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Sample records for crystal process technology

  1. Designing Robust Process Analytical Technology (PAT) Systems for Crystallization Processes: A Potassium Dichromate Crystallization Case Study

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin; Sin, Gürkan

    2013-01-01

    The objective of this study is to test and validate a Process Analytical Technology (PAT) system design on a potassium dichromate crystallization process in the presence of input uncertainties using uncertainty and sensitivity analysis. To this end a systematic framework for managing uncertaintie...

  2. Process Analytical Technology for Crystallization of Active Pharmaceutical Ingredients

    DEFF Research Database (Denmark)

    Malwade, Chandrakant Ramkrishna; Qu, Haiyan

    2018-01-01

    . Crystallization with its ability to engineer the final product to the desired qualities such as purity, polymorphic form, particle size and shape is one of the most important steps involved in manufacturing of APIs. Therefore, development of crystallization processes with better understanding of process...... of crystallization processes in manufacturing of APIs. Results: Firstly, various steps involved in the drug development process are introduced briefly with emphasis on crystallization as one of the most important steps in manufacturing of drug products. Secondly, Critical Quality Attributes (CQAs) of drug products......, their dependence on material attributes of APIs and role of crystallization in manipulating material attributes of APIs has been discussed. Finally, application of PAT tools such as advanced process analyzers for continuous monitoring, chemometric methods for multivariate data analysis, and control strategy...

  3. A Robust Process Analytical Technology (PAT) System Design for Crystallization Processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin; Sin, Gürkan; Gernaey, Krist

    2013-01-01

    A generic computer-aided framework for systematic design of a process monitoring and control system for crystallization processes has been developed to study various aspects of crystallization operations. The design framework contains a generic multidimensional modelling framework, a tool for gen...

  4. Introducing uncertainty analysis of nucleation and crystal growth models in Process Analytical Technology (PAT) system design of crystallization processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin; Sin, Gürkan; Gernaey, Krist

    2013-01-01

    This paper presents the application of uncertainty and sensitivity analysis as part of a systematic modelbased process monitoring and control (PAT) system design framework for crystallization processes. For the uncertainty analysis, the Monte Carlo procedure is used to propagate input uncertainty...

  5. Introducing uncertainty analysis of nucleation and crystal growth models in Process Analytical Technology (PAT) system design of crystallization processes.

    Science.gov (United States)

    Samad, Noor Asma Fazli Abdul; Sin, Gürkan; Gernaey, Krist V; Gani, Rafiqul

    2013-11-01

    This paper presents the application of uncertainty and sensitivity analysis as part of a systematic model-based process monitoring and control (PAT) system design framework for crystallization processes. For the uncertainty analysis, the Monte Carlo procedure is used to propagate input uncertainty, while for sensitivity analysis, global methods including the standardized regression coefficients (SRC) and Morris screening are used to identify the most significant parameters. The potassium dihydrogen phosphate (KDP) crystallization process is used as a case study, both in open-loop and closed-loop operation. In the uncertainty analysis, the impact on the predicted output of uncertain parameters related to the nucleation and the crystal growth model has been investigated for both a one- and two-dimensional crystal size distribution (CSD). The open-loop results show that the input uncertainties lead to significant uncertainties on the CSD, with appearance of a secondary peak due to secondary nucleation for both cases. The sensitivity analysis indicated that the most important parameters affecting the CSDs are nucleation order and growth order constants. In the proposed PAT system design (closed-loop), the target CSD variability was successfully reduced compared to the open-loop case, also when considering uncertainty in nucleation and crystal growth model parameters. The latter forms a strong indication of the robustness of the proposed PAT system design in achieving the target CSD and encourages its transfer to full-scale implementation. Copyright © 2013 Elsevier B.V. All rights reserved.

  6. Patterning technology for solution-processed organic crystal field-effect transistors

    Science.gov (United States)

    Li, Yun; Sun, Huabin; Shi, Yi; Tsukagoshi, Kazuhito

    2014-01-01

    Organic field-effect transistors (OFETs) are fundamental building blocks for various state-of-the-art electronic devices. Solution-processed organic crystals are appreciable materials for these applications because they facilitate large-scale, low-cost fabrication of devices with high performance. Patterning organic crystal transistors into well-defined geometric features is necessary to develop these crystals into practical semiconductors. This review provides an update on recentdevelopment in patterning technology for solution-processed organic crystals and their applications in field-effect transistors. Typical demonstrations are discussed and examined. In particular, our latest research progress on the spin-coating technique from mixture solutions is presented as a promising method to efficiently produce large organic semiconducting crystals on various substrates for high-performance OFETs. This solution-based process also has other excellent advantages, such as phase separation for self-assembled interfaces via one-step spin-coating, self-flattening of rough interfaces, and in situ purification that eliminates the impurity influences. Furthermore, recommendations for future perspectives are presented, and key issues for further development are discussed. PMID:27877656

  7. Patterning technology for solution-processed organic crystal field-effect transistors

    Directory of Open Access Journals (Sweden)

    Yun Li

    2014-04-01

    Full Text Available Organic field-effect transistors (OFETs are fundamental building blocks for various state-of-the-art electronic devices. Solution-processed organic crystals are appreciable materials for these applications because they facilitate large-scale, low-cost fabrication of devices with high performance. Patterning organic crystal transistors into well-defined geometric features is necessary to develop these crystals into practical semiconductors. This review provides an update on recent development in patterning technology for solution-processed organic crystals and their applications in field-effect transistors. Typical demonstrations are discussed and examined. In particular, our latest research progress on the spin-coating technique from mixture solutions is presented as a promising method to efficiently produce large organic semiconducting crystals on various substrates for high-performance OFETs. This solution-based process also has other excellent advantages, such as phase separation for self-assembled interfaces via one-step spin-coating, self-flattening of rough interfaces, and in situ purification that eliminates the impurity influences. Furthermore, recommendations for future perspectives are presented, and key issues for further development are discussed.

  8. Crystal-Clear Technology.

    Science.gov (United States)

    Ondris-Crawford, Renate J.; And Others

    1993-01-01

    Provides diagrams to aid in discussing polymer dispersed liquid crystal (PDLC) technology. Equipped with a knowledge of PDLC, teachers can provide students with insight on how the gap between basic science and technology is bridged. (ZWH)

  9. Enhancing crystalline properties of a cardiovascular active pharmaceutical ingredient using a process analytical technology based crystallization feedback control strategy.

    Science.gov (United States)

    Saleemi, Ali N; Steele, Gerry; Pedge, Nicholas I; Freeman, Anthony; Nagy, Zoltan K

    2012-07-01

    Pharmaceutical regulatory bodies require minimal presence of solvent in an active pharmaceutical ingredient (API) after crystallization. From a processing point of view bigger crystals with minimal agglomeration and uniform size distribution are preferred to avoid solvent inclusion and for improved downstream processing. The current work addresses these issues encountered during the production of the potential anti-arrhythmic cardiovascular drug, AZD7009. This paper demonstrates that by applying the automated direct nucleation control (ADNC) approach problems with agglomeration and solvent inclusion were resolved. This model free approach automatically induces temperature cycles in the system, with the number of cycles, temperature range and adaptive heating and cooling rates determined to maintain the number of particles in the system, as measured by a focused beam reflectance measurement (FBRM) probe, within a constant range during the crystallization. The ADNC approach was able to produce larger and more uniform crystals and also removed the residual solvent trapped between the crystals compared to the typical crystallization operation using linear cooling profile. The results illustrate the application of process analytical technologies, such as FBRM and ATR-UV-vis spectroscopy, for the design of optimal crystallization operating conditions for the production of pharmaceuticals, and demonstrate that the ADNC approach can be used for rapid crystallization development for APIs exhibiting problems with agglomeration and solvent inclusion. Copyright © 2012 Elsevier B.V. All rights reserved.

  10. Development of Auto-Seeding System Using Image Processing Technology in the Sapphire Crystal Growth Process via the Kyropoulos Method

    Directory of Open Access Journals (Sweden)

    Churl Min Kim

    2017-04-01

    Full Text Available The Kyropoulos (Ky and Czochralski (Cz methods of crystal growth are used for large-diameter single crystals. The seeding process in these methods must induce initial crystallization by initiating contact between the seed crystals and the surface of the melted material. In the Ky and Cz methods, the seeding process lays the foundation for ingot growth during the entire growth process. When any defect occurs in this process, it is likely to spread to the entire ingot. In this paper, a vision system was constructed for auto seeding and for observing the surface of the melt in the Ky method. An algorithm was developed to detect the time when the internal convection of the melt is stabilized by observing the shape of the spoke pattern on the melt material surface. Then, the vision system and algorithm were applied to the growth furnace, and the possibility of process automation was examined for sapphire growth. To confirm that the convection of the melt was stabilized, the position of the island (i.e., the center of a spoke pattern was detected using the vision system and image processing. When the observed coordinates for the center of the island were compared with the coordinates detected from the image processing algorithm, there was an average error of 1.87 mm (based on an image with 1024 × 768 pixels.

  11. Development of technologically important crystals and devices

    International Nuclear Information System (INIS)

    Singh, S.G.; Tyagi, M.; Desai, D.G.; Singh, A.K.; Tiwari, Babita; Sen, Shashwati; Chauhan, A.K.; Gadkari, S.C.

    2011-01-01

    Device-grade single crystals of technologically important materials for use as scintillators in nuclear radiation detection, lasers and optical devices are grown in Crystal Technology Section of the Technical Physics Division. The expertise has been developed to establish crystal growth processes and design and fabricate crystal growth equipment. In addition, single crystals of new materials to be used in neutron and gamma detection are also being studied and developed currently. The processing, characterization and testing of devices are carried out using in-house facilities as well as in collaboration with other Divisions. (author)

  12. Process Analytical Technology in Freeze-Drying: Detection of the Secondary Solute + Water Crystallization with Heat Flux Sensors.

    Science.gov (United States)

    Wang, Qiming; Shalaev, Evgenyi

    2017-11-03

    In situ and non-invasive detection of solute crystallization during freeze-drying would facilitate cycle optimization and scale-up from the laboratory to commercial manufacturing scale. The objective of the study is to evaluate heat flux sensor (HFS) as a tool for monitoring solute crystallization and other first-order phase transitions (e.g., onset of freezing). HFS is a thin-film differential thermopile, which acts as a transducer to generate an electrical signal proportional to the total heat applied to its surface. In this study, HFS is used to detect both primary (ice formation) and secondary (also known as eutectic) solute + water crystallization during cooling and heating of solutions in a freeze-dryer. Binary water-solute mixtures with typical excipients concentrations (e.g., 0.9% of NaCl and 5% mannitol) and fill volumes (1 to 3 ml/vial) are studied. Secondary crystallization is detected by the HFS during cooling in all experiments with NaCl solutions, whereas timing of mannitol crystallization depends on the cooling conditions. In particular, mannitol crystallization takes place during cooling, if the cooling rate is lower than the critical value. On the other hand, if the cooling rate exceeds the critical cooling rate, mannitol crystallization during cooling is prevented, and crystallization occurs during subsequent warming or annealing. It is also observed that, while controlled ice nucleation allows initiation of the primary freezing event in different vials simultaneously, there is a noticeable vial-to-vial difference in the timing of secondary crystallization. The HFS could be a valuable process monitoring tool for non-invasive detection of various crystallization events during freeze-drying manufacturing.

  13. On-line near infrared spectroscopy as a Process Analytical Technology (PAT) tool to control an industrial seeded API crystallization.

    Science.gov (United States)

    Schaefer, C; Lecomte, C; Clicq, D; Merschaert, A; Norrant, E; Fotiadu, F

    2013-09-01

    The final step of an active pharmaceutical ingredient (API) manufacturing synthesis process consists of a crystallization during which the API and residual solvent contents have to be quantified precisely in order to reach a predefined seeding point. A feasibility study was conducted to demonstrate the suitability of on-line NIR spectroscopy to control this step in line with new version of the European Medicines Agency (EMA) guideline [1]. A quantitative method was developed at laboratory scale using statistical design of experiments (DOE) and multivariate data analysis such as principal component analysis (PCA) and partial least squares (PLS) regression. NIR models were built to quantify the API in the range of 9-12% (w/w) and to quantify the residual methanol in the range of 0-3% (w/w). To improve the predictive ability of the models, the development procedure encompassed: outliers elimination, optimum model rank definition, spectral range and spectral pre-treatment selection. Conventional criteria such as, number of PLS factors, R(2), root mean square errors of calibration, cross-validation and prediction (RMSEC, RMSECV, RMSEP) enabled the selection of three model candidates. These models were tested in the industrial pilot plant during three technical campaigns. Results of the most suitable models were evaluated against to the chromatographic reference methods. Maximum relative bias of 2.88% was obtained about API target content. Absolute bias of 0.01 and 0.02% (w/w) respectively were achieved at methanol content levels of 0.10 and 0.13% (w/w). The repeatability was assessed as sufficient for the on-line monitoring of the 2 analytes. The present feasibility study confirmed the possibility to use on-line NIR spectroscopy as a PAT tool to monitor in real-time both the API and the residual methanol contents, in order to control the seeding of an API crystallization at industrial scale. Furthermore, the successful scale-up of the method proved its capability to be

  14. Technology of gallium nitride crystal growth

    CERN Document Server

    Ehrentraut, Dirk; Bockowski, Michal

    2010-01-01

    This book deals with the important technological aspects of the growth of GaN single crystals by HVPE, MOCVD, ammonothermal and flux methods for the purpose of free-standing GaN wafer production. Leading experts from industry and academia report in a very comprehensive way on the current state-of-the-art of the growth technologies and optical and structural properties of the GaN crystals are compared.

  15. Photonic Crystals: Physics and Technology

    CERN Document Server

    Sibilia, Concita; Marciniak, Marian; Szoplik, Tomasz

    2008-01-01

    The aim of the work is give an overview of the activity in the field of Photonic Crystal developed in the frame of COST P11 action . The main objective of the COST P11 action was to unify and coordinate national efforts aimed at studying linear and nonlinear optical interactions with Photonic Crystals (PCs), without neglecting an important aspect related to the material research as idea and methods of realizations of 3D PC, together with the development and implementation of measurement techniques for the experimental evaluation of their potential applications in different area, as for example telecommunication with novel optical fibers, lasers, nonlinear multi-functionality, display devices , opto-electronics, sensors. The book contain contributions from authors who gave their lecture at the Cost P11 Training School. Training School was held at the Warsaw University (2007) and National Institute of Telecommunications (May 23), Warsaw. It was attended by 23 students. The focus of the School was on the work of...

  16. Recent Developments in the Crystallization Process: Toward the Pharmaceutical Industry

    Directory of Open Access Journals (Sweden)

    Zhenguo Gao

    2017-06-01

    Full Text Available Crystallization is one of the oldest separation and purification unit operations, and has recently contributed to significant improvements in producing higher-value products with specific properties and in building efficient manufacturing processes. In this paper, we review recent developments in crystal engineering and crystallization process design and control in the pharmaceutical industry. We systematically summarize recent methods for understanding and developing new types of crystals such as co-crystals, polymorphs, and solvates, and include several milestones such as the launch of the first co-crystal drug, Entresto (Novartis, and the continuous manufacture of Orkambi (Vertex. Conventional batch and continuous processes, which are becoming increasingly mature, are being coupled with various control strategies and the recently developed crystallizers are thus adapting to the needs of the pharmaceutical industry. The development of crystallization process design and control has led to the appearance of several new and innovative crystallizer geometries for continuous operation and improved performance. This paper also reviews major recent progress in the area of process analytical technology.

  17. Steering a crystallization process to reduce crystal polydispersity; case study of insulin crystallization

    Science.gov (United States)

    Nanev, Christo N.; Petrov, Kostadin P.

    2017-12-01

    The use of the classical nucleation-growth-separation principle (NGSP) was restricted hitherto to nucleation kinetics studies only. A novel application of the NGSP is proposed. To reduce crystal polydispersity internal seeding of equally-sized crystals is suggested, the advantage being avoidance of crystal grinding, sieving and any introduction of impurities. In the present study, size distributions of grown insulin crystals are interpreted retrospectively to select the proper nucleation stage parameters. The conclusion is that when steering a crystallization process aimed at reducing crystal polydispersity, the shortest possible nucleation stage duration has to be chosen because it renders the closest size distribution of the nucleated crystal seeds. Causes of inherent propensity to increasing crystal polydispersity during prolonged growth are also explored. Step sources of increased activity, present in some crystals while absent in others, are pointed as the major polydispersity cause. Insulin crystal morphology is also considered since it determines the dissolution rate of a crystalline medicine.

  18. Pyro processing technology at KAERI

    International Nuclear Information System (INIS)

    Lee, Hansoo; Kim, Eungho; Park, Seongwon

    2008-01-01

    KAERI has studied on the pyro processing as a spent fuel treatment method for more than decade. The process includes voloxidation, electroreduction, electrorefining with solid and liquid cathodes, and waste salt treatment. Each process has developed its own characteristics which are suitable for treating high mass flow. In the electroreduction process, a magnesia filter was used for integrated electrolytic reduction. More than 99% of reduction yield was achieved. Electrorefining process employs the continuous operation concept. Uranium deposits on the surface of graphite cathode and it is stripped off spontaneously to the bottom of the reactor, which allows continuous operation. Crystallization method was used for treating waste salt. Pure salt is recovered by Czochralski method or zone freezing method and subsequently recycled to the reactor. These advanced technologies ensure the operation of pyro processing in a larger scale

  19. Technology or Process First?

    DEFF Research Database (Denmark)

    Siurdyban, Artur Henryk; Svejvig, Per; Møller, Charles

    between them using strategic alignment, Enterprise Systems and Business Process Management theories. We argue that the insights from these cases can lead to a better alignment between process and technology. Implications for practice include the direction towards a closer integration of process......Enterprise Systems Management (ESM) and Business Pro- cess Management (BPM), although highly correlated, have evolved as alternative and mutually exclusive approaches to corporate infrastruc- ture. As a result, companies struggle to nd the right balance between technology and process factors...... in infrastructure implementation projects. The purpose of this paper is articulate a need and a direction to medi- ate between the process-driven and the technology-driven approaches. Using a cross-case analysis, we gain insight into two examples of sys- tems and process implementation. We highlight the dierences...

  20. Desalination processes and technologies

    International Nuclear Information System (INIS)

    Furukawa, D.H.

    1996-01-01

    Reasons of the development of desalination processes, the modern desalination technologies, such as multi-stage flash evaporation, multi-effect distillation, reverse osmosis, and the prospects of using nuclear power for desalination purposes are discussed. 9 refs

  1. Alignment technology and applications of liquid crystal devices

    CERN Document Server

    Takatoh, Kohki; Hasegawa, Ray; Koden, Mitsushiro; Itoh, Nobuyuki; Hasegawa, Masaki

    2005-01-01

    Alignment phenomena are characteristic of liquid crystalline materials, and understanding them is critically important in understanding the essential features and behavior of liquid crystals and the performance of Liquid Crystal Devices (LCDs). Furthermore, in LCD production lines, the alignment process is of practical importance. Alignment Technologies and Applications of Liquid Crystal Devices demonstrates both the fundamental and practical aspects of alignment phenomena in liquid crystals. The physical basis of alignment phenomena is first introduced in order to aid the understanding of the various physical phenomena observed in the interface between liquid crystalline materials and alignment layer surfaces. Methods for the characterization of surfaces, which induce the alignment phenomena, and of the alignment layer itself are introduced. These methods are useful for the research of liquid crystalline materials and devices in academic research as well as in industry. In the practical sections, the alignme...

  2. Liquid crystals. Oligomeric and polymeric materials for soft photonic technologies

    CERN Document Server

    Coles, M J

    2002-01-01

    The current pace of today's information technologies might lead the casual observer to believe that this is all new. However the reality is that, as with most things, this is really a long evolution of processes based on tried, tested and re-adapted techniques. This thesis represents 12 years of predominantly technology driven research and covers a whole range of characterising, evaluating and fabricating devices based on liquid crystalline systems. Firstly polymer liquid crystals are discussed with respect to the fabrication of a flexible substrate display based on standard printing techniques and this is shown to have improved display viewing properties over a standard polymer dispersed liquid crystal (PDLC) device. Following on from this work is presented that involves the production of regular grid arrays in isotropic polymers that are used as control structures in nematic liquid crystal systems. This progresses onto a now patented device that allows the production of robust ferroelectric devices based on...

  3. Effective removal of ammonia nitrogen from waste seawater using crystal seed enhanced struvite precipitation technology with response surface methodology for process optimization.

    Science.gov (United States)

    Song, Weilong; Li, Zhipeng; Liu, Feng; Ding, Yi; Qi, Peishi; You, Hong; Jin, Chao

    2018-01-01

    Traditional biological treatment was not effective for removing nitrogen from saline wastewater due to the inhibition of high salinity on biomass activity. In this context, a method of removing ammonia nitrogen from waste seawater was proposed by struvite precipitation which was enhanced by seeding technique. The abundant magnesium contained in waste seawater was used as the key component of struvite crystallization without additional magnesium. The effects of pH and P:N molar ratio on ammonia nitrogen removal efficiency were studied. The results showed that optimum pH value was in range of 8.5-10 and the P:N molar ratio should be controlled within 2:1-3:1. XRD and SEM-EDS analyses of the precipitates proved that Ca 2+ and excess Mg 2+ contained in waste seawater inhibited the struvite crystallization by competing PO 4 3- to form by-products. Then, seeding technique for enhancing the struvite crystallization was investigated, and the results indicated that using preformed struvite as crystal seed significantly improved the ammonia nitrogen removal efficiency, especially when initial ammonia nitrogen concentration was relatively low. Moreover, response surface optimization experiment following a Box-Behnken design was conducted. A response surface model was established, based on which optimum process conditions were determined and interactions between various factors were clarified. At last, economic evaluation demonstrated this proposed method was economic feasible.

  4. Geochemical modelization of differentiation processes by crystallization

    International Nuclear Information System (INIS)

    Cebria, J.M.; Lopez Ruiz, J.

    1994-01-01

    During crystallization processes, major and trace elements and stable isotopes fractionate, whereas radiogenic isotopes do not change. The different equations proposed allow us to reproduce the variation in major and trace elements during these differentiation processes. In the case of simple fractional crystallization, the residual liquid is impoverished in compatible elements faster than it is enriched in incompatible elements as crystallization proceeds. During in situ crystallization the incompatible elements evolve in a similar way to the case of simple fractional crystallization but the enrichment rate of the moderately incompatible elements is slower and the compatible elements do not suffer a depletion as strong as the one observed during simple fractional crystallization, even for higher f values. In a periodically replenished magma chamber if all the liquid present is removed at the end of each cycle, the magma follows patterns similar to those generated by simple fractional crystallization. On the contrary, if the liquid fraction that crystallizes during each cycle and the one that is extruded at the end of the cycle are small, the residual liquid shows compositions similar to those that would be obtained by equilibrium crystallization. Crystallization processes modelling is in general less difficult than for partial melting. If a rock series is the result of simple fractional crystallization, a C''i L -C''i L plot in which i is a compatible element and j is highly incompatible, allows us to obtain a good approximation to the initial liquid composition. Additionally, long C''i L -log C''i L diagrams in which i is a highly incompatible element, allow us to identify steps in the process and to calculate the bulk distribution coefficients of the trace elements during each step

  5. Technologies for Optical Processing

    DEFF Research Database (Denmark)

    Stubkjær, Kristian

    2008-01-01

    The article consists of a Powerpoint presentation on technologies for optical processing. The paper concludes that the nonlinear elements based on SOA, fibers and waveguide structures have capabilities of simple processing at data rates of 100-600 Gb/s. Switching powers comparable to electronics...

  6. Photon technology. Laser processing technology; Photon technology. Laser process gijutsu

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1996-03-01

    Survey has been conducted to develop laser processing technology utilizing the interaction between substance and photon. This is a part of the leading research on photon technology development. The photon technology development is aimed at novel technology development highly utilizing the quantum nature of photons. In the field of laser processing, high quality photons are used as tools, special functions of atoms and molecules will be discovered, and processing for functional fabrication (photon machining) will be established. A role of laser processing in industries has become significant, which is currently spreading not only into cutting and welding of materials and scalpels but also into such a special field as ultrafine processing of materials. The spreading is sometimes obstructed due to the difficulty of procurement of suitable machines and materials, and the increase of cost. The purpose of this study is to develop the optimal laser technology, to elucidate the interaction between substance and photon, and to develop the laser system and the transmission and regulation systems which realize the optimal conditions. 387 refs., 115 figs., 25 tabs.

  7. Co-crystallization as a separation technology: controlling product concentrations by co-crystals

    NARCIS (Netherlands)

    Urbanus, J.; Roelands, C.P.M.; Verdoes, D.; Jansens, P.J.; Horst, J.H. ter

    2010-01-01

    Co-crystallization is known as a product formulation technology, but it can also be used as a tool to solve crystallization problems. Product removal by co-crystallization in fermentations is used as a showcase to demonstrate the potential of co-crystallization as a separation technique. In

  8. A Generic Framework for Systematic Design of Process Monitoring and Control System for Crystallization Processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin; Meisler, Kresten Troelstrup; Sin, Gürkan

    Crystallization processes have a wide range of application as a solid-liquid separation technique in the chemical, the pharmaceutical and the food industries, due to the fact that high quality crystalline products can be produced. The main specifications of the crystal product are usually given...... in terms of crystal size, size distribution, shape and purity. However, the main difficulty in crystallization processes is to obtain a uniform and reproducible crystal size distribution (CSD). To this end, supersaturation control is often applied to drive the process within the metastable zone in order......, for control and monitoring purposes, an appropriate Process Analytical Technology (PAT) system ensuring that the critical process variables are measured and maintained within the design limits also needs to be integrated. The objectives of this work are to develop a generic systematic design framework...

  9. VLSI signal processing technology

    CERN Document Server

    Swartzlander, Earl

    1994-01-01

    This book is the first in a set of forthcoming books focussed on state-of-the-art development in the VLSI Signal Processing area. It is a response to the tremendous research activities taking place in that field. These activities have been driven by two factors: the dramatic increase in demand for high speed signal processing, especially in consumer elec­ tronics, and the evolving microelectronic technologies. The available technology has always been one of the main factors in determining al­ gorithms, architectures, and design strategies to be followed. With every new technology, signal processing systems go through many changes in concepts, design methods, and implementation. The goal of this book is to introduce the reader to the main features of VLSI Signal Processing and the ongoing developments in this area. The focus of this book is on: • Current developments in Digital Signal Processing (DSP) pro­ cessors and architectures - several examples and case studies of existing DSP chips are discussed in...

  10. Solution-Phase Processes of Macromolecular Crystallization

    Science.gov (United States)

    Pusey, Marc L.; Minamitani, Elizabeth Forsythe

    2004-01-01

    We have proposed, for the tetragonal form of chicken egg lysozyme, that solution phase assembly processes are needed to form the growth units for crystal nucleation and growth. The starting point for the self-association process is the monomeric protein, and the final crystallographic symmetry is defined by the initial dimerization interactions of the monomers and subsequent n-mers formed, which in turn are a function of the crystallization conditions. It has been suggested that multimeric proteins generally incorporate the underlying multimers symmetry into the final crystallographic symmetry. We posed the question of what happens to a protein that is known to grow as an n-mer when it is placed in solution conditions where it is monomeric. The trypsin-treated, or cut, form of the protein canavalin (CCAN) has been shown to nucleate and grow crystals as a trimer from neutral to slightly acidic solutions. Under these conditions the solution is composed almost wholly of trimers. The insoluble protein can be readily dissolved by weakly basic solution, which results in a solution that is monomeric. There are three possible outcomes to an attempt at crystallization of the protein under monomeric (high pH) conditions: 1) we will obtain the same crystals as under trimer conditions, but at different protein concentrations governed by the self association equilibria; 2) we will obtain crystals having a different symmetry, based upon a monomeric growth unit; 3) we will not obtain crystals. Obtaining the first result would be indicative that the solution-phase self-association process is critical to the crystal nucleation and growth process. The second result would be less clear, as it may also reflect a pH-dependent shift in the trimer-trimer molecular interactions. The third result, particularly for experiments in the transition pH's between trimeric and monomeric CCAN, would indicate that the monomer does not crystallize, and that solution phase self association is not part

  11. Rediscovering ancient glass technologies through the examination of opacifier crystals

    Science.gov (United States)

    Lahlil, S.; Biron, I.; Galoisy, L.; Morin, G.

    2008-07-01

    The aim of the study is to understand how antimonate opacifying crystals were obtained throughout history. Two archaeological glass productions opacified with calcium and lead antimonates are studied in this paper, in order to rediscover ancient opaque glass technologies: Roman mosaic tesserae (1st cent. B.C. 4th cent. A.D.) and Nevers lampworking glass (18th cent. A.D.). The fine examination of crystalline phases and of the vitreous matrix is undertaken using various and complementary techniques. Results are compared with a modern reference production, for which the technological process is well known. We demonstrate that Ca-antimonate opacifiers in Roman mosaic tesserae, as well as in Nevers lampworking glass, were obtained by in situ crystallization. Nevertheless, Roman and Nevers glass would have undergone different firing processes. We propose that the addition of previously synthesized crystals or the use of “anime” could be the process used to obtain Pb-antimonate opacified glass, for both productions studied. We demonstrate that CaO, PbO and Sb2O3 concentrations in the bulk compositions and in the matrices, and their evolution with the crystallinity ratio, offer robust criteria for the distinction of the opacification process used. Also, the different crystalline structures help to provide information on the experimental conditions.

  12. Simulation and optimization of fractional crystallization processes

    DEFF Research Database (Denmark)

    Thomsen, Kaj; Rasmussen, Peter; Gani, Rafiqul

    1998-01-01

    and optimization of fractional crystallization processes are shown. In one of these examples, a process with multiple steady states is analyzed. The thermodynamic model applied for describing the highly non-ideal aqueous electrolyte systems is the Extended UNIQUAC model. (C) 1998 Published by Elsevier Science Ltd....... All rights reserved....

  13. Modelling and control of crystallization process

    Directory of Open Access Journals (Sweden)

    S.K. Jha

    2017-03-01

    Full Text Available Batch crystallizers are predominantly used in chemical industries like pharmaceuticals, food industries and specialty chemicals. The nonlinear nature of the batch process leads to difficulties when the objective is to obtain a uniform Crystal Size Distribution (CSD. In this study, a linear PI controller is designed using classical controller tuning methods for controlling the crystallizer outlet temperature by manipulating the inlet jacket temperature; however, the response is not satisfactory. A simple PID controller cannot guarantee a satisfactory response that is why an optimal controller is designed to keep the concentration and temperature in a range that suits our needs. Any typical process operation has constraints on states, inputs and outputs. So, a nonlinear process needs to be operated satisfying the constraints. Hence, a nonlinear controller like Generic Model Controller (GMC which is similar in structure to the PI controller is implemented. It minimizes the derivative of the squared error, thus improving the output response of the process. Minimization of crystal size variation is considered as an objective function in this study. Model predictive control is also designed that uses advanced optimization algorithm to minimize the error while linearizing the process. Constraints are fed into the MPC toolbox in MATLAB and Prediction, Control horizons and Performance weights are tuned using Sridhar and Cooper Method. Performances of all the three controllers (PID, GMC and MPC are compared and it is found that MPC is the most superior one in terms of settling time and percentage overshoot.

  14. Liquid crystals. Oligomeric and polymeric materials for soft photonic technologies

    International Nuclear Information System (INIS)

    Coles, Marcus James

    2002-01-01

    The current pace of today's information technologies might lead the casual observer to believe that this is all new. However the reality is that, as with most things, this is really a long evolution of processes based on tried, tested and re-adapted techniques. This thesis represents 12 years of predominantly technology driven research and covers a whole range of characterising, evaluating and fabricating devices based on liquid crystalline systems. Firstly polymer liquid crystals are discussed with respect to the fabrication of a flexible substrate display based on standard printing techniques and this is shown to have improved display viewing properties over a standard polymer dispersed liquid crystal (PDLC) device. Following on from this work is presented that involves the production of regular grid arrays in isotropic polymers that are used as control structures in nematic liquid crystal systems. This progresses onto a now patented device that allows the production of robust ferroelectric devices based on PDLC technology. Whilst the development of production techniques is important for the advancement of devices it would not be possible to keep up the pace without continued research into the basic liquid crystalline systems. The final chapter reviews work currently under supervision of the author based on flexoelectric effects in symmetric bimesogens. These materials possess responses times of the order of ∼100μs with an effective optic axis switching angle that is linear with the applied field and can be in well in excess of 90 deg. (author)

  15. Conformal transistor arrays based on solution-processed organic crystals.

    Science.gov (United States)

    Zhao, Xiaoli; Zhang, Bing; Tang, Qingxin; Ding, Xueyan; Wang, Shuya; Zhou, Yuying; Tong, Yanhong; Liu, Yichun

    2017-11-13

    Conformal transistor array based on solution-processed organic crystals, which can provide sensory and scanning features for monitoring, biofeedback, and tracking of physiological function, presents one of the most promising technologies for future large-scale low-cost wearable and implantable electronics. However, it is still a huge challenge for the integration of solution-processed organic crystals into conformal FETs owing to a generally existing swelling phenomenon of the elastic materials and the lack of the corresponding device fabrication technology. Here, we present a promising route to fabricate a conformal field-effect transistor (FET) array based on solution-processed TIPS-pentacene single-crystal micro/nanowire array. By simply drop-casting the organic solution on an anti-solvent photolithography-compatible electrode with bottom-contact coplanar configuration, the transistor array can be formed and can conform onto uneven objects. Excellent electrical properties with device yield as high as 100%, field-effect mobility up to 0.79 cm 2 V -1 s -1 , low threshold voltage, and good device uniformity are demonstrated. The results open up the capability of solution-processed organic crystals for conformal electronics, suggesting their substantial promise for next-generation wearable and implantable electronics.

  16. Particle processing technology

    Science.gov (United States)

    Yoshio, Sakka

    2014-02-01

    In recent years, there has been strong demand for the development of novel devices and equipment that support advanced industries including IT/semiconductors, the environment, energy and aerospace along with the achievement of higher efficiency and reduced environmental impact. Many studies have been conducted on the fabrication of innovative inorganic materials with novel individual properties and/or multifunctional properties including electrical, dielectric, thermal, optical, chemical and mechanical properties through the development of particle processing. The fundamental technologies that are key to realizing such materials are (i) the synthesis of nanoparticles with uniform composition and controlled crystallite size, (ii) the arrangement/assembly and controlled dispersion of nanoparticles with controlled particle size, (iii) the precise structural control at all levels from micrometer to nanometer order and (iv) the nanostructural design based on theoretical/experimental studies of the correlation between the local structure and the functions of interest. In particular, it is now understood that the application of an external stimulus, such as magnetic energy, electrical energy and/or stress, to a reaction field is effective in realizing advanced particle processing [1-3]. This special issue comprises 12 papers including three review papers. Among them, seven papers are concerned with phosphor particles, such as silicon, metals, Si3N4-related nitrides, rare-earth oxides, garnet oxides, rare-earth sulfur oxides and rare-earth hydroxides. In these papers, the effects of particle size, morphology, dispersion, surface states, dopant concentration and other factors on the optical properties of phosphor particles and their applications are discussed. These nanoparticles are classified as zero-dimensional materials. Carbon nanotubes (CNT) and graphene are well-known one-dimensional (1D) and two-dimensional (2D) materials, respectively. This special issue also

  17. SiMo Ductile Iron Crystallization Process

    Directory of Open Access Journals (Sweden)

    Stawarz M.

    2017-03-01

    Full Text Available The article presents crystallization process of silicon molybdenum ductile cast iron (SiMo. The alloy with 5% silicon content and with variable amounts of Mo in a range of 0-1% was chosen for the research. The carbon content in the analysed alloys did not exceed 3,1%. The studies of crystallization process were based on thermal - derivative analysis (TDA. Chemical composition of all examined samples was analysed with the use of LECO spectrometer. Additionally, the carbon and the sulphur content was determined basing on carbon and sulphur LECO analyser. For metallographic examination, the scanning electron microscopy (SEM with EDS analyser was used. Disclosed phases have been also tested with the use of X-ray diffraction. The results allowed the description of crystallization processes of silicon molybdenum ductile cast iron using thermal - derivative analysis (TDA. Conducted studies did not allow for the clear identification of all complex phases containing molybdenum, occurring at the grain boundaries. Therefore, the further stages of the research could include the use of a transmission electron microscope to specify the description of complex compounds present in the alloy.

  18. The impact of space research on semiconductor crystal growth technology

    Science.gov (United States)

    Witt, A. F.

    1983-01-01

    Crystal growth experiments in reduced gravity environment and related ground-based research have contributed significantly to the establishment of a scientific basis for semiconductor growth from the melt. NASA-sponsored research has been instrumental in the introduction of heat pipes for heat and mass transfer control in crystal growth and in the development of magnetic field induced melt stabilization, approaches primarily responsible for recent advances in crystal growth technology.

  19. Discotic nematic liquid crystals: science and technology.

    Science.gov (United States)

    Bisoyi, Hari Krishna; Kumar, Sandeep

    2010-01-01

    The nematic phase of discotic liquid crystals, although rarely observed, has made very significant progress over the past three decades since their discovery. It has made its way from a mere scientific curiosity to application in commodities. The negative birefringence films formed by polymerized nematic discotic liquid crystals have been commercialized as compensation films to enlarge the viewing angle and enhance the contrast ratio of commonly used twisted nematic liquid-crystal displays. High strength and high performance carbon fibers for industrial applications have been obtained from the carbonaceous mesophase and a liquid-crystal display device with wide and symmetrical viewing angle has been demonstrated by using discotic nematic liquid crystals. Discotic films with patterned colours have been obtained from cholesteric lyo-mesophases of discotic liquid crystals. Various molecular architectures have been designed and synthesized to exhibit the discotic nematic phase over a wide range of temperature. This critical review focuses on the synthesis and physical properties of these fascinating materials. It deals with the structure of various nematic phases, different discotic cores exhibiting the nematic phase, novel designing and transition temperature engineering principles, alignment and physical properties, and finally the application of discotic nematic LCs as the active switching component and as optical compensation films for widening the viewing angle and contrast ratio of liquid-crystal display devices (98 references).

  20. Numerical modeling in photonic crystals integrated technology: the COPERNICUS Project

    DEFF Research Database (Denmark)

    Malaguti, Stefania; Armaroli, Andrea; Bellanca, Gaetano

    2011-01-01

    Photonic crystals will play a fundamental role in the future of optical communications. The relevance of the numerical modeling for the success of this technology is assessed by using some examples concerning the experience of the COPERNICUS Project.......Photonic crystals will play a fundamental role in the future of optical communications. The relevance of the numerical modeling for the success of this technology is assessed by using some examples concerning the experience of the COPERNICUS Project....

  1. Flat display panel in liquid crystal technology

    Science.gov (United States)

    Steinbeck, J.; Schiekel, M.; Unbehaun, R.; Herzog, H. J.; Haeberle, G.; Biskupek, R.

    1980-06-01

    Liquid crystal display panels were built using matrix configurations. With predeformed liquid crystal structures, steep electro-optic characteristics, and small on-off switching ratios, electrically controllable birefringence is obtainable. This allows the addressing of projection color matrix displays with up to 90 scanned lines in a two color representation and up to 40 lines in a four color representation at a rate of 50 frames per sec. The same holds for predeformed liquid crystals having the advantage of low operating voltages, such as commercially available CMOS IC's Matrix displays with 32 x 32 and 80 x 80 picture elements with the corresponding electronic addressing devices for projection images with controllable color were assembled. Using these twisted nematic (TN) liquid crystal displays, the possibility of color switching filters in a sequential color selection mode was investigated. An experimental setup consisting of a CRT with two color phosphor screen, a color switching filter with a TN cell, and on electronic addressing device for the synchronized switching of image signals and of the corresponding colors is described.

  2. Development of advanced Czochralski growth process to produce low cost 150 kg silicon ingots from a single crucible for technology readiness. [crystal growth

    Science.gov (United States)

    Lane, R. L.

    1981-01-01

    Six growth runs used the Kayex-Hameo Automatic Games Logic (AGILE) computer based system for growth from larger melts in the Mod CG2000. The implementation of the melt pyrometer sensor allowed for dip temperature monitoring and usage by the operator/AGILE system. Use of AGILE during recharge operations was successfully evaluated. The tendency of crystals to lose cylindrical shape (spiraling) continued to be a problem. The hygrometer was added to the Furnace Gas Analysis System and used on several growth runs. The gas chromatograph, including the integrator, was also used for more accurate carbon monoxide concentration measurements. Efforts continued for completing the automation of the total Gas Analysis System. An economic analysis, based on revised achievable straight growth rate, is presented.

  3. Fundamentals of semiconductor processing technology

    CERN Document Server

    El-Kareh, Badih

    1995-01-01

    The drive toward new semiconductor technologies is intricately related to market demands for cheaper, smaller, faster, and more reliable circuits with lower power consumption. The development of new processing tools and technologies is aimed at optimizing one or more of these requirements. This goal can, however, only be achieved by a concerted effort between scientists, engineers, technicians, and operators in research, development, and manufac­ turing. It is therefore important that experts in specific disciplines, such as device and circuit design, understand the principle, capabil­ ities, and limitations of tools and processing technologies. It is also important that those working on specific unit processes, such as lithography or hot processes, be familiar with other unit processes used to manufacture the product. Several excellent books have been published on the subject of process technologies. These texts, however, cover subjects in too much detail, or do not cover topics important to modem tech­ n...

  4. Systematic Modelling and Crystal Size Distribution Control for Batch Crystallization Processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli; Singh, Ravendra; Sin, Gürkan

    Crystallization processes form an important class of separation methods that are frequently used in the chemical, the pharmaceutical and the food industry. The specifications of the crystal product are usually given in terms of crystal size, shape and purity. In order to predict the desired cryst...

  5. Ionizing Radiation Processing Technology

    International Nuclear Information System (INIS)

    Rida Tajau; Kamarudin Hashim; Jamaliah Sharif; Ratnam, C.T.; Keong, C.C.

    2017-01-01

    This book completely brief on the basic concept and theory of ionizing radiation in polymers material processing. Besides of that the basic concept of polymerization addition, cross-linking and radiation degradation also highlighted in this informative book. All of the information is from scientific writing based on comprehensive scientific research in polymerization industry which using the radiation ionizing. It is very useful to other researcher whose study in Nuclear Sciencea and Science of Chemical and Material to use this book as a guideline for them in future scientific esearch.

  6. Plasma technology in metallurgical processing

    Energy Technology Data Exchange (ETDEWEB)

    Haile, O.

    1995-12-31

    This literature work is mainly focusing on the mechanisms of plasma technology and telling about metallurgical processing, particularly iron and steelmaking as well as the advantage of the unique properties of plasma. The main advantages of plasma technology in metallurgical operations is to direct utilization of naturally available raw materials and fuels without costly upgrading andlor beneficiation, improved environmental impact, improve process control, significant amplification of reactor and process equipment utilization and increased efficiency of raw materials, energy and man power. This literature survey is based on the publication `plasma technology in metallurgical processing` presents a comprehensive account of the physical, electrical, and mechanical aspects of plasma production and practical processing. The applications of plasma technology in metallurgical processing are covered in depth with special emphasis on developments in promising early stages. Plasma technology of today is mature in the metallurgical process applications. A few dramatic improvements are expected in the near future this giving an impetus to the technologists for the long range planning. (18 refs.) (author)

  7. Radiation processing technology in Malaysia

    International Nuclear Information System (INIS)

    Khairul Zaman Hj Mohd Dahlan

    2004-01-01

    Radiation processing technology is widely used in industry to enhance efficiency and productivity, improve product quality and competitiveness. Efforts have been made by MINT to expand the application of radiation processing technology for modification of indigenous materials such as natural rubber and rubber based products, palm oil and palm oil based products and polysaccharide into new and high value added products. This paper described MINT experiences on developing products through R and D from the laboratory to the pilot plant stage and commercialization. The paper also explained some issues and challenges that MINT encountered in the process of commercialization of its R and D results. (author)

  8. On-line monitoring of the crystallization process: relationship between crystal size and electrical impedance spectra

    International Nuclear Information System (INIS)

    Zhao, Yanlin; Yao, Jun; Wang, Mi

    2016-01-01

    On-line monitoring of crystal size in the crystallization process is crucial to many pharmaceutical and fine-chemical industrial applications. In this paper, a novel method is proposed for the on-line monitoring of the cooling crystallization process of L-glutamic acid (LGA) using electrical impedance spectroscopy (EIS). The EIS method can be used to monitor the growth of crystal particles relying on the presence of an electrical double layer on the charged particle surface and the polarization of double layer under the excitation of alternating electrical field. The electrical impedance spectra and crystal size were measured on-line simultaneously by an impedance analyzer and focused beam reflectance measurement (FBRM), respectively. The impedance spectra were analyzed using the equivalent circuit model and the equivalent circuit elements in the model can be obtained by fitting the experimental data. Two equivalent circuit elements, including capacitance ( C 2 ) and resistance ( R 2 ) from the dielectric polarization of the LGA solution and crystal particle/solution interface, are in relation with the crystal size. The mathematical relationship between the crystal size and the equivalent circuit elements can be obtained by a non-linear fitting method. The function can be used to predict the change of crystal size during the crystallization process. (paper)

  9. Molecular Imprinting Technology in Quartz Crystal Microbalance (QCM Sensors

    Directory of Open Access Journals (Sweden)

    Sibel Emir Diltemiz

    2017-02-01

    Full Text Available Molecularly imprinted polymers (MIPs as artificial antibodies have received considerable scientific attention in the past years in the field of (biosensors since they have unique features that distinguish them from natural antibodies such as robustness, multiple binding sites, low cost, facile preparation and high stability under extreme operation conditions (higher pH and temperature values, etc.. On the other hand, the Quartz Crystal Microbalance (QCM is an analytical tool based on the measurement of small mass changes on the sensor surface. QCM sensors are practical and convenient monitoring tools because of their specificity, sensitivity, high accuracy, stability and reproducibility. QCM devices are highly suitable for converting the recognition process achieved using MIP-based memories into a sensor signal. Therefore, the combination of a QCM and MIPs as synthetic receptors enhances the sensitivity through MIP process-based multiplexed binding sites using size, 3D-shape and chemical function having molecular memories of the prepared sensor system toward the target compound to be detected. This review aims to highlight and summarize the recent progress and studies in the field of (biosensor systems based on QCMs combined with molecular imprinting technology.

  10. Molecular Imprinting Technology in Quartz Crystal Microbalance (QCM) Sensors.

    Science.gov (United States)

    Emir Diltemiz, Sibel; Keçili, Rüstem; Ersöz, Arzu; Say, Rıdvan

    2017-02-24

    Molecularly imprinted polymers (MIPs) as artificial antibodies have received considerable scientific attention in the past years in the field of (bio)sensors since they have unique features that distinguish them from natural antibodies such as robustness, multiple binding sites, low cost, facile preparation and high stability under extreme operation conditions (higher pH and temperature values, etc.). On the other hand, the Quartz Crystal Microbalance (QCM) is an analytical tool based on the measurement of small mass changes on the sensor surface. QCM sensors are practical and convenient monitoring tools because of their specificity, sensitivity, high accuracy, stability and reproducibility. QCM devices are highly suitable for converting the recognition process achieved using MIP-based memories into a sensor signal. Therefore, the combination of a QCM and MIPs as synthetic receptors enhances the sensitivity through MIP process-based multiplexed binding sites using size, 3D-shape and chemical function having molecular memories of the prepared sensor system toward the target compound to be detected. This review aims to highlight and summarize the recent progress and studies in the field of (bio)sensor systems based on QCMs combined with molecular imprinting technology.

  11. Beam Technologies for Integrated Processing

    Science.gov (United States)

    1992-03-01

    magnetic media on tape to optical coatings on polymeric materials. The technologies have progressed in the area of PVD to plasma-assisted CVD ( PACVD ...evaporation of boric acid in an ammonia plasma. Enhanced CVD processes have taken the form of either thermally assisted CVD or PACVD for thermal and electron...temperature-induced irreversible structural or electrical changes. A further process improvement, known as remote PACVD , is used to protect both the

  12. Distillation process using microchannel technology

    Science.gov (United States)

    Tonkovich, Anna Lee [Dublin, OH; Simmons, Wayne W [Dublin, OH; Silva, Laura J [Dublin, OH; Qiu, Dongming [Carbondale, IL; Perry, Steven T [Galloway, OH; Yuschak, Thomas [Dublin, OH; Hickey, Thomas P [Dublin, OH; Arora, Ravi [Dublin, OH; Smith, Amanda [Galloway, OH; Litt, Robert Dwayne [Westerville, OH; Neagle, Paul [Westerville, OH

    2009-11-03

    The disclosed invention relates to a distillation process for separating two or more components having different volatilities from a liquid mixture containing the components. The process employs microchannel technology for effecting the distillation and is particularly suitable for conducting difficult separations, such as the separation of ethane from ethylene, wherein the individual components are characterized by having volatilities that are very close to one another.

  13. Investigation of lactose crystallization process during condensed milk cooling using native vacuum-crystallizer

    Directory of Open Access Journals (Sweden)

    E. I. Dobriyan

    2016-01-01

    Full Text Available One of the most general defects of condensed milk with sugar is its consistency heterogeneity – “candying”. The mentioned defect is conditioned by the presence of lactose big crystals in the product. Lactose crystals size up to 10 µm is not organoleptically felt. The bigger crystals impart heterogeneity to the consistency which can be evaluated as “floury”, “sandy”, “crunch on tooth”. Big crystals form crystalline deposit on the can or industrial package bottom in the form of thick layer. Industrial processing of the product with the defective process of crystallization results in the expensive equipment damage of the equipment at the confectionary plant accompanied with heavy losses. One of the factors influencing significantly lactose crystallization is the product cooling rate. Vacuum cooling is the necessary condition for provision of the product consistency homogeneity. For this purpose the vacuum crystallizers of “Vigand” company, Germany, are used. But their production in the last years has been stopped. All-Russian dairy research institute has developed “The references for development of the native vacuum crystallizer” according to which the industrial model has been manufactured. The produced vacuum – crystallizer test on the line for condensed milk with sugar production showed that the product cooling on the native vacuum-crystallizer guarantees production of the finished product with microstructure meeting the requirements of State standard 53436–2009 “Canned Milk. Milk and condensed cream with sugar”. The carried out investigations evidences that the average lactose crystals size in the condensed milk with sugar cooled at the native crystallizer makes up 6,78 µm. The granulometric composition of the product crystalline phase cooled at the newly developed vacuum-crystallizer is completely identical to granulometric composition of the product cooled at “Vigand” vacuum-crystallizer.

  14. Technology development life cycle processes.

    Energy Technology Data Exchange (ETDEWEB)

    Beck, David Franklin

    2013-05-01

    This report and set of appendices are a collection of memoranda originally drafted in 2009 for the purpose of providing motivation and the necessary background material to support the definition and integration of engineering and management processes related to technology development. At the time there was interest and support to move from Capability Maturity Model Integration (CMMI) Level One (ad hoc processes) to Level Three. As presented herein, the material begins with a survey of open literature perspectives on technology development life cycles, including published data on %E2%80%9Cwhat went wrong.%E2%80%9D The main thrust of the material presents a rational expose%CC%81 of a structured technology development life cycle that uses the scientific method as a framework, with further rigor added from adapting relevant portions of the systems engineering process. The material concludes with a discussion on the use of multiple measures to assess technology maturity, including consideration of the viewpoint of potential users.

  15. Liquid crystals based sensing platform-technological aspects.

    Science.gov (United States)

    Hussain, Zakir; Qazi, Farah; Ahmed, Muhammad Imran; Usman, Adil; Riaz, Asim; Abbasi, Amna Didar

    2016-11-15

    In bulk phase, liquid crystalline molecules are organized due to non-covalent interactions and due to delicate nature of the present forces; this organization can easily be disrupted by any small external stimuli. This delicate nature of force balance in liquid crystals organization forms the basis of Liquid-crystals based sensing scheme which has been exploited by many researchers for the optical visualization and sensing of many biological interactions as well as detection of number of analytes. In this review, we present not only an overview of the state of the art in liquid crystals based sensing scheme but also highlight its limitations. The approaches described below revolve around possibilities and limitations of key components of such sensing platform including bottom substrates, alignments layers, nature and type of liquid crystals, sensing compartments, various interfaces etc. This review also highlights potential materials to not only improve performance of the sensing scheme but also to bridge the gap between science and technology of liquid crystals based sensing scheme. Copyright © 2016 Elsevier B.V. All rights reserved.

  16. A systematic framework for design of process monitoring and control (PAT) systems for crystallization processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin; Sin, Gürkan; Gernaey, Krist

    2013-01-01

    A generic computer-aided framework for systematic design of a process monitoring and control system for crystallization processes has been developed to study various aspects of crystallization operations.The systematic design framework contains a generic crystallizer modelling toolbox, a tool for...

  17. Crystallization processes derived from the interaction of urine and dolostone

    Science.gov (United States)

    Cámara, Beatriz; Alvarez de Buergo, Monica; Fort, Rafael

    2015-04-01

    (these 3 sections, a) b) c) represent the first one centimeter of the specimen from the bottom); d) and the fourth and top section, which shows no influence by the effect of urine capillary absorption. The obtained results showed, from bottom to top, the following crystallized salts: a) abundant prismatic crystals enriched in P and Ca (calcium phosphate); b) amorphous round-shaped potassium sulfate crystals and cubic sodium chloride crystals embedded in an organic matrix; d) cubic sodium chloride crystals are dominant. In the unaffected area, no other crystals were detected different from the carbonate minerals forming the rock. These results are in accordance to which has already been published by the authors in granitic materials (Cámara et al 2014). Acknowledgements: to Geomateriales 2 programme (S2013/MIT-2914) funded by the Community of Madrid. Cámara B., Alvarez de Buergo, M.; Fort, R.; Ascaso, C. de los Rios, A.; Gomez-Heras, M. 2014. Another source of soluble salts in urban environments due to recent social behaviour pattern in historical centres. In: Science, Technology and Cultural Heritage (edited by M.A. Rogerio-Candelera), 89-94. CRC Press-Balkema, Taylor and Francis. ISBN 9781138027442 - CAT# K25502

  18. Process for Forming a High Temperature Single Crystal Canted Spring

    Science.gov (United States)

    DeMange, Jeffrey J (Inventor); Ritzert, Frank J (Inventor); Nathal, Michael V (Inventor); Dunlap, Patrick H (Inventor); Steinetz, Bruce M (Inventor)

    2017-01-01

    A process for forming a high temperature single crystal canted spring is provided. In one embodiment, the process includes fabricating configurations of a rapid prototype spring to fabricate a sacrificial mold pattern to create a ceramic mold and casting a canted coiled spring to form at least one canted coil spring configuration based on the ceramic mold. The high temperature single crystal canted spring is formed from a nickel-based alloy containing rhenium using the at least one coil spring configuration.

  19. Single crystal Processing and magnetic properties of gadolinium nickel

    Energy Technology Data Exchange (ETDEWEB)

    Shreve, Andrew John [Iowa State Univ., Ames, IA (United States)

    2012-01-01

    GdNi is a rare earth intermetallic material that exhibits very interesting magnetic properties. Spontaneous magnetostriction occurs in GdNi at T{sub C}, on the order of 8000ppm strain along the c-axis and only until very recently the mechanism causing this giant magnetostriction was not understood. In order to learn more about the electronic and magnetic structure of GdNi, single crystals are required for anisotropic magnetic property measurements. Single crystal processing is quite challenging for GdNi though since the rare-earth transition-metal composition yields a very reactive intermetallic compound. Many crystal growth methods are pursued in this study including crucible free methods, precipitation growths, and specially developed Bridgman crucibles. A plasma-sprayed Gd2O3 W-backed Bridgman crucible was found to be the best means of GdNi single crystal processing. With a source of high-quality single crystals, many magnetization measurements were collected to reveal the magnetic structure of GdNi. Heat capacity and the magnetocaloric effect are also measured on a single crystal sample. The result is a thorough report on high quality single crystal processing and the magnetic properties of GdNi.

  20. Technologies to support industrial processes

    International Nuclear Information System (INIS)

    Palazzi, G.; Savelli, D.

    1989-05-01

    Control and measuring techniques applied to industry have the common aim of increasing safety, reliability and plant availability. The industrial monitoring system needs a lot of sensors, whose signals, elaborated and interpreted, allow one to define the best working condition; moreover control instruments perform a diagnosis related to damages and breakages. The Experimental Engineering Division of ENEA's Thermal Reactor Department has developed sensors and measuring apparatus and has acquired advanced control techniques. All these systems, containing an original software, have been applied to industrial process problems and/or to experimental facilities both to increase reliability and to understand better process physics. Division activities are grouped in four sectors: non-destructive examinations (ultrasonic, eddy current, thermography, holographic interpherometry, penetrant liquids and magnetoscopy); innovative sensors (heated thermocouples, optical fiber sensors); advanced measuring systems (laser technology for fluidodynamic measures, nuclear radiation techniques, infrared measuring, mass spectrometer, hot-film anemometer, chromatographic apparatus); advanced technologies for diagnosis and signal analysis (digital image processing, statistical analysis). (author)

  1. Membrane processes in nuclear technologies

    International Nuclear Information System (INIS)

    Zakrzewska-Trznadel, G.

    2006-01-01

    The treatment of radioactive wastes is necessary taking into account the potential hazard of radioactive substances to human health and surrounding environment. The choice of appropriate technology depends on capital and operational costs, wastes amount and their characteristics, appointed targets of the process, e.g. the values of decontamination factors and volume reduction coefficients. The conventional technologies applied for radioactive waste processing, such as precipitation coupled with sedimentation, ion exchange and evaporation have many drawbacks. These include high energy consumption and formation of secondary wastes, e.g. the sludge from sediment tanks, spent ion exchange adsorbents and regeneration solutions. There are also many limitations of such processes, i.e. foaming and drop entrainment in evaporators, loses of solvents and production of secondary wastes in solvent extraction or bed clogging in ion exchange columns. Membrane processes as the newest achievement of the process engineering can successfully supersede many non-effective, out-of-date methods. But in some instances they can also complement these methods whilst improving the parameters of effluents and purification economy. This monograph presents own research data on the application of recent achievements in the area of membrane processes for solving selected problems in nuclear technology. Relatively big space was devoted to the use of membrane processing of low and intermediate radioactive liquid wastes because of numerous applications of these processes in nuclear centres over the world and also because of the interests of the author that was reflected by her recent research projects and activity. This work presents a review on the membrane methods recently introduced into the nuclear technology against the background of the other, commonly applied separation techniques, with indications of the possibilities and prospects for their further developments. Particular attention was paid

  2. Dissolution enhancement of Deflazacort using hollow crystals prepared by antisolvent crystallization process.

    Science.gov (United States)

    Paulino, A S; Rauber, G; Campos, C E M; Maurício, M H P; de Avillez, R R; Capobianco, G; Cardoso, S G; Cuffini, S L

    2013-05-13

    Deflazacort (DFZ), a derivate of prednisolone, is a poorly soluble drug which has been proposed to have major advantages over other corticosteroids. Poorly soluble drugs present limited bioavailability due to their low solubility and dissolution rate and several strategies have been developed in order to find ways to improve them. In general, pharmaceutical laboratories use a micronized process to reduce the particle size in order to increase the dissolution of the drugs. However, this process causes changes such as polymorphic transitions, particle agglomeration and a reduction in fluidity and wettability. These solid-state properties affect the dissolution behavior and stability performance of drugs. Crystallization techniques are widely used in the pharmaceutical industry and antisolvent crystallization has been used to obtain ultrafine particles. In this study, DFZ was investigated in terms of its antisolvent crystallization in different solvents and under various preparation conditions (methanol/water ratio, stirring and evaporation rate, etc.), in order to compare the physicochemical properties between crystallized samples and raw materials available on the Brazilian market with and without micronization. Crystalline structure, morphology, and particle size, and their correlation with the Intrinsic Dissolution Rate (IDR) and dissolution profile as relevant biopharmaceutical properties were studied. Crystallization conditions were achieved which provided crystalline samples of hollow-shaped crystals with internal channels, which increased the dissolution rate of DFZ. The antisolvent crystallization process allowed the formation of hollow crystals, which demonstrated a better dissolution profile than the raw material (crystalline and micronized), making this a promising technique as a crystallization strategy for improving the dissolution and thus the bioavailability of poorly soluble drugs. Copyright © 2013 Elsevier B.V. All rights reserved.

  3. Stimulated Brillouin processes in crystals and glasses

    International Nuclear Information System (INIS)

    Faris, G.W.; Hickman, A.P.

    1992-02-01

    The basic physics and material properties needed to describe and predict the Brillouin gain for a variety of materials have been investigated. Lawrence Livermore National Laboratory (LLNL) has identified transverse stimulated Brillouin scattering (SBS) as an important limiting mechanism in high power laser fusion systems. At sufficiently high laser intensities, SBS drives acoustic vibrations that can damage optical components. SRI has performed measurements and developed the corresponding theory for stimulated Brillouin gain spectroscopy in anisotropic crystals. Absolute Brillouin steady-state gain coefficients, linewidths, and frequency shifts have been determined at 532 nm for a number of optical materials of interest to LLNL. This knowledge can be used to select optical materials and devise suppression schemes that will allow much higher laser fluences to be used in laser fusion

  4. Downstream Processability of Crystal Habit-Modified Active Pharmaceutical Ingredient

    DEFF Research Database (Denmark)

    Pudasaini, Nawin; Upadhyay, Pratik Pankaj; Parker, Christian Richard

    2017-01-01

    Efficient downstream processing of active pharmaceutical ingredients (APIs) can depend strongly on their particulate properties, such as size and shape distributions. Especially in drug products with high API content, needle-like crystal habit of an API may show compromised flowability...... and tabletability, creating significant processability difficulties on a production scale. However, such a habit can be adapted to the needs of downstream processing. To this end, we modified the needle-like crystal habit of the model API 5-aminosalicylic acid (5-ASA). This study reports processability assessment...

  5. European consumers' acceptance of beef processing technologies

    DEFF Research Database (Denmark)

    de Barcellos, Marcia Dutra; Kügler, Jens Oliver; Grunert, Klaus G.

    2010-01-01

    ' beef were considered negative outcomes of technological innovations. Beef processing technologies were predominantly perceived as valuable options for convenience shoppers and less demanding consumers. Overall, respondents supported the development of 'non-invasive' technologies that were able...

  6. Commercial Parts Technology Qualification Processes

    Science.gov (United States)

    Cooper, Mark S.

    2013-01-01

    Many high-reliability systems, including space systems, use selected commercial parts (including Plastic Encapsulated Microelectronics or PEMs) for unique functionality, small size, low weight, high mechanical shock resistance, and other factors. Predominantly this usage is subjected to certain 100% tests (typically called screens) and certain destructive tests usually (but not always) performed on the flight lot (typically called qualification tests). Frequently used approaches include those documented in EEE-INST-002 and JPL DocID62212 (which are sometimes modified by the particular aerospace space systems manufacturer). In this study, approaches from these documents and several space systems manufacturers are compared to approaches from a launch systems manufacturer (SpaceX), an implantable medical electronics manufacturer (Medtronics), and a high-reliability transport system process (automotive systems). In the conclusions section, these processes are outlined for all of these cases and presented in tabular form. Then some simple comparisons are made. In this introduction section, the PEM technology qualification process is described, as documented in EEE-INST-002 (written by the Goddard Space Flight Center, GSFC), as well as the somewhat modified approach employed at the Jet Propulsion Laboratory (JPL). Approaches used at several major NASA contractors are also described

  7. Management of Technology - a political process approach

    DEFF Research Database (Denmark)

    Koch, Christian

    1999-01-01

    Most management of technology writings fail to address enterprise developments as political processes, where visions, coalitions and emergence are central features. The paper report of a participants observation study of management of technology processes.......Most management of technology writings fail to address enterprise developments as political processes, where visions, coalitions and emergence are central features. The paper report of a participants observation study of management of technology processes....

  8. Photodynamic Processes in Fluoride Crystals Doped with Ce3+

    Directory of Open Access Journals (Sweden)

    Pavlov V.V.

    2015-01-01

    Full Text Available Integrated studies of photoelectric phenomena and their associated photodynamic processes in LiCaAlF6, LiLuF4, LiYF4, LiY0,5Lu0,5F4, SrAlF5 crystals doped with Ce3+ ions have been carried out using the combination of the methods of optical and dielectric spectroscopy. The numerical values of the basic parameters of photodynamic processes and their spectral dependence in 240 – 310 nm spectral range are evaluated. It has been shown that the most probable process, which leads to the photoionization of Ce3+ ions in LiYxLu1-xF4:Ce3+ (x=0; 0,5; 1 and LiCaAlF6:Ce3+ crystals, is excited-state absorption to the states of mixed configurations of Ce3+ ions localized near/in the conduction band of crystal.

  9. Advances in fntd technology: Instrumentation, image processing and applications

    Science.gov (United States)

    Bartz, James Andrew

    Fluorescent Nuclear Track Detectors (FNTDs), based on Al2O 3:C,Mg single crystal material, enable diffraction limited imaging of ionization patterns. This fast, luminescent material is thermally and optically stable. This work expands and assesses the capability of FNTD technology to measure radiation dose quickly and accurately, especially neutron radition. Developments in FNTD instrumentation, software, image reconstruction, image processing and data processing improved ease of use, productivity and reliability and brought the technology into commercial viability. Descriptions of these developments are presented. Additionally, these developments were assessed and were found to comply with ANSI and ISO standards for personnel neutron dosimetry. (Abstract shortened by ProQuest.).

  10. Effect of process parameters on crystal size and morphology of lactose in ultrasound-assisted crystallization

    Energy Technology Data Exchange (ETDEWEB)

    Patel, S.R.; Murthy, Z.V.P. [Chemical Engineering Department, S.V. National Institute of Technology, Surat - 395 007, Gujarat (India)

    2011-03-15

    {alpha}-lactose monohydrate is widely used as a pharmaceutical excipient. Drug delivery system requires the excipient to be of narrow particle size distribution with regular particle shape. Application of ultrasound is known to increase or decrease the growth rate of certain crystal faces and controls the crystal size distribution. In the present paper, effect of process parameters such as sonication time, anti-solvent concentration, initial lactose concentration and initial pH of sample on lactose crystal size, shape and thermal transition temperature was studied. The parameters were set according to the L{sub 9}-orthogonal array method at three levels and recovered lactose from whey by sonocrystallization. The recovered lactose was analyzed by particle size analyzer, scanning electron microscopy and differential scanning calorimeter. It was found that the morphology of lactose crystal was rod/needle like shape. Crystal size distribution of lactose was observed to be influenced by different process parameters. From the results of analysis of variance, the sonication time interval was found to be the most significant parameter affecting the volume median diameter of lactose with the highest percentage contribution (74.28%) among other parameters. (copyright 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  11. Photonic Crystal Nanocavity Devices for Nonlinear Signal Processing

    DEFF Research Database (Denmark)

    Yu, Yi

    , membranization of InP/InGaAs structure and wet etching. Experimental investigation of the switching dynamics of InP photonic crystal nanocavity structures are carried out using short-pulse homodyne pump-probe techniques, both in the linear and nonlinear region where the cavity is perturbed by a relatively small......This thesis deals with the investigation of InP material based photonic crystal cavity membrane structures, both experimentally and theoretically. The work emphasizes on the understanding of the physics underlying the structures’ nonlinear properties and their applications for all-optical signal...... processing. Based on the previous fabrication recipe developed in our III-V platform, several processing techniques are developed and optimized for the fabrication of InP photonic crystal membrane structures. Several key issues are identified to ensure a good device quality such as air hole size control...

  12. Buried waste integrated demonstration technology integration process

    International Nuclear Information System (INIS)

    Ferguson, J.S.; Ferguson, J.E.

    1992-04-01

    A Technology integration Process was developed for the Idaho National Energy Laboratories (INEL) Buried Waste Integrated Demonstration (BWID) Program to facilitate the transfer of technology and knowledge from industry, universities, and other Federal agencies into the BWID; to successfully transfer demonstrated technology and knowledge from the BWID to industry, universities, and other Federal agencies; and to share demonstrated technologies and knowledge between Integrated Demonstrations and other Department of Energy (DOE) spread throughout the DOE Complex. This document also details specific methods and tools for integrating and transferring technologies into or out of the BWID program. The document provides background on the BWID program and technology development needs, demonstrates the direction of technology transfer, illustrates current processes for this transfer, and lists points of contact for prospective participants in the BWID technology transfer efforts. The Technology Integration Process was prepared to ensure compliance with the requirements of DOE's Office of Technology Development (OTD)

  13. Stability and servo-control of the crystal pulling process

    International Nuclear Information System (INIS)

    Johansen, T.H.

    1990-11-01

    The paper analyzes why the crystal pulling process needs servo-control, and how it can be implemented. Special emphasis is put on the fundamental question of inherent stability, and how to interpret the signal from a balance when the weighing method is used for cystal diameter detection. 15 refs., 13 figs

  14. Iron crystallization in a fluidized-bed Fenton process.

    Science.gov (United States)

    Boonrattanakij, Nonglak; Lu, Ming-Chun; Anotai, Jin

    2011-05-01

    The mechanisms of iron precipitation and crystallization in a fluidized-bed reactor were investigated. Within the typical Fenton's reagent dosage and pH range, ferric ions as a product from ferrous ion oxidation would be supersaturated and would subsequently precipitate out in the form of ferric hydroxide after the initiation of the Fenton reaction. These precipitates would simultaneously crystallize onto solid particles in a fluidized-bed Fenton reactor if the precipitation proceeded toward heterogeneous nucleation. The heterogeneous crystallization rate was controlled by the fluidized material type and the aging/ripening period of the crystallites. Iron crystallization onto the construction sand was faster than onto SiO(2), although the iron removal efficiencies at 180 min, which was principally controlled by iron hydroxide solubility, were comparable. To achieve a high iron removal rate, fluidized materials have to be present at the beginning of the Fenton reaction. Organic intermediates that can form ferro-complexes, particularly volatile fatty acids, can significantly increase ferric ion solubility, hence reducing the crystallization performance. Therefore, the fluidized-bed Fenton process will achieve exceptional performance with respect to both organic pollutant removal and iron removal if it is operated with the goal of complete mineralization. Crystallized iron on the fluidized media could slightly retard the successive crystallization rate; thus, it is necessary to continuously replace a portion of the iron-coated bed with fresh media to maintain iron removal performance. The iron-coated construction sand also had a catalytic property, though was less than those of commercial goethite. Copyright © 2011 Elsevier Ltd. All rights reserved.

  15. Multi-dimensional population balance models of crystallization processes

    DEFF Research Database (Denmark)

    Meisler, Kresten Troelstrup; von Solms, Nicolas

    A generic and model-based framework for batch cooling crystallization operations has been extended to incorporate continuous and fed-batch processes. Modules for the framework have been developed, including a module for reactions, allowing the study of reactive crystallization within the framework......, analyzed, used for simulation and stored again. The model library facilitates comparison of expressions for kinetic phenomena and is tightly integrated with the model analysis tools of the framework.Through the framework, a model for a crystallization operation may be systematically generated...... and parameters for the simulation can be found in the database. A procedure for parameter estimation has been illustrated based on experimental work. The identifiability of the models has been discussed in relation to parameter estimation using sensitivity analysis. Some important identifiability issues have...

  16. A Generic Framework for Systematic Design of Process Monitoring and Control System for Crystallization Processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin; Meisler, Kresten Troelstrup; Sin, Gürkan

    2012-01-01

    Crystallization processes have a wide range of application as a solid-liquid separation technique in the chemical, the pharmaceutical and the food industries, due to the fact that high quality crystalline products can be produced. The main specifications of the crystal product are usually given i...

  17. 76 FR 37344 - Technology Evaluation Process

    Science.gov (United States)

    2011-06-27

    ...-NOA-0039] Technology Evaluation Process AGENCY: Office of Energy Efficiency and Renewable Energy... evaluation process. The stakeholder comment period is being extended an additional 30 days to give potential... seeks comments and information related to a commercial buildings technology evaluation process. DOE is...

  18. Perspectives on Multienzyme Process Technology

    DEFF Research Database (Denmark)

    Santacoloma, Paloma A.; Woodley, John M.

    2014-01-01

    There is little doubt that chemical processing of the future will involve an increasing number of biocatalytic processes using more than one enzyme. There are good reasons for developing such innovative biocatalytic processes and interesting new biocatalyst and process options will be introduced....

  19. Supercritical fluid technologies for ceramic-processing applications

    International Nuclear Information System (INIS)

    Matson, D.W.; Smith, R.D.

    1989-01-01

    This paper reports on the applications of supercritical fluid technologies for ceramic processing. The physical and chemical properties of these densified gases are summarized and related to their use as solvents and processing media. Several areas are identified in which specific ceramic processes benefit from the unique properties of supercritical fluids. The rapid expansion of supercritical fluid solutions provides a technique for producing fine uniform powders and thin films of widely varying materials. Supercritical drying technologies allow the formation of highly porous aerogel products with potentially wide application. Hydrothermal processes leading to the formation of large single crystals and microcrystalline powders can also be extended into the supercritical regime of water. Additional applications and potential applications are identified in the areas of extraction of binders and other additives from ceramic compacts, densification of porous ceramics, the formation of powders in supercritical micro-emulsions, and in preceramic polymer processing

  20. Process technologies for water desalination

    International Nuclear Information System (INIS)

    Ramilo, Lucia B.; Gomez de Soler, Susana M.; Coppari, Norberto R.

    2003-01-01

    The use of the nuclear energy for simultaneous electricity and potable water production is an attractive, technically feasible, and safe alternative to fossil energy options. In Argentina the nuclear desalination option is being studied together with the alternative uses of the innovative advanced Argentinean CAREM reactor, in the research contract CNEA - IAEA to evaluate projects of nuclear desalination. The objective and scope of this work is to know the advantages and disadvantages of each desalination technology, distinctive characteristics of each of them, that make them adapt better to different uses and outline conditions and analysis of related antecedents of its use in the world. In this report a summarized description of those technologies is included by way of introduction, so as to highlight the main advantages and disadvantages of each of them. The improvements and innovations found in the last years for the different technologies are also included. (author)

  1. Processing techniques applying laser technology

    International Nuclear Information System (INIS)

    Yamada, Yuji; Makino Yoshinobu

    2000-01-01

    The requirements for the processing of nuclear energy equipment include high precision, low distortion, and low heat input. Toshiba has developed laser processing techniques for cutting, welding, and surface heat treatment of nuclear energy equipment because the zone affected by distortion and heat in laser processing is very small. Laser processing contributes to the manufacturing of high-quality and high-reliability equipment and reduces the manufacturing period. (author)

  2. Magmatic Processes and Systems Deduced from Single Crystals

    Science.gov (United States)

    Davidson, J.; Bezard, R. C.; Morgan, D. J.; Ginibre, C.

    2014-12-01

    When crystals grow in liquids the composition of their outermost layer will reflect that of the host with which they are in equilibrium and will therefore record the liquid composition, pressure and temperature.. Following separation from their sources, magmas differentiate. This change in liquid composition is driven largely by crystallisation in response to cooling or decompression. Other open system processes such as mixing and contamination are common. These can lead to abrupt changes in trace element and isotopic composition, accompanied by petrographic features, such as dissolution surfaces or zones of melt inclusions. Where such careful mineral-scale studies have been performed, the prevalence of open system processes is clear. In many cases these are shown by core-rim isotopic variations. Crystal-scale compositional variations in the context of whole rock compositions and petrography have allowed us to show crustal assimilation even from regions of supposedly oceanic crust such as the Lesser Antilles. In tandem with tracking magma evolution, core-rim analyses of appropriate crystals have also provided diffusion profiles which reflect timescales of magmatic processes. A key point, long recognised by Bruce Marsh, is that in situ geochemical data should be considered in a petrographic context in order to gain the most (and most credible) insights on the workings of magma systems from hand specimen to whole volcano/pluton scales: The petrographic microscope is not dead yet Identification of magmatic processes from in situ scrutiny allows us to synthesise the architectures and inner workings of magma systems. The evidence for interaction among magmas in many systems is compelling and suggests that many exist as stacked dike-sill arrangements with wall-rock focussed crystal growth and mush zones. These are consistent with many of the systematics suggested some time ago by Bruce Marsh

  3. Determinants of improved cassava processing technologies' (ICPT ...

    African Journals Online (AJOL)

    Determinants of improved cassava processing technologies' (ICPT) utilization among rural processors in Oyo State. ... Journal of Agriculture, Forestry and the Social Sciences ... Abstract. The study examined the factors determining the utilization of Improved Cassava Processing Technologies (ICPTs) in Oyo State, Nigeria.

  4. Radioactive Dry Process Material Treatment Technology Development

    Energy Technology Data Exchange (ETDEWEB)

    Park, J. J.; Hung, I. H.; Kim, K. K. (and others)

    2007-06-15

    The project 'Radioactive Dry Process Material Treatment Technology Development' aims to be normal operation for the experiments at DUPIC fuel development facility (DFDF) and safe operation of the facility through the technology developments such as remote operation, maintenance and pair of the facility, treatment of various high level process wastes and trapping of volatile process gases. DUPIC Fuel Development Facility (DFDF) can accommodate highly active nuclear materials, and now it is for fabrication of the oxide fuel by dry process characterizing the proliferation resistance. During the second stage from march 2005 to February 2007, we carried out technology development of the remote maintenance and the DFDF's safe operation, development of treatment technology for process off-gas, and development of treatment technology for PWR cladding hull and the results was described in this report.

  5. The Center for Environmental Technology Innovative Technology Screening Process

    International Nuclear Information System (INIS)

    Bertrand, C.M.

    1995-02-01

    The Center for Environmental Technology's (CET) mission is to provide a fully integrated system for accelerated evaluation, development, commercialization, and public acceptance of creative environmental solutions which match the foremost demands in today's environmentally sensitive world. In short, CET will create a means to provide quick, effective solutions for environmental needs. To meet this mission objective, CET has created a unique and innovative approach to eliminating the usual barriers in developing and testing environmental technologies. The approach paves the way for these emerging, cutting-edge technologies by coordinating environmental restoration and waste management activities of industry, universities, and the government to: efficiently and effectively transfer technology to these users, provide market-driven, cost-effective technology programs to the public and DOE, and aid in developing innovative ideas by initiating efforts between DOE facilities and private industry. The central part to this mission is selecting and evaluating specific innovative technologies for demonstration and application at United States Department of Energy (DOE) installations. The methodology and criteria used for this selection, which is called the CET Innovative Technology Screening Process, is the subject of this paper. The selection criteria used for the screening process were modeled after other DOE technology transfer programs and were further developed by CET's Technology Screening and Evaluation Board (TSEB). The process benefits both CET and the proposing vendors by providing objective selection procedures based on predefined criteria. The selection process ensures a rapid response to proposing vendors, all technologies will have the opportunity to enter the selection process, and all technologies are evaluated on the same scale and with identical criteria

  6. Separation process using microchannel technology

    Science.gov (United States)

    Tonkovich, Anna Lee [Dublin, OH; Perry, Steven T [Galloway, OH; Arora, Ravi [Dublin, OH; Qiu, Dongming [Bothell, WA; Lamont, Michael Jay [Hilliard, OH; Burwell, Deanna [Cleveland Heights, OH; Dritz, Terence Andrew [Worthington, OH; McDaniel, Jeffrey S [Columbus, OH; Rogers, Jr; William, A [Marysville, OH; Silva, Laura J [Dublin, OH; Weidert, Daniel J [Lewis Center, OH; Simmons, Wayne W [Dublin, OH; Chadwell, G Bradley [Reynoldsburg, OH

    2009-03-24

    The disclosed invention relates to a process and apparatus for separating a first fluid from a fluid mixture comprising the first fluid. The process comprises: (A) flowing the fluid mixture into a microchannel separator in contact with a sorption medium, the fluid mixture being maintained in the microchannel separator until at least part of the first fluid is sorbed by the sorption medium, removing non-sorbed parts of the fluid mixture from the microchannel separator; and (B) desorbing first fluid from the sorption medium and removing desorbed first fluid from the microchannel separator. The process and apparatus are suitable for separating nitrogen or methane from a fluid mixture comprising nitrogen and methane. The process and apparatus may be used for rejecting nitrogen in the upgrading of sub-quality methane.

  7. Process Guide for Deburring Technologies

    Energy Technology Data Exchange (ETDEWEB)

    Frey, David L.

    2012-10-25

    This report is an updated and consolidated view of the current deburring processes at the Kansas City Plant (KCP). It includes specific examples of current burr problems and the methods used for their detection. Also included is a pictorial review of the large variety of available deburr tools, along with a complete numerical listing of existing tools and their descriptions. The process for deburring all the major part feature categories is discussed.

  8. Photonic crystals: features and applications (physics research and technology)

    CERN Document Server

    2013-01-01

    The present book is focused on the study of unprecedented control and manipulation of light by photonic crystals (PCs) and their applications. These are micro- or usually nano-structures composed of periodic indexes of refraction of dielectrics with high refractive index contrast. They exhibit optical frequency band gaps in analogy to electronic bands for a periodic potential of a semiconductor crystal lattice. The gemstone opal and butterflys feathers colours are already referred to as natural examples of photonic crystals. The characteristics of such supper-lattices were first reported by Yablonovitch in 1987. The exploitation of photonic crystals is a promising tool in communication, sensors, optical computing, and nanophotonics. Discussed are the various features of one-dimensional (1D) and two-dimensional (2D) photonic crystals, photonic quasi crystals, heterostuctures and PC fibres under a variety of conditions using several materials, and metamaterials. It also focuses on the applications of PCs in opt...

  9. Electrochromic Windows: Advanced Processing Technology

    Energy Technology Data Exchange (ETDEWEB)

    SAGE Electrochromics, Inc

    2006-12-13

    This project addresses the development of advanced fabrication capabilities for energy saving electrochromic (EC) windows. SAGE EC windows consist of an inorganic stack of thin films deposited onto a glass substrate. The window tint can be reversibly changed by the application of a low power dc voltage. This property can be used to modulate the amount of light and heat entering buildings (or vehicles) through the glazings. By judicious management of this so-called solar heat gain, it is possible to derive significant energy savings due to reductions in heating lighting, and air conditioning (HVAC). Several areas of SAGE’s production were targeted during this project to allow significant improvements to processing throughput, yield and overall quality of the processing, in an effort to reduce the cost and thereby improve the market penetration. First, the overall thin film process was optimized to allow a more robust set of operating points to be used, thereby maximizing the yield due to the thin film deposition themselves. Other significant efforts aimed at improving yield were relating to implementing new procedures and processes for the manufacturing process, to improve the quality of the substrate preparation, and the quality of the IGU fabrication. Furthermore, methods for reworking defective devices were developed, to enable devices which would otherwise be scrapped to be made into useful product. This involved the in-house development of some customized equipment. Finally, the improvements made during this project were validated to ensure that they did not impact the exceptional durability of the SageGlass® products. Given conservative estimates for cost and market penetration, energy savings due to EC windows in residences in the US are calculated to be of the order 0.026 quad (0.026×1015BTU/yr) by the year 2017.

  10. Quantum information processing : science & technology.

    Energy Technology Data Exchange (ETDEWEB)

    Horton, Rebecca; Carroll, Malcolm S.; Tarman, Thomas David

    2010-09-01

    Qubits demonstrated using GaAs double quantum dots (DQD). The qubit basis states are the (1) singlet and (2) triplet stationary states. Long spin decoherence times in silicon spurs translation of GaAs qubit in to silicon. In the near term the goals are: (1) Develop surface gate enhancement mode double quantum dots (MOS & strained-Si/SiGe) to demonstrate few electrons and spin read-out and to examine impurity doped quantum-dots as an alternative architecture; (2) Use mobility, C-V, ESR, quantum dot performance & modeling to feedback and improve upon processing, this includes development of atomic precision fabrication at SNL; (3) Examine integrated electronics approaches to RF-SET; (4) Use combinations of numerical packages for multi-scale simulation of quantum dot systems (NEMO3D, EMT, TCAD, SPICE); and (5) Continue micro-architecture evaluation for different device and transport architectures.

  11. Wood Technology: Techniques, Processes, and Products

    Science.gov (United States)

    Oatman, Olan

    1975-01-01

    Seven areas of wood technology illustrates applicable techniques, processes, and products for an industrial arts woodworking curriculum. They are: wood lamination; PEG (polyethylene glycol) diffusion processes; wood flour and/or particle molding; production product of industry; WPC (wood-plastic-composition) process; residential construction; and…

  12. Crystallization process and magnetic properties of amorphous iron oxide nanoparticles

    International Nuclear Information System (INIS)

    Phu, N D; Luong, N H; Chau, N; Hai, N H; Ngo, D T; Hoang, L H

    2011-01-01

    This paper studied the crystallization process, phase transition and magnetic properties of amorphous iron oxide nanoparticles prepared by the microwave heating technique. Thermal analysis and magnetodynamics studies revealed many interesting aspects of the amorphous iron oxide nanoparticles. The as-prepared sample was amorphous. Crystallization of the maghemite γ-Fe 2 O 3 (with an activation energy of 0.71 eV) and the hematite α-Fe 2 O 3 (with an activation energy of 0.97 eV) phase occurred at around 300 deg. C and 350 deg. C, respectively. A transition from the maghemite to the hematite occurred at 500 deg. C with an activation energy of 1.32 eV. A study of the temperature dependence of magnetization supported the crystallization and the phase transformation. Raman shift at 660 cm -1 and absorption band in the infrared spectra at 690 cm -1 showed the presence of disorder in the hematite phase on the nanoscale which is supposed to be the origin of the ferromagnetic behaviour of that antiferromagnetic phase.

  13. Current developments in CZ Si crystal growing technology; Aktuelle Entwicklungen in der Zuechtungstechnologie von CZ-Si-Kristallen

    Energy Technology Data Exchange (ETDEWEB)

    Altekrueger, Burkhard; Volk, Michael [PVA TePla AG, Wettenberg (Germany)

    2011-02-15

    The industrial growing of increasingly large and perfect silicon (Si) monocrystals for applications in microelectronics and photovoltaics requires continuous improvement of process control and growing technology. Continuous adaptation and optimization of system technology in terms of reliability, process flexibility and dimensioning are also necessary. The basic principles of industrial silicon crystal growing and the resultant requirements for the Si process and system technologies are described in the first part of this series of articles. The constantly increasing requirements for the performance and complexity of the electronic circuits (chips) in accordance with Moore's Law mean that the requirements for the perfection and dimensions of monocrystalline Si wafers and Si crystals are also continuously rising. After the introduction of the 300 mm Si wafer generation in recent years, the next Si wafer generation (450 mm) is therefore being discussed already. The technological and economic effects of these constantly increasing requirements for the necessary system technologies will be set out and discussed in the subsequent articles on the basis of current Si CZ crystal growing systems as well as new system concepts. (orig.)

  14. Microwave plasma emerging technologies for chemical processes

    NARCIS (Netherlands)

    de la Fuente, Javier F.; Kiss, Anton A.; Radoiu, Marilena T.; Stefanidis, Georgios D.

    2017-01-01

    Microwave plasma (MWP) technology is currently being used in application fields such as semiconductor and material processing, diamond film deposition and waste remediation. Specific advantages of the technology include the enablement of a high energy density source and a highly reactive medium,

  15. Control of Process Operations and Monitoring of Product Qualities through Generic Model-based Framework in Crystallization Processes

    DEFF Research Database (Denmark)

    Abdul Samad, Noor Asma Fazli Bin

    A generic and systematic model-based framework for the design of a process monitoring and control system to achieve the desired crystal size distribution (CSD) and crystal shape for a wide range of crystallization processes has been developed. This framework combines a generic multi-dimensional m...

  16. TECHNOLOGICAL PROCESS OF EFFLUENTS DEPHENOLYSATION

    Directory of Open Access Journals (Sweden)

    В. Трачевський

    2011-02-01

    Full Text Available The one of the important physical factors impacting on the environmental safety of industrial wastewater generated in the production of paints and varnishes is considered. Identification wastewater formation sources, composition, its amount in a particular type of resin is an essential point for developing methods of cleaning industrial wastewater treatment design and industrial plants. Deep cleaning of wastewater from phenol is a major challenge. Studies that mostly focused on the known methods of disposal of waste waters from phenol have been analyzed. It was shown that the shortcomings of many methods of sewage treatment of phenols by condensation at atmospheric pressure are the long duration of the process, significant cost of heat, and large residual phenol concentration in water, respectively. The most effective method of reducing the concentration of phenol in waste water is its oxidation in MnO2 suspension. The interaction of manganese oxides with sulfuric acid produces oxygen, which can oxidise phenol contained in the waste water. As a result of wastewater treatment of phenolic resins by manganese oxides in acidic sulfate medium phenol concentration  was decreased by 98.6 - 99.6%.

  17. Process analytical technology (PAT) for biopharmaceuticals

    DEFF Research Database (Denmark)

    Glassey, Jarka; Gernaey, Krist; Clemens, Christoph

    2011-01-01

    Process analytical technology (PAT), the regulatory initiative for building in quality to pharmaceutical manufacturing, has a great potential for improving biopharmaceutical production. The recommended analytical tools for building in quality, multivariate data analysis, mechanistic modeling, nov...

  18. Membrane-Based Technologies in the Pharmaceutical Industry and Continuous Production of Polymer-Coated Crystals/Particles.

    Science.gov (United States)

    Chen, Dengyue; Sirkar, Kamalesh K; Jin, Chi; Singh, Dhananjay; Pfeffer, Robert

    2017-01-01

    Membrane technologies are of increasing importance in a variety of separation and purification applications involving liquid phases and gaseous mixtures. Although the most widely used applications at this time are in water treatment including desalination, there are many applications in chemical, food, healthcare, paper and petrochemical industries. This brief review is concerned with existing and emerging applications of various membrane technologies in the pharmaceutical and biopharmaceutical industry. The goal of this review article is to identify important membrane processes and techniques which are being used or proposed to be used in the pharmaceutical and biopharmaceutical operations. How novel membrane processes can be useful for delivery of crystalline/particulate drugs is also of interest. Membrane separation technologies are extensively used in downstream processes for bio-pharmaceutical separation and purification operations via microfiltration, ultrafiltration and diafiltration. Also the new technique of membrane chromatography allows efficient purification of monoclonal antibodies. Membrane filtration techniques of reverse osmosis and nanofiltration are being combined with bioreactors and advanced oxidation processes to treat wastewaters from pharmaceutical plants. Nanofiltration with organic solvent-stable membranes can implement solvent exchange and catalyst recovery during organic solvent-based drug synthesis of pharmaceutical compounds/intermediates. Membranes in the form of hollow fibers can be conveniently used to implement crystallization of pharmaceutical compounds. The novel crystallization methods of solid hollow fiber cooling crystallizer (SHFCC) and porous hollow fiber anti-solvent crystallization (PHFAC) are being developed to provide efficient methods for continuous production of polymer-coated drug crystals in the area of drug delivery. This brief review provides a general introduction to various applications of membrane technologies in

  19. Method for thermal processing alumina-enriched spinel single crystals

    Science.gov (United States)

    Jantzen, Carol M.

    1995-01-01

    A process for age-hardening alumina-rich magnesium aluminum spinel to obtain the desired combination of characteristics of hardness, clarity, flexural strength and toughness comprises selection of the time-temperature pair for isothermal heating followed by quenching. The time-temperature pair is selected from the region wherein the precipitate groups have the characteristics sought. The single crystal spinel is isothermally heated and will, if heated long enough pass from its single phase through two pre-precipitates and two metastable precipitates to a stable secondary phase precipitate within the spinel matrix. Quenching is done slowly at first to avoid thermal shock, then rapidly.

  20. Wafer level 3-D ICs process technology

    CERN Document Server

    Tan, Chuan Seng; Reif, L Rafael

    2009-01-01

    This book focuses on foundry-based process technology that enables the fabrication of 3-D ICs. The core of the book discusses the technology platform for pre-packaging wafer lever 3-D ICs. However, this book does not include a detailed discussion of 3-D ICs design and 3-D packaging. This is an edited book based on chapters contributed by various experts in the field of wafer-level 3-D ICs process technology. They are from academia, research labs and industry.

  1. TEXACO GASIFICATION PROCESS - INNOVATIVE TECHNOLOGY EVALUATION REPORT

    Science.gov (United States)

    This report summarizes the evaluation of the Texaco Gasification Process (TGP) conducted under the U.S. Environmental Protection Agency (EPA) Superfund Innovative Technology Evaluation (SITE) Program. The Texaco Gasification Process was developed by Texaco Inc. The TGP is a comm...

  2. Laser Processing Technology using Metal Powders

    International Nuclear Information System (INIS)

    Jang, Jeong-Hwan; Moon, Young-Hoon

    2012-01-01

    The purpose of this paper is to review the state of laser processing technology using metal powders. In recent years, a series of research and development efforts have been undertaken worldwide to develop laser processing technologies to fabricate metal-based parts. Layered manufacturing by the laser melting process is gaining ground for use in manufacturing rapid prototypes (RP), tools (RT) and functional end products. Selective laser sintering / melting (SLS/SLM) is one of the most rapidly growing rapid prototyping techniques. This is mainly due to the processes's suitability for almost any materials, including polymers, metals, ceramics and many types of composites. The interaction between the laser beam and the powder material used in the laser melting process is one of the dominant phenomena defining feasibility and quality. In the case of SLS, the powder is not fully melted during laser scanning, therefore the SLS-processed parts are not fully dense and have relatively low strength. To overcome this disadvantage, SLM and laser cladding (LC) processes have been used to enable full melting of the powder. Further studies on the laser processing technology will be continued due to the many potential applications that the technology offers.

  3. ADEPT2 - Next Generation Process Management Technology

    NARCIS (Netherlands)

    Dadam, P.; Rinderle, S.B.; Reichert, M.U.; Jurisch, M.; Acker, H.; Göser, K.; Kreher, U; Lauer, M.

    If current process management systems shall be applied to a broad spectrum of applications, they will have to be significantly improved with respect to their technological capabilities. In particular, in dynamic environments it must be possible to quickly implement and deploy new processes, to

  4. Optimization of processing technology of Rhizoma Pinelliae ...

    African Journals Online (AJOL)

    Methods: Orthogonal design method was applied to analyze the effects of factors such as licorice concentration volume, soaking time and processing temperature on processing technology of Rhizoma Pinelliae Praeparatum; MTT assay and flow cytometry were used to determine the inhibitory effect of Rhizoma Pinelliae ...

  5. Membrane technology in chemical process industry

    International Nuclear Information System (INIS)

    Bhattacharjee, B.

    2002-01-01

    The technology developments in current century will mainly focus on the energy, safe and effective utilization of available natural resources and environment. Production and effective use of water resource at industrial level will directly affect the environment. Similarly the various means of energy production and its consumption will also bear a direct impact on environment. In any chemical industry a large portion of energy consumption goes to separation process which in turn affect the cost of production as well as total cost of the plant. Therefore, minimization of energy consumption, finding out new nondestructive separation technology and reutilization of all recovered process streams are the new thrust area for chemical industries. In view of this, a comparatively new separation technology, 'Membrane Science and Technology' is available to the chemical industry. The potential of this technology is immense because of its simple operation, less chemical additives requirement, less energy consumption and easy adoptability to the existing process. This technology is often considered as energy efficient, environmentally benign and clean technology

  6. Business process modeling for processing classified documents using RFID technology

    Directory of Open Access Journals (Sweden)

    Koszela Jarosław

    2016-01-01

    Full Text Available The article outlines the application of the processing approach to the functional description of the designed IT system supporting the operations of the secret office, which processes classified documents. The article describes the application of the method of incremental modeling of business processes according to the BPMN model to the description of the processes currently implemented (“as is” in a manual manner and target processes (“to be”, using the RFID technology for the purpose of their automation. Additionally, the examples of applying the method of structural and dynamic analysis of the processes (process simulation to verify their correctness and efficiency were presented. The extension of the process analysis method is a possibility of applying the warehouse of processes and process mining methods.

  7. Manufacturing technology and process for BWR fuel

    International Nuclear Information System (INIS)

    Kato, Shigeru

    1996-01-01

    Following recent advanced technologies, processes and requests of the design changes of BWR fuel, Nuclear Fuel Industries, Ltd. (NFI) has upgraded the manufacturing technology and honed its own skills to complete its brand-new automated facility in Tokai in the latter half of 1980's. The plant uses various forms of automation throughout the manufacturing process: the acceptance of uranium dioxide powder, pelletizing, fuel rod assembling, fuel bundle assembling and shipment. All processes are well computerized and linked together to establish the integrated control system with three levels of Production and Quality Control, Process Control and Process Automation. This multi-level system plays an important role in the quality assurance system which generates the highest quality of fuels and other benefits. (author)

  8. Fluidization technologies: Aerodynamic principles and process engineering.

    Science.gov (United States)

    Dixit, Rahul; Puthli, Shivanand

    2009-11-01

    The concept of fluidization has been adapted to different unit processes of pharmaceutical product development. Till date a lot of improvements have been made in the engineering design to achieve superior process performance. This review is focused on the fundamental principles of aerodynamics and hydrodynamics associated with the fluidization technologies. Fluid-bed coating, fluidized bed granulation, rotor processing, hot melt granulation, electrostatic coating, supercritical fluid based fluidized bed technology are highlighted. Developments in the design of processing equipments have been explicitly elucidated. This article also discusses processing problems from the operator's perspective along with latest developments in the application of these principles. (c) 2009 Wiley-Liss, Inc. and the American Pharmacists Association

  9. Application of quartz crystal microbalance technology in tribological investigation

    Science.gov (United States)

    The last fifteen years have seen considerable growth in the application of quartz crystal microbalance (QCM) to explore the tribological characteristics of materials. This article reviews some of the advances made in characterizing frictional properties of materials using the QCM, especially with di...

  10. Kinetic crystallization separation process of the inositol isomers by controlling metastable zones

    Science.gov (United States)

    Konuki, Kaname; Hirasawa, Izumi

    2013-06-01

    D-chiro-inositol (DCI) is prepared by the immobilized enzyme reaction which uses myo-inositol (MI) as the substrate and the conversion rate is about 13%. The aim of this study was to develop a separation method for high purity DCI crystals from a reaction solution including low purity DCI only by the crystallization process. We succeeded in separating DCI crystals of 96% purity by water cooling crystallization, but it was presumed that scale-up was difficult. Although we tried anti-solvent crystallization similar to water cooling crystallization, high purity DCI crystals were not obtained. Therefore, we proposed the crystallization separation process by controlling metastable zones. The purity of a desired compound is controlled by this process, because solid-liquid separation is achieved before crystallization of compound in metastable zone. By the crystallization using this method, the DCI crystals of 97% purity were obtained. Although the yield per batch is about 50%, the actual yield is improved as the last mother liquor returns into the process of the following batch. When this process was repeated, the purity and the yield of DCI were reproduced and the robustness of this process was proved. It is expected that scale-up of this process will be successful, and this purification method could be applicable to similar systems such as separation of isomers and analogs.

  11. Reconfigurable Photonic Crystals Enabled by Multistimuli-Responsive Shape Memory Polymers Possessing Room Temperature Shape Processability.

    Science.gov (United States)

    Fang, Yin; Leo, Sin-Yen; Ni, Yongliang; Wang, Junyu; Wang, Bingchen; Yu, Long; Dong, Zhe; Dai, Yuqiong; Basile, Vito; Taylor, Curtis; Jiang, Peng

    2017-02-15

    Traditional shape memory polymers (SMPs) are mostly thermoresponsive, and their applications in nano-optics are hindered by heat-demanding programming and recovery processes. By integrating a polyurethane-based shape memory copolymer with templating nanofabrication, reconfigurable/rewritable macroporous photonic crystals have been demonstrated. This SMP coupled with the unique macroporous structure enables unusual all-room-temperature shape memory cycles. "Cold" programming involving microscopic order-disorder transitions of the templated macropores is achieved by mechanically deforming the macroporous SMP membranes. The rapid recovery of the permanent, highly ordered photonic crystal structure from the temporary, disordered configuration can be triggered by multiple stimuli including a large variety of vapors and solvents, heat, and microwave radiation. Importantly, the striking chromogenic effects associated with these athermal and thermal processes render a sensitive and noninvasive optical methodology for quantitatively characterizing the intriguing nanoscopic shape memory effects. Some critical parameters/mechanisms that could significantly affect the final performance of SMP-based reconfigurable photonic crystals including strain recovery ratio, dynamics and reversibility of shape recovery, as well as capillary condensation of vapors in macropores, which play a crucial role in vapor-triggered recovery, can be evaluated using this new optical technology.

  12. Science and technology roadmap for graphene, related two-dimensional crystals, and hybrid systems

    DEFF Research Database (Denmark)

    Ferrari, Andrea C.; Bonaccorso, Francesco; Falko, Vladimir

    2015-01-01

    We present the science and technology roadmap (STR) for graphene, related twodimensional (2d) crystals, and hybrid systems, targeting an evolution in technology, that might lead to impacts and benefits reaching into most areas of society. The roadmap was developed within the framework of the Euro...

  13. Image processing technology for nuclear facilities

    International Nuclear Information System (INIS)

    Lee, Jong Min; Lee, Yong Beom; Kim, Woong Ki; Park, Soon Young

    1993-05-01

    Digital image processing technique is being actively studied since microprocessors and semiconductor memory devices have been developed in 1960's. Now image processing board for personal computer as well as image processing system for workstation is developed and widely applied to medical science, military, remote inspection, and nuclear industry. Image processing technology which provides computer system with vision ability not only recognizes nonobvious information but processes large information and therefore this technique is applied to various fields like remote measurement, object recognition and decision in adverse environment, and analysis of X-ray penetration image in nuclear facilities. In this report, various applications of image processing to nuclear facilities are examined, and image processing techniques are also analysed with the view of proposing the ideas for future applications. (Author)

  14. BUSINESS PROCESS MANAGEMENT SYSTEMS TECHNOLOGY COMPONENTS ANALYSIS

    Directory of Open Access Journals (Sweden)

    Andrea Giovanni Spelta

    2007-05-01

    Full Text Available The information technology that supports the implementation of the business process management appproach is called Business Process Management System (BPMS. The main components of the BPMS solution framework are process definition repository, process instances repository, transaction manager, conectors framework, process engine and middleware. In this paper we define and characterize the role and importance of the components of BPMS's framework. The research method adopted was the case study, through the analysis of the implementation of the BPMS solution in an insurance company called Chubb do Brasil. In the case study, the process "Manage Coinsured Events"" is described and characterized, as well as the components of the BPMS solution adopted and implemented by Chubb do Brasil for managing this process.

  15. Exploring novel food proteins and processing technologies

    NARCIS (Netherlands)

    Avila Ruiz, Geraldine

    2016-01-01

    Foods rich in protein are nowadays high in demand worldwide. To ensure a sustainable supply and a high quality of protein foods, novel food proteins and processing technologies need to be explored to understand whether they can be used for the development of high-quality protein foods. Therefore,

  16. Improvisation during Process-Technology Adoption

    DEFF Research Database (Denmark)

    Tjørnehøj, Gitte; Mathiassen, Lars

    2010-01-01

    Most software firms struggle to take advantage of the potential benefits of software process improvement (SPI) as they adopt this technology into the complex and dynamic realities of their day-to-day operation. Such efforts are therefore typically fluctuating between management's attempt to contr...

  17. Influence Processes for Information Technology Acceptance

    DEFF Research Database (Denmark)

    Bhattacherjee, Anol; Sanford, Clive Carlton

    2006-01-01

    This study examines how processes of external influence shape information technology acceptance among potential users, how such influence effects vary across a user population, and whether these effects are persistent over time. Drawing on the elaboration-likelihood model (ELM), we compared two...

  18. Development of Food Preservation and Processing Technologies by Radiation Technology

    International Nuclear Information System (INIS)

    Byun, Myung Woo; Lee, Ju Won; Kim, Jae Hun

    2007-07-01

    To secure national food resources, development of energy-saving food processing and preservation technologies, establishment of method on improvement of national health and safety by development of alternative techniques of chemicals and foundation of the production of hygienic food and public health related products by irradiation technology were studied. Results at current stage are following: As the first cooperative venture business technically invested by National Atomic Research Development Project, institute/company's [technology-invested technology foundation No. 1] cooperative venture, Sun-BioTech Ltd., was founded and stated its business. This suggested new model for commercialization and industrialization of the research product by nation-found institute. From the notice of newly approved product list about irradiated food, radiation health related legal approval on 7 food items was achieved from the Ministry of health and wellfare, the Korea Food and Drug Administration, and this contributed the foundation of enlargement of practical use of irradiated food. As one of the foundation project for activation of radiation application technology for the sanitation and secure preservation of special food, such as military meal service, food service for patient, and food for sports, and instant food, such as ready-to-eat/ready-to-cook food, the proposal for radiation application to the major military commander at the Ministry of National Defence and the Joint Chiefs of Staff was accepted for the direction of military supply development in mid-termed plan for the development of war supply. Especially, through the preliminary research and the development of foundation technology for the development of the Korean style space food and functional space food, space Kimch with very long shelf life was finally developed. The development of new item/products for food and life science by combining RT/BT, the development of technology for the elimination/reduction of

  19. Development of Food Preservation and Processing Technologies by Radiation Technology

    Energy Technology Data Exchange (ETDEWEB)

    Byun, Myung Woo; Lee, Ju Won; Kim, Jae Hun (and others)

    2007-07-15

    To secure national food resources, development of energy-saving food processing and preservation technologies, establishment of method on improvement of national health and safety by development of alternative techniques of chemicals and foundation of the production of hygienic food and public health related products by irradiation technology were studied. Results at current stage are following: As the first cooperative venture business technically invested by National Atomic Research Development Project, institute/company's [technology-invested technology foundation No. 1] cooperative venture, Sun-BioTech Ltd., was founded and stated its business. This suggested new model for commercialization and industrialization of the research product by nation-found institute. From the notice of newly approved product list about irradiated food, radiation health related legal approval on 7 food items was achieved from the Ministry of health and wellfare, the Korea Food and Drug Administration, and this contributed the foundation of enlargement of practical use of irradiated food. As one of the foundation project for activation of radiation application technology for the sanitation and secure preservation of special food, such as military meal service, food service for patient, and food for sports, and instant food, such as ready-to-eat/ready-to-cook food, the proposal for radiation application to the major military commander at the Ministry of National Defence and the Joint Chiefs of Staff was accepted for the direction of military supply development in mid-termed plan for the development of war supply. Especially, through the preliminary research and the development of foundation technology for the development of the Korean style space food and functional space food, space Kimch with very long shelf life was finally developed. The development of new item/products for food and life science by combining RT/BT, the development of technology for the elimination/reduction of

  20. Improving drug manufacturing with process analytical technology.

    Science.gov (United States)

    Rodrigues, Licinia O; Alves, Teresa P; Cardoso, Joaquim P; Menezes, José C

    2006-01-01

    Within the process analytical technology (PAT) framework, as presented in the US Food and Drug Administration guidelines, the aim is to design, develop and operate processes consistently to ensure a pre-defined level of quality at the end of the manufacturing process. Three PAT implementation scenarios can be envisaged. Firstly, PAT could be used in its most modest version (in an almost non-PAT manner) to simply replace an existing quality control protocol (eg, using near-infrared spectroscopy for an in-process quality control, such as moisture content). Secondly, the use of in-process monitoring and process analysis could be integrated to enhance process understanding and operation for an existing industrial process. Thirdly, PAT could be used extensively and exclusively throughout development, scale-up and full-scale production of a new product and process. Although the first type of implementations are well known, reports of the second and third types remain scarce. Herein, results obtained from PAT implementations of the second and third types are described for two industrial processes for preparing bulk active pharmaceutical ingredients, demonstrating the benefits in terms of increased process understanding and process control.

  1. Development of large area Multi-coloured Multifunctional Displays (MFA) in liquid crystal technology

    Science.gov (United States)

    Briegel, J.; Fahrenschon, K.; Keiner, H.; Marzel, O.; Schwedes, W.; Steinbeck, J.; Wiemer, W.

    1983-05-01

    Large area liquid crystal displays for automotive application including corresponding flat illumination systems and methods for integrating the driver IC's on the liquid crystal cell are discussed. Manufacturing technologies applicable for large quantity series production were worked out, and prototypes were delivered to the automotive industry, mainly the dynamic scattering mode and field effect displays (twisted nematic). The twisted nematic displays are preferred for automotive applications.

  2. Energy conversion technology by chemical processes

    Energy Technology Data Exchange (ETDEWEB)

    Oh, I.W.; Yoon, K.S.; Cho, B.W. [Korea Inst. of Science and Technology, Seoul (Korea, Republic of)] [and others

    1996-12-01

    The sharp increase in energy usage according to the industry development has resulted in deficiency of energy resources and severe pollution problems. Therefore, development of the effective way of energy usage and energy resources of low pollution is needed. Development of the energy conversion technology by chemical processes is also indispensable, which will replace the pollutant-producing and inefficient mechanical energy conversion technologies. Energy conversion technology by chemical processes directly converts chemical energy to electrical one, or converts heat energy to chemical one followed by heat storage. The technology includes batteries, fuel cells, and energy storage system. The are still many problems on performance, safety, and manufacturing of the secondary battery which is highly demanded in electronics, communication, and computer industries. To overcome these problems, key components such as carbon electrode, metal oxide electrode, and solid polymer electrolyte are developed in this study, followed by the fabrication of the lithium secondary battery. Polymer electrolyte fuel cell, as an advanced power generating apparatus with high efficiency, no pollution, and no noise, has many applications such as zero-emission vehicles, on-site power plants, and military purposes. After fabricating the cell components and operating the single cells, the fundamental technologies in polymer electrolyte fuel cell are established in this study. Energy storage technology provides the safe and regular heat energy, irrespective of the change of the heat energy sources, adjusts time gap between consumption and supply, and upgrades and concentrates low grade heat energy. In this study, useful chemical reactions for efficient storage and transport are investigated and the chemical heat storage technology are developed. (author) 41 refs., 90 figs., 20 tabs.

  3. Improvisation during Process-Technology Adoption

    DEFF Research Database (Denmark)

    Tjørnehøj, Gitte; Mathiassen, Lars

    2010-01-01

    firm, SmallSoft, over a 10-year period (1996–2005). We found that micro-level and macro-level improvisations interacted, often in uncoordinated ways, to shape SPI technology adoption at SmallSoft. The improvisations enhanced employee creativity, motivation and empowerment, created momentum......Most software firms struggle to take advantage of the potential benefits of software process improvement (SPI) as they adopt this technology into the complex and dynamic realities of their day-to-day operation. Such efforts are therefore typically fluctuating between management's attempt to control...

  4. Multiscale modelling and simulation of single crystal superalloy turbine blade casting during directional solidification process

    Directory of Open Access Journals (Sweden)

    Xu Qingyan

    2014-07-01

    Full Text Available As the key parts of an aero-engine, single crystal (SX superalloy turbine blades have been the focus of much attention. However, casting defects often occur during the manufacturing process of the SX turbine blades. Modeling and simulation technology can help to optimize the manufacturing process of SX blades. Multiscale coupled models were proposed and used to simulate the physical phenomena occurring during the directional solidification (DS process. Coupled with heat transfer (macroscale and grain growth (meso-scale, 3D dendritic grain growth was calculated to show the competitive grain growth at micro-scale. SX grain selection behavior was studied by the simulation and experiments. The results show that the geometrical structure and technical parameters had strong influences on the grain selection effectiveness. Based on the coupled models, heat transfer, grain growth and microstructure evolution of a complex hollow SX blade were simulated. Both the simulated and experimental results show that the stray grain occurred at the platform of the SX blade when a constant withdrawal rate was used in manufacturing process. In order to avoid the formation of the stray crystal, the multi-scale coupled models and the withdrawal rate optimized technique were applied to the same SX turbine blade. The modeling results indicated that the optimized variable withdrawal rate can achieve SX blade castings with no stray grains, which was also proved by the experiments.

  5. In-line monitoring and interpretation of an indomethacin anti-solvent crystallization process by near-infrared spectroscopy (NIRS).

    Science.gov (United States)

    Lee, Hea-Eun; Lee, Min-Jeong; Kim, Woo-Sik; Jeong, Myung-Yung; Cho, Young-Sang; Choi, Guang Jin

    2011-11-28

    PAT (process analytical technology) has been emphasized as one of key elements for the full implementation of QbD (quality-by-design) in the pharmaceutical area. NIRS (near-infrared spectroscopy) has been studied intensively as an in-line/on-line monitoring tool in chemical and biomedical industries. A precise and reliable monitoring of the particle characteristics during crystallization along with a suitable control strategy should be highly encouraged for the conformance to new quality system of pharmaceutical products. In this study, the anti-solvent crystallization process of indomethacin (IMC) was monitored using an in-line NIRS. IMC powders were produced via anti-solvent crystallization using two schemes; 'S-to-A' (solvent-to-antisolvent) and 'A-to-S' (antisolvent-to-solvent). In-line NIR spectra were analyzed by a PCA (principal component analysis) method. Although pure α-form IMC powder was resulted under A-to-S scheme, a mixture of the α-form and γ-form was produced for S-to-A case. By integrating the PCA results with off-line characterization (SEM, XRD, DSC) data, the crystallization process under each scheme was elucidated by three distinct consecutive steps. It was demonstrated that in-line NIRS, combined with PCA, can be very useful to monitor in real time and interpret the anti-solvent crystallization process with respect to the polymorphism and particle size. Copyright © 2011 Elsevier B.V. All rights reserved.

  6. Control of processes using isotopic diagnostic's technologies

    International Nuclear Information System (INIS)

    Vargas, Celso; Chaverri, Oscar; Chine, Bruno; Conejo, Mario

    2005-01-01

    The Escuela de Ciencias e Ingenieria de los Materiales of the Instituto Tecnologico de Costa Rica, in cooperation with OIEA, develops a project of dowry of capacity oriented to the formation of professionals and equipment for the use of two important technologies of isotopic diagnostic. The first of them is the technology of tracers that operates the unique properties that present different radioactive isotopics like open sources. The second one well known as scanning or profile gamma, uses sealed source, of the some nature that the previous ones, to obtain profiles in different processes and thus to determine its internal condition and operation. The objective of this article is to present both technologies, its benefits and to promote the use in the country [es

  7. Waste processing building with incineration technology

    Science.gov (United States)

    Wasilah, Wasilah; Zaldi Suradin, Muh.

    2017-12-01

    In Indonesia, waste problem is one of major problem of the society in the city as part of their life dynamics. Based on Regional Medium Term Development Plan of South Sulawesi Province in 2013-2018, total volume and waste production from Makassar City, Maros, Gowa, and Takalar Regency estimates the garbage dump level 9,076.949 m3/person/day. Additionally, aim of this design is to present a recommendation on waste processing facility design that would accommodate waste processing process activity by incineration technology and supported by supporting activity such as place of education and research on waste, and the administration activity on waste processing facility. Implementation of incineration technology would reduce waste volume up to 90% followed by relative negative impact possibility. The result planning is in form of landscape layout that inspired from the observation analysis of satellite image line pattern of planning site and then created as a building site pattern. Consideration of building orientation conducted by wind analysis process and sun path by auto desk project Vasari software. The footprint designed by separate circulation system between waste management facility interest and the social visiting activity in order to minimize the croos and thus bring convenient to the building user. Building mass designed by inseparable connection series system, from the main building that located in the Northward, then connected to a centre visitor area lengthways, and walked to the waste processing area into the residue area in the Southward area.

  8. Application of pyrolysis process to remove and recover liquid crystal and films from waste liquid crystal display glass

    International Nuclear Information System (INIS)

    Lu, Rixin; Ma, En; Xu, Zhenming

    2012-01-01

    Highlights: ► Pyrolysis process can recycle the liquid crystal and films from liquid crystal display glass successfully. ► The removal of organic parts from the liquid crystal glass reached 87.87 wt%. ► The mechanism analysis of pyrolysis process explains the whole pyrolysis process perfect. ► All pyrolysis products can be tilized by a reasonable way. - Abstract: Liquid crystal display (LCD) glass mainly consists of polarizing film, liquid crystal and glass substrate. Removing and recovering the liquid crystal and films from the LCD glass effectively has important significance for recovering the other parts. This study proposed a pyrolysis process to recover the organic parts from LCD glass. Through thermal gravimetric analysis, the pyrolysis temperature of the LCD glass could be chosen at 850 K. The removal rate of organic parts from LCD glass reached 87.87 wt%. Pyrolysis products consisted of 66.82 wt% oils, 21.01 wt% gaseous and 12.13 wt% residues. In addition, the oils contained 46.27 wt% acetic acid and 32.94 wt% triphenyl phosphate. Then, the pyrolysis mechanisms and products sources of the liquid crystal glass have been analyzed based on the information of bonds energy. The pyrolysis mechanism analysis proved that the products mainly consisted of acetic acid, triphenyl phosphate and C, which is consistent to the results of GC–MS analysis. A reasonable way has been put forward to recycle the pyrolysis products: acetic acid and triphenyl phosphate can be collected by distillation, the rest oils and gases can be used as fuel and the remained glass can be used to extract indium and to produce building materials.

  9. The Plasma Hearth Process Technology Development Project

    International Nuclear Information System (INIS)

    Geimer, R.; Batdorf, J.; Wolfe, P.

    1993-01-01

    The US DOE Office of Technology Development (OTD) is currently evaluating the Plasma Hearth Process (PHP) for potential treatment of several DOE waste types. The PHP is a high-temperature vitrification process that has potential application for a wide range of mixed waste types in both the low-level and transuranic mixed waste categories. The PHP is being tested under both the OTD Mixed Waste Integrated Program and the Buried Waste Integrated Demonstration. Initial testing has been completed on several different surrogate waste forms that are representative of some of the DOE mixed waste streams. Destruction of organic material exceeds that of conventional incineration technologies. The vitrified residual has leaching characteristics comparable to glass formulations produced in the high-level waste program. The first phase of the PHP demonstration project has been successfully completed, and the project is currently beginning a comprehensive second phase of development and testing

  10. Developing technological process of obtaining giality casts

    Directory of Open Access Journals (Sweden)

    A. Issagulov

    2014-10-01

    Full Text Available The article considers the process of manufacturing castings using sand-resin forms and alloying furnace. Were the optimal technological parameters of manufacturing shell molds for the manufacture of castings of heating equipment. Using the same upon receipt of castings by casting in shell molds furnace alloying and deoxidation of the metal will provide consumers with quality products and have a positive impact on the economy in general engineering.

  11. Similarity search processing. Paralelization and indexing technologies.

    Directory of Open Access Journals (Sweden)

    Eder Dos Santos

    2015-08-01

    The next Scientific-Technical Report addresses the similarity search and the implementation of metric structures on parallel environments. It also presents the state of the art related to similarity search on metric structures and parallelism technologies. Comparative analysis are also proposed, seeking to identify the behavior of a set of metric spaces and metric structures over processing platforms multicore-based and GPU-based.

  12. Design and optimization of sustainable process technologies

    DEFF Research Database (Denmark)

    Mussatto, Solange I.; Qin, Fen; Yamakawa, Celina Kiyomi

    The development of sustainable processes and innovative strategies that can accelerate the transition to a bio-economyis one of the main goals of the current societyin order to have a future less dependent on oil and with lower carbon emissions. The use of biomass as a feedstock for bioprocesses......, minimizing the costs and maximizing the efficiencyand productivity.Once the optimal conditions are identified, the process scale-up can be then evaluated. This could be translated in a faster time to market for newprocess technologies....

  13. Digital signal processing - growth of a technology

    International Nuclear Information System (INIS)

    Peek, J.B.H.

    1985-01-01

    The rapid development of microelectronics has led to an increasing extent in circuits and systems for digital signal processing. This happened first in professional applications, e.g. geophysics, astronomy and space flight, and now, with the Compact Disc player, these techniques have entered the consumer field. In the near future digital TV applications will undoubtedly follow. This article outlines a number of the developments behind the advancing 'digitization' of modern technology. The article also considers the main advantages and disadvantages of digital signal processing the main modules now used and some common applications. Particular attention is paid to medical applications. (Auth.)

  14. Radiation processing: a versatile technology for industry

    International Nuclear Information System (INIS)

    Cabalfin, E.G.

    1996-01-01

    Soon after the discovery of x-ray in 1895 and radioactivity in 1896, it was recognized that ionizing radiation can modify the chemical, physical and/or biological properties of materials. However, it was only in the late 50's, when large radiation sources become available, has this unique property of radiation found industrial applications in radiation processing. Today, radiation processing has been used by industry in such diverse applications, such as radiation sterilization/decontamination of medical products, pharmaceuticals, cosmetics and their raw materials; radiation cross-linking of wire and cable insulation; production of heat shrinkable materials and polymer foam; and radiation curing of coatings, adhesives and inks on a wide variety of substrates. In addition to being a clean environment-friendly technology, radiation processing can also be used for the conservation of the environment by such processes as radiation treatment of flue gases to remove SO 2 and NO x and disinfection of sewage sludge. Because of the many advantages offered by radiation processing, industry is showing strong interest in the technology as evidenced by the growing number of industrial radiation facilities in many countries. (author)

  15. The Search for New Information Processing technologies

    Science.gov (United States)

    Cavin, Ralph K.

    2005-03-01

    Our society has benefited from the ‘Golden Age of Electronics’ for the last half century. The ubiquitous transistor, in its many manifestations, has enabled an explosion of capabilities in information processing, communications, and sensing that has spurred exponential growth in performance-benefit ratios. Much of the credit for this progress is due to the continued scaling of the silicon integrated circuit (IC) components and to the associated efficient fabrication processes that have made the IC affordable. There is a growing realization, from simple physics arguments, that as minimum features sizes approach the ten nanometer regime, scaling will very likely slow and eventually end. This doesn’t mean that the MOSFET will disappear, but more likely that it will need to be supplemented by other device and interconnect technologies if the exponential gains are to continue. In this talk we discuss the basis for the projected limitation of scaling of charge-based devices for logic and memory devices. We argue that a fundamental consideration for all devices, including those based on charge, relates to the capacity to manage heat generated by circuit operation. Our preference is for devices that operate at room temperature since the energy costs for cooling the devices must also be charged against the overall system energy consumption. (Cooling costs increase as a power of the difference between the ambient and the target temperature.) Therefore we seek new state variables to serve as an alternative to electrical charge for future information processing technologies. These technologies must provide the potential for sustaining exponential performance-cost benefits with time. The search must not only focus on device structures but on the underlying materials and process technologies that enable these structures. Indeed, to obtain extremely scaled CMOS, new materials and processes must also be developed. In this talk, we survey some of the candidates for

  16. Towards protein crystallization as a process step in downstream processing of therapeutic antibodies: screening and optimization at microbatch scale.

    Directory of Open Access Journals (Sweden)

    Yuguo Zang

    Full Text Available Crystallization conditions of an intact monoclonal IgG4 (immunoglobulin G, subclass 4 antibody were established in vapor diffusion mode by sparse matrix screening and subsequent optimization. The procedure was transferred to microbatch conditions and a phase diagram was built showing surprisingly low solubility of the antibody at equilibrium. With up-scaling to process scale in mind, purification efficiency of the crystallization step was investigated. Added model protein contaminants were excluded from the crystals to more than 95%. No measurable loss of Fc-binding activity was observed in the crystallized and redissolved antibody. Conditions could be adapted to crystallize the antibody directly from concentrated and diafiltrated cell culture supernatant, showing purification efficiency similar to that of Protein A chromatography. We conclude that crystallization has the potential to be included in downstream processing as a low-cost purification or formulation step.

  17. Robotic inspection technology-process an toolbox

    Energy Technology Data Exchange (ETDEWEB)

    Hermes, Markus [ROSEN Group (United States). R and D Dept.

    2005-07-01

    Pipeline deterioration grows progressively with ultimate aging of pipeline systems (on-plot and cross country). This includes both, very localized corrosion as well as increasing failure probability due to fatigue cracking. Limiting regular inspecting activities to the 'scrapable' part of the pipelines only, will ultimately result into a pipeline system with questionable integrity. The confidence level in the integrity of these systems will drop below acceptance levels. Inspection of presently un-inspectable sections of the pipeline system becomes a must. This paper provides information on ROSEN's progress on the 'robotic inspection technology' project. The robotic inspection concept developed by ROSEN is based on a modular toolbox principle. This is mandatory. A universal 'all purpose' robot would not be reliable and efficient in resolving the postulated inspection task. A preparatory Quality Function Deployment (QFD) analysis is performed prior to the decision about the adequate robotic solution. This enhances the serviceability and efficiency of the provided technology. The word 'robotic' can be understood in its full meaning of Recognition - Strategy - Motion - Control. Cooperation of different individual systems with an established communication, e.g. utilizing Bluetooth technology, support the robustness of the ROSEN robotic inspection approach. Beside the navigation strategy, the inspection strategy is also part of the QFD process. Multiple inspection technologies combined on a single carrier or distributed across interacting container must be selected with a clear vision of the particular goal. (author)

  18. Prize for Industrial Applications of Physics: Reflective Cholesteric Liquid Crystals - Innovations in Materials, Display Technology, and Commercialization

    Science.gov (United States)

    Khan, Asad

    Reflective Cholesteric Liquid Crystals have been the subject of much research, development, and commercialization - in display technology as well as other embodiments, such as sensors, privacy films, etc. The liquid Crystal Institute (LCI) at Kent State University (KSU) served as a hot bed of much of the research and development in this field in the early 1990's. From here, the reflective technology was licensed to Kent Displays (KDI) to further develop and commercialize. The 90's saw some development in flexible technologies, drive scheme, display design, as well as materials. The early part of the century took a turn with a strong effort in encapsulation based flexible display development. In 2006, KDI engineers and technologists started firming up ambitious plans for the world's first roll-to-roll manufacturing line for bistable cholesteric displays. In 2009, this became a reality! In early 2010, the first eWriter product was launched into the consumer market under the brand Boogie Board®. Within months, this became a success forcing the rapid development of the manufacturing process for the flexible displays. Today, the company has two manufacturing lines, 24 hour roll-to-roll production of flexible displays, millions of Boogie Board products in the global market place, and a growing OEM business in the Boogie Board technology. KDI continues to do basic research, development, and exploration in the bistable display field. It also has had to become an expert in the supply chain management of the unique raw materials needed for flexible display manufacturing, while still managing global operations with sales offices in several continents and a growing and diversified group of individuals. In this presentation, we will present the story, research, development, technology, and latest trends in bistable cholesteric liquid crystal materials with a particular emphasis on the eWriter technology and market.

  19. Radioisotopes technology used to probe process problems

    International Nuclear Information System (INIS)

    Anon.

    1992-01-01

    With the move to a greater degree of sophistication in industrial processes has come a need for improved measurement control methods as well as for efficient techniques for investigating process problems. Radioisotope-based technology, because of its unique benefits, is playing an increasing role in assisting mining and industry to satisfy the critical needs for efficiency in investigating process problems. More than twenty years of experience in the application of radioisotope and radiation techniques to the practical problems of industry has resulted in the Atomic Energy Corporation of South Africa having accumulated both extensive expertise and the facilities to carry out wide-ranging investigations, and to provide a large variety of cost effective services. Some of these are described. 2 figs., 2 ills

  20. Laser Processed Condensing Heat Exchanger Technology Development

    Science.gov (United States)

    Hansen, Scott; Wright, Sarah; Wallace, Sarah; Hamilton, Tanner; Dennis, Alexander; Zuhlke, Craig; Roth, Nick; Sanders, John

    2017-01-01

    The reliance on non-permanent coatings in Condensing Heat Exchanger (CHX) designs is a significant technical issue to be solved before long-duration spaceflight can occur. Therefore, high reliability CHXs have been identified by the Evolvable Mars Campaign (EMC) as critical technologies needed to move beyond low earth orbit. The Laser Processed Condensing Heat Exchanger project aims to solve these problems through the use of femtosecond laser processed surfaces, which have unique wetting properties and potentially exhibit anti-microbial growth properties. These surfaces were investigated to identify if they would be suitable candidates for a replacement CHX surface. Among the areas researched in this project include microbial growth testing, siloxane flow testing in which laser processed surfaces were exposed to siloxanes in an air stream, and manufacturability.

  1. ANALYSIS ON TECHNOLOGICAL PROCESSES CLEANING OIL PIPELINES

    Directory of Open Access Journals (Sweden)

    Mariana PǍTRAŞCU

    2015-05-01

    Full Text Available In this paper the researches are presented concerning the technological processes of oil pipelines.We know several technologies and materials used for cleaning the sludge deposits, iron and manganese oxides, dross, stone, etc.de on the inner walls of drinking water pipes or industries.For the oil industry, methods of removal of waste materials and waste pipes and liquid and gas transport networks are operations known long, tedious and expensive. The main methods and associated problems can be summarized as follows: 1 Blowing with compressed air.2 manual or mechanical brushing, sanding with water or dry.3 Wash with water jet of high pressure, solvent or chemical solution to remove the stone and hard deposits.4 The combined methods of cleaning machines that use water jets, cutters, chains, rotary heads cutters, etc.

  2. New radiation technologies and methods for control of technological processes in metallurgy

    International Nuclear Information System (INIS)

    Zaykin, Yu.

    1996-01-01

    Radiation Technology of Metal and Ceramic Production with Enhanced Service Properties. Based on application of radiation technique in powder metallurgy the new technology for obtaining metals, alloys and ceramic materials with high service properties is worked out. Radiation processing of powder materials at the certain stage of the process leads to profound structure alterations at all further stages and eventually effects the properties of the resulting product. Theoretical calculation and experimental studies of electron-positron annihilation in powder-pressed samples showed that irradiation caused powder particles surface state changes favorable for further sintering and crystallization processes development. It is shown that irradiation of metal powders and powder-pressed samples by high energy electrons is technologically most efficient. The right choice of the type-and the mode of the radiation processing makes it possible to obtain metals, alloys and ceramic materials (Mo,Fe, W, Al, Ni, Cu, stainless steels, ceramics, etc.) with homogeneous structure and stable enhanced service properties. The project on radiation technology application to powder metallurgy represented by a group of authors was awarded with the diploma and the gold medal at the 22 International Exhibition of Inventions (Geneva, 1994). New Technologic Opportunities of the Chromium-Nickel Alloys Processing To obtain the required phase-structure state special methods of the chromium-nickel alloy processing for sensitive elastic devices production were worked out combining plastic deformation, thermal and radiation processing. It is shown that h-gbb phase transfer not observed before is possible in extremely non-equilibrium conditions under electron irradiation. It is established that the complex reaction of recrystallization and gb-phase deposition proceeds under electron irradiation at the room temperature when the certain threshold plastic deformation degree is reached that leads to the same

  3. Technological yields of sources for radiation processing

    International Nuclear Information System (INIS)

    Zagorski, Z.P.

    1993-01-01

    The present report is prepared for planners of radiation processing of any material. Calculations are focused on accelerators of electrons, divided into two groups: versatile linacs of energy up to 13 MeV, and accelerators of lower energy, below 2 MeV, of better energy yield but of limited applications. The calculations are connected with the confrontation of the author's technological expectations during the preparation of the linac project in the late '60s, with the results of 25 years of exploitation of the machine. One has to realize that from the 200 kW input power from the mains, only 5 kW of bent and scanned beam is recovered on the conveyor. That power is only partially used for radiation induced phenomena, because of the demanded homogeneity of the dose, of the mode of packing of the object and its shape, of edges of the scanned area and in the spaces between boxes, and of loses during the idle time due to the tuning of the machine and dosimetric operations. The use of lower energy accelerators may be more economical than that of linacs in case of objects of specific type. At the first stage already, that is of the conversion of electrical power into that of low energy electron beam, the yield is 2-3 times better than in the case of linacs. Attention has been paid to the technological aspects of electron beam conversion into the more penetrating Bremsstrahlung similar to gamma radiation. The advantages of technologies, which make possible a control of the shape of the processed object are stressed. Special attention is focused to the relation between the yield of processing and the ratio between the maximum to the minimum dose in the object under the irradiation. (author). 14 refs, 14 figs

  4. Comparing composts formed by different technological processing

    Science.gov (United States)

    Lyckova, B.; Mudrunka, J.; Kucerova, R.; Glogarova, V.

    2017-10-01

    The presented article compares quality of composts which were formed by different technological processes. The subject to comparison was a compost which was created in a closed fermenter where ideal conditions for decomposition and organic substances conversion were ensured, with compost which was produced in an open box of community composting. The created composts were analysed to determine whether it is more important for the final compost to comply with the composting conditions or better sorting of raw materials needed for compost production. The results of the carried out experiments showed that quality of the resulting compost cannot be determined unequivocally.

  5. A review of the technology and process on integrated circuits failure analysis applied in communications products

    Science.gov (United States)

    Ming, Zhimao; Ling, Xiaodong; Bai, Xiaoshu; Zong, Bo

    2016-02-01

    The failure analysis of integrated circuits plays a very important role in the improvement of the reliability in communications products. This paper intends to mainly introduce the failure analysis technology and process of integrated circuits applied in the communication products. There are many technologies for failure analysis, include optical microscopic analysis, infrared microscopic analysis, acoustic microscopy analysis, liquid crystal hot spot detection technology, optical microscopic analysis technology, micro analysis technology, electrical measurement, microprobe technology, chemical etching technology and ion etching technology. The integrated circuit failure analysis depends on the accurate confirmation and analysis of chip failure mode, the search of the root failure cause, the summary of failure mechanism and the implement of the improvement measures. Through the failure analysis, the reliability of integrated circuit and rate of good products can improve.

  6. Process Intensification in Crystallization: Submicron Particle Generation Using Alternative Energy Forms

    OpenAIRE

    Radacsi, N.

    2012-01-01

    Crystallization is one of the oldest separation and product formation techniques that continues to be in use today. Despite its long history, it only started to develop significantly in the past few decades. In this thesis, the application of Process Intensification in crystallization is investigated. Process Intensification is a set of often radically innovative principles in process and equipment design, which can bring significant benefits in terms of process and chain efficiency, capital ...

  7. Optimization of induced crystallization reaction in a novel process of nutrients removal coupled with phosphorus recovery from domestic wastewater

    Directory of Open Access Journals (Sweden)

    Zou Haiming

    2017-12-01

    Full Text Available Phosphorus removal and recovery from domestic wastewater is urgent nowadays. A novel process of nutrients removal coupled with phosphorus recovery from domestic sewage was proposed and optimization of induced crystallization reaction was performed in this study. The results showed that 92.3% of phosphorus recovery via induced Hydroxyapatite crystallization was achieved at the optimum process parameters: reaction time of 80 min, seed crystal loads of 60 g/L, pH of 8.5, Ca/P mole ratio of 2.0 and 4.0 L/min aeration rate when the PO43--P concentration was 10 mg/L in the influent, displaying an excellent phosphorus recovery performance. Importantly, it was found that the effect of reaction temperature on induced Hydroxyapatite crystallization was slight, thus favoring practical application of phosphorus recovery method described in this study. From these results, the proposed method of induced HAP crystallization to recover phosphorus combined with nutrients removal can be an economical and effective technology, probably favoring the water pollution control and phosphate rock recycle.

  8. crystal

    Science.gov (United States)

    Yu, Yi; Huang, Yisheng; Zhang, Lizhen; Lin, Zhoubin; Sun, Shijia; Wang, Guofu

    2014-07-01

    A Nd3+:Na2La4(WO4)7 crystal with dimensions of ϕ 17 × 30 mm3 was grown by the Czochralski method. The thermal expansion coefficients of Nd3+:Na2La4(WO4)7 crystal are 1.32 × 10-5 K-1 along c-axis and 1.23 × 10-5 K-1 along a-axis, respectively. The spectroscopic characteristics of Nd3+:Na2La4(WO4)7 crystal were investigated. The Judd-Ofelt theory was applied to calculate the spectral parameters. The absorption cross sections at 805 nm are 2.17 × 10-20 cm2 with a full width at half maximum (FWHM) of 15 nm for π-polarization, and 2.29 × 10-20 cm2 with a FWHM of 14 nm for σ-polarization. The emission cross sections are 3.19 × 10-20 cm2 for σ-polarization and 2.67 × 10-20 cm2 for π-polarization at 1,064 nm. The fluorescence quantum efficiency is 67 %. The quasi-cw laser of Nd3+:Na2La4(WO4)7 crystal was performed. The maximum output power is 80 mW. The slope efficiency is 7.12 %. The results suggest Nd3+:Na2La4(WO4)7 crystal as a promising laser crystal fit for laser diode pumping.

  9. Melting processes of oligomeric α and β isotactic polypropylene crystals at ultrafast heating rates

    Energy Technology Data Exchange (ETDEWEB)

    Ji, Xiaojing [School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072 (China); He, Xuehao, E-mail: xhhe@tju.edu.cn, E-mail: scjiang@tju.edu.cn [Department of Chemistry, School of Science, Tianjin University, and Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Tianjin 300072 (China); Jiang, Shichun, E-mail: xhhe@tju.edu.cn, E-mail: scjiang@tju.edu.cn [School of Material, Tianjin University, Tianjin 300072 (China)

    2014-02-07

    The melting behaviors of α (stable) and β (metastable) isotactic polypropylene (iPP) crystals at ultrafast heating rates are simulated with atomistic molecular dynamics method. Quantitative information about the melting processes of α- and β-iPP crystals at atomistic level is achieved. The result shows that the melting process starts from the interfaces of lamellar crystal through random dislocation of iPP chains along the perpendicular direction of lamellar crystal structure. In the melting process, the lamellar crystal gradually expands but the corresponding thickness decreases. The analysis shows that the system expansion lags behind the crystallinity decreasing and the lagging extents for α- and β-iPP are significantly different. The apparent melting points of α- and β-iPP crystals rise with the increase of the heating rate and lamellar crystal thickness. The apparent melting point of α-iPP crystal is always higher than that of β-iPP at differently heating rates. Applying the Gibbs-Thomson rule and the scaling property of the melting kinetics, the equilibrium melting points of perfect α- and β-iPP crystals are finally predicted and it shows a good agreement with experimental result.

  10. Process of making cryogenically cooled high thermal performance crystal optics

    Science.gov (United States)

    Kuzay, T.M.

    1992-06-23

    A method is disclosed for constructing a cooled optic wherein one or more cavities are milled, drilled or formed using casting or ultrasound laser machining techniques in a single crystal base and filled with porous material having high thermal conductivity at cryogenic temperatures. A non-machined strain-free single crystal can be bonded to the base to produce superior optics. During operation of the cooled optic, N[sub 2] is pumped through the porous material at a sub-cooled cryogenic inlet temperature and with sufficient system pressure to prevent the fluid bulk temperature from reaching saturation. 7 figs.

  11. The review of recent carbonate minerals processing technology

    Science.gov (United States)

    Solihin

    2018-02-01

    Carbonate is one of the groups of minerals that can be found in relatively large amount in the earth crust. The common carbonate minerals are calcium carbonate (calcite, aragonite, depending on its crystal structure), magnesium carbonate (magnesite), calcium-magnesium carbonate (dolomite), and barium carbonate (barite). A large amount of calcite can be found in many places in Indonesia such as Padalarang, Sukabumi, and Tasikmalaya (West Java Provence). Dolomite can be found in a large amount in Gresik, Lamongan, and Tuban (East Java Provence). Magnesite is quite rare in Indonesia, and up to the recent years it can only be found in Padamarang Island (South East Sulawesi Provence). The carbonate has been being exploited through open pit mining activity. Traditionally, calcite can be ground to produce material for brick production, be carved to produce craft product, or be roasted to produce lime for many applications such as raw materials for cement, flux for metal smelting, etc. Meanwhile, dolomite has traditionally been used as a raw material to make brick for local buildings and to make fertilizer for coconut oil plant. Carbonate minerals actually consist of important elements needed by modern application. Calcium is one of the elements needed in artificial bone formation, slow release fertilizer synthesis, dielectric material production, etc. Magnesium is an important material in automotive industry to produce the alloy for vehicle main parts. It is also used as alloying element in the production of special steel for special purpose. Magnesium oxide can be used to produce slow release fertilizer, catalyst and any other modern applications. The aim of this review article is to present in brief the recent technology in processing carbonate minerals. This review covers both the technology that has been industrially proven and the technology that is still in research and development stage. One of the industrially proven technologies to process carbonate mineral is

  12. Statistical processing of technological and radiochemical data

    International Nuclear Information System (INIS)

    Lahodova, Zdena; Vonkova, Kateřina

    2011-01-01

    The project described in this article had two goals. The main goal was to compare technological and radiochemical data from two units of nuclear power plant. The other goal was to check the collection, organization and interpretation of routinely measured data. Monitoring of analytical and radiochemical data is a very valuable source of knowledge for some processes in the primary circuit. Exploratory analysis of one-dimensional data was performed to estimate location and variability and to find extreme values, data trends, distribution, autocorrelation etc. This process allowed for the cleaning and completion of raw data. Then multiple analyses such as multiple comparisons, multiple correlation, variance analysis, and so on were performed. Measured data was organized into a data matrix. The results and graphs such as Box plots, Mahalanobis distance, Biplot, Correlation, and Trend graphs are presented in this article as statistical analysis tools. Tables of data were replaced with graphs because graphs condense large amounts of information into easy-to-understand formats. The significant conclusion of this work is that the collection and comprehension of data is a very substantial part of statistical processing. With well-prepared and well-understood data, its accurate evaluation is possible. Cooperation between the technicians who collect data and the statistician who processes it is also very important. (author)

  13. Process Intensification in Crystallization : Submicron Particle Generation Using Alternative Energy Forms

    NARCIS (Netherlands)

    Radacsi, N.

    2012-01-01

    Crystallization is one of the oldest separation and product formation techniques that continues to be in use today. Despite its long history, it only started to develop significantly in the past few decades. In this thesis, the application of Process Intensification in crystallization is

  14. A new crystallization process in polypropylene highly filled with calcium carbonate

    NARCIS (Netherlands)

    Schawe, Jurgen E.K.; Vermeulen, Paul A.; van Drongelen, Martin

    2015-01-01

    The influence of high amounts of calcium carbonate filler on the crystallization behavior of polypropylene (PP) is investigated by differential scanning calorimetry (DSC) and fast scanning DSC measurements. The non-isothermal crystallization process at industrially relevant cooling rates of about

  15. Crystallization processes in an amorphous Co-Fe-Cr-Si-B alloy under isothermal annealing

    Science.gov (United States)

    Fedorets, A. N.; Pustovalov, E. V.; Plotnikov, V. S.; Modin, E. B.; Kraynova, G. S.; Frolov, A. M.; Tkachev, V. V.; Tsesarskaya, A. K.

    2017-09-01

    Research present the crystallization processes investigation of the amorphous Co67Fe3Cr3Si15B12 alloy. In-situ experiments on heating in a transmission electron microscope (TEM) column were carried out. Critical temperatures influencing material structure are determined. The onset temperature of material crystallization was determined.

  16. Hard Fats As Additives In Palm Oil And Its Relationships To Crystallization Process And Polymorphism

    OpenAIRE

    de Oliveira; Glazieli Marangoni; Ribeiro; Ana Paula Badan; dos Santos; Adenilson Oliveira; Cardoso; Lisandro Pavie; Kieckbusch; Theo Guenter

    2016-01-01

    The application of palm oil in fat-based product can be inappropriate due to its low crystallization rates and formation of crystalline clusters in post-processing stages. The adjustment of these properties can be achieved with the addition of hard fats, which are low-cost industrial products resulting from the process of total catalytic hydrogenation of liquid oils. During the crystallization of palm oil, these components can act as preferential nuclei in a crystalline ordering process, and ...

  17. Acoustic on-line monitoring of solution crystallization process in pure and impure media

    OpenAIRE

    Gherras, Nesrine; Serris, Eric; Févotte, Gilles

    2011-01-01

    International audience; We show that acoustic emission (AE) is a very attractive non intrusive technique for monitoring crystallization processes. AE has been successfully applied in many fields of material sciences and it was also used in the pharmaceutical industry for monitoring various chemical engineering processes including fluidized bed granulation, fluidized bed coating, powder compaction, etc. However, few studies deal with the use of AE to monitoring crystallization processes. The o...

  18. Development of Industrial Process Diagnosis and Measurement Technology

    International Nuclear Information System (INIS)

    Jung, Sung Hee; Kim, Jong Bum; Moon, Jin Ho

    2010-04-01

    Section 1. Industrial Gamma CT Technology for Process Diagnosis: The project is aimed to develop industrial process gamma tomography system for investigation on structural and physical malfunctioning and process media distribution by means of sealed gamma source and radioactive materials. Section 2. Development of RI Hydraulic Detection Technology for Industrial Application: The objectives in this study are to develop the evaluation technology of the hydrological characteristics and the hydraulic detection technology using radioisotope, and to analyze the hydrodynamics and pollutant transport in water environment like surface and subsurface. Section 3. Development of RT-PAT System for Powder Process Diagnosis: The objective of this project is the development of a new radiation technology to improve the accuracy of the determination of moisture content in a powder sample by using radiation source through the so-called RT-PAT (Radiation Technology-Process Analytical Technology), which is a new concept of converging technology between the radiation technology and the process analytical technology

  19. Development of industrial process diagnosis and measurement technology

    International Nuclear Information System (INIS)

    Jung, Sunghee; Kim, Jongbum; Moon, Jinho; Suh, Kyungsuk; Kim, Jongyun

    2012-04-01

    Section1. Industrial Gamma CT Technology for Process Diagnosis The project is aimed to develop industrial process gamma tomography system for investigation on structural and physical malfunctioning and process media distribution by means of sealed gamma source and radioactive materials. Section2. Development of RI Hydraulic Detection Technology for Industrial Application The objectives in this study are to develop the evaluation technology of the hydrological characteristics and the hydraulic detection technology using radioisotope, and to analyze the hydrodynamics and pollutant transport in water environment like surface and subsurface. Section3. Development of RT-PAT System for Powder Process Diagnosis The objective of this project is the development of a new radiation technology to improve the accuracy of the determination of moisture content in a powder sample by using radiation source through the so-called RT-PAT (Radiation Technology-Process Analytical Technology), which is a new concept of converging technology between the radiation technology and the process analytical technology

  20. Crystal-Tolerant Glass Approach For Mitigation Of Crystal Accumulation In Continuous Melters Processing Radioactive Waste

    International Nuclear Information System (INIS)

    Kruger, Albert A.; Rodriguez, Carmen P.; Lang, Jesse B.; Huckleberry, Adam R.; Matyas, Josef; Owen, Antoinette T.

    2012-01-01

    High-level radioactive waste melters are projected to operate in an inefficient manner as they are subjected to artificial constraints, such as minimum liquidus temperature (T L ) or maximum equilibrium fraction of crystallinity at a given temperature. These constraints substantially limit waste loading, but were imposed to prevent clogging of the melter with spinel crystals [(Fe, Ni, Mn, Zn)(Fe, Cr) 2 O 4 ]. In the melter, the glass discharge riser is the most likely location for crystal accumulation during idling because of low glass temperatures, stagnant melts, and small diameter. To address this problem, a series of lab-scale crucible tests were performed with specially formulated glasses to simulate accumulation of spinel in the riser. Thicknesses of accumulated layers were incorporated into empirical model of spinel settling. In addition, T L of glasses was measured and impact of particle agglomeration on accumulation rate was evaluated. Empirical model predicted well the accumulation of single crystals and/or smallscale agglomerates, but, excessive agglomeration observed in high-Ni-Fe glass resulted in an under-prediction of accumulated layers, which gradually worsen over time as an increased number of agglomerates formed. Accumulation rate of ∼14.9 +- 1 nm/s determined for this glass will result in ∼26 mm thick layer in 20 days of melter idling

  1. Software engineering technology transfer: Understanding the process

    Science.gov (United States)

    Zelkowitz, Marvin V.

    1993-01-01

    Technology transfer is of crucial concern to both government and industry today. In this report, the mechanisms developed by NASA to transfer technology are explored and the actual mechanisms used to transfer software development technologies are investigated. Time, cost, and effectiveness of software engineering technology transfer is reported.

  2. Plasma spray technology process parameters and applications

    International Nuclear Information System (INIS)

    Sreekumar, K.P.; Karthikeyan, J.; Ananthapadmanabhan, P.V.; Venkatramani, N.; Chatterjee, U.K.

    1991-01-01

    The current trend in the structural design philosophy is based on the use of substrate with the necessary mechanical properties and a thin coating to exhibit surface properties. Plasma spray process is a versatile surface coating technique which finds extensive application in meeting advance technologies. This report describes the plasma spray technique and its use in developing coatings for various applications. The spray system is desribed in detail including the different variables such as power input to the torch, gas flow rate, powder properties, powder injection, etc. and their interrelation in deciding the quality of the coating. A brief write-up on the various plasma spray coatings developed for different applications is also included. (author). 15 refs., 15 figs., 2 tabs

  3. Image processing of small protein-crystals in electron microscopy

    International Nuclear Information System (INIS)

    Feinberg, D.A.

    1978-11-01

    This electron microscope study was undertaken to determine whether high resolution reconstructed images could be obtained from statistically noisy micrographs by the super-position of several small areas of images of well-ordered crystals of biological macromolecules. Methods of rotational and translational alignment which use Fourier space data were demonstrated to be superior to methods which use Real space image data. After alignment, the addition of the diffraction patterns of four small areas did not produce higher resolution because of unexpected image distortion effects. A method was developed to determine the location of the distortion origin and the coefficients of spiral distortion and pincushion/barrel distortion in order to make future correction of distortions in electron microscope images of large area crystals

  4. Image processing of small protein-crystals in electron microscopy

    Energy Technology Data Exchange (ETDEWEB)

    Feinberg, D.A.

    1978-11-01

    This electron microscope study was undertaken to determine whether high resolution reconstructed images could be obtained from statistically noisy micrographs by the super-position of several small areas of images of well-ordered crystals of biological macromolecules. Methods of rotational and translational alignment which use Fourier space data were demonstrated to be superior to methods which use Real space image data. After alignment, the addition of the diffraction patterns of four small areas did not produce higher resolution because of unexpected image distortion effects. A method was developed to determine the location of the distortion origin and the coefficients of spiral distortion and pincushion/barrel distortion in order to make future correction of distortions in electron microscope images of large area crystals.

  5. Application of Java technology in radiation image processing

    International Nuclear Information System (INIS)

    Cheng Weifeng; Li Zheng; Chen Zhiqiang; Zhang Li; Gao Wenhuan

    2002-01-01

    The acquisition and processing of radiation image plays an important role in modern application of civil nuclear technology. The author analyzes the rationale of Java image processing technology which includes Java AWT, Java 2D and JAI. In order to demonstrate applicability of Java technology in field of image processing, examples of application of JAI technology in processing of radiation images of large container have been given

  6. COMPLEX PROCESSING TECHNOLOGY OF TOMATO RAW MATERIALS

    Directory of Open Access Journals (Sweden)

    A. M. Gadzhieva

    2015-01-01

    Full Text Available Tomatoes grown in the central and southern parts of the country, which contain 5-6 % of solids, including 0.13 % of pectin, 0.86 % of fat, 0.5 % of organic acids; 0.5 % minerals, etc. were used as a subject of research. These tomatoes, grown in the mountains, on soils with high salinity, contain high amounts of valuable components and have a long-term preservation. For the extraction of valuable components from dried tomato pomace CO2 extraction method was applied. Technological and environmental feasibility of tomatoes stage drying in the atmosphere of inert gas in solar dry kiln were evaluated; production scheme of dried tomatoes is improved; a system for tomato pomace drying is developed; a production scheme of powders of pulp, skin and seeds of tomatoes is developed. Combined method of tomato pomace drying involves the simultaneous use of the electromagnetic field of low and ultra-high frequency and blowing product surface with hot nitrogen. Conducting the drying process in an inert gas atmosphere of nitrogen intensified the process of moisture removing from tomatoes. The expediency of using tomato powder as enriching additive was proved. Based on the study of the chemical composition of the tomato powder made from Dagestan varieties of tomatoes, and on the organoleptic evaluation and physico-chemical studies of finished products, we have proved the best degree of recoverability of tomato powder during the production of reconstituted juice and tomato beverages.

  7. Process technology - rare and refractory metals

    International Nuclear Information System (INIS)

    Gupta, C.K.; Bose, D.K.

    1989-01-01

    India has fairly rich resreves of rare and refractory metals. Abundant sources of ilmenite, rutile, zircon and rare earths are found in the placer deposits of the southern and eastern coasts of the country. Columbite-tantalite occur in mica and the mining belts of Bihar and cassiterite deposits are found in Bastar (Madhya Pradesh). Vanadium as a minor associate occurs in bauxites and in the vast deposits of titaniferrous magnetites. Over the years, research and development and pilot plant works in many research organisations in India have built up a sound technological base in the country for process metallurgy of many refractory and rare earth metals starting from their indigenous sources. The present paper provides a comprehensive view of the developments that have taken place till now on the processing of various refractory and rare earth metals with particular reference to the extensive work carried out at the Department of Atomic Energy. The coverage includes mineral benification separation of individual elements, preparation of pure intermediates, techniques of reduction to metal and final purification. The paper also reviews some of the recent developments that have been taken place in these fields and the potential application of these metals in the foreseeable future. (author). 22 refs., 18 fi g., 7 tabs

  8. Embedded RF Photonic Crystals as Routing and Processing Devices in Naval Aperstructures

    National Research Council Canada - National Science Library

    Prather, Dennis W

    2008-01-01

    .... To address these issues, we utilize advanced artificial materials - photonic crystals (PhCs) and meta-material - to construct a sensing head with minaturized antennas as RF receivers and embedded signal channelization for pre-processing...

  9. Effect of processing parameters of rotary ultrasonic machining on surface integrity of potassium dihydrogen phosphate crystals

    Directory of Open Access Journals (Sweden)

    Jianfu Zhang

    2015-09-01

    Full Text Available Potassium dihydrogen phosphate is an important optical crystal. However, high-precision processing of large potassium dihydrogen phosphate crystal workpieces is difficult. In this article, surface roughness and subsurface damage characteristics of a (001 potassium dihydrogen phosphate crystal surface produced by traditional and rotary ultrasonic machining are studied. The influence of process parameters, including spindle speed, feed speed, type and size of sintered diamond wheel, ultrasonic power, and selection of cutting fluid on potassium dihydrogen phosphate crystal surface integrity, was analyzed. The surface integrity, especially the subsurface damage depth, was affected significantly by the ultrasonic power. Metal-sintered diamond tools with high granularity were most suitable for machining potassium dihydrogen phosphate crystal. Cutting fluid played a key role in potassium dihydrogen phosphate crystal machining. A more precise surface can be obtained in machining with a higher spindle speed, lower feed speed, and using kerosene as cutting fluid. Based on the provided optimized process parameters for machining potassium dihydrogen phosphate crystal, a processed surface quality with Ra value of 33 nm and subsurface damage depth value of 6.38 μm was achieved.

  10. A Sensor Fusion Algorithm for Filtering Pyrometer Measurement Noise in the Czochralski Crystallization Process

    OpenAIRE

    Komperød, Magnus; Bones, John Atle; Lie, Bernt

    2011-01-01

    The Czochralski (CZ) crystallization process is used to produce monocrystalline silicon for solar cell wafers and electronics. Tight temperature control of the molten silicon is most important for achieving high crystal quality. SINTEF Materials and Chemistry operates a CZ process. During one CZ batch, two pyrometers were used for temperature measurement. The silicon pyrometer measures the temperature of the molten silicon. This pyrometer is assumed to be accurate, but has much high-frequency...

  11. Diamond MEMS: wafer scale processing, devices, and technology insertion

    Science.gov (United States)

    Carlisle, J. A.

    2009-05-01

    Diamond has long held the promise of revolutionary new devices: impervious chemical barriers, smooth and reliable microscopic machines, and tough mechanical tools. Yet it's been an outsider. Laboratories have been effectively growing diamond crystals for at least 25 years, but the jump to market viability has always been blocked by the expense of diamond production and inability to integrate with other materials. Advances in chemical vapor deposition (CVD) processes have given rise to a hierarchy of carbon films ranging from diamond-like carbon (DLC) to vapor-deposited diamond coatings, however. All have pros and cons based on structure and cost, but they all share some of diamond's heralded attributes. The best performer, in theory, is the purest form of diamond film possible, one absent of graphitic phases. Such a material would capture the extreme hardness, high Young's modulus and chemical inertness of natural diamond. Advanced Diamond Technologies Inc., Romeoville, Ill., is the first company to develop a distinct chemical process to create a marketable phase-pure diamond film. The material, called UNCD® (for ultrananocrystalline diamond), features grain sizes from 3 to 300 nm in size, and layers just 1 to 2 microns thick. With significant advantages over other thin films, UNCD is designed to be inexpensive enough for use in atomic force microscopy (AFM) probes, microelectromechanical machines (MEMS), cell phone circuitry, radio frequency devices, and even biosensors.

  12. Ion Implantation Processing Technologies for Telecommunications Electronics

    Energy Technology Data Exchange (ETDEWEB)

    Haynes, T E

    2000-05-01

    The subject CRADA was a collaboration between Oak Ridge National Laboratory and Bell Laboratories, Lucent Technologies (formerly AT and T Bell Laboratories) to explore the development of ion implantation technologies for silicon integrated circuit (IC) manufacturing.

  13. Research on macro- and microsegregation in semiconductor crystals grown from the melt under the direction of August F. Witt at the Massachusetts Institute of Technology

    Science.gov (United States)

    Wang, C. A.; Carlson, D.; Motakef, S.; Wiegel, M.; Wargo, M. J.

    2004-03-01

    The birth of the modern age of semiconductor electronics in the 1950s required the production of single crystals from the melt. In the early years of this technology, crystals exhibited non-uniform distributions of chemical and structural defects, which directly affected devices produced from this material. Uniform distribution and control of dopants, unintentional impurities, and native defects were identified as critical requirements for continued advances in device technology. However, since at that time fundamental understanding of cause and effect relationships between crystal growth parameters and the ultimate properties of the materials produced was absent, such desirable properties were unattainable. Nevertheless, it was recognized that segregation plays a key role in the creation of non-uniformities. Macrosegregation, a consequence of the directional solidification process, is generally controlled by diffusion and convective melt flows. Microsegregation is governed by local perturbations at the crystal-melt interface. Time-dependent thermal and melt velocity fields at the crystal-melt interface impact the microscopic rate of growth and the solute diffusion boundary layer. Identification of the fundamental parameters that govern axial and radial macro- and microsegregation during bulk semiconductor crystal growth was the research focus during the early years. Key contributions were made by Prof. August F. Witt and his research group. One of the major contributions was the development of quantitative analytical tools for characterization of the crystal growth process. These tools provided the foundation for understanding the origin and nature of segregation phenomena during crystal growth from the melt. This paper is a brief review of his work.

  14. Silicon crystals: Process for manufacturing wafer-like silicon crystals with a columnar structure

    Science.gov (United States)

    Authier, B.

    1978-01-01

    Wafer-like crystals suitable for making solar cells are formed by pouring molten Si containing suitable dopants into a mold of the desired shape and allowing it to solidify in a temperature gradient, whereby the large surface of the melt in contact with the mold is kept at less than 200 D and the free surface is kept at a temperature of 200-1000 D higher, but below the melting point of Si. The mold can also be made in the form of a slit, whereby the 2 sides of the mold are kept at different temperatures. A mold was milled in the surface of a cylindrical graphite block 200 mm in diameter. The granite block was induction heated and the bottom of the mold was cooled by means of a water-cooled Cu plate, so that the surface of the mold in contact with one of the largest surfaces of the melt was held at approximately 800 D. The free surface of the melt was subjected to thermal radiation from a graphite plate located 2 mm from the surface and heated to 1500 D. The Si crystal formed after slow cooling to room temperature had a columnar structure and was cut with a diamond saw into wafers approximately 500 mm thick. Solar cells prepared from these wafers had efficiencies of 10 to 11%.

  15. A Design Process for Creative Technology

    NARCIS (Netherlands)

    Mader, Angelika H.; Eggink, Wouter; Bohemia, E.; Eger, A.; Eggink, W.; Kovacevic, A.; Parkinson, B; Wits, W.

    Creative Technology is a new bachelor programme at the University of Twente. Goal of Creative Technology is to design products and applications that improve the quality of daily life in its manifold aspects, building on Information and Communication Technology (ICT). The application domains range

  16. Technology strategy for subsea processing and transport; Technology Target Areas; TTA6 - Subsea processing and transportation

    Energy Technology Data Exchange (ETDEWEB)

    2008-07-01

    OG21 (www.OG21.org) Norway's official technology strategy for the petroleum sector issued a revised strategy document in November 2005 (new strategy planned in 2009). In this document 'Subsea processing and transport' was identified as one of the eight new technology target areas (TTAs). The overall OG21 strategy document is on an aggregated level, and therefore the Board of OG21 decided that a sub-strategy for each TTA was needed. This document proposes the sub-strategy for the technology target area 'Subsea processing and transport' which covers the technology and competence necessary to effectively transport well stream to a platform or to onshore facilities. This includes multiphase flow modelling, flow assurance challenges to avoid problems with hydrates, asphaltenes and wax, subsea or downhole fluid conditioning including bulk water removal, and optionally complete water removal, and sand handling. It also covers technologies to increase recovery by pressure boosting from subsea pumping and/or subsea compression. Finally it covers technologies to facilitate subsea processing such as control systems and power supply. The vision of the Subsea processing and transport TTA is: Norway is to be the leading international knowledge- and technology cluster in subsea processing and transport: Sustain increased recovery and accelerated production on the NCS by applying subsea processing and efficient transport solutions; Enable >500 km gas/condensate multiphase well stream transport; Enable >200 km oil-dominated multiphase well stream transport; Enable well stream transport of complex fluids; Enable subsea separation, boosting compression, and water injection; Enable deepwater developments; Enable environmentally friendly and energy efficient field development. Increase the export of subsea processing and transport technology: Optimize technology from the NCS for application worldwide; Develop new technology that can meet the challenges found in

  17. Focused beam reflectance measurement as a tool for in situ monitoring of the lactose crystallization process.

    Science.gov (United States)

    Pandalaneni, K; Amamcharla, J K

    2016-07-01

    Lactose accounts for about 75 and 85% of the solids in whey and deproteinized whey, respectively. Production of lactose is usually carried out by a process called crystallization. Several factors including rate of cooling, presence of impurities, and mixing speed influence the crystal size characteristics. To optimize the lactose crystallization process parameters to maximize the lactose yield, it is important to monitor the crystallization process. However, efficient in situ tools to implement at concentrations relevant to the dairy industry are lacking. The objective of the present work was to use a focused beam reflectance measurement (FBRM) system for in situ monitoring of lactose crystallization at supersaturated concentrations (wt/wt) 50, 55, and 60% at 20 and 30°C. The FBRM data were compared with Brix readings collected using a refractometer during isothermal crystallization. Chord length distributions obtained from FBRM in the ranges of lactose crystallization at various concentrations and temperatures was successfully assessed in the study. Copyright © 2016 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

  18. Small angle neutron scattering study of the initial stage of lysozyme crystallization process

    International Nuclear Information System (INIS)

    Minezaki, Yoshiaki; Tanaka, Ichiro; Niimura, Nobuo; Ataka, Mituo; Katsura, Tatsuo.

    1993-01-01

    Despite the enormous amount of information obtained from atomic resolution crystal data, the difficulties encountered in growing crystals preclude structural X-ray studies for the majority of known isolated proteins. The protein crystal growth process can be studied by electron microscopy and by light scattering, and recently Ataka and Asai have discussed the kinetics on lysozyme crystal growth. We have conducted small angle neutron scattering (SANS) experiments on the time evolution from the initial stages to the visible size of crystallization of hen egg-white lysozyme. SANS from several kinds of solutions have been carried out. The SANS result showed the distinctive change of time evolution. We have also conducted the experiments under various unsaturated conditions using SANS. From these experiments, we found that even under unsaturated conditions, aggregation of lysozyme was found to be started, against the result of light-scattering experiments. (author)

  19. Uncertainty modeling process for semantic technology

    Directory of Open Access Journals (Sweden)

    Rommel N. Carvalho

    2016-08-01

    Full Text Available The ubiquity of uncertainty across application domains generates a need for principled support for uncertainty management in semantically aware systems. A probabilistic ontology provides constructs for representing uncertainty in domain ontologies. While the literature has been growing on formalisms for representing uncertainty in ontologies, there remains little guidance in the knowledge engineering literature for how to design probabilistic ontologies. To address the gap, this paper presents the Uncertainty Modeling Process for Semantic Technology (UMP-ST, a new methodology for modeling probabilistic ontologies. To explain how the methodology works and to verify that it can be applied to different scenarios, this paper describes step-by-step the construction of a proof-of-concept probabilistic ontology. The resulting domain model can be used to support identification of fraud in public procurements in Brazil. While the case study illustrates the development of a probabilistic ontology in the PR-OWL probabilistic ontology language, the methodology is applicable to any ontology formalism that properly integrates uncertainty with domain semantics.

  20. A Low-Cost System Based on Image Analysis for Monitoring the Crystal Growth Process

    Directory of Open Access Journals (Sweden)

    Fabrício Venâncio

    2017-05-01

    Full Text Available Many techniques are used to monitor one or more of the phenomena involved in the crystallization process. One of the challenges in crystal growth monitoring is finding techniques that allow direct interpretation of the data. The present study used a low-cost system, composed of a commercial webcam and a simple white LED (Light Emitting Diode illuminator, to follow the calcium carbonate crystal growth process. The experiments were followed with focused beam reflectance measurement (FBRM, a common technique for obtaining information about the formation and growth of crystals. The images obtained in real time were treated with the red, blue, and green (RGB system. The results showed a qualitative response of the system to crystal formation and growth processes, as there was an observed decrease in the signal as the growth process occurred. Control of the crystal growth was managed by increasing the viscosity of the test solution with the addition of monoethylene glycol (MEG at 30% and 70% in a mass to mass relationship, providing different profiles of the RGB average curves. The decrease in the average RGB value became slower as the concentration of MEG was increased; this reflected a lag in the growth process that was proven by the FBRM.

  1. Waste Heat Recovery and Recycling in Thermal Separation Processes: Distillation, Multi-Effect Evaporation (MEE) and Crystallization Processes

    Energy Technology Data Exchange (ETDEWEB)

    Emmanuel A. Dada; Chandrakant B. Panchal; Luke K. Achenie; Aaron Reichl; Chris C. Thomas

    2012-12-03

    Evaporation and crystallization are key thermal separation processes for concentrating and purifying inorganic and organic products with energy consumption over 1,000 trillion Btu/yr. This project focused on a challenging task of recovering low-temperature latent heat that can have a paradigm shift in the way thermal process units will be designed and operated to achieve high-energy efficiency and significantly reduce the carbon footprint as well as water footprint. Moreover, this project has evaluated the technical merits of waste-heat powered thermal heat pumps for recovery of latent heat from distillation, multi-effect evaporation (MEE), and crystallization processes and recycling into the process. The Project Team has estimated the potential energy, economics and environmental benefits with the focus on reduction in CO2 emissions that can be realized by 2020, assuming successful development and commercialization of the technology being developed. Specifically, with aggressive industry-wide applications of heat recovery and recycling with absorption heat pumps, energy savings of about 26.7 trillion Btu/yr have been estimated for distillation process. The direct environmental benefits of this project are the reduced emissions of combustible products. The estimated major reduction in environmental pollutants in the distillation processes is in CO2 emission equivalent to 3.5 billion lbs/year. Energy consumption associated with water supply and treatments can vary between 1,900 kWh and 23,700 kWh per million-gallon water depending on sources of natural waters [US DOE, 2006]. Successful implementation of this technology would significantly reduce the demand for cooling-tower waters, and thereby the use and discharge of water treatment chemicals. The Project Team has also identified and characterized working fluid pairs for the moderate-temperature heat pump. For an MEE process, the two promising fluids are LiNO3+KNO3+NANO3 (53:28:19 ) and LiNO3+KNO3+NANO2

  2. Low Temperature Synthesis of Metal Oxides by a Supercritical Seed Enhanced Crystallization (SSEC) Process

    DEFF Research Database (Denmark)

    Jensen, Henrik; Brummerstedt Iversen, Steen; Joensen, Karsten Dan

    2006-01-01

    material. The nanocrystalline product is obtained without having to resort to costly post-reaction processing and the product is obtained directly after the SSEC process. TiO2 powders produced by the SSEC process were shown to have a crystallinity of 60 % and a crystal size of 7.3 ± 2.6 nm...

  3. Technology for Obtaining Large Size Complex Oxide Crystals for Experiments on Muon-Electron Conversion Registration in High Energy Physics

    Directory of Open Access Journals (Sweden)

    Gerasymov, Ya.

    2014-11-01

    Full Text Available Technological approaches for qualitative large size scintillation crystals growing based on rare-earth silicates are proposed. A method of iridium crucibles charging using eutectic phase instead of a oxyorthosilicate was developed.

  4. Adoption of improved oil palm processing technology in Umuahia ...

    African Journals Online (AJOL)

    It was found that a large percentage of the respondents were aware of the 5 improved oil palm processing technologies with friends and relatives as major source of information. Adoption was significant for 3 out of 5 technologies under study. The major constraints to improved oil palm processing technologies were high ...

  5. The Process of Accepting Technology Innovation for Rural Teachers

    Science.gov (United States)

    Cerovski, Jeremy

    2016-01-01

    In order for educational leaders to facilitate effectively the integration of technology, an understanding of the process rural teachers experience with technology integration is critical. The goal of the qualitative study was to discover and understand rural teachers' process for accepting technology innovation in order to improve the…

  6. TECHNOLOGY SUMMARY ADVANCING TANK WASTE RETRIEVAL AND PROCESSING

    Energy Technology Data Exchange (ETDEWEB)

    SAMS TL; MENDOZA RE

    2010-08-11

    This technology overview provides a high-level summary of technologies being investigated and developed by Washington River Protection Solutions (WRPS) to advance Hanford Site tank waste retrieval and processing. Technology solutions are outlined, along with processes and priorities for selecting and developing them.

  7. TECHNOLOGY SUMMARY ADVANCING TANK WASTE RETREIVAL AND PROCESSING

    Energy Technology Data Exchange (ETDEWEB)

    SAMS TL

    2010-07-07

    This technology overview provides a high-level summary of technologies being investigated and developed by Washington River Protection Solutions (WRPS) to advance Hanford Site tank waste retrieval and processing. Technology solutions are outlined, along with processes and priorities for selecting and developing them.

  8. Integrating Digital Technologies in Teaching Learning Process

    Science.gov (United States)

    Nagarajan, R.; Velmanirajan, K.; Kanna, K. Sankesh

    2013-01-01

    India has made impressive strides in the application of information and communication technology in recent years and this has reflected in a vibrant and fast growing economy. It is now an acknowledged world leader in the knowledge industry. In this paper an attempt is made to highlight the role of Information and Communication Technology (ICT) in…

  9. Knowledge and cognitive process dimensions of Technology ...

    African Journals Online (AJOL)

    Technology was introduced into the South African school curriculum in recognition of the need to produce more engineers, technicians and artisans and thus to be a vehicle to develop readiness for a competitive and technology-driven economy (Department of Basic Education, 2011). Bloch (2007) avers that it is due to the ...

  10. A Technology Approach to Improving Process Management

    Science.gov (United States)

    Dray, Lori; Strasburger, Tom

    2013-01-01

    It is impossible to ignore how technology is infiltrating education. Interactive projectors and other technologies give teachers and students the opportunity to bring lessons to life. Some districts are replacing textbooks with digital content, allowing students to interact with content in new ways. Galion City School District in Galion, Ohio, is…

  11. Electron microscopic studies on the initial process of lysozyme crystal growth

    Science.gov (United States)

    Michinomae, M.; Mochizuki, M.; Ataka, M.

    1999-02-01

    The initial process of lysozyme crystallization has been investigated by negatively stained electron microscopy. In the initial process of crystallization, two steps were distinguished by the appearance of associating protein molecules. One is the formation of the short threads, and the other the formation of the spherical structure (looks like a rice-ball). From among the mass of the rice-balls, larger structure appears. Some of them show the arrangement of molecules as a crystalline lattice. The spacing between the molecules agrees with one of the lattice constants known for the tetragonal lysozyme crystals. The rice-balls may be taken into crystals as essential growth units. Similarly, the thread-like structures may be the unit to form the rice-balls that appear in the next step.

  12. Crystal Plasticity Modeling of Microstructure Evolution and Mechanical Fields During Processing of Metals Using Spectral Databases

    Science.gov (United States)

    Knezevic, Marko; Kalidindi, Surya R.

    2017-05-01

    This article reviews the advances made in the development and implementation of a novel approach to speeding up crystal plasticity simulations of metal processing by one to three orders of magnitude when compared with the conventional approaches, depending on the specific details of implementation. This is mainly accomplished through the use of spectral crystal plasticity (SCP) databases grounded in the compact representation of the functions central to crystal plasticity computations. A key benefit of the databases is that they allow for a noniterative retrieval of constitutive solutions for any arbitrary plastic stretching tensor (i.e., deformation mode) imposed on a crystal of arbitrary orientation. The article emphasizes the latest developments in terms of embedding SCP databases within implicit finite elements. To illustrate the potential of these novel implementations, the results from several process modeling applications including equichannel angular extrusion and rolling are presented and compared with experimental measurements and predictions from other models.

  13. Plan for advanced microelectronics processing technology application

    Energy Technology Data Exchange (ETDEWEB)

    Goland, A.N.

    1990-10-01

    The ultimate objective of the tasks described in the research agreement was to identify resources primarily, but not exclusively, within New York State that are available for the development of a Center for Advanced Microelectronics Processing (CAMP). Identification of those resources would enable Brookhaven National Laboratory to prepare a program plan for the CAMP. In order to achieve the stated goal, the principal investigators undertook to meet the key personnel in relevant NYS industrial and academic organizations to discuss the potential for economic development that could accompany such a Center and to gauge the extent of participation that could be expected from each interested party. Integrated of these discussions was to be achieved through a workshop convened in the summer of 1990. The culmination of this workshop was to be a report (the final report) outlining a plan for implementing a Center in the state. As events unfolded, it became possible to identify the elements of a major center for x-ray lithography on Lone Island at Brookhaven National Laboratory. The principal investigators were than advised to substitute a working document based upon that concept in place of a report based upon the more general CAMP workshop originally envisioned. Following that suggestion from the New York State Science and Technology Foundation, the principals established a working group consisting of representatives of the Grumman Corporation, Columbia University, the State University of New York at Stony Brook, and Brookhaven National Laboratory. Regular meetings and additional communications between these collaborators have produced a preproposal that constitutes the main body of the final report required by the contract. Other components of this final report include the interim report and a brief description of the activities which followed the establishment of the X-ray Lithography Center working group.

  14. Coronagraph Focal-Plane Phase Masks Based on Photonic Crystal Technology: Recent Progress and Observational Strategy

    Science.gov (United States)

    Murakami, Naoshi; Nishikawa, Jun; Sakamoto, Moritsugu; Ise, Akitoshi; Oka, Kazuhiko; Baba, Naoshi; Murakami, Hiroshi; Tamura, Motohide; Traub, Wesley A.; Mawet, Dimitri; hide

    2012-01-01

    Photonic crystal, an artificial periodic nanostructure of refractive indices, is one of the attractive technologies for coronagraph focal-plane masks aiming at direct imaging and characterization of terrestrial extrasolar planets. We manufactured the eight-octant phase mask (8OPM) and the vector vortex mask (VVM) very precisely using the photonic crystal technology. Fully achromatic phase-mask coronagraphs can be realized by applying appropriate polarization filters to the masks. We carried out laboratory experiments of the polarization-filtered 8OPM coronagraph using the High-Contrast Imaging Testbed (HCIT), a state-of-the-art coronagraph simulator at the Jet Propulsion Laboratory (JPL). We report the experimental results of 10-8-level contrast across several wavelengths over 10% bandwidth around 800nm. In addition, we present future prospects and observational strategy for the photonic-crystal mask coronagraphs combined with differential imaging techniques to reach higher contrast. We proposed to apply a polarization-differential imaging (PDI) technique to the VVM coronagraph, in which we built a two-channel coronagraph using polarizing beam splitters to avoid a loss of intensity due to the polarization filters. We also proposed to apply an angular-differential imaging (ADI) technique to the 8OPM coronagraph. The 8OPM/ADI mode avoids an intensity loss due to a phase transition of the mask and provides a full field of view around central stars. We present results of preliminary laboratory demonstrations of the PDI and ADI observational modes with the phase-mask coronagraphs.

  15. Decision Gate Process for Assessment of a Technology Development Portfolio

    Science.gov (United States)

    Kohli, Rajiv; Fishman, Julianna; Hyatt, Mark

    2012-01-01

    The NASA Dust Management Project (DMP) was established to provide technologies (to TRL 6 development level) required to address adverse effects of lunar dust to humans and to exploration systems and equipment, which will reduce life cycle cost and risk, and will increase the probability of sustainable and successful lunar missions. The technology portfolio of DMP consisted of different categories of technologies whose final product is either a technology solution in itself, or one that contributes toward a dust mitigation strategy for a particular application. A Decision Gate Process (DGP) was developed to assess and validate the achievement and priority of the dust mitigation technologies as the technologies progress through the development cycle. The DGP was part of continuous technology assessment and was a critical element of DMP risk management. At the core of the process were technology-specific criteria developed to measure the success of each DMP technology in attaining the technology readiness levels assigned to each decision gate. The DGP accounts for both categories of technologies and qualifies the technology progression from technology development tasks to application areas. The process provided opportunities to validate performance, as well as to identify non-performance in time to adjust resources and direction. This paper describes the overall philosophy of the DGP and the methodology for implementation for DMP, and describes the method for defining the technology evaluation criteria. The process is illustrated by example of an application to a specific DMP technology.

  16. Crystallization characteristics of cast aluminum alloys during a unidirectional solidification process

    International Nuclear Information System (INIS)

    Okayasu, Mitsuhiro; Takeuchi, Shuhei

    2015-01-01

    The crystal orientation characteristics of cast Al–Si, Al–Cu and Al–Mg alloys produced by a unidirectional solidification process are examined. Two distinct crystal orientation patterns are observed: uniform and random formation. A uniform crystal orientation is created by columnar growth of α-Al dendrites in the alloys with low proportions of alloying element, e.g., the Al–Si alloy (with Si <12.6%) and the Al–Cu and Al–Mg alloys (with Cu and Mg <2%). A uniformly organized crystal orientation with [100] direction is created by columnar growth of α-Al dendrites. With increasing proportion of alloying element (>2% Cu or Mg), the uniform crystal orientations collapse in the Al–Cu and Al–Mg alloys, owing to interruption of the columnar α-Al dendrite growth as a result of different dynamics of the alloying atoms and the creation of a core for the eutectic phases. For the hypo-eutectic Al–Si alloys, a uniform crystal orientation is obtained. In contrast, a random orientation can be detected in the hyper-eutectic Al–Si alloy (15% Si), which results from interruption of the growth of the α-Al dendrites due to precipitation of primary Si particles. There is no clear effect of crystal formation on ultimate tensile strength (UTS), whereas crystal orientation does influence the material ductility, with the alloys with a uniform crystal orientation being elongated beyond their UTS points and with necking occurring in the test specimens. In contrast, the alloys with a nonuniform crystal orientation are not elongated beyond their UTS points

  17. Crystallization characteristics of cast aluminum alloys during a unidirectional solidification process

    Energy Technology Data Exchange (ETDEWEB)

    Okayasu, Mitsuhiro, E-mail: mitsuhiro.okayasu@utoronto.ca; Takeuchi, Shuhei

    2015-05-01

    The crystal orientation characteristics of cast Al–Si, Al–Cu and Al–Mg alloys produced by a unidirectional solidification process are examined. Two distinct crystal orientation patterns are observed: uniform and random formation. A uniform crystal orientation is created by columnar growth of α-Al dendrites in the alloys with low proportions of alloying element, e.g., the Al–Si alloy (with Si <12.6%) and the Al–Cu and Al–Mg alloys (with Cu and Mg <2%). A uniformly organized crystal orientation with [100] direction is created by columnar growth of α-Al dendrites. With increasing proportion of alloying element (>2% Cu or Mg), the uniform crystal orientations collapse in the Al–Cu and Al–Mg alloys, owing to interruption of the columnar α-Al dendrite growth as a result of different dynamics of the alloying atoms and the creation of a core for the eutectic phases. For the hypo-eutectic Al–Si alloys, a uniform crystal orientation is obtained. In contrast, a random orientation can be detected in the hyper-eutectic Al–Si alloy (15% Si), which results from interruption of the growth of the α-Al dendrites due to precipitation of primary Si particles. There is no clear effect of crystal formation on ultimate tensile strength (UTS), whereas crystal orientation does influence the material ductility, with the alloys with a uniform crystal orientation being elongated beyond their UTS points and with necking occurring in the test specimens. In contrast, the alloys with a nonuniform crystal orientation are not elongated beyond their UTS points.

  18. Phosphates (V) recovery from phosphorus mineral fertilizers industry wastewater by continuous struvite reaction crystallization process.

    Science.gov (United States)

    Hutnik, Nina; Kozik, Anna; Mazienczuk, Agata; Piotrowski, Krzysztof; Wierzbowska, Boguslawa; Matynia, Andrzej

    2013-07-01

    Continuous DT MSMPR (Draft Tube Mixed Suspension Mixed Product Removal) crystallizer was provided with typical wastewater from phosphorus mineral fertilizers industry (pH < 4, 0.445 mass % of PO4(3-), inorganic impurities presence), dissolved substrates (magnesium and ammonium chlorides) and solution alkalising the environment of struvite MgNH4PO4·6H2O reaction crystallization process. Research ran in constant temperature 298 K assuming stoichiometric proportions of substrates or 20% excess of magnesium ions. Influence of pH (8.5-10) and mean residence time (900-3600 s) on product size distribution, its chemical composition, crystals shape, size-homogeneity and process kinetics was identified. Crystals of mean size ca. 25-37 μm and homogeneity CV 70-83% were produced. The largest crystals, of acceptable homogeneity, were produced using 20% excess of magnesium ions, pH 9 and mean residence time 3600 s. Under these conditions nucleation rate did not exceed 9 × 10(7) 1/(s m(3)) according to SIG (Size Independent Growth) MSMPR kinetic model. Linear crystal growth rate was 4.27 × 10(-9) m/s. Excess of magnesium ions influenced struvite reaction crystallization process yield advantageously. Concentration of phosphate(V) ions decreased from 0.445 to 9.2 × 10(-4) mass %. This can be regarded as a very good process result. In product crystals, besides main component - struvite, all impurities from wastewater were detected analytically. Copyright © 2013 Elsevier Ltd. All rights reserved.

  19. Creep of crystals: High-temperature deformation processes in metals, ceramics and minerals

    Science.gov (United States)

    Poirier, J. P.

    An introductory text describing high-temperature deformation processes in metals, ceramics, and minerals is presented. Among the specific topics discussed are: the mechanical aspects of crystal deformation; lattice defects; and phenomenological and thermodynamical analysis of quasi-steady-state creep. Consideration is also given to: dislocation creep models; the effect of hydrostatic pressure on deformation; creep polygonization; and dynamic recrystallization. The status of experimental techniques for the study of transformation plasticity in crystals is also discussed.

  20. Single-Photon Technologies Based on Quantum-Dots in Photonic Crystals

    DEFF Research Database (Denmark)

    Lehmann, Tau Bernstorff

    In this thesis, the application of semiconductor quantum-dots in photonic crystals is explored as aresource for single-photon technology.Two platforms based on photonic crystals, a cavity and a waveguide, are examined as platformssingle-photon sources. Both platforms demonstrate strong single-photon...... purity under quasi-resonantexcitation. Furthermore the waveguide based platform demonstrates indistinguishable single-photonsat timescales up to 13 ns.A setup for active demultiplexing of single-photons to a three-fold single-photon state is proposed.Using a fast electro-optical modulator, single-photons...... from a quantum-dot are routed on timescalesof the exciton lifetime. Using active demultiplexing a three-fold single-photon state is generated at anextracted rate of 2:03 ±0:49 Hz.An on-chip power divider integrated with a quantum-dot is investigated. Correlation measurementof the photon statistic...

  1. Mineralization Process of Biocemented Sand and Impact of Bacteria and Calcium Ions Concentrations on Crystal Morphology

    OpenAIRE

    Xu, Guobin; Tang, Yang; Lian, Jijian; Yan, Yue; Fu, Dengfeng

    2017-01-01

    Microbial-induced calcite precipitation (MICP) is a sustainable technique used to improve sandy soil. Analysis of the mineralization process, as well as different bacterial suspensions and calcium concentrations on the crystal morphology, revealed that the mineralization process included four stages: self-organised hydrolysis of microorganisms, molecular recognition and interface interaction, growth modulation, and epitaxial growth. By increasing bacterial suspensions and calcium concentratio...

  2. Optimization of process parameters by Taguchi robust design method for the development of nano-crystals of sirolimus using sonication based crystallization

    Energy Technology Data Exchange (ETDEWEB)

    Gandhi, P.J.; Murthy, Z.V.P. [Chemical Engineering Department, S.V. National Institute of Technology, Surat, Gujarat (India); Pati, R.K. [Quantitative Methods and Operations Management, Indian Institute of Management, Kozhikode, Kerala (India)

    2012-01-15

    Taguchi method is widely used by the engineers and researchers across the globe for optimization of process parameters in view of cost, economy and time. Ultrasound based sonication process was used for deriving the nano-crystals of sirolimus in a narrow range. Seven critical process parameters with three levels were optimized with L{sub 18} array design. Crystal size analysis with its zeta potential measured and found that the crystals derived are stable in nature. Also SEM analysis carried out to know size and shape of the crystals and found that the crystals obtained are spherical in nature. Purity of the crystals derived checked with the help of melting point, TLC and HPLC procedures. Characterization of nano-crystals made with Fourier transform infrared spectroscopy and X-ray diffraction analysis. Correlation between the zeta potential and crystal size has been established with the help of scientific and statistical methods. Detailed statistical analysis such as t -test, regression and descriptive statistics of the results has been carried out to explore further information and interactions of process parameters. (copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  3. Integrated modelling in materials and process technology

    DEFF Research Database (Denmark)

    Hattel, Jesper Henri

    2008-01-01

    Integrated modelling of entire process sequences and the subsequent in-service conditions, and multiphysics modelling of the single process steps are areas that increasingly support optimisation of manufactured parts. In the present paper, three different examples of modelling manufacturing...... processes from the viewpoint of combined materials and process modelling are presented: solidification of thin walled ductile cast iron, integrated modelling of spray forming and multiphysics modelling of friction stir welding. The fourth example describes integrated modelling applied to a failure analysis...

  4. Novel technologies for the lost foam casting process

    Science.gov (United States)

    Jiang, Wenming; Fan, Zitian

    2018-03-01

    Lost foam casting (LFC) is a green precision casting process categorized as a near net forming technology. Yet, despite its popularity, it still suffers from some technological problems, such as poor filling ability of the castings, coarse and non-dense microstructure, low mechanical properties for the Al and Mg LFC processes, and defective carburization for the low carbon steel LFC process. These drawbacks restrict the development and widespread application of the LFC process. To solve these problems, the present study developed several novel LFC technologies, namely, LFC technologies under vacuum and low pressure, vibration solidification, and pressure solidification conditions; expendable shell casting technology; and preparation technology of bimetallic castings based on the LFC process. The results showed that the LFC under vacuum and low pressure evidently improved the filling ability and solved the oxidization problem of the alloys, which is suitable for producing complex and thinwall castings. The vibration and pressure solidifications increased the compactness of the castings and refined the microstructure, significantly improving the mechanical properties of the castings. The expendable shell casting technology could solve the pore, carburization, and inclusion defects of the traditional LFC method, obtaining castings with acceptable surface quality. Moreover, the Al/Mg and Al/Al bimetallic castings with acceptable metallurgical bonding were successfully fabricated using the LFC process. These proposed novel LFC technologies can solve the current technological issues and promote the technological progress of the LFC process.

  5. Optimization of processing technology of Rhizoma Pinelliae ...

    African Journals Online (AJOL)

    The fundamental purpose for processing tra- ditional Chinese Medicine is to attenuate toxicity and enhance efficacy. The processing of Rhizoma Pinelliae. Praeparatum is a typical representative. Through dif- ferent approaches of processing, toxic constituents of. Rhizoma Pinelliae are reduced, thus extending its range.

  6. Optimization of processing technology of Rhizoma Pinelliae ...

    African Journals Online (AJOL)

    and Alum', General Records", processing with licorice and ginger in "Zhu Shi", Ming Dynasty's processing- with licorice and lime in the "Compendium of Mate- ria Medica", and processing with ethanol and ginger in the "Prescriptions for Universal Relief", Qing Dynas- ty's "Supplement to Compendium of Materia Medica".

  7. Advanced Manufacturing Office Clean Water Processing Technologies

    Energy Technology Data Exchange (ETDEWEB)

    None

    2018-03-01

    The DOE Office of Energy Efficiency and Renewable Energy (EERE)’s Advanced Manufacturing Office partners with industry, small business, universities, and other stakeholders to identify and invest in emerging technologies with the potential to create high-quality domestic manufacturing jobs and enhance the global competitiveness of the United States.

  8. Laboratory Investigation of Contact Freezing and the Aerosol to Ice Crystal Transformation Process

    Energy Technology Data Exchange (ETDEWEB)

    Shaw, Raymond A. [Michigan Technological Univ., Houghton, MI (United States)

    2014-10-28

    This project has been focused on the following objectives: 1. Investigations of the physical processes governing immersion versus contact nucleation, specifically surface-induced crystallization; 2. Development of a quadrupole particle trap with full thermodynamic control over the temperature range 0 to –40 °C and precisely controlled water vapor saturation ratios for continuous, single-particle measurement of the aerosol to ice crystal transformation process for realistic ice nuclei; 3. Understanding the role of ice nucleation in determining the microphysical properties of mixed-phase clouds, within a framework that allows bridging between laboratory and field measurements.

  9. Radiation Evaluation and Concept Development for Analog Probability Processing Technology

    Data.gov (United States)

    National Aeronautics and Space Administration — Analog probability processing technology has the ability to provide game-changing performance advances and power savings for on-board data processing applications....

  10. Borassus flabellifer L. Brown Crystal Sugar Processing (The Study of Sap pH and Fine Crystal Sucrose (FCS Concentration

    Directory of Open Access Journals (Sweden)

    Azmi Alvian Gabriel

    2017-04-01

    Full Text Available Nira as one of the Borassus flabellirer L. products has a similar characteristics with other agricultural commodities that are easily damaged. This research aims to know the influence of nira’s pH and concentration addition of FCS against characteristics of the brown crystal sugar. Research compiled by using Randomized Block Design (RBD which comprises two factors consisting of 3 levels with 3 times replication. The first factor is pH or degree of nira acidity which consists of 3 level (6.50 (± 0.10; 7.00 (± 0.10; 7.50 (± 0.10 and the second factor is addition of FCS concentration consisting of 3 level (5%; 10%; 15% (b/v. The analyzes used include analysis of organoleptic (color, aroma, taste as well as physical and chemical analyzes (sucrose content, moisture content, ash content, reducing sugar content, insoluble solid content. The analysis results of raw material showed that the pH of palm sap affect the amount of total sugar because the fermentation process. The addition of 10% FCS provides organoleptic results with the best reception at the brown crystal sugar. Physical and chemical test results of products with the best treatment showed that the levels of sucrose in brown crystal sugar was 81.483% in accordance with the minimum requirements specified Indonesian Industrial Standard (IIS, water content of 6.32% dry basis , ash content of 1.78%, reducing sugar amounted to 5.18%, and insoluble solid content of 0.089%.

  11. FY97 Materials & Processes Technology Area Plan

    Science.gov (United States)

    1996-09-01

    preproduction ability. Concentrator with Refractive verdsion engines. Trimarc is "--To meet 1700*F - 2800*F Linear Element Technology). 40% lighter than...graph- can also be used as acuators for tios of 1986 engine per- ite foams for structures. ailerons, flaps and landing gear formance baseline...Aerial Aluminum Garnet SCARLET - Solar Concentrator Vehicle Ni - Nickel with Refractive Linear Ele- UHF - Ultra High Frequency NLO - Nonlinear Optical or

  12. Refining processes in the copper casting technology

    OpenAIRE

    Rzadkosz, S.; Kranc, M.; Garbacz-Klempka, A.; Kozana, J.; Piękoś, M.

    2015-01-01

    The paper presents the analysis of technology of copper and alloyed copper destined for power engineering casts. The casts quality was assessed based on microstructure, chemical content analysis and strength properties tests. Characteristic deoxidising (Logas, Cup) and modifying (ODM2, Kupmod2) formulas were used for the copper where high electrical conductivity was required. Chosen examples of alloyed copper with varied Cr and Zr content were studied, and the optimal heat treatment parameter...

  13. Managing Technological Change: The Process is Key

    Science.gov (United States)

    1989-01-01

    performance suggestive of an electronic sweatshop or informa- and the quality of their work lives has been significantly im- tion assembly line than a...changc the rescrvations system, but without docu- systems, databases, and software applications that comprise mentation or access to the person who...and task HAS BEEN SEEN that instead of trying to minimize change. level, the technology’s inherent flexibili- AS A ITATI particularly with respect to

  14. Application of supercritical carbon dioxide extrusion in food processing technology

    OpenAIRE

    Panak-Balentić Jelena; Ačkar Đurđica; Jozinović Antun; Babić Jurislav; Miličević Borislav; Jokić Stela; Pajin Biljana; Šubarić Drago

    2017-01-01

    Extrusion process is one of the most important innovations of the 20th century applied in many industries. Extrusion is a technology that is increasingly used for the production of various food products, especially snacks and breakfast cereals. Supercritical carbon dioxide (CO2) as a non-toxic, non-flammable and inexpensive, is applied in many processes, including the extrusion technology. Supercritical CO2 extrusion process (SCFX) found its application primarily in the processing and manufac...

  15. Process induced disorder in crystalline materials: differentiating defective crystals from the amorphous form of griseofulvin.

    Science.gov (United States)

    Feng, Tao; Pinal, Rodolfo; Carvajal, M Teresa

    2008-08-01

    This research investigates milling induced disorder in crystalline griseofulvin. Griseofulvin was subjected to cryogenic milling for various lengths of time. For comparison, the amorphous form of griseofulvin was also prepared by the quench melt method. Different analytical techniques were used to study the differences between the cryomilled, amorphous and crystalline forms of the drug. Cryogenic milling of griseofulvin progressively reduces the crystallinity of the drug by inducing crystal defects, rather than amorphous materials. Raman analysis provides evidence of structural differences between the two. The differences between the defective crystals produced by milling and the amorphous form are significant enough as to be measurable in their bulk thermal properties. Defective crystals show significant decrease in the heat of fusion as a function of milling time but do not exhibit a glass transition nor recrystallization from the amorphous form. Crystal defects undergo recrystallization upon heating at temperatures well below the glass transition temperature (T(g)) in a process that is separate and completely independent from the crystallization of the amorphous griseofulvin, observed above T(g). Physical mixtures of defective crystals and amorphous drug demonstrate that the thermal events associated with each form persist in the mixtures, unaffected by the presence of the other form.

  16. Hybrid process technologies in the financial sector

    DEFF Research Database (Denmark)

    Debois, Søren; Hildebrandt, Thomas; Marquard, Morten

    2015-01-01

    the variants of the process that are relevant to them. This paper reports on a project we undertook with such a credit institute where we investigated and addressed these issues by providing a hybrid solution, allowing processes to be modelled using our constraint-based modelling tools, but also supporting...

  17. Thermodynamics for separation-process technology

    Energy Technology Data Exchange (ETDEWEB)

    Prausnitz, J.M.

    1995-10-01

    When contemplating or designing a separation process, every chemical engineer at once recognizes the thermodynamic boundary conditions that must be satisfied: when a mixture is continuously processed to yield at least partially purified products, energy and mass must be conserved and work must be done. In his daily tasks, a chemical engineer uses thermodynamic concepts as tacit, almost subconscious, knowledge. Thus, qualitative thermodynamics significantly informs process conception at its most fundamental level. However, quantitative design requires detailed knowledge of thermodynamic relations and physical chemistry. Most process engineers, concerned with flow sheets and economics, cannot easily command that detailed knowledge and therefore it is advantageous for them to maintain close contact with those specialists who do. Quantitative chemical thermodynamics provides an opportunity to evaluate possible separation processes not only because it may give support to the process engineer`s bold imagination but also because, when coupled with molecular models, it can significantly reduce the experimental effort required to determine an optimum choice of process alternatives. Six examples are presented to indicate the application of thermodynamics for conventional and possible future separation processes.

  18. Semantic Technology Recommendation Based on the Analytic Network Process

    OpenAIRE

    Radulovic, F.; García-Castro, Raúl

    2012-01-01

    Semantic technologies have become widely adopted in recent years, and choosing the right technologies for the problems that users face is often a difficult task. This paper presents an application of the Analytic Network Process for the recommendation of semantic technologies, which is based on a quality model for semantic technologies. Instead of relying on expert-based comparisons of alternatives, the comparisons in our framework depend on real evaluation results. Furthermore, the recommend...

  19. A Survey on Evaluation Factors for Business Process Management Technology

    NARCIS (Netherlands)

    Mutschler, B.B.; Reichert, M.U.

    2006-01-01

    Estimating the value of business process management (BPM) technology is a difficult task to accomplish. Computerized business processes have a strong impact on an organization, and BPM projects have a long-term cost amortization. To systematically analyze BPM technology from an economic-driven

  20. Normal processes of phonon-phonon scattering and thermal conductivity of germanium crystals with isotopic disorder

    CERN Document Server

    Kuleev, I G

    2001-01-01

    The effect of normal processes of the phonon-phonon scattering on the thermal conductivity of the germanium crystals with various isotopic disorder degrees is considered. The phonon pulse redistribution in the normal scattering processes both inside each oscillatory branch (the Simons mechanism) and between various phonon oscillatory branches (the Herring mechanism) is accounted for. The contributions of the longitudinal and cross-sectional phonons drift motion into the thermal conductivity are analyzed. It is shown that the pulse redistribution in the Herring relaxation mechanism leads to essential suppression of the longitudinal phonons drift motion in the isotopically pure germanium crystals. The calculations results of thermal conductivity for the Herring relaxation mechanism agree well with experimental data on the germanium crystals with various isotopic disorder degrees

  1. Mineralization Process of Biocemented Sand and Impact of Bacteria and Calcium Ions Concentrations on Crystal Morphology

    Directory of Open Access Journals (Sweden)

    Guobin Xu

    2017-01-01

    Full Text Available Microbial-induced calcite precipitation (MICP is a sustainable technique used to improve sandy soil. Analysis of the mineralization process, as well as different bacterial suspensions and calcium concentrations on the crystal morphology, revealed that the mineralization process included four stages: self-organised hydrolysis of microorganisms, molecular recognition and interface interaction, growth modulation, and epitaxial growth. By increasing bacterial suspensions and calcium concentrations, the crystal morphology changed from hexahedron to oblique polyhedron to ellipsoid; the best crystal structure occurs at OD600 = 1.0 and [Ca2+] = 0.75 mol/l. It should be noted that interfacial hydrogen bonding is the main force that binds the loose sand particles. These results will help in understanding the mechanism of MICP.

  2. Some technological procedures and equipment for hydrothermal growth of single crystals

    International Nuclear Information System (INIS)

    Popolitov, V.I.; Lobachev, A.N.; Shapiro, A.Y.

    1986-01-01

    The authors have designed, installed and tested a quartz reactor with 200 cm 3 volume in order to directly observe the process of dissolution of solid ingredients, and the synthesis and seeded growth of crystals. The reactor is illustrated. Two C-A thermocouples were used during the experiments to measure the temperature distribution along the outer wall of the reactor in the upper and lower zone. A method is described that was used to grow pyro-and feroelectric single crystals from the ABO 4 group (A-Sb 3+ , Bi 3+ ; B-Nb 5+ , Ta 5+ , Sb 5+ ), and in particular SbSbO 4 , SbNbO 4 , and SbTaO 4

  3. Selecting and controlling API crystal form for pharmaceutical development--strategies and processes.

    Science.gov (United States)

    Yin, Shawn X; Grosso, John A

    2008-11-01

    The success of designing, developing, manufacturing and introducing oral dosage forms of pharmaceutical products into the market relies on many steps, processes, stages and usually three phases of clinical trials. One key process is selecting an appropriate active pharmaceutical ingredient (API) crystal or amorphous form for the final dosage product: the ultimate goal of this selection process is to ensure that the manufactured product contains a stable and bioavailable active ingredient. A thorough knowledge of the solid-state chemistry of the API, the related excipients and the processes to make the product are critical in meeting this goal. Through recently published literature and the authors' experiences, this review describes the concepts and approaches that are used in the development of a truly knowledge-based crystalline API form selection process and highlights the appropriate studies which fit the Quality by Design (QbD) framework for pharmaceutical development activities. This review also discusses the potential API crystal form transformations in the API crystallization, post-crystallization and formulation stages, which are demonstrated by case study examples.

  4. Simulation of warpage induced by non-isothermal crystallization of co-polypropylene during the SLS process

    Science.gov (United States)

    Amado, Antonio; Schmid, Manfred; Wegener, Konrad

    2015-05-01

    Polymer processing using Additive Manufacturing Technologies (AM) has experienced a remarkable growth during the last years. The application range has been expanding rapidly, particularly driven by the so-called consumer 3D printing sector. However, for applications demanding higher requirements in terms of thermo-mechanical properties and dimensional accuracy the long established AM technologies such as Selective Laser Sintering (SLS) do not depict a comparable development. The higher process complexity hinders the number of materials that can be currently processed and the interactions between the different physics involved have not been fully investigated. In case of thermoplastic materials the crystallization kinetics coupled to the shrinkage strain development strongly influences the stability of the process. Thus, the current investigation presents a transient Finite Element simulation of the warpage effect during the SLS process of a new developed polyolefin (co-polypropylene) coupling the thermal, mechanical and phase change equations that control the process. A thermal characterization of the material was performed by means of DSC, integrating the Nakamura model with the classical Hoffmann-Lauritzen theory. The viscoelastic behavior was measured using a plate-plate rheometer at different degrees of undercooling and a phase change-temperature superposition principle was implemented. Additionally, for validation porpoises the warpage development of the first sintered layers was captured employing an optical device. The simulation results depict a good agreement with experimental measurements of deformation, describing the high sensitivity of the geometrical accuracy of the sintered parts related to the processing conditions.

  5. Conjoint Management of Business Processes and Information Technologies

    DEFF Research Database (Denmark)

    Siurdyban, Artur

    and improve business processes. As a consequence, there is a growing need to address managerial aspects of the relationships between information technologies and business processes. The aim of this PhD study is to investigate how the practice of conjoint management of business processes and information...... technologies can be supported and improved. The study is organized into five research papers and this summary. Each paper addresses a different aspect of conjoint management of business processes and information technologies, i.e. problem development and managerial practices on software...... and information technologies in a project environment. It states that both elements are intrinsically related and should be designed and considered together. The second case examines the relationships between information technology management and business process management. It discusses the multi-faceted role...

  6. COMPLEX PROCESSING TECHNOLOGY OF TOMATO RAW MATERIALS

    OpenAIRE

    A. M. Gadzhieva; G. I. Kasianov

    2015-01-01

    Tomatoes grown in the central and southern parts of the country, which contain 5-6 % of solids, including 0.13 % of pectin, 0.86 % of fat, 0.5 % of organic acids; 0.5 % minerals, etc. were used as a subject of research. These tomatoes, grown in the mountains, on soils with high salinity, contain high amounts of valuable components and have a long-term preservation. For the extraction of valuable components from dried tomato pomace CO2 extraction method was applied. Technological and environm...

  7. Modeling of processing technologies in food industry

    Science.gov (United States)

    Korotkov, V. G.; Sagitov, R. F.; Popov, V. P.; Bachirov, V. D.; Akhmadieva, Z. R.; TSirkaeva, E. A.

    2018-03-01

    Currently, the society is facing an urgent need to solve the problems of nutrition (products with increased nutrition value) and to develop energy-saving technologies for food products. A mathematical modeling of heat and mass transfer of polymer materials in the extruder is rather successful these days. Mathematical description of movement and heat exchange during extrusion of gluten-protein-starch-containing material similar to pasta dough in its structure, were taken as a framework for the mathematical model presented in this paper.

  8. Best available technology equivalent controls for B Plant Process Condensate: Tank farm process technology section

    International Nuclear Information System (INIS)

    1988-11-01

    This report evaluates whether proposed controls for the B Plant Process Condensate effluent stream are equivalent to Best Available Technology (BAT) economically achievable. Methods to determine whether the proposed controls for the BCP were equivalent to BAT originated from the Guidance Document for the Hanford Site. The BAT performance standards, which originate from the Clean Water Act, are to be applied to all contaminated liquid effluent discharges currently going to the soil column at the Hanford Site. The B Plant BAT evaluation addressed pollutants that had not been regulated traditionally under Federal or State water-pollution control programs. As a result, only comparisons could be made to existing radiation and water quality standards, and a BAT determination based on the effluent guidelines method (as outlined in the BAT Guidance Document) was not possible. Due to the variability and inconsistency of factors with comparable streams, such as the effluent stream at the Savannah River Plant, a BAT determination by the technology transfer method and treatability studies method was not possible. By using the generic treatment systems method, a one-or two-stage treatment system for dissolved solids removal was concluded to be equivalent to BAT. By performing two economic achievability tests, a one-stage treatment system consisting of mixed bed ion exchange columns was considered to be cost effective and equivalent to BAT. 13 refs., 4 figs., 5 tabs

  9. FY-2010 Process Monitoring Technology Final Report

    Energy Technology Data Exchange (ETDEWEB)

    Orton, Christopher R.; Bryan, Samuel A.; Casella, Amanda J.; Hines, Wes; Levitskaia, Tatiana G.; henkell, J.; Schwantes, Jon M.; Jordan, Elizabeth A.; Lines, Amanda M.; Fraga, Carlos G.; Peterson, James M.; Verdugo, Dawn E.; Christensen, Ronald N.; Peper, Shane M.

    2011-01-01

    During FY 2010, work under the Spectroscopy-Based Process Monitoring task included ordering and receiving four fluid flow meters and four flow visible-near infrared spectrometer cells to be instrumented within the centrifugal contactor system at Pacific Northwest National Laboratory (PNNL). Initial demonstrations of real-time spectroscopic measurements on cold-stream simulants were conducted using plutonium (Pu)/uranium (U) (PUREX) solvent extraction process conditions. The specific test case examined the extraction of neodymium nitrate (Nd(NO3)3) from an aqueous nitric acid (HNO3) feed into a tri-n-butyl phosphate (TBP)/ n-dodecane solvent. Demonstration testing of this system included diverting a sample from the aqueous feed meanwhile monitoring the process in every phase using the on-line spectroscopic process monitoring system. The purpose of this demonstration was to test whether spectroscopic monitoring is capable of determining the mass balance of metal nitrate species involved in a cross-current solvent extraction scheme while also diverting a sample from the system. The diversion scenario involved diverting a portion of the feed from a counter-current extraction system while a continuous extraction experiment was underway. A successful test would demonstrate the ability of the process monitoring system to detect and quantify the diversion of material from the system during a real-time continuous solvent extraction experiment. The system was designed to mimic a PUREX-type extraction process with a bank of four centrifugal contactors. The aqueous feed contained Nd(NO3)3 in HNO3, and the organic phase was composed of TBP/n-dodecane. The amount of sample observed to be diverted by on-line spectroscopic process monitoring was measured to be 3 mmol (3 x 10-3 mol) Nd3+. This value was in excellent agreement with the 2.9 mmol Nd3+ value based on the known mass of sample taken (i.e., diverted) directly from the system feed solution.

  10. Conductivity equations of protons transporting through 2D crystals obtained with the rate process theory and free volume concept

    Science.gov (United States)

    Hao, Tian; Xu, Yuanze; Hao, Ting

    2018-04-01

    The Eyring's rate process theory and free volume concept are employed to treat protons (or other particles) transporting through a 2D (two dimensional) crystal like graphene and hexagonal boron nitride. The protons are assumed to be activated first in order to participate conduction and the conduction rate is dependent on how much free volume available in the system. The obtained proton conductivity equations show that only the number of conduction protons, proton size and packing structure, and the energy barrier associated with 2D crystals are critical; the quantization conductance is unexpectedly predicted with a simple Arrhenius type temperature dependence. The predictions agree well with experimental observations and clear out many puzzles like much smaller energy barrier determined from experiments than from the density function calculations and isotope separation rate independent of the energy barrier of 2D crystals, etc. Our work may deepen our understandings on how protons transport through a membrane and has direct implications on hydrogen related technology and proton involved bioprocesses.

  11. Application of thermal technologies for processing of radioactive waste

    International Nuclear Information System (INIS)

    2006-12-01

    The primary objective of this publication is to provide an overview of the various thermal technologies for processing various solid, liquid, organic and inorganic radioactive waste streams. The advantages, limitations and operating experience of various thermal technologies are explained. This publication also goes beyond previous work on thermal processes by addressing the applicability of each technology to national or regional nuclear programmes of specific relative size (major advanced programmes, small to medium programmes, and emerging programmes with other nuclear applications). The most commonly used thermal processing technologies are reviewed, and the key factors influencing the selection of thermal technologies as part of a national waste management strategy are discussed. Accordingly, the structure and content of this publication is intended to assist decision-makers, regulators, and those charged with developing such strategies to identify and compare thermal technologies for possible inclusion in the mix of available, country-specific waste management processes. This publication can be used most effectively as an initial cutting tool to identify whether any given technology will best serve the local waste management strategy in terms of the waste generated, technical complexity, available economic resources, environmental impact considerations, and end product (output) of the technology. If multiple thermal technologies are being actively considered, this publication should be instrumental in comparing the technologies and assisting the user to reach an informed decision based on local needs, economics and priorities. A detailed set of conclusions is provided in Section 7

  12. Risk calculations in the manufacturing technology selection process

    DEFF Research Database (Denmark)

    Farooq, S.; O'Brien, C.

    2010-01-01

    and supports an industrial manager in achieving objective and comprehensive decisions regarding selection of a manufacturing technology. Originality/value - The paper explains the process of risk calculation in manufacturing technology selection by dividing the decision-making environment into manufacturing...... in the shape of opportunities and threats in different decision-making environments. Practical implications - The research quantifies the risk associated with different available manufacturing technology alternatives. This quantification of risk crystallises the process of technology selection decision making......Purpose - The purpose of this paper is to present result obtained from a developed technology selection framework and provide a detailed insight into the risk calculations and their implications in manufacturing technology selection process. Design/methodology/approach - The results illustrated...

  13. Process for making unsaturated hydrocarbons using microchannel process technology

    Science.gov (United States)

    Tonkovich, Anna Lee [Dublin, OH; Yuschak, Thomas [Lewis Center, OH; LaPlante, Timothy J [Columbus, OH; Rankin, Scott [Columbus, OH; Perry, Steven T [Galloway, OH; Fitzgerald, Sean Patrick [Columbus, OH; Simmons, Wayne W [Dublin, OH; Mazanec, Terry Daymo, Eric

    2011-04-12

    The disclosed invention relates to a process for converting a feed composition comprising one or more hydrocarbons to a product comprising one or more unsaturated hydrocarbons, the process comprising: flowing the feed composition and steam in contact with each other in a microchannel reactor at a temperature in the range from about 200.degree. C. to about 1200.degree. C. to convert the feed composition to the product, the process being characterized by the absence of catalyst for converting the one or more hydrocarbons to one or more unsaturated hydrocarbons. Hydrogen and/or oxygen may be combined with the feed composition and steam.

  14. The temperature gradient on section of casting in process of primary crystallization of chromium cast iron

    Directory of Open Access Journals (Sweden)

    A. Studnicki

    2008-08-01

    Full Text Available The methodology of defining in article was introduced the temperature gradient in process of primary crystallization during cooling the casting from chromium cast iron on basis of measurements of thermal field in test DTA-K3. Insert also the preliminary results of investigations of influence temperature gradient on structure of studied wear resistance chromium cast iron.

  15. The applications of silicon liquid crystal light valves to optical data processing: A review

    Science.gov (United States)

    Efron, U.; Soffer, B. H.; Caulfield, H. J.

    1984-01-01

    The applications of the photo-activated, the CCD-addressed, and the variable-grating mode liquid crystal light valves (LCLVs) to optical data processing are described. These applications include image correlation, level slicing, spectral analysis and correlation, bi-spectral image division, and matrix-matrix multiplication.

  16. Application of membrane technologies for liquid radioactive waste processing

    International Nuclear Information System (INIS)

    2004-01-01

    Membrane separation processes have made impressive progress since the first synthesis of membranes almost 40 years ago. This progress was driven by strong technological needs and commercial expectations. As a result the range of successful applications of membranes and membrane processes is continuously broadening. In addition, increasing application of membrane processes and technologies lies in the increasing variations of the nature and characteristics of commercial membranes and membrane apparatus. The objective of the report is to review the information on application of membrane technologies in the processing of liquid radioactive waste. The report covers the various types of membranes, equipment design, range of applications, operational experience and the performance characteristics of different membrane processes. The report aims to provide Member States with basic information on the applicability and limitations of membrane separation technologies for processing liquid radioactive waste streams

  17. Refining processes in the copper casting technology

    Directory of Open Access Journals (Sweden)

    S. Rzadkosz

    2015-01-01

    Full Text Available The paper presents the analysis of technology of copper and alloyed copper destined for power engineering casts. The casts quality was assessed based on microstructure, chemical content analysis and strength properties tests. Characteristic deoxidising (Logas, Cup and modifying (ODM2, Kupmod2 formulas were used for the copper where high electrical conductivity was required. Chosen examples of alloyed copper with varied Cr and Zr content were studied, and the optimal heat treatment parameters were tested for a chosen chromium copper content, based on the criterion of hardness and electrical conductivity tests. Searching for materials with high wear resistance, the influence of variable silicone content on the properties of CuNiSi alloy was researched.

  18. Gasification — the process and the technology

    NARCIS (Netherlands)

    van Swaaij, Willibrordus Petrus Maria

    1981-01-01

    Thermochemical gasification of biomass can produce low, medium and high calorific value gases. The characteristics, applications and potential of the different processes and reactor types are discussed. The introduction of biomass gasification on a large or intermediate scale for the production of

  19. Educational Design and Construction: Processes and Technologies

    NARCIS (Netherlands)

    McKenney, Susan; Reeves, Thomas C.; Gros, Begona; Kinshuk,; Maina, Marcelo

    2015-01-01

    There are no one-size-fits-all steps for tackling different design challenges within the context of education. There are, however, processes and activities that are often useful. Developing a repertoire so that designers can select and use the most fruitful and fitting approaches for specific

  20. The role of the amorphous phase in the re-crystallization process of cold-crystallized poly(ethylene terephthalate)

    Science.gov (United States)

    Pieruccini, M.; Flores, A.; Nöchel, U.; di Marco, G.; Stribeck, N.; Baltá Calleja, F. J.

    2008-12-01

    The process of re-crystallization in poly(ethylene terephthalate) is studied by means of X-ray diffraction (SAXS and WAXS) and dynamical mechanical thermal analysis. Samples cold-crystallized for 9h at the temperatures T c = 100 fcir#circ;C and T c = 160 fcir#circ;C, i.e. in the middle of the α relaxation region and close to its upper bound, respectively, are analyzed. During heating from room temperature, a structural rearrangement of the stacks is always found at T r ≃ T c + 20 fcir#circ;C. This process is characterized by a decrease of the linear crystallinity, irrespective of Tc; on the other hand, the WAXS crystallinity never increases with T below Tc+30fcir#circ;C. The lamellar thickness in the low-Tc sample decreases significantly after the structural transition, whereas in the high-Tc sample the lamellar thickness remains almost unchanged. In both, high- and low-Tc, the interlamellar thickness increases above Tr. Moreover, the high-Tc sample shows a lower rate of decrease of the mechanical performance with increasing T as the threshold Tr is crossed. This result is interpreted in terms of the formation of rigid amorphous domains where the chains are partially oriented. The presence of these domains would determine i) the stabilization of the crystalline lamellae from the thermodynamic point of view and ii) the increase of the elastic modulus of the amorphous interlamellar regions. This idea is discussed by resorting to a phase diagram. An estimation of the chemical-potential increase of the interlamellar amorphous regions, due to the enhancement of the structural constraints hindering segmental mobility, is offered. Finally, previous calculations developed within the framework of the Gaussian chain model (F.J. Baltá Calleja et al., Phys. Rev. B 75, 224201 (2007)) are used here to estimate the degree of chain orientation induced by the structural transition of the stacks.

  1. On the Benefit of Using Mobile Technologies in Business Processes

    OpenAIRE

    Deibert, Sina; Rothlauf, Franz

    2006-01-01

    The rapid technical progress in the development of mobile devices and technologies offers new possibilities for improving and streamlining the performance of business processes. However, only few successful mobile applications exist in the business area. This paper discusses the benefits an enterprise can gain by using mobile technologies in business processes. It presents general indicators to measure the performance of business processes and shows how these indicators must be adapted to be ...

  2. Technology Summary Advancing Tank Waste Retrieval And Processing

    International Nuclear Information System (INIS)

    Sams, T.L.; Mendoza, R.E.

    2010-01-01

    This technology overview provides a high-level summary of technologies being investigated and developed by Washington River Protection Solutions (WRPS) to advance Hanford Site tank waste retrieval and processing. Technology solutions are outlined, along with processes and priorities for selecting and developing them. This technology overview provides a high-level summary of technologies being investigated, developed, and deployed by WRPS to advance Hanford Site tank waste retrieval and processing. Transformational technologies are needed to complete Hanford tank waste retrieval and treatment by 12/31/2047. Hanford's underground waste storage tanks hold approximately 57 million gallons of radiochemical waste from nuclear defense production - more tank waste than any other site in the United States. In addition, the waste is uniquely complicated because it contains constituents from at least six major radiochemical processes and several lesser processes. It is intermixed and complexed more than any other waste collection known to exist in the world. The multi-faceted nature of Hanford's tank waste means that legally binding agreements in the Federal Facility Agreement and Consent Order (known as the Tri-Party Agreement) and between the Department of Energy (DOE) and its contractors may not be met using current vitrification schedules, plans, and methods. WRPS and the DOE are developing, testing, and deploying technologies to meet the necessary commitments and complete the DOE's River Protection Project (RPP) mission within environmentally acceptable requirements. Technology solutions are outlined, along with processes and priorities for selecting and developing them. DOE's Office of Environmental Management (EM) identifies the environmental management technology needs and the activities necessary to address them. The U.S. Congress then funds these activities through EM or the DOE field offices. Finally, an array of entities that include DOE site prime contractors and

  3. Measurements of processes in ruthenium oxide film electrodes with the quartz-crystal microbalance technique

    International Nuclear Information System (INIS)

    Buttry, D.; Gottesfeld, S.

    1987-01-01

    The authors describe the first application of the quartz-crystal microbalance (QCM) technique for monitoring electrochemical processes in oxide film electrodes. They have investigated a film of ruthenium oxide, applied by the thermal decomposition of ruthenium chloride onto one side of the quartz-crystal. The quartz-crystal was precoated with gold keyhole patterns on both sides for inducing the 5 MHz resonance, followed by a thin Ti layer to ensure good adherence of the ruthenium oxide. Ruthenium oxide films are being investigated at Los Alamos for potential use in electrochemical capacitors. The material exhibits large charge capacity per geometric area and fast charge-discharge rates. Different possible processes can be responsible for charge compensation in such oxide materials, including those associated with simple double-layer charging, with pseudocapacitance, and with ion insertion into the small grains of the high-surface-area oxide material. The dynamics of such processes are determined, for a given oxide film, by the nature of the electrolyte and the resulting mechanism of charge-compensation. The QCM technique provides interesting information on these processes, as well as on film hydration and film dissolution process. The authors' initial results are presented in this paper. The results demonstrate the QCM as a sensitive tool for following not only ionic insertion processes during potential modulation, but also processes of film swelling and film dissolution

  4. Electrostatic coating technologies for food processing.

    Science.gov (United States)

    Barringer, Sheryl A; Sumonsiri, Nutsuda

    2015-01-01

    The application of electrostatics in both powder and liquid coating can improve the quality of food, such as its appearance, aroma, taste, and shelf life. Coatings can be found most commonly in the snack food industry, as well as in confectionery, bakery, meat and cheese processing. In electrostatic powder coating, the most important factors influencing coating quality are powder particle size, density, flowability, charge, and resistivity, as well as the surface properties and characteristics of the target. The most important factors during electrostatic liquid coating, also known as electrohydrodynamic coating, include applied voltage and electrical resistivity and viscosity of the liquid. A good understanding of these factors is needed for the design of optimal coating systems for food processing.

  5. Innovative Pedagogical Processes Involving Educational Technology

    DEFF Research Database (Denmark)

    Weitze, Charlotte Lærke

    This design-based research project investigates the elements, methods, processes and practices that can contribute to the creation of reflected, innovative and motivating learning designs for teachers and students in a hybrid synchronous video-mediated teaching context, with a focus on how...... about how design and learning processes can support continuous pedagogical innovation and competence development. The objective of the learning designs was to create motivating learning experiences for the students in the hybrid synchronous video-mediated learning environment, to which end...... it experimented with gamified learning designs. This involved the students designing digital games while implementing learning goals from their curriculum. The project thus created knowledge about which learning designs and competence development models were possible in this environment, which learning designs...

  6. Kinetic studies on the degradation of crystal violet by the Fenton oxidation process.

    Science.gov (United States)

    Wu, H; Fan, M M; Li, C F; Peng, M; Sheng, L J; Pan, Q; Song, G W

    2010-01-01

    The degradation of dye crystal violet (CV) by Fenton oxidation process was investigated. The UV-Vis spectrogram has shown that CV can be degraded effectively by Fenton oxidation process. Different system variables namely initial H(2)O(2) concentration, initial Fe(2 + ) concentration and reaction temperature, which have effect on the degradation of CV by Fenton oxidation process, have been studied systematically. The degradation kinetics of CV was also elucidated based on the experimental data. The degradation of CV obeys the first-order reaction kinetics. The kinetic model can be described as k=1.5 exp(-(7.5)/(RT))[H(2)O(2)](0)(0.8718)[Fe(2+)](0)(0.5062). According to the IR spectrogram, it is concluded that the benzene ring of crystal violet has been destroyed by Fenton oxidation. The result will be useful in treating dyeing wastewater containing CV by Fenton oxidation process.

  7. Non-classical crystallization of thin films and nanostructures in CVD and PVD processes

    CERN Document Server

    Hwang, Nong Moon

    2016-01-01

    This book provides a comprehensive introduction to a recently-developed approach to the growth mechanism of thin films and nanostructures via chemical vapour deposition (CVD). Starting from the underlying principles of the low pressure synthesis of diamond films, it is shown that diamond growth occurs not by individual atoms but by charged nanoparticles. This newly-discovered growth mechanism turns out to be general to many CVD and some physical vapor deposition (PVD) processes. This non-classical crystallization is a new paradigm of crystal growth, with active research taking place on growth in solution, especially in biomineralization processes. Established understanding of the growth of thin films and nanostructures is based around processes involving individual atoms or molecules. According to the author’s research over the last two decades, however, the generation of charged gas phase nuclei is shown to be the rule rather than the exception in the CVD process, and charged gas phase nuclei are actively ...

  8. Hydrometallurgical Processing Technology of Titanomagnetite Ores

    Directory of Open Access Journals (Sweden)

    Victor Ivanovich Sachkov

    2017-12-01

    Full Text Available In this paper, we study the possibility of obtaining iron and titanium-vanadium concentrates with highest contents of iron and titanium, respectively, through hydrometallurgical processing of the titanomagnetite ores of the Chineisk deposit. We varied two key parameters to determine the efficiency of the process: (a concentration of leaching solution (ammonium fluoride; and (b acidity of solution. Ammonium fluoride concentration was varied from 0.08 mol/L to 4.2 mol/L with the other fixed parameters. It was shown that optimum ammonium fluoride concentration for leaching the ore is 0.42 mol/L; at these concentrations iron and titanium contents are about 62.8 wt % and 3.5 wt % in solid phase, respectively. The acidity of solution was changed by adding of hydrofluoric acid with varied concentration (from 0.86 mol/L to 4.07 mol/L to ammonium fluoride solution with fixed concentration of 0.42 mol/L. The best results (degree of titanium extraction = 63.7% were obtained when using a solution of hydrofluoric acid with concentration 4.07 mol/L. In this case, the addition of acid makes it possible to increase the Fe/Ti ratio by 3.4 times in comparison with the original ore. Thus, we conclude that acidity and the concentration of ammonium fluoride solution significantly influences the selectivity of the hydrometallurgical process.

  9. Crystallization process of Fe80P20-xSix amorphous alloys

    International Nuclear Information System (INIS)

    Ohnuma, Masato; Sasaki, Osamu; Kuwano, Hisashi; Katano, Susumu; Morii, Yukio; Funahashi, Satoru; Child, H.R.; Hamaguchi, Yoshikazu.

    1993-01-01

    The crystallization process of Fe 80 P 20-x Si x amorphous alloys has been studied by electrical resistivity, X-ray diffraction, neutron diffraction, and transmission electron microscopy. This process is classified into two different patterns with a boundary of 6 at%Si. In the alloys containing less than 6 at%Si, α-Fe and Fe 3 P, both of which are stable phases, precipitate from the amorphous matrix directly. In the crystallization of the amorphous alloys containing over 6 at%Si, two complex phases are observed in the early stages. We found that these two phases are isostructural with the α-Mn type and β-Mn type phase. After these two metastable phases disappear, another metastable phase which is probably Fe 2 P appears. In the final stage of the crystallization, however, existing crystalline phases are stable α-Fe (or ordered Fe 3 Si) and Fe 3 P. In the isothermal crystallization process of the Fe 80 P 14 Si 6 amorphous alloy, only the α-Mn type phase is observed as the metastable phase at high temperatures such as 683, 703 and 723 K; however, at a lower temperature such as 668 K, no metastable phase is observed. The precipitation of the metastable α-Mn type and/or β-Mn type phases, which consist of the Frank-Kasper coordination polyhedra, can be closely related to the local structure in these amorphous alloys. (author)

  10. Technology Estimating: A Process to Determine the Cost and Schedule of Space Technology Research and Development

    Science.gov (United States)

    Cole, Stuart K.; Reeves, John D.; Williams-Byrd, Julie A.; Greenberg, Marc; Comstock, Doug; Olds, John R.; Wallace, Jon; DePasquale, Dominic; Schaffer, Mark

    2013-01-01

    NASA is investing in new technologies that include 14 primary technology roadmap areas, and aeronautics. Understanding the cost for research and development of these technologies and the time it takes to increase the maturity of the technology is important to the support of the ongoing and future NASA missions. Overall, technology estimating may help provide guidance to technology investment strategies to help improve evaluation of technology affordability, and aid in decision support. The research provides a summary of the framework development of a Technology Estimating process where four technology roadmap areas were selected to be studied. The framework includes definition of terms, discussion for narrowing the focus from 14 NASA Technology Roadmap areas to four, and further refinement to include technologies, TRL range of 2 to 6. Included in this paper is a discussion to address the evaluation of 20 unique technology parameters that were initially identified, evaluated and then subsequently reduced for use in characterizing these technologies. A discussion of data acquisition effort and criteria established for data quality are provided. The findings obtained during the research included gaps identified, and a description of a spreadsheet-based estimating tool initiated as a part of the Technology Estimating process.

  11. Performance Analyses in an Assistive Technology Service Delivery Process

    DEFF Research Database (Denmark)

    Petersen, Anne Karin

    Performance Analyses in an Assistive Technology Service Delivery Process.Keywords: process model, occupational performance, assistive technologiesThe Poster is about teaching students, using models and theory in education and practice. It is related to Occupational therapy process and professional...... af top-til-bund, klientcentreret og aktivitetsbaseret interventioner, ERGO/MunksgaardFisher, A. &, Griswold, L. A., 2014. Performance Skills. I: B.Schell red.2014 Occupational Therapy. Willard &Spackman’s occupational therapy. -12th ed., p.249-264Cook A.M., Polgar J.M. (2015) Assistive Technologies...

  12. FEATURES OF USING AUGMENTED REALITY TECHNOLOGY TO SUPPORT EDUCATIONAL PROCESSES

    Directory of Open Access Journals (Sweden)

    Yury A. Kravchenko

    2014-01-01

    Full Text Available The paper discusses the concept and technology of augmented reality, the rationale given the relevance and timeliness of its use to support educational processes. Paper is a survey and study of the possibility of using augmented reality technology in education. Architecture is proposed and constructed algorithms of the software system management QR-codes media objects. An overview of the features and uses of augmented reality technology to support educational processes is displayed, as an option of a new form of visual demonstration of complex objects, models and processes

  13. Application of image processing technology in yarn hairiness detection

    Directory of Open Access Journals (Sweden)

    Guohong ZHANG

    2016-02-01

    Full Text Available Digital image processing technology is one of the new methods for yarn detection, which can realize the digital characterization and objective evaluation of yarn appearance. This paper overviews the current status of development and application of digital image processing technology used for yarn hairiness evaluation, and analyzes and compares the traditional detection methods and this new developed method. Compared with the traditional methods, the image processing technology based method is more objective, fast and accurate, which is the vital development trend of the yarn appearance evaluation.

  14. [Mechanized system for planning technological processes].

    Science.gov (United States)

    Pashchenko, V S; Shapiro, A M

    1977-01-01

    A mechanized system for the production processes planning involving the use of an electronic code device for data preparation on a punched tape of the "EPECT-IT" type, at the base of which there are classifiers of standard operations and transitions to individual design members, is considered. A fragment of the classifier and a skeleton diagram of the system are presented. It is pointed out that the use of the system helps improve the quality of the design work, as well as to yield considerable economic advantages. The system is in operation at some enterprises of the medical engineering industry.

  15. [Study on baking processing technology of hui medicine Aconitum flavum].

    Science.gov (United States)

    Fu, Xue-yan; Zhang, Bai-tong; Li, Ting-ting; Dong, Lin; Hao, Wen-jing; Yu, Liang

    2013-12-01

    To screen and optimize the processing technology of Aconitum flavum. The acute-toxicity, anti-inflammatory and analgesic experiments were used as indexes. Four processing methods, including decoction, streaming, baking and processing with Chebulae Fructus decoction, were compared to screen the optimum processing method for Aconitum flavum. The baking time was also optimized. The optimal baked technology was that 1-2 mm decoction pieces was baked at 105 degrees C for 3 hours. The baking method is proved to be the optimal processing method of Aconitum flavum. It is shown that this method is simple and stable.

  16. FMR linewidth and the crystallization processes in Co-based amorphous microwires

    Energy Technology Data Exchange (ETDEWEB)

    Chrischon, D.S.; Beck, F. [Departamento de Física, Universidade Federal de Santa Maria (UFSM), Santa Maria, 97105-900 RS (Brazil); Sossmeier, K.D. [Instituto Latino-Americano de Ciências da Vida e da Natureza, Universidade Federal da Integração Latino-Americana (UNILA), Foz do Iguaçu, 85867-970 PR (Brazil); Carara, M., E-mail: marcos.carara@gmail.com [Departamento de Física, Universidade Federal de Santa Maria (UFSM), Santa Maria, 97105-900 RS (Brazil)

    2013-06-15

    The ferromagnetic resonance (FMR) technique has been used for many years as a tool to characterize the dynamic magnetic properties of bulk, thin film magnetic materials and microwires. Also, the FMR linewidth is associated to the dissipative processes involved on the magnetization dynamics. Such dissipative channels may be separated in two groups: intrinsic and extrinsic ones. While the first one is related mainly to the Landau–Lifshitz (LL) and eddy-currents damping mechanisms, the second one take in to account contributions coming from the inhomogeneities in the sample. Each one of these relaxation processes contributes to the FMR linewidth in a different frequency and/or magnetic field range and they can be separated by an appropriate FMR linewidth measurement. This work presents FMR measurements, obtained by the impedance method, ranging from 100 KHz to 1.8 GHz, in Joule annealed Co-based amorphous microwires. It is shown that the crystallization process can be followed by the evaluation of the extrinsic magnetization damping terms, specifically analyzing contributions from inhomogeneities to the FMR linewidth. From the fitting of models which consider LL damping term, anisotropy dispersion and magnon scattering to the experimental data, three ranges of annealing temperatures can be distinguished in terms of spin dynamics on the studied samples: annealing temperatures lower than the Curie temperature, a temperature range between the Curie and the crystallization temperature and another temperature range above the crystallization temperature. - Highlights: ► This work presents FMR linewidth measurements on Co-based amorphous microwires. ► Crystallization process can be followed by the evaluation of the damping terms. ► Three ranges of annealing temperatures can be distinguished in terms of spin dynamics. ► The temperature ranges are: below the T{sub Curie}, above the T{sub Crystal} and between both.

  17. Crystal engineering of lactose using electrospray technology: carrier for pulmonary drug delivery.

    Science.gov (United States)

    Patil, Sharvil; Mahadik, Abhijeet; Nalawade, Pradeep; More, Priyesh

    2017-12-01

    Dry powder inhalers (DPIs) consisting of a powder mixture containing coarse carrier particles (generally lactose) and micronized drug particles are used for lung drug delivery. The effective drug delivery to the lungs depends on size and shape of carrier particles. Thus, various methods have been proposed for engineering lactose particles to enhance drug delivery to lungs. The objective of current work was to assess suitability of electrospray technology toward crystal engineering of lactose. Further, utility of the prepared lactose particles as a carrier in DPI was evaluated. Saturated lactose solutions were electrosprayed to obtain electrosprayed lactose (EL) particles. The polymorphic form of EL was determined using Fourier transform infrared spectroscopy, powder X-ray diffractometry, and differential scanning calorimetry. In addition, morphological, surface textural, and flow properties of EL were determined using scanning electron microscopy and Carr's index, respectively. The aerosolization properties of EL were determined using twin-stage impinger and compared with commercial lactose particles [Respitose ® (SV003, Goch, Germany)] used in DPI formulations. EL was found to contain both isomers (α and β) of lactose having flow properties comparable to Respitose ® (SV003). In addition, the aerosolization properties of EL were found to be significantly improved when compared to Respitose ® (SV003) which could be attributed to morphological (high elongation ratio) and surface characteristic (smooth surface) alterations induced by electrospray technology. Electrospray technology can serve as an alternative technique for continuous manufacturing of engineered lactose particles which can be used as a carrier in DPI formulations.

  18. Status and prospect of radiation processing technology in Malaysia

    International Nuclear Information System (INIS)

    Khairul Zaman Hj Mohd Dahlan; Nahrul Khair Alang Md Rashid

    2001-01-01

    Radiation processing technology in Malaysia is gaining acceptance by the local industry. The technology has proven to enhance the industrial efficiency, productivity and improve product quality and competitiveness. For many years, variety of radiation crosslinkable materials based on synthetic polymers have been produced either in the form of thermoplastic resins, polymer blends or composites. Today, effort is being focused towards producing environmentally friendly and biodegradable materials using natural polymers. The government of Malaysia through the Malaysian Institute for Nuclear Technology Research (MINT) has developed research program to utilize indigenous materials such as natural rubber, palm oil and polysaccharide. Radiation processing technology is used to process (crosslink/grafting/curing) the materials at a competitive cost. This technology can be applied in several industrial sectors such as automobile, aerospace, construction and healthcare. (author)

  19. Status and prospect of radiation processing technology in Malaysia

    Energy Technology Data Exchange (ETDEWEB)

    Khairul Zaman Hj. Mohd Dahlan; Nahrul Khair Alang Md Rashid [Malaysian Institute for Nuclear Technology Research (MINT), Bangi, Selangor Darul Ehsan (Malaysia)

    2001-03-01

    Radiation processing technology in Malaysia is gaining acceptance by the local industry. The technology has proven to enhance the industrial efficiency, productivity and improve product quality and competitiveness. For many years, variety of radiation crosslinkable materials based on synthetic polymers have been produced either in the form of thermoplastic resins, polymer blends or composites. Today, effort is being focused towards producing environmentally friendly and biodegradable materials using natural polymers. The government of Malaysia through the Malaysian Institute for Nuclear Technology Research (MINT) has developed research program to utilize indigenous materials such as natural rubber, palm oil and polysaccharide. Radiation processing technology is used to process (crosslink/grafting/curing) the materials at a competitive cost. This technology can be applied in several industrial sectors such as automobile, aerospace, construction and healthcare. (author)

  20. Dry process fuel performance technology development

    Energy Technology Data Exchange (ETDEWEB)

    Kang, Kweon Ho; Kim, K. W.; Kim, B. K. (and others)

    2006-06-15

    The objective of the project is to establish the performance evaluation system of DUPIC fuel during the Phase III R and D. In order to fulfil this objectives, property model development of DUPIC fuel and irradiation test was carried out in Hanaro using the instrumented rig. Also, the analysis on the in-reactor behavior analysis of DUPIC fuel, out-pile test using simulated DUPIC fuel as well as performance and integrity assessment in a commercial reactor were performed during this Phase. The R and D results of the Phase III are summarized as follows: Fabrication process establishment of simulated DUPIC fuel for property measurement, Property model development for the DUPIC fuel, Performance evaluation of DUPIC fuel via irradiation test in Hanaro, Post irradiation examination of irradiated fuel and performance analysis, Development of DUPIC fuel performance code (KAOS)

  1. Process Technology for Immobilized Lipasecatalyzed Reactions

    DEFF Research Database (Denmark)

    Xu, Yuan

    (e.g. a hydrophobic carrier for the immobilized lipase and the capabilities to provide sufficient mixing as well as stepwise/continuous feeding of ethanol to the reactor). An STR is efficient for batch operation while a PBR is efficient for a continuous production. An STR can more easily provide...... sufficient external mass transfer for a reaction, but will lead to more mechanical damage of the biocatalyst particles, than a PBR. A reactor combination of CSTR with PBR can couple the advantages of both, delivering an efficient continuous process. The second case study (esterification) shares some similar......-catalyzed transesterification is that it is multi-phasic system. The by-product glycerol can potentially impose inhibitory effects on immobilized lipases and likewise the un-dissolved ethanol can inhibit the lipase. The options for addressing these issues can be used as the basis for selecting the biocatalyst and the reactor...

  2. Dry process fuel performance technology development

    International Nuclear Information System (INIS)

    Kang, Kweon Ho; Kim, K. W.; Kim, B. K.

    2006-06-01

    The objective of the project is to establish the performance evaluation system of DUPIC fuel during the Phase III R and D. In order to fulfil this objectives, property model development of DUPIC fuel and irradiation test was carried out in Hanaro using the instrumented rig. Also, the analysis on the in-reactor behavior analysis of DUPIC fuel, out-pile test using simulated DUPIC fuel as well as performance and integrity assessment in a commercial reactor were performed during this Phase. The R and D results of the Phase III are summarized as follows: Fabrication process establishment of simulated DUPIC fuel for property measurement, Property model development for the DUPIC fuel, Performance evaluation of DUPIC fuel via irradiation test in Hanaro, Post irradiation examination of irradiated fuel and performance analysis, Development of DUPIC fuel performance code (KAOS)

  3. Efficiency of Traditional Food Processing Technology in the Locality ...

    African Journals Online (AJOL)

    This paper identified the efficiency of traditional food processing technology which is the set of methods and techniques used for transforming raw food ingredients into food or other forms for consumption by human or animals either in the home or by the food processing industry. Food processing has also helped to create ...

  4. A Process for Technology Prioritization in a Competitive Environment

    Science.gov (United States)

    Stephens, Karen; Herman, Melody; Griffin, Brand

    2006-01-01

    This slide presentation reviews NASA's process for prioritizing technology requirements where there is a competitive environment. The In-Space Propulsion Technology (ISPT) project is used to exemplify the process. The ISPT project focuses on the mid level Technology Readiness Level (TRL) for development. These are TRL's 4 through 6, (i.e. Technology Development and Technology Demonstration. The objective of the planning activity is to identify the current most likely date each technology is needed and create ISPT technology development schedules based on these dates. There is a minimum of 4 years between flight and pacing mission. The ISPT Project needed to identify the "pacing mission" for each technology in order to provide funding for each area. Graphic representations show the development of the process. A matrix shows which missions are currently receiving pull from the both the Solar System Exploration and the Sun-Solar System Connection Roadmaps. The timeframes of the pacing missions technologies are shown for various types of propulsion. A pacing mission that was in the near future serves to increase the priority for funding. Adaptations were made when budget reductions precluded the total implementation of the plan.

  5. Information Technologies and Globalization: New Perspectives of Teaching Learning Process

    Science.gov (United States)

    Hussain, Irshad

    2008-01-01

    This article discusses how information technologies and globalization have opened new avenues and horizons for educators and learners. It discusses different experiences of using information and communication technologies (ICTs) in teaching learning process the world over in the age of globalization. It focuses on the ways these new trends have…

  6. Research on Implementing Big Data: Technology, People, & Processes

    Science.gov (United States)

    Rankin, Jenny Grant; Johnson, Margie; Dennis, Randall

    2015-01-01

    When many people hear the term "big data", they primarily think of a technology tool for the collection and reporting of data of high variety, volume, and velocity. However, the complexity of big data is not only the technology, but the supporting processes, policies, and people supporting it. This paper was written by three experts to…

  7. SpaceCube Technology Brief Hybrid Data Processing System

    Science.gov (United States)

    Petrick, Dave

    2016-01-01

    The intent of this presentation is to give status to multiple audience types on the SpaceCube data processing technology at GSFC. SpaceCube has grown to support multiple missions inside and outside of NASA, and we are being requested to give technology overviews in various forums.

  8. Neural network model for the on-line monitoring of a crystallization process

    Directory of Open Access Journals (Sweden)

    Guardani R.

    2001-01-01

    Full Text Available This paper presents the results of the application of a recently developed technique, based on Neural Networks (NN, in the recognition of angular distribution patterns of light scattered by particles in suspension, for the purpose of estimating concentration and crystal size distribution (CSD in a precipitation process based on the addition of antisolvent (a model system consisting of sodium chloride, water and ethanol. In the first step, in NN model was fitted, using particles with different size distributions and concentrations. Then the model was used to monitor the process, thus enabling a fast and reliable estimation of supersaturation and CSD. Such information, which is difficult to obtain by any other means, can be used in the study of fundamental aspects of crystallization and precipitation processes.

  9. Economic analysis of crystal growth in space

    Science.gov (United States)

    Ulrich, D. R.; Chung, A. M.; Yan, C. S.; Mccreight, L. R.

    1972-01-01

    Many advanced electronic technologies and devices for the 1980's are based on sophisticated compound single crystals, i.e. ceramic oxides and compound semiconductors. Space processing of these electronic crystals with maximum perfection, purity, and size is suggested. No ecomonic or technical justification was found for the growth of silicon single crystals for solid state electronic devices in space.

  10. Business modeling process for university’s technology transfer offices

    Directory of Open Access Journals (Sweden)

    Marin Alexandru

    2017-07-01

    Full Text Available The present paper is devoted to analyze the appropriate recommendations to increase the effectiveness of technology transfer centers from Romanian National Network for Innovation and Technology Transfer - ReNITT, hosted by universities. The study is focused on the definition of a conceptual frame to develop specific business models, by the specialized compartments from technology/knowledge transfer entities, and using the specific instruments of business modeling process. The qualitative and quantitative analysis of the 8 steps scheduling of pairing the building blocks of the Business Models Canvas, corresponding to the specific technology transfer models, and taking into account the elements of the value chain of technology transfer and making connections with technology readiness level, allows a clarification of this relative “fuzzy” and complicated modeling process of university’s Technology Transfer Offices activities, gathering in a concentrated format all necessary information. According to their mission, objectives and strategies, universities decide upon a certain business model for the Technology Transfer Offices, adaptable to client segment and value proposition to attain, by the offered services portfolio. In conclusion, during their activities, Technology Transfer Offices identify, validate and exploit the opportunities originated from applicative research results, by “technology push” methods. Also, there are necessary specific competences (human and material to develop externally aware business models starting from real needs of the clients, by “market pull” techniques, that would contribute to enhance the endogenous innovation potential of firms.

  11. Information Technology in Small Medium Enterprise: Logistic and Production Processes

    Directory of Open Access Journals (Sweden)

    Maurizio Pighin

    2017-01-01

    Full Text Available This paper presents and discuss a survey which describes how small-medium enterprises (SMEs implement and use their information system with respect to their logistic and production processes. The study first describes the rationale of the research, then it identifies the characteristics of the companies and detects their general attitude towards information technology (IT. In the following section the paper presents a set of detailed processes to verify the structure and workflow of companies and how IT supports their processes. In the last part we study the influence of some company characteristics to effective use of processes and to different technological approaches, to support defined logistic and production processes. The novelty of the study and its interest, both in academic and institutional context as in the real world, resides in the opportunity to verify and understand the different attitudes of SMEs towards information technology in defining, organizing, planning and control their processes.

  12. Innovation in Construction: Learning Processes in implementing new Technologies

    DEFF Research Database (Denmark)

    Clausen, Lennie

    1999-01-01

    The article is concerned with the question: How do construction firms implement new technology on construction projects? A model of the implementation process is presented based on a review of the construction innovation literature, innovation theory, and organisational learning theories....

  13. Magsonic™ Carbothermal Technology Compared with the Electrolytic and Pidgeon Processes

    Science.gov (United States)

    Prentice, Leon H.; Haque, Nawshad

    A broad technology comparison of carbothermal magnesium production with present technologies has not been previously presented. In this paper a comparative analysis of CSIRO's MagSonic™ process is made with the electrolytic and Pidgeon processes. The comparison covers energy intensity (GJ/tonne Mg), labor intensity (person-hours/tonne Mg), capital intensity (USD/tonne annual Mg installed capacity), and Global Warming Potential (GWP, tonnes CO2-equivalent/tonne Mg). Carbothermal technology is advantageous on all measures except capital intensity (where it is roughly twice the capital cost of a similarly-sized Pidgeon plant). Carbothermal and electrolytic production can have comparatively low environmental impacts, with typical emissions one-sixth those of the Pidgeon process. Despite recent progress, the Pidgeon process depends upon abundant energy and labor combined with few environmental constraints. Pressure is expected to increase on environmental constraints and labor and energy costs over the coming decade. Carbothermal reduction technology appears to be competitive for future production.

  14. TECHNOLOGICAL PROCESSES OF PRODUCTION OF THE MASS FUNCTION CAST BARS

    Directory of Open Access Journals (Sweden)

    A. N. Krutilin

    2012-01-01

    Full Text Available A number of scientifically grounded technical decisions, the whole set of which has enabled to create technological processes of production of high-quality cast bars of mass appointment is offered.

  15. Thermal food processing: new technologies and quality issues

    National Research Council Canada - National Science Library

    Sun, Da-Wen

    2012-01-01

    .... The editor of Thermal Food Processing: New Technologies and Quality Issues presents a comprehensive reference through authors that assist in meeting this challenge by explaining the latest developments and analyzing the latest trends...

  16. Properties of the Sodium Naproxen-Lactose-Tetrahydrate Co-Crystal upon Processing and Storage

    Directory of Open Access Journals (Sweden)

    Ioana Sovago

    2016-04-01

    Full Text Available Co-crystals and co-amorphous systems are two strategies to improve the physical properties of an active pharmaceutical ingredient and, thus, have recently gained considerable interest both in academia and the pharmaceutical industry. In this study, the behavior of the recently identified sodium naproxen-lactose-tetrahydrate co-crystal and the co-amorphous mixture of sodium, naproxen, and lactose was investigated. The structure of the co-crystal is described using single-crystal X-ray diffraction. The structural analysis revealed a monoclinic lattice, space group P21, with the asymmetric unit containing one molecule of lactose, one of naproxen, sodium, and four water molecules. Upon heating, it was observed that the co-crystal transforms into a co-amorphous system due to the loss of its crystalline bound water. Dehydration and co-amorphization were studied using synchrotron X-ray radiation and thermogravimetric analysis (TGA. Subsequently, different processing techniques (ball milling, spray drying, and dehydration were used to prepare the co-amorphous mixture of sodium, naproxen, and lactose. X-ray powder diffraction (XRPD revealed the amorphous nature of the mixtures after preparation. Differential scanning calorimetry (DSC analysis showed that the blends were single-phase co-amorphous systems as indicated by a single glass transition temperature. The samples were subsequently tested for physical stability under dry (silica gel at 25 and 40 °C and humid conditions (25 °C/75% RH. The co-amorphous samples stored at 25 °C/75% RH quickly recrystallized into the co-crystalline state. On the other hand, the samples stored under dry conditions remained physically stable after five months of storage, except the ball milled sample stored at 40 °C which showed signs of recrystallization. Under these dry conditions, however, the ball-milled co-amorphous blend crystallized into the individual crystalline components.

  17. Highly oriented Bi-system bulk sample prepared by a decomposition-crystallization process

    International Nuclear Information System (INIS)

    Xi Zhengping; Zhou Lian; Ji Chunlin

    1992-01-01

    A decomposition-crystallization method, preparing highly oriented Bi-system bulk sample is reported. The effects of processing parameter, decomposition temperature, cooling rate and post-treatment condition on texture and superconductivity are investigated. The method has successfully prepared highly textured Bi-system bulk samples. High temperature annealing does not destroy the growing texture, but the cooling rate has some effect on texture and superconductivity. Annealing in N 2 /O 2 atmosphere can improve superconductivity of the textured sample. The study on the superconductivity of the Bi(Pb)-Sr-Ca-Cu-O bulk material has been reported in numerous papers. The research on J c concentrates on the tape containing the 2223 phase, with very few studies on the J c of bulk sample. The reason for the lack of studies is that the change of superconducting phases at high temperatures has not been known. The authors have reported that the 2212 phase incongruently melted at about 875 degrees C and proceeded to orient the c-axis perpendicular to the surface in the process of crystallization of the 2212 phase. Based on that result, a decomposition-crystallization method was proposed to prepare highly oriented Bi-system bulk sample. In this paper, the process is described in detail and the effects of processing parameters on texture and superconductivity are reported

  18. Radiation processing technology in the 21st century

    International Nuclear Information System (INIS)

    Miyuki Hagiwara

    1997-01-01

    The address discusses the following issue - towards the 21st century, we are required more and more to create innovative technologies to solve problems about environment, energy, natural resources, materials, health care, food and others which are the great concern to human beings. For the radiation processing technology to survive, it will be required to provide answers to those problems. The use of radiation of polymer modification will remain as an important field of the radiation application. Some other promising polymer processing can be cited as those which will grow in near future; for environment technology - polymeric fibers grafted with ion exchange residues to remove toxic metals for cleaning industrial waste water; For health care technology - crosslinked polyvinylalcohol hydrogel for wound dressing (irradiation of hydrogel); For high performance materials technology - less toxic crosslinked natural rubber latex (irradiation of emulsion), abrasion resistant crosslinked PTFE (irradiation at high temperature)

  19. Effect of power history on the shape and the thermal stress of a large sapphire crystal during the Kyropoulos process

    Science.gov (United States)

    Nguyen, Tran Phu; Chuang, Hsiao-Tsun; Chen, Jyh-Chen; Hu, Chieh

    2018-02-01

    In this study, the effect of the power history on the shape of a sapphire crystal and the thermal stress during the Kyropoulos process are numerically investigated. The simulation results show that the thermal stress is strongly dependent on the power history. The thermal stress distributions in the crystal for all growth stages produced with different power histories are also studied. The results show that high von Mises stress regions are found close to the seed of the crystal, the highly curved crystal surface and the crystal-melt interface. The maximum thermal stress, which occurs at the crystal-melt interface, increases significantly in value as the crystal expands at the crown. After this, there is reduction in the maximum thermal stress as the crystal lengthens. There is a remarkable enhancement in the maximum von Mises stress when the crystal-melt interface is close to the bottom of the crucible. There are two obvious peaks in the maximum Von Mises stress, at the end of the crown stage and in the final stage, when cracking defects can form. To alleviate this problem, different power histories are considered in order to optimize the process to produce the lowest thermal stress in the crystal. The optimal power history is found to produce a significant reduction in the thermal stress in the crown stage.

  20. Investigation of the crystallization process of titanium alloy ingots produced by vacuum arc melting method

    International Nuclear Information System (INIS)

    Tetyukhin, V.V.; Kurapov, V.N.; Trubin, A.N.; Demchenko, M.V.; Lazarev, V.G.; Ponedilko, S.V.; Dubrovina, N.T.; Kurapova, L.A.

    1978-01-01

    The process of crystallization and hardening of the VT3-1 and VT9 titanium alloys ingots during the vacuum-arc remelting (VAR) has been studied. In order to investigate the kinetics of the hole shape changing and the peculiarities of the ingot formation during the VAR, the radiography method has been used. It is established that the VAR of the titanium alloy ingots is basically a continuous process. An intense heating of the liquid bath mirror and the availability of high temperature gradients in the hole are the typical features of the VAR process

  1. Reactor and process design in sustainable energy technology

    CERN Document Server

    Shi, Fan

    2014-01-01

    Reactor Process Design in Sustainable Energy Technology compiles and explains current developments in reactor and process design in sustainable energy technologies, including optimization and scale-up methodologies and numerical methods. Sustainable energy technologies that require more efficient means of converting and utilizing energy can help provide for burgeoning global energy demand while reducing anthropogenic carbon dioxide emissions associated with energy production. The book, contributed by an international team of academic and industry experts in the field, brings numerous reactor design cases to readers based on their valuable experience from lab R&D scale to industry levels. It is the first to emphasize reactor engineering in sustainable energy technology discussing design. It provides comprehensive tools and information to help engineers and energy professionals learn, design, and specify chemical reactors and processes confidently. Emphasis on reactor engineering in sustainable energy techn...

  2. Advanced Process Technology: Combi Materials Science and Atmospheric Processing (Fact Sheet)

    Energy Technology Data Exchange (ETDEWEB)

    2011-06-01

    Capabilities fact sheet for the National Center for Photovoltaics: Process Technology and Advanced Concepts -- High-Throughput Combi Material Science and Atmospheric Processing that includes scope, core competencies and capabilities, and contact/web information.

  3. Crystallization Process of Protein Rv0731c from Mycobacterium Tuberculosis for a Successful Atomic Resolution Crystal Structure at 1.2 Angstrom

    Energy Technology Data Exchange (ETDEWEB)

    Zhu, Liang Cong

    2009-06-08

    Proteins are bio-macromolecules consisting of basic 20 amino acids and have distinct three-dimensional folds. They are essential parts of organisms and participate in every process within cells. Proteins are crucial for human life, and each protein within the body has a specific function, such as antibodies, contractile proteins, enzymes, hormonal proteins, structural proteins, storage proteins and transport proteins. Determining three-dimensional structure of a protein can help researchers discover the remarkable protein folding, binding site, conformation and etc, in order to understand well of protein interaction and aid for possible drug design. The research on protein structure by X-ray protein crystallography carried by Li-Wei Hung's research group in the Physical Bioscience Division at Lawrence Berkeley National Laboratory (LBNL) is focusing on protein crystallography. The research in this lab is in the process of from crystallizing the proteins to determining the three dimensional crystal structures of proteins. Most protein targets are selected from Mycobacterium Tuberculosis. TB (Tuberculosis) is a possible fatal infectious disease. By studying TB target protein can help discover antituberculer drugs, and find treatment for TB. The high-throughput mode of crystallization, crystal harvesting, crystal screening and data collection are applied to the research pipeline (Figure 1). The X-ray diffraction data by protein crystals can be processed and analyzed to result in a three dimensional representation of electron density, producing a detailed model of protein structure. Rv0731c is a conserved hypothetical protein with unknown function from Mycobacterium Tuberculosis. This paper is going to report the crystallization process and brief structure information of Rv0731c.

  4. Characteristics of indomethacin-saccharin (IMC-SAC) co-crystals prepared by an anti-solvent crystallization process.

    Science.gov (United States)

    Chun, Nan-Hee; Wang, In-Chun; Lee, Min-Jeong; Jung, Yun-Taek; Lee, Sangkil; Kim, Woo-Sik; Choi, Guang J

    2013-11-01

    The creation of co-crystals of various insoluble drug substances has been extensively investigated as a promising approach to improve their pharmaceutical performance. In this study, co-crystal powders of indomethacin and saccharin (IMC-SAC) were prepared by an anti-solvent (water) addition and compared with co-crystals by evaporation method. No successful synthesis of a pharmaceutical co-crystal powder via an anti-solvent approach has been reported. Among solvents examined, methanol was practically the only one that resulted in the formation of highly pure IMC-SAC co-crystal powders by anti-solvent approach. The mechanism of a preferential formation of IMC-SAC co-crystal to IMC was explained with two aspects: phase solubility diagram and solution complexation concept. Accordingly, the anti-solvent approach can be considered as a competitive route for producing pharmaceutical co-crystal powders with acceptable properties. Copyright © 2013 Elsevier B.V. All rights reserved.

  5. Probing polymer crystallization at processing-relevant cooling rates with synchrotron radiation

    Energy Technology Data Exchange (ETDEWEB)

    Cavallo, Dario, E-mail: Dario.cavallo@unige.it [University of Genoa, Dept. of Chemistry and Industrial Chemistry, Via Dodecaneso 31, 16146 Genoa (Italy); Portale, Giuseppe [ESRF, Dubble CRG, Netherlands Organization of Scientific Research (NWO), 38043 Grenoble (France); Androsch, René [Martin-Luther-University Halle-Wittenberg, Center of Engineering Sciences, D-06099 Halle/S. (Germany)

    2015-12-17

    Processing of polymeric materials to produce any kind of goods, from films to complex objects, involves application of flow fields on the polymer melt, accompanied or followed by its rapid cooling. Typically, polymers solidify at cooling rates which span over a wide range, from a few to hundreds of °C/s. A novel method to probe polymer crystallization at processing-relevant cooling rates is proposed. Using a custom-built quenching device, thin polymer films are ballistically cooled from the melt at rates between approximately 10 and 200 °C/s. Thanks to highly brilliant synchrotron radiation and to state-of-the-art X-ray detectors, the crystallization process is followed in real-time, recording about 20 wide angle X-ray diffraction patterns per second while monitoring the instantaneous sample temperature. The method is applied to a series of industrially relevant polymers, such as isotactic polypropylene, its copolymers and virgin and nucleated polyamide-6. Their crystallization behaviour during rapid cooling is discussed, with particular attention to the occurrence of polymorphism, which deeply impact material’s properties.

  6. Quality improvement of CdZnTe single crystal by ultrasound processing

    Science.gov (United States)

    Lisiansky, M.; Berner, A.; Korchnoy, V.

    2017-06-01

    Intrinsic defects and contaminations removal from the undoped p-type Cd0.96Zn0.04Te single crystals has been achieved by the ultrasound vibration processing at the room temperature. Surface analysis based on Auger Electron Spectroscopy, Energy Dispersive Spectroscopy, and Scanning Electron Spectroscopy shows a significant reconstruction of the crystal surface after processing, namely, the appearance of numerous "volcano craters" and triangle-shaped defects with a typical size of 0.2-5.0 μm. Elemental analysis of these defects shows that they are Te inclusions emerged on the surface. The regular crystal surface outside the defects also displays a considerable enrichment by Te. Distinct presence of copper is found in both the thin surface layer and in the defects emerged on the surface. The surface reconstruction is associated with a remarkable change in the bulk material properties, electrical (an increase in the resistivity by a factor of ∼6) and optical (an IR transmittance increase). A post-polishing following the ultrasound processing makes the CdZnTe material more stable and reliable for a wide range of device applications.

  7. Effect of hydrothermal process for inorganic alumina sol on crystal structure of alumina gel

    Directory of Open Access Journals (Sweden)

    K. Yamamura

    2016-09-01

    Full Text Available This paper reports the effect of a hydrothermal process for alumina sol on the crystal structure of alumina gel derived from hydrothermally treated alumina sol to help push forward the development of low temperature synthesis of α-Al2O3. White precipitate of aluminum hydroxide was prepared with a homogeneous precipitation method using aluminum nitrate and urea in aqueous solution. The obtained aluminum hydroxide precipitate was peptized by using acetic acid at room temperature, which resulted in the production of a transparent alumina sol. The alumina sol was treated with a hydrothermal process and transformed into an alumina gel film by drying at room temperature. Crystallization of the alumina gel to α-Al2O3 with 900 °C annealing was dominant for a hydrothermal temperature of 100 °C and a hydrothermal time of 60 min, as production of diaspore-like species was promoted with the hydrothermal temperature and time. Excess treatments with hydrothermal processes at higher hydrothermal temperature for longer hydrothermal time prevented the alumina gel from being crystallized to α-Al2O3 because the excess hydrothermal treatments promoted production of boehmite.

  8. Stakeholder and Process Alignment in Navy Installation Technology Transitions

    Science.gov (United States)

    2017-02-01

    report : We have numerous technical success stories that are not fully integrated because of certain circumstances or conditions— some of which are totally...simultaneously integrate tech- nologies with existing systems, secure stakeholder support and integrate with shore planning and funding, program and...process requirements, the ARLs measure progress across three domains: technology integration , stakeholders and processes. Hurdles in any one of

  9. Distributed automatic control of technological processes in conditions of weightlessness

    Science.gov (United States)

    Kukhtenko, A. I.; Merkulov, V. I.; Samoylenko, Y. I.; Ladikov-Royev, Y. P.

    1986-01-01

    Some problems associated with the automatic control of liquid metal and plasma systems under conditions of weightlessness are examined, with particular reference to the problem of stability of liquid equilibrium configurations. The theoretical fundamentals of automatic control of processes in electrically conducting continuous media are outlined, and means of using electromagnetic fields for simulating technological processes in a space environment are discussed.

  10. STUDENTS READINESS TO USE INFORMATION TECHNOLOGY IN UNIVERSITIES EDUCATIONAL PROCESS

    Directory of Open Access Journals (Sweden)

    V. Denysenko

    2015-03-01

    Full Text Available The article analyzes the problem of readiness of students of different specialties to use information technology in the educational process of higher education. Particular attention is paid to contemporary processes of globalization and informatization of higher education as a priority trends of modern Ukrainian society. Experimental data provided in the publication are comparative characteristics of the students using different specialty areas and preparation of information technologies in education. Computerization of the educational process - one of the main priorities in the development of higher education, a new stage for the entire higher education system, promising improvements in the direction of learning in higher education

  11. Application of information and communication technology in process reengineering

    Directory of Open Access Journals (Sweden)

    Đurović Aleksandar M.

    2014-01-01

    Full Text Available This paper examines the role of information communication technologies in reengineering processes. General analysis of a process will show that information communication technologies improve their efficiency. Reengineering model based on the BPMN 2.0 standard will be applied to the process of seeking internship/job by students from Faculty of Transport and Traffic Engineering. In the paper, after defining the technical characteristics and required functionalities, web / mobile application is proposed, enabling better visibility of traffic engineers to companies seeking that education profile.

  12. [Technology development as social process: prospects and frontiers of social scientific elucidation of technological advancement].

    Science.gov (United States)

    Dierkes, M

    1990-05-01

    This article provides an overview of the new developments in social scientific technology research which have changed considerably as a result of public debate and reactions to the importance of advancements in technology. The shift in emphasis, away from the effects of technology to its shaping, is described and certain hypotheses and concepts of advancement in the study of the social conditions underlying technical development processes are presented.

  13. Mobile Technology and CAD Technology Integration in Teaching Architectural Design Process for Producing Creative Product

    Science.gov (United States)

    Bin Hassan, Isham Shah; Ismail, Mohd Arif; Mustafa, Ramlee

    2011-01-01

    The purpose of this research is to examine the effect of integrating the mobile and CAD technology on teaching architectural design process for Malaysian polytechnic architectural students in producing a creative product. The website is set up based on Caroll's minimal theory, while mobile and CAD technology integration is based on Brown and…

  14. Technology Summary Advancing Tank Waste Retreival And Processing

    International Nuclear Information System (INIS)

    Sams, T.L.

    2010-01-01

    This technology overview provides a high-level summary of technologies being investigated and developed by Washington River Protection Solutions (WRPS) to advance Hanford Site tank waste retrieval and processing. Technology solutions are outlined, along with processes and priorities for selecting and developing them. Hanford's underground waste storage tanks hold approximately 57 million gallons of radiochemical waste from nuclear defense production - more tank waste than any other site in the United States. In addition, the waste is uniquely complicated since it contains constituents from at least six major radiochemical processes and several lesser processes. It is intermixed and complexed more than any other waste collection known to exist in the world. The multi-faceted nature of Hanford's tank waste means that legally binding agreements in the Federal Facility Agreement and Consent Order (known as the Tri-Party Agreement) and between the Department of Energy (DOE) and its contractors may not be met using current vitrification schedules, plans and methods. WRPS and the DOE are therefore developing, testing, and deploying technologies to ensure that they can meet the necessary commitments and complete the DOE's River Protection Project (RPP) mission within environmentally acceptable requirements. Technology solutions are outlined, along with processes and priorities for selecting and developing them.

  15. The Impact Of Optical Storage Technology On Image Processing Systems

    Science.gov (United States)

    Garges, Daniel T.; Durbin, Gerald T.

    1984-09-01

    The recent announcement of commercially available high density optical storage devices will have a profound impact on the information processing industry. Just as the initial introduction of random access storage created entirely new processing strategies, optical technology will allow dramatic changes in the storage, retrieval, and dissemination of engineering drawings and other pictorial or text-based documents. Storage Technology Corporation has assumed a leading role in this arena with the introduction of the 7600 Optical Storage Subsystem, and the formation of StorageTek Integrated Systems, a subsidiary chartered to incorporate this new technology into deliverable total systems. This paper explores the impact of optical storage technology from the perspective of a leading-edge manufacturer and integrator.

  16. Hybrid microcircuit technology handbook materials, processes, design, testing and production

    CERN Document Server

    Licari, James J

    1998-01-01

    The Hybrid Microcircuit Technology Handbook integrates the many diverse technologies used in the design, fabrication, assembly, and testing of hybrid segments crucial to the success of producing reliable circuits in high yields. Among these are: resistor trimming, wire bonding, die attachment, cleaning, hermetic sealing, and moisture analysis. In addition to thin films, thick films, and assembly processes, important chapters on substrate selections, handling (including electrostatic discharge), failure analysis, and documentation are included. A comprehensive chapter of design guidelines will

  17. PROCESS CONTROL IN THE EDUCATION OF ORGANIC CHEMICAL TECHNOLOGY

    OpenAIRE

    Csontos, lstván; Department of Organic Chemical Technology, Budapest University of Technology and Economics; Marosi, György; Department of Organic Chemical Technology, Budapest University of Technology and Economics; Faigl, Ferenc; Department of Organic Chemical Technology, Budapest University of Technology and Economics

    2013-01-01

    Laboratory practices for demonstrating the importance of advanced process control methods in the organic chemical technologies have been elaborated. It required the development of a system tha tintegrates the advantages of a reaction calorimeter and a model system of industrial controlled reactors. The hardware and software configuration support the transfer of elaborated control programs of reactions from laboratory level to the industrial technology. General control algorithms of diazotizat...

  18. Advanced fuel cycle on the basis of pyroelectrochemical process for irradiated fuel reprocessing and vibropacking technology

    International Nuclear Information System (INIS)

    Mayorshin, A.A.; Skiba, O.V.; Tsykanov, V.A.; Golovanov, V.N.; Bychkov, A.V.; Kisly, V.A.; Bobrov, D.A.

    2000-01-01

    For advanced nuclear fuel cycle in SSC RIAR there is developed the pyroelectrochemical process to reprocess irradiated fuel and produce granulated oxide fuel UO 2 , PuO 2 or (U,Pu)O 2 from chloride melts. The basic technological stage is the extraction of oxides as a crystal product with the methods either of the electrolysis (UO 2 and UO 2 -PuO 2 ) or of the precipitating crystalIization (PuO 2 ). After treating the granulated fuel is ready for direct use to manufacture vibropacking fuel pins. Electrochemical model for (U,Pu)O 2 coprecipitation is described. There are new processes being developed: electroprecipitation of mixed oxides - (U,Np)O 2 , (U,Pu,Np)O 2 , (U,Am)O 2 and (U,Pu,Am)O 2 . Pyroelectrochemical production of mixed actinide oxides is used both for reprocessing spent fuel and for producing actinide fuel. Both the efficiency of pyroelectrochemical methods application for reprocessing nuclear fuel and of vibropac technology for plutonium recovery are estimated. (author)

  19. Cogeneration technology alternatives study. Volume 2: Industrial process characteristics

    Science.gov (United States)

    1980-01-01

    Information and data for 26 industrial processes are presented. The following information is given for each process: (1) a description of the process including the annual energy consumption and product production and plant capacity; (2) the energy requirements of the process for each unit of production and the detailed data concerning electrical energy requirements and also hot water, steam, and direct fired thermal requirements; (3) anticipated trends affecting energy requirements with new process or production technologies; and (4) representative plant data including capacity and projected requirements through the year 2000.

  20. Polypropylene containing Ti- and Al-polyhedral oligomeric silsesquioxanes: crystallization process and thermal properties

    Science.gov (United States)

    Carniato, Fabio; Fina, Alberto; Tabuani, Daniela; Boccaleri, Enrico

    2008-11-01

    This paper deals with the preparation and characterization of isotactic polypropylene (PP) containing different metal-polyhedral oligomeric silsesquioxanes (M-POSS). Two M-POSS, Ti(IV)- and Al(III)-isobutyl-POSS, defined by a monomeric structure, were selected for dispersion, and particular attention was paid to the assessment of the morphology, crystallization process and thermal behavior of M-POSS/PP composites, using SEM and TEM microscopy, x-ray diffraction (XRD), FTIR and Raman spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and gas chromatography/mass spectrometry. The study of M-POSS/PP thermal degradation showed that Ti-POSS and Al-POSS induce different effects on the thermoxidative behavior of the polypropylene matrix, showing a clear specificity of the metal center on the PP degradation pathway. In particular, Ti-POSS showed a significant stabilization of PP when heating under air, whereas limited effects were observed with Al-POSS. Moreover, Ti-POSS was also found to affect PP crystallization, driving the crystallization process along specific crystallographic directions.

  1. Polypropylene containing Ti- and Al-polyhedral oligomeric silsesquioxanes: crystallization process and thermal properties.

    Science.gov (United States)

    Carniato, Fabio; Fina, Alberto; Tabuani, Daniela; Boccaleri, Enrico

    2008-11-26

    This paper deals with the preparation and characterization of isotactic polypropylene (PP) containing different metal-polyhedral oligomeric silsesquioxanes (M-POSS). Two M-POSS, Ti(IV)- and Al(III)-isobutyl-POSS, defined by a monomeric structure, were selected for dispersion, and particular attention was paid to the assessment of the morphology, crystallization process and thermal behavior of M-POSS/PP composites, using SEM and TEM microscopy, x-ray diffraction (XRD), FTIR and Raman spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and gas chromatography/mass spectrometry. The study of M-POSS/PP thermal degradation showed that Ti-POSS and Al-POSS induce different effects on the thermoxidative behavior of the polypropylene matrix, showing a clear specificity of the metal center on the PP degradation pathway. In particular, Ti-POSS showed a significant stabilization of PP when heating under air, whereas limited effects were observed with Al-POSS. Moreover, Ti-POSS was also found to affect PP crystallization, driving the crystallization process along specific crystallographic directions.

  2. Data processing for elliptical crystal spectrometer used in Z-pinch diagnostic

    International Nuclear Information System (INIS)

    Li Jing; Xie Weiping; Huang Xianbin; Yang Libing; Cai Hongchun; Xiao Shali

    2010-01-01

    Elliptical crystal spectrometers are key instruments to detect the line spectra of soft X-rays in Z-pinch diagnostics. This paper deals with the data processing for an elliptical crystal spectrometer. Taking the diagnostic results obtained in a neon gas-puff Z-pinch experiment as an example, the detailed processes, such as changing the optical density to X-ray intensity according a calibrated film response curve, determining the X-ray energy of the measured spectrum using the energy and the order number of scanned point of identified spectral lines, and correcting the intensity of spectrum using the formula given by Henke are discussed. In the Henke's formula, the effect of nonuniform dispersion, integrated reflectivity of crystals and transmission of X-ray filters are considered. The final unfolding results are presented, including the relative intensities of several neon K-shell lines (H α , He α and He β , etc.) given by Lorentz fitting. The relative errors of the spectral intensities are also briefly discussed. (authors)

  3. Multi-scale simulation of single crystal hollow turbine blade manufactured by liquid metal cooling process

    Directory of Open Access Journals (Sweden)

    Xuewei Yan

    2018-02-01

    Full Text Available Liquid metal cooling (LMC process as a powerful directional solidification (DS technique is prospectively used to manufacture single crystal (SC turbine blades. An understanding of the temperature distribution and microstructure evolution in LMC process is required in order to improve the properties of the blades. For this reason, a multi-scale model coupling with the temperature field, grain growth and solute diffusion was established. The temperature distribution and mushy zone evolution of the hollow blade was simulated and discussed. According to the simulation results, the mushy zone might be convex and ahead of the ceramic beads at a lower withdrawal rate, while it will be concave and laggard at a higher withdrawal rate, and a uniform and horizontal mushy zone will be formed at a medium withdrawal rate. Grain growth of the blade at different withdrawal rates was also investigated. Single crystal structures were all selected out at three different withdrawal rates. Moreover, mis-orientation of the grains at 8 mm/min reached ~30°, while it was ~5° and ~15° at 10 mm/min and 12 mm/min, respectively. The model for predicting dendritic morphology was verified by corresponding experiment. Large scale for 2D dendritic distribution in the whole sections was investigated by experiment and simulation, and they presented a well agreement with each other. Keywords: Hollow blade, Single crystal, Multi-scale simulation, Liquid metal cooling

  4. Applying Trusted Network Technology To Process Control Systems

    Science.gov (United States)

    Okhravi, Hamed; Nicol, David

    Interconnections between process control networks and enterprise networks expose instrumentation and control systems and the critical infrastructure components they operate to a variety of cyber attacks. Several architectural standards and security best practices have been proposed for industrial control systems. However, they are based on older architectures and do not leverage the latest hardware and software technologies. This paper describes new technologies that can be applied to the design of next generation security architectures for industrial control systems. The technologies are discussed along with their security benefits and design trade-offs.

  5. Image processing technologies in nuclear power plant monitoring

    International Nuclear Information System (INIS)

    Kubo, Katsumi; Kanemoto, Shigeru; Shimada, Hideo.

    1995-01-01

    Various monitoring activities are carried out in nuclear power plants to ensure that the high reliability requirements of such plants are met. Inspection patrols by operators are important for detecting small anomalies in equipment. Vibration, temperature, and visual images are major forms of information used in equipment inspections. We are developing remote automatic inspection technologies comprising image sensing of equipment conditions and automatic recognition of the images. This paper shows examples of image processing technologies, such as equipment monitoring using three-dimensional graphic plant models and vibration/temperature image data, and intelligent image recognition technology for detecting steam leakage. (author)

  6. Synthesis and crystal kinetics of cerium oxide nanocrystallites prepared by co-precipitation process

    International Nuclear Information System (INIS)

    Shih, C.J.; Chen, Y.J.; Hon, M.H.

    2010-01-01

    Cerium oxide nanocrystallites were synthesized at a relatively low temperature using cerium nitrate as starting materials in a water solution by a co-precipitation process. Effect of calcination temperature on the crystallite growth of cerium oxide nano-powders was investigated by X-ray diffraction, transmission electron microscopy and electron diffraction. The crystallization temperature of the cerium oxide powders was estimated to be about 273 K by XRD analysis. When calcined from 473 to 1273 K, the crystallization of the face-centered cubic phase was observed by XRD. The crystallite size of the cerium oxide increased from 10.0 to 43.8 nm with calcining temperature increasing from 673 to 1273 K. The activation energy for growth of cerium oxide nanoparticles was found to be 16.0 kJ mol -1 .

  7. Synthesis and crystal kinetics of cerium oxide nanocrystallites prepared by co-precipitation process

    Energy Technology Data Exchange (ETDEWEB)

    Shih, C.J., E-mail: cjshih@kmu.edu.tw [Department of Fragrance and Cosmetics Science, Kaohsiung Medical University, 100 Shi-Chuan 1st Road, Kaohsiung 807, Taiwan (China); Chen, Y.J. [Institute of Biomedical Sciences, National Sun Yat-Sen University, Kaohsiung 804, Taiwan (China); Hon, M.H. [Department of Materials Science and Engineering, National Cheng Kung University, Tainan 701, Taiwan (China)

    2010-05-15

    Cerium oxide nanocrystallites were synthesized at a relatively low temperature using cerium nitrate as starting materials in a water solution by a co-precipitation process. Effect of calcination temperature on the crystallite growth of cerium oxide nano-powders was investigated by X-ray diffraction, transmission electron microscopy and electron diffraction. The crystallization temperature of the cerium oxide powders was estimated to be about 273 K by XRD analysis. When calcined from 473 to 1273 K, the crystallization of the face-centered cubic phase was observed by XRD. The crystallite size of the cerium oxide increased from 10.0 to 43.8 nm with calcining temperature increasing from 673 to 1273 K. The activation energy for growth of cerium oxide nanoparticles was found to be 16.0 kJ mol{sup -1}.

  8. Heat and mass transfer in semiconductor melts during single-crystal growth processes

    Science.gov (United States)

    Kakimoto, Koichi

    1995-03-01

    The quality of large semiconductor crystals grown from melts is significantly affected by the heat and mass transfer in the melts. The current understanding of the phenomena, especially melt convection, is reviewed starting from the results of visualization using model fluids or silicon melt, and continuing to the detailed numerical calculations needed for quantitative modeling of processing with solidification. The characteristics of silicon flows are also reviewed by focusing on the Coriolis force in the rotating melt. Descriptions of flow instabilities are included that show the level of understanding of melt convection with a low Prandtl number. Based on hydrodynamics, the origin of the silicon flow structure is reviewed, and it is discussed whether silicon flow is completely turbulent or has an ordered structure. The phase transition from axisymmetric to nonaxisymmetric flow is discussed using different geometries. Additionally, surface-tension-driven flow is reviewed for Czochralski crystal growth systems.

  9. Virtual Reality in Presentation of the Underground Mine Technological Process

    Directory of Open Access Journals (Sweden)

    Kodym Oldøich

    2003-09-01

    Full Text Available Virtual Reality in Presentation of the Underground Mine Technological Process focuses on methods of presentation of an underground mine technologies in intranet technology. It shows usage of platform independent VRML client for presentation of static and dynamic information about technological process. Bi-directional interactions between client and process information database are solved.Based on analysis of technological process of underground mine a database structure was designed. It is skeleton for storing all information about any underground mine. This skeleton can be modified in any direction. Data in this "static model" of underground mine can be applied for visualization in VRML environment. In this way it is possible to simplify and unify a user's front-end for all kinds of tasks.All designed scenes can be interactively displayed in full view or in any detail view, so that a user is able to recognize every important part of installed equipment, its stage, technical parameters and other information. If manufacturers of mining equipment will supply VRML model of their real products everybody would be able to place it into VRML scene and learn everything about it.This work explores and tries to enlighten some of the areas and available approaches compliant with VRML 97 specification of modifying static scene by its browser. Concepts of animation pipeline, inside and outside scripting in scene displayed and authoring of VRML targeted geometry are discussed including database connectivity.

  10. A Micro-Comb Test System for In Situ Investigation of Infiltration and Crystallization Processes

    Directory of Open Access Journals (Sweden)

    Dominik Gruber

    2017-10-01

    Full Text Available The investigation of mineralization and demineralization processes is important for the understanding of many phenomena in daily life. Many crystalline materials are exposed to decay processes, resulting in lesions, cracks, and cavities. Historical artifacts, for example, often composed of calcium carbonate (CaCO3, are damaged by exposure to acid rain or temperature cycles. Another example for lesions in a crystalline material is dental caries, which lead to the loss of dental hard tissue, mainly composed of hydroxyapatite (HAp. The filling of such cavities and lesions, to avoid further mineral loss and enable or support the remineralization, is a major effort in both areas. Nevertheless, the investigation of the filling process of these materials into the cavities is difficult due to the non-transparency and crystallinity of the concerned materials. In order to address this problem, we present a transparent, inexpensive, and reusable test system for the investigation of infiltration and crystallization processes in situ, being able to deliver datasets that could potentially be used for quantitative evaluation of the infiltration process. This was achieved using a UV-lithography-based micro-comb test system (MCTS, combined with self-assembled monolayers (SAMs to mimic the surface tension/wettability of different materials, like marble, sandstone, or human enamel. Moreover, the potential of this test system is illustrated by infiltration of a CaCO3 crystallization solution and a hydroxyapatite precursor (HApP into the MCTS.

  11. Effect of controlled crucible movement on melting process and carbon contamination in Czochralski silicon crystal growth

    Science.gov (United States)

    Liu, Xin; Han, Xue-Feng; Nakano, Satoshi; Kakimoto, Koichi

    2018-02-01

    In Czochralski silicon (CZ-Si) crystal growth, packed Si chunks experience collapse and volume shrinkage during the melting process. The axial movements of the crucible and the melting of the Si feedstock lead to dynamic thermal and flow fields and affect mass transport. To study the effect of crucible movement on the melting process and carbon (C) contamination, the cases of fixed and lifting crucible were investigated by the transient global simulation with dynamic mesh deformation. The gap width between the gas-guide and the top surface of Si feedstock was kept constant during the crucible lifting process. Impurity and species transport in Si feedstock and argon gas was investigated for the cases with the fixed and lifting crucibles. The comparison of C accumulation processes indicated that the lifting crucible case resulted in higher C contamination than that found in the fixed crucible case. Furthermore, lifting crucible cases with different gap widths were investigated to elaborate strategies for controlling the crucible movement for its effect on the melting process and C contamination in CZ-Si crystal growth. It was observed that the optimum gap width for C reduction results from the trade-off between the back diffusion and gas convection.

  12. Natural language processing in psychiatry. Artificial intelligence technology and psychopathology.

    Science.gov (United States)

    Garfield, D A; Rapp, C; Evens, M

    1992-04-01

    The potential benefit of artificial intelligence (AI) technology as a tool of psychiatry has not been well defined. In this essay, the technology of natural language processing and its position with regard to the two main schools of AI is clearly outlined. Past experiments utilizing AI techniques in understanding psychopathology are reviewed. Natural language processing can automate the analysis of transcripts and can be used in modeling theories of language comprehension. In these ways, it can serve as a tool in testing psychological theories of psychopathology and can be used as an effective tool in empirical research on verbal behavior in psychopathology.

  13. Methodology and Results of Mathematical Modelling of Complex Technological Processes

    Science.gov (United States)

    Mokrova, Nataliya V.

    2018-03-01

    The methodology of system analysis allows us to draw a mathematical model of the complex technological process. The mathematical description of the plasma-chemical process was proposed. The importance the quenching rate and initial temperature decrease time was confirmed for producing the maximum amount of the target product. The results of numerical integration of the system of differential equations can be used to describe reagent concentrations, plasma jet rate and temperature in order to achieve optimal mode of hardening. Such models are applicable both for solving control problems and predicting future states of sophisticated technological systems.

  14. Kinetic Study of Crystallization Process in Fe32Ni36Cr14P12B6 Metallic Glass

    International Nuclear Information System (INIS)

    Lad, Kirit; Pratap, Arun; Rao, T. L. Shanker

    2010-01-01

    Kinetics of crystallization process in a Fe-based metallic glass 2826A (Fe 32 Ni 36 Cr 14 P 12 B 6 ) has been studied with the help of differential scanning calorimetry(DSC). It is found that the 2826A metallic glass exhibits two overlapping crystallization peaks. The activation energy for crystallization (E) and the Avrami exponent (n) for the two crystallization peaks have been obtained using the Kolmogorov-Jhonson-Mehl-Avrami (KJMA) equation. The so-obtained values of E and n have been utilized to derive normalized heat flow curves. It has been observed that the theoretical heat flow curves obtained using KJMA equation show large deviations from the experimental curves for the first peak whereas the curves are in very close agreement for the second peak. This suggests that kinetics of crystallization process during the first peak cannot be described correctly in KJMA formalism.

  15. Kinetic Study of Crystallization Process in Fe32Ni36Cr14P12B6 Metallic Glass

    Science.gov (United States)

    Lad, Kirit; Rao, T. L. Shanker; Pratap, Arun

    2010-06-01

    Kinetics of crystallization process in a Fe-based metallic glass 2826A (Fe32Ni36Cr14P12B6) has been studied with the help of differential scanning calorimetry(DSC). It is found that the 2826A metallic glass exhibits two overlapping crystallization peaks. The activation energy for crystallization (E) and the Avrami exponent (n) for the two crystallization peaks have been obtained using the Kolmogorov-Jhonson-Mehl-Avrami (KJMA) equation. The so-obtained values of E and n have been utilized to derive normalized heat flow curves. It has been observed that the theoretical heat flow curves obtained using KJMA equation show large deviations from the experimental curves for the first peak whereas the curves are in very close agreement for the second peak. This suggests that kinetics of crystallization process during the first peak cannot be described correctly in KJMA formalism.

  16. MODEL OF QUALITY MANAGEMENT OF TECHNOLOGICAL PROCESSES OF THE GRAIN PROCESSING AND MILL ENTERPRISES

    Directory of Open Access Journals (Sweden)

    M. M. Blagoveshchenskaia

    2014-01-01

    Full Text Available Summary. In the work the model of quality management of technological processes of the grain processing and mill enterprises is presented. It is shown that flour-grinding production is an important part of agro-industrial complex because it provides production of the main food product of people – flour. The analytical indicators of quality of technological process are presented. The matrix of expert estimates of i-th level of quality for the set combinations of parameters values according to the scheme of complete factorial experiment is made. Considered a model for the calculation of the raw material preparation for milling, which characterizes the main qualities of the processed raw materials. For the purpose of management of quality of technological processes of flour mill the mathematical model which includes calculation of two groups of indicators of an assessment is developed: qualities of preparation of raw materials for a grinding and qualities of conducting technological process. The algorithm of an analytical assessment of indicators of quality of technological process of the flour-grinding enterprises, including the selection of waste, selection of bran, a compliance rate of output of flour-grinding products, compliance rate of moisture products, is offered. The assessment of quality management of technological process of a high-quality grinding on the example of several leading flour-grinding enterprises of Central Federal District is carried out. The two-dimensional model of quality management of technological process based on an analytical indicators of an assessment of quality, an assessment of quality of preparation the raw materials for a grinding and an optimum effective condition of technological process is constructed. It is shown that quality management at the enterprise provides collecting, processing and the analysis of information on a condition of material streams and productions on all of their stages.

  17. New media technologies and mass media reform processes

    Directory of Open Access Journals (Sweden)

    Tomić Boban

    2017-01-01

    Full Text Available This paper reviews and assesses the chances for survival and development of the media in Serbia and ib the region, from the perspective of new information and communication technologies (ICT applied in media business. In the paper theoretical method is used and harmonized with the needs of describing the problems and the observed processes and phenomena, as well as empirical method which is used for collecting and interpreting concrete facts and data on the observed processes and phenomena. The starting point lies in the fact that modern media is definitely, more and more, dependent on new technologies. A part of the new technologies is used in the process of collecting, selecting and editing media content, while the other part of the technology is used in the process of dissemination and propulsion of media content to the mass audience, and also in the feedback function as well. The technology revolution, which we describe, started with mp3, jpg and avi files, and continues with internet broadcasting, social networks, cloud technologies and new digital platforms which are used by today's media for distribution of media content. The particularity of the media in the region lies in the fact that they operating in the societes with delay of political and economic transition, so all the productive resources of society, due to this backlog, are slower adapted to the new conditions of business in the digital era. The consequences that have arisen from such dynamics of development make many media in Serbia and the region quite dysfunctional, especially those who were exposed during this transition to long-standing legal, economic and program crises. That is why most of the existing media in Serbia, especially small ones, are unprepared for modernization and they are not ready for re-modeling in accordance with the new technological circumstances.

  18. A Process Analytical Technology (PAT) approach to control a new API manufacturing process: development, validation and implementation.

    Science.gov (United States)

    Schaefer, Cédric; Clicq, David; Lecomte, Clémence; Merschaert, Alain; Norrant, Edith; Fotiadu, Frédéric

    2014-03-01

    Pharmaceutical companies are progressively adopting and introducing Process Analytical Technology (PAT) and Quality-by-Design (QbD) concepts promoted by the regulatory agencies, aiming the building of the quality directly into the product by combining thorough scientific understanding and quality risk management. An analytical method based on near infrared (NIR) spectroscopy was developed as a PAT tool to control on-line an API (active pharmaceutical ingredient) manufacturing crystallization step during which the API and residual solvent contents need to be precisely determined to reach the predefined seeding point. An original methodology based on the QbD principles was designed to conduct the development and validation of the NIR method and to ensure that it is fitted for its intended use. On this basis, Partial least squares (PLS) models were developed and optimized using chemometrics methods. The method was fully validated according to the ICH Q2(R1) guideline and using the accuracy profile approach. The dosing ranges were evaluated to 9.0-12.0% w/w for the API and 0.18-1.50% w/w for the residual methanol. As by nature the variability of the sampling method and the reference method are included in the variability obtained for the NIR method during the validation phase, a real-time process monitoring exercise was performed to prove its fit for purpose. The implementation of this in-process control (IPC) method on the industrial plant from the launch of the new API synthesis process will enable automatic control of the final crystallization step in order to ensure a predefined quality level of the API. In addition, several valuable benefits are expected including reduction of the process time, suppression of a rather difficult sampling and tedious off-line analyses. © 2013 Published by Elsevier B.V.

  19. Some novel concepts in radiation processing technology applications

    International Nuclear Information System (INIS)

    Varshney, Lalit

    2014-01-01

    Search for better materials and processes has been a part of the evolution of mankind and it still continues to be so as it is being realized that earth's resources are not everlasting and effect of rapid growth on environment may adversely affect the future development. Sustainable development is the only choice for today for long term survival. Better quality and high functional materials, made by superior technologies are being demanded by the society. Radiation processing technology has significantly contributed to meet the expectation of the people in providing superior products and processes while preserving the environment. Processes are being developed where resources are fully utilized with maximum advantages and little disturbance to the environment. More than 1500 electron beam accelerators and about 500 Gamma Irradiators are presently in use and many are being deployed for radiation processing of medical supplies, pharmaceuticals and herbal materials, treat effluents and preserve food and agricultural products and several industrial products. DAE has an ambitious plan to deploy radiation technology for societal benefits in India. In the presentations some interesting applications of Radiation Processing Technology will be discussed which includes (1) Radiation Processing of Cashew Apple fruit for bio-ethanol production (2) High Energy Battery separators (3) Plant Growth Promoters and (4) Tunable biodegradability. The discussion would reveal how a waste product like cashew apple can be converted to useful materials and advanced materials like HEB separators and Tunable Biodegradable films can be made using radiation technology. Use of radiation de-polymerized polysaccharides in some experiments have shown unexpected increase in agriculture output giving new concepts to increase the productivity. (author)

  20. Wireless sensor technology for in-situ plasma process monitoring

    Science.gov (United States)

    Gahan, David

    2015-09-01

    There is an increasing demand for plasma measurement and control solutions to cope with the growing complexity of integrated circuit manufacture in the semiconductor industry. Standard plasma diagnostic instruments used in research, such as the Langmuir probe, are not suitable for use in the production environment for myriad reasons - contamination of the process being one of the main concerns. Silicon wafer based wireless sensors, which measure temperature during the process, have gained the most traction with tool manufacturers and chip makers - albeit during process development or the PM cycle rather than live production. In this presentation we will discuss two novel wireless technologies that have the potential for use in process tools. The first is an ion detector embedded in a silicon wafer. The sensor measures the average ion flux and the maximum ion energy during the process. This information is stored and is downloaded later for analysis. The second technology consists of a wireless sensor that sits inside the process and communicates data in real time to a detector installed on the rf power line. This platform is similar to RFID technology and can be combined with various sensor types to transmit data to the user during the process.

  1. Charge exchange processes of high energy heavy ions channeled in crystals

    International Nuclear Information System (INIS)

    Andriamonje, S.; Dural, J.; Toulemonde, M.; Groeneveld, K.O.; Maier, R.; Quere, Y.

    1990-01-01

    The interaction of moving ions with single crystals is very sensitive to the orientation of the incident beam with respect to the crystalline directions of the target. The experiments show that high energy heavy ion channeling deeply modifies the slowing down and charge exchange processes. In this review, we describe the opportunity offered by channeling conditions to study the charge exchange processes. Some aspects of the charge exchange processes with high energy channeled heavy ions are selected from the extensive literature published over the past few years on this subject. Special attention is given to the work performed at the GANIL facility on the study of Radiative Electron Capture (REG), Electron Impact Ionisation (EII), and convoy electron emission. Finally we emphasize the interest of studying resonant charge exchange processes such as Resonant Coherent Excitation (RCE), Resonant Transfer and Excitation (RTE) or Dielectronic Recombination (DR) and the recently proposed Nuclear Excitation by Electron Capture (NEEC)

  2. Crystal fractionation processes at Baru volcano from the deep to shallow crust

    Science.gov (United States)

    Hidalgo, Paulo J.; Rooney, Tyrone O.

    2010-12-01

    Linking shallow and deep crustal processes at volcanic arcs is an important component in evaluating the growth and evolution of the continental crust. Commonly, deep crustal processes and the nature of subarc lithosphere are studied long after the volcanism has ceased in obducted arc terranes. In active arcs, studies of deep crustal processes focus on cumulates derived from middle-lower crustal levels. Although uncommon in the erupted magmas, these cumulates are required by crustal differentiation models of arc magmatism. Quaternary magmas at Baru volcano in Panama contain ubiquitous amphibole-bearing cumulates that provide an opportunity to probe the magma plumbing system of an active arc volcano. We have determined that these cumulates are related to their host magmas by crystal fractionation processes. Pressure and temperature estimates for amphiboles within these cumulates and the host rock are consistent with sampling of mush/magma zones from throughout the arc crust. These mush zones would be localized in deep hot crustal zones where magmatic differentiation of water-saturated arc magmas takes place by crystallization of amphibole-rich cumulates. The identification of middle-lower crustal cumulates is not exclusive to Baru volcano; similar cumulates are common throughout the Panamanian arc and are consistent with a widespread amphibole-rich layer present within the arc crust of Panama. Our results highlight the importance of amphibole fractionation in the differentiation sequence of island arcs effectively driving the residual magma to the average andesitic composition of the continental crust.

  3. Influence of cutting parameters on the depth of subsurface deformed layer in nano-cutting process of single crystal copper.

    Science.gov (United States)

    Wang, Quanlong; Bai, Qingshun; Chen, Jiaxuan; Su, Hao; Wang, Zhiguo; Xie, Wenkun

    2015-12-01

    Large-scale molecular dynamics simulation is performed to study the nano-cutting process of single crystal copper realized by single-point diamond cutting tool in this paper. The centro-symmetry parameter is adopted to characterize the subsurface deformed layers and the distribution and evolution of the subsurface defect structures. Three-dimensional visualization and measurement technology are used to measure the depth of the subsurface deformed layers. The influence of cutting speed, cutting depth, cutting direction, and crystallographic orientation on the depth of subsurface deformed layers is systematically investigated. The results show that a lot of defect structures are formed in the subsurface of workpiece during nano-cutting process, for instance, stair-rod dislocations, stacking fault tetrahedron, atomic clusters, vacancy defects, point defects. In the process of nano-cutting, the depth of subsurface deformed layers increases with the cutting distance at the beginning, then decreases at stable cutting process, and basically remains unchanged when the cutting distance reaches up to 24 nm. The depth of subsurface deformed layers decreases with the increase in cutting speed between 50 and 300 m/s. The depth of subsurface deformed layer increases with cutting depth, proportionally, and basically remains unchanged when the cutting depth reaches over 6 nm.

  4. Lipid Processing Technology: Building a Multilevel Modeling Network

    DEFF Research Database (Denmark)

    Díaz Tovar, Carlos Axel; Mustaffa, Azizul Azri; Mukkerikar, Amol

    2011-01-01

    of a master parameter table; iii) development of a model library consisting of new and adopted process models of unit operations involved in lipid processing technologies, validation of the developed models using operating data collected from existing process plants, and application of validated models......The aim of this work is to present the development of a computer aided multilevel modeling network for the systematic design and analysis of processes employing lipid technologies. This is achieved by decomposing the problem into four levels of modeling: i) pure component property modeling...... and a lipid-database of collected experimental data from industry and generated data from validated predictive property models, as well as modeling tools for fast adoption-analysis of property prediction models; ii) modeling of phase behavior of relevant lipid mixtures using the UNIFACCI model, development...

  5. Physicochemical properties of dicesium tetravalent plutonium hexanitrate in uranium crystallization process

    Energy Technology Data Exchange (ETDEWEB)

    Nakahara, M; Koizumi, T [Nuclear Fuel Cycle Engineering Laboratories, Japan Atomic Energy Agency, 4-33 Muramatsu, Tokai-mura, Naka-gun, Ibaraki 319-1194 (Japan); Nomura, K, E-mail: nakahara.masaumi@jaea.go.jp [Advanced Nuclear System Reserch and Development Directorate, Japan Atomic Energy Agency, 4-33 Muramatsu, Tokai-mura, Naka-gun, Ibaraki 319-1194 (Japan)

    2010-03-15

    Tetravalent Pu reacts with Cs ions to form the crystalline precipitate of Cs{sub 2}Pu(NO{sub 3}){sub 6}under certain chemical conditions during the U crystallization process. The Cs{sub 2}Pu(NO{sub 3}){sub 6}precipitate reduces the decontamination factor (DF) of Cs to U in the crystal after being washed. The solubility and thermal properties of Cs{sub 2}Pu(NO{sub 3}){sub 6} were studied with the aim of providing a characterization estimate. The solubility of Cs{sub 2}Pu(NO{sub 3}){sub 6} increased with decreases in HNO{sub 3} concentration. Loss in weight of the compound caused by thermal degradation of Cs{sub 2}Pu(NO{sub 3}){sub 6} to Cs{sub 2}PuO{sub 2}(NO{sub 3}){sub 4} was observed at 245 deg. C in thermal analysis. A uranyl nitrate hexahydrate (UNH) crystal was obtained by cooling irradiated fast reactor core fuel dissolver solution. The DF of Cs decreased with increasing the HNO{sub 3} concentration of the mother liquor because more Cs{sub 2}Pu(NO{sub 3}){sub 6} precipitates with high concentration of HNO{sub 3}.

  6. Achievement report for fiscal 1997. Technological development for practical application of a solar energy power generation system /development of technology to manufacture solar cells/development of technology to manufacture thin film solar cells (development of technology to manufacture materials and substrates (development of technology to manufacture silicon crystal based high-quality materials and substrates)); 1997 nendo taiyoko hatsuden system jitsuyoka gijutsu kaihatsu seika hokokusho. Taiyo denchi seizo gijutsu kaihatsu, usumaku taiyo denchi seizo gijutsu kaihatsu, zairyo kiban seizo gijutsu kaihatsu (silicon kesshokei kohinshitsu zairyo kiban no seizo gujutsu kaihatsu)

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1998-03-01

    It is intended to develop thin film solar cells capable of mass production with high photo-stability and at low cost. Thus, the objective of the present research is to analyze the growth process of micro crystal silicon based thin films, the crystal being a high quality silicon crystal based material, and develop technology to manufacture high-quality micro crystal silicon thin films based on the findings therefrom. It was found that, when silicon source is available in cathode, pure hydrogen plasma forms micro crystal silicon films by using the plasma as a result of the chemical transportation effect from the silicon source. It was revealed that the crystal formation due to hydrogen plasma exposure is performed substantially by the crystals forming the films due to the chemical transportation effect, rather than crystallization in the vicinity of the surface. The crystal formation under this experiment was concluded that the formation takes place during film growth accompanied by diffusion of film forming precursors on the surface on which the film grows. According to the result obtained so far, the most important issue in the future is particularly the control of crystal growing azimuth by reducing the initially formed amorphous layer by controlling the stress in the initial phase for film formation, and by controlling the film forming precursors. (NEDO)

  7. Pretreatment Technologies of Lignocellulosic Materials in Bioethanol Production Process

    Directory of Open Access Journals (Sweden)

    Mohamad Rusdi Hidayat

    2013-06-01

    Full Text Available Bioethanol is one type of biofuel that developed significantly. The utilization of bioethanol is not only limited for fuel, but also could be used as material for various industries such as pharmaceuticals, cosmetics, and food. With wide utilization and relatively simple production technology has made bioethanol as the most favored biofuel currently. The use of lignocellulosic biomass, microalgae, seaweeds, even GMO (Genetically modified organisms as substrates for bioethanol production has been widely tested. Differences in the materials eventually led to change in the production technology used. Pretreatment technology in the bioethanol production using lignocellulosic currently experiencing rapid development. It is a key process and crucial for the whole next steps. Based on the advantages and disadvantages from all methods, steam explotion and liquid hot water methods are the most promising  pretreatment technology available.

  8. A Voice Processing Technology for Rural Specific Context

    Science.gov (United States)

    He, Zhiyong; Zhang, Zhengguang; Zhao, Chunshen

    Durian the promotion and applications of rural information, different geographical dialect voice interaction is a very complex issue. Through in-depth analysis of TTS core technologies, this paper presents the methods of intelligent segmentation, word segmentation algorithm and intelligent voice thesaurus construction in the different dialects context. And then COM based development methodology for specific context voice processing system implementation and programming method. The method has a certain reference value for the rural dialect and voice processing applications.

  9. [Inheritance and innovation of traditional processing technology of Chinese medicine].

    Science.gov (United States)

    Yang, Ming; Zhong, Ling-Yun; Xue, Xiao; Liu, Rong-Hua; Gong, Qian-Feng

    2016-02-01

    To discuss the inheritance and innovation study of Chinese medicine processing technology from three aspects: inheritance, standardization and industrial innovation development, propose "three lacks" in inheritance, "six lacks of standardization, and one lack of unity" in standardization, and "three emphasizing and three despising aspects" in industrial innovation, and propose feasible solutions for the above mentioned problems, providing a good foundation for inheritance and innovation of Chinese medicine processing. Copyright© by the Chinese Pharmaceutical Association.

  10. Moulded Pulp Manufacturing: Overview and Prospects for the Process Technology

    DEFF Research Database (Denmark)

    Didone, Mattia; Saxena, Prateek; Meijer, Ellen Brilhuis

    2017-01-01

    . The goal of this paper is to give an overview of the main aspects involved in the manufacture of moulded pulp products. This includes a classification of moulded pulp products, historical and current applications, production processes, materials, mechanical properties and environmental sustainability....... Moreover, based on the latest research in the field, an innovative drying technique that utilizes concepts derived from impulse drying is presented, and the implementation of this process technology is discussed....

  11. Microscale technology and biocatalytic processes: Opportunities and challenges for synthesis

    DEFF Research Database (Denmark)

    Wohlgemuth, Roland; Plazl, Igor; Žnidaršič-Plazl, Polona

    2015-01-01

    Despite the expanding presence of microscale technology in chemical synthesis and energy production as well as in biomedical devices and analytical and diagnostic tools, its potential in biocatalytic processes for pharmaceutical and fine chemicals, as well as related industries, has not yet been ......, and the future outlook for the implementation of these key green engineering methods and the role of supporting tools such as mathematical models to establish sustainable production processes are discussed....

  12. Status of electron beam processing technology in Malaysia

    International Nuclear Information System (INIS)

    Ghazali, Zulkafli; Dahlan, Khairul Zaman; Aiasah, S.H.; Khomsaton, A.B.; Ting, T.M.

    2003-01-01

    The electron beam processing in Malaysia starting in 1991 at MINT (Malaysian Institute for Nuclear Technology Research) has been focussed on medical product sterilization, curing of surface coating and polymer modifications. Subsequent installation of accelerators by private companies promoted the development of radiation processing technologies for the use of production of heat-shrinkable products, pilot-scale flue gas purification, as well as wires, cables, tubes and hydrogels. Decomposition of a wide range of volatile organic compounds from industrial exhausts (car painting lines, volatile dioxin and furan from municipal waste incinerators) and purification of liquid wastewater and drinking water are also being under R and D work. Malaysia will continue to play an active part in the program on radiation technology to strengthen environmentally sustainable development in line with FNCA objectives. (S. Ohno)

  13. DUPIC nuclear fuel manufacturing and process technology development at KAERI

    International Nuclear Information System (INIS)

    Yim, Sung Paal; Lee, Jung Won; Kim, Jong Ho; Kim, Soo Sung; Kim, Woong Ki; Yang, Myung Seung

    2000-01-01

    DUPIC fuel cycle development project in KAERI of Korea was initiated in 1991 and has advanced in relevant technologies for last 10 years. The project includes five different topics such as nuclear fuel manufacturing, compatibility evaluation, performance evaluation, manufacturing facility management, and safeguards. The contents and results of DUPIC R and D up to now are as follow: - the basic foundation was established for the critically required pelletizing technology and powder treatment technology for DUPIC. - development of DUPIC process line and deployment of 20 each process equipment and examination instruments in DFDF. - powder and pellet characterization study was done at PIEF based on the simfuel study results, and 30 DUPIC pellets were successfully produced. - the manufactured pellets were used for sample fuel rods irradiated in July,2000 in HANARO research reactor in KAERI and has been under post irradiation examination. (Hong, J. S.)

  14. Advanced Fabrication of Single-Crystal Diamond Membranes for Quantum Technologies

    Directory of Open Access Journals (Sweden)

    Michel Challier

    2018-03-01

    Full Text Available Many promising applications of single crystal diamond and its color centers as sensor platform and in photonics require free-standing membranes with a thickness ranging from several micrometers to the few 100 nm range. In this work, we present an approach to conveniently fabricate such thin membranes with up to about one millimeter in size. We use commercially available diamond plates (thickness 50 μ m in an inductively coupled reactive ion etching process which is based on argon, oxygen and SF 6 . We thus avoid using toxic, corrosive feed gases and add an alternative to previously presented recipes involving chlorine-based etching steps. Our membranes are smooth (RMS roughness <1 nm and show moderate thickness variation (central part: <1 μ m over ≈200 × 200 μ m 2 . Due to an improved etch mask geometry, our membranes stay reliably attached to the diamond plate in our chlorine-based as well as SF 6 -based processes. Our results thus open the route towards higher reliability in diamond device fabrication and up-scaling.

  15. Use of indigenous technology in processing and utilization of non ...

    African Journals Online (AJOL)

    Information used for this paper came from both primary and secondary sources. Ten (10) respondents were interviewed from each secondary source of information. The use of indigenous technology to process these forest products to forest foods is currently limited by use of crude methods, inability to expand production ...

  16. Lipid Processing Technology: Building a Multilevel Modeling Network

    DEFF Research Database (Denmark)

    Díaz Tovar, Carlos Axel; Mustaffa, Azizul Azri; Mukkerikar, Amol

    2011-01-01

    The aim of this work is to present the development of a computer aided multilevel modeling network for the systematic design and analysis of processes employing lipid technologies. This is achieved by decomposing the problem into four levels of modeling: i) pure component property modeling...

  17. Adoption of improved technologies in soyabean processing and ...

    African Journals Online (AJOL)

    adequate information and limited understanding. To increase protein food intake, adoption of soyabean improved technologies should be encouraged. Efforts should be made by extension workers to create more awareness on the importance of these innovations and on methods of processing. This way, consumption of ...

  18. An assessment of oil processing methods and technology in Taraba ...

    African Journals Online (AJOL)

    Objective: The study assessed the various methods and technology of vegetable oil processing in Taraba State. Methods: A total of 250 questionnaires were administered to vegetable oil processors with indepth interview of 28 respondents who were randomly selected based on a preliminary study in six (6) Local ...

  19. Transition process from emerging NDT technology to production inspection application

    Science.gov (United States)

    Jappe, William; Wood, Nancy; Johnson, Maurice

    1995-07-01

    The successful application of emerging NDT technologies for specific aging aircraft inspections requires an integration of efforts between aircraft operators, airframe manufacturers, NDT equipment designers, and government regulators. This paper describes the development process that was followed to establish an alternate inspection technique for a DC-10 crown skin butt joint inspection. Initial investigation, intermediate development, and final evaluations are discussed.

  20. Perception of Modern Processing Technology by Shea Butter ...

    African Journals Online (AJOL)

    The study examined the perception of Shea butter processors to modern processing technology in Kwara State. Multi stage sampling procedure was used to select 120 respondents. Data was collected using interview schedule and analysed with both descriptive and inferential statistics. Results revealed that 88.3% of the ...

  1. Pellet manufacturing by extrusion-spheronization using process analytical technology

    DEFF Research Database (Denmark)

    Sandler, Niklas; Rantanen, Jukka; Heinämäki, Jyrki

    2005-01-01

    The aim of this study was to investigate the phase transitions occurring in nitrofurantoin and theophylline formulations during pelletization by extrusion-spheronization. An at-line process analytical technology (PAT) approach was used to increase the understanding of the solid-state behavior of ...

  2. Sustaining high energy efficiency in existing processes with advanced process integration technology

    International Nuclear Information System (INIS)

    Zhang, Nan; Smith, Robin; Bulatov, Igor; Klemeš, Jiří Jaromír

    2013-01-01

    Highlights: ► Process integration with better modelling and more advanced solution methods. ► Operational changes for better environmental performance through optimisation. ► Identification of process integration technology for operational optimisation. ► Systematic implementation procedure of process integration technology. ► A case study with crude oil distillation to demonstrate the operational flexibility. -- Abstract: To reduce emissions in the process industry, much emphasis has been put on making step changes in emission reduction, by developing new process technology and making renewable energy more affordable. However, the energy saving potential of existing systems cannot be simply ignored. In recent years, there have been significant advances in process integration technology with better modelling techniques and more advanced solution methods. These methods have been applied to the new design and retrofit studies in the process industry. Here attempts are made to apply these technologies to improve the environmental performance of existing facilities with operational changes. An industrial project was carried out to demonstrate the importance and effectiveness of exploiting the operational flexibility for energy conservation. By applying advanced optimisation technique to integrate the operation of distillation and heat recovery in a crude oil distillation unit, the energy consumption was reduced by 8% without capital expenditure. It shows that with correctly identified technology and the proper execution procedure, significant energy savings and emission reduction can be achieved very quickly without major capital expenditure. This allows the industry to improve its economic and environment performance at the same time.

  3. Development of new processing technology for ruminant feed

    International Nuclear Information System (INIS)

    Mat Rasol Awang; Hassan Hamdani Mutaat; Zainun Said; Alias Saidali; Erwan Md Ariff

    2002-01-01

    The technology for production ruminant feed from agriculture by-product remains scare despite plentiful availability of feeding materials worldwide. Factors that prohibit the process technology development suggested that their peculiar physical make up, high cost of production and inferior product quality compared to established raw material, had consequently impeding the effort. In Malaysia, only two pilot plants exist; they demonstrate utilization of Oil Palm Frond (OPF) into feed. In the case of OPF in situ utilization as feed, farmers use chipper machine or shredder to process it. Other by-products have not been successfully exploited, except for Palm Kernel Cake (PKC) and Palm Oil Mill Effluent (POME) that already in commercial operation. In view of the by-product availability as feeding material in ruminant feeding system and availability of new chipper and shredder machines, the prospect of processing agriculture by-products into feed is expected to be a promising business venture. This paper describes the technology for production of new feed from oil palm Empty Fruit Bunch (EFB). It elaborates on Sterifeed Plant Operation based on plant capacity of 0.5 ton/day production. The operation aspects discuss raw materials handling and processing as well as transforming the products into marketable forms. In this process EFB is initially predigested by fungi in solid state fermentation process into feed materials; the product is ready to be fed in fresh form to animal. The operation exercise has established actual process flow, identified problems and process drawbacks. Based on this experience, availability of localized raw materials EFB at the palm oil mill and rapid development of processing machinery, it is very likely that a commercially viable feed processing plant can be established in the near future. In addition, establishing more data on product quality by further test and characterization of the new feed may contribute to success of the project. (Author)

  4. Thermo-tunable hybrid photonic crystal fiber based on solution-processed chalcogenide glass nanolayers

    DEFF Research Database (Denmark)

    Markos, Christos

    2016-01-01

    The possibility to combine silica photonic crystal fiber (PCF) as low-loss platform with advanced functional materials, offers an enormous range of choices for the development of fiber-based tunable devices. Here, we report a tunable hybrid silica PCF with integrated As2S3 glass nanolayers inside...... antiresonances by taking advantage the high thermo-optic coefficient of the solution-processed nanolayers. Two different hybrid fiber structures, with core diameter 10 and 5 mu m, were developed and characterized using a supercontinuum source. The maximum sensitivity was measured to be as high as 3.6 nm...

  5. Modern processing technologies and food quality. 18th Food Technology Days '97 dedicated to prof. F. Bitenc

    International Nuclear Information System (INIS)

    Zlender, Bozidar; Gasperlin, Lea; Hocevar, Ivica; Slemenik, Barbka; Hocevar, Polona

    1997-01-01

    Modern processing technologies and food quality. Proceedings of thematic survey of topics in food science and technology and nutrition for postgraduate students, Ljubljana Univ. (Slovenia). Biotechnical Fac., Food Science and Technology Dept

  6. Twinning processes in Cu-Al-Ni martensite single crystals investigated by neutron single crystal diffraction method

    Czech Academy of Sciences Publication Activity Database

    Molnar, P.; Šittner, P.; Novák, V.; Lukáš, Petr

    2008-01-01

    Roč. 481, Sp.Iss.SI (2008), s. 513-517 ISSN 0921-5093 R&D Projects: GA AV ČR IAA100480704 Institutional research plan: CEZ:AV0Z10480505 Keywords : Cu-Al-Ni * single crystals * neutron diffraction Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.806, year: 2008

  7. The crystal structure of the Escherichia coli autoinducer-2 processing protein LsrF.

    Directory of Open Access Journals (Sweden)

    Zamia Diaz

    2009-08-01

    Full Text Available Many bacteria produce and respond to the quorum sensing signal autoinducer-2 (AI-2. Escherichia coli and Salmonella typhimurium are among the species with the lsr operon, an operon containing AI-2 transport and processing genes that are up regulated in response to AI-2. One of the Lsr proteins, LsrF, has been implicated in processing the phosphorylated form of AI-2. Here, we present the structure of LsrF, unliganded and in complex with two phospho-AI-2 analogues, ribose-5-phosphate and ribulose-5-phosphate. The crystal structure shows that LsrF is a decamer of (alphabeta(8-barrels that exhibit a previously unseen N-terminal domain swap and have high structural homology with aldolases that process phosphorylated sugars. Ligand binding sites and key catalytic residues are structurally conserved, strongly implicating LsrF as a class I aldolase.

  8. Recent Advances in Food Processing Using High Hydrostatic Pressure Technology.

    Science.gov (United States)

    Wang, Chung-Yi; Huang, Hsiao-Wen; Hsu, Chiao-Ping; Yang, Binghuei Barry

    2016-01-01

    High hydrostatic pressure is an emerging non-thermal technology that can achieve the same standards of food safety as those of heat pasteurization and meet consumer requirements for fresher tasting, minimally processed foods. Applying high-pressure processing can inactivate pathogenic and spoilage microorganisms and enzymes, as well as modify structures with little or no effects on the nutritional and sensory quality of foods. The U.S. Food and Drug Administration (FDA) and the U.S. Department of Agriculture (USDA) have approved the use of high-pressure processing (HPP), which is a reliable technological alternative to conventional heat pasteurization in food-processing procedures. This paper presents the current applications of HPP in processing fruits, vegetables, meats, seafood, dairy, and egg products; such applications include the combination of pressure and biopreservation to generate specific characteristics in certain products. In addition, this paper describes recent findings on the microbiological, chemical, and molecular aspects of HPP technology used in commercial and research applications.

  9. Self-Growth of Centimeter-Scale Single Crystals by Normal Sintering Process in Modified Potassium Sodium Niobate Ceramics

    Science.gov (United States)

    Ahn, Cheol-Woo; Lee, Ho-Yong; Han, Guifang; Zhang, Shujun; Choi, Si-Young; Choi, Jong-Jin; Kim, Jong-Woo; Yoon, Woon-Ha; Choi, Joon-Hwan; Park, Dong-Soo; Hahn, Byung-Dong; Ryu, Jungho

    2015-01-01

    In this manuscript, an interesting phenomenon is reported. That is the self-growth of single crystals in Pb-free piezoelectric ceramics. These crystals are several centimeters in size. They are grown without any seed addition through a normal sintering process in modified potassium sodium niobate ceramics. It has been achieved by the composition designed to compensate the Na+ loss which occurs during the liquid phase sintering. The composition of the crystals is (K0.4925Na0.4925−xBa0.015+x/2)Nb0.995+xO3 [x is determined by the Na+ loss, due to Na2O volatilization]. These crystals have high piezoelectric voltage coefficients (g33, 131 10−3Vm/N), indicating that they are good candidates for piezoelectric sensors and energy harvesting devices. We hope that this report can offer the opportunity for many researchers to have an interest in these crystals. PMID:26631973

  10. Strategies for Derisking Translational Processes for Biomedical Technologies.

    Science.gov (United States)

    Abou-El-Enein, Mohamed; Duda, Georg N; Gruskin, Elliott A; Grainger, David W

    2017-02-01

    Inefficient translational processes for technology-oriented biomedical research have led to some prominent and frequent failures in the development of many leading drug candidates, several designated investigational drugs, and some medical devices, as well as documented patient harm and postmarket product withdrawals. Derisking this process, particularly in the early stages, should increase translational efficiency and streamline resource utilization, especially in an academic setting. In this opinion article, we identify a 12-step guideline for reducing risks typically associated with translating medical technologies as they move toward prototypes, preclinical proof of concept, and possible clinical testing. Integrating the described 12-step process should prove valuable for improving how early-stage academic biomedical concepts are cultivated, culled, and manicured toward intended clinical applications. Copyright © 2016 Elsevier Ltd. All rights reserved.

  11. Introduction of Virtualization Technology to Multi-Process Model Checking

    Science.gov (United States)

    Leungwattanakit, Watcharin; Artho, Cyrille; Hagiya, Masami; Tanabe, Yoshinori; Yamamoto, Mitsuharu

    2009-01-01

    Model checkers find failures in software by exploring every possible execution schedule. Java PathFinder (JPF), a Java model checker, has been extended recently to cover networked applications by caching data transferred in a communication channel. A target process is executed by JPF, whereas its peer process runs on a regular virtual machine outside. However, non-deterministic target programs may produce different output data in each schedule, causing the cache to restart the peer process to handle the different set of data. Virtualization tools could help us restore previous states of peers, eliminating peer restart. This paper proposes the application of virtualization technology to networked model checking, concentrating on JPF.

  12. Improving Logistics Processes in Industry Using Web Technologies

    Directory of Open Access Journals (Sweden)

    Jánošík Ján

    2016-12-01

    Full Text Available The aim of this paper is to propose the concept of a system that takes advantage of web technologies and integrates them into the management process and management of internal stocks which may relate to external applications and creates the conditions to transform a Computerized Control of Warehouse Stock (CCWS in the company. The importance of implementing CCWS is in the elimination of the claims caused by the human factor, as well as to allow the processing of information for analytical purposes and their subsequent use to improve internal processes. Using CCWS in the company would also facilitate better use of the potential tools Business Intelligence and Data Mining.

  13. HTR process heat applications, status of technology and economical potential

    International Nuclear Information System (INIS)

    Barnet, H.

    1997-01-01

    The technical and industrial feasibility of the production of high temperature heat from nuclear fuel is presented. The technical feasibility of high temperature heat consuming processes is reviewed and assessed. The conclusion is drawn that the next technological step for pilot plant scale demonstration is the nuclear heated steam reforming process. The economical potential of HTR process heat applications is reviewed: It is directly coupled to the economical competitiveness of HTR electricity production. Recently made statements and pre-conditions on the economic competitiveness in comparison to world market coal are reported. (author). 8 figs

  14. Technology and equipment for processing diamond materials of modern electronics

    Directory of Open Access Journals (Sweden)

    Mityagin A. Yu.

    2009-02-01

    Full Text Available The methods of selection and sorting of diamonds according to their physical properties by modern physical methods of the analysis are developed, as well as the technologies of precision laser cutting of diamonds, their processing on a basis of thermochemical reactions in gas environment. The experimental installation for polishing and grinding of diamond plates, installation for slicing, installation for plasma-chemical processing are created. The techniques of surface roughness measurement of the processed plates and control of roughness parameters are developed. Some experimental results are given.

  15. INFORMATION TECHNOLOGIES IN THE PROCESS OF TRAINING MARITIME SPECIALISTS

    Directory of Open Access Journals (Sweden)

    Ulyana Lyashenko

    2015-10-01

    Full Text Available The article represents main questions concerning usage of the newest information-communicative technologies of maritime educational establishments in the process of training specialists of corresponding specialities; reviews the problem of training cadets of Maritime educational institutions by means of information technologies while studying professionally focused disciplines; means of implementation information technologies into the educational process and their practical usage in future professional activity on board a ship are disclosed; the importance of online communications in teaching foreign language speaking, listening comprehension, writing and test tasks implementation to control forming of cadet’s lexical, phonetic and grammar skills are proved; presentations of authentic professionally oriented materials from the newest electronic sources on lectures on disciplines «Marine diesel installations», «Power management system», «Radio-navigational devices and systems». The author of the article grounds practicability of implementation of the newest information communicative technologies into educational process in classroom and extracurricular work, cadets are given an opportunity to get authentic professionally focused information on professional discipline, to extend knowledge on these disciplines and to realize control of formation corresponding competences.

  16. Application of radiation technology to sewage sludge processing: A review

    International Nuclear Information System (INIS)

    Wang Jianlong; Wang Jiazhuo

    2007-01-01

    Sewage sludge is unwanted residual solid wastes generated in wastewater treatment and its management is one of the most critical environmental issues of today. The treatment and disposal of sludge contribute a considerable proportion of the cost for running a wastewater treatment plant. The increasing amount of swage sludge and more and more legislative regulation of its disposal have stimulated the need for developing new technologies to process sewage sludge efficiently and economically. One ideal consideration is to recycle it after proper treatment. Radiation technology is regarded to be a promising alternative for its high efficiency in pathogen inactivation, organic pollutants oxidation, odor nuisance elimination and some other characteristics enhancement, which will facilitate the down-stream process of sludge treatment and disposal. Here we present a brief review of application of radiation technology on sewage sludge processing. Some basic information of two currently available irradiation systems and fundamental radiation chemistry are introduced firstly; then the world-wide application of this promising technology is reviewed; various effects of radiation on sludge is discussed in detail; and some concluding remarks are given and some future directions are also proposed

  17. Knowledge and cognitive process dimensions of Technology teachers' lesson objectives

    Directory of Open Access Journals (Sweden)

    David Mathumbu

    2014-03-01

    Full Text Available A clearly stated lesson objective is considered an essential component of a well-planned lesson. Many teachers of Technology, a relatively new subject in South African schools, teach Technology with rather limited training both in content and methodological approaches. This study sought to investigate and classify lesson objectives framed or implied by teachers in their lesson plans according to knowledge and cognitive process dimensions. The two-dimensional Taxonomy Table introduced by Krathwohl was adapted for Technology and formed the framework for this study. It was found that most of the directly stated objectives are directed to the lower level of the cognitive process dimension and address mainly factual knowledge, while no activities or lesson components address meta-cognitive knowledge. Some lesson objectives inferred from planned assessment activities placed higher demands on learners' cognitive domain. A recommendation flowing from the study is that, during pre-service training and in-service teacher support processes, the importance of clear lesson objectives should be emphasised and that assessments planned for such lessons should closely match the lesson objectives. Further research is also needed on the reasons why low cognitive demands are made in the teaching of Technology.

  18. Application of Electro-Technologies in Processing of Flax Fiber

    Directory of Open Access Journals (Sweden)

    G. S. Vijaya Raghavan

    2013-08-01

    Full Text Available Flax fibers used for various applications are obtained from flax stems. Retting followed by drying and mechanical separation leads to the production of fibers. This review article discusses the application of electro-technologies in the production of bast fibers from the flax stem. In these technologies, flax stems harvested from the field are subjected to microwave assisted retting, followed by electro–osmotic dewatering which reduces the water content of the stems. Dewatered stems are transferred to a microwave chamber for further drying, thus retted stems are obtained for further processing.

  19. TECHNOLOGICAL PROCESS MODELING AIMING TO IMPROVE ITS OPERATIONS MANAGEMENT

    Directory of Open Access Journals (Sweden)

    Ivan Mihajlović

    2011-11-01

    Full Text Available This paper presents the modeling procedure of one real technological system. In this study, thecopper extraction from the copper flotation waste generated at the Bor Copper Mine (Serbia, werethe object of modeling. Sufficient data base for statistical modeling was constructed using theorthogonal factorial design of the experiments. Mathematical model of investigated system wasdeveloped using the combination of linear and multiple linear statistical analysis approach. Thepurpose of such a model is obtaining optimal states of the system that enable efficient operationsmanagement. Besides technological and economical, ecological parameters of the process wereconsidered as crucial input variables.

  20. Rates and processes of crystallization in on-axis and off-axis MOR basaltic melts

    Science.gov (United States)

    Zellmer, Georg F.; Dulski, Peter; Iizuka, Yoshiyuki; Perfit, Michael R.

    2012-12-01

    Residence times of olivine and plagioclase phenocrysts and xenocrysts in mid-ocean ridge (MOR) basaltic melts have been studied since the mid 1980s using geospeedometric techniques (i.e. using diffusion of major and trace elements) in order to constrain the processes of melt ascent and differentiation in this important magmatic setting. Residence times range from a few hours to several years, but potential links between these timescales and specific tectonomagmatic variables such as spreading rate and relative locations of eruption site and ridge axis have remained elusive. Here we demonstrate how incomplete chemical diffusion of Sr within plagioclase crystals from MOR basalts erupted in on- and off-axis settings on a number of ridges with variable spreading rates provide geospeedometric constraints. We combine electron probe microanalytical crystal maps with detailed laser ablation profiles of almost 70 plagioclase crystals from the fast spreading East Pacific Rise (EPR) at 9-10°N, the intermediate spreading Gorda and Juan de Fuca (JdF) ridges, and the ultraslow spreading Gakkel ridge to calculate crystal residence times. These range from a few days to several months. The scarcity of residence times exceeding years corroborates previous data indicating that most of the growth of plagioclase phenocrysts occurs within the conduit at the onset of and during eruption on the sea floor, and extends this result to the fast-spreading EPR. Further, statistical analysis is employed to show for the first time that residence times are systematically longer at slower spreading rates, in off-axis samples, and samples sourced from laterally distal axial melt lenses. Plagioclase textures and residence time variations appear to be linked to differences in the dynamics of late-stage, pre-eruptive magma storage and ascent in the different tectonomagmatic settings investigated. In the future, geospeedometric work on MOR samples will be required to assess if the effect of spreading

  1. The Contextualized Technology Adaptation Process (CTAP): Optimizing Health Information Technology to Improve Mental Health Systems

    Science.gov (United States)

    Lyon, Aaron R.; Wasse, Jessica Knaster; Ludwig, Kristy; Zachry, Mark; Bruns, Eric J.; Unützer, Jürgen; McCauley, Elizabeth

    2015-01-01

    Health information technologies have become a central fixture in the mental healthcare landscape, but few frameworks exist to guide their adaptation to novel settings. This paper introduces the Contextualized Technology Adaptation Process (CTAP) and presents data collected during Phase 1 of its application to measurement feedback system development in school mental health. The CTAP is built on models of human-centered design and implementation science and incorporates repeated mixed methods assessments to guide the design of technologies to ensure high compatibility with a destination setting. CTAP phases include: (1) Contextual evaluation, (2) Evaluation of the unadapted technology, (3) Trialing and evaluation of the adapted technology, (4) Refinement and larger-scale implementation, and (5) Sustainment through ongoing evaluation and system revision. Qualitative findings from school-based practitioner focus groups are presented, which provided information for CTAP Phase 1, contextual evaluation, surrounding education sector clinicians’ workflows, types of technologies currently available, and influences on technology use. Discussion focuses on how findings will inform subsequent CTAP phases, as well as their implications for future technology adaptation across content domains and service sectors. PMID:25677251

  2. The Contextualized Technology Adaptation Process (CTAP): Optimizing Health Information Technology to Improve Mental Health Systems.

    Science.gov (United States)

    Lyon, Aaron R; Wasse, Jessica Knaster; Ludwig, Kristy; Zachry, Mark; Bruns, Eric J; Unützer, Jürgen; McCauley, Elizabeth

    2016-05-01

    Health information technologies have become a central fixture in the mental healthcare landscape, but few frameworks exist to guide their adaptation to novel settings. This paper introduces the contextualized technology adaptation process (CTAP) and presents data collected during Phase 1 of its application to measurement feedback system development in school mental health. The CTAP is built on models of human-centered design and implementation science and incorporates repeated mixed methods assessments to guide the design of technologies to ensure high compatibility with a destination setting. CTAP phases include: (1) Contextual evaluation, (2) Evaluation of the unadapted technology, (3) Trialing and evaluation of the adapted technology, (4) Refinement and larger-scale implementation, and (5) Sustainment through ongoing evaluation and system revision. Qualitative findings from school-based practitioner focus groups are presented, which provided information for CTAP Phase 1, contextual evaluation, surrounding education sector clinicians' workflows, types of technologies currently available, and influences on technology use. Discussion focuses on how findings will inform subsequent CTAP phases, as well as their implications for future technology adaptation across content domains and service sectors.

  3. Choices of capture chromatography technology in antibody manufacturing processes.

    Science.gov (United States)

    DiLeo, Michael; Ley, Arthur; Nixon, Andrew E; Chen, Jie

    2017-11-15

    The capture process employed in monoclonal antibody downstream purification is not only the most critically impacted process by increased antibody titer resulting from optimized mammalian cell culture expression systems, but also the most important purification step in determining overall process throughput, product quality, and economics. Advances in separation technology for capturing antibodies from complex feedstocks have been one focus of downstream purification process innovation for past 10 years. In this study, we evaluated new generation chromatography resins used in the antibody capture process including Protein A, cation exchange, and mixed mode chromatography to address the benefits and unique challenges posed by each chromatography approach. Our results demonstrate the benefit of improved binding capacity of new generation Protein A resins, address the concern of high concentration surge caused aggregation when using new generation cation exchange resins with over 100mg/mL binding capacity, and highlight the potential of multimodal cation exchange resins for capture process design. The new landscape of capture chromatography technologies provides options to achieve overall downstream purification outcome with high product quality and process efficiency. Copyright © 2017 Elsevier B.V. All rights reserved.

  4. Redox process catalysed by growing crystal-strengite, FePO4,2H2O, crystallizing from solution with iron(II) and hydroxylamine

    Science.gov (United States)

    Lundager Madsen, Hans Erik

    2014-09-01

    In an attempt to grow pure crystals of the iron(II) phosphate vivianite, Fe3(PO4)2,8H2O, from a solution of Mohr's salt, Fe(NH4)2(SO4)2,6H2O, added to a solution of ammonium phosphate, hydroxylammonium chloride, NH3OHCl, was added to the iron(II) stock solution to eliminate oxidation of iron(II) by oxygen from the air. However, the effect turned out to be the opposite of the expected: whereas hydroxylamine reduces iron(III) in bulk solution, it acted as a strong oxidant in the presence of growing iron phosphate crystals, causing the crystallization of the iron(III) phosphate strengite, FePO4,2H2O, as the only solid phase. Evidently the crystal surface catalyses oxidation of iron(II) by hydroxylamine. The usual composite kinetics of spiral growth and surface nucleation was found. The surface-nucleation part yielded edge free energy λ in the range 12-45 pJ/m, virtually independent of temperature and in the range typical for phosphates of divalent metals. The scatter of values for λ presumably arises from contributions from different crystal forms to the overall growth rate. The low mean value points to strong adsorption of iron(II), which is subsequently oxidized at the crystal surface, forming strengite. The state of the system did not tend to thermodynamic equilibrium, but to a metastable state, presumably controlled by the iron(II) rich surface layer of the crystal. In addition to crystal growth, it was possible to measure nucleation kinetics by light scattering (turbidimetry). A point of transition from heterogeneous to homogeneous nucleation was found, and from the results for the homogeneous domain a rather precise value of crystal surface free energy γ=55 mJ/m2 was found. This is a relatively low value as well, indicating that the redox process plays a role already at the nucleation stage.

  5. Using CASE to Exploit Process Modeling in Technology Transfer

    Science.gov (United States)

    Renz-Olar, Cheryl

    2003-01-01

    A successful business will be one that has processes in place to run that business. Creating processes, reengineering processes, and continually improving processes can be accomplished through extensive modeling. Casewise(R) Corporate Modeler(TM) CASE is a computer aided software engineering tool that will enable the Technology Transfer Department (TT) at NASA Marshall Space Flight Center (MSFC) to capture these abilities. After successful implementation of CASE, it could then go on to be applied in other departments at MSFC and other centers at NASA. The success of a business process is dependent upon the players working as a team and continuously improving the process. A good process fosters customer satisfaction as well as internal satisfaction in the organizational infrastructure. CASE provides a method for business process success through functions consisting of systems and processes business models; specialized diagrams; matrix management; simulation; report generation and publishing; and, linking, importing, and exporting documents and files. The software has an underlying repository or database to support these functions. The Casewise. manual informs us that dynamics modeling is a technique used in business design and analysis. Feedback is used as a tool for the end users and generates different ways of dealing with the process. Feedback on this project resulted from collection of issues through a systems analyst interface approach of interviews with process coordinators and Technical Points of Contact (TPOCs).

  6. Technological and life cycle assessment of organics processing odour control technologies

    International Nuclear Information System (INIS)

    Bindra, Navin; Dubey, Brajesh; Dutta, Animesh

    2015-01-01

    As more municipalities and communities across developed world look towards implementing organic waste management programmes or upgrading existing ones, composting facilities are emerging as a popular choice. However, odour from these facilities continues to be one of the most important concerns in terms of cost & effective mitigation. This paper provides a technological and life cycle assessment of some of the different odour control technologies and treatment methods that can be implemented in organics processing facilities. The technological assessment compared biofilters, packed tower wet scrubbers, fine mist wet scrubbers, activated carbon adsorption, thermal oxidization, oxidization chemicals and masking agents. The technologies/treatment methods were evaluated and compared based on a variety of operational, usage and cost parameters. Based on the technological assessment it was found that, biofilters and packed bed wet scrubbers are the most applicable odour control technologies for use in organics processing faculties. A life cycle assessment was then done to compare the environmental impacts of the packed-bed wet scrubber system, organic (wood-chip media) bio-filter and inorganic (synthetic media) bio-filter systems. Twelve impact categories were assessed; cumulative energy demand (CED), climate change, human toxicity, photochemical oxidant formation, metal depletion, fossil depletion, terrestrial acidification, freshwater eutrophication, marine eutrophication, terrestrial eco-toxicity, freshwater eco-toxicity and marine eco-toxicity. The results showed that for all impact categories the synthetic media biofilter had the highest environmental impact, followed by the wood chip media bio-filter system. The packed-bed system had the lowest environmental impact for all categories. - Highlights: • Assessment of odour control technologies for organics processing facilities. • Comparative life cycle assessment of three odour control technologies was conducted

  7. Technological and life cycle assessment of organics processing odour control technologies

    Energy Technology Data Exchange (ETDEWEB)

    Bindra, Navin [School of Engineering, University of Guelph, 50 Stone Road East, Guelph, Ontario N1G2W1 (Canada); Dubey, Brajesh, E-mail: bkdubey@civil.iitkgp.ernet.in [School of Engineering, University of Guelph, 50 Stone Road East, Guelph, Ontario N1G2W1 (Canada); Environmental Engineering Division, Department of Civil Engineering, Indian Institute of Technology, Kharagpur, West Bengal 721302 (India); Dutta, Animesh [School of Engineering, University of Guelph, 50 Stone Road East, Guelph, Ontario N1G2W1 (Canada)

    2015-09-15

    As more municipalities and communities across developed world look towards implementing organic waste management programmes or upgrading existing ones, composting facilities are emerging as a popular choice. However, odour from these facilities continues to be one of the most important concerns in terms of cost & effective mitigation. This paper provides a technological and life cycle assessment of some of the different odour control technologies and treatment methods that can be implemented in organics processing facilities. The technological assessment compared biofilters, packed tower wet scrubbers, fine mist wet scrubbers, activated carbon adsorption, thermal oxidization, oxidization chemicals and masking agents. The technologies/treatment methods were evaluated and compared based on a variety of operational, usage and cost parameters. Based on the technological assessment it was found that, biofilters and packed bed wet scrubbers are the most applicable odour control technologies for use in organics processing faculties. A life cycle assessment was then done to compare the environmental impacts of the packed-bed wet scrubber system, organic (wood-chip media) bio-filter and inorganic (synthetic media) bio-filter systems. Twelve impact categories were assessed; cumulative energy demand (CED), climate change, human toxicity, photochemical oxidant formation, metal depletion, fossil depletion, terrestrial acidification, freshwater eutrophication, marine eutrophication, terrestrial eco-toxicity, freshwater eco-toxicity and marine eco-toxicity. The results showed that for all impact categories the synthetic media biofilter had the highest environmental impact, followed by the wood chip media bio-filter system. The packed-bed system had the lowest environmental impact for all categories. - Highlights: • Assessment of odour control technologies for organics processing facilities. • Comparative life cycle assessment of three odour control technologies was conducted

  8. Information Technology Process Improvement Decision-Making: An Exploratory Study from the Perspective of Process Owners and Process Managers

    Science.gov (United States)

    Lamp, Sandra A.

    2012-01-01

    There is information available in the literature that discusses information technology (IT) governance and investment decision making from an executive-level perception, yet there is little information available that offers the perspective of process owners and process managers pertaining to their role in IT process improvement and investment…

  9. Numerical Simulation of Directional Solidification Process of Single Crystal Ni- Based Superalloy Casting

    Directory of Open Access Journals (Sweden)

    Szeliga D.

    2017-06-01

    Full Text Available The analysis of influence of mould withdrawal rate on the solidification process of CMSX-4 single crystal castings produced by Bridgman method was presented in this paper. The predicted values of temperature gradient, solidification and cooling rate, were determined at the longitudinal section of casting blade withdrawn at rate from 1 to 6mm/min using ProCAST software. It was found that the increase of withdrawal rate of ceramic mould results in the decrease of temperature gradient and the growth of cooling rate, along blade height. Based on results of solidification parameter G/R (temperature gradient/solidification rate, maximum withdrawal rate of ceramic mould (3.5 mm/min, which ensures lower susceptibility to formation process of new grain defects in single crystal, was established. It was proved that these defects can be formed in the bottom part of casting at withdrawal rate of 4 mm/min. The increase of withdrawal rate to 5 and 6 mm/min results in additional growth of susceptibility of defects formation along the whole height of airfoil.

  10. Database mirroring in fault-tolerant continuous technological process control

    Directory of Open Access Journals (Sweden)

    R. Danel

    2015-10-01

    Full Text Available This paper describes the implementations of mirroring technology of the selected database systems – Microsoft SQL Server, MySQL and Caché. By simulating critical failures the systems behavior and their resilience against failure were tested. The aim was to determine whether the database mirroring is suitable to use in continuous metallurgical processes for ensuring the fault-tolerant solution at affordable cost. The present day database systems are characterized by high robustness and are resistant to sudden system failure. Database mirroring technologies are reliable and even low-budget projects can be provided with a decent fault-tolerant solution. The database system technologies available for low-budget projects are not suitable for use in real-time systems.

  11. Effect of the Crystallization Process on the Marginal and Internal Gaps of Lithium Disilicate CAD/CAM Crowns

    Directory of Open Access Journals (Sweden)

    Jae-Hong Kim

    2016-01-01

    Full Text Available The aim of this study is to quantify the effect of the crystallization process on lithium disilicate ceramic crowns fabricated using a computer-aided design/computer-aided manufacturing (CAD/CAM system and to determine whether the effect of crystallization is clinically acceptable by comparing values of fit before and after the crystallization process. The mandibular right first molar was selected as the abutment for the experiments. Fifteen working models were prepared. Lithium disilicate crowns appropriate for each abutment were prepared using a commercial CAD/CAM system. Gaps in the marginal area and 4 internal areas of each crown were measured twice—before and after crystallization—using the silicone replica technique. The mean values of fit before and after crystallization were analyzed using a paired t-test to examine whether the conversion that occurred during crystallization affected marginal and internal gaps (α=0.05. Gaps increased in the marginal area and decreased in the internal areas after crystallization. There were statistically significant differences in all of the investigated areas (P<0.05. None of the values for marginal and internal fit of lithium disilicate CAD/CAM crowns after crystallization exceeded 120 μm, which is the clinically acceptable threshold.

  12. IMPROVING THE QUALITY OF MAINTENANCE PROCESSES USING INFORMATION TECHNOLOGY

    Directory of Open Access Journals (Sweden)

    Zora Arsovski

    2008-06-01

    Full Text Available In essence, process of maintaining equipment is a support process, because it indirectly contributes to operational ability of the production process necessary for the supply chain of the new value. Taking into account increased levels of automatization and quality, this proces s becomes more and more significant and for some branches of industry, even crucial. Due to the fact that the quality of the entire process is more and more dependent on the maintenance process, these processes must be carefully designed and effectively im plemented. There are various techniques and approaches at our disposal, such as technical, logistical and intensive application of the information - communication technologies. This last approach is presented in this work. It begins with organizational goa ls, especially quality objectives. Then, maintenance processes and integrated information system structures are defined. Maintenance process quality and improvement processes are defined using a set of performances, with a special emphasis placed on effectiveness and quality economics. At the end of the work, information system for improving maintenance economics is structured. Besides theoretical analysis, work also presents results authors obtained analyzing food industry, metal processing industry an d building materials industry.

  13. Virtual Crystallizer

    Energy Technology Data Exchange (ETDEWEB)

    Land, T A; Dylla-Spears, R; Thorsness, C B

    2006-08-29

    Large dihydrogen phosphate (KDP) crystals are grown in large crystallizers to provide raw material for the manufacture of optical components for large laser systems. It is a challenge to grow crystal with sufficient mass and geometric properties to allow large optical plates to be cut from them. In addition, KDP has long been the canonical solution crystal for study of growth processes. To assist in the production of the crystals and the understanding of crystal growth phenomena, analysis of growth habits of large KDP crystals has been studied, small scale kinetic experiments have been performed, mass transfer rates in model systems have been measured, and computational-fluid-mechanics tools have been used to develop an engineering model of the crystal growth process. The model has been tested by looking at its ability to simulate the growth of nine KDP boules that all weighed more than 200 kg.

  14. Radioactive Waste Conditioning, Immobilisation, And Encapsulation Processes And Technologies: Overview And Advances (Chapter 7)

    Energy Technology Data Exchange (ETDEWEB)

    Jantzen, Carol M. [Savannah River National Lab., Aiken SC (United States); Lee, William E. [Imperial College, London (United Kingdom). Dept. of Materials; Ojovan, Michael I. [Univ. of Sheffield (United Kingdom). Dept. of Materials Science and Engineering

    2012-10-19

    The main immobilization technologies that are available commercially and have been demonstrated to be viable are cementation, bituminization, and vitrification. Vitrification is currently the most widely used technology for the treatment of high level radioactive wastes (HLW) throughout the world. Most of the nations that have generated HLW are immobilizing in either alkali borosilicate glass or alkali aluminophosphate glass. The exact compositions of nuclear waste glasses are tailored for easy preparation and melting, avoidance of glass-in-glass phase separation, avoidance of uncontrolled crystallization, and acceptable chemical durability, e.g., leach resistance. Glass has also been used to stabilize a variety of low level wastes (LLW) and mixed (radioactive and hazardous) low level wastes (MLLW) from other sources such as fuel rod cladding/decladding processes, chemical separations, radioactive sources, radioactive mill tailings, contaminated soils, medical research applications, and other commercial processes. The sources of radioactive waste generation are captured in other chapters in this book regarding the individual practices in various countries (legacy wastes, currently generated wastes, and future waste generation). Future waste generation is primarily driven by interest in sources of clean energy and this has led to an increased interest in advanced nuclear power production. The development of advanced wasteforms is a necessary component of the new nuclear power plant (NPP) flowsheets. Therefore, advanced nuclear wasteforms are being designed for robust disposal strategies. A brief summary is given of existing and advanced wasteforms: glass, glass-ceramics, glass composite materials (GCM’s), and crystalline ceramic (mineral) wasteforms that chemically incorporate radionuclides and hazardous species atomically in their structure. Cementitious, geopolymer, bitumen, and other encapsulant wasteforms and composites that atomically bond and encapsulate

  15. Structural evolution process of isotactic polypropylene in the isothermal crystallization from the melt

    Energy Technology Data Exchange (ETDEWEB)

    Reddy, Kummetha Raghunatha; Tashiro, Kohji; Hanesaka, Makoto [Department of Future Industry-Oriented Basic Science and Materials, Graduate School of Engineering, Toyota Technological Institute, Tempaku, Nagoya 468-8511 (Japan); Sakurai, Takashi; Yamaguchi, Noburu [Petrochemical Research Laboratory, Sumitomo Chemical Co. Ltd., Chiba 299-0295 (Japan); Sasaki, Sono; Masunaga, Hiroyasu; Takata, Masaki, E-mail: ktashiro@toyota-ti.ac.j [Japan Synchrotron Radiation Research Institute (JASRI), Kouto, Sayo-gun, Hyogo, 679-5198 (Japan)

    2009-08-01

    The melt-isothermal crystallization behaviour has been investigated for isotactic polypropylene (iPP) by means of time-resolved simultaneous measurements of small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) using synchrotron radiation source in SPring-8. The time-resolved Fourier-transform infrared spectral (FTIR) measurements were also performed to clarify the formation process of helices. The SAXS data were analyzed on the basis of Guinier (isolated domains) and Debye-Bueche (correlated domains) theories and correlation function (stacked lamellae). The results were combined with the FTIR data, allowing us to draw the concrete structural evolution process including the formation of regular helices and their growth, the correlation of higher density domains consisting of these helices, and the increment of correlation between the neighbouring lamellae to build up the stacked lamellar structure of higher crystallinity.

  16. Analysis of Surface Chemistry and Detector Performance of Chemically Process CdZnTe crystals

    Energy Technology Data Exchange (ETDEWEB)

    HOSSAIN, A.; Yang, G.; Sutton, J.; Zergaw, T.; Babalola, O. S.; Bolotnikov, A. E.; Camarda. ZG. S.; Gul, R.; Roy, U. N., and James, R. B.

    2015-10-05

    The goal is to produce non-conductive smooth surfaces for fabricating low-noise and high-efficiency CdZnTe devices for gamma spectroscopy. Sample preparation and results are discussed. The researachers demonstrated various bulk defects (e.g., dislocations and sub-grain boundaries) and surface defects, and examined their effects on the performance of detectors. A comparison study was made between two chemical etchants to produce non-conductive smooth surfaces. A mixture of bromine and hydrogen peroxide proved more effective than conventional bromine etchant. Both energy resolution and detection efficiency of CZT planar detectors were noticeably increased after processing the detector crystals using improved chemical etchant and processing methods.

  17. Process of technology management in SMEs of the metal processing industry – the case study investigation

    Directory of Open Access Journals (Sweden)

    Krawczyk-Dembicka Elżbieta

    2017-03-01

    Full Text Available The main purpose of this work is to identify the factors that influence the process of technology management in the sector of small- and medium-sized enterprises of the metal processing industry, considering the shape and course required to achieve modern operation conditions by enterprises in the market.

  18. Role of health-keeping technologies in educational process

    Directory of Open Access Journals (Sweden)

    Voloshin O. R.

    2012-07-01

    Full Text Available The value of health-keeping technologies in educational process is considered. Theoretical methodological approaches of their interpretation are exposed. The making forming for the man of conscious motivation in relation to the maintainance of individual health is shown. Valeological and ecological values are analysed. The features of introduction of health-keeping technologies in a modern educational process are certain. The complex estimation of terms of education and studies, which allow to provide the good state of health of young people, care of high level of their self-realization, skills of healthy way of life, is resulted, to carry out monitoring of indexes of individual development, forecast the possible changes of health. It is marked on the necessity of providing of harmonious development of natural capabilities of personality: its mind, moral and aesthetically beautiful senses, requirement in activity, capture initial experience of socializing with people.

  19. Current mechanisms in silicon PIN structures processed with various technologies

    CERN Document Server

    Ruzin, A

    2002-01-01

    This study presents a comparison of dark characteristics of PIN (p sup + -semi-intrinsic-n sup +) structures fabricated with several technologies on high-resistivity silicon wafers. The study considers the temperature dependence of the various current mechanisms. Significant and consistent differences were observed in the reverse current-voltage characteristics of the various samples, while capacitance-voltage profiles remain similar, indicating no process related variations in the effective space charge distribution. The results show that the activation energy of the reverse current in samples processed by various technologies differs, which may indicate that the Shockley Read Hall generation occurs through centers at different energies. Specifically, in some samples the reverse currents are dominated by generation-recombination centers located approx 0.2 eV from the mid-gap, while in other samples the currents are dominated by the 'standard' mid-gap generation-recombination centers. The difference is shown ...

  20. The evolution of waste management processes and technologies in BNFL

    International Nuclear Information System (INIS)

    Asquith, R.W.; Fairhall, G.A.

    1997-01-01

    The treatment of wastes arising from BNFL''s nuclear fuel cycle operations can be traced through a number of phases. The first was the development of vitrification and cementation for fresh arisings. Plants utilising these technologies are now in operation. To handle the mixed, heterogeneous intermediate level wastes, retrieval, segregation and robust treatment processes are at an advanced stage of development, with all plants to be operational from 2002. BNFL is focusing attention on reducing waste management lifetime costs including reducing waste volumes of source. Technologies aimed at significant reductions are now being developed. The final phase, now in progress, recognizes the need for an integrated approach to advanced fuel cycle processes which incorporates BNFL''s holistic concept. (author)

  1. The Aluminum Smelting Process and Innovative Alternative Technologies

    Science.gov (United States)

    Drabløs, Per Arne

    2014-01-01

    Objective: The industrial aluminum production process is addressed. The purpose is to give a short but comprehensive description of the electrolysis cell technology, the raw materials used, and the health and safety relevance of the process. Methods: This article is based on a study of the extensive chemical and medical literature on primary aluminum production. Results: At present, there are two main technological challenges for the process—to reduce energy consumption and to mitigate greenhouse gas emissions. A future step may be carbon dioxide gas capture and sequestration related to the electric power generation from fossil sources. Conclusions: Workers' health and safety have now become an integrated part of the aluminum business. Work-related injuries and illnesses are preventable, and the ultimate goal to eliminate accidents with lost-time injuries may hopefully be approached in the future. PMID:24806723

  2. [Research on increasing X-ray protection capability based on photonic crystal technology].

    Science.gov (United States)

    Li, Ping; Zhao, Peng; Zhang, Rui

    2014-06-01

    Light cannot be propagated within the range of photonic crystal band gaps. Based on this unique property, we proposed a method to improve anti-radiation capability through one-dimensional photonic crystal coating. Using transmission matrix method, we determined the appropriate dielectric materials, thickness and periodic numbers of photonic crystals through Matlab programming simulation. Then, compound one-dimensional photonic crystal coating was designed which was of high anti-radiation rate within the range of X-ray. As is shown through simulation experiments, the reflection rate against X-ray was higher than 90 percent, and the desired anti-radiation effect was achieved. Thus, this method is able to help solve the technical problems facing the inorganic lead glass such as thickness, weightiness, costliness, high lead equivalent, low transparency and high cost. This method has won China's national invention patent approval, and the patent number is 201220228549.2.

  3. Process Technology for Immobilized LipaseProcess Technology for Immobilized Lipase-catalyzed

    DEFF Research Database (Denmark)

    Xu, Yuan

    (e.g. a hydrophobic carrier for the immobilized lipase and the capabilities to provide sufficient mixing as well as stepwise/continuous feeding of ethanol to the reactor). An STR is efficient for batch operation while a PBR is efficient for a continuous production. An STR can more easily provide...... sufficient external mass transfer for a reaction, but will lead to more mechanical damage of the biocatalyst particles, than a PBR. A reactor combination of CSTR with PBR can couple the advantages of both, delivering an efficient continuous process.The second case study (esterification) shares some similar......-catalyzed transesterification is that it is multi-phasic system. The by-product glycerol can potentially impose inhibitory effects on immobilized lipases and likewise the un-dissolved ethanol can inhibit the lipase. The options for addressing these issues can be used as the basis for selecting the biocatalyst and the reactor...

  4. Studies on Separation Process and Production Technology of Boron Isotope

    OpenAIRE

    LI Jian-ping

    2014-01-01

    The boron isotopes separation test was performed by chemical exchange reaction in the benzene ether -three boron fluoride system, which resulted to the boron isotopic enrichment of -10 in the liquid phase, the boron isotopic enrichment of -11 in the gas phase. After then, boron isotope separation trial production has been finished. In this process, the exchange column and complex tower normal operating parameters and the complex tower technology have been obtained, the problems of material di...

  5. Surviving security how to integrate people, process, and technology

    CERN Document Server

    Andress, Amanda

    2003-01-01

    WHY DO I NEED SECURITY? Introduction The Importance of an Effective Security Infrastructure People, Process, and Technology What Are You Protecting Against? Types of Attacks Types of Attackers Security as a Competitive Advantage Choosing a Solution Finding Security Employees The Layered Approach UNDERSTANDING REQUIREMENTS AND RISK What Is Risk? Embracing Risk Information Security Risk Assessment Assessing Risk Insurance SECURITY POLICIES AND PROCEDURES Internal Focus Is Key Security Awareness and Education Policy Life Cycle Developing Policies Components of a Security Policy Sample Security Po

  6. Lignocellulosic ethanol: Technology design and its impact on process efficiency.

    Science.gov (United States)

    Paulova, Leona; Patakova, Petra; Branska, Barbora; Rychtera, Mojmir; Melzoch, Karel

    2015-11-01

    This review provides current information on the production of ethanol from lignocellulosic biomass, with the main focus on relationships between process design and efficiency, expressed as ethanol concentration, yield and productivity. In spite of unquestionable advantages of lignocellulosic biomass as a feedstock for ethanol production (availability, price, non-competitiveness with food, waste material), many technological bottlenecks hinder its wide industrial application and competitiveness with 1st generation ethanol production. Among the main technological challenges are the recalcitrant structure of the material, and thus the need for extensive pretreatment (usually physico-chemical followed by enzymatic hydrolysis) to yield fermentable sugars, and a relatively low concentration of monosaccharides in the medium that hinder the achievement of ethanol concentrations comparable with those obtained using 1st generation feedstocks (e.g. corn or molasses). The presence of both pentose and hexose sugars in the fermentation broth, the price of cellulolytic enzymes, and the presence of toxic compounds that can inhibit cellulolytic enzymes and microbial producers of ethanol are major issues. In this review, different process configurations of the main technological steps (enzymatic hydrolysis, fermentation of hexose/and or pentose sugars) are discussed and their efficiencies are compared. The main features, benefits and drawbacks of simultaneous saccharification and fermentation (SSF), simultaneous saccharification and fermentation with delayed inoculation (dSSF), consolidated bioprocesses (CBP) combining production of cellulolytic enzymes, hydrolysis of biomass and fermentation into one step, together with an approach combining utilization of both pentose and hexose sugars are discussed and compared with separate hydrolysis and fermentation (SHF) processes. The impact of individual technological steps on final process efficiency is emphasized and the potential for use

  7. Army Information Technology Procurement: A Business Process Analysis

    Science.gov (United States)

    2015-03-27

    Education and Training Command In Partial Fulfillment of the Requirements for the Degree of Master of Science in Engineering Management...Brent Langhals, Lt Col, USAF Member John Elshaw, PhD Member Abstract The integration of Information and Communication Technology ( ICT ...the lack transparency in how resources are allocated. This thesis presents a business process analysis of the Army’s ICT procurement system. The

  8. Industrial Maturity of FR Fuel Cycle Processes and Technologies

    International Nuclear Information System (INIS)

    Bruezière, Jérôme

    2013-01-01

    FR fuel cycle processes and technologies have already been proven industrially for Oxide Fuel, and to a lesser extent for metal fuel. In addition, both used oxide fuel reprocessing and fresh oxide fuel manufacturing benefit from similar industrial experience currently deployed for LWR. Alternative fuel type will have to generate very significant benefit in reactor ( safety, cost, … ) to justify corresponding development and industrialization costs

  9. Effectiveness of Information Technology Infrastructure Library Process Implementations by Information Technology Departments within United States Organizations

    Science.gov (United States)

    Persinger, Jon F.

    2010-01-01

    This research study examined whether the overall effectiveness of the Information Technology Infrastructure Library (ITIL) could be predicted by measuring multiple independent variables. The primary variables studied included the number of ITIL process modules adopted and the overall ITIL "maturity level." An online survey was used to…

  10. Technology and plasma-materials interaction processes of tokamak disruptions

    International Nuclear Information System (INIS)

    McGrath, R.T.; Kellman, A.G.

    1992-01-01

    A workshop on the technology and plasma-materials interaction processes of tokamak disruptions was held April 3, 1992 in Monterey, California, as a satellite meeting of the 10th International Conference on Plasma-Surface Interactions. The objective was to bring together researchers working on disruption measurements in operating tokamaks, those performing disruption simulation experiments using pulsed plasma gun, electron beam and laser systems, and computational physicists attempting to model the evolution and plasma-materials interaction processes of tokamak disruptions. This is a brief report on the workshop. 4 refs

  11. Centralisation of informatics (more effective processes via using new technologies)

    International Nuclear Information System (INIS)

    Cocher, L.

    2004-01-01

    In this presentation author deals with next problems of Slovenske elektrarne, Plc (SE): - Centralisation and optimisation of informatics management; - New technologies within Integrated Informatics System IIS-SE: presentation of preliminary Project of 2 nd generation IIS-SE; - Centralisation of the selected data processing. At the present the intensive process of restructuring is taking place in SE, Plc, focused on increasing of the effectiveness of the pursued activities. In connection with this the Informatics section solves two projects: More effective self-management and human resources; Change of Informatics system architecture from decentralised to the centralised ones with an aim to consolidate all information and to make new conditions for higher mobility

  12. Computer-Aided Modeling of Lipid Processing Technology

    DEFF Research Database (Denmark)

    Diaz Tovar, Carlos Axel

    2011-01-01

    increase along with growing interest in biofuels, the oleochemical industry faces in the upcoming years major challenges in terms of design and development of better products and more sustainable processes to make them. Computer-aided methods and tools for process synthesis, modeling and simulation...... are widely used for design, analysis, and optimization of processes in the chemical and petrochemical industries. These computer-aided tools have helped the chemical industry to evolve beyond commodities toward specialty chemicals and ‘consumer oriented chemicals based products’. Unfortunately...... to develop systematic computer-aided methods (property models) and tools (database) related to the prediction of the necessary physical properties suitable for design and analysis of processes employing lipid technologies. The methods and tools include: the development of a lipid-database (CAPEC...

  13. Materials, process, product analysis of coal process technology. Phase I final report

    Energy Technology Data Exchange (ETDEWEB)

    Saxton, J. C.; Roig, R. W.; Loridan, A.; Leggett, N. E.; Capell, R. G.; Humpstone, C. C.; Mudry, R. N.; Ayres, E.

    1976-02-01

    The purpose of materials-process-product analysis is a systematic evaluation of alternative manufacturing processes--in this case processes for converting coal into energy and material products that can supplement or replace petroleum-based products. The methodological steps in the analysis include: Definition of functional operations that enter into coal conversion processes, and modeling of alternative, competing methods to accomplish these functions; compilation of all feasible conversion processes that can be assembled from combinations of competing methods for the functional operations; systematic, iterative evaluation of all feasible conversion processes under a variety of economic situations, environmental constraints, and projected technological advances; and aggregative assessments (economic and environmental) of various industrial development scenarios. An integral part of the present project is additional development of the existing computer model to include: A data base for coal-related materials and coal conversion processes; and an algorithmic structure that facilitates the iterative, systematic evaluations in response to exogenously specified variables, such as tax policy, environmental limitations, and changes in process technology and costs. As an analytical tool, the analysis is intended to satisfy the needs of an analyst working at the process selection level, for example, with respect to the allocation of RDandD funds to competing technologies.

  14. A Sensor Fusion Algorithm for Filtering Pyrometer Measurement Noise in the Czochralski Crystallization Process

    Directory of Open Access Journals (Sweden)

    M. Komperød

    2011-01-01

    Full Text Available The Czochralski (CZ crystallization process is used to produce monocrystalline silicon for solar cell wafers and electronics. Tight temperature control of the molten silicon is most important for achieving high crystal quality. SINTEF Materials and Chemistry operates a CZ process. During one CZ batch, two pyrometers were used for temperature measurement. The silicon pyrometer measures the temperature of the molten silicon. This pyrometer is assumed to be accurate, but has much high-frequency measurement noise. The graphite pyrometer measures the temperature of a graphite material. This pyrometer has little measurement noise. There is quite a good correlation between the two pyrometer measurements. This paper presents a sensor fusion algorithm that merges the two pyrometer signals for producing a temperature estimate with little measurement noise, while having significantly less phase lag than traditional lowpass- filtering of the silicon pyrometer. The algorithm consists of two sub-algorithms: (i A dynamic model is used to estimate the silicon temperature based on the graphite pyrometer, and (ii a lowpass filter and a highpass filter designed as complementary filters. The complementary filters are used to lowpass-filter the silicon pyrometer, highpass-filter the dynamic model output, and merge these filtered signals. Hence, the lowpass filter attenuates noise from the silicon pyrometer, while the graphite pyrometer and the dynamic model estimate those frequency components of the silicon temperature that are lost when lowpass-filtering the silicon pyrometer. The algorithm works well within a limited temperature range. To handle a larger temperature range, more research must be done to understand the process' nonlinear dynamics, and build this into the dynamic model.

  15. Influence of nanomechanical crystal properties on the comminution process of particulate solids in spiral jet mills.

    Science.gov (United States)

    Zügner, Sascha; Marquardt, Karin; Zimmermann, Ingfried

    2006-02-01

    Elastic-plastic properties of single crystals are supposed to influence the size reduction process of bulk materials during jet milling. According to Pahl [M.H. Pahl, Zerkleinerungstechnik 2. Auflage. Fachbuchverlag, Leipzig (1993)] and H. Rumpf: [Prinzipien der Prallzerkleinerung und ihre Anwendung bei der Strahlmahlung. Chem. Ing. Tech., 3(1960) 129-135.] fracture toughness, maximum strain or work of fracture for example are strongly dependent on mechanical parameters like hardness (H) and young's modulus of elasticity (E). In addition the dwell time of particles in a spiral jet mill proved to correlate with the hardness of the feed material [F. Rief: Ph. D. Thesis, University of Würzburg (2001)]. Therefore 'near-surface' properties have a direct influence on the effectiveness of the comminution process. The mean particle diameter as well as the size distribution of the ground product may vary significantly with the nanomechanical response of the material. Thus accurate measurement of crystals' hardness and modulus is essential to determine the ideal operational micronisation conditions of the spiral jet mill. The recently developed nanoindentation technique is applied to examine subsurface properties of pharmaceutical bulk materials, namely calcite, sodium ascorbate, lactose and sodium chloride. Pressing a small sized tip into the material while continuously recording load and displacement, characteristic diagrams are derived. The mathematical evaluation of the force-displacement-data allows for calculation of the hardness and the elastic modulus of the investigated material at penetration depths between 50-300 nm. Grinding experiments performed with a modified spiral jet mill (Type Fryma JMRS 80) indicate the strong impact of the elastic-plastic properties of a given substance on its breaking behaviour. The fineness of milled products produced at constant grinding conditions but with different crystalline powders varies significantly as it is dependent on the

  16. The fluid phenomena in the crystallization of the protein crystal

    International Nuclear Information System (INIS)

    Duan Li; Kang Qi

    2008-01-01

    This paper reports that an optical diagnostic system consisting of Mach–Zehnder interferometer with a phase shift device and image processor has been used for study of the kinetics of protein crystal growing process. The crystallization process of protein crystal by vapour diffusion is investigated. The interference fringes are observed in real time. The present experiment demonstrates that the diffusion and the sedimentation influence the crystallization of protein crystal which grows in solution, and the concentration capillary convection associated with surface tension occurs at the vicinity of free surface of the protein mother liquor, and directly affects on the outcome of protein crystallization. So far the detailed analysis and the important role of the fluid phenomena in protein crystallization have been discussed a little in both space- and ground-based crystal growth experiments. It is also found that these fluid phenomena affect the outcome of protein crystallization, regular growth, and crystal quality. This may explain the fact that many results of space-based investigation do not show overall improvement. (cross-disciplinary physics and related areas of science and technology)

  17. Role of BRIT in promoting radiation processing technology in India

    International Nuclear Information System (INIS)

    Bandi, L.N.

    2014-01-01

    Some of the major applications of radiation processing include: the sterilization of products such as medical devices to kill bacteria or in the case of food, hygienize the product; the treatment of export bulk commodities such as tropical fruits to extend shelf life by slowing the ripening process and inhibiting sprouting and to kill quarantine pests such as fruit flies. Radiation processing is a value addition process. Taking note of these benefits, Department of Atomic Energy, Government of India constituted Board of Radiation and Isotope Technology (BRIT) in March 1989 by carving it out from Bhabha Atomic Research Centre, Mumbai. The mandate given to BRIT was to extend commercial applications of radioisotopes and radiation in the areas of Health, Agriculture, Industry and Research without losing sight of societal obligations. So far Department of Atomic Energy has set up three demonstration plants, namely, Isomed, RPP, Vashi and Krushak for high, medium and low dose applications of radiation respectively. The safe and business like operation of these facilities amply demonstrated the embedded safety and commercial viability of this technology

  18. The influence of strong crystalline fields on QED-processes investigated using diamond crystals to crystals in $\\gamma, \\gamma$ colliders

    CERN Document Server

    Uggerhøj, Erik

    2002-01-01

    The very recent indications of Higgs-candidates at CERN have led to a strong interest in new types of facilities like high-energy photon colliders. This again leads to a search for strong high-energy gamma sources. In the present paper it is shown that single crystals are unique radiators due to the strong crystalline fields of 10/sup 12/ V /cm or more, in which incident particles move over very large distances (~100 mu m). Along axes, radiation emission and energy loss is enhanced more than two orders of magnitude. This dramatic effect loads to radiation cooling followed by capture to high-lying channeling states. The radiation is emitted in the forward angular cone of 40 mu rad or less. In the planar cases certain incident directions give hard photons with an intensity ~10 times the normal coherent bremsstrahlung. Therefore, in general, crystals turn out to be very interesting gamma -sources for photo production and coming gamma , gamma colliders. (10 refs).

  19. Evaluation of Brine Processing Technologies for Spacecraft Wastewater

    Science.gov (United States)

    Shaw, Hali L.; Flynn, Michael; Wisniewski, Richard; Lee, Jeffery; Jones, Harry; Delzeit, Lance; Shull, Sarah; Sargusingh, Miriam; Beeler, David; Howard, Jeanie; hide

    2015-01-01

    Brine drying systems may be used in spaceflight. There are several advantages to using brine processing technologies for long-duration human missions including a reduction in resupply requirements and achieving high water recovery ratios. The objective of this project was to evaluate four technologies for the drying of spacecraft water recycling system brine byproducts. The technologies tested were NASA's Forward Osmosis Brine Drying (FOBD), Paragon's Ionomer Water Processor (IWP), NASA's Brine Evaporation Bag (BEB) System, and UMPQUA's Ultrasonic Brine Dewatering System (UBDS). The purpose of this work was to evaluate the hardware using feed streams composed of brines similar to those generated on board the International Space Station (ISS) and future exploration missions. The brine formulations used for testing were the ISS Alternate Pretreatment and Solution 2 (Alt Pretreat). The brines were generated using the Wiped-film Rotating-disk (WFRD) evaporator, which is a vapor compression distillation system that is used to simulate the function of the ISS Urine Processor Assembly (UPA). Each system was evaluated based on the results from testing and Equivalent System Mass (ESM) calculations. A Quality Function Deployment (QFD) matrix was also developed as a method to compare the different technologies based on customer and engineering requirements.

  20. Layers And Processes In The Model Of Technological Postal System

    Directory of Open Access Journals (Sweden)

    Madleňáková Lucia

    2015-12-01

    Full Text Available The paper include important aspects of layer model of postal technological system such as makes the possibility to define rules for regulating, technical and technological requirements and interfaces to communicate with other postal systems. The current postal reform is mainly attributable to release of network access and ensuring full interoperability between technological systems. Not only to ensure the development and protection of competition but also in respect to the conservation of requirements to provide the universal service, which is the performance of public interest. There is a space here to examine the postal system, not only from a procedural point of view, but to be viewed as an open communication system. It is possible to find there the commonalities with other communication sector branches and to handle the technological postal system in more layers; similarly as the electronic communication systems are handled. Model of layer postal system, based not only on the processes but on layers functionality, will enable to identify communication protocols and interfaces determining interoperability. It also opens the question of appropriate regulation model.

  1. Integrated membrane distillation-crystallization: process design and cost estimations for seawater treatment and fluxes of single salt solutions

    NARCIS (Netherlands)

    Creusen, R.J.M.; Medevoort, J. van; Roelands, C.P.M.; Renesse van Duivenbode, J.A.D. van; Hanemaaijer, J.H.; Leerdam, R.C. van

    2013-01-01

    The goal of this research is to design an integrated membrane distillation-crystallization (MDC) process for desalination of seawater with pure water and dry salts as the only products. The process is based on a combination of membrane distillation (MD) and osmotic distillation (OD) steps with

  2. Advanced modeling of management processes in information technology

    CERN Document Server

    Kowalczuk, Zdzislaw

    2014-01-01

    This book deals with the issues of modelling management processes of information technology and IT projects while its core is the model of information technology management and its component models (contextual, local) describing initial processing and the maturity capsule as well as a decision-making system represented by a multi-level sequential model of IT technology selection, which acquires a fuzzy rule-based implementation in this work. In terms of applicability, this work may also be useful for diagnosing applicability of IT standards in evaluation of IT organizations. The results of this diagnosis might prove valid for those preparing new standards so that – apart from their own visions – they could, to an even greater extent, take into account the capabilities and needs of the leaders of project and manufacturing teams. The book is intended for IT professionals using the ITIL, COBIT and TOGAF standards in their work. Students of computer science and management who are interested in the issue of IT...

  3. HEALTH TECHNOLOGY ASSESSMENT, DELIBERATIVE PROCESS, AND ETHICALLY CONTESTED ISSUES.

    Science.gov (United States)

    Daniels, Norman; van der Wilt, Gert Jan

    2016-01-01

    Healthcare technology assessment (HTA) aims to support decisions as to which technologies should be used in which situations to optimize value. Because such decisions will create winners and losers, they are bound to be controversial. HTA, then, faces a dilemma: should it stay away from such controversies, remaining a source of incomplete advice and risking an important kind of marginalization, or should it enter the controversy? The question is a challenging one, because we lack agreement on principles that are fine grained enough to tell us what choices we should make. In this study, we will argue that HTA should take a stand on ethical issues raised by the technology that is being investigated. To do so, we propose adding a form of procedural justice to HTA to arrive at decisions that the public can regard as legitimate and fair. A fair process involves deliberation about the reasons, evidence, and rationales that are considered relevant to meeting population-health needs fairly. One important way to make sure that there is real deliberation about relevant reasons is to include a range of stakeholders in the deliberative process. To illustrate how such deliberation might work, we use the case of cochlear implants for deaf children.

  4. IR spectroscopy together with multivariate data analysis as a process analytical tool for in-line monitoring of crystallization process and solid-state analysis of crystalline product

    DEFF Research Database (Denmark)

    Pöllänen, Kati; Häkkinen, Antti; Reinikainen, Satu-Pia

    2005-01-01

    Fourier transform infra red (ATR-FTIR) spectroscopy provides valuable information on process, which can be utilized for more controlled crystallization processes. Diffuse reflectance Fourier transform infra red (DRIFT-IR) is applied for polymorphic characterization of crystalline product using X......Crystalline product should exist in optimal polymorphic form. Robust and reliable method for polymorph characterization is of great importance. In this work, infra red (IR) spectroscopy is applied for monitoring of crystallization process in situ. The results show that attenuated total reflection...... techniques provide the powerful tool for rapid evaluation of spectral data and also enable more reliable quantification of polymorphic composition of samples being mixtures of two or more polymorphs. This opens new perspectives for understanding crystallization processes and increases the level of safety...

  5. A combinaison of UV curing technology with ATL process

    Science.gov (United States)

    Balbzioui, I.; Hasiaoui, B.; Barbier, G.; L'hostis, G.; Laurent, F.; Ibrahim, A.; Durand, B.

    2017-10-01

    In order to reduce the time and the cost of manufacturing composite, UV curing technology combined with automated tape placement process (ATL) based on reverse approach by working with a fixed head was studied in this article. First, a brief description of the developed head placement is presented. Mechanical properties are then evaluated by varying process parameters, including compaction force and tape placement speed. Finally, a parametric study is carried out to identify suitable materials and process parameters to manufacture a photo composite material with high mechanical performances. The obtained results show that UV curing is a very good alternative for thermal polymerization because of its fast cure speed due to less dependency on temperature.

  6. Actinide solution processing at the Rocky Flats Environmental Technology Site

    International Nuclear Information System (INIS)

    1995-04-01

    The Department of Energy (DOE) has prepared an Environmental Assessment (EA), DOE/EA-1039, for radioactive solution removal and processing at Rocky Flats Environmental Technology Site, Golden, Colorado. The proposal for solution removal and processing is in response to independent safety assessments and an agreement with the State of Colorado to remove mixed residues at Rocky Flats and reduce the risk of future accidents. Monthly public meetings were held during the scoping and preparation of the EA. The scope of the EA included evaluations of alternative methods and locations of solution processing. A comment period from February 20, 1995 through March 21, 1995 was provided to the public and the State of Colorado to offer written comment on the EA. Comments were received from the State of Colorado and the U.S. Environmental Protection Agency. A response to the agency comments is included in the Final EA

  7. Crystallization of nuclear glass under a thermal gradient: application to the self-crucible produced in the skull melting process

    International Nuclear Information System (INIS)

    Delattre, O.

    2013-01-01

    In the context of the vitrification of high level nuclear waste, a new industrial process has been launched in 2010 at the La Hague factory: The skull melting process. This setup applies thermal gradients to the melt, which leads to the formation of a solid layer of glass: the 'self-crucible'. The question would be to know whether these thermal gradients have an impact or not on the crystallization behaviour of the considered glasses in the self crucible. In order to answer that question, the crystallization of two glass compositions of nuclear interest has been investigated with an image analysis based method in isothermal and thermal gradient heat treatments conditions. The isothermal experiments allow for the quantification (growth speed, nucleation, crystallized fraction) of the crystallization of apatites (660 C-900 C) and powellites (630 C-900 C). The comparison of the results obtained through these two types of experimentations allows us to conclude that there is no impact of the thermal gradient on the crystallization of the studied glass compositions. In order to complete the image analysis study (based on surfaces), in and ex situ microtomography experiments have been performed at ESRF (Grenoble) on the ID19 beamline. This study allowed us to follow the crystallization of apatites in a simplified glass and to confirm the reliability of the image analysis method based on the analysis of surfaces. (author) [fr

  8. Development of photonic crystals using sol-gel process for high power laser applications

    International Nuclear Information System (INIS)

    Benoit, Florence

    2015-01-01

    Three-dimensional photonic crystals (PCs) are periodic materials with a modulated refractive index on a length scale close to the light wavelength. This optical property allows the preparation of specific optical components like highly reflective mirrors. Moreover, these structured materials might have a high laser-induced damage threshold (LIDT) in the sub-nanosecond range compared to multilayered dielectric mirrors. This property is obtained because only one high LIDT material (silica) is used. In this work, we present the development of 3D PCs with narrow-sized colloidal silica particles, prepared by sol-gel process and deposited with Langmuir-Blodgett technique. Different syntheses routes have been investigated and compared regarding the optical properties of the PCs. A numerical model based on an ideal opal network including defect influence is used to explain these experimental results. (author) [fr

  9. An Effective Deuterium Exchange Method for Neutron Crystal Structure Analysis with Unfolding-Refolding Processes.

    Science.gov (United States)

    Kita, Akiko; Morimoto, Yukio

    2016-02-01

    A method of hydrogen/deuterium (H/D) exchange with an unfolding-refolding process has been applied to hen egg-white lysozyme (HWL), and accurate evaluation of its deuteration was carried out by time-of-flight mass spectroscopy. Neutron crystallography requires a suitable crystal with enough deuterium exchanged in the protein to decrease incoherent scattering from hydrogens. It is very expensive to prepare a fully deuterated protein, and therefore a simple H/D exchange technique is desirable for this purpose. Acid or base addition to protein solutions with heating effectively increased the number of deuterium up to more than 20 % of that of all hydrogen atoms, and refolded structures were determined by X-ray structure analysis at 1.8 Å resolution. Refolded HWL had increased deuterium content in its protein core and its native structure, determined at atomic resolution, was fully preserved.

  10. In situ diagnostics of the crystal-growth process through neutron imaging

    DEFF Research Database (Denmark)

    Tremsin, Anton S.; Makowska, Malgorzata Grazyna; Perrodin, Didier

    2016-01-01

    Neutrons are known to be unique probes in situations where other types of radiation fail to penetrate samples and their surrounding structures. In this paper it is demonstrated how thermal and cold neutron radiography can provide time-resolved imaging of materials while they are being processed (e...... in concentration of one of the elements with a sufficient neutron attenuation cross section. Tomographic imaging of the BaBrCl:0.1% Eu sample reveals a strong correlation between crystal fractures and Eu-deficient clusters. The results of these experiments demonstrate the unique capabilities of neutron imaging......, as limited by the resolution of the present experiments). It is also demonstrated that the dopant concentration can be quantified even for very low concentration levels (∼ 0.1%) in 10 mm thick samples. The interface between the solid and liquid phases can also be imaged, provided there is a sufficient change...

  11. Commentary: how can technology help us understand the communication process?

    Science.gov (United States)

    Keyton, Joann

    2012-08-01

    In this commentary, the author reflects on the articles chosen for the special section on communications analysis. These articles problematize communication and raise an interesting set of questions for both human factors and communication scholars to ponder. In the end, both sets of scholars seek the same goal: How do we better examine communication to improve it? Problematizing communication requires scholars to challenge their fundamental assumptions about the phenomenon as well as to tease out the distinctions of methodological approaches typically used by both human factors and communication scholars. Human factors scholars tend to favor forms of communication in which technology or task roles control who can communicate and how. Communication scholars tend to favor contexts in which information flows more freely with fewer explicit restrictions. Creating opportunities to collaborate in research on the communication process may create the best understanding of technology that can better serve our understanding of communication.

  12. Technological Innovation: Concept, Process, Typology and Implications in the Economy

    Directory of Open Access Journals (Sweden)

    Mihaela DIACONU

    2011-10-01

    Full Text Available Growing interest worldwide to boost innovation in business sector activities, especially the technology, is intended to maintain or increase national economic competitiveness, inclusively as an effect of awareness concerning the effects resulting from economic activity on consumption of resources and environment, which requires design of new patterns of production and consumption. In this paper we review the most important contributions in the literature in terms of the implications of technological innovation in the economy, at the microand macroeconomic level, viewing the organization's ability to generate new ideas in support of increasing production, employment and environmental protection, starting from the concepts of innovation, innovation process and, respectively, from the innovation typology analysis.

  13. Nuclear reactor fuel cycle technology with pyroelectrochemical processes

    International Nuclear Information System (INIS)

    Skiba, O.V.; Maershin, A.A.; Bychkov, A.V.; Zhdanov, A.N.; Kislyj, V.A.; Vavilov, S.K.; Babikov, L.G.

    1999-01-01

    A group of dry technologies and processes of vibro-packing granulated fuel in combination with unique properties of vibro-packed FEs make it possible to implement a new comprehensive approach to the fuel cycle with plutonium fuel. Testing of a big number of FEs with vibro-packed U-Pu oxide fuel in the BOR-60 reactor, successful testing of experimental FSAs in the BN-600 rector, reliable operation of the experimental and research complex facilities allow to make the conclusion about a real possibility to develop a safe, economically beneficial U-Pu fuel cycle based on the technologies enumerated above and to use both reactor-grade and weapon-grade plutonium in nuclear reactors with a reliable control and accounting system [ru

  14. Missile signal processing common computer architecture for rapid technology upgrade

    Science.gov (United States)

    Rabinkin, Daniel V.; Rutledge, Edward; Monticciolo, Paul

    2004-10-01

    Interceptor missiles process IR images to locate an intended target and guide the interceptor towards it. Signal processing requirements have increased as the sensor bandwidth increases and interceptors operate against more sophisticated targets. A typical interceptor signal processing chain is comprised of two parts. Front-end video processing operates on all pixels of the image and performs such operations as non-uniformity correction (NUC), image stabilization, frame integration and detection. Back-end target processing, which tracks and classifies targets detected in the image, performs such algorithms as Kalman tracking, spectral feature extraction and target discrimination. In the past, video processing was implemented using ASIC components or FPGAs because computation requirements exceeded the throughput of general-purpose processors. Target processing was performed using hybrid architectures that included ASICs, DSPs and general-purpose processors. The resulting systems tended to be function-specific, and required custom software development. They were developed using non-integrated toolsets and test equipment was developed along with the processor platform. The lifespan of a system utilizing the signal processing platform often spans decades, while the specialized nature of processor hardware and software makes it difficult and costly to upgrade. As a result, the signal processing systems often run on outdated technology, algorithms are difficult to update, and system effectiveness is impaired by the inability to rapidly respond to new threats. A new design approach is made possible three developments; Moore's Law - driven improvement in computational throughput; a newly introduced vector computing capability in general purpose processors; and a modern set of open interface software standards. Today's multiprocessor commercial-off-the-shelf (COTS) platforms have sufficient throughput to support interceptor signal processing requirements. This application

  15. Process design and simulation for optimizing the oxygen concentration in Czochralski-grown single-crystal silicon

    International Nuclear Information System (INIS)

    Jung, Y. J.; Kim, W. K.; Jung, J. H.

    2014-01-01

    The highest-concentration impurity in a single-crystal silicon ingot is oxygen, which infiltrates the ingot during growth stage. This oxygen adversely affects the wafer is quality. This study was aimed at finding an optimal design for the Czochralski (Cz) process to enable high-quality and low cost (by reducing power consumption) wafer production by controlling the oxygen concentration in the silicon ingots. In the Cz process, the characteristics of silicon ingots during crystallization are greatly influenced by the design and the configuration of the hot zone, and by crystallization rate. In order to identify process conditions for obtaining an optimal oxygen concentration of 11 - 13 ppma (required for industrial-grade ingots), designed two shield shapes for the hot zone. Furthermore, oxygen concentrations corresponding to these two shapes were compared by evaluating each shape at five different production speeds. In addition, simulations were performed to identify the optimal shield design for industrial applications.

  16. Process design and simulation for optimizing the oxygen concentration in Czochralski-grown single-crystal silicon

    Energy Technology Data Exchange (ETDEWEB)

    Jung, Y. J.; Kim, W. K.; Jung, J. H. [Yeungnam University, Gyeongsan (Korea, Republic of)

    2014-08-15

    The highest-concentration impurity in a single-crystal silicon ingot is oxygen, which infiltrates the ingot during growth stage. This oxygen adversely affects the wafer is quality. This study was aimed at finding an optimal design for the Czochralski (Cz) process to enable high-quality and low cost (by reducing power consumption) wafer production by controlling the oxygen concentration in the silicon ingots. In the Cz process, the characteristics of silicon ingots during crystallization are greatly influenced by the design and the configuration of the hot zone, and by crystallization rate. In order to identify process conditions for obtaining an optimal oxygen concentration of 11 - 13 ppma (required for industrial-grade ingots), designed two shield shapes for the hot zone. Furthermore, oxygen concentrations corresponding to these two shapes were compared by evaluating each shape at five different production speeds. In addition, simulations were performed to identify the optimal shield design for industrial applications.

  17. Anodic processes in the chemical and electrochemical etching of Si crystals in acid-fluoride solutions: Pore formation mechanism

    Energy Technology Data Exchange (ETDEWEB)

    Ulin, V. P.; Ulin, N. V.; Soldatenkov, F. Yu., E-mail: f.soldatenkov@mail.ioffe.ru [Ioffe Physical–Technical Institute (Russian Federation)

    2017-04-15

    The interaction of heavily doped p- and n-type Si crystals with hydrofluoric acid in the dark with and without contact with metals having greatly differing work functions (Ag and Pd) is studied. The dependences of the dissolution rates of Si crystals in HF solutions that contain oxidizing agents with different redox potentials (FeCl{sub 3}, V{sub 2}O{sub 5} and CrO{sub 3}) on the type and level of silicon doping are determined. Analysis of the experimental data suggests that valence-band holes in silicon are not directly involved in the anodic reactions of silicon oxidation and dissolution and their generation in crystals does not limit the rate of these processes. It is also shown that the character and rate of the chemical process leading to silicon dissolution in HF-containing electrolytes are determined by the interfacial potential attained at the semiconductor–electrolyte interface. The mechanism of electrochemical pore formation in silicon crystals is discussed in terms of selfconsistent cooperative reactions of nucleophilic substitution between chemisorbed fluorine anions and coordination- saturated silicon atoms in the crystal subsurface layer. A specific feature of these reactions for silicon crystals is that vacant nonbonding d{sup 2}sp{sup 3} orbitals of Si atoms, associated with sixfold degenerate states corresponding to the Δ valley of the conduction band, are involved in the formation of intermediate complexes. According to the suggested model, the pore-formation process spontaneously develops in local regions of the interface under the action of the interfacial potential in the adsorption layer and occurs as a result of the detachment of (SiF{sub 2}){sub n} polymer chains from the crystal. Just this process leads to the preferential propagation of pores along the <100> crystallographic directions. The thermodynamic aspects of pore nucleation and the effect of the potential drop across the interface, conduction type, and free-carrier concentration

  18. Trapping technology for gaseous fission products from voloxidation process

    International Nuclear Information System (INIS)

    Shin, Jin Myeong; Park, J. J.; Park, G. I.; Jung, I. H.; Lee, H. H.; Kim, G. H.; Yang, M. S.

    2005-05-01

    The objective of this report is to review the different technologies for trapping the gaseous wastes containing Cs, Ru, Tc, 14 C, Kr, Xe, I and 3 H from a voloxidation process. Based on literature reviews and KAERI's experimental results on the gaseous fission products trapping, appropriate trapping method for each fission product has been selected considering process reliability, simplicity, decontamination factor, availability, and disposal. Specifically, the most promising trapping method for each fission product has been proposed for the development of the INL off-gas trapping system. A fly ash filter is proposed as a trapping media for a cesium trapping unit. In addition, a calcium filter is proposed as a trapping media for ruthenium, technetium, and 14 C trapping unit. In case of I trapping unit, AgX is proposed. For Kr and Xe, adsorption on solid is proposed. SDBC (Styrene Divinyl Benzene Copolymer) is also proposed as a conversion media to HTO for 3 H. This report will be used as a useful means for analyzing the known trapping technologies and help selecting the appropriate trapping methods for trapping volatile and semi-volatile fission products, long-lived fission products, and major heat sources generated from a voloxidation process. It can also be used to design an off-gas treatment system

  19. Staging Co-design Processes for Self-care Technologies

    DEFF Research Database (Denmark)

    Brodersen, Søsser Grith Kragh; Lindegaard, Hanne

    2016-01-01

    field studies in people’s homes and discuss how to stage design processes with the people who are actually going to use the self-care technologies—not only end-users, but also many other actors, such as relatives, caregivers, and municipality and company staff. Specifically, we describe how challenges......Many new healthcare technologies are currently being implemented in people’s homes in order to facilitate self-care. Socially innovative design is challenging, since it requires an intimate understanding of people’s abilities and daily practices. In this article, we highlight the need to perform...

  20. Instrument maintenance of ultrasonic influences parameters measurement in technological processes

    Directory of Open Access Journals (Sweden)

    Tomal V. S.

    2008-04-01

    Full Text Available The contact and non-contact vibration meters for intermittent and continuous control of the vibration amplitude in the ultrasonic technological equipment have been developed. And in order to estimate the cavitation intensity in liquids the authors have developed cavitation activity indicators and cavitation sensitivity meters, allowing to measure the magnitude of the signal level in the range of maximum spectral density of cavitation noise. The developed instruments allow to improve the quality of products, reduce the defect rate and power consumption of equipment by maintaining optimum conditions of the process.

  1. The processing technology of bread crumbs sterilization by irradiation

    International Nuclear Information System (INIS)

    Zhu Jiating; Li Zhengkui; Zhao Yongfu; Zhang Weidong; Jin Jie; Wu Lei; Wang Xinghai

    2003-01-01

    The processing technology of bread crumbs sterilization by irradiation was studied. The results demonstrated that dose heterogeneity had osculatory connection with pile height and turning, sterilization effect had positive correlation with the irradiation dose and negative correlation with colour. Compared with the CK, the content of crud protein, fat, carbohydrate, microelement and amino acid in irradiated bread crumbs had no obvious change. It is recommended that the range of best sterilization dose be 6-10 kGy and the shelf time of bread crumbs be extended to one year

  2. Novel casting processes for single-crystal turbine blades of superalloys

    Science.gov (United States)

    Ma, Dexin

    2018-03-01

    This paper presents a brief review of the current casting techniques for single-crystal (SC) blades, as well as an analysis of the solidification process in complex turbine blades. A series of novel casting methods based on the Bridgman process were presented to illustrate the development in the production of SC blades from superalloys. The grain continuator and the heat conductor techniques were developed to remove geometry-related grain defects. In these techniques, the heat barrier that hinders lateral SC growth from the blade airfoil into the extremities of the platform is minimized. The parallel heating and cooling system was developed to achieve symmetric thermal conditions for SC solidification in blade clusters, thus considerably decreasing the negative shadow effect and its related defects in the current Bridgman process. The dipping and heaving technique, in which thinshell molds are utilized, was developed to enable the establishment of a high temperature gradient for SC growth and the freckle-free solidification of superalloy castings. Moreover, by applying the targeted cooling and heating technique, a novel concept for the three-dimensional and precise control of SC growth, a proper thermal arrangement may be dynamically established for the microscopic control of SC growth in the critical areas of large industrial gas turbine blades.

  3. DUPIC nuclear fuel manufacturing and process technology development

    Energy Technology Data Exchange (ETDEWEB)

    Yang, Myung Seung; Park, J. J.; Lee, J. W. [and others

    2000-05-01

    In this study, DUPIC fuel fabrication technology and the active fuel laboratory were developed for the study of spent nuclear fuel. A new nuclear fuel using highly radioactive nuclear materials can be studied at the active fuel laboratory. Detailed DUPIC fuel fabrication process flow was developed considering the manufacturing flow, quality control process and material accountability. The equipment layout of about twenty DUPIC equipment at IMEF M6 hot cell was established for the minimization of the contamination during DUPIC processes. The characteristics of the SIMFUEL powder and pellets was studied in terms of milling conditions. The characteristics of DUPIC powder and pellet was studied by using 1 kg of spent PWR fuel at PIEF nr.9405 hot cell. The results were used as reference process conditions for following DUPIC fuel fabrication at IMEF M6. Based on the reference fabrication process conditions, the main DUPIC pellet fabrication campaign has been started at IMEF M6 using 2 kg of spent PWR fuel since 2000 January. As of March 2000, about thirty DUPIC pellets were successfully fabricated.

  4. DUPIC nuclear fuel manufacturing and process technology development

    International Nuclear Information System (INIS)

    Yang, Myung Seung; Park, J. J.; Lee, J. W.

    2000-05-01

    In this study, DUPIC fuel fabrication technology and the active fuel laboratory were developed for the study of spent nuclear fuel. A new nuclear fuel using highly radioactive nuclear materials can be studied at the active fuel laboratory. Detailed DUPIC fuel fabrication process flow was developed considering the manufacturing flow, quality control process and material accountability. The equipment layout of about twenty DUPIC equipment at IMEF M6 hot cell was established for the minimization of the contamination during DUPIC processes. The characteristics of the SIMFUEL powder and pellets was studied in terms of milling conditions. The characteristics of DUPIC powder and pellet was studied by using 1 kg of spent PWR fuel at PIEF nr.9405 hot cell. The results were used as reference process conditions for following DUPIC fuel fabrication at IMEF M6. Based on the reference fabrication process conditions, the main DUPIC pellet fabrication campaign has been started at IMEF M6 using 2 kg of spent PWR fuel since 2000 January. As of March 2000, about thirty DUPIC pellets were successfully fabricated

  5. Active Shop Scheduling Of Production Process Based On RFID Technology

    Directory of Open Access Journals (Sweden)

    Cuihua Chao

    2016-01-01

    Full Text Available In industry 4.0 environment, intelligent technology is almost applied to all parts of the manufacturing process, such as process design, job shop scheduling, etc.. This paper presents an efficient approach to job shop scheduling actively by using RFID to collect real-time manufacturing data. Identified the workpiece by RFID which needs to be machined, it can “ask for” the resource actively for the following process. With these active asking-for strategy, a double genetically encoded improved genetic algorithm is proposed for achieving active job shop scheduling solution during the actual manufacturing process. A case was used to evaluate its effectiveness. Meanwhile, , it can effectively and actively carry out job shop scheduling and has much better convergence effect comparing with basic genetic algorithm. And the job shop scheduler in management center can use the proposed algorithm to get the satisfied scheduling result timely by reducing waiting time and making begin time earlier during transmission between manufacturing process, which makes the scheduling result feasible and accurate.

  6. Research on application of computer technologies in jewelry process

    Directory of Open Access Journals (Sweden)

    Junbo Xia

    2017-06-01

    Full Text Available Jewelry production is a process of precious raw materials and low losses in processing. The traditional manual mode is unable to meet the needs of enterprises in reality, while the involvement of computer technology can just solve this practical problem. At present, the problem of restricting the application for computer in jewelry production is mainly a failure to find a production model that can serve the whole industry chain with the computer as the core of production. This paper designs a “synchronous and diversified” production model with “computer aided design technology” and “rapid prototyping technology” as the core, and tests with actual production cases, and achieves certain results, which are forward-looking and advanced.

  7. Centralisation of informatics (more effective processes via using new technologies)

    International Nuclear Information System (INIS)

    Cocher, L.

    2004-01-01

    In this paper author deals with next problems of Slovenske elektrarne, Plc (SE): - Centralisation and optimisation of informatics management; - New technologies within Integrated Informatics System IIS-SE: presentation of preliminary Project of 2 nd generation IIS-SE; - Centralisation of the selected data processing. At the present the intensive process of restructuring is taking place in SE, Plc, focused on increasing of the effectiveness of the pursued activities. In connection with this the Informatics section solves two projects: More effective self-management and human resources; Change of Informatics system architecture from decentralised to the centralised ones with an aim to consolidate all information and to make new conditions for higher mobility. (author)

  8. Environmental assessment for the Processing and Environmental Technology Laboratory (PETL)

    International Nuclear Information System (INIS)

    1995-09-01

    The U.S. Department of Energy (DOE) has prepared an environmental assessment (EA) on the proposed Processing and Environmental Technology Laboratory (PETC) at Sandia National Laboratories/New Mexico (SNL/NM). This facility is needed to integrate, consolidate, and enhance the materials science and materials process research and development (R ampersand D) currently in progress at SNL/NM. Based on the analyses in the EA, DOE has determined that the proposed action is not a major Federal action significantly affecting the quality of the human environment within the meaning of the National Environmental Policy Act (NEPA) of 1969. Therefore, an environmental impact statement is not required, and DOE is issuing this Finding of No Significant Impact (FONSI)

  9. Virtual Welded - Joint Design Integrating Advanced Materials and Processing Technology

    Energy Technology Data Exchange (ETDEWEB)

    Yang, Zhishang; Ludewig, Howard W.; Babu, S. Suresh

    2005-06-30

    Virtual Welede-Joint Design, a systematic modeling approach, has been developed in this project to predict the relationship of welding process, microstructure, properties, residual stress, and the ultimate weld fatique strength. This systematic modeling approach was applied in the welding of high strength steel. A special welding wire was developed in this project to introduce compressive residual stress at weld toe. The results from both modeling and experiments demonstrated that more than 10x fatique life improvement can be acheived in high strength steel welds by the combination of compressive residual stress from the special welding wire and the desired weld bead shape from a unique welding process. The results indicate a technology breakthrough in the design of lightweight and high fatique performance welded structures using high strength steels.

  10. The evolution of waste management processes and technologies in BNFL

    International Nuclear Information System (INIS)

    Asquith, R. W.; Fairhall, G. A.

    1997-01-01

    The treatment of wastes arising from BNFL's nuclear fuel cycle operations can be traced through a number of phases. The first was the development of vitrification and cementation for fresh arising and plants are now in operation. To handle the mixed, heterogeneous intermediate level wastes, retrieval, segregation and robust treatment processes are at an advanced stage of development, with all plants to be operational from 2002. BNFL is focusing attention on reducing waste management lifetime costs including reducing waste volumes of source. Technologies aimed at significant reductions are now being developed. The final phase, now in progress, recognizes the need for an integrated approach to advanced fuel cycle processes which incorporates BNFL holistic concept. (author) 6 refs., 1 fig

  11. Environmental assessment for the Processing and Environmental Technology Laboratory (PETL)

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1995-09-01

    The U.S. Department of Energy (DOE) has prepared an environmental assessment (EA) on the proposed Processing and Environmental Technology Laboratory (PETC) at Sandia National Laboratories/New Mexico (SNL/NM). This facility is needed to integrate, consolidate, and enhance the materials science and materials process research and development (R&D) currently in progress at SNL/NM. Based on the analyses in the EA, DOE has determined that the proposed action is not a major Federal action significantly affecting the quality of the human environment within the meaning of the National Environmental Policy Act (NEPA) of 1969. Therefore, an environmental impact statement is not required, and DOE is issuing this Finding of No Significant Impact (FONSI).

  12. Effect of surfactants or a water soluble polymer on the crystal transition of clarithromycin during a wet granulation process.

    Science.gov (United States)

    Nozawa, Kenji; Iwao, Yasunori; Noguchi, Shuji; Itai, Shigeru

    2015-11-10

    To generate products containing a stable form of clarithromycin (CAM) (form II) regardless of the initial crystal form of CAM or type of granulation solvent, the effects of five surfactants, or a water-soluble polymer (macrogol 400) were determined on the crystal transition of CAM. The metastable form (form I) was kneaded with water, after adding surfactants, or a water-soluble polymer. Form II was also kneaded with ethanol, after adding the same additives. The resulting samples were analyzed by powder X-ray diffraction. Form I was completely converted to form II by a wet granulation using water with additives bearing polyoxyethylene chains such as polysorbate 80 (PS80), polyoxyl 40 stearate or macrogol 400. The granulation of the form II using ethanol with these additives did not result in a crystal transition to form I. Furthermore, CAM tablets were manufactured using granules with PS80, and these crystal forms and dissolution behaviors were investigated. As a result, the wet granulation of CAM with PS80 gave CAM tablets containing only form II and PS80 did not have any adverse effects on tablet characteristics. Therefore, these data suggests that the crystal form of CAM can be controlled to be form II using a wet granulation process with additives bearing polyoxyethylene chains regardless of the initial crystal form of CAM or type of granulation solvent. Copyright © 2015 Elsevier B.V. All rights reserved.

  13. Crystal Structure of the HEAT Domain from the Pre-mRNA Processing Factor Symplekin

    Energy Technology Data Exchange (ETDEWEB)

    Kennedy, Sarah A.; Frazier, Monica L.; Steiniger, Mindy; Mast, Ann M.; Marzluff, William F.; Redinbo, Matthew R.; (UNC)

    2010-09-30

    The majority of eukaryotic pre-mRNAs are processed by 3'-end cleavage and polyadenylation, although in metazoa the replication-dependent histone mRNAs are processed by 3'-end cleavage but not polyadenylation. The macromolecular complex responsible for processing both canonical and histone pre-mRNAs contains the {approx} 1160-residue protein Symplekin. Secondary-structural prediction algorithms identified putative HEAT domains in the 300 N-terminal residues of all Symplekins of known sequence. The structure and dynamics of this domain were investigated to begin elucidating the role Symplekin plays in mRNA maturation. The crystal structure of the Drosophila melanogaster Symplekin HEAT domain was determined to 2.4 {angstrom} resolution with single-wavelength anomalous dispersion phasing methods. The structure exhibits five canonical HEAT repeats along with an extended 31-amino-acid loop (loop 8) between the fourth and fifth repeat that is conserved within closely related Symplekin sequences. Molecular dynamics simulations of this domain show that the presence of loop 8 dampens correlated and anticorrelated motion in the HEAT domain, therefore providing a neutral surface for potential protein-protein interactions. HEAT domains are often employed for such macromolecular contacts. The Symplekin HEAT region not only structurally aligns with several established scaffolding proteins, but also has been reported to contact proteins essential for regulating 3'-end processing. Together, these data support the conclusion that the Symplekin HEAT domain serves as a scaffold for protein-protein interactions essential to the mRNA maturation process.

  14. Minimally Processed Functional Foods: Technological and Operational Pathways.

    Science.gov (United States)

    Rodgers, Svetlana

    2016-10-01

    This paper offers a concise review of technical and operational concepts underpinning commercialization of minimally processed functional foods (FFs), foods with fresh-like qualities commanding premium prices. The growing number of permitted nutritional content/health claims, many of which relate to well-being, coupled with emerging extraction and food processing technologies offers new exciting opportunities for small and medium size enterprises (SMEs) specializing in fresh produce to play an active role in the health market. Supporting SMEs, governments could benefit from savings in healthcare costs and value creation in the economy. Consumers could benefit from novel FF formats such as refrigerated RTE (ready-to-eat) meals, a variety of fresh-like meat-, fish-, and egg-based products, fresh-cut fruits and vegetables, cereal-based fermented foods and beverages. To preserve these valuable commodities, mild biological (enzymatic treatment, fermentation and, bio-preservation) and engineering solutions are needed. The latter include nonthermal techniques such as high-pressure treatment, cook-chill, sous-vide, mirco-encapsulation, vacuum impregnation and others. "De-constructive" culinary techniques such as 3D food printing and molecular gastronomy as well as developments in nutrigenomics and digital technologies facilitate novel product formats, personalization and access to niche markets. In the operational sense, moving from nourishment to health improvement demands a shift from defensive market-oriented to offensive market-developing strategies including collaborative networks with research organizations. © 2016 Institute of Food Technologists®.

  15. Efficient Separations and Processing Crosscutting Program. Technology summary

    International Nuclear Information System (INIS)

    1995-06-01

    The Efficient Separations and Processing (ESP) Crosscutting Program was created in 1991 to identify, develop, and perfect separations technologies and processes to treat wastes and address environmental problems throughout the DOE Complex. The ESP funds several multi-year tasks that address high-priority waste remediation problems involving high-level, low-level, transuranic, hazardous, and mixed (radioactive and hazardous) wastes. The ESP supports applied research and development (R and D) leading to demonstration or use of these separations technologies by other organizations within DOE-EM. Treating essentially all DOE defense wastes requires separation methods that concentrate the contaminants and/or purify waste streams for release to the environment or for downgrading to a waste form less difficult and expensive to dispose of. Initially, ESP R and D efforts focused on treatment of high-level waste (HLW) from underground storage tanks (USTs) because of the potential for large reductions in disposal costs and hazards. As further separations needs emerge and as waste management and environmental restoration priorities change, the program has evolved to encompass the breadth of waste management and environmental remediation problems

  16. Using information technology to support knowledge conversion processes

    Directory of Open Access Journals (Sweden)

    2001-01-01

    Full Text Available One of the main roles of Information Technology in Knowledge Management programs is to accelerate the speed of knowledge transfer and creation. The Knowledge Management tools intend to help the processes of collecting and organizing the knowledge of groups of individuals in order to make this knowledge available in a shared base. Due to the largeness of the concept of knowledge, the software market for Knowledge Management seems to be quite confusing. Technology vendors are developing different implementations of the Knowledge Management concepts in their software products. Because of the variety and quantity of Knowledge Management tools available on the market, a typology may be a valuable aid to organizations that are looking for answers to specific needs. The objective of this article is to present guidelines that help to design such a typology. Knowledge Management solutions such as intranet systems, Electronic Document Management (EDM, groupware, workflow, artificial intelligence-based systems, Business Intelligence (BI, knowledge map systems, innovation support, competitive intelligence tools and knowledge portals are discussed in terms of their potential contributions to the processes of creating, registering and sharing knowledge. A number of Knowledge Management tools (Lotus Notes, Microsoft Exchange, Business Objects, Aris Toolset, File Net, Gingo, Vigipro, Sopheon have been checked. The potential of each category of solutions to support the transfer of tacit and/or explicit knowledge and to facilitate the knowledge conversion spiral in the sense of Nonaka and Takeuchi (1995 is discussed.

  17. Use of radiation processing technology gradually expands in industry

    International Nuclear Information System (INIS)

    Anon.

    1989-01-01

    The use of radioisotopes and radiation is expanding in the fields of industries and medicine with a high potentiality of the application to environmental protection. The technology transfer on the use of isotopes and radiation is progressing in the framework of international cooperation. But the industry has maintained wait and see attitude on the commercialization of food irradiation. Such present features were the highlight in the 19th Japan Conference on Radiation and Radioisotopes held on November 14-16. 72 papers from 19 countries were presented and discussed in 13 sessions. The progress of accelerator technology has contributed to the expansion of radiation processing market. The importance of the application of isotopes and radiation to environmental protection has been gradually acknowledged, and the electron beam treatment of flue gas for acid rain abatement and the elimination of chlorinated ethylene from drinking water were discussed. Drastic change has not been seen in the climate of food irradiation, however there are several positive indicators which support the prediction of slow but steady progress in the commercialization of the process and the trade of irradiated foods. (K.I.)

  18. Initial crystallization and growth in melt processing of large-domain YBa2Cu3Ox for magnetic levitation

    International Nuclear Information System (INIS)

    Shi, D.

    1994-10-01

    Crystallization temperature in YBa 2 Cu 3 O x (123) during peritectic reaction has been studied by differential thermal analysis (DTA) and optical microscopy. It has been found that YBa 2 Cu 3 O x experiences partial melting near 1,010 C during heating while crystallization takes place at a much lower temperature range upon cooling indicating a delayed nucleation process. A series of experiments have been conducted to search for the initial crystallization temperature in the Y 2 BaCuO x + liquid phase field. The authors have found that the slow-cool period (1 C/h) for the 123 grain texturing can start at as low as 960 C. This novel processing has resulted in high-quality, large-domain, strongly pinned 123 magnetic levitators

  19. FOOD PROCESSING TECHNOLOGY AS A MEDIATOR OF FUNCTIONALITY. STRUCTURE-PROPERTY-PROCESS RELATIONSHIPS

    Directory of Open Access Journals (Sweden)

    Ester Betoret

    2015-02-01

    Full Text Available During the last years, the food industry has been facing technical and economic changes both in society and in the food processing practices, paying high attention to food products that meet the consumers´ demands. In this direction, the study areas in food process and products have evolved mainly from safety to other topics such as quality, environment or health. The improvement of the food products is now directed towards ensuring nutritional and specific functional benefits. Regarding the processes evolution, they are directed to ensure the quality and safety of environmentally friendly food products produced optimizing the use of resources, minimally affecting or even enhancing their nutritional and beneficial characteristics. The product structure both in its raw form and after processing plays an important role maintaining, enhancing and delivering the bioactive compounds in the appropriate target within the organism. The aim of this review is to make an overview on some synergistic technologies that can constitute a technological process to develop functional foods, enhancing the technological and/or nutritional functionality of the food products in which they are applied. More concretely, the effect of homogenization, vacuum impregnation and drying operations on bioactive compounds have been reviewed, focusing on the structure changes produced and its relationship on the product functionality, as well as on the parameters and the strategies used to quantify and increase the achieved functionality.

  20. Developing a model for assessing biomass processing technologies within a local biomass processing depot.

    Science.gov (United States)

    Bals, Bryan D; Dale, Bruce E

    2012-02-01

    One solution to the supply chain challenges of cellulosic biofuels is a network of local biomass processing depots (LBPDs) that can produce stable, dense, intermediate commodities and valuable co-products prior to shipping to a refinery. A techno-economic model of an LBPD facility that could incorporate multiple technologies and products was developed in Microsoft Excel to be used to economically and environmentally evaluate potential LBPD systems. In this study, three technologies (ammonia fiber expansion or AFEX™ pretreatment, fast pyrolysis, and leaf protein processing) were assessed for profitability. Pyrolysis was slightly profitable under the base conditions, leaf protein processing was highly unprofitable, and AFEX was profitable if biomass drying was not required. This model can be adapted to multiple feedstocks and end uses, including both economic and environmental modeling. Copyright © 2011 Elsevier Ltd. All rights reserved.

  1. A Technological Comparison of Six Processes for the Production of Reduction-Grade Alumina from Non-Bauxitic Raw Materials

    Science.gov (United States)

    Bengtson, K. B.

    The U. S. Bureau of Mines, by means of a contract with Kaiser Engineers and with Kaiser Aluminum & Chemical Corporation as a subcontractor, has sponsored a technological and an economic evaluation of six candidate processes for the manufacture of alumina from certain U. S. raw materials other than bauxite. This paper describes each process. Flow diagrams and the total energy requirement for each process are included. Important characteristics affecting the economics of producing alumina by each process are discussed, and some presently unsolved technical problems are identified. The extraction of alumina from clay via hydrochloric acid with iron separation by solvent extraction, and the crystallization of intermediate AlCl3·6H2O through the introduction of HCl gas into the pregnant mother liquor, appears to be technically feasible and the most attractive of the six raw material/process combinations.

  2. Technical Reviews on Pattern Recognition in Process Analytical Technology

    International Nuclear Information System (INIS)

    Kim, Jong Yun; Choi, Yong Suk; Ji, Sun Kyung; Park, Yong Joon; Song, Kyu Seok; Jung, Sung Hee

    2008-12-01

    Pattern recognition is one of the first and the most widely adopted chemometric tools among many active research area in chemometrics such as design of experiment(DoE), pattern recognition, multivariate calibration, signal processing. Pattern recognition has been used to identify the origin of a wine and the time of year that the vine was grown by using chromatography, cause of fire by using GC/MS chromatography, detection of explosives and land mines, cargo and luggage inspection in seaports and airports by using a prompt gamma-ray activation analysis, and source apportionment of environmental pollutant by using a stable isotope ratio mass spectrometry. Recently, pattern recognition has been taken into account as a major chemometric tool in the so-called 'process analytical technology (PAT)', which is a newly-developed concept in the area of process analytics proposed by US Food and Drug Administration (US FDA). For instance, identification of raw material by using a pattern recognition analysis plays an important role for the effective quality control of the production process. Recently, pattern recognition technique has been used to identify the spatial distribution and uniformity of the active ingredients present in the product such as tablet by transforming the chemical data into the visual information

  3. Cogeneration Technology Alternatives Study (CTAS). Volume 3: Industrial processes

    Science.gov (United States)

    Palmer, W. B.; Gerlaugh, H. E.; Priestley, R. R.

    1980-01-01

    Cogenerating electric power and process heat in single energy conversion systems rather than separately in utility plants and in process boilers is examined in terms of cost savings. The use of various advanced energy conversion systems are examined and compared with each other and with current technology systems for their savings in fuel energy, costs, and emissions in individual plants and on a national level. About fifty industrial processes from the target energy consuming sectors were used as a basis for matching a similar number of energy conversion systems that are considered as candidate which can be made available by the 1985 to 2000 time period. The sectors considered included food, textiles, lumber, paper, chemicals, petroleum, glass, and primary metals. The energy conversion systems included steam and gas turbines, diesels, thermionics, stirling, closed cycle and steam injected gas turbines, and fuel cells. Fuels considered were coal, both coal and petroleum based residual and distillate liquid fuels, and low Btu gas obtained through the on site gasification of coal. An attempt was made to use consistent assumptions and a consistent set of ground rules specified by NASA for determining performance and cost. Data and narrative descriptions of the industrial processes are given.

  4. RNA Crystallization

    Science.gov (United States)

    Golden, Barbara L.; Kundrot, Craig E.

    2003-01-01

    RNA molecules may be crystallized using variations of the methods developed for protein crystallography. As the technology has become available to syntheisize and purify RNA molecules in the quantities and with the quality that is required for crystallography, the field of RNA structure has exploded. The first consideration when crystallizing an RNA is the sequence, which may be varied in a rational way to enhance crystallizability or prevent formation of alternate structures. Once a sequence has been designed, the RNA may be synthesized chemically by solid-state synthesis, or it may be produced enzymatically using RNA polymerase and an appropriate DNA template. Purification of milligram quantities of RNA can be accomplished by HPLC or gel electrophoresis. As with proteins, crystallization of RNA is usually accomplished by vapor diffusion techniques. There are several considerations that are either unique to RNA crystallization or more important for RNA crystallization. Techniques for design, synthesis, purification, and crystallization of RNAs will be reviewed here.

  5. Reduction of carbon contamination during the melting process of Czochralski silicon crystal growth

    Science.gov (United States)

    Liu, Xin; Gao, Bing; Nakano, Satoshi; Kakimoto, Koichi

    2017-09-01

    Generation, incorporation, and accumulation of carbon (C) were investigated by transient global simulations of heat and mass transport during the melting process of Czochralski silicon (CZ-Si) crystal growth. Contact reaction between the quartz crucible and graphite susceptor was introduced as an extra origin of C contamination. The contribution of the contact reaction on C accumulation is affected by the back diffusion of C monoxide (CO) from the gap between the gas-guide and the crucible. The effect of the gas-guide coating on C reduction was elucidated by taking the reaction between the silicon carbide (SiC) coating and gaseous Si monoxide (SiO) into account. Application of the SiC coating on the gas-guide could effectively reduce the C contamination because of its higher thermochemical stability relative to that of graphite. Gas flow control on the back diffusion of the generated CO was examined by the parametric study of argon gas flow rate. Generation and back diffusion of CO were both effectively suppressed by the increase in the gas flow rate because of the high Péclet number of species transport. Strategies for C content reduction were discussed by analyzing the mechanisms of C accumulation process. According to the elucidated mechanisms of C accumulation, the final C content depends on the growth duration and contamination flux at the gas/melt interface.

  6. Modification of growth interface of CdZnTe crystals in THM process by ACRT

    Science.gov (United States)

    Zhou, Boru; Jie, Wanqi; Wang, Tao; Yin, Liying; Yang, Fan; Zhang, Binbin; Xi, Shouzhi; Dong, Jiangpeng

    2018-02-01

    The accelerated crucible rotation technique (ACRT) was introduced in the traveling heater method (THM) growth process of detector-grade CdZnTe (CZT) crystals to regulate the convection in the melt and to modify the growth interface morphology. Several ingots with the diameter of 53 mm were grown by THM with/without ACRT. The ingots were quenched during the growth to show both macroscopic and microscopic morphologies of the growth interfaces. The results show that by using ACRT the growth interface can be changed from a concave one to the flat or even convex one depending on the ACRT parameters, which is favorable for reducing nucleation in the melt to get larger CZT grains. Meanwhile, by using ACRT in THM process, the microscopic interface was changed from a diffused one to cellular or even planar one (at suitable ACRT parameters), through which the trapped Te inclusions was decreased for one order. An ingot grown by THM with constant rotation rate of 40 rpm was also grown, which have also reduced the interface curvature in macro-scale and Te inclusions to some extent, but the effects are not as significant as ACRT with high crucible rotation rate.

  7. Thermo-tunable hybrid photonic crystal fiber based on solution-processed chalcogenide glass nanolayers

    Science.gov (United States)

    Markos, Christos

    2016-08-01

    The possibility to combine silica photonic crystal fiber (PCF) as low-loss platform with advanced functional materials, offers an enormous range of choices for the development of fiber-based tunable devices. Here, we report a tunable hybrid silica PCF with integrated As2S3 glass nanolayers inside the air-capillaries of the fiber based on a solution-processed glass approach. The deposited high-index layers revealed antiresonant transmission windows from ~500 nm up to ~1300 nm. We experimentally demonstrate for the first time the possibility to thermally-tune the revealed antiresonances by taking advantage the high thermo-optic coefficient of the solution-processed nanolayers. Two different hybrid fiber structures, with core diameter 10 and 5 μm, were developed and characterized using a supercontinuum source. The maximum sensitivity was measured to be as high as 3.6 nm/°C at 1300 nm. The proposed fiber device could potentially constitute an efficient route towards realization of monolithic tunable fiber filters or sensing elements.

  8. Microbial ecology and starter culture technology in coffee processing.

    Science.gov (United States)

    Vinícius de Melo Pereira, Gilberto; Soccol, Vanete Thomaz; Brar, Satinder Kaur; Neto, Ensei; Soccol, Carlos Ricardo

    2017-09-02

    Coffee has been for decades the most commercialized food product and most widely consumed beverage in the world, with over 600 billion cups served per year. Before coffee cherries can be traded and processed into a final industrial product, they have to undergo postharvest processing on farms, which have a direct impact on the cost and quality of a coffee. Three different methods can be used for transforming the coffee cherries into beans, known as wet, dry, and semi-dry methods. In all these processing methods, a spontaneous fermentation is carried out in order to eliminate any mucilage still stuck to the beans and helps improve beverage flavor by microbial metabolites. The microorganisms responsible for the fermentation (e.g., yeasts and lactic acid bacteria) can play a number of roles, such as degradation of mucilage (pectinolytic activity), inhibition of mycotoxin-producing fungi growth, and production of flavor-active components. The use of starter cultures (mainly yeast strains) has emerged in recent years as a promising alternative to control the fermentation process and to promote quality development of coffee product. However, scarce information is still available about the effects of controlled starter cultures in coffee fermentation performance and bean quality, making it impossible to use this technology in actual field conditions. A broader knowledge about the ecology, biochemistry, and molecular biology could facilitate the understanding and application of starter cultures for coffee fermentation process. This review provides a comprehensive coverage of these issues, while pointing out new directions for exploiting starter cultures in coffee processing.

  9. A study of the ion-beam process technology

    International Nuclear Information System (INIS)

    Kanayama, Toshihiko

    1990-01-01

    This paper concerns the ion-beam technology for fabrication of semiconductor devices. The purpose of the present work is to find out useful irradiation effects of ion beams and to develop them into fabrication-process technologies. In particular, the advantage of the focused ion beam (FIB) is pursued to be utilized in fabrication of fine structures; the mask for the x-ray lithography is selected as a test target for this purpose. The mechanism of each irradiation effect is also investigated in detail to give the basis of the process developed. This paper consists of seven chapters. The first one gives an overview of the present work. Chapter 2 deals with ion-bombardment effect on the internal stress of deposited metals. The subject of Chapter 3 is the enhancement effect of chemical etching rate by ion bombardment. This chapter also discusses pattern replicability of the synchrotron-radiation x-ray lithography using the exposure results of the x-ray masks fabricated with the Al 2 O 3 resist and the stress compensation technique discussed in Chapter 2. Chapter 4 is devoted to the atomic intermixing effect caused by ion bombardment. The purpose of the latter half of this chapter is to demonstrate that this mixing effect has a high spatial resolution and deserves to be used as a definition process of fine structures by the FIB. Chapter 5 describes a unique effect of the ion beam: solid phase epitaxy of amorphous Si induced by bombardment at elevated temperatures. Chapter 6 demonstrates that maskless ion implantation using the FIB is a very efficient and productive technique for fabrication of small Hall sensors with sub-micron feature sizes. Finally, Chapter 7 summarizes the conclusions obtained in this work. (J.P.N.) 270 refs

  10. Development of large Grain/Single Crystal Niobium Cavity Technology at Jefferson Lab

    Energy Technology Data Exchange (ETDEWEB)

    Peter Kneisel; J. Sekutowicz; T. Carneiro; G. Ciovati

    2006-10-31

    Approximately two years ago we started to develop high performance niobium accelerating cavities based on large grain or single crystal high purity niobium. We have fabricated and tested 15 single cell cavities of various shapes and frequencies between 1300 MHz and 2300 MHz using material from a total of 9 different very large grain niobium ingots from four niobium suppliers. The materials differed not only in grain sizes, but also in RRR ? value and in the amount of Ta contained in the material. In one ingot supplied by CBMM the central grain exceeded 7 inches in diameter and this was used to fabricate two 2.2 GHz cavities. A single crystal 1300 MHz mono-cell cavity was also produced at DESY by rolling out a single crystal to the size required for this cavity. It was sent to Jlab for surface treatment and testing. In addition, we have fabricated three 7-cell cavities: two of the Jlab high gradient (HG) shape and one of the ILC Low Loss shape. Two 9-cell TESLA shape cavities are presently in fabrication at Jlab and are close to completion.

  11. Additive Manufacturing of Single-Crystal Superalloy CMSX-4 Through Scanning Laser Epitaxy: Computational Modeling, Experimental Process Development, and Process Parameter Optimization

    Science.gov (United States)

    Basak, Amrita; Acharya, Ranadip; Das, Suman

    2016-08-01

    This paper focuses on additive manufacturing (AM) of single-crystal (SX) nickel-based superalloy CMSX-4 through scanning laser epitaxy (SLE). SLE, a powder bed fusion-based AM process was explored for the purpose of producing crack-free, dense deposits of CMSX-4 on top of similar chemistry investment-cast substrates. Optical microscopy and scanning electron microscopy (SEM) investigations revealed the presence of dendritic microstructures that consisted of fine γ' precipitates within the γ matrix in the deposit region. Computational fluid dynamics (CFD)-based process modeling, statistical design of experiments (DoE), and microstructural characterization techniques were combined to produce metallurgically bonded single-crystal deposits of more than 500 μm height in a single pass along the entire length of the substrate. A customized quantitative metallography based image analysis technique was employed for automatic extraction of various deposit quality metrics from the digital cross-sectional micrographs. The processing parameters were varied, and optimal processing windows were identified to obtain good quality deposits. The results reported here represent one of the few successes obtained in producing single-crystal epitaxial deposits through a powder bed fusion-based metal AM process and thus demonstrate the potential of SLE to repair and manufacture single-crystal hot section components of gas turbine systems from nickel-based superalloy powders.

  12. Process Analytical Technology (PAT): batch-to-batch reproducibility of fermentation processes by robust process operational design and control.

    Science.gov (United States)

    Gnoth, S; Jenzsch, M; Simutis, R; Lübbert, A

    2007-10-31

    The Process Analytical Technology (PAT) initiative of the FDA is a reaction on the increasing discrepancy between current possibilities in process supervision and control of pharmaceutical production processes and its current application in industrial manufacturing processes. With rigid approval practices based on standard operational procedures, adaptations of production reactors towards the state of the art were more or less inhibited for long years. Now PAT paves the way for continuous process and product improvements through improved process supervision based on knowledge-based data analysis, "Quality-by-Design"-concepts, and, finally, through feedback control. Examples of up-to-date implementations of this concept are presented. They are taken from one key group of processes in recombinant pharmaceutical protein manufacturing, the cultivations of genetically modified Escherichia coli bacteria.

  13. Amelogenin processing by MMP-20 prevents protein occlusion inside calcite crystals.

    Science.gov (United States)

    Bromley, Keith M; Lakshminarayanan, Rajamani; Thompson, Mitchell; Lokappa, Sowmya B; Gallon, Victoria A; Cho, Kang R; Qiu, S Roger; Moradian-Oldak, Janet

    2012-10-03

    Calcite crystals were grown in the presence of full-length amelogenin and during its proteolysis by recombinant human matrix metalloproteinase 20 (rhMMP-20). Recombinant porcine amelogenin (rP172) altered the shape of calcite crystals by inhibiting the growth of steps on the {104} faces and became occluded inside the crystals. Upon co-addition of rhMMP-20, the majority of the protein was digested resulting in a truncated amelogenin lacking the C-terminal segment. In rP172-rhMMP-20 samples, the occlusion of amelogenin into the calcite crystals was drastically decreased. Truncated amelogenin (rP147) and the 25-residue C-terminal domain produced crystals with regular shape and less occluded organic material. Removal of the C-terminal diminished the affinity of amelogenin to the crystals and therefore prevented occlusion. We hypothesize that HAP and calcite interact with amelogenin in a similar manner. In the case of each material, full-length amelogenin binds most strongly, truncated amelogenin binds weakly and the C-terminus alone has the weakest interaction. Regarding enamel crystal growth, the prevention of occlusion into maturing enamel crystals might be a major benefit resulting from the selective cleavage of amelogenin at the C-terminus by MMP-20. Our data have important implications for understanding the hypomineralized enamel phenotype in cases of amelogenesis imperfecta resulting from MMP-20 mutations and will contribute to the design of enamel inspired biomaterials.

  14. Properties of the Sodium Naproxen-Lactose-Tetrahydrate Co-Crystal upon Processing and Storage

    DEFF Research Database (Denmark)

    Sovago, Ioana; Wang, Wenbo; Qiu, Danwen

    2016-01-01

    Co-crystals and co-amorphous systems are two strategies to improve the physical properties of an active pharmaceutical ingredient and, thus, have recently gained considerable interest both in academia and the pharmaceutical industry. In this study, the behavior of the recently identified sodium...... naproxen-lactose-tetrahydrate co-crystal and the co-amorphous mixture of sodium, naproxen, and lactose was investigated. The structure of the co-crystal is described using single-crystal X-ray diffraction. The structural analysis revealed a monoclinic lattice, space group P21, with the asymmetric unit...... containing one molecule of lactose, one of naproxen, sodium, and four water molecules. Upon heating, it was observed that the co-crystal transforms into a co-amorphous system due to the loss of its crystalline bound water. Dehydration and co-amorphization were studied using synchrotron X-ray radiation...

  15. Investigation of process equipment in petrochemical industry using radioisotope technology

    International Nuclear Information System (INIS)

    Mohammed, M. S.

    2007-04-01

    Applications of radioisotope technology have proved it self to be an effective techniques for troubleshooting and optimizing industrial process in petrochemical industry. In this study, Khartoum refinery was investigated by gamma scanning technique for better understanding of malfunctions, the scanning were carried out using 60 C gamma radiation source with activity of 50 mCi on fractionator and stripper columns, obtained results showed that all trays of the fractionator column were in place but weeping was evident due to fouling or partial tray damage. For the stripper column, results obtained showed that all trays were on their positions and no process anomalies taking place. Heat exchanger was also examined using radiotracer technique with respect to leak detection and residence time distribution. The investigations were carried out using 82 Br in the form of di-bromo-para-bensene (C 6 H 4 Br 2 ) as a radiotracer. No leak was recorded and the residence time distribution results showed that the process functions were quite normal. Leak was examined using 99m Tc as a radiotracer detection to demonstrate the potentials of the technique. The testing was conducted using reflux condenser. Obtained results proved that the technique is sensitive, reliable and can be adopted to investigate heat exchangers in industrial systems.(Author)

  16. Process technology of luwak coffee through bioreactor utilization

    Science.gov (United States)

    Hadipernata, M.; Nugraha, S.

    2018-01-01

    Indonesia has an advantage in producing exotic coffee that is Luwak coffee. Luwak coffee is produced from the fermentation process in digestion of civet. Luwak coffee production is still limited due to the difficulty level in the use of civet animals as the only medium of Luwak coffee making. The research was conducted by developing technology of luwak coffee production through bioreactor utilization and addition the bacteria isolate from gastric of civet. The process conditions in the bioreactor which include temperature, pH, and bacteria isolate of civet are adjusted to the process that occurs in civet digestion, including peristaltic movement on the stomach and small intestine of the civet will be replaced by the use of propellers that rotate on the bioreactor. The result of research showed that proximat analysis data of artificial/bioreactor luwak coffee did not significant different with original luwak coffee. However, the original luwak coffee has higher content of caffeine compared to bioreactor luwak coffee. Based on the cuping test the bioreactor luwak coffee has a value of 84.375, while the original luwak coffee is 84.875. As the result, bioreactor luwak coffee has excellent taste that similiar with original luwak coffee taste.

  17. THz spectroscopy: An emerging technology for pharmaceutical development and pharmaceutical Process Analytical Technology (PAT) applications

    Science.gov (United States)

    Wu, Huiquan; Khan, Mansoor

    2012-08-01

    As an emerging technology, THz spectroscopy has gained increasing attention in the pharmaceutical area during the last decade. This attention is due to the fact that (1) it provides a promising alternative approach for in-depth understanding of both intermolecular interaction among pharmaceutical molecules and pharmaceutical product quality attributes; (2) it provides a promising alternative approach for enhanced process understanding of certain pharmaceutical manufacturing processes; and (3) the FDA pharmaceutical quality initiatives, most noticeably, the Process Analytical Technology (PAT) initiative. In this work, the current status and progress made so far on using THz spectroscopy for pharmaceutical development and pharmaceutical PAT applications are reviewed. In the spirit of demonstrating the utility of first principles modeling approach for addressing model validation challenge and reducing unnecessary model validation "burden" for facilitating THz pharmaceutical PAT applications, two scientific case studies based on published THz spectroscopy measurement results are created and discussed. Furthermore, other technical challenges and opportunities associated with adapting THz spectroscopy as a pharmaceutical PAT tool are highlighted.

  18. Intelligent technologies in process of highly-precise products manufacturing

    Science.gov (United States)

    Vakhidova, K. L.; Khakimov, Z. L.; Isaeva, M. R.; Shukhin, V. V.; Labazanov, M. A.; Ignatiev, S. A.

    2017-10-01

    One of the main control methods of the surface layer of bearing parts is the eddy current testing method. Surface layer defects of bearing parts, like burns, cracks and some others, are reflected in the results of the rolling surfaces scan. The previously developed method for detecting defects from the image of the raceway was quite effective, but the processing algorithm is complicated and lasts for about 12 ... 16 s. The real non-stationary signals from an eddy current transducer (ECT) consist of short-time high-frequency and long-time low-frequency components, therefore a transformation is used for their analysis, which provides different windows for different frequencies. The wavelet transform meets these conditions. Based on aforesaid, a methodology for automatically detecting and recognizing local defects in bearing parts surface layer has been developed on the basis of wavelet analysis using integral estimates. Some of the defects are recognized by the amplitude component, otherwise an automatic transition to recognition by the phase component of information signals (IS) is carried out. The use of intelligent technologies in the manufacture of bearing parts will, firstly, significantly improve the quality of bearings, and secondly, significantly improve production efficiency by reducing (eliminating) rejections in the manufacture of products, increasing the period of normal operation of the technological equipment (inter-adjustment period), the implementation of the system of Flexible facilities maintenance, as well as reducing production costs.

  19. Radiation processing technology for industrial waste water treatment

    International Nuclear Information System (INIS)

    2011-01-01

    Radiation sterilization technology, cross-linked polymers and curing, food and environmental applications of the radiation is widely used for many years. At the same time, drinking water and wastewater treatment are the part of the radiation technology applications. For this purpose, drinking water and wastewater treatment plants in various countries has been established. In this project, gamma / electron beam radiation treatment is intended to be used for the treatment of alkaloid, textiles and polychlorinated biphenyls (PCBs) wastewater. In this regard, the chemical characterization of wastewater, the interaction with radiation, biological treatment and determination of toxicological properties are the laboratory studies milestones. After laboratory studies, the establishment of a pilot scale treatment plant has been planned. Within the framework of the project a series of dye used in textile industry were examined. Besides the irradiation, the changes in treatment efficiency were investigated by using of oxygen and hydrogen peroxide in conjunction with the irradiation. Same working methods were implemented in the wastewater treatment of Bolvadin Opium Alkaloid Factory as well. In addition to chemical analysis in this study, aerobic and anaerobic biological treatment process also have been applied. Standard reference materials has been used for the marine sediment study contaminated with polychlorinated biphenyls.

  20. Small Scale Turbopump Manufacturing Technology and Material Processes

    Science.gov (United States)

    Alvarez, Erika; Morgan, Kristin; Wells, Doug; Zimmerman, Frank

    2011-01-01

    As part of an internal research and development project, NASA Marshall Space Flight Center (MSFC) has been developing a high specific impulse 9,000-lbf LOX/LH2 pump-fed engine testbed with the capability to throttle 10:1. A Fuel Turbopump (FTP) with the ability to operate across a speed range of 30,000-rpm to 100,000-rpm was developed and analyzed. This small size and flight-like Fuel Turbopump has completed the design and analysis phase and is currently in the manufacturing phase. This paper highlights the manufacturing and processes efforts to fabricate an approximately 20-lb turbopump with small flow passages, intricately bladed components and approximately 3-in diameter impellers. As a result of the small scale and tight tolerances of the hardware on this turbopump, several unique manufacturing and material challenges were encountered. Some of the technologies highlighted in this paper include the use of powder metallurgy technology to manufacture small impellers, electron beam welding of a turbine blisk shroud, and casting challenges. The use of risk reduction efforts such as non-destructive testing (NDT) and evaluation (NDE), fractography, material testing, and component spin testing are also discussed in this paper.

  1. Synthesis and post-processing of nanomaterials using microreaction technology

    International Nuclear Information System (INIS)

    Chang, Chih-Hung; Paul, Brian K.; Remcho, Vincent T.; Atre, Sundar; Hutchison, James E.

    2008-01-01

    A critical barrier to the routine use of nanomaterials is the tedious, expensive means of their synthesis. Microreaction technology takes advantage of the large surface area-to-volume ratios within microchannel structures to accelerate heat and mass transport. This accelerated transport allows for rapid changes in reaction temperatures and concentrations leading to more uniform heating and mixing which can have dramatic impacts on macromolecular yields and nanoparticle size distributions. Benefits of microreaction technology include higher yield and reactant conversion, better energy efficiency and less by-product generation. Microreactors can help minimize the environmental impact of nanoproduction by enabling solvent free mixing, integrated separation techniques and reagent recycling. The possibility of synthesizing nanomaterials in the required volumes at the point-of-use eliminates the need to store and transport potentially hazardous materials and provides the flexibility for tailoring complex functional nanomaterials. Recognizing these benefits for nanosynthesis, continuous flow microreactors have been used by several research groups to synthesize and characterize nanomaterials. An overview of these efforts and issues related to scale up and other post synthesis processes such as separation and deposition are presented in this paper.

  2. Experimental Conditions to Obtain Photopolymerization Induced Phase Separation Process in Liquid Crystal-Photopolymer Composite Materials under Laser Exposure

    Directory of Open Access Journals (Sweden)

    Manuel Ortuño

    2014-01-01

    Full Text Available We analyze the experimental conditions necessary to obtain a photopolymerization induced phase separation process inside liquid crystal-photopolymer composite materials. Composites stored for 24 hours perform poorly in hologram recording but a good result is obtained if they are used recently prepared. We use a procedure combining heat and sonication to disarrange the liquid crystal structures formed during storage of the composite. We also propose incoherent light treatment after recording the hologram in order to evaluate if the phase separation evolved correctly during hologram recording.

  3. Technology of irradiation processing for checking garlic sprouting

    International Nuclear Information System (INIS)

    Chen Yuntang

    1999-01-01

    Study on technology of irradiation processing for checking garlic sprouting was carried out. The results are as follows. 1. the suitable irradiation time of garlic could be prolonged when the garlic was preserved at low temperature (-2 +- 1 degree C). When the garlic was stored till the end of the year and then irradiated, the sprouting could be checked effectively. When the garlic was stored till the next March, the effect of sprouting inhibition decreased; 2. When garlic was irradiated at suitable time and then subsequently stored at low temperature, the effect of sprouting inhibition was the same as that with cold storage before irradiation. However, if the cold storage period was rather long, the effect was not as good as that with cold storage after irradiation; 3. Browning of irradiated garlic did not occur when the garlic was preserved at low temperature (-2 +- 1 degree C), indicating that the browning of sprout and bud was caused by higher storage temperature

  4. Carotenoids Functionality, Sources, and Processing by Supercritical Technology: A Review

    Directory of Open Access Journals (Sweden)

    Natália Mezzomo

    2016-01-01

    Full Text Available Carotenoid is a group of pigments naturally present in vegetal raw materials that have biological properties. These pigments have been used mainly in food, pharmaceutical, and cosmetic industries. Currently, the industrial production is executed through chemical synthesis, but natural alternatives of carotenoid production/attainment are in development. The carotenoid extraction occurs generally with vegetal oil and organic solvents, but supercritical technology is an alternative technique to the recovery of these compounds, presenting many advantages when compared to conventional process. Brazil has an ample diversity of vegetal sources inadequately investigated and, then, a major development of optimization and validation of carotenoid production/attainment methods is necessary, so that the benefits of these pigments can be delivered to the consumer.

  5. Technological processes - environment - ecological problems. Tehnoloski procesi - okruzenje - ekoloski problemi

    Energy Technology Data Exchange (ETDEWEB)

    Hovanec, G.; Knezevic, D.; Bicanski, J.; Monevski, B.; Milovic, M. (Rudarski Institut, Zemun (Yugoslavia))

    1990-01-01

    Deals with environmental pollution caused by coal fired power plants and by ore mining and ore processing plants in Yugoslavia. Air, land and water pollution by Serbian zinc and copper flotation plants is described. Various technological features of zinc flotation plants and their waste disposal methods as well as copper mines are provided. Measures aimed at reducing land and water pollution recommended by the Mining Institute in Zemun are highlighted. Air, land and water pollution by major Yugoslav power plants is further reviewed. These plants, fired by low grade lignite and brown coal, produce 11 Mt/a of slag and fly ash. Chemical ash properties, features of ash disposal sites and measures for recultivating devastated land in the vicinity of power plants are pointed out. 2 tabs.

  6. Effect of the packing structure of silicon chunks on the melting process and carbon reduction in Czochralski silicon crystal growth

    Science.gov (United States)

    Liu, Xin; Nakano, Satoshi; Kakimoto, Koichi

    2017-06-01

    Carbon (C) contamination in Czochralski silicon (CZ-Si) crystal growth mainly originates from carbon monoxide (CO) generation on the graphite components, which reaches a maximum during the melting stage. Loading a crucible with poly-Si feedstock includes many technical details for optimization of the melting and growth processes. To investigate the effect of the packing structure of Si chunks on C accumulation in CZ-Si crystal growth, transient global simulations of heat and mass transport were performed for the melting process with different packing structures of poly-Si. The heat transport modeling took into account the effective thermal conductivity (ETC) of the Si feedstock, which is affected by the packing structure. The effect of the chunk size on the melting process and C accumulation were investigated by parametric studies of different packing structures. The heat transport and melting process in the crucible were affected by the ETC and the emissivity of the Si feedstock. It was found that smaller Si chunks packed in the upper part could speed up the melting process and smooth the power profile. Decreasing the duration of the melting process is favorable for reduction of C contamination in the Si feedstock. Parametric studies indicated that optimization of the melting process by the packing structure is possible and essential for C reduction in CZ-Si crystal growth.

  7. 49 CFR 232.503 - Process to introduce new brake system technology.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 4 2010-10-01 2010-10-01 false Process to introduce new brake system technology... Technology § 232.503 Process to introduce new brake system technology. (a) Pursuant to the procedures... brake system technology, prior to implementing the plan. (b) Each railroad shall complete a pre-revenue...

  8. Twinning dislocation and twin propagation process in a nickel-base single crystal TMS-82 superalloy

    Energy Technology Data Exchange (ETDEWEB)

    Lv, Xianzi; Zhang, Jianxin [Shandong Univ., Jinan (China). Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials; Harada, Hiroshi [National Institute for Materials Science, Ibaraki (Japan)

    2014-03-15

    Thermomechanical fatigue cyclic loading tests have been carried out along the <001> orientation and the formation of twins during thermomechanical fatigue processing has been studied in detail in a nickel-base single crystal TMS-82 superalloy. The twinning dislocation is determined to be 1/6<112> in the γ' phase except for the 1/3<112> dislocation, which operates on every successive {111} plane. The 1/6<112> twinning dislocations can move independently in both γ and γ' phases. Although movement of a single 1/6<112> twining dislocation may destroy the ordering of γ' phase, its existence is rationalized on the basis of crystallographic analysis. The movement of a 1/3<112> dislocation on a single {111} plane will lead to a high-energy stacking sequence of head-to-head of two neighboring {111} layer atoms in the L1{sub 2} structure. Pre-existing dislocations have a significant effect on the growth of deformation twins. In the dislocation-free area, the twin can propagate without any notable impediment to lead to a twin plate with equal width. High dislocation density may hinder the propagation of twins to varying degrees. (orig.)

  9. Adsorption of crystal violet with diatomite earth&carbon by a modification of hydrothermal carbonization process.

    Science.gov (United States)

    Zhang, Yanzhuo; Li, Jun; Chen, Guanghui; Bian, Wei; Lu, Yun; Li, Wenjing; Zheng, Zhaoming; Cheng, Xiaojie

    2016-01-01

    The high colority and difficulty of decolorization are the most important tasks on printing and dyeing wastewater. This study investigates the ability of diatomite earth&carbon (DE&C) as an adsorbent to removal crystal violet (CV) from aqueous solutions. Fourier transform infrared spectroscopy results indicate the importance of functional groups during the adsorption of CV. The obtained N2 adsorption-desorption isotherm values accord with well IUPAC type II. Our calculations determined a surface area of 73.15 m(2) g(-1) for DE&C and an average pore diameter of 10.56 nm. Equilibrium data of the adsorption process fitted very well to the Langmuir model (R(2) > 0.99). The results of kinetics study showed that the pseudo-second-order model fitted to the experimental data well. The thermodynamic parameters were also evaluated. ΔH° 0 and ΔG° dye. Furthermore the positive value of ΔS° reflected good affinity of the CV dye.

  10. Crystallization Process of Heat-treated Amorphous Ni-P Alloy Coating

    Directory of Open Access Journals (Sweden)

    JIN Shi-wei

    2016-09-01

    Full Text Available Amorphous Ni-P alloy coatings were prepared on 45 carbon steel blocks using electrodeposition method. The thermal effect and quality change of Ni-P alloy coating under heating rate of 20℃/min were analyzed by differential scanning calorimetry (DSC and thermogravimetry (TG. Coatings were heat-treated at 300℃ and 400℃ for 0, 15, 30, 45, 60, 75min respectively, coating surface was characterized by scanning electron microscope (SEM, energy dispersive spectrometer (EDS, X-ray diffraction (XRD, microhardness tester. The result shows that the exothermic peak of Ni-P alloy coating appears at 284.8℃, coating quality and elemental composition are stable during the heat treatment. Crystallization process experiences a transformation of amorphous, metastable state NiP and Ni5P2, stable state Ni3P. The microhardness of coating can be improved remarkably after heat treatment, namely, the maximum value of heat-treated coating is 1036.56HV, which is nearly 2 times as hard as as-deposited coating. The corrosion resistance of heat-treated Ni-P alloy coating in NaCl solution is inferior to as-deposited coating, but they are both much better than 45 carbon steel substrate.

  11. The peculiarities of water crystallization and ice melting processes in the roots of one-year plants (Plantago major L.).

    Science.gov (United States)

    Bakradze, N; Kiziria, E; Sokhadze, V; Gogichaishvili, S

    2008-01-01

    Results are presented of a water phase transition study in plantain (Plantago major L.) roots, which were used as a model system to research the peculiarities of water crystallization and ice melting processes in complex heterogeneous biological systems. It was confirmed that water in such systems is crystallized in two clearly distinguished temperature ranges: -10 to -25 degree capital ES, Cyrillic and -25 to -45 degree capital ES, Cyrillic. These water fractions are conditionally attributed to extracellular (-10 to -25 degree capital ES, Cyrillic) and intracellular (-25 to -45 degree capital ES, Cyrillic) solutions. A possible explanation is given for such significant supercooling of the intracellular solution. The values of osmotic pressures of extra- and intracellular solutions were determined according to ice melting curves. It is noted that the intracellular solution, which crystallized at lower temperatures, had a lower osmotic pressure.

  12. The Influence of Various Process Parameters on Dissolution Kinetics and Mechanism of Struvite Seed Crystals

    Science.gov (United States)

    Ariyanto, Eko; Ang, Ha Ming; Sen, Tushar Kanti

    2017-09-01

    The basic understanding of struvite dissolution chemistry is essential to designers and operators for anticipating struvite problem and remediating existing struvite damage in a wastewater treatment. The dissolution kinetic of struvite seed crystals is very important parameters to determine a solid substance entering in solvent to yield a solution. In this study the dissolution kinetics of struvite crystals (MgNH4PO4·6H2O) in deionized water was investigated in a batch crystallizer. The effects of stirrer speeds, temperature and seed crystals size on the dissolution rate were determined. The results showed that an increase of struvite dissolution rate with increasing stirring speed. Struvite dissolution occurred via a diffusion-controlled mechanism in the range of stirrer speeds 120-400 rpm but became interfacial-reaction-controlling at over 400 rpm. The influence of temperature on dissolution kinetic of struvite crystals was also investigated at stirrer speeds of 200 and 500 rpm. The dissolution rates increased with an increase in the temperature for both stirrer speeds. The change in activation energies at different stirrer speeds confirmed that the change of dissolution mechanism from a diffusion-controlled mechanism at low stirrer speeds to an interfacial-reaction-controlled mechanism at higher stirrer speeds. The dissolution rate of struvite crystals increased with smaller crystal sizes.

  13. Role of radiation processing in technological development of the world

    International Nuclear Information System (INIS)

    Chmielewski, G. Andrzej.; Berejka, J. Anthony.

    2012-01-01

    Full text: Radiation processing is based on application of gamma industrial sources and electron accelerators. Recently development of high power accelerators made a operation mode of e/X as a viable tool for these applications as well. Included in this are service type facilities operated in Research and Development centers. When other uses are taken into account, there are in total over 300 gamma irradiators being operated for a variety of purposes in 55 different countries. 100-120 gamma irradiators are located in Europe and in the United States. Recent developments in very high current accelerators show considerable promise for the industrial use of X rays as a future technology of choice. X ray comparable in penetration to gamma rays. The use of high energy X rays for sterilizing medical devices was proposed during the 1960th, but not implemented until the late 1990th. X-rays are comparable in penetration to gamma emissions from radioactive isotopes, but being electrically sourced can be turned on or off not posing the storage, supply and transport issues associated with the use of isotopes. The development of nana-composites, which is only a few years old, is very promising. This includes the development of nano-gels. This nano-gels can be used for drug or vaccine delivery and are especially suited for the delivery of anti-cancer agents into tumor tissues. The use of natural polymers and fibers is another growing area in the use of radiation processing. Radiation processing is also being used to enhance befoul manufacture. Food the hygenization is other important application of radiation processing and finally environmental applications are still challenging field or radiation use.

  14. Traditional fish processing: technology, quality development and evaluation

    International Nuclear Information System (INIS)

    Nketsia-Tabiri, J.

    1994-01-01

    Traditional fish processing technologies are important in the preservation and utilization of fish in many developing countries. These technologies as well as the quality of the products arc poorly defined and understood. This study therefore investigated the production, quality characteristics and utilization of traditional cured fish products using field surveys and laboratory techniques. It was found that simple traditional technologies for smoking, salting and drying are used to process fish in Ghana; infrastructural requirements for traditional fish processing have high local material input. The cured fish products have distinct sensory, physico-chemical properties and variable storage characteristics. Processors' perceptions of important quality attributes of cured fish products were linked to storage, marketing and other product delivery characteristics. Consumers' perceptions and expectations of desirable quality attributes however were found to he dependent upon the type of cured fish product and the food in which it is used. Cost was found to be the most important factor influencing the utilization of animal protein foods; other factors were nutritional quality, beliefs and food habits. Animal protein consumers showed a high preference for fish in general and cured fish products in particular. U sing central composite rotatable design for k = 3, representing salting time (0 - 24), drying temperature (40°C - 60°C) and drying time (6 - 20 hours), equations for predicting objective and subjective quality indices were developed. The critical salting time for attaining minimum moisture content were 20.5, 12 and 8.5 hours respectively for products dried at 40°C, 50°C and 60°C. At each salting time, the mean hardness score was dependent on the drying temperature and drying time whilst the mean colour and overall acceptability scores were influenced by drying temperature. It was found that the long salting time (24-72 hours) and drying time (5

  15. Progress in liquid crystal (LC) science and technology in honor of Kobayashi's 80th birthday

    CERN Document Server

    Kwok, Hoi-Sing; Ong, Hiap L

    2013-01-01

    The presence of liquid crystal displays (LCDs) marks the advances in mobile phones and television development over the last few decades. Japanese companies were the first to commercialize passive-matrix TNLCDs and, later on, high-resolution activematrix LCDs.Prof. Shunsuke Kobayashi has made essential contributions to Japan's prominence in LCD development throughout this period. He is well-known not only for his own groundbreaking research, but also for the training of many prominent figures in the display industry, both in Japan and in other countries.This book brings together many prominent

  16. Feasibility study on co-processing technology; Co-processing gijutsu no kigyoka kanosei chosa

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1997-03-01

    Co-processing is a technology producing light oil by hydrocracking of mixtures of coal and heavy oils (tar sand bitumen, heavy oil) as rich resources. The feasibility study on co-processing technology was carried out to improve its profitability and promote its practical use. The United States DOE is promoting the co-processing program to enhance reaction rates through utilization of modified catalysts and optimization of the first and second stage temperatures, and to perform catalyst activity screening including new high- activity ebullated-bed catalysts, dispersed catalysts, extrusion molded catalysts, and combinations of them. DOE is also promoting the study on the reactant/product of coal- derived liquid and/or petroleum derived residues, improvement of a liquid yield and product quality in a two-stage reactor, and optimization of the co-processing system by interstage hydrotreating. Two test results showed higher effectiveness than previous ones. In addition, the possibility of the co-processing system was studied by autoclave test of coal/oil sand bitumen. Its feasibility in China was also studied. 44 figs., 31 tabs.

  17. Solution processed deposition of electron transport layers on perovskite crystal surface—A modeling based study

    Energy Technology Data Exchange (ETDEWEB)

    Mortuza, S.M.; Taufique, M.F.N.; Banerjee, Soumik, E-mail: soumik.banerjee@wsu.edu

    2017-02-01

    Highlights: • The model determined the surface coverage of solution-processed film on perovskite. • Calculated surface density map provides insight into morphology of the monolayer. • Carbonyl oxygen atom of PCBM strongly attaches to the (110) surface of perovskite. • Uniform distribution of clusters on perovskite surface at lower PCBM concentration. • Deposition rate of PCBM on the surface is very high at initial stage of film growth. - Abstract: The power conversion efficiency (PCE) of planar perovskite solar cells (PSCs) has reached up to ∼20%. However, structural and chemicals defects that lead to hysteresis in the perovskite based thin film pose challenges. Recent work has shown that thin films of [6,6]-phenyl-C61-butyric acid methyl ester (PCBM) deposited on the photo absorption layer, using solution processing techniques, minimize surface pin holes and defects thereby increasing the PCE. We developed and employed a multiscale model based on molecular dynamics (MD) and kinetic Monte Carlo (kMC) to establish a relationship between deposition rate and surface coverage on perovskite surface. The MD simulations of PCBMs dispersed in chlorobenzene, sandwiched between (110) perovskite substrates, indicate that PCBMs are deposited through anchoring of the oxygen atom of carbonyl group to the exposed lead (Pb) atom of (110) perovskite surface. Based on rates of distinct deposition events calculated from MD, kMC simulations were run to determine surface coverage at much larger time and length scales than accessible by MD alone. Based on the model, a generic relationship is established between deposition rate of PCBMs and surface coverage on perovskite crystal. The study also provides detailed insights into the morphology of the deposited film.

  18. Solution processed deposition of electron transport layers on perovskite crystal surface—A modeling based study

    International Nuclear Information System (INIS)

    Mortuza, S.M.; Taufique, M.F.N.; Banerjee, Soumik

    2017-01-01

    Highlights: • The model determined the surface coverage of solution-processed film on perovskite. • Calculated surface density map provides insight into morphology of the monolayer. • Carbonyl oxygen atom of PCBM strongly attaches to the (110) surface of perovskite. • Uniform distribution of clusters on perovskite surface at lower PCBM concentration. • Deposition rate of PCBM on the surface is very high at initial stage of film growth. - Abstract: The power conversion efficiency (PCE) of planar perovskite solar cells (PSCs) has reached up to ∼20%. However, structural and chemicals defects that lead to hysteresis in the perovskite based thin film pose challenges. Recent work has shown that thin films of [6,6]-phenyl-C61-butyric acid methyl ester (PCBM) deposited on the photo absorption layer, using solution processing techniques, minimize surface pin holes and defects thereby increasing the PCE. We developed and employed a multiscale model based on molecular dynamics (MD) and kinetic Monte Carlo (kMC) to establish a relationship between deposition rate and surface coverage on perovskite surface. The MD simulations of PCBMs dispersed in chlorobenzene, sandwiched between (110) perovskite substrates, indicate that PCBMs are deposited through anchoring of the oxygen atom of carbonyl group to the exposed lead (Pb) atom of (110) perovskite surface. Based on rates of distinct deposition events calculated from MD, kMC simulations were run to determine surface coverage at much larger time and length scales than accessible by MD alone. Based on the model, a generic relationship is established between deposition rate of PCBMs and surface coverage on perovskite crystal. The study also provides detailed insights into the morphology of the deposited film.

  19. Forensic print extraction using 3D technology and its processing

    Science.gov (United States)

    Rajeev, Srijith; Shreyas, Kamath K. M.; Panetta, Karen; Agaian, Sos S.

    2017-05-01

    Biometric evidence plays a crucial role in criminal scene analysis. Forensic prints can be extracted from any solid surface such as firearms, doorknobs, carpets and mugs. Prints such as fingerprints, palm prints, footprints and lip-prints can be classified into patent, latent, and three-dimensional plastic prints. Traditionally, law enforcement officers capture these forensic traits using an electronic device or extract them manually, and save the data electronically using special scanners. The reliability and accuracy of the method depends on the ability of the officer or the electronic device to extract and analyze the data. Furthermore, the 2-D acquisition and processing system is laborious and cumbersome. This can lead to the increase in false positive and true negative rates in print matching. In this paper, a method and system to extract forensic prints from any surface, irrespective of its shape, is presented. First, a suitable 3-D camera is used to capture images of the forensic print, and then the 3-D image is processed and unwrapped to obtain 2-D equivalent biometric prints. Computer simulations demonstrate the effectiveness of using 3-D technology for biometric matching of fingerprints, palm prints, and lip-prints. This system can be further extended to other biometric and non-biometric modalities.

  20. Technological process for production of persimmon and strawberry vinegars

    Directory of Open Access Journals (Sweden)

    Claudio Hidalgo

    2010-08-01

    Full Text Available Claudio Hidalgo1, Estibaliz Mateo1, Ana Belen Cerezo2, Maria-Jesús Torija1, Albert Mas11Biotecnologia Enològica, Departament de Bioquimica i Biotecnologia, Facultat d’Enologia, Universitat Rovira i Virgili, Marcel-li Domingo, Tarragona; 2Área de Nutrición y Bromatología, Facultad de Farmacia, Universidad de Sevilla, Sevilla, SpainAbstract: Fruit surplus is common in intensive agriculture in many countries. This ecologic and economic problem requires alternative uses to be found for fruit. The aim of this study was to use surplus fruit to produce vinegar by traditional methods (alcoholic fermentation and acetification from persimmon and strawberry. The process was performed with naturally occurring microorganisms and compared with inoculated commercial wine yeast for alcoholic fermentation. Alcoholic fermentation proceeded faster when inoculated due to the length of the lag phases observed in spontaneous fermentations. The alcoholic fermentations of strawberry mash were faster than those of persimmon mash. In contrast, acetifications were much faster in persimmon (30 days than in strawberry (70 days, in the latter some acetifications were not finished. From the technologic point of view, to produce persimmon and strawberry wine and vinegar, it is better to avoid fruit pressing and perform the process with fruit mash. Inoculation is recommended for persimmon and is necessary for strawberry.Keywords: wine, vinegar, fruit seasonings, acetic acid bacteria

  1. Acoustic monitoring of rotating machine by advanced signal processing technology

    International Nuclear Information System (INIS)

    Kanemoto, Shigeru

    2010-01-01

    The acoustic data remotely measured by hand held type microphones are investigated for monitoring and diagnosing the rotational machine integrity in nuclear power plants. The plant operator's patrol monitoring is one of the important activities for condition monitoring. However, remotely measured sound has some difficulties to be considered for precise diagnosis or quantitative judgment of rotating machine anomaly, since the measurement sensitivity is different in each measurement, and also, the sensitivity deteriorates in comparison with an attached type sensor. Hence, in the present study, several advanced signal processing methods are examined and compared in order to find optimum anomaly monitoring technology from the viewpoints of both sensitivity and robustness of performance. The dimension of pre-processed signal feature patterns are reduced into two-dimensional space for the visualization by using the standard principal component analysis (PCA) or the kernel based PCA. Then, the normal state is classified by using probabilistic neural network (PNN) or support vector data description (SVDD). By using the mockup test facility of rotating machine, it is shown that the appropriate combination of the above algorithms gives sensitive and robust anomaly monitoring performance. (author)

  2. Technological foundations of processing tomato pomace in feed additives

    Directory of Open Access Journals (Sweden)

    B. Yegorov

    2015-05-01

    Full Text Available Introduction. Search for new types of alternative raw material for the efficient development of poultry industry and problem of waste disposal of canning industry made it necessary to develop a method of processing tomato pomace in feed additives. Materials and methods. Sampling, preparation and testing were carried out by general and specific organ oleptic and physical-technological methods of assessment and analysis of the properties of raw materials and finished products. Results. Incorporation of tomato pomace in the feed additive reduces the cost of raw materials and expenses associated with moistening of the mixture before extrusion and incorporation of chalk feed will solve the problem of calcium imbalance of laying hens. It was found that extrusion process has improved the physical properties of feed additive and showed the possibility of its use as a feed component: moisture content decreased by 34.5 %, the angle of repose increased by 11.4 %, flowability decreased by 39.7 % and bulk density decreased by 32.3 %. Conclusions. The resulting feed additive will solve the problem of diversification of raw materials, waste, calcium imbalance of laying hens and reduce expenses on compound animal feedstuff production.

  3. THE ANALYSIS OF TECHNOLOGICAL PROCESS OF EXPEDITIONARY MAINTENANCE OF MOTOR TRANSPOR

    Directory of Open Access Journals (Sweden)

    V. S. Naumov

    2009-03-01

    Full Text Available The basic technological operations of the automobile freight forwarding process have been determined. The base algorithms of the freight forwarding technological process have been proposed. The fundamental flow charts of technological process in use have been formalized and analyzed.

  4. Technology Estimating 2: A Process to Determine the Cost and Schedule of Space Technology Research and Development

    Science.gov (United States)

    Cole, Stuart K.; Wallace, Jon; Schaffer, Mark; May, M. Scott; Greenberg, Marc W.

    2014-01-01

    As a leader in space technology research and development, NASA is continuing in the development of the Technology Estimating process, initiated in 2012, for estimating the cost and schedule of low maturity technology research and development, where the Technology Readiness Level is less than TRL 6. NASA' s Technology Roadmap areas consist of 14 technology areas. The focus of this continuing Technology Estimating effort included four Technology Areas (TA): TA3 Space Power and Energy Storage, TA4 Robotics, TA8 Instruments, and TA12 Materials, to confine the research to the most abundant data pool. This research report continues the development of technology estimating efforts completed during 2013-2014, and addresses the refinement of parameters selected and recommended for use in the estimating process, where the parameters developed are applicable to Cost Estimating Relationships (CERs) used in the parametric cost estimating analysis. This research addresses the architecture for administration of the Technology Cost and Scheduling Estimating tool, the parameters suggested for computer software adjunct to any technology area, and the identification of gaps in the Technology Estimating process.

  5. Oxidation and crystallization behavior of calcium europium silicon nitride thin films during rapid thermal processing

    Energy Technology Data Exchange (ETDEWEB)

    Jong, M. de, E-mail: m.dejong-1@tudelft.nl [Faculty of Applied Science, Delft University of Technology, Mekelweg 15, 2629JB Delft (Netherlands); Enter, V.E. van, E-mail: vvanenter@gmail.com [Faculty of Applied Science, Delft University of Technology, Mekelweg 15, 2629JB Delft (Netherlands); Schuring, E.W., E-mail: schuring@ecn.nl [Energy Center of the Netherlands, Westerduinweg 3, 1755LE Petten (Netherlands); Kolk, E. van der, E-mail: e.vanderkolk@tudelft.nl [Faculty of Applied Science, Delft University of Technology, Mekelweg 15, 2629JB Delft (Netherlands)

    2016-03-31

    Luminescent thin films were fabricated on silicon wafers using reactive magnetron sputtering of Ca, Si and Eu in Ar/N{sub 2} atmosphere. In order to activate the luminescence, the as-deposited nitride films were heated to 1100 °C by a rapid thermal processing treatment. X-ray diffraction measurements reveal the crystal phases that form during thermal treatment. By recording scanning electron microscopy images of the surface and the cross-section of the film at different radial locations, the formation of different layers with a thickness depending on the radial position is revealed. Energy dispersive x-ray spectroscopy analysis of these cross-sections reveals the formation of an oxide top layer and a nitride bottom layer. The thickness of the top layer increases as a function of radial position on the substrate and the thickness of the bottom layer decreases accordingly. The observation of different 4f{sup 6}5d{sup 1} → 4f{sup 7} Eu{sup 2+} luminescence emission bands at different radial positions correspond to divalent Eu doped Ca{sub 3}Si{sub 2}O{sub 4}N{sub 2}, Ca{sub 2}SiO{sub 4} and CaSiO{sub 3}, which is in agreement with the phases identified by X-ray diffraction analysis. A mechanism for the observed oxidation process of the nitride films is proposed that consists of a stepwise oxidation from the as-deposited amorphous nitride state to crystalline Ca{sub 3}Si{sub 2}O{sub 4}N{sub 2}, to Ca{sub 2}SiO{sub 4} and finally CaSiO{sub 3}. The oxidation rate and final state of oxidation show a strong temperature–time dependency during anneal treatment. - Highlights: • A thin film of nitridated Ca, Si and Eu was deposited using magnetron sputtering. • Rapid thermal processing (RTP) results in Eu{sup 2+} doped Ca{sub 3}Si{sub 2}O{sub 4}N{sub 2}, Ca{sub 2}SiO{sub 4}, and CaSiO{sub 3}. • Oxidation rate differs with radial position due to a temperature gradient during RTP. • Cross-section SEM–EDX shows how the oxidation progresses in lateral direction.

  6. Numerical and experimental study of a solid pellet feed continuous Czochralski growth process for silicon single crystals

    Science.gov (United States)

    Anselmo, A.; Prasad, V.; Koziol, J.; Gupta, K. P.

    1993-07-01

    A polysilicon pellets (≅1 mm diameter) feed continuous Czochralski (CCZ) growth process for silicon single crystals is proposed and investigated. Experiments in an industrial puller (14-18 inch diameter crucible) successfully demonstrate the feasibility of this process. The advantages of the proposed scheme are: a steady state growth process, a low aspect ratio melt, uniformity of heat addition and a growth apparatus with single crucible and no baffle(s). The addition of dopant with the solid charge will allow a better control of oxygen concentration leading to crystals of uniform properties and better quality. This paper presents theoretical results on melting of fully and partially immersed silicon spheres and numerical solutions on temperature and flow fields in low aspect ration melts with and without the addition of solid pellets. The theoretical and experimental results obtained thus far show a great promise for the proposed scheme.

  7. Advances in process overlay: alignment solutions for future technology nodes

    Science.gov (United States)

    Megens, Henry; van Haren, Richard; Musa, Sami; Doytcheva, Maya; Lalbahadoersing, Sanjay; van Kemenade, Marc; Lee, Hyun-Woo; Hinnen, Paul; van Bilsen, Frank

    2007-03-01

    Semiconductor industry has an increasing demand for improvement of the total lithographic overlay performance. To improve the level of on-product overlay control the number of alignment measurements increases. Since more mask levels will be integrated, more alignment marks need to be printed when using direct-alignment (also called layer-to-layer alignment). Accordingly, the alignment mark size needs to become smaller, to fit all marks into the scribelane. For an in-direct alignment scheme, e.g. a scheme that aligns to another layer than the layer to which overlay is being measured, the number of needed alignment marks can be reduced. Simultaneously there is a requirement to reduce the size of alignment mark sub-segmentations without compromising the alignment and overlay performance. Smaller features within alignment marks can prevent processing issues like erosion, dishing and contamination. However, when the sub-segmentation size within an alignment mark becomes comparable to the critical dimension, and thus smaller than the alignment-illuminating wavelength, polarization effects might start to occur. Polarization effects are a challenge for optical alignment systems to maintain mark detectability. Nevertheless, this paper shows how to actually utilize those effects in order to obtain enhanced alignment and overlay performance to support future technology nodes. Finally, another challenge to be met for new semiconductor product technologies is the ability to align through semi-opaque materials, like for instance new hard-mask materials. Enhancement of alignment signal strength can be reached by adapting to new alignment marks that generate a higher alignment signal. This paper provides a description of an integral alignment solution that meets with these emerging customer application requirements. Complying with these requirements will significantly enhance the flexibility in production strategies while maintaining or improving the alignment and overlay

  8. Development and Utilization of Technology on Indian Mango Fruit Processing

    Directory of Open Access Journals (Sweden)

    Rosenda A. Bronce

    2015-11-01

    Full Text Available This project aimed to develop and utilize technology on Indian mango fruit processing. Chemical properties of matured unripe and ripe Indian mangoes were determined in terms of total sugar, reducing sugar, starch, titratable acidity and pH. Fermentation parameters investigated in the study were amount of sugar added (20 and 25% fermentation medium, acidity of fermentation medium (addition of 1.33 and 1.66 grams of citric acid for ripe and dilution of water for unripe, degree of ripening of Indian mango fruits (ripe and unripe and ageing period (3 and 4 months. Sixteen treatments were done in triplicates and a composite sample was taken from each treatment for sensory evaluation. Results of the preference test were subjected to statistical analysis. The physicochemical properties of Indian mango wine produced using best fermentation parameters were determined. Appropriate packaging material was selected and packaging design was developed for Indian mango wine. Project cooperators were selected and the technology was transferred through training and production runs. Results of preference test showed that the wine with best sensory properties was prepared using matured unripe Indian mango diluted with water and added with 25% sugar. According to the panel of sensory experts, the taste of Indian mango wine was strong with proper blending of sweetness and sourness, its mouth feel was smooth and good balance, aroma was hot pungent and its color and appearance was clear and light yellow. Its titratable acidity was 0.622%, pH was 5, alcohol content was 11% and brix was 5°.

  9. Pure & crystallized 2D Boron Nitride sheets synthesized via a novel process coupling both PDCs and SPS methods

    Science.gov (United States)

    Yuan, Sheng; Linas, Sébastien; Journet, Catherine; Steyer, Philippe; Garnier, Vincent; Bonnefont, Guillaume; Brioude, Arnaud; Toury, Bérangère

    2016-02-01

    Within the context of emergent researches linked to graphene, it is well known that h-BN nanosheets (BNNSs), also referred as 2D BN, are considered as the best candidate for replacing SiO2 as dielectric support or capping layers for graphene. As a consequence, the development of a novel alternative source for highly crystallized h-BN crystals, suitable for a further exfoliation, is a prime scientific issue. This paper proposes a promising approach to synthesize pure and well-crystallized h-BN flakes, which can be easily exfoliated into BNNSs. This new accessible production process represents a relevant alternative source of supply in response to the increasing need of high quality BNNSs. The synthesis strategy to prepare pure h-BN is based on a unique combination of the Polymer Derived Ceramics (PDCs) route with the Spark Plasma Sintering (SPS) process. Through a multi-scale chemical and structural investigation, it is clearly shown that obtained flakes are large (up to 30 μm), defect-free and well crystallized, which are key-characteristics for a subsequent exfoliation into relevant BNNSs.

  10. Influence of Crucible Thermal Conductivity on Crystal Growth in an Industrial Directional Solidification Process for Silicon Ingots

    Directory of Open Access Journals (Sweden)

    Zaoyang Li

    2016-01-01

    Full Text Available We carried out transient global simulations of heating, melting, growing, annealing, and cooling stages for an industrial directional solidification (DS process for silicon ingots. The crucible thermal conductivity is varied in a reasonable range to investigate its influence on the global heat transfer and silicon crystal growth. It is found that the crucible plays an important role in heat transfer, and therefore its thermal conductivity can influence the crystal growth significantly in the entire DS process. Increasing the crucible thermal conductivity can shorten the time for melting of silicon feedstock and growing of silicon crystal significantly, and therefore large thermal conductivity is helpful in saving both production time and power energy. However, the high temperature gradient in the silicon ingots and the locally concave melt-crystal interface shape for large crucible thermal conductivity indicate that high thermal stress and dislocation propagation are likely to occur during both growing and annealing stages. Based on the numerical simulations, some discussions on designing and choosing the crucible thermal conductivity are presented.

  11. University Technology Transfer Information Processing from the Attention Based View

    Science.gov (United States)

    Hamilton, Clovia

    2015-01-01

    Between 2005 and 2011, there was no substantial growth in licenses executed by university technology transfer offices. Since the passage of the Bayh Dole Act of 1980, universities have owned technological inventions afforded by federal research funding. There are still university technology transfer offices that struggle with increasing their…

  12. Process automation using combinations of process and machine control technologies with application to a continuous dissolver

    International Nuclear Information System (INIS)

    Spencer, B.B.; Yarbro, O.O.

    1991-01-01

    Operation of a continuous rotary dissolver, designed to leach uranium-plutonium fuel from chopped sections of reactor fuel cladding using nitric acid, has been automated. The dissolver is a partly continuous, partly batch process that interfaces at both ends with batchwise processes, thereby requiring synchronization of certain operations. Liquid acid is fed and flows through the dissolver continuously, whereas chopped fuel elements are fed to the dissolver in small batches and move through the compartments of the dissolver stagewise. Sequential logic (or machine control) techniques are used to control discrete activities such as the sequencing of isolation valves. Feedback control is used to control acid flowrates and temperatures. Expert systems technology is used for on-line material balances and diagnostics of process operation. 1 ref., 3 figs

  13. Application of reutilization technology to waste from liquid crystal display (LCD) industry.

    Science.gov (United States)

    Liu, Wei T; Li, Kung C

    2010-01-01

    This investigation studies the recycling utility of two major waste products from the liquid crystal display (LCD) industry, panel glass and calcium fluoride sludge, which remain after the treatment of waste water. Waste panel glass was mixed with calcium fluoride sludge in various ratios and then subject to conditioning and melting treatment in order to yield glass-ceramics. Heavy metal leaching tests indicated that reductive conditions lowered the heavy metal concentrations in the leachate to an order of magnitude below that in the waste glass and sludge. A 5:5 (wt%) mixture of glass and sludge melted at 1200 degrees C for 60 min achieves a specific gravity, water absorption, unit mass, porosity ratio, and soundness that meet the American Society for Testing and Materials (ASTM) standard for fine aggregates. Therefore, waste panel glass can indeed be efficiently recycled into a useful construction material.

  14. P2O5-doping in waste glasses: evolution of viscosity and crystallization processes

    Science.gov (United States)

    Tarrago, Mariona; Espuñes, Alex; Garcia-Valles, Maite; Martinez, Salvador

    2015-04-01

    Current concern for environmental preservation is the main motive for the study of new, more sustainable materials. Increasing amounts of sewage sludge are produced in wastewater treatment plants over the world every day. This fact represents a major problem for the municipalities and industries due to the volume of waste and also to the contaminant elements it may bear, which require expensive conditions for disposal in landfills. Vitrification is an established technique in the inertization of different types of toxic wastes (such as nuclear wastes and contaminated soils) that has been used successfully for sewage sludge. Glasses of basaltic composition (43.48SiO2-14.00Al2O3-12.86Fe2O3-10.00CaO-9.94MgO-3.27Na2O-1.96K2O-0.17MnO-0.55P2O5-2.48TiO2) are used as a laboratory analogous of wastes such as sewage sludge and galvanic sludge to study the properties of the inertization matrix. This basaltic matrix is doped by adding 1%, 2%, 3%, 4% and 20% of P5O5 in order to cover the compositional range of phosphate in sewage sludge encountered in the literature. In this study, the focus has been placed in the effect of the concentration of phosphate (P2O5) in glass stability, thermal properties and evolution of viscosity with temperature. The dependence of viscosity on temperature and the thermal behaviour of these glasses are critical parameters in the design of their production process. Regarding the compositional limits of the mixture, it has been observed that melt reactivity is much increased when P2O5 content is over 4%, hindering the glass conformation process. Moreover, stanfieldite (calcium and magnesium phosphate) crystallized during glass making when phosphate concentration approached 20%, hence establishing the upper limit for glass stability. Viscosity is also dramatically increased in this range, hence requiring production amends. Differential thermal analysis has provided nucleation and crystallization temperatures of the glasses around 915°C and 1050

  15. Modeling the Technological Process for Harvesting of Agricultural Produce

    Science.gov (United States)

    Shepelev, S. D.; Shepelev, V. D.; Almetova, Z. V.; Shepeleva, N. P.; Cheskidov, M. V.

    2018-01-01

    The efficiency and the parameters of harvesting as a technological process being substantiated make it possible to reduce the cost of production and increase the profit of enterprises. To increase the efficiency of combine harvesters when the level of technical equipment declines is possible due to their efficient operating modes within daily and every season. Therefore, the correlation between the operational daily time and the seasonal load of combine harvesters is found, with the increase in the seasonal load causing the prolonged duration of operational daily time for harvesters being determined. To increase the efficient time of the seasonal load is possible due to a reasonable ratio of crop varieties according to their ripening periods, the necessary quantity of machines thereby to be reduced up to 40%. By timing and field testing the operational factor of the useful shift time of combine harvesters and the efficient modes of operating machines are defined, with the alternatives for improving the technical readiness of combine harvesters being identified.

  16. Hemimorphite Ores: A Review of Processing Technologies for Zinc Extraction

    Science.gov (United States)

    Chen, Ailiang; Li, Mengchun; Qian, Zhen; Ma, Yutian; Che, Jianyong; Ma, Yalin

    2016-10-01

    With the gradual depletion of zinc sulfide ores, exploration of zinc oxide ores is becoming more and more important. Hemimorphite is a major zinc oxide ore, attracting much attention in the field of zinc metallurgy although it is not the major zinc mineral. This paper presents a critical review of the treatment for extraction of zinc with emphasis on flotation, pyrometallurgical and hydrometallurgical methods based on the properties of hemimorphite. The three-dimensional framework structure of hemimorphite with complex linkage of its structural units lead to difficult desilicification before extracting zinc in the many metallurgical technologies. It is found that the flotation method is generally effective in enriching zinc minerals from hemimorphite ores into a high-grade concentrate for recovery of zinc. Pure zinc can be produced from hemimorphite or/and willemite with a reducing reagent, like methane or carbon. Leaching reagents, such as acid and alkali, can break the complex structure of hemimorphite to release zinc in the leached solution without generation of silica gel in the hydrometallurgical process. For optimal zinc extraction, combing flotation with pyrometallurgical or hydrometallurgical methods may be required.

  17. The process of justifying assisted reproductive technologies in Iran.

    Science.gov (United States)

    Gooshki, Ehsan Shamsi; Allahbedashti, Neda

    2015-01-01

    Infertility is medically defined as one year of unprotected intercourse that does not result in pregnancy. Infertility is a noticeable medical problem in Iran, and about a quarter of Iranian couples experience primary infertility at some point in their lives. Since having children is a basic social value in Iran, infertility has an adverse effect on the health of the couple and affects their well-being. The various methods of assisting infertile couples raise several ethical questions and touch upon certain sensitive points. Although the present Iranian legislative system, which is based on the Shi'a school of Islam, has legalised some aspects of assisted reproductive technologies (ARTs), given the absence of a general officially ratified act (official pathway), such medical interventions are usually justified through a fatwa system (non-official pathway). Officially registered married couples can access almost all ART methods, including third-party gamete donation, if they use such pathways. The process of justifying ART interventions generally began when in vitro fertilisation was given the nod and later, Ayatollah Khamenei (the political-religious leader of the country) issued a fatwa which permitted gamete donation by third parties. This open juristic approach paved the way for the ratification of the Embryo Donation to Infertile Spouses Act in 2003.

  18. Growing Larger Crystals for Neutron Diffraction

    Science.gov (United States)

    Pusey, Marc

    2003-01-01

    Obtaining crystals of suitable size and high quality has been a major bottleneck in macromolecular crystallography. With the advent of advanced X-ray sources and methods the question of size has rapidly dwindled, almost to the point where if one can see the crystal then it was big enough. Quality is another issue, and major national and commercial efforts were established to take advantage of the microgravity environment in an effort to obtain higher quality crystals. Studies of the macromolecule crystallization process were carried out in many labs in an effort to understand what affected the resultant crystal quality on Earth, and how microgravity improved the process. While technological improvements are resulting in a diminishing of the minimum crystal size required, neutron diffraction structural studies still require considerably larger crystals, by several orders of magnitude, than X-ray studies. From a crystal growth physics perspective there is no reason why these 'large' crystals cannot be obtained: the question is generally more one of supply than limitations mechanism. This talk will discuss our laboratory s current model for macromolecule crystal growth, with highlights pertaining to the growth of crystals suitable for neutron diffraction studies.

  19. Crystallization, data collection and processing of the chymotrypsin–BTCI–trypsin ternary complex

    Energy Technology Data Exchange (ETDEWEB)

    Esteves, Gisele Ferreira; Teles, Rozeni Chagas Lima; Cavalcante, Nayara Silva; Neves, David; Ventura, Manuel Mateus [Laboratório de Biofísica, Instituto de Ciências Biológicas, Universidade de Brasília, 70910-900 Brasília-DF (Brazil); Barbosa, João Alexandre Ribeiro Gonçalves, E-mail: joao@lnls.br [Center for Structural Molecular Biology (CeBiME), Brazilian Synchrotron Light Laboratory (LNLS), CP 6192, 13083-970 Campinas-SP (Brazil); Freitas, Sonia Maria de, E-mail: joao@lnls.br [Laboratório de Biofísica, Instituto de Ciências Biológicas, Universidade de Brasília, 70910-900 Brasília-DF (Brazil)

    2007-12-01

    A ternary complex of the proteinase inhibitor (BTCI) with trypsin and chymotrypsin was crystallized and its crystal structure was solved by molecular replacement. A ternary complex of the black-eyed pea trypsin and chymotrypsin inhibitor (BTCI) with trypsin and chymotrypsin was crystallized by the sitting-drop vapour-diffusion method with 0.1 M HEPES pH 7.5, 10%(w/v) polyethylene glycol 6000 and 5%(v/v) 2-methyl-2,4-pentanediol as precipitant. BTCI is a small protein with 83 amino-acid residues isolated from Vigna unguiculata seeds and is able to inhibit trypsin and chymotrypsin simultaneously by forming a stable ternary complex. X-ray data were collected from a single crystal of the trypsin–BTCI–chymotrypsin ternary complex to 2.7 Å resolution under cryogenic conditions. The structure of the ternary complex was solved by molecular replacement using the crystal structures of the BTCI–trypsin binary complex (PDB code) and chymotrypsin (PDB code) as search models.

  20. New technology in everyday life - social processes and environmental impact

    DEFF Research Database (Denmark)

    Røpke, Inge

    2001-01-01

    aspect both of changes in everyday life and of the environmental impact of everyday-life activities. Technological change is often seen as an important part of the solutions to environmental problems, however, when technological change is seen from the perspective of everyday life, this image becomes...... more complex. In this paper technological changes are explored from the perspective of consumption and everyday life, and it is argued that environmental impacts arise through the interplay of technology, consumption and everyday life. Firstly, because technological renewals form integral parts......In the environmental debate it is increasingly acknowledged that our way of life has profound environmental consequences. Therefore, it becomes ever more important to focus on and to understand how everyday life is formed and how it changes over time. Changing technology constitutes an important...