become clustered and form dislocation networks which results in formation of amorphous phases. copyright 1996 The American Physical Society

  20. Monomial Crystals and Partition Crystals

    Science.gov (United States)

    Tingley, Peter

    2010-04-01

    Recently Fayers introduced a large family of combinatorial realizations of the fundamental crystal B(Λ0) for ^sln, where the vertices are indexed by certain partitions. He showed that special cases of this construction agree with the Misra-Miwa realization and with Berg's ladder crystal. Here we show that another special case is naturally isomorphic to a realization using Nakajima's monomial crystal.

  1. Remote assessment of cultural heritage environments with wireless sensor array networks.

    Science.gov (United States)

    Agbota, Henoc; Mitchell, John E; Odlyha, Marianne; Strlič, Matija

    2014-05-19

    The logistics and cost of environmental monitoring can represent challenges for heritage managers, partly because of the sheer number of environmental parameters to consider. There is a need for a system, capable of monitoring the holistic impact of the environment on cultural materials while remaining relatively easy to use and providing remote access. This paper describes a dosimetric system based on piezoelectric quartz crystal technology. The prototype sensing module consists of an array of piezoelectric quartz crystals (PQC) coated with different metals (Fe, Cu, Ni and Sn) and includes a temperature and relative humidity sensor. The communication module involves an 802.15.4 low-power radio and a GPRS gateway which allows real time visualisation of the measurements online. An energy management protocol ensures that the system consumes very low power between measurements. The paper also describes the results and experiences from two heritage field deployments, at Apsley House in London, UK, and at the Royal Palaces of Abomey in Benin. Evaluation of PQC measurements, temperature, relative humidity and the rate of successful transmission over the communication systems are also reported.

  2. A liquid-crystal-on-silicon color sequential display using frame buffer pixel circuits

    Science.gov (United States)

    Lee, Sangrok

    Next generation liquid-crystal-on-silicon (LCOS) high definition (HD) televisions and image projection displays will need to be low-cost and high quality to compete with existing systems based on digital micromirror devices (DMDs), plasma displays, and direct view liquid crystal displays. In this thesis, a novel frame buffer pixel architecture that buffers data for the next image frame while displaying the current frame, offers such a competitive solution is presented. The primary goal of the thesis is to demonstrate the LCOS microdisplay architecture for high quality image projection displays and at potentially low cost. The thesis covers four main research areas: new frame buffer pixel circuits to improve the LCOS performance, backplane architecture design and testing, liquid crystal modes for the LCOS microdisplay, and system integration and demonstration. The design requirements for the LCOS backplane with a 64 x 32 pixel array are addressed and measured electrical characteristics matches to computer simulation results. Various liquid crystal (LC) modes applicable for LCOS microdisplays and their physical properties are discussed. One- and two-dimensional director simulations are performed for the selected LC modes. Test liquid crystal cells with the selected LC modes are made and their electro-optic effects are characterized. The 64 x 32 LCOS microdisplays fabricated with the best LC mode are optically tested with interface circuitry. The characteristics of the LCOS microdisplays are summarized with the successful demonstration.

  3. Photosensitive and temperature-dependent I–V characteristics of p-NiO film/n-ZnO nanorod array heterojunction diode

    Energy Technology Data Exchange (ETDEWEB)

    Long, Hao; Ai, Lei [Key Laboratory of Artificial Micro- and Nano-structures of Ministry of Education of China, Department of Electronic Science and Technology, School of Physics and Technology, Wuhan University, Wuhan, Hubei 430072 (China); Li, Songzhan [Key Laboratory of Artificial Micro- and Nano-structures of Ministry of Education of China, Department of Electronic Science and Technology, School of Physics and Technology, Wuhan University, Wuhan, Hubei 430072 (China); School of Electronic and Electrical Engineering, Wuhan Textile University, Wuhan, Hubei 430073 (China); Huang, Huihui; Mo, Xiaoming; Wang, Haoning; Chen, Zhao; Liu, Yuping [Key Laboratory of Artificial Micro- and Nano-structures of Ministry of Education of China, Department of Electronic Science and Technology, School of Physics and Technology, Wuhan University, Wuhan, Hubei 430072 (China); Fang, Guojia, E-mail: gjfang@whu.edu.cn [Key Laboratory of Artificial Micro- and Nano-structures of Ministry of Education of China, Department of Electronic Science and Technology, School of Physics and Technology, Wuhan University, Wuhan, Hubei 430072 (China)

    2014-05-01

    Highlights: • A p-NiO film/n-ZnO nanorod array heterojunction was prepared. • The heterojunction shows good morphology and crystal properties. • The diode exhibits excellent rectifying behavior. • The diode exhibits strong temperature dependent I–V properties. • The hybrid diode shows good photosensitivity under the ultraviolet irradiation. - Abstract: A p-NiO film/n-ZnO nanorod (NR) array heterojunction was prepared by deposition of NiO film on ZnO NRs using radio-frequency reactive magnetron sputtering. The well-aligned ZnO NRs were fabricated by a simple and economic hydrothermal method on a ZnO:Al-coated glass substrate. Good morphology and crystal properties of the fabricated ZnO NRs and NiO film were confirmed by scanning electron microscopy and X-ray diffraction. The p–n heterojunction exhibits excellent rectifying behaviour and strong temperature-dependent current–voltage properties in the range from −50 to 80 °C. The hybrid NR heterojunction diode shows good photosensitivity under the irradiation of 365 nm ultraviolet light. These results present potential applications in future microelectronic devices based on NiO films and the one-dimensional ZnO nanomaterials.

  4. A review of array radars

    Science.gov (United States)

    Brookner, E.

    1981-10-01

    Achievements in the area of array radars are illustrated by such activities as the operational deployment of the large high-power, high-range-resolution Cobra Dane; the operational deployment of two all-solid-state high-power, large UHF Pave Paws radars; and the development of the SAM multifunction Patriot radar. This paper reviews the following topics: array radars steered in azimuth and elevation by phase shifting (phase-phase steered arrays); arrays steered + or - 60 deg, limited scan arrays, hemispherical coverage, and omnidirectional coverage arrays; array radars steering electronically in only one dimension, either by frequency or by phase steering; and array radar antennas which use no electronic scanning but instead use array antennas for achieving low antenna sidelobes.

  5. Fully automatic characterization and data collection from crystals of biological macromolecules.

    Science.gov (United States)

    Svensson, Olof; Malbet-Monaco, Stéphanie; Popov, Alexander; Nurizzo, Didier; Bowler, Matthew W

    2015-08-01

    Considerable effort is dedicated to evaluating macromolecular crystals at synchrotron sources, even for well established and robust systems. Much of this work is repetitive, and the time spent could be better invested in the interpretation of the results. In order to decrease the need for manual intervention in the most repetitive steps of structural biology projects, initial screening and data collection, a fully automatic system has been developed to mount, locate, centre to the optimal diffraction volume, characterize and, if possible, collect data from multiple cryocooled crystals. Using the capabilities of pixel-array detectors, the system is as fast as a human operator, taking an average of 6 min per sample depending on the sample size and the level of characterization required. Using a fast X-ray-based routine, samples are located and centred systematically at the position of highest diffraction signal and important parameters for sample characterization, such as flux, beam size and crystal volume, are automatically taken into account, ensuring the calculation of optimal data-collection strategies. The system is now in operation at the new ESRF beamline MASSIF-1 and has been used by both industrial and academic users for many different sample types, including crystals of less than 20 µm in the smallest dimension. To date, over 8000 samples have been evaluated on MASSIF-1 without any human intervention.

  6. Formation of nano-sized pinholes array in thin Ni film on MgO(100) substrate

    Energy Technology Data Exchange (ETDEWEB)

    Lin Chuan; Naramoto, Hiroshi; Xu Yonghua; Kitazawa, Sin-iti; Narumi, Kazumasa; Sakai, Seiji

    2003-10-22

    We have grown thin Ni films with various thicknesses on polished MgO(100) single crystal substrates in an e-gun evaporation system. The morphology of the as-deposited films was characterized with atomic force microscopy. Pinholes with average diameter of 5-10 nm are found in the film with thickness from 1 to 15 nm, and pinholes array was observed in the film 10 nm thick. The origin of such structure formation is discussed in terms of the elastic strain energy.

  7. Unifying the crystallization behavior of hexagonal and square crystals with the phase-field-crystal model

    International Nuclear Information System (INIS)

    Yang Tao; Chen Zheng; Zhang Jing; Wang Yongxin; Lu Yanli

    2016-01-01

    By employing the phase-field-crystal models, the atomic crystallization process of hexagonal and square crystals is investigated with the emphasis on the growth mechanism and morphological change. A unified regime describing the crystallization behavior of both crystals is obtained with the thermodynamic driving force varying. By increasing the driving force, both crystals (in the steady-state) transform from a faceted polygon to an apex-bulged polygon, and then into a symmetric dendrite. For the faceted polygon, the interface advances by a layer-by-layer (LL) mode while for the apex-bulged polygonal and the dendritic crystals, it first adopts the LL mode and then transits into the multi-layer (ML) mode in the later stage. In particular, a shift of the nucleation sites from the face center to the area around the crystal tips is detected in the early growth stage of both crystals and is rationalized in terms of the relation between the crystal size and the driving force distribution. Finally, a parameter characterizing the complex shape change of square crystal is introduced. (paper)

  8. Characteristics of NaI detector in positron imaging device HEADTOME employing circular ring array

    International Nuclear Information System (INIS)

    Miura, Shuichi; Kanno, Iwao; Aizawa, Yasuo; Murakami, Matsutaro; Uemura, Kazuo

    1984-01-01

    In positron emission computed tomographs employing circular ring arrays of detectors, the performance of the imaging device has been specified ultimately by the characteristics of the detector. The responses of NaI detector were studied when detecting positron annihilation photon (511 keV). The study was mainly by using the NaI detector used in hybrid emission computed tomography (CT) ''HEADTOME'' we had developed. A series of measurements were carried out positioning two detectors with 40 cm distance and scanning 22 Na point source in water. Both detectors was inclined from 0 0 through 30 0 to change incident angle of positron annihilation toward crystal face. Energy window was set from 100 to 700 keV. The results were presented as follows; 1 Shortening the crystal length from 7 to 5 cm made sensitivity decrease about 10% and resolution deteriorate about 1 mm (FWHM). 2 As the results of varying the width of the crystal, 20 mm width was optimal at any incident angle. 3 The lead septum between the detectors was the thickness of 4 mm enough to reject multiple detector interactions (crosstalk). 4 Beam mask which was made of lead in order to improve spatial resolution and placed on crystal face worked effectively for incident angles from 0 0 to 15 0 but degraded uniformity of spatial resolution from 0 0 to through 30 0 . (author)

  9. Modification of Thermal Emission via Metallic Photonic Crystals

    International Nuclear Information System (INIS)

    Norris, David J.; Stein, Andreas; George, Steven M.

    2012-01-01

    Photonic crystals are materials that are periodically structured on an optical length scale. It was previously demonstrated that the glow, or thermal emission, of tungsten photonic crystals that have a specific structure - known as the 'woodpile structure' - could be modified to reduce the amount of infrared radiation from the material. This ability has implications for improving the efficiency of thermal emission sources and for thermophotovoltaic devices. The study of this effect had been limited because the fabrication of metallic woodpile structures had previously required a complex fabrication process. In this project we pursued several approaches to simplify the fabrication of metallic photonic crystals that are useful for modification of thermal emission. First, we used the self-assembly of micrometer-scale spheres into colloidal crystals known as synthetic opals. These opals can then be infiltrated with a metal and the spheres removed to obtain a structure, known as an inverse opal, in which a three-dimensional array of bubbles is embedded in a film. Second, we used direct laser writing, in which the focus of an infrared laser is moved through a thin film of photoresist to form lines by multiphoton polymerization. Proper layering of such lines can lead to a scaffold with the woodpile structure, which can be coated with a refractory metal. Third, we explored a completely new approach to modified thermal emission - thin metal foils that contain a simple periodic surface pattern, as shown in Fig. 1. When such a foil is heated, surface plasmons are excited that propagate along the metal interface. If these waves strike the pattern, they can be converted into thermal emission with specific properties.

  10. Patterned Colloidal Photonic Crystals.

    Science.gov (United States)

    Hou, Jue; Li, Mingzhu; Song, Yanlin

    2018-03-01

    Colloidal photonic crystals (PCs) have been well developed because they are easy to prepare, cost-effective, and versatile with regards to modification and functionalization. Patterned colloidal PCs contribute a novel approach to constructing high-performance PC devices with unique structures and specific functions. In this review, an overview of the strategies for fabricating patterned colloidal PCs, including patterned substrate-induced assembly, inkjet printing, and selective immobilization and modification, is presented. The advantages of patterned PC devices are also discussed in detail, for example, improved detection sensitivity and response speed of the sensors, control over the flow direction and wicking rate of microfluidic channels, recognition of cross-reactive molecules through an array-patterned microchip, fabrication of display devices with tunable patterns, well-arranged RGB units, and wide viewing-angles, and the ability to construct anti-counterfeiting devices with different security strategies. Finally, the perspective of future developments and challenges is presented. © 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

  11. Patterning of Perovskite Single Crystals

    KAUST Repository

    Corzo, Daniel

    2017-06-12

    As the internet-of-things hardware integration continues to develop and the requirements for electronics keep diversifying and expanding, the necessity for specialized properties other than the classical semiconductor performance becomes apparent. The success of emerging semiconductor materials depends on the manufacturability and cost as much as on the properties and performance they offer. Solution-based semiconductors are an emerging concept that offers the advantage of being compatible with large-scale manufacturing techniques and have the potential to yield high-quality electronic devices at a lower cost than currently available solutions. In this work, patterns of high-quality MAPbBr3 perovskite single crystals in specific locations are achieved through the modification of the substrate properties and solvent engineering. The fabrication of the substrates involved modifying the surface adhesion forces through functionalization with self-assembled monolayers and patterning them by photolithography processes. Spin coating and blade coating were used to deposit the perovskite solution on the modified silicon substrates. While single crystal perovskites were obtained with the modification of substrates alone, solvent engineering helped with improving the Marangoni flows in the deposited droplets by increasing the contact angle and lowering the evaporation rate, therefore controlling and improving the shape of the grown perovskite crystals. The methodology is extended to other types of perovskites such as the transparent MAPbCl3 and the lead-free MABi2I9, demonstrating the adaptability of the process. Adapting the process to electrode arrays opened up the path towards the fabrication of optoelectronic devices including photodetectors and field-effect transistors, for which the first iterations are demonstrated. Overall, manufacturing and integration techniques permitting the fabrication of single crystalline devices, such as the method in this thesis work, are

  12. The EUROBALL array

    International Nuclear Information System (INIS)

    Rossi Alvarez, C.

    1998-01-01

    The quality of the multidetector array EUROBALL is described, with emphasis on the history and formal organization of the related European collaboration. The detector layout is presented together with the electronics and Data Acquisition capabilities. The status of the instrument, its performances and the main features of some recently developed ancillary detectors will also be described. The EUROBALL array is operational in Legnaro National Laboratory (Italy) since April 1997 and is expected to run up to November 1998. The array represents a significant improvement in detector efficiency and sensitivity with respect to the previous generation of multidetector arrays

  13. High-voltage electron-microscopical observation of crack-tip dislocations in silicon crystals

    International Nuclear Information System (INIS)

    Tanaka, Masaki; Higashida, Kenji

    2005-01-01

    Crack-tip dislocations in silicon single crystals were observed by high-voltage electron microscopy. Cracks were introduced into silicon wafers at room temperature by a Vickers indenter. The indented specimens were annealed at 823 K in order to activate dislocation emission from the crack tip under the residual stress due to the indentation. In the specimen without annealing, no dislocations were observed around the crack. On the other hand, in the specimen after the annealing, the aspect of the early stage of dislocation emission was observed, where dislocations were emitted not as a perfect dislocation but as a partial dislocation in the hinge-type plastic zone. Prominent dislocation arrays that were emitted from a crack tip were also observed, and they were found to be of shielding type, which increases the fracture toughness of those crystals

  14. Fully automatic characterization and data collection from crystals of biological macromolecules

    International Nuclear Information System (INIS)

    Svensson, Olof; Malbet-Monaco, Stéphanie; Popov, Alexander; Nurizzo, Didier; Bowler, Matthew W.

    2015-01-01

    A fully automatic system has been developed that performs X-ray centring and characterization of, and data collection from, large numbers of cryocooled crystals without human intervention. Considerable effort is dedicated to evaluating macromolecular crystals at synchrotron sources, even for well established and robust systems. Much of this work is repetitive, and the time spent could be better invested in the interpretation of the results. In order to decrease the need for manual intervention in the most repetitive steps of structural biology projects, initial screening and data collection, a fully automatic system has been developed to mount, locate, centre to the optimal diffraction volume, characterize and, if possible, collect data from multiple cryocooled crystals. Using the capabilities of pixel-array detectors, the system is as fast as a human operator, taking an average of 6 min per sample depending on the sample size and the level of characterization required. Using a fast X-ray-based routine, samples are located and centred systematically at the position of highest diffraction signal and important parameters for sample characterization, such as flux, beam size and crystal volume, are automatically taken into account, ensuring the calculation of optimal data-collection strategies. The system is now in operation at the new ESRF beamline MASSIF-1 and has been used by both industrial and academic users for many different sample types, including crystals of less than 20 µm in the smallest dimension. To date, over 8000 samples have been evaluated on MASSIF-1 without any human intervention

  15. Fully automatic characterization and data collection from crystals of biological macromolecules

    Energy Technology Data Exchange (ETDEWEB)

    Svensson, Olof; Malbet-Monaco, Stéphanie; Popov, Alexander; Nurizzo, Didier, E-mail: nurizzo@esrf.fr [European Synchrotron Radiation Facility, 71 Avenue des Martyrs, CS 40220, 38043 Grenoble (France); Bowler, Matthew W., E-mail: nurizzo@esrf.fr [European Molecular Biology Laboratory, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); Université Grenoble Alpes–EMBL–CNRS, Grenoble Outstation, 71 Avenue des Martyrs, CS 90181, 38042 Grenoble (France); European Synchrotron Radiation Facility, 71 Avenue des Martyrs, CS 40220, 38043 Grenoble (France)

    2015-07-31

    A fully automatic system has been developed that performs X-ray centring and characterization of, and data collection from, large numbers of cryocooled crystals without human intervention. Considerable effort is dedicated to evaluating macromolecular crystals at synchrotron sources, even for well established and robust systems. Much of this work is repetitive, and the time spent could be better invested in the interpretation of the results. In order to decrease the need for manual intervention in the most repetitive steps of structural biology projects, initial screening and data collection, a fully automatic system has been developed to mount, locate, centre to the optimal diffraction volume, characterize and, if possible, collect data from multiple cryocooled crystals. Using the capabilities of pixel-array detectors, the system is as fast as a human operator, taking an average of 6 min per sample depending on the sample size and the level of characterization required. Using a fast X-ray-based routine, samples are located and centred systematically at the position of highest diffraction signal and important parameters for sample characterization, such as flux, beam size and crystal volume, are automatically taken into account, ensuring the calculation of optimal data-collection strategies. The system is now in operation at the new ESRF beamline MASSIF-1 and has been used by both industrial and academic users for many different sample types, including crystals of less than 20 µm in the smallest dimension. To date, over 8000 samples have been evaluated on MASSIF-1 without any human intervention.

  16. Preparation of Microcrystals of Piroxicam Monohydrate by Antisolvent Precipitation via Microfabricated Metallic Membranes with Ordered Pore Arrays.

    Science.gov (United States)

    Othman, Rahimah; Vladisavljević, Goran T; Simone, Elena; Nagy, Zoltan K; Holdich, Richard G

    2017-12-06

    Microcrystals of piroxicam (PRX) monohydrate with a narrow size distribution were prepared from acetone/PRX solutions by antisolvent crystallization via metallic membranes with ordered pore arrays. Crystallization was achieved by controlled addition of the feed solution through the membrane pores into a well-stirred antisolvent. A complete transformation of an anhydrous form I into a monohydrate form of PRX was confirmed by Raman spectroscopy and differential scanning calorimetry. The size of the crystals was 7-34 μm and was controlled by the PRX concentration in the feed solution (15-25 g L -1 ), antisolvent/solvent volume ratio (5-30), and type of antisolvent (Milli-Q water or 0.1-0.5 wt % aqueous solutions of hydroxypropyl methyl cellulose (HPMC), poly(vinyl alcohol) or Pluronic P-123). The smallest crystals were obtained by injecting 25 g L -1 PRX solution through a stainless-steel membrane with a pore size of 10 μm into a 0.06 wt % HPMC solution stirred at 1500 rpm using an antisolvent/solvent ratio of 20. HPMC provided better steric stabilization of microcrystals against agglomeration than poly(vinyl alcohol) and Pluronic P-123, due to hydrogen bonding interactions with PRX and water. A continuous production of large PRX monohydrate microcrystals with a volume-weighted mean diameter above 75 μm was achieved in a continuous stirred membrane crystallizer. Rapid pouring of Milli-Q water into the feed solution resulted in a mixture of highly polydispersed prism-shaped and needle-shaped crystals.

  17. Controlling statics and dynamics of colloids by photo-patterned liquid crystals (Conference Presentation)

    Science.gov (United States)

    Lavrentovich, Oleg D.; Peng, Chenhui; Guo, Yubing; Shiyanovskii, Sergij V.; Wei, Qi-Huo

    2016-09-01

    Transport of fluids and particles at the microscale is an important theme both in fundamental and applied science. We demonstrate how an advanced approach to photo-induced alignment of liquid crystals can be used to generate nonlinear electrokinetics. The photoalignment technique is based on irradiation of a photosensitive substrate with light through nanoaperture arrays in metal films. The resulting pattern of surface alignment induces predesigned 2D and 3D distortions of local molecular orientation. In presence of a static electric field, these distortions generate spatial charge and drive electrokinetic flows of the new type, in which the velocities depend on the square of the applied electric field. The patterned liquid crystal electrolyte converts the electric energy into the flows and transport of embedded particles of any type (fluid, solid, gaseous) along a predesigned trajectory, posing no limitation on the electric nature (charge, polarizability) of these particles and interfaces. The patterned liquid crystal electrolyte induces persistent vortices of controllable rotation speed and direction that are quintessential for micro- and nanoscale mixing applications.

  18. Semi-Dirac points in phononic crystals

    KAUST Repository

    Zhang, Xiujuan

    2014-01-01

    A semi-Dirac cone refers to a peculiar type of dispersion relation that is linear along the symmetry line but quadratic in the perpendicular direction. It was originally discovered in electron systems, in which the associated quasi-particles are massless along one direction, like those in graphene, but effective-mass-like along the other. It was reported that a semi-Dirac point is associated with the topological phase transition between a semi-metallic phase and a band insulator. Very recently, the classical analogy of a semi-Dirac cone has been reported in an electromagnetic system. Here, we demonstrate that, by accidental degeneracy, two-dimensional phononic crystals consisting of square arrays of elliptical cylinders embedded in water are also able to produce the particular dispersion relation of a semi-Dirac cone in the center of the Brillouin zone. A perturbation method is used to evaluate the linear slope and to affirm that the dispersion relation is a semi-Dirac type. If the scatterers are made of rubber, in which the acoustic wave velocity is lower than that in water, the semi-Dirac dispersion can be characterized by an effective medium theory. The effective medium parameters link the semi-Dirac point to a topological transition in the iso-frequency surface of the phononic crystal, in which an open hyperbola is changed into a closed ellipse. This topological transition results in drastic change in wave manipulation. On the other hand, the theory also reveals that the phononic crystal is a double-zero-index material along the x-direction and photonic-band-edge material along the perpendicular direction (y-direction). If the scatterers are made of steel, in which the acoustic wave velocity is higher than that in water, the effective medium description fails, even though the semi-Dirac dispersion relation looks similar to that in the previous case. Therefore different wave transport behavior is expected. The semi-Dirac points in phononic crystals described in

  19. Sub-coherent growth of ZnO nanorod arrays on three-dimensional graphene framework as one-bulk high-performance photocatalyst

    Science.gov (United States)

    Yu, Mei; Ma, Yuxiao; Liu, Jianhua; Li, Xinjie; Li, Songmei; Liu, Shenyao

    2016-12-01

    Highly ordered ZnO nanorod arrays were grown vertically on the surface of three-dimensional graphene (3DG) framework bulk to prepare a one-bulk structure. In such structure, ZnO exhibits outstanding photocatalyst performance due to its hybridization with 3DG. The sub-coherency between ZnO and 3DG ensures the template-free growth of ZnO nanorod arrays and the exposing of its most active crystal surfaces {0001}. The hybridization prevents the agglomeration of ZnO nanoparticles, helping the formation of nanorod array morphology, enhancing the mass transfer of reactants and the separation of photogenerated holes. In the efficiency test, with tiny amount of ZnO catalyst (∼5.03 × 10-3 g), the concentration of methyl orange decreased to ∼11% of the initial value within four hours. The structure possesses high average photocatalytic efficiency of 6.56 × 10-3 h-1, much higher than that of bare ZnO nanorods.

  20. Storage array reflection considerations

    International Nuclear Information System (INIS)

    Haire, M.J.; Jordan, W.C.; Taylor, R.G.

    1997-01-01

    The assumptions used for reflection conditions of single containers are fairly well established and consistently applied throughout the industry in nuclear criticality safety evaluations. Containers are usually considered to be either fully water reflected (i.e., surrounded by 6 to 12 in. of water) for safety calculations or reflected by 1 in. of water for nominal (structural material and air) conditions. Tables and figures are usually available for performing comparative evaluations of containers under various loading conditions. Reflection considerations used for evaluating the safety of storage arrays of fissile material are not as well established. When evaluating arrays, it has become more common for analysts to use calculations to demonstrate the safety of the array configuration. In performing these calculations, the analyst has considerable freedom concerning the assumptions made for modeling the reflection of the array. Considerations are given for the physical layout of the array with little or no discussion (or demonstration) of what conditions are bounded by the assumed reflection conditions. For example, an array may be generically evaluated by placing it in a corner of a room in which the opposing walls are far away. Typically, it is believed that complete flooding of the room is incredible, so the array is evaluated for various levels of water mist interspersed among array containers. This paper discusses some assumptions that are made regarding storage array reflection