Internal rotation in trifluoromethylsulfur pentafluoride: CF3SF5 by Fourier transform microwave spectroscopy

Science.gov (United States)

Hirota, Eizi; Kawasima, Yoshiyuki; Ajiki, Ken

2017-12-01

Trifluoromethylsulfur pentafluoride CF3SF5, which has been attracting much attention because of its unusually large global warming potential, was investigated by Fourier transform microwave spectroscopy in order to determine the twelve-fold potential barrier to internal rotation in this molecule. We have found the V12 value to be close to zero. Relaxation among internal-rotation and overall-rotation levels was found inhomogeneous, resulting in distributions quite different from thermal in low-temperature molecular beam, which might affect significantly thermodynamic properties of the molecule. Rotational spectra of the 13C species and the 34S species were also observed in natural abundance, leading to the rs Csbnd S bond length of 1.8808 (7) Å.

Design of a Compact Wideband Antenna Array for Microwave Imaging Applications

Directory of Open Access Journals (Sweden)

J. Puskely

2013-12-01

Full Text Available In the paper, wideband antenna arrays aimed at microwave imaging applications and SAR applications operating at Ka band were designed. The antenna array feeding network is realized by a low-loss SIW technology. Moreover, we have replaced the large feed network comprised of various T and Y junctions by a simple broadband network of compact size to more reduce losses in the substrate integrated waveguide and also save space on the PCB. The designed power 8-way divider is complemented by a wideband substrate integrated waveguide to a grounded coplanar waveguide transition and directly connected to the antenna elements. The measured results of antenna array are consistent with our simulation. Obtained results of the developed array demonstrated improvement compared to previously developed binary feed networks with microstrip or SIW splitters.

HIGH-RESOLUTION FOURIER-TRANSFORM MICROWAVE SPECTROSCOPY OF METHYL- AND DIMETHYLNAPTHALENES

Energy Technology Data Exchange (ETDEWEB)

Schnitzler, Elijah G.; Zenchyzen, Brandi L. M.; Jäger, Wolfgang, E-mail: wolfgang.jaeger@ualberta.ca [Department of Chemistry, University of Alberta, Edmonton, Alberta, T6G 2G2 (Canada)

2015-06-01

High-resolution pure rotational spectra of four alkylnaphthalenes were measured in the range of 6–15 GHz using a molecular-beam Fourier-transform microwave spectrometer. Both a- and b-type transitions were observed for 1-methylnaphthalene (1-MN), 1,2-dimethylnaphthalene (1,2-DMN), and 1,3-dimethylnaphthalene (1,3-DMN); only a-type transitions were observed for 2-methylnaphthalene (2-MN). Geometry optimization and vibrational analysis calculations at the B3LYP/6-311++G(d,p) level of theory aided in the assignments of the spectra and the characterization of the structures. Differences between the experimental and predicted rotational constants are small, and they can be attributed in part to low-lying out-of-plane vibrations, which distort the alkylnaphthalenes out of their equilibrium geometries. Splittings of rotational lines due to methyl internal rotation were observed in the spectra of 2-MN, 1,2-DMN, and 1,3-DMN, and allowed for the determination of the barriers to methyl internal rotation, which are compared to values from density functional theory calculations. All four species are moderately polar, so they are candidate species for detection by radio astronomy, by targeting the transition frequencies reported here.

An introduction to Fourier series and integrals

CERN Document Server

Seeley, Robert T

2006-01-01

This compact guide emphasizes the relationship between physics and mathematics, introducing Fourier series in the way that Fourier himself used them: as solutions of the heat equation in a disk. 1966 edition.

Intelligent Controller for a Compact Wide-Band Compositional Infrared Fourier Transform Spectrometer

Science.gov (United States)

Yiu, P.; Keymeulen, D.; Berisford, D. F.; Hand, K. P.; Carlson, R. W.

2013-12-01

This paper presents the design and integration of an intelligent controller for CIRIS (Compositional InfraRed Interferometric Spectrometer) on a stand-alone field programmable gate array (FPGA) architecture. CIRIS is a novel take on traditional Fourier Transform Spectrometers (FTS) and replaces linearly moving mirrors (characteristic of Michelson interferometers) with a constant-velocity rotating refractor to variably phase shift and alter the path length of incoming light. This design eliminates the need for periodically accelerating/decelerating mirrors inherent to canonical Michelson designs and allows for a compact and robust device that is intrinsically radiation-hard, making it ideal for spaceborne measurements in the near-IR to thermal-IR band (2-12 μm) on planetary exploration missions. A traditional Michelson FTS passes a monochromatic light source (incident light from the sample) through a system of refractors/mirrors followed by a mirror moving linearly in the plane of the incident light. This process selectively blocks certain wavelengths and permits measurement of the sample's absorption rates as a function of the wavelengths blocked to produce an 'inteferogram.' This is subsequently processed using a Fourier transform to obtain the sample's spectrum and ascertain the sample's composition. With our prototype CIRIS instrument in development at Design and Prototype Inc. and NASA-JPL, we propose the use of a rotating refractor spinning at a constant velocity to variably phase shift incident light to the detector as an alternative to a linearly moving mirror. This design eliminates sensitivity to vibrations, minimizing path length and non-linear errors due to minor perturbations to the system, in addition to facilitating compact design critical to meeting the strict volume requirements of spacecraft. Further, this is done without sacrificing spectral resolution or throughput when compared to Michelson or diffractive designs. While Michelson designs

A New Compact Octagonal Shape Perfect Metamaterial Absorber for Microwave Applications

Directory of Open Access Journals (Sweden)

Mohammad Jakir Hossain

2017-12-01

Full Text Available A new compact octagonal shape perfect metamaterial absorber (PMA design, numerical simulation, fabrication, and investigational verification of unit cell that is based on a simple structure are presented in this paper. The suggested structure comprised of three layers, in which interact to produce the plasmonic resonances. The finite-integration technique (FIT based Computer Simulation Technology (CST microwave electromagnetic simulator was utilized to examine the design parameters and conduct absorption analysis. The design structure exhibited peak absorption values as 99.64% and 99.95% at frequencies 8.08 GHz and 11.41 GHz, respectively. The absorption characteristics were analysed using the polarization angle of the structure, layer thickness, PMA with resistive load, and number of rings. An N5227A vector network analyser was used for the measurement. The measured results of the fabricated prototype were in good agreement with the simulation results. The suggested perfect absorber structure enables innumerable application aimed at X-band for applications like, defence, security, and stealth technology.

Fourier-like frames on locally compact abelian groups

DEFF Research Database (Denmark)

Christensen, Ole; Goh, Say Song

2015-01-01

We consider a class of functions, defined on a locally compact abelian group by letting a class of modulation operators act on a countable collection of functions. We derive sufficient conditions for such a class of functions to form a Bessel sequence or a frame and for two such systems to be dual...... frames. Explicit constructions are obtained via various generalizations of the classical B-splines to the setting of locally compact abelian groups. (C) 2014 Elsevier Inc. All rights reserved....

Lacunary Fourier Series and a Qualitative Uncertainty Principle for ...

Indian Academy of Sciences (India)

We define lacunary Fourier series on a compact connected semisimple Lie group . If f ∈ L 1 ( G ) has lacunary Fourier series and vanishes on a non empty open subset of , then we prove that vanishes identically. This result can be viewed as a qualitative uncertainty principle.

Effective High-Frequency Permeability of Compacted Metal Powders

Science.gov (United States)

Volkovskaya, I. I.; Semenov, V. E.; Rybakov, K. I.

2018-03-01

We propose a model for determination of the effective complex permeability of compacted metal-powder media. It is based on the equality of the magnetic moment in a given volume of the media with the desired effective permeability to the total magnetic moment of metal particles in the external high-frequency magnetic field, which arises due to excitation of electric eddy currents in the particles. Calculations within the framework of the proposed model allow us to refine the values of the real and imaginary components of the permeability of metal powder compacts in the microwave band. The conditions of applicability of the proposed model are formulated, and their fulfillment is verified for metal powder compacts in the microwave and millimeter wavelength bands.

Surface Fourier-transform lens using a metasurface

International Nuclear Information System (INIS)

Li, Yun Bo; Cai, Ben Geng; Cheng, Qiang; Cui, Tie Jun

2015-01-01

We propose a surface (or 2D) Fourier-transform lens using a gradient refractive index (GRIN) metasurface in the microwave band, which is composed of sub-wavelength quasi-periodical metallic patches on a grounded dielectric substrate. Such a metasurface supports the transverse magnetic (TM) modes of surface waves. To gradually change the size of textures, we obtain different surface refractive indices, which can be tailored to fit the required refractive-index profile of a surface Fourier-transform lens. According to the theory of spatial Fourier transformation, we make use of the proposed lens to realize surface plane-wave scanning under different feeding locations. The simulation and experimental results jointly confirm the validity of the surface Fourier-transform lens. The proposed method can also be extended to the terahertz frequency. (paper)

Metasurface Enabled Wide-Angle Fourier Lens.

Science.gov (United States)

Liu, Wenwei; Li, Zhancheng; Cheng, Hua; Tang, Chengchun; Li, Junjie; Zhang, Shuang; Chen, Shuqi; Tian, Jianguo

2018-06-01

Fourier optics, the principle of using Fourier transformation to understand the functionalities of optical elements, lies at the heart of modern optics, and it has been widely applied to optical information processing, imaging, holography, etc. While a simple thin lens is capable of resolving Fourier components of an arbitrary optical wavefront, its operation is limited to near normal light incidence, i.e., the paraxial approximation, which puts a severe constraint on the resolvable Fourier domain. As a result, high-order Fourier components are lost, resulting in extinction of high-resolution information of an image. Other high numerical aperture Fourier lenses usually suffer from the bulky size and costly designs. Here, a dielectric metasurface consisting of high-aspect-ratio silicon waveguide array is demonstrated experimentally, which is capable of performing 1D Fourier transform for a large incident angle range and a broad operating bandwidth. Thus, the device significantly expands the operational Fourier space, benefitting from the large numerical aperture and negligible angular dispersion at large incident angles. The Fourier metasurface will not only facilitate efficient manipulation of spatial spectrum of free-space optical wavefront, but also be readily integrated into micro-optical platforms due to its compact size. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Fourier Transform Microwave Spectroscopy of Multiconformational Molecules and Van Der Waals Complexes.

Science.gov (United States)

Hight Walker, Angela Renee

1995-01-01

With the use of a Fourier transform microwave (FTM) spectrometer, structural determinations of two types of species; multiconformational molecules and van der Waals complexes, have been performed. Presented in this thesis are three sections summarizing this research effort. The first section contains a detailed explanation of the FTM instrument. In Section II, the study of three multiconformational molecules is presented as two chapters. Finally, three chapters in Section III outline the work still in progress on many van der Waals complexes. Section I was written to be a "manual" for the FTM spectrometer and to aid new additions to the group in their understanding of the instrument. An instruction guide is necessary for home-built instruments such as this one due to their unique design and application. Vital techniques and theories are discussed and machine operation is outlined. A brief explanation of general microwave spectroscopy as performed on an FTM spectrometer is also given. Section II is composed of two chapters pertaining to multiconformational molecules. In Chapter 2, a complete structural analysis of dipropyl ether is reported. The only conformer assigned had C_{rm s} symmetry. Many transitions are yet unassigned. Chapter 3 summarizes an investigation of two nitrosamines; methyl ethyl and methyl propyl nitrosamine. Only one conformer was observed for methyl ethyl nitrosamine, but two were assigned to methyl propyl nitrosamine. Nuclear hyperfine structure and internal methyl rotation complicated the spectra. The final section, Section III, contains the ongoing progress on weakly bound van der Waals complexes. The analysis of the OCS--HBr complex identified the structure as quasi-linear with large amplitude bending motions. Five separate isotopomers were assigned. Transitions originating from the HBr--DBr complex were measured and presented in Chapter 5. Although early in the analysis, the structure was determined to be bent and deuterium bonded. The

Ultra-Compact linear chirped microwave signal generator

DEFF Research Database (Denmark)

Yan, Siqi; Zhou, Feng; Dong, Jianji

2017-01-01

A novel concept to generate linear chirped microwave signal is proposed and experimentally verified. The frequency to time mapping method is used while the Mach-Zehnder interferometer based on the photonic crystal waveguide is employed as the key device with its significant advantages of the ultra...

Microwave heating application in calcination and SYNROC formation

International Nuclear Information System (INIS)

Ambashta, R.D.; Wattal, P.K.; Malav, R.K.; Mallik, G.K.

2006-01-01

Microwave for calcination of titanate based ceramic wasteform (SYNROC) is being reported for the first time in this paper. Although major constituents in SYNROC were non microwave active, the combination with microwave active constituents rendered the mixture calcinable. Calcine was sintered at 1150 degC under hot uniaxial conditions at an applied pressure of ∼30 MPa. XRD shows presence of major phases of SYNROC in the compacted sample. (author)

Design of a Solenoid Magnet for a Microwave Ion Source

International Nuclear Information System (INIS)

Cho, Yong Sub; Kwon, Hyeok Jung; Kim, Dae Il

2011-01-01

A microwave ion source has many advantages, such as long-life time, low emittance, high brightness, and compactness. Also it is a big merit that 2.45GHz rf systems are easily available and inexpensive. Due to the reasons microwave ion sources are very attractive for industrial applications. But microwave ion sources need a solenoid magnet which is usually an electromagnet with a DC current power supply. The electromagnet solenoids of microwave ion sources can be installed in two methods. The first method is to use isolation transformer to supply electrical power to DC current power supply for the magnets. In this case the magnet is compact because it has the same potential with the extraction voltage. The second method is to put an electrical insulator, such as G10, between ion sources and magnets. In this case the solenoid magnet is bigger than one in the first method, especially for higher extraction voltage, because the space for the insulator is required. Permanent magnets can be a good candidate to make microwave ion source more compact. But it is difficult to control the magnetic field profile and the magnetic flux density for the permanent magnet solenoids. Due to the reason, in the case that the best performances in many operating conditions should be achieved by adjusting the profile and strength of the solenoid, electromagnet is better than permanent magnet. But in the case of industrial applications where operating conditions is usually fixed and the compactness is required, permanent magnet is better choice to build an ion source

Trends of microwave dielectric materials for antenna application

International Nuclear Information System (INIS)

Sulong, T. A. T.; Osman, R. A. M.; Idris, M. S.

2016-01-01

Rapid development of a modern microwave communication system requires a high quality microwave dielectric ceramic material to be used as mobile and satellite communication. High permittivity of dielectric ceramics leads to fabrication of compact device for electronic components. Dielectric ceramics which used for microwave applications required three important parameters such as high or appropriate permittivity (ε_r), high quality factor (Q _f ≥ 5000 GH z) and good temperature coefficient of resonant frequency (τ_f). This paper review of various dielectric ceramic materials used as microwave dielectric materials and related parameters for antenna applications.

Trends of microwave dielectric materials for antenna application

Energy Technology Data Exchange (ETDEWEB)

Sulong, T. A. T., E-mail: tuanamirahtuansulong@gmail.com; Osman, R. A. M., E-mail: rozana@unimap.edu.my [School of Microelectronic Engineering, Universiti Malaysia Perlis, Pauh Putra Campus, 02600 Arau, Perlis (Malaysia); Idris, M. S., E-mail: sobri@unimap.edu.my [Sustainable Engineering Research Cluster, School of Material Engineering, Universiti Malaysia Perlis, Blok B, Taman Pertiwi Indah, Seriab, 01000 Kangar, Perlis (Malaysia)

2016-07-19

Rapid development of a modern microwave communication system requires a high quality microwave dielectric ceramic material to be used as mobile and satellite communication. High permittivity of dielectric ceramics leads to fabrication of compact device for electronic components. Dielectric ceramics which used for microwave applications required three important parameters such as high or appropriate permittivity (ε{sub r}), high quality factor (Q {sub f} ≥ 5000 GH z) and good temperature coefficient of resonant frequency (τ{sub f}). This paper review of various dielectric ceramic materials used as microwave dielectric materials and related parameters for antenna applications.

A Fourier analysis for a fast simulation algorithm. [for switching converters

Science.gov (United States)

King, Roger J.

1988-01-01

This paper presents a derivation of compact expressions for the Fourier series analysis of the steady-state solution of a typical switching converter. The modeling procedure for the simulation and the steady-state solution is described, and some desirable traits for its matrix exponential subroutine are discussed. The Fourier analysis algorithm was tested on a phase-controlled parallel-loaded resonant converter, providing an experimental confirmation.

Monolithic Microwave Integrated Circuits Based on GaAs Mesfet Technology

Science.gov (United States)

Bahl, Inder J.

Advanced military microwave systems are demanding increased integration, reliability, radiation hardness, compact size and lower cost when produced in large volume, whereas the microwave commercial market, including wireless communications, mandates low cost circuits. Monolithic Microwave Integrated Circuit (MMIC) technology provides an economically viable approach to meeting these needs. In this paper the design considerations for several types of MMICs and their performance status are presented. Multifunction integrated circuits that advance the MMIC technology are described, including integrated microwave/digital functions and a highly integrated transceiver at C-band.

A Review on Passive and Integrated Near-Field Microwave Biosensors

Science.gov (United States)

Guha, Subhajit; Jamal, Farabi Ibne

2017-01-01

In this paper we review the advancement of passive and integrated microwave biosensors. The interaction of microwave with biological material is discussed in this paper. Passive microwave biosensors are microwave structures, which are fabricated on a substrate and are used for sensing biological materials. On the other hand, integrated biosensors are microwave structures fabricated in standard semiconductor technology platform (CMOS or BiCMOS). The CMOS or BiCMOS sensor technology offers a more compact sensing approach which has the potential in the future for point of care testing systems. Various applications of the passive and the integrated sensors have been discussed in this review paper. PMID:28946617

Package Holds Five Monolithic Microwave Integrated Circuits

Science.gov (United States)

Mysoor, Narayan R.; Decker, D. Richard; Olson, Hilding M.

1996-01-01

Packages protect and hold monolithic microwave integrated circuit (MMIC) chips while providing dc and radio-frequency (RF) electrical connections for chips undergoing development. Required to be compact, lightweight, and rugged. Designed to minimize undesired resonances, reflections, losses, and impedance mismatches.

Microwave superheaters for fusion

International Nuclear Information System (INIS)

Campbell, R.B.; Hoffman, M.A.; Logan, B.G.

1987-01-01

The microwave superheater uses the synchrotron radiation from a thermonuclear plasma to heat gas seeded with an alkali metal to temperatures far above the temperature of material walls. It can improve the efficiency of the Compact Fusion Advanced Rankine (CFAR) cycle described elsewhere in these proceedings. For a proof-of-principle experiment using helium, calculations show that a gas superheat ΔT of 2000 0 K is possible when the wall temperature is maintained at 1000 0 K. The concept can be scaled to reactor grade systems. Because of the need for synchrotron radiation, the microwave superheater is best suited for use with plasmas burning an advanced fuel such as D- 3 He. 5 refs

Compact continuous HF microwave-discharge mixing laser

International Nuclear Information System (INIS)

Gagne, J.M.; Bertrand, L.; Conturie, Y.; Mah, S.Q.; Monchalin, J.P.

1975-01-01

The performance of a continuous chemical laser is discussed. Fluorine atoms are produced in a SF 6 + He mixture by means of a microwave-discharge apparatus that operates in a continuous mode. A maximum output power of 4 W is obtained for a 5 cm length of amplifying medium; this power output is primarily due to P transitions from the 1-0 and 2-1 bands. Weak transitions in the 3-2 band are also observed. The maximum value of measured gain is 0.11 cm -1 ; good agreement is obtained between theoretical and experimental values of gain. (auth)

Development of a High-Throughput Microwave Imaging System for Concealed Weapons Detection

Science.gov (United States)

2016-07-15

hardware. Index Terms—Microwave imaging, multistatic radar, Fast Fourier Transform (FFT). I. INTRODUCTION Near-field microwave imaging is a non- ionizing ...real-time microwave camera at 24 ghz,” IEEE Transactions on Antennas and Propagation , vol. 60, no. 2, pp. 1114– 1125, 2012. [2] E. C. Fear, X. Li, S. C...on Biomedical Engineering, vol. 49, no. 8, pp. 812–822, 2002. [3] D. M. Sheen, D. L. McMakin, and T. E. Hall, “Three-dimensional millimeter- wave

On frame properties for Fourier-like systems

DEFF Research Database (Denmark)

Christensen, Ole; Osgooei, Elnaz

2013-01-01

Fourier-like systems are formed by multiplying a class of exponentials with a set of window functions. Via the Fourier transform they are equivalent to shift-invariant systems. We present sufficient and easily verifiable conditions for such systems to form a frame with a dual frame having the same...... structure. An attractive class of frames is formed by letting the window functions be trigonometric polynomials, restricted to compact intervals. We prove, under weak conditions, that such systems generate a frame with a dual that is also generated by a trigonometric polynomial. For polynomial windows......, a result of this type does not hold. Throughout the paper the results are related to the well established theory for Gabor systems....

Continuous microwave flow synthesis of mesoporous hydroxyapatite

International Nuclear Information System (INIS)

Akram, Muhammad; Alshemary, Ammar Z.; Goh, Yi-Fan; Wan Ibrahim, Wan Aini; Lintang, Hendrik O.; Hussain, Rafaqat

2015-01-01

We have successfully used continuous microwave flow synthesis (CMFS) technique for the template free synthesis of mesoporous hydroxyapatite. The continuous microwave flow reactor consisted of a modified 2.45 GHz household microwave, peristaltic pumps and a Teflon coil. This cost effective and efficient system was exploited to produce semi-crystalline phase pure nano-sized hydroxyapatite. Effect of microwave power, retention time and the concentration of reactants on the phase purity, degree of crystallinity and surface area of the final product was studied in detail. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) were used to study the phase purity and composition of the product, while transmission electron microscopy (TEM) was used to study the effect of process parameters on the morphology of hydroxyapatite. The TEM analysis confirmed the formation of spherical particles at low microwave power; however the morphology of the particles changed to mesoporous needle and rod-like structure upon exposing the reaction mixture to higher microwave power and longer retention time inside the microwave. The in-vitro ion dissolution behavior of the as synthesized hydroxyapatite was studied by determining the amount of Ca 2+ ion released in SBF solution. - Highlights: • Continuous microwave flow synthesis method was used to prepare hydroxyapatite. • Increase in microwave power enhanced the degree of crystallinity. • TEM images confirmed the presence of mesopores on the surface of HA

Continuous microwave flow synthesis of mesoporous hydroxyapatite

Energy Technology Data Exchange (ETDEWEB)

Akram, Muhammad; Alshemary, Ammar Z.; Goh, Yi-Fan; Wan Ibrahim, Wan Aini [Department of Chemistry, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor (Malaysia); Lintang, Hendrik O. [Centre for Sustainable Nanomaterials (CSNano), Ibnu Sina Institute for Scientific and Industrial Research, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor (Malaysia); Hussain, Rafaqat, E-mail: rafaqat@kimia.fs.utm.my [Centre for Sustainable Nanomaterials (CSNano), Ibnu Sina Institute for Scientific and Industrial Research, Universiti Teknologi Malaysia, 81310 UTM Johor Bahru, Johor (Malaysia)

2015-11-01

We have successfully used continuous microwave flow synthesis (CMFS) technique for the template free synthesis of mesoporous hydroxyapatite. The continuous microwave flow reactor consisted of a modified 2.45 GHz household microwave, peristaltic pumps and a Teflon coil. This cost effective and efficient system was exploited to produce semi-crystalline phase pure nano-sized hydroxyapatite. Effect of microwave power, retention time and the concentration of reactants on the phase purity, degree of crystallinity and surface area of the final product was studied in detail. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) were used to study the phase purity and composition of the product, while transmission electron microscopy (TEM) was used to study the effect of process parameters on the morphology of hydroxyapatite. The TEM analysis confirmed the formation of spherical particles at low microwave power; however the morphology of the particles changed to mesoporous needle and rod-like structure upon exposing the reaction mixture to higher microwave power and longer retention time inside the microwave. The in-vitro ion dissolution behavior of the as synthesized hydroxyapatite was studied by determining the amount of Ca{sup 2+} ion released in SBF solution. - Highlights: • Continuous microwave flow synthesis method was used to prepare hydroxyapatite. • Increase in microwave power enhanced the degree of crystallinity. • TEM images confirmed the presence of mesopores on the surface of HA.

Recent advances in processing and applications of microwave ferrites

International Nuclear Information System (INIS)

Harris, Vincent G.; Geiler, Anton; Chen Yajie; Yoon, Soack Dae; Wu Mingzhong; Yang, Aria; Chen Zhaohui; He Peng; Parimi, Patanjali V.; Zuo Xu; Patton, Carl E.; Abe, Manasori; Acher, Olivier

2009-01-01

Next generation magnetic microwave devices will be planar, smaller, weigh less, and perform well beyond the present state-of-the-art. For this to become a reality advances in ferrite materials must first be realized. These advances include self-bias magnetization, tunability of the magnetic anisotropy, low microwave loss, and volumetric and weight reduction. To achieve these goals one must turn to novel materials processing methods. Here, we review recent advances in the processing of microwave ferrites. Attention is paid to the processing of ferrite films by pulsed laser deposition, liquid phase epitaxy, spin spray ferrite plating, screen printing, and compaction of quasi-single crystals. Conventional and novel applications of ferrite materials, including microwave non-reciprocal passive devices, microwave signal processing, negative index metamaterial-based electronics, and electromagnetic interference suppression are discussed.

Continuous microwave flow synthesis of mesoporous hydroxyapatite.

Science.gov (United States)

Akram, Muhammad; Alshemary, Ammar Z; Goh, Yi-Fan; Wan Ibrahim, Wan Aini; Lintang, Hendrik O; Hussain, Rafaqat

2015-11-01

We have successfully used continuous microwave flow synthesis (CMFS) technique for the template free synthesis of mesoporous hydroxyapatite. The continuous microwave flow reactor consisted of a modified 2.45GHz household microwave, peristaltic pumps and a Teflon coil. This cost effective and efficient system was exploited to produce semi-crystalline phase pure nano-sized hydroxyapatite. Effect of microwave power, retention time and the concentration of reactants on the phase purity, degree of crystallinity and surface area of the final product was studied in detail. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) were used to study the phase purity and composition of the product, while transmission electron microscopy (TEM) was used to study the effect of process parameters on the morphology of hydroxyapatite. The TEM analysis confirmed the formation of spherical particles at low microwave power; however the morphology of the particles changed to mesoporous needle and rod-like structure upon exposing the reaction mixture to higher microwave power and longer retention time inside the microwave. The in-vitro ion dissolution behavior of the as synthesized hydroxyapatite was studied by determining the amount of Ca(2+) ion released in SBF solution. Copyright © 2015 Elsevier B.V. All rights reserved.

A monolithic integrated photonic microwave filter

Science.gov (United States)

Fandiño, Javier S.; Muñoz, Pascual; Doménech, David; Capmany, José

2017-02-01

Meeting the increasing demand for capacity in wireless networks requires the harnessing of higher regions in the radiofrequency spectrum, reducing cell size, as well as more compact, agile and power-efficient base stations that are capable of smoothly interfacing the radio and fibre segments. Fully functional microwave photonic chips are promising candidates in attempts to meet these goals. In recent years, many integrated microwave photonic chips have been reported in different technologies. To the best of our knowledge, none has monolithically integrated all the main active and passive optoelectronic components. Here, we report the first demonstration of a tunable microwave photonics filter that is monolithically integrated into an indium phosphide chip. The reconfigurable radiofrequency photonic filter includes all the necessary elements (for example, lasers, modulators and photodetectors), and its response can be tuned by means of control electric currents. This is an important step in demonstrating the feasibility of integrated and programmable microwave photonic processors.

CMB in a box: Causal structure and the Fourier-Bessel expansion

International Nuclear Information System (INIS)

Abramo, L. Raul; Reimberg, Paulo H.; Xavier, Henrique S.

2010-01-01

This paper makes two points. First, we show that the line-of-sight solution to cosmic microwave anisotropies in Fourier space, even though formally defined for arbitrarily large wavelengths, leads to position-space solutions which only depend on the sources of anisotropies inside the past light cone of the observer. This foretold manifestation of causality in position (real) space happens order by order in a series expansion in powers of the visibility γ=e -μ , where μ is the optical depth to Thomson scattering. We show that the contributions of order γ N to the cosmic microwave background (CMB) anisotropies are regulated by spacetime window functions which have support only inside the past light cone of the point of observation. Second, we show that the Fourier-Bessel expansion of the physical fields (including the temperature and polarization momenta) is an alternative to the usual Fourier basis as a framework to compute the anisotropies. The viability of the Fourier-Bessel series for treating the CMB is a consequence of the fact that the visibility function becomes exponentially small at redshifts z>>10 3 , effectively cutting off the past light cone and introducing a finite radius inside which initial conditions can affect physical observables measured at our position x-vector=0 and time t 0 . Hence, for each multipole l there is a discrete tower of momenta k il (not a continuum) which can affect physical observables, with the smallest momenta being k 1l ∼l. The Fourier-Bessel modes take into account precisely the information from the sources of anisotropies that propagates from the initial value surface to the point of observation - no more, no less. We also show that the physical observables (the temperature and polarization maps), and hence the angular power spectra, are unaffected by that choice of basis. This implies that the Fourier-Bessel expansion is the optimal scheme with which one can compute CMB anisotropies.

Miniaturized Fourier-plane fiber scanner for OCT endoscopy

International Nuclear Information System (INIS)

Vilches, Sergio; Kretschmer, Simon; Ataman, Çağlar; Zappe, Hans

2017-01-01

A forward-looking endoscopic optical coherence tomography (OCT) probe featuring a Fourier-plane fiber scanner is designed, manufactured and characterized. In contrast to common image-plane fiber scanners, the Fourier-plane scanner is a telecentric arrangement that eliminates vignetting and spatial resolution variations across the image plane. To scan the OCT beam in a spiral pattern, a tubular piezoelectric actuator is used to resonate an optical fiber bearing a collimating GRIN lens at its tip. The free-end of the GRIN lens sits at the back focal plane of an objective lens, such that its rotation replicates the beam angles in the collimated region of a classical telecentric 4f optical system. Such an optical arrangement inherently has a low numerical aperture combined with a relatively large field-of-view, rendering it particularly useful for endoscopic OCT imaging. Furthermore, the optical train of the Fourier-plane scanner is shorter than that of a comparable image-plane scanner by one focal length of the objective lens, significantly shortening the final arrangement. As a result, enclosed within a 3D printed housing of 2.5 mm outer diameter and 15 mm total length, the developed probe is the most compact forward-looking endoscopic OCT imager to date. Due to its compact form factor and compatibility with real-time OCT imaging, the developed probe is also ideal for use in the working channel of flexible endoscopes as a potential optical biopsy tool. (paper)

Miniaturized Fourier-plane fiber scanner for OCT endoscopy

Science.gov (United States)

Vilches, Sergio; Kretschmer, Simon; Ataman, Çağlar; Zappe, Hans

2017-10-01

A forward-looking endoscopic optical coherence tomography (OCT) probe featuring a Fourier-plane fiber scanner is designed, manufactured and characterized. In contrast to common image-plane fiber scanners, the Fourier-plane scanner is a telecentric arrangement that eliminates vignetting and spatial resolution variations across the image plane. To scan the OCT beam in a spiral pattern, a tubular piezoelectric actuator is used to resonate an optical fiber bearing a collimating GRIN lens at its tip. The free-end of the GRIN lens sits at the back focal plane of an objective lens, such that its rotation replicates the beam angles in the collimated region of a classical telecentric 4f optical system. Such an optical arrangement inherently has a low numerical aperture combined with a relatively large field-of-view, rendering it particularly useful for endoscopic OCT imaging. Furthermore, the optical train of the Fourier-plane scanner is shorter than that of a comparable image-plane scanner by one focal length of the objective lens, significantly shortening the final arrangement. As a result, enclosed within a 3D printed housing of 2.5 mm outer diameter and 15 mm total length, the developed probe is the most compact forward-looking endoscopic OCT imager to date. Due to its compact form factor and compatibility with real-time OCT imaging, the developed probe is also ideal for use in the working channel of flexible endoscopes as a potential optical biopsy tool.

The total column of CO2 and CH4 measured with a compact Fourier transform spectrometer at NASA Armstrong Flight Research Center and Railroad Valley, Nevada, USA

Science.gov (United States)

Kawakami, S.; Shiomi, K.; Suto, H.; Kuze, A.; Hillyard, P. W.; Tanaka, T.; Podolske, J. R.; Iraci, L. T.; Albertson, R. T.

2014-12-01

The total columns of carbon dioxide (XCO2) and methane (XCH4) were measured with a compact Fourier transform spectrometer (FTS) at NASA Armstrong Flight Research Center (AFRC) and Railroad Valley, Nevada, USA (RRV) during a vicarious calibration campaign in June 2014. The campaign was performed to estimate changes in the radiometric response of the Thermal and Near Infrared Sensor for carbon Observations Fourier Transform Spectrometer (TANSO-FTS) and the Cloud and Aerosol Imager (TANSO-CAI) aboard Greenhouse gases Observing SATellite (GOSAT). TANSO-FTS measures spectra of radiance scattered by the Earth surface with high- and medium-gain depending on the surface reflectance. At high reflectance areas, such as deserts over north Africa and Australia, TANSO-FTS collects spectra with medium-gain. There was differences on atmospheric pressure and XCO2 retrieved from spectra obtained between high-gain and medium-gain. Because the retrieved products are useful for evaluating the difference of spectral qualities between high- and medium-gain, this work is an attempt to collect validation data for spectra with medium-gain of TANSO-FTS at remote and desert area with a compact and medium-spectral resolution instrument. As a compact FTS, EM27/SUN was used. It was manufactured and newly released on April 1, 2014 by Bruker. It is robust and operable in a high temperature environment. It was housed in a steel box to protect from dust and rain and powered by Solar panels. It can be operated by such a remote and desert area, like a RRV. Over AFRC and RRV, vertical profiles of CO2 and CH4 were measured using the Alpha Jet research aircraft as part of the Alpha Jet Atmospheric eXperiment (AJAX) of ARC, NASA. The values were calibrated to standard gases. To make the results comparable to WMO (World Meteorological Organization) standards, the retrieved XCO2 and XCH4 values are divided by a calibration factor. This values were determined by comparisons with in situ profiles measured by

Vibrational analysis of Fourier transform spectrum of the B 3− u (0

Indian Academy of Sciences (India)

... microwave, was recorded on BOMEM DA8 Fourier transform spectrometer at an apodized resolution of 0.035 cm-1. Vibrational constants were improved by putting the wave number of band origins in Deslandre table. The vibrational analysis was supported by determining the Franck–Condon factor and -centroid values.

RF Testing Of Microwave Integrated Circuits

Science.gov (United States)

Romanofsky, R. R.; Ponchak, G. E.; Shalkhauser, K. A.; Bhasin, K. B.

1988-01-01

Fixtures and techniques are undergoing development. Four test fixtures and two advanced techniques developed in continuing efforts to improve RF characterization of MMIC's. Finline/waveguide test fixture developed to test submodules of 30-GHz monolithic receiver. Universal commercially-manufactured coaxial test fixture modified to enable characterization of various microwave solid-state devices in frequency range of 26.5 to 40 GHz. Probe/waveguide fixture is compact, simple, and designed for non destructive testing of large number of MMIC's. Nondestructive-testing fixture includes cosine-tapered ridge, to match impedance wavequide to microstrip. Advanced technique is microwave-wafer probing. Second advanced technique is electro-optical sampling.

Compact antennas for wireless communications and terminals theory and design

CERN Document Server

Laheurte, Jean-Marc

2012-01-01

Compact Antennas for Wireless Communications and Terminals deals with compact microwave antennas and, more specifically, with the planar version of these antennas. Planar antennas are the most appropriate type of antenna in modern communication systems and more generally in all applications requiring miniaturization, integration and conformation such as in mobile phone handsets.The book is suitable for students, engineers and scientists eager to understand the principles of planar and small antennas, their design and fabrication issues, and modern aspects such as UWB antennas, recon

Study of additive manufactured microwave cavities for pulsed optically pumped atomic clock applications

Science.gov (United States)

Affolderbach, C.; Moreno, W.; Ivanov, A. E.; Debogovic, T.; Pellaton, M.; Skrivervik, A. K.; de Rijk, E.; Mileti, G.

2018-03-01

Additive manufacturing (AM) of passive microwave components is of high interest for the cost-effective and rapid prototyping or manufacture of devices with complex geometries. Here, we present an experimental study on the properties of recently demonstrated microwave resonator cavities manufactured by AM, in view of their applications to high-performance compact atomic clocks. The microwave cavities employ a loop-gap geometry using six electrodes. The critical electrode structures were manufactured monolithically using two different approaches: Stereolithography (SLA) of a polymer followed by metal coating and Selective Laser Melting (SLM) of aluminum. The tested microwave cavities show the desired TE011-like resonant mode at the Rb clock frequency of ≈6.835 GHz, with a microwave magnetic field highly parallel to the quantization axis across the vapor cell. When operated in an atomic clock setup, the measured atomic Rabi oscillations are comparable to those observed for conventionally manufactured cavities and indicate a good uniformity of the field amplitude across the vapor cell. Employing a time-domain Ramsey scheme on one of the SLA cavities, high-contrast (34%) Ramsey fringes are observed for the Rb clock transition, along with a narrow (166 Hz linewidth) central fringe. The measured clock stability of 2.2 × 10-13 τ-1/2 up to the integration time of 30 s is comparable to the current state-of-the-art stabilities of compact vapor-cell clocks based on conventional microwave cavities and thus demonstrates the feasibility of the approach.

Synthesis of nitrogen-doped graphene via solid microwave method

Energy Technology Data Exchange (ETDEWEB)

Zhang, Li, E-mail: zhangli379@sohu.com [School of Electrical Engineering, Dalian University of Technology, Dalian, Liaoning 116024 (China); Ji, Bingcheng, E-mail: debbo.jee@outlook.com [School of Electrical Engineering, Dalian University of Technology, Dalian, Liaoning 116024 (China); Wang, Kai [School of Electrical Engineering, Dalian University of Technology, Dalian, Liaoning 116024 (China); Song, Jinyan [School of Information Engineering, Dalian Ocean University, Dalian, Liaoning 116024 (China)

2014-07-01

Graphical abstract: - Highlights: • A direct solid microwave method is developed to prepare nitrogen-doped graphene. • The method consists of two steps, namely the functionalization and microwave irradiation. • Melamine can serve as not only functionalizing agent but also nitrogen source. - Abstract: In this paper, we propose a solid microwave-mediated method for scalable production of nitrogen-doped graphene sheets (NGS) using low-cost industrial material melamine as functionalizing agent and nitrogen source. The strong interaction of microwaves with graphene oxide has been fully utilized to generate in situ heating that induces the decompose melamine and nitrogen doping of graphene. The morphology, structure, and components of the as-produced nitrogen-doped graphene are characterized by scanning electron microscopy (SEM), transmission electron microscope (TEM), Brunauer–Emmett–Teller (BET), pore-size distribution (PSD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectra (XPS), X-ray diffraction (XRD), and Raman spectroscopy. The results show NGS can be successfully synthesized via this strategy.

Synthesis of nitrogen-doped graphene via solid microwave method

International Nuclear Information System (INIS)

Zhang, Li; Ji, Bingcheng; Wang, Kai; Song, Jinyan

2014-01-01

Graphical abstract: - Highlights: • A direct solid microwave method is developed to prepare nitrogen-doped graphene. • The method consists of two steps, namely the functionalization and microwave irradiation. • Melamine can serve as not only functionalizing agent but also nitrogen source. - Abstract: In this paper, we propose a solid microwave-mediated method for scalable production of nitrogen-doped graphene sheets (NGS) using low-cost industrial material melamine as functionalizing agent and nitrogen source. The strong interaction of microwaves with graphene oxide has been fully utilized to generate in situ heating that induces the decompose melamine and nitrogen doping of graphene. The morphology, structure, and components of the as-produced nitrogen-doped graphene are characterized by scanning electron microscopy (SEM), transmission electron microscope (TEM), Brunauer–Emmett–Teller (BET), pore-size distribution (PSD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectra (XPS), X-ray diffraction (XRD), and Raman spectroscopy. The results show NGS can be successfully synthesized via this strategy

Multiband Rectenna for Microwave Applications Rectenna

OpenAIRE

Okba , Abderrahim; Takacs , Alexandru; Aubert , Hervé; Charlot , Samuel; Calmon , Pierre-François

2016-01-01

International audience; This paper reports a multiband rectenna (rectifier + antenna) suitable for the electromagnetic energy harvesting of the spill-over loss of microwave antennas placed on board of geostationary satellites. Such rectenna is used for powering autonomous wireless sensors for satellite health monitoring. The topology of the rectenna is presented. The experimental results demonstrate that the proposed compact rectenna can harvest efficiently the incident electromagnetic energy...

Infrared and microwave properties of polypyrrole/multi-walled carbon nanotube composites

Energy Technology Data Exchange (ETDEWEB)

Gao, Qi; Wang, Yongsheng, E-mail: yshwang@bjtu.edu.cn; He, Dawei, E-mail: dwhe@bjtu.edu.cn; Gao, Lei; Zhou, Yikang; Fu, Ming

2014-08-01

This study analyses the formation of polypyrrole/multi-walled carbon nanotube (PPy/MWCNT) composite materials using chemical oxidation with varying amounts of MWCNTs added. The samples are characterized by scanning electron microscopy, Fourier transform infrared emission spectroscopy, a four-probe method, and infrared thermal imaging using electromagnetic parameters. According to the test results, it is seen that the formation of PPy with the addition of MWCNTs can affect the material’s infrared properties and increase the material’s microwave return losses (up to −19 dB). This production procedure can also make the peak frequency of the microwave return losses adjustable, and the composite’s infrared and microwave performance becomes compatible and adjustable. - Highlights: • A one step in-situ synthesis method of PPy/MWCNT polymerization is proposed. • The composites were used for infrared camouflage and for their microwave properties. • The microwave return losses and infrared emissivity of the composites are adjustable. • The mechanism relies on changes in the composites’ conductivity.

Infrared and microwave properties of polypyrrole/multi-walled carbon nanotube composites

International Nuclear Information System (INIS)

Gao, Qi; Wang, Yongsheng; He, Dawei; Gao, Lei; Zhou, Yikang; Fu, Ming

2014-01-01

This study analyses the formation of polypyrrole/multi-walled carbon nanotube (PPy/MWCNT) composite materials using chemical oxidation with varying amounts of MWCNTs added. The samples are characterized by scanning electron microscopy, Fourier transform infrared emission spectroscopy, a four-probe method, and infrared thermal imaging using electromagnetic parameters. According to the test results, it is seen that the formation of PPy with the addition of MWCNTs can affect the material’s infrared properties and increase the material’s microwave return losses (up to −19 dB). This production procedure can also make the peak frequency of the microwave return losses adjustable, and the composite’s infrared and microwave performance becomes compatible and adjustable. - Highlights: • A one step in-situ synthesis method of PPy/MWCNT polymerization is proposed. • The composites were used for infrared camouflage and for their microwave properties. • The microwave return losses and infrared emissivity of the composites are adjustable. • The mechanism relies on changes in the composites’ conductivity

Microwave Imaging Sensor Using Compact Metamaterial UWB Antenna with a High Correlation Factor

Directory of Open Access Journals (Sweden)

Md. Moinul Islam

2015-07-01

Full Text Available The design of a compact metamaterial ultra-wideband (UWB antenna with a goal towards application in microwave imaging systems for detecting unwanted cells in human tissue, such as in cases of breast cancer, heart failure and brain stroke detection is proposed. This proposed UWB antenna is made of four metamaterial unit cells, where each cell is an integration of a modified split ring resonator (SRR, capacitive loaded strip (CLS and wire, to attain a design layout that simultaneously exhibits both a negative magnetic permeability and a negative electrical permittivity. This design results in an astonishing negative refractive index that enables amplification of the radiated power of this reported antenna, and therefore, high antenna performance. A low-cost FR4 substrate material is used to design and print this reported antenna, and has the following characteristics: thickness of 1.6 mm, relative permeability of one, relative permittivity of 4.60 and loss tangent of 0.02. The overall antenna size is 19.36 mm × 27.72 mm × 1.6 mm where the electrical dimension is 0.20 λ × 0.28 λ × 0.016 λ at the 3.05 GHz lower frequency band. Voltage Standing Wave Ratio (VSWR measurements have illustrated that this antenna exhibits an impedance bandwidth from 3.05 GHz to more than 15 GHz for VSWR < 2 with an average gain of 4.38 dBi throughout the operating frequency band. The simulations (both HFSS and computer simulation technology (CST and the measurements are in high agreement. A high correlation factor and the capability of detecting tumour simulants confirm that this reported UWB antenna can be used as an imaging sensor.

The Microwave Spectrum of Methyl Vinyl Ketone Revisited

Science.gov (United States)

Wilcox, David S.; Shirar, Amanda J.; Williams, Owen L.; Dian, Brian C.

2011-06-01

A chirped-pulse Fourier transform microwave spectrometer was used to record the rotational spectrum of methyl vinyl ketone (MVK, 3-butene-2-one) from 6 to 18.9 GHz. Two stable conformations were identified: the previously documented antiperiplanar (ap) conformer and synperiplanar (sp), which is reported for the first time in this microwave study. Methyl torsional analysis with XIAM resulted in V3 barrier heights of 433.8(1) and 376.6(2) Cm-1 for ap- and sp-MVK, respectively. Heavy atom isotopic species were detected in natural abundance allowing bond lengths and angles of the molecular frames to be calculated through Kraitchman analysis. A comparison with ab initio calculations is included.

Photoluminescence enhancement of porous silicon particles by microwave-assisted activation

Energy Technology Data Exchange (ETDEWEB)

Xia, Bing [Key Laboratory of Forest Genetics and Biotechnology (Ministry of Education of China), Nanjing Forestry University, Nanjing 210037 (China); Advanced Analysis and Testing Center, Nanjing Forestry University, Nanjing 210037 (China); Zhang, Wenyi; Dong, Chen; Shi, Jisen [Key Laboratory of Forest Genetics and Biotechnology (Ministry of Education of China), Nanjing Forestry University, Nanjing 210037 (China); Bao, Weiyi [Advanced Analysis and Testing Center, Nanjing Forestry University, Nanjing 210037 (China); Zhang, Junfeng [State Key Laboratory of Pharmaceutical Biotechnology, School of Life Sciences, Nanjing University, Nanjing 210093 (China)

2012-11-15

Photoluminescence (PL) of porous silicon (PSi) particles can be significantly enhanced in some organic solvents (i.e., ethanol or dimethyl sulfoxide) under microwave irradiation. Fourier transform infrared spectra, dynamic-light-scattering measurements, and scanning electron microscopy had been adopted to explore the mechanism of PL enhancement of PSi particles under microwave irradiation, which is attributed to the formation of higher porosity and the growth of silicon oxide by microwave-assisted wet etching. Compared with that fabricated by ultrasonication, smaller luminescent PSi nanoparticles (average size {proportional_to}60 nm) with stronger orange-red fluorescence (PL quantum yield {proportional_to}14.8%) and higher dispersibility can be large-scale prepared for cellular imaging and drug delivery in biomedical applications. (Copyright copyright 2012 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

Microwave-assisted acid pretreatment of alkali lignin: Effect on characteristics and pyrolysis behavior.

Science.gov (United States)

Duan, Dengle; Ruan, Roger; Wang, Yunpu; Liu, Yuhuan; Dai, Leilei; Zhao, Yunfeng; Zhou, Yue; Wu, Qiuhao

2018-03-01

This study performed microwave-assisted acid pretreatment on pure lignin. The effects of microwave temperature, microwave time, and hydrochloric acid concentration on characteristics and pyrolysis behavior of lignin were examined. Results of ultimate analysis revealed better properties of all pretreated samples than those of raw lignin. Fourier transform infrared spectroscopy analysis showed breakage of βO4 bond and aliphatic side chain, decrease in OH groups, and formation of CO groups in pretreatment. Microwave temperature exerted more significant influence on lignin structure. Thermal stability of treated lignin was improved and insensitive to short microwave time and acid concentration under mild conditions. Resulting from improved alkyl-phenols and decreased alkoxy-phenols, microwave-assisted acid pretreatment of lignin yielded bio-oil with excellent quality. Total yield of phenols in pyrolysis vapors (200 °C) improved to 14.15%, whereas that of guaiacols decreased to 22.36%. This study shows that microwave-assisted acid pretreatment is a promising technology for lignin conversion. Copyright © 2017 Elsevier Ltd. All rights reserved.

The Fourier U(2 Group and Separation of Discrete Variables

Directory of Open Access Journals (Sweden)

Kurt Bernardo Wolf

2011-06-01

Full Text Available The linear canonical transformations of geometric optics on two-dimensional screens form the group Sp(4,R, whose maximal compact subgroup is the Fourier group U(2_F; this includes isotropic and anisotropic Fourier transforms, screen rotations and gyrations in the phase space of ray positions and optical momenta. Deforming classical optics into a Hamiltonian system whose positions and momenta range over a finite set of values, leads us to the finite oscillator model, which is ruled by the Lie algebra so(4. Two distinct subalgebra chains are used to model arrays of N^2 points placed along Cartesian or polar (radius and angle coordinates, thus realizing one case of separation in two discrete coordinates. The N^2-vectors in this space are digital (pixellated images on either of these two grids, related by a unitary transformation. Here we examine the unitary action of the analogue Fourier group on such images, whose rotations are particularly visible.

SnO2*CoO ceramic obtained by microwave sintering

International Nuclear Information System (INIS)

Bordignon, M.A.N; Moura, F.; Zaghete, M.A.; Varela, J.A.; Perazolli, L.

2009-01-01

This work consists in the sintering study of CoO doped SnO 2 using microwave sintering oven and silicon carbide as a susceptor. The powders were obtained by dry oxides mixture and conformed in cylindrical shapes with 6mmx8mm and green density to 60%. Then the compacts were sintering up to 1.050 deg C, using heating rate of 50 deg C/min and isotherm up to 30min. The densities obtained were above 95% for both techniques. It was observed that occurred a temperature reducing of 400 deg C and time reducing of 210min to obtain the same densities, when was used the microwave oven without the phenomena of thermal runaway. So the sintered compacts were accomplished using DRX and SEM. It was made the electrical characterization (current x voltage) and it was found to have great potential in the production of dense ceramic-based SnO 2 with low resistivity to obtain electro-ceramic devices. (author)

Compact cryogenic attachment for Moessbauer spectroscopy with microwave excitation

International Nuclear Information System (INIS)

Didenko, N.P.; Amelin, G.P.; Zelentsov, V.I.; Kaminskii, V.L.; Fedorov, N.P.; Fal'kovich, V.M.

1989-01-01

A compact cryogenic attachment is described that is placed on a standard helium Dewar flask and permits recording of Moessbauer spectra with excitation by millimeter-band radiation in the temperature range of 4.3-300 K. The design of the attachment allows operation with various gamma-radiation detectors in both horizontal and vertical Moessbauer measurement geometries and its placement in superconducting magnets with a large warm zone

Design and experiment of a cross-shaped mode converter for high-power microwave applications

Energy Technology Data Exchange (ETDEWEB)

Peng, Shengren, E-mail: 785751053@qq.com; Yuan, Chengwei; Zhong, Huihuang; Fan, Yuwei [College of Optoelectronic Science and Engineering, National University of Defense Technology, Changsha 410073 (China)

2013-12-15

A compact mode converter, which is capable of converting a TM{sub 01} mode into a circularly polarized TE{sub 11} mode, was developed and experimentally studied with high-power microwaves. The converter, consisting of two turnstile junctions, is very short along the wave propagation direction, and therefore is suitable for designing compact and axially aligned high-power microwave radiation systems. In this paper, the principle of a converter working at 1.75 GHz is demonstrated, as well as the experimental results. The experimental and simulation results are in good agreement. At the center frequency, the conversion efficiency is more than 95%, the measured axial ratio is about 0.4 dB, and the power-handing capacity is excess of 1.9 GW.

The hyperbolic chemical bond: Fourier analysis of ground and first excited state potential energy curves of HX (X = H-Ne).

Science.gov (United States)

Harrison, John A

2008-09-04

RHF/aug-cc-pVnZ, UHF/aug-cc-pVnZ, and QCISD/aug-cc-pVnZ, n = 2-5, potential energy curves of H2 X (1) summation g (+) are analyzed by Fourier transform methods after transformation to a new coordinate system via an inverse hyperbolic cosine coordinate mapping. The Fourier frequency domain spectra are interpreted in terms of underlying mathematical behavior giving rise to distinctive features. There is a clear difference between the underlying mathematical nature of the potential energy curves calculated at the HF and full-CI levels. The method is particularly suited to the analysis of potential energy curves obtained at the highest levels of theory because the Fourier spectra are observed to be of a compact nature, with the envelope of the Fourier frequency coefficients decaying in magnitude in an exponential manner. The finite number of Fourier coefficients required to describe the CI curves allows for an optimum sampling strategy to be developed, corresponding to that required for exponential and geometric convergence. The underlying random numerical noise due to the finite convergence criterion is also a clearly identifiable feature in the Fourier spectrum. The methodology is applied to the analysis of MRCI potential energy curves for the ground and first excited states of HX (X = H-Ne). All potential energy curves exhibit structure in the Fourier spectrum consistent with the existence of resonances. The compact nature of the Fourier spectra following the inverse hyperbolic cosine coordinate mapping is highly suggestive that there is some advantage in viewing the chemical bond as having an underlying hyperbolic nature.

The microwave spectrum of ferrocenecarboxylic acid

Science.gov (United States)

Pejlovas, Aaron M.; Zhou, Zunwu; Kukolich, Stephen G.

2017-08-01

The microwave spectrum was measured for ferrocenecarboxylic acid in the 4.8-9.8 GHz range using a pulsed-beam Fourier transform microwave spectrometer. 27 transitions were measured and assigned, which include a-, b-, and c-type rotational transitions. From the measured transitions, the rotational and centrifugal distortion constants were determined. The values determined are A = 1138.0162(13) MHz, B = 653.81796(54) MHz, C = 559.83162(47) MHz, DJ = 0.0675(52) kHz, DJK = -0.157(36) kHz, DK = 0.193(47) kHz, and dJ = 0.0194(22) kHz. MP2 and B3LYP gas phase structure optimizations were performed with the aug-cc-pVTZ basis and the B3LYP method yielded rotational constants that were in far better agreement with the experimentally determined values than the MP2 results.

The limit distribution in the q-CLT for q\\,\\geqslant \\,1 is unique and can not have a compact support

Science.gov (United States)

Umarov, Sabir; Tsallis, Constantino

2016-10-01

In a paper by Umarov et al (2008 Milan J. Math. 76 307-28), a generalization of the Fourier transform, called the q-Fourier transform, was introduced and applied for the proof of a q-generalized central limit theorem (q-CLT). Subsequently, Hilhorst illustrated (2009 Braz. J. Phys. 39 371-9 2010 J. Stat. Mech. P10023) that the q-Fourier transform for q\\gt 1, is not invertible in the space of density functions. Indeed, using an invariance principle, he constructed a family of densities with the same q-Fourier transform and noted that ‘as a consequence, the q-CLT falls short of achieving its stated goal’. The distributions constructed there have compact support. We prove now that the limit distribution in the q-CLT is unique and can not have a compact support. This result excludes all the possible counterexamples which can be constructed using the invariance principle and fills the gap mentioned by Hilhorst.

Remotely powered and controlled EAPap actuator by amplitude modulated microwaves

International Nuclear Information System (INIS)

Yang, Sang Yeol; Mahadeva, Suresha K; Kim, Jaehwan

2013-01-01

This paper reports on a remotely powered and controlled Electro-Active Paper (EAPap) actuator without onboard controller using amplitude modulated microwaves. A rectenna is a key element for microwave power transmission that converts microwaves into dc power through coupling and rectification. In this study, the concept of a remotely controlled and powered EAPap actuator is proposed by means of modulating microwaves with a control signal and demodulating it through the rectenna rectification. This concept is applied to a robust EAPap actuator, namely cellulose–polypyrrole–ionic liquid (CPIL) EAPap. Details of fabrication and characterization of the rectenna and the CPIL-EAPap actuator are explained. Also, the charge accumulation problem of the actuator is explained and resolved by connecting an additional resistor. Since this idea can eliminate the onboard controller by supplying the operating signal through modulation, a compact and lightweight actuator can be achieved, which is useful for biomimetic robots and remotely driven actuators. (technical note)

125-GHz Microwave Signal Generation Employing an Integrated Pulse Shaper

DEFF Research Database (Denmark)

Liao, Shasha; Ding, Yunhong; Dong, Jianji

2017-01-01

We propose and experimentally demonstrate an on-chip pulse shaper for 125-GHz microwave waveform generation. The pulse shaper is implemented based on a silicon-on-insulator (SOI) platform that has a structure with eight-tap finite impulse response (FIR) and there is an amplitude modulator on each...... of the generated microwave waveforms is larger than 100 GHz, and it has wide bandwidth when changing the time delay of the adjacent taps and compactness, capability for integration with electronics and small power consumption are also its merits.......We propose and experimentally demonstrate an on-chip pulse shaper for 125-GHz microwave waveform generation. The pulse shaper is implemented based on a silicon-on-insulator (SOI) platform that has a structure with eight-tap finite impulse response (FIR) and there is an amplitude modulator on each...

Multiband rectenna for microwave applications

Science.gov (United States)

Okba, Abderrahim; Takacs, Alexandru; Aubert, Hervé; Charlot, Samuel; Calmon, Pierre-François

2017-02-01

This paper reports a multiband rectenna (rectifier + antenna) suitable for the electromagnetic energy harvesting of the spill-over loss of microwave antennas placed on board of geostationary satellites. Such rectenna is used for powering autonomous wireless sensors for satellite health monitoring. The topology of the rectenna is presented. The experimental results demonstrate that the proposed compact rectenna can harvest efficiently the incident electromagnetic energy at three different frequencies that are close to the resonant frequencies of the cross-dipoles implemented in the antenna array. xml:lang="fr"

Synthesis and characterization of NiO-YSZ-CeO_2 composites with microwave-assisted hydrothermal treatment

International Nuclear Information System (INIS)

Pinheiro, Lucas Batochi

2013-01-01

In the present work, it was evaluated the effects of a microwave-assisted hydrothermal (MWH) treatment on structural, thermal and electrical properties of NiO-YSZ- CeO_2 composites synthesized by hydroxide coprecipitation method. Simultaneous thermogravimetry and differential thermal analysis (TG/DTA) in conjunction with x-ray diffraction (XRD) measurements showed that MWH treatment contributed to enhanced nickel hydroxide crystallization. The linear shrinkage of the ceramic compacts was observed by thermomechanical analysis (TMA) and the results indicated a higher sinterability for the samples MWH-treated. The compacts were sintered in a conventional resistive and in a microwave furnace. This sintered compacts had their microstructure analyzed by scanning electron microscopy (SEM) and electrical properties investigated by impedance spectroscopy (IS). The SEM images showed phase homogeneity and sub-micrometric grains with irregular shapes. The IS data revealed that the MWH-treated samples have a conductivity increase for temperatures above 500 deg C regardless the sintering process. (author)

Vibrational analysis of Fourier transform spectrum of the A3Π0–X1Σ ...

Indian Academy of Sciences (India)

Abstract. The emission spectrum of InBr molecule has been recorded in the region. 350–400 nm on BOMEM DA8 Fourier transform spectrometer at an apodized resolu- tion of 0.06 cm−1 using microwave excitation technique. About 61 violet degraded and single headed bands have been recorded and are classified into ...

Fourier Hull Fatigue Assessment Method’s Proposing and Software Development

Directory of Open Access Journals (Sweden)

Jing Chen

2014-05-01

Full Text Available In this paper, based on the spectral analysis and the strain energy theory, the systematic errors of Rain-flow Counting Method have been quantitatively analyzed, from which a Fourier Counting Method is put forward. And according to this new method, software has been developed combined with sampling data of the real container ship via rigorous theoretical derivation and compact modular design, which has certain theoretical innovation significance and practical value.

Fourier-muunnoksesta

OpenAIRE

NIEMELÄ, EERO

2008-01-01

Tutkielman aiheena on Fourier-muunnoksen esittely. Tarkoituksena on erityisesti johdatella lukija Fourier-sarjan ja -muunnoksen käsitteisiin. Fourier-muunnosten teoria kuuluu yleisempään Fourier-analyysin aihepiiriin. Fourier-analyysin keskiössä on tulos, jonka mukaan tietyt ehdot täyttävää funktiota voidaan approksimoida mielivaltaisen tarkasti niin sanotun Fourier-sarjan avulla. Osoitamme, että 2\\pi-jaksollisen funktion Lebesgue-neliöintegroituvuus takaa suppenevan Fourier-sarjakehitelm...

Model-independent test for scale-dependent non-Gaussianities in the cosmic microwave background.

Science.gov (United States)

Räth, C; Morfill, G E; Rossmanith, G; Banday, A J; Górski, K M

2009-04-03

We present a model-independent method to test for scale-dependent non-Gaussianities in combination with scaling indices as test statistics. Therefore, surrogate data sets are generated, in which the power spectrum of the original data is preserved, while the higher order correlations are partly randomized by applying a scale-dependent shuffling procedure to the Fourier phases. We apply this method to the Wilkinson Microwave Anisotropy Probe data of the cosmic microwave background and find signatures for non-Gaussianities on large scales. Further tests are required to elucidate the origin of the detected anomalies.

App. 1. Fourier series and Fourier transform

International Nuclear Information System (INIS)

Anon.

1977-01-01

Definitions, formulas and practical properties in quantum mechanics are presented: Fourier series (development of periodic function, Bessel-Parseval equality); Fourier transform (Parseval-Plancherel formula, Fourier transform in three-dimensional space) [fr

A Short Biography of Joseph Fourier and Historical Development of Fourier Series and Fourier Transforms

Science.gov (United States)

Debnath, Lokenath

2012-01-01

This article deals with a brief biographical sketch of Joseph Fourier, his first celebrated work on analytical theory of heat, his first great discovery of Fourier series and Fourier transforms. Included is a historical development of Fourier series and Fourier transforms with their properties, importance and applications. Special emphasis is made…

Compact 3D quantum memory

Science.gov (United States)

Xie, Edwar; Deppe, Frank; Renger, Michael; Repp, Daniel; Eder, Peter; Fischer, Michael; Goetz, Jan; Pogorzalek, Stefan; Fedorov, Kirill G.; Marx, Achim; Gross, Rudolf

2018-05-01

Superconducting 3D microwave cavities offer state-of-the-art coherence times and a well-controlled environment for superconducting qubits. In order to realize at the same time fast readout and long-lived quantum information storage, one can couple the qubit to both a low-quality readout and a high-quality storage cavity. However, such systems are bulky compared to their less coherent 2D counterparts. A more compact and scalable approach is achieved by making use of the multimode structure of a 3D cavity. In our work, we investigate such a device where a transmon qubit is capacitively coupled to two modes of a single 3D cavity. External coupling is engineered so that the memory mode has an about 100 times larger quality factor than the readout mode. Using an all-microwave second-order protocol, we realize a lifetime enhancement of the stored state over the qubit lifetime by a factor of 6 with a fidelity of approximately 80% determined via quantum process tomography. We also find that this enhancement is not limited by fundamental constraints.

Fourier transform digital holographic adaptive optics imaging system

Science.gov (United States)

Liu, Changgeng; Yu, Xiao; Kim, Myung K.

2013-01-01

A Fourier transform digital holographic adaptive optics imaging system and its basic principles are proposed. The CCD is put at the exact Fourier transform plane of the pupil of the eye lens. The spherical curvature introduced by the optics except the eye lens itself is eliminated. The CCD is also at image plane of the target. The point-spread function of the system is directly recorded, making it easier to determine the correct guide-star hologram. Also, the light signal will be stronger at the CCD, especially for phase-aberration sensing. Numerical propagation is avoided. The sensor aperture has nothing to do with the resolution and the possibility of using low coherence or incoherent illumination is opened. The system becomes more efficient and flexible. Although it is intended for ophthalmic use, it also shows potential application in microscopy. The robustness and feasibility of this compact system are demonstrated by simulations and experiments using scattering objects. PMID:23262541

Peroxydisulfate initiated synthesis of potato starch-graft-poly(acrylonitrile under microwave irradiation

Directory of Open Access Journals (Sweden)

2007-01-01

Full Text Available Potato starch-graft-poly(acrylonitrile could be efficiently synthesized using small concentration of ammonium peroxydisulfate (0.0014M in aqueous medium under microwave irradiation. A representative microwave synthesized graft copolymer was characterized using Fourier Transform Infrared Spectroscopy, X-ray Diffraction, Scanning Electron Microscopy and Thermogravimetric Analysis. Under microwave conditions oxygen removal from the reaction vessel was not required and the graft copolymer was obtained in high yield using very small amount of ammonium peroxydisulfate, however using the same amount of ammonium peroxydisulfate (0.0014M on thermostatic water bath no grafting was observed up to 98°C (even in inert atmosphere. Raising the concentration of the initiator to 0.24 M resulted into 10% grafting at 50 °C but in inert atmosphere.The viscosity/shear stability of the grafted starch (aqueous solution and water/saline retention ability of the microwave synthesized graft copolymer were also studied and compared with that of the native potato starch.

Characterization of low-temperature microwave loss of thin aluminum oxide formed by plasma oxidation

Energy Technology Data Exchange (ETDEWEB)

Deng, Chunqing, E-mail: cdeng@uwaterloo.ca; Otto, M.; Lupascu, A., E-mail: alupascu@uwaterloo.ca [Institute for Quantum Computing, Department of Physics and Astronomy, and Waterloo Institute for Nanotechnology, University of Waterloo, Waterloo, Ontario N2L 3G1 (Canada)

2014-01-27

We report on the characterization of microwave loss of thin aluminum oxide films at low temperatures using superconducting lumped resonators. The oxide films are fabricated using plasma oxidation of aluminum and have a thickness of 5 nm. We measure the dielectric loss versus microwave power for resonators with frequencies in the GHz range at temperatures from 54 to 303 mK. The power and temperature dependence of the loss are consistent with the tunneling two-level system theory. These results are relevant to understanding decoherence in superconducting quantum devices. The obtained oxide films are thin and robust, making them suitable for capacitors in compact microwave resonators.

Additional conformer observed in the microwave spectrum of methyl vinyl ketone

Science.gov (United States)

Wilcox, David S.; Shirar, Amanda J.; Williams, Owen L.; Dian, Brian C.

2011-05-01

A chirped-pulse Fourier transform microwave spectrometer was used to record the rotational spectrum of methyl vinyl ketone (MVK, 3-butene-2-one). Two stable conformations were identified: the previously documented antiperiplanar (ap) conformer and synperiplanar (sp), which is reported for the first time in this microwave study. Methyl torsional analysis resulted in V3 barrier heights of 433.8(1) and 376.6(2) cm-1 for ap- and sp-MVK, respectively. Heavy atom isotopic species of both conformers were detected in natural abundance allowing bond lengths and angles of the molecular frames to be calculated through Kraitchman analysis. A comparison with ab initio calculations is included.

Joseph F. Keithley Award For Advances in Measurement Science Talk: Precision Noise Measurements at Microwave and Optical Frequencies

Science.gov (United States)

Ivanov, Eugene

2010-03-01

The quest to detect Gravitational Waves resulted in a number of important developments in the fields of oscillator frequency stabilization and precision noise measurements. This was due to the realization of similarities between the principles of high sensitivity measurements of weak mechanical forces and phase/amplitude fluctuations of microwave signals. In both cases interferometric carrier suppression and low-noise amplification of the residual noise sidebands were the main factors behind significant improvements in the resolution of spectral measurements. In particular, microwave frequency discriminators with almost thermal noise limited sensitivity were constructed leading to microwave oscillators with more than 25dB lower phase noise than the previous state-of-the-art. High power solid-state microwave amplifiers offered further opportunity of oscillator phase noise reduction due to the increased energy stored in the high-Q resonator of the frequency discriminator. High power microwave oscillators with the phase noise spectral density close to -160dBc/Hz at 1kHz Fourier frequency have been recently demonstrated. The principles of interferometric signal processing have been applied to the study of noise phenomena in microwave components which were considered to be ``noise free''. This resulted in the first experimental evidence of phase fluctuations in microwave circulators. More efficient use of signal power enabled construction of the ``power recycled'' interferometers with spectral resolution of -200dBc/Hz at 1kHz Fourier frequency. This has been lately superseded by an order of magnitude with a waveguide interferometer due to its higher power recycling factor. A number of opto-electronic measurement systems were developed to characterize the fidelity of frequency transfer from the optical to the microwave domain. This included a new type of a phase detector capable of measuring phase fluctuations of the weak microwave signals extracted from the demodulated

Microwave and thermal curing of an epoxy resin for microelectronic applications

Energy Technology Data Exchange (ETDEWEB)

Johnston, K. [Institute of Chemical Sciences, School of Engineering and Physical Sciences, Heriot-Watt University, Edinburgh EH14 4AS (United Kingdom); Pavuluri, S.K.; Leonard, M.T.; Desmulliez, M.P.Y. [MIcroSystems Engineering Centre (MISEC), Institute of Signals, Sensors and Systems, School of Engineering and Physical Sciences, Heriot-Watt University, Edinburgh EH14 4AS (United Kingdom); Arrighi, V., E-mail: v.arrighi@hw.ac.uk [Institute of Chemical Sciences, School of Engineering and Physical Sciences, Heriot-Watt University, Edinburgh EH14 4AS (United Kingdom)

2015-09-20

Graphical abstract: - Highlights: • Thermal and microwave curing of a commercial epoxy resin EO1080 are compared. • Microwave curing increases cure rate and does not adversely affect properties. • The curing of EO1080 is generally autocatalytic but deviates at high conversion. • Microwave radiation has a more complex effect on curing kinetics. - Abstract: Microwave curing of thermosetting polymers has a number of advantages to natural or thermal oven curing and is considered a cost-effective alternative. Here we present a detailed study of a commercially available epoxy resin, EO1080. Samples that are thermally cured are compared to curing using a recently developed modular microwave processing system. For commercial purposes it is crucial to demonstrate that microwave curing does not adversely affect the thermal and chemical properties of the material. Therefore, the kinetics of cure and various post cure properties of the resin are investigated. Attenuated Total Reflectance Fourier-Transform Infrared (ATR-FTIR) analysis shows no significant difference between the conventionally and microwave cured samples. Differential scanning calorimetry (DSC) is used to monitor the kinetics of the curing reaction, as well as determine the thermal and ageing properties of the material. As expected, the rate of curing is higher when using microwave energy and we attempt to quantify differences compared to conventional thermal curing. No change in glass transition temperature (T{sub g}) is observed. For the first time, enthalpy relaxation measurements performed on conventional and microwave cured samples are reported and these indicate similar ageing properties at any given temperature under T{sub g}.

Microwave and thermal curing of an epoxy resin for microelectronic applications

International Nuclear Information System (INIS)

Johnston, K.; Pavuluri, S.K.; Leonard, M.T.; Desmulliez, M.P.Y.; Arrighi, V.

2015-01-01

Graphical abstract: - Highlights: • Thermal and microwave curing of a commercial epoxy resin EO1080 are compared. • Microwave curing increases cure rate and does not adversely affect properties. • The curing of EO1080 is generally autocatalytic but deviates at high conversion. • Microwave radiation has a more complex effect on curing kinetics. - Abstract: Microwave curing of thermosetting polymers has a number of advantages to natural or thermal oven curing and is considered a cost-effective alternative. Here we present a detailed study of a commercially available epoxy resin, EO1080. Samples that are thermally cured are compared to curing using a recently developed modular microwave processing system. For commercial purposes it is crucial to demonstrate that microwave curing does not adversely affect the thermal and chemical properties of the material. Therefore, the kinetics of cure and various post cure properties of the resin are investigated. Attenuated Total Reflectance Fourier-Transform Infrared (ATR-FTIR) analysis shows no significant difference between the conventionally and microwave cured samples. Differential scanning calorimetry (DSC) is used to monitor the kinetics of the curing reaction, as well as determine the thermal and ageing properties of the material. As expected, the rate of curing is higher when using microwave energy and we attempt to quantify differences compared to conventional thermal curing. No change in glass transition temperature (T g ) is observed. For the first time, enthalpy relaxation measurements performed on conventional and microwave cured samples are reported and these indicate similar ageing properties at any given temperature under T g

Preparation of ultrafiltration membrane by phase separation coupled with microwave irradiation

Energy Technology Data Exchange (ETDEWEB)

Suryani, Puput Eka [Department of Chemical Engineering, Faculty of Engineering, Diponegoro University Jl. Prof. Soedarto, Semarang 50275, Central Java (Indonesia); Department of Chemical Engineering, Faculty of Engineering, UniversitasMuhammadiyah Surakarta Jl. Jendral Ahmad Yani, Surakarta 57102, Central Java (Indonesia); Purnama, Herry [Department of Chemical Engineering, Faculty of Engineering, UniversitasMuhammadiyah Surakarta Jl. Jendral Ahmad Yani, Surakarta 57102, Central Java (Indonesia); Susanto, Heru, E-mail: heru.susanto@undip.ac.id [Department of Chemical Engineering, Faculty of Engineering, Diponegoro University Jl. Prof. Soedarto, Semarang 50275, Central Java (Indonesia)

2015-12-29

Preparation of low fouling ultrafiltration membrane is still a big challenge in the membrane field. In this paper, polyether sulfone (PES) ultrafiltration membranes were prepared by non-solvent-induced phase separation (NIPS) coupled with microwave irradiation. Polyethylene glycol (PEG) and polyethylene glycol methacrylate (PEGMA) were used as additives to improve membrane hydrophilicity. In this study, the concentration of additive, irradiation time and microwave power was varied. The membranes were characterized by scanning electron microscopy (SEM) and Fourier transform infrared (FTIR) spectroscopy, while the performances were tested by adsorptive and ultrafiltration fouling experiments. The results show that the irradiation time and irradiation power are very important parameter that influence the membrane characteristic. In addition, type and concentration of additive are other important parameters. The results suggest that microwave irradiation is the most important parameter influencing the membrane characteristic. Both pure water flux and fouling resistance increase with increasing irradiation time, power irradiation, and additive concentration. PES membrane with addition of 10% w/w PEG and irradiated by 130 W microwave power for 180 seconds is the best membrane performance.

The Structure and Molecular Parameters of Camphene Determined by Fourier Transform Microwave Spectroscopy and Quantum Chemical Calculations

Science.gov (United States)

Neeman, Elias M.; Dréan, Pascal; Huet, T. R.

2016-06-01

The emission of volatile organic compounds, from plants has strong revelance for plant physiology, plant ecology and atmospheric chemistry. Camphene (C10H16) is a bicyclic monoterpene which is emitted in the atmosphere by biogenic sources. The structure of the unique stable conformer was optimized using density functional theory and ab initio calculations. The rotational spectrum of camphene was recorded in a supersonic jet expansion with a Fourier transform microwave spectrometer over the range 2-20 GHz. Signals from the parent species and from the ten 13C isotopomers were observed in natural abundance. The rotational and centrifugal distortion parameters were fitted to a Watson's Hamiltonian in the A-reduction. A magnetic hyperfine structure associated with the pairs of hydrogen nuclei in the methylene groups was observed and modeled.The rotational constants coupled to the equilibrium structure calculations were used to determine the r_0 and the r_m(1) gas-phase geometries of the carbon skeleton. The present work provides the first spectroscopic characterization of camphene in the gas phase and these results are also relevant for ozonolysis kinetics study through Criegee intermediates. R. Baraldi, F. Rapparini, O. Facini, D. Spano and P. Duce, Journal of Mediterranean Ecology, Vol.6, No.1, (2005). A. Bracho-Nunez, N. M. Knothe, S. Welter, M. Staudt, W. R. Costa, M. A. R. Liberato, M. T. F. Piedade, and J. Kesselmeier Biogeosciences, 10, 5855-5873, (2013). Minna Kivimäenpää, Narantsetseg Magsarjav, Rajendra Ghimire, Juha-Matti Markkanen, Juha Heijari, Martti Vuorinen and Jarmo K. Holopainen, Atmospheric Environment, 60, 477-485, (2012). R.C. de M. Oliveira and G. F. Bauerfeldt, J. Phys. Chem. A, 119 2802-2812 (2015)

Compact high-current, subnanosecond electron accelerator

Energy Technology Data Exchange (ETDEWEB)

Shpak, V G; Shunajlov, S A; Ulmaskulov, M R; Yalandin, M I [Russian Academy of Sciences, Ekaterinburg (Russian Federation). Inst. of Electrophysics; Pegel, I V [Russian Academy of Sciences, Tomsk (Russian Federation). High-Current Electronics Inst.; Tarakanov, V P [Russian Academy of Sciences, Moscow (Russian Federation). High-Temperature Inst.

1997-12-31

A compact subnanosecond, high-current electron accelerator producing an annular electron beam of duration up to 300 - 400 ps, energy about 250 keV, and current up to 1 kA has been developed to study transient processes in pulsed power microwave devices. The measuring and recording techniques used to experimentally investigate the dynamics of the beam current pulse and the transformation of the electron energy during the transportation of the beam in a longitudinal magnetic field are described. The experimental data obtained are compared with the predictions of a numerical simulation. (author). 6 figs., 5 refs.

Surface modification of titanium hydride with epoxy resin via microwave-assisted ball milling

International Nuclear Information System (INIS)

Ning, Rong; Chen, Ding; Zhang, Qianxia; Bian, Zhibing; Dai, Haixiong; Zhang, Chi

2014-01-01

Highlights: • TiH 2 was modified with epoxy resin by microwave-assisted ball milling. • The epoxy ring was opened under the coupling effect of microwave and ball milling. • Microwave-assisted ball milling improved the compatibility of TiH 2 with epoxy. - Abstract: Surface modification of titanium hydride with epoxy resin was carried out via microwave-assisted ball milling and the products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermo-gravimetry (TG) and Fourier transform infrared spectroscopy (FT-IR). A sedimentation test was performed to investigate the compatibility of the modified nano titanium hydride with the epoxy resin. The results show that the epoxy resin molecules were grafted on the surface of nano titanium hydride particles during the microwave-assisted ball milling process, which led to the improvement of compatibility between the nanoparticles and epoxy resin. According to the FT-IR, the grafting site was likely to be located around the epoxy group due to the fact that the epoxy ring was opened. However, compared with microwave-assisted ball milling, the conventional ball milling could not realize the surface modification, indicating that the coupling effect of mechanical force and microwave played a key role during the process

Computer simulations of compact toroid formation and acceleration

International Nuclear Information System (INIS)

Peterkin, R.E. Jr.; Sovinec, C.R.

1990-01-01

Experiments to form, accelerate, and focus compact toroid plasmas will be performed on the 9.4 MJ SHIVA STAR fast capacitor bank at the Air Force Weapons Laboratory during the 1990. The MARAUDER (magnetically accelerated rings to achieve ultrahigh directed energy and radiation) program is a research effort to accelerate magnetized plasma rings with the masses between 0.1 and 1.0 mg to velocities above 10 8 cm/sec and energies above 1 MJ. Research on these high-velocity compact toroids may lead to development of very fast opening switches, high-power microwave sources, and an alternative path to inertial confinement fusion. Design of a compact toroid accelerator experiment on the SHIVA STAR capacitor bank is underway, and computer simulations with the 2 1/2-dimensional magnetohydrodynamics code, MACH2, have been performed to guide this endeavor. The compact toroids are produced in a magnetized coaxial plasma gun, and the acceleration will occur in a configuration similar to a coaxial railgun. Detailed calculations of formation and equilibration of a low beta magnetic force-free configuration (curl B = kB) have been performed with MACH2. In this paper, the authors discuss computer simulations of the focusing and acceleration of the toroid

Liquefaction behaviors of bamboo residues in a glycerol-based solvent using microwave energy

Science.gov (United States)

Jiulong Xie; Chung-Yun Hse; Todd F. Shupe; Jinqiu Qi; Hui Pan

2014-01-01

Liquefaction of bamboo was performed in glycerol–methanol as co-solvent using microwave energy and was evaluated by characterizing the liquefied residues. High efficiency conversion of bamboo was achieved under mild reaction conditions. Liquefaction temperature and time interacted to affect the liquefaction reaction. Fourier transform infrared analyzes of the residues...

Rapid synthesis of single-phase bismuth ferrite by microwave-assisted hydrothermal method

Energy Technology Data Exchange (ETDEWEB)

Cao, Wenqian [College of Materials Science and Engineering, China Jiliang University, 258 Xueyuan Street, Xiasha Higher Education District, Hangzhou 310018, Zhejiang Province (China); Chen, Zhi, E-mail: zchen0@gmail.com [College of Materials Science and Engineering, China Jiliang University, 258 Xueyuan Street, Xiasha Higher Education District, Hangzhou 310018, Zhejiang Province (China); Gao, Tong; Zhou, Dantong; Leng, Xiaonan; Niu, Feng [College of Materials Science and Engineering, China Jiliang University, 258 Xueyuan Street, Xiasha Higher Education District, Hangzhou 310018, Zhejiang Province (China); Zhu, Yuxiang [College of Materials Science and Engineering, China Jiliang University, 258 Xueyuan Street, Xiasha Higher Education District, Hangzhou 310018, Zhejiang Province (China); Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin (China); Qin, Laishun, E-mail: qinlaishun@yeah.net [College of Materials Science and Engineering, China Jiliang University, 258 Xueyuan Street, Xiasha Higher Education District, Hangzhou 310018, Zhejiang Province (China); Wang, Jiangying; Huang, Yuexiang [College of Materials Science and Engineering, China Jiliang University, 258 Xueyuan Street, Xiasha Higher Education District, Hangzhou 310018, Zhejiang Province (China)

2016-06-01

This paper describes on the fast synthesis of bismuth ferrite by the simple microwave-assisted hydrothermal method. The phase transformation and the preferred growth facets during the synthetic process have been investigated by X-ray diffraction. Bismuth ferrite can be quickly prepared by microwave hydrothermal method by simply controlling the reaction time, which is further confirmed by Fourier Transform infrared spectroscopy and magnetic measurement. - Graphical abstract: Single-phase BiFeO{sub 3} could be realized at a shortest reaction time of 65 min. The reaction time has strong influences on the phase transformation and the preferred growth facets. - Highlights: • Rapid synthesis (65 min) of BiFeO{sub 3} by microwave-assisted hydrothermal method. • Reaction time has influence on the purity and preferred growth facets. • FTIR and magnetic measurement further confirm the pure phase.

Rapid synthesis of single-phase bismuth ferrite by microwave-assisted hydrothermal method

International Nuclear Information System (INIS)

Cao, Wenqian; Chen, Zhi; Gao, Tong; Zhou, Dantong; Leng, Xiaonan; Niu, Feng; Zhu, Yuxiang; Qin, Laishun; Wang, Jiangying; Huang, Yuexiang

2016-01-01

This paper describes on the fast synthesis of bismuth ferrite by the simple microwave-assisted hydrothermal method. The phase transformation and the preferred growth facets during the synthetic process have been investigated by X-ray diffraction. Bismuth ferrite can be quickly prepared by microwave hydrothermal method by simply controlling the reaction time, which is further confirmed by Fourier Transform infrared spectroscopy and magnetic measurement. - Graphical abstract: Single-phase BiFeO_3 could be realized at a shortest reaction time of 65 min. The reaction time has strong influences on the phase transformation and the preferred growth facets. - Highlights: • Rapid synthesis (65 min) of BiFeO_3 by microwave-assisted hydrothermal method. • Reaction time has influence on the purity and preferred growth facets. • FTIR and magnetic measurement further confirm the pure phase.

Vibration-rotation spectrum of BH X1Σ+ by Fourier transform emission spectroscopy

Science.gov (United States)

Pianalto, F. S.; O'Brien, L. C.; Keller, P. C.; Bernath, P. F.

1988-06-01

The vibration-rotation emission spectrum of the BH X1Σ+ state was observed with the McMath Fourier transform spectrometer at Kitt Peak. The 1-0, 2-1, and 3-2 bands were observed in a microwave discharge of B2H6 in He. Spectroscopic constants of the individual vibrational levels and equilibrium molecular constants were determined. An RKR potential curve was calculated from the equilibrium constants. Alfred P. Sloan Fellow; Camille and Henry Dreyfus Teacher-Scholar.

Microwave and conventional preparation of Zinc borate glass: Eu3+ ion as luminescent probe

International Nuclear Information System (INIS)

Mandal, Ashis K.; Balaji, S.; Sen, Ranjan

2014-01-01

Highlights: • IR transparent Zinc borate glass is prepared using microwave heating. • Glass transition temperature of microwave melted glass is found higher than that of glass prepared in conventional melting. • Low OH concentration in glass can be prepared in microwave heating. • We report higher reduction of Eu 3+ to Eu 2+ in microwave processing of Zinc borate glass. - Abstract: Transparent Zinc borate glass is melted using microwave energy as an alternative heating route to conventional resistive heating. A comparative study of the properties of the glasses prepared by both the methods is conducted by adopting X-ray diffraction (XRD), Differential scanning calorimetry (DSC), UV–VIS–NIR spectroscopy, Fourier transform infrared (FTIR) spectroscopy, Refractive Indices (RI). Amorphous nature of samples is confirmed by X-ray diffraction study. Glass transition temperature (T g ) of microwave melted glass is found ∼7–9 °C higher than that of glass prepared in conventional melting. OH content is found less than 250 ppm in microwave melted glass whereas it is above 330 ppm in conventional melted glasses. Photoluminescence study of Eu 2 O 3 doped glass prepared in microwave heating indicates higher reduction of Eu 3+ → Eu 2+ than the glass melted in conventional route. Thus, microwave processing can be an alternative energy efficient, time saving, environmental friendly glass preparation method

Exploring the conformational landscape of menthol, menthone, and isomenthone: A microwave study

Directory of Open Access Journals (Sweden)

David eSchmitz

2015-03-01

Full Text Available The rotational spectra of the monoterpenoids menthol, menthone, and isomenthone are reportedin the frequency range of 2−8.5GHz, obtained with broadband Fourier-transform microwave spectroscopy.For menthol only one conformation was identified under the cold conditions of the molecularjet, whereas three conformations were observed for menthone and one for isomenthone. Theconformational space of the different molecules was extensively studied using quantum chemicalcalculations, and the results were compared with molecular parameters obtained by the measurements.Finally, a computer program is presented, which was developed to automatically identifydifferent species in a dense broadband microwave spectrum using calculated ab initio rotationalconstants as input.

Preparation and characterization of flexible ferromagnetic nanocomposites for microwave applications

International Nuclear Information System (INIS)

Thomas, Teena; Kanoth, Bipinbal P.; Nijas, C.M.; Joy, P.A.; Joseph, Joseph M.; Kuthirummal, Narayanan; Thachil, Eby T.

2015-01-01

Highlights: • Fe 3 O 4 nanoparticles (∼20 nm) were synthesised by co-precipitation method. • Nanoparticles were homogeneously distributed in natural rubber through latex stage processing. • Mechanical properties and magnetic properties of composites improved with loading Fe 3 O 4 nanoparticles. • Imaginary part of permeability increases with nanoparticle loading improving the microwave absorption characteristics. • Infrared spectra reveal strong interaction between NR and iron oxide nanoparticles. - Abstract: Magnetic Fe 3 O 4 nanoparticles (∼20 nm) were synthesized using the chemical co-precipitation method with a view of developing flexible and easily processable ferromagnetic materials with high mouldability to be used as microwave absorbers. The nanoparticles prepared were incorporated into natural rubber through latex stage processing. This novel processing method gives better dispersion of particles in the rubber matrix. The composites were characterized using XRD, SEM, vibrating sample magnetometer, dynamic mechanical analyzer, cavity perturbation, thermogravimetry (TGA), and Fourier transform infrared photoacoustic spectroscopy (FTIR-PAS). A notable improvement in the mechanical properties of composites was observed upon adding Fe 3 O 4 particles. Magnetic and microwave characteristics of the composites indicate the formation of a flexible ferromagnetic material with good microwave absorption characteristics

Design of a portable optical emission tomography system for microwave induced compact plasma for visible to near-infrared emission lines

Energy Technology Data Exchange (ETDEWEB)

Rathore, Kavita, E-mail: kavira@iitk.ac.in, E-mail: pmunshi@iitk.ac.in, E-mail: sudeepb@iitk.ac.in; Munshi, Prabhat, E-mail: kavira@iitk.ac.in, E-mail: pmunshi@iitk.ac.in, E-mail: sudeepb@iitk.ac.in [Nuclear Engineering and Technology Programme, Indian Institute of Technology Kanpur, Kanpur (India); Bhattacharjee, Sudeep, E-mail: kavira@iitk.ac.in, E-mail: pmunshi@iitk.ac.in, E-mail: sudeepb@iitk.ac.in [Department of Physics, Indian Institute of Technology Kanpur, Kanpur 208016 (India)

2016-03-15

A new non-invasive diagnostic system is developed for Microwave Induced Plasma (MIP) to reconstruct tomographic images of a 2D emission profile. A compact MIP system has wide application in industry as well as research application such as thrusters for space propulsion, high current ion beams, and creation of negative ions for heating of fusion plasma. Emission profile depends on two crucial parameters, namely, the electron temperature and density (over the entire spatial extent) of the plasma system. Emission tomography provides basic understanding of plasmas and it is very useful to monitor internal structure of plasma phenomena without disturbing its actual processes. This paper presents development of a compact, modular, and versatile Optical Emission Tomography (OET) tool for a cylindrical, magnetically confined MIP system. It has eight slit-hole cameras and each consisting of a complementary metal–oxide–semiconductor linear image sensor for light detection. The optical noise is reduced by using aspheric lens and interference band-pass filters in each camera. The entire cylindrical plasma can be scanned with automated sliding ring mechanism arranged in fan-beam data collection geometry. The design of the camera includes a unique possibility to incorporate different filters to get the particular wavelength light from the plasma. This OET system includes selected band-pass filters for particular argon emission 750 nm, 772 nm, and 811 nm lines and hydrogen emission H{sub α} (656 nm) and H{sub β} (486 nm) lines. Convolution back projection algorithm is used to obtain the tomographic images of plasma emission line. The paper mainly focuses on (a) design of OET system in detail and (b) study of emission profile for 750 nm argon emission lines to validate the system design.

Electromagnetic radiation in a semi-compact space

Science.gov (United States)

Iso, Satoshi; Kitazawa, Noriaki; Yokoo, Sumito

2018-02-01

In this note, we investigate the electromagnetic radiation emitted from a revolving point charge in a compact space. If the point charge is circulating with an angular frequency ω0 on the (x , y)-plane at z = 0 with boundary conditions, x ∼ x + 2 πR and y ∼ y + 2 πR, it emits radiation into the z-direction of z ∈ [ - ∞ , + ∞ ]. We find that the radiation shows discontinuities as a function of ω0 R at which a new propagating mode with a different Fourier component appears. For a small radius limit ω0 R ≪ 1, all the Fourier modes except the zero mode on (x , y)-plane are killed, but an effect of squeezing the electric field totally enhances the radiation. In the large volume limit ω0 R → ∞, the energy flux of the radiation reduces to the expected Larmor formula.

Fourier series

CERN Document Server

Tolstov, Georgi P

1962-01-01

Richard A. Silverman's series of translations of outstanding Russian textbooks and monographs is well-known to people in the fields of mathematics, physics, and engineering. The present book is another excellent text from this series, a valuable addition to the English-language literature on Fourier series.This edition is organized into nine well-defined chapters: Trigonometric Fourier Series, Orthogonal Systems, Convergence of Trigonometric Fourier Series, Trigonometric Series with Decreasing Coefficients, Operations on Fourier Series, Summation of Trigonometric Fourier Series, Double Fourie

Enhanced photocatalytic activity of microwave treated TiO2 pillared montmorillonite

International Nuclear Information System (INIS)

Sun Shenmei; Jiang Yinshan; Yu Lixin; Li Fangfei; Yang Zhengwen; Hou Tianyi; Hu Daqiang; Xia Maosheng

2006-01-01

TiO 2 pillared montmorillonite synthesized by microwave irradiation, exhibited good photocatalytic degradation performance of methyl orange, whose pseudo first order reaction rate constant was nearly four times than that of conventional method, because of its enhanced crystalline, preferred anatase phase and improved porosity performance, which were analysed by X-ray diffraction (XRD), far Fourier transform infrared ray spectroscopy (FTIR) and nitrogen adsorption isotherms

An integrated continuous class-F-1 mode power amplifier design approach for microwave enhanced portable diagnostic applications

OpenAIRE

Imtiaz, Azeem; Lees, Jonathan; Choi, Heungjae; Joshi, Lovleen Tina

2015-01-01

© 2015 IEEE. This paper presents a novel technique for designing a microwave power delivery system targeted at compact and portable microwave-assisted diagnostic healthcare applications to help tackle the growing problem of anti-microbial resistance. The arrangement comprises a purpose-built cylindrical cavity resonator within which, the bacterial samples are exposed, driven by a high-efficiency 10-W GaN amplifier, critically coupled via a simple, adjustable internal loop antenna. The experim...

Broadband W-band Rapid Frequency Sweep Considerations for Fourier Transform EPR.

Science.gov (United States)

Strangeway, Robert A; Hyde, James S; Camenisch, Theodore G; Sidabras, Jason W; Mett, Richard R; Anderson, James R; Ratke, Joseph J; Subczynski, Witold K

2017-12-01

A multi-arm W-band (94 GHz) electron paramagnetic resonance spectrometer that incorporates a loop-gap resonator with high bandwidth is described. A goal of the instrumental development is detection of free induction decay following rapid sweep of the microwave frequency across the spectrum of a nitroxide radical at physiological temperature, which is expected to lead to a capability for Fourier transform electron paramagnetic resonance. Progress toward this goal is a theme of the paper. Because of the low Q-value of the loop-gap resonator, it was found necessary to develop a new type of automatic frequency control, which is described in an appendix. Path-length equalization, which is accomplished at the intermediate frequency of 59 GHz, is analyzed. A directional coupler is favored for separation of incident and reflected power between the bridge and the loop-gap resonator. Microwave leakage of this coupler is analyzed. An oversize waveguide with hyperbolic-cosine tapers couples the bridge to the loop-gap resonator, which results in reduced microwave power and signal loss. Benchmark sensitivity data are provided. The most extensive application of the instrument to date has been the measurement of T 1 values using pulse saturation recovery. An overview of that work is provided.

Synthesis of polymer-derived ceramic Si(B)CN-carbon nanotube composite by microwave-induced interfacial polarization.

Science.gov (United States)

Bhandavat, R; Kuhn, W; Mansfield, E; Lehman, J; Singh, G

2012-01-01

We demonstrate synthesis of a polymer-derived ceramic (PDC)-multiwall carbon nanotube (MWCNT) composite using microwave irradiation at 2.45 GHz. The process takes about 10 min of microwave irradiation for the polymer-to-ceramic conversion. The successful conversion of polymer coated carbon nanotubes to ceramic composite is chemically ascertained by Fourier transform-infrared and X-ray photoelectron spectroscopy and physically by thermogravimetric analysis and transmission electron microscopy characterization. Frequency dependent dielectric measurements in the S-Band (300 MHz to 3 GHz) were studied to quantify the extent of microwave-CNT interaction and the degree of selective heating available at the MWCNT-polymer interface. Experimentally obtained return loss of the incident microwaves in the specimen explains the reason for heat generation. The temperature-dependent permittivity of polar molecules further strengthens the argument of internal heat generation. © 2011 American Chemical Society

Gas Measurement Using Static Fourier Transform Infrared Spectrometers.

Science.gov (United States)

Köhler, Michael H; Schardt, Michael; Rauscher, Markus S; Koch, Alexander W

2017-11-13

Online monitoring of gases in industrial processes is an ambitious task due to adverse conditions such as mechanical vibrations and temperature fluctuations. Whereas conventional Fourier transform infrared (FTIR) spectrometers use rather complex optical and mechanical designs to ensure stable operation, static FTIR spectrometers do not require moving parts and thus offer inherent stability at comparatively low costs. Therefore, we present a novel, compact gas measurement system using a static single-mirror Fourier transform spectrometer (sSMFTS). The system works in the mid-infrared range from 650 cm - 1 to 1250 cm - 1 and can be operated with a customized White cell, yielding optical path lengths of up to 120 cm for highly sensitive quantification of gas concentrations. To validate the system, we measure different concentrations of 1,1,1,2-Tetrafluoroethane (R134a) and perform a PLS regression analysis of the acquired infrared spectra. Thereby, the measured absorption spectra show good agreement with reference data. Since the system additionally permits measurement rates of up to 200 Hz and high signal-to-noise ratios, an application in process analysis appears promising.

Fast compact algorithms and software for spline smoothing

CERN Document Server

Weinert, Howard L

2012-01-01

Fast Compact Algorithms and Software for Spline Smoothing investigates algorithmic alternatives for computing cubic smoothing splines when the amount of smoothing is determined automatically by minimizing the generalized cross-validation score. These algorithms are based on Cholesky factorization, QR factorization, or the fast Fourier transform. All algorithms are implemented in MATLAB and are compared based on speed, memory use, and accuracy. An overall best algorithm is identified, which allows very large data sets to be processed quickly on a personal computer.

High power microwave source development

Science.gov (United States)

Benford, James N.; Miller, Gabriel; Potter, Seth; Ashby, Steve; Smith, Richard R.

1995-05-01

The requirements of this project have been to: (1) improve and expand the sources available in the facility for testing purposes and (2) perform specific tasks under direction of the Defense Nuclear Agency about the applications of high power microwaves (HPM). In this project the HPM application was power beaming. The requirements of this program were met in the following way: (1) We demonstrated that a compact linear induction accelerator can drive HPM sources at repetition rates in excess of 100 HZ at peak microwave powers of a GW. This was done for the relativistic magnetron. Since the conclusion of this contract such specifications have also been demonstrated for the relativistic klystron under Ballistic Missile Defense Organization funding. (2) We demonstrated an L band relativistic magnetron. This device has been used both on our single pulse machines, CAMEL and CAMEL X, and the repetitive system CLIA. (3) We demonstrated that phase locking of sources together in large numbers is a feasible technology and showed the generation of multigigawatt S-band radiation in an array of relativistic magnetrons.

Ultra-compact microwave filters using kinetic inductance microstrip

International Nuclear Information System (INIS)

Pond, J.M.; Carroll, K.R.; Cukauskas, E.J.

1991-01-01

This paper reports on multi-pole microwave filters designed and fabricated using microstrip transmission line sections which consist of two very thin films of sputtered niobium nitride (NbN) separated by another very thin film of sputtered Si. Since the thicknesses of all three films are much less than the superconducting penetration depth, the kinetic inductance is significantly greater than the magnetic inductance. As a result, the phase velocity of a microstrip transmission line is much less than the free space speed of light. Since resonant structures are reduced in size proportionately, the size and weight of microstrip circuits can be greatly reduced. Prototype filters consisting of four open circuit half-wavelength microstrip stubs separated by full-wavelength microstrip sections have been measured. The circuits are connected to 34 mil diameter coaxial cable via an intermediate coplanar waveguide section. Passbands of 4 GHz separated by 3 GHz reject bands have been measured in a structure which occupies less than 0.5 cm 2 including the coplanar waveguide transitions. Higher-order passbands, although possessing an increased insertion loss, maintain filter passband characteristics through 20.0 GHz

Fourier rebinning and consistency equations for time-of-flight PET planograms.

Science.gov (United States)

Li, Yusheng; Defrise, Michel; Matej, Samuel; Metzler, Scott D

2016-01-01

Due to the unique geometry, dual-panel PET scanners have many advantages in dedicated breast imaging and on-board imaging applications since the compact scanners can be combined with other imaging and treatment modalities. The major challenges of dual-panel PET imaging are the limited-angle problem and data truncation, which can cause artifacts due to incomplete data sampling. The time-of-flight (TOF) information can be a promising solution to reduce these artifacts. The TOF planogram is the native data format for dual-panel TOF PET scanners, and the non-TOF planogram is the 3D extension of linogram. The TOF planograms is five-dimensional while the objects are three-dimensional, and there are two degrees of redundancy. In this paper, we derive consistency equations and Fourier-based rebinning algorithms to provide a complete understanding of the rich structure of the fully 3D TOF planograms. We first derive two consistency equations and John's equation for 3D TOF planograms. By taking the Fourier transforms, we obtain two Fourier consistency equations and the Fourier-John equation, which are the duals of the consistency equations and John's equation, respectively. We then solve the Fourier consistency equations and Fourier-John equation using the method of characteristics. The two degrees of entangled redundancy of the 3D TOF data can be explicitly elicited and exploited by the solutions along the characteristic curves. As the special cases of the general solutions, we obtain Fourier rebinning and consistency equations (FORCEs), and thus we obtain a complete scheme to convert among different types of PET planograms: 3D TOF, 3D non-TOF, 2D TOF and 2D non-TOF planograms. The FORCEs can be used as Fourier-based rebinning algorithms for TOF-PET data reduction, inverse rebinnings for designing fast projectors, or consistency conditions for estimating missing data. As a byproduct, we show the two consistency equations are necessary and sufficient for 3D TOF planograms

A fast non-Fourier method for Landau-fluid operators

Energy Technology Data Exchange (ETDEWEB)

Dimits, A. M., E-mail: dimits1@llnl.gov; Joseph, I.; Umansky, M. V. [Lawrence Livermore National Laboratory, L-637, P.O. Box 808, Livermore, California 94511-0808 (United States)

2014-05-15

An efficient and versatile non-Fourier method for the computation of Landau-fluid (LF) closure operators [Hammett and Perkins, Phys. Rev. Lett. 64, 3019 (1990)] is presented, based on an approximation by a sum of modified-Helmholtz-equation solves (SMHS) in configuration space. This method can yield fast-Fourier-like scaling of the computational time requirements and also provides a very compact data representation of these operators, even for plasmas with large spatial nonuniformity. As a result, the method can give significant savings compared with direct application of “delocalization kernels” [e.g., Schurtz et al., Phys. Plasmas 7, 4238 (2000)], both in terms of computational cost and memory requirements. The method is of interest for the implementation of Landau-fluid models in situations where the spatial nonuniformity, particular geometry, or boundary conditions render a Fourier implementation difficult or impossible. Systematic procedures have been developed to optimize the resulting operators for accuracy and computational cost. The four-moment Landau-fluid model of Hammett and Perkins has been implemented in the BOUT++ code using the SMHS method for LF closure. Excellent agreement has been obtained for the one-dimensional plasma density response function between driven initial-value calculations using this BOUT++ implementation and matrix eigenvalue calculations using both Fourier and SMHS non-Fourier implementations of the LF closures. The SMHS method also forms the basis for the implementation, which has been carried out in the BOUT++ code, of the parallel and toroidal drift-resonance LF closures. The method is a key enabling tool for the extension of gyro-Landau-fluid models [e.g., Beer and Hammett, Phys. Plasmas 3, 4046 (1996)] to codes that treat regions with strong profile variation, such as the tokamak edge and scrapeoff-layer.

Wave scattering theory a series approach based on the Fourier transformation

CERN Document Server

Eom, Hyo J

2001-01-01

The book provides a unified technique of Fourier transform to solve the wave scattering, diffraction, penetration, and radiation problems where the technique of separation of variables is applicable. The book discusses wave scattering from waveguide discontinuities, various apertures, and coupling structures, often encountered in electromagnetic, electrostatic, magnetostatic, and acoustic problems. A system of simultaneous equations for the modal coefficients is formulated and the rapidly-convergent series solutions amenable to numerical computation are presented. The series solutions find practical applications in the design of microwave/acoustic transmission lines, waveguide filters, antennas, and electromagnetic interference/compatibilty-related problems.

Microwave Irradiation of Nanohydroxyapatite from Chicken Eggshells and Duck Eggshells

Directory of Open Access Journals (Sweden)

Nor Adzliana Sajahan

2014-01-01

Full Text Available Due to similarity in composition to the mineral component of bones and human hard tissues, hydroxyapatite with chemical formula Ca10(PO46(OH2 has been widely used in medical field. Both chicken and duck eggshells are mainly composed of calcium carbonate. An attempt has been made to fabricate nanohydroxyapatite (nHA by chicken (CES and duck eggshells (DES as calcium carbonate source (CaCO3. CES and DES were reacted with diammonium hydrogen [(NH42HPO4] solution and subjected to microwave heating at 15 mins. Under the effect of microwave irradiation, nHA was produced directly in the solution and involved in crystallographic transformation. Sample characterization was done using by X-ray diffraction (XRD, fourier transform infrared spectroscopy (FTIR, and scanning electron microscopy (SEM.

Angular acceptance analysis of an infrared focal plane array with a built-in stationary Fourier transform spectrometer.

Science.gov (United States)

Gillard, Frédéric; Ferrec, Yann; Guérineau, Nicolas; Rommeluère, Sylvain; Taboury, Jean; Chavel, Pierre

2012-06-01

Stationary Fourier transform spectrometry is an interesting concept for building reliable field or embedded spectroradiometers, especially for the mid- and far- IR. Here, a very compact configuration of a cryogenic stationary Fourier transform IR (FTIR) spectrometer is investigated, where the interferometer is directly integrated in the focal plane array (FPA). We present a theoretical analysis to explain and describe the fringe formation inside the FTIR-FPA structure when illuminated by an extended source positioned at a finite distance from the detection plane. The results are then exploited to propose a simple front lens design compatible with a handheld package.

Using Multilayered Substrate Integrated Waveguide to Design Microwave Gain Equalizer

Directory of Open Access Journals (Sweden)

Yongfei Wang

2014-01-01

Full Text Available This paper presents the design and experiment of a novel microwave gain equalizer based on the substrate integrated waveguide (SIW technique. The proposed equalizer is formed by an SIW loaded by SIW resonators, which has very compact structure and can compensate for gain slope of microwave systems. Equivalent circuit analysis is given about the proposed structure for a better insight into the structure’s response. A Ku-Band equalizer with four SIW resonators is simulated and fabricated with a multilayer printed circuit board process. The measured results show good performance and agreement with the simulated results; an attenuation slope of −4.5 dB over 12.5–13.5 GHz is reached with a size reduction of 76%.

Preparation and characterization of flexible ferromagnetic nanocomposites for microwave applications

Energy Technology Data Exchange (ETDEWEB)

Thomas, Teena; Kanoth, Bipinbal P. [Department of Polymer Science & Rubber Technology, Cochin University of Science & Technology, Cochin, 682022, Kerala (India); Nijas, C.M. [Department of Electronics, Cochin University of Science & Technology, Cochin, 682022, Kerala (India); Joy, P.A. [Physical and Materials Chemistry Division, National Chemical Laboratory, Pune 411008 (India); Joseph, Joseph M. [Inter University Centre for Nanomaterials and Devices, Cochin University of Science & Technology, Cochin 682022, Kerala (India); Kuthirummal, Narayanan, E-mail: kuthirummaln@cofc.edu [Department of Physics and Astronomy, College of Charleston, Charleston, SC 29424 (United States); Thachil, Eby T., E-mail: ethachil@gmail.com [Department of Polymer Science & Rubber Technology, Cochin University of Science & Technology, Cochin, 682022, Kerala (India)

2015-10-15

Highlights: • Fe{sub 3}O{sub 4} nanoparticles (∼20 nm) were synthesised by co-precipitation method. • Nanoparticles were homogeneously distributed in natural rubber through latex stage processing. • Mechanical properties and magnetic properties of composites improved with loading Fe{sub 3}O{sub 4} nanoparticles. • Imaginary part of permeability increases with nanoparticle loading improving the microwave absorption characteristics. • Infrared spectra reveal strong interaction between NR and iron oxide nanoparticles. - Abstract: Magnetic Fe{sub 3}O{sub 4} nanoparticles (∼20 nm) were synthesized using the chemical co-precipitation method with a view of developing flexible and easily processable ferromagnetic materials with high mouldability to be used as microwave absorbers. The nanoparticles prepared were incorporated into natural rubber through latex stage processing. This novel processing method gives better dispersion of particles in the rubber matrix. The composites were characterized using XRD, SEM, vibrating sample magnetometer, dynamic mechanical analyzer, cavity perturbation, thermogravimetry (TGA), and Fourier transform infrared photoacoustic spectroscopy (FTIR-PAS). A notable improvement in the mechanical properties of composites was observed upon adding Fe{sub 3}O{sub 4} particles. Magnetic and microwave characteristics of the composites indicate the formation of a flexible ferromagnetic material with good microwave absorption characteristics.

Microwave antenna holography

Science.gov (United States)

Rochblatt, David J.; Seidel, Boris L.

1992-01-01

This microwave holography technique utilizes the Fourier transform relation between the complex far field radiation pattern of an antenna and the complex aperture field distribution. Resulting aperture phase and amplitude distribution data can be used to precisely characterize various crucial performance parameters, including panel alignment, panel shaping, subreflector position, antenna aperture illumination, directivity at various frequencies, and gravity deformation effects. The methodology of data processing presented here was successfully applied to the Deep Space Network (DSN) 34-m beam waveguide antennas. The antenna performance was improved at all operating frequencies by reducing the main reflector mechanical surface rms error to 0.43 mm. At Ka-band (32 GHz), the estimated improvement is 4.1 dB, resulting in an aperture efficiency of 52 percent. The performance improvement was verified by efficiency measurements and additional holographic measurements.

400 kV injector compact ECR ion source

International Nuclear Information System (INIS)

Constantin, F.; Catana, D.; Macovei, M.; Ivanov, E.

1997-01-01

Obtaining multiple ionised ions is a fundamental problem for some applications and research. Multiple ionised ions can be produced from electronic bombardment, when n·τ≥5·10 9 cm -3 · s, where n is the density of electrons (in cm -3 ) and τ is the time of interaction between electrons and ions . The relative speed of electrons and ions determines the equilibrium between the stripping process of the atom's electrons and their capture. An ion source with high ionisation efficiency and large output current is the ECR source (Electron Cyclotron Resonance). Using an ECR source with permanent magnets as ion source for the injector will lead to following advantages: - the possibility to obtain multiple ionised particles; - an increase of ion beam intensities; - the expanding of accelerator activities; - a longer working time, due to magnetron lifetime. The ECR ion source is robust, compact and capable of high intensities of extracted ion current. The large functional domain for the residual gas pressure allows the production of multiple charged ions. The source can be easily integrated in the TRILAC's injection structure. We realised a compact microwave ion source which has an axial magnetic field generated by a permanent magnet of Co-Sm. 1200 G magnetic field is greater than the 875 G magnetic field corresponding to the electron-cyclotron frequency of 2.45 GHz. The microwave generator is a magnetron (2.45 GHz and 200 W in continuos wave). The microwave is fed through a coaxial connector on the top of flange. The test was made on He gas at a pressure between 8· 10 -4 and 5·10 -2 torr. The ion beam current was measured vs. extracted potential from 3 kV to 10 kV and has a dependence according to U 3/2 law. A maximal ion current of 300 μA at 10 kV extraction potential was measured. Dimension of ECR ion source, including Einzel lens are φ=12 cm and h=16 cm. (authors)

Microwave-ultrasound combined reactor suitable for atmospheric sample preparation procedure of biological and chemical products

NARCIS (Netherlands)

Lagha, A.; Chemat, S.; Bartels, P.V.; Chemat, F.

1999-01-01

A compact apparatus in which a specific position can be irradiated by microwaves (MW) and ultrasound (US) simultaneously has been developed. The MW-US reactor has been designed for atmospheric pressure digestion and dissolution of biological and chemical products. The reactor can treat a range of

Microwave absorbing properties of polyaniline/multi-walled carbon nanotube composites with various polyaniline contents

International Nuclear Information System (INIS)

Ting, T.H.; Jau, Y.N.; Yu, R.P.

2012-01-01

Polyaniline/multi-walled carbon nanotube (PANI/MWNT) composites were synthesized using in situ polymerization at different aniline/multi-walled carbon nanotube weight ratios (Ani/MWNT = 1/2, 1/1, 2/1 and 3/1) and introduced into an epoxy resin to act as a microwave absorber. The spectroscopic characterization of the process of formation of PANI/MWNT composites were studied using Fourier transform infrared spectroscopy, an ultraviolet-visible spectrophotometer, X-ray diffraction, scanning electron microscopy, transmission electron microscopy and electron spin resonance. The microwave absorbing properties were investigated by measuring complex permittivity, complex permeability and reflection loss in the 2-18 and 18-40 GHz microwave frequency range, using the free space method. The results showed that the addition of PANI was useful for achieving a large absorption over a wide frequency range, especially for higher frequency values.

Treatment of nitridation by microwave post discharge plasma in an AISI 4140 steel

International Nuclear Information System (INIS)

Medina F, A.; Rodriguez L, V.; Zamora R, L.; Oseguera P, J.

1998-01-01

The objective of this work is to determine through X-ray diffraction, microhardness measurement and scanning electron microscopy those main operation parameters of the microwave post discharge treatment (temperature of treatment, gas mixture and permanence time) nitriding an AISI 4140 steel and to characterize the compact layer of nitrides formed during the treatment. (Author)

Microwave pre-heating of natural rubber using a rectangular wave guide (MODE: TE10

Directory of Open Access Journals (Sweden)

Doo-ngam, N.

2007-11-01

Full Text Available This paper presents an application of microwave radiation for pre-heating of natural rubbercompounding with various sulphur contents. The natural rubber-compounding was pre-heated by microwave radiation using a rectangular wave guide system (MODE: TE10 operating at frequency of 2.45 GHz in which the power can vary from 0 to 1500 W. In the present work, the influence of power input, sample thickness, and sulphur content were examined after applying microwave radiation to the rubber samples. Results are discussed regarding the thermal properties, 3-D network, dielectric properties and chemical structures. From the result, firstly, it was found that microwave radiation can be applied to pre-heating natural rubber-compounding before the vulcanization process. Secondly, microwave radiation was very useful for pre-heating natural rubber-compounding that has a thickness greater than 5mm. Thirdly, crosslinking in natural rubber-compounding may occurs after pre-heating by microwave radiation though Fourier Transform Infrared Spectroscopy(FTIR. Finally, there a little effect of sulphur content on temperature profiles after applying microwave radiation to the natural rubber-compounding. Moreover, natural rubber-compounding without carbon black showed a lower heat absorption compared with natural rubbercompounding filled carbon black. This is due to the difference in dielectric loss factor. This preliminary result will be useful information in terms of microwave radiation for pre-heating natural rubber-compounding and rubber processing in industry.

Beyond Fourier

Science.gov (United States)

Hoch, Jeffrey C.

2017-10-01

Non-Fourier methods of spectrum analysis are gaining traction in NMR spectroscopy, driven by their utility for processing nonuniformly sampled data. These methods afford new opportunities for optimizing experiment time, resolution, and sensitivity of multidimensional NMR experiments, but they also pose significant challenges not encountered with the discrete Fourier transform. A brief history of non-Fourier methods in NMR serves to place different approaches in context. Non-Fourier methods reflect broader trends in the growing importance of computation in NMR, and offer insights for future software development.

Beyond Fourier.

Science.gov (United States)

Hoch, Jeffrey C

2017-10-01

Non-Fourier methods of spectrum analysis are gaining traction in NMR spectroscopy, driven by their utility for processing nonuniformly sampled data. These methods afford new opportunities for optimizing experiment time, resolution, and sensitivity of multidimensional NMR experiments, but they also pose significant challenges not encountered with the discrete Fourier transform. A brief history of non-Fourier methods in NMR serves to place different approaches in context. Non-Fourier methods reflect broader trends in the growing importance of computation in NMR, and offer insights for future software development. Copyright © 2017 Elsevier Inc. All rights reserved.

A compact 5.5 GHz band-rejected UWB antenna using complementary split ring resonators.

Science.gov (United States)

Islam, M M; Faruque, M R I; Islam, M T

2014-01-01

A band-removal property employing microwave frequencies using complementary split ring resonators (CSRRs) is applied to design a compact UWB antenna wishing for the rejection of some frequency band, which is meanwhile exercised by the existing wireless applications. The reported antenna comprises optimization of a circular radiating patch, in which slotted complementary SRRs are implanted. It is printed on low dielectric FR4 substrate material fed by a partial ground plane and a microstrip line. Validated results exhibit that the reported antenna shows a wide bandwidth covering from 3.45 to more than 12 GHz, with a compact dimension of 22 × 26 mm(2), and VSWR WLAN band.

Frequency and amplitude modulation of ultra-compact terahertz quantum cascade lasers using an integrated avalanche diode oscillator.

Science.gov (United States)

Castellano, Fabrizio; Li, Lianhe; Linfield, Edmund H; Davies, A Giles; Vitiello, Miriam S

2016-03-15

Mode-locked comb sources operating at optical frequencies underpin applications ranging from spectroscopy and ultrafast physics, through to absolute frequency measurements and atomic clocks. Extending their operation into the terahertz frequency range would greatly benefit from the availability of compact semiconductor-based sources. However, the development of any compact mode-locked THz laser, which itself is inherently a frequency comb, has yet to be achieved without the use of an external stimulus. High-power, electrically pumped quantum cascade lasers (QCLs) have recently emerged as a promising solution, owing to their octave spanning bandwidths, the ability to achieve group-velocity dispersion compensation and the possibility of obtaining active mode-locking. Here, we propose an unprecedented compact architecture to induce both frequency and amplitude self-modulation in a THz QCL. By engineering a microwave avalanche oscillator into the laser cavity, which provides a 10 GHz self-modulation of the bias current and output power, we demonstrate multimode laser emission centered around 3 THz, with distinct multiple sidebands. The resulting microwave amplitude and frequency self-modulation of THz QCLs opens up intriguing perspectives, for engineering integrated self-mode-locked THz lasers, with impact in fields such as nano- and ultrafast photonics and optical metrology.

Producing Lignin-Based Polyols through Microwave-Assisted Liquefaction for Rigid Polyurethane Foam Production

Directory of Open Access Journals (Sweden)

Bai-Liang Xue

2015-02-01

Full Text Available Lignin-based polyols were synthesized through microwave-assisted liquefaction under different microwave heating times (5–30 min. The liquefaction reactions were carried out using polyethylene glycol (PEG-400/glycerol as liquefying solvents and 97 wt% sulfur acid as a catalyst at 140 °C. The polyols obtained were analyzed for their yield, composition and structural characteristics using gel permeation chromatography (GPC, Fourier transform infrared (FT-IR and nuclear magnetic resonance (NMR spectra. FT-IR and NMR spectra showed that the liquefying solvents reacted with the phenol hydroxyl groups of the lignin in the liquefied product. With increasing microwave heating time, the viscosity of polyols was slightly increased and their corresponding molecular weight (MW was gradually reduced. The optimal condition at the microwave heating time (5 min ensured a high liquefaction yield (97.47% and polyol with a suitable hydroxyl number (8.628 mmol/g. Polyurethane (PU foams were prepared by polyols and methylene diphenylene diisocyanate (MDI using the one-shot method. With the isocyanate/hydroxyl group ([NCO]/[OH] ratio increasing from 0.6 to 1.0, their mechanical properties were gradually increased. This study provided some insight into the microwave-assisted liquefied lignin polyols for the production of rigid PU foam.

Microwave-Promoted Synthesis of Sulfonated Metallophthalocyanines and Aggregation in Different Solvents

Directory of Open Access Journals (Sweden)

Zhenhua Cheng

2015-01-01

Full Text Available Five metallosulfophthalocyanines (Fe, Ni, Zn, Co, and Cu compounds were synthesized by microwave irradiation. Compared to the conventional method of synthesis in terms of reaction time and yields, the microwave-promoted synthesis is preferred with high product yield and short reaction time. All synthesized products were characterized with MALDI-TOF mass spectrum, Fourier transform infrared spectroscopy (FT-IR, ultraviolet-visible spectroscopy (UV-Vis, and X-ray diffraction (XRD. Aggregation behavior of the five metallosulfophthalocyanines (MSPc in different solvents was studied by UV-Vis spectroscopy separately in N,N-dimethyl formamide (DMF and NaOH aqueous solution (5%wt. A redshift of maximum absorption wavelength and deviations from Lambert-Beer law with increasing the concentration were observed. The dimerization equilibrium constants (K of the five MSPc were determined, respectively.

Fourier phase in Fourier-domain optical coherence tomography

Science.gov (United States)

Uttam, Shikhar; Liu, Yang

2015-01-01

Phase of an electromagnetic wave propagating through a sample-of-interest is well understood in the context of quantitative phase imaging in transmission-mode microscopy. In the past decade, Fourier-domain optical coherence tomography has been used to extend quantitative phase imaging to the reflection-mode. Unlike transmission-mode electromagnetic phase, however, the origin and characteristics of reflection-mode Fourier phase are poorly understood, especially in samples with a slowly varying refractive index. In this paper, the general theory of Fourier phase from first principles is presented, and it is shown that Fourier phase is a joint estimate of subresolution offset and mean spatial frequency of the coherence-gated sample refractive index. It is also shown that both spectral-domain phase microscopy and depth-resolved spatial-domain low-coherence quantitative phase microscopy are special cases of this general theory. Analytical expressions are provided for both, and simulations are presented to explain and support the theoretical results. These results are further used to show how Fourier phase allows the estimation of an axial mean spatial frequency profile of the sample, along with depth-resolved characterization of localized optical density change and sample heterogeneity. Finally, a Fourier phase-based explanation of Doppler optical coherence tomography is also provided. PMID:26831383

Fourier phase in Fourier-domain optical coherence tomography.

Science.gov (United States)

Uttam, Shikhar; Liu, Yang

2015-12-01

Phase of an electromagnetic wave propagating through a sample-of-interest is well understood in the context of quantitative phase imaging in transmission-mode microscopy. In the past decade, Fourier-domain optical coherence tomography has been used to extend quantitative phase imaging to the reflection-mode. Unlike transmission-mode electromagnetic phase, however, the origin and characteristics of reflection-mode Fourier phase are poorly understood, especially in samples with a slowly varying refractive index. In this paper, the general theory of Fourier phase from first principles is presented, and it is shown that Fourier phase is a joint estimate of subresolution offset and mean spatial frequency of the coherence-gated sample refractive index. It is also shown that both spectral-domain phase microscopy and depth-resolved spatial-domain low-coherence quantitative phase microscopy are special cases of this general theory. Analytical expressions are provided for both, and simulations are presented to explain and support the theoretical results. These results are further used to show how Fourier phase allows the estimation of an axial mean spatial frequency profile of the sample, along with depth-resolved characterization of localized optical density change and sample heterogeneity. Finally, a Fourier phase-based explanation of Doppler optical coherence tomography is also provided.

Carbonated hydrocalumite synthesized by the microwave method as a possible antacid

Energy Technology Data Exchange (ETDEWEB)

Linares, Carlos F., E-mail: clinares@uc.edu.ve [Unidad de Síntesis de Materiales y Metales de Transición, Facultad de Ciencias y Tecnología, Departamento de Química, Universidad de Carabobo, Valencia, Edo, Carabobo Apartado Postal 3336 (Venezuela, Bolivarian Republic of); Moscosso, Joel; Alzurutt, Victor; Ocanto, Freddy; Bretto, Pablo [Unidad de Síntesis de Materiales y Metales de Transición, Facultad de Ciencias y Tecnología, Departamento de Química, Universidad de Carabobo, Valencia, Edo, Carabobo Apartado Postal 3336 (Venezuela, Bolivarian Republic of); González, Gema [Laboratorio de Materiales, Centro Tecnológico, Instituto Venezolano de Investigaciones Científicas (IVIC), Carretera Panamericana Km 11 Altos de Pipe, Los Teques (Venezuela, Bolivarian Republic of)

2016-04-01

A carbonated hydrocalumite was synthesized by the microwave method for being used as antacid. The gel was formed using Ca and Al nitrate solutions in a basic medium (NaOH + Na{sub 2}CO{sub 3}), then, this gel was aged and heated in a domestic microwave for 2.5 min (1250 W). The obtained white solid was washed with distilled water, dried in an oven at 100 °C for 18 h and characterized by different techniques such as: X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FT-IR), BET surface area measurements, scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX). Finally, the carbonated hydrocalumite was tested as antacid by using a synthetic gastric juice and its activity was compared with a commercial antacid formulated with hydrotalcite. Results showed that the carbonated hydrocalumite was more effective than that commercial antacid. - Highlights: • Carbonated hydrocalumite was synthesized by the microwave method. • The aging time was drastically reduced. • Carbonated hydrocalumite was more active as antacid than a commercial antacid based on hydrotalcites.

Hyperspectral imaging using the single-pixel Fourier transform technique

Science.gov (United States)

Jin, Senlin; Hui, Wangwei; Wang, Yunlong; Huang, Kaicheng; Shi, Qiushuai; Ying, Cuifeng; Liu, Dongqi; Ye, Qing; Zhou, Wenyuan; Tian, Jianguo

2017-03-01

Hyperspectral imaging technology is playing an increasingly important role in the fields of food analysis, medicine and biotechnology. To improve the speed of operation and increase the light throughput in a compact equipment structure, a Fourier transform hyperspectral imaging system based on a single-pixel technique is proposed in this study. Compared with current imaging spectrometry approaches, the proposed system has a wider spectral range (400-1100 nm), a better spectral resolution (1 nm) and requires fewer measurement data (a sample rate of 6.25%). The performance of this system was verified by its application to the non-destructive testing of potatoes.

Approximating the Analytic Fourier Transform with the Discrete Fourier Transform

OpenAIRE

Axelrod, Jeremy

2015-01-01

The Fourier transform is approximated over a finite domain using a Riemann sum. This Riemann sum is then expressed in terms of the discrete Fourier transform, which allows the sum to be computed with a fast Fourier transform algorithm more rapidly than via a direct matrix multiplication. Advantages and limitations of using this method to approximate the Fourier transform are discussed, and prototypical MATLAB codes implementing the method are presented.

Microwave frequency sweep interferometer for plasma density measurements in ECR ion sources: Design and preliminary results

Energy Technology Data Exchange (ETDEWEB)

Torrisi, Giuseppe [INFN - Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy); University Mediterranea of Reggio Calabria, Reggio Calabria (Italy); Mascali, David; Neri, Lorenzo; Leonardi, Ornella; Celona, Luigi; Castro, Giuseppe; Agnello, Riccardo; Caruso, Antonio; Passarello, Santi; Longhitano, Alberto; Gammino, Santo [INFN - Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy); Sorbello, Gino [INFN - Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy); University of Catania, Catania, Italy and INFN-LNS, Catania (Italy); Isernia, Tommaso [University Mediterranea of Reggio Calabria, Reggio Calabria (Italy)

2016-02-15

The Electron Cyclotron Resonance Ion Sources (ECRISs) development is strictly related to the availability of new diagnostic tools, as the existing ones are not adequate to such compact machines and to their plasma characteristics. Microwave interferometry is a non-invasive method for plasma diagnostics and represents the best candidate for plasma density measurement in hostile environment. Interferometry in ECRISs is a challenging task mainly due to their compact size. The typical density of ECR plasmas is in the range 10{sup 11}–10{sup 13} cm{sup −3} and it needs a probing beam wavelength of the order of few centimetres, comparable to the chamber radius. The paper describes the design of a microwave interferometer developed at the LNS-INFN laboratories based on the so-called “frequency sweep” method to filter out the multipath contribution in the detected signals. The measurement technique and the preliminary results (calibration) obtained during the experimental tests will be presented.

Microwave assisted synthesis of hydroxyapatite nano strips

Energy Technology Data Exchange (ETDEWEB)

Ruban Kumar, A.; Kalainathan, S.; Saral, A.M. [School of Advanced Sciences, VIT University, Vellore 632014, Tamil Nadu (India)

2010-07-15

Synthesis of hydroxyapatite (HAP) nano strips was carried out by chemical precipitation method followed by microwave irradiation. The microwave assisted reactions proceed at fast rates. It is found that the presence of the complex reagent EDTA plays an important role in the morphological changes of nanostructure hydroxyapatite. EDTA acts as a hexadentate unit by wrapping itself around the Ca{sup 2+} metal ion with, four oxygen and two nitrogen atoms and forms several five member chelate rings. The relative specific surface energies associated with the facets of the crystal determines the shape of the crystal. Scanning electron microscopy revealed the presence of hydroxyapatite nano strips with the range 50-100 nm in EDTA influenced HAP powders. Fourier transform-infrared spectroscopy (FT-IR) result combined with the X-ray diffraction (XRD) indicates the presence of amorphous hydroxyapatite (HAP) in the as-prepared material. X-ray patterns collected on the powder after heat-treatment at 1100 C for 2 h in air exhibits single phase of HAP. (copyright 2010 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

The Fourier Transform Microwave (ftmw) Spectra of Cyclohexene Oxide and its Argon Complex

Science.gov (United States)

Frohman, Daniel J.; Novick, Stewart E.; Pringle, Wallace C.

2012-06-01

The microwave spectrum of cyclohexene oxide and its isotopologues have been observed and assigned, improving upon previous rotational studies of this molecule. Additionally, the 17O isotopomer of cyclohexene oxide and the Ar complex of the normal isotopologue of cyclohexene oxide have been fit for the first time. Fits for the 13C-cyclohexene oxide Ar complexes will also be presented. Tatsuya Ikeda, Roger Kewley, and R. F. Curl, Jr. J. Mol. Spectrosc., 4} (1972), 459-469. Raquel Sánchez, Susana Blanco, Juan C. López, and José L. Alonso. J. Mol. Struct., 780-781 (2006), 57-64.

Measurements of beam current density and proton fraction of a permanent-magnet microwave ion source

Energy Technology Data Exchange (ETDEWEB)

Waldmann, Ole; Ludewigt, Bernhard [Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States)

2011-11-15

A permanent-magnet microwave ion source has been built for use in a high-yield, compact neutron generator. The source has been designed to produce up to 100 mA of deuterium and tritium ions. The electron-cyclotron resonance condition is met at a microwave frequency of 2.45 GHz and a magnetic field strength of 87.5 mT. The source operates at a low hydrogen gas pressure of about 0.15 Pa. Hydrogen beams with a current density of 40 mA/cm{sup 2} have been extracted at a microwave power of 450 W. The dependence of the extracted proton beam fraction on wall materials and operating parameters was measured and found to vary from 45% for steel to 95% for boron nitride as a wall liner material.

Synthesis and characterization of some metal oxide nanocrystals by microwave irradiation

Energy Technology Data Exchange (ETDEWEB)

Rashad, M.; Gaber, A.; Abdelrahim, M. A.; Abdel-Baset, A. M. [Physics Department, Faculty of Science, Assiut University, 71516 Assiut (Egypt); Moharram, A. H. [Physics Dept., College of Science and Arts, King Abdulaziz Univ., Rabigh 21911 (Saudi Arabia)

2013-12-16

Copper oxide and cobalt oxide (CuO, Co3O4) nanocrystals (NCs) have been successfully prepared in a short time using microwave irradiation. The resulted powders of nanocrystals (NCs) were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Thermogravimetric analysis (TGA) measurements are also studied. Fourier-transform infrared (FT-IR) and UV–visible absorption spectroscopy of both kind of nanoparticels are illustrated. Optical absorption analysis indicated the direct band gap for both kinds of nanocrystals.

Fourier-Hermite communications; where Fourier meets Hermite

NARCIS (Netherlands)

Korevaar, C.W.; Kokkeler, Andre B.J.; de Boer, Pieter-Tjerk; Smit, Gerardus Johannes Maria

A new signal set, based on the Fourier and Hermite signal bases, is introduced. It combines properties of the Fourier basis signals with the perfect time-frequency localization of the Hermite functions. The signal set is characterized by both a high spectral efficiency and good time-frequency

H∞ Robust Control of a Large-Piston MEMS Micromirror for Compact Fourier Transform Spectrometer Systems

Directory of Open Access Journals (Sweden)

Huipeng Chen

2018-02-01

Full Text Available Incorporating linear-scanning micro-electro-mechanical systems (MEMS micromirrors into Fourier transform spectral acquisition systems can greatly reduce the size of the spectrometer equipment, making portable Fourier transform spectrometers (FTS possible. How to minimize the tilting of the MEMS mirror plate during its large linear scan is a major problem in this application. In this work, an FTS system has been constructed based on a biaxial MEMS micromirror with a large-piston displacement of 180 μm, and a biaxial H∞ robust controller is designed. Compared with open-loop control and proportional-integral-derivative (PID closed-loop control, H∞ robust control has good stability and robustness. The experimental results show that the stable scanning displacement reaches 110.9 μm under the H∞ robust control, and the tilting angle of the MEMS mirror plate in that full scanning range falls within ±0.0014°. Without control, the FTS system cannot generate meaningful spectra. In contrast, the FTS yields a clean spectrum with a full width at half maximum (FWHM spectral linewidth of 96 cm−1 under the H∞ robust control. Moreover, the FTS system can maintain good stability and robustness under various driving conditions.

H∞ Robust Control of a Large-Piston MEMS Micromirror for Compact Fourier Transform Spectrometer Systems.

Science.gov (United States)

Chen, Huipeng; Li, Mengyuan; Zhang, Yi; Xie, Huikai; Chen, Chang; Peng, Zhangming; Su, Shaohui

2018-02-08

Incorporating linear-scanning micro-electro-mechanical systems (MEMS) micromirrors into Fourier transform spectral acquisition systems can greatly reduce the size of the spectrometer equipment, making portable Fourier transform spectrometers (FTS) possible. How to minimize the tilting of the MEMS mirror plate during its large linear scan is a major problem in this application. In this work, an FTS system has been constructed based on a biaxial MEMS micromirror with a large-piston displacement of 180 μm, and a biaxial H∞ robust controller is designed. Compared with open-loop control and proportional-integral-derivative (PID) closed-loop control, H∞ robust control has good stability and robustness. The experimental results show that the stable scanning displacement reaches 110.9 μm under the H∞ robust control, and the tilting angle of the MEMS mirror plate in that full scanning range falls within ±0.0014°. Without control, the FTS system cannot generate meaningful spectra. In contrast, the FTS yields a clean spectrum with a full width at half maximum (FWHM) spectral linewidth of 96 cm -1 under the H∞ robust control. Moreover, the FTS system can maintain good stability and robustness under various driving conditions.

Novel Low Loss Wide-Band Multi-Port Integrated Circuit Technology for RF/Microwave Applications

Science.gov (United States)

Simons, Rainee N.; Goverdhanam, Kavita; Katehi, Linda P. B.; Burke, Thomas P. (Technical Monitor)

2001-01-01

In this paper, novel low loss, wide-band coplanar stripline technology for radio frequency (RF)/microwave integrated circuits is demonstrated on high resistivity silicon wafer. In particular, the fabrication process for the deposition of spin-on-glass (SOG) as a dielectric layer, the etching of microvias for the vertical interconnects, the design methodology for the multiport circuits and their measured/simulated characteristics are graphically illustrated. The study shows that circuits with very low loss, large bandwidth, and compact size are feasible using this technology. This multilayer planar technology has potential to significantly enhance RF/microwave IC performance when combined with semi-conductor devices and microelectromechanical systems (MEMS).

Fourier transform NMR

International Nuclear Information System (INIS)

Hallenga, K.

1991-01-01

This paper discusses the concept of Fourier transformation one of the many precious legacies of the French mathematician Jean Baptiste Joseph Fourier, essential for understanding the link between continuous-wave (CW) and Fourier transform (FT) NMR. Although in modern FT NMR the methods used to obtain a frequency spectrum from the time-domain signal may vary greatly, from the efficient Cooley-Tukey algorithm to very elaborate iterative least-square methods based other maximum entropy method or on linear prediction, the principles for Fourier transformation are unchanged and give invaluable insight into the interconnection of many pairs of physical entities called Fourier pairs

Optic-microwave mixing velocimeter for superhigh velocity measurement

International Nuclear Information System (INIS)

Weng Jidong; Wang Xiang; Tao Tianjiong; Liu Cangli; Tan Hua

2011-01-01

The phenomenon that a light beam reflected off a moving object experiences a Doppler shift in its frequency underlies practical interferometric techniques for remote velocity measurements, such as velocity interferometer system for any reflector (VISAR), displacement interferometer system for any reflector (DISAR), and photonic Doppler velocimetry (PDV). While VISAR velocimeters are often bewildered by the fringe loss upon high-acceleration dynamic process diagnosis, the optic-fiber velocimeters such as DISAR and PDV, on the other hand, are puzzled by high velocity measurement over 10 km/s, due to the demand for the high bandwidth digitizer. Here, we describe a new optic-microwave mixing velocimeter (OMV) for super-high velocity measurements. By using currently available commercial microwave products, we have constructed a simple, compact, and reliable OMV device, and have successfully obtained, with a digitizer of bandwidth 6 GH only, the precise velocity history of an aluminum flyer plate being accelerated up to 11.2 km/s in a three stage gas-gun experiment.

Multichannel microwave interferometer with an antenna switching system for electron density measurement in a laboratory plasma experiment

Energy Technology Data Exchange (ETDEWEB)

Kawamori, Eiichirou; Lin, Yu-Hsiang [Institute of Space and Plasma Sciences, National Cheng Kung University, Tainan 70101, Taiwan (China); Mase, Atsushi [Art, Science and Technology Center for Cooperative Research, Kyushu University, Kasuga 816-8580 (Japan); Nishida, Yasushi; Cheng, C. Z. [Institute of Space and Plasma Sciences, National Cheng Kung University, Tainan 70101, Taiwan (China); Plasma and Space Science Center, National Cheng Kung University, Tainan 70101, Taiwan (China)

2014-02-15

This study presents a simple and powerful technique for multichannel measurements of the density profile in laboratory plasmas by microwave interferometry. This technique uses electromechanical microwave switches to temporally switch the connection between multiple receiver antennas and one phase-detection circuit. Using this method, the phase information detected at different positions is rearranged into a time series that can be acquired from a minimum number of data acquisition channels (e.g., two channels in the case of quadrature detection). Our successfully developed multichannel microwave interferometer that uses the antenna switching method was applied to measure the radial electron density profiles in a magnetized plasma experiment. The advantage of the proposed method is its compactness and scalability to multidimensional measurement systems at low cost.

The design of 28 GHz ECR Ion Source for the Compact Linear Accelerator in Korea

International Nuclear Information System (INIS)

MiSook, Won; ByoungSeob, Lee; JinYong, Park; DongJun Park; JongPil, Kim; JongSeong, Bae; JungKeum, Ahn; SonJong, Wang; Nakagawa, T.

2012-01-01

The construction of a compact linear accelerator is in progress by Korea Basic Science Institute. The main capability of this facility is the production of multiply ionized metal clusters and the generation more intense beams of highly charged ions for material, medical and nuclear physical research. To produce the intense beam of highly charged ions, we will construct an Electron Cyclotron Resonance Ion Source (ECRIS) using 28 GHz microwaves. For this ECRIS, the design of a superconducting magnet, microwave inlet, beam extraction and plasma chamber was completed. Also we are constructing a superconducting magnet system. In this poster, we will report the current status of development of our 28 GHz ECRIS. (authors)

Microwave-Assisted Synthesis of Chitosan/Polyvinyl Alcohol Silver Nanoparticles Gel for Wound Dressing Applications

Directory of Open Access Journals (Sweden)

Nguyen Thi Hiep

2016-01-01

Full Text Available The purpose of this study was to fabricate chitosan/poly(vinyl alcohol/Ag nanoparticles (CPA gels with microwave-assistance for skin applications. Microwave irradiation was employed to reduce silver ions to silver nanoparticles and to crosslink chitosan (CS with polyvinyl alcohol (PVA. The presence of silver nanoparticles in CPA gels matrix was examined using UV-Vis spectroscopy, transmission electron microscopy, and X-ray diffraction. The interaction of CS and PVA was analysed by Fourier transform infrared spectroscopy. The release of silver ions was determined by atomic absorption spectrometry. The antimicrobial properties of CPA gels against P. aeruginosa and S. aureus were investigated using agar diffusion method. Finally, the biocompatibility and wound-healing ability of the gels were studied using fibroblast cells (in vitro and mice models (in vivo. In conclusion, the results showed that CPA gels were successfully fabricated using microwave irradiation method. These gels can be applied to heal an open wound thanks to their antibacterial activity and biocompatibility.

On complex-valued deautoconvolution of compactly supported functions with sparse Fourier representation

International Nuclear Information System (INIS)

Bürger, Steven; Flemming, Jens; Hofmann, Bernd

2016-01-01

Convergence rates results for the Tikhonov regularization of nonlinear ill-posed operator equations are missing, even for a Hilbert space setting, if a range type source condition fails and if moreover nonlinearity conditions of tangential cone type cannot be shown. This situation applies for a deautoconvolution problem in complex-valued L 2 -spaces over finite real intervals, occurring in a slightly generalized version in laser optics. For this problem we show that the lack of applicable convergence rates results can be overcome under the assumption that the solution of the operator equation has a sparse Fourier representation. Precisely, we derive a variational source condition for that case, which implies a convergence rate immediately. The surprising observation is that a sparsity assumption imposed on the solution leads to success, although the used norm square is not known to be a sparsity promoting penalty in the Tikhonov functional. (paper)

Measurements of beam current density and proton fraction of a permanent-magnet microwave ion source.

Science.gov (United States)

Waldmann, Ole; Ludewigt, Bernhard

2011-11-01

A permanent-magnet microwave ion source has been built for use in a high-yield, compact neutron generator. The source has been designed to produce up to 100 mA of deuterium and tritium ions. The electron-cyclotron resonance condition is met at a microwave frequency of 2.45 GHz and a magnetic field strength of 87.5 mT. The source operates at a low hydrogen gas pressure of about 0.15 Pa. Hydrogen beams with a current density of 40 mA/cm(2) have been extracted at a microwave power of 450 W. The dependence of the extracted proton beam fraction on wall materials and operating parameters was measured and found to vary from 45% for steel to 95% for boron nitride as a wall liner material. © 2011 American Institute of Physics

Influence of PVP molecular weight on the microwave assisted in situ amorphization of indomethacin

DEFF Research Database (Denmark)

Doreth, Maria; Löbmann, Korbinian; Priemel, Petra

2018-01-01

. After plasticization by moisture, PVP K12 reached a Tg below ambient temperature (16 ± 2 °C) indicating that the Tg of the plasticized polymer is a key factor for the success of in situ amorphization. DSC analysis showed that the amorphized drug was part of a ternary glass solution consisting of IND......, PVP K12 and water. In dissolution tests, IND:PVP K12 compacts showed a delayed initial drug release due to a lack of compact disintegration, but reached a higher total drug release eventually. In summary, this study showed that the microwave assisted in situ amorphization was highly dependent...... on the Tg of the plasticized polymer....

Compact system for high-speed velocimetry using heterodyne techniques

International Nuclear Information System (INIS)

Strand, O. T.; Goosman, D. R.; Martinez, C.; Whitworth, T. L.; Kuhlow, W. W.

2006-01-01

We have built a high-speed velocimeter that has proven to be compact, simple to operate, and fairly inexpensive. This diagnostic is assembled using off-the-shelf components developed for the telecommunications industry. The main components are fiber lasers, high-bandwidth high-sample-rate digitizers, and fiber optic circulators. The laser is a 2 W cw fiber laser operating at 1550 nm. The digitizers have 8 GHz bandwidth and can digitize four channels simultaneously at 20 GS/s. The maximum velocity of this system is ∼5000 m/s and is limited by the bandwidth of the electrical components. For most applications, the recorded beat frequency is analyzed using Fourier transform methods, which determine the time response of the final velocity time history. Using the Fourier transform method of analysis allows multiple velocities to be observed simultaneously. We have obtained high-quality data on many experiments such as explosively driven surfaces and gas gun assemblies

Microwave-assisted synthesis of CuInSe{sub 2} nanoparticles in low-absorbing solvents

Energy Technology Data Exchange (ETDEWEB)

Oleksak, Richard P.; Flynn, Brendan T.; Herman, Gregory S. [School of Chemical, Biological and Environmental Engineering, Oregon State University, Corvallis, OR (United States); Schut, David M. [Voxtel Inc., Eugene, OR (United States)

2014-01-15

Copper indium diselenide (CIS) nanoparticles were synthesized using a microwave-assisted one-pot solvothermal approach. For these studies high microwave-absorbing precursors were used in combination with low microwave absorbing solvents tri-n-octylphosphine (TOP) and oleic acid (OA) to investigate the effect of selective heating of the precursors on nanoparticle synthesis. High-resolution transmission electron microscopy (TEM) results indicated that the nanoparticles were spherical, crystalline and 4-5 nm in diameter. X-ray diffraction (XRD) results indicated that the nanoparticles had a body-centered tetragonal structure with planar defects that decreased in concentration with increasing reaction temperature and reaction time. The nanoparticle compositions varied depending on the reaction conditions and the compositions were found to approach stoichiometry for increased reaction times. Fourier transform infrared (FTIR) spectroscopy indicated both solvents adsorbed to the nanoparticle surface and energy dispersive spectroscopy indicated that these ligands became chlorinated during the reaction. The uniform temperature profile offered by the microwave heating allowed for highly reproducible batch-to-batch reactions, allowing for tight control over composition and defect concentration. (copyright 2014 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim)

Fourier rebinning and consistency equations for time-of-flight PET planograms

International Nuclear Information System (INIS)

Li, Yusheng; Matej, Samuel; Metzler, Scott D; Defrise, Michel

2016-01-01

Due to the unique geometry, dual-panel PET scanners have many advantages in dedicated breast imaging and on-board imaging applications since the compact scanners can be combined with other imaging and treatment modalities. The major challenges of dual-panel PET imaging are the limited-angle problem and data truncation, which can cause artifacts due to incomplete data sampling. The time-of-flight (TOF) information can be a promising solution to reduce these artifacts. The TOF planogram is the native data format for dual-panel TOF PET scanners, and the non-TOF planogram is the 3D extension of linogram. The TOF planograms is five-dimensional while the objects are three-dimensional, and there are two degrees of redundancy. In this paper, we derive consistency equations and Fourier-based rebinning algorithms to provide a complete understanding of the rich structure of the fully 3D TOF planograms. We first derive two consistency equations and John’s equation for 3D TOF planograms. By taking the Fourier transforms, we obtain two Fourier consistency equations (FCEs) and the Fourier–John equation (FJE), which are the duals of the consistency equations and John’s equation, respectively. We then solve the FCEs and FJE using the method of characteristics. The two degrees of entangled redundancy of the 3D TOF data can be explicitly elicited and exploited by the solutions along the characteristic curves. As the special cases of the general solutions, we obtain Fourier rebinning and consistency equations (FORCEs), and thus we obtain a complete scheme to convert among different types of PET planograms: 3D TOF, 3D non-TOF, 2D TOF and 2D non-TOF planograms. The FORCEs can be used as Fourier-based rebinning algorithms for TOF-PET data reduction, inverse rebinnings for designing fast projectors, or consistency conditions for estimating missing data. As a byproduct, we show the two consistency equations are necessary and sufficient for 3D TOF planograms. Finally, we give

Efficient temporal compression of coherent nanosecond pulses in compact SBS generator-amplifier setup

OpenAIRE

Schiemann, S.; Ubachs, W.M.G.; Hogervorst, W.

1997-01-01

A pulse compressor based on stimulated Brillouin scattering (SBS) in liquids is experimentally and theoretically investigated. It allows for the compression of Fourier-transform limited nanosecond pulses of several hundreds of millijoules of energy with both high conversion efficiency and a high temporal compression factor. The two-cell generator-amplifier arrangement is of a compact design not requiring external attenuation of the generator cell input energy. Pulses from an injection-seeded,...

SIBI: A compact hyperspectral camera in the mid-infrared

Science.gov (United States)

Pola Fossi, Armande; Ferrec, Yann; Domel, Roland; Coudrain, Christophe; Guerineau, Nicolas; Roux, Nicolas; D'Almeida, Oscar; Bousquet, Marc; Kling, Emmanuel; Sauer, Hervé

2015-10-01

Recent developments in unmanned aerial vehicles have increased the demand for more and more compact optical systems. In order to bring solutions to this demand, several infrared systems are being developed at ONERA such as spectrometers, imaging devices, multispectral and hyperspectral imaging systems. In the field of compact infrared hyperspectral imaging devices, ONERA and Sagem Défense et Sécurité have collaborated to develop a prototype called SIBI, which stands for "Spectro-Imageur Birefringent Infrarouge". It is a static Fourier transform imaging spectrometer which operates in the mid-wavelength infrared spectral range and uses a birefringent lateral shearing interferometer. Up to now, birefringent interferometers have not been often used for hyperspectral imaging in the mid-infrared because of the lack of crystal manufacturers, contrary to the visible spectral domain where the production of uniaxial crystals like calcite are mastered for various optical applications. In the following, we will present the design and the realization of SIBI as well as the first experimental results.

Compact and high-resolution optical orbital angular momentum sorter

Directory of Open Access Journals (Sweden)

Chenhao Wan

2017-03-01

Full Text Available A compact and high-resolution optical orbital angular momentum (OAM sorter is proposed and demonstrated. The sorter comprises a quadratic fan-out mapper and a dual-phase corrector positioned in the pupil plane and the Fourier plane, respectively. The optical system is greatly simplified compared to previous demonstrations of OAM sorting, and the performance in resolution and efficiency is maintained. A folded configuration is set up using a single reflective spatial light modulator (SLM to demonstrate the validity of the scheme. The two phase elements are implemented on the left and right halves of the SLM and connected by a right-angle prism. Experimental results demonstrate the high resolution of the compact OAM sorter, and the current limit in efficiency can be overcome by replacing with transmissive SLMs and removing the beam splitters. This novel scheme paves the way for the miniaturization and integration of high-resolution OAM sorters.

Supercapacitors studies on BiPO4 nanoparticles synthesized via a simple microwave approach

Directory of Open Access Journals (Sweden)

S. Vadivel

2017-07-01

Full Text Available BiPO4 nanomaterial was synthesized using EDTA (ethylene diamine tetra acetic acid as the surfactant via a simple microwave method. The structure and morphology of BiPO4 were systematically characterized by X-ray diffraction (XRD, Fourier-transform infrared spectroscopy (FT-IR, and scanning electron microscopy (FE-SEM studies. The obtained BiPO4 nanoparticles were, on average, 150–300 nm. The electrochemical results showed that the specific capacitance of BiPO4 obtained using the microwave route was up to 104 Fg−1 at a current density of 1 Ag−1 with a large potential window of 1.7 V. The material showed excellent cycling stability (92% capacitance retention after 500 cycles at a current density of 1 Ag−1.

Picosecond pulses from wavelength-swept continuous-wave Fourier domain mode-locked lasers.

Science.gov (United States)

Eigenwillig, Christoph M; Wieser, Wolfgang; Todor, Sebastian; Biedermann, Benjamin R; Klein, Thomas; Jirauschek, Christian; Huber, Robert

2013-01-01

Ultrafast lasers have a crucial function in many fields of science; however, up to now, high-energy pulses directly from compact, efficient and low-power semiconductor lasers are not available. Therefore, we introduce a new approach based on temporal compression of the continuous-wave, wavelength-swept output of Fourier domain mode-locked lasers, where a narrowband optical filter is tuned synchronously to the round-trip time of light in a kilometre-long laser cavity. So far, these rapidly swept lasers enabled orders-of-magnitude speed increase in optical coherence tomography. Here we report on the generation of ~60-70 ps pulses at 390 kHz repetition rate. As energy is stored optically in the long-fibre delay line and not as population inversion in the laser-gain medium, high-energy pulses can now be generated directly from a low-power, compact semiconductor-based oscillator. Our theory predicts subpicosecond pulses with this new technique in the future.

On Fourier re-expansions

OpenAIRE

Liflyand, E.

2012-01-01

We study an extension to Fourier transforms of the old problem on absolute convergence of the re-expansion in the sine (cosine) Fourier series of an absolutely convergent cosine (sine) Fourier series. The results are obtained by revealing certain relations between the Fourier transforms and their Hilbert transforms.

Simultaneous microwave photonic and phononic band gaps in piezoelectric–piezomagnetic superlattices with three types of domains in a unit cell

Energy Technology Data Exchange (ETDEWEB)

Tang, Zheng-hua [Xiangnan University-Gospell Joint Laboratory of Microwave Communication Technology, Xiangnan University, Chenzhou 423000 (China); Jiang, Zheng-Sheng [National Laboratory of Solid State Microstructures and Department of Physics, Nanjing University, Nanjing 210093 (China); Chen, Tao [Laboratory of Quantum Information and Quantum Materials, School of Physics and Telecommunication Engineering, South China Normal University, Guangzhou 510006 (China); Lei, Da-Jun [Xiangnan University-Gospell Joint Laboratory of Microwave Communication Technology, Xiangnan University, Chenzhou 423000 (China); Yan, Wen-Yan, E-mail: yanwenyan88@126.com [School of Software and Communication Engineering, Xiangnan University, Chenzhou 423000 (China); Qiu, Feng; Huang, Jian-Quan; Deng, Hai-Ming; Yao, Min [Xiangnan University-Gospell Joint Laboratory of Microwave Communication Technology, Xiangnan University, Chenzhou 423000 (China)

2016-04-29

A novel phoxonic crystal using the piezoelectric (PMN-PT) and piezomagnetic (CoFe{sub 2}O{sub 4}) superlattices with three types of domains in a unit cell (PPSUC) is present, in which dual microwave photonic and phononic band gaps can be obtained simultaneously. Two categories of phononic band gaps, originating from both the Bragg scattering of acoustic waves in periodic structures at the Brillouin zone boundary and the electromagnetic wave-lattice vibration couplings near the Brillouin zone center, can be observed in the phononic band structures. The general characteristics of the microwave photonic band structures are similar to those of pure piezoelectric or piezomagnetic superlattices, with the major discrepancy being the appearance of nearly dispersionless branches within the microwave photonic band gaps, which show an extremely large group velocity delay. Thus, the properties may also be applied to compact acoustic-microwave devices. - Highlights: • Dual microwave photonic and phononic band gaps can coexist in the PPSUC. • Two categories of phononic band gaps with different mechanism can be obtained. • Nearly dispersionless branches appear in the microwave photonic band gaps.

Carbonated hydrocalumite synthesized by the microwave method as a possible antacid.

Science.gov (United States)

Linares, Carlos F; Moscosso, Joel; Alzurutt, Victor; Ocanto, Freddy; Bretto, Pablo; González, Gema

2016-04-01

A carbonated hydrocalumite was synthesized by the microwave method for being used as antacid. The gel was formed using Ca and Al nitrate solutions in a basic medium (NaOH+Na2CO3), then, this gel was aged and heated in a domestic microwave for 2.5 min (1250 W). The obtained white solid was washed with distilled water, dried in an oven at 100 °C for 18 h and characterized by different techniques such as: X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FT-IR), BET surface area measurements, scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX). Finally, the carbonated hydrocalumite was tested as antacid by using a synthetic gastric juice and its activity was compared with a commercial antacid formulated with hydrotalcite. Results showed that the carbonated hydrocalumite was more effective than that commercial antacid. Copyright © 2016 Elsevier B.V. All rights reserved.

A Compact 5.5 GHz Band-Rejected UWB Antenna Using Complementary Split Ring Resonators

Directory of Open Access Journals (Sweden)

M. M. Islam

2014-01-01

Full Text Available A band-removal property employing microwave frequencies using complementary split ring resonators (CSRRs is applied to design a compact UWB antenna wishing for the rejection of some frequency band, which is meanwhile exercised by the existing wireless applications. The reported antenna comprises optimization of a circular radiating patch, in which slotted complementary SRRs are implanted. It is printed on low dielectric FR4 substrate material fed by a partial ground plane and a microstrip line. Validated results exhibit that the reported antenna shows a wide bandwidth covering from 3.45 to more than 12 GHz, with a compact dimension of 22 × 26 mm2, and VSWR < 2, observing band elimination of 5.5 GHz WLAN band.

A microwave powered sensor assembly for microwave ovens

DEFF Research Database (Denmark)

2016-01-01

The present invention relates to a microwave powered sensor assembly for micro- wave ovens. The microwave powered sensor assembly comprises a microwave antenna for generating an RF antenna signal in response to microwave radiation at a predetermined excitation frequency. A dc power supply circuit...... of the microwave powered sensor assembly is operatively coupled to the RF antenna signal for extracting energy from the RF antenna signal and produce a power supply voltage. A sensor is connected to the power supply voltage and configured to measure a physical or chemical property of a food item under heating...... in a microwave oven chamber....

Microwave engineering

CERN Document Server

Pozar, David M

2012-01-01

The 4th edition of this classic text provides a thorough coverage of RF and microwave engineering concepts, starting from fundamental principles of electrical engineering, with applications to microwave circuits and devices of practical importance.  Coverage includes microwave network analysis, impedance matching, directional couplers and hybrids, microwave filters, ferrite devices, noise, nonlinear effects, and the design of microwave oscillators, amplifiers, and mixers. Material on microwave and RF systems includes wireless communications, radar, radiometry, and radiation hazards. A large

Design of a Narrow Bandwidth Bandpass Filter Using Compact Spiral Resonator with Chirality

Directory of Open Access Journals (Sweden)

Weiping Li

2016-01-01

Full Text Available In this article, a compact narrow-bandpass filter with high selectivity and improved rejection level is presented. For miniaturization, a pair of double negative (DNG cells consisting of quasi-planar chiral resonators are cascaded and electrically loaded to a microstrip transmission line; short ended stubs are introduced to expand upper rejection band. The structure is analyzed using equivalent circuit models and simulated based on EM simulation software. For validation, the proposed filter is fabricated and measured. The measured results are in good agreement with the simulated ones. By comparing to other filters in the references, it is shown that the proposed filter has the advantage of skirt selectivity and compact size, so it can be integrated more conveniently in modern wireless communication systems and microwave planar circuits.

Principles of Fourier analysis

CERN Document Server

Howell, Kenneth B

2001-01-01

Fourier analysis is one of the most useful and widely employed sets of tools for the engineer, the scientist, and the applied mathematician. As such, students and practitioners in these disciplines need a practical and mathematically solid introduction to its principles. They need straightforward verifications of its results and formulas, and they need clear indications of the limitations of those results and formulas.Principles of Fourier Analysis furnishes all this and more. It provides a comprehensive overview of the mathematical theory of Fourier analysis, including the development of Fourier series, "classical" Fourier transforms, generalized Fourier transforms and analysis, and the discrete theory. Much of the author''s development is strikingly different from typical presentations. His approach to defining the classical Fourier transform results in a much cleaner, more coherent theory that leads naturally to a starting point for the generalized theory. He also introduces a new generalized theory based ...

A compact, high resolution Michelson interferometer for atmospheric spectroscopy in the near ultraviolet

Science.gov (United States)

Sander, Stanley P.; Cageao, Richard P.; Friedl, Randall R.

1993-01-01

A new, compact Fourier Transform Michelson interferometer (FTUV) with an apodized resolving power greater than 300,000 at 300 nm, high throughput and wide spectral coverage has been developed. The objectives include atmospheric spectroscopy (direct solar absorption and solar scattering) and laboratory spectroscopy of transient species. In this paper, we will briefly describe the prototype FTUV instrument and the results of preliminary laboratory investigations of OH and ClO spectra in emission and absorption.

Microwave induced plasma for solid fuels and waste processing: A review on affecting factors and performance criteria.

Science.gov (United States)

Ho, Guan Sem; Faizal, Hasan Mohd; Ani, Farid Nasir

2017-11-01

High temperature thermal plasma has a major drawback which consumes high energy. Therefore, non-thermal plasma which uses comparatively lower energy, for instance, microwave plasma is more attractive to be applied in gasification process. Microwave-induced plasma gasification also carries the advantages in terms of simplicity, compactness, lightweight, uniform heating and the ability to operate under atmospheric pressure that gains attention from researchers. The present paper synthesizes the current knowledge available for microwave plasma gasification on solid fuels and waste, specifically on affecting parameters and their performance. The review starts with a brief outline on microwave plasma setup in general, and followed by the effect of various operating parameters on resulting output. Operating parameters including fuel characteristics, fuel injection position, microwave power, addition of steam, oxygen/fuel ratio and plasma working gas flow rate are discussed along with several performance criteria such as resulting syngas composition, efficiency, carbon conversion, and hydrogen production rate. Based on the present review, fuel retention time is found to be the key parameter that influences the gasification performance. Therefore, emphasis on retention time is necessary in order to improve the performance of microwave plasma gasification of solid fuels and wastes. Copyright © 2017 Elsevier Ltd. All rights reserved.

A near-field scanning microwave microscope based on a superconducting resonator for low power measurements.

Science.gov (United States)

de Graaf, S E; Danilov, A V; Adamyan, A; Kubatkin, S E

2013-02-01

We report on the design and performance of a cryogenic (300 mK) near-field scanning microwave microscope. It uses a microwave resonator as the near-field sensor, operating at a frequency of 6 GHz and microwave probing amplitudes down to 100 μV, approaching low enough photon population (N ∼ 1000) of the resonator such that coherent quantum manipulation becomes feasible. The resonator is made out of a miniaturized distributed fractal superconducting circuit that is integrated with the probing tip, micromachined to be compact enough such that it can be mounted directly on a quartz tuning-fork, and used for parallel operation as an atomic force microscope (AFM). The resonator is magnetically coupled to a transmission line for readout, and to achieve enhanced sensitivity we employ a Pound-Drever-Hall measurement scheme to lock to the resonance frequency. We achieve a well localized near-field around the tip such that the microwave resolution is comparable to the AFM resolution, and a capacitive sensitivity down to 6.4 × 10(-20) F/Hz, limited by mechanical noise. We believe that the results presented here are a significant step towards probing quantum systems at the nanoscale using near-field scanning microwave microscopy.

Portable Wideband Microwave Imaging System for Intracranial Hemorrhage Detection Using Improved Back-projection Algorithm with Model of Effective Head Permittivity

Science.gov (United States)

Mobashsher, Ahmed Toaha; Mahmoud, A.; Abbosh, A. M.

2016-02-01

Intracranial hemorrhage is a medical emergency that requires rapid detection and medication to restrict any brain damage to minimal. Here, an effective wideband microwave head imaging system for on-the-spot detection of intracranial hemorrhage is presented. The operation of the system relies on the dielectric contrast between healthy brain tissues and a hemorrhage that causes a strong microwave scattering. The system uses a compact sensing antenna, which has an ultra-wideband operation with directional radiation, and a portable, compact microwave transceiver for signal transmission and data acquisition. The collected data is processed to create a clear image of the brain using an improved back projection algorithm, which is based on a novel effective head permittivity model. The system is verified in realistic simulation and experimental environments using anatomically and electrically realistic human head phantoms. Quantitative and qualitative comparisons between the images from the proposed and existing algorithms demonstrate significant improvements in detection and localization accuracy. The radiation and thermal safety of the system are examined and verified. Initial human tests are conducted on healthy subjects with different head sizes. The reconstructed images are statistically analyzed and absence of false positive results indicate the efficacy of the proposed system in future preclinical trials.

Custom chipset and compact module design for a 75–110 GHz laboratory signal source

International Nuclear Information System (INIS)

Morgan, Matthew A; Boyd, Tod A; Castro, Jason J

2016-01-01

We report on the development and characterization of a compact, full-waveguide bandwidth (WR-10) signal source for general-purpose testing of mm-wave components. The monolithic microwave integrated circuit (MMIC) based multichip module is designed for compactness and ease-of-use, especially in size-constrained test sets such as a wafer probe station. It takes as input a cm-wave continuous-wave (CW) reference and provides a factor of three frequency multiplication as well as amplification, output power adjustment, and in situ output power monitoring. It utilizes a number of custom MMIC chips such as a Schottky-diode limiter and a broadband mm-wave detector, both designed explicitly for this module, as well as custom millimeter-wave multipliers and amplifiers reported in previous papers. (paper)

Preparation and characterization of activated carbon from pistachio nut shells via microwave-induced chemical activation

Energy Technology Data Exchange (ETDEWEB)

Foo, K. Y. [School of Chemical Engineering, Engineering Campus, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia); Hameed, B.H., E-mail: chbassim@eng.usm.my [School of Chemical Engineering, Engineering Campus, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang (Malaysia)

2011-07-15

In this work, pistachio nut shell, a biomass residue abundantly available from the pistachio nut processing industries, was utilized as a feedstock for the preparation of activated carbon (PSAC) via microwave assisted KOH activation. The activation step was performed at the microwave input power of 600 W and irradiation time of 7 min. The porosity, functional and surface chemistry were featured by means of low temperature nitrogen adsorption, scanning electron microscopy and Fourier transform infrared spectroscopy. Result showed that the BET surface area, Langmuir surface area, and total pore volume of PSAC were 700.53 m{sup 2} g{sup -1}, 1038.78 m{sup 2} g{sup -1} and 0.375 m{sup 3} g{sup -1}, respectively. The adsorptive property of PSAC was tested using methylene blue dye as the targeted adsorbate. Equilibrium data was best fitted by the Langmuir isotherm model, showing a monolayer adsorption capacity of 296.57 mg g{sup -1}. The study revealed the potentiality of microwave-induced activation as a viable activation method. -- Highlights: {yields} Pistachio nut shell activated carbon (PSAC) was prepared via microwave assisted KOH activation. {yields} The activation step was performed at the microwave input power of 600 W and irradiation time of 7 min. {yields} BET surface area of PSAC was 700.53 m{sup 2}/g. {yields} Monolayer adsorption capacity of PSAC for MB was 296.57 mg/g.

Preparation and characterization of activated carbon from pistachio nut shells via microwave-induced chemical activation

International Nuclear Information System (INIS)

Foo, K.Y.; Hameed, B.H.

2011-01-01

In this work, pistachio nut shell, a biomass residue abundantly available from the pistachio nut processing industries, was utilized as a feedstock for the preparation of activated carbon (PSAC) via microwave assisted KOH activation. The activation step was performed at the microwave input power of 600 W and irradiation time of 7 min. The porosity, functional and surface chemistry were featured by means of low temperature nitrogen adsorption, scanning electron microscopy and Fourier transform infrared spectroscopy. Result showed that the BET surface area, Langmuir surface area, and total pore volume of PSAC were 700.53 m 2 g -1 , 1038.78 m 2 g -1 and 0.375 m 3 g -1 , respectively. The adsorptive property of PSAC was tested using methylene blue dye as the targeted adsorbate. Equilibrium data was best fitted by the Langmuir isotherm model, showing a monolayer adsorption capacity of 296.57 mg g -1 . The study revealed the potentiality of microwave-induced activation as a viable activation method. -- Highlights: → Pistachio nut shell activated carbon (PSAC) was prepared via microwave assisted KOH activation. → The activation step was performed at the microwave input power of 600 W and irradiation time of 7 min. → BET surface area of PSAC was 700.53 m 2 /g. → Monolayer adsorption capacity of PSAC for MB was 296.57 mg/g.

Microwave imaging

CERN Document Server

Pastorino, Matteo

2010-01-01

An introduction to the most relevant theoretical and algorithmic aspects of modern microwave imaging approaches Microwave imaging-a technique used in sensing a given scene by means of interrogating microwaves-has recently proven its usefulness in providing excellent diagnostic capabilities in several areas, including civil and industrial engineering, nondestructive testing and evaluation, geophysical prospecting, and biomedical engineering. Microwave Imaging offers comprehensive descriptions of the most important techniques so far proposed for short-range microwave imaging-in

Limit theorems for Markov chains and stochastic properties of dynamical systems by quasi-compactness

CERN Document Server

Hervé, Loïc

2001-01-01

This book shows how techniques from the perturbation theory of operators, applied to a quasi-compact positive kernel, may be used to obtain limit theorems for Markov chains or to describe stochastic properties of dynamical systems. A general framework for this method is given and then applied to treat several specific cases. An essential element of this work is the description of the peripheral spectra of a quasi-compact Markov kernel and of its Fourier-Laplace perturbations. This is first done in the ergodic but non-mixing case. This work is extended by the second author to the non-ergodic case. The only prerequisites for this book are a knowledge of the basic techniques of probability theory and of notions of elementary functional analysis.

Microwave Synthesis Of Polyols For Urethane Materials

International Nuclear Information System (INIS)

Zeltins, V; Cabulis, U; Abolins, A; Gaidukovs, S

2016-01-01

The preparation of polyurethane (PU) polyols processed with the use of microwave (MW) irradiation heating polyols is reported. The PU polyols were consisted from bio-based rapeseed oil (RO) and recycled polyethylene terephthalate (PET) components are reported. Obtained MW polyols were compared to the conventional PU polyols synthesized by traditional heating in oil bath. The polyols have the similar properties. The obtained MW assisted polyols were characterized by Fourier transform infrared spectroscopy (FT-IR) measurements. Acid number, hydroxyl value, moisture content and viscosity of the MW synthesized polyols were measured. The obtained polyols consisted from about 34% RO and 23% PET components. The advantages of the very fast reaction rate for preparation of PU polyols, by using MW instead of the conventional heating process, are shown. (paper)

Experimental demonstration of subwavelength domino plasmon devices for compact high-frequency circuit.

Science.gov (United States)

Ma, Y G; Lan, L; Zhong, S M; Ong, C K

2011-10-24

In optical frequency, surface plasmons of metal provide us a prominent way to build compact photonic devices or circuits with non-diffraction limit. It is attributed by their extraordinary electromagnetic confining effect. But in the counterpart of lower frequencies, plasmonics behavior of metal is screened by eddy current induced in a certain skin depth. To amend this, spoof plasmons engineered by artificial structures have been introduced to mimic surface plasmons in these frequencies. But it is less useful for practical application due to their weak field confinement as manifested by large field decaying length in the upper dielectric space. Recently, a new type of engineered plasmons, domino plasmon was theoretically proposed to produce unusual field confinement and waveguiding capabilities that make them very attractive for ultra-compact device applications [Opt. Exp. 18, 754-764 (2010)]. In this work, we implemented these ideas and built three waveguiding devices based on domino plasmons. Their strong capabilities to produce versatile and ultra-compact devices with multiple electromagnetic functions have been experimentally verified in microwaves. And that can be extended to THz regime to pave the way for a new class of integrated wave circuits. © 2011 Optical Society of America

Automatic Fourier transform and self-Fourier beams due to parabolic potential

Energy Technology Data Exchange (ETDEWEB)

Zhang, Yiqi, E-mail: zhangyiqi@mail.xjtu.edu.cn [Key Laboratory for Physical Electronics and Devices of the Ministry of Education & Shaanxi Key Lab of Information Photonic Technique, Xi’an Jiaotong University, Xi’an 710049 (China); Liu, Xing [Key Laboratory for Physical Electronics and Devices of the Ministry of Education & Shaanxi Key Lab of Information Photonic Technique, Xi’an Jiaotong University, Xi’an 710049 (China); Belić, Milivoj R., E-mail: milivoj.belic@qatar.tamu.edu [Science Program, Texas A& M University at Qatar, P.O. Box 23874 Doha (Qatar); Zhong, Weiping [Department of Electronic and Information Engineering, Shunde Polytechnic, Shunde 528300 (China); Petrović, Milan S. [Institute of Physics, P.O. Box 68, 11001 Belgrade (Serbia); Zhang, Yanpeng, E-mail: ypzhang@mail.xjtu.edu.cn [Key Laboratory for Physical Electronics and Devices of the Ministry of Education & Shaanxi Key Lab of Information Photonic Technique, Xi’an Jiaotong University, Xi’an 710049 (China)

2015-12-15

We investigate the propagation of light beams including Hermite–Gauss, Bessel–Gauss and finite energy Airy beams in a linear medium with parabolic potential. Expectedly, the beams undergo oscillation during propagation, but quite unexpectedly they also perform automatic Fourier transform, that is, periodic change from the beam to its Fourier transform and back. In addition to oscillation, the finite-energy Airy beams exhibit periodic inversion during propagation. The oscillating period of parity-asymmetric beams is twice that of the parity-symmetric beams. Based on the propagation in parabolic potential, we introduce a class of optically-interesting beams that are self-Fourier beams—that is, the beams whose Fourier transforms are the beams themselves.

Microwave-assisted synthesis of iron oxide nanoparticles in biocompatible organic environment

Science.gov (United States)

Aivazoglou, E.; Metaxa, E.; Hristoforou, E.

2018-04-01

The development of magnetite and maghemite particles in uniform nanometer size has triggered the interest of the research community due to their many interesting properties leading to a wide range of applications, such as catalysis, nanomedicine-nanobiology and other engineering applications. In this study, a simple, time-saving and low energy-consuming, microwave-assisted synthesis of iron oxide nanoparticles, is presented. The nanoparticles were prepared by microwave-assisted synthesis using polyethylene glycol (PEG) or PEG and β-cyclodextrin (β-CD)/water solutions of chloride salts of iron in the presence of ammonia solution. The prepared nano-powders were characterized using X-Ray Diffraction (XRD), Transition Electron Microscopy (TEM), Fourier-transform Infrared Spectroscopy (FTIR), Raman Spectroscopy, Vibrating Sample Magnetometer (VSM), X-Ray Photoelectron Spectroscopy (XPS) and Thermal analysis (TG/DSC). The produced nanoparticles are crystallized mostly in the magnetite and maghemite lattice exhibiting very similar shape and size, with indications of partial PEG coating. Heating time, microwave power and presence of PEG, are the key factors shaping the size properties of nanoparticles. The average size of particles ranges from 10.3 to 19.2 nm. The nanoparticles exhibit a faceted morphology, with zero contamination levels. The magnetic measurements indicate that the powders are soft magnetic materials with negligible coercivity and remanence, illustrating super-paramagnetic behavior.

Efficient evaluation of the Fourier transform over products of Slater-type orbitals on different centers

International Nuclear Information System (INIS)

Niehaus, T A; Lopez, R; Rico, J F

2008-01-01

Using the shift-operator technique, a compact formula for the Fourier transform of a product of two Slater-type orbitals located on different atomic centers is derived. The result is valid for arbitrary quantum numbers and was found to be numerically stable for a wide range of geometrical parameters and momenta. Details of the implementation are presented together with benchmark data for representative integrals. We also discuss the assets and drawbacks of alternative algorithms available and analyze the numerical efficiency of the new scheme

Computing exact Fourier series coefficients of IC rectilinear polygons from low-resolution fast Fourier coefficients

Science.gov (United States)

Scheibler, Robin; Hurley, Paul

2012-03-01

We present a novel, accurate and fast algorithm to obtain Fourier series coefficients from an IC layer whose description consists of rectilinear polygons on a plane, and how to implement it using off-the-shelf hardware components. Based on properties of Fourier calculus, we derive a relationship between the Discrete Fourier Transforms of the sampled mask transmission function and its continuous Fourier series coefficients. The relationship leads to a straightforward algorithm for computing the continuous Fourier series coefficients where one samples the mask transmission function, compute its discrete Fourier transform and applies a frequency-dependent multiplicative factor. The algorithm is guaranteed to yield the exact continuous Fourier series coefficients for any sampling representing the mask function exactly. Computationally, this leads to significant saving by allowing to choose the maximal such pixel size and reducing the fast Fourier transform size by as much, without compromising accuracy. In addition, the continuous Fourier series is free from aliasing and follows closely the physical model of Fourier optics. We show that in some cases this can make a significant difference, especially in modern very low pitch technology nodes.

Use of Fourier transforms for asynoptic mapping: Applications to the Upper Atmosphere Research Satellite microwave limb sounder

Science.gov (United States)

Elson, Lee S.; Froidevaux, Lucien

1993-01-01

Fourier analysis has been applied to data obtained from limb viewing instruments on the Upper Atmosphere Research Satellite. A coordinate system rotation facilitates the efficient computation of Fourier transforms in the temporal and longitudinal domains. Fields such as ozone (O3), chlorine monoxide (ClO), temperature, and water vapor have been transformed by this process. The transforms have been inverted to provide maps of these quantities at selected times, providing a method of accurate time interpolation. Maps obtained by this process show evidence of both horizontal and vertical transport of important trace species such as O3 and ClO. An examination of the polar regions indicates that large-scale planetary variations are likely to play a significant role in transporting midstratospheric O3 into the polar regions. There is also evidence that downward transport occurs, providing a means of moving O3 into the polar vortex at lower altitudes. The transforms themselves show the structure and propagation characteristics of wave variations.

A Compact Microwave Microfluidic Sensor Using a Re-Entrant Cavity.

Science.gov (United States)

Hamzah, Hayder; Abduljabar, Ali; Lees, Jonathan; Porch, Adrian

2018-03-19

A miniaturized 2.4 GHz re-entrant cavity has been designed, manufactured and tested as a sensor for microfluidic compositional analysis. It has been fully evaluated experimentally with water and common solvents, namely methanol, ethanol, and chloroform, with excellent agreement with the expected behaviour predicted by the Debye model. The sensor's performance has also been assessed for analysis of segmented flow using water and oil. The samples' interaction with the electric field in the gap region has been maximized by aligning the sample tube parallel to the electric field in this region, and the small width of the gap (typically 1 mm) result in a highly localised complex permittivity measurement. The re-entrant cavity has simple mechanical geometry, small size, high quality factor, and due to the high concentration of electric field in the gap region, a very small mode volume. These factors combine to result in a highly sensitive, compact sensor for both pure liquids and liquid mixtures in capillary or microfluidic environments.

[Cosmic Microwave Background (CMB) Anisotropies

Science.gov (United States)

Silk, Joseph

1998-01-01

One of the main areas of research is the theory of cosmic microwave background (CMB) anisotropies and analysis of CMB data. Using the four year COBE data we were able to improve existing constraints on global shear and vorticity. We found that, in the flat case (which allows for greatest anisotropy), (omega/H)0 less than 10(exp -7), where omega is the vorticity and H is the Hubble constant. This is two orders of magnitude lower than the tightest, previous constraint. We have defined a new set of statistics which quantify the amount of non-Gaussianity in small field cosmic microwave background maps. By looking at the distribution of power around rings in Fourier space, and at the correlations between adjacent rings, one can identify non-Gaussian features which are masked by large scale Gaussian fluctuations. This may be particularly useful for identifying unresolved localized sources and line-like discontinuities. Levin and collaborators devised a method to determine the global geometry of the universe through observations of patterns in the hot and cold spots of the CMB. We have derived properties of the peaks (maxima) of the CMB anisotropies expected in flat and open CDM models. We represent results for angular resolutions ranging from 5 arcmin to 20 arcmin (antenna FWHM), scales that are relevant for the MAP and COBRA/SAMBA space missions and the ground-based interferometer. Results related to galaxy formation and evolution are also discussed.

Microwave-assisted combustion synthesis of NiAl intermetallics in a single mode applicator: Modeling and optimisation

International Nuclear Information System (INIS)

Poli, G.; Sola, R.; Veronesi, P.

2006-01-01

The microwave-assisted combustion synthesis of NiAl intermetallics in a single mode applicator has been simulated numerically and performed with the aim of achieving the highest yields, energy efficiency and process reproducibility. The electromagnetic field modeling of the microwave system allowed to chose the proper experimental set-up and the materials more suitable for the application, minimising the reflected power and the risks of arcing. In all the experimental conditions tested, conversions of 3-5 g 1:1 atomic ratio Ni and Al powder compacts into NiAl ranged from 98.7% to 100%, requiring from 30 to 180 s with power from 500 to 1500 W. The optimisation procedure allowed to determine and quantify the effects of the main process variables on the ignition time, the NiAl yields and the specific energy consumption, leading to a fast, reproducible and cost-effective process of microwave-assisted combustion synthesis of NiAl intermetallics

Fractional finite Fourier transform.

Science.gov (United States)

Khare, Kedar; George, Nicholas

2004-07-01

We show that a fractional version of the finite Fourier transform may be defined by using prolate spheroidal wave functions of order zero. The transform is linear and additive in its index and asymptotically goes over to Namias's definition of the fractional Fourier transform. As a special case of this definition, it is shown that the finite Fourier transform may be inverted by using information over a finite range of frequencies in Fourier space, the inversion being sensitive to noise. Numerical illustrations for both forward (fractional) and inverse finite transforms are provided.

Fourier series, Fourier transform and their applications to mathematical physics

CERN Document Server

Serov, Valery

2017-01-01

This text serves as an introduction to the modern theory of analysis and differential equations with applications in mathematical physics and engineering sciences.  Having outgrown from a series of half-semester courses given at University of Oulu, this book consists of four self-contained parts. The first part, Fourier Series and the Discrete Fourier Transform, is devoted to the classical one-dimensional trigonometric Fourier series with some applications to PDEs and signal processing.  The second part, Fourier Transform and Distributions, is concerned with distribution theory of L. Schwartz and its applications to the Schrödinger and magnetic Schrödinger operations.  The third part, Operator Theory and Integral Equations, is devoted mostly to the self-adjoint but unbounded operators in Hilbert spaces and their applications to integral equations in such spaces. The fourth and final part, Introduction to Partial Differential Equations, serves as an introduction to modern methods for classical theory o...

A compact high-gradient 25 MeV 17 GHz RF linac for free-electron laser research

International Nuclear Information System (INIS)

Danly, B.G.; Chen, S.C.; Kreischer, K.E.

1995-01-01

A new compact high-gradient (60 MeV/m) high-frequency (17.136 GHz) RF linac is presently under construction by Haimson Research Corp. (HRC) for installation at the MIT Plasma Fusion Center in the High-Gradient Accelerator and High Power Microwave Laboratory. This accelerator will utilize an existing traveling-wave relativistic klystron (TWRK) which is now operation at MIT with 25 MW power, 67 dB gain, and 52% efficiency at 17.136 GHz

Microwave Ovens

Science.gov (United States)

... Products and Procedures Home, Business, and Entertainment Products Microwave Ovens Share Tweet Linkedin Pin it More sharing ... 1030.10 - Microwave Ovens Required Reports for the Microwave Oven Manufacturers or Industry Exemption from Certain Reporting ...

Microwave-assisted rapid extracellular synthesis of stable bio-functionalized silver nanoparticles from guava ( Psidium guajava) leaf extract

Science.gov (United States)

Raghunandan, Deshpande; Mahesh, Bedre D.; Basavaraja, S.; Balaji, S. D.; Manjunath, S. Y.; Venkataraman, A.

2011-05-01

Our research interest centers on microwave-assisted rapid extracellular synthesis of bio-functionalized silver nanoparticles of 26 ± 5 nm from guava ( Psidium guajava) leaf extract with control over dimension and composition. The reaction occurs very rapidly as the formation of spherical nanoparticles almost completed within 90 s. The probable pathway of the biosynthesis is suggested. Appearance, crystalline nature, size and shape of nanoparticles are understood by UV-vis (UV-vis spectroscopy), FTIR (fourier transform infrared spectroscopy), XRD (X-ray diffraction), FESEM (field emission scanning electron microscopy) and TEM (transmission electron microscopy) techniques. Microwave-assisted route is selected for the synthesis of silver nanoparticles to carry out the reaction fast, suppress the enzymatic action and to keep the process environmentally clean and green.

Microwave-assisted rapid extracellular synthesis of stable bio-functionalized silver nanoparticles from guava (Psidium guajava) leaf extract

Energy Technology Data Exchange (ETDEWEB)

Raghunandan, Deshpande [H.K.E.S' s College of Pharmacy (India); Mahesh, Bedre D. [Gulbarga University, Materials Chemistry Laboratory, Department of Material Science (India); Basavaraja, S. [Jawaharlal Nehru Centre for Advanced Scientific Research, Veeco-India Nanotechnology Laboratory (India); Balaji, S. D. [Gulbarga University, Materials Chemistry Laboratory, Department of Material Science (India); Manjunath, S. Y. [Sri Krupa, Institute of Pharmaceutical Science (India); Venkataraman, A., E-mail: raman_chem@rediffmail.com [Gulbarga University, Materials Chemistry Laboratory, Department of Material Science (India)

2011-05-15

Our research interest centers on microwave-assisted rapid extracellular synthesis of bio-functionalized silver nanoparticles of 26 {+-} 5 nm from guava (Psidium guajava) leaf extract with control over dimension and composition. The reaction occurs very rapidly as the formation of spherical nanoparticles almost completed within 90 s. The probable pathway of the biosynthesis is suggested. Appearance, crystalline nature, size and shape of nanoparticles are understood by UV-vis (UV-vis spectroscopy), FTIR (fourier transform infrared spectroscopy), XRD (X-ray diffraction), FESEM (field emission scanning electron microscopy) and TEM (transmission electron microscopy) techniques. Microwave-assisted route is selected for the synthesis of silver nanoparticles to carry out the reaction fast, suppress the enzymatic action and to keep the process environmentally clean and green.

Microwave-assisted rapid extracellular synthesis of stable bio-functionalized silver nanoparticles from guava (Psidium guajava) leaf extract

International Nuclear Information System (INIS)

Raghunandan, Deshpande; Mahesh, Bedre D.; Basavaraja, S.; Balaji, S. D.; Manjunath, S. Y.; Venkataraman, A.

2011-01-01

Our research interest centers on microwave-assisted rapid extracellular synthesis of bio-functionalized silver nanoparticles of 26 ± 5 nm from guava (Psidium guajava) leaf extract with control over dimension and composition. The reaction occurs very rapidly as the formation of spherical nanoparticles almost completed within 90 s. The probable pathway of the biosynthesis is suggested. Appearance, crystalline nature, size and shape of nanoparticles are understood by UV–vis (UV–vis spectroscopy), FTIR (fourier transform infrared spectroscopy), XRD (X-ray diffraction), FESEM (field emission scanning electron microscopy) and TEM (transmission electron microscopy) techniques. Microwave-assisted route is selected for the synthesis of silver nanoparticles to carry out the reaction fast, suppress the enzymatic action and to keep the process environmentally clean and green.

Selective microwave sensors exploiting the interaction of analytes with trap states in TiO2 nanotube arrays

Science.gov (United States)

Zarifi, M. H.; Farsinezhad, S.; Abdolrazzaghi, M.; Daneshmand, M.; Shankar, K.

2016-03-01

Sensing of molecular analytes by probing the effects of their interaction with microwaves is emerging as a cheap, compact, label-free and highly sensitive detection and quantification technique. Microstrip ring-type resonators are particularly favored for this purpose due to their planar sensing geometry, electromagnetic field enhancements in the coupling gap and compatibility with established printed circuit board manufacturing. However, the lack of selectivity in what is essentially a permittivity-sensing method is an impediment to wider adoption and implementation of this sensing platform. By placing a polycrystalline anatase-phase TiO2 nanotube membrane in the coupling gap of a microwave resonator, we engineer selectivity for the detection and differentiation of methanol, ethanol and 2-propanol. The scavenging of reactive trapped holes by aliphatic alcohols adsorbed on TiO2 is responsible for the alcohol-specific detection while the different short chain alcohols are distinguished on the basis of differences in their microwave response. Electrodeless microwave sensors which allow spectral and time-dependent monitoring of the resonance frequency and quality factor provide a wealth of information in comparison with electrode-based resistive sensors for the detection of volatile organic compounds. A high dynamic range (400 ppm-10 000 ppm) is demonstrated for methanol detection.Sensing of molecular analytes by probing the effects of their interaction with microwaves is emerging as a cheap, compact, label-free and highly sensitive detection and quantification technique. Microstrip ring-type resonators are particularly favored for this purpose due to their planar sensing geometry, electromagnetic field enhancements in the coupling gap and compatibility with established printed circuit board manufacturing. However, the lack of selectivity in what is essentially a permittivity-sensing method is an impediment to wider adoption and implementation of this sensing platform

Microwave emission from flaring magnetic loops

International Nuclear Information System (INIS)

Vlahos, L.

1980-01-01

The microwave emission from a flaring loop is considered. In particular the author examines the question: What will be the characteristics of the radio emission at centimeter wavelengths from a small compact flaring loop when the mechanism which pumps magnetic energy into the plasma in the form of heating and/or electron acceleration satisfies the conditions: (a) the magnetic energy is released in a small volume compared to the volume of the loop, and the rate at which magnetic energy is transformed into plasma energy is faster than the energy losses from the same volume. This causes a local enhancement of the temperature by as much as one or two orders of magnitude above the coronal temperature; (b) The bulk of the energy released goes into heating the plasma and heats primarily the electrons. (Auth.)

Realization of Miniaturized Multi-/Wideband Microwave Front-Ends

Science.gov (United States)

Al Shamaileh, Khair A.

The ever-growing demand toward designing microwave front-end components with enhanced access to the radio spectrum (e.g., multi-/wideband functionality) and improved physical features (e.g., miniaturized circuitry, ease and cost of fabrication) is becoming more paramount than ever before. This dissertation proposes new design methodologies, simulations, and experimental validations of passive front-ends (i.e., antennas, couplers, dividers) at microwave frequencies. The presented design concepts optimize both electrical and physical characteristics without degrading the intended performance. The developed designs are essential to the upcoming wireless technologies. The first proposed component is a compact ultra-wideband (UWB) Wilkinson power divider (WPD). The design procedure is accomplished by replacing the uniform transmission lines in each arm of the conventional single-frequency divider with impedance-varying profiles governed by a truncated Fourier series. While such non-uniform transmission lines (NTLs) are obtained through the even-mode analysis, three isolation resistors are optimized in the odd-mode circuit to achieve proper isolation and output ports matching over the frequency range of interest. The proposed design methodology is systematic, and results in single-layered and compact structures. For verification purposes, an equal split WPD is designed, simulated, and measured. The obtained results show that the input and output ports matching as well as the isolation between the output ports are below --10 dB; whereas the transmission parameters vary between --3.2 dB and --5 dB across the 3.1--10.6 GHz band. The designed divider is expected to find applications in UWB antenna diversity, multiple-input-multiple-output (MIMO) schemes, and antenna arrays feeding networks. The second proposed component is a wideband multi-way Bagley power divider (BPD). Wideband functionality is achieved by replacing the single-frequency matching uniform microstrip lines in

Fourier band-power E/B-mode estimators for cosmic shear

Energy Technology Data Exchange (ETDEWEB)

Becker, Matthew R.; Rozo, Eduardo

2016-01-20

We introduce new Fourier band-power estimators for cosmic shear data analysis and E/B-mode separation. We consider both the case where one performs E/B-mode separation and the case where one does not. The resulting estimators have several nice properties which make them ideal for cosmic shear data analysis. First, they can be written as linear combinations of the binned cosmic shear correlation functions. Secondly, they account for the survey window function in real-space. Thirdly, they are unbiased by shape noise since they do not use correlation function data at zero separation. Fourthly, the band-power window functions in Fourier space are compact and largely non-oscillatory. Fifthly, they can be used to construct band-power estimators with very efficient data compression properties. In particular, we find that all of the information on the parameters Ωm, σ8 and ns in the shear correlation functions in the range of ~10–400 arcmin for single tomographic bin can be compressed into only three band-power estimates. Finally, we can achieve these rates of data compression while excluding small-scale information where the modelling of the shear correlation functions and power spectra is very difficult. Given these desirable properties, these estimators will be very useful for cosmic shear data analysis.

Analysis of laboratory compaction methods of roller compacted concrete

Science.gov (United States)

Trtík, Tomáš; Chylík, Roman; Bílý, Petr; Fládr, Josef

2017-09-01

Roller-Compacted Concrete (RCC) is an ordinary concrete poured and compacted with machines typically used for laying of asphalt road layers. One of the problems connected with this technology is preparation of representative samples in the laboratory. The aim of this work was to analyse two methods of preparation of RCC laboratory samples with bulk density as the comparative parameter. The first method used dynamic compaction by pneumatic hammer. The second method of compaction had a static character. The specimens were loaded by precisely defined force in laboratory loading machine to create the same conditions as during static rolling (in the Czech Republic, only static rolling is commonly used). Bulk densities obtained by the two compaction methods were compared with core drills extracted from real RCC structure. The results have shown that the samples produced by pneumatic hammer tend to overestimate the bulk density of the material. For both compaction methods, immediate bearing index test was performed to verify the quality of compaction. A fundamental difference between static and dynamic compaction was identified. In static compaction, initial resistance to penetration of the mandrel was higher, after exceeding certain limit the resistance was constant. This means that the samples were well compacted just on the surface. Specimens made by pneumatic hammer actively resisted throughout the test, the whole volume was uniformly compacted.

Microwave spectra and molecular structures of (Z)-pent-2-en-4-ynenitrile and maleonitrile.

Science.gov (United States)

Halter, R J; Fimmen, R L; McMahon, R J; Peebles, S A; Kuczkowski, R L; Stanton, J F

2001-12-12

Accurate equilibrium structures have been determined for (Z)-pent-2-en-4-ynenitrile (8) and maleonitrile (9) by combining microwave spectroscopy data and ab initio quantum chemistry calculations. The microwave spectra of 10 isotopomers of 8 and 5 isotopomers of 9 were obtained using a pulsed nozzle Fourier transform microwave spectrometer. The ground-state rotational constants were adjusted for vibration-rotation interaction effects calculated from force fields obtained from ab initio calculations. The resultant equilibrium rotational constants were used to determine structures that are in very good agreement with those obtained from high-level ab initio calculations (CCSD(T)/cc-pVTZ). The geometric parameters in 8 and 9 are very similar; they also do not differ significantly from the all-carbon analogue, (Z)-hex-3-ene-1,5-diyne (7), the parent molecule for the Bergman cyclization. A small deviation from linearity about the alkyne and cyano linkages is observed for 7-9 and several related species where accurate equilibrium parameters are available. The data on 7-9 should be of interest to radioastronomy and may provide insights on the formation and interstellar chemistry of unsaturated species such as the cyanopolyynes.

A Compact Microwave Microfluidic Sensor Using a Re-Entrant Cavity

Directory of Open Access Journals (Sweden)

Hayder Hamzah

2018-03-01

Full Text Available A miniaturized 2.4 GHz re-entrant cavity has been designed, manufactured and tested as a sensor for microfluidic compositional analysis. It has been fully evaluated experimentally with water and common solvents, namely methanol, ethanol, and chloroform, with excellent agreement with the expected behaviour predicted by the Debye model. The sensor’s performance has also been assessed for analysis of segmented flow using water and oil. The samples’ interaction with the electric field in the gap region has been maximized by aligning the sample tube parallel to the electric field in this region, and the small width of the gap (typically 1 mm result in a highly localised complex permittivity measurement. The re-entrant cavity has simple mechanical geometry, small size, high quality factor, and due to the high concentration of electric field in the gap region, a very small mode volume. These factors combine to result in a highly sensitive, compact sensor for both pure liquids and liquid mixtures in capillary or microfluidic environments.

Microwave measurements of the spectra and molecular structure for phthalic anhydride

Science.gov (United States)

Pejlovas, Aaron M.; Sun, Ming; Kukolich, Stephen G.

2014-05-01

The microwave rotational spectrum for phthalic anhydride (PhA) has been measured in the 4-14 GHz microwave region using a pulsed-beam Fourier transform (PBFT) Flygare-Balle type microwave spectrometer. Initially, the molecular structure was calculated using Gaussian 09 suite with mp2/6-311++G** basis and the calculations were used in predicting spectra for the measured isotopologues. The experimental rotational transition frequencies were measured and used to calculate the rotational and centrifugal distortion constants. The rotational constants for the normal isotopologue, four unique 13C substituted isotopologues and two 18O isotologues, were used in a least squares fit to determine nearly all structural parameters for this molecule. Since no substitutions were made at hydrogen sites, the calculated positions of the hydrogen atoms relative to the bonded carbon atoms were used in the structure determination. The rotational constants for the parent isotopologue were determined to be A = 1801.7622(9) MHz, B = 1191.71816(26) MHz, C = 717.44614(28) MHz. Small values for the centrifugal distortion constants were obtained; DJ = 0.0127 kHz, DJK = 0.0652 kHz, and DK = -0.099 kHz, indicating a fairly rigid structure. The structure of PhA is planar with a negative inertial defect of Δ = -0.154 amu Å2. Structural parameters from the mp2 and DFT calculations are in quite good agreement with measured parameters.

Microwave assisted synthesis and characterization of magnesium substituted calcium phosphate bioceramics

Energy Technology Data Exchange (ETDEWEB)

Khan, Nida Iqbal [Interdisciplinary Research Centre in Biomedical Materials, COMSATS Institute of Information Technology, M. A. Jinnah Campus, Defence Road, Off Raiwind Road, Lahore (Pakistan); Medical Implant Technology Group (MEDITEG), Faculty of Bioscience and Medical Engineering, Universiti Teknologi Malaysia, 81310 Skudai, Johor Darul Takzim (Malaysia); Ijaz, Kashif; Zahid, Muniza; Khan, Abdul S. [Interdisciplinary Research Centre in Biomedical Materials, COMSATS Institute of Information Technology, M. A. Jinnah Campus, Defence Road, Off Raiwind Road, Lahore (Pakistan); Abdul Kadir, Mohammed Rafiq [Medical Implant Technology Group (MEDITEG), Faculty of Bioscience and Medical Engineering, Universiti Teknologi Malaysia, 81310 Skudai, Johor Darul Takzim (Malaysia); Hussain, Rafaqat [Department of Chemistry, Faculty of Science, Universiti Teknologi Malaysia, Skudai, Johore (Malaysia); Anis-ur-Rehman [Department of Physics, COMSATS Institute of Information Technology, Chakshahzad Campus, Islamabad (Pakistan); Darr, Jawwad A. [Clean Materials Technology Group, Department of Chemistry, University College London, Christopher Ingold Laboratories, 20 Gordon Street, London WC1H 0AJ (United Kingdom); Ihtesham-ur-Rehman [The Kroto Research Institute, North Campus, University of Sheffield, Broad Lane, Sheffield S3 7HQ (United Kingdom); Chaudhry, Aqif A., E-mail: aqifanwar@ciitlahore.edu.pk [Interdisciplinary Research Centre in Biomedical Materials, COMSATS Institute of Information Technology, M. A. Jinnah Campus, Defence Road, Off Raiwind Road, Lahore (Pakistan)

2015-11-01

Hydroxyapatite is used extensively in hard tissue repair due to its biocompatibility and similarity to biological apatite, the mineral component of bone. It differs subtly in composition from biological apatite which contains other ions such as magnesium, zinc, carbonate and silicon (believed to play biological roles). Traditional methods of hydroxyapatite synthesis are time consuming and require strict reaction parameter control. This paper outlines synthesis of magnesium substituted hydroxyapatite using simple microwave irradiation of precipitated suspensions. Microwave irradiation resulted in a drastic decrease in ageing times of amorphous apatitic phases. Time taken to synthesize hydroxyapatite (which remained stable upon heat treatment at 900 °C for 1 h) reduced twelve folds (to 2 h) as compared to traditionally required times. The effects of increasing magnesium concentration in the precursors on particle size, surface area, phase-purity, agglomeration and thermal stability, were observed using scanning electron microscopy, BET surface area analysis, X-ray diffraction and photo acoustic Fourier transform infra-red spectroscopy. Porous agglomerates were obtained after a brief heat-treatment (1 h) at 900 °C. - Highlights: • Microwave irradiation of suspensions of calcium phosphates accelerated maturation. • Reactions took 2 h to complete as compared to 18 h required traditionally. • Magnesium contents higher than 1 wt.% lead to the presence of non-apatitic phases. • Agglomerates with micron and sub-micron porosity were obtained after heat-treatment.

Microwave-assisted synthesis of iron oxide nanoparticles in biocompatible organic environment

Directory of Open Access Journals (Sweden)

E. Aivazoglou

2018-04-01

Full Text Available The development of magnetite and maghemite particles in uniform nanometer size has triggered the interest of the research community due to their many interesting properties leading to a wide range of applications, such as catalysis, nanomedicine-nanobiology and other engineering applications. In this study, a simple, time-saving and low energy-consuming, microwave-assisted synthesis of iron oxide nanoparticles, is presented. The nanoparticles were prepared by microwave-assisted synthesis using polyethylene glycol (PEG or PEG and β-cyclodextrin (β-CD/water solutions of chloride salts of iron in the presence of ammonia solution. The prepared nano-powders were characterized using X-Ray Diffraction (XRD, Transition Electron Microscopy (TEM, Fourier-transform Infrared Spectroscopy (FTIR, Raman Spectroscopy, Vibrating Sample Magnetometer (VSM, X-Ray Photoelectron Spectroscopy (XPS and Thermal analysis (TG/DSC. The produced nanoparticles are crystallized mostly in the magnetite and maghemite lattice exhibiting very similar shape and size, with indications of partial PEG coating. Heating time, microwave power and presence of PEG, are the key factors shaping the size properties of nanoparticles. The average size of particles ranges from 10.3 to 19.2 nm. The nanoparticles exhibit a faceted morphology, with zero contamination levels. The magnetic measurements indicate that the powders are soft magnetic materials with negligible coercivity and remanence, illustrating super-paramagnetic behavior.

Microwave-assisted hydrothermal synthesis of biocompatible silver sulfide nanoworms

Science.gov (United States)

Xing, Ruimin; Liu, Shanhu; Tian, Shufang

2011-10-01

In this study, silver sulfide nanoworms were prepared via a rapid microwave-assisted hydrothermal method by reacting silver nitrate and thioacetamide in the aqueous solution of the Bovine Serum Albumin (BSA) protein. The morphology, composition, and crystallinity of the nanoworms were characterized by field emission scanning electron microscopy (FESEM), X-ray powder diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED), X-ray energy dispersive spectroscopy (EDS), and Fourier transform infrared (FTIR) spectroscopy. The results show that the nanoworms were assembled by multiple adjacent Ag2S nanoparticles and stabilized by a layer of BSA attached to their surface. The nanoworms have the sizes of about 50 nm in diameter and hundreds of nanometers in length. The analyses of high-resolution TEM and their correlative Fast Fourier Transform (FFT) indicate that the adjacent Ag2S nanoparticles grow by misoriented attachment at the connective interfaces to form the nanoworm structure. In vitro assays on the human cervical cancer cell line HeLa show that the nanoworms exhibit good biocompatibility due to the presence of BSA coating. This combination of features makes the nanoworms attractive and promising building blocks for advanced materials and devices.

Microwave energy transmission

Energy Technology Data Exchange (ETDEWEB)

Matsumoto, Hiroshi [Kyoto Univ. (Japan)

1989-03-05

Laying stress on the technological problems and effect on the environment of microwave energy transmission, recent scientific and engineering problems and related subjects are described. Because no fuel is required for the solar power generation, the power generation system can not be considered as an expensive one when the unit cost of energy is taken into consideration. Some of the important technological problems in the microwave energy transmission are accurate microwave beam control technology to receiving stations and improvement in the efficiency of transmission system. Microwave energy beam has effects on living bodies, communication, and plasma atmosphere of the earth. Microwave energy transmission using a space flyer unit is scheduled. Its objective is the development of microwave wireless transmission technology and the study of the correlation between high power microwave and ionosphere plasma. Experiments on such a small scale application as a microwave driven space ship to bring results seem also important. 12 refs., 13 figs.

Biopolymers Regulate Silver Nanoparticle under Microwave Irradiation for Effective Antibacterial and Antibiofilm Activities.

Directory of Open Access Journals (Sweden)

Palaniyandi Velusamy

Full Text Available In the current study, facile synthesis of carboxymethyl cellulose (CMC and sodium alginate capped silver nanoparticles (AgNPs was examined using microwave radiation and aniline as a reducing agent. The biopolymer matrix embedded nanoparticles were synthesized under various experimental conditions using different concentrations of biopolymer (0.5, 1, 1.5, 2%, volumes of reducing agent (50, 100, 150 μL, and duration of heat treatment (30 s to 240 s. The synthesized nanoparticles were analyzed by scanning electron microscopy, UV-Vis spectroscopy, X-ray diffraction, and Fourier transform infrared spectroscopy for identification of AgNPs synthesis, crystal nature, shape, size, and type of capping action. In addition, the significant antibacterial efficacy and antibiofilm activity of biopolymer capped AgNPs were demonstrated against different bacterial strains, Staphylococcus aureus MTCC 740 and Escherichia coli MTCC 9492. These results confirmed the potential for production of biopolymer capped AgNPs grown under microwave irradiation, which can be used for industrial and biomedical applications.

Review on Microwave-Matter Interaction Fundamentals and Efficient Microwave-Associated Heating Strategies

Science.gov (United States)

Sun, Jing; Wang, Wenlong; Yue, Qinyan

2016-01-01

Microwave heating is rapidly emerging as an effective and efficient tool in various technological and scientific fields. A comprehensive understanding of the fundamentals of microwave–matter interactions is the precondition for better utilization of microwave technology. However, microwave heating is usually only known as dielectric heating, and the contribution of the magnetic field component of microwaves is often ignored, which, in fact, contributes greatly to microwave heating of some aqueous electrolyte solutions, magnetic dielectric materials and certain conductive powder materials, etc. This paper focuses on this point and presents a careful review of microwave heating mechanisms in a comprehensive manner. Moreover, in addition to the acknowledged conventional microwave heating mechanisms, the special interaction mechanisms between microwave and metal-based materials are attracting increasing interest for a variety of metallurgical, plasma and discharge applications, and therefore are reviewed particularly regarding the aspects of the reflection, heating and discharge effects. Finally, several distinct strategies to improve microwave energy utilization efficiencies are proposed and discussed with the aim of tackling the energy-efficiency-related issues arising from the application of microwave heating. This work can present a strategic guideline for the developed understanding and utilization of the microwave heating technology. PMID:28773355

The torsional barriers of two equivalent methyl internal rotations in 2,5-dimethylfuran investigated by microwave spectroscopy

Science.gov (United States)

Van, Vinh; Bruckhuisen, Jonas; Stahl, Wolfgang; Ilyushin, Vadim; Nguyen, Ha Vinh Lam

2018-01-01

The microwave spectrum of 2,5-dimethylfuran was recorded using two pulsed molecular jet Fourier transform microwave spectrometers which cover the frequency range from 2 to 40 GHz. The internal rotations of two equivalent methyl tops with a barrier height of approximately 439.15 cm-1 introduce torsional splittings of all rotational transitions in the spectrum. For the spectral analysis, two different computer programs were applied and compared, the PAM-C2v-2tops code based on the principal axis method which treats several torsional states simultaneously, and the XIAM code based on the combined axis method, yielding accurate molecular parameters. The experimental work was supplemented by quantum chemical calculations. Two-dimensional potential energy surfaces depending on the torsional angles of both methyl groups were calculated and parametrized.

Contribution to the microwave characterisation of superconductive materials by means of sapphire resonators

International Nuclear Information System (INIS)

Hanus, Xavier

1993-01-01

The objective of this research thesis is to find a compact resonant structure which would allow the residual surface impedance of superconductive samples to be simply, quickly and economically characterised. The author first explains why he decided to use a sapphire single-crystal as inner dielectric, given some performance reached by resonant structures equipped with such inner dielectrics, and given constraints adopted from the start. He explains the origin of microwave losses which appear in this type of resonant structure, i.e. respectively the surface impedance as far as metallic losses are concerned, and the sapphire dielectric loss angle for as far as dielectric losses are concerned. The experimental installation and the principle of microwave measurements are described. The performance of different possible solutions of resonant structures from starting criteria is presented. The solution of the cavity-sapphire with a TE 011 resonant mode is derived [fr

Effect of microwave treatment on structure of binders based on sodium carboxymethyl starch: FT-IR, FT-Raman and XRD investigations.

Science.gov (United States)

Kaczmarska, Karolina; Grabowska, Beata; Spychaj, Tadeusz; Zdanowicz, Magdalena; Sitarz, Maciej; Bobrowski, Artur; Cukrowicz, Sylwia

2018-06-15

The paper deals with the influence of the microwave treatment on sodium carboxymethyl starch (CMS-Na) applied as a binder for moulding sands. The Fourier transformation infrared spectrometry (FT-IR), Raman spectroscopy (FT-Raman) and XRD analysis data of native potato starch and three different carboxymethyl starches (CMS-Na) with various degree of substitution (DS) before and after exposition to microwave radiation have been compared. FT-IR studies showed that polar groups present in CMS-Na structure take part in the formation of new hydrogen bonds network after water evaporation. However, these changes depend on DS value of the modified starch. The FT-Raman study confirmed that due to the impact on the samples by microwave, the changes of intensity in the characteristic bands associated with the crystalline regions in the sample were noticed. The X-ray diffraction data for microwave treated CMS-Na samples have been compared with the diffractograms of initial materials and analysis of XRD patterns confirmed that microwave-treated samples exhibit completely amorphous structure. Analysis of structural changes allows to state that the binding of sand grains in moulding sand with CMS-Na polymeric binder consists in the formation of hydrogen bonds networks (physical cross-linking). Copyright © 2018 Elsevier B.V. All rights reserved.

Effect of microwave treatment on structure of binders based on sodium carboxymethyl starch: FT-IR, FT-Raman and XRD investigations

Science.gov (United States)

Kaczmarska, Karolina; Grabowska, Beata; Spychaj, Tadeusz; Zdanowicz, Magdalena; Sitarz, Maciej; Bobrowski, Artur; Cukrowicz, Sylwia

2018-06-01

The paper deals with the influence of the microwave treatment on sodium carboxymethyl starch (CMS-Na) applied as a binder for moulding sands. The Fourier transformation infrared spectrometry (FT-IR), Raman spectroscopy (FT-Raman) and XRD analysis data of native potato starch and three different carboxymethyl starches (CMS-Na) with various degree of substitution (DS) before and after exposition to microwave radiation have been compared. FT-IR studies showed that polar groups present in CMS-Na structure take part in the formation of new hydrogen bonds network after water evaporation. However, these changes depend on DS value of the modified starch. The FT-Raman study confirmed that due to the impact on the samples by microwave, the changes of intensity in the characteristic bands associated with the crystalline regions in the sample were noticed. The X-ray diffraction data for microwave treated CMS-Na samples have been compared with the diffractograms of initial materials and analysis of XRD patterns confirmed that microwave-treated samples exhibit completely amorphous structure. Analysis of structural changes allows to state that the binding of sand grains in moulding sand with CMS-Na polymeric binder consists in the formation of hydrogen bonds networks (physical cross-linking).

The rotational spectrum of CuCCH(X̃  1Σ+): a Fourier transform microwave discharge assisted laser ablation spectroscopy and millimeter/submillimeter study.

Science.gov (United States)

Sun, M; Halfen, D T; Min, J; Harris, B; Clouthier, D J; Ziurys, L M

2010-11-07

The pure rotational spectrum of CuCCH in its ground electronic state (X̃  (1)Σ(+)) has been measured in the frequency range of 7-305 GHz using Fourier transform microwave (FTMW) and direct absorption millimeter/submillimeter methods. This work is the first spectroscopic study of CuCCH, a model system for copper acetylides. The molecule was synthesized using a new technique, discharge assisted laser ablation spectroscopy (DALAS). Four to five rotational transitions were measured for this species in six isotopologues ((63)CuCCH, (65)CuCCH, (63)Cu(13)CCH, (63)CuC(13)CH, (63)Cu(13)C(13)CH, and (63)CuCCD); hyperfine interactions arising from the copper nucleus were resolved, as well as smaller splittings in CuCCD due to deuterium quadrupole coupling. Five rotational transitions were also recorded in the millimeter region for (63)CuCCH and (65)CuCCH, using a Broida oven source. The combined FTMW and millimeter spectra were analyzed with an effective Hamiltonian, and rotational, electric quadrupole (Cu and D) and copper nuclear spin-rotation constants were determined. From the rotational constants, an r(m)(2) structure for CuCCH was established, with r(Cu-C) = 1.8177(6) Å, r(C-C) = 1.2174(6) Å, and r(C-H) = 1.046(2) Å. The geometry suggests that CuCCH is primarily a covalent species with the copper atom singly bonded to the C≡C-H moiety. The copper quadrupole constant indicates that the bonding orbital of this atom may be sp hybridized. The DALAS technique promises to be fruitful in the study of other small, metal-containing molecules of chemical interest.

Characterization of Orthorhombic α-MoO3 Microplates Produced by a Microwave Plasma Process

International Nuclear Information System (INIS)

Klinbumrung, A.; Thongtem, S.; Thongtem, T.; Thongtem, S.; Thongtem, T.

2012-01-01

Orthorhombic α-MoO 3 microplates were produced from (NH 4 ) 6 Mo 7 O 24 H 2 O solid powder by a 900 W microwave plasma for 40, 50, and 60?min. Phase, morphologies, and vibration modes were characterized by X-ray diffraction (XRD), selected area electron diffraction (SAED), scanning electron microscopy (SEM), and Raman and Fourier transform infrared (FTIR) spectroscopy. Sixty min processing resulted in the best crystallization of the α-MoO 3 phase, with photoluminescence (PL) in a wavelength range of 430-440 nm.

Proposal of AAA-battery-size one-shot ATR Fourier spectroscopic imager for on-site analysis: Simultaneous measurement of multi-components with high accuracy

Science.gov (United States)

Hosono, Satsuki; Qi, Wei; Sato, Shun; Suzuki, Yo; Fujiwara, Masaru; Hiramatsu, Hiroyuki; Suzuki, Satoru; Abeygunawardhana, P. K. W.; Wada, Kenji; Nishiyama, Akira; Ishimaru, Ichiro

2015-03-01

For simultaneous measurement of multi-components on-site like factories, the ultra-compact (diameter: 9[mm], length: 45[mm], weight: 200[g]) one-shot ATR (Attenuated Total Reflection) Fourier spectroscopic imager was proposed. Because the proposed one-shot Fourier spectroscopic imaging is based on spatial-phase-shift interferometer, interferograms could be obtained with simple optical configurations. We introduced the transmission-type relativeinclined phase-shifter, that was constructed with a cuboid prism and a wedge prism, onto the optical Fourier transform plane of infinity corrected optical systems. And also, small light-sources and cameras in the mid-infrared light region, whose size are several millimeter on a side, are essential components for the ultra-compact spectroscopic configuration. We selected the Graphite light source (light source area: 1.7×1.7[mm], maker: Hawkeye technologies) whose radiation factor was high. Fortunately, in these days we could apply the cost-effective 2-dimensional light receiving device for smartphone (e.g. product name: LEPTON, maker: FLIR, price: around 400USD). In the case of alcoholic drinks factory, conventionally workers measure glucose and ethanol concentrations by bringing liquid solution back to laboratories every day. The high portable spectroscopy will make it possible to measure multi-components simultaneously on manufacturing scene. But we found experimentally that absorption spectrum of glucose and water and ethanol were overlapped each other in near infrared light region. But for mid-infrared light region, we could distinguish specific absorption peaks of glucose (@10.5[μm]) and ethanol (@11.5[μm]) independently from water absorption. We obtained standard curve between absorption (@9.6[μm]) and ethanol concentration with high correlation coefficient 0.98 successfully by ATR imaging-type 2-dimensional Fourier spectroscopy (wavelength resolution: 0.057[μm]) with the graphite light source (maker: Hawkeye

Fourier transforms principles and applications

CERN Document Server

Hansen, Eric W

2014-01-01

Fourier Transforms: Principles and Applications explains transform methods and their applications to electrical systems from circuits, antennas, and signal processors-ably guiding readers from vector space concepts through the Discrete Fourier Transform (DFT), Fourier series, and Fourier transform to other related transform methods.  Featuring chapter end summaries of key results, over two hundred examples and four hundred homework problems, and a Solutions Manual this book is perfect for graduate students in signal processing and communications as well as practicing engineers.

Fast microwave assisted pyrolysis of biomass using microwave absorbent.

Science.gov (United States)

Borges, Fernanda Cabral; Du, Zhenyi; Xie, Qinglong; Trierweiler, Jorge Otávio; Cheng, Yanling; Wan, Yiqin; Liu, Yuhuan; Zhu, Rongbi; Lin, Xiangyang; Chen, Paul; Ruan, Roger

2014-03-01

A novel concept of fast microwave assisted pyrolysis (fMAP) in the presence of microwave absorbents was presented and examined. Wood sawdust and corn stover were pyrolyzed by means of microwave heating and silicon carbide (SiC) as microwave absorbent. The bio-oil was characterized, and the effects of temperature, feedstock loading, particle sizes, and vacuum degree were analyzed. For wood sawdust, a temperature of 480°C, 50 grit SiC, with 2g/min of biomass feeding, were the optimal conditions, with a maximum bio-oil yield of 65 wt.%. For corn stover, temperatures ranging from 490°C to 560°C, biomass particle sizes from 0.9mm to 1.9mm, and vacuum degree lower than 100mmHg obtained a maximum bio-oil yield of 64 wt.%. This study shows that the use of microwave absorbents for fMAP is feasible and a promising technology to improve the practical values and commercial application outlook of microwave based pyrolysis. Copyright © 2014 Elsevier Ltd. All rights reserved.

Design of a Microwave Duplexer without Ferrite and without Magnet

Directory of Open Access Journals (Sweden)

F. Mejri

2018-06-01

Full Text Available In this paper we present the design, realization and characterization of a microwave duplexer, compact, easy to realize and integrate into systems such as ground penetrating radars. It is made without the use of ferrite or magnet. This device is designed in the S band and made in micro-ribbon technology. It consists of a power divider and two RF amplifiers, low gain, using a BFR91 bipolar transistor. The latter is frequently available and inexpensive. Measurements made on a vector network analyzer have shown a low insertion loss with insulation considered satisfactory – for low power applications - between the transmitter (Tx and the receiver (Rx circuits.

Direct fourier method reconstruction based on unequally spaced fast fourier transform

International Nuclear Information System (INIS)

Wu Xiaofeng; Zhao Ming; Liu Li

2003-01-01

First, We give an Unequally Spaced Fast Fourier Transform (USFFT) method, which is more exact and theoretically more comprehensible than its former counterpart. Then, with an interesting interpolation scheme, we discusse how to apply USFFT to Direct Fourier Method (DFM) reconstruction of parallel projection data. At last, an emulation experiment result is given. (authors)

SnO{sub 2}{sup *}CoO ceramic obtained by microwave sintering; Ceramicas de SnO{sub 2} {sup *}CoO obtidas por sinterizacao microondas

Energy Technology Data Exchange (ETDEWEB)

Bordignon, M.A.N; Moura, F.; Zaghete, M.A.; Varela, J.A.; Perazolli, L. [Universidade Estadual Paulista (UNESP), Araraquara, SP (Brazil). Chemistry Institute. Dept. de Biochemistry and Technological Chemistryl

2009-07-01

This work consists in the sintering study of CoO doped SnO{sub 2} using microwave sintering oven and silicon carbide as a susceptor. The powders were obtained by dry oxides mixture and conformed in cylindrical shapes with 6mmx8mm and green density to 60%. Then the compacts were sintering up to 1.050 deg C, using heating rate of 50 deg C/min and isotherm up to 30min. The densities obtained were above 95% for both techniques. It was observed that occurred a temperature reducing of 400 deg C and time reducing of 210min to obtain the same densities, when was used the microwave oven without the phenomena of thermal runaway. So the sintered compacts were accomplished using DRX and SEM. It was made the electrical characterization (current x voltage) and it was found to have great potential in the production of dense ceramic-based SnO{sub 2} with low resistivity to obtain electro-ceramic devices. (author)

Synthesis of magnetite nanoparticles by microwave irradiation and characterization

International Nuclear Information System (INIS)

Holland, Helber; Yamaura, Mitiko

2009-01-01

Nanometer-scale magnetic particles have been research target because of their peculiar magnetic properties as observed in magnetite nanoparticles. These nanoparticles exhibit superparamagnetic characteristics with potential applications in biomedical, environmental, and engineering fields. In this work, magnetite nanoparticles from Fe 2+ ions were obtained from two different processes, by precipitation and heating in a boiling water bath and by precipitation and heating in a domestic microwave oven. Influence of heating time of both systems for obtaining of magnetite particles was investigated. The characterization of the products was done by Scanning Electron Microscopy to determine the morphology, X-ray Diffractometry to estimate the crystal structure and the size of crystallite and Fourier Transform Infrared Spectroscopy to show the principal bands of absorption. (author)

On the Fourier integral theorem

NARCIS (Netherlands)

Koekoek, J.

1987-01-01

Introduction. In traditional proofs of convergence of Fourier series and of the Fourier integraI theorem basic tools are the theory of Dirichlet integraIs and the Riemann-Lebesgue lemma. Recently CHERNOFF [I) and REoIlEFFER (2) gave new proofs of convergenceof Fourier series which make no use of the

Design of a microwave calorimeter for the microwave tokamak experiment

International Nuclear Information System (INIS)

Marinak, M.

1988-01-01

The initial design of a microwave calorimeter for the Microwave Tokamak Experiment is presented. The design is optimized to measure the refraction and absorption of millimeter rf microwaves as they traverse the toroidal plasma of the Alcator C tokamak. Techniques utilized can be adapted for use in measuring high intensity pulsed output from a microwave device in an environment of ultra high vacuum, intense fields of ionizing and non-ionizing radiation and intense magnetic fields. 16 refs

Microwave power engineering applications

CERN Document Server

Okress, Ernest C

2013-01-01

Microwave Power Engineering, Volume 2: Applications introduces the electronics technology of microwave power and its applications. This technology emphasizes microwave electronics for direct power utilization and transmission purposes. This volume presents the accomplishments with respect to components, systems, and applications and their prevailing limitations in the light of knowledge of the microwave power technology. The applications discussed include the microwave heating and other processes of materials, which utilize the magnetron predominantly. Other applications include microwave ioni

Advances in microwaves 8

CERN Document Server

Young, Leo

2013-01-01

Advances in Microwaves, Volume 8 covers the developments in the study of microwaves. The book discusses the circuit forms for microwave integrated circuits; the analysis of microstrip transmission lines; and the use of lumped elements in microwave integrated circuits. The text also describes the microwave properties of ferrimagnetic materials, as well as their interaction with electromagnetic waves propagating in bounded waveguiding structures. The integration techniques useful at high frequencies; material technology for microwave integrated circuits; specific requirements on technology for d

Fourier transformation for engineering and natural science

International Nuclear Information System (INIS)

Klingen, B.

2001-01-01

The following topics are covered: functions, Dirac delta function, Fourier operators, Fourier integrals, Fourier transformation and periodic functions, discrete Fourier transformations and discrete filters, applications. (WL)

Nanosize Fe x O y @SBA-3: A Comparative Study Between Conventional and Microwave Assisted Synthesis.

Science.gov (United States)

Barik, Sunita; Badamali, Sushanta K; Sahoo, Sagarika; Behera, Nandakishor; Dapurkar, Sudhir E

2018-01-01

The present study is focussed on development of highly dispersed nanosize iron oxide (FexOy) particles within the uniform mesopore channels of SBA-3. Herein we report a comparative study between conventional incipient wetness and microwave assisted synthesis routes adopted to devise nanoparticles. The developed materials are characterised by following X-ray diffraction, high resolution transmission electron microscopy, proton induced X-ray emission, diffuse reflectance UV-visible spectroscopy, thermogravimetry and Fourier transform infrared spectroscopy. Mesoporous siliceous SBA-3 was prepared at room temperature to obtain samples with good crystallinity and ordered pore structure. Pore channels of SBA-3 were used as nanoreactor for developing iron oxide nanoparticles. Iron oxide nanoparticles developed under microwave activation showed uniform distribution within the SBA-3 structure along with retaining the orderness of the pore architecture. On the contrary, iron oxides developed under incipient wetness method followed by conventional heating resulted in agglomeration of nanoparticles along with significant loss in SBA-3 pore structure. Proton induced X-ray emission studies revealed the extremely high purity of the samples and almost thrice higher amount of iron oxide particles are encapsulated within the host by microwave assisted preparation as compared to incipient/conventional heating method.

Fourier analysis an introduction

CERN Document Server

Stein, Elias M

2003-01-01

This first volume, a three-part introduction to the subject, is intended for students with a beginning knowledge of mathematical analysis who are motivated to discover the ideas that shape Fourier analysis. It begins with the simple conviction that Fourier arrived at in the early nineteenth century when studying problems in the physical sciences--that an arbitrary function can be written as an infinite sum of the most basic trigonometric functions.The first part implements this idea in terms of notions of convergence and summability of Fourier series, while highlighting applications such as th

Microwave undulator

International Nuclear Information System (INIS)

Batchelor, K.

1986-03-01

The theory of a microwave undulator utilizing a plane rectangular waveguide operating in the TE/sub 10n/ mode and other higher order modes is presented. Based on this, a possible undulator configuration is analyzed, leading to the conclusion that the microwave undulator represents a viable option for undulator wavelength down to about 1 cm where peak voltage and available microwave power considerations limit effectiveness. 4 refs., 4 figs

A measure on the set of compact Friedmann-Lemaitre-Robertson-Walker models

International Nuclear Information System (INIS)

Roukema, Boudewijn F; Blanloeil, Vincent

2010-01-01

Compact, flat Friedmann-Lemaitre-Robertson-Walker (FLRW) models have recently regained interest as a good fit to the observed cosmic microwave background temperature fluctuations. However, it is generally thought that a globally, exactly flat FLRW model is theoretically improbable. Here, in order to obtain a probability space on the set F of compact, comoving, 3-spatial sections of FLRW models, a physically motivated hypothesis is proposed, using the density parameter Ω as a derived rather than fundamental parameter. We assume that the processes that select the 3-manifold also select a global mass-energy and a Hubble parameter. The requirement that the local and global values of Ω are equal implies a range in Ω that consists of a single real value for any 3-manifold. Thus, the obvious measure over F is the discrete measure. Hence, if the global mass-energy and Hubble parameter are a function of 3-manifold choice among compact FLRW models, then probability spaces parametrized by Ω do not, in general, give a zero probability of a flat model. Alternatively, parametrization by a spatial size parameter, the injectivity radius r inj , suggests the Lebesgue measure. In this case, the probability space over the injectivity radius implies that flat models occur almost surely (a.s.), in the sense of probability theory, and non-flat models a.s. do not occur.

A measure on the set of compact Friedmann-Lemaitre-Robertson-Walker models

Energy Technology Data Exchange (ETDEWEB)

Roukema, Boudewijn F [Torun Centre for Astronomy, Nicolaus Copernicus University, ul. Gagarina 11, 87-100 Torun (Poland); Blanloeil, Vincent [IRMA, Departement de Mathematiques, Universite de Strasbourg, 7 rue Rene Descartes, 67084 Strasbourg, Cedex (France)

2010-12-21

Compact, flat Friedmann-Lemaitre-Robertson-Walker (FLRW) models have recently regained interest as a good fit to the observed cosmic microwave background temperature fluctuations. However, it is generally thought that a globally, exactly flat FLRW model is theoretically improbable. Here, in order to obtain a probability space on the set F of compact, comoving, 3-spatial sections of FLRW models, a physically motivated hypothesis is proposed, using the density parameter {Omega} as a derived rather than fundamental parameter. We assume that the processes that select the 3-manifold also select a global mass-energy and a Hubble parameter. The requirement that the local and global values of {Omega} are equal implies a range in {Omega} that consists of a single real value for any 3-manifold. Thus, the obvious measure over F is the discrete measure. Hence, if the global mass-energy and Hubble parameter are a function of 3-manifold choice among compact FLRW models, then probability spaces parametrized by {Omega} do not, in general, give a zero probability of a flat model. Alternatively, parametrization by a spatial size parameter, the injectivity radius r{sub inj}, suggests the Lebesgue measure. In this case, the probability space over the injectivity radius implies that flat models occur almost surely (a.s.), in the sense of probability theory, and non-flat models a.s. do not occur.

Three-Dimensional Microwave Imaging for Indoor Environments

Science.gov (United States)

Scott, Simon

Microwave imaging involves the use of antenna arrays, operating at microwave and millimeter-wave frequencies, for capturing images of real-world objects. Typically, one or more antennas in the array illuminate the scene with a radio-frequency (RF) signal. Part of this signal reflects back to the other antennas, which record both the amplitude and phase of the reflected signal. These reflected RF signals are then processed to form an image of the scene. This work focuses on using planar antenna arrays, operating between 17 and 26 GHz, to capture three-dimensional images of people and other objects inside a room. Such an imaging system enables applications such as indoor positioning and tracking, health monitoring and hand gesture recognition. Microwave imaging techniques based on beamforming cannot be used for indoor imaging, as most objects lie within the array near-field. Therefore, the range-migration algorithm (RMA) is used instead, as it compensates for the curvature of the reflected wavefronts, hence enabling near-field imaging. It is also based on fast-Fourier transforms and is therefore computationally efficient. A number of novel RMA variants were developed to support a wider variety of antenna array configurations, as well as to generate 3-D velocity maps of objects moving around a room. The choice of antenna array configuration, microwave transceiver components and transmit power has a significant effect on both the energy consumed by the imaging system and the quality of the resulting images. A generic microwave imaging testbed was therefore built to characterize the effect of these antenna array parameters on image quality in the 20 GHz band. All variants of the RMA were compared and found to produce good quality three-dimensional images with transmit power levels as low as 1 muW. With an array size of 80x80 antennas, most of the imaging algorithms were able to image objects at 0.5 m range with 12.5 mm resolution, although some were only able to achieve

Variable frequency microwave heating apparatus

Energy Technology Data Exchange (ETDEWEB)

Bible, D.W.; Lauf, R.J.; Johnson, A.C.; Thigpen, L.T.

1999-10-05

A variable frequency microwave heating apparatus (10) designed to allow modulation of the frequency of the microwaves introduced into a multi-mode microwave cavity (34) for testing or other selected applications. The variable frequency microwave heating apparatus (10) includes a microwave signal generator (12) and a high-power microwave amplifier (20) or a high-power microwave oscillator (14). A power supply (22) is provided for operation of the high-power microwave oscillator (14) or microwave amplifier (20). A directional coupler (24) is provided for detecting the direction and amplitude of signals incident upon and reflected from the microwave cavity (34). A first power meter (30) is provided for measuring the power delivered to the microwave furnace (32). A second power meter (26) detects the magnitude of reflected power. Reflected power is dissipated in the reflected power load (28).

Freeze drying vs microwave drying–methods for synthesis of sinteractive thoria powders

Energy Technology Data Exchange (ETDEWEB)

Annie, D.; Chandramouli, V. [Materials Chemistry Division, Chemistry Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, 602103 (India); Anthonysamy, S., E-mail: sas@igcar.gov.in [Materials Chemistry Division, Chemistry Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, 602103 (India); Ghosh, Chanchal; Divakar, R. [Materials Synthesis and Structural Characterization Division, Materials and Metallurgy Group, Indira Gandhi Centre for Atomic Research, Kalpakkam, 602103 (India)

2017-02-15

Thoria powders were synthesized by oxalate precipitation from an aqueous solution of the nitrate. The filtered precipitates were freeze dried or microwave dried before being calcined at 1073 K. The thoria powders obtained were characterized for crystallite size, specific surface area, bulk density, particle size distribution and residual carbon. Microstructure of the product was studied using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Sinterability of the synthesized powders was studied by measuring the density of the sintered compacts. Powders that can be consolidated and sintered to densities ∼96% theoretical density (TD) at 1773 K were obtained.

Jean Baptiste Joseph Fourier

Science.gov (United States)

Sterken, C.

2003-03-01

This paper gives a short account of some key elements in the life of Jean Baptiste Joseph Fourier (1768-1830), specifically his relation to Napoleon Bonaparte. The mathematical approach to Fourier series and the original scepticism by French mathematicians are briefly illustrated.

Advanced microwave processing concepts

Energy Technology Data Exchange (ETDEWEB)

Lauf, R.J.; McMillan, A.D.; Paulauskas, F.L. [Oak Ridge National Laboratory, TN (United States)

1995-05-01

The purpose of this work is to explore the feasibility of several advanced microwave processing concepts to develop new energy-efficient materials and processes. The project includes two tasks: (1) commercialization of the variable-frequency microwave furnace; and (2) microwave curing of polymer composites. The variable frequency microwave furnace, whose initial conception and design was funded by the AIC Materials Program, will allow us, for the first time, to conduct microwave processing studies over a wide frequency range. This novel design uses a high-power traveling wave tube (TWT) originally developed for electronic warfare. By using this microwave source, one can not only select individual microwave frequencies for particular experiments, but also achieve uniform power densities over a large area by the superposition of many different frequencies. Microwave curing of thermoset resins will be studied because it hold the potential of in-situ curing of continuous-fiber composites for strong, lightweight components. Microwave heating can shorten curing times, provided issues of scaleup, uniformity, and thermal management can be adequately addressed.

Fourier Transform Mass Spectrometry

Science.gov (United States)

Scigelova, Michaela; Hornshaw, Martin; Giannakopulos, Anastassios; Makarov, Alexander

2011-01-01

This article provides an introduction to Fourier transform-based mass spectrometry. The key performance characteristics of Fourier transform-based mass spectrometry, mass accuracy and resolution, are presented in the view of how they impact the interpretation of measurements in proteomic applications. The theory and principles of operation of two types of mass analyzer, Fourier transform ion cyclotron resonance and Orbitrap, are described. Major benefits as well as limitations of Fourier transform-based mass spectrometry technology are discussed in the context of practical sample analysis, and illustrated with examples included as figures in this text and in the accompanying slide set. Comparisons highlighting the performance differences between the two mass analyzers are made where deemed useful in assisting the user with choosing the most appropriate technology for an application. Recent developments of these high-performing mass spectrometers are mentioned to provide a future outlook. PMID:21742802

Digital Fourier analysis fundamentals

CERN Document Server

Kido, Ken'iti

2015-01-01

This textbook is a thorough, accessible introduction to digital Fourier analysis for undergraduate students in the sciences. Beginning with the principles of sine/cosine decomposition, the reader walks through the principles of discrete Fourier analysis before reaching the cornerstone of signal processing: the Fast Fourier Transform. Saturated with clear, coherent illustrations, "Digital Fourier Analysis - Fundamentals" includes practice problems and thorough Appendices for the advanced reader. As a special feature, the book includes interactive applets (available online) that mirror the illustrations.  These user-friendly applets animate concepts interactively, allowing the user to experiment with the underlying mathematics. For example, a real sine signal can be treated as a sum of clockwise and counter-clockwise rotating vectors. The applet illustration included with the book animates the rotating vectors and the resulting sine signal. By changing parameters such as amplitude and frequency, the reader ca...

Microwave assisted scalable synthesis of titanium ferrite nanomaterials

Science.gov (United States)

Shukla, Abhishek; Bhardwaj, Abhishek K.; Singh, S. C.; Uttam, K. N.; Gautam, Nisha; Himanshu, A. K.; Shah, Jyoti; Kotnala, R. K.; Gopal, R.

2018-04-01

Titanium ferrite magnetic nanomaterials are synthesized by one-step, one pot, and scalable method assisted by microwave radiation. Effects of titanium content and microwave exposure time on size, shape, morphology, yield, bonding nature, crystalline structure, and magnetic properties of titanium ferrite nanomaterials are studied. As-synthesized nanomaterials are characterized by X-ray diffraction (XRD), ultraviolet-visible absorption spectroscopy (UV-Vis), attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), Raman spectroscopy, transmission electron microscopy (TEM), and vibrating sample magnetometer measurements. XRD measurements depict the presence of two phases of titanium ferrite into the same sample, where crystallite size increases from ˜33 nm to 37 nm with the increase in titanium concentration. UV-Vis measurement showed broad spectrum in the spectral range of 250-600 nm which reveals that its characteristic peaks lie between ultraviolet and visible region; ATR-FTIR and Raman measurements predict iron-titanium oxide structures that are consistent with XRD results. The micrographs of TEM and selected area electron diffraction patterns show formation of hexagonal shaped particles with a high degree of crystallinity and presence of multi-phase. Energy dispersive spectroscopy measurements confirm that Ti:Fe compositional mass ratio can be controlled by tuning synthesis conditions. Increase of Ti defects into titanium ferrite lattice, either by increasing titanium precursor or by increasing exposure time, enhances its magnetic properties.

Fourier transform nuclear magnetic resonance

International Nuclear Information System (INIS)

Geick, R.

1981-01-01

This review starts with the basic principles of resonance phenomena in physical systems. Especially, the connection is shown between the properties of these systems and Fourier transforms. Next, we discuss the principles of nuclear magnetic resonance. Starting from the general properties of physical systems showing resonance phenomena and from the special properties of nuclear spin systems, the main part of this paper reviews pulse and Fourier methods in nuclear magnetic resonance. Among pulse methods, an introduction will be given to spin echoes, and, apart from the principle of Fourier transform nuclear magnetic resonance, an introduction to the technical problems of this method, e.g. resolution in the frequency domain, aliasing, phase and intensity errors, stationary state of the spin systems for repetitive measurements, proton decoupling, and application of Fourier methods to systems in a nonequilibrium state. The last section is devoted to special applications of Fourier methods and recent developments, e.g. measurement of relaxation times, solvent peak suppression, 'rapid scan'-method, methods for suppressing the effects of dipolar coupling in solids, two-dimensional Fourier transform nuclear magnetic resonance, and spin mapping or zeugmatography. (author)

Generalized Fourier transforms classes

DEFF Research Database (Denmark)

Berntsen, Svend; Møller, Steen

2002-01-01

The Fourier class of integral transforms with kernels $B(\\omega r)$ has by definition inverse transforms with kernel $B(-\\omega r)$. The space of such transforms is explicitly constructed. A slightly more general class of generalized Fourier transforms are introduced. From the general theory...

Practical microwave electron devices

CERN Document Server

Meurant, Gerard

2013-01-01

Practical Microwave Electron Devices provides an understanding of microwave electron devices and their applications. All areas of microwave electron devices are covered. These include microwave solid-state devices, including popular microwave transistors and both passive and active diodes; quantum electron devices; thermionic devices (including relativistic thermionic devices); and ferrimagnetic electron devices. The design of each of these devices is discussed as well as their applications, including oscillation, amplification, switching, modulation, demodulation, and parametric interactions.

Optimization for ultrasonic-microwave synergistic extraction of polysaccharides from Cornus officinalis and characterization of polysaccharides.

Science.gov (United States)

Yin, Xiulian; You, Qinghong; Jiang, Zhonghai; Zhou, Xinghai

2016-02-01

Ultrasonic-microwave synergistic extraction (UMSE) of polysaccharides from Cornus officinalis was optimized by response surface methodology (RSM). The effect of four different factors on the yield of C. officinalis polysaccharides (COP) was studied. RSM results showed that the optimal conditions were extraction time of 31.49823 min, microwave power of 99.39769 W, and water-to-raw material ratio of 28.16273. The COP yield was 11.38±0.31% using the modified optimal conditions, which was consistent with the value predicted by the model. The crude COP was purified by DEAE-Cellulose 52 chromatography and Sephadex G-100 chromatography. Five fractions, namely, crude COP, COP-1, COP-2, COP-3, and COP-4, were obtained. Monosaccharide composition analysis revealed that the COP was composed of glucose, arabinose, fucose, xylose, mannose, and rhamnose. Preliminary structural characterizations of COP were conducted by scanning electron microscopy and Fourier transform infrared spectroscopy. Copyright © 2015 Elsevier B.V. All rights reserved.

Experimental and numerical studies of microwave-plasma interaction in a MWPECVD reactor

Directory of Open Access Journals (Sweden)

A. Massaro

2016-12-01

Full Text Available This work deals with and proposes a simple and compact diagnostic method able to characterize the interaction between microwave and plasma without the necessity of using an external diagnostic tool. The interaction between 2.45 GHz microwave and plasma, in a typical ASTeX-type reactor, is investigated from experimental and numerical view points. The experiments are performed by considering plasmas of three different gas mixtures: H2, CH4-H2 and CH4-H2-N2. The two latter are used to deposit synthetic undoped and n-doped diamond films. The experimental setup equipped with a matching network enables the measurements of very low reflected power. The reflected powers show ripples due to the mismatching between wave and plasma impedance. Specifically, the three types of plasma exhibit reflected power values related to the variation of electron-neutral collision frequency among the species by changing the gas mixture. The different gas mixtures studied are also useful to test the sensitivity of the reflected power measurements to the change of plasma composition. By means of a numerical model, only the interaction of microwave and H2 plasma is examined allowing the estimation of plasma and matching network impedances and of reflected power that is found about eighteen times higher than that measured.

Microwave-Assisted Synthesis of Alumina Nanoparticles Using Some Plants Extracts

Directory of Open Access Journals (Sweden)

Meisam Hasanpoor

2017-01-01

Full Text Available In present study we used five green plants for microwave assisted synthesis of Alumina nanoparticles from Aluminum nitrate. Structural characterization was studied using x-ray diffraction that showed semi- crystalline and possibly, amorphous structure. Fourier infrared spectroscopy was used to determine Al-O bond and functional groups responsible for synthesis of nanoparticles. FTIR confirmed existence of Al-O band and bio-functional groups, originated from plant extract. Morphology and size of nanoparticles were investigated using scanning electron microscopy, transmission electron microscopy and atomic force microscopy techniques. It was observed that nanoparticles have near-spherical shape. Average size of clusters of nanoparticles varied with different routes from of 60 nm to 300 nm. AFM images showed that Individual nanoparticles were less than 10 nm.

Magnesium Borate Synthesis by Microwave Energy: A New Method

Directory of Open Access Journals (Sweden)

Azmi Seyhun Kipcak

2013-01-01

Full Text Available Magnesium borates are one of the major groups of boron minerals that have important properties such as high heat and corrosion resistances and high coefficients of elasticity. In this study, magnesium borate minerals are synthesized using boric acid and magnesium oxide with a new method of microwave, and the synthesized minerals are characterized by various analysis techniques. The results show that pure, “magnesium borate hydrate” minerals are obtained at the end of various steps. The characterization of the products is determined with the techniques of X-Ray Diffraction (XRD, Fourier Transform Infrared Spectroscopy (FT-IR, Raman Spectroscopy, and Scanning Electron Microscopy (SEM. Additionally, overall “magnesium borate hydrate” yields are calculated and found about 67% at 270 W, 8 minutes and 360 W, 3 minutes of reaction times, respectively.

Conformational effects on the torsional barriers in m-methylanisole studied by microwave spectroscopy

Science.gov (United States)

Ferres, Lynn; Stahl, Wolfgang; Nguyen, Ha Vinh Lam

2018-03-01

The microwave spectrum of m-methylanisole (also known as 3-methylanisole, or 3-methoxytoluene) was measured using a pulsed molecular jet Fourier transform microwave spectrometer operating in the frequency range of 2-26.5 GHz. Quantum chemical calculations predicted two conformers with the methoxy group in trans or cis position related to the ring methyl group, both of which were assigned in the experimental spectrum. Due to the internal rotation of the ring methyl group, all rotational transitions introduced large A-E splittings up to several GHz, which were analyzed with a newly developed program, called aixPAM, working in the principal axis system. There are significant differences in the V3 potential barriers of 55.7693(90) cm-1 and 36.6342(84) cm-1 determined by fitting 223 and 320 torsional components of the cis and the trans conformer, respectively. These values were compared with those found in other m-substituted toluenes as well as in o- and p-methylanisole. A comparison between the aixPAM and the XIAM code (using a combined axis system) was also performed.

Microwave heating type evaporator

International Nuclear Information System (INIS)

Taura, Masazumi; Nishi, Akio; Morimoto, Takashi; Izumi, Jun; Tamura, Kazuo; Morooka, Akihiko.

1987-01-01

Purpose: To prevent evaporization stills against corrosion due to radioactive liquid wastes. Constitution: Microwaves are supplied from a microwave generator by way of a wave guide tube and through a microwave permeation window to the inside of an evaporatization still. A matching device is attached to the wave guide tube for transmitting the microwaves in order to match the impedance. When the microwaves are supplied to the inside of the evaporization still, radioactive liquid wastes supplied from a liquid feed port by way of a spray tower to the inside of the evaporization still is heated and evaporated by the induction heating of the microwaves. (Seki, T.)

The microwave market

International Nuclear Information System (INIS)

Bybokas, J.

1989-01-01

As superconductors move from the laboratory to the marketplace, it becomes more important for researchers and manufacturers to understand the markets for this technology. The large market for microwave systems represents a major opportunity for high-T c superconductors. Conductor losses are a primary design limitation in conventional microwave systems. The low losses of superconductors at microwave frequencies will allow component designers and system designers to improve their products in many ways. The most important market segments for microwave systems are outlined in this discussion

Tunable fractional-order Fourier transformer

International Nuclear Information System (INIS)

Malyutin, A A

2006-01-01

A fractional two-dimensional Fourier transformer whose orders are tuned by means of optical quadrupoles is described. It is shown that in the optical scheme considered, the Fourier-transform order a element of [0,1] in one of the mutually orthogonal planes corresponds to the transform order (2-a) in another plane, i.e., to inversion and inverse Fourier transform of the order a. (laser modes and beams)

Microwave generation and complex microwave responsivity measurements on small Dayem bridges

DEFF Research Database (Denmark)

Pedersen, Niels Falsig; Sørensen, O; Mygind, Jesper

1977-01-01

Measurements of the active properties of a Dayem micro-bridge at X-band frequencies is described. The bridge was mounted in a microwave cavity designed to match the bridge properly and the microwave output from the cavity was detected using a sensitive X-band spectrometer. Microwave power...

Unconventional methods of imaging: computational microscopy and compact implementations

Science.gov (United States)

McLeod, Euan; Ozcan, Aydogan

2016-07-01

In the past two decades or so, there has been a renaissance of optical microscopy research and development. Much work has been done in an effort to improve the resolution and sensitivity of microscopes, while at the same time to introduce new imaging modalities, and make existing imaging systems more efficient and more accessible. In this review, we look at two particular aspects of this renaissance: computational imaging techniques and compact imaging platforms. In many cases, these aspects go hand-in-hand because the use of computational techniques can simplify the demands placed on optical hardware in obtaining a desired imaging performance. In the first main section, we cover lens-based computational imaging, in particular, light-field microscopy, structured illumination, synthetic aperture, Fourier ptychography, and compressive imaging. In the second main section, we review lensfree holographic on-chip imaging, including how images are reconstructed, phase recovery techniques, and integration with smart substrates for more advanced imaging tasks. In the third main section we describe how these and other microscopy modalities have been implemented in compact and field-portable devices, often based around smartphones. Finally, we conclude with some comments about opportunities and demand for better results, and where we believe the field is heading.

Microwave photonics

CERN Document Server

Lee, Chi H

2006-01-01

Wireless, optical, and electronic networks continue to converge, prompting heavy research into the interface between microwave electronics, ultrafast optics, and photonic technologies. New developments arrive nearly as fast as the photons under investigation, and their commercial impact depends on the ability to stay abreast of new findings, techniques, and technologies. Presenting a broad yet in-depth survey, Microwave Photonics examines the major advances that are affecting new applications in this rapidly expanding field.This book reviews important achievements made in microwave photonics o

General Correlation Theorem for Trinion Fourier Transform

OpenAIRE

Bahri, Mawardi

2017-01-01

- The trinion Fourier transform is an extension of the Fourier transform in the trinion numbers setting. In this work we derive the correlation theorem for the trinion Fourier transform by using the relation between trinion convolution and correlation definitions in the trinion Fourier transform domains.

Fourier Series, the DFT and Shape Modelling

DEFF Research Database (Denmark)

Skoglund, Karl

2004-01-01

This report provides an introduction to Fourier series, the discrete Fourier transform, complex geometry and Fourier descriptors for shape analysis. The content is aimed at undergraduate and graduate students who wish to learn about Fourier analysis in general, as well as its application to shape...

Microscopic molecular dynamics characterization of the second-order non-Navier-Fourier constitutive laws in the Poiseuille gas flow

Energy Technology Data Exchange (ETDEWEB)

Rana, A.; Ravichandran, R. [School of Mechanical and Aerospace Engineering, Gyeongsang National University, Jinju, Gyeongnam 52828 (Korea, Republic of); Park, J. H.; Myong, R. S., E-mail: myong@gnu.ac.kr [School of Mechanical and Aerospace Engineering, Gyeongsang National University, Jinju, Gyeongnam 52828 (Korea, Republic of); Research Center for Aircraft Parts Technology, Gyeongsang National University, Jinju, Gyeongnam 52828 (Korea, Republic of)

2016-08-15

The second-order non-Navier-Fourier constitutive laws, expressed in a compact algebraic mathematical form, were validated for the force-driven Poiseuille gas flow by the deterministic atomic-level microscopic molecular dynamics (MD). Emphasis is placed on how completely different methods (a second-order continuum macroscopic theory based on the kinetic Boltzmann equation, the probabilistic mesoscopic direct simulation Monte Carlo, and, in particular, the deterministic microscopic MD) describe the non-classical physics, and whether the second-order non-Navier-Fourier constitutive laws derived from the continuum theory can be validated using MD solutions for the viscous stress and heat flux calculated directly from the molecular data using the statistical method. Peculiar behaviors (non-uniform tangent pressure profile and exotic instantaneous heat conduction from cold to hot [R. S. Myong, “A full analytical solution for the force-driven compressible Poiseuille gas flow based on a nonlinear coupled constitutive relation,” Phys. Fluids 23(1), 012002 (2011)]) were re-examined using atomic-level MD results. It was shown that all three results were in strong qualitative agreement with each other, implying that the second-order non-Navier-Fourier laws are indeed physically legitimate in the transition regime. Furthermore, it was shown that the non-Navier-Fourier constitutive laws are essential for describing non-zero normal stress and tangential heat flux, while the classical and non-classical laws remain similar for shear stress and normal heat flux.

USE OF THE MICROWAVE RADIATION FOR UPGRADING OF A BIOMASS ALCOHOLIC FERMENTATION

Directory of Open Access Journals (Sweden)

Anna Nowicka

2017-04-01

Full Text Available Perform pretreatment is crucial particularly in the case of the use of hard-degradable biomass, the biochemical susceptibility to degradation, for example, alcoholic fermentation is limited. Biomass disintegration processes lead to the destruction of compact structures and release of the organic substance to the phase dissolved in a resultant increase in the concentration of dissolved easily degradable organic substances. Effective pretreatment should meet several criteria, including ensuring the separation of lignin from cellulose, to increase the share of amorphous cellulose, provide a higher porosity substrates, eliminate waste sugars limit formation of inhibitors, minimize energy costs. The aim of this paper is to show the possibilities of using electromagnetic microwave radiation for pre-treatment plant biomass before the fermentation process of alcohol and comparison of the effectiveness of the described method with other commonly used techniques of pre-treatment. The substrate subjected to microwave treatment has a fast rate of hydrolysis and a high content of glucose in the hydrolyzate, which increases the efficiency of the production of bioethanol.

Microwave Irradiation

Indian Academy of Sciences (India)

Way to Eco-friendly, Green Chemistry. Rashmi ... The rapid heating of food in the kitchen using microwave ovens ... analysis; application to waste treatment; polymer technology; ... of microwave heating in organic synthesis since the first contri-.

Fourier techniques in X-ray timing

NARCIS (Netherlands)

van der Klis, M.

1988-01-01

Basic principles of Fourier techniques often used in X-ray time series analysis are reviewed. The relation between the discrete Fourier transform and the continuous Fourier transform is discussed to introduce the concepts of windowing and aliasing. The relation is derived between the power spectrum

Demonstration of Efficient Nonreciprocity in a Microwave Optomechanical Circuit*

Science.gov (United States)

Peterson, G. A.; Lecocq, F.; Cicak, K.; Simmonds, R. W.; Aumentado, J.; Teufel, J. D.

2017-07-01

The ability to engineer nonreciprocal interactions is an essential tool in modern communication technology as well as a powerful resource for building quantum networks. Aside from large reverse isolation, a nonreciprocal device suitable for applications must also have high efficiency (low insertion loss) and low output noise. Recent theoretical and experimental studies have shown that nonreciprocal behavior can be achieved in optomechanical systems, but performance in these last two attributes has been limited. Here, we demonstrate an efficient, frequency-converting microwave isolator based on the optomechanical interactions between electromagnetic fields and a mechanically compliant vacuum-gap capacitor. We achieve simultaneous reverse isolation of more than 20 dB and insertion loss less than 1.5 dB. We characterize the nonreciprocal noise performance of the device, observing that the residual thermal noise from the mechanical environments is routed solely to the input of the isolator. Our measurements show quantitative agreement with a general coupled-mode theory. Unlike conventional isolators and circulators, these compact nonreciprocal devices do not require a static magnetic field, and they allow for dynamic control of the direction of isolation. With these advantages, similar devices could enable programmable, high-efficiency connections between disparate nodes of quantum networks, even efficiently bridging the microwave and optical domains.

Mouse Embryo Compaction.

Science.gov (United States)

White, M D; Bissiere, S; Alvarez, Y D; Plachta, N

2016-01-01

Compaction is a critical first morphological event in the preimplantation development of the mammalian embryo. Characterized by the transformation of the embryo from a loose cluster of spherical cells into a tightly packed mass, compaction is a key step in the establishment of the first tissue-like structures of the embryo. Although early investigation of the mechanisms driving compaction implicated changes in cell-cell adhesion, recent work has identified essential roles for cortical tension and a compaction-specific class of filopodia. During the transition from 8 to 16 cells, as the embryo is compacting, it must also make fundamental decisions regarding cell position, polarity, and fate. Understanding how these and other processes are integrated with compaction requires further investigation. Emerging imaging-based techniques that enable quantitative analysis from the level of cell-cell interactions down to the level of individual regulatory molecules will provide a greater understanding of how compaction shapes the early mammalian embryo. © 2016 Elsevier Inc. All rights reserved.

Effects of microwave irradiation treatment on physicochemical characteristics of Chinese low-rank coals

International Nuclear Information System (INIS)

Ge, Lichao; Zhang, Yanwei; Wang, Zhihua; Zhou, Junhu; Cen, Kefa

2013-01-01

Highlights: • Typical Chinese lignites with various ranks are upgraded through microwave. • The pore distribution extends to micropore region, BET area and volume increase. • FTIR show the change of microstructure and improvement in coal rank after upgrading. • Upgraded coals exhibit weak combustion similar to Da Tong bituminous coal. • More evident effects are obtained for raw brown coal with relative lower rank. - Abstract: This study investigates the effects of microwave irradiation treatment on coal composition, pore structure, coal rank, function groups, and combustion characteristics of typical Chinese low-rank coals. Results showed that the upgrading process (microwave irradiation treatment) significantly reduced the coals’ inherent moisture, and increased their calorific value and fixed carbon content. It was also found that the upgrading process generated micropores and increased pore volume and surface area of the coals. Results on the oxygen/carbon ratio parameter indicated that the low-rank coals were upgraded to high-rank coals after the upgrading process, which is in agreement with the findings from Fourier transform infrared spectroscopy. Unstable components in the coal were converted into stable components during the upgrading process. Thermo-gravimetric analysis showed that the combustion processes of upgraded coals were delayed toward the high-temperature region, the ignition and burnout temperatures increased, and the comprehensive combustion parameter decreased. Compared with raw brown coals, the upgraded coals exhibited weak combustion characteristics similar to bituminous coal. The changes in physicochemical characteristics became more notable when processing temperature increased from 130 °C to 160 °C or the rank of raw brown coal was lower. Microwave irradiation treatment could be considered as an effective dewatering and upgrading process

Preparation and characterization of novel glass–ceramic tile with microwave absorption properties from iron ore tailings

International Nuclear Information System (INIS)

Yao, Rui; Liao, SongYi; Dai, ChangLu; Liu, YuChen; Chen, XiaoYu; Zheng, Feng

2015-01-01

A novel glass–ceramic tile consisting of one glass–ceramic layer (GC) attaining microwave absorption properties atop ceramic substrate was prepared through quench-heat treatment route derived from iron ore tailings (IOTs) and commercial raw materials (purity range 73–99%). X-ray diffraction (XRD), SEM, Energy dispersive X-ray spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR), Physical property measurement system (PPMS) and Vector network analyzer (VNA) measurements were carried out to investigate phase, microstructure, magnetic and microwave absorption aspects of the glass–ceramic layer. Roughly 80.6±1.7 wt% borosilicate glass and 19.4±1.7 wt% spinel ferrite with chemical formula of (Zn 2+ 0.17 Fe 3+ 0.83 )[Fe 3+ 1.17 Fe 2+ 0.06 Ni 2+ 0.77 ]O 4 were found among the tested samples. Absorption of Electromagnetic wave by 3 mm thick glass–ceramic layer at frequency of 2–18 GHz reached peak reflection loss (RL) of −17.61 dB (98.27% microwave absorption) at 10.31 GHz. Altering the thickness of the glass–ceramic layer can meet the requirements of different level of microwave absorption. - Highlights: • Iron ore tailings (IOTs) have been used as one of the main raw materials. • Glass–ceramic tile contains spinel ferrite has been prepared. • The cation distribution of the spinel ferrite has been calculated. • The intrinsic complex permeability and permittivity have been evaluated

Studies on the effect of the axial magnetic field on the x-ray bremsstrahlung in a 2.45 GHz permanent magnet microwave ion source

International Nuclear Information System (INIS)

Kumar, Narender; Rodrigues, G.; Lakshmy, P. S.; Mathur, Y.; Ahuja, R.; Kanjilal, D.; Baskaran, R.

2014-01-01

A compact microwave ion source has been designed and developed for operation at a frequency of 2.45 GHz. The axial magnetic field is based on two permanent magnet rings, operating in the “off-resonance” mode and is tunable by moving the permanent magnets. In order to understand the electron energy distribution function, x-ray bremsstrahlung has been measured in the axial direction. Simulation studies on the x-ray bremsstrahlung have been carried out to compare with the experimental results. The effect of the axial magnetic field with respect to the microwave launching position and the position of the extraction electrode on the x-ray bremsstrahlung have been studied

Studies on the effect of the axial magnetic field on the x-ray bremsstrahlung in a 2.45 GHz permanent magnet microwave ion source

Energy Technology Data Exchange (ETDEWEB)

Kumar, Narender; Rodrigues, G., E-mail: gerosro@gmail.com; Lakshmy, P. S.; Mathur, Y.; Ahuja, R.; Kanjilal, D. [Inter University Accelerator Centre, Aruna Asaf Ali Marg, New Delhi (India); Baskaran, R. [Indira Gandhi Centre for Atomic Research, Kalpakkam, Tamilnadu (India)

2014-02-15

A compact microwave ion source has been designed and developed for operation at a frequency of 2.45 GHz. The axial magnetic field is based on two permanent magnet rings, operating in the “off-resonance” mode and is tunable by moving the permanent magnets. In order to understand the electron energy distribution function, x-ray bremsstrahlung has been measured in the axial direction. Simulation studies on the x-ray bremsstrahlung have been carried out to compare with the experimental results. The effect of the axial magnetic field with respect to the microwave launching position and the position of the extraction electrode on the x-ray bremsstrahlung have been studied.

Studies on the effect of the axial magnetic field on the x-ray bremsstrahlung in a 2.45 GHz permanent magnet microwave ion source.

Science.gov (United States)

Kumar, Narender; Rodrigues, G; Lakshmy, P S; Baskaran, R; Mathur, Y; Ahuja, R; Kanjilal, D

2014-02-01

A compact microwave ion source has been designed and developed for operation at a frequency of 2.45 GHz. The axial magnetic field is based on two permanent magnet rings, operating in the "off-resonance" mode and is tunable by moving the permanent magnets. In order to understand the electron energy distribution function, x-ray bremsstrahlung has been measured in the axial direction. Simulation studies on the x-ray bremsstrahlung have been carried out to compare with the experimental results. The effect of the axial magnetic field with respect to the microwave launching position and the position of the extraction electrode on the x-ray bremsstrahlung have been studied.

Quadrature formulas for Fourier coefficients

KAUST Repository

Bojanov, Borislav

2009-09-01

We consider quadrature formulas of high degree of precision for the computation of the Fourier coefficients in expansions of functions with respect to a system of orthogonal polynomials. In particular, we show the uniqueness of a multiple node formula for the Fourier-Tchebycheff coefficients given by Micchelli and Sharma and construct new Gaussian formulas for the Fourier coefficients of a function, based on the values of the function and its derivatives. © 2009 Elsevier B.V. All rights reserved.

Transmission spectra changes produced by decreasing compactness of opal-like structures

Science.gov (United States)

Andueza, A.; Echeverría, R.; Morales, P.; Sevilla, J.

2009-01-01

Artificial opal-like structures based on spheres and colloidal particles have been fabricated in a controlled way, presenting optical band-gap properties in the optical frequency range. Nonclose packed artificial opals have also been fabricated and studied recently. In order to gain a better understanding of these phenomena, we have studied macroscopic models of nonclose packed fcc lattices using glass spheres (ɛ =7) of 8 mm diameter, and measuring in the microwave region (from 10 to 30 GHz). The results have shown a Bragg resonance tunable with filling factor of the opal, and a strong rejected band similar, also present in close packed samples, much less affected by compactness. The relation of this high order band with spheres single layer behavior is also discussed.

The fractional Fourier transform and applications

Science.gov (United States)

Bailey, David H.; Swarztrauber, Paul N.

1991-01-01

This paper describes the 'fractional Fourier transform', which admits computation by an algorithm that has complexity proportional to the fast Fourier transform algorithm. Whereas the discrete Fourier transform (DFT) is based on integral roots of unity e exp -2(pi)i/n, the fractional Fourier transform is based on fractional roots of unity e exp -2(pi)i(alpha), where alpha is arbitrary. The fractional Fourier transform and the corresponding fast algorithm are useful for such applications as computing DFTs of sequences with prime lengths, computing DFTs of sparse sequences, analyzing sequences with noninteger periodicities, performing high-resolution trigonometric interpolation, detecting lines in noisy images, and detecting signals with linearly drifting frequencies. In many cases, the resulting algorithms are faster by arbitrarily large factors than conventional techniques.

Fourier Series Optimization Opportunity

Science.gov (United States)

Winkel, Brian

2008-01-01

This note discusses the introduction of Fourier series as an immediate application of optimization of a function of more than one variable. Specifically, it is shown how the study of Fourier series can be motivated to enrich a multivariable calculus class. This is done through discovery learning and use of technology wherein students build the…

Compactly supported Wannier functions and algebraic K -theory

Science.gov (United States)

Read, N.

2017-03-01

In a tight-binding lattice model with n orbitals (single-particle states) per site, Wannier functions are n -component vector functions of position that fall off rapidly away from some location, and such that a set of them in some sense span all states in a given energy band or set of bands; compactly supported Wannier functions are such functions that vanish outside a bounded region. They arise not only in band theory, but also in connection with tensor-network states for noninteracting fermion systems, and for flat-band Hamiltonians with strictly short-range hopping matrix elements. In earlier work, it was proved that for general complex band structures (vector bundles) or general complex Hamiltonians—that is, class A in the tenfold classification of Hamiltonians and band structures—a set of compactly supported Wannier functions can span the vector bundle only if the bundle is topologically trivial, in any dimension d of space, even when use of an overcomplete set of such functions is permitted. This implied that, for a free-fermion tensor network state with a nontrivial bundle in class A, any strictly short-range parent Hamiltonian must be gapless. Here, this result is extended to all ten symmetry classes of band structures without additional crystallographic symmetries, with the result that in general the nontrivial bundles that can arise from compactly supported Wannier-type functions are those that may possess, in each of d directions, the nontrivial winding that can occur in the same symmetry class in one dimension, but nothing else. The results are obtained from a very natural usage of algebraic K -theory, based on a ring of polynomials in e±i kx,e±i ky,..., which occur as entries in the Fourier-transformed Wannier functions.

An alternative path to the boundary: The CFT as the Fourier space of AdS

Science.gov (United States)

Tolfree, Ian M.

2009-12-01

In this thesis we shed new light on the conjectured duality between an n + 1 dimensional theory of gravity in anti de Sitter space (AdS) and an n dimensional conformal field theory (CFT) by showing that the CFT can be interpreted as the Fourier space of AdS. We then make use of this to gain insight into the nature of black hole entropy. In the first part of this thesis, we give an introduction to the ideas of and review the basics of the AdS/CFT. In the next section we make use of well known integral geometry techniques to derive the Fourier transformation of a function on AdS and see it is a function with compact support on the boundary. Comparing this to the literature, we find that the Green's functions from the literature are actually the Fourier weights of the transformation and that the boundary values of fields appearing in the correspondence are the Fourier coefficients of the transformation. One is thus left to interpret the CFT as the quantized version of a classical theory in AdS and the dual operator as the Fourier coefficients. Group theoretic considerations are discussed in relation to the transformation and its potential use in constructing QCD like theories. In the last section, we then build upon this to study the BTZ black hole. Named after its authors, Banados, Teitelboim and Zanelli, the BTZ black hole is a three dimensional (two space plus one time dimension) black hole in anti de Sitter space. Following standard procedures for modifying Fourier Transformations to accommodate quotient spaces we arrive at a mapping in a black hole background consistent with known results that yields the exact micro-states of a scalar field in a black hole background. We find that the micro-states are the Fourier coefficients on the boundary, which transform under the principal series representation of SL(2, R). Using the knowledge of how to represent a bulk scalar field in the CFT, and knowing how a black hole interacts with a scalar field, we deduce the

Classical Fourier analysis

CERN Document Server

Grafakos, Loukas

2014-01-01

The main goal of this text is to present the theoretical foundation of the field of Fourier analysis on Euclidean spaces. It covers classical topics such as interpolation, Fourier series, the Fourier transform, maximal functions, singular integrals, and Littlewood–Paley theory. The primary readership is intended to be graduate students in mathematics with the prerequisite including satisfactory completion of courses in real and complex variables. The coverage of topics and exposition style are designed to leave no gaps in understanding and stimulate further study. This third edition includes new Sections 3.5, 4.4, 4.5 as well as a new chapter on “Weighted Inequalities,” which has been moved from GTM 250, 2nd Edition. Appendices I and B.9 are also new to this edition.  Countless corrections and improvements have been made to the material from the second edition. Additions and improvements include: more examples and applications, new and more relevant hints for the existing exercises, new exercises, and...

Microwave processed NiMg ferrite: Studies on structural and magnetic properties

International Nuclear Information System (INIS)

Chandra Babu Naidu, K.; Madhuri, W.

2016-01-01

Ferrites are magnetic semiconductors realizing an important role in electrical and electronic circuits where electrical and magnetic property coupling is required. Though ferrite materials are known for a long time, there is a large scope in the improvement of their properties (vice sintering and frequency dependence of electrical and magnetic properties) with the current technological trends. Forth coming technology is aimed at miniaturization and smart gadgets, electrical components like inductors and transformers cannot be included in integrated circuits. These components are incorporated into the circuit as surface mount devices whose fabrication involves low temperature co-firing of ceramics and microwave monolithic integrated circuits technologies. These technologies demand low temperature sinter-ability of ferrites. This article presents low temperature microwave sintered Ni–Mg ferrites of general chemical formula Ni_1_−_xMg_xFe_2O_4 (x=0, 0.2, 0.4, 0.5, 0.6, 0.8, 1) for potential applications as transformer core materials. The series of ferrites are characterized using X-ray diffractometer, scanning electron microscopy, Fourier transform infrared and vibrating sample magnetometer for investigating structural, morphological and magnetic properties respectively. The initial permeability is studied with magnesium content, temperature and frequency in the temperature range of 308 K–873 K and 42 Hz–5 MHz. - Highlights: • First article on microwave processed NiMgFe_2O_4 giving. • The article gives systematic magnetic studies. • Cation distribution is discussed based on magnetic moments from VSM. • Promising candidates for transformer core and soft magnet manufacturing.

Microwave processed NiMg ferrite: Studies on structural and magnetic properties

Energy Technology Data Exchange (ETDEWEB)

Chandra Babu Naidu, K.; Madhuri, W., E-mail: madhuriw12@gmail.com

2016-12-15

Ferrites are magnetic semiconductors realizing an important role in electrical and electronic circuits where electrical and magnetic property coupling is required. Though ferrite materials are known for a long time, there is a large scope in the improvement of their properties (vice sintering and frequency dependence of electrical and magnetic properties) with the current technological trends. Forth coming technology is aimed at miniaturization and smart gadgets, electrical components like inductors and transformers cannot be included in integrated circuits. These components are incorporated into the circuit as surface mount devices whose fabrication involves low temperature co-firing of ceramics and microwave monolithic integrated circuits technologies. These technologies demand low temperature sinter-ability of ferrites. This article presents low temperature microwave sintered Ni–Mg ferrites of general chemical formula Ni{sub 1−x}Mg{sub x}Fe{sub 2}O{sub 4} (x=0, 0.2, 0.4, 0.5, 0.6, 0.8, 1) for potential applications as transformer core materials. The series of ferrites are characterized using X-ray diffractometer, scanning electron microscopy, Fourier transform infrared and vibrating sample magnetometer for investigating structural, morphological and magnetic properties respectively. The initial permeability is studied with magnesium content, temperature and frequency in the temperature range of 308 K–873 K and 42 Hz–5 MHz. - Highlights: • First article on microwave processed NiMgFe{sub 2}O{sub 4} giving. • The article gives systematic magnetic studies. • Cation distribution is discussed based on magnetic moments from VSM. • Promising candidates for transformer core and soft magnet manufacturing.

Review of Microwave Photonics Technique to Generate the Microwave Signal by Using Photonics Technology

Science.gov (United States)

Raghuwanshi, Sanjeev Kumar; Srivastav, Akash

2017-12-01

Microwave photonics system provides high bandwidth capabilities of fiber optic systems and also contains the ability to provide interconnect transmission properties, which are virtually independent of length. The low-loss wide bandwidth capability of optoelectronic systems makes them attractive for the transmission and processing of microwave signals, while the development of high-capacity optical communication systems has required the use of microwave techniques in optical transmitters and receivers. These two strands have led to the development of the research area of microwave photonics. So, we can considered microwave photonics as the field that studies the interaction between microwave and optical waves for applications such as communications, radars, sensors and instrumentations. In this paper we have thoroughly reviewed the microwave generation techniques by using photonics technology.

Progress in CPI Microwave Tube Development

Science.gov (United States)

Wright, Edward L.; Bohlen, Heinz

2006-01-01

CPI continues its role as a leading supplier of state-of-the-art, high-power microwave tubes; from linear beam, velocity- and density-modulated devices, to high frequency gyro-devices. Klystrons are the device-of-choice for many high-power microwave applications, and can provide multi-megawatts to multi-kilowatts of power from UHF to W-band, respectively. A number of recent and on-going developments will be described. At UHF frequencies, the inductive output tube (IOT) has replaced the klystron for terrestrial NTSC and HDTV broadcast, due to its high efficiency and linearity, and is beginning to see use in scientific applications requiring 300 kW or less. Recent advances have enabled use well into L-band. CPI has developed a number of multiple-beam amplifiers. The VKL-8301 multiple-beam klystron (MBK) was built for the TESLA V/UV and x-ray FEL projects, and is a candidate RF source for the International Linear Collider (ILC). We have also contributed to the development of the U.S. Naval Research Laboratory (NRL) high-power fundamental-mode S-band MBK. The VHP-8330B multiple-beam, high-order mode (HOM) IOT shows great promise as a compact, CW UHF source for high power applications. These topics will be discussed, along with CPI's development capabilities for new and novel applications. Most important is our availability to provide design and fabrication services to organizations requiring CPI's manufacturing and process control infrastructure to build and test state-of-the-art devices.

Microwave heating denitration device

International Nuclear Information System (INIS)

Sato, Hajime; Morisue, Tetsuo.

1984-01-01

Purpose: To suppress energy consumption due to a reflection of microwaves. Constitution: Microwaves are irradiated to the nitrate solution containing nuclear fuel materials, to cause denitrating reaction under heating and obtain oxides of the nuclear fuel materials. A microwave heating and evaporation can for reserving the nitrate solution is disposed slantwise relative to the horizontal plane and a microwave heating device is connected to the evaporation can, and inert gases for agitation are supplied to the solution within the can. Since the evaporation can is slanted, wasteful energy consumption due to the reflection of the microwaves can be suppressed. (Moriyama, K.)

Small-scale fluctuations in the microwave background radiation and multiple gravitational lensing

International Nuclear Information System (INIS)

Kashlinsky, A.

1988-01-01

It is shown that multiple gravitational lensing of the microwave background radiation (MBR) by static compact objects significantly attenuates small-scale fluctuations in the MBR. Gravitational lensing, by altering trajectories of MBR photons reaching an observer, leads to (phase) mixing of photons from regions with different initial fluctuations. As a result of this diffusion process the original fluctuations are damped on scales up to several arcmin. An equation that describes this process and its general solution are given. It is concluded that the present upper limits on the amplitude of the MBR fluctuations on small scales cannot constrain theories of galaxy formation. 25 references

Plasma relativistic microwave electronics

International Nuclear Information System (INIS)

Kuzelev, M.V.; Loza, O.T.; Rukhadze, A.A.; Strelkov, P.S.; Shkvarunets, A.G.

2001-01-01

One formulated the principles of plasma relativistic microwave electronics based on the induced Cherenkov radiation of electromagnetic waves at interaction of a relativistic electron beam with plasma. One developed the theory of plasma relativistic generators and accelerators of microwave radiation, designed and studied the prototypes of such devices. One studied theoretically the mechanisms of radiation, calculated the efficiencies and the frequency spectra of plasma relativistic microwave generators and accelerators. The theory findings are proved by the experiment: intensity of the designed sources of microwave radiation is equal to 500 μW, the frequency of microwave radiation is increased by 7 times (from 4 up to 28 GHz), the width of radiation frequency band may vary from several up to 100%. The designed sources of microwave radiation are no else compared in the electronics [ru

Cpuf: Chirped-Pulse Microwave Spectroscopy in Pulsed Uniform Supersonic Flows

Science.gov (United States)

Suits, Arthur; Abeysekera, Chamara; Zack, Lindsay N.; Joalland, Baptiste; Ariyasingha, Nuwandi M.; Park, Barratt; Field, Robert W.; Sims, Ian

2015-06-01

Chirped-pulse Fourier-transform microwave spectroscopy has stimulated a resurgence of interest in rotational spectroscopy owing to the dramatic reduction in spectral acquisition time it enjoys when compared to cavity-based instruments. This suggests that it might be possible to adapt the method to study chemical reaction dynamics and even chemical kinetics using rotational spectroscopy. The great advantage of this would be clear, quantifiable spectroscopic signatures for polyatomic products as well as the possibility to identify and characterize new radical reaction products and transient intermediates. To achieve this, however, several conditions must be met: 1) products must be thermalized at low temperature to maximize the population difference needed to achieve adequate signal levels and to permit product quantification based on the rotational line strength; 2) a large density and volume of reaction products is also needed to achieve adequate signal levels; and 3) for kinetics studies, a uniform density and temperature is needed throughout the course of the reaction. These conditions are all happily met by the uniform supersonic flow produced from a Laval nozzle expansion. In collaboration with the Field group at MIT we have developed a new instrument we term a CPUF (Chirped-pulse/Uniform Flow) spectrometer in which we can study reaction dynamics, photochemistry and kinetics using broadband microwave and millimeter wave spectroscopy as a product probe. We will illustrate the performance of the system with a few examples of photodissociation and reaction dynamics, and also discuss a number of challenges unique to the application of chirped-pulse microwave spectroscopy in the collisional environment of the flow. Future directions and opportunities for application of CPUF will also be explored.

The Barrier Properties of PET Coated DLC Film Deposited by Microwave Surface-Wave PECVD

Science.gov (United States)

Yin, Lianhua; Chen, Qiang

2017-12-01

In this paper we report the investigation of diamond-like carbon (DLC) deposited by microwave surface-wave plasma enhanced chemical vapor deposition (PECVD) on the polyethylene terephthalate (PET) web for the purpose of the barrier property improvement. In order to characterize the properties of DLC coatings, we used several substrates, silicon wafer, glass, and PET web and KBr tablet. The deposition rate was obtained by surface profiler based on the DLC deposited on glass substrates; Fourier transform infrared spectroscope (FTIR) was carried out on KBr tablets to investigate chemical composition and bonding structure; the morphology of the DLC coating was analyzed by atomic force microscope (AFM) on Si substrates. For the barrier properties of PET webs, we measured the oxygen transmission rate (OTR) and water vapor transmission rate (WVTR) after coated with DLC films. We addressed the film barrier property related to process parameters, such as microwave power and pulse parameter in this work. The results show that the DLC coatings can greatly improve the barrier properties of PET webs.

High yield and facile microwave-assisted synthesis of conductive H_2SO_4 doped polyanilines

International Nuclear Information System (INIS)

Gizdavic-Nikolaidis, Marija R.; Jevremovic, Milutin M.; Milenkovic, Maja; Allison, Morgan C.; Stanisavljev, Dragomir R.; Bowmaker, Graham A.; Zujovic, Zoran D.

2016-01-01

The microwave-assisted synthesis of polyaniline (PANI) was performed using ammonium persulphate (APS) as oxidizing agent in 0.5 M–2.5 M concentration range of aqueous sulphuric acid (H_2SO_4) at 93 W applied microwave power of 10 min duration. The microwave (MW) synthesized PANIs had 3 times higher yield in comparison to PANI samples prepared using a classical method, CS (0 W MW power) at the same temperature for 10 min synthesis duration period. Fourier Transform Infrared (FTIR) and UV–Vis spectroscopies confirmed the formation of PANI structure in all products. The influence of H_2SO_4 acid dopant on the spin concentration of MW and CS H_2SO_4 doped PANI samples were examined by EPR spectroscopy, while the morphological characteristics were investigated by using scanning electron microscopy (SEM). XRD results showed amorphous phases in both MW and CS H_2SO_4 doped PANI samples. Conductivity measurements revealed ∼1.5 times higher conductivity values for MW H_2SO_4 doped PANI samples in comparison with PANI samples prepared by the CS method under same condition. The influence of sulfate anion in comparison to chloride anion as a dopant on morphological, dopant levels and conductivity properties of MW PANI samples were also investigated. - Highlights: • Nanoporous microwave synthesized doped polyanilines as chemical sensor material. • Morphology and physical properties of polyanilines depend on acid concentration. • Spin concentration is determined by the nature of the polyaniline synthesis.

A compact very wideband amplifying filter based on RTD loaded composite right/left-handed transmission lines.

Science.gov (United States)

Abu-Marasa, Mahmoud O Mahmoud; El-Khozondar, Hala Jarallah

2015-01-01

The composite right/left-handed (CRLH) transmission line (TL) is presented as a general TL possessing both left-handed (LH) and right-handed (RH) natures. RH materials have both positive permittivity and positive permeability, and LH materials have both negative permittivity and negative permeability. This paper aims to design and analyze nonlinear CRLH-TL transmission line loaded with resonant tunneling diode (RTD). The main application of this design is a very wideband and compact filter that amplifies the travelling signal. We used OrCAD and ADS software to analyze the proposed circuit. CRLH-TL consists of a microstrip line which is loaded with complementary split-rings resonators (CSRRs), series gaps, and shunt inductor connected parallel to the RTD. The designed structure possess a wide band that ranges from 5 to 10.5 GHz and amplifies signal up to 50 %. The proposed design is of interest to microwave compact component designers.

Microwave engineering concepts and fundamentals

CERN Document Server

Khan, Ahmad Shahid

2014-01-01

Detailing the active and passive aspects of microwaves, Microwave Engineering: Concepts and Fundamentals covers everything from wave propagation to reflection and refraction, guided waves, and transmission lines, providing a comprehensive understanding of the underlying principles at the core of microwave engineering. This encyclopedic text not only encompasses nearly all facets of microwave engineering, but also gives all topics—including microwave generation, measurement, and processing—equal emphasis. Packed with illustrations to aid in comprehension, the book: •Describes the mathematical theory of waveguides and ferrite devices, devoting an entire chapter to the Smith chart and its applications •Discusses different types of microwave components, antennas, tubes, transistors, diodes, and parametric devices •Examines various attributes of cavity resonators, semiconductor and RF/microwave devices, and microwave integrated circuits •Addresses scattering parameters and their properties, as well a...

Microwave Measurements

CERN Document Server

Skinner, A D

2007-01-01

The IET has organised training courses on microwave measurements since 1983, at which experts have lectured on modern developments. Their lecture notes were first published in book form in 1985 and then again in 1989, and they have proved popular for many years with a readership beyond those who attended the courses. The purpose of this third edition of the lecture notes is to bring the latest techniques in microwave measurements to this wider audience. The book begins with a survey of the theory of current microwave circuits and continues with a description of the techniques for the measureme

Design and manufacture of large lightweight composite reflectors for microwave testing

Science.gov (United States)

Towers, P.

The installation of the largest compact microwave test range constructed to date prompted the design and manufacture of a 250-sq ft parabolic reflector supported by a lightweight, dimensionally stable structure that could be produced at relatively low cost to high tolerances. These tolerances had, moreover, to be maintained during transport and erection in an indoor test range that was remote from the manufacturing site. The dish designed to meet these requirements consisted of an 'egg box' structure with epoxy/glass composite skin-aluminum honeycomb core sandwich construction. Tiles of this same material formed the substrate for a strickled syntactic-filled epoxy resin grout that was subsequently machined to form the silver-coated reflector surface.

Methyl internal rotation in the microwave spectrum of vinyl acetate.

Science.gov (United States)

Nguyen, Ha Vinh Lam; Jabri, Atef; Van, Vinh; Stahl, Wolfgang

2014-12-26

The rotational spectrum of vinyl acetate, CH3(CO)OCH═CH2, was measured using two molecular beam Fourier transform microwave spectrometers operating in the frequency range from 2 to 40 GHz. Large splittings up to 2 GHz occurred due to the internal rotation of the acetyl methyl group CH3CO with a V3 potential of 151.492(34) cm(-1), much larger than the barrier of approximately 100 cm(-1) often found in acetates. The torsional transitions were fitted using three different programs XIAM, ERHAM, and BELGI-Cs, whereby the rotational constants, centrifugal distortion constants, and the internal rotation parameters could be determined with very high accuracy. The experimental results were supported by quantum chemical calculations. For a conformational analysis, potential energy surfaces were calculated.

A combined source of electron bunches and microwave power

International Nuclear Information System (INIS)

Xie, J.L.; Wang, F.Y.; Yang, X.P.; Shen, B.; Gu, W.; Zhang, L.W.

2003-01-01

In this article, the possibility of using a high power klystron amplifier simultaneously as a microwave power source as usual and an electron bunches source by extracting the spent beam with a magnet and also as an oscillator by feedback is investigated. The purpose of this study is to demonstrate the feasibility of constructing a very compact electron linear accelerator or for other applications of electron bunches. The feasibility of the idea was first examined by computer simulation of the electron motion in a 5 MW klystron and the characteristics of the klystron spent beam. Experimental study was then carried out by installing a radio frequency cavity and a Faraday cage in sequence at the exit end of a bending magnet located at the top of the klystron collector. The energy and current of the chopped spent electron beam can then be measured. By properly choosing the feedback circuit elements, the frequency stability of the klystron in oscillator mode was proved to be good enough for linac operation. According to the results presented in this article, it is evident that an extremely compact linac for research and education with better affordability can be constructed to promote the applications of linacs

Teaching Fourier optics through ray matrices

International Nuclear Information System (INIS)

Moreno, I; Sanchez-Lopez, M M; Ferreira, C; Davis, J A; Mateos, F

2005-01-01

In this work we examine the use of ray-transfer matrices for teaching and for deriving some topics in a Fourier optics course, exploiting the mathematical simplicity of ray matrices compared to diffraction integrals. A simple analysis of the physical meaning of the elements of the ray matrix provides a fast derivation of the conditions to obtain the optical Fourier transform. We extend this derivation to fractional Fourier transform optical systems, and derive the order of the transform from the ray matrix. Some examples are provided to stress this point of view, both with classical and with graded index lenses. This formulation cannot replace the complete explanation of Fourier optics provided by the wave theory, but it is a complementary tool useful to simplify many aspects of Fourier optics and to relate them to geometrical optics

X-ray interferometric Fourier holography

International Nuclear Information System (INIS)

Balyan, M.K.

2016-01-01

The X-ray interferometric Fourier holography is proposed and theoretically investigated. Fourier The X-ray interferometric Young fringes and object image reconstruction are investigated. It is shown that the interference pattern of two slits formed on the exit surface of the crystal-analyzer (the third plate of the interferometer) is the X-ray interferometric Young fringes. An expression for X-ray interferometric Young fringes period is obtained. The subsequent reconstruction of the slit image as an object is performed by means of Fourier transform of the intensity distribution on the hologram. Three methods of reconstruction of the amplitude transmission complex function of the object are presented: analytical - approximate method, method of iteration and step by step method. As an example the X-ray Fourier interferometric hologram recording and the complex amplitude transmission function reconstruction for a beryllium circular wire are considered

Proceedings of microwave processing of materials 3

International Nuclear Information System (INIS)

Beatty, R.L.

1992-01-01

This book contains proceedings of the third MRS Symposium on Microwave Processing of Materials. Topics covered include: Microwave Processing Overviews, Numerical Modeling Techniques, Microwave Processing System Design, Microwave/Plasma Processing, Microwave/Materials Interactions, Microwave Processing of Ceramics, Microwave Processing of Polymers, Microwave Processing of Hazardous Wastes, Microwave NDE Techniques and Dielectric Properties and Measurements

The microwave effects on the properties of alumina at high frequencies of microwave sintering

International Nuclear Information System (INIS)

Sudiana, I. Nyoman; Ngkoimani, La Ode; Usman, Ida; Mitsudo, Seitaro; Sako, Katsuhide; Inagaki, Shunsuke; Aripin, H.

2016-01-01

Microwave sintering of materials has attracted much research interest because of its significant advantages (e.g. reduced sintering temperatures and soaking times) over the conventional heating. Most researchers compared processes that occurred during the microwave and conventional heating at the same temperature and time. The enhancements found in the former method are indicated as a 'non-thermal effect' which is usually used for explaining the phenomena in microwave processing. Numerous recent studies have been focused on the effect to elucidate the microwave interaction mechanism with materials. Moreover, recent progress on microwave sources such as gyrotrons has opened the possibility for processing materials by using a higher microwave frequency. Therefore, the technology is expected to exhibit a stronger non-thermal effect. This paper presents results from a series of experiments to study the non-thermal effect on microwave sintered alumina. Sintering by using a wide rage of microwave frequencies up to 300 GHz as well as a conventional furnace was carried out. The linear shrinkages of samples for each sintering method were measured. Pores and grains taken from scanning electron microstructure (SEM) images of cut surfaces were also examined. The results of a comparative study of the shrinkages and microstructure evolutions of the sintered samples under annealing in microwave heating systems and in an electric furnace were analyzed. A notably different behavior of the shrinkages and microstructures of alumina after being annealed was found. The results suggested that microwave radiations provided an additional force for mass transports. The results also indicated that the sintering process depended on microwave frequencies.

The microwave effects on the properties of alumina at high frequencies of microwave sintering

Energy Technology Data Exchange (ETDEWEB)

Sudiana, I. Nyoman, E-mail: sudiana75@yahoo.com; Ngkoimani, La Ode; Usman, Ida [Department of Physics, Faculty of Mathematic and Natural Science, Halu Oleo University, Kampus Bumi Tridharma Anduonohu, Kendari 93232 (Indonesia); Mitsudo, Seitaro; Sako, Katsuhide; Inagaki, Shunsuke [Research Center for Development of Far-Infrared Region, University of Fukui, 3-9-1 Bunkyo, Fukui-shi 910-8507 (Japan); Aripin, H. [Center for Material Processing and Renewable Energy, Faculty of Learning Teacher and Education Science, Siliwangi University, Jl. Siliwangi 24 Tasikmalaya 46115, West Java (Indonesia)

2016-03-11

Microwave sintering of materials has attracted much research interest because of its significant advantages (e.g. reduced sintering temperatures and soaking times) over the conventional heating. Most researchers compared processes that occurred during the microwave and conventional heating at the same temperature and time. The enhancements found in the former method are indicated as a 'non-thermal effect' which is usually used for explaining the phenomena in microwave processing. Numerous recent studies have been focused on the effect to elucidate the microwave interaction mechanism with materials. Moreover, recent progress on microwave sources such as gyrotrons has opened the possibility for processing materials by using a higher microwave frequency. Therefore, the technology is expected to exhibit a stronger non-thermal effect. This paper presents results from a series of experiments to study the non-thermal effect on microwave sintered alumina. Sintering by using a wide rage of microwave frequencies up to 300 GHz as well as a conventional furnace was carried out. The linear shrinkages of samples for each sintering method were measured. Pores and grains taken from scanning electron microstructure (SEM) images of cut surfaces were also examined. The results of a comparative study of the shrinkages and microstructure evolutions of the sintered samples under annealing in microwave heating systems and in an electric furnace were analyzed. A notably different behavior of the shrinkages and microstructures of alumina after being annealed was found. The results suggested that microwave radiations provided an additional force for mass transports. The results also indicated that the sintering process depended on microwave frequencies.

Microwave-assisted Chemical Transformations

Science.gov (United States)

In recent years, there has been a considerable interest in developing sustainable chemistries utilizing green chemistry principles. Since the first published report in 1986 by Gedye and Giguere on microwave assisted synthesis in household microwave ovens, the use of microwaves as...

Widely tunable quantum cascade laser-based terahertz source.

Science.gov (United States)

Danylov, Andriy A; Light, Alexander R; Waldman, Jerry; Erickson, Neal; Qian, Xifeng

2014-07-10

A compact, tunable, ultranarrowband terahertz source, Δν∼1  MHz, is demonstrated by upconversion of a 2.324 THz, free-running quantum cascade laser with a THz Schottky-diode-balanced mixer using a swept, synthesized microwave source to drive the nonlinearity. Continuously tunable radiation of 1 μW power is demonstrated in two frequency regions: ν(Laser) ± 0 to 50 GHz and ν(Laser) ± 70 to 115 GHz. The sideband spectra were characterized with a Fourier-transform spectrometer, and the radiation was tuned through CO, HDO, and D2O rotational transitions.

Cosmic Microwave Background Timeline

Science.gov (United States)

Cosmic Microwave Background Timeline 1934 : Richard Tolman shows that blackbody radiation in an will have a blackbody cosmic microwave background with temperature about 5 K 1955: Tigran Shmaonov anisotropy in the cosmic microwave background, this strongly supports the big bang model with gravitational

Treatment of nitridation by microwave post discharge plasma in an AISI 4140 steel; Tratamiento de nitruracion por plasma post-descarga micro-ondas en un acero AISI 4140

Energy Technology Data Exchange (ETDEWEB)

Medina F, A. [Instituto Tecnologico de Morelia, Morelia e Instituto Nacional de Investigaciones Nucleares, A.P. 18-1027, 11801 Mexico D.F. (Mexico); Rodriguez L, V.; Zamora R, L. [ININ, Mexico D.F. (Mexico); Oseguera P, J

1998-07-01

The objective of this work is to determine through X-ray diffraction, microhardness measurement and scanning electron microscopy those main operation parameters of the microwave post discharge treatment (temperature of treatment, gas mixture and permanence time) nitriding an AISI 4140 steel and to characterize the compact layer of nitrides formed during the treatment. (Author)

On fractional Fourier transform moments

NARCIS (Netherlands)

Alieva, T.; Bastiaans, M.J.

2000-01-01

Based on the relation between the ambiguity function represented in a quasi-polar coordinate system and the fractional power spectra, the fractional Fourier transform moments are introduced. Important equalities for the global second-order fractional Fourier transform moments are derived and their

Fourier analysis and stochastic processes

CERN Document Server

Brémaud, Pierre

2014-01-01

This work is unique as it provides a uniform treatment of the Fourier theories of functions (Fourier transforms and series, z-transforms), finite measures (characteristic functions, convergence in distribution), and stochastic processes (including arma series and point processes). It emphasises the links between these three themes. The chapter on the Fourier theory of point processes and signals structured by point processes is a novel addition to the literature on Fourier analysis of stochastic processes. It also connects the theory with recent lines of research such as biological spike signals and ultrawide-band communications. Although the treatment is mathematically rigorous, the convivial style makes the book accessible to a large audience. In particular, it will be interesting to anyone working in electrical engineering and communications, biology (point process signals) and econometrics (arma models). A careful review of the prerequisites (integration and probability theory in the appendix, Hilbert spa...

A simple approach to Fourier aliasing

International Nuclear Information System (INIS)

Foadi, James

2007-01-01

In the context of discrete Fourier transforms the idea of aliasing as due to approximation errors in the integral defining Fourier coefficients is introduced and explained. This has the positive pedagogical effect of getting to the heart of sampling and the discrete Fourier transform without having to delve into effective, but otherwise long and structured, introductions to the topic, commonly met in advanced, specialized books

Advances in microwaves 7

CERN Document Server

Young, Leo

2013-01-01

Advances in Microwaves, Volume 7 covers the developments in the study of microwaves. The book discusses the effect of surface roughness on the propagation of the TEM mode, as well as the voltage breakdown of microwave antennas. The text also describes the theory and design considerations of single slotted-waveguide linear arrays and the techniques and theories that led to the achievement of wide bandwidths and ultralow noise temperatures for communication applications. The book will prove invaluable to microwave engineers.

Compact Polarimetry Potentials

Science.gov (United States)

Truong-Loi, My-Linh; Dubois-Fernandez, Pascale; Pottier, Eric

2011-01-01

The goal of this study is to show the potential of a compact-pol SAR system for vegetation applications. Compact-pol concept has been suggested to minimize the system design while maximize the information and is declined as the ?/4, ?/2 and hybrid modes. In this paper, the applications such as biomass and vegetation height estimates are first presented, then, the equivalence between compact-pol data simulated from full-pol data and compact-pol data processed from raw data as such is shown. Finally, a calibration procedure using external targets is proposed.

Influence of preparation methods of microwave, sol-gel, and hydrothermal on structural and optical properties of lanthania nanoparticles

Energy Technology Data Exchange (ETDEWEB)

Goharshadi, Elaheh K.; Mahvelati, Tahereh; Yazdanbakhsh, Mohammad [Ferdowsi Univ., Mashhad (Iran, Islamic Republic of). Dept. of Chemistry

2016-01-15

In this work, the nearly pure hexagonal phase of lanthania nanoparticles (NPs) was successfully synthesized using three methods: microwave, sol-gel, and hydrothermal. The samples were characterized using nine techniques including powder X-ray powder diffraction, thermogravimetry, transmission electron microscopy, scanning electron microscopy, field emission microscopy, energy-dispersive X-ray spectroscopy, Fourier transform infrared spectroscopy, far infrared spectroscopy, and ultraviolet-visible absorption spectroscopy. This study showed that the method of synthesizing lanthania NPs can affect the size, which in turn has impact on structural, morphological, and optical properties.

Microwave processing heats up

Science.gov (United States)

Microwaves are a common appliance in many households. In the United States microwave heating is the third most popular domestic heating method food foods. Microwave heating is also a commercial food processing technology that has been applied for cooking, drying, and tempering foods. It's use in ...

The European Microwave Week 2008 and its Microwave Conferences

NARCIS (Netherlands)

Hoogeboom, P.; Van Vliet, F.

2009-01-01

Under the auspices of the European Microwave Association (EuMA) the 11th annual European Microwave Week was organized in the Amsterdam RAI Congress Centre, The Netherlands, 27-31 October 2008. This major event consisted this year of five conferences, an exhibition, and various side events. The 38th

Compaction of FGD-gypsum

NARCIS (Netherlands)

Stoop, B.T.J.; Larbi, J.A.; Heijnen, W.M.M.

1996-01-01

It is shown that it is possible to produce compacted gypsum with a low porosity and a high strength on a laboratory scale by uniaxial compaction of flue gas desulphurization (FGD-) gypsum powder. Compacted FGD-gypsum cylinders were produced at a compaction pres-sure between 50 and 500 MPa yielding

(U) Influence of Compaction Model Form on Planar and Cylindrical Compaction Geometries

Energy Technology Data Exchange (ETDEWEB)

Fredenburg, David A. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Carney, Theodore Clayton [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Fichtl, Christopher Allen [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Ramsey, Scott D. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2018-01-05

The dynamic compaction response of CeO₂ is examined within the frameworks of the Ramp and P-a compaction models. Hydrocode calculations simulating the dynamic response of CeO₂ at several distinct pressures within the compaction region are investigated in both planar and cylindrically convergent geometries. Findings suggest additional validation of the compaction models is warranted under complex loading configurations.

Microwave-assisted methyl esters synthesis of Kapok (Ceiba pentandra seed oil: parametric and optimization study

Directory of Open Access Journals (Sweden)

Awais Bokhari

2015-09-01

Full Text Available The depleting fossil fuel reserves and increasing environmental concerns have continued to stimulate research into biodiesel as a green fuel alternative produced from renewable resources. In this study, Kapok (Ceiba pentandra oil methyl ester was produced by using microwave-assisted technique. The optimum operating conditions for the microwave-assisted transesterification of Kapok seed oil including temperature, catalyst loading, methanol to oil molar ratio, and irradiation time were investigated by using Response Surface Methodology (RSM based on Central Composite Design (CCD. A maximum conversion of 98.9 % was obtained under optimum conditions of 57.09 °C reaction temperature, 2.15 wt% catalyst (KOH loading, oil to methanol molar ratio of 1:9.85, and reaction time of 3.29 min. Fourier Transform Infra-Red (FT-IR spectroscopy was performed to verify the conversion of the fatty acid into methyl esters. The properties of Kapok oil methyl ester produced under the optimum conditions were characterized and found in agreement with the international ASTM D 6751 and EN 14214 standards.

Preparation and characterization of novel glass–ceramic tile with microwave absorption properties from iron ore tailings

Energy Technology Data Exchange (ETDEWEB)

Yao, Rui; Liao, SongYi [School of Materials Science and Engineering, Central South University, Changsha 410083 (China); Dai, ChangLu [Guangdong Bode Fine Building Material Co. Ltd., Foshan 528000 (China); Liu, YuChen; Chen, XiaoYu [School of Materials Science and Engineering, Central South University, Changsha 410083 (China); Zheng, Feng, E-mail: fzheng@csu.edu.cn [School of Materials Science and Engineering, Central South University, Changsha 410083 (China); Phase diagrams and materials design center, Central South University, Changsha 410083 (China)

2015-03-15

A novel glass–ceramic tile consisting of one glass–ceramic layer (GC) attaining microwave absorption properties atop ceramic substrate was prepared through quench-heat treatment route derived from iron ore tailings (IOTs) and commercial raw materials (purity range 73–99%). X-ray diffraction (XRD), SEM, Energy dispersive X-ray spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR), Physical property measurement system (PPMS) and Vector network analyzer (VNA) measurements were carried out to investigate phase, microstructure, magnetic and microwave absorption aspects of the glass–ceramic layer. Roughly 80.6±1.7 wt% borosilicate glass and 19.4±1.7 wt% spinel ferrite with chemical formula of (Zn{sup 2+}{sub 0.17}Fe{sup 3+}{sub 0.83})[Fe{sup 3+}{sub 1.17}Fe{sup 2+}{sub 0.06}Ni{sup 2+}{sub 0.77}]O{sub 4} were found among the tested samples. Absorption of Electromagnetic wave by 3 mm thick glass–ceramic layer at frequency of 2–18 GHz reached peak reflection loss (RL) of −17.61 dB (98.27% microwave absorption) at 10.31 GHz. Altering the thickness of the glass–ceramic layer can meet the requirements of different level of microwave absorption. - Highlights: • Iron ore tailings (IOTs) have been used as one of the main raw materials. • Glass–ceramic tile contains spinel ferrite has been prepared. • The cation distribution of the spinel ferrite has been calculated. • The intrinsic complex permeability and permittivity have been evaluated.

Electro-Optical Imaging Fourier-Transform Spectrometer

Science.gov (United States)

Chao, Tien-Hsin; Zhou, Hanying

2006-01-01

An electro-optical (E-O) imaging Fourier-transform spectrometer (IFTS), now under development, is a prototype of improved imaging spectrometers to be used for hyperspectral imaging, especially in the infrared spectral region. Unlike both imaging and non-imaging traditional Fourier-transform spectrometers, the E-O IFTS does not contain any moving parts. Elimination of the moving parts and the associated actuator mechanisms and supporting structures would increase reliability while enabling reductions in size and mass, relative to traditional Fourier-transform spectrometers that offer equivalent capabilities. Elimination of moving parts would also eliminate the vibrations caused by the motions of those parts. Figure 1 schematically depicts a traditional Fourier-transform spectrometer, wherein a critical time delay is varied by translating one the mirrors of a Michelson interferometer. The time-dependent optical output is a periodic representation of the input spectrum. Data characterizing the input spectrum are generated through fast-Fourier-transform (FFT) post-processing of the output in conjunction with the varying time delay.

The derivative-free Fourier shell identity for photoacoustics.

Science.gov (United States)

Baddour, Natalie

2016-01-01

In X-ray tomography, the Fourier slice theorem provides a relationship between the Fourier components of the object being imaged and the measured projection data. The Fourier slice theorem is the basis for X-ray Fourier-based tomographic inversion techniques. A similar relationship, referred to as the 'Fourier shell identity' has been previously derived for photoacoustic applications. However, this identity relates the pressure wavefield data function and its normal derivative measured on an arbitrary enclosing aperture to the three-dimensional Fourier transform of the enclosed object evaluated on a sphere. Since the normal derivative of pressure is not normally measured, the applicability of the formulation is limited in this form. In this paper, alternative derivations of the Fourier shell identity in 1D, 2D polar and 3D spherical polar coordinates are presented. The presented formulations do not require the normal derivative of pressure, thereby lending the formulas directly adaptable for Fourier based absorber reconstructions.

Advances in microwaves 3

CERN Document Server

Young, Leo

2013-01-01

Advances in Microwaves, Volume 3 covers the advances and applications of microwave signal transmission and Gunn devices. This volume contains six chapters and begins with descriptions of ground-station antennas for space communications. The succeeding chapters deal with beam waveguides, which offer interesting possibilities for transmitting microwave energy, as well as with parallel or tubular beams from antenna apertures. A chapter discusses the electron transfer mechanism and the velocity-field characteristics, with a particular emphasis on the microwave properties of Gunn oscillators. The l

Technical use of compact micro-onde devices

International Nuclear Information System (INIS)

Sortais, P.; Lamy, T.; Medard, J.; Angot, J.; Sudraud, P.; Salord, O.; Homri, S.

2012-01-01

Due to the very small size of a COMIC (Compact MIcrowave and Coaxial) device [P. Sortais, T. Lamy, J. Medard, J. Angot, L. Latrasse, and T. Thuillier, Rev. Sci. Instrum. 81, 02B31 (2010)] it is possible to install such plasma or ion source inside very different technical environments. New applications of such a device are presented, mainly for industrial applications. We have now designed ion sources for highly focused ion beam devices, ion beam machining ion guns, or thin film deposition machines. We will mainly present new capabilities opened by the use of a multi-beam system for thin film deposition based on sputtering by medium energy ion beams. With the new concept of multi-beam sputtering (MBS), it is possible to open new possibilities concerning the ion beam sputtering (IBS) technology, especially for large size deposition of high uniformity thin films. By the use of multi-spots of evaporation, each one corresponding to an independent tuning of an individual COMIC ion source, it will be very easy to co-evaporate different components.

Technical use of compact micro-onde devices

Energy Technology Data Exchange (ETDEWEB)

Sortais, P.; Lamy, T.; Medard, J.; Angot, J. [Laboratoire de Physique Subatomique et de Cosmologie de Grenoble - UJF-CNRS/IN2P3 - INPG, 53, rue des Martyrs, 38026 Grenoble Cedex (France); Sudraud, P.; Salord, O.; Homri, S. [Orsay Physics S.A., 95 avenue des Monts Aureliens, F-13710 Fuveau (France)

2012-02-15

Due to the very small size of a COMIC (Compact MIcrowave and Coaxial) device [P. Sortais, T. Lamy, J. Medard, J. Angot, L. Latrasse, and T. Thuillier, Rev. Sci. Instrum. 81, 02B31 (2010)] it is possible to install such plasma or ion source inside very different technical environments. New applications of such a device are presented, mainly for industrial applications. We have now designed ion sources for highly focused ion beam devices, ion beam machining ion guns, or thin film deposition machines. We will mainly present new capabilities opened by the use of a multi-beam system for thin film deposition based on sputtering by medium energy ion beams. With the new concept of multi-beam sputtering (MBS), it is possible to open new possibilities concerning the ion beam sputtering (IBS) technology, especially for large size deposition of high uniformity thin films. By the use of multi-spots of evaporation, each one corresponding to an independent tuning of an individual COMIC ion source, it will be very easy to co-evaporate different components.

Implementation of quantum and classical discrete fractional Fourier transforms

Science.gov (United States)

Weimann, Steffen; Perez-Leija, Armando; Lebugle, Maxime; Keil, Robert; Tichy, Malte; Gräfe, Markus; Heilmann, René; Nolte, Stefan; Moya-Cessa, Hector; Weihs, Gregor; Christodoulides, Demetrios N.; Szameit, Alexander

2016-01-01

Fourier transforms, integer and fractional, are ubiquitous mathematical tools in basic and applied science. Certainly, since the ordinary Fourier transform is merely a particular case of a continuous set of fractional Fourier domains, every property and application of the ordinary Fourier transform becomes a special case of the fractional Fourier transform. Despite the great practical importance of the discrete Fourier transform, implementation of fractional orders of the corresponding discrete operation has been elusive. Here we report classical and quantum optical realizations of the discrete fractional Fourier transform. In the context of classical optics, we implement discrete fractional Fourier transforms of exemplary wave functions and experimentally demonstrate the shift theorem. Moreover, we apply this approach in the quantum realm to Fourier transform separable and path-entangled biphoton wave functions. The proposed approach is versatile and could find applications in various fields where Fourier transforms are essential tools. PMID:27006089

Implementation of quantum and classical discrete fractional Fourier transforms.

Science.gov (United States)

Weimann, Steffen; Perez-Leija, Armando; Lebugle, Maxime; Keil, Robert; Tichy, Malte; Gräfe, Markus; Heilmann, René; Nolte, Stefan; Moya-Cessa, Hector; Weihs, Gregor; Christodoulides, Demetrios N; Szameit, Alexander

2016-03-23

Fourier transforms, integer and fractional, are ubiquitous mathematical tools in basic and applied science. Certainly, since the ordinary Fourier transform is merely a particular case of a continuous set of fractional Fourier domains, every property and application of the ordinary Fourier transform becomes a special case of the fractional Fourier transform. Despite the great practical importance of the discrete Fourier transform, implementation of fractional orders of the corresponding discrete operation has been elusive. Here we report classical and quantum optical realizations of the discrete fractional Fourier transform. In the context of classical optics, we implement discrete fractional Fourier transforms of exemplary wave functions and experimentally demonstrate the shift theorem. Moreover, we apply this approach in the quantum realm to Fourier transform separable and path-entangled biphoton wave functions. The proposed approach is versatile and could find applications in various fields where Fourier transforms are essential tools.

An optical Fourier transform coprocessor with direct phase determination.

Science.gov (United States)

Macfaden, Alexander J; Gordon, George S D; Wilkinson, Timothy D

2017-10-20

The Fourier transform is a ubiquitous mathematical operation which arises naturally in optics. We propose and demonstrate a practical method to optically evaluate a complex-to-complex discrete Fourier transform. By implementing the Fourier transform optically we can overcome the limiting O(nlogn) complexity of fast Fourier transform algorithms. Efficiently extracting the phase from the well-known optical Fourier transform is challenging. By appropriately decomposing the input and exploiting symmetries of the Fourier transform we are able to determine the phase directly from straightforward intensity measurements, creating an optical Fourier transform with O(n) apparent complexity. Performing larger optical Fourier transforms requires higher resolution spatial light modulators, but the execution time remains unchanged. This method could unlock the potential of the optical Fourier transform to permit 2D complex-to-complex discrete Fourier transforms with a performance that is currently untenable, with applications across information processing and computational physics.

Microwave heating processes involving carbon materials

Energy Technology Data Exchange (ETDEWEB)

Menendez, J.A.; Arenillas, A.; Fidalgo, B.; Fernandez, Y.; Zubizarreta, L.; Calvo, E.G.; Bermudez, J.M. [Instituto Nacional del Carbon, CSIC, Apartado 73, 33080 Oviedo (Spain)

2010-01-15

Carbon materials are, in general, very good absorbents of microwaves, i.e., they are easily heated by microwave radiation. This characteristic allows them to be transformed by microwave heating, giving rise to new carbons with tailored properties, to be used as microwave receptors, in order to heat other materials indirectly, or to act as a catalyst and microwave receptor in different heterogeneous reactions. In recent years, the number of processes that combine the use of carbons and microwave heating instead of other methods based on conventional heating has increased. In this paper some of the microwave-assisted processes in which carbon materials are produced, transformed or used in thermal treatments (generally, as microwave absorbers and catalysts) are reviewed and the main achievements of this technique are compared with those obtained by means of conventional (non microwave-assisted) methods in similar conditions. (author)

Reducing aberration effect of Fourier transform lens by modifying Fourier spectrum of diffractive optical element in beam shaping optical system.

Science.gov (United States)

Zhang, Fang; Zhu, Jing; Song, Qiang; Yue, Weirui; Liu, Jingdan; Wang, Jian; Situ, Guohai; Huang, Huijie

2015-10-20

In general, Fourier transform lenses are considered as ideal in the design algorithms of diffractive optical elements (DOEs). However, the inherent aberrations of a real Fourier transform lens disturb the far field pattern. The difference between the generated pattern and the expected design will impact the system performance. Therefore, a method for modifying the Fourier spectrum of DOEs without introducing other optical elements to reduce the aberration effect of the Fourier transform lens is proposed. By applying this method, beam shaping performance is improved markedly for the optical system with a real Fourier transform lens. The experiments carried out with a commercial Fourier transform lens give evidence for this method. The method is capable of reducing the system complexity as well as improving its performance.

Generalized fiber Fourier optics.

Science.gov (United States)

Cincotti, Gabriella

2011-06-15

A twofold generalization of the optical schemes that perform the discrete Fourier transform (DFT) is given: new passive planar architectures are presented where the 2 × 2 3 dB couplers are replaced by M × M hybrids, reducing the number of required connections and phase shifters. Furthermore, the planar implementation of the discrete fractional Fourier transform (DFrFT) is also described, with a waveguide grating router (WGR) configuration and a properly modified slab coupler.

Handbook of Fourier analysis & its applications

CERN Document Server

Marks, Robert J

2009-01-01

Fourier analysis has many scientific applications - in physics, number theory, combinatorics, signal processing, probability theory, statistics, option pricing, cryptography, acoustics, oceanography, optics and diffraction, geometry, and other areas. In signal processing and related fields, Fourier analysis is typically thought of as decomposing a signal into its component frequencies and their amplitudes. This practical, applications-based professional handbook comprehensively covers the theory and applications of Fourier Analysis, spanning topics from engineering mathematics, signal process

Microwave Sensors for Breast Cancer Detection.

Science.gov (United States)

Wang, Lulu

2018-02-23

Breast cancer is the leading cause of death among females, early diagnostic methods with suitable treatments improve the 5-year survival rates significantly. Microwave breast imaging has been reported as the most potential to become the alternative or additional tool to the current gold standard X-ray mammography for detecting breast cancer. The microwave breast image quality is affected by the microwave sensor, sensor array, the number of sensors in the array and the size of the sensor. In fact, microwave sensor array and sensor play an important role in the microwave breast imaging system. Numerous microwave biosensors have been developed for biomedical applications, with particular focus on breast tumor detection. Compared to the conventional medical imaging and biosensor techniques, these microwave sensors not only enable better cancer detection and improve the image resolution, but also provide attractive features such as label-free detection. This paper aims to provide an overview of recent important achievements in microwave sensors for biomedical imaging applications, with particular focus on breast cancer detection. The electric properties of biological tissues at microwave spectrum, microwave imaging approaches, microwave biosensors, current challenges and future works are also discussed in the manuscript.

Applications of Fourier transforms to generalized functions

CERN Document Server

Rahman, M

2011-01-01

This book explains how Fourier transforms can be applied to generalized functions. The generalized function is one of the important branches of mathematics and is applicable in many practical fields. Its applications to the theory of distribution and signal processing are especially important. The Fourier transform is a mathematical procedure that can be thought of as transforming a function from its time domain to the frequency domain.The book contains six chapters and three appendices. Chapter 1 deals with preliminary remarks on Fourier series from a general point of view and also contains an introduction to the first generalized function. Chapter 2 is concerned with the generalized functions and their Fourier transforms. Chapter 3 contains the Fourier transforms of particular generalized functions. The author has stated and proved 18 formulas dealing with the Fourier transforms of generalized functions, and demonstrated some important problems of practical interest. Chapter 4 deals with the asymptotic esti...

Optimizing the conditions for the microwave-assisted direct liquefaction of Ulva prolifera for bio-oil production using response surface methodology

International Nuclear Information System (INIS)

Liu, Junhai; Zhuang, Yingbin; Li, Yan; Chen, Limei; Guo, Jingxue; Li, Demao; Ye, Naihao

2013-01-01

Microwave-assisted direct liquefaction (MADL) of Ulva prolifera was performed in ethylene glycol (EG) using sulfuric acid (H 2 SO 4 ) as a catalyst. Response Surface Methodology (RSM) based on central composite rotatable design (CCRD) was employed to optimize the conditions of three independent variables (catalyst content, solvent-to-feedstock ratio and temperature) for the liquefaction yield. And the bio-oil was analyzed by elementary analysis, Fourier transform infrared spectroscopic analysis (FT-IR) and gas chromatography–mass spectrometry (GC–MS). The maximum liquefaction yield was 93.17%, which was obtained under a microwave power of 600 W for 30 min at 165 °C with a solvent-to-feedstock ratio of 18.87:1 and 4.93% sulfuric acid. The bio-oil was mainly composed of phthalic acid esters, alkenes and a fatty acid methyl ester with a long chain from C 16 to C 20 . - Highlights: • Ulva prolifera was converted to bio-oil through microwave-assisted direct liquefaction. • Response surface methodology was used to optimize the liquefaction technology. • A maximum liquefaction rate of 93.17 wt% bio-oil was obtained. • The bio-oil was composed of carboxylic acids and esters

The influence of microwave irradiation on rocks for microwave-assisted underground excavation

Directory of Open Access Journals (Sweden)

Ferri Hassani

2016-02-01

Full Text Available Demand is growing for explosive-free rock breakage systems for civil and mining engineering, and space industry applications. This paper highlights the work being undertaken in the Geomechanics Laboratory of McGill University to make a real application of microwave-assisted mechanical rock breakage to full-face tunneling machines and drilling. Comprehensive laboratory tests investigated the effect of microwave radiation on temperature profiles and strength reduction in hard rocks (norite, granite, and basalt for a range of exposure times and microwave power levels. The heating rate on the surface of the rock specimens linearly decreased with distance between the sample and the microwave antenna, regardless of microwave power level and exposure time. Tensile and uniaxial compressive strengths were reduced with increasing exposure time and power level. Scanning electron micrographs (SEMs highlighted fracture development in treated basalt. It was concluded that the microwave power level has a strong positive influence on the amount of heat damage induced to the rock surface. Numerical simulations of electric field intensity and wave propagation conducted with COMSOL Multiphysics® software generated temperature profiles that were in close agreement with experimental results.

Synthesis of nano-hydroxyapatite (nHA) from waste mussel shells using a rapid microwave method

Energy Technology Data Exchange (ETDEWEB)

Shavandi, Amin, E-mail: amin.shavandi@postgrad.otago.ac.nz [Department of Food Sciences, University of Otago, Dunedin (New Zealand); Bekhit, Alaa El-Din A. [Department of Food Sciences, University of Otago, Dunedin (New Zealand); Ali, Azam [Department of Applied Sciences, University of Otago, Dunedin (New Zealand); Sun, Zhifa [Department of Physics, University of Otago, Dunedin (New Zealand)

2015-01-15

Nano-crystalline hydroxyapatite (HA, Ca{sub 10}(PO{sub 4}){sub 6}(OH){sub 2}) was produced from waste mussel shells using a rapid microwave irradiation method. Mussel shells were converted to rod like nano-crystalline HA particles of 30–70 nm long using 0.1 M EDTA as a chelating agent for 30 min after an appropriate pre-treatment and an irradiation step in a microwave with a power of 1.1 kW. The produced HA was characterised using X-ray diffraction (XRD), scanning electron microscopy (SEM) coupled with energy-dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM), thermo gravimetric analysis (TGA), Fourier transform infrared spectroscopy (FT-IR) and inductively coupled plasma mass spectrometry (ICP-MS) to determine the morphology, particle size, crystal phases, elemental composition and thermal behaviour. Furthermore, to benchmark the synthesized HA obtained from mussel shells, it was compared with a commercially pure HA (Sigma–Aldrich). The thermal analysis showed that the synthesized HA has remarkable heat stability at 1000 °C, and the XRD and FTIR results showed a high purity of the synthesized HA powders. Compared to the conventional hydrothermal treatment, microwave-assisted method has the advantages of an increased rate of HA formation. The obtained HA have potential engineering applications as materials for bone-tissues. - Highlights: • Waste mussel shells were successfully converted to nano sized hydroxyapatite. • Microwave-assisted technique accelerated the conversion process. • The physicochemical properties of the produced hydroxyapatite are reported. • The prepared hydroxyapatite has nano sized particles of less than 100 nm.

Microwave, sonochemical and combustion synthesized CuO nanostructures and their electrical and bactericidal properties

International Nuclear Information System (INIS)

Karunakaran, C.; Manikandan, G.; Gomathisankar, P.

2013-01-01

Highlights: •CuO nanoleaves synthesized by CTAB-assisted hydrothermal method. •CuO nanodiscs synthesized by CTAB-assisted sonochemical method. •Combustion synthesized CuO is highly porous. •Synthetic method and morphology influence CuO bactericidal activity. -- Abstract: Cetyltrimethylammonium bromide (CTAB)-assisted microwave synthesis of CuO provides nanoleaves and in the absence of CTAB the shape of CuO is irregular. Sonochemical synthesis of CuO using CTAB gives nanodiscs whereas irregularly shaped flake-like structure is obtained without CTAB. Combustion synthesized CuO is highly porous with innumerable large holes. CTAB does not provide any structure in combustion synthesis. Transmission electron micrographs (TEM) display the constituent nanoparticles of microwave and sonochemically synthesized CuO. The powder X-ray diffractogram (XRD) shows the sample obtained by sonochemical method in the absence of CTAB as a mixture of monoclinic CuO, cubic Cu 2 O, and orthorhombic Cu(OH) 2 . But the rest of the samples are pure CuO in monoclinic phase. The selected area electron diffractograms (SAED) of the microwave and sonochemically synthesized samples, in the presence as well as in the absence of CTAB, confirm the monoclinic phase of CuO and indicates the presence of amorphous CuO in traces. All the samples are characteristic of Fourier Transform infrared (FT-IR) Cu–O stretching frequencies. The method of synthesis and also the morphology influence the electrical properties as well as the bactericidal activity of CuO

[Study on friction and wear properties of dental zirconia ceramics processed by microwave and conventional sintering methods].

Science.gov (United States)

Guoxin, Hu; Ying, Yang; Yuemei, Jiang; Wenjing, Xia

2017-04-01

This study evaluated the wear of an antagonist and friction and wear properties of dental zirconia ceramic that was subjected to microwave and conventional sintering methods. Ten specimens were fabricated from Lava brand zirconia and randomly assigned to microwave and conventional sintering groups. A profile tester for surface roughness was used to measure roughness of the specimens. Wear test was performed, and steatite ceramic was used as antagonist. Friction coefficient curves were recorded, and wear volume were calculated. Finally, optical microscope was used to observe the surface morphology of zirconia and steatite ceramics. Field emission scanning electron microscopy was used to observe the microstructure of zirconia. Wear volumes of microwave and conventionally sintered zirconia were (6.940±1.382)×10⁻², (7.952±1.815) ×10⁻² mm³, respectively. Moreover, wear volumes of antagonist after sintering by the considered methods were (14.189±4.745)×10⁻², (15.813±3.481)×10⁻² mm³, correspondingly. Statistically significant difference was not observed in the wear resistance of zirconia and wear volume of steatite ceramic upon exposure to two kinds of sintering methods. Optical microscopy showed that ploughed surfaces were apparent in zirconia. The wear surface of steatite ceramic against had craze, accompanied by plough. Scanning electron microscopy showed that zirconia was sintered compactly when subjected to both conventional sintering and microwave methods, whereas grains of zirconia sintered by microwave alone were smaller and more uniform. Two kinds of sintering methods are successfully used to produce dental zirconia ceramics with similar friction and wear properties.
.

Non-equilibrium Microwave Plasma for Efficient High Temperature Chemistry.

Science.gov (United States)

van den Bekerom, Dirk; den Harder, Niek; Minea, Teofil; Gatti, Nicola; Linares, Jose Palomares; Bongers, Waldo; van de Sanden, Richard; van Rooij, Gerard

2017-08-01

A flowing microwave plasma based methodology for converting electric energy into internal and/or translational modes of stable molecules with the purpose of efficiently driving non-equilibrium chemistry is discussed. The advantage of a flowing plasma reactor is that continuous chemical processes can be driven with the flexibility of startup times in the seconds timescale. The plasma approach is generically suitable for conversion/activation of stable molecules such as CO2, N2 and CH4. Here the reduction of CO2 to CO is used as a model system: the complementary diagnostics illustrate how a baseline thermodynamic equilibrium conversion can be exceeded by the intrinsic non-equilibrium from high vibrational excitation. Laser (Rayleigh) scattering is used to measure the reactor temperature and Fourier Transform Infrared Spectroscopy (FTIR) to characterize in situ internal (vibrational) excitation as well as the effluent composition to monitor conversion and selectivity.

Fourier Series

Indian Academy of Sciences (India)

The theory of Fourier series deals with periodic functions. By a periodic ..... including Dirichlet, Riemann and Cantor occupied themselves with the problem of ... to converge only on a set which is negligible in a certain sense (Le. of measure ...

Thermoactivation of viruses by microwaves

Energy Technology Data Exchange (ETDEWEB)

Mahnel, H.; von Brodorotti, H.S.

1981-01-01

Eight different viruses, suspended in drinking water, were examined for their ability to be inactivated by microwaves from a microwave oven. Up to a virus content of 10/sup 5/ TCID/sub 50//ml inactivation was successful within a few minutes of microwave treatment and occurred in parallel to the heat stability of the viruses. Evidence for direct effects of microwaves on viruses could not be detected. 7 of the viruses studied were inactivated rapidly when temperatures of 50 to 65/sup 0/C under microwave treatment were reached in the flowing water, while a bovine parvovirus was only inactivated by temperatures above 90/sup 0/C. The advantages of a thermal virus-decontamination of fluids and material by microwaves are discussed.

Alternating multivariate trigonometric functions and corresponding Fourier transforms

International Nuclear Information System (INIS)

Klimyk, A U; Patera, J

2008-01-01

We define and study multivariate sine and cosine functions, symmetric with respect to the alternating group A n , which is a subgroup of the permutation (symmetric) group S n . These functions are eigenfunctions of the Laplace operator. They determine Fourier-type transforms. There exist three types of such transforms: expansions into corresponding sine-Fourier and cosine-Fourier series, integral sine-Fourier and cosine-Fourier transforms, and multivariate finite sine and cosine transforms. In all these transforms, alternating multivariate sine and cosine functions are used as a kernel

Fourier transform n.m.r. spectroscopy

International Nuclear Information System (INIS)

Shaw, D.

1976-01-01

This book is orientated to techniques rather than applications. The basic theory of n.m.r. is dealt with in a unified approach to the Fourier theory. The middle section of the book concentrates on the practical aspects of Fourier n.m.r., both instrumental and experimental. The final chapters briefly cover general application of n.m.r., but concentrate strongly on those areas where Fourier n.m.r. can give information which is not available by conventional techniques

Fourier transform n. m. r. spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Shaw, D [Varian Ltd., Walton (UK)

1976-01-01

This book is orientated to techniques rather than applications. The basic theory of n.m.r. is dealt with in a unified approach to the Fourier theory. The middle section of the book concentrates on the practical aspects of Fourier n.m.r., both instrumental and experimental. The final chapters briefly cover general application of n.m.r., but concentrate strongly on those areas where Fourier n.m.r. can give information which is not available by conventional techniques.

Properties of the distributional finite Fourier transform

OpenAIRE

Carmichael, Richard D.

2016-01-01

The analytic functions in tubes which obtain the distributional finite Fourier transform as boundary value are shown to have a strong boundedness property and to be recoverable as a Fourier-Laplace transform, a distributional finite Fourier transform, and as a Cauchy integral of a distribution associated with the boundary value.

Generalized Fourier transforms classes

DEFF Research Database (Denmark)

Berntsen, Svend; Møller, Steen

2002-01-01

The Fourier class of integral transforms with kernels $B(\\omega r)$ has by definition inverse transforms with kernel $B(-\\omega r)$. The space of such transforms is explicitly constructed. A slightly more general class of generalized Fourier transforms are introduced. From the general theory foll...... follows that integral transform with kernels which are products of a Bessel and a Hankel function or which is of a certain general hypergeometric type have inverse transforms of the same structure....

Microwave. Instructor's Edition. Louisiana Vocational-Technical Education.

Science.gov (United States)

Blanton, William

This publication contains related study assignments and job sheets for a course in microwave technology. The course is organized into 12 units covering the following topics: introduction to microwave, microwave systems, microwave oscillators, microwave modulators, microwave transmission lines, transmission lines, detectors and mixers, microwave…

Advances in microwaves

CERN Document Server

Young, Leo

1967-01-01

Advances in Microwaves, Volume 2 focuses on the developments in microwave solid-state devices and circuits. This volume contains six chapters that also describe the design and applications of diplexers and multiplexers. The first chapter deals with the parameters of the tunnel diode, oscillators, amplifiers and frequency converter, followed by a simple physical description and the basic operating principles of the solid state devices currently capable of generating coherent microwave power, including transistors, harmonic generators, and tunnel, avalanche transit time, and diodes. The next ch

Characterization of microwave plasma in a multicusp using 2D emission based tomography: Bessel modes and wave absorption

Science.gov (United States)

Rathore, Kavita; Bhattacharjee, Sudeep; Munshi, Prabhat

2017-06-01

A tomographic method based on the Fourier transform is used for characterizing a microwave plasma in a multicusp (MC), in order to obtain 2D distribution of plasma emissions, plasma (electron) density (Ne) and temperature (Te). The microwave plasma in the MC is characterized as a function of microwave power, gas pressure, and axial distance. The experimentally obtained 2D emission profiles show that the plasma emissions are generated in a circular ring shape. There are usually two bright rings, one at the plasma core and another near the boundary. The experimental results are validated using a numerical code that solves Maxwell's equations inside a waveguide filled with a plasma in a magnetic field, with collisions included. It is inferred that the dark and bright circular ring patterns are a result of superposition of Bessel modes (TE11 and TE21) of the wave electric field inside the plasma filled MC, which are in reasonable agreement with the plasma emission profiles. The tomographically obtained Ne and Te profiles indicate higher densities in the plasma core (˜1010 cm-3) and enhanced electron temperature in the ECR region (˜13 eV), which are in agreement with earlier results using a Langmuir probe and optical emission spectroscopy (OES) diagnostics.

Simulated experiment for elimination of chemical and biological warfare agents by making use of microwave plasma torch

International Nuclear Information System (INIS)

Hong, Yong C.; Kim, Jeong H.; Uhm, Han S.

2004-01-01

The threat of chemical and biological warfare agents in a domestic terrorist attack and in military conflict is increasing worldwide. Elimination and decontamination of chemical and biological warfare (CBW) agents are immediately required after such an attack. Simulated experiment for elimination of CBW agents by making use of atmospheric-pressure microwave plasma torches is carried out. Elimination of biological warfare agents indicated by the vitrification or burnout of sewage sludge powders and decomposition of toluene gas as a chemical agent stimulant are presented. A detailed characterization for the elimination of the simulant chemicals using Fourier transform infrared and gas chromatography is also presented

Simulated experiment for elimination of chemical and biological warfare agents by making use of microwave plasma torch

Science.gov (United States)

Hong, Yong C.; Kim, Jeong H.; Uhm, Han S.

2004-02-01

The threat of chemical and biological warfare agents in a domestic terrorist attack and in military conflict is increasing worldwide. Elimination and decontamination of chemical and biological warfare (CBW) agents are immediately required after such an attack. Simulated experiment for elimination of CBW agents by making use of atmospheric-pressure microwave plasma torches is carried out. Elimination of biological warfare agents indicated by the vitrification or burnout of sewage sludge powders and decomposition of toluene gas as a chemical agent stimulant are presented. A detailed characterization for the elimination of the simulant chemicals using Fourier transform infrared and gas chromatography is also presented.

Study on the synthesis and physicochemical properties of starch acetate with low substitution under microwave assistance.

Science.gov (United States)

Lin, Derong; Zhou, Wei; Zhao, Jingjing; Lan, Weijie; Chen, Rongming; Li, Yutong; Xing, Baoshan; Li, Zhuohao; Xiao, Mengshi; Wu, Zhijun; Li, Xindan; Chen, Rongna; Zhang, Xingwen; Chen, Hong; Zhang, Qing; Qin, Wen; Li, Suqing

2017-10-01

In this study, synthesis and physicochemical properties of starch acetate with low substitution under microwave were studied. A three-level-three-factorial Central Composite Design using Response Surface Methodology (RSM) was employed to optimize the reaction conditions. The optimal parameters are as follows: amount of acetic anhydride of 12%, radiation time of 11min, and microwave power of 100W. These optimal conditions predicted by RSM were confirmed that the degree of substitution (DS) of acetate starch is 0.0691mg/g and the physical and chemical properties of natural corn starch (NCS) and corn starch acetate (ACS) were further studied.The transparency, water separation, water absorption, expansion force, and solubility of ACS low substitution are better than NCS, while the NCS's hydrolysis percentage is higher than ACS, which indicate that the modified corn starch has better performance than native corn starch. The surface morphology of the corn starch acetate was examined by scanning electron microscope (SEM), which showed that it had a smooth surface and a spherical and polygonal shape. However, samples' shape is irregular. Crystal structure was observed by X-ray diffraction, and the ACS can determine the level of microwave technology that can destroy the extent of the crystal and amorphous regions. Fourier transform infrared (FTIR) spectroscopy shows that around 1750cm -1 carbonyl signal determines acetylation bonding successfully. Copyright © 2017 Elsevier B.V. All rights reserved.

Diffusion through statically compacted clay

International Nuclear Information System (INIS)

Ho, C.L.; Shebl, M.A.A.

1994-01-01

This paper presents experimental work on the effect of compaction on contaminant flow through clay liners. The experimental program included evaluation of soil properties, compaction, permeability and solute diffusion. A permeameter was built of non reactive materials to test samples compacted at different water contents and compactive efforts. The flow of a permeating solute, LiCl, was monitored. Effluent samples were collected for solute concentration measurements. The concentrations were measured by performing atomic adsorption tests. The analyzed results showed different diffusion characteristics when compaction conditions changed. At each compactive effort, permeability decreased as molding water content increased. Consequently, transit time (measured at relative concentration 50%) increased and diffusivity decreased. As compactive effort increased for soils compacted dry of optimum, permeability and diffusion decreased. On the other hand, as compactive effort increased for soils compacted wet of optimum, permeability and diffusivity increased. Tortuosity factor was indirectly measured from the diffusion and retardation rate. Tortuosity factor also decreased as placement water content was increased from dry of optimum to wet of optimum. Then decreases were more pronounced for low compactive effort tests. 27 refs., 7 figs., 5 tabs

Mapped Fourier Methods for stiff problems in toroidal geometry

OpenAIRE

Guillard , Herve

2014-01-01

Fourier spectral or pseudo-spectral methods are usually extremely efficient for periodic problems. However this efficiency is lost if the solutions have zones of rapid variations or internal layers. For these cases, a large number of Fourier modes are required and this makes the Fourier method unpractical in many cases. This work investigates the use of mapped Fourier method as a way to circumvent this problem. Mapped Fourier method uses instead of the usual Fourier interpolant the compositio...

Incubator embedded cell culture imaging system (EmSight) based on Fourier ptychographic microscopy.

Science.gov (United States)

Kim, Jinho; Henley, Beverley M; Kim, Charlene H; Lester, Henry A; Yang, Changhuei

2016-08-01

Multi-day tracking of cells in culture systems can provide valuable information in bioscience experiments. We report the development of a cell culture imaging system, named EmSight, which incorporates multiple compact Fourier ptychographic microscopes with a standard multiwell imaging plate. The system is housed in an incubator and presently incorporates six microscopes. By using the same low magnification objective lenses as the objective and the tube lens, the EmSight is configured as a 1:1 imaging system that, providing large field-of-view (FOV) imaging onto a low-cost CMOS imaging sensor. The EmSight improves the image resolution by capturing a series of images of the sample at varying illumination angles; the instrument reconstructs a higher-resolution image by using the iterative Fourier ptychographic algorithm. In addition to providing high-resolution brightfield and phase imaging, the EmSight is also capable of fluorescence imaging at the native resolution of the objectives. We characterized the system using a phase Siemens star target, and show four-fold improved coherent resolution (synthetic NA of 0.42) and a depth of field of 0.2 mm. To conduct live, long-term dopaminergic neuron imaging, we cultured ventral midbrain from mice driving eGFP from the tyrosine hydroxylase promoter. The EmSight system tracks movements of dopaminergic neurons over a 21 day period.

Self-Compacting Concrete

OpenAIRE

Okamura, Hajime; Ouchi, Masahiro

2003-01-01

Self-compacting concrete was first developed in 1988 to achieve durable concrete structures. Since then, various investigations have been carried out and this type of concrete has been used in practical structures in Japan, mainly by large construction companies. Investigations for establishing a rational mix-design method and self-compactability testing methods have been carried out from the viewpoint of making self-compacting concrete a standard concrete.

Preparation and Characterization of Liquisolid Compacts for Improved Dissolution of Telmisartan

Directory of Open Access Journals (Sweden)

Naveen Chella

2014-01-01

Full Text Available The objective of the present work was to obtain pH independent and improved dissolution profile for a poorly soluble drug, telmisartan using liquisolid compacts. Liquisolid compacts were prepared using Transcutol HP as vehicle, Avicel PH102 as carrier, and Aerosil 200 as a coating material. The formulations were evaluated for drug excipient interactions, change in crystallinity of drug, flow properties, and general quality control tests of tablets using Fourier transform infrared (FTIR spectroscopy, differential scanning calorimetry (DSC, X-ray diffraction (XRD, angle of repose, and various pharmacopoeial tests. In vitro dissolution studies were performed at three pH conditions (1.2, 4.5 and 7.4. Stability studies were performed at 40°C and 75% RH for three months. The formulation was found to comply with Indian pharmacopoeial limits for tablets. FTIR studies confirmed no interaction between drug and excipients. XRD and DSC studies indicate change/reduction in crystallinity of drug. Dissolution media were selected based on the solubility studies. The optimized formulation showed pH independent release profile with significant improvement P<0.005 in dissolution compared to plain drug and conventional marketed formulation. No significant difference was seen in the tablet properties, and drug release profile after storage for 3 months.

Synthesis, characterization of nickel aluminate nanoparticles by microwave combustion method and their catalytic properties

Energy Technology Data Exchange (ETDEWEB)

Ragupathi, C. [Catalysis and Nanomaterials Research Laboratory, Department of Chemistry, Loyola College (Autonomous), Chennai 600034 (India); Vijaya, J. Judith, E-mail: jjvijayaloyola@yahoo.co.in [Catalysis and Nanomaterials Research Laboratory, Department of Chemistry, Loyola College (Autonomous), Chennai 600034 (India); Kennedy, L. John [Materials Division, School of Advanced Sciences, Vellore Institute of Technology (VIT) University, Chennai Campus, Chennai 600127 (India)

2014-05-01

Highlights: • Simple route for the preparation of nickel aluminate. • NiAl{sub 2}O{sub 4} microwave absorbent was invented by a simple method. • High specific surface area was obtained at low temperature. • Evaluation of magnetic, optical and catalytic properties. - Abstract: Microwave combustion method (MCM) is a direct method to synthesize NiAl{sub 2}O{sub 4} nanoparticles and for the first time we report the using of Sesame (Sesame indicum L.) plant extract in the present study. Solutions of metal nitrates and plant extract as a gelling agent are subsequently combusted using microwave. The structure and morphology of NiAl{sub 2}O{sub 4} nanoparticles are investigated by X-ray diffraction (XRD), Fourier transforms infrared spectra (FT-IR), high resolution scanning electron microscopy (HR-SEM), energy dispersive X-ray analysis (EDX), high resolution transmission electron microscopy (HR-TEM), diffuse reflectance spectroscopy (DRS) and photoluminescence (PL) spectroscopy, Brunauer–Emmett–Teller (BET) analysis and vibrating sample magnetometer (VSM). XRD pattern confirmed the formation of cubic phase NiAl{sub 2}O{sub 4}. The formation of NiAl{sub 2}O{sub 4} is also confirmed by FT-IR. The formation of NiAl{sub 2}O{sub 4} nanoparticles is confirmed by HR-SEM and HR-TEM. Furthermore, the microwave combustion leads to the formation of fine particles with uniform morphology. The magnetic properties of the synthesized NiAl{sub 2}O{sub 4} nano and microstructures were investigated by vibrating sample magnetometer (VSM) and their hysteresis loops were obtained at room temperature. Further, NiAl{sub 2}O{sub 4} prepared by MCM using Sesame (S. indicum L.) plant extract is tested for the catalytic activity toward the oxidation of benzyl alcohol.

High yield and facile microwave-assisted synthesis of conductive H{sub 2}SO{sub 4} doped polyanilines

Energy Technology Data Exchange (ETDEWEB)

Gizdavic-Nikolaidis, Marija R., E-mail: m.gizdavic@auckland.ac.nz [School of Chemical Sciences, The University of Auckland, Private Bag 92019, Auckland Mail Centre, Auckland, 1142 (New Zealand); Faculty of Physical Chemistry, Studentski Trg 12-16, PO Box 137, 11001, Belgrade (Serbia); Jevremovic, Milutin M. [Public Company Nuclear Facilities of Serbia, 12-14 Mike Petrovica Alasa, Vinca, 11351, Belgrade (Serbia); Milenkovic, Maja [Faculty of Physical Chemistry, Studentski Trg 12-16, PO Box 137, 11001, Belgrade (Serbia); Allison, Morgan C. [School of Chemical Sciences, The University of Auckland, Private Bag 92019, Auckland Mail Centre, Auckland, 1142 (New Zealand); Stanisavljev, Dragomir R. [Faculty of Physical Chemistry, Studentski Trg 12-16, PO Box 137, 11001, Belgrade (Serbia); Bowmaker, Graham A. [School of Chemical Sciences, The University of Auckland, Private Bag 92019, Auckland Mail Centre, Auckland, 1142 (New Zealand); Zujovic, Zoran D. [School of Chemical Sciences, The University of Auckland, Private Bag 92019, Auckland Mail Centre, Auckland, 1142 (New Zealand); MacDiarmid Institute for Advanced Materials and Nanotechnology, Victoria University of Wellington, PO Box 600, Wellington, 6140 (New Zealand); Institute of General and Physical Chemistry, Studentski Trg 12-16, 11001, Belgrade (Serbia)

2016-04-15

The microwave-assisted synthesis of polyaniline (PANI) was performed using ammonium persulphate (APS) as oxidizing agent in 0.5 M–2.5 M concentration range of aqueous sulphuric acid (H{sub 2}SO{sub 4}) at 93 W applied microwave power of 10 min duration. The microwave (MW) synthesized PANIs had 3 times higher yield in comparison to PANI samples prepared using a classical method, CS (0 W MW power) at the same temperature for 10 min synthesis duration period. Fourier Transform Infrared (FTIR) and UV–Vis spectroscopies confirmed the formation of PANI structure in all products. The influence of H{sub 2}SO{sub 4} acid dopant on the spin concentration of MW and CS H{sub 2}SO{sub 4} doped PANI samples were examined by EPR spectroscopy, while the morphological characteristics were investigated by using scanning electron microscopy (SEM). XRD results showed amorphous phases in both MW and CS H{sub 2}SO{sub 4} doped PANI samples. Conductivity measurements revealed ∼1.5 times higher conductivity values for MW H{sub 2}SO{sub 4} doped PANI samples in comparison with PANI samples prepared by the CS method under same condition. The influence of sulfate anion in comparison to chloride anion as a dopant on morphological, dopant levels and conductivity properties of MW PANI samples were also investigated. - Highlights: • Nanoporous microwave synthesized doped polyanilines as chemical sensor material. • Morphology and physical properties of polyanilines depend on acid concentration. • Spin concentration is determined by the nature of the polyaniline synthesis.

Gold Nanoparticle Microwave Synthesis

Energy Technology Data Exchange (ETDEWEB)

Krantz, Kelsie E. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Christian, Jonathan H. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Coopersmith, Kaitlin [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Washington, II, Aaron L. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Murph, Simona H. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

2016-07-27

At the nanometer scale, numerous compounds display different properties than those found in bulk material that can prove useful in areas such as medicinal chemistry. Gold nanoparticles, for example, display promise in newly developed hyperthermia therapies for cancer treatment. Currently, gold nanoparticle synthesis is performed via the hot injection technique which has large variability in final particle size and a longer reaction time. One underdeveloped area by which these particles could be produced is through microwave synthesis. To initiate heating, microwaves agitate polar molecules creating a vibration that gives off the heat energy needed. Previous studies have used microwaves for gold nanoparticle synthesis; however, polar solvents were used that partially absorbed incident microwaves, leading to partial thermal heating of the sample rather than taking full advantage of the microwave to solely heat the gold nanoparticle precursors in a non-polar solution. Through this project, microwaves were utilized as the sole heat source, and non-polar solvents were used to explore the effects of microwave heating only as pertains to the precursor material. Our findings show that the use of non-polar solvents allows for more rapid heating as compared to polar solvents, and a reduction in reaction time from 10 minutes to 1 minute; this maximizes the efficiency of the reaction, and allows for reproducibility in the size/shape of the fabricated nanoparticles.

Gold Nanoparticle Microwave Synthesis

International Nuclear Information System (INIS)

Krantz, Kelsie E.; Christian, Jonathan H.; Coopersmith, Kaitlin; Washington II, Aaron L.; Murph, Simona H.

2016-01-01

At the nanometer scale, numerous compounds display different properties than those found in bulk material that can prove useful in areas such as medicinal chemistry. Gold nanoparticles, for example, display promise in newly developed hyperthermia therapies for cancer treatment. Currently, gold nanoparticle synthesis is performed via the hot injection technique which has large variability in final particle size and a longer reaction time. One underdeveloped area by which these particles could be produced is through microwave synthesis. To initiate heating, microwaves agitate polar molecules creating a vibration that gives off the heat energy needed. Previous studies have used microwaves for gold nanoparticle synthesis; however, polar solvents were used that partially absorbed incident microwaves, leading to partial thermal heating of the sample rather than taking full advantage of the microwave to solely heat the gold nanoparticle precursors in a non-polar solution. Through this project, microwaves were utilized as the sole heat source, and non-polar solvents were used to explore the effects of microwave heating only as pertains to the precursor material. Our findings show that the use of non-polar solvents allows for more rapid heating as compared to polar solvents, and a reduction in reaction time from 10 minutes to 1 minute; this maximizes the efficiency of the reaction, and allows for reproducibility in the size/shape of the fabricated nanoparticles.

Polyphase-discrete Fourier transform spectrum analysis for the Search for Extraterrestrial Intelligence sky survey

Science.gov (United States)

Zimmerman, G. A.; Gulkis, S.

1991-01-01

The sensitivity of a matched filter-detection system to a finite-duration continuous wave (CW) tone is compared with the sensitivities of a windowed discrete Fourier transform (DFT) system and an ideal bandpass filter-bank system. These comparisons are made in the context of the NASA Search for Extraterrestrial Intelligence (SETI) microwave observing project (MOP) sky survey. A review of the theory of polyphase-DFT filter banks and its relationship to the well-known windowed-DFT process is presented. The polyphase-DFT system approximates the ideal bandpass filter bank by using as few as eight filter taps per polyphase branch. An improvement in sensitivity of approx. 3 dB over a windowed-DFT system can be obtained by using the polyphase-DFT approach. Sidelobe rejection of the polyphase-DFT system is vastly superior to the windowed-DFT system, thereby improving its performance in the presence of radio frequency interference (RFI).

Non-self-sustained microwave discharge and the concept of a microwave air jet engine

International Nuclear Information System (INIS)

Batanov, G M; Gritsinin, S I; Kossyi, I A

2002-01-01

A new type of microwave discharge - near-surface non-self-sustained discharge (NSND) - has been realized and investigated. A physical model of this discharge is presented. For the first time NSND application for microwave air jet engines has been proposed. Measurements under laboratory conditions modelling the microwave air jet engine operation shows the qualitative agreement between the model of NSND and actual processes near the target irradiated by a powerful microwave beam. Characteristic dependences of recoil momentum of target on the background pressure and microwave pulse duration obtained in experiments are presented. Measured cost of thrust produced by the NSND is no more than 3.0 kW N -1 , which is close to the predicted values

Self-Fourier functions and coherent laser combination

International Nuclear Information System (INIS)

Corcoran, C J; Pasch, K A

2004-01-01

The Gaussian and Comb functions are generally quoted as being the two basic functions that are their own Fourier transforms. In 1991, Caola presented a recipe for generating functions that are their own Fourier transforms by symmetrizing any transformable function and then adding its own Fourier transform to it. In this letter, we present a new method for generating a set of functions that are exactly their own Fourier transforms, and which have direct application to laser cavity design for a wide variety of applications. The generated set includes the Gaussian and Comb functions as special cases and forms a continuous bridge of functions between them. The new generating method uses the Gaussian and Comb functions as bases and does not rely on the Fourier operator itself. This self-Fourier function promises to be particularly useful in high-power laser design through coherent laser beam combination. Although these results are presented in a single dimension as with a linear array, the results are equally valid in two dimensions. (letter to the editor)

Content adaptive illumination for Fourier ptychography.

Science.gov (United States)

Bian, Liheng; Suo, Jinli; Situ, Guohai; Zheng, Guoan; Chen, Feng; Dai, Qionghai

2014-12-01

Fourier ptychography (FP) is a recently reported technique, for large field-of-view and high-resolution imaging. Specifically, FP captures a set of low-resolution images, under angularly varying illuminations, and stitches them together in the Fourier domain. One of FP's main disadvantages is its long capturing process, due to the requisite large number of incident illumination angles. In this Letter, utilizing the sparsity of natural images in the Fourier domain, we propose a highly efficient method, termed adaptive Fourier ptychography (AFP), which applies content adaptive illumination for FP, to capture the most informative parts of the scene's spatial spectrum. We validate the effectiveness and efficiency of the reported framework, with both simulated and real experiments. Results show that the proposed AFP could shorten the acquisition time of conventional FP, by around 30%-60%.

Compaction of Ti–6Al–4V powder using high velocity compaction technique

International Nuclear Information System (INIS)

Khan, Dil Faraz; Yin, Haiqing; Li, He; Qu, Xuanhui; Khan, Matiullah; Ali, Shujaat; Iqbal, M. Zubair

2013-01-01

Highlights: • We compacted Ti–6Al–4V powder by HVC technique. • As impact force rises up, the green density of the compacts increases gradually. • At impact force 1.857 kN relative sintered density of the compacts reaches 99.88%. • Spring back of the green compact’s decreases gradually with increasing impact force. • Mechanical properties of the samples increases with increasing impact force. - Abstract: High velocity compaction technique was applied to the compaction of pre-alloyed, hydride–dehydride Ti–6Al–4V powder. The powder was pressed in single stroke with a compaction speed of 7.10–8.70 ms −1 . When the speed was 8.70 ms −1 , the relative density of the compacts reaches up to 85.89% with a green density of 3.831 g cm −3 . The green samples were sintered at 1300 °C in Ar-gas atmosphere. Scanning electron microscope (SEM) was used to examine the surface of the sintered samples. Density and mechanical properties such as Vickers micro hardness and bending strength of the powder samples were investigated. Experimental results indicated that with the increase in impact force, the density and mechanical properties of the compacts increased. The sintered compacts exhibited a maximum relative density of 99.88% with a sintered density of 4.415 g cm −3 , hardness of 364–483 HV and the bending strength in the range of 103–126.78 MPa. The springback of the compacts decreased with increasing impact force

Parameter prediction for microwave garnets

International Nuclear Information System (INIS)

Ramer, R.

1996-01-01

Full text: Linearity of the microwave parameters (resonance linewidth ΔH and effective linewidth ΔH eff ) is demonstrated and their use in the Computer-aided design (CAD)/Computer-aided manufacturing (CAM) of new microwave garnets is proposed. Such an approach would combine a numerical database of microwave data and several computational programs. The model is an applied formulation of the analysis of a wide range of microwave garnets

Sobolev Spaces on Locally Compact Abelian Groups: Compact Embeddings and Local Spaces

Directory of Open Access Journals (Sweden)

Przemysław Górka

2014-01-01

Full Text Available We continue our research on Sobolev spaces on locally compact abelian (LCA groups motivated by our work on equations with infinitely many derivatives of interest for string theory and cosmology. In this paper, we focus on compact embedding results and we prove an analog for LCA groups of the classical Rellich lemma and of the Rellich-Kondrachov compactness theorem. Furthermore, we introduce Sobolev spaces on subsets of LCA groups and study its main properties, including the existence of compact embeddings into Lp-spaces.

(Anti)symmetric multivariate exponential functions and corresponding Fourier transforms

International Nuclear Information System (INIS)

Klimyk, A U; Patera, J

2007-01-01

We define and study symmetrized and antisymmetrized multivariate exponential functions. They are defined as determinants and antideterminants of matrices whose entries are exponential functions of one variable. These functions are eigenfunctions of the Laplace operator on the corresponding fundamental domains satisfying certain boundary conditions. To symmetric and antisymmetric multivariate exponential functions there correspond Fourier transforms. There are three types of such Fourier transforms: expansions into the corresponding Fourier series, integral Fourier transforms and multivariate finite Fourier transforms. Eigenfunctions of the integral Fourier transforms are found

Stabilization of compactible waste

International Nuclear Information System (INIS)

Franz, E.M.; Heiser, J.H. III; Colombo, P.

1990-09-01

This report summarizes the results of series of experiments performed to determine the feasibility of stabilizing compacted or compactible waste with polymers. The need for this work arose from problems encountered at disposal sites attributed to the instability of this waste in disposal. These studies are part of an experimental program conducted at Brookhaven National Laboratory (BNL) investigating methods for the improved solidification/stabilization of DOE low-level wastes. The approach taken in this study was to perform a series of survey type experiments using various polymerization systems to find the most economical and practical method for further in-depth studies. Compactible dry bulk waste was stabilized with two different monomer systems: styrene-trimethylolpropane trimethacrylate (TMPTMA) and polyester-styrene, in laboratory-scale experiments. Stabilization was accomplished by wetting or soaking compactible waste (before or after compaction) with monomers, which were subsequently polymerized. Three stabilization methods are described. One involves the in-situ treatment of compacted waste with monomers in which a vacuum technique is used to introduce the binder into the waste. The second method involves the alternate placement and compaction of waste and binder into a disposal container. In the third method, the waste is treated before compaction by wetting the waste with the binder using a spraying technique. A series of samples stabilized at various binder-to-waste ratios were evaluated through water immersion and compression testing. Full-scale studies were conducted by stabilizing two 55-gallon drums of real compacted waste. The results of this preliminary study indicate that the integrity of compacted waste forms can be readily improved to ensure their long-term durability in disposal environments. 9 refs., 10 figs., 2 tabs

A study on microwave oxidation of landfill leachate—Contributions of microwave-specific effects

International Nuclear Information System (INIS)

Chou, Yu-Chieh; Lo, Shang-Lien; Kuo, Jeff; Yeh, Chih-Jung

2013-01-01

Highlights: ► pH has an insignificant effect on TOC removals and 550 W has a well performance. ► MOP has well removals of color, UV 254 , and TOC at 550 W/85 °C. ► TOC removals were higher at higher microwave setting (550 W vs. 128 W). ► The microwave-specific effects on TOC removal were usually synergistic in MOP. ► COD analyses showed persulfate decayed rapidly in either MOP or CHO treatment. -- Abstract: Microwave oxidation process (MOP) was evaluated for treatment of landfill leachate. The experimental parameters include pH, temperature, oxidant doses, microwave power setting, and irradiation time. The study explored the microwave-specific effects of the MOP. The contributions of pure thermal, persulfate oxidation and microwave irradiation on TOC removal were quantified. It was then found the combinations of them were usually synergistic in MOP except two of them were antagonistic (128 W/85 °C/1 M Na 2 S 2 O 8 and 128 W/85 °C/2 M Na 2 S 2 O 8 ). At the highest temperature tested (85 °C) in this study, microwave irradiation may cause generation and termination of oxidizing radicals at adverse rates. The study also found that persulfate decayed rapidly in either MOP or conventional heating oxidation (CHO) treatment of landfill leachate

Micro-Spec: A High Performance Compact Spectrometer for Submillimeter Astronomy

Science.gov (United States)

Hsieh, Wen-Ting; Moseley, Harvey; Stevenson, Thomas; Brown, Ari; Patel, Amil; U-Yen, Kongpop; Ehsan, Negar; Caltado, Giuseppe; Wollock, Edward

2012-01-01

We describe the micro-Spec, an extremely compact high performance spectrometer for the submillimeter and millimeter spectral ranges. We have designed a fully integrated submillimeter spectrometer based on superconducting microstrip technology and fabricated its critical elements. Using low loss transmission lines, we can produce a fully integrated high resolution submillimeter spectrometer on a single four inch Si wafer. A resolution of 500 can readily be achieved with standard fabrication tolerance, higher with phase trimming. All functions of the spectrometer are integrated - light is coupled to the micro strip circuit with a planar antenna, the spectra discrimination is achieved using a synthetic grating, orders are separated using a built-in planar filter, and the light is detected using photon counting Microwave Kinetic Inductance Detectors (MKID). We will discus the design principle of the instrument, describe its technical advantages, and report the progress on the development of the instrument.

Mu-Spec: A High Performance Compact Spectrometer for Submillimeter Astronomy

Science.gov (United States)

Hsieh, Wen-Ting; Moseley, Harvey; Stevenson, Thomas; Brown, Ari; Patel, Amil; U-yen, Kongpop; Ehsan, Negar; Cataldo, Giuseppe; Wollack, Ed

2012-01-01

We describe the Mu-Spec, an extremely compact high performance spectrometer for the submillimeter and millimeter spectral ranges. We have designed a fully integrated submillimeter spectrometer based on superconducting microstrip technology and fabricated its critical elements. Using low loss transmission lines, we can produce a fully integrated high resolution submillimeter spectrometer on a single four inch Si wafer. A resolution of 500 can readily be achieved with standard fabrication tolerance, higher with phase trimming. All functions of the spectrometer are integrated - light is coupled to the microstrip circuit with a planar antenna, the spectra discrimination is achieved using a synthetic grating, orders are separated using a built-in planar filter, and the light is detected using photon counting Microwave Kinetic Inductance Detectors (MKID). We will discus the design principle of the instrument, describe its technical advantages, and report the progress on the development of the instrument.

Non-Ionizing Radiation Used in Microwave Ovens

Science.gov (United States)

... Non-Ionizing Radiation Used in Microwave Ovens Non-Ionizing Radiation Used in Microwave Ovens Explore the interactive, virtual ... can do Where to learn more About Non-Ionizing Radiation Used in Microwave Ovens Microwave Oven. Microwave ovens ...

Modeling microwave/electron-cloud interaction

International Nuclear Information System (INIS)

Mattes, M; Sorolla, E; Zimmermann, F

2013-01-01

Starting from the separate codes BI-RME and ECLOUD or PyECLOUD, we are developing a novel joint simulation tool, which models the combined effect of a charged particle beam and of microwaves on an electron cloud. Possible applications include the degradation of microwave transmission in telecommunication satellites by electron clouds; the microwave-transmission techniques being used in particle accelerators for the purpose of electroncloud diagnostics; the microwave emission by the electron cloud itself in the presence of a magnetic field; and the possible suppression of electron-cloud formation in an accelerator by injecting microwaves of suitable amplitude and frequency. A few early simulation results are presented. (author)

Fourier phasing with phase-uncertain mask

International Nuclear Information System (INIS)

Fannjiang, Albert; Liao, Wenjing

2013-01-01

Fourier phasing is the problem of retrieving Fourier phase information from Fourier intensity data. The standard Fourier phase retrieval (without a mask) is known to have many solutions which cause the standard phasing algorithms to stagnate and produce wrong or inaccurate solutions. In this paper Fourier phase retrieval is carried out with the introduction of a randomly fabricated mask in measurement and reconstruction. Highly probable uniqueness of solution, up to a global phase, was previously proved with exact knowledge of the mask. Here the uniqueness result is extended to the case where only rough information about the mask’s phases is assumed. The exponential probability bound for uniqueness is given in terms of the uncertainty-to-diversity ratio of the unknown mask. New phasing algorithms alternating between the object update and the mask update are systematically tested and demonstrated to have the capability of recovering both the object and the mask (within the object support) simultaneously, consistent with the uniqueness result. Phasing with a phase-uncertain mask is shown to be robust with respect to the correlation in the mask as well as the Gaussian and Poisson noises. (paper)

Effects of lignocellulosic composition and microwave power level on the gaseous product of microwave pyrolysis

International Nuclear Information System (INIS)

Huang, Yu-Fong; Chiueh, Pei-Te; Kuan, Wen-Hui; Lo, Shang-Lien

2015-01-01

Agricultural residues are abundant resources to produce renewable energy and valuable chemicals. This study focused on the effects of lignocellulosic composition and microwave power level on the gaseous product of microwave pyrolysis of agricultural residues. When agricultural residues were under microwave radiation within 10 min, the maximum temperatures of approximately 320, 420, and 530 °C were achieved at the microwave power levels of 300, 400, and 500 W, respectively. Gas yield increased with increasing microwave power level, whereas solid and liquid yields decreased. Besides, gaseous products with higher H 2 content and higher calorific values can be obtained at higher microwave power levels. In addition to microwave power level, lignocellulosic composition was also an important factor. H 2 and CO 2 yields increased with increasing hemicellulose content, whereas CH 4 and CO yields increased with increasing cellulose content. Four empirical equations were derived to present the contributions of lignocellulosic materials to the yields of gaseous components. - Highlights: • About 530 °C was reached within 10 min at a microwave power level of 500 W. • Gas yield increased with increasing microwave power level. • A high correlation between hemicellulose content and either H 2 or CO 2 yield. • A high correlation between cellulose content and either CH 4 or CO yield. • Empirical equations depict contribution of lignocellulosic content to gas yield

Phase-coded microwave signal generation based on a single electro-optical modulator and its application in accurate distance measurement.

Science.gov (United States)

Zhang, Fangzheng; Ge, Xiaozhong; Gao, Bindong; Pan, Shilong

2015-08-24

A novel scheme for photonic generation of a phase-coded microwave signal is proposed and its application in one-dimension distance measurement is demonstrated. The proposed signal generator has a simple and compact structure based on a single dual-polarization modulator. Besides, the generated phase-coded signal is stable and free from the DC and low-frequency backgrounds. An experiment is carried out. A 2 Gb/s phase-coded signal at 20 GHz is successfully generated, and the recovered phase information agrees well with the input 13-bit Barker code. To further investigate the performance of the proposed signal generator, its application in one-dimension distance measurement is demonstrated. The measurement accuracy is less than 1.7 centimeters within a measurement range of ~2 meters. The experimental results can verify the feasibility of the proposed phase-coded microwave signal generator and also provide strong evidence to support its practical applications.

Group-invariant finite Fourier transforms

International Nuclear Information System (INIS)

Shenefelt, M.H.

1988-01-01

The computation of the finite Fourier transform of functions is one of the most used computations in crystallography. Since the Fourier transform involved in 3-dimensional, the size of the computation becomes very large even for relatively few sample points along each edge. In this thesis, there is a family of algorithms that reduce the computation of Fourier transform of functions respecting the symmetries. Some properties of these algorithms are: (1) The algorithms make full use of the group of symmetries of a crystal. (2) The algorithms can be factored and combined according to the prime factorization of the number of points in the sample space. (3) The algorithms are organized into a family using the group structure of the crystallographic groups to make iterative procedures possible

Integrated microwave photonics

NARCIS (Netherlands)

Marpaung, D.A.I.; Roeloffzen, C.G.H.; Heideman, Rene; Leinse, Arne; Sales, S.; Capmany, J.

2013-01-01

Microwave photonics (MWP) is an emerging field in which radio frequency (RF) signals are generated, distributed, processed and analyzed using the strength of photonic techniques. It is a technology that enables various functionalities which are not feasible to achieve only in the microwave domain. A

On the inverse windowed Fourier transform

OpenAIRE

Rebollo Neira, Laura; Fernández Rubio, Juan Antonio

1999-01-01

The inversion problem concerning the windowed Fourier transform is considered. It is shown that, out of the infinite solutions that the problem admits, the windowed Fourier transform is the "optimal" solution according to a maximum-entropy selection criterion. Peer Reviewed

Uniaxial backfill block compaction

International Nuclear Information System (INIS)

Koskinen, V.

2012-05-01

The main parts of the project were: to make a literature survey of the previous uniaxial compaction experiments; do uniaxial compaction tests in laboratory scale; and do industrial scale production tests. Object of the project was to sort out the different factors affecting the quality assurance chain of the backfill block uniaxial production and solve a material sticking to mould problem which appeared during manufacturing the blocks of bentonite and cruched rock mixture. The effect of mineralogical and chemical composition on the long term functionality of the backfill was excluded from the project. However, the used smectite-rich clays have been tested for mineralogical consistency. These tests were done in B and Tech OY according their SOPs. The objective of the Laboratory scale tests was to find right material- and compaction parameters for the industrial scale tests. Direct comparison between the laboratory scale tests and industrial scale tests is not possible because the mould geometry and compaction speed has a big influence for the compaction process. For this reason the selected material parameters were also affected by the previous compaction experiments. The industrial scale tests were done in summer of 2010 in southern Sweden. Blocks were done with uniaxial compaction. A 40 tons of the mixture of bentonite and crushed rock blocks and almost 50 tons of Friedland-clay blocks were compacted. (orig.)

Quantitative characterization of chitosan in the skin by Fourier-transform infrared spectroscopic imaging and ninhydrin assay: application in transdermal sciences.

Science.gov (United States)

Nawaz, A; Wong, T W

2016-07-01

The chitosan has been used as the primary excipient in transdermal particulate dosage form design. Its distribution pattern across the epidermis and dermis is not easily accessible through chemical assay and limited to radiolabelled molecules via quantitative autoradiography. This study explored Fourier-transform infrared spectroscopy imaging technique with built-in microscope as the means to examine chitosan molecular distribution over epidermis and dermis with the aid of histology operation. Fourier-transform infrared spectroscopy skin imaging was conducted using chitosan of varying molecular weights, deacetylation degrees, particle sizes and zeta potentials, obtained via microwave ligation of polymer chains at solution state. Both skin permeation and retention characteristics of chitosan increased with the use of smaller chitosan molecules with reduced acetyl content and size, and increased positive charge density. The ratio of epidermal to dermal chitosan content decreased with the use of these chitosan molecules as their accumulation in dermis (3.90% to 18.22%) was raised to a greater extent than epidermis (0.62% to 1.92%). A larger dermal chitosan accumulation nonetheless did not promote the transdermal polymer passage more than the epidermal chitosan. A small increase in epidermal chitosan content apparently could fluidize the stratum corneum and was more essential to dictate molecular permeation into dermis and systemic circulation. The histology technique aided Fourier-transform infrared spectroscopy imaging approach introduces a new dimension to the mechanistic aspect of chitosan in transdermal delivery. © 2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.

Hyperbolic Cross Truncations for Stochastic Fourier Cosine Series

Science.gov (United States)

Zhang, Zhihua

2014-01-01

Based on our decomposition of stochastic processes and our asymptotic representations of Fourier cosine coefficients, we deduce an asymptotic formula of approximation errors of hyperbolic cross truncations for bivariate stochastic Fourier cosine series. Moreover we propose a kind of Fourier cosine expansions with polynomials factors such that the corresponding Fourier cosine coefficients decay very fast. Although our research is in the setting of stochastic processes, our results are also new for deterministic functions. PMID:25147842

A Unified Method of Finding Laplace Transforms, Fourier Transforms, and Fourier Series. [and] An Inversion Method for Laplace Transforms, Fourier Transforms, and Fourier Series. Integral Transforms and Series Expansions. Modules and Monographs in Undergraduate Mathematics and Its Applications Project. UMAP Units 324 and 325.

Science.gov (United States)

Grimm, C. A.

This document contains two units that examine integral transforms and series expansions. In the first module, the user is expected to learn how to use the unified method presented to obtain Laplace transforms, Fourier transforms, complex Fourier series, real Fourier series, and half-range sine series for given piecewise continuous functions. In…

Characterization of ceramic powder compacts

International Nuclear Information System (INIS)

Yanai, K.; Ishimoto, S.; Kubo, T.; Ito, K.; Ishikawa, T.; Hayashi, H.

1995-01-01

UO 2 and Al 2 O 3 powder packing structures in cylindrical powder compacts are observed by scanning electron microscopy using polished cross sections of compacts fixed by low viscosity epoxy resin. Hard aggregates which are not destroyed during powder compaction are observed in some of the UO 2 powder compacts. A technique to measure local density in powder compacts is developed based on counting characteristic X-ray intensity by energy dispersive X-ray analysis (EDX). The local density of the corner portion of the powder compact fabricated by double-acting dry press is higher than that of the inner portion. ((orig.))

A Note on Fourier and the Greenhouse Effect

OpenAIRE

Postma, Joseph E.

2015-01-01

Joseph Fourier's discovery of the greenhouse effect is discussed and is compared to the modern conception of the greenhouse effect. It is confirmed that what Fourier discovered is analogous to the modern concept of the greenhouse effect. However, the modern concept of the greenhouse effect is found to be based on a paradoxical analogy to Fourier's greenhouse work and so either Fourier's greenhouse work, the modern conception of the greenhouse effect, or the modern definition of heat is incorr...

Microwave plasma initiated graft copolymerization modification of monomers onto PTFE surface

International Nuclear Information System (INIS)

Guan Weishu; Wen Yunjian; Fang Yan; Yin Yongxiang

1996-02-01

A graft copolymerization modification technique of monomers onto polytetrafluoroethylene (PTFE) surface initiated by a 2.45 GHz non-equilibrium microwave plasma has been investigated. Standard X-Ray Photoelectron Spectroscopy (XPS), Attenuated Total Reflectance-Fourier Transform Infrared Spectroscopy (ATR-FTIR), Scanning Electron Microscopy (sEM) and wetting techniques were used for examination and analysis of samples. Considerable changes in chemical structure, composition and in morphology of grafted surface of PTFE were found. Results showed the occurrence of noticeable defluorination and cross-linked structure on grafted surface, and indicated that different kinds and contents of oxygen-containing functional groups were introduced into the surface of PTFE. Wetting and adhesion experiment of the sample proved that significant improvements in hydrophilicity and adhesion of surface were exhibited. These results confirmed the success of grafting. (8 refs., 7 figs., 1 tab.)

Microwave Resonators and Filters

Science.gov (United States)

2015-12-22

1 Microwave Resonators and Filters Daniel E. Oates MIT Lincoln Laboratory 244 Wood St. Lexington, MA 02478 USA Email: oates@ll.mit.edu...explained in other chapters, the surface resistance of superconductors at microwave frequencies can be as much as three orders of magnitude lower than the...resonators and filters in the first edition of this handbook (Z.-Y. Shen 2003) discussed the then state of the art of microwave frequency applications

Three dimensional image reconstruction in the Fourier domain

International Nuclear Information System (INIS)

Stearns, C.W.; Chesler, D.A.; Brownell, G.L.

1987-01-01

Filtered backprojection reconstruction algorithms are based upon the relationship between the Fourier transform of the imaged object and the Fourier transforms of its projections. A new reconstruction algorithm has been developed which performs the image assembly operation in Fourier space, rather than in image space by backprojection. This represents a significant decrease in the number of operations required to assemble the image. The new Fourier domain algorithm has resolution comparable to the filtered backprojection algorithm, and, after correction by a pointwise multiplication, demonstrates proper recovery throughout image space. Although originally intended for three-dimensional imaging applications, the Fourier domain algorithm can also be developed for two-dimensional imaging applications such as planar positron imaging systems

Feasibility of microwave interferometry and fourier-transform spectrometry for high-spectral-resolution sensing

Energy Technology Data Exchange (ETDEWEB)

Gerstl, S.; Cooke, B.; Jacobson, A.; Love, S.; Zardecki, A.

1996-09-01

This is the final report of a one-year, Laboratory-Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). The primary objective of this project was to perform the necessary research and development to determine the feasibility of new ideas that, if successful, could lead to the development of future new programs in high-spectral resolution remote sensing. In active remote sensing systems, the solar illumination of a scene is replaced by a man-made source, preferably a laser beam. However, when laser beams are propagated through a scattering medium, like air, random optical path fluctuations comparable to the optical wavelength are generated giving rise to the speckle effect, which is the most severe perturbation in active remote sensing systems. The limitations introduced by the speckle effect degrade or negate the data interpretation. We sought to introduce better physical models of beam scattering that allow a more realistic simulation environment to be developed that, when applied to experimental data sets, improve their interpretability and increase the information content. Improved beam propagation models require improved knowledge of the spatio-temporal distribution of the scattering and absorbing medium. In the free atmosphere the largest contributor is water vapor in the lower troposphere. We tested the feasibility of using microwave interferometry to measure water-vapor irregularities in the boundary layer. Knowledge of these distributions enable much improved atmospheric correction algorithms for satellite imagery of the earth`s surface to be developed. For hyperspectral active remote sensing systems it is necessary to perform very high-resolution spectral measurements of the reflected laser light. Such measurements are possible with optical interferometers.

Probing the local microwave properties of superconducting thin films by a scanning microwave near-field microscope

CERN Document Server

Wu, L Y; Wang, K L; Jiang, T; Kang, L; Yang, S Z; Wu, P H

2002-01-01

In this paper, we present our approach to probe the local microwave properties of superconducting thin films by using the microwave near-field scanning technique. We have employed a coaxial cavity together with a niobium tip as the probe and established a scanning sample stage cooled by liquid nitrogen to study thin film devices at low temperature in our scanning microwave near-field microscope. Nondestructive images have been obtained on the inhomogeneity of the YBaCuO superconducting thin films at microwave frequency. We believe that these results would be helpful in evaluating the microwave performance of the devices.

A novel rhombohedron-like nickel ferrite nanostructure: Microwave combustion synthesis, structural characterization and magnetic properties

Directory of Open Access Journals (Sweden)

G. Suresh Kumar

2016-09-01

Full Text Available Research on nickel ferrite nanostructures has drawn a great interest because of its inherent chemical, physical and electronic properties. In this study, we have synthesized rhombohedron – like nickel ferrite nanostructure by a rapid microwave assisted combustion method using ethylenediamminetetraacetic acid as a chelating agent. X-ray diffraction, Fourier transform infrared spectrometer, transmission electron microscope and energy dispersive X-ray microanalyser were used to characterize the prepared sample. The magnetic behaviour was analysed by means of field dependent magnetization measurement which indicates that the prepared sample exhibits a soft ferromagnetic nature with saturation magnetization of 63.034 emu/g. This technique can be a potential method to synthesize novel nickel ferrite nanostructure with improved magnetic properties.

Passive Microwave Components and Antennas

DEFF Research Database (Denmark)

State-of-the-art microwave systems always require higher performance and lower cost microwave components. Constantly growing demands and performance requirements of industrial and scientific applications often make employing traditionally designed components impractical. For that reason, the design...... and development process remains a great challenge today. This problem motivated intensive research efforts in microwave design and technology, which is responsible for a great number of recently appeared alternative approaches to analysis and design of microwave components and antennas. This book highlights...... techniques. Modelling and computations in electromagnetics is a quite fast-growing research area. The recent interest in this field is caused by the increased demand for designing complex microwave components, modeling electromagnetic materials, and rapid increase in computational power for calculation...

Fourier techniques and applications

CERN Document Server

1985-01-01

The first systematic methods of Fourier analysis date from the early eighteenth century with the work of Joseph Fourier on the problem of the flow of heat. (A brief history is contained in the first paper.) Given the initial tempera­ ture at all points of a region, the problem was to determine the changes in the temperature distribution over time. Understanding and predicting these changes was important in such areas as the handling of metals and the determination of geological and atmospheric temperatures. Briefly, Fourier noticed that the solution of the heat diffusion problem was simple if the initial temperature dis­ tribution was sinusoidal. He then asserted that any distri­ bution can be decomposed into a sum of sinusoids, these being the harmonics of the original function. This meant that the general solution could now be obtained by summing the solu­ tions of the component sinusoidal problems. This remarkable ability of the series of sinusoids to describe all "reasonable" functions, the sine qua n...

Microwave Tokamak Experiment

International Nuclear Information System (INIS)

Anon.

1988-01-01

The Microwave Tokamak Experiment, now under construction at the Laboratory, will use microwave heating from a free-electron laser. The intense microwave pulses will be injected into the tokamak to realize several goals, including a demonstration of the effects of localized heat deposition within magnetically confined plasma, a better understanding of energy confinement in tokamaks, and use of the new free-electron laser technology for plasma heating. The experiment, soon to be operational, provides an opportunity to study dense plasmas heated by powers unprecedented in the electron-cyclotron frequency range required by the especially high magnetic fields used with the MTX and needed for reactors. 1 references, 5 figures, 3 tables

Design of a Compact Planar Rectenna for Wireless Power Transfer in the ISM Band

Directory of Open Access Journals (Sweden)

Fang Zhang

2014-01-01

Full Text Available This paper presents a compact planar rectenna with high conversion efficiency in the ISM band. The proposed rectenna is developed by the decomposing of a planar rectenna topology into two functional parts and then recombining the two parts into a new topology to make the rectenna size reduction. The operation mechanism of the antenna and rectifying circuit in the proposed novel topology is explained and the design methodology is presented in detail. The proposed topology not only reduces the rectenna design cycle time but also leads to easy realization at the required frequency ranges with a very low cost. For validation, a 2.45 GHz rectenna system is designed and measured to show their microwave performances.

MECHANICS OF DYNAMIC POWDER COMPACTION PROCESS

OpenAIRE

Nurettin YAVUZ

1996-01-01

In recent years, interest in dynamic compaction methods of metal powders has increased due to the need to improve compaction properties and to increase production rates of compacts. In this paper, review of dynamic and explosive compaction of metal powders are given. An attempt is made to get a better understanding of the compaction process with the mechanicis of powder compaction.

Preparation and investigation of structural, magnetic and microwave absorption properties of cerium doped barium hexaferrite

Directory of Open Access Journals (Sweden)

P Kameli

2015-01-01

Full Text Available In this study the structure, magnetic and microwave absorption properties of cerium (Ce doped barium hexaferrite with general formulae BaCexFe12-xO19 (x=0.0, 0.05, 0.1, 0.15, 0.2 have been investigated. These samples have been prepared by sol- gel method. Influence of replacing Fe+3 ion by rare- earth Ce+3 ion on the structural, magnetic and microwave absorption properties have been investigated by X- ray diffraction (XRD, Fourier transform infrared (FT-IR, Vibrating sample magnetometer (VSM and vector network analyzer (VNA. X-ray diffraction analysis indicated that the samples are of single phase with space group p63/mmc. The magnetic properties of samples indicated that with the Ce doping the saturation magnetization show no regular behavior. Moreover, coercivity (Hc first decreased and reached to the minimum value for x=0.1 sample and then increased with Ce content increasing. Also, measurement of electromagnetic wave absorption in X and Ku frequency bands indicated that the maximum of reflection loss obtained for x=0.15 sample. Moreover, result indicated that absorption peak shifted toward a lower frequency when thickness was increased.

An Evaluation of Antarctica as a Calibration Target for Passive Microwave Satellite Missions

Science.gov (United States)

Kim, Edward

2012-01-01

Passive microwave remote sensing at L-band (1.4 GHz) is sensitive to soil moisture and sea surface salinity, both important climate variables. Science studies involving these variables can now take advantage of new satellite L-band observations. The first mission with regular global passive microwave observations at L-band is the European Space Agency's Soil Moisture and Ocean Salinity (SMOS), launched November, 2009. A second mission, NASA's Aquarius, was launched June, 201l. A third mission, NASA's Soil Moisture Active Passive (SMAP) is scheduled to launch in 2014. Together, these three missions may provide a decade-long data record -- provided that they are intercalibrated. The intercalibration is best performed at the radiance (brightness temperature) level, and Antarctica is proving to be a key calibration target. However, Antarctica has thus far not been fully characterized as a potential target. This paper will present evaluations of Antarctica as a microwave calibration target for the above satellite missions. Preliminary analyses have identified likely target areas, such as the vicinity of Dome-C and larger areas within East Antarctica. Physical sources of temporal and spatial variability of polar firn are key to assessing calibration uncertainty. These sources include spatial variability of accumulation rate, compaction, surface characteristics (dunes, micro-topography), wind patterns, and vertical profiles of density and temperature. Using primarily SMOS data, variability is being empirically characterized and attempts are being made to attribute observed variability to physical sources. One expected outcome of these studies is the potential discovery of techniques for remotely sensing--over all of Antarctica--parameters such as surface temperature.

An Lp−Lq version of Hardy's theorem for spherical Fourier transform on semisimple Lie groups

Directory of Open Access Journals (Sweden)

S. Ben Farah

2004-01-01

Full Text Available We consider a real semisimple Lie group G with finite center and K a maximal compact subgroup of G. We prove an Lp−Lq version of Hardy's theorem for the spherical Fourier transform on G. More precisely, let a, b be positive real numbers, 1≤p, q≤∞, and f a K-bi-invariant measurable function on G such that ha−1f∈Lp(G and eb‖λ‖2ℱ(f∈Lq(+* (ha is the heat kernel on G. We establish that if ab≥1/4 and p or q is finite, then f=0 almost everywhere. If ab<1/4, we prove that for all p, q, there are infinitely many nonzero functions f and if ab=1/4 with p=q=∞, we have f=const ha.

Medical preparation container comprising microwave powered sensor assembly

DEFF Research Database (Denmark)

2016-01-01

The present invention relates to a medical preparation container which comprises a microwave powered sensor assembly. The microwave powered sensor assembly comprises a sensor configured to measure a physical property or chemical property of a medical preparation during its heating in a microwave ...... oven. The microwave powered sensor assembly is configured for harvesting energy from microwave radiation emitted by the microwave oven and energize the sensor by the harvested microwave energy.......The present invention relates to a medical preparation container which comprises a microwave powered sensor assembly. The microwave powered sensor assembly comprises a sensor configured to measure a physical property or chemical property of a medical preparation during its heating in a microwave...

Microwave and RF engineering

CERN Document Server

Sorrentino, Roberto

2010-01-01

An essential text for both students and professionals, combining detailed theory with clear practical guidance This outstanding book explores a large spectrum of topics within microwave and radio frequency (RF) engineering, encompassing electromagnetic theory, microwave circuits and components. It provides thorough descriptions of the most common microwave test instruments and advises on semiconductor device modelling. With examples taken from the authors' own experience, this book also covers:network and signal theory;electronic technology with guided electromagnetic pr

A new twist to fourier transforms

CERN Document Server

Meikle, Hamish D

2004-01-01

Making use of the inherent helix in the Fourier transform expression, this book illustrates both Fourier transforms and their properties in the round. The author draws on elementary complex algebra to manipulate the transforms, presenting the ideas in such a way as to avoid pages of complicated mathematics. Similarly, abbreviations are not used throughout and the language is kept deliberately clear so that the result is a text that is accessible to a much wider readership.The treatment is extended with the use of sampled data to finite and discrete transforms, the fast Fourier transform, or FFT, being a special case of a discrete transform. The application of Fourier transforms in statistics is illustrated for the first time using the examples operational research and later radar detection. In addition, a whole chapter on tapering or weighting functions is added for reference. The whole is rounded off by a glossary and examples of diagrams in three dimensions made possible by today's mathematics programs

Synthesis of a ternary Ag/RGO/ZnO nanocomposite via microwave irradiation and its application for the degradation of Rhodamine B under visible light.

Science.gov (United States)

Surendran, Divya Kollikkara; Xavier, Marilyn Mary; Viswanathan, Vandana Parakkal; Mathew, Suresh

2017-06-01

Reduced graphene oxide supporting plasmonic photocatalyst (Ag) on ZnO has been synthesized via a facile two-step microwave synthesis using RGO/ZnO and AgNO 3 . First step involves fabrication of RGO/ZnO via microwave irradiation. The nanocomposites were characterized by X-ray diffraction analysis, transmission electron microscopy, Fourier transform infrared spectroscopy, and Raman spectroscopy. Ag/RGO/ZnO shows enhanced photoactivity under visible light for the degradation of Rhodamine B. Enhanced charge separation and migration have been assigned using UV-vis diffuse reflectance spectra, photoluminescence spectra, electrochemical impedance spectra, and TCSPC analysis. The improved photoactivity of Ag/RGO/ZnO can be ascribed to the prolonged lifetime of photogenerated electron-hole pairs and effective interfacial hybridization between RGO and Ag with ZnO nanoparticles. Ag nanoparticles can absorb visible light via surface plasmon resonance to enhance photocatalytic activity.

Spark plasma sintering and microwave electromagnetic properties of MnFe{sub 2}O{sub 4} ceramics

Energy Technology Data Exchange (ETDEWEB)

Penchal Reddy, M., E-mail: drlpenchal@gmail.com [Center for Advanced Materials, Qatar University, Doha 2713 (Qatar); Mohamed, A.M.A. [Center for Advanced Materials, Qatar University, Doha 2713 (Qatar); Department of Metallurgical and Materials Engineering, Faculty of Petroleum and Mining Engineering, Suez University, Suez 4372 (Egypt); Venkata Ramana, M. [Department of Physics, National Taiwan Normal University, Taipei 11677, Taiwan (China); Zhou, X.B.; Huang, Q. [Division of Functional Materials and Nanodevices, Ningbo Institute of Materials Technology and Engineering, Ningbo 315201 (China)

2015-12-01

MnFe{sub 2}O{sub 4} ferrite powder was synthesized by a facile one-pot hydrothermal route and then consolidated into dense nanostructured compacts by the spark plasma sintering (SPS) technique. The effect of sintering temperature, on densification, morphology, magnetic and microwave absorption properties was examined. Spark plasma sintering resulted in uniform microstructure, as well as maximum relative density of 98%. The magnetic analysis indicated that the MnFe{sub 2}O{sub 4} ferrite nanoparticles showed ferrimagnetic behavior. Moreover, the dielectric loss and magnetic loss properties of MnFe{sub 2}O{sub 4} ferrite nanoparticles were both enhanced due to its better dipole polarization, interfacial polarization and shape anisotropy. It is believed that such spark plasma sintered ceramic material will be applied widely in microwave absorbing area. - Highlights: • Successful synthesis of dense MnFe{sub 2}O{sub 4} ceramics using spark plasma sintering. • Lower temperature and shorter sintering time, compared to conventional methods. • Optimal sintering condition was achieved. • The magnetic properties of the sintered samples are sensitive to the density and microstructure.

Investigations on structural and optical properties of starch capped ZnS nanoparticles synthesized by microwave irradiation method

Science.gov (United States)

Lalithadevi, B.; Mohan Rao, K.; Ramananda, D.

2018-05-01

Following a green synthesis method, zinc sulfide (ZnS) nanoparticles were prepared by chemical co-precipitation technique using starch as capping agent. Microwave irradiation was used as heating source. X-ray diffraction studies indicated that nanopowders obtained were polycrystalline possessing ZnS simple cubic structure. Transmission electron microscopic studies indicated that starch limits the agglomeration by steric stabilization. Interaction between ZnS and starch was confirmed by Fourier transform infrared spectroscopy as well as Raman scattering studies. Quantum size effects were observed in optical absorption studies while quenching of defect states on nanoparticles was improved with increase in starch addition as indicated by photoluminescence spectra.

Discussion on Microwave-Matter Interaction Mechanisms by In Situ Observation of "Core-Shell" Microstructure during Microwave Sintering.

Science.gov (United States)

Liu, Wenchao; Xu, Feng; Li, Yongcun; Hu, Xiaofang; Dong, Bo; Xiao, Yu

2016-02-23

This research aims to deepen the understanding of the interaction mechanisms between microwave and matter in a metal-ceramic system based on in situ synchrotron radiation computed tomography. A special internal "core-shell" microstructure was discovered for the first time and used as an indicator for the interaction mechanisms between microwave and matter. Firstly, it was proved that the microwave magnetic field acted on metal particles by way of inducing an eddy current in the surface of the metal particles, which led to the formation of a "core-shell" microstructure in the metal particles. On this basis, it was proposed that the ceramic particles could change the microwave field and open a way for the microwave, thereby leading to selective heating in the region around the ceramic particles, which was verified by the fact that all the "core-shell" microstructure was located around ceramic particles. Furthermore, it was indicated that the ceramic particles would gather the microwaves, and might lead to local heating in the metal-ceramic contact region. The focusing of the microwave was proved by the quantitative analysis of the evolution rate of the "core-shell" microstructure in a different region. This study will help to reveal the microwave-matter interaction mechanisms during microwave sintering.

Microwave firing of MnZn-ferrites

International Nuclear Information System (INIS)

Tsakaloudi, V.; Papazoglou, E.; Zaspalis, V.T.

2004-01-01

Microwave firing is evaluated in comparison to conventional firing for MnZn-ferrites. For otherwise identical conditions, microwave firing results to higher densities and coarser microstructures. Initial magnetic permeability values (25 kHz, 25 deg. C, <0.1 mT) after conventional firing are approximately 5000, but the corresponding values after microwave firing are approximately 6000. Unlike the conventional firing process, the final density after microwave firing is increased by increasing the prefiring temperature. As appears from the results of this study, microwave firing could be in principle a promising MnZn-ferrite firing technology for materials to be used in high magnetic permeability applications. No advantages of microwave firing are evident for materials intended to be used in high field power applications

Wigner distribution and fractional Fourier transform

NARCIS (Netherlands)

Alieva, T.; Bastiaans, M.J.; Boashash, B.

2003-01-01

We have described the relationship between the fractional Fourier transform and the Wigner distribution by using the Radon-Wigner transform, which is a set of projections of the Wigner distribution as well as a set of squared moduli of the fractional Fourier transform. We have introduced the concept

Fourier plane imaging microscopy

Energy Technology Data Exchange (ETDEWEB)

Dominguez, Daniel, E-mail: daniel.dominguez@ttu.edu; Peralta, Luis Grave de [Department of Physics, Texas Tech University, Lubbock, Texas 79409 (United States); Nano Tech Center, Texas Tech University, Lubbock, Texas 79409 (United States); Alharbi, Nouf; Alhusain, Mdhaoui [Department of Physics, Texas Tech University, Lubbock, Texas 79409 (United States); Bernussi, Ayrton A. [Nano Tech Center, Texas Tech University, Lubbock, Texas 79409 (United States); Department of Electrical and Computer Engineering, Texas Tech University, Lubbock, Texas 79409 (United States)

2014-09-14

We show how the image of an unresolved photonic crystal can be reconstructed using a single Fourier plane (FP) image obtained with a second camera that was added to a traditional compound microscope. We discuss how Fourier plane imaging microscopy is an application of a remarkable property of the obtained FP images: they contain more information about the photonic crystals than the images recorded by the camera commonly placed at the real plane of the microscope. We argue that the experimental results support the hypothesis that surface waves, contributing to enhanced resolution abilities, were optically excited in the studied photonic crystals.

Controlled Microwave Heating Accelerates Rolling Circle Amplification.

Directory of Open Access Journals (Sweden)

Takeo Yoshimura

Full Text Available Rolling circle amplification (RCA generates single-stranded DNAs or RNA, and the diverse applications of this isothermal technique range from the sensitive detection of nucleic acids to analysis of single nucleotide polymorphisms. Microwave chemistry is widely applied to increase reaction rate as well as product yield and purity. The objectives of the present research were to apply microwave heating to RCA and indicate factors that contribute to the microwave selective heating effect. The microwave reaction temperature was strictly controlled using a microwave applicator optimized for enzymatic-scale reactions. Here, we showed that microwave-assisted RCA reactions catalyzed by either of the four thermostable DNA polymerases were accelerated over 4-folds compared with conventional RCA. Furthermore, the temperatures of the individual buffer components were specifically influenced by microwave heating. We concluded that microwave heating accelerated isothermal RCA of DNA because of the differential heating mechanisms of microwaves on the temperatures of reaction components, although the overall reaction temperatures were the same.

Controlled Microwave Heating Accelerates Rolling Circle Amplification.

Science.gov (United States)

Yoshimura, Takeo; Suzuki, Takamasa; Mineki, Shigeru; Ohuchi, Shokichi

2015-01-01

Rolling circle amplification (RCA) generates single-stranded DNAs or RNA, and the diverse applications of this isothermal technique range from the sensitive detection of nucleic acids to analysis of single nucleotide polymorphisms. Microwave chemistry is widely applied to increase reaction rate as well as product yield and purity. The objectives of the present research were to apply microwave heating to RCA and indicate factors that contribute to the microwave selective heating effect. The microwave reaction temperature was strictly controlled using a microwave applicator optimized for enzymatic-scale reactions. Here, we showed that microwave-assisted RCA reactions catalyzed by either of the four thermostable DNA polymerases were accelerated over 4-folds compared with conventional RCA. Furthermore, the temperatures of the individual buffer components were specifically influenced by microwave heating. We concluded that microwave heating accelerated isothermal RCA of DNA because of the differential heating mechanisms of microwaves on the temperatures of reaction components, although the overall reaction temperatures were the same.

Microwave Accelerated Polymerization of 2-Phenyl-2-Oxazoline: Microwave or Temperature Effects?

NARCIS (Netherlands)

Hoogenboom, R.; Leenen, M.A.M.; Wiesbrock, F.D.; Schubert, U.S.

2005-01-01

Summary: Investigations regarding the cationic ring-opening polymerization of 2-phenyl-2-oxazoline under microwave irradiation and conventional heating are reported. This study was inspired by contradictory reports of the (non-)existence of non-thermal microwave effects that might accelerate the

Clastic compaction unit classification based on clay content and integrated compaction recovery using well and seismic data

Directory of Open Access Journals (Sweden)

Zhong Hong

2016-11-01

Full Text Available Abstract Compaction correction is a key part of paleo-geomorphic recovery methods. Yet, the influence of lithology on the porosity evolution is not usually taken into account. Present methods merely classify the lithologies as sandstone and mudstone to undertake separate porosity-depth compaction modeling. However, using just two lithologies is an oversimplification that cannot represent the compaction history. In such schemes, the precision of the compaction recovery is inadequate. To improve the precision of compaction recovery, a depth compaction model has been proposed that involves both porosity and clay content. A clastic lithological compaction unit classification method, based on clay content, has been designed to identify lithological boundaries and establish sets of compaction units. Also, on the basis of the clastic compaction unit classification, two methods of compaction recovery that integrate well and seismic data are employed to extrapolate well-based compaction information outward along seismic lines and recover the paleo-topography of the clastic strata in the region. The examples presented here show that a better understanding of paleo-geomorphology can be gained by applying the proposed compaction recovery technology.

Proposal of a novel compact P-band magnetically insulated transmission line oscillator with inclined vanes

Science.gov (United States)

Zhang, Xiaoping; Dang, Fangchao; Li, Yangmei; Jin, Zhenxing

2015-06-01

In this paper, we present a novel compact P-band magnetically insulated transmission line oscillator (MILO) with specially inclined slow-wave-structure (SWS) vanes to decrease its total dimension and weight. The dispersion characteristics of the inclined SWS are investigated in detail and made comparisons with that of the traditional straight SWS. The results show that the inclined SWS is more advantageous in operating on a steady frequency in a wide voltage range and has a better asymmetric mode segregation and a relatively large band-gap between the TM00 and TM01 modes which are in favor of avoiding the asymmetric and transverse mode competition. Besides, the transverse dimension of the proposed novel inclined SWS with the same operation frequency is decreased by about 50%, and correspondingly the device volume shrinks remarkably to its 0.35 times. In particle-in-cell simulation, the electron bunching spokes are obviously formed in the inclined SWS, and a P-band high-power microwave with a power of 5.8 GW, frequency of 645 MHz, and efficiency of 17.2% is generated by the proposed device, which indicates the feasibility of the compact design with the inclined vanes at the P-band.

Microwave ablation devices for interventional oncology.

Science.gov (United States)

Ward, Robert C; Healey, Terrance T; Dupuy, Damian E

2013-03-01

Microwave ablation is one of the several options in the ablation armamentarium for the treatment of malignancy, offering several potential benefits when compared with other ablation, radiation, surgical and medical treatment modalities. The basic microwave system consists of the generator, power distribution system and antennas. Often under image (computed tomography or ultrasound) guidance, a needle-like antenna is inserted percutaneously into the tumor, where local microwave electromagnetic radiation is emitted from the probe's active tip, producing frictional tissue heating, capable of causing cell death by coagulation necrosis. Half of the microwave ablation systems use a 915 MHz generator and the other half use a 2450 MHz generator. To date, there are no completed clinical trials comparing microwave devices head-to-head. Prospective comparisons of microwave technology with other treatment alternatives, as well as head-to-head comparison with each microwave device, is needed if this promising field will garner more widespread support and use in the oncology community.

Use of the liquisolid compact technique for improvement of the dissolution rate of valsartan

Directory of Open Access Journals (Sweden)

Naveen Chella

2012-10-01

Full Text Available The aim of this study was to improve the dissolution rate of the poorly soluble drug valsartan by delivering the drug as a liquisolid compact. Liquisolid compacts were prepared using propylene glycol as solvent, Avicel PH102 as carrier, and Aerosil 200 as the coating material. The crystallinity of the newly formulated drug and the interaction between excipients was examined by X-ray powder diffraction and Fourier-transform infrared spectroscopy, respectively. The dissolution studies for the liquisolid formulation and the marketed product were carried out at different pH values. The results showed no change in the crystallinity of the drug and no interaction between excipients. The dissolution efficiency of valsartan at 15 min was increased from 4.02% for plain drug and 13.58% for marketed product to 29.47% for the liquisolid formulation. The increase in the dissolution rate was also found to be significant compared to the marketed product at lower pH values, simulating the gastric environment where valsartan is largely absorbed. The liquisolid technique appears to be a promising approach for improving the dissolution of poorly soluble drugs like valsartan.

Effect of residual water content on the physico-chemical properties of sucralfate dried gel obtained by microwave drying.

Science.gov (United States)

Gainotti, Alessandro; Losi, Elena; Bettini, Ruggero; Colombo, Paolo; Sonvico, Fabio; Baroni, Daniela; Santi, Patrizia; Colombo, Gaia

2005-08-01

The purpose of this study was to investigate the physico-chemical characteristics of sucralfate humid gel dried by microwaves, in relation to the residual water content. Differential scanning calorimetry (DSC) allowed for the determination of the water state in sucralfate samples. Fourier-transform infrared (FT-IR) spectroscopy was used to monitor the changes in sucralfate gel structure induced by the microwave drying. A boundary value of total water content for sucralfate gel samples was found at 42% (w/w). Below this value only bound water was present, whereas above this value, the increase in total water was due to free water. In the physical form of gel, the strength of the coordination between sulfate anions and the positively charged aluminum hydroxide was dependent on the residual water content. The study of the sedimentation behavior of water suspensions prepared with dried sucralfate allowed for the evaluation of the retention of gel properties. We found that the microwave drying process affected the sedimentation of sucralfate dried gel suspensions independent of the residual water content: when suspensions were prepared from sucralfate dried gel powders containing more than 42% (w/w) of residual water, the sedimentation ratio was higher than 0.9. The non-gel powder suspension showed a sedimentation ratio of 0.68 +/- 0.02, whereas the sucralfate humid gel suspension did not sediment.

Study of federal microwave standards

Energy Technology Data Exchange (ETDEWEB)

David, L.

1980-08-01

Present and future federal regulatory processes which may impact the permissible levels of microwave radiation emitted by the SPS Microwave Power Transmission (MPTS) were studied. An historical development of US occupational and public microwave standards includes an overview of Western and East European philosophies of environmental protection and neurophysiology which have led to the current widely differing maximum permissible exposure limits to microwaves. The possible convergence of microwave standards is characterized by a lowering of Western exposure levels while Eastern countries consider standard relaxation. A trend toward stricter controls on activities perceived as harmful to public health is under way as is interest in improving the federal regulatory process. Particularly relevant to SPS is the initiation of long-term, low-level microwave exposure programs. Coupled with new developments in instrumentation and dosimetry, the results from chronic exposure program and population exposure studies could be expected within the next five to ten years. Also discussed is the increasing public concern that rf energy is yet another hazardous environmental agent.

Replica Fourier Transform: Properties and applications

International Nuclear Information System (INIS)

Crisanti, A.; De Dominicis, C.

2015-01-01

The Replica Fourier Transform is the generalization of the discrete Fourier Transform to quantities defined on an ultrametric tree. It finds use in conjunction of the replica method used to study thermodynamics properties of disordered systems such as spin glasses. Its definition is presented in a systematic and simple form and its use illustrated with some representative examples. In particular we give a detailed discussion of the diagonalization in the Replica Fourier Space of the Hessian matrix of the Gaussian fluctuations about the mean field saddle point of spin glass theory. The general results are finally discussed for a generic spherical spin glass model, where the Hessian can be computed analytically

Effect of modified graphene and microwave irradiation on the mechanical and thermal properties of poly(styrene-co-methyl methacrylate)/graphene nanocomposites

KAUST Repository

Zubair, Mukarram

2014-08-04

The effect of modified graphene (MG) and microwave irradiation on the interaction between graphene (G) and poly(styrene-co-methyl meth acrylate) [P(S-co-MMA)] polymer matrix has been studied in this article. Modification of graphene was performed using nitric acid. P(S-co-MMA) polymer was blended via melt blending with pristine and MG. The resultant nanocomposites were irradiated under microwave at three different time intervals (5, 10, and 20 min). Compared to pristine graphene, MG showed improved interaction with P(S-co-MMA) polymer (P) after melt mixing and microwave irradiation. The mechanism of improved dispersion and interaction of modified graphene with P(S-co-MMA) polymer matrix during melt mixing and microwave irradiation is due to the presence of oxygen functionalities on the surface of MG as confirmed from Fourier transform infrared spectroscopy. The formation of defects on modified graphene and free radicals on P(S-co-MMA) polymer chains after irradiation as explained by Raman spectroscopy and X-Ray diffraction studies. The nanocomposites with 0.1 wt% G and MG have shown a 26% and 38% increase in storage modulus. After irradiation (10 min), the storage modulus further improved to 11.9% and 27.6% of nanocomposites. The glass transition temperature of nanocomposites also improved considerably after melt mixing and microwave irradiation (but only for polymer MG nanocomposite). However, at higher irradiation time (20 min), degradation of polymer nanocomposites occurred. State of creation of crosslink network after 10 min of irradiation and degradation after 20 min of irradiation of nanocomposites was confirmed from SEM studies. Copyright © 2014 John Wiley & Sons, Ltd.

Development task of compact reactor

International Nuclear Information System (INIS)

Kurushima, Morihiro

1982-01-01

In the Ministry of International Trade and Industry, studies proceed on the usage of compact medium and small LWRs. As such, the reactors from 100 to 200 MW may meet varieties of demands in scale and kind in view of the saving of petroleum and the economy of nuclear power. In this case, the technology of light water reactors with already established safety will be suitable for the development of compact reactors. The concept of ''nuclear power community'' using the compact reactors in local society and industrial zones was investigated. The following matters are described: need for the introduction of compact reactors, the survey on the compact reactor systems, and the present status and future problems for compact reactor usage. (J.P.N.)

Microwave processing of radioactive materials-I

International Nuclear Information System (INIS)

White, T.L.; Berry, J.B.

1989-01-01

This paper is the first of two papers that reviews the major past and present applications of microwave energy for processing radioactive materials, with particular emphasis on processing radioactive wastes. Microwave heating occurs through the internal friction produced inside a dielectric material when its molecules vibrate in response to an oscillating microwave field. For this presentation, we shall focus on the two FCC-approved microwave frequencies for industrial, scientific, and medical use, 915 and 2450 MHz. Also, because of space limitations, we shall postpone addressing plasma processing of hazardous wastes using microwave energy until a later date. 13 refs., 4 figs

The morphing of geographical features by Fourier transformation.

Science.gov (United States)

Li, Jingzhong; Liu, Pengcheng; Yu, Wenhao; Cheng, Xiaoqiang

2018-01-01

This paper presents a morphing model of vector geographical data based on Fourier transformation. This model involves three main steps. They are conversion from vector data to Fourier series, generation of intermediate function by combination of the two Fourier series concerning a large scale and a small scale, and reverse conversion from combination function to vector data. By mirror processing, the model can also be used for morphing of linear features. Experimental results show that this method is sensitive to scale variations and it can be used for vector map features' continuous scale transformation. The efficiency of this model is linearly related to the point number of shape boundary and the interceptive value n of Fourier expansion. The effect of morphing by Fourier transformation is plausible and the efficiency of the algorithm is acceptable.

Microwave processing of ceramic oxide filaments

Energy Technology Data Exchange (ETDEWEB)

Vogt, G.J.; Katz, J.D. [Los Alamos National Laboratory, NM (United States)

1995-05-01

The objective of the microwave filament processing project is to develop microwave techniques at 2.45 GHZ to manufacture continuous ceramic oxide filaments. Microwave processing uses the volumetric absorption of microwave power in oxide filament tows to drive off process solvents, to burn out organic binders, and to sinter the dried fibers to produce flexible, high-strength ceramic filaments. The technical goal is to advance filament processing technology by microwave heating more rapidly with less energy and at a lower cost than conventional processing, but with the same quality as conventional processing. The manufacturing goal is to collaborate with the 3M Company, a US manufacturer of ceramic oxide filaments, to evaluate the technology using a prototype filament system and to transfer the microwave technology to the 3M Company.

Photonic linear chirped microwave signal generation based on the ultra-compact spectral shaper using the slow light effect

DEFF Research Database (Denmark)

Yan, Siqi; Gao, Shengqian; Zhou, Feng

2017-01-01

A novel concept to generate a linear chirped microwave signal is proposed and experimentally demonstrated. The frequency to time mapping method is employed, where the photonic crystal waveguide Mach-Zehnder interferometer structure acts as the spectral shaper thanks to the slow light effect. By o....... The utilization of the slow light effect brings in significant advantages, including the ultra-small footprint of 0.096 mm(2) and simple structure to our scheme, which may be of great importance towards its potential applications. (C) 2017 Optical Society of America...

Fourier Series

Indian Academy of Sciences (India)

polynomials are dense in the class of continuous functions! The body of literature dealing with Fourier series has reached epic proportions over the last two centuries. We have only given the readers an outline of the topic in this article. For the full length episode we refer the reader to the monumental treatise of. A Zygmund.

Some Applications of Fourier's Great Discovery for Beginners

Science.gov (United States)

Kraftmakher, Yaakov

2012-01-01

Nearly two centuries ago, Fourier discovered that any periodic function of period T can be presented as a sum of sine waveforms of frequencies equal to an integer times the fundamental frequency [omega] = 2[pi]/T (Fourier's series). It is impossible to overestimate the importance of Fourier's discovery, and all physics or engineering students…

Evaluating superconductors for microwave applications

International Nuclear Information System (INIS)

Hammond, B.; Bybokas, J.

1989-01-01

It is becoming increasingly obvious that some of the earliest applications for high Tc superconductors will be in the microwave market. While this is a major opportunity for the superconductor community, it also represents a significant challenge. At DC or low frequencies a superconductor can be easily characterized by simple measurements of resistivity and magnetic susceptibility versus temperature. These parameters are fundamental to superconductor characterization and various methods exist for measuring them. The only valid way to determine the microwave characteristics of a superconductor is to measure it at microwave frequencies. It is for this reason that measuring microwave surface resistance has emerged as one of the most demanding and telling tests for materials intended for high frequency applications. In this article, the theory of microwave surface resistance is discussed. Methods for characterizing surface resistance theoretically and by practical implementation are described

THz Imaging by a Wide-band Compact FEL

CERN Document Server

Uk Jeong Young; Cheol Lee Byung; Hee-Park, S

2004-01-01

We have developed a laboratory-scale users facility with a compact THz FEL. The FEL operates in the wide wavelength range of 100–1200 μm, which corresponds to 0.3-3 THz. THz radiation from the FEL shows well collimated Gaussian spatial distribution and narrow spectral width of 0.3 μm, which is Fourier transform limited by the estimated pulse duration of 20 ps. The main application of the FEL is THz imaging for bio-medical researches. We are developing THz imaging techniques by 2-D scanning, single pulse capturing with the electro-optic method, and 3-D holography. High power, coherent, and pulsed feature of the FEL radiation is expected to show much better performance in advanced THz imaging of 3-D tomography by comparing with incoherent and weak THz sources. By controlling the optical delay between reference beam and scattered light from an object, we can get its 3-D tomography by the holograms. The coherent and pulse length of the FEL beam is measured to be 3-6 mm. In this paper we will show a...

Visualization of the microwave beam generated by a plasma relativistic microwave amplifier

Energy Technology Data Exchange (ETDEWEB)

Alekseev, I. S.; Ivanov, I. E.; Strelkov, P. S., E-mail: strelkov@fpl.gpi.ru [Russian Academy of Science, Prokhorov General Physics Institute (Russian Federation); Tarakanov, V. P., E-mail: karat@msk.su [Russian Academy of Sciences, Joint Institute for High Temperatures (Russian Federation); Ulyanov, D. K. [Russian Academy of Science, Prokhorov General Physics Institute (Russian Federation)

2017-03-15

A method based on the detection of emission of a dielectric screen with metal microinclusions in open air is applied to visualize the transverse structure of a high-power microwave beam. In contrast to other visualization techniques, the results obtained in this work provide qualitative information not only on the electric field strength, but also on the structure of electric field lines in the microwave beam cross section. The interpretation of the results obtained with this method is confirmed by numerical simulations of the structure of electric field lines in the microwave beam cross section by means of the CARAT code.

Compaction dynamics of crunchy granular material

Directory of Open Access Journals (Sweden)

Guillard François

2017-01-01

Full Text Available Compaction of brittle porous material leads to a wide variety of densification patterns. Static compaction bands occurs naturally in rocks or bones, and have important consequences in industry for the manufacturing of powder tablets or metallic foams for example. Recently, oscillatory compaction bands have been observed in brittle porous media like snow or cereals. We will discuss the great variety of densification patterns arising during the compaction of puffed rice, including erratic compaction at low velocity, one or several travelling compaction bands at medium velocity and homogeneous compaction at larger velocity. The conditions of existence of each pattern are studied thanks to a numerical spring lattice model undergoing breakage and is mapped to the phase diagram of the patterns based on dimensionless characteristic quantities. This also allows to rationalise the evolution of the compaction behaviour during a single test. Finally, the localisation of compaction bands is linked to the strain rate sensitivity of the material.

Compaction dynamics of crunchy granular material

Science.gov (United States)

Guillard, François; Golshan, Pouya; Shen, Luming; Valdès, Julio R.; Einav, Itai

2017-06-01

Compaction of brittle porous material leads to a wide variety of densification patterns. Static compaction bands occurs naturally in rocks or bones, and have important consequences in industry for the manufacturing of powder tablets or metallic foams for example. Recently, oscillatory compaction bands have been observed in brittle porous media like snow or cereals. We will discuss the great variety of densification patterns arising during the compaction of puffed rice, including erratic compaction at low velocity, one or several travelling compaction bands at medium velocity and homogeneous compaction at larger velocity. The conditions of existence of each pattern are studied thanks to a numerical spring lattice model undergoing breakage and is mapped to the phase diagram of the patterns based on dimensionless characteristic quantities. This also allows to rationalise the evolution of the compaction behaviour during a single test. Finally, the localisation of compaction bands is linked to the strain rate sensitivity of the material.

A microwave-augmented plasma torch module

International Nuclear Information System (INIS)

Kuo, S P; Bivolaru, Daniel; Williams, Skip; Carter, Campbell D

2006-01-01

A new plasma torch device which combines arc and microwave discharges to enhance the size and enthalpy of the plasma torch is described. A cylindrical-shaped plasma torch module is integrated into a tapered rectangular cavity to form a microwave adaptor at one end, which couples the microwave power injected into the cavity from the other end to the arc plasma generated by the torch module. A theoretical study of the microwave coupling from the cavity to the plasma torch, as the load, is presented. The numerical results indicate that the microwave power coupling efficiency exceeds 80%. Operational tests of the device indicate that the microwave power is coupled to the plasma torch and that the arc discharge power is increased. The addition of microwave energy enhances the height, volume and enthalpy of the plasma torch when the torch operates at a low airflow rate, and even when the flow speed is supersonic, a noticeable microwave effect on the plasma torch is observed. In addition, the present design allows the torch to be operated as both a fuel injector and igniter. Ignition of ethylene fuel injected through the centre of a tungsten carbide tube acting as the central electrode is demonstrated

Microfabricated Microwave-Integrated Surface Ion Trap

Science.gov (United States)

Revelle, Melissa C.; Blain, Matthew G.; Haltli, Raymond A.; Hollowell, Andrew E.; Nordquist, Christopher D.; Maunz, Peter

2017-04-01

Quantum information processing holds the key to solving computational problems that are intractable with classical computers. Trapped ions are a physical realization of a quantum information system in which qubits are encoded in hyperfine energy states. Coupling the qubit states to ion motion, as needed for two-qubit gates, is typically accomplished using Raman laser beams. Alternatively, this coupling can be achieved with strong microwave gradient fields. While microwave radiation is easier to control than a laser, it is challenging to precisely engineer the radiated microwave field. Taking advantage of Sandia's microfabrication techniques, we created a surface ion trap with integrated microwave electrodes with sub-wavelength dimensions. This multi-layered device permits co-location of the microwave antennae and the ion trap electrodes to create localized microwave gradient fields and necessary trapping fields. Here, we characterize the trap design and present simulated microwave performance with progress towards experimental results. This research was funded, in part, by the Office of the Director of National Intelligence (ODNI), Intelligence Advanced Research Projects Activity (IARPA).

Projective Fourier duality and Weyl quantization

International Nuclear Information System (INIS)

Aldrovandi, R.; Saeger, L.A.

1996-08-01

The Weyl-Wigner correspondence prescription, which makes large use of Fourier duality, is reexamined from the point of view of Kac algebras, the most general background for non-commutative Fourier analysis allowing for that property. It is shown how the standard Kac structure has to be extended in order to accommodate the physical requirements. An Abelian and a symmetric projective Kac algebras are shown to provide, in close parallel to the standard case, a new dual framework and a well-defined notion of projective Fourier duality for the group of translations on the plane. The Weyl formula arises naturally as an irreducible component of the duality mapping between these projective algebras. (author). 29 refs

Advances in microwaves 4

CERN Document Server

Young, Leo

2013-01-01

Advances in Microwaves, Volume 4 covers some innovations in the devices and applications of microwaves. This volume contains three chapters and begins with a discussion of the application of microwave phasers and time delay elements as beam steering elements in array radars. The next chapter provides first an overview of the technical aspects and different types of millimeter waveguides, followed by a survey of their application to railroads. The last chapter examines the general mode of conversion properties of nonuniform waveguides, such as waveguide tapers, using converted Maxwell's equatio

Summary of Self-compacting Concrete Workability

OpenAIRE

GUO Gui-xiang; Duan Hong-jun

2015-01-01

On the basis of a large number of domestic and foreign literature, situation and development of self-compacting concrete is introduced. Summary of the compacting theory of self-compacting concrete. And some of the factors affecting the workability of self-compacting concrete were discussed and summarized to a certain extent. Aims to further promote the application and research of self-compacting concrete

Model Compaction Equation

African Journals Online (AJOL)

The currently proposed model compaction equation was derived from data sourced from the. Niger Delta and it relates porosity to depth for sandstones under hydrostatic pressure condition. The equation is useful in predicting porosity and compaction trend in hydrostatic sands of the. Niger Delta. GEOLOGICAL SETTING OF ...

Microwave dynamics of high aspect ratio superconducting nanowires studied using self-resonance

Science.gov (United States)

Santavicca, Daniel F.; Adams, Jesse K.; Grant, Lierd E.; McCaughan, Adam N.; Berggren, Karl K.

2016-06-01

We study the microwave impedance of extremely high aspect ratio (length/width ≈ 5000) superconducting niobium nitride nanowires. The nanowires are fabricated in a compact meander geometry that is in series with the center conductor of a 50 Ω coplanar waveguide transmission line. The transmission coefficient of the sample is measured up to 20 GHz. At high frequency, a peak in the transmission coefficient is seen. Numerical simulations show that this is a half-wave resonance along the length of the nanowire, where the nanowire acts as a high impedance, slow wave transmission line. This resonance sets the upper frequency limit for these nanowires as inductive elements. Fitting simulations to the measured resonance enables a precise determination of the nanowire's complex sheet impedance at the resonance frequency. The real part is a measure of dissipation, while the imaginary part is dominated by kinetic inductance. We characterize the dependence of the sheet resistance and sheet inductance on both temperature and current and compare the results to recent theoretical predictions for disordered superconductors. These results can aid in the understanding of high frequency devices based on superconducting nanowires. They may also lead to the development of novel superconducting devices such as ultra-compact resonators and slow-wave structures.

Pyrolysis of tyre powder using microwave thermogravimetric analysis: Effect of microwave power.

Science.gov (United States)

Song, Zhanlong; Yang, Yaqing; Zhou, Long; Zhao, Xiqiang; Wang, Wenlong; Mao, Yanpeng; Ma, Chunyuan

2017-02-01

The pyrolytic characteristics of tyre powder treated under different microwave powers (300, 500, and 700 W) were studied via microwave thermogravimetric analysis. The product yields at different power levels were studied, along with comparative analysis of microwave pyrolysis and conventional pyrolysis. The feedstock underwent preheating, intense pyrolysis, and final pyrolysis in sequence. The main and secondary weight loss peaks observed during the intense pyrolysis stage were attributed to the decomposition of natural rubbers and synthetic rubbers, respectively. The total mass loss rates, bulk temperatures, and maximum temperatures were distinctively higher at higher powers. However, the maximum mass loss rate (0.005 s -1 ), the highest yields of liquid product (53%), and the minimum yields of residual solid samples (43.83%) were obtained at 500 W. Compared with conventional pyrolysis, microwave pyrolysis exhibited significantly different behaviour with faster reaction rates, which can decrease the decomposition temperatures of both natural and synthetic rubber by approximately 110 °C-140 °C.

Note: Coincidence measurements of 3He and neutrons from a compact D-D neutron generator

Science.gov (United States)

Ji, Q.; Lin, C.-J.; Tindall, C.; Garcia-Sciveres, M.; Schenkel, T.; Ludewigt, B. A.

2017-05-01

Tagging of neutrons (2.45 MeV) with their associated 3He particles from deuterium-deuterium (D-D) fusion reactions has been demonstrated in a compact neutron generator setup enabled by a high brightness, microwave-driven ion source with a high fraction of deuterons. Energy spectra with well separated peaks of the D-D fusion reaction products, 3He, tritons, and protons, were measured with a silicon PIN diode. The neutrons were detected using a liquid scintillator detector with pulse shape discrimination. By correlating the 3He detection events with the neutron detection in time, we demonstrated the tagging of emitted neutrons with 3He particles detected with a Si PIN diode detector mounted inside the neutron generator vacuum vessel.

Abatement of fluorinated compounds using a 2.45 GHz microwave plasma torch with a reverse vortex plasma reactor

Energy Technology Data Exchange (ETDEWEB)

Kim, J.H.; Cho, C.H.; Shin, D.H. [Plasma Technology Research Center, National Fusion Research Institute, 814-2 Oxikdo-dong, Gunsan-city, Jeollabuk-do (Korea, Republic of); Hong, Y.C., E-mail: ychong@nfri.re.kr [Plasma Technology Research Center, National Fusion Research Institute, 814-2 Oxikdo-dong, Gunsan-city, Jeollabuk-do (Korea, Republic of); Shin, Y.W. [Plasma Technology Research Center, National Fusion Research Institute, 814-2 Oxikdo-dong, Gunsan-city, Jeollabuk-do (Korea, Republic of); School of Advanced Green Energy and Environments, Handong Global University, Heunghae-eup, Buk-gu, Pohang-city, Gyeongbuk (Korea, Republic of)

2015-08-30

Highlights: • We developed a microwave plasma torch with reverse vortex reactor (RVR). • We calculated a volume fraction and temperature distribution of discharge gas and waste. • The performance of reverse vortex reactor increased from 29% to 43% than conventional vortex reactor. - Abstract: Abatement of fluorinated compounds (FCs) used in semiconductor and display industries has received an attention due to the increasingly stricter regulation on their emission. We have developed a 2.45 GHz microwave plasma torch with reverse vortex reactor (RVR). In order to design a reverse vortex plasma reactor, we calculated a volume fraction and temperature distribution of discharge gas and waste gas in RVR by ANSYS CFX of computational fluid dynamics (CFD) simulation code. Abatement experiments have been performed with respect to SF{sub 6}, NF{sub 3} by varying plasma power and N{sub 2} flow rates, and FCs concentration. Detailed experiments were conducted on the abatement of NF{sub 3} and SF{sub 6} in terms of destruction and removal efficiency (DRE) using Fourier transform infrared (FTIR). The DRE of 99.9% for NF{sub 3} was achieved without an additive gas at the N{sub 2} flow rate of 150 liter per minute (L/min) by applying a microwave power of 6 kW with RVR. Also, a DRE of SF{sub 6} was 99.99% at the N{sub 2} flow rate of 60 L/min using an applied microwave power of 6 kW. The performance of reverse vortex reactor increased about 43% of NF{sub 3} and 29% of SF{sub 6} abatements results definition by decomposition energy per liter more than conventional vortex reactor.

Improved foilless Ku-band transit-time oscillator for generating gigawatt level microwave with low guiding magnetic field

Energy Technology Data Exchange (ETDEWEB)

Ling, Junpu; He, Juntao, E-mail: hejuntao12@163.com; Zhang, Jiande; Jiang, Tao; Hu, Yi [College of Optoelectronic Science and Engineering, National University of Defense Technology, Changsha 410073 (China)

2014-09-15

An improved foilless Ku-band transit-time oscillator with low guiding magnetic field is proposed and investigated in this paper. With a non-uniform buncher and a coaxial TM{sub 02} mode dual-resonant reflector, this improved device can output gigawatt level Ku-band microwave with relatively compact radial dimensions. Besides the above virtue, this novel reflector also has the merits of high TEM reflectance, being more suitable for pre-modulating the electron beam and enhancing the conversion efficiency. Moreover, in order to further increase the conversion efficiency and lower the power saturation time, a depth-tunable coaxial collector and a resonant cavity located before the extractor are employed in our device. Main structure parameters of the device are optimized by particle in cell simulations. The typical simulation result is that, with a 380 kV, 8.2 kA beam guided by a magnetic field of about 0.6 T, 1.15 GW microwave pulse at 14.25 GHz is generated, yielding a conversion efficiency of about 37%.

Generalized Fourier slice theorem for cone-beam image reconstruction.

Science.gov (United States)

Zhao, Shuang-Ren; Jiang, Dazong; Yang, Kevin; Yang, Kang

2015-01-01

The cone-beam reconstruction theory has been proposed by Kirillov in 1961, Tuy in 1983, Feldkamp in 1984, Smith in 1985, Pierre Grangeat in 1990. The Fourier slice theorem is proposed by Bracewell 1956, which leads to the Fourier image reconstruction method for parallel-beam geometry. The Fourier slice theorem is extended to fan-beam geometry by Zhao in 1993 and 1995. By combining the above mentioned cone-beam image reconstruction theory and the above mentioned Fourier slice theory of fan-beam geometry, the Fourier slice theorem in cone-beam geometry is proposed by Zhao 1995 in short conference publication. This article offers the details of the derivation and implementation of this Fourier slice theorem for cone-beam geometry. Especially the problem of the reconstruction from Fourier domain has been overcome, which is that the value of in the origin of Fourier space is 0/0. The 0/0 type of limit is proper handled. As examples, the implementation results for the single circle and two perpendicular circle source orbits are shown. In the cone-beam reconstruction if a interpolation process is considered, the number of the calculations for the generalized Fourier slice theorem algorithm is O(N^4), which is close to the filtered back-projection method, here N is the image size of 1-dimension. However the interpolation process can be avoid, in that case the number of the calculations is O(N5).

Corrected Fourier series and its application to function approximation

Directory of Open Access Journals (Sweden)

Qing-Hua Zhang

2005-01-01

Full Text Available Any quasismooth function f(x in a finite interval [0,x0], which has only a finite number of finite discontinuities and has only a finite number of extremes, can be approximated by a uniformly convergent Fourier series and a correction function. The correction function consists of algebraic polynomials and Heaviside step functions and is required by the aperiodicity at the endpoints (i.e., f(0≠f(x0 and the finite discontinuities in between. The uniformly convergent Fourier series and the correction function are collectively referred to as the corrected Fourier series. We prove that in order for the mth derivative of the Fourier series to be uniformly convergent, the order of the polynomial need not exceed (m+1. In other words, including the no-more-than-(m+1 polynomial has eliminated the Gibbs phenomenon of the Fourier series until its mth derivative. The corrected Fourier series is then applied to function approximation; the procedures to determine the coefficients of the corrected Fourier series are illustrated in detail using examples.

Compact radiometric microwave calibrator

International Nuclear Information System (INIS)

Fixsen, D. J.; Wollack, E. J.; Kogut, A.; Limon, M.; Mirel, P.; Singal, J.; Fixsen, S. M.

2006-01-01

The calibration methods for the ARCADE II instrument are described and the accuracy estimated. The Steelcast coated aluminum cones which comprise the calibrator have a low reflection while maintaining 94% of the absorber volume within 5 mK of the base temperature (modeled). The calibrator demonstrates an absorber with the active part less than one wavelength thick and only marginally larger than the mouth of the largest horn and yet black (less than -40 dB or 0.01% reflection) over five octaves in frequency

Hyperfine structure measurements of neutral iodine atom (127I) using Fourier Transform Spectrometry

Science.gov (United States)

Ashok, Chilukoti; Vishwakarma, S. R.; Bhatt, Himal; Ankush, B. K.; Deo, M. N.

2018-01-01

We report the hyperfine Structure (hfs) splitting observations of neutral iodine atom (II) in the 6000 - 10,000 cm-1 near infrared spectral region. The measurements were carried out using a high-resolution Fourier Transform Spectrometer (FTS), where an electrodeless discharge lamp (EDL), excited using microwaves, was employed as the light source and InGaAs as the light detector. A specially designed setup was used to lower the plasma temperature of the medium so as to reduce the Doppler width and consequently to increase the spectral resolution of hfs components. A total of 183 lines with hfs splitting have been observed, out of which hfs in 53 spectral lines are reported for the first time. On the basis of hfs analysis, we derived the magnetic dipole and electric quadrupole coupling constants, A and B respectively for 30 even and 30 odd energy levels and are compared with the values available in the literature. New hfs values for 5 even and 4 odd levels are also reported here for the first time.

Digital microwave communication engineering point-to-point microwave systems

CERN Document Server

Kizer, George

2013-01-01

The first book to cover all engineering aspects of microwave communication path design for the digital age Fixed point-to-point microwave systems provide moderate-capacity digital transmission between well-defined locations. Most popular in situations where fiber optics or satellite communication is impractical, it is commonly used for cellular or PCS site interconnectivity where digital connectivity is needed but not economically available from other sources, and in private networks where reliability is most important. Until now, no book has adequately treated all en

Fourier transforms in radar and signal processing

CERN Document Server

Brandwood, David

2011-01-01

Fourier transforms are used widely, and are of particular value in the analysis of single functions and combinations of functions found in radar and signal processing. Still, many problems that could have been tackled by using Fourier transforms may have gone unsolved because they require integration that is difficult and tedious. This newly revised and expanded edition of a classic Artech House book provides you with an up-to-date, coordinated system for performing Fourier transforms on a wide variety of functions. Along numerous updates throughout the book, the Second Edition includes a crit

PROGRAMMING THE MICROWAVE-OVEN

NARCIS (Netherlands)

KOK, LP; VISSER, PE; BOON, ME

1994-01-01

Microwaves can be used to stimulate chemical bonding, diffusion of reagents into and out of the specimen, and coagulation processes in preparatory techniques. Temperature plays an important role in these processes. There are several ways of controlling the temperature of microwave-exposed tissue,

Microwave Enhanced Reactive Distillation

NARCIS (Netherlands)

Altman, E.

2011-01-01

The application of electromagnetic irradiation in form of microwaves (MW) has gathered the attention of the scientific community in recent years. MW used as an alternative energy source for chemical syntheses (microwave chemistry) can provide clear advantages over conventional heating methods in

MICROWAVES IN ORGANIC SYNTHESIS

Science.gov (United States)

The effect of microwaves, a non-ionizing radiation, on organic reactions is described both in polar solvents and under solvent-free conditions. The special applications are highlighted in the context of solventless organic synthesis which involve microwave (MW) exposure of neat r...

Comparison of microwave hydrodistillation and solvent-free microwave extraction of essential oil from Melaleuca leucadendra Linn

Science.gov (United States)

Ismanto, A. W.; Kusuma, H. S.; Mahfud, M.

2017-12-01

The comparison of solvent-free microwave extraction (SFME) and microwave hydrodistillation (MHD) in the extraction of essential oil from Melaleuca leucadendra Linn. was examined. Dry cajuput leaves were used in this study. The purpose of this study is also to determine optimal condition (microwave power). The relative electric consumption of SFME and MHD methods are both showing 0,1627 kWh/g and 0,3279 kWh/g. The results showed that solvent-free microwave extraction methods able to reduce energy consumption and can be regarded as a green technique for extraction of cajuput oil.

Pharmaceutical powder compaction technology

National Research Council Canada - National Science Library

Çelik, Metin

2011-01-01

... through the compaction formulation process and application. Compaction of powder constituents both active ingredient and excipients is examined to ensure consistent and reproducible disintegration and dispersion profiles...

Quantum teleportation of propagating quantum microwaves

Energy Technology Data Exchange (ETDEWEB)

Di Candia, R.; Felicetti, S.; Sanz, M. [University of the Basque Country UPV/EHU, Department of Physical Chemistry, Bilbao (Spain); Fedorov, K.G.; Menzel, E.P. [Bayerische Akademie der Wissenschaften, Walther-Meissner-Institut, Garching (Germany); Technische Universitaet Muenchen, Physik-Department, Garching (Germany); Zhong, L.; Deppe, F.; Gross, R. [Bayerische Akademie der Wissenschaften, Walther-Meissner-Institut, Garching (Germany); Technische Universitaet Muenchen, Physik-Department, Garching (Germany); Nanosystems Initiative Munich (NIM), Muenchen (Germany); Marx, A. [Bayerische Akademie der Wissenschaften, Walther-Meissner-Institut, Garching (Germany); Solano, E. [University of the Basque Country UPV/EHU, Department of Physical Chemistry, Bilbao (Spain); Basque Foundation for Science, IKERBASQUE, Bilbao (Spain)

2015-12-15

Propagating quantum microwaves have been proposed and successfully implemented to generate entanglement, thereby establishing a promising platform for the realisation of a quantum communication channel. However, the implementation of quantum teleportation with photons in the microwave regime is still absent. At the same time, recent developments in the field show that this key protocol could be feasible with current technology, which would pave the way to boost the field of microwave quantum communication. Here, we discuss the feasibility of a possible implementation of microwave quantum teleportation in a realistic scenario with losses. Furthermore, we propose how to implement quantum repeaters in the microwave regime without using photodetection, a key prerequisite to achieve long distance entanglement distribution. (orig.)

Quantum teleportation of propagating quantum microwaves

International Nuclear Information System (INIS)

Di Candia, R.; Felicetti, S.; Sanz, M.; Fedorov, K.G.; Menzel, E.P.; Zhong, L.; Deppe, F.; Gross, R.; Marx, A.; Solano, E.

2015-01-01

Propagating quantum microwaves have been proposed and successfully implemented to generate entanglement, thereby establishing a promising platform for the realisation of a quantum communication channel. However, the implementation of quantum teleportation with photons in the microwave regime is still absent. At the same time, recent developments in the field show that this key protocol could be feasible with current technology, which would pave the way to boost the field of microwave quantum communication. Here, we discuss the feasibility of a possible implementation of microwave quantum teleportation in a realistic scenario with losses. Furthermore, we propose how to implement quantum repeaters in the microwave regime without using photodetection, a key prerequisite to achieve long distance entanglement distribution. (orig.)

The microwave era is just beginning

International Nuclear Information System (INIS)

Grad, P.

1989-01-01

Microwave energy applicators in curing rubber products and in ceramic manufacture are enunciated by some of the participants at the First Australian Symposium on Microwave Power Applications held in February 1989 at Wollongong. The advantages and disadvantages of microwave heating over conventional methods are stated

Nanostructure sword-like ZnO wires: Rapid synthesis and characterization through a microwave-assisted route

International Nuclear Information System (INIS)

Kajbafvala, Amir; Shayegh, Mohammad Reza; Mazloumi, Mahyar; Zanganeh, Saeid; Lak, Aidin; Mohajerani, Matin Sadat; Sadrnezhaad, S.K.

2009-01-01

Nanostructure sword-like ZnO wires with diameters of about 80-250 nm and the length of ∼1-4 μm have been synthesized by a fast, simple and template-free microwave-assisted method. X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy and room temperature photoluminescence (PL) measurements was used for characterization of the as-prepared products. The nanostructure sword-like ZnO wires have high crystallinity with the average crystallite size of about 53 nm and show a UV emission and a visible green band in their PL spectrum. The possible growth mechanism of the nanostructures along the crystallographic direction and subsequent formation of wires were also investigated

The broadband microwave spectra of the monoterpenoids thymol and carvacrol: Conformational landscape and internal dynamics

Energy Technology Data Exchange (ETDEWEB)

Schmitz, D.; Shubert, V. A. [Max Planck Institute for the Structure and Dynamics of Matter, Hamburg (Germany); The Center for Free-Electron Laser Science, Hamburg (Germany); Giuliano, B. M. [Center for Astrobiology, INTA-CSIC, Torrejón de Ardoz, Madrid (Spain); Schnell, M., E-mail: melanie.schnell@mpsd.mpg.de [Max Planck Institute for the Structure and Dynamics of Matter, Hamburg (Germany); The Center for Free-Electron Laser Science, Hamburg (Germany); The Hamburg Centre for Ultrafast Imaging, Universität Hamburg, Hamburg (Germany)

2014-07-21

The rotational spectra of the monoterpenoids thymol and carvacrol are reported in the frequency range 2–8.5 GHz, obtained with broadband Fourier-transform microwave spectroscopy. For carvacrol four different conformations were identified in the cold conditions of the molecular jet, whereas only three conformations were observed for thymol. The rotational constants and other molecular parameters are reported and compared with quantum chemical calculations. For both molecules, line splittings due to methyl group internal rotation were observed and the resulting barrier heights could be determined. The experimental barrier heights, 4.0863(25) kJ/mol for trans-carvacrol-A, 4.4024(16) kJ/mol for trans-carvacrol-B, and 0.3699(11) kJ/mol for trans-thymol-A, are compared with similar molecules.

The broadband microwave spectra of the monoterpenoids thymol and carvacrol: Conformational landscape and internal dynamics

International Nuclear Information System (INIS)

Schmitz, D.; Shubert, V. A.; Giuliano, B. M.; Schnell, M.

2014-01-01

The rotational spectra of the monoterpenoids thymol and carvacrol are reported in the frequency range 2–8.5 GHz, obtained with broadband Fourier-transform microwave spectroscopy. For carvacrol four different conformations were identified in the cold conditions of the molecular jet, whereas only three conformations were observed for thymol. The rotational constants and other molecular parameters are reported and compared with quantum chemical calculations. For both molecules, line splittings due to methyl group internal rotation were observed and the resulting barrier heights could be determined. The experimental barrier heights, 4.0863(25) kJ/mol for trans-carvacrol-A, 4.4024(16) kJ/mol for trans-carvacrol-B, and 0.3699(11) kJ/mol for trans-thymol-A, are compared with similar molecules

Fan beam image reconstruction with generalized Fourier slice theorem.

Science.gov (United States)

Zhao, Shuangren; Yang, Kang; Yang, Kevin

2014-01-01

For parallel beam geometry the Fourier reconstruction works via the Fourier slice theorem (or central slice theorem, projection slice theorem). For fan beam situation, Fourier slice can be extended to a generalized Fourier slice theorem (GFST) for fan-beam image reconstruction. We have briefly introduced this method in a conference. This paper reintroduces the GFST method for fan beam geometry in details. The GFST method can be described as following: the Fourier plane is filled by adding up the contributions from all fanbeam projections individually; thereby the values in the Fourier plane are directly calculated for Cartesian coordinates such avoiding the interpolation from polar to Cartesian coordinates in the Fourier domain; inverse fast Fourier transform is applied to the image in Fourier plane and leads to a reconstructed image in spacial domain. The reconstructed image is compared between the result of the GFST method and the result from the filtered backprojection (FBP) method. The major differences of the GFST and the FBP methods are: (1) The interpolation process are at different data sets. The interpolation of the GFST method is at projection data. The interpolation of the FBP method is at filtered projection data. (2) The filtering process are done in different places. The filtering process of the GFST is at Fourier domain. The filtering process of the FBP method is the ramp filter which is done at projections. The resolution of ramp filter is variable with different location but the filter in the Fourier domain lead to resolution invariable with location. One advantage of the GFST method over the FBP method is in short scan situation, an exact solution can be obtained with the GFST method, but it can not be obtained with the FBP method. The calculation of both the GFST and the FBP methods are at O(N^3), where N is the number of pixel in one dimension.

Fourier spectral simulations for wake fields in conducting cavities

International Nuclear Information System (INIS)

Min, M.; Chin, Y.-H.; Fischer, P.F.; Chae, Y.-Chul; Kim, K.-J.

2007-01-01

We investigate Fourier spectral time-domain simulations applied to wake field calculations in two-dimensional cylindrical structures. The scheme involves second-order explicit leap-frogging in time and Fourier spectral approximation in space, which is obtained from simply replacing the spatial differentiation operator of the YEE scheme by the Fourier differentiation operator on nonstaggered grids. This is a first step toward investigating high-order computational techniques with the Fourier spectral method, which is relatively simple to implement.

Microwave power engineering generation, transmission, rectification

CERN Document Server

Okress, Ernest C

1968-01-01

Microwave Power Engineering, Volume 1: Generation, Transmission, Rectification considers the components, systems, and applications and the prevailing limitations of the microwave power technology. This book contains four chapters and begins with an introduction to the basic concept and developments of microwave power technology. The second chapter deals with the development of the main classes of high-power microwave and optical frequency power generators, such as magnetrons, crossed-field amplifiers, klystrons, beam plasma amplifiers, crossed-field noise sources, triodes, lasers. The third

Anisotropic Material Behavior of Uni-axially Compacted Graphite Matrix for HTGR Fuel Compact Fabrication

Energy Technology Data Exchange (ETDEWEB)

Lee, Young-Woo; Yeo, Seunghwan; Yoon, Ji-Hae; Cho, Moon Sung [KAERI, Daejeon (Korea, Republic of)

2016-05-15

In developing the fuel compact fabrication technology, and fuel graphite material to meet the required material properties, it is essential to investigate the relationship among the process parameters of the matrix graphite powder preparation, the fabrication parameters of fuel element green compact and the heat treatments conditions and the material properties of fuel element. It was observed, during this development, that the pressing technique employed for the compaction fabrication prior to the two successive heat treatments (carbonization and final high temperature heat treatment) was of extreme importance in determining the material properties of the final compact product. In this work, the material behavior of the uni-axially pressed graphite matrix during the carbonization and final heat treatment are evaluated and summarized along the different directions, viz., perpendicular and parallel directions to pressing direction. In this work, the dimensional variations and variations in thermal expansion, thermal conductivity and Vickers hardness of the graphite matrix compact samples in the axial and radial directions prepared by uni-axial pressing are evaluated, and compared with those of samples prepared by cold isostatic pressing with the available data. From this work, the followings are observed. 1) Dimensional changes of matrix graphite green compacts during carbonization show that the difference in radial and axial variations shows a large anisotropic behavior in shrinkage. The radial variation is very small while the axial variation is large. During carbonization, the stresses caused by the force would be released in to the axial direction together with the phenolic resin vapor. 2) Dimensional variation of compact samples in perpendicular and parallel directions during carbonization shows a large difference in behavior when compact sample is prepared by uni-axial pressing. However, when compact sample is prepared by cold isostatic pressing, there is

Anisotropic Material Behavior of Uni-axially Compacted Graphite Matrix for HTGR Fuel Compact Fabrication

International Nuclear Information System (INIS)

Lee, Young-Woo; Yeo, Seunghwan; Yoon, Ji-Hae; Cho, Moon Sung

2016-01-01

In developing the fuel compact fabrication technology, and fuel graphite material to meet the required material properties, it is essential to investigate the relationship among the process parameters of the matrix graphite powder preparation, the fabrication parameters of fuel element green compact and the heat treatments conditions and the material properties of fuel element. It was observed, during this development, that the pressing technique employed for the compaction fabrication prior to the two successive heat treatments (carbonization and final high temperature heat treatment) was of extreme importance in determining the material properties of the final compact product. In this work, the material behavior of the uni-axially pressed graphite matrix during the carbonization and final heat treatment are evaluated and summarized along the different directions, viz., perpendicular and parallel directions to pressing direction. In this work, the dimensional variations and variations in thermal expansion, thermal conductivity and Vickers hardness of the graphite matrix compact samples in the axial and radial directions prepared by uni-axial pressing are evaluated, and compared with those of samples prepared by cold isostatic pressing with the available data. From this work, the followings are observed. 1) Dimensional changes of matrix graphite green compacts during carbonization show that the difference in radial and axial variations shows a large anisotropic behavior in shrinkage. The radial variation is very small while the axial variation is large. During carbonization, the stresses caused by the force would be released in to the axial direction together with the phenolic resin vapor. 2) Dimensional variation of compact samples in perpendicular and parallel directions during carbonization shows a large difference in behavior when compact sample is prepared by uni-axial pressing. However, when compact sample is prepared by cold isostatic pressing, there is

Fourier series and orthogonal polynomials

CERN Document Server

Jackson, Dunham

2004-01-01

This text for undergraduate and graduate students illustrates the fundamental simplicity of the properties of orthogonal functions and their developments in related series. Starting with a definition and explanation of the elements of Fourier series, the text follows with examinations of Legendre polynomials and Bessel functions. Boundary value problems consider Fourier series in conjunction with Laplace's equation in an infinite strip and in a rectangle, with a vibrating string, in three dimensions, in a sphere, and in other circumstances. An overview of Pearson frequency functions is followe

Microwave-assisted organic and polymer chemistry

NARCIS (Netherlands)

Hoogenboom, R.; Schubert, U.S.

2009-01-01

The first ACS symposium on Microwave-Assisted Chemistry: Organic and Polymer Synthesis, held as part of the ACS National meeting in Philadelphia, in August 2008, aimed at various topics of the use of microwave irradiation. The symposium found that specific heating effects, such as higher microwave

Balanced microwave filters

CERN Document Server

Hong, Jiasheng; Medina, Francisco; Martiacuten, Ferran

2018-01-01

This book presents and discusses strategies for the design and implementation of common-mode suppressed balanced microwave filters, including, narrowband, wideband, and ultra-wideband filters This book examines differential-mode, or balanced, microwave filters by discussing several implementations of practical realizations of these passive components. Topics covered include selective mode suppression, designs based on distributed and semi-lumped approaches, multilayer technologies, defect ground structures, coupled resonators, metamaterials, interference techniques, and substrate integrated waveguides, among others. Divided into five parts, Balanced Microwave Filters begins with an introduction that presents the fundamentals of balanced lines, circuits, and networks. Part 2 covers balanced transmission lines with common-mode noise suppression, including several types of common-mode filters and the application of such filters to enhance common-mode suppression in balanced bandpass filters. Next, Part 3 exa...

Coupled microwave/photoassisted methods for environmental remediation.

Science.gov (United States)

Horikoshi, Satoshi; Serpone, Nick

2014-11-05

The microwave-induced acceleration of photocatalytic reactions was discovered serendipitously in the late 1990s. The activity of photocatalysts is enhanced significantly by both microwave radiation and UV light. Particularly relevant, other than as a heat source, was the enigmatic phenomenon of the non-thermal effect(s) of the microwave radiation that facilitated photocatalyzed reactions, as evidenced when examining various model contaminants in aqueous media. Results led to an examination of the possible mechanism(s) of the microwave effect(s). In the present article we contend that the microwaves' non-thermal effect(s) is an important factor in the enhancement of TiO2-photoassisted reactions involving the decomposition of organic pollutants in model wastewaters by an integrated (coupled) microwave-/UV-illumination method (UV/MW). Moreover, such coupling of no less than two irradiation methods led to the fabrication and ultimate investigation of microwave discharged electrodeless lamps (MDELs) as optimal light sources; their use is also described. The review focuses on the enhanced activity of photocatalytic reactions when subjected to microwave radiation and concentrates on the authors' research of the past few years.

Mechanism for microwave heating of 1-(4'-cyanophenyl)-4-propylcyclohexane characterized by in situ microwave irradiation NMR spectroscopy.

Science.gov (United States)

Tasei, Yugo; Yamakami, Takuya; Kawamura, Izuru; Fujito, Teruaki; Ushida, Kiminori; Sato, Motoyasu; Naito, Akira

2015-05-01

Microwave heating is widely used to accelerate organic reactions and enhance the activity of enzymes. However, the detailed molecular mechanism for the effect of microwave on chemical reactions is not yet fully understood. To investigate the effects of microwave heating on organic compounds, we have developed an in situ microwave irradiation NMR spectroscopy. (1)H NMR spectra of 1-(4'-cyanophenyl)-4-propylcyclohexane (PCH3) in the liquid crystalline and isotropic phases were observed under microwave irradiation. When the temperature was regulated at slightly higher than the phase transition temperature (Tc=45 °C) under a gas flow temperature control system, liquid crystalline phase mostly changed to the isotropic phase. Under microwave irradiation and with the gas flow temperature maintained at 20 °C, which is 25 °C below the Tc, the isotropic phase appeared stationary as an approximately 2% fraction in the liquid crystalline phase. The temperature of the liquid crystalline state was estimated to be 38 °C according to the line width, which is at least 7 °C lower than the Tc. The temperature of this isotropic phase should be higher than 45 °C, which is considered to be a non-equilibrium local heating state induced by microwave irradiation. Microwaves at a power of 195 W were irradiated to the isotropic phase of PCH3 at 50 °C and after 2 min, the temperature reached 220 °C. The temperature of PCH3 under microwave irradiation was estimated by measurement of the chemical shift changes of individual protons in the molecule. These results demonstrate that microwave heating generates very high temperature within a short time using an in situ microwave irradiation NMR spectrometer. Copyright © 2015 Elsevier Inc. All rights reserved.

Recent results of studies of plasma fluctuations in stellarators by microwave scattering technique

International Nuclear Information System (INIS)

Skvortsova, N.N.; Batanov, G.M.; Kolik, L.V.; Petrov, A.E.; Pshenichnikov, A.A.; Sarksyan, K.A.; Kharchev, N.K.; Khol'nov, Yu.V.; Kubo, S.; Sanchez, J.

2005-01-01

Microwave scattering diagnostics are described that allow direct measurements of the turbulent processes in a high-temperature plasma of magnetic confinement systems. Plasma density fluctuations in the heating region of the L-2M stellarator were measured from microwave scattering at the fundamental and the second harmonics of the heating gyrotron radiation. In the TJ-II stellarator, a separate 2-mm microwave source was used to produce a probing beam; the measurements were performed at the middle of the plasma radius. Plasma density fluctuations in the axial (heating) region of the LHD stellarator were measured from microwave scattering at the fundamental harmonic of the heating gyrotron radiation. Characteristic features of fluctuations, common for all three devices, are revealed with the methods of statistical and spectral analysis. These features are the wide frequency Fourier and wavelet spectra, autocorrelation functions with slowly decreasing tails, and non-Gaussian probability distributions of the magnitudes and the increments of the magnitude of fluctuations. The drift-dissipative instability and the instability driven by trapped electrons are examined as possible sources of turbulence in a high-temperature plasma. Observations showed the high level of coherence between turbulent fluctuations in the central region and at the edge of the plasma in L-2M. It is shown in L-2M that the relative intensity of the second harmonic of gyrotron radiation on the axis of a microwave beam after quasi-optical filtering in a four-mirror quasi-optical transmission line is about -50 dB of the total radiation intensity. Spatiotemporal structures in plasma density fluctuations were observed in the central region of the plasma column. The correlation time between the structures was found to be on the order of 1 ms. It is shown that, the spectrum of the signal from the second-harmonic scattering extends to higher frequencies in comparison with that from the fundamental

Weakly compact operators and interpolation

OpenAIRE

Maligranda, Lech

1992-01-01

The class of weakly compact operators is, as well as the class of compact operators, a fundamental operator ideal. They were investigated strongly in the last twenty years. In this survey, we have collected and ordered some of this (partly very new) knowledge. We have also included some comments, remarks and examples. The class of weakly compact operators is, as well as the class of compact operators, a fundamental operator ideal. They were investigated strongly in the last twenty years. I...

Tunable Multiband Microwave Photonic Filters

Directory of Open Access Journals (Sweden)

Mable P. Fok

2017-11-01

Full Text Available The increasing demand for multifunctional devices, the use of cognitive wireless technology to solve the frequency resource shortage problem, as well as the capabilities and operational flexibility necessary to meet ever-changing environment result in an urgent need of multiband wireless communications. Spectral filter is an essential part of any communication systems, and in the case of multiband wireless communications, tunable multiband RF filters are required for channel selection, noise/interference removal, and RF signal processing. Unfortunately, it is difficult for RF electronics to achieve both tunable and multiband spectral filtering. Recent advancements of microwave photonics have proven itself to be a promising candidate to solve various challenges in RF electronics including spectral filtering, however, the development of multiband microwave photonic filtering still faces lots of difficulties, due to the limited scalability and tunability of existing microwave photonic schemes. In this review paper, we first discuss the challenges that were facing by multiband microwave photonic filter, then we review recent techniques that have been developed to tackle the challenge and lead to promising developments of tunable microwave photonic multiband filters. The successful design and implementation of tunable microwave photonic multiband filter facilitate the vision of dynamic multiband wireless communications and radio frequency signal processing for commercial, defense, and civilian applications.

q-Generalization of the inverse Fourier transform

International Nuclear Information System (INIS)

Jauregui, M.; Tsallis, C.

2011-01-01

A wide class of physical distributions appears to follow the q-Gaussian form, which plays the role of attractor according to a q-generalized Central Limit Theorem, where a q-generalized Fourier transform plays an important role. We introduce here a method which determines a distribution from the knowledge of its q-Fourier transform and some supplementary information. This procedure involves a recently q-generalized representation of the Dirac delta and the class of functions on which it acts. The present method conveniently extends the inverse of the standard Fourier transform, and is therefore expected to be very useful in the study of many complex systems. - Highlights: → We present a method to invert the q-Fourier transform of a distribution. → We illustrate when Dirac delta can be represented using q-exponentials. → We describe a family of functions for which this new representation works.

Fast Fourier single-pixel imaging via binary illumination.

Science.gov (United States)

Zhang, Zibang; Wang, Xueying; Zheng, Guoan; Zhong, Jingang

2017-09-20

Fourier single-pixel imaging (FSI) employs Fourier basis patterns for encoding spatial information and is capable of reconstructing high-quality two-dimensional and three-dimensional images. Fourier-domain sparsity in natural scenes allows FSI to recover sharp images from undersampled data. The original FSI demonstration, however, requires grayscale Fourier basis patterns for illumination. This requirement imposes a limitation on the imaging speed as digital micro-mirror devices (DMDs) generate grayscale patterns at a low refreshing rate. In this paper, we report a new strategy to increase the speed of FSI by two orders of magnitude. In this strategy, we binarize the Fourier basis patterns based on upsampling and error diffusion dithering. We demonstrate a 20,000 Hz projection rate using a DMD and capture 256-by-256-pixel dynamic scenes at a speed of 10 frames per second. The reported technique substantially accelerates image acquisition speed of FSI. It may find broad imaging applications at wavebands that are not accessible using conventional two-dimensional image sensors.

Modeling and prediction of extraction profile for microwave-assisted extraction based on absorbed microwave energy.

Science.gov (United States)

Chan, Chung-Hung; Yusoff, Rozita; Ngoh, Gek-Cheng

2013-09-01

A modeling technique based on absorbed microwave energy was proposed to model microwave-assisted extraction (MAE) of antioxidant compounds from cocoa (Theobroma cacao L.) leaves. By adapting suitable extraction model at the basis of microwave energy absorbed during extraction, the model can be developed to predict extraction profile of MAE at various microwave irradiation power (100-600 W) and solvent loading (100-300 ml). Verification with experimental data confirmed that the prediction was accurate in capturing the extraction profile of MAE (R-square value greater than 0.87). Besides, the predicted yields from the model showed good agreement with the experimental results with less than 10% deviation observed. Furthermore, suitable extraction times to ensure high extraction yield at various MAE conditions can be estimated based on absorbed microwave energy. The estimation is feasible as more than 85% of active compounds can be extracted when compared with the conventional extraction technique. Copyright © 2013 Elsevier Ltd. All rights reserved.

Microwave assisted centrifuge and related methods

Science.gov (United States)

Meikrantz, David H [Idaho Falls, ID

2010-08-17

Centrifuge samples may be exposed to microwave energy to heat the samples during centrifugation and to promote separation of the different components or constituents of the samples using a centrifuge device configured for generating microwave energy and directing the microwave energy at a sample located in the centrifuge.

Prospects of microwave processing: An overview

Indian Academy of Sciences (India)

Administrator

wave heating. In addition, microwave energy is being explored for the sintering of metal powders also. Ceramic and metal nanopowders have been sintered in microwave. Furthermore, initiatives have been taken to process the amorphous materials (e.g. glass) by microwave heating. Besides this, an attempt has been made ...

Understanding the microwave annealing of silicon

Directory of Open Access Journals (Sweden)

Chaochao Fu

2017-03-01

Full Text Available Though microwave annealing appears to be very appealing due to its unique features, lacking an in-depth understanding and accurate model hinder its application in semiconductor processing. In this paper, the physics-based model and accurate calculation for the microwave annealing of silicon are presented. Both thermal effects, including ohmic conduction loss and dielectric polarization loss, and non-thermal effects are thoroughly analyzed. We designed unique experiments to verify the mechanism and extract relevant parameters. We also explicitly illustrate the dynamic interaction processes of the microwave annealing of silicon. This work provides an in-depth understanding that can expedite the application of microwave annealing in semiconductor processing and open the door to implementing microwave annealing for future research and applications.

The Entropy of Co-Compact Open Covers

Directory of Open Access Journals (Sweden)

Steven Bourquin

2013-06-01

Full Text Available Co-compact entropy is introduced as an invariant of topological conjugation for perfect mappings defined on any Hausdorff space (compactness and metrizability are not necessarily required. This is achieved through the consideration of co-compact covers of the space. The advantages of co-compact entropy include: (1 it does not require the space to be compact and, thus, generalizes Adler, Konheim and McAndrew’s topological entropy of continuous mappings on compact dynamical systems; and (2 it is an invariant of topological conjugation, compared to Bowen’s entropy, which is metric-dependent. Other properties of co-compact entropy are investigated, e.g., the co-compact entropy of a subsystem does not exceed that of the whole system. For the linear system, (R; f, defined by f(x = 2x, the co-compact entropy is zero, while Bowen’s entropy for this system is at least log 2. More generally, it is found that co-compact entropy is a lower bound of Bowen’s entropies, and the proof of this result also generates the Lebesgue Covering Theorem to co-compact open covers of non-compact metric spaces.

47 CFR 101.141 - Microwave modulation.

Science.gov (United States)

2010-10-01

... 47 Telecommunication 5 2010-10-01 2010-10-01 false Microwave modulation. 101.141 Section 101.141... SERVICES Technical Standards § 101.141 Microwave modulation. (a) Microwave transmitters employing digital modulation techniques and operating below 25.25 GHz (except for MVDDS stations in the 12,200-12,700 MHz band...

Double Fourier analysis for Emotion Identification in Voiced Speech

International Nuclear Information System (INIS)

Sierra-Sosa, D.; Bastidas, M.; Ortiz P, D.; Quintero, O.L.

2016-01-01

We propose a novel analysis alternative, based on two Fourier Transforms for emotion recognition from speech. Fourier analysis allows for display and synthesizes different signals, in terms of power spectral density distributions. A spectrogram of the voice signal is obtained performing a short time Fourier Transform with Gaussian windows, this spectrogram portraits frequency related features, such as vocal tract resonances and quasi-periodic excitations during voiced sounds. Emotions induce such characteristics in speech, which become apparent in spectrogram time-frequency distributions. Later, the signal time-frequency representation from spectrogram is considered an image, and processed through a 2-dimensional Fourier Transform in order to perform the spatial Fourier analysis from it. Finally features related with emotions in voiced speech are extracted and presented. (paper)

Pulsed microwave discharge at atmospheric pressure for NOx decomposition

International Nuclear Information System (INIS)

Baeva, M; Gier, H; Pott, A; Uhlenbusch, J; Hoeschele, J; Steinwandel, J

2002-01-01

A 3.0 GHz pulsed microwave source operated at atmospheric pressure with a pulse power of 1.4 MW, a maximum repetition rate of 40 Hz, and a pulse length of 3.5 μs is experimentally studied with respect to the ability to remove NO x from synthetic exhaust gases. Experiments in gas mixtures containing N 2 /O 2 /NO with typically 500 ppm NO are carried out. The discharge is embedded in a high-Q microwave resonator, which provides a reliable plasma ignition. Vortex flow is applied to the exhaust gas to improve gas treatment. Concentration measurements by Fourier transform infrared spectroscopy confirm an NO x reduction of more than 90% in the case of N 2 /NO mixtures. The admixture of oxygen lowers the reductive potential of the reactor, but NO x reduction can still be observed up to 9% O 2 concentration. Coherent anti-Stokes Raman scattering technique is applied to measure the vibrational and rotational temperature of N 2 . Gas temperatures of about 400 K are found, whilst the vibrational temperature is 3000-3500 K in pure N 2 . The vibrational temperature drops to 1500 K when O 2 and/or NO are present. The randomly distributed relative frequency of occurrence of selected breakdown field intensities is measured by a calibrated, short linear-antenna. The breakdown field strength in pure N 2 amounts to 2.2x10 6 V m -1 , a value that is reproducible within 2%. In the case of O 2 and/or NO admixture, the frequency distribution of the breakdown field strength scatters more and extends over a range from 3 to 8x10 6 V m -1

Microwave-assisted one-pot synthesis of metal/metal oxide nanoparticles on graphene and their electrochemical applications

International Nuclear Information System (INIS)

Wang Shuangyin; Jiang San Ping; Wang Xin

2011-01-01

Graphical abstract: Display Omitted Research highlights: → Microwave polyol method is efficient to deposit nanoparticles on graphene. → SnO 2 /graphene is more efficient than graphene for supercapacitor. → PtRu/graphene is more active than commercial PtRu/C for methanol oxidation. - Abstract: An effective synthesis strategy of hybrid metal (PtRu)/metal oxide (SnO 2 ) nanoparticles on graphene nanocomposites is developed using a microwave-assisted one-pot reaction process. The mixture of ethylene glycol (EG) and water is used as both solvent and reactant. In the reaction system for the synthesis of SnO 2 /graphene nanocomposite, EG not only reduces graphene oxide (GO) to graphene, but also results in the formation of SnO 2 facilitated by the presence of a small amount of water. On the other hand, in the reaction system for preparation of PtRu/graphene nanocomposites, EG acts as solvent and reducing agent for reduction of PtRu nanoparticles from their precursors and reduction of graphene from graphene oxide. Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and transmission electron microscopy (TEM) characterizations confirm the feasibility of the microwave-assisted reaction system to simultaneously reduce graphene oxide and to form SnO 2 or PtRu nanoparticles. The as-synthesized SnO 2 /graphene hybrid composites show a much higher supercapacitance than the pure graphene, and the as-prepared PtRu/graphene show much better electrocatalytic activity for methanol oxidation compared to the commercial E-TEK PtRu/C electrocatalysts.

Microwave-gamma ray water in crude monitor

International Nuclear Information System (INIS)

Paap, H.J.

1984-01-01

A microwave-gamma ray water-in-crude monitoring system measures the percent quantity of fresh water or salt water in crude oil flowing in a pipe line. The system includes a measuring cell arranged with the pipe line so that the crude oil flows through the measuring cell. A microwave transmitter subsystem and a gamma ray source are arranged with the measuring cell so that microwave energy and gamma rays are transmitted through the measuring cell. A microwave receiving subsystem and a gamma ray detector provide signals corresponding to received microwave energy and to the received gamma rays, respectively. Apparatus connected to the microwave receiver and to the gamma ray detector provides an indication of the percentage of water in the crude oil

Microwave heating in solid-phase peptide synthesis

DEFF Research Database (Denmark)

Pedersen, Søren Ljungberg; Shelton, Anne Pernille Tofteng; Malik, Leila

2012-01-01

synthesis, precise microwave irradiation to heat the reaction mixture during coupling and N(a)-deprotection has become increasingly popular. It has often provided dramatic reductions in synthesis times, accompanied by an increase in the crude peptide purity. Microwave heating has been proven especially...... relevant for sequences which might form ß-sheet type structures and for sterically difficult couplings. The beneficial effect of microwave heating appears so far to be due to the precise nature of this type of heating, rather than a peptide-specific microwave effect. However, microwave heating...... in microwave heating for peptide synthesis, with a focus on systematic studies and general protocols, as well as important applications. The assembly of ß-peptides, peptoids and pseudopeptides are also evaluated in this critical review (254 references)....

Development and studies on a compact electron cyclotron resonance plasma source

Science.gov (United States)

Ganguli, A.; Tarey, R. D.; Arora, N.; Narayanan, R.

2016-04-01

It is well known that electron cyclotron resonance (ECR) produced plasmas are efficient, high-density plasma sources and have many industrial applications. The concept of a portable compact ECR plasma source (CEPS) would thus become important from an application point of view. This paper gives details of such a CEPS that is both portable and easily mountable on a chamber of any size. It uses a fully integrated microwave line operating at 2.45 GHz, up to 800 W, cw. The required magnetic field is produced by a set of suitably designed NdFeB ring magnets; the device has an overall length of  ≈60 cm and weighs  ≈14 kg including the permanent magnets. The CEPS was attached to a small experimental chamber to judge its efficacy for plasma production. In the pressure range of 0.5-10 mTorr and microwave power of  ≈400-500 W the experiments indicate that the CEPS is capable of producing high-density plasma (≈9  ×  1011-1012 cm-3) with bulk electron temperature in the range  ≈2-3 eV. In addition, a warm electron population with density and temperature in the range ≈7  ×  108-109 cm-3 and  ≈45-80 eV, respectively has been detected. This warm population plays an important role at high pressures in maintaining the high-density plasma, when plasma flow from the CEPS into the test chamber is strongly affected.

Empirical modeling of drying kinetics and microwave assisted extraction of bioactive compounds from Adathoda vasica

Directory of Open Access Journals (Sweden)

Prithvi Simha

2016-03-01

Full Text Available To highlight the shortcomings in conventional methods of extraction, this study investigates the efficacy of Microwave Assisted Extraction (MAE toward bioactive compound recovery from pharmaceutically-significant medicinal plants, Adathoda vasica and Cymbopogon citratus. Initially, the microwave (MW drying behavior of the plant leaves was investigated at different sample loadings, MW power and drying time. Kinetics was analyzed through empirical modeling of drying data against 10 conventional thin-layer drying equations that were further improvised through the incorporation of Arrhenius, exponential and linear-type expressions. 81 semi-empirical Midilli equations were derived and subjected to non-linear regression to arrive at the characteristic drying equations. Bioactive compounds recovery from the leaves was examined under various parameters through a comparative approach that studied MAE against Soxhlet extraction. MAE of A. vasica reported similar yields although drastic reduction in extraction time (210 s as against the average time of 10 h in the Soxhlet apparatus. Extract yield for MAE of C. citratus was higher than the conventional process with optimal parameters determined to be 20 g sample load, 1:20 sample/solvent ratio, extraction time of 150 s and 300 W output power. Scanning Electron Microscopy and Fourier Transform Infrared Spectroscopy were performed to depict changes in internal leaf morphology.

Single beam Fourier transform digital holographic quantitative phase microscopy

Energy Technology Data Exchange (ETDEWEB)

Anand, A., E-mail: arun-nair-in@yahoo.com; Chhaniwal, V. K.; Mahajan, S.; Trivedi, V. [Optics Laboratory, Applied Physics Department, Faculty of Technology and Engineering, M.S. University of Baroda, Vadodara 390001 (India); Faridian, A.; Pedrini, G.; Osten, W. [Institut für Technische Optik, Universität Stuttgart, Pfaffenwaldring 9, 70569 Stuttgart (Germany); Dubey, S. K. [Siemens Technology and Services Pvt. Ltd, Corporate Technology—Research and Technology Centre, Bangalore 560100 (India); Javidi, B. [Department of Electrical and Computer Engineering, U-4157, University of Connecticut, Storrs, Connecticut 06269-2157 (United States)

2014-03-10

Quantitative phase contrast microscopy reveals thickness or height information of a biological or technical micro-object under investigation. The information obtained from this process provides a means to study their dynamics. Digital holographic (DH) microscopy is one of the most used, state of the art single-shot quantitative techniques for three dimensional imaging of living cells. Conventional off axis DH microscopy directly provides phase contrast images of the objects. However, this process requires two separate beams and their ratio adjustment for high contrast interference fringes. Also the use of two separate beams may make the system more vulnerable to vibrations. Single beam techniques can overcome these hurdles while remaining compact as well. Here, we describe the development of a single beam DH microscope providing whole field imaging of micro-objects. A hologram of the magnified object projected on to a diffuser co-located with a pinhole is recorded with the use of a commercially available diode laser and an arrayed sensor. A Fourier transform of the recorded hologram directly yields the complex amplitude at the image plane. The method proposed was investigated using various phase objects. It was also used to image the dynamics of human red blood cells in which sub-micrometer level thickness variation were measurable.