WorldWideScience

Sample records for carbon-cluster mass calibration

  1. Carbon-cluster mass calibration at SHIPTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Chaudhuri, Ankur

    2007-12-10

    fusion-evaporation reaction {sup 92}Mo({sup 58}Ni,xpyn) at SHIP (Separator for Heavy Ion reaction Products) at GSI. Among the measured nuclei {sup 147}Ho has the lowest half life (5.8 s). A relative mass uncertainty of 5 x 10{sup -8} was obtained from the mass measurements using carbon clusters as calibrants. (orig.)

  2. A carbon cluster ion source for mass calibration at TRIGA-TRAP

    International Nuclear Information System (INIS)

    TRIGA-TRAP is a high-precision penning trap mass spectrometer installed at the research reactor TRIGA Mainz in order to determine the masses of short-lived fission products and - in addition to that - also the masses of actinide elements ranging from uranium up to californium. In order to determine precisely the masses of the nuclides of interest, the superconducting magnet providing the strong magnetic field for the Penning trap has to be calibrated by measuring the cyclotron frequency of an ion with well-known mass, which is, if possible, an isobaric nuclide of the ion of interest. Therefore, the best possible choice for mass calibration is to use carbon clusters as mass references, as demonstrated at the ISOLTRAP facility at ISOLDE/CERN. A laser ablation ion source for the production of carbon clusters has been developed using a frequency-doubled Nd:YAG laser. The design, current status, and results of the production of carbon cluster ions, using C60 and Sigradure registered samples, as well as other ions are presented

  3. Carbon clusters for absolute mass measurements at ISOLTRAP

    CERN Document Server

    Blaum, K; Herfurth, F; Kellerbauer, A G; Kluge, H J; Kuckein, M; Sauvan, E; Scheidenberger, C; Schweikhard, L

    2002-01-01

    The cyclotron frequencies of singly charged carbon clusters C/sub n //sup +/ (n >or= 2) were measured with the Penning-trap mass spectrometer ISOLTRAP at ISOLDE/CERN. The present limit of mass accuracy delta m/m = 1.2.10/sup -8/ and the extent of the mass- dependent systematic shift ( delta m/m)/sub sys/ = 1.7(0.6).10/sup -10//u.(m - m/sub ref/) of the setup were investigated for the first time. In addition, absolute mass measurements by use of pure clusters of the most abundant carbon isotope /sup 12/C are now possible at ISOLTRAP. (15 refs).

  4. Accuracy studies with carbon clusters at the Penning trap mass spectrometer TRIGA-TRAP

    Science.gov (United States)

    Ketelaer, J.; Beyer, T.; Blaum, K.; Block, M.; Eberhardt, K.; Eibach, M.; Herfurth, F.; Smorra, C.; Nagy, Sz.

    2010-05-01

    Extensive cross-reference measurements of well-known frequency ratios using various sizes of carbon cluster ions 12Cn + (10≤n≤23) were performed to determine the effects limiting the accuracy of mass measurements at the Penning-trap facility TRIGA-TRAP. Two major contributions to the uncertainty of a mass measurement have been identified. Fluctuations of the magnetic field cause an uncertainty in the frequency ratio due to the required calibration by a reference ion of uf(νref)/νref = 6(2) × 10-11/min × Δt. A mass-dependent systematic shift of the frequency ratio of epsilonm(r)/r = -2.2(2) × 10-9 × (m-mref)/u has been found as well. Finally, the nuclide 197Au was used as a cross-check since its mass is already known with an uncertainty of 0.6 keV.

  5. The Turn Over of the Odd-even Pattern in Mass Spectra of Carbon Cluster Anions

    Institute of Scientific and Technical Information of China (English)

    NI Guoquan; LIU Bingchen; ZHAI Huajin

    2000-01-01

    @@ Although investigations by many authorsd on the properties of carbon cluster anions by mass spectrometry and photoelectron spectroscopy last more than a decade[1~3], a general conclusion concerning the various features of the carbon clusters generated most commonly in laser vaporization/molecular beam sources has not yet been reached. In this Letter we report that the turn-over of the odd-even patter in relative abundance in the mass spectra of carbon clusters and the "manipulation" of the pattern can be realized in a controlled way by altering the vaporizing laser intensity, the backing pressure and the conductance of carries gas.

  6. Two Types of Mass Abundance Distributions for Anionic Carbon Clusters Investigated by Laser Vaporization and Pulsed Molecular Beam Techniques

    Institute of Scientific and Technical Information of China (English)

    ZHAI Hua-Jin; LIU Bing-Chen; NI Guo-Quan; XUZhi-Zhan

    2000-01-01

    Two types of mass spectra for anionic carbon clusters Cn- have been revealed using laser vaporization and pulsed molecular beam techniques. The less structured mass spectrum characteristic of the magic-numbers at n = 5, 8,11, 15, and 17 is established at the early stage of the cluster formation process, namely, in the laser vaporization process. The more structured one is featured for a regular odd-even alternation and the magic numbers at n =10, 12, 16, 18, 22, and 28, and has been developed only after extensive clustering and qnenching processes, where low-energy electron attachment plays a vital role. Transition between these two types of mass spectra can be realized by controlling either the strength of the pulsed gas flow or the synchronism between the gas flow and the laser vaporization.

  7. An Effective Method of Producing Small Neutral Carbon Clusters

    Institute of Scientific and Technical Information of China (English)

    XIA Zhu-Hong; CHEN Cheng-Chu; HSU Yen-Chu

    2007-01-01

    An effective method of producing small neutral carbon clusters Cn (n = 1-6) is described. The small carbon clusters (positive or negative charge or neutral) are formed by plasma which are produced by a high power 532nm pulse laser ablating the surface of the metal Mn rod to react with small hydrocarbons supplied by a pulse valve, then the neutral carbon clusters are extracted and photo-ionized by another laser (266nm or 355nm) in the ionization region of a linear time-of-flight mass spectrometer. The distributions of the initial neutral carbon clusters are analysed with the ionic species appeared in mass spectra. It is observed that the yield of small carbon clusters with the present method is about 10 times than that of the traditional widely used technology of laser vaporization of graphite.

  8. Calibrating optical bubble size by the displaced-mass method.

    NARCIS (Netherlands)

    Leifer, I.; Leeuw, G. de; Kunz, G.; Cohen, L.H.

    2003-01-01

    Bubble sizing by optical means is very common, but requires calibration by non-optical means. This is particularly important since apparent bubble size increases with decreasing threshold intensity. A calibration experiment was conducted comparing the displaced water mass from captured bubbles with

  9. A portable, automated, inexpensive mass and balance calibration system

    International Nuclear Information System (INIS)

    Reliable mass measurements are essential for a nuclear production facility or process control laboratory. DOE Order 5630.2 requires that traceable standards be used to calibrate and monitor equipment used for nuclear material measurements. To ensure the reliability of mass measurements and to comply with DOE traceability requirements, a portable, automated mass and balance calibration system is used at the Savannah River Plant. Automation is achieved using an EPSON HX-20 notebook computer, which can be operated via RS232C interfacing to electronic balances or function with manual data entry if computer interfacing is not feasible. This economical, comprehensive, user-friendly system has three main functions in a mass measurement control program (MMCP): balance certification, calibration of mass standards, and daily measurement of traceable standards. The balance certification program tests for accuracy, precision, sensitivity, linearity, and cornerloading versus specific requirements. The mass calibration program allows rapid calibration of inexpensive mass standards traceable to certified Class S standards. This MMCP permits daily measurement of traceable standards to monitor the reliability of balances during routine use. The automated system verifies balance calibration, stores results for future use, and provides a printed control chart of the stored data. Another feature of the system permits three different weighing routines that accommodate their need for varying degrees of reliability in routine weighing operations

  10. Charm Quark Mass with Calibrated Uncertainty

    CERN Document Server

    Erler, Jens; Spiesberger, Hubert

    2016-01-01

    We determine the charm quark mass $\\hat{m}_c$ from QCD sum rules of moments of the vector current correlator calculated in perturbative QCD at ${\\cal O} (\\hat\\alpha_s^3)$. Only experimental data for the charm resonances below the continuum threshold are needed in our approach, while the continuum contribution is determined by requiring self-consistency between various sum rules. Existing data from the continuum region can then be used to bound the theoretic uncertainty. Our result is $\\hat{m}_c(\\hat{m}_c) = 1272 \\pm 8$~MeV for $\\hat\\alpha_s(M_Z) = 0.1182$.

  11. Advanced Mass Calibration and Visualization for FT-ICR Mass Spectrometry Imaging

    OpenAIRE

    Smith, Donald F.; Kharchenko, Andriy; Konijnenburg, Marco; Klinkert, Ivo; Pasa-Tolic, Ljiljana; Ron M A Heeren

    2013-01-01

    Mass spectrometry imaging by Fourier transform ion cyclotron resonance yields hundreds of unique peaks, many of which cannot be resolved by lower performance mass spectrometers. The high mass accuracy and high mass resolving power allow confident identification of small molecules and lipids directly from biological tissue sections. Here, calibration strategies for Fourier transform ion cyclotron resonance mass spectrometry imaging were investigated. Sub parts-per-million mass accuracy is demo...

  12. Top Quark Mass Calibration for Monte Carlo Event Generators

    CERN Document Server

    Butenschoen, Mathias; Hoang, Andre H; Mateu, Vicent; Preisser, Moritz; Stewart, Iain W

    2016-01-01

    The most precise top quark mass measurements use kinematic reconstruction methods, determining the top mass parameter of a Monte Carlo event generator, $m_t^{\\rm MC}$. Due to hadronization and parton shower dynamics, relating $m_t^{\\rm MC}$ to a field theory mass is difficult. We present a calibration procedure to determine this relation using hadron level QCD predictions for observables with kinematic mass sensitivity. Fitting $e^+e^-$ 2-Jettiness calculations at NLL/NNLL order to Pythia 8.205, $m_t^{\\rm MC}$ differs from the pole mass by $900$/$600$ MeV, and agrees with the MSR mass within uncertainties, $m_t^{\\rm MC}\\simeq m_{t,1\\,{\\rm GeV}}^{\\rm MSR}$.

  13. Carbon cluster ions for a study of the accuracy of ISOLTRAP

    CERN Document Server

    Kellerbauer, A G; Bollen, G; Herfurth, F; Kluge, H J; Kuckein, M; Sauvan, E; Scheidenberger, C; Schweikhard, L

    2003-01-01

    Cyclotron frequency measurements of singly charged carbon clusters $^{12}$C$_{n}^{+}$ were carried out with the ISOLTRAP apparatus. The carbon cluster ions were produced externally by use of laser- induced desorption, fragmentation, and ionization of C$_{60}$ fullerenes. They were injected into and stored in the Penning trap system. The observation of carbon clusters of different sizes has provided detailed insight into the final mass uncertainty achievable with ISOLTRAP and yielded a value of $u(m)/m = 8 \\times 10^{-9}$. Since the unified atomic mass unit is defined as 1/12 the mass of the $^{12}$C atom, ISOLTRAP can now be used to carry out absolute mass measurements.

  14. Calibrating the Planck Cluster Mass Scale with CLASH

    CERN Document Server

    Penna-Lima, M; Rozo, E; Melin, J -B; Merten, J; Evrard, A E; Postman, M; Rykoff, E

    2016-01-01

    We determine the mass scale of Planck galaxy clusters using gravitational lensing mass measurements from the Cluster Lensing And Supernova survey with Hubble (CLASH). We compare the lensing masses to the Planck Sunyaev-Zeldovich (SZ) mass proxy for 21 clusters in common, employing a Bayesian analysis to simultaneously fit an idealized CLASH selection function and the distribution between the measured observables and true cluster mass. We use a tiered analysis strategy to explicitly demonstrate the importance of priors on weak lensing mass accuracy. In the case of an assumed constant bias, $b_{SZ}$, between true cluster mass, $M_{500}$, and the Planck mass proxy, $M_{PL}$, our analysis constrains $1- b_{SZ} = 0.73 \\pm 0.10$ when moderate priors on weak lensing accuracy are used. Our analyses explicitly accounts for possible selection bias effects in this calibration sourced by the CLASH selection function. Our constraint on the cluster mass scale is consistent with recent results from the Weighing the Giants p...

  15. Stellar masses calibrated with micro-lensed quasars

    CERN Document Server

    Schechter, Paul L; Pooley, David; Wambsganss, Joachim

    2014-01-01

    We measure the stellar mass surface densities of early type galaxies by observing the micro-lensing of macro-lensed quasars caused by individual stars, including stellar remnants, brown dwarfs and red dwarfs too faint to produce photometric or spectroscopic signatures. Our method measures the graininess of the gravitational potential, in contrast to methods that decompose a smooth total gravitational potential into two smooth components, one stellar and one dark. We find the median likelihood value for the calibration factor F by which Salpeter stellar masses (with a low mass cutoff of 0.1 solar masses) must be multiplied is 1.23, with a one sigma confidence range of 0.77 < F < 2.10.

  16. Ionization Thresholds of Small Carbon Clusters: Tunable VUVExperiments and Theory

    Energy Technology Data Exchange (ETDEWEB)

    Belau, Leonid; Wheeler, Steven E.; Ticknor, Brian W.; Ahmed,Musahid; Leone, Stephen R.; Allen, Wesley D.; Schaefer III, Henry F.; Duncan, Michael A.

    2007-07-31

    Small carbon clusters (Cn, n = 2-15) are produced in amolecular beam by pulsed laser vaporization and studied with vacuumultraviolet (VUV) photoionization mass spectrometry. The required VUVradiation in the 8-12 eV range is provided by the Advanced Light Source(ALS) at the Lawrence Berkeley National Laboratory. Mass spectra atvarious ionization energies reveal the qualitative relative abundances ofthe neutral carbon clusters produced. By far the most abundant species isC3. Using the tunability of the ALS, ionization threshold spectra arerecorded for the clusters up to 15 atoms in size. The ionizationthresholds are compared to those measured previously with charge-transferbracketing methods. To interpret the ionization thresholds for differentcluster sizes, new ab initio calculations are carried out on the clustersfor n = 4-10. Geometric structures are optimized at the CCSD(T) levelwith cc-pVTZ (or cc-pVDZ) basis sets, and focal point extrapolations areapplied to both neutral and cation species to determine adiabatic andvertical ionization potentials. The comparison of computed and measuredionization potentials makes it possible to investigate the isomericstructures of the neutral clusters produced in this experiment. Themeasurements are inconclusive for the n = 4-6 species because ofunquenched excited electronic states. However, the data provide evidencefor the prominence of linear structures for the n = 7, 9, 11, 13 speciesand the presence of cyclic C10.

  17. Advanced Mass Calibration and Visualization for FT-ICR Mass Spectrometry Imaging

    CERN Document Server

    Smith, Donald F; Konijnenburg, Marco; Klinkert, Ivo; Pasa-Tolic, Ljiljana; Heeren, Ron M A

    2013-01-01

    Mass spectrometry imaging by Fourier transform ion cyclotron resonance yields hundreds of unique peaks, many of which cannot be resolved by lower performance mass spectrometers. The high mass accuracy and high mass resolving power allow confident identification of small molecules and lipids directly from biological tissue sections. Here, calibration strategies for Fourier transform ion cyclotron resonance mass spectrometry imaging were investigated. Sub parts-per-million mass accuracy is demonstrated over an entire tissue section. Ion abundance fluctuations are corrected for by addition of total and relative ion abundances for a root-mean-square error of 0.158 ppm on 16,764 peaks. A new approach for visualization of Fourier transform ion cyclotron resonance mass spectrometry imaging data at high resolution is presented. The Mosaic Data-cube provides a flexible means to visualize the entire mass range at a mass spectral bin width of 0.001 Dalton. The high resolution Mosaic Data-cube resolves spectral features ...

  18. Calibration of evolutionary diagnostics in high-mass star formation

    CERN Document Server

    Molinari, Sergio; Elia, Davide; Cesaroni, Riccardo; Testi, Leonardo; Robitaille, Thomas

    2016-01-01

    The evolutionary classification of massive clumps that are candidate progenitors of high-mass young stars and clusters relies on a variety of independent diagnostics based on observables from the near-infrared to the radio. A promising evolutionary indicator for massive and dense cluster-progenitor clumps is the L/M ratio between the bolometric luminosity and the mass of the clumps. With the aim of providing a quantitative calibration for this indicator we used SEPIA/APEX to obtain CH3C2H(12-11) observations, that is an excellent thermometer molecule probing densities > 10^5 cm^-3 , toward 51 dense clumps with M>1000 solar masses, and uniformly spanning -2 10 we detect all the clumps, with a gas temperature rising with Log(L/M), marking the appearance of a qualitatively different heating source within the clumps; such values are found towards clumps with UCHII counterparts, suggesting that the quantitative difference in T - L/M behaviour above L/M >10 is due to the first appearance of ZAMS stars in the clump...

  19. Photodissociation and stability of carbon clusters; Photodissociation et stabilite d`agregats de carbone

    Energy Technology Data Exchange (ETDEWEB)

    Bouyer, R.

    1995-04-01

    This work is devoted to the study of the dissociation of ionised carbon clusters (containing 16 to 36 atoms) after photoexcitation by a UV-visible laser pulse. It contributes to experimental studies on formation mechanisms of carbon clusters, and particularly fullerenes. Its first aim is the knowledge of the internal energy of the clusters before dissociation. In the first part, a general overview summarizes the theoretical and experimental studies devoted to energetics (structure, stability, dissociation) of carbon clusters containing less than 60 atoms. In the second part, two techniques for producing mass-selected carbon clusters are described. The particular characteristics for such a production in a direct vaporization source are compared to those in a collisional-cooled source. The question of stability of intermediate-size clusters is asked. We study the photoabsorption spectroscopy of carbon clusters in the third part. A model for sequential absorption of several photons is developed, and used to analyze cluster dissociation versus the photoexcitation laser fluence. The absolute photoabsorption cross sections, and the number of absorbed photons are deduced. For some cluster sizes, laser wavelength scanning leads to evidence for existence of several clusters structures (or so-called isomers). The last part deals with photo dissociation mechanisms. Dissociation is found to occur after single-photon absorption, or after vibrational heating of the clusters. In that latter case, a statistical model including restricted intramolecular vibrational energy redistribution is used to calculate dissociation energies from measured fragmentation times of well-defined internal energy states. These energies, which are characteristic of cyclic structures, are then used to a better understanding of carbon cluster formation in a direct vaporization source. (Author). 76 refs., 63 figs., 23 tabs.

  20. Standard practice for alternate actinide calibration for inductively coupled plasma-mass spectrometry

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2004-01-01

    1.1 This practice provides guidance for an alternate linear calibration for the determination of selected actinide isotopes in appropriately prepared aqueous solutions by Inductively Coupled Plasma-Mass Spectrometry (ICP-MS). This alternate calibration is mass bias adjusted using thorium-232 (232Th) and uranium-238 (238U) standards. One of the benefits of this standard practice is the ability to calibrate for the analysis of highly radioactive actinides using calibration standards at much lower specific activities. Environmental laboratories may find this standard practice useful if facilities are not available to handle the highly radioactive standards of the individual actinides of interest. 1.2 The instrument response for a series of determinations of known concentration of 232Th and 238U defines the mass versus response relationship. For each standard concentration, the slope of the line defined by 232Th and 238U is used to derive linear calibration curves for each mass of interest using interference equ...

  1. Reactions of carbon cluster ions stored in an RF trap

    International Nuclear Information System (INIS)

    Reactions of carbon cluster ions with O2 were studied by using an RF ion trap in which cluster ions of specific size produced by laser ablation could be stored selectively. Reaction rate constants for positive and negative carbon cluster ions were estimated. In the case of the positive cluster ions, these were consistent with the previous experimental results using FTMS. Negative carbon cluster ions C-n (n=4-8) were much less reactive than positive cluster ions. The CnO- products were seen only in n=4 and 6. (orig.)

  2. Establishment of the platinum-iridium kilogram mass standards at NMIJ after the Extraordinary Calibrations

    Science.gov (United States)

    Mizushima, Shigeki; Fujii, Kenichi

    2016-04-01

    The Bureau International des Poids et Mesures has carried out calibrations of the platinum-iridium kilogram mass standards by referencing the international prototype of the kilogram for the first time since the third periodic verification of national prototypes of the kilogram was carried out in 1988-92. This calibration campaign was designated ‘Extraordinary Calibrations’ in the second phase, in which two platinum-iridium kilogram mass standards of the National Metrology Institute of Japan were calibrated with a standard uncertainty of 3.5 μg. By adding these new calibration data into our data sets from 1991, we established our mass unit with a standard uncertainty of 3.3 μg by least-squares analysis using an exponential model, which is useful for compensating for mass increase after cleaning the mass standards. Moreover, it was found that our established mass unit following the Extraordinary Calibrations shifted against our previously maintained mass unit by  -20.8 μg as of the beginning of 2015. The analysis with a linear model revealed that the amount of mass increase over time of some standards was significantly smaller than that suggested at the third periodic verification of national prototypes of the kilogram. The analysis with the exponential model gave an exponent of 0.217 with a standard uncertainty of 0.057. This suggests that the mass increase due to surface contamination cannot be explained by a diffusion-limited process.

  3. Calibration of matrix-assisted laser desorption/ionization time-of-flight peptide mass fingerprinting spectra

    DEFF Research Database (Denmark)

    Hjernø, Karin; Højrup, Peter

    2007-01-01

    This chapter describes a number of aspects important for calibration of matrix-assisted laser desorption/ionization time-of-flight spectra prior to peptide mass fingerprinting searches. Both multipoint internal calibration and mass defect-based calibration is illustrated. The chapter describes ho...

  4. Calibration of the NASA Glenn Research Center 16 in. Mass-Flow Plug

    Science.gov (United States)

    Davis, David O.; Friedlander, David J.; Saunders, J. David; Frate, Franco C.; Foster, Lancert E.

    2014-01-01

    The results of an experimental calibration of the NASA Glenn Research Center 16 in. Mass-Flow Plug (MFP) are presented and compared to a previously obtained calibration of a 15 in. Mass-Flow Plug. An ASME low-beta, long-radius nozzle was used as the calibration reference. The discharge coefficient for the ASME nozzle was obtained by numerically simulating the flow through the nozzle from the WIND-US code. The results showed agreement between the 15 and 16 in. MFPs for area ratios (MFP to pipe area ratio) greater than 0.6 but deviate at area ratios below this value for reasons that are not fully understood. A general uncertainty analysis was also performed and indicates that large uncertainties in the calibration are present for low MFP area ratios.

  5. Calibration of the NASA GRC 16 In. Mass-Flow Plug

    Science.gov (United States)

    Davis, David O.; Friedlander, David J.; Saunders, J. David; Frate, Franco C.; Foster, Lancert E.

    2012-01-01

    The results of an experimental calibration of the NASA Glenn Research Center 16 in. Mass-Flow Plug (MFP) are presented and compared to a previously obtained calibration of a 15 in. Mass-Flow Plug. An ASME low-beta, long-radius nozzle was used as the calibration reference. The discharge coefficient for the ASME nozzle was obtained by numerically simulating the flow through the nozzle from the WIND-US code. The results showed agreement between the 15 in. and 16 in. MFPs for area ratios (MFP to pipe area ratio) greater than 0.6 but deviate at area ratios below this value for reasons that are not fully understood. A general uncertainty analysis was also performed and indicates that large uncertainties in the calibration are present for low MFP area ratios.

  6. Calibration of the Top-Quark Monte Carlo Mass

    Science.gov (United States)

    Kieseler, Jan; Lipka, Katerina; Moch, Sven-Olaf

    2016-04-01

    We present a method to establish, experimentally, the relation between the top-quark mass mtMC as implemented in Monte Carlo generators and the Lagrangian mass parameter mt in a theoretically well-defined renormalization scheme. We propose a simultaneous fit of mtMC and an observable sensitive to mt, which does not rely on any prior assumptions about the relation between mt and mtMC. The measured observable is independent of mtMC and can be used subsequently for a determination of mt. The analysis strategy is illustrated with examples for the extraction of mt from inclusive and differential cross sections for hadroproduction of top quarks.

  7. Induced Dual-Nanospray: A Novel Internal Calibration Method for Convenient and Accurate Mass Measurement

    Science.gov (United States)

    Li, Yafeng; Zhang, Ning; Zhou, Yueming; Wang, Jianing; Zhang, Yiming; Wang, Jiyun; Xiong, Caiqiao; Chen, Suming; Nie, Zongxiu

    2013-09-01

    Accurate mass information is of great importance in the determination of unknown compounds. An effective and easy-to-control internal mass calibration method will dramatically benefit accurate mass measurement. Here we reported a simple induced dual-nanospray internal calibration device which has the following three advantages: (1) the two sprayers are in the same alternating current field; thus both reference ions and sample ions can be simultaneously generated and recorded. (2) It is very simple and can be easily assembled. Just two metal tubes, two nanosprayers, and an alternating current power supply are included. (3) With the low-flow-rate character and the versatility of nanoESI, this calibration method is capable of calibrating various samples, even untreated complex samples such as urine and other biological samples with small sample volumes. The calibration errors are around 1 ppm in positive ion mode and 3 ppm in negative ion mode with good repeatability. This new internal calibration method opens up new possibilities in the determination of unknown compounds, and it has great potential for the broad applications in biological and chemical analysis.

  8. Calibration of the top-quark Monte-Carlo mass

    Energy Technology Data Exchange (ETDEWEB)

    Kieseler, Jan; Lipka, Katerina [DESY Hamburg (Germany); Moch, Sven-Olaf [Hamburg Univ. (Germany). II. Inst. fuer Theoretische Physik

    2015-11-15

    We present a method to establish experimentally the relation between the top-quark mass m{sup MC}{sub t} as implemented in Monte-Carlo generators and the Lagrangian mass parameter m{sub t} in a theoretically well-defined renormalization scheme. We propose a simultaneous fit of m{sup MC}{sub t} and an observable sensitive to m{sub t}, which does not rely on any prior assumptions about the relation between m{sub t} and m{sup MC}{sub t}. The measured observable is independent of m{sup MC}{sub t} and can be used subsequently for a determination of m{sub t}. The analysis strategy is illustrated with examples for the extraction of m{sub t} from inclusive and differential cross sections for hadro-production of top-quarks.

  9. Calibration of the Top-Quark Monte-Carlo Mass

    CERN Document Server

    Kieseler, Jan; Moch, Sven-Olaf

    2015-01-01

    We present a method to establish experimentally the relation between the top-quark mass $m_t^{MC}$ as implemented in Monte-Carlo generators and the Lagrangian mass parameter $m_t$ in a theoretically well-defined renormalization scheme. We propose a simultaneous fit of $m_t^{MC}$ and an observable sensitive to $m_t$, which does not rely on any prior assumptions about the relation between $m_t$ and $m_t^{MC}$. The measured observable is independent of $m_t^{MC}$ and can be used subsequently for a determination of $m_t$. The analysis strategy is illustrated with examples for the extraction of $m_t$ from inclusive and differential cross sections for hadro-production of top-quarks.

  10. Calibration of the top-quark Monte-Carlo mass

    International Nuclear Information System (INIS)

    We present a method to establish experimentally the relation between the top-quark mass mMCt as implemented in Monte-Carlo generators and the Lagrangian mass parameter mt in a theoretically well-defined renormalization scheme. We propose a simultaneous fit of mMCt and an observable sensitive to mt, which does not rely on any prior assumptions about the relation between mt and mMCt. The measured observable is independent of mMCt and can be used subsequently for a determination of mt. The analysis strategy is illustrated with examples for the extraction of mt from inclusive and differential cross sections for hadro-production of top-quarks.

  11. A novel ion source for the calibration of an MRTOF Mass Spectrograph to be used in superheavy elements mass measurements

    CERN Document Server

    Naimi, S; Ito, Y; Mita, H; Okada, K; Ozawa, A; Schury, P; Sonoda, T; Takamine, A; Wada, M; Wollnik, H

    2012-01-01

    A novel ion source based on electrospray ionization and radiofrequency carpet technique has been built. This ion source is designed to deliver relatively heavy molecules for the calibration of a multi reflection time-of-flight mass spectrograph (MRTOF-MS) that will be used for direct mass measurements of superheavy elements. The operation of the ion source as well as the analysis by the MRTOF-MS with heavy molecular ions is described.

  12. Calibration of mass spectrometric measurements of gas phase reactions on steel surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Falk, H., E-mail: heinzfalk@unitybox.de [Scientific Consultancy, Kleve (Germany); Falk, M. [Falk Steuerungssysteme GmbH, Stadthagen (Germany); Wuttke, T. [FuE-EV ThyssenKrupp Steel Europe, Dortmund (Germany)

    2015-03-01

    The sampling of the surface-near gas composition using a mass spectrometer (MS-Probe) is a valuable tool within a hot dip process simulator. Since reference samples with well characterized surface coverage are usually not available, steel samples can deliver quantifiable amounts of the process relevant species H{sub 2}O, CO and H{sub 2} using the decarburization reaction with water vapor. Such “artificial calibration samples” (ACS) can be used for the calibration of the MS-Probe measurements. The carbon release rate, which is governed by the diffusion law, was determined by GDOES, since the diffusion coefficients of carbon in steel samples are usually not known. The measured carbon concentration profiles in the ACS after the thermal treatment confirmed the validity of the diffusion model described in this paper. The carbon bulk concentration > 100 ppm is sufficient for the use of a steel material as ACS. The experimental results reported in this paper reveal, that with the MS-Probe the LOQ of less than one monolayer of iron oxide can be achieved. - Highlights: • Gas to surface reactions at steel sheets is monitored with a mass spectrometer on-line. • The experimental data are calibrated in absolute terms as oxide mass densities. • Standard steel samples can be used for the calibration procedure. • Additional GDOES analysis of the carbon depletion in the calibration samples was carried out. • Limits of quantitation below one monolayer of oxide surface coverage were achieved.

  13. A dynamical calibration of the mass-luminosity relation at very low stellar masses and young ages.

    Science.gov (United States)

    Close, Laird M; Lenzen, Rainer; Guirado, Jose C; Nielsen, Eric L; Mamajek, Eric E; Brandner, Wolfgang; Hartung, Markus; Lidman, Chris; Biller, Beth

    2005-01-20

    Mass is the most fundamental parameter of a star, yet it is also one of the most difficult to measure directly. In general, astronomers estimate stellar masses by determining the luminosity and using the 'mass-luminosity' relationship, but this relationship has never been accurately calibrated for young, low-mass stars and brown dwarfs. Masses for these low-mass objects are therefore constrained only by theoretical models. A new high-contrast adaptive optics camera enabled the discovery of a young (50 million years) companion only 0.156 arcseconds (2.3 au) from the more luminous (> 120 times brighter) star AB Doradus A. Here we report a dynamical determination of the mass of the newly resolved low-mass companion AB Dor C, whose mass is 0.090 +/- 0.005 solar masses. Given its measured 1-2-micrometre luminosity, we have found that the standard mass-luminosity relations overestimate the near-infrared luminosity of such objects by about a factor of approximately 2.5 at young ages. The young, cool objects hitherto thought to be substellar in mass are therefore about twice as massive, which means that the frequency of brown dwarfs and planetary mass objects in young stellar clusters has been overestimated.

  14. PAS-cal: a Generic Recombinant Peptide Calibration Standard for Mass Spectrometry

    OpenAIRE

    Breibeck, Joscha; Serafin, Adam; Reichert, Andreas; Maier, Stefan; Küster, Bernhard; Skerra, Arne

    2014-01-01

    We describe the design, preparation, and mass-spectrometric characterization of a new recombinant peptide calibration standard with uniform biophysical and ionization characteristics for mass spectrometry. “PAS-cal” is an artificial polypeptide concatamer of peptide cassettes with varying lengths, each composed of the three small, chemically stable amino acids Pro, Ala, and Ser, which are interspersed by Arg residues to allow site-specific cleavage with trypsin. PAS-cal is expressed at high y...

  15. Reconciling Planck cluster counts and cosmology: Chandra/XMM instrumental calibration and hydrostatic mass bias

    CERN Document Server

    Israel, Holger; Nevalainen, Jukka; Massey, Richard; Reiprich, Thomas

    2014-01-01

    The temperature of X-ray emitting gas $T_X$ is often used to infer the total mass of galaxy clusters (under the assumption of hydrostatic equilibrium). Unfortunately, XMM-Newton and Chandra observatories measure inconsistent temperatures for the same gas, due to uncertain instrumental calibration. We translate the relative bias in $T_X$ measurements of Schellenberger et al. (2014) into a bias on inferred mass for a sample of clusters with homogeneous weak lensing (WL) masses, to simultaneously examine the hydrostatic bias and instrument calibration. Israel et al. (2014) found consistent WL and Chandra hydrostatic X-ray masses for a sample of clusters at $z$~0.5 and masses of a few $10^{14}$ $M_{\\odot}$. We find their XMM-Newton masses to be lower by $b^{xcal}=15$-$20$ % than their Chandra masses. At the massive end ($>5\\cdot 10^{14}$ $M_{\\odot}$), the XMM-Newton masses are ~35% lower than the WL masses. Assuming that the true hydrostatic bias is 20 %, as indicated by simulations, our results for the massive e...

  16. Energy Calibration of the BaBar EMC Using the Pi0 Invariant Mass Method

    Energy Technology Data Exchange (ETDEWEB)

    Tanner, David J.; /Manchester U.

    2007-04-06

    The BaBar electromagnetic calorimeter energy calibration method was compared with the local and global peak iteration procedures, of Crystal Barrel and CLEO-II. An investigation was made of the possibility of {Upsilon}(4S) background reduction which could lead to increased statistics over a shorter time interval, for efficient calibration runs. The BaBar software package was used with unreconstructed data to study the energy response of the calorimeter, by utilizing the {pi}{sup 0} mass constraint on pairs of photon clusters.

  17. Hydrophilic carbon clusters as therapeutic, high capacity antioxidants

    OpenAIRE

    Samuel, Errol L. G.; Duong, MyLinh T.; Bitner, Brittany R.; Marcano, Daniela C.; James M. Tour; Kent, Thomas A

    2014-01-01

    Oxidative stress reflects an excessive accumulation of reactive oxygen species (ROS) and is a hallmark of several acute and chronic human pathologies. While many antioxidants have been investigated, the majority have demonstrated poor efficacy in clinical trials. Here, we discuss limitations of current antioxidants and describe a new class of nanoparticle antioxidants, poly(ethylene glycol)-functionalized hydrophilic carbon clusters (PEG-HCCs). PEG-HCCs show high capacity to annihilate ROS su...

  18. Calibration of the Quadrupole Mass Spectrometer of the Sample Analysis at Mars Instrument Suite

    Science.gov (United States)

    Mahaffy, P. R.; Trainer, M. G.; Eigenbrode, J. L.; Franz, H. B.; Stern, J. C.; Harpold, D.; Conrad, P. G.; Raaen, E.; Lyness, E.

    2011-01-01

    The SAM suite of instruments on the "Curiosity" Rover of the Mars Science Laboratory (MSL) is designed to provide chemical and isotopic analysis of organic and inorganic volatiles for both atmospheric and solid samples. The mission of the MSL investigations is to advance beyond the successful search for aqueous transformation in surface environments at Mars toward a quantitative assessment of habitability and preservation through a series of chemical and geological measurements. The SAM suite was delivered in December 2010 (Figure 1) to the Jet Propulsion Laboratory for integration into the Curiosity Rover. We previously outlined the range of SAM solid and gas calibrations implemented or planned and here we discuss a specific set of calibration experiments to establish the response of the SAM Quadrupole Mass Spectrometer (QMS) to the four most abundant gases in the Martian atmosphere CO2, N2, Ar, and O2, A full SAM instrument description and calibration report is presently in preparation.

  19. Using inductively coupled plasma-mass spectrometry for calibration transfer between environmental CRMs.

    Science.gov (United States)

    Turk, G C; Yu, L L; Salit, M L; Guthrie, W F

    2001-06-01

    Multielement analyses of environmental reference materials have been performed using existing certified reference materials (CRMs) as calibration standards for inductively coupled plasma-mass spectrometry. The analyses have been performed using a high-performance methodology that results in comparison measurement uncertainties that are significantly less than the uncertainties of the certified values of the calibration CRM. Consequently, the determined values have uncertainties that are very nearly equivalent to the uncertainties of the calibration CRM. Several uses of this calibration transfer are proposed, including, re-certification measurements of replacement CRMs, establishing traceability of one CRM to another, and demonstrating the equivalence of two CRMs. RM 8704, a river sediment, was analyzed using SRM 2704, Buffalo River Sediment, as the calibration standard. SRM 1632c, Trace Elements in Bituminous Coal, which is a replacement for SRM 1632b, was analyzed using SRM 1632b as the standard. SRM 1635, Trace Elements in Subbituminous Coal, was also analyzed using SRM 1632b as the standard. PMID:11451248

  20. Mass Spectrometric Calibration of Controlled Fluoroform Leak Rate Devices Technique and Uncertainty Analysis

    CERN Document Server

    Balsley, S D; Laduca, C A

    2003-01-01

    Controlled leak rate devices of fluoroform on the order of 10 sup - sup 8 atm centre dot cc sec sup - sup 1 at 25 C are used to calibrate QC-1 War Reserve neutron tube exhaust stations for leak detection sensitivity. Close-out calibration of these tritium-contaminated devices is provided by the Gas Dynamics and Mass Spectrometry Laboratory, Organization 14406, which is a tritium analytical facility. The mass spectrometric technique used for the measurement is discussed, as is the first principals calculation (pressure, volume, temperature and time). The uncertainty of the measurement is largely driven by contributing factors in the determination of P, V and T. The expanded uncertainty of the leak rate measurement is shown to be 4.42%, with a coverage factor of 3 (k=3).

  1. The development of an efficient mass balance approach for the purity assignment of organic calibration standards.

    Science.gov (United States)

    Davies, Stephen R; Alamgir, Mahiuddin; Chan, Benjamin K H; Dang, Thao; Jones, Kai; Krishnaswami, Maya; Luo, Yawen; Mitchell, Peter S R; Moawad, Michael; Swan, Hilton; Tarrant, Greg J

    2015-10-01

    The purity determination of organic calibration standards using the traditional mass balance approach is described. Demonstrated examples highlight the potential for bias in each measurement and the need to implement an approach that provides a cross-check for each result, affording fit for purpose purity values in a timely and cost-effective manner. Chromatographic techniques such as gas chromatography with flame ionisation detection (GC-FID) and high-performance liquid chromatography with UV detection (HPLC-UV), combined with mass and NMR spectroscopy, provide a detailed impurity profile allowing an efficient conversion of chromatographic peak areas into relative mass fractions, generally avoiding the need to calibrate each impurity present. For samples analysed by GC-FID, a conservative measurement uncertainty budget is described, including a component to cover potential variations in the response of each unidentified impurity. An alternative approach is also detailed in which extensive purification eliminates the detector response factor issue, facilitating the certification of a super-pure calibration standard which can be used to quantify the main component in less-pure candidate materials. This latter approach is particularly useful when applying HPLC analysis with UV detection. Key to the success of this approach is the application of both qualitative and quantitative (1)H NMR spectroscopy. PMID:26342310

  2. The Stellar Masses of Disk Galaxies and the Calibration of Color-Mass to Light Ratio Relations

    CERN Document Server

    McGaugh, Stacy

    2013-01-01

    We present new Spitzer 3.6 micron observations of a sample of disk galaxies spanning over 10 magnitudes in luminosity and ranging in gas fraction from ~10% to over 90%. We use these data to test population synthesis prescriptions for computing stellar mass. Many commonly employed models fail to provide self-consistent stellar masses in the sense that the stellar mass estimated from the optical luminosity typically exceeds that estimated from the near-infrared (NIR) luminosity. This problem is present in models both with and without TP-AGB stars, but is more severe in the former. Self-consistency can be achieved if NIR mass-to-light ratios are approximately constant with a mean value near 0.5 Msun/Lsun at 3.6 microns. We use the Baryonic Tully-Fisher relation calibrated by gas rich galaxies to provide an independent estimate of the color-mass to light ratio relation. This approach also suggests that the typical 3.6 micron mass-to-light ratio is 0.5 (0.65 in the K band) for rotationally supported galaxies. Thes...

  3. QconCAT standard for calibration of ion mobility-mass spectrometry systems.

    Science.gov (United States)

    Chawner, Ross; McCullough, Bryan; Giles, Kevin; Barran, Perdita E; Gaskell, Simon J; Eyers, Claire E

    2012-11-01

    Ion mobility-mass spectrometry (IM-MS) is a useful technique for determining information about analyte ion conformation in addition to mass/charge ratio. The physical principles that govern the mobility of an ion through a gas in the presence of a uniform electric field are well understood, enabling rotationally averaged collision cross sections (Ω) to be directly calculated from measured drift times under well-defined experimental conditions. However, such "first principle" calculations are not straightforward for Traveling Wave (T-Wave) mobility separations due to the range of factors that influence ion motion through the mobility cell. If collision cross section information is required from T-Wave mobility separations, then calibration of the instruments using known standards is essential for each set of experimental conditions. To facilitate such calibration, we have designed and generated an artificial protein based on the QconCAT technology, QCAL-IM, which upon proteolysis can be used as a universal ion mobility calibration standard. This single unique standard enables empirical calculation of peptide ion collision cross sections from the drift time on a T-Wave mobility instrument.

  4. Stacked Weak Lensing Mass Calibration: Estimators, Systematics, and Impact on Cosmological Parameter Constraints

    Energy Technology Data Exchange (ETDEWEB)

    Rozo, Eduardo; /U. Chicago /Chicago U., KICP; Wu, Hao-Yi; /KIPAC, Menlo Park; Schmidt, Fabian; /Caltech

    2011-11-04

    When extracting the weak lensing shear signal, one may employ either locally normalized or globally normalized shear estimators. The former is the standard approach when estimating cluster masses, while the latter is the more common method among peak finding efforts. While both approaches have identical signal-to-noise in the weak lensing limit, it is possible that higher order corrections or systematic considerations make one estimator preferable over the other. In this paper, we consider the efficacy of both estimators within the context of stacked weak lensing mass estimation in the Dark Energy Survey (DES). We find that the two estimators have nearly identical statistical precision, even after including higher order corrections, but that these corrections must be incorporated into the analysis to avoid observationally relevant biases in the recovered masses. We also demonstrate that finite bin-width effects may be significant if not properly accounted for, and that the two estimators exhibit different systematics, particularly with respect to contamination of the source catalog by foreground galaxies. Thus, the two estimators may be employed as a systematic cross-check of each other. Stacked weak lensing in the DES should allow for the mean mass of galaxy clusters to be calibrated to {approx}2% precision (statistical only), which can improve the figure of merit of the DES cluster abundance experiment by a factor of {approx}3 relative to the self-calibration expectation. A companion paper investigates how the two types of estimators considered here impact weak lensing peak finding efforts.

  5. The important role of evolution in the Planck $Y_{SZ}$-mass calibration

    CERN Document Server

    Andreon, S

    2014-01-01

    In light of the tension between cosmological parameters from Planck cosmic microwave background and galaxy clusters, we revised the Planck analysis of the $Y_{SZ}$-mass calibration allowing for evolution to be determined by the data instead than imposed as external constraint. Our analysis uses the very same data used by the Planck team in order to emphasize that differences in the results comes from differences in the analysis assumptions. The evolution derived from the Planck sample of 71 calibrating clusters with $0.05mass relation turns out to be $1.50\\pm0.07$, shallower by $4.8\\sigma$ than the value derived assuming self-similar evolution, effectively a mass-dependent bias. The non self-similar evolution of $Y_{SZ}$ has to be accounted for in analyses aimed to establish biases of Planck masses because degenerate with it.

  6. The important role of evolution in the Planck YSZ-mass calibration

    Science.gov (United States)

    Andreon, S.

    2014-10-01

    In light of the tension between cosmological parameters from Planck cosmic microwave background and galaxy clusters, we revised the Planck analysis of the YSZ-mass calibration to allow evolution to be determined by the data instead of being imposed as an external constraint. Our analysis uses the very same data and Malmquist bias corrections as used by the Planck team in order to emphasize that differences in the results come from differences in the assumptions. The evolution derived from 71 calibrating clusters, with 0.05 < z < 0.45, is proportional to E2.5 ± 0.4(z), so inconsistent with the self-similar evolution (E2/3) assumed by previous analyses. When allowing for evolution, the slope of YSZ-mass relation turns out to be 1.51 ± 0.07, which is shallower by 4.8σ than the value derived when assuming self-similar evolution, introducing a mass-dependent bias. The non-self-similar evolution of YSZ has to be accounted for in analyses aimed to establish the biases of Planck masses.

  7. Calibrating the Mass-Luminosity Relation at the End of the Main Sequence

    Science.gov (United States)

    Henry, Todd

    2000-07-01

    This is a continuation of GO 6047/6566/7493/8282. We use HST-FGS3/1R to calibrate the mass-luminosity relation {MLR} for stars less massive than 0.2 Msun, with special emphasis on objects near the stellar/brown dwarf border. Our goals are to determine Mv values to 0.10 magnitude, masses to 5%, and more than double the number of objects with masses determined to be less than 0.20 Msun. This program uses the combination of HST-FGS3/1R at optical wavelengths and ground-based infrared speckle work to examine nearby, subarcsecond binary systems. Several of the objects included have M main sequence, and making them brown dwarf candidates.

  8. Calibration of a surface mass balance model for global-scale applications

    Directory of Open Access Journals (Sweden)

    R. H. Giesen

    2012-12-01

    Full Text Available Global applications of surface mass balance models have large uncertainties, as a result of poor climate input data and limited availability of mass balance measurements. This study addresses several possible consequences of these limitations for the modelled mass balance. This is done by applying a simple surface mass balance model that only requires air temperature and precipitation as input data, to glaciers in different regions. In contrast to other models used in global applications, this model separately calculates the contributions of net solar radiation and the temperature-dependent fluxes to the energy balance. We derive a relation for these temperature-dependent fluxes using automatic weather station (AWS measurements from glaciers in different climates. With local, hourly input data, the model is well able to simulate the observed seasonal variations in the surface energy and mass balance at the AWS sites. Replacing the hourly local data by monthly gridded climate data removes summer snowfall and winter melt events and, hence, influences the modelled mass balance most on locations with a small seasonal temperature cycle. Modelled winter mass balance profiles are fitted to observations on 82 glaciers in different regions to determine representative values for the multiplication factor and vertical gradient of precipitation. For 75 of the 82 glaciers, the precipitation provided by the climate dataset has to be multiplied with a factor above unity; the median factor is 2.5. The vertical precipitation gradient ranges from negative to positive values, with more positive values for maritime glaciers and a median value of 1.5 mm a−1 m−1. With calibrated precipitation, the modelled annual mass balance gradient closely resembles the observations on the 82 glaciers, the absolute values are matched by adjusting either the incoming solar radiation, the temperature-dependent flux or the air temperature. The mass balance

  9. Calibration of a surface mass balance model for global-scale applications

    Science.gov (United States)

    Giesen, R. H.; Oerlemans, J.

    2012-12-01

    Global applications of surface mass balance models have large uncertainties, as a result of poor climate input data and limited availability of mass balance measurements. This study addresses several possible consequences of these limitations for the modelled mass balance. This is done by applying a simple surface mass balance model that only requires air temperature and precipitation as input data, to glaciers in different regions. In contrast to other models used in global applications, this model separately calculates the contributions of net solar radiation and the temperature-dependent fluxes to the energy balance. We derive a relation for these temperature-dependent fluxes using automatic weather station (AWS) measurements from glaciers in different climates. With local, hourly input data, the model is well able to simulate the observed seasonal variations in the surface energy and mass balance at the AWS sites. Replacing the hourly local data by monthly gridded climate data removes summer snowfall and winter melt events and, hence, influences the modelled mass balance most on locations with a small seasonal temperature cycle. Modelled winter mass balance profiles are fitted to observations on 82 glaciers in different regions to determine representative values for the multiplication factor and vertical gradient of precipitation. For 75 of the 82 glaciers, the precipitation provided by the climate dataset has to be multiplied with a factor above unity; the median factor is 2.5. The vertical precipitation gradient ranges from negative to positive values, with more positive values for maritime glaciers and a median value of 1.5 mm a-1 m-1. With calibrated precipitation, the modelled annual mass balance gradient closely resembles the observations on the 82 glaciers, the absolute values are matched by adjusting either the incoming solar radiation, the temperature-dependent flux or the air temperature. The mass balance sensitivity to changes in temperature is

  10. SDSSJ14584479+3720215: A Benchmark JHK Blazar Light Curve from the 2MASS Calibration Scans

    CERN Document Server

    Davenport, James R A; Becker, Andrew C; Macleod, Chelsea L; Cutri, Roc M

    2015-01-01

    Active galactic nuclei (AGNs) are well-known to exhibit flux variability across a wide range of wavelength regimes, but the precise origin of the variability at different wavelengths remains unclear. To investigate the relatively unexplored near-IR variability of the most luminous AGNs, we conduct a search for variability using well sampled JHKs-band light curves from the 2MASS survey calibration fields. Our sample includes 27 known quasars with an average of 924 epochs of observation over three years, as well as one spectroscopically confirmed blazar (SDSSJ14584479+3720215) with 1972 epochs of data. This is the best-sampled NIR photometric blazar light curve to date, and it exhibits correlated, stochastic variability that we characterize with continuous auto-regressive moving average (CARMA) models. None of the other 26 known quasars had detectable variability in the 2MASS bands above the photometric uncertainty. A blind search of the 2MASS calibration field light curves for AGN candidates based on fitting C...

  11. Calibration and intercomparison of acetic acid measurements using proton transfer reaction mass spectrometry (PTR-MS

    Directory of Open Access Journals (Sweden)

    K. B. Haase

    2012-07-01

    Full Text Available Acetic acid is one of the most abundant organic acids in the ambient atmosphere, with maximum mixing ratios reaching into the tens of parts per billion by volume (ppbv range. The identities and associated magnitudes of the major sources and sinks for acetic acid are poorly characterized, due in part to the limitation in available measurement techniques. This paper demonstrates that Proton Transfer Reaction Mass Spectrometry (PTR-MS can reliably quantify acetic acid vapor in ambient air. Three different PTR-MS configurations were calibrated at low ppbv mixing ratios using permeation tubes, which yielded calibration factors between 7.0 and 10.9 normalized counts per second per ppbv (ncps ppbv−1 at a drift tube field strength of 132 townsend (Td. Detection limits ranged from 0.06 to 0.32 ppbv with dwell times of 5 s. These calibration factors showed negligible humidity dependence. Using the experimentally determined calibration factors, PTR-MS measurements of acetic acid during the International Consortium for Atmospheric Research on Transport and Transformation (ICARTT campaign were validated against results obtained using Mist Chambers coupled with Ion Chromatography (MC/IC. An orthogonal least squares linear regression of paired data yielded a slope of 1.14 ± 0.06 (2σ, an intercept of 0.049 ± 20 (2σ ppbv, and an R2 of 0.78. The median mixing ratio of acetic acid on Appledore Island, ME during the ICARTT campaign was 0.530 ± 0.025 ppbv with a minimum of 0.075 ± 0.004 ppbv, and a maximum of 3.555 ± 0.171 ppbv.

  12. Calibration and intercomparison of acetic acid measurements using proton transfer reaction mass spectrometry (PTR-MS)

    Science.gov (United States)

    Haase, K.B.; Keene, W.C.; Pszenny, A.A.P.; Mayne, H.R.; Talbot, R.W.; Sive, B.C.

    2012-01-01

    Acetic acid is one of the most abundant organic acids in the ambient atmosphere, with maximum mixing ratios reaching into the tens of parts per billion by volume (ppbv) range. The identities and associated magnitudes of the major sources and sinks for acetic acid are poorly characterized, due in part to the limitation in available measurement techniques. This paper demonstrates that Proton Transfer Reaction Mass Spectrometry (PTR-MS) can reliably quantify acetic acid vapor in ambient air. Three different PTR-MS configurations were calibrated at low ppbv mixing ratios using permeation tubes, which yielded calibration factors between 7.0 and 10.9 normalized counts per second per ppbv (ncps ppbv−1) at a drift tube field strength of 132 townsend (Td). Detection limits ranged from 0.06 to 0.32 ppbv with dwell times of 5 s. These calibration factors showed negligible humidity dependence. Using the experimentally determined calibration factors, PTR-MS measurements of acetic acid during the International Consortium for Atmospheric Research on Transport and Transformation (ICARTT) campaign were validated against results obtained using Mist Chambers coupled with Ion Chromatography (MC/IC). An orthogonal least squares linear regression of paired data yielded a slope of 1.14 ± 0.06 (2σ), an intercept of 0.049 ± 20 (2σ) ppbv, and an R2 of 0.78. The median mixing ratio of acetic acid on Appledore Island, ME during the ICARTT campaign was 0.530 ± 0.025 ppbv with a minimum of 0.075 ± 0.004 ppbv, and a maximum of 3.555 ± 0.171 ppbv.

  13. Evaluation of Collision Cross Section Calibrants for Structural Analysis of Lipids by Traveling Wave Ion Mobility-Mass Spectrometry.

    Science.gov (United States)

    Hines, Kelly M; May, Jody C; McLean, John A; Xu, Libin

    2016-07-19

    Collision cross section (CCS) measurement of lipids using traveling wave ion mobility-mass spectrometry (TWIM-MS) is of high interest to the lipidomics field. However, currently available calibrants for CCS measurement using TWIM are predominantly peptides that display quite different physical properties and gas-phase conformations from lipids, which could lead to large CCS calibration errors for lipids. Here we report the direct CCS measurement of a series of phosphatidylcholines (PCs) and phosphatidylethanolamines (PEs) in nitrogen using a drift tube ion mobility (DTIM) instrument and an evaluation of the accuracy and reproducibility of PCs and PEs as CCS calibrants for phospholipids against different classes of calibrants, including polyalanine (PolyAla), tetraalkylammonium salts (TAA), and hexakis(fluoroalkoxy)phosphazines (HFAP), in both positive and negative modes in TWIM-MS analysis. We demonstrate that structurally mismatched calibrants lead to larger errors in calibrated CCS values while the structurally matched calibrants, PCs and PEs, gave highly accurate and reproducible CCS values at different traveling wave parameters. Using the lipid calibrants, the majority of the CCS values of several classes of phospholipids measured by TWIM are within 2% error of the CCS values measured by DTIM. The development of phospholipid CCS calibrants will enable high-accuracy structural studies of lipids and add an additional level of validation in the assignment of identifications in untargeted lipidomics experiments. PMID:27321977

  14. LoCuSS: weak-lensing mass calibration of galaxy clusters

    Science.gov (United States)

    Okabe, Nobuhiro; Smith, Graham P.

    2016-10-01

    We present weak-lensing mass measurements of 50 X-ray luminous galaxy clusters at 0.15 ≤ z ≤ 0.3, based on uniform high-quality observations with Suprime-Cam mounted on the 8.2-m Subaru telescope. We pay close attention to possible systematic biases, aiming to control them at the ≲4 per cent level. The dominant source of systematic bias in weak-lensing measurements of the mass of individual galaxy clusters is contamination of background galaxy catalogues by faint cluster and foreground galaxies. We extend our conservative method for selecting background galaxies with (V - i') colours redder than the red sequence of cluster members to use a colour-cut that depends on cluster-centric radius. This allows us to define background galaxy samples that suffer ≤1 per cent contamination, and comprise 13 galaxies per square arcminute. Thanks to the purity of our background galaxy catalogue, the largest systematic that we identify in our analysis is a shape measurement bias of 3 per cent, that we measure using simulations that probe weak shears up to g = 0.3. Our individual cluster mass and concentration measurements are in excellent agreement with predictions of the mass-concentration relation. Equally, our stacked shear profile is in excellent agreement with the Navarro Frenk and White profile. Our new Local Cluster Substructure Survey mass measurements are consistent with the Canadian Cluster Cosmology Project and Cluster Lensing And Supernova Survey with Hubble surveys, and in tension with the Weighing the Giants at ˜1σ-2σ significance. Overall, the consensus at z ≤ 0.3 that is emerging from these complementary surveys represents important progress for cluster mass calibration, and augurs well for cluster cosmology.

  15. Calibration of Dissolved Noble Gas Mass Spectrometric Measurements by an Air-Water Equilibration System

    Science.gov (United States)

    Hillegonds, Darren; Matsumoto, Takuya; Jaklitsch, Manfred; Han, Liang-Feng; Klaus, Philipp; Wassenaar, Leonard; Aggarwal, Pradeep

    2013-04-01

    Precise measurements by mass spectrometry of dissolved noble gases (He, Ar, Ne, Kr, Xe) in water samples require careful calibration against laboratory standards with known concentrations. Currently, air pipettes are used for day-to-day calibrations, making estimation of overall analytical uncertainties for dissolved noble gas measurements in water difficult. Air equilibrated water (AEW) is often used as a matrix-equivalent laboratory standard for dissolved gases in groundwater, because of the well-known and constant fractions of noble gases in the atmosphere. AEW standards, however, are only useful if the temperature and pressure of the gas-water equilibrium can be controlled and measured precisely (i.e., to better than 0.5%); contamination and partial sample degassing must also be prevented during sampling. Here we present the details of a new custom air-water equilibration system which consists of an insulated 600 liter tank filled with deionized water, held isothermally at a precise target temperature (water in the tank are monitored continually, as are atmospheric pressure and air temperature in the laboratory. Different noble gas concentration standards can be reliably produced by accurately controlling the water temperature of the equilibration system. Equilibration characteristics and reproducibility of this system for production of copper tubes containing known amounts of noble gases will be presented.

  16. Calibration of mass spectrometric measurements of gas phase reactions on steel surfaces

    Science.gov (United States)

    Falk, H.; Falk, M.; Wuttke, T.

    2015-03-01

    The sampling of the surface-near gas composition using a mass spectrometer (MS-Probe) is a valuable tool within a hot dip process simulator. Since reference samples with well characterized surface coverage are usually not available, steel samples can deliver quantifiable amounts of the process relevant species H2O, CO and H2 using the decarburization reaction with water vapor. Such "artificial calibration samples" (ACS) can be used for the calibration of the MS-Probe measurements. The carbon release rate, which is governed by the diffusion law, was determined by GDOES, since the diffusion coefficients of carbon in steel samples are usually not known. The measured carbon concentration profiles in the ACS after the thermal treatment confirmed the validity of the diffusion model described in this paper. The carbon bulk concentration > 100 ppm is sufficient for the use of a steel material as ACS. The experimental results reported in this paper reveal, that with the MS-Probe the LOQ of less than one monolayer of iron oxide can be achieved.

  17. Measurements of particle masses of inorganic salt particles for calibration of cloud condensation nuclei counters

    Directory of Open Access Journals (Sweden)

    M. Kuwata

    2009-02-01

    Full Text Available We measured the mobility equivalent critical dry diameter for CCN activation (dcme and the particle mass of size-selected (NH42SO4 and NaCl particles to calibrate a CCN counter (CCNC precisely. The CCNC was operated downstream of a differential mobility analyzer (DMA for the measurement of dcme. The particle mass was measured using an aerosol particle mass analyzer (APM operated downstream of the DMA. The measurement of particle mass was conducted for 50–150-nm particles. Effective densities (ρeff of (NH42SO4 particles were 1.67–1.75 g cm−3, which correspond to the dynamic shape factors (χ of 1.01–1.04. This shows that (NH42SO4 particles are not completely spherical. In the case of NaCl particles, ρeff was 1.75–1.99 g cm−3 and χ was 1.05–1.14, demonstrating that their particle shape was non-spherical. Using these experimental data, the volume equivalent critical dry diameter (dcve was calculated, and it was used as an input parameter for calculations of critical supersaturation (S. Several thermodynamics models were used for the calculation of water activity. When the Pitzer model was employed for the calculations, the critical S calculated for (NH42SO4 and NaCl agreed to well within the uncertainty of 2% (relative. This result demonstrates that the use of the Pitzer model for the calibration of CCNCs gives the most probable value of S.

  18. Electron propagator calculations on linear and branched carbon cluster dianions

    Energy Technology Data Exchange (ETDEWEB)

    Zakrzewski, V.G.; Ortiz, J.V. [Univ. of New Mexico, Albuquerque, NM (United States)

    1994-12-31

    Electron propagator calculations have been performed on linear carbon cluster dianions from C{sub 7}{sup 2-} to C{sub 10}{sup 2-} and on branched C{sub 7}{sup 2-}, C{sub 9}{sup 2-} and C{sub 11}{sup 2-} structures which have a central, tricoordinate carbon bound to three branches with alternating long and short bonds. The more stable, branched isomer of C{sub 7}{sup 2-} has a positive vertical ionization energy, but the linear form does not. While linear C{sub 10}{sup 2-} is stable with respect to electron loss, it is not possible to decide from these calculations whether linear C{sub 8}{sup 2-} and C{sub 9}{sup 2-} have the same property. There is evidence that better calculations would obtain bound C{sub 8}{sup 2-} and C{sub 9}{sup 2-} species. All branched dianions have positive, vertical ionization energies. Feynman-Dyson amplitudes for dianion ionization energies display delocalized {pi} bonding, with the two terminal carbons of the longest branches making the largest contributions.

  19. Calibration of microbolometer infrared cameras for measuring volcanic ash mass loading

    Science.gov (United States)

    Carroll, Russell C.

    Small spacecraft with thermal infrared (TIR) imaging capabilities are needed to detect dangerous levels of volcanic ash that can severely damage jet aircraft engines and must be avoided. Grounding aircraft after a volcanic eruption may cost the airlines millions of dollars per day, while accurate knowledge of volcanic ash density might allow for safely routing aircraft around dangerous levels of volcanic ash. There are currently limited numbers of satellites with TIR imaging capabilities so the elapsed time between revisits can be large, and these instruments can only resolve total mass loading along the line-of-sight. Multiple small satellites could allow for decreased revisit times as well as multiple viewing angles to reveal the three-dimensional structure of the ash cloud through stereoscopic techniques. This paper presents the design and laboratory evaluation of a TIR imaging system that is designed to fit within the resource constraints of a multi-unit CubeSat to detect volcanic ash mass loading. The laboratory prototype of this TIR imaging system uses a commercial off-the shelf (COTS) camera with an uncooled microbolometer sensor, two narrowband filters, a black body source and a custom filter wheel. The infrared imaging system detects the difference in attenuation of volcanic ash at 11 mum and 12 mum by measuring the brightness temperature at each band. The brightness temperature difference method is used to measure the column mass loading. Multi-aspect images and stereoscopic techniques are needed to estimate the mass density from the mass loading, which is the measured mass per unit area. Laboratory measurements are used to characterize the noise level and thermal stability of the sensor. A calibration technique is developed to compensate for sensor temperature drift. The detection threshold of volcanic ash density of this TIR imaging system is found to be from 0.35 mg/m3 to 26 mg/m3 for ash clouds that have thickness of 1 km, while ash cloud densities

  20. CoMaLit-V. Mass forecasting with proxies. Method and application to weak lensing calibrated samples

    CERN Document Server

    Sereno, Mauro

    2016-01-01

    Mass measurements of astronomical objects are most wanted but still elusive. We need them to trace the formation and evolution of cosmic structure but we can get direct measurements only for a minority. This lack can be circumvented with a proxy and a scaling relation. The twofold goal of estimating the unbiased relation and finding the right proxy value to plug in can be hampered by systematics, selection effects, Eddington/Malmquist biases and time evolution. We present a Bayesian hierarchical method which deals with these issues. Masses to be predicted are treated as missing data in the regression and are estimated together with the scaling parameters. The calibration subsample with measured masses does not need to be representative of the full sample. We apply the method to forecast weak lensing calibrated masses of the Planck, redMaPPer and MCXC clusters. Planck masses are biased low with respect to weak lensing calibrated masses, with a bias more pronounced for high redshift clusters. MCXC masses are un...

  1. Precise calibration of LIGO test mass actuators using photon radiation pressure

    CERN Document Server

    Goetz, E; Erickson, S; Savage, R L; González, G; Kawabe, K; Landry, M; Marka, S; O'Reilly, B; Riles, K; Sigg, D; Willems, P

    2009-01-01

    Precise calibration of kilometer-scale interferometric gravitational wave detectors is crucial for source localization and waveform reconstruction. A technique that uses the radiation pressure of a power-modulated auxiliary laser to induce calibrated displacements of one of the ~10 kg arm cavity mirrors, a so-called photon calibrator, has been demonstrated previously and has recently been implemented on the LIGO detectors. In this article, we discuss the inherent precision and accuracy of the LIGO photon calibrators and several improvements that have been developed to reduce the estimated voice coil actuator calibration uncertainties to less than 2 percent (1-sigma). These improvements include accounting for rotation-induced apparent length variations caused by interferometer and photon calibrator beam centering offsets, absolute laser power measurement using temperature-controlled InGaAs photodetectors mounted on integrating spheres and calibrated by NIST, minimizing errors induced by localized elastic defor...

  2. Tuned resonant mass or inerter-based absorbers: unified calibration with quasi-dynamic flexibility and inertia correction

    DEFF Research Database (Denmark)

    Krenk, Steen; Høgsberg, Jan Becker

    2016-01-01

    A common format is developed for a mass and an inerter-based resonant vibration absorber device, operating on the absolute motion and the relative motion at the location of the device, respectively. When using a resonant absorber a specific mode is targeted, but in the calibration of the device i...

  3. Mass evolution of Mediterranean, Black, Red, and Caspian Seas from GRACE and altimetry: accuracy assessment and solution calibration

    Science.gov (United States)

    Loomis, B. D.; Luthcke, S. B.

    2016-09-01

    We present new measurements of mass evolution for the Mediterranean, Black, Red, and Caspian Seas as determined by the NASA Goddard Space Flight Center (GSFC) GRACE time-variable global gravity mascon solutions. These new solutions are compared to sea surface altimetry measurements of sea level anomalies with steric corrections applied. To assess their accuracy, the GRACE- and altimetry-derived solutions are applied to the set of forward models used by GSFC for processing the GRACE Level-1B datasets, with the resulting inter-satellite range-acceleration residuals providing a useful metric for analyzing solution quality. We also present a differential correction strategy to calibrate the time series of mass change for each of the seas by establishing the strong linear relationship between differences in the forward modeled mass and the corresponding range-acceleration residuals between the two solutions. These calibrated time series of mass change are directly determined from the range-acceleration residuals, effectively providing regionally-tuned GRACE solutions without the need to form and invert normal equations. Finally, the calibrated GRACE time series are discussed and combined with the steric-corrected sea level anomalies to provide new measurements of the unmodeled steric variability for each of the seas over the span of the GRACE observation record. We apply ensemble empirical mode decomposition (EEMD) to adaptively sort the mass and steric components of sea level anomalies into seasonal, non-seasonal, and long-term temporal scales.

  4. Collaborative study for the calibration of replacement batches for the heparin low-molecular-mass for assay biological reference preparation.

    Science.gov (United States)

    Terao, E; Daas, A

    2016-01-01

    The European Pharmacopoeia (Ph. Eur.) prescribes the control of the activity of low molecular mass heparins by assays for anti-Xa and anti-IIa activities (monograph 0828), using a reference standard calibrated in International Units (IU). An international collaborative study coded BSP133 was launched in the framework of the Biological Standardisation Programme (BSP) run under the aegis of the Council of Europe and the European Commission to calibrate replacement batches for the dwindling stocks of the Heparin low-molecular-mass for assay Biological Reference Preparation (BRP) batch 8. Thirteen official medicines control and manufacturers laboratories from European and non-European countries took part in this study to calibrate two freeze-dried candidate batches against the 3rd International Standard (IS) for heparin, low molecular weight (11/176; 3rd IS). The Heparin low-molecular-mass for assay BRP (batch 8) was also included in the test panel to check the continuity between subsequent BRP batches. Taking into account the stability data, the results of this collaborative study and on the basis of the central statistical analysis performed at the European Directorate for the Quality of Medicines & HealthCare (EDQM), the 2 candidate batches were officially adopted by the Commission of the European Pharmacopoeia as Heparin low-molecular-mass for assay BRP batches 9 and 10 with assigned anti-Xa activities of 102 and 100 IU/vial and anti-IIa activities of 34 and 33 IU/vial respectively. PMID:27507705

  5. High precision time calibration of the Permo-Triassic boundary mass extinction by U-Pb geochronology

    Science.gov (United States)

    Baresel, Björn; Bucher, Hugo; Brosse, Morgane; Schaltegger, Urs

    2014-05-01

    U-Pb dating using Chemical Abrasion, Isotope Dilution Thermal Ionization Mass Spectrometry (CA-ID-TIMS) is the analytical method of choice for geochronologists, who are seeking highest temporal resolution and a high degree of accuracy for single grains of zircon. The use of double-isotope tracer solutions, cross-calibrated and assessed in different EARTHTIME labs, coinciding with the reassessment of the uranium decay constants and further improvements in ion counting technology led to unprecedented precision better than 0.1% for single grain, and 0.05% for population ages, respectively. These analytical innovations now allow calibrating magmatic and biological timescales at resolution adequate for both groups of processes. To construct a revised and high resolution calibrated time scale for the Permian-Triassic boundary (PTB) we use (i) high-precision U-Pb zircon age determinations of a unique succession of volcanic ash beds interbedded with shallow to deep water fossiliferous sediments in the Nanpanjiang Basin (South China) combined with (ii) accurate quantitative biochronology based on ammonoids and conodonts and (iii) carbon isotope excursions across the PTB. Using these alignments allows (i) positioning the PTB in different depositional environments and (ii) solving age/stratigraphic contradictions generated by the index, water depth-controlled conodont Hindeodus parvus, whose diachronous first occurrences are arbitrarily used for placing the base of the Triassic. This new age framework provides the basis for a combined calibration of chemostratigraphic records with high-resolution biochronozones of the Late Permian and Early Triassic. Besides the general improvement of the radio-isotopic calibration of the PTB at the ±100 ka level, this will also lead to a better understanding of cause and effect relations involved in this mass extinction.

  6. Studies for a top quark mass measurement and development of a jet energy calibration with the ATLAS detector

    Energy Technology Data Exchange (ETDEWEB)

    Jantsch, Andreas

    2012-06-11

    In this thesis, the development of a new jet energy calibration method as well as studies for a top quark mass measurement with the ATLAS detector are presented. The new calibration method considers jet shape variables in order to improve the linearity and resolution of the jet energy response. Promising results are shown for jet events from Monte Carlo simulation as well as from first {radical}(s)=900 GeV proton-proton collision data of the Large Hadron Collider. In addition, Monte Carlo studies for a top quark mass measurement in the lepton plus jets decay channel of top quark pair events are performed. Several top quark reconstruction methods are investigated in pseudo-experiments which are equivalent to an integrated luminosity of L=200 pb{sup -1} at {radical}(s)=10 TeV. Assuming a generated top quark mass of m{sub t}{sup gen}=172.5 GeV, the most promising result is achieved with the Max-p{sub T} reconstruction method which returns a top quark mass of m{sup Max-p{sub Tt,el-channel}}=170.4{+-}2.2 vertical stroke {sub stat.}{+-} 8.8 vertical stroke {sub syst.} GeV in the electron plus jets decay channel including a bias correction of +5.2 GeV for the central top quark mass value.

  7. Calibration of Nu-Instruments Noblesse multicollector mass spectrometers for argon isotopic measurements using a newly developed reference gas

    Science.gov (United States)

    Coble, M.A.; Grove, M.; Calvert, A.T.

    2011-01-01

    The greatest challenge limiting 40Ar/39Ar multicollection measurements is the availability of appropriate standard gasses to intercalibrate detectors. In particular, use of zoom lens ion-optics to steer and focus ion beams into a fixed detector array (i.e., Nu Instruments Noblesse) makes intercalibration of multiple detectors challenging because different ion-optic tuning conditions are required for optimal peak shape and sensitivity at different mass stations. We have found that detector efficiency and mass discrimination are affected by changes in ion-optic tuning parameters. Reliance upon an atmospheric Ar standard to calibrate the Noblesse is problematic because there is no straightforward way to relate atmospheric 40Ar and 36Ar to measurements of 40Ar and 39Ar if they are measured on separate detectors. After exploring alternative calibration approaches, we have concluded that calibration of the Noblesse is best performed using exactly the same source, detector, and ion-optic tuning settings as those used in routine 40Ar/39Ar analysis. To accomplish this, we have developed synthetic reference gasses containing 40Ar, 39Ar and 38Ar produced by mixing gasses derived from neutron-irradiated sanidine with an enriched 38Ar spike. We present a new method for calibrating the Noblesse based on use of both atmospheric Ar and the synthetic reference gasses. By combining atmospheric Ar and synthetic reference gas in different ways, we can directly measure 40Ar/39Ar, 38Ar/39Ar, and 36Ar/39Ar correction factors over ratios that vary from 0.5 to 460. These correction factors are reproducible to better than ??0.5??? (2?? standard error) over intervals spanning ~24h but can vary systematically by ~4% over 2weeks of continuous use when electron multiplier settings are held constant. Monitoring this variation requires daily calibration of the instrument. Application of the calibration method to 40Ar/39Ar multicollection measurements of widely used sanidine reference materials

  8. Large carbon cluster thin film gauges for measuring aerodynamic heat transfer rates in hypersonic shock tunnels

    International Nuclear Information System (INIS)

    Different types of Large Carbon Cluster (LCC) layers are synthesized by a single-step pyrolysis technique at various ratios of precursor mixture. The aim is to develop a fast responsive and stable thermal gauge based on a LCC layer which has relatively good electrical conduction in order to use it in the hypersonic flow field. The thermoelectric property of the LCC layer has been studied. It is found that these carbon clusters are sensitive to temperature changes. Therefore suitable thermal gauges were developed for blunt cone bodies and were tested in hypersonic shock tunnels at a flow Mach number of 6.8 to measure aerodynamic heating. The LCC layer of this thermal gauge encounters high shear forces and a hostile environment for test duration in the range of a millisecond. The results are favorable to use large carbon clusters as a better sensor than a conventional platinum thin film gauge in view of fast responsiveness and stability. (paper)

  9. Modular calibrant sets for the structural analysis of nucleic acids by ion mobility spectrometry mass spectrometry.

    Science.gov (United States)

    Lippens, Jennifer L; Ranganathan, Srivathsan V; D'Esposito, Rebecca J; Fabris, Daniele

    2016-06-20

    This study explored the use of modular nucleic acid (NA) standards to generate calibration curves capable of translating primary ion mobility readouts into corresponding collision cross section (CCS) data. Putative calibrants consisted of single- (ss) and double-stranded (ds) oligo-deoxynucleotides reaching up to ∼40 kDa in size (i.e., 64 bp) and ∼5700 Å(2) in CCS. To ensure self-consistency among reference CCS values, computational data obtained in house were preferred to any experimental or computational data from disparate sources. Such values were obtained by molecular dynamics (MD) simulations and either the exact hard sphere scattering (EHSS) or the projection superposition approximation (PSA) methods, and then plotted against the corresponding experimental values to generate separate calibration curves. Their performance was evaluated on the basis of their correlation coefficients and ability to provide values that matched the CCS of selected test samples mimicking typical unknowns. The results indicated that the predictive power benefited from the exclusion of higher charged species that were more susceptible to the destabilizing effects of Coulombic repulsion. The results revealed discrepancies between EHSS and PSA data that were ascribable to the different approximations used to describe the ion mobility process. Within the boundaries defined by these approximations and the challenges of modeling NA structure in a solvent-free environment, the calibrant sets enabled the experimental determination of CCS with excellent reproducibility (precision) and error (accuracy), which will support the analysis of progressively larger NA samples of biological significance. PMID:27152369

  10. LoCuSS: Calibrating Mass-Observables Scaling Relations for Cluster Cosmology with Subaru Weak Lensing Observations

    CERN Document Server

    Okabe, Nobuhiro; Finoguenov, Alexis; Takada, Masahiro; Smith, Graham P; Umetsu, Keiichi; Futamase, Toshifumi

    2010-01-01

    (Abridged) We present a joint weak-lensing/X-ray study of galaxy cluster mass-observable scaling relations, motivated by the critical importance of accurate calibration of mass proxies for future X-ray missions, including eROSITA. We use a sample of 12 clusters at z\\simeq0.2 that we have observed with Subaru and XMM-Newton to construct relationships between the weak-lensing mass (M), and three X-ray observables: gas temperature (T), gas mass (Mgas), and quasi-integrated gas pressure (Yx) at overdensities of \\Delta=2500, 1000, and 500 with respect to the critical density. We find that Mgas at \\Delta\\le1000 appears to be the most promising mass proxy of the three, because it has the lowest intrinsic scatter in mass at fixed observable: \\sigma _lnM\\simeq0.1, independent of cluster dynamical state. The scatter in mass at fixed T and Yx is a factor of \\sim2-3 larger than at fixed Mgas, which are indicative of the structural segregation that we find in the M-T and M-Yx relationships. Undisturbed clusters are found ...

  11. The transition mass-loss rate: Calibrating the role of line-driven winds in massive star evolution

    CERN Document Server

    Vink, Jorick S

    2012-01-01

    A debate has arisen regarding the importance of stationary versus eruptive mass loss for massive star evolution. The reason is that stellar winds have been found to be clumped, which results in the reduction of unclumped empirical mass-loss rates. Most stellar evolution models employ theoretical mass-loss rates which are already reduced by a moderate factor of ~2-3 compared to non-corrected empirical rates. A key question is whether these reduced rates are of the correct order of magnitude, or if they should be reduced even further, which would mean that the alternative of eruptive mass loss becomes necessary. Here we introduce the transition mass-loss rate (dM/dt)_trans between O and Wolf-Rayet (WR) stars. Its novelty is that it is model independent. All that is required is postulating the spectroscopic transition point in a given data-set, and determining the stellar luminosity, which is far less model dependent than the mass-loss rate. The transition mass-loss rate is subsequently used to calibrate stellar...

  12. Discovery of an M4 Spectroscopic Binary in Upper Scorpius: A Calibration Point for Young Low-Mass Evolutionary Models

    CERN Document Server

    Reiners, A; Reiners, Ansgar; Mohanty, Gibor Basri & Subhanjoy

    2005-01-01

    We report the discovery of a new low-mass spectroscopic (SB2) stellar binary system in the star-forming region of Upper Scorpius. This object, UScoCTIO5, was discovered by Ardila (2000), who assigned it a spectral class of M4. A KeckI HIRES spectrum revealed it to be double-lined, and we then carried out a program at several observatories to determine its orbit. The orbital period is 34 days, and the eccentricity is nearly 0.3. The importance of such a discovery is that it can be used to help calibrate evolutionary models at low masses and young ages. This is one of the outstanding problems in the study of formation mechanisms and initial mass functions at low masses. The orbit allows us to place a lower limit of 0.64 +- 0.02 M_sol on the total system mass. The components appear to be of almost equal mass. We are able to show that this mass is significantly higher than predicted by evolutionary models for an object of this luminosity and age, in agreement with other recent results. More precise determination ...

  13. Mass Calibration and Cosmological Analysis of the SPT-SZ Galaxy Cluster Sample Using Velocity Dispersion $\\sigma_v$ and X-ray $Y_\\textrm{X}$ Measurements

    CERN Document Server

    Bocquet, S; Mohr, J J; Aird, K A; Ashby, M L N; Bautz, M; Bayliss, M; Bazin, G; Benson, B A; Bleem, L E; Brodwin, M; Carlstrom, J E; Chang, C L; Chiu, I; Cho, H M; Clocchiatti, A; Crawford, T M; Crites, A T; Desai, S; de Haan, T; Dietrich, J P; Dobbs, M A; Foley, R J; Forman, W R; Gangkofner, D; George, E M; Gladders, M D; Gonzalez, A H; Halverson, N W; Hennig, C; Hlavacek-Larrondo, J; Holder, G P; Holzapfel, W L; Hrubes, J D; Jones, C; Keisler, R; Knox, L; Lee, A T; Leitch, E M; Liu, J; Lueker, M; Luong-Van, D; Marrone, D P; McDonald, M; McMahon, J J; Meyer, S S; Mocanu, L; Murray, S S; Padin, S; Pryke, C; Reichardt, C L; Rest, A; Ruel, J; Ruhl, J E; Saliwanchik, B R; Sayre, J T; Schaffer, K K; Shirokoff, E; Spieler, H G; Stalder, B; Stanford, S A; Staniszewski, Z; Stark, A A; Story, K; Stubbs, C W; Vanderlinde, K; Vieira, J D; Vikhlinin, A; Williamson, R; Zahn, O; Zenteno, A

    2014-01-01

    We present a velocity dispersion-based mass calibration of the South Pole Telescope Sunyaev-Zel'dovich effect survey (SPT-SZ) galaxy cluster sample. Using a homogeneously selected sample of 100 cluster candidates from 720 deg2 of the survey along with 63 velocity dispersion ($\\sigma_v$) and 16 X-ray Yx measurements of sample clusters, we simultaneously calibrate the mass-observable relation and constrain cosmological parameters. The calibrations using $\\sigma_v$ and Yx are consistent at the $0.6\\sigma$ level, with the $\\sigma_v$ calibration preferring ~16% higher masses. We use the full cluster dataset to measure $\\sigma_8(\\Omega_ m/0.27)^{0.3}=0.809\\pm0.036$. The SPT cluster abundance is lower than preferred by either the WMAP9 or Planck+WMAP9 polarization (WP) data, but assuming the sum of the neutrino masses is $\\sum m_\

  14. Calibration of a surface mass balance model for global-scale applications

    OpenAIRE

    R. H. Giesen; Oerlemans, J.

    2012-01-01

    Global applications of surface mass balance models have large uncertainties, as a result of poor climate input data and limited availability of mass balance measurements. This study addresses several possible consequences of these limitations for the modelled mass balance. This is done by applying a simple surface mass balance model that only requires air temperature and precipitation as input data, to glaciers in different regions. In contrast to other models used in global applications, thi...

  15. Calibration of a surface mass balance model for global-scale applications

    NARCIS (Netherlands)

    Giesen, R. H.; Oerlemans, J.

    2012-01-01

    Global applications of surface mass balance models have large uncertainties, as a result of poor climate input data and limited availability of mass balance measurements. This study addresses several possible consequences of these limitations for the modelled mass balance. This is done by applying a

  16. 液相色谱-质谱联用仪的最佳校准条件的选择%Selection of Optimum Calibration Conditions in Calibrating Liquid Chromatograph-mass Spectrometer

    Institute of Scientific and Technical Information of China (English)

    施江焕

    2013-01-01

    Liquid chromatograph and mass spectrometer was coupled together to the analytical instrument by a certain interface.Based on the working principle and structure of Liquid chromatograph-mass spectrometer,for setting the calibration parameter of the instrument,the technique of selecting optimum calibration conditions in calibrating Liquid chromatograph-mass spectrometer was studied by the analysis of the chromatographic conditions,instrument tuning and mass spectrometry conditions.So it could ensure to calibrate Liquid chromatograph-mass spectrometer accurately and provide some guidance on the calibration for Metrological institutions.%液相色谱-质谱联用仪是将液相色谱仪与质谱仪通过一定的接口耦合到一起的分析仪器.本文从色质谱联用仪的工作原理及结构入手,针对仪器校准时的参数设置,通过分析色谱条件、仪器调谐、质谱条件等因素,介绍了色质联用仪最佳校准条件的选择技巧,有力保证了对液质联用仪进行准确的计量校准,为计量检定机构开展校准工作提供了参考.

  17. Cosmic ray energetics and mass (CREAM) calibrating a cosmic ray calorimeter

    CERN Document Server

    Ganel, O; Ahn, S H; Alford, R; Kim, K C; Lee, M H; Liu, L; Lutz, L; Malinin, A; Schindhelm, E; Wang, J Z; Wu, J; Beatty, J J; Coutu, S; Minnick, S A; Nutter, S; Duvernois, M A; Choi, M J; Kim, H J; Kim, S K; Park, I H; Swordy, S P

    2002-01-01

    CREAM is slated to fly as the first NASA ultra long duration balloon (ULDB) payload in late 2003. On this 60-plus-day flight CREAM is expected to collect more direct high-energy cosmic ray events than the current world total. With three such flights CREAM is expected to have a proton energy reach above 5*10/sup 14/ eV, probing near 100 Te V for the predicted kink in the cosmic-ray proton spectrum. With a transition radiation detector (TRD) above a sampling tungsten /scintillator calorimeter, an in-flight cross-calibration of the absolute energy scale becomes possible with heavy ions. We report on results from a 2001 beam test of the calorimeter in an SPS beam at the European High Energy Physics lab (CERN) and on the planned in- flight calibration. (7 refs).

  18. A solvothermal method for synthesizing monolayer protected amorphous calcium carbonate clusters

    OpenAIRE

    Sun, Shengtong; Gebauer, Denis; Cölfen, Helmut

    2016-01-01

    A solvothermal method was developed for synthesizing organic monolayer protected amorphous calcium carbonate clusters using 10,12-pentacosadiynoic acid as ligand, ethanol as solvent and NaHCO3 decomposition as CO2 source, which can be extended to synthesize other monolayer protected mineral clusters. published

  19. External calibration in gas chromatography-combustion-isotope ratio mass spectrometry measurements of endogenous androgenic anabolic steroids in sports doping control.

    Science.gov (United States)

    Kioussi, Maroula K; Angelis, Yiannis S; Cawley, Adam T; Koupparis, Michalis; Kazlauskas, Rymantas; Brenna, J Thomas; Georgakopoulos, Costas G

    2011-08-19

    An alternative calibration procedure for the gas chromatography-combustion-isotope ratio mass spectrometry (GC-C-IRMS) measurements of the World Antidoping Agency (WADA) Accredited Laboratories is presented. To alleviate the need for externally calibrated CO₂ gas for GC-C-IRMS analysis of urinary steroid metabolites, calibration using an external standard mixture solution of steroids with certified isotopic composition was investigated. The reference steroids of the calibration mixture and routine samples underwent identical instrumental processes. The calibration standards bracketed the entire range of the relevant δ¹³C values for the endogenous and exogenous steroids as well as their chromatographic retention times. The certified δ¹³C values of the reference calibrators were plotted in relation to measured m/z ¹³CO₂/¹²CO₂ (i.e. R(45/44)) mass spectrometric signals of each calibrator. δ¹³C values of the sample steroids were calculated from the least squares fit through the calibration curve. The effect of the external calibration on δ¹³C values, using the same calibration standards and set of urine samples but different brands of GC-C-IRMS instruments, was assessed by an interlaboratory study in the WADA Accredited Laboratories of Sydney, Australia and Athens, Greece. Relative correspondence between the laboratories for determination of androsterone, etiocholanolone, 5β-androstane-3α,17β-diacetate, and pregnanediacetate means were SD(δ¹³C)=0.12‰, 0.58‰, -0.34‰, and -0.40‰, respectively. These data demonstrate that accurate intralaboratory external calibration with certified steroids provided by United States Antidoping Agency (USADA) and without external CO₂ calibration is feasible and directly applicable to the WADA Accredited Laboratories for the harmonization of the GC-C-IRMS measurements.

  20. Calibration of 242 Pu Tracer by Mass Spectrometry%质谱法标定242 Pu指示剂

    Institute of Scientific and Technical Information of China (English)

    李冬梅; 徐江; 杜丽丽

    2014-01-01

    将高纯242 Pu浓度标准溶液与239 Pu混合,质谱法测量R239/242(A)先标定四水硫酸钚中239 Pu的浓度;再将四水硫酸钚与待标定的242 Pu指示剂混合,测量R239/242(A),标定242 Pu 指示剂的浓度。质谱测量还可标定得到242 Pu指示剂中的钚同位素丰度。采用两次同位素稀释质谱法标定242 Pu 指示剂快捷简便,可在2日内完成。测量精度高,242 Pu浓度的相对合成标准不确定度为0.75%,该指示剂可满足高精度分析工作的需求。%242 Pu is commonly employed as tracer for determination of 239 Pu in environmental samples.The 239 Pu concentration in Pu(SO4 )2 ·4H2 O solution was determined by isotope dilution-mass spectrometry (ID-MS)using a high pure 242 Pu spike.Then the 242 Pu tracer in our laboratary was calibrated by ID-MS using the calibrated 239 Pu solution as spike.By meas-uring the atom ratio of 239 Pu to 242 Pu twice by ID-MS,the concentration and abundance of the 242 Pu tracer in laboratary were finally calibrated.This method was proved to be efficient with high precision.The process could be finished within two days with an uncertainty of 0.75%. The calibrated 242 Pu tracer in laboratory could meet the demand of high-precision analysis.

  1. HIFLUGCS: X-ray luminosity -- dynamical mass relation and its implications for mass calibrations with the SPIDERS and 4MOST surveys

    CERN Document Server

    Zhang, Yu-Ying; Schneider, Peter; Clerc, Nicolas; Merloni, Andrea; Schwope, Axel; Borm, Katharina; Andernach, Heinz; Caretta, César A; Wu, Xiang-Ping

    2016-01-01

    We present the X-ray luminosity (L) versus dynamical mass (M) relation for 63 nearby clusters in the HIFLUGCS. The luminosity measurements are obtained based on ~1.3 Ms of clean XMM data and ROSAT pointed observations. The masses are estimated using optical spectroscopic redshifts of 13647 cluster galaxies in total. Given sufficient numbers of member galaxies in computing the dynamical masses, the L-M relations agree between the disturbed and undisturbed clusters. The cool-core clusters still dominate the scatter in the L-M relation even when a core corrected X-ray luminosity is used, which indicates that the scatter mainly reflects the structure formation history of the clusters. As shown by the clusters with a small number of redshifts, the dynamical masses can be underestimated leading to a biased scaling relation. To investigate the potential of spectroscopic surveys to follow up high-redshift galaxy clusters/groups observed in X-ray surveys for the identifications and mass calibrations, we carried out Mo...

  2. Top pairs production and effects of new physics. Jet calibration with W into jet-jet process. Top mass measurement

    International Nuclear Information System (INIS)

    Since it was discovered in 1995 at Fermilab, the top quark is the subject of a great attention. It completes the third quark generation of the standard model of particle physics, and the measurement of its properties constrains strongly this model. It is also a preferential way to probe new physics expected around 1 TeV. This thesis, performed using the Atlas detector at LHC, describes the methods implemented in order to measure precisely the top quark mass in the lepton + jets channel. Several analysis ways are presented in function of the performances of the detector, especially its capacity to identify the b jets. The precise measurement of the top quark mass needs a deep understanding of the jet energy scale. This thesis suggests a strategy to calibrate the light jets using the constraint on the W boson mass, and shows that a precision of 1 GeV2/c2 on the top mass measurement is achievable. An evaluation of the discovery potential of tt-bar resonances, foreseen by models beyond the standard model is also carried out. (author)

  3. Calibration and adjustment of center of mass (COM) based on EKF during in-flight phase

    Institute of Scientific and Technical Information of China (English)

    DONG Feng; LIAO He; JIA ChengLong; XIA XiaoJing

    2009-01-01

    The electrostatic accelerometer, assembled on gravity satellite, serves to measure all non-gravitational accelerations caused by atmosphere drag or solar radiation pressure, etc. The proof-mass center of the accelerometer needs to be precisely positioned at the center of gravity satellite, otherwise, the offset between them will bring measurement disturbance due to angular acceleration of satellite and gradient.Because of installation and measurement errors on the ground, fuel consumption during the in-flight phase and other adverse factors, the offset between the proof-mass center and the satellite center of mass is usually large enough to affect the measurement accuracy of the accelerometer, even beyond its range. Therefore, the offset needs to be measured or estimated, and then be controlled within the measurement requirement of the accelerometer by the center of mass (COM) adjustment mechanism during the life of the satellite. The estimation algorithm based on EKF, which uses the measurement of accelerometer, gyro and magnetometer, is put forward to estimate the offset, and the COM adjustment mechanism then adjusts the satellite center of mass in order to make the offset meet the requirement.With the special configuration layout, the COM adjustment mechanism driven by the stepper motors can separately regulate X, Y and Z axes. The associated simulation shows that the offset can be con-trolled better than 0.03 mm for all the axes with the method mentioned above.

  4. Stacked Weak Lensing Mass Calibration: Estimators, Systematics, and Impact on Cosmological Parameter Constraints

    CERN Document Server

    Rozo, Eduardo; Schmidt, Fabian

    2010-01-01

    When extracting the weak lensing shear signal, one may employ either locally normalized or globally normalized shear estimators. The former is the standard approach when estimating cluster masses, while the latter is the more common method among peak finding efforts. While both approaches have identical signal-to-noise in the weak lensing limit, it is possible that higher order corrections or systematics considerations make one estimator preferable over the other. In this paper, we consider the efficacy of both estimators within the context of stacked weak lensing mass estimation in the Dark Energy Survey (DES). We find the two estimators have nearly identical statistical precision, even after including higher order corrections, but that these corrections must be incorporated into the analysis to avoid observationally relevant biases in the recovered masses. We also demonstrate that finite bin-width effects may be significant if not properly accounted for, and that the two estimators exhibit different systema...

  5. Ab Initio Investigation of the Structures of Fe-Doped Carbon Clusters

    Science.gov (United States)

    Lovato, Christella; Brownrigg, Clifton; Hira, Ajit

    2012-02-01

    We continue our interest in the theoretical study of carbon clusters to examine the effects of the doping of small carbon clusters (Cn, n = 2 - 15) with iron atoms. This work applies the hybrid ab initio methods of quantum chemistry to derive the different FemCn (m = 1-3) geometries. Of particular interest are linear, fan, and cyclic geometries. Electronic energies, rotational constants, dipole moments, and vibrational frequencies for these geometries are calculated. Exploration of the singlet, triplet, quintet, and septet potential energy surfaces is performed. The type of bonding in terms of competition between sp^2 and sp^3 hybridization is examined, with a view to addressing the possibility of the stabilization of the doped carbon nano-particles in a diamond type structure. The potential for the existence of new pathways to the fabrication of nanotubes is explored.

  6. Quantitative sampling and analysis of trace elements in ambient air: impactor characterization and Synchrotron-XRF mass calibration

    Directory of Open Access Journals (Sweden)

    A. Richard

    2010-06-01

    Full Text Available Identification of trace elements in ambient air can add substantial information to pollution source apportionment studies, although they do not contribute significantly to emissions in terms of mass. A method for quantitative size and time-resolved trace element evaluation in ambient aerosols with a rotating drum impactor and synchrotron radiation based X-ray fluorescence is presented. The impactor collection efficiency curves and size segregation characteristics were investigated in an experiment with oil and salt particles. Cutoff diameters were determined through the ratio of size distributions measured with two particles sizers. Furthermore, an external calibration technique to empirically link fluorescence intensities to ambient concentrations was developed. Solutions of elemental standards were applied with an ink-jet printer on thin films and area concentrations were subsequently evaluated with external wet chemical methods. These customized and reusable reference standards enable quantification of different data sets analyzed under varying experimental conditions.

  7. Quantitative sampling and analysis of trace elements in atmospheric aerosols: impactor characterization and Synchrotron-XRF mass calibration

    Directory of Open Access Journals (Sweden)

    A. Richard

    2010-10-01

    Full Text Available Identification of trace elements in ambient air can add substantial information to pollution source apportionment studies, although they do not contribute significantly to emissions in terms of mass. A method for quantitative size and time-resolved trace element evaluation in ambient aerosols with a rotating drum impactor and synchrotron radiation based X-ray fluorescence is presented. The impactor collection efficiency curves and size segregation characteristics were investigated in an experiment with oil and salt particles. Cutoff diameters were determined through the ratio of size distributions measured with two particle sizers. Furthermore, an external calibration technique to empirically link fluorescence intensities to ambient concentrations was developed. Solutions of elemental standards were applied with an ink-jet printer on thin films and area concentrations were subsequently evaluated with external wet chemical methods. These customized and reusable reference standards enable quantification of different data sets analyzed under varying experimental conditions.

  8. Calibration of the Top-Quark Monte Carlo Mass.

    Science.gov (United States)

    Kieseler, Jan; Lipka, Katerina; Moch, Sven-Olaf

    2016-04-22

    We present a method to establish, experimentally, the relation between the top-quark mass m_{t}^{MC} as implemented in Monte Carlo generators and the Lagrangian mass parameter m_{t} in a theoretically well-defined renormalization scheme. We propose a simultaneous fit of m_{t}^{MC} and an observable sensitive to m_{t}, which does not rely on any prior assumptions about the relation between m_{t} and m_{t}^{MC}. The measured observable is independent of m_{t}^{MC} and can be used subsequently for a determination of m_{t}. The analysis strategy is illustrated with examples for the extraction of m_{t} from inclusive and differential cross sections for hadroproduction of top quarks. PMID:27152794

  9. Pseudopotential Density-Functional Calculations for Structures of Small Carbon Clusters CN (N = 2~8)

    Institute of Scientific and Technical Information of China (English)

    BAI Yu-Lin; CHEN Xiang-Rong; YANG Xiang-Dong; LU Peng-Fei

    2004-01-01

    We introduce a first-principles density-functional theory, i.e. the finite-difference pseudopotential densityfunctional theory in real space and the Langevin molecular dynamics annealing technique, to the descriptions of structures and some properties of small carbon clusters (CN, N = 2 ~ 8). It is shown that the odd-numbered clusters have linear structures and most of the even-numbered clusters prefer cyclic structures.

  10. Highly efficient conversion of superoxide to oxygen using hydrophilic carbon clusters

    OpenAIRE

    Samuel, Errol L. G.; Marcano, Daniela C.; Berka, Vladimir; Bitner, Brittany R.; Wu, Gang; Potter, Austin; Fabian, Roderic H.; Pautler, Robia G; Kent, Thomas A; Tsai, Ah-Lim; James M. Tour

    2015-01-01

    Mechanistic studies of nontoxic hydrophilic carbon cluster nanoparticles show that they are able to accomplish the direct conversion of superoxide to dioxygen and hydrogen peroxide. This is accomplished faster than in most single-active-site enzymes, and it is precisely what dioxygen-deficient tissue needs in the face of injury where reactive oxygen species, particularly superoxide, overwhelm the natural enzymes required to remove superoxide. We confirm here that the hydrophilic carbon cluste...

  11. Calibration of centre-of-mass energies at LEP1 for precise measurements of Z properties

    CERN Document Server

    Assmann, R W; Billen, R; Blondel, A; Bravin, Enrico; Bright-Thomas, P G; Camporesi, T; Dehning, Bernd; Drees, A; Duckeck, G; Gascon, J; Geitz, M A; Goddard, B; Hawkes, C M; Henrichsen, K N; Hildreth, M D; Hofmann, A; Jacobsen, R; Koratzinos, M; Lamont, M; Lançon, E; Lucotte, A; Mnich, J; Mugnai, G; Peschardt, E; Placidi, Massimo; Puzo, P; Quast, G; Renton, P B; Rolandi, Luigi; Wachsmuth, H W; Wells, P S; Wenninger, J; Wilkinson, G R; Wyatt, T R; Yamartino, J M; Yip, K

    1999-01-01

    The determination of the centre-of-mass energies from the LEP1 data for 1993, 1994 and 1995 is presented. Accurate knowledge of these energies is crucial in the measurement of the Z resonance param eters. The improved understanding of the LEP energy behaviour accumulated during the 1995 energy scan is detailed, while the 1993 and 1994 measurements are revised. For 1993 these supersede the pr eviously published values. Additional instrumentation has allowed the detection of an unexpectedly large energy rise during physics fills. This new effect is accommodated in the modelling of the beam-energy in 1995 and propagated to the 1993 and 1994 energies. New results are reported on the magnet temperature behaviour which constitutes one of the major corrections to the average LEP ene rgy. The 1995 energy scan took place in conditions very different from the previous years. In particular the interaction-point specific corrections to the centre-of-mass energy in 1995 are more complicated than previously: these arise fr...

  12. LoCuSS: Weak-lensing mass calibration of galaxy clusters

    CERN Document Server

    Okabe, Nobuhiro

    2015-01-01

    We present weak-lensing mass measurements of 50 X-ray luminous galaxy clusters at $0.15\\le z\\le0.3$, based on high quality observations with Suprime-Cam mounted on the 8.2-m Subaru telescope. We pay close attention to possible systematic biases, aiming to control them at the $\\lt4$ per cent level. The dominant source of systematic bias in weak-lensing measurements of the mass of individual galaxy clusters is contamination of background galaxy catalogues by faint cluster and foreground galaxies. We extend our conservative method for selecting background galaxies with $(V-i')$ colours redder than the red sequence of cluster members to use a colour-cut that depends on cluster-centric radius. This allows us to define background galaxy samples that suffer $\\le1$ per cent contamination, and comprise $13$ galaxies per square arcminute. Thanks to the purity of our background galaxy catalogue, the largest systematic in our measurement is a shape measurement bias of $3$ per cent, that we measure using custom-made simul...

  13. Elemental ratio measurements of organic compounds using aerosol mass spectrometry: characterization, improved calibration, and implications

    Directory of Open Access Journals (Sweden)

    M. R. Canagaratna

    2014-07-01

    Full Text Available Elemental compositions of organic aerosol (OA particles provide useful constraints on OA sources, chemical evolution, and effects. The Aerodyne high-resolution time-of-flight aerosol mass spectrometer (HR-ToF-AMS is widely used to measure OA elemental composition. This study evaluates AMS measurements of atomic oxygen-to-carbon (O : C, hydrogen-to-carbon (H : C, organic mass-to-organic carbon (OM : OC, and carbon oxidation state (OSC for a vastly expanded laboratory dataset of multifunctional oxidized OA standards. For the expanded standard dataset, the "Aiken-Explicit" method (Aiken et al., 2008, which uses experimentally measured ion intensities at all ions to determine elemental ratios, reproduces known molecular O : C and H : C ratio values within 20% (average absolute value of relative errors and 12% respectively. The more commonly used "Aiken-Ambient" method, which uses empirically estimated H2O+ and CO+ ion intensities to avoid gas phase air interferences at these ions, reproduces O : C and H : C of multifunctional oxidized species within 28% and 14% of known values. These values are systematically biased low, however, with larger biases observed for alcohols and simple diacids. A detailed examination of the H2O+, CO+, and CO2+ fragments in the high-resolution mass spectra of the standard compounds indicates that the Aiken-Ambient method underestimates the CO+ and H2O+ produced from many oxidized species. Combined AMS-vacuum ultraviolet (VUV ionization measurements indicate that these ions are produced by dehydration and decarboxylation on the AMS vaporizer (usually operated at 600 °C. Thermal decomposition is observed to be efficient at vaporizer temperatures down to 200 °C. These results are used together to develop an "Improved-Ambient" elemental analysis method for AMS spectra measured in air. The Improved-Ambient method reduces the systematic biases and reproduces O : C (H : C ratios of individual oxidized standards within 28% (13

  14. Absolute Magnitude Calibration for Red Giants based on the Colour-Magnitude Diagrams of Galactic Clusters. III-Calibration with 2MASS

    CERN Document Server

    Karaali, S; Gokce, E Yaz

    2012-01-01

    We present two absolute magnitude calibrations, $M_{J}$ and $M_{K_s}$, for red giants with the colour magnitude diagrams of five Galactic clusters with different metallicities i.e. M92, M13, M71, M67, and NGC 6791. The combination of the absolute magnitudes of the red giant sequences with the corresponding metallicities provides calibration for absolute magnitude estimation for red giants for a given colour. The calibrations for $M_{J}$ and $M_{K_s}$ are defined in the colour intervals $1.3\\leq(V-J)_{0}\\leq2.8$ and $1.75 \\leq (V-K_{s})_{0}\\leq 3.80$ mag, respectively, and they cover the metallicity interval $-2.15 \\leq \\lbrack Fe/H \\rbrack \\leq +0.37$ dex. The absolute magnitude residuals obtained by the application of the procedure to another set of Galactic clusters lie in the intervals $-0.08= 0.137$ and $\\sigma_{M_J}=0.080$, and $=0.109$ and $\\sigma_{M_{K_{s}}}=0.123$ mag. The derived relations are applicable to stars older than 4 Gyr, the age of the youngest calibrating cluster.

  15. Supermassive Black Holes in Active Galactic Nuclei. II. Calibration of the Black Hole Mass-Velocity Dispersion Relationship for Active Galactic Nuclei

    DEFF Research Database (Denmark)

    Onken, Christopher A.; Ferrarese, Laura; Merritt, David;

    2004-01-01

    We calibrate reverberation-based black hole masses in active galactic nuclei (AGNs) by using the correlation between black hole mass, M, and bulge/spheroid stellar velocity dispersion, sigma. We use new measurements of sigma for 6 AGNs and published velocity dispersions for 10 others......, in conjunction with improved reverberation mapping results, to determine the scaling factor required to bring reverberation-based black hole masses into agreement with the quiescent galaxy M-sigma relationship. The scatter in the AGN black hole masses is found to be less than a factor of 3. The current...

  16. A Revised Calibration of the Virial Mass Estimator for Black Holes in Active Galaxies Based on Single-epoch H$\\beta$ Spectra

    CERN Document Server

    Ho, Luis C

    2015-01-01

    The masses of supermassive black holes in broad-line active galactic nuclei (AGNs) can be measured through reverberation mapping, but this method currently cannot be applied to very large samples or to high-redshift AGNs. As a practical alternative, one can devise empirical scaling relations, based on the correlation between broad-line region size and AGN luminosity and the relation between black hole mass and bulge stellar velocity dispersion, to estimate the virial masses of black holes from single-epoch spectroscopy. We present a revised calibration of the black hole mass estimator for the commonly used H$\\beta$ emission line. Our new calibration takes into account the recent determination of the virial coefficient for pseudo and classical bulges.

  17. Detection of the linear carbon cluster C10: rotationally resolved diode-laser spectroscopy.

    Science.gov (United States)

    Giesen, T F; Berndt, U; Yamada, K M; Fuchs, G; Schieder, R; Winnewisser, G; Provencal, R A; Keutsch, F N; Van Orden, A; Saykally, R J

    2001-04-17

    Detected in interstellar space and as intermediates in soot formation, molecules of pure carbon in the form of linear chains or ring structures have interested researchers for several decades, who attempt to elucidate their physical properties and the processes govering their formation. A high-resolution infrared spectrometer housing a tunable diode laser and combined with an effective laser ablation source for the cluster production has been used to study the molecular properties of small carbon clusters; reported herein is the first gas-phase spectrum of linear C10.

  18. Residual gas analyzer calibration

    Science.gov (United States)

    Lilienkamp, R. H.

    1972-01-01

    A technique which employs known gas mixtures to calibrate the residual gas analyzer (RGA) is described. The mass spectra from the RGA are recorded for each gas mixture. This mass spectra data and the mixture composition data each form a matrix. From the two matrices the calibration matrix may be computed. The matrix mathematics requires the number of calibration gas mixtures be equal to or greater than the number of gases included in the calibration. This technique was evaluated using a mathematical model of an RGA to generate the mass spectra. This model included shot noise errors in the mass spectra. Errors in the gas concentrations were also included in the valuation. The effects of these errors was studied by varying their magnitudes and comparing the resulting calibrations. Several methods of evaluating an actual calibration are presented. The effects of the number of gases in then, the composition of the calibration mixture, and the number of mixtures used are discussed.

  19. Calibrating convective-core overshooting with eclipsing binary systems. The case of low-mass main-sequence stars

    CERN Document Server

    Valle, G; Moroni, P G Prada; Degl'Innocenti, S

    2016-01-01

    In a robust statistical way, we quantify the uncertainty that affects the calibration of the overshooting efficiency parameter $\\beta$ that is owing to the uncertainty on the observational data in double-lined eclipsing binary systems. We also quantify the bias that is caused by the lack of constraints on the initial helium content and on the efficiencies of the superadiabatic convection and microscopic diffusion. We adopted a modified grid-based SCEPtER pipeline using as observational constraints the effective temperatures, [Fe/H], masses, and radii of the two stars. In a reference scenario of mild overshooting $\\beta = 0.2$ for the synthetic data, we found both large statistical uncertainties and biases on the estimated $\\beta$. For the first 80% of the MS evolution, $\\beta$ is biased and practically unconstrained in the whole explored range [0.0; 0.4]. In the last 5% of the MS the bias vanishes and the $1 \\sigma$ error is about 0.05. For synthetic data computed with $\\beta = 0.0$, the estimated $\\beta$ is ...

  20. High precision and high accuracy isotopic measurement of uranium using lead and thorium calibration solutions by inductively coupled plasma-multiple collector-mass spectrometry

    International Nuclear Information System (INIS)

    A novel method for the high accuracy and high precision measurement of uranium isotopic composition by Inductively Coupled Plasma-Multiple Collector-Mass Spectrometry is discussed. Uranium isotopic samples are spiked with either thorium or lead for use as internal calibration reference materials. This method eliminates the necessity to periodically measure uranium standards to correct for changing mass bias when samples are measured over long time periods. This technique has generated among the highest levels of analytical precision on both the major and minor isotopes of uranium. Sample throughput has also been demonstrated to exceed Thermal Ionization Mass Spectrometry by a factor of four to five

  1. Improved precision and accuracy for high-performance liquid chromatography/Fourier transform ion cyclotron resonance mass spectrometric exact mass measurement of small molecules from the simultaneous and controlled introduction of internal calibrants via a second electrospray nebuliser.

    Science.gov (United States)

    Herniman, Julie M; Bristow, Tony W T; O'Connor, Gavin; Jarvis, Jackie; Langley, G John

    2004-01-01

    The use of a second electrospray nebuliser has proved to be highly successful for exact mass measurement during high-performance liquid chromatography/Fourier transform ion cyclotron resonance mass spectrometry (HPLC/FTICRMS). Much improved accuracy and precision of mass measurement were afforded by the introduction of the internal calibration solution, thus overcoming space charge issues due to the lack of control over relative ion abundances of the species eluting from the HPLC column. Further, issues of suppression of ionisation, observed when using a T-piece method, are addressed and this simple system has significant benefits over other more elaborate approaches providing data that compares very favourably with these other approaches. The technique is robust, flexible and transferable and can be used in conjunction with HPLC, infusion or flow injection analysis (FIA) to provide constant internal calibration signals to allow routine, accurate and precise mass measurements to be recorded.

  2. The photoelectronic behaviors of MoO3-loaded ZrO2/carbon cluster nanocomposite materials

    Science.gov (United States)

    Matsui, H.; Ishiko, A.; Karuppuchamy, S.; Hassan, M. A.; Yoshihara, M.

    2012-03-01

    A novel nano-sized ZrO2/carbon cluster composite materials (Ic's) were successfully obtained by the calcination of ZrCl4/starch complexes I's under an argon atmosphere. Pt- and/or MoO3-loaded ZrO2/carbon clusters composite materials were also prepared by doping Pt and/or MoO3 particles on the surface of Ic's. The surface characterization of the composite materials was carried out using transmission electron microscopy (TEM). The TEM observation of the materials showed the presence of particles with the diameters of a few nanometers, possibly Pt particles, and of 50-100 nm, possibly MoO3 particles, in the matrix. Pt- and/or MoO3-loaded ZrO2/carbon cluster composite materials show the efficient photocatalytic activity under visible light irradiation.

  3. Theoretical study of the nucleation/growth process of carbon clusters under pressure.

    Science.gov (United States)

    Pineau, N; Soulard, L; Los, J H; Fasolino, A

    2008-07-14

    We used molecular dynamics and the empirical potential for carbon LCBOPII to simulate the nucleation/growth process of carbon clusters both in vacuum and under pressure. In vacuum, our results show that the growth process is homogeneous and yields mainly sp(2) structures such as fullerenes. We used an argon gas and Lennard-Jones potentials to mimic the high pressures and temperatures reached during the detonation of carbon-rich explosives. We found that these extreme thermodynamic conditions do not affect substantially the topologies of the clusters formed in the process. However, our estimation of the growth rates under pressure are in much better agreement with the values estimated experimentally than our vacuum simulations. The formation of sp(3) carbon was negligible both in vacuum and under pressure which suggests that larger simulation times and cluster sizes are needed to allow the nucleation of nanodiamonds. PMID:18624553

  4. Gas chromatography-mass spectrometry of ethyl palmitate calibration and resolution with ethyl oleate as biomarker ethanol sub acute in urine application study

    Science.gov (United States)

    Suaniti, Ni Made; Manurung, Manuntun

    2016-03-01

    Gas Chromatography-Mass Spectrometry is used to separate two and more compounds and identify fragment ion specific of biomarker ethanol such as palmitic acid ethyl ester (PAEE), as one of the fatty acid ethyl esters as early detection through conyugated reaction. This study aims to calibrate ethyl palmitate and develop analysis with oleate acid. This methode can be used analysis ethanol and its chemistry biomarker in ethanol sub-acute consumption as analytical forensic toxicology. The result show that ethanol level in urine rats Wistar were 9.21 and decreased 6.59 ppm after 48 hours consumption. Calibration curve of ethyl palmitate was y = 0.2035 x + 1.0465 and R2 = 0.9886. Resolution between ethyl palmitate and oleate were >1.5 as good separation with fragment ion specific was 88 and the retention time was 18 minutes.

  5. Mass segregation and fractal substructure in young massive clusters: (I) the McLuster code and method calibration

    CERN Document Server

    Kuepper, A H W; Kroupa, P; Baumgardt, H

    2011-01-01

    By analysing models of the young massive cluster R136 in 30 Doradus, set-up using the herewith introduced and publicly made available code McLuster, we investigate and compare different methods for detecting and quantifying mass segregation and substructure in non-seeing limited N-body data. For this purpose we generate star cluster models with different degrees of mass segregation and fractal substructure and analyse them. We quantify mass segregation by measuring, from the projected 2d model data, the mass function slope in radial annuli, by looking for colour gradients in radial colour profiles, by measuring Allison's Lambda parameter, and by determining the local stellar surface density around each star. We find that these methods for quantifying mass segregation often produce ambiguous results. Most reliable for detecting mass segregation is the mass function slope method, whereas the colour gradient method is the least practical in an R136-like configuration. The other two methods are more sensitive to ...

  6. Weak-Lensing Mass Calibration of the Atacama Cosmology Telescope Equatorial Sunyaev-Zeldovich Cluster Sample with the Canada-France-Hawaii Telescope Stripe 82 Survey

    CERN Document Server

    Battaglia, N; Miyatake, H; Hasselfield, M; Gralla, M B; Allison, R; Bond, J R; Calabrese, E; Crichton, D; Devlin, M J; Dunkley, J; Dünner, R; Erben, T; Ferrara, S; Halpern, M; Hilton, M; Hill, J C; Hincks, A D; Hložek, R; Huffenberger, K M; Hughes, J P; Kneib, J P; Kosowsky, A; Makler, M; Marriage, T A; Menanteau, F; Miller, L; Moodley, K; Moraes, B; Niemack, M D; Page, L; Shan, H; Sehgal, N; Sherwin, B D; Sievers, J L; Sifón, C; Spergel, D N; Staggs, S T; Taylor, J; Thornton, R; van Waerbeke, L; Wollack, E J

    2015-01-01

    Mass calibration uncertainty is the largest systematic effect for using clusters of galaxies to constrain cosmological parameters. We present weak lensing mass measurements from the Canada-France-Hawaii Telescope Stripe 82 Survey for galaxy clusters selected through their high signal-to-noise thermal Sunyaev-Zeldovich (tSZ) signal measured with the Atacama Cosmology Telescope (ACT). The average weak lensing mass is $\\left(4.8\\pm0.8\\right)\\,\\times10^{14}\\,\\mathrm{M}_\\odot$, consistent with the tSZ mass estimate of $\\left(4.70\\pm1.0\\right)\\,\\times10^{14}\\,\\mathrm{M}_\\odot$ which assumes a universal pressure profile for the cluster gas. Our results are consistent with previous weak-lensing measurements of tSZ-detected clusters from the Planck satellite. When comparing our results, we estimate the Eddington bias correction for the sample intersection of Planck and weak-lensing clusters which was previously neglected.

  7. Weak-lensing mass calibration of the Atacama Cosmology Telescope equatorial Sunyaev-Zeldovich cluster sample with the Canada-France-Hawaii telescope stripe 82 survey

    Science.gov (United States)

    Battaglia, N.; Leauthaud, A.; Miyatake, H.; Hasselfield, M.; Gralla, M. B.; Allison, R.; Bond, J. R.; Calabrese, E.; Crichton, D.; Devlin, M. J.; Dunkley, J.; Dünner, R.; Erben, T.; Ferrara, S.; Halpern, M.; Hilton, M.; Hill, J. C.; Hincks, A. D.; Hložek, R.; Huffenberger, K. M.; Hughes, J. P.; Kneib, J. P.; Kosowsky, A.; Makler, M.; Marriage, T. A.; Menanteau, F.; Miller, L.; Moodley, K.; Moraes, B.; Niemack, M. D.; Page, L.; Shan, H.; Sehgal, N.; Sherwin, B. D.; Sievers, J. L.; Sifón, C.; Spergel, D. N.; Staggs, S. T.; Taylor, J. E.; Thornton, R.; van Waerbeke, L.; Wollack, E. J.

    2016-08-01

    Mass calibration uncertainty is the largest systematic effect for using clusters of galaxies to constrain cosmological parameters. We present weak lensing mass measurements from the Canada-France-Hawaii Telescope Stripe 82 Survey for galaxy clusters selected through their high signal-to-noise thermal Sunyaev-Zeldovich (tSZ) signal measured with the Atacama Cosmology Telescope (ACT). For a sample of 9 ACT clusters with a tSZ signal-to-noise greater than five the average weak lensing mass is (4.8±0.8) ×1014 Msolar, consistent with the tSZ mass estimate of (4.70±1.0) ×1014 Msolar which assumes a universal pressure profile for the cluster gas. Our results are consistent with previous weak-lensing measurements of tSZ-detected clusters from the Planck satellite. When comparing our results, we estimate the Eddington bias correction for the sample intersection of Planck and weak-lensing clusters which was previously excluded.

  8. Testing Newtonian Gravity with AAOmega: Mass-To-Light Profiles and Metallicity Calibrations From 47 Tuc and M55

    CERN Document Server

    Lane, Richard R; Lewis, Geraint F; Ibata, Rodrigo A; Siebert, Arnaud; Bedding, Timothy R; Székely, Péter

    2009-01-01

    Globular clusters are an important test bed for Newtonian gravity in the weak-acceleration regime, which is vital to our understanding of the nature of the gravitational interaction. Recent claims have been made that the velocity dispersion profiles of globular clusters flatten out at large radii, despite an apparent paucity of dark matter in such objects, indicating the need for a modification of gravitational theories. We continue our investigation of this claim, with the largest spectral samples ever obtained of 47 Tucanae and M55. Furthermore, this large sample allows for an accurate metallicity calibration based on the equivalent widths of the calcium triplet lines and K band magnitude of the Tip of the Red Giant Branch. Assuming an isothermal distribution, the rotations of each cluster are also measured with both clusters exhibiting clear rotation signatures. The global velocity dispersions of NGC 121 and Kron 3, two globular clusters in the Small Magellanic Cloud, are also calculated. By applying a sim...

  9. Weak-lensing mass calibration of redMaPPer galaxy clusters in Dark Energy Survey Science Verification data

    CERN Document Server

    Melchior, P; McClintock, T; Varga, T N; Sheldon, E; Rozo, E; Amara, A; Becker, M R; Benson, B A; Bermeo, A; Bridle, S L; Clampitt, J; Dietrich, J P; Hartley, W G; Hollowood, D; Jain, B; Jarvis, M; Jeltema, T; Kacprzak, T; MacCrann, N; Rykoff, E S; Saro, A; Suchyta, E; Troxel, M A; Zuntz, J; Bonnett, C; Plazas, A A; Abbott, T M C; Abdalla, F B; Annis, J; Benoit-Lévy, A; Bernstein, G M; Bertin, E; Brooks, D; Buckley-Geer, E; Rosell, A Carnero; Kind, M Carrasco; Carretero, J; Cunha, C E; D'Andrea, C B; da Costa, L N; Desai, S; Eifler, T F; Flaugher, B; Fosalba, P; García-Bellido, J; Gaztanaga, E; Gerdes, D W; Gruendl, R A; Gschwend, J; Gutierrez, G; Honscheid, K; James, D J; Kirk, D; Krause, E; Kuehn, K; Kuropatkin, N; Lahav, O; Lima, M; Maia, M A G; March, M; Martini, P; Menanteau, F; Miller, C J; Miquel, R; Mohr, J J; Nichol, R C; Ogando, R; Romer, A K; Sanchez, E; Scarpine, V; Sevilla-Noarbe, I; Smith, R C; Soares-Santos, M; Sobreira, F; Swanson, M E C; Tarle, G; Thomas, D; Walker, A R; Weller, J; Zhang, Y

    2016-01-01

    We use weak-lensing shear measurements to determine the mean mass of optically selected galaxy clusters in Dark Energy Survey Science Verification data. In a blinded analysis, we split the sample of more than 8,000 redMaPPer clusters into 15 subsets, spanning ranges in the richness parameter $5 \\leq \\lambda \\leq 180$ and redshift $0.2 \\leq z \\leq 0.8$, and fit the averaged mass density contrast profiles with a model that accounts for seven distinct sources of systematic uncertainty: shear measurement and photometric redshift errors; cluster-member contamination; miscentering; deviations from the NFW halo profile; halo triaxiality; and line-of-sight projections. We combine the inferred cluster masses to estimate the joint scaling relation between mass, richness and redshift, $\\mathcal{M}(\\lambda,z) \\varpropto M_0 \\lambda^{F} (1+z)^{G}$. We find $M_0 \\equiv \\langle M_{200\\mathrm{m}}\\,|\\,\\lambda=30,z=0.5\\rangle=\\left[ 2.35 \\pm 0.22\\ \\rm{(stat)} \\pm 0.12\\ \\rm{(sys)} \\right] \\cdot 10^{14}\\ M_\\odot$, with $F = 1.12...

  10. Calibration and adjustment of center of mass(COM) based on EKF during in-flight phase

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    The electrostatic accelerometer,assembled on gravity satellite,serves to measure all non-gravitational accelerations caused by atmosphere drag or solar radiation pressure,etc.The proof-mass center of the accelerometer needs to be precisely positioned at the center of gravity satellite,otherwise,the offset between them will bring measurement disturbance due to angular acceleration of satellite and gradient.Because of installation and measurement errors on the ground,fuel consumption during the in-flight phase and other adverse factors,the offset between the proof-mass center and the satellite center of mass is usually large enough to affect the measurement accuracy of the accelerometer,even beyond its range.Therefore,the offset needs to be measured or estimated,and then be controlled within the measurement requirement of the accelerometer by the center of mass(COM) adjustment mechanism during the life of the satellite.The estimation algorithm based on EKF,which uses the measurement of accelerometer,gyro and magnetometer,is put forward to estimate the offset,and the COM adjustment mechanism then adjusts the satellite center of mass in order to make the offset meet the requirement.With the special configuration layout,the COM adjustment mechanism driven by the stepper motors can separately regulate X,Y and Z axes.The associated simulation shows that the offset can be con-trolled better than 0.03 mm for all the axes with the method mentioned above.

  11. Fabrication of SO/sub 2/preparation system and calibration of PINSTECH sulfur standard for /sup 34/S/sup 32/S mass spectrometric analysis

    International Nuclear Information System (INIS)

    This report describes the fabrication and standardization of operation procedures of a SO/sub 2/ preparation system used for the extraction of sulfur dioxide gas from sulfur minerals (aqueous sulfate, elemental sulfur, and sulfides) for sulfur isotope ratio measurements on a gas source mass spectrometer for hydrological, geological and environmental applications. SO/sub 2/ preparation procedure as described by Fumitaka Yanagisawa and Hitoshi Sakai (1983) is adopted with some modifications. A chemically pure BaSO/sub 4/ powder is chosen as PINSTECH Sulfur Standard PSS-I for routine laboratory /sup 34/S analysis. PSS-1 is calibrated against the International Atomic Energy Agency (IAEA) standard Cannon Diablo Troilite (CDT) using the NBS-127 sulfur standard Sigma /sup 34/S values of PSS-1 as analyzed at PINSTECH and Institute fur Hydorlogie, Munich are found to be 14.58 +-0.07 % CDT (n=6) and 14.59+-0.15% CDT (n=2) respectively. NBS-127 is BaSO/sub 4/ powder from the National Bureau of Standards, USA and has been calibrated against CDT. Interlaboratory comparison of various standards is also documented. Using this system, the reproducibility of sulfur isotope ratio measurements is better than +-0.2 % (n=10). (author)

  12. Metallicity of M dwarfs I. A photometric calibration and impact on the mass-luminosity relation at the bottom of the main sequence

    CERN Document Server

    Bonfils, X; Udry, S; Santos, N C; Forveille, T; Ségransan, D

    2005-01-01

    We obtained high resolution ELODIE and CORALIE spectra for both components of 20 wide visual binaries composed of an F-, G- or K-dwarf primary and an M-dwarf secondary. We analyse the well understood spectra of the primaries to determine metallicities ([Fe/H]) for these 20 systems, and hence for their M dwarf components. We pool these metallicities with determinations from the literature to obtain a precise (+- 0.2 dex) photometric calibration of M dwarf metallicities. This calibration represents a breakthrough in a field where discussions have had to remain largely qualitative, and it helps us demonstrate that metallicity explains most of the large dispersion in the empirical V-band mass-luminosity relation. We examine the metallicity of the two known M-dwarf planet-host stars, Gl 876 (+0.02 dex) and Gl 436 (-0.03 dex), in the context of preferential planet formation around metal-rich stars. We finally determine the metallicity of the 47 brightest single M dwarfs in a volume limited sample, and compare the m...

  13. Measuring the extent of convective cores in low-mass stars using Kepler data: towards a calibration of core overshooting

    CERN Document Server

    Deheuvels, S; Aguirre, V Silva; Ballot, J; Michel, E; Cunha, M S; Lebreton, Y; Appourchaux, T

    2016-01-01

    Our poor understanding of the boundaries of convective cores generates large uncertainties on the extent of these cores and thus on stellar ages. Our aim is to use asteroseismology to consistently measure the extent of convective cores in a sample of main-sequence stars whose masses lie around the mass-limit for having a convective core. We first test and validate a seismic diagnostic that was proposed to probe in a model-dependent way the extent of convective cores using the so-called $r_{010}$ ratios, which are built with $l=0$ and $l=1$ modes. We apply this procedure to 24 low-mass stars chosen among Kepler targets to optimize the efficiency of this diagnostic. For this purpose, we compute grids of stellar models with both the CESAM2k and MESA evolution codes, where the extensions of convective cores are modeled either by an instantaneous mixing or as a diffusion process. Among the selected targets, we are able to unambiguously detect convective cores in eight stars and we obtain seismic measurements of th...

  14. Effects of functional group modification on the thermal properties of nano-carbon clusters

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Zhenyi, E-mail: zywu@xmu.edu.cn [Xiamen University, Department of Chemistry and College of Chemistry and Chemical Engineering (China); Cai, Xueying [Xiamen University, Xiamen Zhongshan Hospital (China); Yang, Zhiquan [South China University of Technology, School of Environment and Energy, Guangzhou Higher Education Mega Centre (China)

    2015-08-15

    In this paper, the thermal properties including thermal stability, thermal decomposition activation energy and the thermal enthalpy of nano-carbon clusters (NCCs, including fullerene[60](C{sub 60}, with a diameter of 0.71 nm), multi-walled carbon nanotubes(MWCNTs, with a diameter of 10–30 nm and a length of 1–2 µm), single-walled carbon nanotubes (SWCNTs, with a diameter of ∼2 nm and a length of 5–15 µm), ligands of NCC-based terpyridine (NCC-tpy), and NCC-based ruthenium complexes (NCC-tpyRuCl{sub 3}) were systematically studied by method of simultaneous thermogravimetric and differential thermal analysis. The results show that the modification of NCCs with terpyridine leads to a decrease in the thermal stability and in the thermal decomposition activation energy (the thermal decomposition activation energy decreased from 174.4 for C{sub 60}, 144.9 for MWCNTs and 161.2 kJ/mol for SWCNTs to 166.2 for C{sub 60}-tpy, 119.7 for MWCNT-tpy and 85.0 kJ/mol for SWCNT-tpy). But the modification of NCCs with terpyridine results in an increase in the enthalpy change of NCC thermal decomposition reaction. The introduction of the metal ions through complexation further decreases the thermal stability and the thermal decomposition activation energy of NCC-tpyRuCl{sub 3} due to the catalytic oxidation of Ru(III) ions (the activation energy decreases to 124.1 for C{sub 60}-tpyRuCl{sub 3}, 106.4 for MWCNT-tpyRuCl{sub 3} and 41.2 kJ/mol for SWCNT-tpyRuCl{sub 3}). The introduction of the metal ions also leads to a decrease in the enthalpy change of the thermal decomposition reaction.

  15. Top-Quark Pair Production Cross Sections and Calibration of the Top-Quark Monte-Carlo Mass

    CERN Document Server

    AUTHOR|(CDS)2082000

    2015-01-01

    In this thesis, measurements of the production cross sections for top-quark pairs andthe determination of the top-quark mass are presented. Dileptonic decays of top-quarkpairs (tt) with two opposite-charged lepton (electron and muon) candidates in the finalstate are considered. The studied data samples are collected in proton-proton collisionsat the CERN Large Hadron Collider with the CMS detector and correspond to inte√grated luminosities of 5.0 fb−1 and 19.7 fb−1 at center-of-mass energies of s = 7 TeV and√s = 8 TeV, respectively. The cross sections, σtt , are measured in the fiducial detectorvolume (visible phase space), defined by the kinematics of the top-quark decay products,and are extrapolated to the full phase space. The visible cross sections are extracted in asimultaneous binned-likelihood fit to multi-differential distributions of final-state observables, categorized according to the multiplicity of jets associated to b quarks (b jets) andother jets in each event. The fit is perfor...

  16. The end-Cretaceous in the southwestern Tethys (Elles, Tunisia): orbital calibration of paleoenvironmental events before the mass extinction

    Science.gov (United States)

    Thibault, Nicolas; Galbrun, Bruno; Gardin, Silvia; Minoletti, Fabrice; Le Callonnec, Laurence

    2016-04-01

    An integrated study of magnetic mass susceptibility (MS), bulk stable isotopes and calcareous nannofossil paleoecological changes is undertaken on the late Maastrichtian of the Elles section, Tunisia, spanning the last ca. 1 Myr of the Cretaceous. A cyclostratigraphic analysis reveals the presence of Milankovitch frequencies and is used for proposal of two distinct orbital age models and to provide ages of important stratigraphic horizons, relative to the age of the Cretaceous-Paleogene boundary (K-PgB). Principal component analysis (PCA) performed on the nannofossil assemblage reveal two main factors, PCA1, mostly representing fluctuations of D. rotatorius, P. stoveri, Lithraphidites spp., Retecapsa spp., Staurolithites spp., Micula spp., and PCA2, mostly representing fluctuations of A. regularis, C. ehrenbergii, Micula spp., Rhagodiscus spp., W. barnesiae and Zeugrhabdotus spp. Variations in PCA1 and PCA2 match changes in bulk δ13C and δ18O, respectively, and suggest changes in surface-water fertility and temperatures and associated stress. The variations in abundances of high-latitude taxa and the warm-water species Micula murus and in bulk δ18O delineate fast changes in sea-surface paleotemperatures. As in many other sites, an end-Maastrichtian greenhouse warming is highlighted, followed by a short cooling and an additional warm pulse in the last 30 kyr of the Maastrichtian which has rarely been documented so far. Orbital tuning of the delineated climatic events is proposed following the two different age models. Calcareous nannofossil assemblages highlight a decrease in surface-water nutriency, but their species richness remains high through the latest Maastrichtian, indicating, in Tunisia, a weak impact of Deccan volcanism on calcareous nannoplankton diversity before the mass extinction.

  17. Novel calibrations of virial black hole mass estimators in active galaxies based on X-ray luminosity and optical/NIR emission lines

    CERN Document Server

    Ricci, F; Onori, F; Bianchi, S

    2016-01-01

    Accurately weigh the masses of SMBH in AGN is currently possible for only a small group of local and bright broad-line AGN through reverberation mapping (RM). Statistical demographic studies can be carried out considering the empirical scaling relation between the size of the BLR and the AGN optical continuum luminosity. However, there are still biases against low-luminosity or reddened AGN, in which the rest-frame optical radiation can be severely absorbed/diluted by the host and the BLR emission lines could be hard to detect. Our purpose is to widen the applicability of virial-based SE relations to reliably measure the BH masses also for low-luminosity or intermediate/type 2 AGN that are missed by current methodology. We achieve this goal by calibrating virial relations based on unbiased quantities: the hard X-ray luminosities, in the 2-10 keV and 14-195 keV bands, that are less sensitive to galaxy contamination, and the FWHM of the most important rest-frame NIR and optical BLR emission lines. We built a sa...

  18. Multivariate Calibration Approach for Quantitative Determination of Cell-Line Cross Contamination by Intact Cell Mass Spectrometry and Artificial Neural Networks.

    Directory of Open Access Journals (Sweden)

    Elisa Valletta

    Full Text Available Cross-contamination of eukaryotic cell lines used in biomedical research represents a highly relevant problem. Analysis of repetitive DNA sequences, such as Short Tandem Repeats (STR, or Simple Sequence Repeats (SSR, is a widely accepted, simple, and commercially available technique to authenticate cell lines. However, it provides only qualitative information that depends on the extent of reference databases for interpretation. In this work, we developed and validated a rapid and routinely applicable method for evaluation of cell culture cross-contamination levels based on mass spectrometric fingerprints of intact mammalian cells coupled with artificial neural networks (ANNs. We used human embryonic stem cells (hESCs contaminated by either mouse embryonic stem cells (mESCs or mouse embryonic fibroblasts (MEFs as a model. We determined the contamination level using a mass spectra database of known calibration mixtures that served as training input for an ANN. The ANN was then capable of correct quantification of the level of contamination of hESCs by mESCs or MEFs. We demonstrate that MS analysis, when linked to proper mathematical instruments, is a tangible tool for unraveling and quantifying heterogeneity in cell cultures. The analysis is applicable in routine scenarios for cell authentication and/or cell phenotyping in general.

  19. Formation and properties of astrophysical carbonaceous dust. I: ab-initio calculations of the configuration and binding energies of small carbon clusters

    CERN Document Server

    Mauney, Christopher; Lazzati, Davide

    2014-01-01

    The binding energies of n < 100 carbon clusters are calculated using the ab-initio density functional theory code Quantum Espresso. Carbon cluster geometries are determined using several levels of classical techniques and further refined using density functional theory. The resulting energies are used to compute the work of cluster formation and the nucleation rate in a saturated, hydrogen-poor carbon gas. Compared to classical calculations that adopt the capillary approximation, we find that nucleation of carbon clusters is enhanced at low temperatures and depressed at high temperatures. This difference is ascribed to the different behavior of the critical cluster size. We find that the critical cluster size is at n = 27 or n = 8 for a broad range of temperatures and saturations, instead of being a smooth function of such parameters. The results of our calculations can be used to follow carbonaceous cluster/grain formation, stability, and growth in hydrogen poor environments, such as the inner layers of c...

  20. Calibration uncertainty

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Anglov, Thomas

    2002-01-01

    uncertainty was verified from independent measurements of the same sample by demonstrating statistical control of analytical results and the absence of bias. The proposed method takes into account uncertainties of the measurement, as well as of the amount of calibrant. It is applicable to all types......Methods recommended by the International Standardization Organisation and Eurachem are not satisfactory for the correct estimation of calibration uncertainty. A novel approach is introduced and tested on actual calibration data for the determination of Pb by ICP-AES. The improved calibration...

  1. Top pairs production and effects of new physics. Jet calibration with W into jet-jet process. Top mass measurement; Production de paires de Top et effet de Nouvelle Physique. Calibration des jets avec le processus Wen en jet-jet. Mesure de la masse du Top

    Energy Technology Data Exchange (ETDEWEB)

    Cogneras, E

    2007-06-15

    Since it was discovered in 1995 at Fermilab, the top quark is the subject of a great attention. It completes the third quark generation of the standard model of particle physics, and the measurement of its properties constrains strongly this model. It is also a preferential way to probe new physics expected around 1 TeV. This thesis, performed using the Atlas detector at LHC, describes the methods implemented in order to measure precisely the top quark mass in the lepton + jets channel. Several analysis ways are presented in function of the performances of the detector, especially its capacity to identify the b jets. The precise measurement of the top quark mass needs a deep understanding of the jet energy scale. This thesis suggests a strategy to calibrate the light jets using the constraint on the W boson mass, and shows that a precision of 1 GeV{sup 2}/c{sup 2} on the top mass measurement is achievable. An evaluation of the discovery potential of tt-bar resonances, foreseen by models beyond the standard model is also carried out. (author)

  2. High-Precision Mass Measurements of Exotic Nuclei with the Triple-Trap Mass Spectrometer Isoltrap

    CERN Multimedia

    Blaum, K; Zuber, K T; Stanja, J

    2002-01-01

    The masses of close to 200 short-lived nuclides have already been measured with the mass spectrometer ISOLTRAP with a relative precision between 1$\\times$10$^{-7}$ and 1$\\times$10^{-8}$. The installatin of a radio-frequency quadrupole trap increased the overall efficiency by two orders of magnitude which is at present about 1%. In a recent upgrade, we installed a carbon cluster laser ion source, which will allow us to use carbon clusters as mass references for absolute mass measurements. Due to these improvements and the high reliability of ISOLTRAP we are now able to perform accurate high-precision mass measurements all over the nuclear chart. We propose therefore mass measurements on light, medium and heavy nuclides on both sides of the valley of stability in the coming four years. ISOLTRAP is presently the only instrument capable of the high precision required for many of the proposed studies.

  3. Set-up and calibration of an outdoor nozzle-type rainfall simulator for soil erosion studies at the Masse experimental station (central Italy)

    Science.gov (United States)

    Vergni, Lorenzo; Todisco, Francesca

    2016-04-01

    This contribution describes the technical characteristics and the preliminary calibration of a rainfall simulator recently installed by the Department of Agricultural, Food and Environmental Sciences (Perugia University) at the Masse experimental station located 20 km south of Perugia, in the region of Umbria (central Italy). The site includes some USLE plots of different length λ = 11 and 22 m and width w = 2, 4 and 8 m, oriented parallel to a 16 % slope and kept free of vegetation by frequent ploughing. Since 2008, the station enabled to collect data from more than 80 erosive events, that were mainly used to investigate the relationship between rainfall characteristics and soil loss. The relevant soil loss variability that characterizes erosive storm events with similar overall characteristics (duration and/or depth) can be explained by the different rainfall profile of erosive storms and by the different antecedent soil aggregate stability. To analyse in more detail these aspects, recently, the Masse experimental station has been equipped with a semi-portable rainfall simulator placed over two micro-plots of 1x1 m each, having the same topographic and pedologic conditions of the adjacent USLE plots. The rainfall simulator consists of four full-cone spray nozzles for each micro-plot, placed at the angles of a 0.18-m square, centred over the plot at a height of 2.7 m above the ground. The operating pressure is regulated by pressure regulating valves and checked by pressure gauges mounted in correspondence of each nozzle. An electronic control unit regulates the start and stop of the inlet solenoid valves. A range of rainfall intensities can be achieved, by activating different combinations of nozzles (15 different intensities) also during the same simulation trial. The particular design of the plots allows to collect separately the runoff volume deriving from the plots and the water volume fallen outside of the plot. In this way it is possible to derive, by

  4. Calibration campaign against the international prototype of the kilogram in anticipation of the redefinition of the kilogram, part II: evolution of the BIPM as-maintained mass unit from the 3rd periodic verification to 2014

    Science.gov (United States)

    de Mirandés, Estefanía; Barat, Pauline; Stock, Michael; Milton, Martin J. T.

    2016-10-01

    In 2014 the Bureau International des Poids et Mesures (BIPM) carried out a calibration campaign using the international prototype of the kilogram (IPK). This is the second part in a series of publications describing the results of that campaign. As reported in [Metrologia 52 310–6] following the comparisons between the IPK and its official copies, it was found that the BIPM ‘as-maintained mass unit’ was offset by 35 mg from the mass of the IPK in 2014. We report here the results of an investigation into this offset that has considered all data available from internal BIPM mass comparisons carried out between 1992 and 2014. This has enabled us to model the evolution of the offset in the as-maintained mass unit and to identify some possible reasons why it has developed. We also report how the model has been used to estimate corrections to all 1 kg mass calibration certificates issued by the BIPM during this period.

  5. UV spectra of iron-doped carbon clusters FeC_n n = 3-6

    CERN Document Server

    Steglich, Mathias; Johnson, Anatoly; Maier, John P

    2015-01-01

    Electronic transitions of jet-cooled FeC$_n$ clusters ($n = 3 - 6$) were measured between 230 and 300 nm by a mass-resolved 1+1 resonant two-photon ionization technique. Rotational profiles were simulated based on previous calculations of ground state geometries and compared to experimental observations. Reasonable agreement is found for the planar fan-like structure of FeC$_3$. The FeC$_4$ data indicate a shorter distance between the Fe atom and the bent C$_4$ unit of the fan. The transitions are suggested to be $^{3}$A$_{2} \\leftarrow ^{3}$B$_{1}$ for FeC$_3$ and $^{5}$A$_{1} \\leftarrow ^{5}$A$_{1}$ for FeC$_4$. In contrast to the predicted C$_{\\infty \\text{v}}$ geometry, non-linear FeC$_5$ is apparently observed. Line width broadening prevents analysis of the FeC$_6$ spectrum.

  6. New method for calibration of sun photometers

    Institute of Scientific and Technical Information of China (English)

    H.H.Asadov; I.G.Chobanzadeh

    2009-01-01

    A new method for calibration of sun photometers based on Bouguer-Beer law is proposed.The developed basic equation of calibration makes it possible to formulate the derivative methods of calibration on the basis of photometric measurements upon optical air masses,the ratio of which is an integer number.

  7. Systematic Uncertainties in the Spectroscopic Measurements of Neutron-Star Masses and Radii from Thermonuclear X-ray Bursts. III. Absolute Flux Calibration

    OpenAIRE

    Guver, Tolga; Ozel, Feryal; Marshall, Herman; Psaltis, Dimitrios; Guainazzi, Matteo; Diaz-Trigo, Maria

    2015-01-01

    Many techniques for measuring neutron star radii rely on absolute flux measurements in the X-rays. As a result, one of the fundamental uncertainties in these spectroscopic measurements arises from the absolute flux calibrations of the detectors being used. Using the stable X-ray burster, GS 1826-238, and its simultaneous observations by Chandra HETG/ACIS-S and RXTE/PCA as well as by XMM-Newton EPIC-pn and RXTE/PCA, we quantify the degree of uncertainty in the flux calibration by assessing the...

  8. Singly- and doubly-negative carbon clusters in sputtering: Energy spectra, abundance distributions and unimolecular fragmentation

    International Nuclear Information System (INIS)

    The emission of singly- and doubly-charged negative cluster ions in sputtering of graphite by 14.5 keV Cs+ ion bombardment was investigated by mass spectrometry. Specifically, for anionic Cn- (n≤23) and CsCn- (n≤11) and dianionic Cn2- (n≤39) species the emission-energy spectra were recorded and their abundance distributions as a function of cluster size n were determined. The energy spectra provided evidence for cluster decomposition in the ion accelerating region of the spectrometer corresponding to a time scale from some 10-10 s to several 10-8 s. The abundance of these fragment ions are similar to those of the parent ions in terms of the dependence on the size n and their absolute magnitudes converge with increasing cluster size. Due to energetic ejection events, the clusters are sputtered with high internal energies; they cool by unimolecular decomposition. The most probable fragmentation process for Cn- appears to be by evaporation of a neutral C2 molecule. For these decay reactions, the fragmentation-time distributions were derived from the appropriate parts of the energy spectra; they were found to scale exponentially with time. From these data the average lifetimes τ for these unimolecular decompositions were determined. For Cn- the lifetimes slightly increase with n: τ ∼ 8 x 10-9 s at n=6 to τ ∼ 5 x 10-8 s at n=25. Similar values are found for CsCn-, whereas for the dianionic clusters Cn2- they are shorter, τ ∼ (5-7) x 10-9 s for n=12-18. Estimates of internal energies, Eint, of sputtered Cn- clusters were derived from these lifetimes, employing statistical theories of unimolecular decomposition. Values of Eint increase with cluster size n for 5≤n≤25, whereas the average internal energy per constituent atom, Eint/n amounts to ∼1 eV in that range

  9. Photo-electronic behavior of Cu{sub 2}O- and/or CeO{sub 2}-loaded TiO{sub 2}/carbon cluster nanocomposite materials

    Energy Technology Data Exchange (ETDEWEB)

    Matsui, H.; Saitou, Y. [Department of Applied Chemistry, Faculty of Science and Engineering, Kinki University, 3-4-1, Kowakae, Higashiosaka, Osaka 577-8502 (Japan); Karuppuchamy, S., E-mail: chamy@life.kyutech.ac.jp [Graduate School of Life Science and Systems Engineering, Kyushu Institute of Technology, 2-4 Hibikino, Kitakyushu, Fukuoka 808-0196 (Japan); Institute of Bioscience, Universiti Putra Malaysia, 43400 Serdang, Selangor (Malaysia); Hassan, M.A. [Institute of Bioscience, Universiti Putra Malaysia, 43400 Serdang, Selangor (Malaysia); Yoshihara, M. [Department of Applied Chemistry, Faculty of Science and Engineering, Kinki University, 3-4-1, Kowakae, Higashiosaka, Osaka 577-8502 (Japan)

    2012-10-15

    Graphical abstract: Nano-sized TiO{sub 2}/carbon clusters composite materials (I{sub c}'s) have been successfully prepared for the first time by the calcination of TiO(OCOCH{sub 3}CHCOCH{sub 3}){sub 2}/starch complexes (I's) in air. The visible light induced photocatalytic activity of nano-sized TiO{sub 2}/carbon clusters composite materials was observed. Highlights: Black-Right-Pointing-Pointer Nano-sized TiO{sub 2}/carbon cluster composite materials have been synthesized. Black-Right-Pointing-Pointer The surface of the composite was modified with Cu{sub 2}O, CeO{sub 2} and Pt particles. Black-Right-Pointing-Pointer The composite shows the photo-catalytic activity under visible light irradiation. - Abstract: Nano-sized TiO{sub 2}/carbon cluster composite materials have been successfully prepared for the first time by calcination of TiO(OCOCH{sub 3}CHCOCH{sub 3}){sub 2}/starch complexes in air. The surface of composite materials was modified with nano-sized Cu{sub 2}O and CeO{sub 2} particles, followed by the subsequent modification of Pt particles. The composition of the synthesized composite materials was determined using inductively coupled plasma spectroscopy, elemental analysis and surface characterization by transmission electron microscopy. The reduction reaction of methylene blue with the calcined materials under the visible light irradiation has also been examined. The composite material reduced the methylene blue under the irradiation of visible light ({lambda} > 460 nm). The metal oxide-loaded composite materials could also decompose an aqueous silver nitrate solution by visible light irradiation and give O{sub 2} and Ag.

  10. Fragmentation of neutral carbon clusters formed by high velocity atomic collision; Fragmentation d'agregats de carbone neutres formes par collision atomique a haute vitesse

    Energy Technology Data Exchange (ETDEWEB)

    Martinet, G

    2004-05-01

    The aim of this work is to understand the fragmentation of small neutral carbon clusters formed by high velocity atomic collision on atomic gas. In this experiment, the main way of deexcitation of neutral clusters formed by electron capture with ionic species is the fragmentation. To measure the channels of fragmentation, a new detection tool based on shape analysis of current pulse delivered by semiconductor detectors has been developed. For the first time, all branching ratios of neutral carbon clusters are measured in an unambiguous way for clusters size up to 10 atoms. The measurements have been compared to a statistical model in microcanonical ensemble (Microcanonical Metropolis Monte Carlo). In this model, various structural properties of carbon clusters are required. These data have been calculated with Density Functional Theory (DFT-B3LYP) to find the geometries of the clusters and then with Coupled Clusters (CCSD(T)) formalism to obtain dissociation energies and other quantities needed to compute fragmentation calculations. The experimental branching ratios have been compared to the fragmentation model which has allowed to find an energy distribution deposited in the collision. Finally, specific cluster effect has been found namely a large population of excited states. This behaviour is completely different of the atomic carbon case for which the electron capture in the ground states predominates. (author)

  11. Energetics, relative stabilities, and size-dependent properties of nanosized carbon clusters of different families: fullerenes, bucky-diamond, icosahedral, and bulk-truncated structures.

    Science.gov (United States)

    Yu, M; Chaudhuri, I; Leahy, C; Wu, S Y; Jayanthi, C S

    2009-05-14

    Structures and relative stabilities of carbon clusters belonging to different families have been investigated for diameters d simulation. Carbon clusters studied include fullerenes and fullerene-derived structures (e.g., cages and onions), icosahedral structures, bucky-diamond structures, and clusters cut from the bulk diamond with spherical and facetted truncations. The reason for using a semiempirical MD is partly due to the large number of different cases (or carbon allotropes) investigated and partly due to the size of the clusters investigated in this work. The particular flavor of the semiempirical MD scheme is based on a self-consistent and environment-dependent Hamiltonian developed in the framework of linear combination of atomic orbitals. We find that (i) among the families of carbon clusters investigated, fullerene structures have the lowest energy with the relative energy ordering being E(fullerene) structures is likely at d approximately 8 nm, (iii) the highest occupied molecular orbital-lowest unoccupied molecular orbital gap as a function of the diameter for the case of fullerenes shows an oscillatory behavior with the gap ranging from 2 eV to 6 meV, and the gap approaching that of gapless graphite for d > 3.5 nm, and (iv) there can be three types of phase transformations depending on the manner of heating and cooling in our simulated annealing studies: (a) a bucky-diamond structure --> an onionlike structure, (b) an onionlike --> a cage structure, and (c) a bucky-diamond --> a cage structure.

  12. A micro-fluidic sub-microliter sample introduction system for direct analysis of Chinese rice wine by inductively coupled plasma mass spectrometry using external aqueous calibration

    International Nuclear Information System (INIS)

    A microfluidic sub-microliter sample introducing system was developed for direct analysis of Chinese rice wine by inductively coupled plasma mass spectrometry (ICP-MS). It consisted of a microfluidic chip integrating variable-volume sampling channels (0.1–0.8 μL), an eight-way multi-functional valve used in flow injection analysis (FIA), a syringe pump and a peristaltic pump of the Ar ICP-MS instrument. Three solutions, i.e., 15, 40 and 100 g L−1 glucose in 20% ethanol were used to simulate Chinese rice wine of the dry type, the semidry type and the semisweet type, each. The effects of their volume introduced into ICP-MS on the plasma stability and ICP-MS intensities were studied. The experimental results showed that neither alteration of plasma stability nor carbon deposition was observed when the sampling volume of 20% ethanol containing 100 g L−1 glucose was downscaled to 0.8 μL. Further reducing the sampling volume to 0.4 μL, no significant difference between the intensities of multi-element standard prepared in three simulated Chinese rice wine matrices and those in aqueous solution was observed. It indicated no negative effect of Chinese rice wine matrix on the ICP-MS intensities. A sampling volume of 0.4 μL was considered to be a good compromise between sensitivity and matrix effect. The flow rate of the carrier was chosen as 20 μL min−1 for obtaining peaks with the highest peak height within the shortest time. Based on these observations, a microflow injection (μFI) method for the direct determination of cadmium and lead in Chinese rice wine by ICP-MS using an external aqueous calibration was developed. The sample throughput was 45 h−1 with the detection limit of 19.8 and 10.4 ng L−1 for Cd and Pb, respectively. The contents of Cd and Pb in 10 Chinese rice wine samples were measured. The results agreed well with those determined by ICP-MS with the conventional sampling system after microwave assisted digestion. The recoveries of three

  13. A micro-fluidic sub-microliter sample introduction system for direct analysis of Chinese rice wine by inductively coupled plasma mass spectrometry using external aqueous calibration

    Energy Technology Data Exchange (ETDEWEB)

    Cheng, Heyong [Institute of Microanalytical Systems, Department of Chemistry, Zhejiang University, Hangzhou, 310027 (China); College of Material Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou, 310036 (China); Liu, Jinhua [College of Material Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou, 310036 (China); Xu, Zigang [Institute of Analytical and Applied Chemistry, Department of Chemistry, Zhejiang University, Hangzhou, 310027 (China); Yin, Xuefeng, E-mail: yinxf@zju.edu.cn [Institute of Microanalytical Systems, Department of Chemistry, Zhejiang University, Hangzhou, 310027 (China); College of Material Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou, 310036 (China)

    2012-07-15

    A microfluidic sub-microliter sample introducing system was developed for direct analysis of Chinese rice wine by inductively coupled plasma mass spectrometry (ICP-MS). It consisted of a microfluidic chip integrating variable-volume sampling channels (0.1-0.8 {mu}L), an eight-way multi-functional valve used in flow injection analysis (FIA), a syringe pump and a peristaltic pump of the Ar ICP-MS instrument. Three solutions, i.e., 15, 40 and 100 g L{sup -1} glucose in 20% ethanol were used to simulate Chinese rice wine of the dry type, the semidry type and the semisweet type, each. The effects of their volume introduced into ICP-MS on the plasma stability and ICP-MS intensities were studied. The experimental results showed that neither alteration of plasma stability nor carbon deposition was observed when the sampling volume of 20% ethanol containing 100 g L{sup -1} glucose was downscaled to 0.8 {mu}L. Further reducing the sampling volume to 0.4 {mu}L, no significant difference between the intensities of multi-element standard prepared in three simulated Chinese rice wine matrices and those in aqueous solution was observed. It indicated no negative effect of Chinese rice wine matrix on the ICP-MS intensities. A sampling volume of 0.4 {mu}L was considered to be a good compromise between sensitivity and matrix effect. The flow rate of the carrier was chosen as 20 {mu}L min{sup -1} for obtaining peaks with the highest peak height within the shortest time. Based on these observations, a microflow injection ({mu}FI) method for the direct determination of cadmium and lead in Chinese rice wine by ICP-MS using an external aqueous calibration was developed. The sample throughput was 45 h{sup -1} with the detection limit of 19.8 and 10.4 ng L{sup -1} for Cd and Pb, respectively. The contents of Cd and Pb in 10 Chinese rice wine samples were measured. The results agreed well with those determined by ICP-MS with the conventional sampling system after microwave assisted digestion

  14. Use of density functional theory method to calculate structures of neutral carbon clusters Cn (3 ≤ n ≤ 24) and study their variability of structural forms

    International Nuclear Information System (INIS)

    In this work, we present modifications to the well-known basin hopping (BH) optimization algorithm [D. J. Wales and J. P. Doye, J. Phys. Chem. A 101, 5111 (1997)] by incorporating in it the unique and specific nature of interactions among valence electrons and ions in carbon atoms through calculating the cluster’s total energy by the density functional tight-binding (DFTB) theory, using it to find the lowest energy structures of carbon clusters and, from these optimized atomic and electronic structures, studying their varied forms of topological transitions, which include a linear chain, a monocyclic to a polycyclic ring, and a fullerene/cage-like geometry. In this modified BH (MBH) algorithm, we define a spatial volume within which the cluster’s lowest energy structure is to be searched, and introduce in addition a cut-and-splice genetic operator to increase the searching performance of the energy minimum than the original BH technique. The present MBH/DFTB algorithm is, therefore, characteristically distinguishable from the original BH technique commonly applied to nonmetallic and metallic clusters, technically more thorough and natural in describing the intricate couplings between valence electrons and ions in a carbon cluster, and thus theoretically sound in putting these two charged components on an equal footing. The proposed modified minimization algorithm should be more appropriate, accurate, and precise in the description of a carbon cluster. We evaluate the present algorithm, its energy-minimum searching in particular, by its optimization robustness. Specifically, we first check the MBH/DFTB technique for two representative carbon clusters of larger size, i.e., C60 and C72 against the popular cut-and-splice approach [D. M. Deaven and K. M. Ho, Phys. Rev. Lett. 75, 288 (1995)] that normally is combined with the genetic algorithm method for finding the cluster’s energy minimum, before employing it to investigate carbon clusters in the size range C3-C

  15. Systematic Uncertainties in the Spectroscopic Measurements of Neutron-Star Masses and Radii from Thermonuclear X-ray Bursts. III. Absolute Flux Calibration

    CERN Document Server

    Guver, Tolga; Marshall, Herman; Psaltis, Dimitrios; Guainazzi, Matteo; Diaz-Trigo, Maria

    2015-01-01

    Many techniques for measuring neutron star radii rely on absolute flux measurements in the X-rays. As a result, one of the fundamental uncertainties in these spectroscopic measurements arises from the absolute flux calibrations of the detectors being used. Using the stable X-ray burster, GS 1826-238, and its simultaneous observations by Chandra HETG/ACIS-S and RXTE/PCA as well as by XMM-Newton EPIC-pn and RXTE/PCA, we quantify the degree of uncertainty in the flux calibration by assessing the differences between the measured fluxes during bursts. We find that the RXTE/PCA and the Chandra gratings measurements agree with each other within their formal uncertainties, increasing our confidence in these flux measurements. In contrast, XMM-Newton EPIC-pn measures 14.0$\\pm$0.3% less flux than the RXTE/PCA. This is consistent with the previously reported discrepancy with the flux measurements of EPIC-pn, compared to EPIC-MOS1, MOS2 and ACIS-S detectors. We also address the calibration uncertainty in the RXTE/PCA int...

  16. Mercury CEM Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John F. Schabron; Joseph F. Rovani; Susan S. Sorini

    2007-03-31

    The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005, requires that calibration of mercury continuous emissions monitors (CEMs) be performed with NIST-traceable standards. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor generators. The traceability protocol will be written by EPA. Traceability will be based on the actual analysis of the output of each calibration unit at several concentration levels ranging from about 2-40 ug/m{sup 3}, and this analysis will be directly traceable to analyses by NIST using isotope dilution inductively coupled plasma/mass spectrometry (ID ICP/MS) through a chain of analyses linking the calibration unit in the power plant to the NIST ID ICP/MS. Prior to this project, NIST did not provide a recommended mercury vapor pressure equation or list mercury vapor pressure in its vapor pressure database. The NIST Physical and Chemical Properties Division in Boulder, Colorado was subcontracted under this project to study the issue in detail and to recommend a mercury vapor pressure equation that the vendors of mercury vapor pressure calibration units can use to calculate the elemental mercury vapor concentration in an equilibrium chamber at a particular temperature. As part of this study, a preliminary evaluation of calibration units from five vendors was made. The work was performed by NIST in Gaithersburg, MD and Joe Rovani from WRI who traveled to NIST as a Visiting Scientist.

  17. Measurement of the Top Quark Mass with In Situ Jet Energy Scale Calibration Using Hadronic W Boson Decays at CDF-II

    Energy Technology Data Exchange (ETDEWEB)

    Arguin, Jean-Francois [Univ. of Toronto, ON (Canada)

    2006-01-01

    We report a measurement of the top quark mass with the upgraded collider detector at Fermilab (CDF-II). The top quarks are produced in pairs (tt) in proton-antiproton collisions with a center-of-mass energy of 1.96 TeV.

  18. The calibration system for the GERDA experiment

    International Nuclear Information System (INIS)

    The GERDA experiment uses the neutrinoless double beta decay to probe three fundamental questions in neutrino physics - Are they Dirac or Majorana particles? What is their absolute mass? What is the mass hierarchy of the three generations? In my talk I present the calibration system for the Ge semiconductor diodes enriched in Ge-76. The system is used to set the energy scale and calibrate the pulse shapes which will be used to further reject background events. The lowest possible background is crucial for the whole experiment and therefore the calibration system must not interfere with the data acquisition phase while at the same time operate efficiently during the calibration runs.

  19. Pushing the relative mass accuracy limit of ISOLTRAP on exotic nuclei below 10 ppb

    CERN Document Server

    Blaum, K; Bollen, G; Herfurth, F; Kellerbauer, A G; Kluge, H J; Moore, R B; Sauvan, E; Scheidenberger, C; Schwarz, S; Schweikhard, L

    2003-01-01

    The Penning trap mass spectrometer ISOLTRAP plays a leading role in mass spectrometry of short-lived nuclides. The recent installation of a radio-frequency quadrupole trap and a carbon cluster ion source allowed for the first time mass measurements on exotic nuclei with a relative uncertainty of deltam/m approximately equals 1 multiplied by 10**-**8. The status of ISOLTRAP mass spectrometry and recent highlights are presented.

  20. A New 2MASS/2df Selected Sample of Pairs of Galaxies and Calibration of Merging Rate in the Local Universe

    Institute of Scientific and Technical Information of China (English)

    孙艳春; 徐聪; 何香涛

    2003-01-01

    We present a new sample of 37 close major-merger galaxy pairs, selected from the 2-degree field redshift survey of the two-micron all-sky survey (2MASS) galaxies. The selection criteria for our near-infrared pairs are more closely related to galaxy mass (a very important parameter in galaxy evolution models) than those for optical selected samples. Our sample benefits enormously from the high homogeneity and accuracy of the 2MASS database, and false matchings are minimized by the essentially three-dimensional selection procedure. Taking into account the biases, we find that 1.96 (±0.4)% of galaxies are in close major-merger pairs. This indicates a local merging rate of 1.0%, in good agreement with the results in recent studies of optical selected pairs in the local universe. The results derived with our sample have high confidence.

  1. Mercury Continuous Emmission Monitor Calibration

    Energy Technology Data Exchange (ETDEWEB)

    John Schabron; Eric Kalberer; Ryan Boysen; William Schuster; Joseph Rovani

    2009-03-12

    Mercury continuous emissions monitoring systems (CEMs) are being implemented in over 800 coal-fired power plant stacks throughput the U.S. Western Research Institute (WRI) is working closely with the Electric Power Research Institute (EPRI), the National Institute of Standards and Technology (NIST), and the Environmental Protection Agency (EPA) to facilitate the development of the experimental criteria for a NIST traceability protocol for dynamic elemental mercury vapor calibrators/generators. These devices are used to calibrate mercury CEMs at power plant sites. The Clean Air Mercury Rule (CAMR) which was published in the Federal Register on May 18, 2005 and vacated by a Federal appeals court in early 2008 required that calibration be performed with NIST-traceable standards. Despite the vacature, mercury emissions regulations in the future will require NIST traceable calibration standards, and EPA does not want to interrupt the effort towards developing NIST traceability protocols. The traceability procedures will be defined by EPA. An initial draft traceability protocol was issued by EPA in May 2007 for comment. In August 2007, EPA issued a conceptual interim traceability protocol for elemental mercury calibrators. The protocol is based on the actual analysis of the output of each calibration unit at several concentration levels ranging initially from about 2-40 {micro}g/m{sup 3} elemental mercury, and in the future down to 0.2 {micro}g/m{sup 3}, and this analysis will be directly traceable to analyses by NIST. The EPA traceability protocol document is divided into two separate sections. The first deals with the qualification of calibrator models by the vendors for use in mercury CEM calibration. The second describes the procedure that the vendors must use to certify the calibrators that meet the qualification specifications. The NIST traceable certification is performance based, traceable to analysis using isotope dilution inductively coupled plasma/mass

  2. Mass Calibration of Galaxy Clusters at Redshift 0.1-1.0 using Weak Lensing in the Sloan Digital Sky Survey Stripe 82 Co-add

    CERN Document Server

    Wiesner, Matthew P; Soares-Santos, Marcelle

    2015-01-01

    We present mass-richness relations found in the Sloan Digital Sky Survey Stripe 82 co-add. These relations were found using stacked weak lensing shear observed in a large sample of galaxy clusters. These mass-richness relations are presented for four redshift bins, $0.1 < z \\leq 0.4$, $0.4 < z \\leq 0.7$, $0.7 < z \\leq 1.0$ and $0.1 < z \\leq 1.0$. We describe the sample of galaxy clusters and explain how these clusters were found using a Voronoi Tessellation cluster finder. We fit an NFW profile to the stacked weak lensing shear signal in redshift and richness bins in order to measure virial mass $(M_{200})$. We describe several effects that can bias weak lensing measurements, including photometric redshift bias, the effect of the central BCG, halo miscentering, photometric redshift uncertainty and foreground galaxy contamination. We present mass-richness relations using richness measure $N_{VT}$ with each of these effects considered separately as well as considered altogether. We present values fo...

  3. Reference masses for precision mass spectrometry design and implementation of a Pierce geometry to the cluster Ion source at ISOLTRAP

    CERN Document Server

    Lommen, Jonathan

    At the mass spectrometer ISOLTRAP carbon clusters ($^{12}$Cn, 1$\\leqslant$n$\\leqslant$25) are provided as reference masses, which are of particular importance in higher mass ranges (m $\\geqslant$ 200u). In this mass range the measurlment uncertainty is increasingly dominated by the difference of the reference mass and the mass of the ion of interest. Using carbon clusters instead of the common $^{133}$Cs ions, this difference decreases. The carbon clusters are produced in a laser ion source which has been improved in the frame of this thesis. The fluctuations of the count rate have been investigated as a function of the laser energy. Furthermore, the energy density at the target has been increased by implementation of a telescope into the laser beam line, which leads to a more narrow energy distribution of the ions. Through the exact adjustment of timing and length of a pulsed cavity an energy range with constant count rate could be selected. In order to provide ideal starting conditions during and after the ...

  4. Traceable Pyrgeometer Calibrations

    Energy Technology Data Exchange (ETDEWEB)

    Dooraghi, Mike; Kutchenreiter, Mark; Reda, Ibrahim; Habte, Aron; Sengupta, Manajit; Andreas, Afshin; Newman, Martina

    2016-05-02

    This poster presents the development, implementation, and operation of the Broadband Outdoor Radiometer Calibrations (BORCAL) Longwave (LW) system at the Southern Great Plains Radiometric Calibration Facility for the calibration of pyrgeometers that provide traceability to the World Infrared Standard Group.

  5. Entry tank calibration in TOR pilot plant

    International Nuclear Information System (INIS)

    The objective of this communication is the description of calibration measurements used for determining the uranium and plutonium mass entry in the fast neutron fuel reprocessing pilot plant (TOR) of Marcoule

  6. Electromagnetic Calorimeter Calibration with $\\pi^{0}$

    CERN Multimedia

    Puig Navarro, A

    2009-01-01

    Several methods can be used in order to achieve precise calibration of the LHCb Electromagnetic Calorimeter (ECAL) once reasonable cell equalization has been reached. At low transverse energy, the standard calibration procedure is an iterative method based on the fit of the $\\gamma\\gamma$ invariant mass distribution for each cell of the decay $\\pi^{0}\\to\\gamma\\gamma$ with resolved photons. A new technique for generating the combinatorial background of such decays directly from data has been developed. Knowledge of the background could allow an alternative calibration method based on a event by event fit of the same $\\gamma\\gamma$ invariant mass distribution where contributions from groups of cells are considered in a single fit. The background generation procedure and this possible new calibration method are presented in this poster, in addition to an overview of the LHCb Calorimetry system and ECAL calibration techniques.

  7. The Fundamental Plane at z=1.27 First Calibration of the Mass Scale of Red Galaxies at Redshifts z>1

    CERN Document Server

    Van Dokkum, P G; Dokkum, Pieter G. van

    2003-01-01

    We present results on the Fundamental Plane (FP) of early-type galaxies in the cluster RDCS J0848+4453 at z=1.27. Internal velocity dispersions of three K-selected early-type galaxies are determined from deep Keck spectra. Structural parameters are determined from HST NICMOS images. The galaxies show substantial offsets from the FP of the nearby Coma cluster, as expected from passive evolution of their stellar populations. The offsets from the FP can be expressed as offsets in M/L ratio. The M/L ratios of the two most massive galaxies are consistent with an extrapolation of results obtained at z=0.02-0.83. The evolution of early-type galaxies with masses >10^11 M_sun is well described by ln M/L(B) = (-1.06 +- 0.09) z, corresponding to passive evolution of -1.50 +- 0.13 mag at z=1.3. Ignoring selection effects, the best fitting stellar formation redshift is z*=2.6, corresponding to a luminosity weighted age at the epoch of observation of ~2 Gyr. The M/L ratios of these two galaxies are also in excellent agreem...

  8. Development of a multi-variate calibration approach for quantitative analysis of oxidation resistant Mo-Si-B coatings using laser ablation inductively coupled plasma mass spectrometry

    Science.gov (United States)

    Cakara, Anja; Bonta, Maximilian; Riedl, Helmut; Mayrhofer, Paul H.; Limbeck, Andreas

    2016-06-01

    Nowadays, for the production of oxidation protection coatings in ultrahigh temperature environments, alloys of Mo-Si-B are employed. The properties of the material, mainly the oxidation resistance, are strongly influenced by the Si to B ratio; thus reliable analytical methods are needed to assure exact determination of the material composition for the respective applications. For analysis of such coatings, laser ablation inductively coupled mass spectrometry (LA-ICP-MS) has been reported as a versatile method with no specific requirements on the nature of the sample. However, matrix effects represent the main limitation of laser-based solid sampling techniques and usually the use of matrix-matched standards for quantitative analysis is required. In this work, LA-ICP-MS analysis of samples with known composition and varying Mo, Si and B content was carried out. Between known analyte concentrations and derived LA-ICP-MS signal intensities no linear correlation could be found. In order to allow quantitative analysis independent of matrix effects, a multiple linear regression model was developed. Besides the three target analytes also the signals of possible argides (40Ar36Ar and 98Mo40Ar) as well as detected impurities of the Mo-Si-B coatings (108Pd) were considered. Applicability of the model to unknown samples was confirmed using external validation. Relative deviations from the values determined using conventional liquid analysis after sample digestion between 5 and 10% for the main components Mo and Si were observed.

  9. First principle study of magnetic and electronic properties of single X (X = Al, Si) atom added to small carbon clusters (C n X, n = 2-10)

    Science.gov (United States)

    Afshar, M.; Hoseini, S. S.; Sargolzaei, M.

    2016-07-01

    In this paper, the magnetic and electronic properties of single aluminum and silicon atom added to small carbon clusters (C n X; X = Al, Si; n = 2-10) are studied in the framework of generalized-gradient approximation using density functional theory. The calculations were performed for linear, two dimensional and three dimensional clusters based on full-potential local-orbital (FPLO) method. The total energies, HOMO-LUMO energy gap and total magnetic moments of the most stable structures are presented in this work. The calculations show that C n Si clusters have more stability compared to C n Al clusters. In addition, our magnetic calculations were shown that the C n Al isomers are magnetic objects whereas C n Si clusters are nonmagnetic objects.

  10. Nonadditivity of convoy- and secondary-electron yields in the forward-electron emission from thin carbon foils under irradiation of fast carbon-cluster ions

    Science.gov (United States)

    Tomita, S.; Yoda, S.; Uchiyama, R.; Ishii, S.; Sasa, K.; Kaneko, T.; Kudo, H.

    2006-06-01

    We have measured energy spectra of secondary electrons produced by fast-carbon-cluster Cn+ (n=1-4) bombardment of thin carbon foils (3.2, 7.3, 11.9, and 20.3μg/cm2 ). For clusters of identical velocity, the convoy-electron yield is enhanced with increasing cluster size n , while the yield of secondary electrons is reduced. The yield of convoy electrons normalized to the number of injected atoms increases proportionally with cluster size n . This proportionality suggests that there is only a weak vicinage effect on the number of primary electrons scattered by the projectile. The vicinage effect observed in low-energy secondary electrons must therefore arise from either transport or transmission through the surface.

  11. Trinocular Calibration Method Based on Binocular Calibration

    Directory of Open Access Journals (Sweden)

    CAO Dan-Dan

    2012-10-01

    Full Text Available In order to solve the self-occlusion problem in plane-based multi-camera calibration system and expand the measurement range, a tri-camera vision system based on binocular calibration is proposed. The three cameras are grouped into two pairs, while the public camera is taken as the reference to build the global coordinate. By calibration of the measured absolute distance and the true absolute distance, global calibration is realized. The MRE (mean relative error of the global calibration of the two camera pairs in the experiments can be as low as 0.277% and 0.328% respectively. Experiment results show that this method is feasible, simple and effective, and has high precision.

  12. ORNL calibrations facility

    International Nuclear Information System (INIS)

    The ORNL Calibrations Facility is operated by the Instrumentation Group of the Industrial Safety and Applied Health Physics Division. Its primary purpose is to maintain radiation calibration standards for calibration of ORNL health physics instruments and personnel dosimeters. This report includes a discussion of the radioactive sources and ancillary equipment in use and a step-by-step procedure for calibration of those survey instruments and personnel dosimeters in routine use at ORNL

  13. Spiral reader calibration

    International Nuclear Information System (INIS)

    The method to calibrate the spiral reader (SR) is presented. A brief description of the main procedures of the calibration program SCALP, adapted for the IHEP equipment and purposes, is described. The precision characteristics of the IHEP SR have been analysed on the results, presented in the form of diagrams. There is a calibration manual for the user

  14. Mass spectrometric immunoassay

    Science.gov (United States)

    Nelson, Randall W; Williams, Peter; Krone, Jennifer Reeve

    2007-12-04

    Rapid mass spectrometric immunoassay methods for detecting and/or quantifying antibody and antigen analytes utilizing affinity capture to isolate the analytes and internal reference species (for quantification) followed by mass spectrometric analysis of the isolated analyte/internal reference species. Quantification is obtained by normalizing and calibrating obtained mass spectrum against the mass spectrum obtained for an antibody/antigen of known concentration.

  15. Calibration methods for rotating shadowband irradiometers and evaluation of calibration duration

    Directory of Open Access Journals (Sweden)

    W. Jessen

    2015-10-01

    Full Text Available Resource assessment for Concentrated Solar Power (CSP needs accurate Direct Normal Irradiance (DNI measurements. An option for such measurement campaigns are Rotating Shadowband Irradiometers (RSIs with a thorough calibration. Calibration of RSIs and Si-sensors in general is complex because of the inhomogeneous spectral response of such sensors and incorporates the use of several correction functions. A calibration for a given atmospheric condition and air mass might not work well for a different condition. This paper covers procedures and requirements for two calibration methods for the calibration of Rotating Shadowband Irradiometers. The necessary duration of acquisition of test measurements is examined in regard to the site specific conditions at Plataforma Solar de Almeria (PSA in Spain. Data sets of several long-term calibration periods from PSA are used to evaluate the deviation of results from calibrations with varying duration from the long-term result. The findings show that seasonal changes of environmental conditions are causing small but noticeable fluctuation of calibration results. Certain periods (i.e. November to January and April to May show a higher likelihood of particularly adverse calibration results. These effects can partially be compensated by increasing the inclusions of measurements from outside these periods. Consequently, the duration of calibrations at PSA can now be selected depending on the time of the year in which measurements are commenced.

  16. OLI Radiometric Calibration

    Science.gov (United States)

    Markham, Brian; Morfitt, Ron; Kvaran, Geir; Biggar, Stuart; Leisso, Nathan; Czapla-Myers, Jeff

    2011-01-01

    Goals: (1) Present an overview of the pre-launch radiance, reflectance & uniformity calibration of the Operational Land Imager (OLI) (1a) Transfer to orbit/heliostat (1b) Linearity (2) Discuss on-orbit plans for radiance, reflectance and uniformity calibration of the OLI

  17. 40 CFR 1065.790 - Mass standards.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 32 2010-07-01 2010-07-01 false Mass standards. 1065.790 Section 1065... ENGINE-TESTING PROCEDURES Engine Fluids, Test Fuels, Analytical Gases and Other Calibration Standards § 1065.790 Mass standards. (a) PM balance calibration weights. Use PM balance calibration weights...

  18. The GERDA calibration system

    International Nuclear Information System (INIS)

    A system with three identical custom made units is used for the energy calibration of the GERDA Ge diodes. To perform a calibration the 228Th sources are lowered from the parking positions at the top of the cryostat. Their positions are measured by two independent modules. One, the incremental encoder, counts the holes in the perforated steel band holding the sources, the other measures the drive shaft's angular position even if not powered. The system can be controlled remotely by a Labview program. The calibration data is analyzed by an iterative calibration algorithm determining the calibration functions for different energy reconstruction algorithms and the resolution of several peaks in the 228Th spectrum is determined. A Monte Carlo simulation using the GERDA simulation software MAGE has been performed to determine the background induced by the sources in the parking positions.

  19. Sandia WIPP calibration traceability

    International Nuclear Information System (INIS)

    This report summarizes the work performed to establish calibration traceability for the instrumentation used by Sandia National Laboratories at the Waste Isolation Pilot Plant (WIPP) during testing from 1980-1985. Identifying the calibration traceability is an important part of establishing a pedigree for the data and is part of the qualification of existing data. In general, the requirement states that the calibration of Measuring and Test equipment must have a valid relationship to nationally recognized standards or the basis for the calibration must be documented. Sandia recognized that just establishing calibration traceability would not necessarily mean that all QA requirements were met during the certification of test instrumentation. To address this concern, the assessment was expanded to include various activities

  20. Use of density functional theory method to calculate structures of neutral carbon clusters C{sub n} (3 ≤ n ≤ 24) and study their variability of structural forms

    Energy Technology Data Exchange (ETDEWEB)

    Yen, T. W.; Lai, S. K., E-mail: sklai@coll.phy.ncu.edu.tw [Complex Liquids Laboratory, Department of Physics, National Central University, Chungli 320, Taiwan (China)

    2015-02-28

    In this work, we present modifications to the well-known basin hopping (BH) optimization algorithm [D. J. Wales and J. P. Doye, J. Phys. Chem. A 101, 5111 (1997)] by incorporating in it the unique and specific nature of interactions among valence electrons and ions in carbon atoms through calculating the cluster’s total energy by the density functional tight-binding (DFTB) theory, using it to find the lowest energy structures of carbon clusters and, from these optimized atomic and electronic structures, studying their varied forms of topological transitions, which include a linear chain, a monocyclic to a polycyclic ring, and a fullerene/cage-like geometry. In this modified BH (MBH) algorithm, we define a spatial volume within which the cluster’s lowest energy structure is to be searched, and introduce in addition a cut-and-splice genetic operator to increase the searching performance of the energy minimum than the original BH technique. The present MBH/DFTB algorithm is, therefore, characteristically distinguishable from the original BH technique commonly applied to nonmetallic and metallic clusters, technically more thorough and natural in describing the intricate couplings between valence electrons and ions in a carbon cluster, and thus theoretically sound in putting these two charged components on an equal footing. The proposed modified minimization algorithm should be more appropriate, accurate, and precise in the description of a carbon cluster. We evaluate the present algorithm, its energy-minimum searching in particular, by its optimization robustness. Specifically, we first check the MBH/DFTB technique for two representative carbon clusters of larger size, i.e., C{sub 60} and C{sub 72} against the popular cut-and-splice approach [D. M. Deaven and K. M. Ho, Phys. Rev. Lett. 75, 288 (1995)] that normally is combined with the genetic algorithm method for finding the cluster’s energy minimum, before employing it to investigate carbon clusters in the size

  1. Segment Based Camera Calibration

    Institute of Scientific and Technical Information of China (English)

    马颂德; 魏国庆; 等

    1993-01-01

    The basic idea of calibrating a camera system in previous approaches is to determine camera parmeters by using a set of known 3D points as calibration reference.In this paper,we present a method of camera calibration in whih camera parameters are determined by a set of 3D lines.A set of constraints is derived on camea parameters in terms of perspective line mapping.Form these constraints,the same perspective transformation matrix as that for point mapping can be computed linearly.The minimum number of calibration lines is 6.This result generalizes that of Liu,Huang and Faugeras[12] for camera location determination in which at least 8 line correspondences are required for linear computation of camera location.Since line segments in an image can be located easily and more accurately than points,the use of lines as calibration reference tends to ease the computation in inage preprocessing and to improve calibration accuracy.Experimental results on the calibration along with stereo reconstruction are reported.

  2. Lidar Calibration Centre

    Science.gov (United States)

    Pappalardo, Gelsomina; Freudenthaler, Volker; Nicolae, Doina; Mona, Lucia; Belegante, Livio; D'Amico, Giuseppe

    2016-06-01

    This paper presents the newly established Lidar Calibration Centre, a distributed infrastructure in Europe, whose goal is to offer services for complete characterization and calibration of lidars and ceilometers. Mobile reference lidars, laboratories for testing and characterization of optics and electronics, facilities for inspection and debugging of instruments, as well as for training in good practices are open to users from the scientific community, operational services and private sector. The Lidar Calibration Centre offers support for trans-national access through the EC HORIZON2020 project ACTRIS-2.

  3. Equipment for dosemeter calibration

    International Nuclear Information System (INIS)

    The device is used for precise calibration of dosimetric instrumentation, such as used at nuclear facilities. The high precision of the calibration procedure is primarily due to the fact that one single and steady radiation source is used. The accurate alignment of the source and the absence of shielding materials in the beam axis make for high homogeneity of the beam and reproducibility of the measurement; this is also contributed to by the horizontal displacement of the optical bench, which ensures a constant temperature field and the possibility of adjusting the radiation source at a sufficient distance from the instrument to be calibrated. (Z.S.). 3 figs

  4. Calorimeter energy calibration using the energy conservation law

    Indian Academy of Sciences (India)

    Vasily L Morgunov

    2007-12-01

    A new calorimeter energy calibration method was developed for the proposed ILC detectors. The method uses the center-of-mass energy of the accelerator as the reference. It has been shown that using the energy conservation law it is possible to make ECAL and HCAL cross calibration to reach a good energy resolution for the simple calorimeter energy sum.

  5. PERSONALISED BODY COUNTER CALIBRATION USING ANTHROPOMETRIC PARAMETERS.

    Science.gov (United States)

    Pölz, S; Breustedt, B

    2016-09-01

    Current calibration methods for body counting offer personalisation for lung counting predominantly with respect to ratios of body mass and height. Chest wall thickness is used as an intermediate parameter. This work revises and extends these methods using a series of computational phantoms derived from medical imaging data in combination with radiation transport simulation and statistical analysis. As an example, the method is applied to the calibration of the In Vivo Measurement Laboratory (IVM) at Karlsruhe Institute of Technology (KIT) comprising four high-purity germanium detectors in two partial body measurement set-ups. The Monte Carlo N-Particle (MCNP) transport code and the Extended Cardiac-Torso (XCAT) phantom series have been used. Analysis of the computed sample data consisting of 18 anthropometric parameters and calibration factors generated from 26 photon sources for each of the 30 phantoms reveals the significance of those parameters required for producing an accurate estimate of the calibration function. Body circumferences related to the source location perform best in the example, while parameters related to body mass show comparable but lower performances, and those related to body height and other lengths exhibit low performances. In conclusion, it is possible to give more accurate estimates of calibration factors using this proposed approach including estimates of uncertainties related to interindividual anatomical variation of the target population. PMID:26396263

  6. SPOTS Calibration Example

    Directory of Open Access Journals (Sweden)

    Patterson E.

    2010-06-01

    Full Text Available The results are presented using the procedure outlined by the Standardisation Project for Optical Techniques of Strain measurement to calibrate a digital image correlation system. The process involves comparing the experimental data obtained with the optical measurement system to the theoretical values for a specially designed specimen. The standard states the criteria which must be met in order to achieve successful calibration, in addition to quantifying the measurement uncertainty in the system. The system was evaluated at three different displacement load levels, generating strain ranges from 289 µstrain to 2110 µstrain. At the 289 µstrain range, the calibration uncertainty was found to be 14.1 µstrain, and at the 2110 µstrain range it was found to be 28.9 µstrain. This calibration procedure was performed without painting a speckle pattern on the surface of the metal. Instead, the specimen surface was prepared using different grades of grit paper to produce the desired texture.

  7. Traceable Pyrgeometer Calibrations

    Energy Technology Data Exchange (ETDEWEB)

    Dooraghi, Mike; Kutchenreiter, Mark; Reda, Ibrahim; Habte, Aron; Sengupta, Manajit; Andreas, Afshin; Newman, Martina; Webb, Craig

    2016-05-02

    This presentation provides a high-level overview of the progress on the Broadband Outdoor Radiometer Calibrations for all shortwave and longwave radiometers that are deployed by the Atmospheric Radiation Measurement program.

  8. Air Data Calibration Facility

    Data.gov (United States)

    Federal Laboratory Consortium — This facility is for low altitude subsonic altimeter system calibrations of air vehicles. Mission is a direct support of the AFFTC mission. Postflight data merge is...

  9. Approximation Behooves Calibration

    DEFF Research Database (Denmark)

    da Silva Ribeiro, André Manuel; Poulsen, Rolf

    2013-01-01

    Calibration based on an expansion approximation for option prices in the Heston stochastic volatility model gives stable, accurate, and fast results for S&P500-index option data over the period 2005–2009.......Calibration based on an expansion approximation for option prices in the Heston stochastic volatility model gives stable, accurate, and fast results for S&P500-index option data over the period 2005–2009....

  10. Scanner calibration revisited

    Directory of Open Access Journals (Sweden)

    Pozhitkov Alexander E

    2010-07-01

    Full Text Available Abstract Background Calibration of a microarray scanner is critical for accurate interpretation of microarray results. Shi et al. (BMC Bioinformatics, 2005, 6, Art. No. S11 Suppl. 2. reported usage of a Full Moon BioSystems slide for calibration. Inspired by the Shi et al. work, we have calibrated microarray scanners in our previous research. We were puzzled however, that most of the signal intensities from a biological sample fell below the sensitivity threshold level determined by the calibration slide. This conundrum led us to re-investigate the quality of calibration provided by the Full Moon BioSystems slide as well as the accuracy of the analysis performed by Shi et al. Methods Signal intensities were recorded on three different microarray scanners at various photomultiplier gain levels using the same calibration slide from Full Moon BioSystems. Data analysis was conducted on raw signal intensities without normalization or transformation of any kind. Weighted least-squares method was used to fit the data. Results We found that initial analysis performed by Shi et al. did not take into account autofluorescence of the Full Moon BioSystems slide, which led to a grossly distorted microarray scanner response. Our analysis revealed that a power-law function, which is explicitly accounting for the slide autofluorescence, perfectly described a relationship between signal intensities and fluorophore quantities. Conclusions Microarray scanners respond in a much less distorted fashion than was reported by Shi et al. Full Moon BioSystems calibration slides are inadequate for performing calibration. We recommend against using these slides.

  11. Energy calibration via correlation

    CERN Document Server

    Maier, Daniel

    2015-01-01

    The main task of an energy calibration is to find a relation between pulse-height values and the corresponding energies. Doing this for each pulse-height channel individually requires an elaborated input spectrum with an excellent counting statistics and a sophisticated data analysis. This work presents an easy to handle energy calibration process which can operate reliably on calibration measurements with low counting statistics. The method uses a parameter based model for the energy calibration and concludes on the optimal parameters of the model by finding the best correlation between the measured pulse-height spectrum and multiple synthetic pulse-height spectra which are constructed with different sets of calibration parameters. A CdTe-based semiconductor detector and the line emissions of an 241 Am source were used to test the performance of the correlation method in terms of systematic calibration errors for different counting statistics. Up to energies of 60 keV systematic errors were measured to be le...

  12. Calibrating nacelle lidars

    Energy Technology Data Exchange (ETDEWEB)

    Courtney, M.

    2013-01-15

    Nacelle mounted, forward looking wind lidars are beginning to be used to provide reference wind speed measurements for the power performance testing of wind turbines. In such applications, a formal calibration procedure with a corresponding uncertainty assessment will be necessary. This report presents four concepts for performing such a nacelle lidar calibration. Of the four methods, two are found to be immediately relevant and are pursued in some detail. The first of these is a line of sight calibration method in which both lines of sight (for a two beam lidar) are individually calibrated by accurately aligning the beam to pass close to a reference wind speed sensor. A testing procedure is presented, reporting requirements outlined and the uncertainty of the method analysed. It is seen that the main limitation of the line of sight calibration method is the time required to obtain a representative distribution of radial wind speeds. An alternative method is to place the nacelle lidar on the ground and incline the beams upwards to bisect a mast equipped with reference instrumentation at a known height and range. This method will be easier and faster to implement and execute but the beam inclination introduces extra uncertainties. A procedure for conducting such a calibration is presented and initial indications of the uncertainties given. A discussion of the merits and weaknesses of the two methods is given together with some proposals for the next important steps to be taken in this work. (Author)

  13. Variable Acceleration Force Calibration System (VACS)

    Science.gov (United States)

    Rhew, Ray D.; Parker, Peter A.; Johnson, Thomas H.; Landman, Drew

    2014-01-01

    Conventionally, force balances have been calibrated manually, using a complex system of free hanging precision weights, bell cranks, and/or other mechanical components. Conventional methods may provide sufficient accuracy in some instances, but are often quite complex and labor-intensive, requiring three to four man-weeks to complete each full calibration. To ensure accuracy, gravity-based loading is typically utilized. However, this often causes difficulty when applying loads in three simultaneous, orthogonal axes. A complex system of levers, cranks, and cables must be used, introducing increased sources of systematic error, and significantly increasing the time and labor intensity required to complete the calibration. One aspect of the VACS is a method wherein the mass utilized for calibration is held constant, and the acceleration is changed to thereby generate relatively large forces with relatively small test masses. Multiple forces can be applied to a force balance without changing the test mass, and dynamic forces can be applied by rotation or oscillating acceleration. If rotational motion is utilized, a mass is rigidly attached to a force balance, and the mass is exposed to a rotational field. A large force can be applied by utilizing a large rotational velocity. A centrifuge or rotating table can be used to create the rotational field, and fixtures can be utilized to position the force balance. The acceleration may also be linear. For example, a table that moves linearly and accelerates in a sinusoidal manner may also be utilized. The test mass does not have to move in a path that is parallel to the ground, and no re-leveling is therefore required. Balance deflection corrections may be applied passively by monitoring the orientation of the force balance with a three-axis accelerometer package. Deflections are measured during each test run, and adjustments with respect to the true applied load can be made during the post-processing stage. This paper will

  14. HAWC Timing Calibration

    CERN Document Server

    Huentemeyer, Petra; Dingus, Brenda

    2009-01-01

    The High-Altitude Water Cherenkov (HAWC) Experiment is a second-generation highsensitivity gamma-ray and cosmic-ray detector that builds on the experience and technology of the Milagro observatory. Like Milagro, HAWC utilizes the water Cherenkov technique to measure extensive air showers. Instead of a pond filled with water (as in Milagro) an array of closely packed water tanks is used. The event direction will be reconstructed using the times when the PMTs in each tank are triggered. Therefore, the timing calibration will be crucial for reaching an angular resolution as low as 0.25 degrees.We propose to use a laser calibration system, patterned after the calibration system in Milagro. Like Milagro, the HAWC optical calibration system will use ~1 ns laser light pulses. Unlike Milagro, the PMTs are optically isolated and require their own optical fiber calibration. For HAWC the laser light pulses will be directed through a series of optical fan-outs and fibers to illuminate the PMTs in approximately one half o...

  15. Calibration Under Uncertainty.

    Energy Technology Data Exchange (ETDEWEB)

    Swiler, Laura Painton; Trucano, Timothy Guy

    2005-03-01

    This report is a white paper summarizing the literature and different approaches to the problem of calibrating computer model parameters in the face of model uncertainty. Model calibration is often formulated as finding the parameters that minimize the squared difference between the model-computed data (the predicted data) and the actual experimental data. This approach does not allow for explicit treatment of uncertainty or error in the model itself: the model is considered the %22true%22 deterministic representation of reality. While this approach does have utility, it is far from an accurate mathematical treatment of the true model calibration problem in which both the computed data and experimental data have error bars. This year, we examined methods to perform calibration accounting for the error in both the computer model and the data, as well as improving our understanding of its meaning for model predictability. We call this approach Calibration under Uncertainty (CUU). This talk presents our current thinking on CUU. We outline some current approaches in the literature, and discuss the Bayesian approach to CUU in detail.

  16. Polarimetric Palsar Calibration

    Science.gov (United States)

    Touzi, R.; Shimada, M.

    2008-11-01

    Polarimetric PALSAR system parameters are assessed using data sets collected over various calibration sites. The data collected over the Amazonian forest permits validating the zero Faraday rotation hypotheses near the equator. The analysis of the Amazonian forest data and the response of the corner reflectors deployed during the PALSAR acquisitions lead to the conclusion that the antenna is highly isolated (better than -35 dB). Theses results are confirmed using data collected over the Sweden and Ottawa calibration sites. The 5-m height trihedrals deployed in the Sweden calibration site by the Chalmers University of technology permits accurate measurement of antenna parameters, and detection of 2-3 degree Faraday rotation during day acquisition, whereas no Faraday rotation was noted during night acquisition. Small Faraday rotation angles (2-3 degree) have been measured using acquisitions over the DLR Oberpfaffenhofen and the Ottawa calibration sites. The presence of small but still significant Faraday rotation (2-3 degree) induces a CR return at the cross-polarization HV and VH that should not be interpreted as the actual antenna cross-talk. PALSAR antenna is highly isolated (better than -35 dB), and diagonal antenna distortion matrices (with zero cross-talk terms) can be used for accurate calibration of PALSAR polarimetric data.

  17. GTC Photometric Calibration

    Science.gov (United States)

    di Cesare, M. A.; Hammersley, P. L.; Rodriguez Espinosa, J. M.

    2006-06-01

    We are currently developing the calibration programme for GTC using techniques similar to the ones use for the space telescope calibration (Hammersley et al. 1998, A&AS, 128, 207; Cohen et al. 1999, AJ, 117, 1864). We are planning to produce a catalogue with calibration stars which are suitable for a 10-m telescope. These sources will be not variable, non binary and do not have infrared excesses if they are to be used in the infrared. The GTC science instruments require photometric calibration between 0.35 and 2.5 microns. The instruments are: OSIRIS (Optical System for Imaging low Resolution Integrated Spectroscopy), ELMER and EMIR (Espectrógrafo Multiobjeto Infrarrojo) and the Acquisition and Guiding boxes (Di Césare, Hammersley, & Rodriguez Espinosa 2005, RevMexAA Ser. Conf., 24, 231). The catalogue will consist of 30 star fields distributed in all of North Hemisphere. We will use fields containing sources over the range 12 to 22 magnitude, and spanning a wide range of spectral types (A to M) for the visible and near infrared. In the poster we will show the method used for selecting these fields and we will present the analysis of the data on the first calibration fields observed.

  18. TARGETLESS CAMERA CALIBRATION

    Directory of Open Access Journals (Sweden)

    L. Barazzetti

    2012-09-01

    Full Text Available In photogrammetry a camera is considered calibrated if its interior orientation parameters are known. These encompass the principal distance, the principal point position and some Additional Parameters used to model possible systematic errors. The current state of the art for automated camera calibration relies on the use of coded targets to accurately determine the image correspondences. This paper presents a new methodology for the efficient and rigorous photogrammetric calibration of digital cameras which does not require any longer the use of targets. A set of images depicting a scene with a good texture are sufficient for the extraction of natural corresponding image points. These are automatically matched with feature-based approaches and robust estimation techniques. The successive photogrammetric bundle adjustment retrieves the unknown camera parameters and their theoretical accuracies. Examples, considerations and comparisons with real data and different case studies are illustrated to show the potentialities of the proposed methodology.

  19. The MINOS calibration detector

    International Nuclear Information System (INIS)

    This paper describes the MINOS calibration detector (CalDet) and the procedure used to calibrate it. The CalDet, a scaled-down but functionally equivalent model of the MINOS Far and Near detectors, was exposed to test beams in the CERN PS East Area during 2001-2003 to establish the response of the MINOS calorimeters to hadrons, electrons and muons in the range 0.2-10GeV/c. The CalDet measurements are used to fix the energy scale and constrain Monte Carlo simulations of MINOS

  20. Individual dosimetry and calibration

    International Nuclear Information System (INIS)

    In 1995 both the Individual Dosimetry and Calibration Sections worked under the condition of a status quo and concentrated fully on the routine part of their work. Nevertheless, the machine for printing the bar code which will be glued onto the film holder and hence identify the people when entering into high radiation areas was put into operation and most of the holders were equipped with the new identification. As far as the Calibration Section is concerned the project of the new source control system that is realized by the Technical Support Section was somewhat accelerated

  1. 脉冲熔融-飞行时间质谱法分析痕量气体成分的校准方法研究%Research on the calibration method of pulse heating and time-of-flight mass spectrometric determination of trace gases

    Institute of Scientific and Technical Information of China (English)

    杨植岗; 王学华; 胡少成; 徐井然; 吴振宁; 沈学静; 王蓬

    2012-01-01

    Standard gas calibration equipment for the simultaneous determination of O, N, H and Ar was built by combining the gas circuit of pulse heating and time-of-flight mass spectrometer gas analyzer with the six-port injection valve which was normally used in chromatogram. Two processes of purging of quantitative tube and injecting of standard gas can be converted smoothly. Using the equipment, calibration curves of low content O, N, H and Ar were established, and the stability was tested. Samples were analyzed by these calibration curves, and the results matched with the certified values. From the results, it was showed that the problem of Ar reference materials in ultra low content range can be solved by this equipment, and Ar can be analyzed quantitatively. The established calibrating curve by standard gas calibration setup can be used for metal materials analyzing, and good linearization of the calibrating curve can be got.%本文采用色谱用六通阀,结合脉冲熔融-飞行时间质谱元素分析仪的气路流程,自制了应用于氧、氮、氢、氩联测的标气校准装置.实现了定量管冲洗和标气注入两个过程的灵活控制.通过该校准装置,建立了金属材料中的低含量氧、氮、氢和氩工作曲线,验证了校准装置分析的稳定性.采用建立的工作曲线对实际样品进行了分析,结果与认定值一致.标气校准装置的使用弥补了超低含量范围段标准样品缺乏的不足,解决了测氩用标准样品缺失的难题.实验结果表明,应用标气校准装置建立的工作曲线,线性良好,可用于金属材料实际样品的分析.

  2. Computerized Techniques for Calibrating Pressure Balances

    Science.gov (United States)

    Simpson, D. I.

    1994-01-01

    Pressure balances are generally calibrated by the cross-floating technique, where the forces acting on two similar devices in hydrostatic equilibrium are compared. It is a skilled and time-consuming process which has not previously lent itself to significant automation; computers have mostly been used only to calculate results after measurements have been taken. The objective of the present work was to develop real-time computerized measurement techniques to ease the calibration task, which would fully integrate into a single package with versatile software for calculating and displaying results. The calibration process is now conducted by studying graphical computer displays which derive their inputs from differential-pressure transducers and capacitance or optical displacement sensors. The mass imbalance between oil-operated pressure balances is calculated by interpolating between changes in piston rate-of-fall. Differential-pressure transducers are used to estimate mass imbalances between gas-operated balances, and a quick in situ method for determining their sensitivity has been developed. The new techniques have been successfully applied to a variety of pressure balance designs and substantial reductions in calibration times have been achieved. Reduced levels of scatter have revealed small systematic differences between gauge and absolute modes of operation.

  3. Entropic calibration revisited

    Energy Technology Data Exchange (ETDEWEB)

    Brody, Dorje C. [Blackett Laboratory, Imperial College, London SW7 2BZ (United Kingdom)]. E-mail: d.brody@imperial.ac.uk; Buckley, Ian R.C. [Centre for Quantitative Finance, Imperial College, London SW7 2AZ (United Kingdom); Constantinou, Irene C. [Blackett Laboratory, Imperial College, London SW7 2BZ (United Kingdom); Meister, Bernhard K. [Blackett Laboratory, Imperial College, London SW7 2BZ (United Kingdom)

    2005-04-11

    The entropic calibration of the risk-neutral density function is effective in recovering the strike dependence of options, but encounters difficulties in determining the relevant greeks. By use of put-call reversal we apply the entropic method to the time reversed economy, which allows us to obtain the spot price dependence of options and the relevant greeks.

  4. LOFAR Facet Calibration

    Science.gov (United States)

    van Weeren, R. J.; Williams, W. L.; Hardcastle, M. J.; Shimwell, T. W.; Rafferty, D. A.; Sabater, J.; Heald, G.; Sridhar, S. S.; Dijkema, T. J.; Brunetti, G.; Brüggen, M.; Andrade-Santos, F.; Ogrean, G. A.; Röttgering, H. J. A.; Dawson, W. A.; Forman, W. R.; de Gasperin, F.; Jones, C.; Miley, G. K.; Rudnick, L.; Sarazin, C. L.; Bonafede, A.; Best, P. N.; Bîrzan, L.; Cassano, R.; Chyży, K. T.; Croston, J. H.; Ensslin, T.; Ferrari, C.; Hoeft, M.; Horellou, C.; Jarvis, M. J.; Kraft, R. P.; Mevius, M.; Intema, H. T.; Murray, S. S.; Orrú, E.; Pizzo, R.; Simionescu, A.; Stroe, A.; van der Tol, S.; White, G. J.

    2016-03-01

    LOFAR, the Low-Frequency Array, is a powerful new radio telescope operating between 10 and 240 MHz. LOFAR allows detailed sensitive high-resolution studies of the low-frequency radio sky. At the same time LOFAR also provides excellent short baseline coverage to map diffuse extended emission. However, producing high-quality deep images is challenging due to the presence of direction-dependent calibration errors, caused by imperfect knowledge of the station beam shapes and the ionosphere. Furthermore, the large data volume and presence of station clock errors present additional difficulties. In this paper we present a new calibration scheme, which we name facet calibration, to obtain deep high-resolution LOFAR High Band Antenna images using the Dutch part of the array. This scheme solves and corrects the direction-dependent errors in a number of facets that cover the observed field of view. Facet calibration provides close to thermal noise limited images for a typical 8 hr observing run at ∼ 5\\prime\\prime resolution, meeting the specifications of the LOFAR Tier-1 northern survey.

  5. LOFAR facet calibration

    CERN Document Server

    van Weeren, R J; Hardcastle, M J; Shimwell, T W; Rafferty, D A; Sabater, J; Heald, G; Sridhar, S S; Dijkema, T J; Brunetti, G; Brüggen, M; Andrade-Santos, F; Ogrean, G A; Röttgering, H J A; Dawson, W A; Forman, W R; de Gasperin, F; Jones, C; Miley, G K; Rudnick, L; Sarazin, C L; Bonafede, A; Best, P N; Bîrzan, L; Cassano, R; Chyży, K T; Croston, J H; Ensslin, T; Ferrari, C; Hoeft, M; Horellou, C; Jarvis, M J; Kraft, R P; Mevius, M; Intema, H T; Murray, S S; Orrú, E; Pizzo, R; Simionescu, A; Stroe, A; van der Tol, S; White, G J

    2016-01-01

    LOFAR, the Low-Frequency Array, is a powerful new radio telescope operating between 10 and 240 MHz. LOFAR allows detailed sensitive high-resolution studies of the low-frequency radio sky. At the same time LOFAR also provides excellent short baseline coverage to map diffuse extended emission. However, producing high-quality deep images is challenging due to the presence of direction dependent calibration errors, caused by imperfect knowledge of the station beam shapes and the ionosphere. Furthermore, the large data volume and presence of station clock errors present additional difficulties. In this paper we present a new calibration scheme, which we name facet calibration, to obtain deep high-resolution LOFAR High Band Antenna images using the Dutch part of the array. This scheme solves and corrects the direction dependent errors in a number of facets that cover the observed field of view. Facet calibration provides close to thermal noise limited images for a typical 8 hr observing run at $\\sim$ 5arcsec resolu...

  6. Calibration of farmer dosemeters

    International Nuclear Information System (INIS)

    The Farmer Dosemeters of Atomic Energy Medical Centre (AEMC) Jamshoro were calibrated in the Secondary Standard Dosimetry Laboratory (SSDL) at PINSTECH, using the NPL Secondary Standard Therapy level X-ray exposure meter. The results are presented in this report. (authors)

  7. Calibration Of Oxygen Monitors

    Science.gov (United States)

    Zalenski, M. A.; Rowe, E. L.; Mcphee, J. R.

    1988-01-01

    Readings corrected for temperature, pressure, and humidity of air. Program for handheld computer developed to ensure accuracy of oxygen monitors in National Transonic Facility, where liquid nitrogen stored. Calibration values, determined daily, based on entries of data on barometric pressure, temperature, and relative humidity. Output provided directly in millivolts.

  8. Commodity-Free Calibration

    Science.gov (United States)

    2008-01-01

    Commodity-free calibration is a reaction rate calibration technique that does not require the addition of any commodities. This technique is a specific form of the reaction rate technique, where all of the necessary reactants, other than the sample being analyzed, are either inherent in the analyzing system or specifically added or provided to the system for a reason other than calibration. After introduction, the component of interest is exposed to other reactants or flow paths already present in the system. The instrument detector records one of the following to determine the rate of reaction: the increase in the response of the reaction product, a decrease in the signal of the analyte response, or a decrease in the signal from the inherent reactant. With this data, the initial concentration of the analyte is calculated. This type of system can analyze and calibrate simultaneously, reduce the risk of false positives and exposure to toxic vapors, and improve accuracy. Moreover, having an excess of the reactant already present in the system eliminates the need to add commodities, which further reduces cost, logistic problems, and potential contamination. Also, the calculations involved can be simplified by comparison to those of the reaction rate technique. We conducted tests with hypergols as an initial investigation into the feasiblility of the technique.

  9. Measurement System & Calibration report

    DEFF Research Database (Denmark)

    Kock, Carsten Weber; Vesth, Allan

    This Measurement System & Calibration report is describing DTU’s measurement system installed at a specific wind turbine. A major part of the sensors has been installed by others (see [1]) the rest of the sensors have been installed by DTU. The results of the measurements, described in this report...

  10. Calibration with Absolute Shrinkage

    DEFF Research Database (Denmark)

    Øjelund, Henrik; Madsen, Henrik; Thyregod, Poul

    2001-01-01

    In this paper, penalized regression using the L-1 norm on the estimated parameters is proposed for chemometric je calibration. The algorithm is of the lasso type, introduced by Tibshirani in 1996 as a linear regression method with bound on the absolute length of the parameters, but a modification...

  11. NVLAP calibration laboratory program

    Energy Technology Data Exchange (ETDEWEB)

    Cigler, J.L.

    1993-12-31

    This paper presents an overview of the progress up to April 1993 in the development of the Calibration Laboratories Accreditation Program within the framework of the National Voluntary Laboratory Accreditation Program (NVLAP) at the National Institute of Standards and Technology (NIST).

  12. Pleiades Absolute Calibration : Inflight Calibration Sites and Methodology

    Science.gov (United States)

    Lachérade, S.; Fourest, S.; Gamet, P.; Lebègue, L.

    2012-07-01

    In-flight calibration of space sensors once in orbit is a decisive step to be able to fulfil the mission objectives. This article presents the methods of the in-flight absolute calibration processed during the commissioning phase. Four In-flight calibration methods are used: absolute calibration, cross-calibration with reference sensors such as PARASOL or MERIS, multi-temporal monitoring and inter-bands calibration. These algorithms are based on acquisitions over natural targets such as African deserts, Antarctic sites, La Crau (Automatic calibration station) and Oceans (Calibration over molecular scattering) or also new extra-terrestrial sites such as the Moon and selected stars. After an overview of the instrument and a description of the calibration sites, it is pointed out how each method is able to address one or several aspects of the calibration. We focus on how these methods complete each other in their operational use, and how they help building a coherent set of information that addresses all aspects of in-orbit calibration. Finally, we present the perspectives that the high level of agility of PLEIADES offers for the improvement of its calibration and a better characterization of the calibration sites.

  13. Field calibration of cup anemometers

    DEFF Research Database (Denmark)

    Schmidt Paulsen, Uwe; Mortensen, Niels Gylling; Hansen, Jens Carsten;

    2007-01-01

    A field calibration method and results are described along with the experience gained with the method. The cup anemometers to be calibrated are mounted in a row on a 10-m high rig and calibrated in the free wind against a reference cup anemometer. The method has been reported [1] to improve the...... statistical bias on the data relative to calibrations carried out in a wind tunnel. The methodology is sufficiently accurate for calibration of cup anemometers used for wind resource assessments and provides a simple, reliable and cost-effective solution to cup anemometer calibration, especially suited for...

  14. Polarimetric calibration of large mirrors

    CERN Document Server

    Ariste, A Lopez

    2015-01-01

    Aims: To propose a method for the polarimetric calibration of large astronomical mirrors that does not require use of special optical devices nor knowledge of the exact polarization properties of the calibration target. Methods: We study the symmetries of the Mueller matrix of mirrors to exploit them for polarimetric calibration under the assumptions that only the orientation of the linear polarization plane of the calibration target is known with certainty. Results: A method is proposed to calibrate the polarization effects of single astronomical mirrors by the observation of calibration targets with known orientation of the linear polarization. We study the uncertainties of the method and the signal-to-noise ratios required for an acceptable calibration. We list astronomical targets ready for the method. We finally extend the method to the calibration of two or more mirrors, in particular to the case when they share the same incidence plane.

  15. The Calibration Reference Data System

    Science.gov (United States)

    Greenfield, P.; Miller, T.

    2016-07-01

    We describe a software architecture and implementation for using rules to determine which calibration files are appropriate for calibrating a given observation. This new system, the Calibration Reference Data System (CRDS), replaces what had been previously used for the Hubble Space Telescope (HST) calibration pipelines, the Calibration Database System (CDBS). CRDS will be used for the James Webb Space Telescope (JWST) calibration pipelines, and is currently being used for HST calibration pipelines. CRDS can be easily generalized for use in similar applications that need a rules-based system for selecting the appropriate item for a given dataset; we give some examples of such generalizations that will likely be used for JWST. The core functionality of the Calibration Reference Data System is available under an Open Source license. CRDS is briefly contrasted with a sampling of other similar systems used at other observatories.

  16. Lidar calibration experiments

    DEFF Research Database (Denmark)

    Ejsing Jørgensen, Hans; Mikkelsen, T.; Streicher, J.;

    1997-01-01

    A series of atmospheric aerosol diffusion experiments combined with lidar detection was conducted to evaluate and calibrate an existing retrieval algorithm for aerosol backscatter lidar systems. The calibration experiments made use of two (almost) identical mini-lidar systems for aerosol cloud...... detection to test the reproducibility and uncertainty of lidars. Lidar data were obtained from both single-ended and double-ended Lidar configurations. A backstop was introduced in one of the experiments and a new method was developed where information obtained from the backstop can be used in the inversion...... algorithm. Independent in-situ aerosol plume concentrations were obtained from a simultaneous tracer gas experiment with SF6, and comparisons with the two lidars were made. The study shows that the reproducibility of the lidars is within 15%, including measurements from both sides of a plume...

  17. Optical tweezers absolute calibration

    CERN Document Server

    Dutra, R S; Neto, P A Maia; Nussenzveig, H M

    2014-01-01

    Optical tweezers are highly versatile laser traps for neutral microparticles, with fundamental applications in physics and in single molecule cell biology. Force measurements are performed by converting the stiffness response to displacement of trapped transparent microspheres, employed as force transducers. Usually, calibration is indirect, by comparison with fluid drag forces. This can lead to discrepancies by sizable factors. Progress achieved in a program aiming at absolute calibration, conducted over the past fifteen years, is briefly reviewed. Here we overcome its last major obstacle, a theoretical overestimation of the peak stiffness, within the most employed range for applications, and we perform experimental validation. The discrepancy is traced to the effect of primary aberrations of the optical system, which are now included in the theory. All required experimental parameters are readily accessible. Astigmatism, the dominant effect, is measured by analyzing reflected images of the focused laser spo...

  18. Astrid-2 SSC ASUMagnetic Calibration

    DEFF Research Database (Denmark)

    Primdahl, Fritz

    1997-01-01

    Report of the inter calibration between the starcamera and the fluxgate magnetometer onboard the ASTRID-2 satellite. This calibration was performed in the night between the 15. and 16. May 1997 at the Lovö magnetic observatory.......Report of the inter calibration between the starcamera and the fluxgate magnetometer onboard the ASTRID-2 satellite. This calibration was performed in the night between the 15. and 16. May 1997 at the Lovö magnetic observatory....

  19. Program Calibrates Strain Gauges

    Science.gov (United States)

    Okazaki, Gary D.

    1991-01-01

    Program dramatically reduces personnel and time requirements for acceptance tests of hardware. Data-acquisition system reads output from Wheatstone full-bridge strain-gauge circuit and calculates strain by use of shunt calibration technique. Program nearly instantaneously tabulates and plots strain data against load-cell outputs. Modified to acquire strain data for other specimens wherever full-bridge strain-gauge circuits used. Written in HP BASIC.

  20. Mesoscale hybrid calibration artifact

    Science.gov (United States)

    Tran, Hy D.; Claudet, Andre A.; Oliver, Andrew D.

    2010-09-07

    A mesoscale calibration artifact, also called a hybrid artifact, suitable for hybrid dimensional measurement and the method for make the artifact. The hybrid artifact has structural characteristics that make it suitable for dimensional measurement in both vision-based systems and touch-probe-based systems. The hybrid artifact employs the intersection of bulk-micromachined planes to fabricate edges that are sharp to the nanometer level and intersecting planes with crystal-lattice-defined angles.

  1. Quantitative WD-XRF calibration for small ceramic samples and their source material

    OpenAIRE

    De Vleeschouwer, François; Renson, Virginie; Claeys, Philippe; Nys, Karin; Bindler, Richard

    2011-01-01

    International audience A wavelength-dispersive X-ray fluorescence (WD-XRF) calibration is developed for small powdered samples (300mg) with the purpose of analyzing ceramic artifacts that might be available only in limited quantity. This is compared to a conventional calibration using a larger sample mass (2g). The comparison of elemental intensities obtained in both calibrations shows that the decrease in analyzed sample mass results in a linear decrease in measured intensity for the anal...

  2. Dosimetry and Calibration Section

    International Nuclear Information System (INIS)

    The two tasks of the Dosimetry and Calibration Section at CERN are the Individual Dosimetry Service which assures the personal monitoring of about 5000 persons potentially exposed to ionizing radiation at CERN, and the Calibration Laboratory which verifies all the instruments and monitors. This equipment is used by the sections of the RP Group for assuring radiation protection around CERN's accelerators, and by the Environmental Section of TISTE. In addition, nearly 250 electronic and 300 quartz fibre dosimeters, employed in operational dosimetry, are calibrated at least once a year. The Individual Dosimetry Service uses an extended database (INDOS) which contains information about all the individual doses ever received at CERN. For most of 1997 it was operated without the support of a database administrator as the technician who had assured this work retired. The Software Support Section of TIS-TE took over the technical responsibility of the database, but in view of the many other tasks of this Section and the lack of personnel, only a few interventions for solving immediate problems were possible

  3. Calibration of Underwater Sound Transducers

    Directory of Open Access Journals (Sweden)

    H.R.S. Sastry

    1983-07-01

    Full Text Available The techniques of calibration of underwater sound transducers for farfield, near-field and closed environment conditions are reviewed in this paper .The design of acoustic calibration tank is mentioned. The facilities available at Naval Physical & Oceanographic Laboratory, Cochin for calibration of transducers are also listed.

  4. A detector interferometric calibration experiment for high precision astrometry

    CERN Document Server

    Crouzier, A; Henault, F; Leger, A; Cara, C; LeDuigou, J M; Preis, O; Kern, P; Delboulbe, A; Martin, G; Feautrier, P; Stadler, E; Lafrasse, S; Rochat, S; Ketchazo, C; Donati, M; Doumayrou, E; Lagage, P O; Shao, M; Goullioud, R; Nemati, B; Zhai, C; Behar, E; Potin, S; Saint-Pe, M; Dupont, J

    2016-01-01

    Context: Exoplanet science has made staggering progress in the last two decades, due to the relentless exploration of new detection methods and refinement of existing ones. Yet astrometry offers a unique and untapped potential of discovery of habitable-zone low-mass planets around all the solar-like stars of the solar neighborhood. To fulfill this goal, astrometry must be paired with high precision calibration of the detector. Aims: We present a way to calibrate a detector for high accuracy astrometry. An experimental testbed combining an astrometric simulator and an interferometric calibration system is used to validate both the hardware needed for the calibration and the signal processing methods. The objective is an accuracy of 5e-6 pixel on the location of a Nyquist sampled polychromatic point spread function. Methods: The interferometric calibration system produced modulated Young fringes on the detector. The Young fringes were parametrized as products of time and space dependent functions, based on vari...

  5. Calibration effects on orbit determination

    Science.gov (United States)

    Madrid, G. A.; Winn, F. B.; Zielenbach, J. W.; Yip, K. B.

    1974-01-01

    The effects of charged particle and tropospheric calibrations on the orbit determination (OD) process are analyzed. The calibration process consisted of correcting the Doppler observables for the media effects. Calibrated and uncalibrated Doppler data sets were used to obtain OD results for past missions as well as Mariner Mars 1971. Comparisons of these Doppler reductions show the significance of the calibrations. For the MM'71 mission, the media calibrations proved themselves effective in diminishing the overall B-plane error and reducing the Doppler residual signatures.

  6. Ground calibrations of Nuclear Compton Telescope

    Science.gov (United States)

    Chiu, Jeng-Lun; Liu, Zhong-Kai; Bandstra, Mark S.; Bellm, Eric C.; Liang, Jau-Shian; Perez-Becker, Daniel; Zoglauer, Andreas; Boggs, Steven E.; Chang, Hsiang-Kuang; Chang, Yuan-Hann; Huang, Minghuey A.; Amman, Mark; Chiang, Shiuan-Juang; Hung, Wei-Che; Lin, Chih-Hsun; Luke, Paul N.; Run, Ray-Shine; Wunderer, Cornelia B.

    2010-07-01

    The Nuclear Compton Telescope (NCT) is a balloon-borne soft gamma ray (0.2-10 MeV) telescope designed to study astrophysical sources of nuclear line emission and polarization. The heart of NCT is an array of 12 cross-strip germanium detectors, designed to provide 3D positions for each photon interaction with full 3D position resolution to imaging, effectively reduces background, and enables the measurement of polarization. The keys to Compton imaging with NCT's detectors are determining the energy deposited in the detector at each strip and tracking the gamma-ray photon interaction within the detector. The 3D positions are provided by the orthogonal X and Y strips, and by determining the interaction depth using the charge collection time difference (CTD) between the anode and cathode. Calibrations of the energy as well as the 3D position of interactions have been completed, and extensive calibration campaigns for the whole system were also conducted using radioactive sources prior to our flights from Ft. Sumner, New Mexico, USA in Spring 2009, and from Alice Springs, Australia in Spring 2010. Here we will present the techniques and results of our ground calibrations so far, and then compare the calibration results of the effective area throughout NCT's field of view with Monte Carlo simulations using a detailed mass model.

  7. Calibrating Gyrochronology using Kepler Asteroseismic targets

    CERN Document Server

    Angus, Ruth; Foreman-Mackey, Daniel; McQuillan, Amy

    2015-01-01

    Among the available methods for dating stars, gyrochronology is a powerful one because it requires knowledge of only the star's mass and rotation period. Gyrochronology relations have previously been calibrated using young clusters, with the Sun providing the only age dependence, and are therefore poorly calibrated at late ages. We used rotation period measurements of 310 Kepler stars with asteroseismic ages, 50 stars from the Hyades and Coma Berenices clusters and 6 field stars (including the Sun) with precise age measurements to calibrate the gyrochronology relation, whilst fully accounting for measurement uncertainties in all observable quantities. We calibrated a relation of the form $P=A^n\\times(B-V-c)^b$, where $P$ is rotation period in days, $A$ is age in Myr, $B$ and $V$ are magnitudes and $a$, $b$ and $n$ are the free parameters of our model. We found $a = 0.40^{+0.3}_{-0.05}$, $b = 0.31^{+0.05}_{-0.02}$ and $n = 0.55^{+0.02}_{-0.09}$. Markov Chain Monte Carlo methods were used to explore the posteri...

  8. A variable acceleration calibration system

    Science.gov (United States)

    Johnson, Thomas H.

    2011-12-01

    A variable acceleration calibration system that applies loads using gravitational and centripetal acceleration serves as an alternative, efficient and cost effective method for calibrating internal wind tunnel force balances. Two proof-of-concept variable acceleration calibration systems are designed, fabricated and tested. The NASA UT-36 force balance served as the test balance for the calibration experiments. The variable acceleration calibration systems are shown to be capable of performing three component calibration experiments with an approximate applied load error on the order of 1% of the full scale calibration loads. Sources of error are indentified using experimental design methods and a propagation of uncertainty analysis. Three types of uncertainty are indentified for the systems and are attributed to prediction error, calibration error and pure error. Angular velocity uncertainty is shown to be the largest indentified source of prediction error. The calibration uncertainties using a production variable acceleration based system are shown to be potentially equivalent to current methods. The production quality system can be realized using lighter materials and a more precise instrumentation. Further research is needed to account for balance deflection, forcing effects due to vibration, and large tare loads. A gyroscope measurement technique is shown to be capable of resolving the balance deflection angle calculation. Long term research objectives include a demonstration of a six degree of freedom calibration, and a large capacity balance calibration.

  9. SAR antenna calibration techniques

    Science.gov (United States)

    Carver, K. R.; Newell, A. C.

    1978-01-01

    Calibration of SAR antennas requires a measurement of gain, elevation and azimuth pattern shape, boresight error, cross-polarization levels, and phase vs. angle and frequency. For spaceborne SAR antennas of SEASAT size operating at C-band or higher, some of these measurements can become extremely difficult using conventional far-field antenna test ranges. Near-field scanning techniques offer an alternative approach and for C-band or X-band SARs, give much improved accuracy and precision as compared to that obtainable with a far-field approach.

  10. Use of Radiometrically Calibrated Flat-Plate Calibrators in Calibration of Radiation Thermometers

    Science.gov (United States)

    Cárdenas-García, D.; Méndez-Lango, E.

    2015-08-01

    Most commonly used, low-temperature, infrared thermometers have large fields of view sizes that make them difficult to be calibrated with narrow aperture blackbodies. Flat-plate calibrators with large emitting surfaces have been proposed for calibrating these infrared thermometers. Because the emissivity of the flat plate is not unity, its radiance temperature is wavelength dependent. For calibration, the wavelength pass band of the device under test should match that of the reference infrared thermometer. If the device under test and reference radiometer have different pass bands, then it is possible to calculate the corresponding correction if the emissivity of the flat plate is known. For example, a correction of at is required when calibrating a infrared thermometer with a "" radiometrically calibrated flat-plate calibrator. A method is described for using a radiometrically calibrated flat-plate calibrator that covers both cases of match and mismatch working wavelength ranges of a reference infrared thermometer and infrared thermometers to be calibrated with the flat-plate calibrator. Also, an application example is included in this paper.

  11. A Simple Accelerometer Calibrator

    Science.gov (United States)

    Salam, R. A.; Islamy, M. R. F.; Munir, M. M.; Latief, H.; Irsyam, M.; Khairurrijal

    2016-08-01

    High possibility of earthquake could lead to the high number of victims caused by it. It also can cause other hazards such as tsunami, landslide, etc. In that case it requires a system that can examine the earthquake occurrence. Some possible system to detect earthquake is by creating a vibration sensor system using accelerometer. However, the output of the system is usually put in the form of acceleration data. Therefore, a calibrator system for accelerometer to sense the vibration is needed. In this study, a simple accelerometer calibrator has been developed using 12 V DC motor, optocoupler, Liquid Crystal Display (LCD) and AVR 328 microcontroller as controller system. The system uses the Pulse Wave Modulation (PWM) form microcontroller to control the motor rotational speed as response to vibration frequency. The frequency of vibration was read by optocoupler and then those data was used as feedback to the system. The results show that the systems could control the rotational speed and the vibration frequencies in accordance with the defined PWM.

  12. On chromatic and geometrical calibration

    DEFF Research Database (Denmark)

    Folm-Hansen, Jørgen

    1999-01-01

    we present the implementation of a complete calibration method for an accurate colour texture measurement device called VMX2000, the calibration for uneven laser sheet illumination in a flow measuring system and the use of automatic detection of calibration targets for a DLT/warping in a 3D PIV......The main subject of the present thesis is different methods for the geometrical and chromatic calibration of cameras in various environments. For the monochromatic issues of the calibration we present the acquisition of monochrome images, the classic monochrome aberrations and the various sources...... of non-uniformity of the illumination of the image plane. Only the image deforming aberrations and the non-uniformity of illumination are included in the calibration models. The topics of the pinhole camera model and the extension to the Direct Linear Transform (DLT) are described. It is shown how...

  13. Calibration procedure for zenith plummets

    Directory of Open Access Journals (Sweden)

    Jelena GUČEVIĆ

    2013-09-01

    Full Text Available Zenith plummets are used mainly in applied geodesy, in civil engineering surveying, for materialization of the local vertical. The error of the vertical deflection of the instrument is directly transferred to the error of the observing construction. That is why a proper calibration procedure for the zenithlot is required. Metrological laboratory of the Faculty of Civil Engineering in Belgrade developed such calibration procedure. Here we present a mathematical model of the calibration and some selected results.

  14. Calibration procedure for zenith plummets

    OpenAIRE

    Jelena GUČEVIĆ; Delčev, Siniša; Vukan OGRIZOVIĆ

    2013-01-01

    Zenith plummets are used mainly in applied geodesy, in civil engineering surveying, for materialization of the local vertical. The error of the vertical deflection of the instrument is directly transferred to the error of the observing construction. That is why a proper calibration procedure for the zenithlot is required. Metrological laboratory of the Faculty of Civil Engineering in Belgrade developed such calibration procedure. Here we present a mathematical model of the calibration and som...

  15. Calibration of neutron albedo dosemeters.

    Science.gov (United States)

    Schwartz, R B; Eisenhauer, C M

    2002-01-01

    It is shown that by calibrating neutron albedo dosemeters under the proper conditions, two complicating effects will essentially cancel out, allowing accurate calibrations with no need for explicit corrections. The 'proper conditions' are: a large room (> or = 8 m on a side). use of a D2O moderated 252Cf source, and a source-to-phantom calibration distance of approximately 70 cm. PMID:12212898

  16. Radiological Calibration and Standards Facility

    Data.gov (United States)

    Federal Laboratory Consortium — PNNL maintains a state-of-the-art Radiological Calibration and Standards Laboratory on the Hanford Site at Richland, Washington. Laboratory staff provide expertise...

  17. Calibration Techniques for VERITAS

    CERN Document Server

    Hanna, David

    2007-01-01

    VERITAS is an array of four identical telescopes designed for detecting and measuring astrophysical gamma rays with energies in excess of 100 GeV. Each telescope uses a 12 m diameter reflector to collect Cherenkov light from air showers initiated by incident gamma rays and direct it onto a `camera' comprising 499 photomultiplier tubes read out by flash ADCs. We describe here calibration methods used for determining the values of the parameters which are necessary for converting the digitized PMT pulses to gamma-ray energies and directions. Use of laser pulses to determine and monitor PMT gains is discussed, as are measurements of the absolute throughput of the telescopes using muon rings.

  18. RX130 Robot Calibration

    Science.gov (United States)

    Fugal, Mario

    2012-10-01

    In order to create precision magnets for an experiment at Oak Ridge National Laboratory, a new reverse engineering method has been proposed that uses the magnetic scalar potential to solve for the currents necessary to produce the desired field. To make the magnet it is proposed to use a copper coated G10 form, upon which a drill, mounted on a robotic arm, will carve wires. The accuracy required in the manufacturing of the wires exceeds nominal robot capabilities. However, due to the rigidity as well as the precision servo motor and harmonic gear drivers, there are robots capable of meeting this requirement with proper calibration. Improving the accuracy of an RX130 to be within 35 microns (the accuracy necessary of the wires) is the goal of this project. Using feedback from a displacement sensor, or camera and inverse kinematics it is possible to achieve this accuracy.

  19. TOD to TTP calibration

    Science.gov (United States)

    Bijl, Piet; Reynolds, Joseph P.; Vos, Wouter K.; Hogervorst, Maarten A.; Fanning, Jonathan D.

    2011-05-01

    The TTP (Targeting Task Performance) metric, developed at NVESD, is the current standard US Army model to predict EO/IR Target Acquisition performance. This model however does not have a corresponding lab or field test to empirically assess the performance of a camera system. The TOD (Triangle Orientation Discrimination) method, developed at TNO in The Netherlands, provides such a measurement. In this study, we make a direct comparison between TOD performance for a range of sensors and the extensive historical US observer performance database built to develop and calibrate the TTP metric. The US perception data were collected doing an identification task by military personnel on a standard 12 target, 12 aspect tactical vehicle image set that was processed through simulated sensors for which the most fundamental sensor parameters such as blur, sampling, spatial and temporal noise were varied. In the present study, we measured TOD sensor performance using exactly the same sensors processing a set of TOD triangle test patterns. The study shows that good overall agreement is obtained when the ratio between target characteristic size and TOD test pattern size at threshold equals 6.3. Note that this number is purely based on empirical data without any intermediate modeling. The calibration of the TOD to the TTP is highly beneficial to the sensor modeling and testing community for a variety of reasons. These include: i) a connection between requirement specification and acceptance testing, and ii) a very efficient method to quickly validate or extend the TTP range prediction model to new systems and tasks.

  20. Calibration of Nanopositioning Stages

    Directory of Open Access Journals (Sweden)

    Ning Tan

    2015-12-01

    Full Text Available Accuracy is one of the most important criteria for the performance evaluation of micro- and nanorobots or systems. Nanopositioning stages are used to achieve the high positioning resolution and accuracy for a wide and growing scope of applications. However, their positioning accuracy and repeatability are not well known and difficult to guarantee, which induces many drawbacks for many applications. For example, in the mechanical characterisation of biological samples, it is difficult to perform several cycles in a repeatable way so as not to induce negative influences on the study. It also prevents one from controlling accurately a tool with respect to a sample without adding additional sensors for closed loop control. This paper aims at quantifying the positioning repeatability and accuracy based on the ISO 9283:1998 standard, and analyzing factors influencing positioning accuracy onto a case study of 1-DoF (Degree-of-Freedom nanopositioning stage. The influence of thermal drift is notably quantified. Performances improvement of the nanopositioning stage are then investigated through robot calibration (i.e., open-loop approach. Two models (static and adaptive models are proposed to compensate for both geometric errors and thermal drift. Validation experiments are conducted over a long period (several days showing that the accuracy of the stage is improved from typical micrometer range to 400 nm using the static model and even down to 100 nm using the adaptive model. In addition, we extend the 1-DoF calibration to multi-DoF with a case study of a 2-DoF nanopositioning robot. Results demonstrate that the model efficiently improved the 2D accuracy from 1400 nm to 200 nm.

  1. Self Calibrating Interferometric Sensor

    DEFF Research Database (Denmark)

    Sørensen, Henrik Schiøtt

    This thesis deals with the development of an optical sensor based on micro interferometric backscatter detection (MIBD). A price effective, highly sensitive and ready for mass production platform is the goal of this project. The thesis covers three areas. The first part of the thesis deals...... mask. The fabricated micro structures have been electroplated for later injection molding, showing the potential of the MIBD sensor to be mass produced with high reproducibility and sensitivity. In part three MIBD experiments on vital biological systems are described. Label–free binding studies of bio...

  2. Photometric Calibration of Consumer Video Cameras

    Science.gov (United States)

    Suggs, Robert; Swift, Wesley, Jr.

    2007-01-01

    Equipment and techniques have been developed to implement a method of photometric calibration of consumer video cameras for imaging of objects that are sufficiently narrow or sufficiently distant to be optically equivalent to point or line sources. Heretofore, it has been difficult to calibrate consumer video cameras, especially in cases of image saturation, because they exhibit nonlinear responses with dynamic ranges much smaller than those of scientific-grade video cameras. The present method not only takes this difficulty in stride but also makes it possible to extend effective dynamic ranges to several powers of ten beyond saturation levels. The method will likely be primarily useful in astronomical photometry. There are also potential commercial applications in medical and industrial imaging of point or line sources in the presence of saturation.This development was prompted by the need to measure brightnesses of debris in amateur video images of the breakup of the Space Shuttle Columbia. The purpose of these measurements is to use the brightness values to estimate relative masses of debris objects. In most of the images, the brightness of the main body of Columbia was found to exceed the dynamic ranges of the cameras. A similar problem arose a few years ago in the analysis of video images of Leonid meteors. The present method is a refined version of the calibration method developed to solve the Leonid calibration problem. In this method, one performs an endto- end calibration of the entire imaging system, including not only the imaging optics and imaging photodetector array but also analog tape recording and playback equipment (if used) and any frame grabber or other analog-to-digital converter (if used). To automatically incorporate the effects of nonlinearity and any other distortions into the calibration, the calibration images are processed in precisely the same manner as are the images of meteors, space-shuttle debris, or other objects that one seeks to

  3. Calibration of Correlation Radiometers Using Pseudo-Random Noise Signals

    Directory of Open Access Journals (Sweden)

    Sebastián Pantoja

    2009-08-01

    Full Text Available The calibration of correlation radiometers, and particularly aperture synthesis interferometric radiometers, is a critical issue to ensure their performance. Current calibration techniques are based on the measurement of the cross-correlation of receivers’ outputs when injecting noise from a common noise source requiring a very stable distribution network. For large interferometric radiometers this centralized noise injection approach is very complex from the point of view of mass, volume and phase/amplitude equalization. Distributed noise injection techniques have been proposed as a feasible alternative, but are unable to correct for the so-called “baseline errors” associated with the particular pair of receivers forming the baseline. In this work it is proposed the use of centralized Pseudo-Random Noise (PRN signals to calibrate correlation radiometers. PRNs are sequences of symbols with a long repetition period that have a flat spectrum over a bandwidth which is determined by the symbol rate. Since their spectrum resembles that of thermal noise, they can be used to calibrate correlation radiometers. At the same time, since these sequences are deterministic, new calibration schemes can be envisaged, such as the correlation of each receiver’s output with a baseband local replica of the PRN sequence, as well as new distribution schemes of calibration signals. This work analyzes the general requirements and performance of using PRN sequences for the calibration of microwave correlation radiometers, and particularizes the study to a potential implementation in a large aperture synthesis radiometer using an optical distribution network.

  4. Calibration of the CREAM-I calorimeter

    CERN Document Server

    Yoon, Y S; Bagliesi, M G; Bigongiari, G; Ganel, O; Han, J H; Jeon, J A; Kim, K C; Lee, M H; Lutz, L; Maestro, P; Malinin, A; Marrocchesi, P S; Nam, S; Park, I H; Park, N H; Seo, E S; Sina, R; Wu, J; Yang, J; Zei, R; Zinn, S Y

    2010-01-01

    The Cosmic Ray Energetics And Mass (CREAM) calorimeter is designed to measure the spectra of cosmic-ray particles over the energy range from ~10^11 eV to ~10^15 eV. Its first flight as part of the CREAM-I balloon-borne payload in Antarctica during the 2004/05 season resulted in a recordbreaking 42 days of exposure. Calorimeter calibration using various beam test data will be discussed in an attempt to assess the uncertainties of the energy measurements.

  5. Traceable dynamic calibration of force transducers by primary means

    Science.gov (United States)

    Vlajic, Nicholas; Chijioke, Ako

    2016-08-01

    We describe an apparatus for traceable, dynamic calibration of force transducers using harmonic excitation, and report calibration measurements of force transducers using this apparatus. In this system, the force applied to the transducer is produced by the acceleration of an attached mass, and is determined according to Newton’s second law, F  =  ma. The acceleration is measured by primary means, using laser interferometry. The capabilities of this system are demonstrated by performing dynamic calibrations of two shear-web-type force transducers up to a frequency of 2 kHz, with an expanded uncertainty below 1.2%. We give an account of all significant sources of uncertainty, including a detailed consideration of the effects of dynamic tilting (rocking), which is a leading source of uncertainty in such harmonic force calibration systems.

  6. Tectonic calibrations in molecular dating

    Institute of Scientific and Technical Information of China (English)

    Ullasa KODANDARAMAIAH

    2011-01-01

    Molecular dating techniques require the use of calibrations, which are usually fossil or geological vicariance-based.Fossil calibrations have been criticised because they result only in minimum age estimates. Based on a historical biogeographic perspective, Ⅰ suggest that vicariance-based calibrations are more dangerous. Almost all analytical methods in historical biogeography are strongly biased towards inferring vicariance, hence vicariance identified through such methods is unreliable. Other studies, especially of groups found on Gondwanan fragments, have simply assumed vicariance. Although it was previously believed that vicariance was the predominant mode of speciation, mounting evidence now indicates that speciation by dispersal is common, dominating vicariance in several groups. Moreover, the possibility of speciation having occurred before the said geological event cannot be precluded. Thus, geological calibrations can under- or overestimate times, whereas fossil calibrations always result in minimum estimates. Another major drawback of vicariant calibrations is the problem of circular reasoning when the resulting estimates are used to infer ages of biogeographic events. Ⅰ argue that fossil-based dating is a superior alternative to vicariance, primarily because the strongest assumption in the latter, that speciation was caused by the said geological process, is more often than not the most tenuous. When authors prefer to use a combination of fossil and vicariant calibrations, one suggestion is to report results both with and without inclusion of the geological constraints. Relying solely on vicariant calibrations should be strictly avoided.

  7. The Advanced LIGO Photon Calibrators

    CERN Document Server

    Karki, S; Kandhasamy, S; Abbott, B P; Abbott, T D; Anders, E H; Berliner, J; Betzwieser, J; Daveloza, H P; Cahillane, C; Canete, L; Conley, C; Gleason, J R; Goetz, E; Kissel, J S; Izumi, K; Mendell, G; Quetschke, V; Rodruck, M; Sachdev, S; Sadecki, T; Schwinberg, P B; Sottile, A; Wade, M; Weinstein, A J; West, M; Savage, R L

    2016-01-01

    The two interferometers of the Laser Interferometry Gravitaional-wave Observatory (LIGO) recently detected gravitational waves from the mergers of binary black hole systems. Accurate calibration of the output of these detectors was crucial for the observation of these events, and the extraction of parameters of the sources. The principal tools used to calibrate the responses of the second-generation (Advanced) LIGO detectors to gravitational waves are systems based on radiation pressure and referred to as Photon Calibrators. These systems, which were completely redesigned for Advanced LIGO, include several significant upgrades that enable them to meet the calibration requirements of second-generation gravitational wave detectors in the new era of gravitational-wave astronomy. We report on the design, implementation, and operation of these Advanced LIGO Photon Calibrators that are currently providing fiducial displacements on the order of $10^{-18}$ m/$\\sqrt{\\textrm{Hz}}$ with accuracy and precision of better ...

  8. Antenna Calibration and Measurement Equipment

    Science.gov (United States)

    Rochblatt, David J.; Cortes, Manuel Vazquez

    2012-01-01

    A document describes the Antenna Calibration & Measurement Equipment (ACME) system that will provide the Deep Space Network (DSN) with instrumentation enabling a trained RF engineer at each complex to perform antenna calibration measurements and to generate antenna calibration data. This data includes continuous-scan auto-bore-based data acquisition with all-sky data gathering in support of 4th order pointing model generation requirements. Other data includes antenna subreflector focus, system noise temperature and tipping curves, antenna efficiency, reports system linearity, and instrument calibration. The ACME system design is based on the on-the-fly (OTF) mapping technique and architecture. ACME has contributed to the improved RF performance of the DSN by approximately a factor of two. It improved the pointing performances of the DSN antennas and productivity of its personnel and calibration engineers.

  9. Fractal dimension of scattering equivalent section of aerosol and its calibration mechanism

    Institute of Scientific and Technical Information of China (English)

    Fang Gu; Jiahong Zhang; Yulin Chen

    2009-01-01

    The correct calibration of coefficients in the inversion model for aerosol mass concentration is the precondition of obtaining highly precise results.The concept of the fractal dimension of scattering equivalent section is presented,and the calibration mechanism of the fractal dimension is discussed.Based on the calibration mechanism,the stability of the fractal dimension is analyzed.Theoretical analysis and experimental results indicate that the fractal dimension obtained by the intersection point calibration method is stable,while that calibrated by the Gauss-Newton method is instable,which only describes the shape characteristic of a small sample.The study of the calibration mechanism for the fractal dimension markedly enhances the present model for aerosol mass concentration.

  10. Accurate flexural spring constant calibration of colloid probe cantilevers using scanning laser Doppler vibrometry

    Science.gov (United States)

    Gates, Richard S.; Osborn, William A.; Shaw, Gordon A.

    2015-06-01

    Calibration of the flexural spring constant for atomic force microscope (AFM) colloid probe cantilevers provides significant challenges. The presence of a large attached spherical added mass complicates many of the more common calibration techniques such as reference cantilever, Sader, and added mass. Even the most promising option, AFM thermal calibration, can encounter difficulties during the optical lever sensitivity measurement due to strong adhesion and friction between the sphere and a surface. This may cause buckling of the end of the cantilever and hysteresis in the approach-retract curves resulting in increased uncertainty in the calibration. Most recently, a laser Doppler vibrometry thermal method has been used to accurately calibrate the normal spring constant of a wide variety of tipped and tipless commercial cantilevers. This paper describes a variant of the technique, scanning laser Doppler vibrometry, optimized for colloid probe cantilevers and capable of spring constant calibration uncertainties near ±1%.

  11. A calibrated Franklin chimes

    Science.gov (United States)

    Gonta, Igor; Williams, Earle

    1994-05-01

    Benjamin Franklin devised a simple yet intriguing device to measure electrification in the atmosphere during conditions of foul weather. He constructed a system of bells, one of which was attached to a conductor that was suspended vertically above his house. The device is illustrated in a well-known painting of Franklin (Cohen, 1985). The elevated conductor acquired a potential due to the electric field in the atmosphere and caused a brass ball to oscillate between two bells. The purpose of this study is to extend Franklin's idea by constructing a set of 'chimes' which will operate both in fair and in foul weather conditions. In addition, a mathematical relationship will be established between the frequency of oscillation of a metallic sphere in a simplified geometry and the potential on one plate due to the electrification of the atmosphere. Thus it will be possible to calibrate the 'Franklin Chimes' and to obtain a nearly instantaneous measurement of the potential of the elevated conductor in both fair and foul weather conditions.

  12. Self Calibrating Interferometric Sensor

    OpenAIRE

    Sørensen, Henrik Schiøtt; Larsen, Niels Bent

    2006-01-01

    This thesis deals with the development of an optical sensor based on micro interferometric backscatter detection (MIBD). A price effective, highly sensitive and ready for mass production platform is the goal of this project. The thesis covers three areas. The first part of the thesis deals with theoretical models for describing the optical phenomena utilized in this technique. A model based on ray–tracing has been developed and shown to be a valuable tool for describing certain features in th...

  13. OPTEC: A Cubesat for Solar Cell Calibration

    Science.gov (United States)

    Landis, Geoffrey; Hepp, Aloysius; Arutyunov, Dennis; White, Kelsey; Witsberger, Paul

    2014-01-01

    A new type of small spacecraft, the cubesat, has introduced a new concept for extremely small, low-cost missions into space. Cubesats are designed to be launched as secondary payloads on other missions, and are made up of unit elements (U) of size 10 cm by 10 cm by 10 cm, with a nominal mass of no more than 1.33 kg per U. We have designed a cubesat, OPTEC (Orbital Photovoltaic Testbed Cubesat) as a low-cost testbed to demonstrate, calibrate, and test solar cell technologies in space. Size of the cubesat is 2U (10x10x20cm, and the mass 2.66 kg. The cubesat deploys from the International Space Station into Low Earth Orbit at an altitude of about 420 km. Up to two 4x8cm test solar panels can be flown, with full I-V curves and temperature measurements taken.

  14. Mexican national pyronometer network calibration

    Science.gov (United States)

    VAldes, M.; Villarreal, L.; Estevez, H.; Riveros, D.

    2013-12-01

    In order to take advantage of the solar radiation as an alternate energy source it is necessary to evaluate the spatial and temporal availability. The Mexican National Meterological Service (SMN) has a network with 136 meteorological stations, each coupled with a pyronometer for measuring the global solar radiation. Some of these stations had not been calibrated in several years. The Mexican Department of Energy (SENER) in order to count on a reliable evaluation of the solar resource funded this project to calibrate the SMN pyrometer network and validate the data. The calibration of the 136 pyronometers by the intercomparison method recommended by the World Meterological Organization (WMO) requires lengthy observations and specific environmental conditions such as clear skies and a stable atmosphere, circumstances that determine the site and season of the calibration. The Solar Radiation Section of the Instituto de Geofísica of the Universidad Nacional Autónoma de México is a Regional Center of the WMO and is certified to carry out the calibration procedures and emit certificates. We are responsible for the recalibration of the pyronometer network of the SMN. A continuous emission solar simulator with exposed areas with 30cm diameters was acquired to reduce the calibration time and not depend on atmospheric conditions. We present the results of the calibration of 10 thermopile pyronometers and one photovoltaic cell by the intercomparison method with more than 10000 observations each and those obtained with the solar simulator.

  15. Jet Mass Reconstruction with the ATLAS Detector in Run 2

    CERN Document Server

    Jansky, Roland; The ATLAS collaboration

    2016-01-01

    The details of the ATLAS jet mass reconstruction and calibration are presented. In particular, the jet mass scale is calibrated using Monte Carlo simulation for large-radius groomed jets. Corresponding uncertainties are presented. An alternative jet mass definition that incorporates tracking information called the track-assisted jet mass is introduced and its performance is compared to the traditional calorimeter-only jet mass definition. An outlook on future improvments is also given.

  16. Calibration of "Babyline" RP instruments

    CERN Multimedia

    2015-01-01

      If you have old RP instrumentation of the “Babyline” type, as shown in the photo, please contact the Radiation Protection Group (Joffrey Germa, 73171) to have the instrument checked and calibrated. Thank you. Radiation Protection Group

  17. Two-Step Camera Calibration Method Developed for Micro UAV'S

    Science.gov (United States)

    Gašparović, M.; Gajski, D.

    2016-06-01

    The development of unmanned aerial vehicles (UAVs) and continuous price reduction of unmanned systems attracted us to this research. Professional measuring systems are dozens of times more expensive and often heavier than "amateur", non-metric UAVs. For this reason, we tested the DJI Phantom 2 Vision Plus UAV. Phantom's smaller mass and velocity can develop less kinetic energy in relation to the professional measurement platforms, which makes it potentially less dangerous for use in populated areas. In this research, we wanted to investigate the ability of such non-metric UAV and find the procedures under which this kind of UAV may be used for the photogrammetric survey. It is important to emphasize that UAV is equipped with an ultra wide-angle camera with 14MP sensor. Calibration of such cameras is a complex process. In the research, a new two-step process is presented and developed, and the results are compared with standard one-step camera calibration procedure. Two-step process involves initially removed distortion on all images, and then uses these images in the phototriangulation with self-calibration. The paper presents statistical indicators which proved that the proposed two-step process is better and more accurate procedure for calibrating those types of cameras than standard one-step calibration. Also, we suggest two-step calibration process as the standard for ultra-wideangle cameras for unmanned aircraft.

  18. Pressures Detector Calibration and Measurement

    CERN Document Server

    AUTHOR|(CDS)2156315

    2016-01-01

    This is report of my first and second projects (of 3) in NA61. I did data taking and analysis in order to do calibration of pressure detectors and verified it. I analyzed the data by ROOT software using the C ++ programming language. The first part of my project was determination of calibration factor of pressure sensors. Based on that result, I examined the relation between pressure drop, gas flow rate of in paper filter and its diameter.

  19. Beam Imaging and Luminosity Calibration

    CERN Document Server

    Klute, Markus; Salfeld-Nebgen, Jakob

    2016-01-01

    We discuss a method to reconstruct two-dimensional proton bunch densities using vertex distributions accumulated during LHC beam-beam scans. The $x$-$y$ correlations in the beam shapes are studied and an alternative luminosity calibration technique is introduced. We demonstrate the method on simulated beam-beam scans and estimate the uncertainty on the luminosity calibration associated to the beam-shape reconstruction to be below 1\\%.

  20. WFC3: UVIS Dark Calibration

    Science.gov (United States)

    Bourque, Matthew; Biretta, John A.; Anderson, Jay; Baggett, Sylvia M.; Gunning, Heather C.; MacKenty, John W.

    2014-06-01

    Wide Field Camera 3 (WFC3), a fourth-generation imaging instrument on board the Hubble Space Telescope (HST), has exhibited excellent performance since its installation during Servicing Mission 4 in May 2009. The UVIS detector, comprised of two e2v CCDs, is one of two channels available on WFC3 and is named for its ultraviolet and visible light sensitivity. We present the various procedures and results of the WFC3/UVIS dark calibration, which monitors the health and stability of the UVIS detector, provides characterization of hot pixels and dark current, and produces calibration files to be used as a correction for dark current in science images. We describe the long-term growth of hot pixels and the impacts that UVIS Charge Transfer Efficiency (CTE) losses, postflashing, and proximity to the readout amplifiers have on the population. We also discuss the evolution of the median dark current, which has been slowly increasing since the start of the mission and is currently ~6 e-/hr/pix, averaged across each chip. We outline the current algorithm for creating UVIS dark calibration files, which includes aggressive cosmic ray masking, image combination, and hot pixel flagging. Calibration products are available to the user community, typically 3-5 days after initial processing, through the Calibration Database System (CDBS). Finally, we discuss various improvements to the calibration and monitoring procedures. UVIS dark monitoring will continue throughout and beyond HST’s current proposal cycle.

  1. Calibrating Cluster Number Counts with CMB lensing

    CERN Document Server

    Louis, Thibaut

    2016-01-01

    CMB Stage-4 experiments will reduce the uncertainties on the gravitational lensing potential by an order of magnitude compared to current measurements, and will also produce a Sunyaev-Zel'dovich (SZ) cluster catalog containing $\\sim10^{5}$ objects, two orders of magnitudes higher than what is currently available. In this paper we propose to combine these two observables and show that it is possible to calibrate the masses of the full Stage-4 cluster catalog internally owing to the high signal to noise measurement of the CMB lensing convergence field. We find that a CMB Stage-4 experiment will constrain the hydrostatic bias parameter to sub-percent accuracy. We also show constraints on a non parametric $Y-M$ relationship which could be used to study its evolution with mass and redshift. Finally we present a joint likelihood for thermal SZ (tSZ) flux and mass measurements, and show that it could lead to a $\\sim5\\sigma$ detection of the lower limit on the sum of the neutrino masses in the normal hierarchy ($\\sum...

  2. The KLOE Online Calibration System

    Institute of Scientific and Technical Information of China (English)

    E.Pasqualucci

    2001-01-01

    Based on all the features of the KLOE online software,the online calibration system performs current calibration quality checking in real time and starts automatically new calibration procedures when needed.Acalibration manager process controls the system,implementing the interface to the online system,receiving information from the run control and translating its state transitions to a separate state machine.It acts as a " calibration run controller"and performs failure recovery when requested by a set of process checkers.The core of the system is a multi-threaded OO histogram server that receives histogramming commands by remote processes and operates on local ROOT histograms.A client library and C,fortran and C++ application interface libraries allow the user to connect and define his own histogram or read histograms owned by others using an bool-like interface.Several calibration processes running in parallel in a destributed,multiplatform environment can fill the same histograms,allowing fast external information check.A monitor thread allow remote browsing for visual inspection,Pre-filtered data are read in nonprivileged spy mode from the data acquisition system via the Kloe Integrated Dataflow,privileged spy mode from the data acquisiton system via the Kole Integrated Dataflow.The main characteristics of the system are presented.

  3. Testing the precision optical calibration module for PINGU

    Energy Technology Data Exchange (ETDEWEB)

    Jurkovic, Martin; Holzapfel, Kilian [TU Muenchen, Physik-Department, Excellence Cluster Universe, Boltzmannstr. 2, 85748 Garching (Germany); Collaboration: IceCube-Collaboration

    2015-07-01

    The Precision IceCube Next Generation Upgrade (PINGU) is primarily designed to determine the neutrino mass hierarchy. This measurement requires an accurate calibration of the detector in order to reduce systematic uncertainties. The Precision Optical Calibration Modules (POCAM) will be placed in the detector as a well calibrated artificial light source in the ice. The POCAM will be enclosed in a glass sphere identical to those used for the detector modules. To construct and simulate a prototype of the POCAM, every component needs to be analyzed by their optical characteristics and by the behavior in temperatures down to -50 C. Therefore a highly shielded an isolated environment has to be build up. We report the status of the testing environment and the hardware selected.

  4. Power calibrations for TRIGA reactors

    International Nuclear Information System (INIS)

    The purpose of this paper is to establish a framework for the calorimetric power calibration of TRIGA reactors so that reliable results can be obtained with a precision better than ± 5%. Careful application of the same procedures has produced power calibration results that have been reproducible to ± 1.5%. The procedures are equally applicable to the Mark I, Mark II and Mark III reactors as well as to reactors having much larger reactor tanks and to TRIGA reactors capable of forced cooling up to 3 MW in some cases and 15 MW in another case. In the case of forced cooled TRIGA reactors, the calorimetric power calibration is applicable in the natural convection mode for these reactors using exactly the same procedures as are discussed below for the smaller TRIGA reactors (< 2 MW)

  5. Facility for dosimetric instrument calibration

    International Nuclear Information System (INIS)

    A structure is designed consisting of a rotary support of containers with radiation sources and of a rotary plug mounted above the sources. A support post with a slide rest and arms rotating around the post longitudinal axis is mounted in the centre of the container support. THe arms support instruments to be calibrated. The colimation cone of the respective source is directed to the tensor of the instrument being calibrated. The slide rest is balanced using a counterpoise mounted in the support post. Sources are not removed from the containers in source change during measurement. The support can hold more containers and the slide rest can support more instruments to be calibrated than the existing configurations. (M.D.). 2 figs

  6. Towards a Precise Energy Calibration of the CUORE Double Beta Decay Experiment

    Science.gov (United States)

    Dally, Adam G.

    The mass of the neutrino may hold the key to many problems in cosmology and astrophysics. The observation of neutrino oscillations shows that neutrinos have mass, which was something that was not accounted for in the Standard Model of particle physics. This thesis covers topics relating to measuring the value of neutrino mass directly using bolometers. The first section will discuss the neutrino mass and different experiments for measuring the mass using bolometers. The mass of the neutrino can be measured directly from beta-decay or inferred from observation of neutrinoless double beta decay (0nubetabeta). In this work I present Monte Carlo and analytic simulation of the MARE experiment including, pile-up and energy resolution effects. The mass measurement limits of a micro-calorimeter experiments as it relates to the quantity of decays measured is provided. A similar simulation is preformed for the HolMES experiment. The motivation is to determine the sensitivity of such experiments and the detector requirements to reach the goal sensitivity. Another possible method for determining the neutrino mass is to use neutrinoless double beta decay. The second section will cover the Cryogenic Underground Observatory for Rare Events (CUORE) detector calibration system (DCS). CUORE is a neutrinoless double beta decay (0nubetabeta) experiment with an active mass of 206 kg of 130Te. The detector consists of 988 TeO2 bolometers operating at 10 mK. The signature of 0 nubetabeta decay is an excess of events at the Q-value of 2528 keV. Understanding the energy response is critical for event identification, but this presents many challenges. Calibration is necessary to associate a known energy from a gamma with a voltage pulse from the detector. The DCS must overcome many design challenges. The calibration source must be placed safely and reliable within the detector. The temperature of the detector region of the cryostat must not be changed during calibration. To achieve this

  7. Reaction of the C3(X1Σg+) carbon cluster with H2S(X1A1), hydrogen sulfide: Photon-induced formation of C3S, tricarbon sulfur

    International Nuclear Information System (INIS)

    In this paper we report on the neutral-neutral reaction of the C3 carbon cluster with H2S in solid inert argon at 12 K, conditions that mimic, in part, the surfaces of interstellar grains. In the first step of the reaction, a C3•H2S complex is formed via an almost barrierless entrance addition mechanism. This complex, stabilized by an estimated 7.45 kJ/mol (CCSD(T)/aug-cc-pVTZ//B3LYP/6-311++G(d,p) level), is formed by the interaction of a terminal carbon of C3 with a hydrogen in H2S. This con-covalent complex displays a band at 2044.1 cm−1 observed via Fourier transform infrared absorption spectroscopy. With the help of the MP2/aug-ccpVDZ level method, this band is assigned to the CC asymmetric vibration mode. When the complex is exposed to UV-visible photons (hν < 5.5 eV) the tricarbon sulfur C3S molecule is identified, based on the appearance of a characteristic CC stretching band at 2047.5 cm−1. Calculated ground-state potential energy surfaces also confirm the concomitant formation of molecular H2. This facile reaction pathway involves an attainable transition state of 174.4 kJ/mol. Conversely, competing lower-energy reaction pathways that would lead to the generation of H2C3S (propadienethione), or C2H2 (acetylene) and CS, involve much more complex, multi-stage pathways, and are not observed experimentally

  8. Quantitative Analysis of Sulfide Minerals by Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry Using Glass Reference Materials with Matrix Normalization Plus Sulfur Internal Standardization Calibration%玻璃标样结合硫内标归一定量技术在激光剥蚀-等离子体质谱分析硫化物矿物中的应用

    Institute of Scientific and Technical Information of China (English)

    袁继海; 詹秀春; 范晨子; 赵令浩; 孙冬阳; 贾泽荣; 胡明月; 蒯丽君

    2012-01-01

    A novel strategy for microanalysis of sulfides by laser ablation (LA)-ICP-MS was established. In this method, the relative sensitivity factor of Ca relative to S in anhydrite mineral reference material was taken as a transition bridge, by which the relative sensitivity factors of interesting elements in glass reference materials relative to Ca could be converted into relative sensitivity factors relative to S by the transition bridge, then the quantitative analysis of multi-elements in sulfide minerals by multi-glass reference materials with matrix normalization plus sulfur internal standardizationcalibration was carried out. 20 elements in the American polymetal sulfide mineral reference material MASS-1 were analyzed using this new method. The relative errors of major elements in MASS-1 were less than 10% ? And the results of trace elements with reference values were nearly within the uncertainty of the preliminary values. Multi-elements in 12 sulfide single minerals were analyzed by applying this new method. The relative errors of the greatest number of major elements were less than 10% , with which the results of most major elements were accurate than those obtained by MASS-1 as calibration standard with matrix normalization plus internal standardization or internal standard calibration. And the results to trace elements agreed well with the calibrated results by MASS-1 with matrix normalization plus internal standardization or internal standard calibration. This method overcomes the problem of non-matrix matched standards, enables to accurately determine the major composition of sulfur in sulfide minerals and suggests a new approach for analysis of sulfide minerals.%以硬石膏矿物标样中Ca相对于S的灵敏度因子为基准,将玻璃标样中主量和痕量元素相对于Ca的灵敏度因子转换成元素相对于S的灵敏度因子,建立了多玻璃标样结合硫内标归一定量技术分析硫化物单矿物多元素的新方法.利用本方法

  9. NASA's Metrology and Calibration program

    Science.gov (United States)

    Kern, Frederick A.

    1991-01-01

    The success of the National Aeronautics and Space Administration's scientific and engineering projects is often based on the capability and quality of the metrology and calibration programs of its field centers and facilities. A Metrology and Calibration Working Group, having representation from each of the NASA field centers and facilities, was established to develop and implement a program to provide a centralized direction and agency wide focus. A brief history of the Group is presented. The development of the Group's operating philosophy, the long term objectives, the measurement research and development program, and review of accomplishments is discussed.

  10. GREAT/SOFIA atmospheric calibration

    CERN Document Server

    Guan, Xin; Graf, Urs U; Güsten, Rolf; Okada, Yoko; Torres, Miguel Angel Requena; Simon, Robert; Wiesemeyer, Helmut

    2012-01-01

    The GREAT observations need frequency-selective calibration across the passband for the residual atmospheric opacity at flight altitude. At these altitudes the atmospheric opacity has both narrow and broad spectral features. To determine the atmospheric transmission at high spectral resolution, GREAT compares the observed atmospheric emission with atmospheric model predictions, and therefore depends on the validity of the atmospheric models. We discusse the problems identified in this comparison with respect to the observed data and the models, and describe the strategy used to calibrate the science data from GREAT/SOFIA during the first observing periods.

  11. Field calibration of cup anemometers

    DEFF Research Database (Denmark)

    Kristensen, L.; Jensen, G.; Hansen, A.;

    2001-01-01

    . It is concluded that the method has the advantage that many anemometers can be calibrated accurately with a minimum of work and cost. The obvious disadvantage is that the calibration of a set of anemometersmay take more than one month in order to have wind speeds covering a sufficiently large magnitude range...... in a wind direction sector where we can be sure that the instruments are exposed to identical, simultaneous wind flows. Another main conclusion is thatstatistical uncertainty must be carefully evaluated since the individual 10 minute wind-speed averages are not statistically independent....

  12. Performance standard for dose Calibrator

    CERN Document Server

    Darmawati, S

    2002-01-01

    Dose calibrator is an instrument used in hospitals to determine the activity of radionuclide for nuclear medicine purposes. International Electrotechnical Commission (IEC) has published IEC 1303:1994 standard that can be used as guidance to test the performance of the instrument. This paper briefly describes content of the document,as well as explains the assessment that had been carried out to test the instrument accuracy in Indonesia through intercomparison measurement.Its is suggested that hospitals acquire a medical physicist to perform the test for its dose calibrator. The need for performance standard in the form of Indonesia Standard is also touched.

  13. Tank calibration; Arqueacao de tanques

    Energy Technology Data Exchange (ETDEWEB)

    Chan, Ana [PETROBRAS S.A., Rio de Janeiro, RJ (Brazil)

    2003-07-01

    This work relates the analysis of the norms ISO (International Organization for Standardization) for calibration of vertical cylindrical tanks used in fiscal measurement, established on Joint Regulation no 1 of June 19, 2000 between the ANP (National Agency of Petroleum) and the INMETRO (National Institute of Metrology, Normalization and Industrial Quality). In this work a comparison between norms ISO and norms published by the API (American Petroleum Institute) and the IP (Institute of Petroleum) up to 2001 was made. It was concluded that norms ISO are wider than norms API, IP, and INMETRO methods in the calibration of vertical cylindrical tanks. (author)

  14. A simple calibration method for mechanically braked cycle ergometers.

    Science.gov (United States)

    Van Praagh, E; Bedu, M; Roddier, P; Coudert, J

    1992-01-01

    The calibration of cycle ergometers should be checked regularly. Some studies have shown calibration errors of more than 40%. A simple, inexpensive calibrating method for mechanically braked cycle ergometers was developed and tried out on a new type of ergocycle. The cycle ergometer was elevated and the crank replaced by a pulley fitted to the shaft. The crank speed (rpm) increased linearly as a function of time when different masses were applied on the pulley. For a given braking force on the cycle ergometer, different accelerations corresponding to the increased pulley forces could be measured. When extrapolating for zero acceleration, it was possible to determine a "limit-force" which allowed the system to be in equilibrium. Additional force creates motion. The same experiments were repeated with increasing braking forces. Using the differently sized gear sprockets of the transmission system, it was possible to calculate the actual force, including all the resistances. The actual force found by the calibrating method was then compared with the indicated force proposed by the manufacturer. With increasing forces, the relative errors decreased from 9.6 to 2.9%. The cycle ergometer calibrated by this technique meets the standards recommended in exercise physiology. PMID:1544728

  15. Standard practice for torque calibration of testing machines and devices

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2009-01-01

    1.1 This practice covers procedures and requirements for the calibration of torque for static and quasi-static torque capable testing machines or devices. These may, or may not, have torque indicating systems and include those devices used for the calibration of hand torque tools. Testing machines may be calibrated by one of the three following methods or combination thereof: 1.1.1 Use of standard weights and lever arms. 1.1.2 Use of elastic torque measuring devices. 1.1.3 Use of elastic force measuring devices and lever arms. 1.1.4 Any of the methods require a specific uncertainty of measurement and a traceability derived from national standards of mass and length. 1.2 The procedures of 1.1.1, 1.1.2, and 1.1.3 apply to the calibration of the torque-indicating systems associated with the testing machine, such as a scale, dial, marked or unmarked recorder chart, digital display, etc. In all cases the buyer/owner/user must designate the torque-indicating system(s) to be calibrated and included in the repor...

  16. Recommended Inorganic Chemicals for Calibration.

    Science.gov (United States)

    Moody, John R.; And Others

    1988-01-01

    All analytical techniques depend on the use of calibration chemicals to relate analyte concentration to instrumental parameters. Discusses the preparation of standard solutions and provides a critical evaluation of available materials. Lists elements by group and discusses the purity and uses of each. (MVL)

  17. Reliability-Based Code Calibration

    DEFF Research Database (Denmark)

    Faber, M.H.; Sørensen, John Dalsgaard

    2003-01-01

    . Thereafter the code calibration problem is presented in its principal decision theoretical form and it is discussed how acceptable levels of failure probability (or target reliabilities) may be established. Furthermore suggested values for acceptable annual failure probabilities are given for ultimate...

  18. Measurement System and Calibration report

    DEFF Research Database (Denmark)

    Kock, Carsten Weber; Vesth, Allan

    This Measurement System & Calibration report is describing DTU’s measurement system installed at a specific wind turbine. A major part of the sensors has been installed by others (see [1]) the rest of the sensors have been installed by DTU. The results of the measurements, described in this report...

  19. Measurement System and Calibration report

    DEFF Research Database (Denmark)

    Vesth, Allan; Kock, Carsten Weber

    The report describes power curve measurements carried out on a given wind turbine. The measurements are carried out in accordance to Ref. [1]. A site calibration has been carried out; see Ref. [2], and the measured flow correction factors for different wind directions are used in the present...

  20. Scalar Calibration of Vector Magnetometers

    DEFF Research Database (Denmark)

    Merayo, José M.G.; Brauer, Peter; Primdahl, Fritz;

    2000-01-01

    the parameters for a given data set. Therefore, a magnetometer may be characterized inexpensively in the Earth's magnetic-field environment. This procedure has been used successfully in the pre-flight calibration of the state-of-the-art magnetometers on board the magnetic mapping satellites Orsted, Astrid-2...

  1. Approaching a Physical Calibration of the AGB Phase

    Science.gov (United States)

    Marigo, Paola

    2015-08-01

    The widespread impact of Asymptotic Giant Branch (AGB) stars on the observed properties of galaxies is universally accepted. Despite their importance, severe uncertainties plague AGB models and propagate through to current population synthesis studies of galaxies, undermining the interpretation of a galaxy's basic properties (mass, age, chemical evolution, dust budget). The only reliable path forward is to apply a physically-sound calibration of AGB stellar models in which all main physical processes and their interplay are taken into account (e.g., mixing, mass loss, nucleosynthesis, pulsation, molecular chemistry, dust formation). In this context, I will review recent and ongoing efforts to calibrate the evolution of AGB stars, which combine an all-round theoretical approach anchored by stellar physics with exceptionally high quality data of resolved AGB stars in the Milky Way and nearby galaxies.

  2. Radio Interferometric Calibration Using a Riemannian Manifold

    CERN Document Server

    Yatawatta, Sarod

    2013-01-01

    In order to cope with the increased data volumes generated by modern radio interferometers such as LOFAR (Low Frequency Array) or SKA (Square Kilometre Array), fast and efficient calibration algorithms are essential. Traditional radio interferometric calibration is performed using nonlinear optimization techniques such as the Levenberg-Marquardt algorithm in Euclidean space. In this paper, we reformulate radio interferometric calibration as a nonlinear optimization problem on a Riemannian manifold. The reformulated calibration problem is solved using the Riemannian trust-region method. We show that calibration on a Riemannian manifold has faster convergence with reduced computational cost compared to conventional calibration in Euclidean space.

  3. An indigenous cluster beam apparatus with a reflectron time-of-flight mass spectrometer

    Indian Academy of Sciences (India)

    G Raina; G U Kulkarni; R T Yadav; V S Ramamurthy; C N R Rao

    2000-04-01

    The design and fabrication of a Smalley-type cluster source in combination with a reflectron based time-of-flight (TOF) mass spectrometer are reported. The generation of clusters is based on supersonic jet expansion of the sampling plume. Sample cells for both liquid and solid targets developed for this purpose are described. Two pulsed Nd-YAG lasers are used in tandem, one (532 nm) for target vapourization and the other (355 nm) for cluster ionization. Methanol clusters of nuclearity up to 14 (mass 500 amu) were produced from liquid methanol as the test sample. The clusters were detected with a mass resolution of ~ 2500 in the R-TOF geometry. Carbon clusters up to a nuclearity of 28 were obtained using a polyimide target. The utility of the instrument is demonstrated by carrying out experiments to generate mixed clusters from alcohol mixtures.

  4. Radiometric Calibration of Osmi Imagery Using Solar Calibration

    Science.gov (United States)

    Lee, Dong-Han; Kim, Yong-Seung

    2000-12-01

    OSMI (Ocean Scanning Multi-Spectral Imager) raw image data (Level 0) were acquired and radiometrically corrected. We have applied two methods, using solar & dark calibration data from OSMI sensor and comparing with the SeaWiFS data, to the radiometric correction of OSMI raw image data. First, we could get the values of the gain and the offset for each pixel and each band from comparing the solar & dark calibration data with the solar input radiance values, calculated from the transmittance, BRDF (Bidirectional Reflectance Distribution Function) and the solar incidence angle (¥â,¥è) of OSMI sensor. Applying this calibration data to OSMI raw image data, we got the two odd results, the lower value of the radiometric corrected image data than the expected value, and the Venetian Blind Effect in the radiometric corrected image data. Second, we could get the reasonable results from comparing OSMI raw image data with the SeaWiFS data, and get a new problem of OSMI sensor.

  5. Buoyancy contribution to uncertainty of mass, conventional mass and force

    Science.gov (United States)

    Malengo, Andrea; Bich, Walter

    2016-04-01

    The conventional mass is a useful concept introduced to reduce the impact of the buoyancy correction in everyday mass measurements, thus avoiding in most cases its accurate determination, necessary in measurements of ‘true’ mass. Although usage of conventional mass is universal and standardized, the concept is considered as a sort of second-choice tool, to be avoided in high-accuracy applications. In this paper we show that this is a false belief, by elucidating the role played by covariances between volume and mass and between volume and conventional mass at the various stages of the dissemination chain and in the relationship between the uncertainties of mass and conventional mass. We arrive at somewhat counter-intuitive results: the volume of the transfer standard plays a comparatively minor role in the uncertainty budget of the standard under calibration. In addition, conventional mass is preferable to mass in normal, in-air operation, as its uncertainty is smaller than that of mass, if covariance terms are properly taken into account, and the uncertainty over-stating (typically) resulting from neglecting them is less severe than that (always) occurring with mass. The same considerations hold for force. In this respect, we show that the associated uncertainty is the same using mass or conventional mass, and, again, that the latter is preferable if covariance terms are neglected.

  6. SMAP RADAR Calibration and Validation

    Science.gov (United States)

    West, R. D.; Jaruwatanadilok, S.; Chaubel, M. J.; Spencer, M.; Chan, S. F.; Chen, C. W.; Fore, A.

    2015-12-01

    The Soil Moisture Active Passive (SMAP) mission launched on Jan 31, 2015. The mission employs L-band radar and radiometer measurements to estimate soil moisture with 4% volumetric accuracy at a resolution of 10 km, and freeze-thaw state at a resolution of 1-3 km. Immediately following launch, there was a three month instrument checkout period, followed by six months of level 1 (L1) calibration and validation. In this presentation, we will discuss the calibration and validation activities and results for the L1 radar data. Early SMAP radar data were used to check commanded timing parameters, and to work out issues in the low- and high-resolution radar processors. From April 3-13 the radar collected receive only mode data to conduct a survey of RFI sources. Analysis of the RFI environment led to a preferred operating frequency. The RFI survey data were also used to validate noise subtraction and scaling operations in the radar processors. Normal radar operations resumed on April 13. All radar data were examined closely for image quality and calibration issues which led to improvements in the radar data products for the beta release at the end of July. Radar data were used to determine and correct for small biases in the reported spacecraft attitude. Geo-location was validated against coastline positions and the known positions of corner reflectors. Residual errors at the time of the beta release are about 350 m. Intra-swath biases in the high-resolution backscatter images are reduced to less than 0.3 dB for all polarizations. Radiometric cross-calibration with Aquarius was performed using areas of the Amazon rain forest. Cross-calibration was also examined using ocean data from the low-resolution processor and comparing with the Aquarius wind model function. Using all a-priori calibration constants provided good results with co-polarized measurements matching to better than 1 dB, and cross-polarized measurements matching to about 1 dB in the beta release. During the

  7. Calibration of the solar radio spectrometer

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    This paper shows some improvements and new results of calibration of Chinese solar radio spectrometer by analyzing the daily calibration data recorded in the period of 1997-2007. First, the calibration coefficient is fitted for three bands (1.0-2.0 GHz, 2.6-3.8 GHz, 5.2-7.6 GHz) of the spectrometer by using the moving-average method confined by the property of the daily calibration data. By this calibration coefficient, the standard deviation of the calibration result was less than 10 sfu for 95% frequencies of 2.6-3.8 GHz band in 2003. This result is better than that calibrated with the constant coefficient. Second, the calibration coefficient is found in good correlation with local air temperature for most frequencies of 2.6-3.8 GHz band. Moreover, these results are helpful in the research of the quiet solar radio emission.

  8. Calibration of the solar radio spectrometer

    Institute of Scientific and Technical Information of China (English)

    TAN ChengMing; YAN YiHua; TAN BaoLin; XU GuiRong

    2009-01-01

    This paper shows some improvements and new results of calibration of Chinese solar radio spectrom-eter by analyzing the daily calibration data recorded in the period of 1997-2007. First, the calibration coefficient is fitted for three bands (1.0-2.0 GHz, 2.6-3.8 GHz, 5.2-7.6 GHz) of the spectrometer by using the moving-average method confined by the property of the daily calibration data. By this calibration coefficient, the standard deviation of the calibration result was less than 10 sfu for 95% frequencies of 2.6-3.8 GHz band in 2003. This result is better than that calibrated with the constant coefficient. Second, the calibration coefficient is found in good correlation with local air temperature for most frequencies of 2.6-3.8 GHz band. Moreover, these results are helpful in the research of the quiet solar radio emission.

  9. Attitude Sensor and Gyro Calibration for Messenger

    Science.gov (United States)

    O'Shaughnessy, Daniel; Pittelkau, Mark E.

    2007-01-01

    The Redundant Inertial Measurement Unit Attitude Determination/Calibration (RADICAL(TM)) filter was used to estimate star tracker and gyro calibration parameters using MESSENGER telemetry data from three calibration events. We present an overview of the MESSENGER attitude sensors and their configuration is given, the calibration maneuvers are described, the results are compared with previous calibrations, and variations and trends in the estimated calibration parameters are examined. The warm restart and covariance bump features of the RADICAL(TM) filter were used to estimate calibration parameters from two disjoint telemetry streams. Results show that the calibration parameters converge faster with much less transient variation during convergence than when the filter is cold-started at the start of each telemetry stream.

  10. Crop physiology calibration in the CLM

    Directory of Open Access Journals (Sweden)

    I. Bilionis

    2015-04-01

    scalable and adaptive scheme based on sequential Monte Carlo (SMC. The model showed significant improvement of crop productivity with the new calibrated parameters. We demonstrate that the calibrated parameters are applicable across alternative years and different sites.

  11. Calibration and Validation of Measurement System

    DEFF Research Database (Denmark)

    Kofoed, Jens Peter; Riemann, Sven; Knapp, Wilfried

    The report deals with the calibration of the measuring equipment on board the Wave Dragon, Nissum Bredning prototype.......The report deals with the calibration of the measuring equipment on board the Wave Dragon, Nissum Bredning prototype....

  12. Astrid-2 EMMA Magnetic Calibration

    DEFF Research Database (Denmark)

    Merayo, José M.G.; Brauer, Peter; Risbo, Torben;

    1998-01-01

    The Swedish micro-satellite Astrid-2 contains a tri-axial fluxgate magnetometer with the sensor co-located with a Technical University of Denmark (DTU) star camera for absolute attitude, and extended about 0.9 m on a hinged boom. The magnetometer is part of the RIT EMMA electric and magnetic fields...... experiment built as a collaboration between the DTU, Department of Automation and the Department of Plasma Physics, The Alfvenlaboratory, Royal Institute of Technology (RIT), Stockholm. The final magnetic calibration of the Astrid-2 satellite was done at the Lovoe Magnetic Observatory under the Geological...... Survey of Sweden near Stockholm on the night of May 15.-16., 1997. The magnetic calibration and the intercalibration between the star camera and the magnetic sensor was performed by measuring the Earth's magnetic field and simultaneously observing the star sky with the camera. The rotation matrix between...

  13. Calibration of a Parallel Kinematic Machine Tool

    Institute of Scientific and Technical Information of China (English)

    HE Xiao-mei; DING Hong-sheng; FU Tie; XIE Dian-huang; XU Jin-zhong; LI Hua-feng; LIU Hui-lin

    2006-01-01

    A calibration method is presented to enhance the static accuracy of a parallel kinematic machine tool by using a coordinate measuring machine and a laser tracker. According to the established calibration model and the calibration experiment, the factual 42 kinematic parameters of BKX-I parallel kinematic machine tool are obtained. By circular tests the comparison is made between the calibrated and the uncalibrated parameters and shows that there is 80% improvement in accuracy of this machine tool.

  14. Binary Classifier Calibration: Non-parametric approach

    OpenAIRE

    Naeini, Mahdi Pakdaman; Cooper, Gregory F.; Hauskrecht, Milos

    2014-01-01

    Accurate calibration of probabilistic predictive models learned is critical for many practical prediction and decision-making tasks. There are two main categories of methods for building calibrated classifiers. One approach is to develop methods for learning probabilistic models that are well-calibrated, ab initio. The other approach is to use some post-processing methods for transforming the output of a classifier to be well calibrated, as for example histogram binning, Platt scaling, and is...

  15. GREAT/SOFIA atmospheric calibration

    OpenAIRE

    Guan, Xin; Stutzki, Jürgen; Graf, Urs U.; Güsten, Rolf; Okada, Yoko; Torres, Miguel Angel Requena; Simon, Robert; Wiesemeyer, Helmut

    2012-01-01

    The GREAT observations need frequency-selective calibration across the passband for the residual atmospheric opacity at flight altitude. At these altitudes the atmospheric opacity has both narrow and broad spectral features. To determine the atmospheric transmission at high spectral resolution, GREAT compares the observed atmospheric emission with atmospheric model predictions, and therefore depends on the validity of the atmospheric models. We discusse the problems identified in this compari...

  16. Colour calibration for colour reproduction

    OpenAIRE

    Emmel, P.; R. D. Hersch

    2000-01-01

    Due to the proliferation of low-cost colour devices (digital colour cameras, scanners, printers etc.) during the last few years, colour calibration has become an important issue. Such devices should faithfully reproduce colour images, but experience shows they don't. Among the main reasons, we note the diversity of acquisition, display and printing technologies which makes standardization difficult. Each device has a different gamut, i.e. a different set of colours that it can acquire or repr...

  17. Calibrating thermal behavior of electronics

    Science.gov (United States)

    Chainer, Timothy J.; Parida, Pritish R.; Schultz, Mark D.

    2016-05-31

    A method includes determining a relationship between indirect thermal data for a processor and a measured temperature associated with the processor, during a calibration process, obtaining the indirect thermal data for the processor during actual operation of the processor, and determining an actual significant temperature associated with the processor during the actual operation using the indirect thermal data for the processor during actual operation of the processor and the relationship.

  18. Preliminary calibration of the ACP safeguards neutron counter

    Science.gov (United States)

    Lee, T. H.; Kim, H. D.; Yoon, J. S.; Lee, S. Y.; Swinhoe, M.; Menlove, H. O.

    2007-10-01

    The Advanced Spent Fuel Conditioning Process (ACP), a kind of pyroprocess, has been developed at the Korea Atomic Energy Research Institute (KAERI). Since there is no IAEA safeguards criteria for this process, KAERI has developed a neutron coincidence counter to make it possible to perform a material control and accounting (MC&A) for its ACP materials for the purpose of a transparency in the peaceful uses of nuclear materials at KAERI. The test results of the ACP Safeguards Neutron Counter (ASNC) show a satisfactory performance for the Doubles count measurement with a low measurement error for its cylindrical sample cavity. The neutron detection efficiency is about 21% with an error of ±1.32% along the axial direction of the cavity. Using two 252Cf neutron sources, we obtained various parameters for the Singles and Doubles rates for the ASNC. The Singles, Doubles, and Triples rates for a 252Cf point source were obtained by using the MCNPX code and the results for the ft8 cap multiplicity tally option with the values of ɛ, fd, and ft measured with a strong source most closely match the measurement results to within a 1% error. A preliminary calibration curve for the ASNC was generated by using the point model equation relationship between 244Cm and 252Cf and the calibration coefficient for the non-multiplying sample is 2.78×10 5 (Doubles counts/s/g 244Cm). The preliminary calibration curves for the ACP samples were also obtained by using an MCNPX simulation. A neutron multiplication influence on an increase of the Doubles rate for a metal ingot and UO2 powder is clearly observed. These calibration curves will be modified and complemented, when hot calibration samples become available. To verify the validity of this calibration curve, a measurement of spent fuel standards for a known 244Cm mass will be performed in the near future.

  19. Unassisted 3D camera calibration

    Science.gov (United States)

    Atanassov, Kalin; Ramachandra, Vikas; Nash, James; Goma, Sergio R.

    2012-03-01

    With the rapid growth of 3D technology, 3D image capture has become a critical part of the 3D feature set on mobile phones. 3D image quality is affected by the scene geometry as well as on-the-device processing. An automatic 3D system usually assumes known camera poses accomplished by factory calibration using a special chart. In real life settings, pose parameters estimated by factory calibration can be negatively impacted by movements of the lens barrel due to shaking, focusing, or camera drop. If any of these factors displaces the optical axes of either or both cameras, vertical disparity might exceed the maximum tolerable margin and the 3D user may experience eye strain or headaches. To make 3D capture more practical, one needs to consider unassisted (on arbitrary scenes) calibration. In this paper, we propose an algorithm that relies on detection and matching of keypoints between left and right images. Frames containing erroneous matches, along with frames with insufficiently rich keypoint constellations, are detected and discarded. Roll, pitch yaw , and scale differences between left and right frames are then estimated. The algorithm performance is evaluated in terms of the remaining vertical disparity as compared to the maximum tolerable vertical disparity.

  20. Model Calibration in Watershed Hydrology

    Science.gov (United States)

    Yilmaz, Koray K.; Vrugt, Jasper A.; Gupta, Hoshin V.; Sorooshian, Soroosh

    2009-01-01

    Hydrologic models use relatively simple mathematical equations to conceptualize and aggregate the complex, spatially distributed, and highly interrelated water, energy, and vegetation processes in a watershed. A consequence of process aggregation is that the model parameters often do not represent directly measurable entities and must, therefore, be estimated using measurements of the system inputs and outputs. During this process, known as model calibration, the parameters are adjusted so that the behavior of the model approximates, as closely and consistently as possible, the observed response of the hydrologic system over some historical period of time. This Chapter reviews the current state-of-the-art of model calibration in watershed hydrology with special emphasis on our own contributions in the last few decades. We discuss the historical background that has led to current perspectives, and review different approaches for manual and automatic single- and multi-objective parameter estimation. In particular, we highlight the recent developments in the calibration of distributed hydrologic models using parameter dimensionality reduction sampling, parameter regularization and parallel computing.

  1. PACS photometer calibration block analysis

    CERN Document Server

    Moór, A; Kiss, Cs; Balog, Z; Billot, N; Marton, G

    2013-01-01

    The absolute stability of the PACS bolometer response over the entire mission lifetime without applying any corrections is about 0.5% (standard deviation) or about 8% peak-to-peak. This fantastic stability allows us to calibrate all scientific measurements by a fixed and time-independent response file, without using any information from the PACS internal calibration sources. However, the analysis of calibration block observations revealed clear correlations of the internal source signals with the evaporator temperature and a signal drift during the first half hour after the cooler recycling. These effects are small, but can be seen in repeated measurements of standard stars. From our analysis we established corrections for both effects which push the stability of the PACS bolometer response to about 0.2% (stdev) or 2% in the blue, 3% in the green and 5% in the red channel (peak-to-peak). After both corrections we still see a correlation of the signals with PACS FPU temperatures, possibly caused by parasitic h...

  2. 48 CFR 908.7113 - Calibration services.

    Science.gov (United States)

    2010-10-01

    ... 48 Federal Acquisition Regulations System 5 2010-10-01 2010-10-01 false Calibration services. 908... ACQUISITION PLANNING REQUIRED SOURCES OF SUPPLIES AND SERVICES Acquisition of Special Items 908.7113 Calibration services. Orders for calibration services may be placed with the National Institute of...

  3. Net analyte signal calculation for multivariate calibration

    NARCIS (Netherlands)

    Ferre, J.; Faber, N.M.

    2003-01-01

    A unifying framework for calibration and prediction in multivariate calibration is shown based on the concept of the net analyte signal (NAS). From this perspective, the calibration step can be regarded as the calculation of a net sensitivity vector, whose length is the amount of net signal when the

  4. Reevaluation of dating results for some {sup 14}C - AMS applications on the basis of the new calibration curves available

    Energy Technology Data Exchange (ETDEWEB)

    Macario, K.D.; Gomes, P.R.S.; Anjos, R.M. [Universidade Federal Fluminense (UFF), Niteroi, RJ (Brazil). Inst. de Fisica

    2007-03-15

    In this paper we describe briefly some characteristics of the Accelerator Mass Spectrometry (AMS) technique and the need of corrections in the radiocarbon ages by specific calibration curves. Then we discuss previous results of some Brazilian projects where radiocarbon AMS had been applied in order to reevaluate the dates obtained on the basis of the new calibration curves available. (author)

  5. Rest mass or inertial mass?

    OpenAIRE

    Khrapko, R. I.

    2001-01-01

    Rest mass takes the place of inertial mass in modern physics textbooks. It seems to be wrong. But this phenomenon is hidden away by the facts that rest mass adherents busily call rest mass "mass", not rest mass, and the word "mass" is associated with a measure of inertia. This topic has been considered by the author in the article "What is mass?" [1, 2, 3]. Additional arguments to a confirmation of such a thesis are presented here.

  6. Calibration of a total body potassium monitor with an anthropomorphic phantom

    Science.gov (United States)

    Hansen, R. D.; Allen, B. J.

    1996-11-01

    An anthropomorphic phantom was used to calibrate a supine geometry sodium iodide total body potassium monitor. Correction factors accommodating variability in subject size were empirically determined. Measurements on 12 males of weight 45 - 96 kg, height 161 - 184 cm and 18 females of weight 48 - 89 kg, height 153 - 175 cm, showed that the calibration factor was significantly correlated (r = 0.88, p , indicating comparable accuracy to -based calibration procedures. Fat-free mass determined from the potassium measurements of 16 subjects correlated significantly with fat-free mass estimated from skinfold thickness (r = 0.98, p bioimpedance analysis (r = 0.98, p -based methods of calibrating total body potassium monitors.

  7. The Habitable-zone Planet Finder Calibration System

    CERN Document Server

    Halverson, Samuel; Ramsey, Lawrence; Terrien, Ryan; Roy, Arpita; Schwab, Christian; Bender, Chad; Hearty, Fred; Levi, Eric; Osterman, Steve; Ycas, Gabe; Diddams, Scott

    2014-01-01

    We present the design concept of the wavelength calibration system for the Habitable-zone Planet Finder instrument (HPF), a precision radial velocity (RV) spectrograph designed to detect terrestrial-mass planets around M-dwarfs. HPF is a stabilized, fiber-fed, R$\\sim$50,000 spectrograph operating in the near-infrared (NIR) z/Y/J bands from 0.84 to 1.3 microns. For HPF to achieve 1 m s$^{-1}$ or better measurement precision, a unique calibration system, stable to several times better precision, will be needed to accurately remove instrumental effects at an unprecedented level in the NIR. The primary wavelength calibration source is a laser frequency comb (LFC), currently in development at NIST Boulder, discussed separately in these proceedings. The LFC will be supplemented by a stabilized single-mode fiber Fabry-Perot interferometer reference source and Uranium-Neon lamp. The HPF calibration system will combine several other new technologies developed by the Penn State Optical-Infrared instrumentation group to...

  8. Development of Hydrocarbon Flow Calibration Facility as a National Standard

    Science.gov (United States)

    Shimada, Takashi; Doihara, Ryouji; Terao, Yoshiya; Takamoto, Masaki

    A new primary standard for hydrocarbon flow measurements has been constructed at National Metrology Institute of Japan (NMIJ). The facility was designed for the calibration of hydrocarbon flowmeters in the flow rate range between 3 and 300 m3/h. The expanded uncertainty is estimated to be 0.03 % for volumetric flow rate and 0.02 % for mass flow rate (coverage factor: k = 2). The primary standard is based on a static and gravimetric method with a flying start and finish. The facility consists of two test rigs using kerosene and light oil as working fluids. The test lines for the flowmeters are 50, 100 and 150 mm in diameter and three servo positive displacement meters are used as working standards. To verify the calibration performance, a Coriolis flowmeter, a turbine meter and a positive displacement flowmeter have been calibrated at both test rigs. Furthermore, an international comparison with SP, Swedish National Testing Research Institute, was carried out. A screw-type positive displacement flowmeter was selected as the transfer standard and was calibrated at NMIJ and SP. The result shows that the two national standards at the two institutes agree within the quoted expanded uncertainties.

  9. Numerical Analysis of a Radiant Heat Flux Calibration System

    Science.gov (United States)

    Jiang, Shanjuan; Horn, Thomas J.; Dhir, V. K.

    1998-01-01

    A radiant heat flux gage calibration system exists in the Flight Loads Laboratory at NASA's Dryden Flight Research Center. This calibration system must be well understood if the heat flux gages calibrated in it are to provide useful data during radiant heating ground tests or flight tests of high speed aerospace vehicles. A part of the calibration system characterization process is to develop a numerical model of the flat plate heater element and heat flux gage, which will help identify errors due to convection, heater element erosion, and other factors. A 2-dimensional mathematical model of the gage-plate system has been developed to simulate the combined problem involving convection, radiation and mass loss by chemical reaction. A fourth order finite difference scheme is used to solve the steady state governing equations and determine the temperature distribution in the gage and plate, incident heat flux on the gage face, and flat plate erosion. Initial gage heat flux predictions from the model are found to be within 17% of experimental results.

  10. Alignment of the Measurement Scale Mark during Immersion Hydrometer Calibration Using an Image Processing System

    Science.gov (United States)

    Peña-Perez, Luis Manuel; Pedraza-Ortega, Jesus Carlos; Ramos-Arreguin, Juan Manuel; Arriaga, Saul Tovar; Fernandez, Marco Antonio Aceves; Becerra, Luis Omar; Hurtado, Efren Gorrostieta; Vargas-Soto, Jose Emilio

    2013-01-01

    The present work presents an improved method to align the measurement scale mark in an immersion hydrometer calibration system of CENAM, the National Metrology Institute (NMI) of Mexico, The proposed method uses a vision system to align the scale mark of the hydrometer to the surface of the liquid where it is immersed by implementing image processing algorithms. This approach reduces the variability in the apparent mass determination during the hydrostatic weighing in the calibration process, therefore decreasing the relative uncertainty of calibration. PMID:24284770

  11. Calibration and validation of a model describing complete autotrophic nitrogen removal in a granular SBR system

    DEFF Research Database (Denmark)

    Vangsgaard, Anna Katrine; Mutlu, Ayten Gizem; Gernaey, Krist;

    2013-01-01

    steady-state in the biofilm system. For oxygen mass transfer coefficient (kLa) estimation, long-term data, removal efficiencies, and the stoichiometry of the reactions were used. For the dynamic calibration a pragmatic model fitting approach was used - in this case an iterative Monte Carlo based...... screening of the parameter space proposed by Sin et al. (2008) - to find the best fit of the model to dynamic data. Finally, the calibrated model was validated with an independent data set. CONCLUSION: The presented calibration procedure is the first customized procedure for this type of system and is...

  12. Muon Energy Calibration of the MINOS Detectors

    Energy Technology Data Exchange (ETDEWEB)

    Miyagawa, Paul S.

    2004-09-01

    MINOS is a long-baseline neutrino oscillation experiment designed to search for conclusive evidence of neutrino oscillations and to measure the oscillation parameters precisely. MINOS comprises two iron tracking calorimeters located at Fermilab and Soudan. The Calibration Detector at CERN is a third MINOS detector used as part of the detector response calibration programme. A correct energy calibration between these detectors is crucial for the accurate measurement of oscillation parameters. This thesis presents a calibration developed to produce a uniform response within a detector using cosmic muons. Reconstruction of tracks in cosmic ray data is discussed. This data is utilized to calculate calibration constants for each readout channel of the Calibration Detector. These constants have an average statistical error of 1.8%. The consistency of the constants is demonstrated both within a single run and between runs separated by a few days. Results are presented from applying the calibration to test beam particles measured by the Calibration Detector. The responses are calibrated to within 1.8% systematic error. The potential impact of the calibration on the measurement of oscillation parameters by MINOS is also investigated. Applying the calibration reduces the errors in the measured parameters by {approx} 10%, which is equivalent to increasing the amount of data by 20%.

  13. "Calibration-on-the-spot": How to calibrate an EMCCD camera from its images.

    Science.gov (United States)

    Mortensen, Kim I; Flyvbjerg, Henrik

    2016-07-06

    In order to count photons with a camera, the camera must be calibrated. Photon counting is necessary, e.g., to determine the precision of localization-based super-resolution microscopy. Here we present a protocol that calibrates an EMCCD camera from information contained in isolated, diffraction-limited spots in any image taken by the camera, thus making dedicated calibration procedures redundant by enabling calibration post festum, from images filed without calibration information.

  14. Calibration-on-the-spot”: How to calibrate an EMCCD camera from its images

    DEFF Research Database (Denmark)

    Mortensen, Kim; Flyvbjerg, Henrik

    2016-01-01

    In order to count photons with a camera, the camera must be calibrated. Photon counting is necessary, e.g., to determine the precision of localization-based super-resolution microscopy. Here we present a protocol that calibrates an EMCCD camera from information contained in isolated, diffraction......-limited spots in any image taken by the camera, thus making dedicated calibration procedures redundant by enabling calibration post festum, from images filed without calibration information....

  15. Calibration of the Cherenkov Telescope Array

    CERN Document Server

    Gaug, Markus; Berge, David; Reyes, Raquel de los; Doro, Michele; Foerster, Andreas; Maccarone, Maria Concetta; Parsons, Dan; van Eldik, Christopher

    2015-01-01

    The construction of the Cherenkov Telescope Array is expected to start soon. We will present the baseline methods and their extensions currently foreseen to calibrate the observatory. These are bound to achieve the strong requirements on allowed systematic uncertainties for the reconstructed gamma-ray energy and flux scales, as well as on the pointing resolution, and on the overall duty cycle of the observatory. Onsite calibration activities are designed to include a robust and efficient calibration of the telescope cameras, and various methods and instruments to achieve calibration of the overall optical throughput of each telescope, leading to both inter-telescope calibration and an absolute calibration of the entire observatory. One important aspect of the onsite calibration is a correct understanding of the atmosphere above the telescopes, which constitutes the calorimeter of this detection technique. It is planned to be constantly monitored with state-of-the-art instruments to obtain a full molecular and...

  16. Multi-Axis Accelerometer Calibration System

    Science.gov (United States)

    Finley, Tom; Parker, Peter

    2010-01-01

    A low-cost, portable, and simplified system has been developed that is suitable for in-situ calibration and/or evaluation of multi-axis inertial measurement instruments. This system overcomes facility restrictions and maintains or improves the calibration quality for users of accelerometer-based instruments with applications in avionics, experimental wind tunnel research, and force balance calibration applications. The apparatus quickly and easily positions a multi-axis accelerometer system into a precisely known orientation suitable for in-situ quality checks and calibration. In addition, the system incorporates powerful and sophisticated statistical methods, known as response surface methodology and statistical quality control. These methods improve calibration quality, reduce calibration time, and allow for increased calibration frequency, which enables the monitoring of instrument stability over time.

  17. MODIS Instrument Operation and Calibration Improvements

    Science.gov (United States)

    Xiong, X.; Angal, A.; Madhavan, S.; Link, D.; Geng, X.; Wenny, B.; Wu, A.; Chen, H.; Salomonson, V.

    2014-01-01

    Terra and Aqua MODIS have successfully operated for over 14 and 12 years since their respective launches in 1999 and 2002. The MODIS on-orbit calibration is performed using a set of on-board calibrators, which include a solar diffuser for calibrating the reflective solar bands (RSB) and a blackbody for the thermal emissive bands (TEB). On-orbit changes in the sensor responses as well as key performance parameters are monitored using the measurements of these on-board calibrators. This paper provides an overview of MODIS on-orbit operation and calibration activities, and instrument long-term performance. It presents a brief summary of the calibration enhancements made in the latest MODIS data collection 6 (C6). Future improvements in the MODIS calibration and their potential applications to the S-NPP VIIRS are also discussed.

  18. Protocols for calibrating multibeam sonar

    OpenAIRE

    Foote, Kenneth G.; Chu, Dezhang; Hammar, Terence R.; Baldwin, Kenneth C.; Mayer, Larry A.; Hufnagle, Lawrence C. jr.; Jech, J. Michael

    2005-01-01

    Development of protocols for calibrating multibeam sonar by means of the standard-target method is documented. Particular systems used in the development work included three that provide the water-column signals, namely the SIMRAD SM2000/90- and 200-kHz sonars and RESON SeaBat 8101 sonar, with operating frequency of 240 kHz. Two facilities were instrumented specifically for the work: a sea well at the Woods Hole Oceanographic Institution and a large, indoor freshwater tank at the University o...

  19. Calibration of TOB+ Thermometer's Cards

    CERN Document Server

    Banitt, Daniel

    2014-01-01

    Motivation - Under the new upgrade of the CMS detector the working temperature of the trackers had been reduced to -27 Celsius degrees. Though the thermal sensors themselves (Murata and Fenwal thermistors) are effective at these temperatures, the max1542 PLC (programmable logic controller) cards, interpreting the resistance of the thermal sensors into DC counts usable by the DCS (detector control system), are not designed for these temperatures in which the counts exceed their saturation and therefor had to be replaced. In my project I was in charge of handling the emplacement and calibration of the new PLC cards to the TOB (tracker outer barrel) control system.

  20. Mass analysis of cesium ion induced fragmentation of C/sub 60/

    International Nuclear Information System (INIS)

    Results of Cs ion induced C/sub 60/ fragmentation in source of negative ions by cesium sputtering (SNICS) from 5 MeV Tandem accelerator are presented. The mass analysis was performed from bending magnet. Mass spectra of C/sub 60/ fragments are compared with that of graphite under similar conditions. Yield of carbon clusters for both cases is plotted for Cs ion energy range of 2-5 keV. It is observed that heavier clusters appear in the case of C/sub 60/. Intensity of C/sub 2/ is much higher in comparison with other clusters for both C/sub 60/ and graphite due to difference in their bond energies. Prominence of C/sub 2/ yield confirms formation mechanism of C/sub 60/ by addition of C/sub 2/ route. (author)

  1. The. eta. -meson mass

    Energy Technology Data Exchange (ETDEWEB)

    Plouin, F.; Beurtey, R.; Boivin, M.; Milleret, G.; Nakach, A. (Lab. National Saturne, 91 - Gif-sur-Yvette (France)); Fleury, P. (Lab. de Physique Nucleaire et Hautes Energies, Ecole Polytechnique, 91 - Palaiseau (France)); Bachelier, D.; Boyard, J.L.; Hennino, T. (Inst. de Physique Nucleaire, 91 - Orsay (France)); Boudard, A.; Mayer, B. (DAPNIA/SPN, C.E. de Saclay, 91 - Gif-sur-Yvette (France)); Briscoe, W. (Dept. of Physics, George Washington Univ., Washington, DC (United States)); Kessler, R.; Nefkens, B.M.K.; Pillai, C.; Whitten, C. (Dept. of Physics, UCLA, Los Angeles, CA (United States)); Moalem, A. (Ben Gurion Univ. of the Negev, Beer Sheva (Israel)); Wilkin, C. (Univ. Coll. London (United Kingdom))

    1992-02-20

    The mass of the {eta} meson has been measured through the study of the dp{yields}{sup 3}He {eta} reaction near threshold, the beam having been calibrated through comparison with three other nuclear reactions. The value obtained is m{sub {eta}}=547.30{+-}0.15 MeV/c{sup 2}, where the error bar includes both systematic and statistical effects. This is much more precise and significantly lower than the Particle Data Group average, though it is consistent with a previous counter experiment. (orig.).

  2. Pulse-based internal calibration of polarimetric SAR

    DEFF Research Database (Denmark)

    Dall, Jørgen; Skou, Niels; Christensen, Erik Lintz

    1994-01-01

    Internal calibration greatly diminishes the dependence on calibration target deployment compared to external calibration. Therefore the Electromagnetics Institute (EMI) at the Technical University of Denmark (TUD) has equipped its polarimetric SAR, EMISAR, with several calibration loops and devel......Internal calibration greatly diminishes the dependence on calibration target deployment compared to external calibration. Therefore the Electromagnetics Institute (EMI) at the Technical University of Denmark (TUD) has equipped its polarimetric SAR, EMISAR, with several calibration loops...

  3. Input calibration for negative originals

    Science.gov (United States)

    Tuijn, Chris

    1995-04-01

    One of the major challenges in the prepress environment consists of controlling the electronic color reproduction process such that a perfect match of any original can be realized. Whether this goal can be reached depends on many factors such as the dynamic range of the input device (scanner, camera), the color gamut of the output device (dye sublimation printer, ink-jet printer, offset), the color management software etc. The characterization of the color behavior of the peripheral devices is therefore very important. Photographs and positive transparents reflect the original scene pretty well; for negative originals, however, there is no obvious link to either the original scene or a particular print of the negative under consideration. In this paper, we establish a method to scan negatives and to convert the scanned data to a calibrated RGB space, which is known colorimetrically. This method is based on the reconstruction of the original exposure conditions (i.e., original scene) which generated the negative. Since the characteristics of negative film are quite diverse, a special calibration is required for each combination of scanner and film type.

  4. MODIS solar reflective calibration traceability

    Science.gov (United States)

    Xiong, Xiaoxiong; Butler, Jim

    2009-08-01

    Long-term climate data records often consist of observations made by multiple sensors. It is, therefore, extremely important to have instrument overlap, to be able to track instrument stability, to quantify measurement uncertainties, and to establish an absolute measurement scale traceable to the International System of Units (SI). The Moderate Resolution Imaging Spectroradiometer (MODIS) is a key instrument for both the Terra and Aqua missions, which were launched in December 1999 and May 2002, respectively. It has 20 reflective solar bands (RSB) with wavelengths from 0.41 to 2.2μm and observes the Earth at three nadir spatial resolutions: 0.25km, 0.5km, and 1km. MODIS RSB on-orbit calibration is reflectance based with reference to the bi-directional reflectance factor (BRF) of its on-board solar diffuser (SD). The SD BRF characterization was made pre-launch by the instrument vendor using reference samples traceable directly to the National Institute of Standards and Technology (NIST). On-orbit SD reflectance degradation is tracked by an on-board solar diffuser stability monitor (SDSM). This paper provides details of this calibration chain, from pre-launch to on-orbit operation, and associated uncertainty assessments. Using MODIS as an example, this paper also discusses challenges and key design requirements for future missions developed for accurate climate studies.

  5. Crop physiology calibration in CLM

    Directory of Open Access Journals (Sweden)

    I. Bilionis

    2014-10-01

    Full Text Available Farming is using more terrestrial ground, as population increases and agriculture is increasingly used for non-nutritional purposes such as biofuel production. This agricultural expansion exerts an increasing impact on the terrestrial carbon cycle. In order to understand the impact of such processes, the Community Land Model (CLM has been augmented with a CLM-Crop extension that simulates the development of three crop types: maize, soybean, and spring wheat. The CLM-Crop model is a complex system that relies on a suite of parametric inputs that govern plant growth under a given atmospheric forcing and available resources. CLM-Crop development used measurements of gross primary productivity and net ecosystem exchange from AmeriFlux sites to choose parameter values that optimize crop productivity in the model. In this paper we calibrate these parameters for one crop type, soybean, in order to provide a faithful projection in terms of both plant development and net carbon exchange. Calibration is performed in a Bayesian framework by developing a scalable and adaptive scheme based on sequential Monte Carlo (SMC.

  6. MODIS Solar Reflective Calibration Traceability

    Science.gov (United States)

    Xiong, Xiaoxiong; Butler, Jim

    2009-01-01

    Long-term climate data records often consist of observations made by multiple sensors. It is, therefore, extremely important to have instrument overlap, to be able to track instrument stability, to quantify, measurement uncertainties, and to establish absolute scale traceable to the International System of Units (SI). The Moderate Resolution Imaging Spectroradiometer (MODIS) is a key instrument for both the Terra and Aqua missions, which were launched in December 1999 and May 2002, respectively. It has 20 reflective solar bands (RSB) with wavelengths from 0.41 to 2.2 micrometers and observes the Earth at three nadir spatial resolutions: 0.25km, 0.5km, and 1km. MODIS RSB on-orbit calibration is reflectance based with reference to the bidirectional reflectance factor (BRF) of its on-board solar diffuser (SD). The SD BRF characterization was made pre-launch by the instrument vendor using reference samples traceable directly to the National Institute of Standards and Technology (NIST). On-orbit SD reflectance degradation is tracked by an on-board solar diffuser monitor (SDSM). This paper provides details of this calibration chain, from prelaunch to on-orbit operation, and associated uncertainty assessments. Using MODIS as an example, this paper also discusses challenges and key design requirements for future missions developed for accurate climate studies.

  7. FCC-ee: Energy Calibration

    Energy Technology Data Exchange (ETDEWEB)

    Koratzinos, M. [Univ. of Geneva (Switzerland); Blondel, A. [Univ. of Geneva (Switzerland); Gianfelice-Wendt, E. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Zimmermann, F. [European Organization for Nuclear Research (CERN), Geneva (Switzerland)

    2015-06-02

    The FCC-ee aims to improve on electroweak precision measurements, with goals of 100 ke V on the Z mass and width, and a fraction of MeV on the W mass. Compared to LEP, this implies a much improved knowledge of the center-of-mass energy when operating at the Z peak and WW threshold. This can be achieved by making systematic use of resonant depolarization. A number of issues have been identified, due in particular to the long polarization times. However the smaller emittance and energy spread of FCC-ee with respect to LEP should help achieve a much improved performance.

  8. ATLAS jet and missing ET reconstruction, calibration, and performance

    CERN Document Server

    Berta, P; The ATLAS collaboration

    2014-01-01

    ATLAS has achieved a very high precision on jet and missing transverse energy performance by the use of advanced calorimeter-based topological clustering and local cluster calibration, event-by-event pile-up subtraction methods, and in situ techniques to correct for the residual jet energy response difference between data and simulation. Tracking information is being combined with calorimeter to further improve the jet and missing ET performance. ATLAS has also commissioned several new powerful tools for for the analysis and interpretation of hadronic final states at the LHC such as jet substructure, jet mass, quark-gluon discrimination, and jet tagging tools for the identification of boosted heavy particles. An overview of the reconstruction, calibration and performance of jets, missing ET, and jet substructure and tagging at ATLAS is presented.

  9. ATLAS jet and missing-ET reconstruction, calibration, and performance

    CERN Document Server

    Berta, P; The ATLAS collaboration

    2014-01-01

    The ATLAS experiment has achieved a very high precision on jet and missing transverse energy performance by the use of advanced calorimeter-based topological clustering and local cluster calibration, event-by-event pile-up subtraction methods, and in situ techniques to correct for the residual jet energy response difference between data and simulation. Tracking information is being combined with calorimeter to further improve the jet and missing transverse energy performance. ATLAS has also commissioned several new powerful tools for the analysis and interpretation of hadronic final states at the LHC such as jet substructure, jet mass, quark-gluon discrimination, and jet tagging tools for the identification of boosted heavy particles. An overview of the reconstruction, calibration, and performance of jets, missing transverse energy, jet substructure, and jet tagging at ATLAS is presented.

  10. Compton Backscattering for the Calibration of KEDR Tagging System

    CERN Document Server

    Kaminskiy, V V; Zhilich, V N

    2014-01-01

    KEDR detector has the tagging system (TS) to study the gamma-gamma processes. To determine the two-photon invariant mass, the energies of the scattered at small angles electrons and positrons are measured by the magnetic spectrometer embedded into the lattice of the VEPP--4M collider. The energy resolution (scattered electron/positron energy resolution divided by the beam energy) of this spectrometer varies from 0.6% to 0.03% depending on the electron/positron energy. The Compton backscattering of laser radiation on the electron/positron beam is used for the accurate energy scale and resolution calibration of the tagging system. The report covers the design, recent results and current status of the KEDR TS calibration system.

  11. Compton backscattering for the calibration of KEDR tagging system

    Science.gov (United States)

    Kaminskiy, V. V.; Muchnoi, N. Yu; Zhilich, V. N.

    2014-08-01

    KEDR detector has the tagging system (TS) to study the gamma-gamma processes. To determine the two-photon invariant mass, the energies of the scattered at small angles electrons and positrons are measured by the magnetic spectrometer embedded into the lattice of the VEPP-4M collider. The energy resolution (scattered electron/positron energy resolution divided by the beam energy) of this spectrometer varies from 0.6% to 0.03% depending on the electron/positron energy. The Compton backscattering of laser radiation on the electron/positron beam is used for the accurate energy scale and resolution calibration of the tagging system. The report covers the design, recent results and current status of the KEDR TS calibration system.

  12. Another look at volume self-calibration: calibration and self-calibration within a pinhole model of Scheimpflug cameras

    Science.gov (United States)

    Cornic, Philippe; Illoul, Cédric; Cheminet, Adam; Le Besnerais, Guy; Champagnat, Frédéric; Le Sant, Yves; Leclaire, Benjamin

    2016-09-01

    We address calibration and self-calibration of tomographic PIV experiments within a pinhole model of cameras. A complete and explicit pinhole model of a camera equipped with a 2-tilt angles Scheimpflug adapter is presented. It is then used in a calibration procedure based on a freely moving calibration plate. While the resulting calibrations are accurate enough for Tomo-PIV, we confirm, through a simple experiment, that they are not stable in time, and illustrate how the pinhole framework can be used to provide a quantitative evaluation of geometrical drifts in the setup. We propose an original self-calibration method based on global optimization of the extrinsic parameters of the pinhole model. These methods are successfully applied to the tomographic PIV of an air jet experiment. An unexpected by-product of our work is to show that volume self-calibration induces a change in the world frame coordinates. Provided the calibration drift is small, as generally observed in PIV, the bias on the estimated velocity field is negligible but the absolute location cannot be accurately recovered using standard calibration data.

  13. Research of Camera Calibration Based on DSP

    Directory of Open Access Journals (Sweden)

    Zheng Zhang

    2013-09-01

    Full Text Available To take advantage of the high-efficiency and stability of DSP in the data processing and the functions of OpenCV library, this study brought forward a scheme that camera calibration in DSP embedded system calibration. An arithmetic of camera calibration based on OpenCV is designed by analyzing the camera model and lens distortion. The transplantation of EMCV to DSP is completed and the arithmetic of camera calibration is migrated and optimized based on the CCS development environment and the DSP/BIOS system. On the premise of realizing calibration function, this arithmetic improves the efficiency of program execution and the precision of calibration and lays the foundation for further research of the visual location based on DSP embedded system.

  14. Absolute calibration in vivo measurement systems

    International Nuclear Information System (INIS)

    Lawrence Livermore National Laboratory (LLNL) is currently investigating a new method for obtaining absolute calibration factors for radiation measurement systems used to measure internally deposited radionuclides in vivo. Absolute calibration of in vivo measurement systems will eliminate the need to generate a series of human surrogate structures (i.e., phantoms) for calibrating in vivo measurement systems. The absolute calibration of in vivo measurement systems utilizes magnetic resonance imaging (MRI) to define physiological structure, size, and composition. The MRI image provides a digitized representation of the physiological structure, which allows for any mathematical distribution of radionuclides within the body. Using Monte Carlo transport codes, the emission spectrum from the body is predicted. The in vivo measurement equipment is calibrated using the Monte Carlo code and adjusting for the intrinsic properties of the detection system. The calibration factors are verified using measurements of existing phantoms and previously obtained measurements of human volunteers. 8 refs

  15. Herschel SPIRE FTS Relative Spectral Response Calibration

    CERN Document Server

    Fulton, Trevor; Baluteau, Jean-Paul; Benielli, Dominique; Imhof, Peter; Lim, Tanya; Lu, Nanyao; Marchili, Nicola; Naylor, David; Polehampton, Edward; Swinyard, Bruce; Valtchanov, Ivan

    2014-01-01

    Herschel/SPIRE Fourier transform spectrometer (FTS) observations contain emission from both the Herschel Telescope and the SPIRE Instrument itself, both of which are typically orders of magnitude greater than the emission from the astronomical source, and must be removed in order to recover the source spectrum. The effects of the Herschel Telescope and the SPIRE Instrument are removed during data reduction using relative spectral response calibration curves and emission models. We present the evolution of the methods used to derive the relative spectral response calibration curves for the SPIRE FTS. The relationship between the calibration curves and the ultimate sensitivity of calibrated SPIRE FTS data is discussed and the results from the derivation methods are compared. These comparisons show that the latest derivation methods result in calibration curves that impart a factor of between 2 and 100 less noise to the overall error budget, which results in calibrated spectra for individual observations whose n...

  16. Biogeographic calibrations for the molecular clock.

    Science.gov (United States)

    Ho, Simon Y W; Tong, K Jun; Foster, Charles S P; Ritchie, Andrew M; Lo, Nathan; Crisp, Michael D

    2015-09-01

    Molecular estimates of evolutionary timescales have an important role in a range of biological studies. Such estimates can be made using methods based on molecular clocks, including models that are able to account for rate variation across lineages. All clock models share a dependence on calibrations, which enable estimates to be given in absolute time units. There are many available methods for incorporating fossil calibrations, but geological and climatic data can also provide useful calibrations for molecular clocks. However, a number of strong assumptions need to be made when using these biogeographic calibrations, leading to wide variation in their reliability and precision. In this review, we describe the nature of biogeographic calibrations and the assumptions that they involve. We present an overview of the different geological and climatic events that can provide informative calibrations, and explain how such temporal information can be incorporated into dating analyses.

  17. Calibration biases in logical reasoning tasks

    OpenAIRE

    Guillermo Macbeth; Alfredo López Alonso; Eugenia Razumiejczyk; Rodrigo Sosa; Carolina Pereyra; Humberto Fernández

    2013-01-01

    The aim of this contribution is to present an experimental study about calibration in deductive reasoning tasks. Calibration is defi ned as the empirical convergence or divergence between the objective and the subjective success. The underconfi dence bias is understood as the dominance of the former over the latter. The hypothesis of this study states that the form of the propositions presented in the experiment is critical for calibration phenomena. Affi rmative and negative propositions are...

  18. Calibration Procedure for 3D Turning Dynamometer

    DEFF Research Database (Denmark)

    Axinte, Dragos Aurelian; Belluci, Walter

    1999-01-01

    The aim of the static calibration of the dynamometer is to obtain the matrix for evaluating cutting forces through the output voltage of the piezoelectric cells and charge amplifiers. In the same time, it is worth to evaluate the linearity of the dependencies between applied forces and output...... of the piezoelectric cells;5. Mounting of the dynamometer;6. Calibration of the dynamometer;7. Data analysis;8. Uncertainty budget of the calibration....

  19. Calibration of Nacelle-based Lidar instrument

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Courtney, Michael

    This report presents the result of the lidar calibration performed for a two-beam nacelle based lidar at DTU’s test site for large wind turbines at Høvsøre, Denmark. Calibration is here understood as the establishment of a relation between the reference wind speed measurements with measurement...... uncertainties provided by measurement standard and corresponding lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements....

  20. 1987 calibration of the TFTR neutron spectrometers

    Energy Technology Data Exchange (ETDEWEB)

    Barnes, C.W.; Strachan, J.D. (Los Alamos National Lab., NM (USA); Princeton Univ., NJ (USA). Plasma Physics Lab.)

    1989-12-01

    The {sup 3}He neutron spectrometer used for measuring ion temperatures and the NE213 proton recoil spectrometer used for triton burnup measurements were absolutely calibrated with DT and DD neutron generators placed inside the TFTR vacuum vessel. The details of the detector response and calibration are presented. Comparisons are made to the neutron source strengths measured from other calibrated systems. 23 refs., 19 figs., 6 tabs.

  1. Radiocarbon calibration - past, present and future

    Energy Technology Data Exchange (ETDEWEB)

    Plicht, J. van der E-mail: plicht@phys.rug.nl

    2004-08-01

    Calibration of the Radiocarbon timescale is traditionally based on tree-rings dated by dendrochronology. At present, the tree-ring curve dates back to about 9900 BC. Beyond this limit, marine datasets extend the present calibration curve INTCAL98 to about 15 600 years ago. Since 1998, a wealth of AMS measurements became available, covering the complete {sup 14}C dating range. No calibration curve can presently be recommended for the older part of the dating range until discrepancies are resolved.

  2. Axino mass

    CERN Document Server

    Kim, Jihn E

    2012-01-01

    I will talk on my recent works. Axino, related to the SUSY transformation of axion, can mix with Goldstino in principle. In this short talk, I would like to explain what is the axino mass and its plausible mass range. The axino mass is known to have a hierarchical mass structure depending on accidental symmetries. With only one axino, if G_A=0 where G=K+ 2ln|W|, we obtain axino mass= gravitino mass. For G_A nonzero, the axino mass depends on the details of the Kaehler potential. I also comment on the usefulness of a new parametrization of the CKM matrix.

  3. Traveling-wave ion mobility mass spectrometry of protein complexes

    DEFF Research Database (Denmark)

    Salbo, Rune; Bush, Matthew F; Naver, Helle;

    2012-01-01

    The collision cross-section (Ω) of a protein or protein complex ion can be measured using traveling-wave (T-wave) ion mobility (IM) mass spectrometry (MS) via calibration with compounds of known Ω. The T-wave Ω-values depend strongly on instrument parameters and calibrant selection. Optimization of...

  4. MULTIPLE ELECTRONIC CONTROL UNITS CALIBRATION SYSTEM BASED ON EXPLICIT CALIBRATION PROTOCOL AND J1939 PROTOCOL

    Institute of Scientific and Technical Information of China (English)

    YANG Shiwei; ZHU Keqing; XU Quankui; YANG Lin; ZHUO Bin

    2008-01-01

    The rising number of electronic control units (ECUs) in vehicles and the decreasing time to market have led to the need for advanced methods of calibration. A multi-ECU calibration system was developed based on the explicit calibration protocol (XCP) and J1939 communication protocol to satisfy the need of calibrating multiple ECUs simultaneously. The messages in the controller area network (CAN) are defined in the J1939 protocol. Each CAN node can get its own calibration messages and information from other ECUs, and block other messages by qualifying the CAN messages with priority, source or destination address. The data field of the calibration message is designed with the XCP , with CAN acting as the transport layer. The calibration sessions are setup with the event-triggered XCP driver in the master node and the responding XCP driver in the slave nodes. Mirroring calibration variables from ROM to RAM enables the user to calibrate ECUs online. The application example shows that the multi-ECU calibration system can calibrate multiple ECUs simultaneously, and the main program can also accomplish its calculation and send commands to the actuators in time. By the multi-ECU calibration system, the calibration effort and time can be reduced and the variables in ECU can get a better match with the variables of other ECUs.

  5. Efficiency calibration of low background gamma spectrometer

    International Nuclear Information System (INIS)

    A method of efficiency calibration is described. The authors used standard ores of U, Ra and Th (power form), KCl and Cs-137 sources to do calibration volume-sources which were directly placed on the detector end cap. In such a measuring geometry, it is not necessary to make coincidence-summing correction. The efficiency calibration curve obtained by the method were compared with results measured by Am-241, Cd-109 and Eu-152 calibration sources. The agree in the error of about 5%

  6. Calibration metrology for fixed irradiation sensors

    International Nuclear Information System (INIS)

    After having recalled the regulatory and technical framework of the calibration of radioprotection measurement instruments, and outlined some technical and operational constraints, the authors report the development of an in situ calibration methodology, i.e. without displacement of the sensor. After the presentation of the calibration chain (from the measurement given by a fixed sensor to the reference value given by a primary standard), they indicate the definition and calculation of the different calibration coefficients allowing the linking up of the different levels, and also the taking of uncertainties into account. They finally report the validation of results

  7. Research of Camera Calibration Based on DSP

    OpenAIRE

    Zheng Zhang; Yukun Wan; Lixin Cai

    2013-01-01

    To take advantage of the high-efficiency and stability of DSP in the data processing and the functions of OpenCV library, this study brought forward a scheme that camera calibration in DSP embedded system calibration. An arithmetic of camera calibration based on OpenCV is designed by analyzing the camera model and lens distortion. The transplantation of EMCV to DSP is completed and the arithmetic of camera calibration is migrated and optimized based on the CCS development environment and the ...

  8. Sloan Digital Sky Survey Photometric Calibration Revisited

    Energy Technology Data Exchange (ETDEWEB)

    Marriner, John; /Fermilab

    2012-06-29

    The Sloan Digital Sky Survey calibration is revisited to obtain the most accurate photometric calibration. A small but significant error is found in the flat-fielding of the Photometric telescope used for calibration. Two SDSS star catalogs are compared and the average difference in magnitude as a function of right ascension and declination exhibits small systematic errors in relative calibration. The photometric transformation from the SDSS Photometric Telescope to the 2.5 m telescope is recomputed and compared to synthetic magnitudes computed from measured filter bandpasses.

  9. FY2008 Calibration Systems Final Report

    Energy Technology Data Exchange (ETDEWEB)

    Cannon, Bret D.; Myers, Tanya L.; Broocks, Bryan T.

    2009-01-01

    The Calibrations project has been exploring alternative technologies for calibration of passive sensors in the infrared (IR) spectral region. In particular, we have investigated using quantum cascade lasers (QCLs) because these devices offer several advantages over conventional blackbodies such as reductions in size and weight while providing a spectral source in the IR with high output power. These devices can provide a rapid, multi-level radiance scheme to fit any nonlinear behavior as well as a spectral calibration that includes the fore-optics, which is currently not available for on-board calibration systems.

  10. Absolute calibration of the Auger fluorescence detectors

    Energy Technology Data Exchange (ETDEWEB)

    Bauleo, P.; Brack, J.; Garrard, L.; Harton, J.; Knapik, R.; Meyhandan, R.; Rovero, A.C.; /Buenos Aires, IAFE; Tamashiro, A.; Warner, D.

    2005-07-01

    Absolute calibration of the Pierre Auger Observatory fluorescence detectors uses a light source at the telescope aperture. The technique accounts for the combined effects of all detector components in a single measurement. The calibrated 2.5 m diameter light source fills the aperture, providing uniform illumination to each pixel. The known flux from the light source and the response of the acquisition system give the required calibration for each pixel. In the lab, light source uniformity is studied using CCD images and the intensity is measured relative to NIST-calibrated photodiodes. Overall uncertainties are presently 12%, and are dominated by systematics.

  11. Sloan Digital Sky Survey Photometric Calibration Revisited

    Science.gov (United States)

    Marriner, J.

    2016-05-01

    The Sloan Digital Sky Survey calibration is revisited to obtain the most accurate photometric calibration. A small but significant error is found in the flat-fielding of the Photometric telescope used for calibration. Two SDSS star catalogs are compared and the average difference in magnitude as a function of right ascension and declination exhibits small systematic errors in relative calibration. The photometric transformation from the SDSS Photometric Telescope to the 2.5 m telescope is recomputed and compared to synthetic magnitudes computed from measured filter bandpasses.

  12. Calibration services for medical applications of radiation

    Energy Technology Data Exchange (ETDEWEB)

    DeWerd, L.A.

    1993-12-31

    Calibration services for the medical community applications of radiation involve measuring radiation precisely and having traceability to the National Institute of Standards and Technology (NIST). Radiation therapy applications involve the use of ionization chambers and electrometers for external beams and well-type ionization chamber systems as well as radioactive sources for brachytherapy. Diagnostic x-ray applications involve ionization chamber systems and devices to measure other parameters of the x-ray machine, such as non-invasive kVp meters. Calibration laboratories have been established to provide radiation calibration services while maintaining traceability to NIST. New radiation applications of the medical community spur investigation to provide the future calibration needs.

  13. KINIK, Absorber Rod Calibration Kinetics

    International Nuclear Information System (INIS)

    1 - Description of program or function: KINIK is an inverse kinetic code that solves the inverse form of the point kinetic equations using the Runge-Kutta method. An optimization procedure is involved to control the time step and to reduce the running time. Up to 24 delayed neutron groups of different types (in case of heavy water as moderator or beryllium as reflector) are considered. KINIK is commonly applied to determine reactivity worths and to calibrate absorber rods. Following a rod drop, neutron flux or power is recorded as a function of time and used as input. 2 - Method of solution: The inverse point kinetic equations are numerically solved for each time step using the Runge-Kutta method. The input data resulting from measurements are first approximated by polynomials of maximum degree 10 using a least-squares approach

  14. Whole-body detector calibrating with a modular phantom

    International Nuclear Information System (INIS)

    Human body models (phantoms) of various size and weight are produced in order to calibrate gamma spectrometers for accurate activity measurement. The phantoms are built of separate modules with mass of 0.5 kg and size 20 x 14 x 2 cm. There are modules with standard Eu-152 and Am-241 radioactivity designed for homogenous radioactivity imitating and critical organs moulding, as well as 'zero' -phantom modules without activity imitating a standard human body. Human organs are modelled by 11 x 9 x 0.5 cm modules with 0.16 kg mass. The phantoms have been used to obtain calibration curves and absolute efficiencies for selected energies of radionuclides expected to be found in the Kozloduy NPP staff. It is shown that the efficiency depends not only on the mass but on the geometric size of the measured object. Scanning of phantoms has been carried out and a profile of activity obtained. The profile consists of an abrupt rising of the sum of pulses (measuring time - 20 s) when the detector passes from neck to chest, a plateau when it moves over the head or the trunk and gradual decrease over the legs. Profiles of activity in organs are best obtained with a lead collimator. 4 refs., 7 figs., 2 tabs

  15. Clustered Calibration: An Improvement to Radio Interferometric Direction Dependent Self-Calibration

    CERN Document Server

    Kazemi, Sanaz; Zaroubi, Saleem

    2013-01-01

    The new generation of radio synthesis arrays, such as LOFAR and SKA, have been designed to surpass existing arrays in terms of sensitivity, angular resolution and frequency coverage. This evolution has led to the development of advanced calibration techniques that ensure the delivery of accurate results at the lowest possible computational cost. However, the performance of such calibration techniques is still limited by the compact, bright sources in the sky, used as calibrators. It is important to have a bright enough source that is well distinguished from the background noise level in order to achieve satisfactory results in calibration. We present "clustered calibration" as a modification to traditional radio interferometric calibration, in order to accommodate faint sources that are almost below the background noise level into the calibration process. The main idea is to employ the information of the bright sources' measured signals as an aid to calibrate fainter sources that are nearby the bright sources...

  16. Design and Calibration of a Cryogenic Blackbody Calibrator at Centimeter Wavelengths

    CERN Document Server

    Kogut, A J; Fixsen, D J; Limon, M; Mirel, P G A; Levin, S; Seiffert, M; Lubin, P M

    2004-01-01

    We describe the design and calibration of an external cryogenic blackbody calibrator used for the first two flights of the Absolute Radiometer for Cosmology, Astrophysics, and Diffuse Emission (ARCADE) instrument. The calibrator consists of a microwave absorber weakly coupled to a superfluid liquid helium bath. Half-wave corrugations viewed 30 deg off axis reduce the return loss below -35 dB. Ruthenium oxide resistive thermometers embedded within the absorber monitor the temperature across the face of the calibrator. The thermal calibration transfers the calibration of a reference thermometer to the flight thermometers using the flight thermometer readout system. Data taken near the superfluid transition in 8 independent calibrations 4 years apart agree within 0.3 mK, providing an independent verification of the thermometer calibration at temperatures near that of the cosmic microwave background.

  17. The physical principles of XRF calibrations

    International Nuclear Information System (INIS)

    Full text: XRF Control and calibration software has come a long way in recent years. Advances in the multiple regression software sophistication and speed of computers have provided an essential resource to the XRF analyst. Over recent years there has been a trend amongst some analysts to develop XRF calibrations based exclusively on the statistical information given by calibration software. Multiple regression statistics are designed for non-correlated data sets but give unpredictable results if there are significant correlations in the standards used. This is typical for calibrations weighted towards certified reference materials (CRM's) which, being natural materials, contain correlated concentrations. Purely statistical methods in calibration development have applicability only over very short concentration ranges and for materials whose composition varies little. Beyond these ranges, the calibration has the potential to be unstable and has been known to produce significant deviations in analysis of unknown samples. The statistical information generated during XRF calibrations can be a very useful tool when used in conjunction with knowledge of the physics behind the correction factors applied. The matrix coefficients represent physical absorption/enhancement effects within the sample and are not arbitrary numbers used to get a good fit to the calibration line. Inappropriate use of matrix factors and overlap factors can produce low RMS values but erroneous results in unknown samples. This talk will contain examples to demonstrate hazards with different calibration strategies and will include coverage of the following topics: physical effects occurring within the sample as a result of X-ray irradiation; use of multiple regression statistics and what role it plays in the calibration; calibration strategies using synthetic and CRM standards; determining appropriate theoretical and semi-empirical matrix corrections and line overlap factors. Copyright (1999

  18. A simple algorithm improves mass accuracy to 50-100 ppm for delayed extraction linear MALDI-TOF mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Hack, Christopher A.; Benner, W. Henry

    2001-10-31

    A simple mathematical technique for improving mass calibration accuracy of linear delayed extraction matrix assisted laser desorption ionization time-of-flight mass spectrometry (DE MALDI-TOF MS) spectra is presented. The method involves fitting a parabola to a plot of Dm vs. mass data where Dm is the difference between the theoretical mass of calibrants and the mass obtained from a linear relationship between the square root of m/z and ion time of flight. The quadratic equation that describes the parabola is then used to correct the mass of unknowns by subtracting the deviation predicted by the quadratic equation from measured data. By subtracting the value of the parabola at each mass from the calibrated data, the accuracy of mass data points can be improved by factors of 10 or more. This method produces highly similar results whether or not initial ion velocity is accounted for in the calibration equation; consequently, there is no need to depend on that uncertain parameter when using the quadratic correction. This method can be used to correct the internally calibrated masses of protein digest peaks. The effect of nitrocellulose as a matrix additive is also briefly discussed, and it is shown that using nitrocellulose as an additive to a CHCA matrix does not significantly change initial ion velocity but does change the average position of ions relative to the sample electrode at the instant the extraction voltage is applied.

  19. AXAF calibration: the HXDS flow proportional counters

    Science.gov (United States)

    Wargelin, Bradford J.; Kellogg, Edwin M.; McDermott, Walter C.; Evans, Ian N.; Vitek, S. A.

    1997-07-01

    The design, performance, and calibration of the seven flow proportional counters (FPCs) used during AXAF ground calibration are described. Five of the FPCs served as beam normalization detectors (BNDs), and two were used in the telescope focal plane in combination with a set of apertures to measure the point response functions and effective areas of the AXAF mirrors and transmission gratings. The BNDs also provide standards for determining the effective areas of the several telescope/grating/flight-detector combinations. With useful energy resolution and quantum efficiency over the entire 100-eV to 10 keV AXAF energy band, the FPCs provided most of the data acquired during AXAF calibration. Although the principles of proportional counter operation are relatively simple, AXAF's stringent calibration goals require detailed calibration and modeling of such effects as window- support-wire obscuration, window deformation between the support wires, electron diffusion and avalanche processes, gain nonuniformities, and gas pressure and temperature variations. Detector aperture areas and signal processing deadtime must also be precisely determined, and detector degradation during the many months of AXAF calibration must be prevented. The FPC calibration program is based on measurement of individual components (such as window transmission and aperture size) and the relative quantum efficiencies of complete detector systems, as well as absolute QE calibration of selected detectors at the BESSY synchrotron, an x-ray source of precisely known intensity.

  20. Planck 2013 results. V. LFI calibration

    DEFF Research Database (Denmark)

    Planck Collaboration,; Aghanim, N.; Armitage-Caplan, C.;

    2014-01-01

    We discuss the methods employed to photometrically calibrate the data acquired by the Low Frequency Instrument on Planck. Our calibration is based on the Solar Dipole, caused by motion of the Solar System with respect to the CMB rest frame, which provides a signal of a few mK with the same spectr...

  1. Sky camera geometric calibration using solar observations

    Science.gov (United States)

    Urquhart, Bryan; Kurtz, Ben; Kleissl, Jan

    2016-09-01

    A camera model and associated automated calibration procedure for stationary daytime sky imaging cameras is presented. The specific modeling and calibration needs are motivated by remotely deployed cameras used to forecast solar power production where cameras point skyward and use 180° fisheye lenses. Sun position in the sky and on the image plane provides a simple and automated approach to calibration; special equipment or calibration patterns are not required. Sun position in the sky is modeled using a solar position algorithm (requiring latitude, longitude, altitude and time as inputs). Sun position on the image plane is detected using a simple image processing algorithm. The performance evaluation focuses on the calibration of a camera employing a fisheye lens with an equisolid angle projection, but the camera model is general enough to treat most fixed focal length, central, dioptric camera systems with a photo objective lens. Calibration errors scale with the noise level of the sun position measurement in the image plane, but the calibration is robust across a large range of noise in the sun position. Calibration performance on clear days ranged from 0.94 to 1.24 pixels root mean square error.

  2. Optimal, Reliability-Based Code Calibration

    DEFF Research Database (Denmark)

    Sørensen, John Dalsgaard

    2002-01-01

    Reliability based code calibration is considered in this paper. It is described how the results of FORM based reliability analysis may be related to the partial safety factors and characteristic values. The code calibration problem is presented in a decision theoretical form and it is discussed how...

  3. Lidar to lidar calibration phase 2

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Courtney, Michael

    This report presents the results from phase 2 of a lidar to lidar (L2L) calibration procedure. Phase two of the project included two measurement campaigns conducted at given sites. The purpose was to find out if the lidar-to-lidar calibration procedure can be conducted with similar results...

  4. The long term stability of lidar calibrations

    DEFF Research Database (Denmark)

    Courtney, Michael; Gayle Nygaard, Nicolai

    Wind lidars are now used extensively for wind resource measurements. One of the requirements for the data to be accepted in support of project financing (so-called ‘banka-bility’) is to demonstrate the long-term stability of lidar cali-brations. Calibration results for six Leosphere WindCube li...

  5. Microfabricated field calibration assembly for analytical instruments

    Science.gov (United States)

    Robinson, Alex L.; Manginell, Ronald P.; Moorman, Matthew W.; Rodacy, Philip J.; Simonson, Robert J.

    2011-03-29

    A microfabricated field calibration assembly for use in calibrating analytical instruments and sensor systems. The assembly comprises a circuit board comprising one or more resistively heatable microbridge elements, an interface device that enables addressable heating of the microbridge elements, and, in some embodiments, a means for positioning the circuit board within an inlet structure of an analytical instrument or sensor system.

  6. 14 CFR 33.45 - Calibration tests.

    Science.gov (United States)

    2010-01-01

    ... Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Block Tests; Reciprocating Aircraft Engines § 33.45 Calibration tests. (a) Each engine must be subjected to the calibration tests necessary to establish its power characteristics...

  7. Calibration of Ground-based Lidar instrument

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Gómez Arranz, Paula

    This report presents the result of the lidar calibration performed for the given Ground-based Lidar at DTU’s test site for large wind turbines at Høvsøre, Denmark. Calibration is here understood as the establishment of a relation between the reference wind speed measurements with measurement unce...

  8. Calibration of Nacelle-based Lidar instrument

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Courtney, Michael

    This report presents the result of the lidar calibration performed for a two-beam nacelle based lidar at DTU’s test site for large wind turbines at Høvsøre, Denmark. Calibration is here understood as the establishment of a relation between the reference wind speed measurements with measurement un...

  9. Radiocarbon calibration - past, present and future

    NARCIS (Netherlands)

    van der Plicht, J

    2004-01-01

    Calibration of the Radiocarbon timescale is traditionally based on tree-rings dated by dendrochronology. At present, the tree-ring curve dates back to about 9900 BC. Beyond this limit, marine datasets extend the present calibration curve INTCAL98 to about 15600 years ago. Since 1998, a wealth of AMS

  10. Building X-ray Diffraction Calibration Software

    Energy Technology Data Exchange (ETDEWEB)

    Lande, Joshua; /Marlboro Coll.

    2007-10-31

    X-ray diffraction is a technique used to analyze the structure of crystals. It records the interference pattern created when x-rays travel through a crystal. Three dimensional structure can be inferred from these two dimensional diffraction patterns. Before the patterns can be analyzed, diffraction data must be precisely calibrated. Calibration is used to determine the experimental parameters of the particular experiment. This is done by fitting the experimental parameters to the diffraction pattern of a well understood crystal. Fit2D is a software package commonly used to do this calibration but it leaves much to be desired. In particular, it does not give very much control over the calibration of the data, requires a significant amount of manual input, does not allow for the calibration of highly tilted geometries, does not properly explain the assumptions that it is making, and cannot be modified. We build code to do this calibration while at the same time overcoming the limitations of Fit2D. This paper describes the development of the calibration software and the assumptions that are made in doing the calibration.

  11. Astronomical calibration of the Maastrichtian (Late Cretaceous)

    DEFF Research Database (Denmark)

    Husson, Dorothée; Galbrun, Bruno; Laskar, Jacques;

    2011-01-01

    Recent improvements to astronomical modeling of the Solar System have contributed to important refinements of the Cenozoic time scale through astronomical calibration of sedimentary series. We extend this astronomical calibration into the Cretaceous, on the base of the 405 ka orbital eccentricity...

  12. Stellar mass -- halo mass relation and star formation efficiency in high-mass halos

    CERN Document Server

    Kravtsov, Andrey; Meshscheryakov, Alexander

    2014-01-01

    We study relation between stellar mass and halo mass for high-mass halos using a sample of galaxy clusters with accurate measurements of stellar masses from optical and IR data and total masses from X-ray observations. We find that stellar mass of the brightest cluster galaxies (BCGs) scales as M*BCG\\propto M500^a_BCG with the best fit slope of a_BCG~0.35+-0.1 and scatter of M*BCG at a fixed M500 of ~0.2 dex. We show that M*-M relations from abundance matching or halo modelling reported in recent studies underestimate stellar masses of BCGs by a factor of ~2-4, because these studies used stellar mass functions (SMF) based on photometry that severely underestimates the outer surface brightness profiles of massive galaxies. We show that M*-M relation derived using abundance matching with the recent SMF calibration by Bernardi et al. (2013) based on improved photometry is in a much better agreement with the relation we derive. The total stellar mass of galaxies correlates with total mass M500 with the slope of \\...

  13. DECal: A Spectrophotometric Calibration System For DECam

    CERN Document Server

    Marshall, J L; DePoy, D L; Prochaska, Travis; Allen, Richard; Behm, Tyler W; Martin, Emily C; Veal, Brannon; Villanueva,, Steven; Williams, Patrick; Wise, Jason

    2013-01-01

    DECal is a new calibration system for the CTIO 4 m Blanco telescope. It is currently being installed as part of the Dark Energy Survey and will provide both broadband flat fields and narrowband (about 1 nm bandwidth) spectrophotometric calibration for the new Dark Energy Camera (DECam). Both of these systems share a new Lambertian flat field screen. The broadband flat field system uses LEDs to illuminate each photometric filter. The spectrophotometric calibration system consists of a monochromator-based tunable light source that is projected onto the flat field screen using a custom line-to-spot fiber bundle and an engineered diffuser. Several calibrated photodiodes positioned along the beam monitor the telescope throughput as a function of wavelength. This system will measure the wavelength-dependent instrumental response function of the total telescope+instrument system in the range 300 < lambda < 1100nm. The spectrophotometric calibration will be performed regularly (roughly once per month) to determ...

  14. Systems and methods of eye tracking calibration

    DEFF Research Database (Denmark)

    2014-01-01

    Methods and systems to facilitate eye tracking control calibration are provided. One or more objects are displayed on a display of a device, where the one or more objects are associated with a function unrelated to a calculation of one or more calibration parameters. The one or more calibration...... parameters relate to a calibration of a calculation of gaze information of a user of the device, where the gaze information indicates where the user is looking. While the one or more objects are displayed, eye movement information associated with the user is determined, which indicates eye movement of one...... or more eye features associated with at least one eye of the user. The eye movement information is associated with a first object location of the one or more objects. The one or more calibration parameters are calculated based on the first object location being associated with the eye movement information....

  15. Parallel Calibration for Sensor Array Radio Interferometers

    CERN Document Server

    Brossard, Martin; Pesavento, Marius; Boyer, Rémy; Larzabal, Pascal; Wijnholds, Stefan J

    2016-01-01

    In order to meet the theoretically achievable imaging performance, calibration of modern radio interferometers is a mandatory challenge, especially at low frequencies. In this perspective, we propose a novel parallel iterative multi-wavelength calibration algorithm. The proposed algorithm estimates the apparent directions of the calibration sources, the directional and undirectional complex gains of the array elements and their noise powers, with a reasonable computational complexity. Furthermore, the algorithm takes into account the specific variation of the aforementioned parameter values across wavelength. Realistic numerical simulations reveal that the proposed scheme outperforms the mono-wavelength calibration scheme and approaches the derived constrained Cram\\'er-Rao bound even with the presence of non-calibration sources at unknown directions, in a computationally efficient manner.

  16. Dutch X-band SLAR calibration

    Science.gov (United States)

    Groot, J. S.

    1990-01-01

    In August 1989 the NASA/JPL airborne P/L/C-band DC-8 SAR participated in several remote sensing campaigns in Europe. Amongst other test sites, data were obtained of the Flevopolder test site in the Netherlands on August the 16th. The Dutch X-band SLAR was flown on the same date and imaged parts of the same area as the SAR. To calibrate the two imaging radars a set of 33 calibration devices was deployed. 16 trihedrals were used to calibrate a part of the SLAR data. This short paper outlines the X-band SLAR characteristics, the experimental set-up and the calibration method used to calibrate the SLAR data. Finally some preliminary results are given.

  17. The ATLAS Electromagnetic Calorimeter Calibration Workshop

    CERN Multimedia

    Hong Ma; Isabelle Wingerter

    The ATLAS Electromagnetic Calorimeter Calibration Workshop took place at LAPP-Annecy from the 1st to the 3rd of October; 45 people attended the workshop. A detailed program was setup before the workshop. The agenda was organised around very focused presentations where questions were raised to allow arguments to be exchanged and answers to be proposed. The main topics were: Electronics calibration Handling of problematic channels Cluster level corrections for electrons and photons Absolute energy scale Streams for calibration samples Calibration constants processing Learning from commissioning Forty-five people attended the workshop. The workshop was on the whole lively and fruitful. Based on years of experience with test beam analysis and Monte Carlo simulation, and the recent operation of the detector in the commissioning, the methods to calibrate the electromagnetic calorimeter are well known. Some of the procedures are being exercised in the commisssioning, which have demonstrated the c...

  18. Calibration biases in logical reasoning tasks

    Directory of Open Access Journals (Sweden)

    Guillermo Macbeth

    2013-08-01

    Full Text Available The aim of this contribution is to present an experimental study about calibration in deductive reasoning tasks. Calibration is defi ned as the empirical convergence or divergence between the objective and the subjective success. The underconfi dence bias is understood as the dominance of the former over the latter. The hypothesis of this study states that the form of the propositions presented in the experiment is critical for calibration phenomena. Affi rmative and negative propositions are distinguished in their cognitive processing. Results suggests that monotonous compound propositions are prone to underconfi dence. An heuristic approach to this phenomenon is proposed. The activation of a monotony heuristic would produce an illusion of simplicity that generates the calibration bias. These evidence is analysed in the context of the metacognitive modeling of calibration phenomena.

  19. Assessing students' metacognitive calibration with knowledge surveys

    Science.gov (United States)

    Lindsey, Beth A.; Nagel, Megan

    2013-01-01

    "Calibration" is an aspect of metacognition that describes how well students assess their own knowledge. One tool that can help to assess student calibration is the knowledge survey (KS). On a KS, students rate their confidence in their ability to answer questions related to course content. A comparison of a student's confidence level with their actual performance on course exams gives an indication of the student's metacognitive calibration. We report on a study that explores students' responses to a KS in introductory physics and chemistry courses serving both STEM and non-STEM populations. In many courses, Delta (the difference between KS-score and final exam score, a measure of calibration) was anti-correlated with final exam performance. No relationship was found between Delta and students' scientific reasoning abilities. We also report preliminary findings on how calibration differs for questions of a quantitative nature vs. those of a more conceptual nature.

  20. Calibration of phase detector using IQ modulator

    International Nuclear Information System (INIS)

    The beam energy of the J-PARC Linac is calculated by TOF (Time-of-Flight) method with the flight distance and beam phases at the two of measurement points. Because the accuracy of the beam energy measurement is directly depending on the errors in the phase measurement system, all 111 beam phase monitors are calibrated annually. Here, we adopted a calibration method using the IQ modulator as a method for carrying out more simply and accurately, calibration of the phase detection circuit is provided to the phase detection system. In the calibration, we have used the trombone circuit for the adjustment of the reference frequency, but it is thought that the procedure using an IQ modulator is more simple and accurate, and it reduces the time for the calibration. We describe the procedure of the phase detection system and the method of energy calculation. In addition, the general descriptions of the IQ modulation specification and its performances are introduced. (author)

  1. Absolute sensitivity calibration of extreme ultraviolet photoresists

    Energy Technology Data Exchange (ETDEWEB)

    Jones, Juanita; Naulleau, Patrick P.; Gullikson, Eric M.; Aquila, Andrew; George, Simi; Niakoula, Dimitra

    2008-05-16

    One of the major challenges facing the commercialization of extreme ultraviolet (EUV) lithography remains simultaneously achieving resist sensitivity, line-edge roughness, and resolution requirement. Sensitivity is of particular concern owing to its direct impact on source power requirements. Most current EUV exposure tools have been calibrated against a resist standard with the actual calibration of the standard resist dating back to EUV exposures at Sandia National Laboratories in the mid 1990s. Here they report on an independent sensitivity calibration of two baseline resists from the SEMATECH Berkeley MET tool performed at the Advanced Light Source Calibrations and Standards beamline. The results show the baseline resists to be approximately 1.9 times faster than previously thought based on calibration against the long standing resist standard.

  2. Calibration of Sr-90 ophthalmic applicators

    International Nuclear Information System (INIS)

    The purpose of this paper is to alert users of Sr-90 ophthalmic applicators about potential large errors in calibration of these devices. A discrepancy of more than 50% in calibration of Sr-90 ophthalmic applicators between the US National Institute of Standards and Technology (NIST) and one foreign manufacturer (the world's only remaining supplier) has been reported. A single-plane Sr-90 ophthalmic applicator was calibrated by the manufacturer, by NIST, and by the University of Wisconsin. The manufacturer's close rate calibration is confined to a 3-mm-diameter active area, while NIST measures all beta radiation emitted into a 2-PI solid angle. The discrepancy was verified by means of a technique based on that of NIST. Reports of calibrations at NIST of applicators made by several American manufacturers (no longer available) indicate that large discrepancies exist for other manufacturers as well

  3. Design, calibration and operation of Mars lander cameras

    Science.gov (United States)

    Bos, Brent Jon

    2002-09-01

    In the 45 years since the dawn of the space age, there have only been two Mars lander camera designs to successfully operate on the Martian surface. Therefore information on Mars imager design and operation issues is limited. In addition, good examples of Mars lander imager calibration work are almost non-existent. This work presents instrument calibration results for a Mars lander camera originally designed to fly as an instrument onboard the 2001 Mars Surveyor lander as a robotic arm camera (RAC). Test procedures and results are described as well as techniques for improving the accuracy of the calibration data. In addition we describe camera algorithms and operations research results for optimizing imager operations on the Martian surface. Finally, the lessons learned from the 2001 RAC are applied to the preliminary design of a new Mars camera for the Artemis Mars Scout mission. The design utilizes a Bayer color mosaic filter, white light LED's and includes an optical system operating at f/13 with a maximum resolution of 0.11 mrad/pixel. It is capable of imaging in several modes including: stereo, microscopic and panoramic at a mass of 0.3 kg. It will provide planetary geologists with an unprecedented view of the Martian surface.

  4. Selection of stars to calibrate Gaia

    Science.gov (United States)

    Carrasco, J. M.; Voss, H.; Jordi, C.; Fabricius, C.; Pancino, E.; Altavilla, G.

    2015-05-01

    Gaia is an all-sky survey satellite, launched by ESA on 19th December 2013, to obtain parallaxes and proper motions to microarcsecond level precision, radial velocities and astrophysical parameters for about one billion objects down to a limiting magnitude of 20. The chosen strategy to perform the photometric calibration is to split the process into two steps, internal and external calibration. The internal calibration will combine all different transits of a given source to a common reference internal system producing a 'mean' Gaia observation. This internal calibration accounts for the differential instrumental effects (in sensitivity, aperture, PSF, etc.). They depend on the colour and type of the source. For this reason, a selection of calibration sources ensuring a good representation of all kind of observed sources is needed. The entire magnitude and colour range of the sources have to be covered by these calibration stars and for all calibration intervals. It is a challenge to obtain a suitable colour distribution for the standards, especially for bright sources and the daily large scale calibration intervals. Once the mean Gaia observations are produced, a final step, the external calibration, transforms them to absolute fluxes and wavelengths. In principle, few calibration sources are needed (about 200 spectrophotometric standard stars, SPSS, are currently being considered). They need to have accurate determinations of their absolute fluxes and their non-variability need to be ensured below 1% precision. For this purpose, a big international observational effort is being done (using telescopes as 2.2m@CAHA, TNG@LaPalma, NTT@LaSilla, LaRuca@SPM, and others). During this observational effort some cases of non-expected variability of the SPSS candidates have been discovered.

  5. Automation of dosimeters calibration for radiotherapy in secondary dosimetric calibration laboratory of the CPHR

    International Nuclear Information System (INIS)

    This paper presents the design and implementation of an automated system for measurements in the calibration of reference radiation dosimeters. It was made a software application that performs the acquisition of the measured values of electric charge, calculated calibration coefficient and automates the calibration certificate issuance. These values are stored in a log file on a PC. The use of the application improves control over the calibration process, helps to humanize the work and reduces personnel exposure. The tool developed has been applied to the calibration of dosimeters radiation patterns in the LSCD of the Centro de Proteccion e Higiene de las Radiaciones, Cuba

  6. Low Charge and Reduced Mobility of Membrane Protein Complexes Has Implications for Calibration of Collision Cross Section Measurements.

    Science.gov (United States)

    Allison, Timothy M; Landreh, Michael; Benesch, Justin L P; Robinson, Carol V

    2016-06-01

    Ion mobility mass spectrometry of integral membrane proteins provides valuable insights into their architecture and stability. Here we show that, due to their lower charge, the average mobility of native-like membrane protein ions is approximately 30% lower than that of soluble proteins of similar mass. This has implications for drift time measurements, made on traveling wave ion mobility mass spectrometers, which have to be calibrated to extract collision cross sections (Ω). Common calibration strategies employ unfolded or native-like soluble protein standards with masses and mobilities comparable to the protein of interest. We compare Ω values for membrane proteins, derived from standard calibration protocols using soluble proteins, to values measured using an RF-confined drift tube. Our results demonstrate that, while common calibration methods underestimate Ω for native-like or unfolded membrane protein complexes, higher mass soluble calibration standards consistently yield more accurate Ω values. These findings enable us to obtain directly structural information for highly charge-reduced complexes by traveling wave ion mobility mass spectrometry. PMID:27153188

  7. A Cryogenic Infrared Calibration Target

    CERN Document Server

    Wollack, Edward J; Rinehart, Stephan A

    2014-01-01

    A compact cryogenic calibration target is presented that has a peak diffuse reflectance, $R \\le 0.003$, from $800-4,800\\,{\\rm cm}^{-1}$ $(12-2\\,\\mu$m). Upon expanding the spectral range under consideration to $400-10,000\\,{\\rm cm}^{-1}$ $(25-1\\,\\mu$m) the observed performance gracefully degrades to $R \\le 0.02$ at the band edges. In the implementation described, a high-thermal-conductivity metallic substrate is textured with a pyramidal tiling and subsequently coated with a thin lossy dielectric coating that enables high absorption and thermal uniformity across the target. The resulting target assembly is lightweight, has a low-geometric profile, and has survived repeated thermal cycling from room temperature to $\\sim4\\,$K. Basic design considerations, governing equations, and test data for realizing the structure described are provided. The optical properties of selected absorptive materials -- Acktar Fractal Black, Aeroglaze Z306, and Stycast 2850 FT epoxy loaded with stainless steel powder -- are character...

  8. HIBP calibration on WEGA stellarator

    Energy Technology Data Exchange (ETDEWEB)

    Podoba, Yuriy; Otte, Matthias; Wagner, Friedrich [Max-Planck-Institut fuer Plasmaphysik, Greifswald (Germany); Zhezhera, Alexander; Chmyga, Alexander; Kozachok, Alexander; Komarov, Alexander; Bondarenko, Ivan; Deshko, Galina; Khrebtov, Sergey; Krupnik, Ludmila [Kharkov Institute of Plasma Physics, Kharkov (Ukraine)

    2009-07-01

    The heavy ion beam probe (HIBP) is an established non-perturbing diagnostic for determining spatial distributions of plasma potential, density, temperature and poloidal magnetic field of magnetically confined plasmas. These quantities can be determined from the change in the ion beam parameters (charge, intensity and trajectory) passing through a plasma volume due to collisions with electrons and interactions with the confining magnetic field. The WEGA HIBP operates with a Na{sup +} with an energy of 39.5 keV and beam current 35 {mu}A. Conventionally the coordinate mapping of the HIBP is provided by ray tracing calculations of the ion beam in the magnetic field. However, it is very difficult to include all physical effects in the model, thus the result of the calculations may significantly differ from the real probing position. In order to improve the mapping precision an additional measurements of the beam position have been provided using a beam detector array inside the vacuum vessel. This allows to compare the measured and calculated ion beam position in order to find out the reasons for the coordinate mismatch and include adjustments in the calculation code. Results of this calibration are presented in this work.

  9. SMAP Radar Processing and Calibration

    Science.gov (United States)

    West, R.; Jaruwatanadilok, S.; Kwoun, O.; Chaubell, M.

    2013-01-01

    The Soil Moisture Active Passive (SMAP) mission is part of the NASA space-based Earth observation program, and consists of an L-band radar and radiometer scheduled for launch into sun synchronous orbit in late 2014. A joint effort of the Jet Propulsion Laboratory (JPL) and the Goddard Space Flight Center (GSFC), the SMAP mission draws heavily on the design and risk reduction heritage of the Hydrosphere State (Hydros) mission [1], [2]. The SMAP science and applications objectives are to: 1) understand processes that link the terrestrial water, energy and carbon cycles, 2) estimate global water and energy fluxes at the land surface, 3) quantify net carbon flux in boreal landscapes, 4) enhance weather and climate forecast skill, and 5) develop improved flood prediction and drought monitoring capability. To meet these science objectives, SMAP ground processing will combine the attributes of the radar and radiometer observations (in terms of their spatial resolution and sensitivity to soil moisture, surface roughness, and vegetation) to estimate soil moisture with 4% volumetric accuracy at a resolution of 10 km, and freeze-thaw state at a resolution of 1-3 km. Model sensitivities translate the soil moisture accuracy to a radar backscatter accuracy of 1 dB (1 sigma) at 3 km resolution and a brightness temperature accuracy of 1.3 K at 40 km resolution. This paper will describe the level 1 radar processing and calibration challenges and the choices made so far for the algorithms and software implementation.

  10. High Precision Momentum Calibration of the Magnetic Spectrometers at MAMI for Hypernuclear Binding Energy Determination

    CERN Document Server

    Margaryan, A; Achenbach, P; Ajvazyan, R; Elbakyan, H; Montgomery, R; Nakamura, S N; Pochodzalla, J; Schulz, F; Toyama, Y; Zhamkochyan, S

    2016-01-01

    We propose a new method for absolute momentum calibration of magnetic spectrometers used in nuclear physics, using the time-of-flight (TOF), differences of pairs of particles with different masses. In cases where the flight path is not known, a calibration can be determined by using the TOF differences of two pair combinations of three particles. A Cherenkov detector, read out by a radio frequency photomultiplier tube, is considered as the high-resolution and highly stable TOF detector. By means of Monte Carlo simulations it is demonstrated that the magnetic spectrometers at the MAMI electron-scattering facility can be calibrated absolutely with an accuracy $\\delta p/p\\leq 10^{-4}$, which will be crucial for high precision determination of hypernuclear masses.

  11. The mass-luminosity relation for stars of mass 1.0 to 0.08 solar mass

    Science.gov (United States)

    Henry, Todd J.; Mccarthy, Donald W., Jr.

    1993-01-01

    Mass-luminosity relations determined at IR wavelengths are presented for stars with masses 1.0 to 0.08 solar mass. Using IR speckle imaging techniques on a sample of nearby binaries, we have been able to concentrate on the lower main sequence, for which an accurate mass-luminosity calibration has remained problematic. In addition, the mass-visual luminosity relation for stars with 2.0-0.08 solar mass is produced by implementing new photometric relations linking V to JHK wavelengths for the nearby stars, supplemented with eclipsing binary information. These relations predict that objects with masses of about 0.08 solar mass have M(K) of about 10 and M(V) of about 18.

  12. SPRT Calibration Uncertainties and Internal Quality Control at a Commercial SPRT Calibration Facility

    Science.gov (United States)

    Wiandt, T. J.

    2008-06-01

    The Hart Scientific Division of the Fluke Corporation operates two accredited standard platinum resistance thermometer (SPRT) calibration facilities, one at the Hart Scientific factory in Utah, USA, and the other at a service facility in Norwich, UK. The US facility is accredited through National Voluntary Laboratory Accreditation Program (NVLAP), and the UK facility is accredited through UKAS. Both provide SPRT calibrations using similar equipment and procedures, and at similar levels of uncertainty. These uncertainties are among the lowest available commercially. To achieve and maintain low uncertainties, it is required that the calibration procedures be thorough and optimized. However, to minimize customer downtime, it is also important that the instruments be calibrated in a timely manner and returned to the customer. Consequently, subjecting the instrument to repeated calibrations or extensive repeated measurements is not a viable approach. Additionally, these laboratories provide SPRT calibration services involving a wide variety of SPRT designs. These designs behave differently, yet predictably, when subjected to calibration measurements. To this end, an evaluation strategy involving both statistical process control and internal consistency measures is utilized to provide confidence in both the instrument calibration and the calibration process. This article describes the calibration facilities, procedure, uncertainty analysis, and internal quality assurance measures employed in the calibration of SPRTs. Data will be reviewed and generalities will be presented. Finally, challenges and considerations for future improvements will be discussed.

  13. Intercomparison and calibration of dose calibrators used in nuclear medicine facilities

    CERN Document Server

    Costa, A M D

    2003-01-01

    The aim of this work was to establish a working standard for intercomparison and calibration of dose calibrators used in most of nuclear medicine facilities for the determination of the activity of radionuclides administered to patients in specific examinations or therapeutic procedures. A commercial dose calibrator, a set of standard radioactive sources, and syringes, vials and ampoules with radionuclide solutions used in nuclear medicine were utilized in this work. The commercial dose calibrator was calibrated for radionuclide solutions used in nuclear medicine. Simple instrument tests, such as linearity response and variation response with the source volume at a constant source activity concentration were performed. This instrument may be used as a reference system for intercomparison and calibration of other activity meters, as a method of quality control of dose calibrators utilized in nuclear medicine facilities.

  14. Mass spectrometry.

    Science.gov (United States)

    Burlingame, A. L.; Johanson, G. A.

    1972-01-01

    Review of the current state of mass spectrometry, indicating its unique importance for advanced scientific research. Mass spectrometry applications in computer techniques, gas chromatography, ion cyclotron resonance, molecular fragmentation and ionization, and isotope labeling are covered. Details are given on mass spectrometry applications in bio-organic chemistry and biomedical research. As the subjects of these applications are indicated alkaloids, carbohydrates, lipids, terpenes, quinones, nucleic acid components, peptides, antibiotics, and human and animal metabolisms. Particular attention is given to the mass spectra of organo-inorganic compounds, inorganic mass spectrometry, surface phenomena such as secondary ion and electron emission, and elemental and isotope analysis. Further topics include mass spectrometry in organic geochemistry, applications in geochronology and cosmochemistry, and organic mass spectrometry.

  15. The calibration of the central electromagnetic calorimeter of UA1 proton-antiproton experiment at CERN

    International Nuclear Information System (INIS)

    The most important result of the UA1 experiment at CERN has been the discovery of the weak intermediate vector bosons W+, W- and Z0. We describe the calibration of the electromagnetic calorimeter, which gives the signature of the electronic mode of desintegration of the intermediate bosons and measures their masses. We shall discuss this process and give some experimental results

  16. Impact of sound attenuation by suspended sediment on ADCP backscatter calibrations

    NARCIS (Netherlands)

    Sassi, M.G.; Hoitink, A.J.F.; Vermeulen, B.

    2012-01-01

    Although designed for velocity measurements, acoustic Doppler current profilers (ADCPs) are widely being used to monitor suspended particulate matter in rivers and in marine environments. To quantify mass concentrations of suspended matter, ADCP backscatter is generally calibrated with in situ measu

  17. Atmospheric radiocarbon calibration to 45,000 yr BP : Late glacial fluctuations and cosmogenic isotope production

    NARCIS (Netherlands)

    Kitagawa, H; van der Plicht, J

    1998-01-01

    More than 250 carbon-14 accelerator mass spectrometry dates of terrestrial macrofossils from annually laminated sediments from Lake Suigetsu (Japan) provide a first atmospheric calibration for almost the total range of the radiocarbon method (45,000 years before the present), The results confirm the

  18. Calibration of higher eigenmodes of cantilevers

    Science.gov (United States)

    Labuda, Aleksander; Kocun, Marta; Lysy, Martin; Walsh, Tim; Meinhold, Jieh; Proksch, Tania; Meinhold, Waiman; Anderson, Caleb; Proksch, Roger

    2016-07-01

    A method is presented for calibrating the higher eigenmodes (resonant modes) of atomic force microscopy cantilevers that can be performed prior to any tip-sample interaction. The method leverages recent efforts in accurately calibrating the first eigenmode by providing the higher-mode stiffness as a ratio to the first mode stiffness. A one-time calibration routine must be performed for every cantilever type to determine a power-law relationship between stiffness and frequency, which is then stored for future use on similar cantilevers. Then, future calibrations only require a measurement of the ratio of resonant frequencies and the stiffness of the first mode. This method is verified through stiffness measurements using three independent approaches: interferometric measurement, AC approach-curve calibration, and finite element analysis simulation. Power-law values for calibrating higher-mode stiffnesses are reported for several cantilever models. Once the higher-mode stiffnesses are known, the amplitude of each mode can also be calibrated from the thermal spectrum by application of the equipartition theorem.

  19. Preliminary evaluation of a Neutron Calibration Laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Alvarenga, Talysson S.; Neves, Lucio P.; Perini, Ana P.; Sanches, Matias P.; Mitake, Malvina B.; Caldas, Linda V.E., E-mail: talvarenga@ipen.br, E-mail: lpneves@ipen.br, E-mail: aperini@ipen.br, E-mail: msanches@ipen.br, E-mail: mbmitake@ipen.br, E-mail: lcaldas@ipen.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil); Federico, Claudio A., E-mail: claudiofederico@ieav.cta.br [Instituto de Estudos Avancados (IEAv/DCTA), Sao Jose dos Campos, SP (Brazil). Dept. de Ciencia e Tecnologia Aeroespacial

    2013-07-01

    In the past few years, Brazil and several other countries in Latin America have experimented a great demand for the calibration of neutron detectors, mainly due to the increase in oil prospection and extraction. The only laboratory for calibration of neutron detectors in Brazil is localized at the Institute for Radioprotection and Dosimetry (IRD/CNEN), Rio de Janeiro, which is part of the IAEA SSDL network. This laboratory is the national standard laboratory in Brazil. With the increase in the demand for the calibration of neutron detectors, there is a need for another calibration services. In this context, the Calibration Laboratory of IPEN/CNEN, Sao Paulo, which already offers calibration services of radiation detectors with standard X, gamma, beta and alpha beams, has recently projected a new calibration laboratory for neutron detectors. In this work, the ambient equivalent dose rate (H⁎(10)) was evaluated in several positions inside and around this laboratory, using Monte Carlo simulation (MCNP5 code), in order to verify the adequateness of the shielding. The obtained results showed that the shielding is effective, and that this is a low-cost methodology to improve the safety of the workers and evaluate the total staff workload. (author)

  20. Increased Automation in Stereo Camera Calibration Techniques

    Directory of Open Access Journals (Sweden)

    Brandi House

    2006-08-01

    Full Text Available Robotic vision has become a very popular field in recent years due to the numerous promising applications it may enhance. However, errors within the cameras and in their perception of their environment can cause applications in robotics to fail. To help correct these internal and external imperfections, stereo camera calibrations are performed. There are currently many accurate methods of camera calibration available; however, most or all of them are time consuming and labor intensive. This research seeks to automate the most labor intensive aspects of a popular calibration technique developed by Jean-Yves Bouguet. His process requires manual selection of the extreme corners of a checkerboard pattern. The modified process uses embedded LEDs in the checkerboard pattern to act as active fiducials. Images are captured of the checkerboard with the LEDs on and off in rapid succession. The difference of the two images automatically highlights the location of the four extreme corners, and these corner locations take the place of the manual selections. With this modification to the calibration routine, upwards of eighty mouse clicks are eliminated per stereo calibration. Preliminary test results indicate that accuracy is not substantially affected by the modified procedure. Improved automation to camera calibration procedures may finally penetrate the barriers to the use of calibration in practice.

  1. Landsat TM and ETM+ thermal band calibration

    Science.gov (United States)

    Barsi, J.A.; Schott, J.R.; Palluconi, F. D.; Helder, D.L.; Hook, S.J.; Markham, B.L.; Chander, G.; O'Donnell, E. M.

    2003-01-01

    Landsat-5 has been imaging the Earth since March 1984, and Landsat-7 was added to the series of Landsat instruments in April 1999. The Landsat Project Science Office and the Landsat-7 Image Assessment System have been monitoring the on-board calibration of Landsat-7 since launch. Additionally, two separate university teams have been evaluating the on-board thermal calibration of Landsat-7 through ground-based measurements since launch. Although not monitored as closely over its lifetime, a new effort is currently being made to validate the calibration of Landsat-5. Two university teams are beginning to collect ground truth under Landsat-5, along with using other vicarious calibration methods to go back into the archive to validate the history of the calibration of Landsat-5. This paper considers the calibration efforts for the thermal band, band 6, of both the Landsat-5 and Landsat-7 instruments. Though stable since launch, Landsat-7 had an initial calibration error of about 3 K, and changes were made to correct for this beginning 1 October 2000 for data processed with the National Landsat Archive Production System (NLAPS) and beginning 20 December 2000 for data processed with the Landsat Product Generation System (LPGS). Recent results from Landsat-5 vicarious calibration efforts show an offset of –0.7 K over the lifetime of the instrument. This suggests that historical calibration efforts may have been detecting errors in processing systems rather than changes in the instrument. A correction to the Landsat-5 processing has not yet been implemented but will be in the near future.

  2. Calibration of a groundwater flow model with different tracer technologies

    International Nuclear Information System (INIS)

    Full text: This study developed a mechanism to calibrate a regional groundwater flow model for an aquifer system in central Mexico (Guanajuato) by residence time values of a set of different tracers. The used tracers were carbon-14, tritium, chlorofluorocarbons (CFCs), and sulfur hexafluoride (SF6). The applied program for the flow simulations was the modular finite-difference MODFLOW-2000, coupled to the transport model MODPATH. The local recharge estimates obtained from the chloride mass-balance method were regionalised by a Kriging method, whilst hydraulic conductivity values for each geological unit were interpreted from pumping test data. The flow simulation was considered in steady-state conditions (pre-development model). Since the flow domain was complicate and the number of grid cells large, an algebraic multigrid solver was applied rather than the classical iterative methods. The calibration process consisted in adjusting the hydraulic conductivity values until (a) the calculated head distribution matched the observed water level measurements, and (b) the flow balance is satisfied in the whole flow domain (mass balance) and in parts of the flow domain (zone budget), (c) the mean residence time values of carbon-14, tritium, CFCs, and SF6 matched the time of travel of corresponding particles in the flow domain. Since carbon-14 is known to be modified due to geochemical interactions with the aquifer material, a preceding correction by using the program PHREEQC was necessary to obtain reliable mean residence time values. Due to the low time resolution, the tracers for young groundwater (tritium, CFCs, SF6) could be applied in the flow simulation only to indicate if the groundwater is younger or older than 40 to 50 years. This calibration approach was not only useful to quantitatively describe the flow regime of an aquifer system, but also to make some observations to its vulnerability. Comments on the experience of the used tracer technologies in combination

  3. Construction and calibration of a bar weighing lysimeter

    Directory of Open Access Journals (Sweden)

    Daiane Cinque Mariano

    2015-08-01

    Full Text Available Generally, standard lysimeters include a lever-load cell scale, which has become expensive compared to new electronic equipment available for experimental purposes. Currently, lysimeters containing weighing bars with up to 4 load cells are economically feasible. This goal of this study was to present the construction and calibration of four weighing lysimeters built using two rectangular tanks, with a surface area of 1.35 m2 (1 m by 1.35 m and a depth of 1.5 m, loaded on two weighing bars. Each bar had two high accuracy loading cells connected to a junction box and a datalogger by a coaxial cable. Calibration of each lysimeter was performed after field installation. The results showed a linear response (R2 > 0.9999 of electric signal (mV to mass increase or decrease (kg with minimum hysteresis. The mean absolute error of the mass estimate (0.0245 to 0.2844 equivalent-mm and a Willmott index between the observed and estimated data (d = 1.0000 indicate the high precision of the new equipment. The results allow concluding that the lysimeters in this study are appropriate for estimating evapotranspiration and other components of soil water balance.

  4. Cold-spray ionization mass spectrometry: applications in structural coordination chemistry.

    Science.gov (United States)

    Yamaguchi, Kentaro

    2013-01-01

    Electrospray ionization (ESI)-mass spectrometry (MS) is generally used for the characterization of labile supramolecules in which non-covalent bonding interactions are predominant. However, molecular ions are not detected in many cases because of their instability, and even if such ions are detected, thermal decomposition generates fragment ions that also appear in the mass spectrum. Cold-spray ionization (CSI) is designed for the MS detection of labile organic species. It is used to analyze the structures of biomolecular complexes and labile organic species in solution. The method, a variant of ESI-MS, operates at low temperature, allowing simple and precise characterization of labile non-covalent complexes that are difficult or impossible to observe by conventional MS techniques. The CSI method is particularly suitable for elucidating the structures of labile organometallic compounds in solution as it offers a means to investigate the dynamic behavior of unstable molecules and/or labile clusters in solution. Various labile organic compounds are analyzed by using the CSI method in the field of organic chemistry. CSI-MS is also used to investigate the behavior of aggregated steroid compounds, namely, bisguanidinobenzene-benzoic acid complexes, in solution. This method is a powerful tool for analyzing the equilibria of multiply linked self-assembling catenanes in solution. Its application to unstable and complex supramolecules will be shown. We have developed an effective ionization method that uses metal-complex-based ionization probes containing 2,6-bis(oxazolinyl) pyridine (pybox) ligands. Using this method, we were able to detect multiply charged ions of target molecules. This method was proven to effectively ionize large complex molecules, including biomolecules and various supramolecules, as well as carbon clusters, such as fullerenes. Moreover, isotope-labeled pybox-La complexes were used to clearly detect isotopic labeling shifts. Their applications to

  5. Geometric calibration of ERS satellite SAR images

    DEFF Research Database (Denmark)

    Mohr, Johan Jacob; Madsen, Søren Nørvang

    2001-01-01

    Geometric calibration of the European Remote Sensing (ERS) Satellite synthetic aperture radar (SAR) slant range images is important in relation to mapping areas without ground reference points and also in relation to automated processing. The relevant SAR system parameters are discussed...... and calibrated by using the European Space Agency (ESA) transponders at Flevoland. The resulting accuracy of the slant range images corresponds to 10 m horizontally on the ground. The results are verified by using runway intersections and corner reflectors surveyed with differential GPS techniques. Based......, is described to allow other researchers to geometrically calibrate their processing systems...

  6. Calibration of Ground-based Lidar instrument

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Gómez Arranz, Paula

    This report presents the result of the lidar calibration performed for the given Ground-based Lidar at DTU’s test site for large wind turbines at Høvsøre, Denmark. Calibration is here understood as the establishment of a relation between the reference wind speed measurements with measurement...... uncertainties provided by measurement standard and corresponding lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements. The comparison of the lidar measurements of the wind direction with that from wind vanes...... measurements are given for information only....

  7. Calibration of Ground-based Lidar instrument

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Gómez Arranz, Paula

    This report presents the result of the lidar calibration performed for the given Ground-based Lidar at DTU’s test site for large wind turbines at Høvsøre, Denmark. Calibration is here understood as the establishment of a relation between the reference wind speed measurements with measurement...... uncertainties provided by measurement standard and corresponding lidar wind speed indications with associated measurement uncertainties. The lidar calibration concerns the 10 minute mean wind speed measurements. The comparison of the lidar measurements of the wind direction with that from wind vanes...

  8. Global analysis of the phase calibration operation

    Science.gov (United States)

    Lannes, André

    2005-04-01

    A global approach to phase calibration is presented. The corresponding theoretical framework calls on elementary concepts of algebraic graph theory (spanning tree of maximal weight, cycles) and algebraic number theory (lattice, nearest lattice point). The traditional approach can thereby be better understood. In radio imaging and in optical interferometry, the self-calibration procedures must often be conducted with much care. The analysis presented should then help in finding a better compromise between the coverage of the calibration graph (which must be as complete as possible) and the quality of the solution (which must of course be reliable).

  9. Calibration for 3D Structured Light Measurement

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    A calibration procedure was developed for three-dimensional(3D) binocular structured light measurement systems. In virtue of a specially designed pattern, matching points in stereo images are extracted. And then sufficient 3D space points are obtained through pairs of images with the intrinsic and extrinsic parameters of each camera estimated prior and consequently some lights are calibrated by means of multi point fitting. Finally, a mathematical model is applied to interpolate and approximate all dynamic scanning lights based on geometry. The process of calibration method is successfully used in the binocular 3D measurement system based on structured lights and the 3D reconstruction results are satisfying.

  10. Design of a neutron source for calibration

    International Nuclear Information System (INIS)

    The neutron spectra produced by an isotopic neutron source located at the center of moderating media were calculated using Monte Carlo method in the aim to design a neutron source for calibration purposes. To improve the evaluation of the dosimetric quantities, is recommended to calibrate the radiation protection devices with calibrated neutron sources whose neutron spectra being similar to those met in practice. Here, a 239Pu-Be neutron source was inserted in H2O, D2O and polyethylene cylindrical moderators in order to produce neutron spectra that resembles spectra found in workplaces

  11. Calibration boards for the ATLAS LAr calorimeters

    International Nuclear Information System (INIS)

    In order to calibrate the ATLAS Liquid Argon (LAr) calorimeters to an accuracy better than 1%, over 16 bit dynamic range, chips have been designed in DMILL technology. The design and performance of a 16 bit DAC, a static low offset operational amplifier and a digital chip to control the calibration boards are presented. A 8 channels board using these chips has also been realised and carefully measured as this module will be replicated 16 times to design the final 128 channels calibration board. (authors)

  12. GIADA: extended calibration activities before the comet encounter

    Science.gov (United States)

    Accolla, Mario; Sordini, Roberto; Della Corte, Vincenzo; Ferrari, Marco; Rotundi, Alessandra

    2014-05-01

    The Grain Impact Analyzer and Dust Accumulator - GIADA - is one of the payloads on-board Rosetta Orbiter. Its three detection sub-systems are able to measure the speed, the momentum, the mass, the optical cross section of single cometary grains and the dust flux ejected by the periodic comet 67P Churyumov-Gerasimenko. During the Hibernation phase of the Rosetta mission, we have performed a dedicated extended calibration activity on the GIADA Proto Flight Model (accommodated in a clean room in our laboratory) involving two of three sub-systems constituting GIADA, i.e. the Grain Detection System (GDS) and the Impact Sensor (IS). Our aim is to carry out a new set of response curves for these two subsystems and to correlate them with the calibration curves obtained in 2002 for the GIADA payload onboard the Rosetta spacecraft, in order to improve the interpretation of the forthcoming scientific data. For the extended calibration we have dropped or shot into GIADA PFM a statistically relevant number of grains (i.e. about 1 hundred), acting as cometary dust analogues. We have studied the response of the GDS and IS as a function of grain composition, size and velocity. Different terrestrial materials were selected as cometary analogues according to the more recent knowledge gained through the analyses of Interplanetary Dust Particles and cometary samples returned from comet 81P/Wild 2 (Stardust mission). Therefore, for each material, we have produced grains with sizes ranging from 20-500 μm in diameter, that were characterized by FESEM and micro IR spectroscopy. Therefore, the grains were shot into GIADA PFM with speed ranging between 1 and 100 ms-1. Indeed, according to the estimation reported in Fink & Rubin (2012), this range is representative of the dust particle velocity expected at the comet scenario and lies within the GIADA velocity sensitivity (i.e. 1-100 ms-1 for GDSand 1-300 ms-1for GDS+IS 1-300 ms-1). The response curves obtained using the data collected

  13. Champion Island, Galapagos Stable Oxygen Calibration Data

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — Galapagos Coral Stable Oxygen Calibration Data. Sites: Bartolome Island: 0 deg, 17 min S, 90 deg 33 min W. Champion Island: 1 deg, 15 min S, 90 deg, 05 min W....

  14. Bartolome Island, Galapagos Stable Oxygen Calibration Data

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — Galapagos Coral Stable Oxygen Calibration Data. Sites: Bartolome Island: 0 deg, 17'S, 90 deg 33' W. Champion Island: 1 deg, 15'S, 90 deg, 05' W. Urvina Bay (Isabela...

  15. A transmission calibration method for superconducting resonators

    CERN Document Server

    Cataldo, Giuseppe; Barrentine, Emily M; Brown, Ari D; Moseley, Samuel H; U-Yen, Kongpop

    2014-01-01

    A method is proposed and experimentally explored for \\textit{in-situ} calibration of complex transmission data for superconducting microwave resonators. This cryogenic calibration method accounts for the instrumental transmission response between the vector network analyzer reference plane and the device calibration plane. Once calibrated, the observed resonator response was modeled in detail by two approaches. The first, a phenomenological model based on physically realizable rational functions, enables the extraction of multiple resonance frequencies and widths for coupled resonators without explicit specification of the circuit network. In the second, an ABCD-matrix representation for the distributed transmission line circuit is used to model the observed response from the characteristic impedance and propagation constant. When used in conjunction with electromagnetic simulations, the kinetic inductance fraction can be determined with this method with an accuracy of 2%. Datasets for superconducting microst...

  16. Calibration of a photomultiplier array spectrometer

    Science.gov (United States)

    Bailey, Steven A.; Wright, C. Wayne; Piazza, Charles R.

    1989-01-01

    A systematic approach to the calibration of a photomultiplier array spectrometer is presented. Through this approach, incident light radiance derivation is made by recognizing and tracing gain characteristics for each photomultiplier tube.

  17. Calibration of the JEM-EUSO detector

    Directory of Open Access Journals (Sweden)

    Gorodetzky P.

    2013-06-01

    Full Text Available In order to unveil the mystery of ultra high energy cosmic rays (UHECRs, JEM-EUSO (Extreme Universe Space Observatory on-board Japan Experiment Module will observe extensive air showers induced by UHECRs from the International Space Station orbit with a huge acceptance. Calibration of the JEM-EUSO instrument, which consists of Fresnel optics and a focal surface detector with 5000 photomultipliers, is very important to discuss the origin of UHECRs precisely with the observed results. In this paper, the calibration before launch and on-orbit is described. The calibration before flight will be performed as precisely as possible with integrating spheres. In the orbit, the relative change of the performance will be checked regularly with on-board and on-ground light sources. The absolute calibration of photon detection efficiency may be performed with the moon, which is a stable light source in the nature.

  18. Strain Gauges Mounted To Retain Calibration

    Science.gov (United States)

    Butler, Barry L.

    1993-01-01

    Silicon-based semiconductor strain gauges mounted in such way they retain original calibration for several years instead of few months. Improvement effected by bonding gauges to ceramic substrates with glasses instead of epoxies as adhesives.

  19. Calibration of sources for alpha spectroscopy systems

    International Nuclear Information System (INIS)

    This paper describes the calibration methodology for measuring the total alpha activity of plane and thin sources with the Alpha Spectrometer for Silicon Detector in the Nuclear Measures and Dosimetry laboratory at IEAv/CTA. (author)

  20. Absolute calibration technique for spontaneous fission sources

    International Nuclear Information System (INIS)

    An absolute calibration technique for a spontaneously fissioning nuclide (which involves no arbitrary parameters) allows unique determination of the detector efficiency for that nuclide, hence of the fission source strength

  1. Low Power, Self Calibrated Vector Magnetometer Project

    Data.gov (United States)

    National Aeronautics and Space Administration — This Phase I SBIR project investigates a novel approach to vector magnetometry based on high precision measurements of the total magnetic field. The calibration is...

  2. The PREMOS/PICARD instrument calibration

    Science.gov (United States)

    Schmutz, Werner; Fehlmann, André; Hülsen, Gregor; Meindl, Peter; Winkler, Rainer; Thuillier, Gérard; Blattner, Peter; Buisson, François; Egorova, Tatiana; Finsterle, Wolfgang; Fox, Nigel; Gröbner, Julian; Hochedez, Jean-François; Koller, Silvio; Meftah, Mustapha; Meisonnier, Mireille; Nyeki, Stephan; Pfiffner, Daniel; Roth, Hansjörg; Rozanov, Eugene; Spescha, Marcel; Wehrli, Christoph; Werner, Lutz; Wyss, Jules U.

    2009-08-01

    PREMOS is a space experiment scheduled to fly on the French solar mission PICARD. The experiment comprises filter radiometers and absolute radiometers to measure the spectral and total solar irradiance. The aim of PREMOS is to contribute to the long term monitoring of the total solar irradiance, to use irradiance observations for 'nowcasting' the state of the terrestrial middle atmosphere and to provide long term sensitivity calibration for the solar imaging instrument SODISM on PICARD. In this paper we describe the calibration of the instruments. The filter radiometer channels in the visible and near IR were characterized at PMOD/WRC and the UV channels were calibrated at PTB Berlin. The absolute radiometers were compared with the World Radiometric Reference at PMOD/WRC and a power calibration relative to a primary cryogenic radiometer standard was performed in vacuum and air at NPL.

  3. Computer Vision Assisted Virtual Reality Calibration

    Science.gov (United States)

    Kim, W.

    1999-01-01

    A computer vision assisted semi-automatic virtual reality (VR) calibration technology has been developed that can accurately match a virtual environment of graphically simulated three-dimensional (3-D) models to the video images of the real task environment.

  4. Calibration device for ultrasonic inspection equipment

    International Nuclear Information System (INIS)

    The inspection equipment is introduced into the reactor vessel and deposited there. The real inspection of the vessel is performed by means of a manipulator arm carrying an ultrasonic transducer field and being desplaceable along nine axes of motion for the inspection of welds. In order to be sure of adequate testing the origin of the field must exactly be known. This is achieved by means of a calibration unit by which the exact zero position in the vessel is fixed, the position of the ultrasonic transducer is calibrated and its angular position can be determined. It has got a spherical calibration body and at least one inlined reflection surface (tuncated cone surface) that can take a fixed position with respect to the ultrasonic transducer. The calibration body and/or the reflection surface are moved with respect to the ultrasonic transducer until the maximum amplitude of the reflected signal is obtained. (DG)

  5. Low radioactivity spectral gamma calibration facility

    International Nuclear Information System (INIS)

    A low radioactivity calibration facility has been constructed at the Nevada Test Site (NTS). This facility has four calibration models of natural stone that are 3 ft in diameter and 6 ft long, with a 12 in. cored borehole in the center of each model and a lead-shielded run pipe below each model. These models have been analyzed by laboratory natural gamma ray spectroscopy (NGRS) and neutron activation analysis (NAA) for their K, U, and Th content. Also, 42 other elements were analyzed in the NAA. The 222Rn emanation data were collected. Calibrating the spectral gamma tool in this low radioactivity calibration facility allows the spectral gamma log to accurately aid in the recognition and mapping of subsurface stratigraphic units and alteration features associated with unusual concentrations of these radioactive elements, such as clay-rich zones

  6. HPS instrument calibration laboratory accreditation program

    Energy Technology Data Exchange (ETDEWEB)

    Masse, F.X; Eisenhower, E.H.; Swinth, K.L.

    1993-12-31

    The purpose of this paper is to provide an accurate overview of the development and structure of the program established by the Health Physics Society (HPS) for accrediting instrument calibration laboratories relative to their ability to accurately calibrate portable health physics instrumentation. The purpose of the program is to provide radiation protection professionals more meaningful direct and indirect access to the National Institute of Standards and Technology (NIST) national standards, thus introducing a means for improving the uniformity, accuracy, and quality of ionizing radiation field measurements. The process is designed to recognize and document the continuing capability of each accredited laboratory to accurately perform instrument calibration. There is no intent to monitor the laboratory to the extent that each calibration can be guaranteed by the program; this responsibility rests solely with the accredited laboratory.

  7. HPS instrument calibration laboratory accreditation program

    International Nuclear Information System (INIS)

    The purpose of this paper is to provide an accurate overview of the development and structure of the program established by the Health Physics Society (HPS) for accrediting instrument calibration laboratories relative to their ability to accurately calibrate portable health physics instrumentation. The purpose of the program is to provide radiation protection professionals more meaningful direct and indirect access to the National Institute of Standards and Technology (NIST) national standards, thus introducing a means for improving the uniformity, accuracy, and quality of ionizing radiation field measurements. The process is designed to recognize and document the continuing capability of each accredited laboratory to accurately perform instrument calibration. There is no intent to monitor the laboratory to the extent that each calibration can be guaranteed by the program; this responsibility rests solely with the accredited laboratory

  8. Automatic colorimetric calibration of human wounds

    Directory of Open Access Journals (Sweden)

    Meert Theo

    2010-03-01

    Full Text Available Abstract Background Recently, digital photography in medicine is considered an acceptable tool in many clinical domains, e.g. wound care. Although ever higher resolutions are available, reproducibility is still poor and visual comparison of images remains difficult. This is even more the case for measurements performed on such images (colour, area, etc.. This problem is often neglected and images are freely compared and exchanged without further thought. Methods The first experiment checked whether camera settings or lighting conditions could negatively affect the quality of colorimetric calibration. Digital images plus a calibration chart were exposed to a variety of conditions. Precision and accuracy of colours after calibration were quantitatively assessed with a probability distribution for perceptual colour differences (dE_ab. The second experiment was designed to assess the impact of the automatic calibration procedure (i.e. chart detection on real-world measurements. 40 Different images of real wounds were acquired and a region of interest was selected in each image. 3 Rotated versions of each image were automatically calibrated and colour differences were calculated. Results 1st Experiment: Colour differences between the measurements and real spectrophotometric measurements reveal median dE_ab values respectively 6.40 for the proper patches of calibrated normal images and 17.75 for uncalibrated images demonstrating an important improvement in accuracy after calibration. The reproducibility, visualized by the probability distribution of the dE_ab errors between 2 measurements of the patches of the images has a median of 3.43 dE* for all calibrated images, 23.26 dE_ab for all uncalibrated images. If we restrict ourselves to the proper patches of normal calibrated images the median is only 2.58 dE_ab! Wilcoxon sum-rank testing (p Conclusion The investigators proposed an automatic colour calibration algorithm that ensures reproducible colour

  9. A spectrograph for exoplanet observations calibrated at the centimetre-per-second level.

    Science.gov (United States)

    Wilken, Tobias; Curto, Gaspare Lo; Probst, Rafael A; Steinmetz, Tilo; Manescau, Antonio; Pasquini, Luca; González Hernández, Jonay I; Rebolo, Rafael; Hänsch, Theodor W; Udem, Thomas; Holzwarth, Ronald

    2012-05-31

    The best spectrographs are limited in stability by their calibration light source. Laser frequency combs are the ideal calibrators for astronomical spectrographs. They emit a spectrum of lines that are equally spaced in frequency and that are as accurate and stable as the atomic clock relative to which the comb is stabilized. Absolute calibration provides the radial velocity of an astronomical object relative to the observer (on Earth). For the detection of Earth-mass exoplanets in Earth-like orbits around solar-type stars, or of cosmic acceleration, the observable is a tiny velocity change of less than 10 cm s(-1), where the repeatability of the calibration--the variation in stability across observations--is important. Hitherto, only laboratory systems or spectrograph calibrations of limited performance have been demonstrated. Here we report the calibration of an astronomical spectrograph with a short-term Doppler shift repeatability of 2.5 cm s(-1), and use it to monitor the star HD 75289 and recompute the orbit of its planet. This repeatability should make it possible to detect Earth-like planets in the habitable zone of star or even to measure the cosmic acceleration directly.

  10. GIADA - Grain Impact Analyzer and Dust Accumulator - Onboard Rosetta spacecraft: Extended calibrations

    Science.gov (United States)

    Della Corte, V.; Sordini, R.; Accolla, M.; Ferrari, M.; Ivanovski, S.; Rotundi, A.; Rietmeijer, F. J. M.; Fulle, M.; Mazzotta-Epifani, E.; Palumbo, P.; Colangeli, L.; Lopez-Moreno, J. J.; Rodriguez, J.; Morales, R.; Cosi, M.

    2016-09-01

    Despite a long tradition of dust instruments flown on-board space mission, the largest number of these can be considered unique as they used different detection techniques. GIADA (Grain Impact Analyzer and Dust Accumulator), is one of the dust instruments on-board the Rosetta spacecraft and is devoted to measure the dust dynamical parameters in the coma of comet 67P/Churyumov-Gerasimenko. It couples two different techniques to measure the mass and speed of individual dust particles. We report here the results of an extended calibration activity carried-out, during the hibernation phase of the Rosetta mission, on the GIADA Proto Flight Model (PFM) operative in a clean room in our laboratory. The main aims of an additional calibration campaign are: to verify the algorithms and procedures for data calibration developed before Rosetta launch; to improve the comprehension of GIADA response after the increased knowledge on cometary dust, e.g. the composition of dust particles after Stardust mission. These calibration improvements implied a final step, which consisted in defining transfer functions to correlate the new calibration curves obtained for the GIADA PFM to those to be used for GIADA onboard the Rosetta spacecraft. The extended calibration activity allowed us to analyze GIADA data acquired in the 67P/C-G coma permitting to infer additional information on cometary dust particles, e.g. density and tensile strength.

  11. Handbook of mass measurement

    CERN Document Server

    Jones, Frank E

    2002-01-01

    "How much does it weigh?" seems a simple question. To scientists and engineers, however, the answer is far from simple, and determining the answer demands consideration of an almost overwhelming number of factors.With an intriguing blend of history, fundamentals, and technical details, the Handbook of Mass Measurement sets forth the details of achieving the highest precision in mass measurements. It covers the whole field, from the development, calibration, and maintenance of mass standards to detailed accounts of weighing designs, balances, and uncertainty. It addresses the entire measurement process and provides in-depth examinations of the various factors that introduce error.Much of the material is the authors'' own work and some of it is published here for the first time. Jones and Schoonover are both highly regarded veterans of the U.S. National Institute of Standards and Technology. With this handbook, they have provided a service and resource vital to anyone involved not only in the determination of m...

  12. Lidar to lidar calibration phase 1

    DEFF Research Database (Denmark)

    Yordanova, Ginka; Courtney, Michael

    This report presents a feasibility study of a lidar to lidar (L2L) calibration procedure. Phase one of the project was conducted at Høvsøre, Denmark. Two windcubes were placed next to the 116m met mast and different methods were applied to obtain the sensing height error of the lidars. The purpose...... is to find the most consistent method and use it in a potential lidar to lidar calibration procedure....

  13. Hydraulic Calibrator for Strain-Gauge Balances

    Science.gov (United States)

    Skelly, Kenneth; Ballard, John

    1987-01-01

    Instrument for calibrating strain-gauge balances uses hydraulic actuators and load cells. Eliminates effects of nonparallelism, nonperpendicularity, and changes of cable directions upon vector sums of applied forces. Errors due to cable stretching, pulley friction, and weight inaccuracy also eliminated. New instrument rugged and transportable. Set up quickly. Developed to apply known loads to wind-tunnel models with encapsulated strain-gauge balances, also adapted for use in calibrating dynamometers, load sensors on machinery and laboratory instruments.

  14. Calibration and monitoring for crystal calorimetry

    CERN Document Server

    Zhu, Ren Yuan

    2005-01-01

    Crystal calorimetry provides excellent energy resolution in high energy and nuclear physics. The light output of heavy crystal scintillators, however, suffers from not negligible damage in radiation environment. A precision calibration and monitoring thus is crucial for maintaining crystal precision in situ. The performance of calibration and monitoring approaches used by BaBar, CLEO and L3 experiments are presented. The design and construction of a laser- based light monitoring system for CMS PWO calorimeter is also discussed.

  15. Automatic Calibration Of Manual Machine Tools

    Science.gov (United States)

    Gurney, Rex D.

    1990-01-01

    Modified scheme uses data from multiple positions and eliminates tedious positioning. Modification of computer program adapts calibration system for convenient use with manually-controlled machine tools. Developed for use on computer-controlled tools. Option added to calibration program allows data on random tool-axis positions to be entered manually into computer for reduction. Instead of setting axis to predetermined positions, operator merely sets it at variety of arbitrary positions.

  16. Virtual Calibration Chamber CPT on Ticino sand

    OpenAIRE

    Butlanska, Joanna; Arroyo Alvarez de Toledo, Marcos; Gens Solé, Antonio

    2010-01-01

    The following paper surnmarizes results of CPT's performed in virtual calibration chamber (VCC) built with a 3D model based on the distinct element method (DEM). A discrete material tailored to mimic Ticino sand is tested at different densities, stress and stress history. The limit cone tip resistance from the numerical experiments shows quantitative agreement with different empirical curves summarizing previous tests on Ticino sand in physical calibration chambers (ENEL and ISMES).

  17. pH sensor calibration procedure

    OpenAIRE

    Artero Delgado, Carola; Nogueras Cervera, Marc; Manuel Lázaro, Antonio; Prat Tasias, Jordi; Prat Farran, Joana d'Arc

    2013-01-01

    This paper describes the calibration of pH sensor located at the OBSEA marine Observatory. This instrument is based on an industrial pH electrode that is connected to a CTD instrument (Conductivity, Temperature, and Depth ). The calibration of the pH sensor has been done using a high precision spectrophotometer pH meter from Institute of Marine Sciences (ICM), and in this way it has been obtained a numerical function for the p H sensor propor...

  18. Calibration of the Super-Kamiokande Detector

    OpenAIRE

    Abe, K.; Hayato, Y.; Iida, T; Iyogi, K.; Kameda, J.; Kishimoto, Y.; Koshio, Y.; Marti, Ll.; Miura, M.; Moriyama, S.; Nakahata, M.(University of Tokyo, Institute for Cosmic Ray Research, Kamioka Observatory, Kamioka, Japan); Nakano, Y.; Nakayama, S.; Obayashi, Y.; Sekiya, H.

    2013-01-01

    Procedures and results on hardware level detector calibration in Super-Kamiokande (SK) are presented in this paper. In particular, we report improvements made in our calibration methods for the experimental phase IV in which new readout electronics have been operating since 2008. The topics are separated into two parts. The first part describes the determination of constants needed to interpret the digitized output of our electronics so that we can obtain physical numbers such as photon count...

  19. A Method to Test Model Calibration Techniques

    Energy Technology Data Exchange (ETDEWEB)

    Judkoff, Ron; Polly, Ben; Neymark, Joel

    2016-08-26

    This paper describes a method for testing model calibration techniques. Calibration is commonly used in conjunction with energy retrofit audit models. An audit is conducted to gather information about the building needed to assemble an input file for a building energy modeling tool. A calibration technique is used to reconcile model predictions with utility data, and then the 'calibrated model' is used to predict energy savings from a variety of retrofit measures and combinations thereof. Current standards and guidelines such as BPI-2400 and ASHRAE-14 set criteria for 'goodness of fit' and assume that if the criteria are met, then the calibration technique is acceptable. While it is logical to use the actual performance data of the building to tune the model, it is not certain that a good fit will result in a model that better predicts post-retrofit energy savings. Therefore, the basic idea here is that the simulation program (intended for use with the calibration technique) is used to generate surrogate utility bill data and retrofit energy savings data against which the calibration technique can be tested. This provides three figures of merit for testing a calibration technique, 1) accuracy of the post-retrofit energy savings prediction, 2) closure on the 'true' input parameter values, and 3) goodness of fit to the utility bill data. The paper will also discuss the pros and cons of using this synthetic surrogate data approach versus trying to use real data sets of actual buildings.

  20. Calibration analysis for water storage variability of the global hydrological model WGHM

    Directory of Open Access Journals (Sweden)

    S. Werth

    2009-07-01

    Full Text Available This study contributes to an improved global simulation of continental water storage variations by calibrating the WaterGAP Global Hydrology Model (WGHM for 28 of the largest river basins worldwide. Five years (01/2003–12/2007 of satellite-based estimates of total water storage changes from the GRACE mission are combined with river discharge data in a multi-objective calibration framework of the most sensitive WGHM model parameters. The uncertainty and significance of the calibration results is analyzed with respect to errors in the observation data. An independent simulation period (01/2008–12/2008 is used for validation. The contribution of single storage compartments to the total water budget before and after calibration is analyzed in detail. A multi-objective improvement of the model states is obtained for most of the river basins, with mean error reductions up to 110 km3/month for discharge and up to 24 mm of a water mass equivalent column for total water storage changes, as for the Amazon basin. Errors in phase and signal variability of seasonal water mass changes are reduced. The calibration is shown to primarily affect soil water storage in most river basins. The variability of groundwater storage variations is reduced at the global scale after calibration. Structural model errors are identified from a small contribution of surface water storage including wetlands in river basins with large inundation areas, such as the Amazon or the Mississippi. The results demonstrate the value of GRACE data and the multi-objective calibration approach for improvements of large-scale hydrological simulations, as they constitute a starting-point for improvements of model structure. The integration of complimentary observation data to further constrain the simulation of single storage compartments is encouraged.

  1. "Calibration-on-the-spot'': How to calibrate an EMCCD camera from its images

    DEFF Research Database (Denmark)

    Mortensen, Kim; Flyvbjerg, Henrik

    In localization-based microscopy, super-resolution is obtained by analyzing isolated diffraction-limited spots imaged, typically, with EMCCD cameras. To compare experiments and calculate localization precision, the photon-to-signal amplification factor is needed but unknown without a calibration...... of the camera. Here we show how this can be done post festum from just a recorded image. We demonstrate this (i) theoretically, mathematically, (ii) by analyzing images recorded with an EMCCD camera, and (iii) by analyzing simulated EMCCD images for which we know the true values of parameters. In summary, our...... method of calibration-on-the-spot allows calibration of a camera with unknown settings from old images on file, with no other info needed. Consequently, calibration-on-the-spot also makes future camera calibrations before and after measurements unnecessary, because the calibration is encoded in recorded...

  2. Revised landsat-5 thematic mapper radiometric calibration

    Science.gov (United States)

    Chander, G.; Markham, B.L.; Barsi, J.A.

    2007-01-01

    Effective April 2, 2007, the radiometric calibration of Landsat-5 (L5) Thematic Mapper (TM) data that are processed and distributed by the U.S. Geological Survey (USGS) Center for Earth Resources Observation and Science (EROS) will be updated. The lifetime gain model that was implemented on May 5, 2003, for the reflective bands (1-5, 7) will be replaced by a new lifetime radiometric-calibration curve that is derived from the instrument's response to pseudoinvariant desert sites and from cross calibration with the Landsat-7 (L7) Enhanced TM Plus (ETM+). Although this calibration update applies to all archived and future L5 TM data, the principal improvements in the calibration are for the data acquired during the first eight years of the mission (1984-1991), where the changes in the instrument-gain values are as much as 15%. The radiometric scaling coefficients for bands 1 and 2 for approximately the first eight years of the mission have also been changed. Users will need to apply these new coefficients to convert the calibrated data product digital numbers to radiance. The scaling coefficients for the other bands have not changed. ?? 2007 IEEE.

  3. NBS (National Bureau of Standards) measurement services: calibration of beta-particle-emitting ophthalmic applicators. Final report

    International Nuclear Information System (INIS)

    The service provides calibrations for (90)Sr + (90)Y beta-particle ophthalmic applicators. The calibration determines the average surface absorbed-dose rate to water over the active area of the applicator. The technique used is to measure current per unit mass of air at the active surface with an extrapolation ionization chamber, and to convert this into absorbed-dose rate with Bragg-Gray cavity ionization theory. The extrapolation chamber measurements are made in three parts. Data-book measurements and a calibration report are given for one particular applicator

  4. Calibration of the Hydrological Simulation Program Fortran (HSPF) model using automatic calibration and geographical information systems

    Science.gov (United States)

    Al-Abed, N. A.; Whiteley, H. R.

    2002-11-01

    Calibrating a comprehensive, multi-parameter conceptual hydrological model, such as the Hydrological Simulation Program Fortran model, is a major challenge. This paper describes calibration procedures for water-quantity parameters of the HSPF version 10·11 using the automatic-calibration parameter estimator model coupled with a geographical information system (GIS) approach for spatially averaged properties. The study area was the Grand River watershed, located in southern Ontario, Canada, between 79° 30 and 80° 57W longitude and 42° 51 and 44° 31N latitude. The drainage area is 6965 km2. Calibration efforts were directed to those model parameters that produced large changes in model response during sensitivity tests run prior to undertaking calibration. A GIS was used extensively in this study. It was first used in the watershed segmentation process. During calibration, the GIS data were used to establish realistic starting values for the surface and subsurface zone parameters LZSN, UZSN, COVER, and INFILT and physically reasonable ratios of these parameters among watersheds were preserved during calibration with the ratios based on the known properties of the subwatersheds determined using GIS. This calibration procedure produced very satisfactory results; the percentage difference between the simulated and the measured yearly discharge ranged between 4 to 16%, which is classified as good to very good calibration. The average simulated daily discharge for the watershed outlet at Brantford for the years 1981-85 was 67 m3 s-1 and the average measured discharge at Brantford was 70 m3 s-1. The coupling of a GIS with automatice calibration produced a realistic and accurate calibration for the HSPF model with much less effort and subjectivity than would be required for unassisted calibration.

  5. NuSTAR ground calibration: The Rainwater Memorial Calibration Facility (RaMCaF)

    DEFF Research Database (Denmark)

    Brejnholt, Nicolai; Christensen, Finn Erland; Jakobsen, Anders Clemen;

    2011-01-01

    The Nuclear Spectroscopic Telescope Array (NuSTAR) is a NASA Small Explorer mission that will carry the first focusing hard X-ray (5-80 keV ) telescope to orbit. The ground calibration of the three flight optics was carried out at the Rainwater Memorial Calibration Facility (RaMCaF) built for this...... purpose. In this article we present the facility and its use for the ground calibration of the three optics....

  6. Is Your System Calibrated? MRI Gradient System Calibration for Pre-Clinical, High-Resolution Imaging

    OpenAIRE

    James O'Callaghan; Jack Wells; Simon Richardson; Holly Holmes; Yichao Yu; Simon Walker-Samuel; Bernard Siow; Lythgoe, Mark F

    2014-01-01

    High-field, pre-clinical MRI systems are widely used to characterise tissue structure and volume in small animals, using high resolution imaging. Both applications rely heavily on the consistent, accurate calibration of imaging gradients, yet such calibrations are typically only performed during maintenance sessions by equipment manufacturers, and potentially with acceptance limits that are inadequate for phenotyping. To overcome this difficulty, we present a protocol for gradient calibration...

  7. Investigation of ground-based microwave radiometer calibration techniques at 530 hPa

    Directory of Open Access Journals (Sweden)

    G. Maschwitz

    2013-10-01

    Full Text Available Ground-based microwave radiometers (MWR are becoming more and more common for remotely sensing the atmospheric temperature and humidity profile as well as path-integrated cloud liquid water content. The calibration accuracy of the state-of-the-art MWR HATPRO-G2 (Humidity And Temperature Profiler – Generation 2 was investigated during the second phase of the Radiative Heating in Underexplored Bands Campaign (RHUBC-II in northern Chile (5320 m above mean sea level, 530 hPa conducted by the Atmospheric Radiation Measurement (ARM program conducted between August and October 2009. This study assesses the quality of the two frequently used liquid nitrogen and tipping curve calibrations by performing a detailed error propagation study, which exploits the unique atmospheric conditions of RHUBC-II. Both methods are known to have open issues concerning systematic offsets and calibration repeatability. For the tipping curve calibration an uncertainty of ±0.1 to ±0.2 K (K-band and ±0.6 to ±0.7 K (V-band is found. The uncertainty in the tipping curve calibration is mainly due to atmospheric inhomogeneities and the assumed air mass correction for the Earth curvature. For the liquid nitrogen calibration the estimated uncertainty of ±0.3 to ±1.6 K is dominated by the uncertainty of the reflectivity of the liquid nitrogen target. A direct comparison between the two calibration techniques shows that for six of the nine channels that can be calibrated with both methods, they agree within the assessed uncertainties. For the other three channels the unexplained discrepancy is below 0.5 K. Systematic offsets, which may cause the disagreement of both methods within their estimated uncertainties, are discussed.

  8. Energy calibration issues in nuclear resonant vibrational spectroscopy: observing small spectral shifts and making fast calibrations.

    Science.gov (United States)

    Wang, Hongxin; Yoda, Yoshitaka; Dong, Weibing; Huang, Songping D

    2013-09-01

    The conventional energy calibration for nuclear resonant vibrational spectroscopy (NRVS) is usually long. Meanwhile, taking NRVS samples out of the cryostat increases the chance of sample damage, which makes it impossible to carry out an energy calibration during one NRVS measurement. In this study, by manipulating the 14.4 keV beam through the main measurement chamber without moving out the NRVS sample, two alternative calibration procedures have been proposed and established: (i) an in situ calibration procedure, which measures the main NRVS sample at stage A and the calibration sample at stage B simultaneously, and calibrates the energies for observing extremely small spectral shifts; for example, the 0.3 meV energy shift between the 100%-(57)Fe-enriched [Fe4S4Cl4](=) and 10%-(57)Fe and 90%-(54)Fe labeled [Fe4S4Cl4](=) has been well resolved; (ii) a quick-switching energy calibration procedure, which reduces each calibration time from 3-4 h to about 30 min. Although the quick-switching calibration is not in situ, it is suitable for normal NRVS measurements.

  9. The BAHAMAS project: Calibrated hydrodynamical simulations for large-scale structure cosmology

    CERN Document Server

    McCarthy, Ian G; Bird, Simeon; Brun, Amandine M C Le

    2016-01-01

    The evolution of the large-scale distribution of matter is sensitive to a variety of fundamental parameters that characterise the dark matter, dark energy, and other aspects of our cosmological framework. Since the majority of the mass density is in the form of dark matter that cannot be directly observed, to do cosmology with large-scale structure one must use observable (baryonic) quantities that trace the underlying matter distribution in a (hopefully) predictable way. However, recent numerical studies have demonstrated that the mapping between observable and total mass, as well as the total mass itself, are sensitive to unresolved feedback processes associated with galaxy formation, motivating explicit calibration of the feedback efficiencies. Here we construct a new suite of large-volume cosmological hydrodynamical simulations (called BAHAMAS, for BAryons and HAloes of MAssive Systems) where subgrid models of stellar and Active Galactic Nucleus (AGN) feedback have been calibrated to reproduce the present...

  10. A calibration method for proposed XRF measurements of arsenic and selenium in nail clippings.

    Science.gov (United States)

    Gherase, Mihai R; Fleming, David E B

    2011-10-21

    A calibration method for proposed x-ray fluorescence (XRF) measurements of arsenic and selenium in nail clippings is demonstrated. Phantom nail clippings were produced from a whole nail phantom (0.7 mm thickness, 25 × 25 mm(2) area) and contained equal concentrations of arsenic and selenium ranging from 0 to 20 µg g(-1) in increments of 5 µg g(-1). The phantom nail clippings were then grouped in samples of five different masses: 20, 40, 60, 80 and 100 mg for each concentration. Experimental x-ray spectra were acquired for each of the sample masses using a portable x-ray tube and a detector unit. Calibration lines (XRF signal in a number of counts versus stoichiometric elemental concentration) were produced for each of the two elements. A semi-empirical relationship between the mass of the nail phantoms (m) and the slope of the calibration line (s) was determined separately for arsenic and selenium. Using this calibration method, one can estimate elemental concentrations and their uncertainties from the XRF spectra of human nail clippings. PMID:21937772

  11. A calibration method for proposed XRF measurements of arsenic and selenium in nail clippings

    Energy Technology Data Exchange (ETDEWEB)

    Gherase, Mihai R; Fleming, David E B, E-mail: mgherase@mta.ca [Physics Department, Mount Allison University, Sackville, New Brunswick, E4L 1E6 (Canada)

    2011-10-21

    A calibration method for proposed x-ray fluorescence (XRF) measurements of arsenic and selenium in nail clippings is demonstrated. Phantom nail clippings were produced from a whole nail phantom (0.7 mm thickness, 25 x 25 mm{sup 2} area) and contained equal concentrations of arsenic and selenium ranging from 0 to 20 {mu}g g{sup -1} in increments of 5 {mu}g g{sup -1}. The phantom nail clippings were then grouped in samples of five different masses: 20, 40, 60, 80 and 100 mg for each concentration. Experimental x-ray spectra were acquired for each of the sample masses using a portable x-ray tube and a detector unit. Calibration lines (XRF signal in a number of counts versus stoichiometric elemental concentration) were produced for each of the two elements. A semi-empirical relationship between the mass of the nail phantoms (m) and the slope of the calibration line (s) was determined separately for arsenic and selenium. Using this calibration method, one can estimate elemental concentrations and their uncertainties from the XRF spectra of human nail clippings. (note)

  12. A calibration method for proposed XRF measurements of arsenic and selenium in nail clippings

    Science.gov (United States)

    Gherase, Mihai R.; Fleming, David E. B.

    2011-10-01

    A calibration method for proposed x-ray fluorescence (XRF) measurements of arsenic and selenium in nail clippings is demonstrated. Phantom nail clippings were produced from a whole nail phantom (0.7 mm thickness, 25 × 25 mm2 area) and contained equal concentrations of arsenic and selenium ranging from 0 to 20 µg g-1 in increments of 5 µg g-1. The phantom nail clippings were then grouped in samples of five different masses: 20, 40, 60, 80 and 100 mg for each concentration. Experimental x-ray spectra were acquired for each of the sample masses using a portable x-ray tube and a detector unit. Calibration lines (XRF signal in a number of counts versus stoichiometric elemental concentration) were produced for each of the two elements. A semi-empirical relationship between the mass of the nail phantoms (m) and the slope of the calibration line (s) was determined separately for arsenic and selenium. Using this calibration method, one can estimate elemental concentrations and their uncertainties from the XRF spectra of human nail clippings.

  13. Calibrating the CsI(Tl) detectors of the GARFIELD apparatus

    Energy Technology Data Exchange (ETDEWEB)

    Abbondanno, U. E-mail: abbondanno@ts.infn.it; Bruno, M.; Casini, G.; Cavaletti, R.; Cavallaro, Sl.; Chiari, M.; D' Agostino, M.; Gramegna, F.; Lanchais, A.; Margagliotti, G.V.; Mastinu, P.F.; Milazzo, P.M.; Moroni, A.; Nannini, A.; Ordine, A.; Vannini, G.; Vannucci, L

    2002-08-11

    The energy and charge dependence of the light output of the CsI(Tl) detectors of the GARFIELD apparatus has been investigated for heavy ions with 5{<=}Z{<=}16 in the energy range from 2.2 to 8.3 A MeV. The results have been compared to an analytical expression successfully used in previous calibration procedures at higher energies, and a rather good agreement was obtained between measured and calculated quantities. The resulting parameter set was successfully applied to another set of experimental data. The overall result demonstrates the validity of the above mentioned calibration procedure in a wide range of incident ion energies and masses.

  14. Calibrating the CsI(Tl) detectors of the GARFIELD apparatus

    Science.gov (United States)

    Abbondanno, U.; Bruno, M.; Casini, G.; Cavaletti, R.; Cavallaro, Sl.; Chiari, M.; D'Agostino, M.; Gramegna, F.; Lanchais, A.; Margagliotti, G. V.; Mastinu, P. F.; Milazzo, P. M.; Moroni, A.; Nannini, A.; Ordine, A.; Vannini, G.; Vannucci, L.

    2002-08-01

    The energy and charge dependence of the light output of the CsI(Tl) detectors of the GARFIELD apparatus has been investigated for heavy ions with 5⩽ Z⩽16 in the energy range from 2.2 to 8.3 A MeV . The results have been compared to an analytical expression successfully used in previous calibration procedures at higher energies, and a rather good agreement was obtained between measured and calculated quantities. The resulting parameter set was successfully applied to another set of experimental data. The overall result demonstrates the validity of the above mentioned calibration procedure in a wide range of incident ion energies and masses.

  15. Calibrating the CsI(Tl) detectors of the GARFIELD apparatus

    CERN Document Server

    Abbondanno, U; Casini, G; Cavaletti, R; Cavallaro, S; Chiari, M; D'Agostino, M; Gramegna, F; Lanchais, A; Margagliotti, G V; Mastinu, P F; Milazzo, P M; Moroni, A; Nannini, A; Ordine, A; Vannini, G; Vannucci, L

    2002-01-01

    The energy and charge dependence of the light output of the CsI(Tl) detectors of the GARFIELD apparatus has been investigated for heavy ions with 5<=Z<=16 in the energy range from 2.2 to 8.3 A MeV. The results have been compared to an analytical expression successfully used in previous calibration procedures at higher energies, and a rather good agreement was obtained between measured and calculated quantities. The resulting parameter set was successfully applied to another set of experimental data. The overall result demonstrates the validity of the above mentioned calibration procedure in a wide range of incident ion energies and masses.

  16. A Calibration Routine for Efficient ETD in Large-Scale Proteomics

    Science.gov (United States)

    Rose, Christopher M.; Rush, Matthew J. P.; Riley, Nicholas M.; Merrill, Anna E.; Kwiecien, Nicholas W.; Holden, Dustin D.; Mullen, Christopher; Westphall, Michael S.; Coon, Joshua J.

    2015-11-01

    Electron transfer dissociation (ETD) has been broadly adopted and is now available on a variety of commercial mass spectrometers. Unlike collisional activation techniques, optimal performance of ETD requires considerable user knowledge and input. ETD reaction duration is one key parameter that can greatly influence spectral quality and overall experiment outcome. We describe a calibration routine that determines the correct number of reagent anions necessary to reach a defined ETD reaction rate. Implementation of this automated calibration routine on two hybrid Orbitrap platforms illustrate considerable advantages, namely, increased product ion yield with concomitant reduction in scan rates netting up to 75% more unique peptide identifications in a shotgun experiment.

  17. Dynamic Calibration of the NASA Ames Rotor Test Apparatus Steady/Dynamic Rotor Balance

    Science.gov (United States)

    Peterson, Randall L.; vanAken, Johannes M.

    1996-01-01

    The NASA Ames Rotor Test Apparatus was modified to include a Steady/Dynamic Rotor Balance. The dynamic calibration procedures and configurations are discussed. Random excitation was applied at the rotor hub, and vibratory force and moment responses were measured on the steady/dynamic rotor balance. Transfer functions were computed using the load cell data and the vibratory force and moment responses from the rotor balance. Calibration results showing the influence of frequency bandwidth, hub mass, rotor RPM, thrust preload, and dynamic loads through the stationary push rods are presented and discussed.

  18. First mass measurements at LHCb

    CERN Multimedia

    Bressieux, J

    2011-01-01

    The LHC opens new frontiers in heavy flavour physics through an unprecedented statistical reach for a variety of interesting states produced in pp collisions. The LHCb spectrometer provides a good mass resolution and is suitable for spectroscopy studies. We present first preliminary mass measurements of several $b$ hadrons and of the exotic $X(3872)$ meson, reconstructed in final states containing a $J/\\psi$ using the data collected in 2010 by the LHCb experiment. An important aspect of the analysis is the calibration of the momentum scale using $J/\\psi \\to \\mu^+ \\mu^-$ decays, as well as the control of systematic uncertainties. While the already very competitive mass measurements for the $B^+$, $B^0$ and $B^0_s$ mesons receive similar contributions from systematic and statistical uncertainties, those of the $\\Lambda_b$, $B^+_c$ and $X(3872)$ particles are dominated by statistical uncertainties, and will therefore substantially improve with more data in the future.

  19. Mass hysteria

    CERN Document Server

    Hellemans, Alexander

    2004-01-01

    Considerable research is being undertaken to identify the Higgs particle that is believed to give things their mass. According to the standard model, what we call mass is really an indication of how strongly particles interact with an invisible syrupy substance called the Higgs field. Quantum mechanics say that the mass-giving field can also be thought of as a sea of electrically neutral Higgs particles that should be dislodged in collisions between subatomic particles with high enough energies. Particle physicists expect the Higgs to exist only for a fleeting moment before decaying into other particles, which are caught in a detector. (Edited abstract).

  20. Calibration Of Partial-Pressure-Of-Oxygen Sensors

    Science.gov (United States)

    Yount, David W.; Heronimus, Kevin

    1995-01-01

    Report and analysis of, and discussion of improvements in, procedure for calibrating partial-pressure-of-oxygen sensors to satisfy Spacelab calibration requirements released. Sensors exhibit fast drift, which results in short calibration period not suitable for Spacelab. By assessing complete process of determining total drift range available, calibration procedure modified to eliminate errors and still satisfy requirements without compromising integrity of system.

  1. The ISO SWS Calibration: Strategy and Lessons Learned

    NARCIS (Netherlands)

    Roelfsema, P. R.; Valentijn, E. A.; Bauer, O. H.; Beintema, D. A.; Boxhoorn, D. R.; Feuchtgruber, H.; de Graauw, T.; Heras, A. M.; Huygen, R.; Kester, D. J. M.; Lahuis, F.; Leech, K.; Lorente, R.; Morris, P. W.; Salama, A.; Schaeidt, S. G.; Shipman, R. F.; Vandenbussche, B.; Weiprecht, E.

    2003-01-01

    Instrument calibration can be seen as having several different components; clearly there is the use of specific calibration tools according to specific procedures on well defined data sets to yield calibration parameters. Also the application of such calibration parameters to data is part of the gen

  2. 21 CFR 874.1080 - Audiometer calibration set.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Audiometer calibration set. 874.1080 Section 874...) MEDICAL DEVICES EAR, NOSE, AND THROAT DEVICES Diagnostic Devices § 874.1080 Audiometer calibration set. (a) Identification. An audiometer calibration set is an electronic reference device that is intended to calibrate...

  3. The DiskMass Survey : II. Error Budget

    NARCIS (Netherlands)

    Bershady, Matthew A.; Verheijen, Marc A. W.; Westfall, Kyle B.; Andersen, David R.; Swaters, Rob A.; Martinsson, Thomas

    2010-01-01

    We present a performance analysis of the DiskMass Survey. The survey uses collisionless tracers in the form of disk stars to measure the surface density of spiral disks, to provide an absolute calibration of the stellar mass-to-light ratio (Gamma(*)), and to yield robust estimates of the dark-matter

  4. Calibration Matters: Advances in Strapdown Airborne Gravimetry

    Science.gov (United States)

    Becker, D.

    2015-12-01

    Using a commercial navigation-grade strapdown inertial measurement unit (IMU) for airborne gravimetry can be advantageous in terms of cost, handling, and space consumption compared to the classical stable-platform spring gravimeters. Up to now, however, large sensor errors made it impossible to reach the mGal-level using such type IMUs as they are not designed or optimized for this kind of application. Apart from a proper error-modeling in the filtering process, specific calibration methods that are tailored to the application of aerogravity may help to bridge this gap and to improve their performance. Based on simulations, a quantitative analysis is presented on how much IMU sensor errors, as biases, scale factors, cross couplings, and thermal drifts distort the determination of gravity and the deflection of the vertical (DOV). Several lab and in-field calibration methods are briefly discussed, and calibration results are shown for an iMAR RQH unit. In particular, a thermal lab calibration of its QA2000 accelerometers greatly improved the long-term drift behavior. Latest results from four recent airborne gravimetry campaigns confirm the effectiveness of the calibrations applied, with cross-over accuracies reaching 1.0 mGal (0.6 mGal after cross-over adjustment) and DOV accuracies reaching 1.1 arc seconds after cross-over adjustment.

  5. Evolution of Altimetry Calibration and Future Challenges

    Science.gov (United States)

    Fu, Lee-Lueng; Haines, Bruce J.

    2012-01-01

    Over the past 20 years, altimetry calibration has evolved from an engineering-oriented exercise to a multidisciplinary endeavor driving the state of the art. This evolution has been spurred by the developing promise of altimetry to capture the large-scale, but small-amplitude, changes of the ocean surface containing the expression of climate change. The scope of altimeter calibration/validation programs has expanded commensurately. Early efforts focused on determining a constant range bias and verifying basic compliance of the data products with mission requirements. Contemporary investigations capture, with increasing accuracies, the spatial and temporal characteristics of errors in all elements of the measurement system. Dedicated calibration sites still provide the fundamental service of estimating absolute bias, but also enable long-term monitoring of the sea-surface height and constituent measurements. The use of a network of island and coastal tide gauges has provided the best perspective on the measurement stability, and revealed temporal variations of altimeter measurement system drift. The cross-calibration between successive missions provided fundamentally new information on the performance of altimetry systems. Spatially and temporally correlated errors pose challenges for future missions, underscoring the importance of cross-calibration of new measurements against the established record.

  6. WFC3: Improved WFC3 Calibration Products

    Science.gov (United States)

    Gunning, Heather C.; Sosey, M. L.; Anderson, J.; Lee, J. C.; Pirzkal, N.; MacKenty, J. W.; Kozhurina-Platais, V.; Deustua, S. E.; Hammer, D.; Dahlen, T.; Sabbi, E.; Mack, J.; Baggett, S. M.; WFC3 Team

    2014-01-01

    The Wide Field Camera 3 (WFC3) is a fourth-generation UV/visible and IR imaging instrument on the Hubble Space Telescope (HST). Installed in May 2009, during HST servicing mission 4, both channels have been performing very well on-orbit. To provide optimum calibrated data, the WFC3 team routinely updates and refines the calibration software and associated files, designated as calibration products. We present some of the recently improved calibration products that will be of interest to current and future users of WFC3, including information on the chip-dependent zeropoints and flat fields, post-flash calibrations, and detector-to-image distortion corrections. The latter results in four new extensions (two per chip and dimension), in all UVIS FLTs retrieved from MAST after September 10, 2013. The D2IMFILE contains astrometric corrections for shifts of the raw X and Y positions induced by the lithographic-mask pattern. We discuss the migration of CALWF3 from the STSDAS package to HSTCAL, a package independent of IRAF; as a consequence, the IRAF/STSDAS version of CALWF3 is no longer being updated. Finally, we summarize recent improvements to aXe, a PyRAF/IRAF software package that enables automated extraction of spectra from WFC3 slitless spectral (grism) images. Updated versions of aXe are made available as part of the STSDAS testing environment (SSBX).

  7. Adaptable Multivariate Calibration Models for Spectral Applications

    Energy Technology Data Exchange (ETDEWEB)

    THOMAS,EDWARD V.

    1999-12-20

    Multivariate calibration techniques have been used in a wide variety of spectroscopic situations. In many of these situations spectral variation can be partitioned into meaningful classes. For example, suppose that multiple spectra are obtained from each of a number of different objects wherein the level of the analyte of interest varies within each object over time. In such situations the total spectral variation observed across all measurements has two distinct general sources of variation: intra-object and inter-object. One might want to develop a global multivariate calibration model that predicts the analyte of interest accurately both within and across objects, including new objects not involved in developing the calibration model. However, this goal might be hard to realize if the inter-object spectral variation is complex and difficult to model. If the intra-object spectral variation is consistent across objects, an effective alternative approach might be to develop a generic intra-object model that can be adapted to each object separately. This paper contains recommendations for experimental protocols and data analysis in such situations. The approach is illustrated with an example involving the noninvasive measurement of glucose using near-infrared reflectance spectroscopy. Extensions to calibration maintenance and calibration transfer are discussed.

  8. Polarimetric PALSAR System Model Assessment and Calibration

    Science.gov (United States)

    Touzi, R.; Shimada, M.

    2009-04-01

    Polarimetric PALSAR system parameters are assessed using data sets collected over various calibration sites. The data collected over the Amazonian forest permits validating the zero Faraday rotation hypotheses near the equator. The analysis of the Amazonian forest data and the response of the corner reflectors deployed during the PALSAR acquisitions lead to the conclusion that the antenna is highly isolated (better than -35 dB). Theses results are confirmed using data collected over the Sweden and Ottawa calibration sites. The 5-m height trihedrals deployed in the Sweden calibration site by the Chalmers University of technology permits accurate measurement of antenna parameters, and detection of 2-3 degree Faraday rotation during day acquisition, whereas no Faraday rotation was noted during night acquisition. Small Faraday rotation angles (2-3 degree) have been measured using acquisitions over the DLR Oberpfaffenhofen and the Ottawa calibration sites. The presence of small but still significant Faraday rotation (2-3 degree) induces a CR return at the crosspolarization HV and VH that should not be interpreted as the actual antenna cross-talk. PALSAR antenna is highly isolated (better than -35 dB), and diagonal antenna distortion matrices (with zero cross-talk terms) can be used for accurate calibration of PALSAR polarimetric data.

  9. Numerical calibration of a Lorentz force flowmeter

    International Nuclear Information System (INIS)

    Numerical simulation of complex-shaped devices for contactless electromagnetic flow measurement in metallurgy is a challenge for computational magnetohydrodynamics. We report a series of numerical simulations which demonstrate for the first time that it is possible to predict the calibration constant of a generic Lorentz force flowmeter (LFF) with an uncertainty close to the requirements of real-life industrial applications. Our simulations involve both magnetostatic computations of a complex-shaped magnet system and magnetohydrodynamic computations of the flow of a liquid metal in a nozzle under the influence of a predominantly transverse magnetic field. In order to assess the role of turbulence, the simulations have been performed both for laminar and for turbulent flows using Reynolds-averaged Navier–Stokes equations in the latter case. In addition to the numerical simulations we have measured the calibration constant of the considered LFF using room-temperature liquid metal instead of liquid aluminum. A comparison between the numerically predicted and the measured values of the calibration constant shows that they differ by only 3.4%. This result suggests that numerical calibration of a LFF may become an economic alternative to expensive full-scale experimental calibration. (paper)

  10. Various methods and developments for calibrating seismological sensors at EOST

    Science.gov (United States)

    JUND, H.; Bès de Berc, M.; Thore, J.

    2013-12-01

    Calibrating seismic sensors is crucial for knowing the quality of the sensor and generating precise dataless files. We present here three calibration methods that we have developed for the short period and broad band sensors included in the temporary and permanent seismic networks in France. First, in the case of a short-period sensor with no electronics and calibration coil, we inject a sine wave signal into the signal coil. After locking the sensor mass, we first connect a voltage generator of signal waves and a series resistor to the coil. Then, a sinusoidal signal is sent to the sensor signal coil output. Both the voltage at the terminal of the resistor, which gives an image of the intensity entering the signal coil, and the voltage at the terminal of the signal coil are measured. The frequency of the generator then varies in order to find a phase shift between both signals of π/2. The output frequency of the generator corresponds to the image of the natural frequency of the sensor. Second, in the case of all types of sensors provided with a calibration coil, we inject different signals into the calibration coil. We usually apply two signals: a step signal and a sweep (or wobble) signal. A step signal into the calibration coil is equivalent to a Dirac excitation in derived acceleration. The response to this Dirac gives the transfer function of the signal coil, derived two times and without absolute gain. We developed a field-module allowing us to always apply the same excitation to various models of seismometers, in order to compare the results from several instruments previously installed on field. A wobble signal is a signal whose frequency varies. By varying the frequency of the input signal around the sensor's natural frequency, we obtain an immediate response of the sensor in acceleration. This method is particularly suitable in order to avoid any disturbances which may modify the signal of a permanent station. Finally, for the determination of absolute

  11. Scrotal masses

    Science.gov (United States)

    ... The scrotum is the sac that contains the testicles. ... Symptoms include: Enlarged scrotum Painless or painful testicle lump ... If the scrotal mass is part of the testicle, it has a higher risk of being cancerous. ...

  12. SCIAMACHY Level 1 data: calibration concept and in-flight calibration

    NARCIS (Netherlands)

    Lichtenberg, G.; Kleipool, Q.; Krijger, J.M.; Soest, G. van; Hees, R. van; Tilstra, L.G.; Acarreta, J.R.; Aben, I.; Ahlers, B.; Bovensmann, H.; Chance, K.; Gloudemans, A.M.S.; Hoogeveen, R.W.M.; Jongma, R.T.N.; Noël, S.; Piters, A.; Schrijver, H.; Schrijvers, C.; Sioris, C.E.; Skupin, J.; Slijkhuis, S.; Stammes, P.; Wuttke, M.

    2006-01-01

    The calibration of SCIAMACHY was thoroughly checked since the instrument was launched on-board ENVISAT in February 2002. While SCIAMACHY's functional performance is excellent since launch, a number of technical difficulties have appeared, that required adjustments to the calibration. The problems ca

  13. An Optimal Calibration Method for a MEMS Inertial Measurement Unit

    Directory of Open Access Journals (Sweden)

    Bin Fang

    2014-02-01

    Full Text Available An optimal calibration method for a micro-electro-mechanical inertial measurement unit (MIMU is presented in this paper. The accuracy of the MIMU is highly dependent on calibration to remove the deterministic errors of systematic errors, which also contain random errors. The overlapping Allan variance is applied to characterize the types of random error terms in the measurements. The calibration model includes package misalignment error, sensor-to-sensor misalignment error and bias, and a scale factor is built. The new concept of a calibration method, which includes a calibration scheme and a calibration algorithm, is proposed. The calibration scheme is designed by D-optimal and the calibration algorithm is deduced by a Kalman filter. In addition, the thermal calibration is investigated, as the bias and scale factor varied with temperature. The simulations and real tests verify the effectiveness of the proposed calibration method and show that it is better than the traditional method.

  14. e-Calibrations: using the Internet to deliver calibration services in real time at lower cost

    International Nuclear Information System (INIS)

    The National Institute of Standards and Technology (NIST) is expanding into a new frontier in the delivery of measurement services. The Internet will be employed to provide industry with electronic traceability to national standards. This is a radical departure from the traditional modes of traceability and presents many new challenges. The traditional mail-based calibration service relies on sending artifacts to the user, who then mails them back to NIST for evaluation. The new service will deliver calibration results to the industry customer on-demand, in real-time, at a lower cost. The calibration results can be incorporated rapidly into the production process to ensure the highest quality manufacturing. The service would provide the US radiation processing industry with a direct link to the NIST calibration facilities and its expertise, and provide an interactive feedback process between industrial processing and the national measurement standard. Moreover, an Internet calibration system should contribute to the removal of measurement-related trade barriers

  15. New fully empirical calibrations of strong-line metallicity indicators in star forming galaxies

    CERN Document Server

    Curti, M; Mannucci, F; Marconi, A; Maiolino, R; Esposito, S

    2016-01-01

    We derive new empirical calibrations for strong-line diagnostics of gas phase metallicity in local star forming galaxies by uniformly applying the Te method over the full metallicity range probed by the Sloan Digital Sky Survey (SDSS). To measure electron temperatures at high metallicity, where the auroral lines needed are not detected in single galaxies, we stacked spectra of more than 110,000 galaxies from the SDSS in bins of log[O II]/H$\\beta$ and log[O III]/H$\\beta$. This stacking scheme does not assume any dependence of metallicity on mass or star formation rate, but only that galaxies with the same line ratios have the same oxygen abundance. We provide calibrations which span more than 1 dex in metallicity and are entirely defined on a consistent absolute Te metallicity scale for galaxies. We apply our calibrations to the SDSS sample and find that they provide consistent metallicity estimates to within 0.05 dex.

  16. The cryogenic balance design and balance calibration methods

    Science.gov (United States)

    Ewald, B.; Polanski, L.; Graewe, E.

    1992-07-01

    The current status of a program aimed at the development of a cryogenic balance for the European Transonic Wind Tunnel is reviewed. In particular, attention is given to the cryogenic balance design philosophy, mechanical balance design, reliability and accuracy, cryogenic balance calibration concept, and the concept of an automatic calibration machine. It is shown that the use of the automatic calibration machine will improve the accuracy of calibration while reducing the man power and time required for balance calibration.

  17. A Review of Sensor Calibration Monitoring for Calibration Interval Extension in Nuclear Power Plants

    Energy Technology Data Exchange (ETDEWEB)

    Coble, Jamie B.; Meyer, Ryan M.; Ramuhalli, Pradeep; Bond, Leonard J.; Hashemian, Hash; Shumaker, Brent; Cummins, Dara

    2012-08-31

    Currently in the United States, periodic sensor recalibration is required for all safety-related sensors, typically occurring at every refueling outage, and it has emerged as a critical path item for shortening outage duration in some plants. Online monitoring can be employed to identify those sensors that require calibration, allowing for calibration of only those sensors that need it. International application of calibration monitoring, such as at the Sizewell B plant in United Kingdom, has shown that sensors may operate for eight years, or longer, within calibration tolerances. This issue is expected to also be important as the United States looks to the next generation of reactor designs (such as small modular reactors and advanced concepts), given the anticipated longer refueling cycles, proposed advanced sensors, and digital instrumentation and control systems. The U.S. Nuclear Regulatory Commission (NRC) accepted the general concept of online monitoring for sensor calibration monitoring in 2000, but no U.S. plants have been granted the necessary license amendment to apply it. This report presents a state-of-the-art assessment of online calibration monitoring in the nuclear power industry, including sensors, calibration practice, and online monitoring algorithms. This assessment identifies key research needs and gaps that prohibit integration of the NRC-approved online calibration monitoring system in the U.S. nuclear industry. Several needs are identified, including the quantification of uncertainty in online calibration assessment; accurate determination of calibration acceptance criteria and quantification of the effect of acceptance criteria variability on system performance; and assessment of the feasibility of using virtual sensor estimates to replace identified faulty sensors in order to extend operation to the next convenient maintenance opportunity. Understanding the degradation of sensors and the impact of this degradation on signals is key to

  18. Control console of the gamma calibration room

    International Nuclear Information System (INIS)

    The Nuclear Centre of Mexico has a Ionizing Radiation Metrology Center (CMRI). This is in charge of the calibration in Mexico and Latin America of equipment dedicated to radiation measurement as industrial, medical as other fields. The importance to ensure that the equipment stay justly calibrated, it is imposed the necessity of automating the different rooms which the CMRI has. in this case it will be exposed the Calibration room for gamma radiation type. The operation of this application was carried out with the LabVIEW development platform and also in C language. The hardware associated is: personal computer with two cards using the 8255 device, 16 channels with optical isolation to manage input/output TTL type, 16 channels with optical isolation to management of charges to 127 V a.c., and 2 channels for 90V d.c. motors. (Author)

  19. Multichannel radiometer calibration: a new approach

    Science.gov (United States)

    Diaz, Susana; Booth, Charles R.; Armstrong, Roy; Brunat, Claudio; Cabrera, Sergio; Camilion, Carolina; Casiccia, Claudio; Deferrari, Guillermo; Fuenzalida, Humberto; Lovengreen, Charlotte; Paladini, Alejandro; Pedroni, Jorge; Rosales, Alejandro; Zagarese, Horacio; Vernet, Maria

    2005-09-01

    The error in irradiance measured with Sun-calibrated multichannel radiometers may be large when the solar zenith angle (SZA) increases. This could be particularly detrimental in radiometers installed at mid and high latitudes, where SZAs at noon are larger than 50° during part of the year. When a multiregressive methodology, including the total ozone column and SZA, was applied in the calculation of the calibration constant, an important improvement was observed. By combining two different equations, an improvement was obtained at almost all the SZAs in the calibration. An independent test that compared the irradiance of a multichannel instrument and a spectroradiometer installed in Ushuaia, Argentina, was used to confirm the results.

  20. A Calibrating Device for Rogowski Coil Development

    Institute of Scientific and Technical Information of China (English)

    LV Liang; LI Junhao; HUANG Jianjun; JI Shengchang; LI Yanming

    2007-01-01

    A calibrating device for the Rogowski coil is developed,which can be used to calibrate the Rogowski coil having a partial response time within tens of nanoseconds.Its key component is a step current generator,which can generate the output with a rise time of less than 2 ns and a duration of larger than 300 ns.The step current generator is composed by a pulse forming line(PFL)and a pulse transmission line(PTL).A TEM(transverse electromagnetic mode)coaxial measurement unit is used as PTL,and the coil to be calibrated and the referenced standard Rogowski coil can be fixed in the unit.The effect of the dimensions of the TEM unit is discussed theoretically as well as experimentally.

  1. ATLAS Tile calorimeter calibration and monitoring systems

    CERN Document Server

    Chomont, Arthur Rene; The ATLAS collaboration

    2016-01-01

    The ATLAS Tile Calorimeter (TileCal) is the central section of the hadronic calorimeter of the ATLAS experiment and provides important information for reconstruction of hadrons, jets, hadronic decays of tau leptons and missing transverse energy. This sampling calorimeter uses steel plates as absorber and scintillating tiles as active medium. The light produced by the passage of charged particles is transmitted by wavelength shifting fibres to photomultiplier tubes (PMTs), located on the outside of the calorimeter. The readout is segmented into about 5000 cells (longitudinally and transversally), each of them being read out by two PMTs in parallel. To calibrate and monitor the stability and performance of each part of the readout chain during the data taking, a set of calibration systems is used. The TileCal calibration system comprises Cesium radioactive sources, laser and charge injection elements and it allows to monitor and equalize the calorimeter response at each stage of the signal production, from scin...

  2. Oregon State TRIGA reactor power calibration study

    International Nuclear Information System (INIS)

    As a result of a recent review of the Oregon State TRIGA Reactor (OSTR) power calibration procedure, an investigation was performed on the origin and correctness of the OSTR tank factor and the calibration method. It was determined that there was no clear basis for the tank factor which was being used (0.0525 deg. C/kwh) and therefore a new value was calculated (0.0493 deg. C/kwh). The calculational method and likely errors are presented in the paper. In addition, a series of experimental tests were conducted to decide if the power calibration was best performed with or without a mixer, at 100 KW or at 1 MW. The results of these tests along with the final recommendation are presented. (author)

  3. Ion Beam Energy Calibration Method for Accelerator

    International Nuclear Information System (INIS)

    Ion beam energy calibration methods, i e : nuclear reaction method, magnetic field method and calorimeter method were elaborated and studied from its advantage and disadvantage in this paper. Ion beam energy calibration method for accelerator using the method of magnetic field on 3 MV Tandem Accelerator have been carried out at Tiara, JAERI, Japan. The result showed that the energy of ion beam current is 43.56 keV. The result of study conclude that nuclear reaction method generally used to calibrate ion beam energy at the accelerator of energy larger than 2 MeV, calorimetric method for the accelerator electron including linac, magnetic field method for all particle type of accelerator. (author)

  4. Absolute radiometric calibration of the CCRS SAR

    Science.gov (United States)

    Ulander, Lars M. H.; Hawkins, Robert K.; Livingstone, Charles E.; Lukowski, Tom I.

    1991-11-01

    Determining the radar scattering coefficients from SAR (synthetic aperture radar) image data requires absolute radiometric calibration of the SAR system. The authors describe an internal calibration methodology for the airborne Canada Centre for Remote Sensing (CCRS) SAR system, based on radar theory, a detailed model of the radar system, and measurements of system parameters. The methodology is verified by analyzing external calibration data acquired over a 6-month period in 1988 by the C-band radar using HH polarization. The results indicate that the overall error is +/- 0.8 dB (1-sigma) for incidence angles +/- 20 deg from antenna boresight. The dominant error contributions are due to the antenna radome and uncertainties in the elevation angle relative to the antenna boresight.

  5. Kinematic calibration of orthoglide-type mechanisms

    CERN Document Server

    Pashkevich, Anatoly; Wenger, Philippe

    2006-01-01

    The paper proposes a novel calibration approach for the Orthoglide-type mechanisms based on observations of the manipulator leg parallelism during mo-tions between the prespecified test postures. It employs a low-cost measuring system composed of standard comparator indicators attached to the universal magnetic stands. They are sequentially used for measuring the deviation of the relevant leg location while the manipulator moves the TCP along the Cartesian axes. Using the measured differences, the developed algorithm estimates the joint offsets that are treated as the most essential parameters to be adjusted. The sensitivity of the meas-urement methods and the calibration accuracy are also studied. Experimental re-sults are presented that demonstrate validity of the proposed calibration technique

  6. Muon Calibration at SoLid

    CERN Document Server

    Saunders, Daniel

    2016-01-01

    The SoLid experiment aims to make a measurement of very short distance neutrino oscillations using reactor antineutrinos. Key to its sensitivity are the experiments high spatial and energy resolution, combined with a very suitable reactor source and efficient background rejection. The fine segmentation of the detector (cubes of side 5cm), and ability to resolve signals in space and time, gives SoLid the capability to track cosmic muons. In principle a source of background, these turn into a valuable calibration source if they can be cleanly identified. This work presents the first energy calibration results, using cosmic muons, of the 288kg SoLid prototype SM1. This includes the methodology of tracking at SoLid, cosmic ray angular analyses at the reactor site, estimates of the time resolution, and calibrations at the cube level.

  7. Calibration of mixed-polarization interferometric observations

    CERN Document Server

    Marti-Vidal, Ivan; Conway, John; Zensus, Anton J

    2016-01-01

    Heterodyne receivers register the sky signal on either a circular polarization basis (where it is split into left-hand and right-hand circular polarization) or a linear polarization basis (where it is split into horizontal and vertical linear polarization). We study the problem of interferometric observations performed with telescopes that observe on different polarization bases, hence producing visibilities that we call "mixed basis" (i.e., linear in one telescope and circular in the other). We present novel algorithms for the proper calibration and treatment of such interferometric observations and test our algorithms with both simulations and real data. The use of our algorithms will be important for the optimum calibration of forthcoming observations with the Atacama Large mm/submm Array (ALMA) in very-long-baseline interferometry (VLBI) mode. Our algorithms will also allow us to optimally calibrate future VLBI observations at very high data rates (i.e., wide bandwidths), where linear-polarization feeds w...

  8. Status Update: Uranyl Nitrate Calibration Loop Equipment (UNCLE) at ORNL

    International Nuclear Information System (INIS)

    The successful completion of a field trial of safeguards monitoring equipment at a natural uranium conversion plant (NUCP) demonstrated the need for a facility in which to perform full-scale equipment testing under controlled conditions prior to field deployment of safeguards systems at additional plants. Oak Ridge National Laboratory has developed a Uranyl Nitrate Calibration Loop Equipment (UNCLE) facility to simulate the full-scale operating conditions for a purified uranium-bearing aqueous stream exiting the solvent extraction process conducted in an NUCP. In addition to calibrating instruments such as the neutron detector developed at Los Alamos National Laboratory, UNCLE will be used to test other in-line instruments (mass and volumetric flowmeters, spectrophotometers, etc.). UNCLE will be able to test commercially available equipment, such as the Endress+Hauser Promass 83F Coriolis meter that was used in the field test and other equipment that is presently under development. UNCLE is designed to accommodate different pipe sizes, flow rates, solution concentrations, and other variables of interest. Construction is expected to be completed by the end of September 2008 with initial testing beginning later that year. The design and current status of UNCLE will be presented, along with the capabilities of the facility and the proposed test plans.

  9. Calibration of PIXE-SP system of elementary analysis

    International Nuclear Information System (INIS)

    The set-up and calibration of the PIXE-SP System of Elementary Analysis located at the Institute of Physics of the University of Sao Paulo is described. The PIXE-SP, that operates with 8 MeV alpha beam, has been calibrated for elements with Z >= 11, by means of homemade evaporated standard targets of Al, Si, Bacl2, K2CrO4, Ti, Cr, Mn, Fe, Cu, Ge, Ag, Sn, and Au. Those targets are thin, homogeneous, and have been calbrated on a microbalance within an average precision of 6%. The overall precision of the PIXE-SP System is estimated in 10% for elements with 16 2 thick, irradiated with a 10 μC electric charge, shows a minimum of about 0,1 ng (approximated 4 ppm) for Mn. The PIXE-SP System has also been intercalibrated with the PIXE located at University of Gent, Belgium, by means of 12 atmospheric aerosol targets collected on two Batelle Cascade Impactors. The analyzed masses of elements with 16 <= Z < 30 agree within 20%. (Author)

  10. Calibration of the Ogawa passive ozone sampler for aircraft cabins

    Science.gov (United States)

    Bhangar, Seema; Singer, Brett C.; Nazaroff, William W.

    2013-02-01

    Elevated ozone levels in aircraft cabins would pose a health hazard to exposed passengers and crew. The Ogawa passive sampler is a potentially useful tool for measuring in-cabin ozone levels. Accurate interpretation of measured values requires knowing the effective collection rate of the sampler. To calibrate the passive sampler for the aircraft-cabin environment, ozone was measured simultaneously with an Ogawa sampler and an active ozone analyzer that served as a transfer standard, on 11 commercial passenger flights, during Feb-Apr 2007. An empirical pressure-independent effective collection rate that can be used to convert nitrate mass to ozone mixing ratio was determined to be 14.3 ± 0.9 atm cm3 min-1 (mean ± standard error). This value is similar to estimates from other applications where airflow rates are low, such as in personal monitoring and in chamber studies. This study represents the first field calibration of any passive sampler for the aircraft cabin environment.

  11. Precision cluster mass determination from weak lensing

    CERN Document Server

    Mandelbaum, Rachel; Baldauf, Tobias; Smith, Robert E

    2009-01-01

    Weak gravitational lensing has been used extensively in the past decade to constrain the masses of galaxy clusters, and is the most promising observational technique for providing the mass calibration necessary for precision cosmology with clusters. There are several challenges in estimating cluster masses, particularly (a) the sensitivity to astrophysical effects and observational systematics that modify the signal relative to the theoretical expectations, and (b) biases that can arise due to assumptions in the mass estimation method, such as the assumed radial profile of the cluster. All of these challenges are more problematic in the inner regions of the cluster, suggesting that their influence would ideally be suppressed for the purpose of mass estimation. However, at any given radius the differential surface density measured by lensing is sensitive to all mass within that radius, and the corrupted signal from the inner parts is spread out to all scales. We develop a new statistic that is ideal for estima...

  12. The Field White Dwarf Mass Distribution

    CERN Document Server

    Tremblay, P -E; Kalirai, J S; Gaensicke, B T; Gentile-Fusillo, N; Raddi, R

    2016-01-01

    We revisit the properties and astrophysical implications of the field white dwarf mass distribution in preparation of Gaia applications. Our study is based on the two samples with the best established completeness and most precise atmospheric parameters, the volume-complete survey within 20 pc and the Sloan Digital Sky Survey (SDSS) magnitude-limited sample. We explore the modelling of the observed mass distributions with Monte Carlo simulations, but find that it is difficult to constrain independently the initial mass function (IMF), the initial-to-final-mass relation (IFMR), the stellar formation history (SFH), the variation of the Galactic disk vertical scale height as a function of stellar age, and binary evolution. Each of these input ingredients has a moderate effect on the predicted mass distributions, and we must also take into account biases owing to unidentified faint objects (20 pc sample), as well as unknown masses for magnetic white dwarfs and spectroscopic calibration issues (SDSS sample). Never...

  13. Calibration of radiation protection monitoring equipment

    International Nuclear Information System (INIS)

    The facilities and equipment required for calibrating radiation protection monitoring equipment are both complex and expensive. The staff required to operate the equipment and perform the standardization have to be experienced, well trained and technically competent in the use of secondary or primary radiation standards and equipment. Thus an organization cannot commit considerable resources to perform calibration work purely for academic or scientific reasons. In most cases it must be justified by legal requirements pertaining within the country. These legal requirements on measuring devices for radiation protection purposes may be broadly divided into those relating to instruments intended for area monitoring and to those intended for individual monitoring

  14. New volumetric technique for calibrating neutron probes

    International Nuclear Information System (INIS)

    Studies in laboratory conditions were carried out to determine neutron calibration curves. Soils were packer in barrels to attain values of bulk density similar to those in the field. A mariotte reservoir supplies water to the barels in a way that keeps a water table of 10 cm. A water flow is established from this saturated region to the top of the barrel. The water depth is correlated to the numerical integration of the count rate with depth during the process of capillary tise. The coefficient of determination was 0.999. The calibration curve was independent of the initial misture contents of the soil profile. (author)

  15. Time calibration of the ANTARES neutrino telescope

    International Nuclear Information System (INIS)

    The ANTARES deep-sea neutrino telescope comprises a three-dimensional array of photomultipliers to detect the Cherenkov light induced by upgoing relativistic charged particles originating from neutrino interactions in the vicinity of the detector. The large scattering length of light in the deep sea facilitates an angular resolution of a few tenths of a degree for neutrino energies exceeding 10 TeV. In order to achieve this optimal performance, the time calibration procedures should ensure a relative time calibration between the photomultipliers at the level of 1 ns. The methods developed to attain this level of precision are described. (authors)

  16. Intercomparison of Laboratory Radiance Calibration Standards

    Science.gov (United States)

    Pavri, Betina; Chrien, Tom; Green, Robert; Williams, Orlesa

    2000-01-01

    Several standards for radiometric calibration were measured repeatedly with a spectroradiometer in order to understand how they compared in accuracy and stability. The tested radiance standards included a NIST 1000 W bulb and halon panel, two calibrated and stabilized integrating spheres, and a cavity blackbody. Results indicate good agreement between the blackbody and 1000 W bulb/spectralon panel, If these two radiance sources are assumed correct, then the integrating spheres did not conform. to their manufacturer-reported radiances in several regions of the spectrum. More detailed measurements am underway to investigate the discrepancy.

  17. Calibrating Images from the MINERVA Cameras

    Science.gov (United States)

    Mercedes Colón, Ana

    2016-01-01

    The MINiature Exoplanet Radial Velocity Array (MINERVA) consists of an array of robotic telescopes located on Mount Hopkins, Arizona with the purpose of performing transit photometry and spectroscopy to find Earth-like planets around Sun-like stars. In order to make photometric observations, it is necessary to perform calibrations on the CCD cameras of the telescopes to take into account possible instrument error on the data. In this project, we developed a pipeline that takes optical images, calibrates them using sky flats, darks, and biases to generate a transit light curve.

  18. Local Volatility Calibration Using An Adjoint Proxy

    Directory of Open Access Journals (Sweden)

    Gabriel TURINICI

    2008-11-01

    Full Text Available We document the calibration of the local volatility in a framework similar to Coleman, Li and Verma. The quality of a surface is assessed through a functional to be optimized; the specificity of the approach is to separate the optimization (performed with any suitable optimization algorithm from the computation of the functional where we use an adjoint (as in L. Jiang et. al. to obtain an approximation; moreover our main calibration variable is the implied volatility (the procedure can also accommodate the Greeks. The procedure performs well on benchmarks from the literature and on FOREX data.

  19. Calibration of the solar neutrino detectors

    Energy Technology Data Exchange (ETDEWEB)

    Caccianiga, Barbara; Re, Alessandra Carlotta [Universita degli Studi Milano (Italy); INFN, Milano (Italy)

    2016-04-15

    Calibrations have been crucial for the success of solar neutrino experiments. In this contribution we review the calibration strategies adopted by different solar neutrino experiments. In particular, we will emphasize their common critical aspects and their main differences. In order to do so, we will schematically divide the solar neutrino experiments in two groups: those based on radiochemical techniques, i.e. Homestake, Gallex/GNO, SAGE and those based on real-time techniques i.e. Kamiokande, Super-Kamiokande, SNO, Borexino and KamLAND. (orig.)

  20. E-book Management with Calibre Software

    OpenAIRE

    N P, Jamsheer

    2013-01-01

    Keeping pace with the technology is a big challenge for modern libraries. Reading habits and requirements of the library users are changing. Libraries have to provide access to the varying forms of information available. In addition to the conventional book lending, users should be given access to e-books. This artcle examines how to manage e-books in a library using calibre e-book management software. Calibre is a highly user friendly personal e-book manager. This free software can be used i...

  1. Electrical Calibration for Calvet Type Microcalorimetry

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    The deyjce construction and working principle of Calvet type heat conductive microcalorimetry are generally ineroduced in this paper. Based on previous work, we design a reactor vessel and its electrical calibration equipment according to our special study systems. The heat constant of our improved microalorimetry is gotten by means of electrical calibration on the basis of Tian's equation. The results gotten by in tegration method are identical with ones gotten by peak method. It shows that our improved device works well enough to develop further studies.``

  2. On Calibration of pH Meters

    OpenAIRE

    Da-Ming Zhu; Cheng, K. L.

    2005-01-01

    The calibration of pH meters including the pH glass electrode, ISE electrodes, buffers, and the general background for calibration are reviewed. Understanding of basic concepts of pH, pOH, and electrode mechanism is emphasized. New concepts of pH, pOH, as well as critical examination of activity, and activity coefficients are given. The emergence of new solid state pH electrodes and replacement of the salt bridge with a conducting wire have opened up a new horizon for pH measurements. A pH bu...

  3. Photometric calibrations for 21st century science

    Energy Technology Data Exchange (ETDEWEB)

    Kent, Stephen; /Fermilab; Kaiser, Mary Elizabeth; /Johns Hopkins U.; Deustua, Susana E.; /Baltimore, Space Telescope Sci.; Smith, J.Allyn; /Austin Peay State U.; Adelman, Saul; /Citadel Military Coll.; Allam, Sahar S.; /Fermilab; Baptista, Brian; /Indiana U.; Bohlin, Ralph C.; /Baltimore, Space Telescope Sci.; Clem, James L.; /Louisiana State U.; Conley, Alex; /Colorado U.; Edelstein, Jerry; /UC, Berkeley, Space Sci. Dept. /NOAO, Tucson

    2009-02-01

    The answers to fundamental science questions in astrophysics, ranging from the history of the expansion of the universe to the sizes of nearby stars, hinge on our ability to make precise measurements of diverse astronomical objects. As our knowledge of the underlying physics of objects improves along with advances in detectors and instrumentation, the limits on our capability to extract science from measurements is set, not by our lack of understanding of the nature of these objects, but rather by the most mundane of all issues: the precision with which we can calibrate observations in physical units. In principle, photometric calibration is a solved problem - laboratory reference standards such as blackbody furnaces achieve precisions well in excess of those needed for astrophysics. In practice, however, transferring the calibration from these laboratory standards to astronomical objects of interest is far from trivial - the transfer must reach outside the atmosphere, extend over 4{pi} steradians of sky, cover a wide range of wavelengths, and span an enormous dynamic range in intensity. Virtually all spectrophotometric observations today are calibrated against one or more stellar reference sources, such as Vega, which are themselves tied back to laboratory standards in a variety of ways. This system's accuracy is not uniform. Selected regions of the electromagnetic spectrum are calibrated extremely well, but discontinuities of a few percent still exist, e.g., between the optical and infrared. Independently, model stellar atmospheres are used to calibrate the spectra of selected white dwarf stars, e.g. the HST system, but the ultimate accuracy of this system should be verified against laboratory sources. Our traditional standard star systems, while sufficient until now, need to be improved and extended in order to serve future astrophysics experiments. This white paper calls for a program to improve upon and expand the current networks of

  4. SI-Traceable Calibrations of Celestial Objects

    Science.gov (United States)

    Cramer, C. E.; Lykke, K. R.; Woodward, J. T.

    2016-05-01

    Photometric calibration is currently the leading source of systematic uncertainty in supernova surveys that aim to determine the nature of dark energy. The bulk of this uncertainty is due to imperfect knowledge of the spectral energy distribution of stars used as primary standards. We review the challenges associated with establishing an absolute calibration of stellar spectra and describe how it is possible to do better by using recent advances in optical metrology, paying particular attention to the measurement chain establishing SI-traceability and reporting of measurement uncertainties.

  5. Ballistic evaluationof LOVA propellant in high calibre gun

    Directory of Open Access Journals (Sweden)

    A.G.S. Pillai

    2001-04-01

    Full Text Available 'This paper presents the data obrained on dynamic firing of a cellulose acetate binder-based low vulnerability ammunition (LOV A propellant using 120 mm fin-stabilised armour piercing discarding sabot (FSAPDS kinetic energyammunition. An optimised propellant composition formulated ~sing fine RDX as an energetic ingredient and a mixture of cellulose acetate and nitrocellulose as binder was qualified fit for firing in a high calibre gun by its successful static evaluation for absolute ballistics using high pressure closed vessel technique. Dynamic firing of the propellant processed in heptatubular geometry was undertaken to assess the propellant charge mass. This propellant achieved higher muzzle velocity as compared to the standard NQ/M119 triple-base propellant while meeting the non-vulnerability characteristics convincingly.

  6. Evaluation of plasmid and genomic DNA calibrants used for the quantification of genetically modified organisms.

    Science.gov (United States)

    Caprioara-Buda, M; Meyer, W; Jeynov, B; Corbisier, P; Trapmann, S; Emons, H

    2012-07-01

    The reliable quantification of genetically modified organisms (GMOs) by real-time PCR requires, besides thoroughly validated quantitative detection methods, sustainable calibration systems. The latter establishes the anchor points for the measured value and the measurement unit, respectively. In this paper, the suitability of two types of DNA calibrants, i.e. plasmid DNA and genomic DNA extracted from plant leaves, for the certification of the GMO content in reference materials as copy number ratio between two targeted DNA sequences was investigated. The PCR efficiencies and coefficients of determination of the calibration curves as well as the measured copy number ratios for three powder certified reference materials (CRMs), namely ERM-BF415e (NK603 maize), ERM-BF425c (356043 soya), and ERM-BF427c (98140 maize), originally certified for their mass fraction of GMO, were compared for both types of calibrants. In all three systems investigated, the PCR efficiencies of plasmid DNA were slightly closer to the PCR efficiencies observed for the genomic DNA extracted from seed powders rather than those of the genomic DNA extracted from leaves. Although the mean DNA copy number ratios for each CRM overlapped within their uncertainties, the DNA copy number ratios were significantly different using the two types of calibrants. Based on these observations, both plasmid and leaf genomic DNA calibrants would be technically suitable as anchor points for the calibration of the real-time PCR methods applied in this study. However, the most suitable approach to establish a sustainable traceability chain is to fix a reference system based on plasmid DNA.

  7. Calibration Procedures on Oblique Camera Setups

    Science.gov (United States)

    Kemper, G.; Melykuti, B.; Yu, C.

    2016-06-01

    Beside the creation of virtual animated 3D City models, analysis for homeland security and city planning, the accurately determination of geometric features out of oblique imagery is an important task today. Due to the huge number of single images the reduction of control points force to make use of direct referencing devices. This causes a precise camera-calibration and additional adjustment procedures. This paper aims to show the workflow of the various calibration steps and will present examples of the calibration flight with the final 3D City model. In difference to most other software, the oblique cameras are used not as co-registered sensors in relation to the nadir one, all camera images enter the AT process as single pre-oriented data. This enables a better post calibration in order to detect variations in the single camera calibration and other mechanical effects. The shown sensor (Oblique Imager) is based o 5 Phase One cameras were the nadir one has 80 MPIX equipped with a 50 mm lens while the oblique ones capture images with 50 MPix using 80 mm lenses. The cameras are mounted robust inside a housing to protect this against physical and thermal deformations. The sensor head hosts also an IMU which is connected to a POS AV GNSS Receiver. The sensor is stabilized by a gyro-mount which creates floating Antenna -IMU lever arms. They had to be registered together with the Raw GNSS-IMU Data. The camera calibration procedure was performed based on a special calibration flight with 351 shoots of all 5 cameras and registered the GPS/IMU data. This specific mission was designed in two different altitudes with additional cross lines on each flying heights. The five images from each exposure positions have no overlaps but in the block there are many overlaps resulting in up to 200 measurements per points. On each photo there were in average 110 well distributed measured points which is a satisfying number for the camera calibration. In a first step with the help of

  8. CALIBRATION PROCEDURES ON OBLIQUE CAMERA SETUPS

    Directory of Open Access Journals (Sweden)

    G. Kemper

    2016-06-01

    Full Text Available Beside the creation of virtual animated 3D City models, analysis for homeland security and city planning, the accurately determination of geometric features out of oblique imagery is an important task today. Due to the huge number of single images the reduction of control points force to make use of direct referencing devices. This causes a precise camera-calibration and additional adjustment procedures. This paper aims to show the workflow of the various calibration steps and will present examples of the calibration flight with the final 3D City model. In difference to most other software, the oblique cameras are used not as co-registered sensors in relation to the nadir one, all camera images enter the AT process as single pre-oriented data. This enables a better post calibration in order to detect variations in the single camera calibration and other mechanical effects. The shown sensor (Oblique Imager is based o 5 Phase One cameras were the nadir one has 80 MPIX equipped with a 50 mm lens while the oblique ones capture images with 50 MPix using 80 mm lenses. The cameras are mounted robust inside a housing to protect this against physical and thermal deformations. The sensor head hosts also an IMU which is connected to a POS AV GNSS Receiver. The sensor is stabilized by a gyro-mount which creates floating Antenna –IMU lever arms. They had to be registered together with the Raw GNSS-IMU Data. The camera calibration procedure was performed based on a special calibration flight with 351 shoots of all 5 cameras and registered the GPS/IMU data. This specific mission was designed in two different altitudes with additional cross lines on each flying heights. The five images from each exposure positions have no overlaps but in the block there are many overlaps resulting in up to 200 measurements per points. On each photo there were in average 110 well distributed measured points which is a satisfying number for the camera calibration. In a first

  9. Summary of KOMPSAT-5 Calibration and Validation

    Science.gov (United States)

    Yang, D.; Jeong, H.; Lee, S.; Kim, B.

    2013-12-01

    Korean Multi-Purpose Satellite 5 (KOMPSAT-5), equipped with high resolution X-band (9.66 GHz) Synthetic Aperture Radar (SAR), is planning to be launched on August 22, 2013. With the satellite's primary mission objective being providing Geographical Information System (GIS), Ocean monitoring and Land management, and Disaster and ENvironment monitoring (GOLDEN), it is expected that its applications for scientific research on geographical processes will be extensive. In order to meet its mission objective, the KOMPSAT-5 will provide three different kinds of SAR imaging modes; High Resolution Mode (1 m resolution, 5 km swath), Standard Mode (3 m resolution, 30 km swath), and Wide Swath Mode (20 m resolution, 100 km swath). The KOMPSAT-5 will be operated in a 550 km sun-synchronous, dawn- dusk orbit with a 28-day ground repeat cycle providing valuable image information on Earth surface day-or-night and even in bad weather condition. After successful launch of the satellite, it will go through Launch and Early Operation (LEOP) and In-Orbit Testing (IOT) period about for 6 months to carry out various tests on satellite bus and payload systems. The satellite bus system will be tested during the first 3 weeks after the launch focusing on the Attitude and Orbit Control Subsystem (AOCS) and Integrated GPS Occultation Receiver (IGOR) calibration. With the completion of bus system test, the SAR payload system will be calibrated during initial In-Flight check period (11 weeks) by the joint effort of Thales Alenia Space Italy (TAS-I) and Korea Aerospace Research Institute (KARI). The pointing and relative calibration will be carried out during this period by analyzing the doppler frequency and antenna beam pattern of reflected microwave signal from selected regions with uniform backscattering coefficients (e.g. Amazon rainforest). A dedicated SAR calibration, called primary calibration, will be allocated at the end of LEOP for 12 weeks to perform thorough calibration activities

  10. Calibration of Local Area Weather Radar—Identifying significant factors affecting the calibration

    Science.gov (United States)

    Pedersen, Lisbeth; Jensen, Niels Einar; Madsen, Henrik

    2010-07-01

    A Local Area Weather Radar (LAWR) is an X-band weather radar developed to meet the needs of high resolution rainfall data for hydrological applications. The LAWR system and data processing methods are reviewed in the first part of this paper, while the second part of the paper focuses on calibration. The data processing for handling the partial beam filling issue was found to be essential to the calibration. LAWR uses a different calibration process compared to conventional weather radars, which use a power-law relationship between reflectivity and rainfall rate. Instead LAWR uses a linear relationship of reflectivity and rainfall rate as result of the log transformation carried out by the logarithmic receiver as opposed to the linear receiver of conventional weather radars. Based on rain gauge data for a five month period from a dense network of nine gauges within a 500 × 500 m area and data from a nearby LAWR, the existing calibration method was tested and two new methods were developed. The three calibration methods were verified with three external gauges placed in different locations. It can be concluded that the LAWR calibration uncertainties can be reduced by 50% in two out of three cases when the calibration is based on a factorized 3 parameter linear model instead of a single parameter linear model.

  11. Calibration Of A Distributed Hydrological Model Using Satellite Data Of LST And Ground Discharge Measurements

    Science.gov (United States)

    Corbari, Chiara; Manchini, Marco; Li, Jiren; Su, Zhongbo

    2013-12-01

    Calibration and validation of distributed models at basin scale generally refer to external variables, which are integrated catchment model outputs, and usually depend on the comparison between simulated and observed discharges at the available rivers cross sections, which are usually very few. However distributed models allow an internal validation due to their intrinsic structure, so that internal processes and variables of the model can be controlled in each cell of the domain. In particular this work investigates the potentiality to control evapotranspiration and its spatial and temporal variability through the detection of land surface temperature from satellite remote sensing. This study proposes a methodology for the calibration of distributed hydrological models at basin scale through the constraints on an internal model variable using remote sensing data of land surface temperature. The model (FEST-EWB) algorithm solves the system of energy and mass balances in term of the equilibrium pixel temperature or representative equilibrium temperature that governs the fluxes of energy and mass over the basin domain. This equilibrium surface temperature, which is a critical model state variable, is compared to land surface temperature from MODIS and AATSR. So soil hydraulic parameters and vegetation variables will be calibrated according to the comparison between observed and simulated land surface temperature minimizing the errors. A similar procedure will also be applied performing the traditional calibration using only discharge measurements. These analyses are performed for Upper Yangtze River basin (China) in framework of DRAGON-2 and DRAGON-3 Programme funded by NRSCC and ESA.

  12. Calibration of the Atlas electromagnetic calorimeter. Search for the Higgs boson in its invisible decays

    International Nuclear Information System (INIS)

    The most promising channels for an intermediate mass Higgs boson discovery at LHC are leptonic and photonic decays. Therefore, a good uniformity of response of the electromagnetic calorimeter is required to reach the 0.7% constant term needed. This thesis deals with the absolute calibration of this detector. An electrical description of the calibration system, the detector and its read-out chain has been made for a better comprehension of the signal pulse shapes. A method, using a convolution of the calibration waveforms, has been developed to predict physics response, leading to absolute calibration. The level of accuracy obtained allows to reach the 0.3% contribution to the constant term required. Test beam analysis of a prototype module showed the performance of the electromagnetic calorimeter in terms of local resolution and linearity. A uniformity study has been made, leading to a 0.8% dispersion on a Δη x Δφ = 1.2 x 0.75 area. In a second part, the observability of an invisible Higgs boson produced via weak boson fusion at the LHC is presented. A level 1 trigger strategy for this purely jet and missing ET final states is discussed. A method to measure the level of background using physics events is presented. This analysis shows that an invisible branching ratio of 25% could be reached at 95% CL with only 30 fb-1 for a Higgs boson mass of 120 GeV/c2. (author)

  13. Calibration of an optical condensate measurement technique using indirect static headspace gas chromatography.

    Science.gov (United States)

    Hoke, P B; Loconto, P R; McGrath, J J

    2001-12-01

    Researchers in the Department of Mechanical Engineering seek to obtain a means to measure less than 3 mg of H2O that adheres to a metal surface as condensate. The objective is to calibrate optical reflectance measurements of an aluminum surface as a function of the condensate thickness present. Collaboration with the Hazardous Substance Research Center at Michigan State University results in the development of an indirect static headspace gas chromatographic technique capable of measuring H2O in low-milligram quantities. The technique utilizes manual headspace sampling, a megabore capillary column, and a flame ionization detector. A correlation of r2 = 0.999 is obtained for the calibration of the indirect measurement technique. The calibration of the analytical instrument demonstrates adequate precision (calcium carbide to convert the H2O to acetylene. A scaled calibration technique is used to simplify handling trace water volumes. The surface reflectance measurements are found to correlate well (r2 = 0.935) with measurements of the condensate mass. This result facilitates the development of an optical mass-transfer measurement technique. This study focuses on the analytical method and its relationship with engineering research.

  14. Monte Carlo efficiency calibration of a neutron generator-based total-body irradiator

    International Nuclear Information System (INIS)

    Many body composition measurement systems are calibrated against a single-sized reference phantom. Prompt-gamma neutron activation (PGNA) provides the only direct measure of total body nitrogen (TBN), an index of the body's lean tissue mass. In PGNA systems, body size influences neutron flux attenuation, induced gamma signal distribution, and counting efficiency. Thus, calibration based on a single-sized phantom could result in inaccurate TBN values. We used Monte Carlo simulations (MCNP-5; Los Alamos National Laboratory) in order to map a system's response to the range of body weights (65-160 kg) and body fat distributions (25-60%) in obese humans. Calibration curves were constructed to derive body-size correction factors relative to a standard reference phantom, providing customized adjustments to account for differences in body habitus of obese adults. The use of MCNP-generated calibration curves should allow for a better estimate of the true changes in lean tissue mass that many occur during intervention programs focused only on weight loss. (author)

  15. Mass metrology

    CERN Document Server

    Gupta, S V

    2012-01-01

    This book presents the practical aspects of mass measurements. Concepts of gravitational, inertial and conventional mass and details of the variation of acceleration of gravity are described. The Metric Convention and International Prototype Kilogram and BIPM standards are described. The effect of change of gravity on the indication of electronic balances is derived with respect of latitude, altitude and earth topography. The classification of weights by OIML is discussed. Maximum permissible errors in different categories of weights prescribed by national and international organizations are p

  16. SCIAMACHY Level 1 data: calibration concept and in-flight calibration

    Directory of Open Access Journals (Sweden)

    G. Lichtenberg

    2006-01-01

    Full Text Available The calibration of SCIAMACHY was thoroughly checked since the instrument was launched on-board ENVISAT in February 2002. While SCIAMACHY's functional performance is excellent since launch, a number of technical difficulties have appeared, that required adjustments to the calibration. The problems can be separated into three types: (1 Those caused by the instrument and/or platform environment. Among these are the high water content in the satellite structure and/or MLI layer. This results in the deposition of ice on the detectors in channels 7 and 8 which seriously affects the retrievals in the IR, mostly because of the continuous change of the slit function caused by scattering of the light through the ice layer. Additionally a light leak in channel 7 severely hampers any retrieval from this channel. (2 Problems due to errors in the on-ground calibration and/or data processing affecting for example the radiometric calibration. A new approach based on a mixture of on-ground and in-flight data is shortly described here. (3 Problems caused by principal limitations of the calibration concept, e.g. the possible appearance of spectral structures after the polarisation correction due to unavoidable errors in the determination of atmospheric polarisation. In this paper we give a complete overview of the calibration and problems that still have to be solved. We will also give an indication of the effect of calibration problems on retrievals where possible. Since the operational processing chain is currently being updated and no newly processed data are available at this point in time, for some calibration issues only a rough estimate of the effect on Level 2 products can be given. However, it is the intention of this paper to serve as a future reference for detailed studies into specific calibration issues.

  17. Determining Central Black Hole Masses in Distant Active Galaxies

    DEFF Research Database (Denmark)

    Vestergaard, Marianne

    2002-01-01

    An empirical relationship, of particular interest for studies of high redshift active galactic nuclei (AGNs) and quasars, between the masses of their central black-holes and rest-frame ultraviolet (UV) parameters measured in single-epoch AGN spectra is presented. This relationship is calibrated...... black-hole demographics at high redshift as well as to statistically study the fundamental properties of AGNs. The broad line region size - luminosity relationship is key to the calibrations presented here. The fact that its intrinsic scatter is also the main source of uncertainty in the calibrations...

  18. Measurement of top-quark pair production cross sections and calibration of the top-quark Monte-Carlo mass using LHC run I proton-proton collision data at √(s) = 7 and 8 TeV with the CMS experiment

    International Nuclear Information System (INIS)

    In this thesis, measurements of the production cross sections for top-quark pairs and the determination of the top-quark mass are presented. Dileptonic decays of top-quark pairs (t anti t) with two opposite-charged lepton (electron and muon) candidates in the final state are considered. The studied data samples are collected in proton-proton collisions at the CERN Large Hadron Collider with the CMS detector and correspond to integrated luminosities of 5.0 fb-1 and 19.7 fb-1 at center-of-mass energies of √(s) = 7 TeV and √(s) = 8 TeV, respectively. The cross sections, σt anti t, are measured in the fiducial detector volume (visible phase space), defined by the kinematics of the top-quark decay products, and are extrapolated to the full phase space. The visible cross sections are extracted in a simultaneous binned-likelihood fit to multi-differential distributions of final-state observables, categorized according to the multiplicity of jets associated to b quarks (b jets) and other jets in each event. The fit is performed with emphasis on a consistent treatment of correlations between systematic uncertainties and taking into account features of the t anti t event topology. By comparison with predictions from the Standard Model at next-to-next-to leading order (NNLO) accuracy, the top-quark pole mass, mtpole, is extracted from the measured cross sections for different state-of-the-art PDF sets. Furthermore, the top-quark mass parameter used in Monte-Carlo simulations, mtMC, is determined using the distribution of the invariant mass of a lepton candidate and the leading b jet in the event, mlb. Being defined by the kinematics of the top-quark decay, this observable is unaffected by the description of the top-quark production mechanism. Events are selected from the data collected at √(s) = 8 TeV that contain at least two jets and one b jet in addition to the lepton candidate pair. A novel technique is presented, in which fixed-order calculations in quantum

  19. Measurement of top-quark pair production cross sections and calibration of the top-quark Monte-Carlo mass using LHC run I proton-proton collision data at √(s) = 7 and 8 TeV with the CMS experiment

    Energy Technology Data Exchange (ETDEWEB)

    Kieseler, Jan

    2015-12-15

    In this thesis, measurements of the production cross sections for top-quark pairs and the determination of the top-quark mass are presented. Dileptonic decays of top-quark pairs (t anti t) with two opposite-charged lepton (electron and muon) candidates in the final state are considered. The studied data samples are collected in proton-proton collisions at the CERN Large Hadron Collider with the CMS detector and correspond to integrated luminosities of 5.0 fb{sup -1} and 19.7 fb{sup -1} at center-of-mass energies of √(s) = 7 TeV and √(s) = 8 TeV, respectively. The cross sections, σ{sub t} {sub anti} {sub t}, are measured in the fiducial detector volume (visible phase space), defined by the kinematics of the top-quark decay products, and are extrapolated to the full phase space. The visible cross sections are extracted in a simultaneous binned-likelihood fit to multi-differential distributions of final-state observables, categorized according to the multiplicity of jets associated to b quarks (b jets) and other jets in each event. The fit is performed with emphasis on a consistent treatment of correlations between systematic uncertainties and taking into account features of the t anti t event topology. By comparison with predictions from the Standard Model at next-to-next-to leading order (NNLO) accuracy, the top-quark pole mass, m{sub t}{sup pole}, is extracted from the measured cross sections for different state-of-the-art PDF sets. Furthermore, the top-quark mass parameter used in Monte-Carlo simulations, m{sub t}{sup MC}, is determined using the distribution of the invariant mass of a lepton candidate and the leading b jet in the event, m{sub lb}. Being defined by the kinematics of the top-quark decay, this observable is unaffected by the description of the top-quark production mechanism. Events are selected from the data collected at √(s) = 8 TeV that contain at least two jets and one b jet in addition to the lepton candidate pair. A novel technique is

  20. In-Flight Pitot-Static Calibration

    Science.gov (United States)

    Foster, John V. (Inventor); Cunningham, Kevin (Inventor)

    2016-01-01

    A GPS-based pitot-static calibration system uses global output-error optimization. High data rate measurements of static and total pressure, ambient air conditions, and GPS-based ground speed measurements are used to compute pitot-static pressure errors over a range of airspeed. System identification methods rapidly compute optimal pressure error models with defined confidence intervals.